NCG060295_COMPLETE FILE - HISTORICAL_20171220

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT N0.
/v 0Ip'� a g S
DOC TYPE
4HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ �'� � � �a d'D
YYYYMMDD

2
Division of Energy, Mineral, and Land Resources
Land Quality Section 1 Stormwater Program
National Pollutant Discharge Elimination System (NPDES)
Energy. Mineral & PERMIT OWNER AFFILIATION DESIGNATION FORM
[and Resources
ENVIRONMENTAL QUALITY (Individual Legally Responsible for Permit)
Use this form if there has been:
FOR AGENCY USE ONLY
Datc Received
Year I
Month
Da
NO CHANGE in facility ownership or facility name, but the individual
who is legally responsible for the permit has changed.
If the name of the facility has changed, or if the ownership of the facility has changed,
do NOT use this form. Instead, you must fill out a Name -Ownership C��R$e Form
and submit the completed form with all required documentati0A(,S1VE1)jA,_
nc„ -
What does "legally responsible individual" mean? L
The person is either: 201.7
• the responsible corporate officer (for a corporation); Permatt rLIt1y
• the principle executive officer or ranking elected official (for a municipality, state, federal or�RA?gomic
agency);
the general partner or proprietor (for a partnership or sole proprietorship);
or, the duly authorized representative of one of the above.
1) Enter the permit number for which this change in Legally Responsible Individual ("Owner Affiliation")
applies:
Individual Permit (or) Certificate of Coverage
N I C I S I I I I I I j I N I C I G O 6 10 12 9 5
2) Facility Information:
Facility name: Lumber Bridge Plant
Company/Owner Organization: Mountaire Farms
Facility address: 17269 NC 71-Hwy N
Address
Lumber Bridge NC 28357
City State Zip
To find the current legally responsible person associated with your permit, go to this website:
http://deg.nc.g_ov/about/divisions/energy-mineral-land-resources/energy-mineral-land-permits/stonnwater-pro *ram
and run the Permit Contact Summary Report.
3) OLD OWNER AFFILIATION that should be removed:
Previous legally responsible individual: Mari( Chranowski
First MI Last
4) NEW OWNER AFFILIATION (legally responsible for the permit):
Person legally responsible for this permit:
Mike Tirrell
First M I Last
Page 1 of 2
SWU-0WNERAFF11:23March2017

rye
NPDE=S Stormwater Permit OWNER AFFILATION DESIGNATION Form
(if no Facility Name/Ownership Change)
5) Reason for this change:
A result of:
tf other please explain:
VP of Processing Operations
Title
PO Box 1320
Mailing Address
Millsboro DE 19966
City State Zip
( 302 ) 934-4151 [e-mail]
Telephone E-mail Address
Fax Number
® Employee or management change
❑ Inappropriate or incorrect designation before
❑ Other
The certification below must be completed and signed by the permit holder.
PERMITTEE CERTIFICATION:
I, , attest that this application for this change in Owner Affiliation
(person legally responsible for the permit) has been reviewed and is accurate and complete to the best of my
knowledge. I understand that if all required parts of this form are not completed, this change may not be
processed.
Signat Date
PLEASE SEND THE COMPLETED FORM TO:
Division of Energy, Mineral, and Land Resources
Stormwater Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
For more information or staff contacts, please call [phone] or visit the website at:
htip:Hdeg. ne.gov/about/divisions/energy-mineral-land-resources/stormwater
Page 2 of 2
S W U-OWN1iRAFF 11: 23Mar20l 7

NC Division of Energy, Mineral and land Resources
NPDES Stormwater Permit Contacts Summary
NC DEMLR haj the Followlna coijtact d0m-mtj2n i�ur PPjt Data flat<for your eennit as of 3/912017,
Permit Number: NCGD60295
■'.'.+A' lr 11 ��. �.. 'I, 1•7-lM 1+ .l'lll.•i7vi 1 :•I:l''/�
Facility Name: Mountalre Farms Lumber Orfdoe Plant
Facility Addresslt 17269 NC Hwv 71n
Facility Address2i
City, Slate & ZIP: Lumber Rrfdae. NC:28357
Owner InMrmatlon Details•
Owner Name: Mountalre Farms Inc
Owner Types Nan-Govemmeirt Owner Type Group; Oman=gn
Owner Affiliation: Paul Downes Title:
Addressi: PO Box 1320
Addresa2.,
City, State & ZIP:
Work Phone: 302A34-3094 Fax: a02-934-3081
Email Address;
Owner�Conract Person.(tal' M ' I;
Contact Name A9d Ehwl Elz IQ
/M[Ilk
Chntrkr k! ` VP.of Pmooning, OPeretim s PO Box 1320, M19sboro, DE 19988-1329 302-934;,U49' :' 302-934.3081 mchranowskamountalre.rom
M
1 k= ax
Robert Jackson Waste Water Treatment Manager 17259 NC Hwy 71 N, Lumber Bridge, NC 28357 910-3694275 910-843-4256
ZENO
rjackeon®mountalrexom
I / Contact Name �g �g mpg fm l�
IBeth Bise = PO'Box 1320; MIIlsboro; DE'19988;1320 1-302-034.3094. -w_302-934.3081! Ibeise®mountelre.gom
Cantact Name I1119 Add Phone fu Amin
Robert Jacimm 17269 NC Hwy 71 N, Lumber Bridge, NC 910-359-5275 910-843.4256
28357 eeR1—
r l'rlpufltGt� (P;�C1M'
3/9/2017 Page t

Energy, Mineral
and Land Resources
ENVIRONMENTAL QUALITY
June 13, 2016
Mountaire Farms
Attn: Robert Jackson
PO Box 339
Lumber Bridge, NC 28357
PAT MCCRORY
Governor
DONALD R. VAN DER VAART
Subject: COMPLIANCE EVALUATION INSPECTION
NPDES Stormwater General Permit NCG60000
Mountaire Farms Inc.
Mountaire Farms Lumber Bridge Plant, Certificate of Coverage NCG060295
Robeson County
Dear Mr. Jackson:
Secretary
TRACY DAVIS
Director
On June 8, 2016, a site inspection was conducted for the Mountaire Farms Lumber Bridge Plant facility located at 17269
NC Hwy 71 North Robeson County, North Carolina, A copy of the Compliance Inspection Report is enclosed for your
review. Beth Sise was also present during the inspection and her time and assistance is greatly appreciated. The site visit
and file review revealed that the subject facility is covered by NPDES Stormwater General Permit NCG060000, Certificate
of Coverage NCG060295. Permit coverage authorizes the discharge of stormwater from the facility to receiving waters
designated as Big Marsh Swamp, a Class C;Sw waterbody in the Lumber River Basin.
As a result of the inspection, the facility was found to be in compliance with the conditions of the NCGO60000 permit.
Please refer to the enclosed Compliance Inspection Report for additional comments and observations made during the
inspection.
Please be advised that violations of the NPDES Stormwater General Permit are subject to a civil penalty
assessment of up to $25,000 per day for each violation. If you or your staff has any questions, comments, or needs
assistance with understanding any aspect of your permit, please contact me at 910-433-3389 or by e-mail at
nick,[e-mail]
Sincerely,
Nicholas Mills
Environmental Specialist
Enclosure
cc: Beth Sise, Environmental Manager- Mountaire Farms, Inc. (electronic copy)
FRO — DEMLR, Stormwater Files-NCG060295
State of North Carolina I Environmental Quality I Energy, Mineral and Land Resources
Fayetteville Regional Office 1 225 Green Street, Suite 714 1 Fayetteville, NC 29301
910-433-3300

Compliance Inspection Report
Permit: NCG060295 Effective: 12/01/12 Expiration: 10/31/17 owner: Mountaire Farms Inc
SOC: Effective: Expiration: Facility: Mountaire Farms Lumber Bridge Plant
County: Robeson 17269 NC Hwy 71 n
Region: Fayetteville
Lumber Bridge NC 28357
Contact Person: Robert Jackson Title: Waste Water Treatment Manager Phone: [phone]
Directions to Facility:
From the intersection of Hwy 20 and Hwy 71 in Lumber Bridge, NC, take Hwy 71 west approx. 1.70 miles to the Mountaire Plant Site
located on the north side of Hwy 71.
System Classifications:
Primary ORC: Certification: Phone:
Secondary ORC(s):
On -Site Representative(s):
On -site representative
On -site representative
Related Permits:
Inspection Date: 06/08/2016
Primary Inspector: Nick E Mills
Secondary Inspector(s):
Beth B Sise
Robert Jackson
Entry Time: 10:05AM Exlt Time: 11:35AM
877-877-1490
910-359-5275
Phone: [phone]
Mike Lawyer Phone :[phone] Ext.729
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: FoodlTobaccolSoaps/Cosmetics/Public Warehousing Stormwater Discharge COC
Facility Status: Compliant ❑ Not Compliant
Question Areas:
Storm Water
(See attachment summary)
Page: 1

permit; NCGO60296 Owner - Facility: Mountaire Farms Inc
Inspection Date: 06/0812016 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
Monthly monitoring for outfall 001(ditch) and semi annual monitoring for outfall 002 (pond). Facility is in the process
modifying it's current stormwater retension pond. Facility was found to be in compliance with the conditions of the
NCG060000.
Page: 2

4 1 1+
Permit: NCGO60295 Owner - Facility: Mountaire Farms Inc
Inspection Date: 06/0812016 Inspection Type : Compfianca Evaluation Reason for Visit: Routine
Analytical Monitoring Yes No NA NE
Has the facility conducted its Analytical monitoring? ■ ❑ ❑ ❑
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? 0 ❑ ❑ ❑
Comment:
Permit and Outfalls Yes No NA NE
# 1s a copy of the Permit and the Certificate of Coverage available at the site? E ❑ ❑ ❑
# Were all outfalls observed during the inspection? 0 ❑ ❑ ❑
# If the facility has representative outfall status, is it properly documented by the Division? ❑ ❑ M ❑
# Has the facility evaluated all illicit (non stormwater) discharges? ❑ ❑ ❑
Comment:
Qualitativg Monitoring X29 No NA NE
Has the facility conducted its Qualitative Monitoring semi-annually? 0 ❑ ❑ ❑
Comment:
Stormwater Pollution Prevention Plan
Yes No NA HE
Does the site have a Stormwater Pollution Prevention Plan?
0 ❑ ❑ ❑
# Does the Plan include a General Location (USGS) map?
❑ ❑
# Does the Plan include a "Narrative Description of Practices"?
❑ ❑ ❑
# Does the Plan include a detailed site map including outfall locations and drainage areas?
❑ ❑ ❑
# Does the Plan include a list of significant spills occurring during the past 3 years?.
0 ❑ ❑ ❑
# Has the facility evaluated feasible alternatives to current practices?
0 ❑ ❑ ❑
# Does the facility provide all necessary secondary containment?
0 ❑ ❑ ❑
# Does the Plan include a 6MP summary?
E ❑ ❑ ❑
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
❑ ❑ ❑
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
❑ ❑ ❑
# Does the facility provide and document Employee Training?
❑ ❑ ❑
# Does the Plan include a list of Responsible Party(s)?
0 ❑ ❑ ❑
# Is the Plan reviewed and updated annually?
❑ ❑ ❑
# Does the Plan include a Stormwater Facility Inspection Program?
■ ❑ ❑ ❑
Has the Stormwater Pollution Prevention Plan been implemented?
0 ❑ ❑ ❑
Comment:
Page: 3

i
November20, 2014 Geological Resources, Inc.
Mr. James Brown
NCDENR, UST Section
Fayetteville Regional Office
225 Green Street, Suite 71.4
Fayetteville, NC 28301
Re: Initial Assessment Report
Mountaire Spill
17269 North Carolina Highway 71
Lumber Bridge, Robeson County, NC
GRI Project No: 3619
Dear Mr, Brown,
Please find enclosed the referenced report for the above mentioned site. If you have any questions, please do not
hesitate to contact Terry Kennedy at 704-698-1224.
Sincerely,
Geological Resources, Inc.,
kre Donne y
Adm nistrative Assis t
n
Enclosure
Cc: Ms. Jill Smith, Cape Fear Transport
file
A
3502 Hayes Road Monroe, North Carolina 28110
Phone [phone] [phone] 9 Fax [phone]

INITIAL ASSESSMENT REPORT
MOUNTAIRE SPILL
17269 NORTH CAROLINA HIGHWAY 71
LUMBER BRIDGE, NORTH CAROLINA
ROBESON COUNTY
GRI PROJECT N0.3619
Prepared for:
' Cape Fear Transport
Post Office Box 637
Elizabethtown, North Carolina 28337
n
Prepared by:
0
Geological Resources, Inc.
3502 Hayes Road
Monroe, North Carolina 28110
F
November 20, 2014
r
ina M. Teschner, P.G.
Project Manager

TABLE OF CONTENTS
A. SITE INFORMATION .................................................................................. I ............................... I
B. SITE HISTORY AND CHARACTERIZATION ......................................................... ........ I ...... 2
C. SOURCE ]INVESTIGATION ............................. I .......................................................................... 3
D. SUMMARY AND CONCLUSIONS ............................................................................................. 4
E. LIMITATIONS ..................................................... I ........................................................................ 4
TABLE
Table 1: Summary of Soil Sample Analytical Results
FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Soil Quality Map
APPENDICES
Appendix A: Soil Disposal Manifests
Appendix B: Laboratory Analytical Reports

e
I
A. SITE INFORMATION
1. Site Identification:
Date of Report: November 21, 2014
Incident Number: NA
Site Name: Mountaire Spill
Site Address: NC Highway 71 N
City: Lumber Bridge State: NC Zip Code: 17269 County: Robeson
Description of Geographical Data Point: Calculated from topographic map.
Latitude: 34.86885550 N Longitude: 79.1070000' W
2. Contacts Associated with Release
Responsible Party:
Property Owner:
Primary Consultant:
3. Release Information
Date Discovered:
Quantity of Release:
Cause of Release:
Source of Release:
Certification:
I, Terry Kennedy, a
contained in this revs
Geological
certification
Cape Fear Transport
P.O. Box 637
Elizabethtown, North Carolina 28337
910.862.8423
Mountaire Farms of North Carolina, Inc.
17269 NC HWY 71 N
Lumber Bridge, North Carolina 28357
Geological Resources, Inc. (GRI)
3502 Hayes Road
Monroe, North Carolina 28110
704.845,4010
September 17, 2014
Approximately 75 gallons of diesel fuel
Equipment failure
Broken hose
c sokEleologist for Geological Resources, Inc., do certify that the information
jfW'66ect atld 4ccuRte to the best of my knowledge.
CARO 5%
'A'..
a: 143
�.% 11. M o 4�actice geology and engineering in North Carolina. The
the'tsCff3bl on ar -C-127 and C-2727, respectively.
1

L
U
B. SITE HISTORY AND CHARACTERIZATION
1. Non -UST Information:
The Mountaire Farms site is located at 17269 NC Highway 71 North in Lumber Bridge, Robeson County,
North Carolina (Figure 1). On September 17, 2014, during refueling of a 30,000-gallon diesel fuel AST
by Cape Fear Transport, a fuel hose ruptured. The released fuel was mostly retained by the AST's dike
and concrete pad. However, some of the fuel was spilled on the ground surrounding the AST pad and
into a nearby storm drain. The storm drain travels 350 feet west under Chicken Plant Drive and
discharges into a lined retention pond. Fuel entered the retention pond, which was filled with heavy
organic sludge.
2. Historical Information:
' Not applicable.
3. Comprehensive Description of the Release;
On September 17, 2014, a fuel hose ruptured on a tanker truck refueling a 30,000-gallon diesel fuel AST.
The rupture caused the release of approximately 75 gallons of diesel fuel, of which approximately 30
gallons was retained by the AST concrete pad and dike and 45 gallons entered a nearby storm drain. The
storm drain discharged into a lined retention pond. The spill site is an approximately 10' by 50'
rectangular area outside the AST's dike, adjacent to a storm drain. The storm drain discharges into an
approximately 300' by 550' rectangular retention pond (Figure 2). The release was to the surface of the
AST's concrete pad, the surrounding soil, storm drain and a lined retention pond. No ground water or
other surface water bodies were, affected by the release.
4. Description of the Site Characteristics:
The site is a poultry processing plant Iocated in Robeson County, North Carolina. The area is primarily
agricultural with a sparse mixture of residential and commercial properties.
5. Summary of Initial Abatement Actions, Assessment Activities, and Corrective Actions:
Environmental Hydrogeological Consultants, Inc. (EHC) removed approximately 575 gallons of water
and product with a vacuum truck following flushing of the storm drain, Subsequently, GRI supervised
the excavation of petroleum contaminated soils at the site by Cape Fear Transport on September 17, 2014.
Excavation was conducted in the spill area immediately outside the dike. Soil was removed to
approximate depth of 2 feet. Suspect soils were loaded by an excavator directly into truck for transport to
2

a permitted disposal facility. All encountered soils exhibiting petroleum odors were removed. Areas
adjacent to the AST containment dike and at the drain pipe outfall were excavated. A series of absorbent
booms were deployed to recover trace petroleum from the storm drain outfalls. Following excavation,
soil samples were collected from the base of both excavations.
6. Contaminated Soil and Water Storage/Treatment and/or Disposal:
Based on the invoice provided by EHC, a total 575 gallons of petroleum contaminated fluid was
recovered and transported to a permitted disposal facility. A disposal manifest for the liquids has not
been provided to date. Approximately 20.36 tons of petroleum contaminated soils were excavated and
transported to S & R Landfarms, LLC, a permitted disposal facility located " Pair Bluff, North Carolina.
Copies of the soil disposal manifests are provided as Appendix A.
C. SOURCE INVESTIGATION
1. Investigation Performed To -Date to Determine the Source of the Releaset
Not applicable. The source of the release was a ruptured hose on a tanker truck.
2. Excavation and Sampling
Two soil samples were collected from the base of the excavation area and two samples were collected
along the base of the excavation in the retention pond. The collected soil samples were placed into
laboratory -supplied glassware and immediately placed on ice for transport to the laboratory for analyses
for total petroleum hydrocarbons - gasoline -range and -diesel range organics (TPH-GRO and TPH-DRO)
using EPA Methods 3550/5030/8015C. Additional analyses of volatile organic compounds (VOCs) by
EPA Method 8260, semi-VOCs (SVOCs) by EPA Method 8270 and volatile and extractable petroleum
hydrocarbons (VPH and EPH) by MADEP Methods (risk -based analyses) were requested on any soil
sample with reported TPH-DRO and/or TPH-GRO concentrations exceeding the regulatory action levels
(RALs). Concentrations of TPH-DRO that exceeded the RAL were reported in samples DI-1 and DI-2.
Therefore, these samples were further analyzed by EPA Methods 8260 and 8270 and MADEP VPH and
EPPI. No concentrations of contaminants of concern that exceeded the soil -to -water maximum soil
contaminant concentrations (MSCCs) were reported in either sample, Copies of the laboratory analytical
reports are provided as Appendix B.
3

D. SUMMARY AND CONCLUSIONS
• On September 17, 2014, approximately 75 gallons of diesel fuel were released when a fuel hose,
ruptured on a tanker truck refueling an 30,000 gallon AST.
• Approximately 20.36 tons of petroleum affected soils were removed from the site on September
17, 2014 and, transported to S&R Landfarms, LLC.
• 575 gallons of petroleum affected water was removed from the site by EHC on September 17,
2014.
• Concentrations of TPH-DRO that exceeded the RAL were reported in samples DI-1 and DI-2;
i
therefore, risk -based analyses were conducted on those samples. No concentrations of
contaminants of concern that exceeded the soil -to -water MSCCs were reported in either sample.
• Based on the sampling results, no further action is warranted,
E. LIN MATIONS
This report has been prepared for the exclusive use of Cape Fear Transporting for specific application to
the referenced spill site in Lumber Bridge, Robeson County, North Carolina. Site activitics were
conducted in accordance with generally accepted standards of environmental practices; available
information, and our professional, judgment. No other warranty is expressed or implied.
The data presented in this report is indicative of conditions that existed at the precise locations sampled
and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from this data. Although the accuracy of this data cannot
be verified, for the purpose of this report, GRI assumes that it is correct.
4

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TABLE 1
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
MOUNTAEKE SPELL
LUMBER BRIDGA, ROBESON COUNTY
Date: 10/23/14
Analytical Method
SW 946 9015C
EPA Method 9260B and 8270D
MADEP YPH
MADEP EPH
Y
ZO
Q
~
e
a
C
m
r
A
F
y
U
!S
U
Gn
U
U
a
G3
e5
RAL
10
10
NA
NA
NA
NA
NA
NA
3.6
NA
NA
NA
NA
NA
NA
Sotl-to-water
MSCCs
NA
NA
0.0056
4.3
4.9
4.6
0.091
0.16
63
68
540
31
540
NE
31
DI I (27
09/17/14
Excavation
Area I
2 0
<3.3
26.9
<*.0011
<0.0011
m.0011
<0.0028
<0.0031
<0.0021
<0.018
<1.9
<1.9
<1.9
<5.2
<5.2
12.3
DI-2 (21
09/17/14
2.0
<2.9
21.4
<0.00095
m.00095
<0.00095
<0.0025
<0.00095
<0.0019
<0.018
Q6
Q.6
<2.6
8-55 J
14,2
9.15 J
ExAzm
Outfall-1 (2'
09/17/14
2-0
<3.1
<4.2
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
ton
Excavation
Otrtfal!-2 (2�
09/17/14
2.0
<2.8
<4.1
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
S7OC KP1LE 1
091171141
Stockpile
NA
1 10.1 J
559
1 NR
1 NR
I NR
I NR
1 NR
NR
I NR
I NR
1 NR
1 NR
NR
I Nit
I NR
Notes:
• Results reportM in mghg (milligrams per kilogram).
• ft-BGS: feet below ground surface.
• MSCCs: Maxim Soil Cantarmriaut Ooncgrtrations.
• <: Less than the method ddection hilt specified in the laboratory report.
• NA: Not Applicable.
• ML: Not Requested
• J: Estimated valuo.
• Concmtndions in bold fie type exceed the soil -to -water MSCCs.
• Please see the laboratory report far additional detoctabto constituents that did not exceed the soil-to-wata MSCCs.
Page 1 of 1

I
I
I
� r'`[.i.v is - n.-<•.•Yr:. � '
AEPA)Bi1C NONHAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST.
$ERVICES, INC
032555 r.
If waste is asbestos waste, complete Sections I, Il, 111 and IV ^ •�
if waste Is NOT asbestos waste, complete Sections I, II and III
I. GENERATOR {Generator completes is-r} ail: Herr. Inc. if C044 Ticket b
a. Generator's US EPA ID Number
b. Manifest Document Number c, Page 1 of
d. Generator's. Na(rtg end Locatlo r
W�Nkpwo RtQ¢IQ Y�11N31CtpQf��,�(l� I1GGl
e Gneret��'��la'slin� AddCees;
xi{ r i =•c t+r:. 1 r.
7'
f. Phona; r' -
g. Phone;
4f owner of the generating facility differs from the generator, provide:
h. Owner's Name: / L'" '` _'.'. -/r ,ir, e� r e, n•J, '. J C_
1 I.Owner's Phone No.:
I. Waste Profile #
k. Exp, Date
1, Waste Shipping Name and
m. Containers
n. Total
o. Unit
No.
T
Description
Quantity
wwol
�,� ��'' l �f 'lc,•+y
Nettnieum imcarttd Sod
GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable
state law, has been properly described, classified and packaged, and Is In proper condition for transportation according to applicable regulations; AND, If this
waste is a treatment residue of a previously restricted hazardo s waste subject to the Land Disposal Restrictions, I certify and warrant that the waste has
been treated in'accordenc/1e with the requirements of 40 CFR B and Is no 1pn Or a hazardous waste as defined b 40 CFR 2%6)1.
-, I t+ i �'%I •� / �}ti.l•�c��C' 9.r•S-'/
�,e•J �...i..� ��. ei!•i1s+�.'�"
�/ � ��1
p. Generator AtolhorizedAgent Name Print
. SI na urre
r• Date
In. l KAN11'VK I t_K tuenerator com tales ua-q pu i rans orter completes uc-e r
a. �ransporter's Name and Address: i IBtF-lflt ,_
(�t[I}�#r`3$�•� l�ir-�f�jr►s�:�t�di�• .,
b. Phonm t
ate � ;.'tr - :.'% i �•'1 rm•�:4 v, � „ .f .. ,. � � ' ;t •f!1y'rr,..-......_..
III- DESTINATION (Generator comDlete 111a-c and Destination Site comoieles flid-al
6. Ats�reclilly and Slt A40reas:
n I �' A. i.J�tlV•1 ra•a r.
5105`10ro-reM1n .r r,:; U, i, : E? r ! ; ruz r• = •+ .
c. US EPA Number
d, Discrepancy Indication Space:
Con`Wd; IVY M7
b. P lit( - 04T"357-
I hereby certify that the above named material has
been gnpted and to the best of my knowledge the for olno is true and accurate.
e. Name of Authorized AgeM_(Printj
I L SI natu a I ri. Date
IV. ASBESTOS (Generator completes IVS4 and Operator. complete IVg-i)
a. Operator's Name and Addreaw
c. Res 'nsible Agency Name and Address:
b. Phone:
d. Phone:
e, Special Handling Instruction and Additional Information;
f. 0 Friable 0 fSan-F lable O fMh K Fda a Non -Friable
OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name
and are classified, packed, marked and labeled and are In all respects In proper condition for transport by highway acoording to applicable International and
national oveenreerrl t ire ulations.
a. Operator's Name and Title Pdnt
h, Signature
I. Dale'
*Operator raters to the company which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or the demolition or
renovation operation or both
REV 1=1 RETURN TO OPERATOR RS-Ft I

,
I
'fir•
r •REPUBLI'C NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST
SERVICES, INC
p 11
19,32553 If waste is asbestos waste, complete Sections I, 11, 111 and IV
If waste is NOT asbestos waste, complete Sections 1, II and lit
I. GENERATOR (Generator COmDleteS la-rl H1ll.lion. Ific, #1(040 Tickeig __r'• ;
a. Generatoes US FPA ID Number b. Manifest Document Number
c, Page 1 of
d. Generator's M nd t ocalto
r r t fftatctrit,tr�&%N,e?✓ efalGrlgl
� � ,'l.'' ►=r��,W f l z,;+'•�::-r'�� ,''.�'
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e. Ge eretor'$7�lailing A�fdsaL
t�., ',t.: Htur-1rI ---
l;Itt}j �t���� 7tL17gB�.Wt9'i'lt°�34ti;fw
Phone:
If owner of the generating facility differs from the generator, provide,
h. Owner's Name:
1. Owners Phone No,:
J. Waste Profile#
k. Exp. Date
7I. Waste Shipping Name and
Description
m. Containers
n. Total
Quantity
o. Unit
WtlVol
No.
Type
9E 10-12-12015
Ifrinuted 80,
GENERATOR'S CERTIFICATION; I hereby certify that the above named materlat Is not a hazardous waste as defined by 40 CFR 261 or any applicable
state law, has been property described, desslffed and packaged, and is In proper condition for transportation according to applicable regulations; AND, If this
waste is a treatment residue of a previously restricted hazardousAssfe subject to the Land Disposal Restrlctlons, I carliiy and warrant that the waste has
been treated In acc ante with the requirements of 40 CFR 2 ;and is no ton dr lhaza rdous waste as defined by40 CFR ?titr._]
f
!
R. Generator Authorfzed A n Name Print
Signature
r. Date
it. l RAN5PUKI thl Lienerator completes Ifa-t) ana I ran5 over completes tic- '
a. Tranaportees Name and Address:
b. Phone:
c. Driver Name Print d, Signature a. Data
III. DESTINATION (Generator complete Ills-c and Destination Site completesilld-g)
a. Disposal FacllIV anp,Slt dress. cr
c. US EPA Number
d. Discrepancy Indication Space:
611 54o ehead.Rd f-r c v . , c N,1:�c •. R .:
,
Concord-N&18027
b. Phone: 704 - 52-'Mt 'it'3rir
I hereby certify that the above named material has been accepted and to the best of my Knowledge the foranoing
is true and accurate.
e. Name of Authorized Atlent Print
f. Signature
a. Date
IV. ASBESTOS (Generator completes IVa-f and Operatol complete IVg-i)
a. Operaloes Name and Address:
c, Responsible Agency Name and Address:
D. phone:
d. Phone:
e. Special Handling Instructions and Additional information.,
f. Q Friable Q No Friable 13 Both • % Friable % NorrFrlable
OPERATOR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name
and are classified, packed, marked and labeled and are In all respects In pro er condition for transport by highway according to applicable International and
national ov mmental fe laWhs.
liri r+ �'1 !`-• •� (.
t1 �r'.rl
/i ... � r
'r.Y
,jf
�+� . �� �',I•..•S._t..
��
Ooerator's Name and Title Print
h. St nature
I. Date
'Operator refers to the company which owns, leases, operates, controls, or supervises the foci lily being demolished or renovated, or the demolition or
renovation o eretlan or both
REV 101
RETURN TO OPERATOR
RS-F 11

e-Hardeopy 2.0
Aulonaaled Reparl
Qj ,Ill,it I l l
i li !`'i{'N�SOutil@SSA,,
'1! !i+ii', i fix �i' !�!$ IF.''� iils
L" Apt3 0 R App{{,T' O R 1 i:: f
iTec1W " I'Repork for M1yH�
rNNi Il�r r'
o.n�91F9�p =li„i��.�:.. ��itl:YNrtN.• rdl^iw.N,..:... "Stit °.,
GRI (Geological Resources Inc.)
Mountaire Spill; Shannon, NC
Accutest Job Number: FA18486
Sampling Date: 09/17/14
Report to:
GRI (Geological Resources Inc.)
ech@geologicalresourcesinc. com
ATTN: Emily Held
Total number of pages in report. 20
s ��r
Test results contained within this data package meet the requirements Norm Farmer
of the National Environmental Laboratory Accreditation Program Technical Director
and/or stale specific cerdfiation programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366). IL (200063), NC (573). N! (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except In its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
JIM 1 of 20
Accutest Laboratories is the sole authority for authorizing edits or modifications to this AC0LJTEST.
document. Unauthorized modification ofthis report is strictly prohibited. FA111486 ............

Sections;
Table. of Contents
Section1: Sample Summary...................................................................................................
3
Section 2: Summary of Hits....................................................................................................
4
Section3: Sample Results........................................................................................................
5
3.1. FA18486-1: DI-1-2'.......................................................................................................
6
3.2: FA 18486-2: D1-2-2'................................. ......................................................................
8
3.3: FA18486-3: OUTFALL-1-2..........................................................................................
10
3.4. FA18486-4: OUTFALL-2-2'.........................................................................................
12
3.5: FA18486-5: STOCKPILE.............................................................................................
14
Section4: Misc. Forms............................................................................................................
16
4.1. Chain of Custody...........................................................................................................
17
Cm 2 of 20
FA16486 `..... °

U
Accatest LabLink@154778 08:52 16-Oct-2014
Sample Summary
GRI (Geological Resources Inc.)
Job No: FA18486
Mountaire Spill; Shannon, NC
SampleGolled:, _ ::,;.°-...:tMatrix Client
Number Date Time By Received Code Type Sample ID
09/17/14 13:12 TK 09/20/14 SO Soil
IyA1$4i1 ° 09/17/14 13:19 TK 09/20/14 SO Soil
FA1898fi-8 09/17/14
14:59 TK
09/20/14
SO
Soil
FFA18986 4 .;_ 09/17/14
15:03 TK
09/20/14
SO
Soil
FA18486=5 09/17/14 15.30 TK 09/20/14 SO Soil
O1ITFALL'2=2'
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
Iii 3 of 20
.o.ccuTesT
FA18488 "`P"'"" ••

Summary of Hits
Job Number:
FA18486
Account:
GRI (Geological Resources Inc,)
Project:
Mountaire Spill; Shannon, NC
Collected:
09/17/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA18486-1 D1-1-2'
TPH (C10-C28) a
26.9 6.5
FA18486-2 DI-2-2'
TPH (C10-C28)
21.4 6.8
FA18486-3 OUTFALL-1-2'
No hits reported in this sample.
FA18486-4 OUTFALL-2-2'
No hits reported in this sample.
FA18486-5 STOCKPILE
TPH-GRO (C6-C10)
10.1 J._�� 13
TPH (C10-C28) a
559 11
(a) Petroleum hydrocarbon pattern extends beyond C28.
3.9 mg/kg SW846 8015C
4.1 mg/kg SW846 8015C
6.6 mg/kg SW846 8015C
6.8 mg/kg SW846 8015C
Page 1 of 1
r
IM 4 of 20
ACCU-rEST.
FA SM ••"•• "" ••

Section 3
r
�7'IZIt € it6Ey f't i't� 3°�ES'Out3 Was,
AC71
`A E9�gfRiA
aIS'
ij
SamplOWsults 'i �'
B$d�y tly Y
epr, ... �' peq €a 94tu _ - a �P6 �F.�R9E ma
Report of Analysis
C{m 5 of 20
AC C U-res is
M8486 `"'"""'"" ••

Accutest LabLink@154778 08:52.16-Oct-2014
Report of Analysis
lient Sample ID:
DI-1-2'
ab Sample ID:
FA18486-1
latrix:
SO - Soil
lethod:
SW846 8015C
roject:
Mountaire Spill; Shannon, NC
File ID
DF Analyzed By
un #1 CD130160.D 1 09/25/14 JG
un #2
Page 1 of 1 j
Date Sampled: 09/17/14
Date Received: 09/20/14
Percent Solids: 93.9
Prep Date Prep Batch Analytical Batch
n/a n/a GCD5329
Initial Weight Final Volume Methanol Aliquot
Run #1 4.31 g 5.0 ml 100 ul
Run #2
GAS No.
Compound
TPH-GRO (C6-CIO)
CAS No.
Surrogate Recoveries
460.00-4
4-Bromofluorobenzene
98.08-8
aaa-Trifluorotoluene
Result RL
ND 6.5
Run# 1 Run# 2
7796
8N6
ND = Not detected MDL = Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
MDL Units Q
3.3 mg/kg
Limits
56-149%
66-132%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
10 - B of 20
ACCUTEBT.
FAIM86

Accutest LabLink@154778 08:52 16-Oct-2014
Report of Analysis
Client Sample ID: DI-1-2'
Lab Sample ID: FAI8486-1 Date Sampled: 09/17/14
Matrix: SO - Soil Date Received: 09/20/14
Method: SW846 8015C SW846 3546 Percent Solids: 93.9
Project: Mountaire Spill; Shannon, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 J3005369.D 1 09/24/14 SJL 09/24/14 OP53241 GJJ208
Run #2
Initial Weight Final Volume
Run #1 20.4 g 1.0 ml
Run #2
CAS No. Compound Result RL MDL Units Q
TPH (CIO-C28) a `2fi:9 6.5 3.9 mg/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 68%. 56-122%
(a) Petroleum hydrocarbon pattern extends beyond C28.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
Cm 7 of 20
FAI8486 1..... ""'

Accutest LabLink@154778 08:52 16-Oct-2014
Report of Analysis
Client Sample ID: DI-2-2'
Lab Sample ID: FA18486-2 Date Sampled: 09/17/14
Matrix: SO - Soil Date Received: 09/20/14
Method: SW846 8015C Percent Solids: 92.3
Project: Mountaire Spill; Shannon, NC
Page I of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD130161.D 1 09/25/14 JG n/a n/a GCD5329
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.05 g 5.0 ml 100 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C1O)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluarobenzene
98-08-8
aaa-Trifluorotoluene
Result RL
MDL Units Q
OD `� 5.8
2.9 mg/kg
Run# 1 Run# 2
Limits
80%
56-149%
82%�
66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
1�■
jig 8 of 20
skccuTas-r.
FAIS"S..... I -

Accutest LabLink@154778 08:52 16-Oct-2014
Report of Analysis
Client Sample ID:
DI-2-2'
Lab Sample ID:
FA18486-2
Matrix:
SO - Soil
Method:
SW846 8015C SW846 3546
Project:
Mountaire Spill; Shannon, NC
File ID
DF Analyzed By Prep Date
Run #1 JJ005372.1) 1 09/24/14 SJL 09/24/14
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 m]
Run #2
CAS No. Compound
TPH (C10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
Result RL
Run# i Run# 2
Date Sampled: 09/17/14
Date Received: 09/20/14
Percent Solids: 92.3
Page IofI N
1 Z
Prep Batch Analytical Batch
OP53241 GJJ208
MDL Units Q
4.1 mg/kg
Limits
56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
jg 9 of 20
A.CCLJTEaT.
FAMUS "•'•• "" ••

Acculest LabLink@154778 08:52 16-Oct-2014 ,
Report of Analysis
Client Sample ID: OUTFALL-1-2'
Lab Sample ID: FA18486-3 Date Sampled: 09/17/14
Matrix: SO - Sol] Date Received: 09/20/14
Method: SW846 8015C Percent Solids: 91.8
Project: Mountalre Spill; Shannon, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD130162.D 1 09/25/14 JG n/a n/a GCD5329
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.73 g 5.0 ml 100 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-CIO)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
98-08-8
aaa-Trifluorololuene
Result RL MDL Units Q
ND — 6.2 3.1 mg/kg
Run# 1 Run# 2 Limits
789b 56-149%
85%7 66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
F = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
a® 10 of 20
^0OU-rEST.
FA184BO I ...... — —

Accutest LabLink@154778 08:52 16-Oct-2014
Report of Analysis
Client Sample ID.
OUTFALL-1-2'
Lab Sample ID:
FA18486-3
Matrix:
SO - Soil
Method:
SW846 8015C SW846 3546
Project:
Mountaire Spill; Shannon, NC
File ID
DF Analyzed By
Run #1 JJ005373.D
1 09/24/14 SJL
Run #2
Initial Weight . Final Volume
Run # 1 19.6 g 1.0 ml
Run #2
CAS No. Compound
TPH (C10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
Result RL
ND 6.9
Run# 1 Run# 2
Page I of 1 w
Date Sampled: 09/17/14
Date Received: 09/20/14
Percent Solids: 91.8
Prep Date Prep Hatch Analytical Batch
09/24/14 OP53241 GJJ208
MDL Units Q .
4.2 mg/kg
Limits
56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
a® 11 of 20
.ACCUTEST.

Accutest LabLink@154778 08:52 16-Oct-2014
Report of Analysis
Client Sample ID: OUTFALL-2-2'
Lab Sample ID: FA18486-4 Date Sampled: 09/17/14
Matrix: SO - Soil Date Received: 09/20/14
Method: SW846 8015C Percent Solids: 91.9
Project: Mountaire Spill; Shannon, NC
Page 1 of 1 a
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD130163.1) 1 09/25/14 JG n/a n/a GCD5329
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.23 g 5.0 ml 100 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-CIO)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
98-08-8
aaa-Trifluorotoluene
Result RL
MDL Units Q
�N p 5.6
2.8 mg/kg
Run# 1 Run# 2
Limits
56-149%
8596
66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
lm 12 of 20
FAI84H `..... "

Accutest LabL1nk@154778 08:52 16-Oct-2014
Report of Analysis
Client Sample ID: OUTFALL-2-2'
Lab Sample ID: FA18486-4 Date Sampled: 09/17/14
Matrix: SO - Soil Date Received: 09/20/14
Method: SW846 8015C SW846 3546 Percent Solids: 91.9
Project: Mountaire Spill; Shannon, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 JJ005392.1) 1 09/25/14 SJL 09/24/14 OP53241 GJJ209
Run #2
Initial Weight Final Volume
Run #1 20.0 g 1.0 ml
Run #2
CAS No. Compound
TPH (C10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
Result RL MDL Units Q
NU,, 6.8 4.1 mg/kg
Run# 1 Run# 2 Limits
7896 56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
In 13 of 20
FA1"88 "'"`.'" '"'

Accutest LabLink@154778 08:52 16-Oct-2014
Report of Analysis
Client Sample ID: STOCKPILE
Lab Sample ID: F'A18486-5 Date Sampled: 09/17/14
Matrix: SO - Soil Date Received: 09/20/14
Method: SW846 8015C Percent Solids: 54.6
Project: Mountaire Spill; Shannon, NC
Page 1 of 1 w
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD130182.D 1 09/26/14 JG n/a n/a GCD5330
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.09 g 5.0 ml 100 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
98-08-8
aaa-Trifiuorotoluene
Result RL MDL Units Q
10:1 13 6.6 mg/kg J
Run# 1 Run# 2 Limits
N 56-149%
$3% , _ 66-132%
Lw
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
aD 14 of 20
ACC U-rE8T.

Accutest LabLink@154778 08:52 16-Oct72014 .
Report of Analysis
Client Sample ID: STOCKPILE
Lab Sample ID: FA18486-5 Date Sampled: 09/17/14
Matrix: SO - Soil Date Received: 09/20/14
Method: SW846 8015C SW846 3546 Percent Solids: 54.6
Project: Mountaire Spill; Shannon, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 JJ005377.D 1 09/24/14 SJL 09/24/14 OP53241 GJJ208
Run #2
Initial Weight Final Volume
Run #1 20.3 g 1.0 ml
Run #2
CAS No. Compound Result RL MDL Units Q
TPH (C10-C28) a 559 11 6.8 mg/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 70%�7 56-122%
(a) Petroleum hydrocarbon pattern extends beyond C28.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
C[a 15 of 20
ACCU-raa-r.
FAIN86 L....--.

Section 4
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Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Q® 16 of 20
FA18488 "......""'

.� ACCUL L i.auoratorte5 noutneasi 4 186
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Chain of Custody A,,u1,,S.Ja �7PAP�^oF�
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L A o o R A T a R I e e TCL. 407-425-G7W • ]'AX: 407-425-0707
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FA18486: Chain of Custody
Page ] of 4
d 17 of 20
FA184B8 •""""" ••

ACCUTEST LABORATORIES SAMPLE RECEIPT CONFIRMATION
ACCUTES["SJOBNUMBER. d i p L'$& CLIENT: R PROJECT:Se.li
DATEJITME RECEIVED- r) q I tb''1 4 /O 3 d (MMIDDIYY I4;00) NUMBER OF COOLERS RECEIVED: l
METHOD OF DELTVF.RY: FT3D" UPS ACCUTEST COURIER GREYHOUND DELIVERY OTHER
AIRBILLNUMBERS: 9 O l3 Of Lf Y-&'L-
OOLER I ON
CUSTODY SEAT. NOT PRESENT OR NOT INTACT
CHAIN OF CUSTODY NOT RECEIVED (COC)
ANALYSIS REQUESTED IS UNCLEAR OR MISSING
SAMPLE DATES OR TIMES UNCLEAR OR MISSING
—TEMPERATURE CRITERIA NOT MET
TRIC B RMATIO
TRIP BLANK PROVIDED
TRIP BLANK NOT PROVIDED
TRIP BLANK NOT ON COC
TRIP BLANK INTACT
TRH' BLANK NOT INTACT
RECEIVED WATER TRIP BLANK
RECEIVED SOIL TRIP BLANK
h9SC. INFORMATION
NUMBER OP ENCORES ? 254RAM SRAM
NUMBER OF 5035 FIELD KITS ?—
NUMBER OF I.AN FILTERED METALS?
SUMMARY OF COMMENTS:
TEMPERATURE INFORMATION
IR THERM ID I CORR. FACTOR
OBSERVED TEMPS: _
CORRECTED TEMPS: Z -
SAMPLE INFORMATION
INCORRECT NUMBER OF CONTAINERS USED
SAMPLE RECEIVED IMPROPERLY PRESERVED
INSUFFICIENT VOLUME FOR ANALYSIS
DATESrTIMES ON COC DO NOT MATCH SAMPLE LABEL
ID'S ON COC DO NOT MATCH LABEL
VOC VIALS HAVE HEADSPACE (MACRO BUBBLES)
BOTTLES RECEIVED BUT ANALYSIS NOT REQUESTED
NO BOTTLES RECEIVED FOR ANALYSIS REQUESTED
UNCLEAR FALTERING OR COMFOSITINC INSTRUCTIONS
SAMPLE CONTAINER(S) RECEIVED BROKEN
g5035 FIELD KITS NOT RECEIVED WITHIN 41 HOURS
BULK VOA SOIL JARS NOT RECEIVED WTTHLN 48 HOURS
% SOLIDS JAR NOT RECEIVED'
RESIDUAL CHLORINE PRESENT
IA}FICABLE TO EPA 600 SERIES OR NORTH CAROLINA ORGANICSI
67 Z
TFCHNICTAN SIGNATUREMATE 1 EVIEWERSIGNATUREIDATE_
RS O014
receipt confirmation 041514.xfs
FA18486: Chain of Custody
Page 2 of 4
Da) IS of 20
.o.ccu-res-r.
FA1B488—111,1"'••

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FA18486: Chain of Custody
Page 3 of 4
p 19 of 20

Job Change Order: FA18486_9/30/2014
-
A
Requested Date:
9/30/2014 Received Date:
9/20/2014
Account Name:
GRI (Geological Resources Inc.) Due Date:
9/29/2014
Project
Mountaire Spill; Shannon, NC Deliverable:
COMMB
CSR:
MMO TAT (Days)!
7
Sam pie A
Change: Per client request analyze samples for
V8260SL,
FA18486-1
AB8270SL, VMAVPH and BMAEPH,
DI-1-2'
Sample #. Change: Per client request anaym samples for V8260SL,
FA18486-2 ABB270SL, VMAVPH and BMAEPH.
01-2-2'
Above Changes Per: Terry Kennedy Date: 9/3012014 FA18486: Chain of Custody
To Client: This Change Order is confirmation of the revislons, pre0ously discussed with the Aocutest Client Service Page 4 of 4
Page 1 of 1
0° 20 of 20
ACMU-rEST.
FAta4e8 """"""""'

e-Hardcopy 2.4
REP.:.t t li BN IN
y " a tBh BIB
Technical, Repoi for A n ....e.. t. iltt�a B.B.G...l i,Rti ,l.l�.at."�' - � - a ?�B1�dot�` 'tBi�BCxt �h!] iEr7]°a'B:oRt��tl!'Fh:
GRI (Geological Resources Inc.)
Mountaire Spill; Shannon, NC
Accutest Job Number: FA18486R
Sampling Date: 09/17/14
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; �r@geo ogicalresourcesinc.com;
nml @ggeologicalresourcesinc. com
ATTN- Nicole Long
Total number of pages in report: 44
Test results contained within this data package meet the requirements Norm Farmer
of the National Environmental Laboratory Accreditation Program Technical Director
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Certifications: FL 03510), LA (03051), KS (E-10327), IA (366). IL (200063). NC (573). NI (FL002), SC (96038001)
DoD ELAP (L-A•B L2229), CA (04226CA), TX (T104704404), PA (68.03573), VA (460177),
AK, AR, CA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except In Its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
1 of 44
Accutest Laboratories is the sole authority for authorizing edits or modifications to this I�q��vY�g-l;
document. Unauthorized modification of this report is strictly prohibited. FA184ne1i ••�••,�• ••

Table of Contents
-I-
Section1: Sample Summary...................................................................................................
Section2: Summary of Hits....................................................................................................
Section3: Sample Results........................................................................................................
3.1: FA18486-1R: DI-1-2.....................................................................................................
3.2: FA18486-2R: DI-2-2.....................................................................................................
Section4: Misc. Forms............................................................................................................
4.1: Chain of Custody...........................................................................................................
Section 5: GC/MS Volatiles - QC Data Summaries..............................................................
5.1: Method Blank Summary ................................................................................................
5.2: Blank Spike Summary ...................................................................................................
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................
Section 6: GUMS Semi-volatiles - QC Data Summaries.....................................................
6.1: Method Blank Summary................................................................................................
6.2: Blank Spike Summary ...................................................................................................
6.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
Section7: GC Volatiles - QC Data Summaries.....................................................................
7.1: Method Blank Summary ................................................................................................
7.2: Blank Spike/Blank Spike Duplicate Summary..............................................................
7.3: Duplicate Summary.......................................................................................................
Section 8: GC Semi-volatiles - QC Data Summaries............................................................
8.1. Method Blank Summary ................................................................................................
8.2: BIank Spike/Blank Spike Duplicate Summary..............................................................
8.3: Duplicate Summary .......................................................................................................
Sections:
3
5
6
12
1.8
19
23
24
26
28
30
31
33
35
37
38
39
40
41
42
43
44
C° 2 of 44
ACCU- EST.
P UROR ".......—

Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Mountaire Spill; Shannon, NC
Job No: FAI8486R
Sample r Matrix Client
Col,iected., _
Number Date Time By Received Code Type Sample ID
FA18486-:1R,:09/l7/I4 13:12 TK 09/20/14 SO Soil
FA18486 2R 09/17/14 13:19 TK 09/20/14 SO Soil
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
J
0Q 3 of 44
ACCUTarSm
FAIWOR `...........

Summary of Hits
Jab Number:
FA18486R
Account:
GRI (Geological Resources Inc.)
Project:
Mountaire Spill; Shannon, NC
Collected:
09/17/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA18486-1R DI-1-2'
Acetone
Methyl acetate
Benzo(b)fluaranthene
Benzo (k) fluoranthene
Cll-C22 Aromatics (Unadj.)
Cl l-C22 Aromatics
FA18486-2R DI-2-2'
Acetone
C11-C22 Aromatics (Unadj.)
Cll-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Allphatics
Page 1 of 1
0.03911
0.053
0.016
mg/kg
SW846 8260B
0.007.7: J a '
0,026
0,0053
mg/kg
SW846 8260B
,,
02011 Ju;.-;';;
0,21
0.10
mg/kg
MADEP EPH REV 1.1
Ozl'4*11:7
0.21
0.10
mg/kg
MADEP EPH REV 1.1
12 6 10 7.8 mg/kg MADEP EPH REV 1.1
12 3 10 7.8 mg/kg MADEP EPH REV I A
0.048
0,014
mg/kg
SW846 8260B
11
8.0
mg/kg
MADEP EPH REV 1.1
s151
11
8.0
mg/kg
MADEP EPH REV 1.1
8.55 J
11
5.4
rng/kg
MADEP EPH REV 1.1
11
5.4
mg/kg
MADEP EPH REV 1.1
a4 of 44
Ammu-rEST.
FAIS48GR

Section 3
Sample �Resultis . ,
Report of Analysis
00 5 of as
ACCLITEE3-r.
FAISOM "'°"......

Accutest Laboratories .
Report of Analysis
Client Sample ID:
DI-1-2'
Lab Sample ID:
FA18486-1R
Matrix:
SO - Soil
Method:
SW846 8260B
Project:
Mountaire Spill; Shannon, NC
Date Sampled: 09/17/14
Date Received: 09/20/14
Percent Solids: 93.9
Page 1 of 2 j
t
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 H0088050.13 1 09/30/14 EP n/a n/a VH3347
Run #2
Initial Weight
Run # 1 5.07 g
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
71-43-2
Benzene
75-27-4
Bromodichloromethane
75-25-2
Bromoform
104-51-8
n-Butylbenzene
108-90-7
Chlorobenzene
75-00-3
Chloroethane
67-66-3
Chloroform
75-15-0
Carbon disulfide
56-23-5
Carbon tetrachloride
110-82-7
Cyclohexane
75-34-3
1,1-Dichloroethane
75-35-4
1,1-Dichloroethylene
96-12-8
1, 2-Dibromo-3-chloropropane
106-93-4
1, 2-Dibromoethane
107-06-2
1,2-Dichloroethane
78-87-5
1,2-Dichloropropane
124-48-1
Dibromochloromethane
75-71-8
Dichlorodifluoromethane
156-59-2
cis-1, 2•Dichloroethylene
10061-01-5
cis-1,3-Dichloropropene
541-73-1
m-Dichlorobenzene
95-50-1
o-Dichlorobenzene
106-46-7
p-Dichlorobenzene
156-60-5
trans- 1, 2-Dichloroethylene
10061-02-6
trans- 1, 3 -Dichloropropene
100-41-4
Ethylbenzene
591-78-6
2-Hexanone
98-82-8
Isopropylbenzene
108-10-1
4-Methyl-2-pentanone
79-20-9
Methyl acetate
74-83-9
Methyl bromide
0.053
0.016
mg/kg
0.0053
0.0011
mg/kg
0.0053
.0.0011
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0024
mg/kg
0.0053
0:0012
mg/kg
0.0053
0,0011
mg/kg
0.0053
0,0015
mg/kg
0.0053
0.0011
mg/kg
0.0053
0,0011
mg/kg
0,0053
0.0011
mg/kg
0.0053
0.0022
mg/kg
0.0053
0.0019
mg/kg
0.0053
0.0011
mg/kg
0.0053
0,0011
mg/kg
0.0053
0.0011
mg/kg
0.0053
0,0013
mg/kg
0,0053
0.0011
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0012
mg/kg
0.0053
0.0014
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0011
mg/kg
0.026
0.0051
mg/kg
0.0053
0.0011
mglkg
0.026
0.0053
mg/kg
0.026
0.0053
mg/kg
0.0053
0,0020
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
a� 6 of 44
ACOUTEBT.
FAI84HR "......"'"

Accutest Laboratories
Report of Analysis Page 2 of 2
"lient Sample ID: DI-1-2'
. ab Sample ID: FA18486-1R Date Sampled: 09/17/14
Matrix: SO - Soi] Date Received: 09/20/14
Method: SW846 8260B Percent Solids: 93.9
?roject: Mountaire Spill; Shannon, NC
VOA Special List
CAS No. Compound
74-87-3
Methyl chloride
108-87-2
Methylcyclohexane
75-09-2
Methylene chloride
78-93-3
Methyl ethyl ketone
1634-04-4
Methyl Tert Butyl Ether
91-20-3
Naphthalene
103-65-1
n-Propylbenzene
100-42-5
Styrene
71-55-6
1,1,1-Trlchloroethane
79-34-5.
1, 1, 2,2 -Tetrachloroethane
79-00-5
1, 1, 2-Trichloroethane
120-82-1
1,2,4-Trichlorobenzene
95-63-6
1,2,4-Trimethylbenzene
108-67-8
1, 3 , 5-Trimethylbenzene
127-18-4
Tetrackloroethylene
108-88-3
Toluene
79-01-6
Trichloroethylene
75-69-4
Trichlorofluoromethane
75-01-4
Vinyl chloride
1330-20-7
Xylene (total)
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
17060-07-0 1, 2-Dichloroethane-D4
Result RL MDL Units Q
0.0053
0,0021
mg/kg
0.0053
0.0011
mg/kg
0,011
0,0042
mg/kg
0.026
0.0079
mg/kg
0.0053
0.0011
mg/kg
0,0053
0,0021
mg/kg
0.0053
0.0011.
mg/kg
0.0053
0.0011
mg/kg
0,0053
0.0011
mg/kg
0,0053
0.0015
mg/kg
0.0053
0.0017
mg/kg
0.0053
0.0012
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0013
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0011
mg/kg
0.0053
0.0011
mg/kg
0.016
0.0028
mg/kg
Run# 1 Run# 2 Limits
75-124%
103%
75-126%
�10296 '�
71-133%
112°/%
72-135%
ND = Not detected MDL = Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N W Indicates presumptive evidence of a compound
a0 7 of 44
ACCIJT�t�`T:
FA18466R ...........•

Accutest Laboratories
Report of Analysis
Page 1 of 2
Client Sample ID:
DI-1-2'
Lab Sample ID:
FA18486-1R
Date Sampled: 09/17/14
Matrix:
SO - Soil
Date Received: 09/20/14
Method:
SW846 8270D
SW846 3550C
Percent Solids: 93.9
Project:
Mountaire Spill; Shannon, NC
File ID
DF
Analyzed By Prep Date
Prep Batch Analytical Batch
Run #1 L0679694.1) 1
10/03/14 FS 10/01/14
OP53341 SL3533
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result R.L MDL Units Q
65-85-0
Benzoic Acid
95-57-8
2-Chlorophenol
59-50-7
4-Chloro-3-methyl phenol
120-83-2
2,4-Diehlorophenol
105-67-9
2,4-Dimethylphenol
51-28-5
2,4-Dinitrophenol
534-52-1
4,6-Dinitro-o-cresol
95-48-7
2-Methylphenol
3&4-Methylphenol
88-75-5
2-Nitraphenol
100-02-7
4-Nitraphenol
87-86-5
Pentachlorophenol
108-95-2
Phenol
88-06-2
2,4,6-Trichlorophenol
83-32-9
Acenaphthene
208-96-8
Acenaphthylene
120-12-7
Anthracene
56-55-3
Benzo(a)anthracene
50-32-8
Benzo(a)pyrene
205-99-2
Benzo(b)fluoranthene
191-24-2
Benzo(g,h,i)perylene
207-08-9
Benzo(k)fluoranthene
101-55-3
4-Bromophenyl phenyl ether
85-68-7
Butyl benzyl phthalate
91-58-7
2-Chloronaphthalene
106-47-8
4-Chloroaniline
218-01-9
Chrysene
111-91-1
bis(2-Chloroethoxy)methane
111-44-4
bis(2-Chloroelhyl)ether
108-60-1
bis(2-Chlorolsopropyl)ether
7005-72-3
4-Chlorophenyl phenyl ether
121-14-2
2,4-Dinitrotoluene
0.89
0.18
mg/kg
0.18
0,018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.020
mg/kg
0.89
0.18
mg/kg
0.35
0.071
mg/kg
0.18
0.018
mg/kg
0.18
0.035
mg/kg
0.18
0.018
mg/kg
0.89
0.14
mg/kg
0.89
0.14
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0,18
0.022
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0,018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.019
mg/kg
0.18
0.018
mg/kg
0.18
0.035
mg/kg
0.18
0.021
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0,18
0.026
mg/kg
0.18
0.020
rrmg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
a® 8 of"
ACCU-rEBT.
FA WOR "......""'

Accutest Laboratories
Report of Analysis
Client Sample ID: DI-1-2'
Lab Sample ID: FA18486-IR Date Sampled: 09/17/14
Matrix: SO - Soil Date Received: 09/20/14
Method: SW846 8270D SW846 3550C Percent Solids: 93.9
Project: Mountaire Spill; Shannon, NC
ABN Special List
CAS No. Compound
606-20-2
2,6-Dinitrotoluene
91-94-1
3, 3'-Dichlorobenzidtne
53-70-3
Dibenzo(a,h)anthracene
132-64-9
Dibenzofuran
84-74-2
Di-n-butyl phthalate
117-84-0
Di-n-octyl phthalate
84-66-2
Diethyl phthalate
131-11-3
Dimethyl phthalate
117-81-7
bis(2-Ethylhexyl)phthalate
206-44-0
Fluoranthene
86-73-7
Fluorene
118-74-1
Hexachlorobenzene
87-68-3
Hexachlorobutadiene
77-47-4
Hexachlorocyclopentadiene
67-72-1
Hexachloroethane
193-39-5
Indeno (1, 2 , 3-cd) pyrene
78-59-1
Isophorone
91-57-6
2-Methylnaphthalene
91-20-3
Naphthalene
98-95-3
Nitrobenzene
621-64-7
N-Nitroso-di-n- pro pylamine
86-30-6
N-Nitrosodiphenylamine
85-01-8
Phenanthrene
129-00-0
Pyrene
CAS No. Surrogate Recoveries
367-12-4
2-Fluorophenol
4165-62-2
Phenol-d5
118-79-6
2,4,6-Tribromophenol
4165-60-0
Nitrobenzene-d5
321-60-8
2-Fluorobiphenyl
1718-51-0
Terphenyl-d14
Result
Run# 1
RL MDL Units Q
0.18
0.019
mg/kg
0.18
0,018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.35
0.035
mg/kg
0.18
0.035
mg/kg
0.35
0,035
mg/kg
0.18
0,035
mg/kg
0.35
0.035
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018.
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0,018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
Run# 2 Limits
40-102%
41-100%
42-108%
40-105%
43-107%
45-119%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit 13 = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
0S 9 of 44
ACCUTEST.
FA18496R """'°""`

Accutest Laboratories
Report of Analysis
Client Sample 1D:
DI-1-2'
Lab Sample ID:
FA18486-1R
Matrix:
SO - Soil
Method:
MADEP VPH REV 1,1
Project:
Mountalre Spill; Shannon, NC
File ID
DF Analyzed By
Run #1 UV066166.1) 1 10/02/14 AH
Run #2
Page 1 of I
Date Sampled: 09/17/14
Date Received: 09/20/14
Percent Solids: 93.9
Prep Date Prep Batch Analytical Batch
n/a n/a GUV3514
Initial Weight Final Volume Methanol Aliquot
Run #1 5.30 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.
Compound
71-43-2
Benzene
100.41-4
Ethylbenzene
1634-04-4
Methyl Teri Butyl Ether
91-20-3
Naphthalene
108-88-3
Toluene
m,p-Xylene
95-47-6
o-Xylene
C5- C8 Aliphatics (Unadj.)
C9- C12 Aliphatics (Unadj.)
C9- C10 Aromatics (Unadj.)
C5- C8 Aliphatics
C9- C12 Aliphatics
C9- C10 Aromatics
CAS No.
Surrogate Recoveries
460-00-4
BFB
460-00-4
BFB
Result
Run# 1
RL
MDL
Units Q
0.054
0.054
mg/kg
0.11
0.054
mg/kg
0.11
0.054
mg/kg
0.27
0.16
mg/kg
0.11
0,054
mg/kg
0.22
0.11
mg/kg
0.11
0.054
mg/kg
5.4
1.9
mg/kg
5.4
1.9
mg/kg
5.4
1.9
mg/kg
5.4
1.9
mg/kg
5.4
1.9
mg/kg
5.4
1.9
mg/kg
Run# 2 Limits
70-130%
70-130%
ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
110 of 44
s CCtJ-rF=s-:
FA18MR `"'""""""'

Accutest Laboratories.
Report of Analysis
3ient Sample ID: DI-1-2'
,ab Sample ID: FA18496-1R Date Sampled: 09/17/14
latrix: SO - Soil Date Received: 09/20/14
4thod: MADPP EPH REV 1.1 SW846 3546 Percent Solids: 93.9
'roject: Mountaire Spill; Shannon, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN010700.1) 1 10/09/14 NAF 10/01/14 OP53355 GNN466
Run #2
Initial Weight Final Volume
Run # 1 20.5 g 2.0 ml
Run #2
MAEPH List
CAS No.
Compound
83-32-9
Acenaphthene
208-96-8
Acenaphthylene
120-12-7
Anthracene
56-55-3
Benzo(a)anthracene
50-32-8
Benzo(a)pyrene
205-99-2
Benzo(b)fluoranthene
191-24-2
Benzo(g,h,i)perylene
207-08-9
Benzo(k)fluoranthene
218-01-9
Chrysene
53-70-3
Dibenzo(a,h)anthracene
206-44-0
Fluoranthene
86-73-7
Fluorene
193-39-5
Indeno (1, 2,3-cd) pyrene
91-57-6
2-Methyinaphthalene
91-20-3
Naphthalene
85-01-8
Phenanthrene
129-00-0
Pyrene
Cll-C22 Aromatics (Unadj.)
Cll-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Aliphatics
CAS No.
Surrogate Recoveries
3386-33-2
1-Chlorooctadecane
580-13-2
2-Bromonaphthalene
84-15-1
o-Terphenyl
321-60-8•
2-Fluorobiphenyl
Result
Run# 1
RL MDL Units Q
0.21
0.10
mg/kg
0.21
0.10
mg/kg
0.21
0.10
mg/kg
0.21
0.10
mg/kg
0.21
0.10
mg/kg
0.21
0.10
mg/kg j
0.21
0.10
mg/kg
0.21
0.10
mg/kg j
0.21
0.10
mg/kg
0.21
0.10
mg/kg
0.21
0.10
mg/kg
0.21
0.10
mg/kg
0.21
0.10
mg/kg
0.21
0.10
mg/kg
0.21
0.10
mg/kg
0.21
0.10
mg/kg
0.21
0.10
mg/kg
10
7.8
mg/kg
10
7.8
mg/kg
10
5.2
mg/kg
10
5.2
mg/kg
Run# 2 Limits
40-140%
40-140%
40-140%
40-140%
ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
so 11 of 44
FAINUR

Acculest Laboratories
Report of Analysis Page I of 2
Client Sample ID: DI-2-2'
Lab Sample ID: FA18486-211 Date Sampled: 09/17/14
Matrix: SO - Soil Date Received: 09/20/14
Method: SW846 8260B Percent Solids: 92.3
Project: Mountaire Spill; Shannon, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 H0088051.D 1 09/30/14 EP n/a n/a VH3347
Run #2
Initial Weight
Run # l 5.69 g
Run #2
VOA Special List
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
71-43-2
Benzene
75-27-4
Bromodichlaromethane
75-25-2
Bromoform
104-51-8
n-Butylbenzene
108-90-7
Chlorobenzene
75-00-3
Chloroethane
67-66-3
Chloroform
75-15-0
Carbon disulfide
56-23-5
Carbon tetrachloride
110-82-7
Cyclohexane
75-34-3
1,1-Dichloroethane
75-35-4
1, 1 -Dichloroethylene
96-12-8
1,2-Dibromo-3-chloropropane
106-93-4
1, 2-Dibromoethane
107-06-2
1,2-Dlchloroethane
78-87-5
1,2-Dichloropropane
124-48-1
Dibromochloromethane
75-71-8
Dichlorodifluoromethane
156-59-2
cis- 1, 2-Dichloroethylene
10061-01-5
cis- 1, 3-Dichlaropropene
541-73-1
m-Dichlorobenzene
95-50-1
o-Dichlorobenzene
106-46-7
p-Dichlorobenzene
156-60-5
trans- l,2-Dichloroethylene
10061-02-6
trans-1,3-Dichloropropene
100-41-4
Ethylbenzene
591-78-6
2-Hexanone
98-82-8
Isopropylbenzene
108-10-1
4 -Methyl-2-pentanone
79-20-9
Methyl acetate
74-83-9
Methyl bromide
0.048
0.0048
0.0048
0.0048
0.0048
0.0048
0.0048
0.0048
0.0048
0.0048
0.0048
0.0048
0.0048
0.0048
0.0048
0,0048
0.0048
0.0048
0.0048
0,0048
0.0048
0.0048
0.0048
0.0048
0.0048
0.0048
0.0048
0.024
0,0048
0,024
0.024
0,0048
0.014
0,00095
0,00095
0.0010
0.00095
0.00095
0.0022
0.0011
0.00095
0.0013
0.0010
0,00095
0.00095
0.0020
0.0017
0.00095
0.00095
0.00095
0.0012
0.00095
0.00095
0,00095
0.00095
0,0011
0.0013
0.00095
0.00095
0.0047
0.00095
0.0048
0.0048
0.0018
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
a12 of 44
ACCUTEBT.
FAIMOR `"'""'"""'

Acculest Laboratories
Report of Analysis
Client Sample ID: DI-2-2'
Lab Sample ID: FA18486-21t Date Sampled: 09/17/14
Matrix: SO - Soil Date Received: 09/20/14
Method: SW846 8260E Percent Solids: 92.3
Project: Mountaire Spill; Shannon, NC
VOA Special List
CAS No. Compound
74-87-3
Methyl chloride
108-87-2
Methylcyclohexane
75-09-2
Methylene chloride
78-93-3
Methyl ethyl ketone
1634-04-4
Methyl Tert Butyl Ether
91-20-3
Naphthalene
103-65-1
n-Propylbenzene
100-42-5
Styrene
71-55-6
1.1,1-Trichloroethane
79-34-5
1, 1, 2,2 -Tetrachloroethane
79-00-5
1,1,2-Trichloroethane
120-82-1
1,2,4-Trichlorobenzene
95-63-6
1, 2,4-Trimethylbenzene
108-67-8
1,3, 5-Trimethylbenzene
127-18-4
Tetrachloroethylene
108-88-3
Toluene
79-01-6
Trichloroethylene
75-69-4
Trichlorofluoromethane
75-01-4
Vinyl chloride
1330-20-7
Xylene (total)
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
17060-07-0 1, 2-Dichloroethane-D4
Result
Run# 1
RL MDL Units Q
0.0048
0.0019 mg/kg
0.0048
0.00095 mg/kg
0.0095
0.0038 mg/kg
0.024
0.0071 mg/kg
0.0048
0.00095 mg/kg
0.0048
0.0019 mg/kg
0.0048
0.00095 mg/kg
0,0048
0,00095 mg/kg
0.0048
0.00095 mg/kg
0.0048
0.0013 mg/kg
0,0048
0.0015 mg/kg
0,0048
0,0011 mg/kg
0.0048
0.00095 mg/kg
0.0048
0.00095 mg/kg
0.0048
0,0012 mg/kg
0.0048
0.00095 mg/kg
0.0048
0,00097 mg/kg
0,0048
0.00095 mg/kg
0.0048
0,00097 mg/kg
0,014
0.0025 mg/kg
Run## 2 Limits
75-124%
75-126`Yo
71-133%
72-135%
Page 2 of 2
ND = Not detected MDL m Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
n 13 of"
ACCU-rEST.
FAISISSR "'""'"""'

Accutest Laboratories
Report of Analysis
Client Sample ID:
DI-2-2'
Lab Sample ID:
FA18486-211
Matrix:
SO - Soil
Method:
SW846 8270D SW846 3550C
Project:
Mountaire Spill; Shannon, NC
Date Sampled: 09/17/14
Date Received: 09/20/14
Percent Solids: 92.3
Page I of 2 N
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 L0679695.1) 1 10/03/14 FS 10/01/14 OP53341 SL3533
Run #2
Initial Weight Final Volume
Run # 1 30.0 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound
65-85-0
Benzoic Acid
95-57-8
2-Chlorophenol
59-50-7
4-Chloro-3-methyl phenol
120-83-2
2,4-Dichlorophenol
105-67-9
2,4-Dimethylphenol
51-28-5
2,4-Dinitrophenol
534-52-1
4 , 6-Dinitro-o-cresol
95-48-7
2-Methylphenol
3&4-Methylphenol
88-75-5
2-Nitrophenol
100-02-7
4-Nitrophenol
87-86-5
Pentachlorophenol
108-95-2
Phenol
88-06-2
2,4,6-Trichlorophenol
83-32-9
Acenaphthene
208-96-8
Acenaphthylene
120-12-7
Anthracene
56-55-3
Benzo(a)anthracene
50-32-8
Benzo(a)pyrene
205-99-2
Benzo(b)fluoranthene
191-24-2
Benzo(g,h,i)perylene
207-08-9
Benzo(k)fluoranthene
101-55-3
4-Bromophenyl phenyl ether
85-68-7
Butyl benzyl phthalate
91-58-7
2-Chloronaphthalene
106-47-8
4-Chloroaniline
218-01-9
Chrysene
111-91-1
bis(2-Chloroethoxy)methane
111-44-4
bis(2-Chloroethyl)ether
108-60-1
bis(2-Chloroisopropyl)ether
7005-72-3
4-Chlorophenyl phenyl ether
121-14-2
2,4-Dinitrotoluene
Result RL MDL Units Q
0.90
0.18
mg/kg
0.18
0.018
mg/kg
0,18
0.018
mg/kg
0.18
0.019
mg/kg
0.18
0,020
mg/kg
0.90
0.18
mg/kg
0.36
0.072
mg/kg
0.18
0.018
mg/kg
0.18
0.036
mg/kg
0.18
0.018
mg/kg
0.90
0.14
mg/kg
0.90
0.14
mg/kg
0.18
0.018
mg/kg
0.18
0,018
mg/kg
0.18
0.023
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0,018
mg/kg
0.18
0.018
mg/kg
0.18
0.020
mg/kg
0.18
0.018
mg/kg
0.18
0.036
mg/kg
0.18
0.021
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.019
mg/kg
0.18
0.027
mg/kg
0.18
0.021
mg/kg
ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
In 14 of 44
ACCU7EBT
FA1849SR "'.........

Accutest Laboratories
Report of Analysis
Client Sample ID: DI-2-2'
Lab Sample ID: FA18486-211 Date Sampled: 09/17/14
Matrix: SO - Soil Date Received: 09/20/14
Method: SW846 8270D SW846 3550C Percent Solids: 92.3
Project: Mountaire Spill; Shannon, NC
ABN Special List
CAS No. Compound
606-20-2
2,6-Dinitroioluene
91-94-1
3,3'-Dichlorobenzidine
53-70-3
Dibenzo(a,h)anthracene
132-64-9
Dibenzofuran-
84-74-2
Di-n-butyl phthalate
117-84-0
Di-n-octyl phthalate
84-66-2
Diethyl phthalate
131-11-3
Dimethyl phthalate
117-81-7
bis(2-Ethylhexyl)phthalate
206-44-0
Fluoranthene
86-73-7
Fluorene
118-74-1
Hexachlorobenzene
87-68-3
Hexachlorobutadiene
77-47-4
Hexachlorocyclopentadiene
67-72-1
Hexachloroethane
193-39-5
Indeno(1,2,3-cd)pyrene
78-59-1
Isophorone
91-57-6
2-Methylnaphthalene
91-20-3
Naphthalene
98-95-3
Nitrobenzene
621-64-7
N-Nitroso-di-n-propylamine
86-30-6
N-Nitrosodiphenylamine
85-01-8
Phenanlhrene
129-00-0
Pyrene
CAS No. Surrogate Recoveries
367-12-4
2-Fluorophenol
4165-62-2
Phenol-d5
118-79-6
2,4,6-Tribromophenol
4165-60-0
Nitrobenzene-d5
321-60-8
2-Fluorobiphenyl
1718-51-0
Terphenyl-d14
Result RL MDL Units Q
Run# I
0.18
0.020
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.36
0.036
mg/kg
0.18
0.036
mg/kg
0.36
0.036
mg/kg
0.18
0.036
mg/kg
0.36
0.036
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mglkg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0,018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
0.18
0.018
mg/kg
Run# 2 Limits
40-102%
41-100%
42-108%
40-105%
43-107%
45-119%
Page 2 of 2
ND Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
i 15 of 44
ACGLJTEST.
FAlBMBR "......""'

Accutest Laboratories
Report of Analysis
Client Sample ID:
DI-2-2'
Lab Sample ID:
FA18486-21Z
Matrix:
SO - Soil
Method:
MADEP VPH REV 1.1
Project:
Mountaire Spill; Shannon, NC
File ID
DF Analyzed By
Run #1 UV066167.1) 1 10/02/14 AH
Run #2
Page 1 of I N
Date Sampled: 09/17/14
Date Received: 09/20/14
Percent Solids: 92.3
Prep Date Prep Batch Analytical Batch
n/a n/a GUV3514
Initial Weight Final Volume Methanol Aliquot
Run #1 4.02 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.
Compound
71-43-2
Benzene
100-41-4
Ethylbenzene
1634-04-4
Methyl Ter( Butyl Ether
91-20-3
Naphthalene
108-88-3
Toluene
m,p-Xylene
95-47-6
o-Xylene
C5- C8 Aliphatics (Unadj.)
C9- C12 Aliphatics (Unadj )
C9- C10 Aromatics (Unadj.)
C5- C8 Aliphatics
C9- C12 Aliphatics
C9- C10 Aromatics
CAS No.
Surrogate Recoveries
460-00-4
BFB
460-00-4
BFB
Result , RL MDL Units Q
N, .D2�E =�^ rt �r
'ND' S
0.073
0.073
mg/kg
"`
0.15
0.073
mg/kg
0.15
0.073
mg/kg
ND:`
0.36
0.22
mglkg
0.15
0.073
mg/kg
NO
0.29
0.15
mg/kg
ND'''° �,..°'' ' "
0.15
0.073
mg/kg
,ND� , a,;.
7.3
2.6
mg/kg
ND
7.3
2.6
mg/kg
7.3
2.6
mg/kg
ND
7.3
2.6
mg/kg
jIVp on ' :I'll
7.3
2.6
mg/kg
ND`
7.3
2.6
mg/kg
Run# 1
Run# 2
Limits
110%
70-130%
70-130%
ND = Not detected MDL = Method Detection Limit
RL W Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
16 of 44
FA18WR "•.........

Accutest Laboratories
Report of Analysis
Client Sample ID: DI-2-2'
Lab Sample ID: FA18486-211 Date Sampled: 09/17/14
Matrix: SO - Soil Date Received: 09/20/14
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 92.3
Project: Mountaire Spill; Shannon, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN010701.1) 1 10/09/14 NAF 10/01/14 OP53355 GNN466
Run #2
Initial Weight Final Volume
Run #1 20.2 g 2.0 ml
Run #2
MAEPH List
CAS No.
Compound
83-32-9
Acenaphthene
208-96-8
Acenaphthylene
120-12-7
Anthracene
56-55-3
Benzo(a)anthracene
50-32-8
Benzo(a)pyrene
205-99-2
Benzo(b)fluoranthene
191-24-2
Benzo(g,h,i)perylene
207-08-9
Benzo(k)fluoranthene
218-01-9
Chrysene
53-70-3
Dibenzo(a,h)anthracene
206-44-0
Fluoranthene
86-73-7
Fluorene
193-39-5
Indeno (1, 2,3-cd) pyrene
91-57-6
2-Methylnaphthalene
91-20-3
Naphthalene
85-01-8
Phenanthrene
129-00-0
Pyrene
C11-C22 Aromatics (Unadj.)
C1 i-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Aliphatics
CAS No.
Surrogate Recoveries
3386-33-2
1-Chlorooctadecane
580-13-2
2-Bromonaphthalene
84-15-1
o-Terphenyl
321-60-8
2-Fluorobiphenyl
Result
Run# I
RL MDL Units Q
0.2I
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
0.21
0.11
mg/kg
11
8.o
mg/kg J
11
8.0
mg/kg J
11
5.4
mg/kg J
11
5.4
mg/kg
Run# 2 Limits
40-140%
40-140%
40-140%
40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
a97 of 44
ACCIJTES-r.
FA18486R "'""'"""'

Section 4
{
Mist. Farms e �9'� ;.x.,.�, , a �� I
7 ,.,.. ,
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
I18 of 44
Akccu-rEa-r.
FAIBMSR ............

me Accutm tiavoratortes 3outneast 1136
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FA18486R: Chain of Custody
Page 1 of 4
[a 19 of 44
^CCU-rea-r
FAI80SIR - ..........

ACCUTEST LABORATORIES SAMPLE RECEIPT CONFIRMATION
ACCUTEST'S JOB NUMBER: El p 14 T& CLIENT: G. (Z1-- _ . -- PROJECT:J'U1ns 4%A c j L S'p : l (
DAT&MME RECEIVED: r) y f 0 3 b _(MMlDD1YY 24:60I NUMBER OF COOLERS RECEIVED:
METHOD OF DELIVERY: FEbE7t UPS ACCUTEST COURIER GREYHOUND DELIVERY OTHER
AIRBILLNUMBERS: 8013 UlZS-Y7't
LR INFORMATION
CUSTODY SEAL NOT PRESENT OR NOT INTACT
CHAIN OF CUSTODY NOT RECEIVED (COC)
ANALYSTS REQUESTED IS UNCLEAR OR MISSING
SAMPLE DATES OR TIMES UNCLEAR OR MISSING
—TEMPERATURE CRITERIA NOT MET
TRIP BLANK INFORM I ON
TRIP BLANK PROVIDED
P BLANK NOT PROVIDED
TRIP BLANK NOT ON COC
BLANK INTACT
TRIP BLANK NOT INTACT
RECEIVED WATER TRIP BLANK
ECEIVED SOIL TRIP BLANK
MISC. INFORMATION
NUM(ItkOFENCORES? 25-CRAM SCRAM
NUMBER OF 5035 FIELD KITS ?
NUMBER OF LAB FILTERED METALS ?
SUMMARY OF COMMENTS:
JEMPERATURE INFQBMAIION
III THERM ID 1 CORR. FACTOR
OBSERVED TEMPS: ')_`i
CORRECTED TEMPS: -2-7
SAMPLE INFORMATION
CORRECT NUMBER OF CONTAINERS USED
JHPLE RECEIVED IMPROPERLY PRESERVED
SUFFICIENT VOLUME FOR ANALYSIS
1TE5f('1'MES ON COC DO NOT MATCH SAMPLE LABEL
'S ON COC DO NOT MATCH LABEL
)C VIALS HAVE HEADSPACE (MACRO BUBBLES)
)TILES RECEIVED BUT ANALYSIS NOT REQUESTED
) BOTTLES RECEIVED FOR ANALYSIS REQUESTED
CLEAR FILTERING OR COMPOSITTNG INSTRUCTIONS
MPLE CONTAINER(S) RECEIVED BROKEN
15 FIELD KITS NOT RECEIVED WITHIN 48 HOURS
lK VOA SOIL JARS NOT RECEIVED WITHIN 48 HOURS
SOLIbS JAR NOT RECEIVED
;SIDUAL CHLORINE PRESENT
(APPTCABLE TO EPA 600 SERFS OR NORTH CAROLINA ORGANICSI
TECHNICIAN SIGNATURFJDATB REVIEWER SIGNATURE/DATE
RS UN14
receipt confirmation 041514.xis
A
L
FA1.8486R: Chain of Custody
Page 2 of 4
ap 20 of 44
ACCL_ITEST.
FA18486R ...........•

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Job Change Order: FA18486_9/30/2014
Requested Date:
9/3012014 Received Date:
9/20/2014
Account Name:
GRI (Geological Resources Inc.) Due Date:
9/29/2014
Project
Mountaire Spill; Shannon, NC Deliverable:
COMMB
CSR:
MMD TAT (Days):
7
Sample A
Change: Per client request analyze samples for V8260SL,
FA18486.1
AB8270SL, VMAVPH and BMAEPH.
D I-1-2'
Sample #: Change: Per client request analyze samples fof V8260SL,
FA18486-2 AB8270SL, VMAVPH and BMAEPH.
DI.2.2`
Above Changes Per: Terry Kennedy Date: 913012014 FAl 848GR: Chain of Custody
To Client: This Change Orderis confirmation Df the revisions, previously discussed with the Accuteat Client Service Page 4 of 4
Page 1 of 1
Q£22 of 44 ACCLJTEBT.
FA18488R "•"'• ""

Section 5
f
SOUtFI®pp�g�pSt,
60
III iir kE.il!°1lrta{ dJlid�dturi
GC/MS Volatiles
.4.s ittsw h , .. ,
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Qa 23 of 44
ACCLJTEST.
FAIWOR "```"'"""'

Method Blank Summary Page I of 2
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Sample
File ID DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VH3347-MB
H0088037.D 1
09/30/14
EP
n/a
n/a
VH3347
The QC reported here applies to the following samples: Method: SW846 8260E
FA18486-lR, FA18486-21Z
CAS No. Compound
67-64-1
Acetone
71-43-2
Benzene
75-27-4
Bromodichloromethane
75-25-2
Bromoform
104-51-8
n-Butylbenzene
108-90-7
Chlorobenzene
75-00-3
Chloroethane
67-66-3
Chloroform
75-15-0
Carbon disulfide
56-23-5
Carbon tetrachloride
110-82-7
Cyclohexane
75-34-3
1,1-Dichloroethane
75-35-4
1,1-Dichloroethylene
96-12-8
1, 2-Dibromo-3-chloropropane
106-93-4
1, 2-Dibromoethane
107-06-2
1,2-Dichloroethane
78-87-5
1,2-Dichloropropane
124-48-1
Dibromochloromethane
75-71-8
Dichlorodifiuoromethane
156-59-2
cis- 1, 2-Dichloroethylene
10061-01-5 cis- 1, 3-Dichloropropene
541-73-1
m-Dichlorobenzene
95-50-1
o-Dichlorobenzene
106-46-7
p-Dichlorobenzene
156-60-5
trans-1,2-Dichloroethylene
10061-02-6 trans- 1, 3-Dichloropropene
100-41-4
Ethylbenzene
591-78-6
2-Hexanone
98-82-8
Isopropylbenzene
108-10 -1
4 -Methyl-2-pentanone
79-20-9
Methyl acetate
74-83-9
Methyl bromide
74-87-3
Methyl chloride
108-87-2
Methylcyclohexane
75-09-2
Methylene chloride
78-93-3
Methyl ethyl ketone
Result
RL MDL Units Q
50
15
ug/kg
5.0
1.0
ug/kg
5.0
1.0
ug/kg
5.0
Li
ug/kg
5.0
1.0
ug/kg
5.0
1.0
ug/kg
5.0
2.3
ug/kg
5.0
1.1
ug/kg
5.0
1.0
ug/kg
5.o
1.4
ug/kg
5.0
1.1
ug/kg
5.0
1.0
ug/kg
5.0
1.0
ug/kg
5.0
2.1
ug/kg
5.0
1.8
ug/kg
5.0
1.0
ug/kg
5.0
1.0
ug/kg
5.0
1.0
ug/kg
5.0
1.3
ug/kg
5.0
1.0
ug/kg
5.0
1.0
ug/kg
5.0
1.0
ug/kg
5.0
1.0
ug/kg
5.0
1.1
ug/kg
5.0
1.3
ug/kg
5.0
1.0
ug/kg
5.0
1.0
ug/kg
25
4.9
ug/kg
5.0
1.0
ug/kg
25
5.0
ug/kg
25
5.0
ug/kg
5.0
1.9
ug/kg
5.0
2.0
ug/kg
5.0
1.0
ug/kg
10
4.0
ug/kg
25
7.5
ug/kg
® 24 of 44
ACCUTEST.
FAIMIBBR "'"",.,""""

_. _:.. Method Blank Summary _ . _.... - ......... ...
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Page 2 of 2
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VH3347-MB H0088037.D 1 09/30/14 EP n/a n/a VH3347
The QC reported here applies to the following samples:
FA18486-1R, FA18486-2R
CAS No. Compound
1634-04-4
Methyl Tert Butyl Ether
91-20-3
Naphthalene
103-65-1
n-Propylbenzene
100-42-5
Styrene
71-55-6
1, 1, 1 -Trichloroethane
79-34-5
1.1,2,2-Tetrachloroethane
79-00-5
1,1,2-Trichloroethane
120-82-1
1,2,4-Trichlorobenzene
95-63-6
1, 2 A-Trimethylbenzene
108-67-8
1,3,5-Trimethylbenzene
127-18-4
Tetrachloroethylene
108-88-3
Toluene
79-01-6
Trichloroethylene
75-69-4
Trlchlorofluoromethane
75-01-4
Vinyl chloride
1330-20-7
Xylene (total)
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
17060-07-0 1,2-Dichloroethane-D4
Result RL MDL
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5,0
15
Limits
1.0
2.0
1.0
1.0
1.0
1.4
1.6
1.2
1.0
1.0
1.3
1.0
1.0
1.0
1.0
2.7
75-124%
75-126%
71-133%
72-135%
Method: SW846 8260B
Units Q
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
�im 26 of 44
ACCUTE8T.
FAIM86R "'°"'°""'

Blank Spike Summary
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VH3347-BS
H0088036.D
1
09/30/14
EP
n/a
n/a
VH3347
The QC reported here applies to the following samples:
FA18486-1R, FA18486-21Z
CAS No. Compound
Spike BSP BSP
ug/kg ug/kg %
67-64-1
Acetone
250
229
71-43-2
Benzene
50
48.0
75-27-4
Bromodichloromethane
50
43.5
75-25-2
Bromoform
50
47.1
104-51-8
n-Butylbenzene
50
51.4
108-90-7
Chiorobenzene
50
56.1
75-00-3
Chloroethane
50
50.3
67-66-3
Chloroform
50
47.2
75-15-0
Carbon disulfide
50
48.9
56-23-5
Carbon tetrachloride
50
49.2
110-82-7
Cyclohexane
50
43.9
75-34-3
1, 1 -Dichloroethane
50
46.3
75-35-4
l,l-Dichloroethylene
50
48.2
96-12-8
1,2-Dibromo-3-chloropropane
50
48.8
106-93-4
1,2-Dibromoethane
50
53.7
107-06-2
1,2-Dichloroethane
50
49.0
78-87-5
1,2-Dichloropropane
50
47.1
124-48-1
Dibromochloromethane
50
44.7
75-71-8
Dichlorodifluoromethane
50
51.1
156-59-2
cis- 1, 2-Dichloroethylene
50
47.6
10061-01-5 cis-1,3-Dichloropropene
50
42.8
541-73-1
m-Dichlorobenzene _
50
58.0
95-50-1
o-Dichlorobenzene
50
58.1
106-46-7
p-Dichlorobenzene
50
52.1
156-60-5
trans- 1, 2 -Dichloroethylene
50
46.1
10061-02-6 trans- 1,3-Dichloropropene
50
50.4
100-41-4
Ethylbenzene
50
52.7
591-78-6
2-Hexanone
250
221
98-82-8
Isopropylbenzene
50
57.5
108-10-1
4-Methyl-2-pentanone
250
254
79-20-9
Methyl acetate
250
282
74-83-9
Methyl bromide
50
50.2
74-87-3
Methyl chloride
50
49.2
108-87-2
Methylcyclohexane
50
45.6
75-09-2
Methylene chloride
50
44.8
78-93-3
Methyl ethyl ketone
250
223
* W Outside of Control Limits.
12
89 =' a
102
.
Limits
61-152
76-126
74-130
76-127
71-128
81-129
68-133
72-123
72-122
78-133
73-126
73-125
81-136
70-137
77-126
74-128
74-125
76-127
68-168
74-126
80-123
81-129
80-129
76-130
70-127
75-131
77-123
72-133
80-136
76-132
67-137
65-139
71-144
75-128
74-137
75-137
Method: SW846 8260B
126 of 44
ACCUTES-n
FAI84UR "'""""""'

Blank Spike Summary _. .
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Page 2 of 2
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
7-13S H0088036.D 1 09/30/14 EP nla nla VH3347
The QC reported here applies to the following samples:
FA18486-1R, FA18486-2R
Spike
BSP
BSP
CAS No.
Compound
uglkg
ug/kg
%
Limits
1634-04-4
Methyl Tert Butyl Ether
50
46.7
TY777,
77-120
91-20-3
Naphthalene
50
48.7
97
79-129
103-65-1
n-Propylbenzene
50
56.8
3 5hf '
i11'4'';
80-135
100-42-5
Styrene
50
47.4
95 '^.:
78-125
71-55-6
1, 1. 1 -Trichloroethane
50
49.0
�98
70-129
79-34-5
1, 1. 2,2 -Tetrachloroethane
50
52.3
105p "
71-126
79-00-5
1, 1, 2-Trichloroethane
50
50.0
400`_�,
74-124
120-82-1
1,2,4-Trichlorobenzene
50
52.9
'106.01
78-130
95-63-6
1,2,4-Trimethylbenzene
50
52.3
.=
74-123
108 fi7 8
1,3,5 Trimethylbenzene
50
50.8
1020.r!
73-122
127-18-4
Tetrachloroethylene
50
53.3
t107..--,
79-130
108-88-3
Toluene
50
51.9104.."
76-124
79-01-6
Trichloroethylene
50
49.0
98, ; '',
75-128
75-69-4
Trichlorofluoromethane
50
50.7
it01
73-145
75-01-4
Vinyl chloride
50
48.597..;�
76-141
1330-20-7
Xylene (total)
150
168
14u1 ' C8 A'
11f280-129
CAS No.
Surrogate Recoveries
BSP
Limits
1868-53-7
Dibromofluoromethane
98%' 1J ^`i
75-124%
2037-26-5
Toluene-D8
100% ;.:
..:.:..
75-126%
460-00-4
4-Bromofluorobenzene
99%
71-133%
17060-07-0
1,2-Dichloroethane-D9
9$
72-135%
* = Outside of Control Limits.
Method: SW846 8260B
a27 of 44
AC✓CUTEST.
FA18*BR `...........

Matrix Spike/Matrix Spike Duplicate Summary Page I of
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA18574-IMS
H0088054.1)
1
09/30/14
EP
n/a
n/a
VH3347
FA18574-1MSD
H0088055.D
1
09/30/14
EP
n/a
n/a
VH3347
FA18574-1
H0088038.D
1
09/30/14
EP
n/a
n/a
VH3347
FA18574-1
H0088048.D
1
09/30/14
EP
n/a
n/a
VH3347
The QC reported here applies to the following samples:
FA18486-1R, FA18486-2R
FA18574-1 Spike MS MS
CAS No, Compound ug/kg Q ug/kg ug/kg %
Method: SW846 8260B
Spike MSD MSD Limits
ug/kg ug/kg % RPD ReQWD
67-64-1
Acetone
ND
279000
284000
102.,:
279000
253000
71-43-2
Benzene
ND
55700
52900
'95'p�NV
55700
55400
75-27-4
Bromodichloromethane
ND
55700
47100
85
55700
49100
75-25-2
Bromoform
ND
55700
53100
95y��`
55700
52500
104-51-8
n-Butylbenzene
10500 a
55700
54800
�90
55700
68600
108-90-7
Chlorobenzene
ND
55700
58400
' 1,lM ld.'���
55700
65000
75-00-3
Chlvroethane
ND
55700
56500
1'O1'
55700
56700
67-66-3
Chloroform
ND
55700
52700
95
55700
54500
75-15-0
Carbon disulfide
ND
55700
54000
97:'?''`
55700
57400
56-23-5
Carbon tetrachloride
ND
55700
53300
96 ..11
55700
56600
110-82-7
Cyclohexane
ND
55700
4910088;%<'
:
55700
51700
75-34-3
1,1-Dichloroethane
ND
55700
52500
'94 ,..;.
55700
53800
75-35 4
1,1 Dichlvraethylene
ND
55700
53400
gg�uxk=`
55700
55500
96-12-8
1,2-Dibromo-3-chloropropane
ND
55700
66900120
55700
67000
106-93-4
1,2-Dibromoethane
ND
55700
59500
°107t
55700
62500
107-06.2
1,2-Dichloroethane
ND
55700
54500
�98�'
55700
55100
78-87-5
1,2-Dichloropropane
ND
55700
53900
97 �gy
55700
55600
124-48-1
Dibromochloromethane
ND
55700
48600
8,7.,'r "
55700
51200
75-71-8
Dichlorodifluoromethane
ND
55700
58700
' f M ,
55700
57300
156-59-2
cis- 1, 2 -Dichloroethylene
ND
55700
54200
971POR
55700
55500
10061-01-5
cis- 1, 3-Dichloropropene
ND
55700
46600
84''' <':
55700
49700
541 73 1
m Dichlorobenzene
ND
55700
56100
101���„!
55700
64400
95-50-1
o-Dichlorobenzene
ND
55700
58600
105
55700
65400
106-46-7
p-Dichlorobenzene
ND
55700
50300
90
55700
58700
156-60-5
trans-1,2-Dichloroethylene
ND
55700
51300
9 1
55700
52500
10061-02-6
trans- 1,3-Dichloropropene
ND
55700
54600
_
98
55700
57900
100-41-4
Ethylbenzene
25500a
55700
83000
�'
h100':',"1"1'..'
55700
89100
591-78-6
2-Hexanone
ND
279000
278000
279000
256000
98-82-8
Isopropylbenzene
8320a
55700
66900
105'' �e
55700
77200
108-10-1
4-Methyl-2-pentanone
ND
279000
308000
.111
279000
290000
79-20-9
Methyl acetate
ND
279000
351000
'1216 "
279000
336000
74-83-9
Methyl bromide
ND
55700
55500
1[10,. '°'"
55700
55300
74-87-3
Methyl chloride
ND
55700
55400
99'
55700
57200
108-87-2
Methylcyclohexane
118 j
55700
50100
'6p'9"' .'
55700
53800
75-09-2
Methylene chloride
ND
55700
50600
.91} '
55700
52700
78-93-3
Methyl ethyl ketone
ND
279000
291000
104
279000
262000
* = Outside of Control Limits.
61-152/27
76-126/26
74-130/25
76-127/26
71-128/35
81-129/29
68-133/29
72-123/26
72-122/29
78-133/29
73-126/32
73-125/27
81-136/28
70-137/29
77-126/26
74-128/23
74-125/25
76-127/27
68-168/29
74-126/26
80-123/26
81-129/33
80-129/32
76-130/32
70-127/27
75-131/28
77-123/31
72-133/26
80-136/32
76-132/26
67-137/30
65-139/31
71-144/27
75-128/31
74-137/28
75-137/25
Q28 of 44
ACCUTEa-r
FAI848GR "....... r•

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FAI8486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Page 2 of 2
;ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
?A18574-1MS
H0088054.D
1
09/30/14
EP
nla
n/a
VH3347
'A18574-IMSD
1-10088055.13
1
09/30/14
EP
n/a
n/a
VH3347
aA18574-1
H008$03$.D
I
09/30/14
EP
n/a
n/a
VH3347
?A18574-1
H0088048.D
1
09/30/14
EP
n/a
n/a
VH3347
The QC reported here applies to the following samples: Method: SW846 8260E
FA18486-1R, FA18486-2R
FA18574-1 Spike MS MS Spike MSD MSD Limits
CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD RecJRPD
1634-04-4 Methyl Tert Butyl Ether ND 55700 55400 99 . !' 55700 54200 9V7.12 ._' 77-120/24
91-20-3 Naphthalene 36100 a 55700 98900 113 55700 96200 108 3 79-129/33
103 fi5 1 n-Prapylbenzene 3780D a 55700 93500 100 55700 105000 121r1, 12 ':' 80-135/33
100-42-5 Styrene 242 J 55700 49300 88 11 55700 56000 . 4. T 78-125/30
71-55-6 1, 1. 1 -Trichloroethane ND 55700 53500 96 °. 55700 56100 10F 5 µ, 70-129/27
79-34-5 1, 1, 2,2-Tetrachloroethane ND 55700 60300 108q 55700 57300 103 5 ,i. 71-126/30
79-00-5 1,1,2-Trichloroethane ND 55700 58900 106 55700 59700 107, 1 74-124/28
120-82-1 1,2,9-Trichlorobenzene ND 55700 50500 91 55700 60100 108 117078130134
95-63-6 1,2,4-Trimethylbenzene 385000b 55700 414000 743* 55700 414000 743* 0 74-123/34
108-67-8 1,3,5-Trimethylbenzene 109000 b 55700 164000 Qq,�"_. 55700 169000 la`., J0, q 73-122/33
127-18-4 Tetrachloroethylene ND 55700 57500 103 55700 64300 115 11.- 79-130/3I
108-88-3 Toluene 10400 55700 65300 r99 f ' " 55700 69700 p106 76-124130
79-01-6 Trichloroethylene ND 55700 51800 93 55700 56000 ll}l, 8 75-128/27
75-69-4 Trichlorofluoromethane ND . 55700 54100 97 $5700 55600 100 3 73 145/31
75-01-4 Vinyl chloride ND 55700 54200 97 55700 53700 96. 1 76-141/27
1330-20-7 Xylene (total) 302000 b 167400 496000 '1'16,^ 167000 500000 14$ 1�{1 80 128/30
CAS No. Surrogate Recoveries MS MSD FAI8574-1 FA18574-1 Limits
1868-53-7 Dibromofluoromethane 97% B%" " $7%,yid NIP777] 91�96 '" 75-124%
2037-26-5 Toluene-138 101% " 102% fi 103% 100%' 75-126%
lwewtln,?'a g " y
460-00-4 4-Bromofluorobenzene 102% 401% 10$
�% ��9�� 99% 71-133%
17060-07-0 1, 2- Dichloroethane-D4 170.P 92% _� 9996 " `� 10196i��_ ^' 72-135`Yo
(a) Result is from Run #2.
(b) Result is from Run U.
* = Outside of Control Limits.
In 29 of 44
ACCUTEST.
FA154HR L..... " ••

Section 6
[ a.05
4if1 RI I I -1 j" NI €
� I � I u 131u ��cSoutheast
swr'' �sds 3.1 EI I '14S
a
■_ ,i �� S�PPb� '}���N �lI
tl
_klkik,i.•�4i:il:ila�?N�51;3A�ti�68d4�ixt:'�f
GC/MS Semi-,. Wi es
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
30 of 44
ACClJTE9T.
FAIUBGR `"'""'"""'

Method Blank Summary
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill, Shannon, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53341-MB
L0679680.D
1
10/03/14
FS
10/01/14
OP53341
SL3533
The QC reported here applies to the following samples; Method: SW846 8270D
FA18486-1R, FA18486-211
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
95-57-8
2-Chlorophenol
59-50-7
4-Chloro-3-methyl phenol
120-83-2
2,4-Dichlorophenoi
105-67-9
2,4-Dimethylphenol
51-28-5
2,4-Dinitrophenol
534-52-1
4, 6-Dinitro-o-cresol
95-48-7
2-Methylphenol
3&4-Methylphenol
88-75-5
2-Nitrophenol
100-02-7
4-Nitrophenol
87-86-5
Pentachlorophenol
108-95-2
Phenol
88-06-2
2,4,6-Trichlorophenol
83-32-9
Acenaphthene
208-96-8
Acenaphthylene
120-12-7
Anthracene
56-55-3
Benzo(a)anthracene
50-32-8
Benzo(a)pyrene
205-99-2
Benzo(b)fluoranthene
191-24-2
Benzo(g;,h,i)perylene
207-08-9
Benzo(k)fluoranthene
101-55-3
4-Bromophenyl phenyl ether
85-68-7
Butyl benzyl phthalate
91-58-7
2-Chloronaphihalene
106-47-8
4-Chloroaniline
218-01-9
Chrysene
111-91-1
bis(2-Chloroethoxy)methane
111-44-4
his (2-Chloroethyl)ether
108-60-1
bis(2-Chloroisopropyl)ether
7005-72-3
4-Chlorophenyl phenyl ether
121-14-2
2,4-Dinitrotoluene
606-20-2
2,6-Dinitrotoluene
91-94-1
3,3'-Dichlorobenzidine
53-70-3
Dibenzo(a,h)anthracene
132-6 0
Dibenzofuran
830
170
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
18
ug/kg
830
170
ug/kg
330
67
ug/kg
170
17
ug/kg
170
33
ug/kg
170
17
uglkg
830
130
ug/kg
830
130
ug/kg
170
17
ug/kg
170
17
ug/kg
170
21
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
18
ug/kg
170
17
ug/kg
170
33
ug/kg
170
20
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
25
ug/kg
170
19
ug/kg
170
18
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
JIM
31 of 44
A=MU-rEST.

Method Blank Summary .
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
..Page 2 of 2.
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
)P53341-MB
L0679680.1)
1
10/03/14
FS
10/01/14
OP53341
SL3533
The QC reported here applies to the following samples: Method: SW846 8270D
FA18486-1R, FA18486-ZR
CAS No. Compound Result RL MDL Units Q
84-74-2
Di-n-butyl phthalate
117-84-0
Di-n-octyl phthalate
84-66-2
Diethyl phthalate
131-11-3
Dimethyl phthalate
117-81-7
bis(2-Ethylhexyl)phthalate
206-44-0
Fluoranthene
86-73-7
Fluorene
118-74-1
Hexachlorobenzene
87-68-3
Hexachlorobutadiene
77-47-4
Hexachlorocyclopentadiene
67-72-1
Hexachloroethane
193-39-5
Indeno(1,2,3-cd)pyrene
78-59-1
Isophorone
91-57-6
2-Methylnaphthalene
91-20-3
Naphthalene
98-95-3.
Nitrobenzene
621-64-7
N-Nitroso-di-n-propylamine
86-30-6
N-Nitrosodiphenylamine
85-01-8
Phenanthrene
129-00-0
Pyrene
CAS No. Surrogate Recoveries
367-12-4
2-Fluorophenol
4165-62-2
Phenol-d5
118-79-6
2,4,6-Tribromophenol
4165-60-0
Nitrobenzene-d5
321-60-8
2-Fluorobiphenyl
1718-51-0
Terphenyl-dl4
330
33
ug/kg
170
33
ug/kg
330
33
ug/kg
170
33
ug/kg
330
33
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
170
17
ug/kg
Limits
7$96 41-100%
42-108%
8196��j�'F"., 40-105%
�,.... .
77'96` 43-107%
87% k 45-119%
Ch
J
i
I32 of 44
ACOU-rEST
FAID48Ot `'"'°""""'

Blank -Spike Summary
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Page I of 2 .
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53341-BS
L0679679.1)
1
10/03/14
FS
10/01/14
OP53341
SL3533
The QC reported here applies to the following samples:
FA18486-1R, FA18486-ZR
Spike
BSP
BSP
CAS No,
Compound
ug/kg
ug/kg
%
Limits
65-85-0
Benzoic Acid
3330
2910
87 'PO''.'
36-118
95-57-8
2-Chlorophenol
1670
1160
'70 "' � `
48-104
59-50-7
4-Chloro-3-methyl phenol
1670
1280
!77;L�aa
52-108
120-83-2
2,4-Dichlorophenol
1670
1240
74" ;,
51-105
105-67-9'
2,4-Dimethylphenol
1670
1330
E806jj:(,,`
43-96
51-28-5
2,4-Dinitrophenol
3330
3240
97
40-119
534-52-1
4,6-Dinitro-o-cresol
3330
2820
`85�@dEb_ `
64-121
95-48-7
2-Methylphenol
1670
1200
72
46-107
3&4-Methylphenol
3330
2480
74 ��Pl
44-111
88-75-5
2-Nitrophenol
1670
1200
72'-
10e
49-104
100-02-7
4-Nitrophenol
3330
2600
780'
56-116
87-86-5
Pentachlorophenol
3330
2650
80
61-114
108-95-2
Phenol
1670
1190
l,f4OA7
45-110
88-06-2
2,4,6-Trichlorophenol
1670
1210
73
56-109
83-32-9
Acenaphthene
1670
1280
17:;O�=E-
56-109
208-96 8
Acenaphthylene
1670
1270T6
56-106
120-12-7
Anthracene
1670
1310
7gq"_`°;
61-110
56-55-3
Benzo(a)anthracene
1670
1320
T9
66-111
50-32-8
Benzo(a)pyrene
1670
1260
76
59-104
205-99-2
Benzo(b)fluoranthene
1670
1290
77.q,'
67-113
191-24-2
Benzo(g,h,i)perylene
1670
1290
77 ' ':
67-113
207-08-9
Benzo(k)fluoranthene
1670
1350
VV
67-114
101-55-3
4-Bromophenyl phenyl ether
1670
1100
66 V
62-110
85-68-7
Butyl benzyl phthalate
1670
1330
;8Q04;
65-113
91-58-7
2-Chloronaphthalene
1670
1160
TFD': R-F
53-106
106-47-8
4-Chloroaniline
1670
1210
T3-�,-:
30-115
218-01-9
Chrysene
1670
1350
81F:',i;
65 112
111-91-1
bis(2-Chloroethoxy)methane
1670
1230
74 .;:;;
48-105
111-44-4
bis (2 -Chloroethyl) ether
1670
1130
681" -:
46-103
108-60-1
his (2-Chloroisopropyl) ether
1670
1120
67
40-110
7005-72-3
4-Chlorophenyl phenyl ether
1670
1190
7L' ' `'
58-106
121-14-2
2,4-Dinitrotoluene
1670
1240
T.4;;,;.'
59-109
606-20-2
2,6-Dinitrotoluene
1670
1250
75';°'`k'
61-107
91-94-1
3,3'-Dichlorobenzidine
1670
1170
70. :`
36-114
53-70-3
Dibenzo(a,h)anthracene
1670
1320
U91''
68-115
132-64-9
Dibenzofuran
1670
1260
76 F
57-108
* = Outside of Control Limits.
Method: SW846 8270D
a33 of 44
A U-rEST.
FA18MOR "......""'

Blank Spike Summary. ,
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Page of.2..
'ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
)P53341-BS
L0679679.13
1
10/03/14
FS
10/01/14
OP53341
SL3533
The QC reported here applies to the following samples:
FA18486-1R, FA18486-2R
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
84-74-2
Di-n-butyl phthalate
1670
1320
63-108
-T9 "
117-84-0
Di-n-octyl phthalate
1670
1370
82 i�v,
64-119
84 66 2
Diethyl phthalate
1670
125075'
k�. ''
61-109
131-11-3
Dimethyl phthalate
1670
1250
75„ ,�o
59-108
117-81-7
bis(2-Ethylhexyl)phthalate
1670
1350
81" ` ;
64-115
206-44-0
Fluoranthene
1670
1270
-76 -
60-108
86-73-7
Fluorene
1670
1290
77 9 �,,-..�
58-109
118-74-1
Hexachlorobenzene
1670
1140
68
59-111
87-68-3
Hexachlorobutadiene
1670
1190
71 .; ;,
41-108
77-47-4
Hexachlorocyclopentadiene
1670
1060
64''° '`'`
49-110
67-72-1
Hexachloroethane
1670
1060
t4
40-105
193-39-5
Indeno(1,2,3-cd)pyrene
1670
1180
°fir;,:,
66-116
78-59-1
Isophorone
1670
1230
17�1
T4
42-89
91-57-6
2-Methylnaphthalene
1670
1250
75y
47-106
91-20-3
Naphthalene
1670
1220
73' `
44-104
98-95-3
Nitrobenzene
1670
1190
71 :;;;::
43-108
621 64 7
N Nitroso-di n propylamine
1670
1220
73,'='''"
48-108
86-30-6
N-Nitrosodiphenylamine
1670
1310
°79!
62-110
85-01-8
Phenanthrene
1670
1280
77 ``
63-111
129-00-0
Pyrene
1670
1300
F28' '`
65-115
CAS No.
Surrogate Recoveries
BSP
Limits
367-12-4
2-Fluorophenol
70%`^:"
40-102%
4165-62-2
Phenol-d5
75.9fo y9
41-100%
118-79-6
2,4,6-Tribromophenol
42-108%
Nitrobenzene-d5
%4165-60-0
321-60-8
2-Fluorobiphenyl
43-107%
1718-51-0
Terphenyl-d19
87�40-105%
45-119%
* = Outside of Control Limits.
Method: SW846 8270D
0
iv
Q® 34 of 44
�.ccuY�srt
FAI84BOR ............

Matrix. Sp ike/Matr ix Spike Duplicate Summary.
Job Number: FAI8486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Page 1 of 2
Sample
File ID DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53341-MS
L0679687.1) 1
10/03/14
FS
10/01/14
OP53341
SL3533
OP53341-MSD
L0679688.D 1
10/03/14
FS
10/01/14
OP53341
SL3533
FA18707-6
L0679764.D 1
10/06/14
FS
10/01/14
OP53341
SL3536
The QC reported here applies to the following samples:
FA18486-1R, FA18486-2R
CAS No. Compound
FA18707-6 Spike MS MS
ug/kg Q ug/kg ug/kg %
Method: SW846 8270D
Spike MSD MSD Limits
ug/kg ug/kg % RPD Rec/RPD
65-85-0
Benzoic Acid
ND
3630
3550
98 '
3630
3560
95-57-8
2-Chlorophenol
ND
1820
1060
58`''r ,,"
1820
1190
59-50-7
4-Chloro-3-methyl phenol
ND
1820
1440
79`
1820
1500
120-83-2
2,4-Dichlorophenol
ND
1820
1270
70
�7�7w
1820
1390
105-67-9
2,4-Dimethylphenol
ND
1820
1390
1820
1500
51-28-5
2,4-Dinitrophenol
ND
3630
3100
85'_;;°-
3630
2850
534-52-1 -
4,6-Dinitro-o-cresol
ND
3630
2480
fi$ a
3630
2450
95-48-7
2-Methylphenol
ND
1820
1170
89
1820
1270
3&4-Methylphenol
ND
3630
2430
3630
2650
88-75-5
2-Nitrophenol
ND
1820
1130
62''' `"
1820
1240
100-02-7
4-Nitrophenol
ND
3630
3310
91d :..a;'
3630
3170
87-86-5
Pentachlorophenol
ND
3630
3240
89' : `
3630
3170
108-95-2
Phenol
ND
1820
1090
.60 °.°;'.
1820
1160
88-06-2
2,4,6-Trichlorophenol
ND
1820
1380
7�6,,
1820
1430
83-32-9
Acenaphthene
ND
1820
1390
77F?w
1820
1450
208-96-8
Acenaphthylene
1310
J
1820
1420
6a* ,...„
1820
1490
120-12-7
Anthracene
1510
J
1820
1580
4."-`''" i
1820
1550
56-55-3
Benzo(a)anthracene
3860
J
1820
1720
„1l8*,e
1820
1660
50-32-8
205-99-2
Benzo(a)pyrene
Benzo(b)fluoranthene
5210
7990
J
1820
1820
1660
1910
-196`4
:,-35*,81
1820
1820
1610
1760
191-24-2
Benzo(g,h,l)perylene
5000
j
1820
1740
-180" a
1820
1750
207-08-9
Benzo(k)fluoranthene
6420
1820'
1690
-26k*,a
1820
1760
101-55-3
4-Bromophenyl phenyl ether
ND
1820
1190
613''
1820
1300
85-68-7
Butyl benzyl phthalate
ND
1820
1620
.89 .:;: ;;
1820
1650
91-58-7
2-Chloronaphthalene
ND
1820
1250
69 `9 i
1820
1300
106-47-8
4-Chloroaniline
ND
1820
1040
57 "
1820
1060
218-01-9
Chrysene
6360
1820
1850
-248*
1820
1840
111-91-1
bis(2-Chloroethoxy)methane
ND
1820
1160
64; .;'
1820
1250
111-44-4
bis (2-Chloroethyl) ether
ND
1820
940
52
1820
1050
108-60-1
bis(2-Chloroisopropyl)ether
ND
1820
970
53_ g'
1820
1090
7005-72-3
4-Chlorophenyl phenyl ether
ND
1820
1290
y,W..
71
1820
-1370
121-14-2
2,4-Dinitrotoluene
ND
1820
1430
29,.�_=.;
1820
1430
606-20-2
2,6-Dinitrotoluene
ND
1820
1370
75
1820
1440
91-94-1
3,3'-Dichlorobenzidine
ND
1820
285
'16*`"",
1820
350
53-70-3
Dibenzo(a,h)anthracene
1060
J
1820
1670
34* .,
1820
1640
132-64-9
Dibenzofuran
ND
1820
1370
75
1820
1420
* = Outside of Control Limits.
36-118/41
48-104/26
52-108/21
51-105/27
43-96/23
40-119/32
64-121/29
46-107/24
44-111/24
49-104/27
56-116/23
61-114/23
45-110/24
56-109/25
56-109/23
56-106/23
61-110/21
66-111/23
59-104/23
67-113/24
67-113/21
67-114/22
62-110/21
65-113/20
53-106/23
30-115/30
65-112/25
48-105/24
46-103/27
40-110/25
58-106/21
59-109/20
61-107/22
36-114/28
68-115/23
57-108/22
0 35 of 44
ACcu-r-EST.
FA1848SR "....-""

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Page 2 of 2 ,... .
'ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
)P53341-MS
L0679687.13
1
10/03/14
FS
10/01/14
OP53341
SL3533
)P53341-MSD
L0679688.13
1
10/03/14
FS
10/01/14
OP53341
SL3533
`A18707-6
L0679764.D
1
10/06/14
FS
10/01/14
OP53341
SL3536
The QC reported here applies to the following samples:
FA18486-1R, FA18486-211
Method: SW846 8270D
FA18707-6
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg
Q
ug/kg
ug/kg
%
ug/kg
ug/kg
% RPD
Red"D
84-74-2
Di-n-butyl phthalate
ND
1820
1510
83t
1820
1504
63-108/19
83"
1 `:fir,,
117-84-0
Di-n-octyl phthalate
ND
1820
1650
' '
1820
1650
91�
011
64-119/21
84-66-2
Dieihyl phthalate
1840
J
1820
1510
t91
-18'
1820
1520
-18*
l.:I i -
61-109120
131-11-3
Dimethyl phthalate
ND
1820
1420
78� ' °
1820
1450
80 ;'`°
2 M
59-108/20
117 81 7
bis(2-Ethylhexyl)phthalate
ND
1820
1670
92
1820
1700
99
2
64-115/23
206-44-0
Fluoranthene
5480
1820
1730
.�
207*a
1820
1560
,
t21t3*
$ 10 '
60 108/25
86-73-7
Fluorene
ND
1820
1440
r79'
1820
1460
80
1
58-109/21
118-74-1
Hexachlorobenzene
ND
1820
1260
�69,��t$�
1820
1260
69 :To °?
0
59 111121
87-68-3
I- lexachiorobutadiene
N❑
1820
1080
59
1820
1210
6T
11
41108/27
77-47-4
Hexachlorocyclopentadiene
ND
1820
784
43*+
1820
887
49`
12°yF,
49-110/31
67-72-1
Hexachloroethane
ND
1820
868
48
1820
975
54
<12..
40-105/32
193-39-5
Indeno(1,2,3-cd)pyrene
5600
1820
1670
-216* a
I820
1610
220*
tl 4��p '
66-116/22
78-59-1
Isophorone
ND
1820
1190
6fi;...:
1820
1290
71 --'
8, '�
42-89/22
91-57-6
2-Methylnaphthalene
719
]
1820
1260
30* ,,
1820
1350
3":
7'
47-106/27
91-20-3
Naphthalene
ND
1820
1160
64
1820
1270
7^0
9
44-104/27
98-95-3
Nitrobenzene
ND
1820
1060
�58ro °
1820
1170
6c�10`aa
43-108/25
621-69 7
N-Nitroso-di n propylamine
ND
1820
1080
59
1820
1200
6B,
11 M;
48-108/27
86-30-6
N-Nitrosodiphenylamine
ND
1820
1530
84�
11'''
1820
1560
86oi
2 i�
62-110/21
85-01-8
Phenanthrene
2330
]
1820
1580
,-91*
1820
1550
43*
2x
63 111/22
129-00-0
Pyrene
7390
1820
1830
-306*
1820
1810
=307�*8 1 ' E'''
65-115/25
CAS No.
Surrogate Recoveries
MS
MSD
FA18707-6
Limits
367-12 4 2-Fluarophenol 55% 61%, 56% 40-102%
4165-62-2 Phenol-d5 65% 70% 58 � ` 41-100%
118-79-6 2,4,6-Tribromophenol $4%84% 77%" 42-108%
4165-60-0 Nitrobenzene-d5 58% "' 64°rii' 70% 40 105%
321-60-8 2-Fluorobiphenyt 699 73 j7J. 43-107%
1718 51 0 Terphenyl d14 H. I 91>m�. 45-119%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
CD
w
10 36 of 44
ACCUT'EST.
PAUMUR ".......-

Section 7
"SoutH'east
� 1 �-t�B�
. ACCU'pi IEE
+'T
GC, -No.�la.:tiles
ugpPPAPOW 41,
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
N
Q0 37 of 44
ACCLJT�ST.
FA1848OR ...... " ••

Method Blank Summary
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GUV3514-MB
UV066149.D
1
10/01/14
AH
n/a
n/a
GUV3514
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
FA18486-1R, FA18486-2R
CAS No. Compound Result RL MDL Units Q
71-43-2 Benzene ND 51 51 ug/kg
100-41-4 Ethylbenzene h1D5H �pF��F°'���� 100 51 ug/kg
1634-04-4 Methyl Ter( Butyl Ether ND' 100 51 ug/kg
91-20-3 Naphthalene ND,260 150 ug/kg
108-88-3 Toluene 100 51 ug/kg
m,p-Xylene ND 200 100 ug/kg
95-47-6 o-Xylene Np 100 51 ug/kg
C5- C8 Aliphatics (Unadj.) Nfl' ";; 5100 1800 ug/kg
C9- C12 Aliphatics (Unadj.) ND 5100 1800 ug/kg
C9. C10 Aromatics (Unadj.) ND ''" 5100 1800 ug/kg
CAS No.
Surrogate Recoveries
Limits
460-00-4
BFB
83%
70-130%
460-00-4
BFS
8$%:. ;£ s "'
70-130%
■® 38 of 44
FAI54UR "'""""""'

Blank Spike/Blank-Spike. Duplicate Summary
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
. ..Pagel. of 1
Sample
File 1D DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GUV3514-BS
UV066146.D 1
10/01/14
AH
n/a
n/a
CUV3514
GUV3514-BSD
UV066147.D 1
10/01/14
AH
n/a
n/a
GUV3514
The QC reported here applies to the following samples: Method; MADEP VPH REV 1.1
FA18486-1R, FA18486-211
Spike
BSP
BSP
BSD
BSD
CAS No.
Compound
ug/kg
ug/kg
%
ug/kg
%
71-43-2
Benzene
4160
3880
4010
96
93 ;;
100-41-4
Ethylbenzene
4160
3920
.94 =F:
4050
97
1634-04-4
Methyl Tert Butyl Ether
4160
3900
94
4130
99
91-20-3
Naphthalene
4160
3780
91 <<°
3890
93
108-88-3
Toluene
4160
3890
93. jj
4020
m,p-Xy1ene
8320
7920
95
8180
98
95-47-6
o-Xylene
4160
3850
93°
3980
96��
C5- C8 Aliphatics (Unadj.)
12500
14700
148
15400
123l".
C9- C12 Aliphatics (Unadj.)
8320
7520
911. .:
7680
92
C9- C10 Aromatics (Unadj.)
4160
3970
95,:x
4030
97_
CAS No.
Surrogate Recoveries
460-00-4
BFB
460-00-4
BFB
* = Outside of Control Limits.
BSP BSD Limits
70-130%
70-130%
Limits
RPD
, RerJRPD
3 ' '
70-130/25
3
70-130/25
.fi ":..
70-130/25
3 a
70-130/25
3..
70-130/25
35' , ;;^
70-130/25
3 kw^;
70-130/25
'5 ;t:
70-130/25
2.
70-130/25
2'1:_
70 130125
N
i�
O® 39 of 44
^CCU7ea7:
FA1W6R `""""'""".

Duplicate Summary
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Page 1 of 1. I _
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA18574-1DUP
UV066151.D
10
10/01/14
AH
n/a
n/a
GUV3514
FA18574-1
UV066150.1)
10
10/01/14
AH
n/a
n/a
GUV3514
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
FA18486-1R, FA18486-2R w
FA18574-1 DUP
CAS No. Compound ug/kg Q ug/kg . Q RPD Limits
71-43-2 Benzene ND ND nc':a>+ 50
100-41-4 Ethylbenzene 34100 35500 9's,;l: 50
1634-04-4 Methyl Teri Butyl Ether ND ND 06;.L 50
91-20 3 Naphthalene 50000 52400 5''E 50
108-88-3 Toluene 12000 12400 `31' 50
m,p-Xylene 203000 2110004 `r 50
95-47-6 o-Xylene 143000 149000 4 50
C5- C8 Aliphatics (Unadj.) ND ND nc 50
C9- C12 Aliphatics (Unadj.) 766000 766000 0 50
C9- C10 Aromatics (Unadj.) 1780000 1860000 4 50
C5- C8 Aliphatics ND ND nc 50
C9- C12 Aliphatics 385000 j 371000 J 9 50
C9- C10 Aromatics 1780000 1860000 4 :..1 50
CAS No. Surrogate Recoveries DUP FA18574-1 Limits
460-00-4 BFB Orb* aF i'4 « 096* a��70-130%
460-00-4 BFB 096* a 70 130%i
(a) Outside control limits due to dilution.
* = Outside of Control Limits.
a® 40 of 44
ACCI -rea-n
FAISUGR "°"""""'

Section 8
GC Semi-volatiles
,.
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
a
I41 of 44
ACCU7EST.
FA18MOR ...........

Method Blank Summary
Job Number: FAI8486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53355-MB
NN010685.1)
1
10/08/14
NAF
10/01/14
OP53355
GNN465
The QC reported here applies to the following samples:
FA18486-1R, FA18486-212
CAS No. Compound
83-32-9
Acenaphthene
208-96-8 •
Acenaphthylene
120-12-7
Anthracene
56-55-3
Benzo(a)anthracene
50-32-8
Benzo(a)pyrene
205-99-2
Benzo(b)fluoranthene
191-24-2
Benzo(g,h,i)perylene
207-08-9
Benzo(k)fluoranthene
218-01-9
Chrysene
53-70-3
Dibenzo(a,h)anthracene
206-44-0
Fluoranthene
86-73-7
Fluorene
193-39-5
Indeno(i,2,3-cd)pyrene
91-57-6
2-Methylnaphthalene
91-20-3
Naphthalene
85-01-8
Phenanthrene
129-00-0
Pyrene
C11-C22 Aromatics (Unadj.)
Cll-C22 Aromatics
C9-C18 Aliphatics
C19-C36 Aliphatics
CAS No. Surrogate Recoveries
3386-33-2
1-Chlorooctadecane
580-13-2
2-Bromonaphthalene
84-15-1
o-Terphenyl
321-60-8
2-Fluorobiphenyl
Result
Method: MADEP EPH REV 1.1
RL MDL Units Q
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg .
200
100
ug/kg
200
100
ug/kg
200
100
ug/kg
10000
7500
ug/kg
10000
7500
ug/kg
10000
5000
ug/kg
10000
5000
ug/kg
Limits
40-140%
40-140%
40-140%
40-140%
a42 of 44
ACGUTEST
FAI"BBR `.....

Blank Spike/Blank Spike Duplicate Summary_
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill: Shannon, NC
Page 1 of I
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53355-BS
NN010683.D
1
10/08/14
, NAF
10/01/14
OP53355
GNN465
OP53355-BSD
NN010684.1)
1
10/08/14
NAF
10/01/14
OP53355
GNN465
The QC reported here applies to the following samples:
FA18486-1R, FA18486-2R
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
83-32-9
Acenaphthene
5000
3660
208-96-8
Acenaphthylene
5000
3800
76.
120-12-7
Anthracene
5000
4160
83 '.
56-55-3
Benzo(a)anthracene
5000
4350
87.?
50-32-8
Benzo(a)pyrene
5000
4750
95;'a
205-99-2
Benzo(b)fluoranthene
5000
-4630
93
191-24-2
Benzo(g h,i)perylene
5000
5050
IN
207-08-9
Benzo(k)fluoranthene
5000
4660
3�
218-01-9
Chrysene
5000
4450
953-70-3
Dibenzo(a,h)anthracene
5000
5060
qF
["8
206-44-0
Fluoranthene
5000
4240
5;"-;
86-73-7
Fluorene
5000
3880
8
193-39-5
Indeno(1,2,3-cd)pyrene
5000
5050
1pl
91-57-6
2-Methylnaphthalene
5000
3480
;70
91-20-3
Naphthalene
5000
3120
$2 `.
85-01-8
Phenanlhrene
5000
4130
83
129-00-0
Pyrene
5000
4290
86.
Cll-C22 Aromatics (Unadj.)
85000
74600
88`
C9-C18 Aliphatics
30000
22800
76
C19-06 Aliphatics
40000
34600
CAS No. Surrogate Recoveries
3386-33-2 1-Chlorooctadecane
580-13-2 2-Bromonaphthalene
84-15-1 o-Terphenyl
321-60-8 2-Fluorobiphenyl
Sample Compound
OP53355-BS 2-Methylnaphthalene
OP53355-BS Naphthalene
OP53355-BSD 2-Methylnaphthalene
OP53355-BSD Naphthalene
* = Outside of Control Limits.
Method: MADEP EPH REV 1.1
BSD BSD
ug/kg %
3330
3520
3940
4180
4550
4470
4880
4440
4280
4830
4060
3610
4810
3230
2920
3910
4180
71100
20000
30800
BSP
BSD
Limits
9%
40-140%
%
k8-4
40-140%
E
90-140%Y
88% 17,9% 40-140%
Limits
RPD Rec/RPD
Col #1 Col #2 Breakthrough Limit
3480
ND
0.0%
5.0
3120
ND
0.0%
5.0
3230
ND
0.0%
5.0
2920
ND
0.0%
5.0
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30 .
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30
40-140/30
10 43 of 44
ACCLJTEST.
FAI"88R

--..Duplicate Summary ......
Job Number: FA18486R
Account: GRINCC GRI (Geological Resources Inc.)
Project: Mountaire Spill; Shannon, NC
.. Page 1 of 1
sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
DP53355-DUP
NN010689.1)
8
10/08/14
NAF
10/01/14
OP53355
GNN465
FA18756-18
NN010707.D
16
10/09/14
NAF
10/01/14
OP53355
GNN466
The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1
FA18486-1R, FA18486-2R
FA18756-1 DUP
CAS No. Compound ug/kg Q ug/kg Q RPD Limits
83-32-9
Acenaphthene
3900 U
ND
nc
30 b
208-9C6
Acenaphthylene
3900 U
ND
nc,,;.;'
30 b
120-12-7
Anthracene
3900 U
ND
nc; '..
30 b
56-55-3
Benzo(a)anthracene
3900 U
ND
iic', _
30 b
50-32-8
Benzo(a)pyrene
3900 U
ND
nc' `
30. b
205-99-2
Benzo(b)fluoranthene
3900 U
ND
nc
30 b
191-24-2
Benzo(g,h,i)perylene
3900 U
ND
nc,
30 b
207-08-9
Benzo(k)fluoranthene
3900 U
ND
nc- .
30 b
218-01-9
Chrysene
3900 U
ND
ncs
30 b
53-70-3
Dibenzo(a,h)anthracene
3900 U
ND
nc. ::`
30 b
206-44-0
Fluoranthene
3900 U
ND
�nc.,:.
30 b
86-73-7
Fluorene
3900 U
ND
30 b
193-39-5
Indeno(1,2,3-cd)pyrene
3900 U
ND
nc��
30 b
91-57-6
2-Methylnaphthalene
3900 U
ND
nc'..
30 b
91-20-3
Naphthalene
3900 U
ND
nc
30 b
85-01-8
' Phenanthrene
3900 U
ND
nc
30 b
129-00-0
Pyrene
3900 U
ND
nc'
30 b
Cll-C22 Aromatics (Unadj.)
409000
494000
19
30 b
CII-C22 Aromatics
409000
494000
30 b
C9-C18 Aliphatics
1030000
1150000
bll
30 b
C19-06 Aliphatics
1490000
1550000
J
30 b
CAS No.
Surrogate Recoveries
DUP
FA18756-1
Limits
3386-33-2
1-Chlorooctadecane
50%
5396 ::::: ;
40-140%
580-13-2
2-Bromonaphthalene
109%
89% . '
40-140%
84-15-1
o-Terphenyl
61%
69% ` ; '::f[.
40-140%
321-60-8
2-Fluorobiphenyl
8296
72°%'
40-140%
(a) Sample received beyond hold time.
(b) Advisory control limits.
* = Outside of Control Limits.
Q® 44 of 44
ACCU_rEST.
FA18488R `"'."'°""

January 27, 2014
Mr. Bradley Bennett
Supervisor, Stormwater Permitting Unit
North Carolina Dept. of Environment & Natural Resources
1617 Mail Service Center
Raleigh NC 27699-1617
RE: Permit No. NCG060295
Dear Mr. Bennett:
Please be advised that since the issuance of our Stormwater General Permit on 121112012,
Mountaire Farms Inc. — Lumber Bridge Processing Plant has exceeded the benchmark
value on four occasions. The parameters exceeded were; COD, with a benchmark of 120
mgll, (results ranging from 139 — 262 mgll) and TSS, with a benchmark of 100 mg/l,
(results ranging from 124 — 215 mg/l).
Because of these exceedances, the facility now falls into the Tier Three category as
described in the Stormwater General Permit.
Should you have any questions, please contact me at 302-934-3094.
Sincerely,
Beth B. Sise
Environmental Manager
Cc: John Wren, Mountaire Farms
David Kirby Mountaire Farms
f
yr•r ���
Robert Jackson, Mountaire Farms
.�
. r`
Mountaire Farms of Delaware, Inc.
p0. Box 1320, Millsboro, Delaware 19966
[phone] Toll Free [phone]
"We measure quality by how well we service our internal and external customers"

NCDEE R
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Charles Wakild, P. E.
Governor
Robert Jackson
Mountaire Farms Inc
17269 NC Hwy 71N
Lumber Bridge, NC 28357
Dear Permittee:
Director
December 4, 2012
Dee Freeman
Secretary
Subject: NPDES Stormwater Permit Coverage Renewal
Mountaire Farms Inc
CDC Number NCG060295
Robeson County
In response to your renewal application for continued coverage under stormwater General Permit NCGO60000
the Division of Water Quality (DWQ) is forwarding herewith the reissued General Permit. This permit is
reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of
Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated October
15, 2007 (or as subsequently amended).
The following information is included with your permit package:
• A new Certificate of Coverage (CDC)
• A copy of General Permit NCG060000
• A copy of the Technical Bulletin for the General Permit
• Two copies of the Discharge Monitoring Report (DMR) Form
• Two copies of the Qualitative Monitoring Report Form
The General Permit authorizes discharges of stormwater, and it specifies your obligations for discharge
controls, management, monitoring, and record keeping. Please review the new permit to familiarize yourself
with all the changes in the reissued permit. Your facility has six (6) months from the time of receipt of the
permit to update your current SPPP to reflect all new permit requirements.
The first sample period of your permit begins January 1, 2013. Your facility must sample a "measureable
storm event" beginning during the periods beginning January 1 and July 1 of every year (or, if applicable,
report "No Flow," as outlined In Part III, Section E). Also, please note that Tier 3 Actions in Part II of your
permit are triggered by benchmark exceedances on four occasions beginning on the effective date of this
permit and do not count prior exceedances.
The more significant changes in the General Permit since your last CDC was issued are noted either in the
Draft Permit Fact Sheet that accompanied the public notice (http://portal.ncdenr.orglwebZwq/ws/su/current-
notices), or in the Response to Comments / Summary of Changes and Technical Bulletin documents that are
posted on the Stormwater Permitting Unit's website with the new General Permit. Please visit
http://Portal.ncdenr.org/web/wq/ws/su/npdessw (click on `General Permits' tab) to review that information
for your specific General Permit carefully.
1617 Mail Service Center, Raleigh, North Carolina 27699.1617
Location: 512 N. Salisl.�usy St. Raleigh, North Carolina 27604
Phone:91H07-630f, FAX:[phone]
Internet:www.ncwate;,uali .o
An Ly;al Opportunity l A!, n,!;ve A tion Employer
One
No>I-hCarolina
�r turally.

Robert Jackson
December 4, 2012
Page 2 of 2
Some of the changes include:
Part ll:
• Section A: The Stormwater Pollution Prevention Plan (SPPP) section, if applicable, has been updated
to the most current language of our permits. Additional conditions for specific industry sectors have
been added to the SPPP requirements in some cases.
• Sections B, C: Failure to perform analytical stormwater monitoring may result in the Division requiring
that the permittee begin a monthly sampling scheme.
• Sections B, C. A lower TSS benchmark of 50 mg/I for HQW, ORW, PNA and Tr Waters applies to these
more sensitive waters.
• Sections B, C. The monitoring parameter Oil & Grease (O&G) has been replaced by the parameter
Total Petroleum Hydrocarbons (TPH) for vehicle maintenance areas, and in some cases, other
analytical monitoring requirements.
• Sections B, C, D: Inability to sample due to adverse weather must be recorded in the SPPP, or in
separate on -site records if your General Permit does not require an SPPP. Adverse weather is defined
in the "Definitions" section of the permit.
• Sections B, C: The term "Representative Storm Event" has been replaced by "Measurable Storm
Event." A measurable storm event is defined in the permit.
• Section D: If the permittee fails to respond effectively to problems identified by qualitative
monitoring, DWQ may require the permittee to perform corrective action.
Please review Parts III and IV to understand the Standard Conditions of your new NPDES General Permit,
including Compliance and Liability, Reporting, Monitoring and Records requirements; Operation and
Maintenance obligations; and Definitions. Please note that all samples analyzed in accordance with the terms
of this permit must be submitted to the Division on Discharge Monitoring Report (DMR) forms available on
the Stormwater Permitting Unit's website above. DMR forms must be delivered to the Division no later than
30 days from the date the facility receives the sampling results from the laboratory. Also note that existing
permittees do not need to submit a renewal request prior to expiration unless directed by the Division.
Your coverage under the General Permit is transferable only through the specific action of DWQ. This permit
does not affect the legal requirements to obtain other permits which may be required by DENR, nor does it
relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law,
rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit
package, please contact the Division's Stormwater Permitting Unit at [phone].
Sincerely,
for Charles Wakild, P.E.
cc: DWQ Central Files
Stormwater Permitting Unit Files
Fayetteville Regional Office

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG060000
CERTIFICATE OF COVERAGE No. NCG060295
STORMWATER
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Mountaire Farms Inc
is hereby authorized to discharge stormwater from a facility located at:
Mountaire Farms Inc
17269 NC Hwy 71 N
Lumber Bridge
Robeson County
to receiving waters designated as Big Marsh Swamp (Marsh Swamp) (Lake McNeill, Odom
Pond), a class C;Sw waterbody in the Lumber River Basin in accordance with the effluent
limitations, monitoring requirements, and other conditions set forth in Parts I, I1, III, and IV of
General Permit No. NCG060000 as attached.
This certificate of coverage shall become effective December 4, 2012.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this 41h day of December, 2012.
for Charles Wakild, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

- A - NA
NCDENR
North Carolina Department of Environment and Natural Resources
Beverly Eaves Perdue
Governor
Scott Varner
Mountaire Farms of North Carolina
PO Box 339
Lumber Bridge, NC 28357-0339
Dear Permittee:
Division of Water Quality
Charles Wakild, P.E.
Director
March 5, 2012
Subject: NPDES Stormwater Permit Coverage Renewal
Mountaire Farms of North Carolina
COC Number NCG060295
Robeson County
Dee Freeman
Secretary
Your facility is currently covered for stormwater discharge under General Permit NCG060000. This permit expires on
10/31/2012. The Division staff is currently in the process of renewing this permit. When a draft is available for
notice and public comment, it will be posted on our website at http://Oortal.ncdenr.org/web/wcl/ws/su/public-notices.
Please continue to check this website to review and comment on proposed changes to the permit. Once the permit
is reissued, your facility would be eligible for continued coverage under the reissued permit.
To assure consideration for continued coverage under the general permit, you must apply to the Division of Water
Quality (DWQ) for renewal of your permit, Enclosed you will find a Permit Coverage Renewal Application Form. The
application must be completed and returned by May 4, 2012. Letters confirming our receipt of the completed
application will not be sent,
Failure to request renewal within the time period specified may result in a civil assessment of at least $250.00.
Larger penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your
facility without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and
could result in assessments of civil penalties of up to $25,000 per day.
"No exposure exclusion" is now available to industrial facilities in any of the categories of "storm water discharges
associated with industrial activity," (except construction activities). If you feel your facility can certify a condition of
.,no exposure", i.e. the facility' industrial materials and operations are not exposed to stormwater, you can apply for
the no exposure exclusion. For additional information contact the Central Office Stormwater Staff member listed
below or check the Stormwater Permitting Unit Web Site at http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-5.
If the subject stormwater discharge to waters of the state has been terminated, please complete the enclosed
Rescission Request Form. Mailing instructions can be found on the bottom of the form. You will be notified when
the rescission process has been completed.
If you have any questions regarding the permit renewal procedures please contact Bradley Bennett of the Central
Office Stormwater Permitting Unit at [phone].
Sincerely,
Bradley Bennett
Supervisor, Stormwater Permitting Unit
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Raleigh, North Carolina 27604
Phone: [phone] FAX: [phone] l Customer Sarvice: 1-877-623-6748
In ternet.' www.ncwaterqua5ty.org
An Equal opportunity 1 Affirmative Adon Employer
NorthCarolina
Natura!!if

af""rfa Permit Coverage
pRenewal Application Form
National Pollutant Discharge Elimination System Certificate of Coverage Number
��`�
Stormwater General Permit NCG060000 - NCGO60295
The following is the information currently in our database for your facility. Please review this information carefully and make all
corrections/ additions as necessary in the space provided to the right of the current information.
Owner Affiliation Information
Owner / Organization Name:
Owner Contact:
Mailing Address:
Phone Number:
Fax Number:
E-mail address:
* Reissued Permit will be mailed to the owner address
Mountaire Farms Of North Carolina _
Scott Varner
PO Box 339
Lumber Bridge, NC 283570339
800-862-0720 Ext.
910-843-4256
Facility/Permit ContacUnformation
Facility Name: Mountaire Farms of North Carolina
Facility Physical Address: 17269 NC Hwy 71 N
Facility Contact:
Mailing Address:
Phone Number:
Fax Number:
E-mail address:
Discharge -Information
Receiving Stream:
Stream Class:
Basin:
Sub -Basin:
Number of Outfalls:
Lumber Bridge, NC 28357
Robert Jackson
17269 NC Hwy 71 N
Lumber Bridge,NC 28357
800-962-0720 Ext.
910-843-4256
Big Marsh Swamp (Marsh Swamp) (Lake McNeill,
C;Sw
Lumber River Basin
03-07-53
Impaired Waiers/TMOL
Does this facility discharge to waters listed as impaired or waters with a finalized TMDL? ❑ Yes 0 No ❑ Don't Know
for information on these waters refer to http://h2o. enrstate.nc.us/su/Impaired Waters 7MDL /
CERTIFICATION
I certify that I am familiar with the information contained in the application and that to the best of my knowledge and
belief such information is true, complete and accurate.
Signature
Print or type name of person signing above
Date
Title
SW General Permit Coverage Renewal
Please return this completed renewal application form to: Stormwater Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

MrvM
Mliu-"n'taim
rE e,lr Yrxrn�� Cltict en
December 14, 2009
Mr. Mike Lawyer
Environmental Specialist
North Carolina Dept. of Environment & Natural Resources
225 Green Street
Suite 714
Fayetteville NC 28301
RE: Permit No. NCG060295
Dear Mr. Lawyer:
DEC 2 8 2009
DWQ
Mountaire Farms of NC — Lumber Bridge Processing Plant is currently constructing a
concrete containment area with shelter for the storage of drums and totes as was our
commitment. In a previous correspondence to you, dated April 6, 2009, the plan was to
have this project completed by December 1, 2009.
Please be advised that this capital project is underway, however the completion date is
estimated to be February 22, 2010. This project, once completed will satisfy the
secondary containment requirement for multiple containers with a capacity of more than
1320 gallons stored outside.
Should you have any questions, please contact me at 302-934-3094.
Sincerely,
Beth B. Sise
Environmental Manager
Cc: John Wren, Mountaire Farms r �Iv—,—, , —,.
Robert Jackson, Mountaire Farms
Halley Ondona, Mountaire Farms V11%
Scott Varner, Mountaire Farms
Mountaire Farms of Delaware, Inc.
PO. Box 1320, Millshoro, Delaware 19966
(302) 934-1 100 Toll Pree [phone]
"We measure quality by how well we service our internal and external customers "

Lawyer, Mike
From:
Lawyer, Mike
Sent:
Wednesday, April 15, 2009 10:21 AM
To:
'[e-mail]'
cc:
'[e-mail]'
Subject:
outfall monitoring
Beth and Robert,
As I discussed with Beth several days ago, monitoring at the outfall adjacent to the entrance road should continue. I
recognize that this goes against what I wrote in my recent inspection report, but it was recently brought to my attention
that entrance/haul roads where materials and/or products are transported in and out of a facility is considered as part
of that facility's industrial activity. There is the potential for spills, leaks, etc. to occur along this road and therefore
monitoring should occur per the conditions of the general permit. A printed copy of this e-mail will be placed in our files
for the facility and I recommend that you do the same. If you have any questions or concerns pertaining to this or any
other issues in regards to the general permit, please contact me.
Thanks,
Mike
Michael Lawyer
Environmental Specialist
NCDENR-Division of Water Quality
Surface Water Protection Section
Fayetteville Regional Office
Direct: [phone]
Main: [phone]
Fax: [phone]
mike,lawV_ rr,@ncdenr.gov
*E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be
disclosed to third parties.

N. C hi I Ll P!
s
f•i•r��•It l�tur,�� (7rir�urtr
April 6, 2009
Mr. Mike Lawyer
Environmental Specialist
North Carolina Dept. of Environment & Natural Resources
225 Green Street
Suite 714
Fayetteville NC 28301
RE: Permit No, NCG060295
Dear Mr. Lawyer:
� 4R_�Ro
D
Iva0610
DWQ
This letter is in response to your correspondence regarding the Stormwatcr Compliance
Evaluation Inspection which took place at our Lumber Bridge Processing Plant on February 25,
2009. Thank you for your input during the stormwater inspection.
You requested a written response for the following items: 1) revise the SPPP site map to include
the additional employee parking, 2) include an evaluation of feasible alternatives to current
practices in the SPPP, and 3) secondary containment is required for multiple containers with a
capacity of more than 1320 gallons stored outside.
As of this date, the revisions to the SPPP have been completed. Also, an assessment has been
performed on the totes and drums stored outside to determine if it would be possible to relocate
these items indoors. While we are doing our best to keep as many totes and drums inside, we
have determined that outdoor containment will be needed. This will be a capital project to
construct a concrete containment with shelter. Mountaire plans to have this project completed by
December 1, 2009.
Should you have any questions, please contact our Environmental Manager, Beth Sise at 302-
934-3094.
Sincerely,
�,o�v ?
Scott Varner
Director of Processing Operations
Cc: John Wren, Mountaire Farms
Robert Jackson, Mountaire Farms
Beth Sise, Mountaire Farms
Mountaire Farms of Delaware, Inc.
P.O. Box 1320, Millsboro, Delaware 19966
(-302) 934-1100 Toll Free [phone]
"We measure quality by how well we service our internal and external customers"

A IT
C1::J ER
North Carolina Department of Environment and Natural Resources
Division of VVater Quality
Be'veriv Eaves Perdue C been K SLliiinS
Giverncr Director
March 3, 2009
Mountaire Farms of North Carolina
Attn: Scott Vanier, Director of Processing Operations
PO Box 339
Lumber Bridge, NC 28357-0339
Subject: COMPLIANCE EVALUATION INSPECTION
Mountaire Farms of North Carolina
NPDES Stormwater General Permit-NCG060295
Robeson Counter
Dear Mr. Varner:
Dee Freerian
Secr�tury
On February 25, 2009, I, Michael Lawyer from the Fayetteville Regional Office of the Division of
Water Quality, conducted a site inspection at the Mountaire Farms of North Carolina facility located at
17269 NC Hwy 71N in Lumber Bridge, Robeson County, North Carolina. A copy of the Compliance Inspection
Report is enclosed for your review. Mr. Robert Jackson, Waste Water Treatment Manager, Ms. Beth Sise,
Environmental Manager, and Mr. John Wren, Director of Engineering & Environmental Services, were also
present during the inspection and their time and assistance is greatly appreciated. Stormwater from this facility
drains to Big Marsh Swamp, a Class C,Sw stream located in the Lumber River Basin. The site visit and file
review revealed that the subject facility is covered by NPDES Stormwater General Permit-NCG060295.
Accordingly, the following observations were noted during the Division of Water Quality inspection:
1) Stormwater Pollution Prevention Plan (SPPP)
A Stormwater Pollution Prevention Plan (SPPP) has been developed, recorded, and properly implemented.
1'es ® No ❑
2) Qualitative Monitoring
Qualitative monitoring has been conducted and recorded in accordance with permit requirements.
es■ No
3) Analytical Monitoring
Analytical monitoring has been conducted and recorded in accordance with permit requirements.
es ■ No ❑
Lo.-71bi: - 5 (3mnn Sueca, ,Salle 71it, Fayettevllle, North Carolina 28301
Phone: a 10-133-330C. � FAY,; 910-486.07071 C.islomoi Service: 1.877.023.674E
In1eY11P,i; �`IN1l4.nCll4+IL'fr r;alir,l.gf{�
Onc
NcwtiC 1ai-O;1JI
A,' E'!Ij, : Cl:pc,t:I 1:lv 1 „f5rm;r1J(? r+c,ticir Einiilrr.r

Other Observations:
Please refer to the enclosed Compliance Inspection Report For additional comments and observations made
during the inspection.
Requested Response:
You are asked to respond to this office, in writing, by April 6, 2009, Your response should include a
plan of action pertaining to the secondary containment requirements for all storage areas of liquid materials as
well as revisions to the S PP as detailed in the inspection report.
Please be advised that violations of the NPD1ErJS General Permit are subject to a civil penalty -
assessment of up to $25,000 per day for each violation. If you of your staff has any questions, continents, or
needs assistance with understanding any aspect of your permit, please do not hesitate to contact me at (910)
433-3329.
Sincerely,
Michael Lawyer
Environmental Specialist
Enclosure
cc: Robert Jackson, Waste Water Treatment Manager (same address)
Beth B. Sise, Environmental Manager-Mountaire Farms of Delaware
PO Box 1320
Millsboro, DE 19966-1320
FRO -Surface Water Protection
NPS-Assistance & Compliance Oversight Unit
DWQ Central Files
" 5 Gru�;n Sheri. S6te ?14, Fa f-;ItrVWr. r4orih 2a301
?h,�n �0-•:� 3-, t`'; �A.?C 910-48ri-[)707 Lislomer Sei A; 1-877-623-674
m;9raCI: wvra.n.;w:a�eru:�aliiy.arg
:r,a,, ^.,r., r;iv .liir rw• e ;,rn 1:nV0ver

I
Permit: NCG060295
SOC:
County: Robeson
Region: Fayetteville
Compliance Inspection Report
Effective: 11/01/07 Expiration: 10/31/12 Owner: Mountaire Farms Of North Carolina
Effective: Expiration: Facility: Mountaire Farms of North Carolina
17269 NC Hwy 71 N
Contact Person: Robert Jackson
Directions to Facility:
1.95 South to NC Highway 20. Left on NC Highway 71
System Classifications:
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
On -site representative John Wren
On -site representative Beth B Sise
On -site representative Robert Jackson
Related Permits:
Title: Waste Water Treatment M
Certification:
Lumber Bridge NC 28357
Phone: [phone]
Phone:
Phone: [phone]
Phone: [phone]
Phone: [phone]
Inspection Date: 02/25/2009 Entry Time: 09:10 M Exit Time: 11:30 AM
Primary Inspector: Mike Lawyer Phone: [phone]
33Z9
Belinda S Henson Phone: [phone] E>;.72$'
33zG
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Food/Tobacco/SoapstCosmetics/Public Warehousing
Stormwater Discharge COC
Facility Status: ■ Compliant ❑ Not Compliant
Question Areas:
E Storm Water
(See attachment summary)
Page: 1

•y.
Permit: NCG060295 Owner - Facility: Mountaire Farms Of North Carolina
Inspection Date: M25I2009 Inspection Type: Compliance Evaivalion Reason for Visit: Routine
Inspection Summary:
Met with Mr. Robert Jackson, Waste Water Treatment Manager, Ms. Beth Sise, Environmental Manager, and Mr. John
Wren, Director of Engineering & Environmental Services. Conducted review of the facility's Stormwater Pollution
Prevention Plan (SWPPP), which contains all required components with the exception of an evaluation of feasible
alernatives to current practices. The SWPPP also needs some minor revisions to the site map concerning expansion of
the employee parking area. Facility has identified two outfalls, 001 near the entrance to the plant at the employee parking
area and 002 at the retention pond located at the rear of the facility. Qualitative Monitoring records were available for
review for both outfalls, however Analytical Monitoring at outfall 001 was missed previously and sampled just prior to the
inspection so results had not been received. Due to the nature of runoff received and discharged at outfall 001 coming
from the employee parking area, which is not considered as an industrial activity, personnel were advised that monitoring
at this location could cease, According to facility personnel, the retention pond with outfall 002 rarely.discharges and
records have been submitted indicating 'No Flow', which were also available for review. During the site evaluation, a
couple of areas were observed where numerous totes and barrels are stored without secondary containment. Personne!
were advised of the secondary containment requirements in the general permit for storage areas with multiple containers
with a capacity of more than 1,320 gallons, A written response should be submitted to the regional office concerning the
aforementioned revisions to the SWPPP and plan of action regarding the provision of secondary containment around all
outside storage areas of liquid materials.
Page: 2

u
N
Permit: NCG060295 Owner • Facility: Mountaire Farms Of North Carolina
Inspection Date: 02/25/2009 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Stormwater Pollution Prevention Plan
Yes
No
NA
NE
Does the site have a Stormwater Pollution Prevention Plan?
■
❑
# Does the Plan include a General Location (USGS) map?
■
0
n
0
# Does the Plan include a "Narrative Description of Practices"?
■
n
n
n
# Does the Plan include a detailed site map including outfall locations and drainage areas?
■
0
0
0
# Does the Plan include a list of significant spills occurring during the past 3 years?
■
M
M
n
# Has the facility evaluated feasible alternatives to current practices?
n
■
n
n
# Does the facility provide all necessary secondary containment?
Cl
■
0
0
# Does the Plan include a BMP summary?
O
n
n
Cl
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
0
n
0
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
■
n
n
n
# Does the facility provide and document Employee Training?
■
0
n
n
# Does the Plan include a list of Responsible Party(s)?
■
0
0
0
# Is the Plan reviewed and updated annually?
■
o
n
n
# Does the Plan include a Stormwater Facility Inspection Program?
■
❑
❑
n
Has the Stormwater Pollution Prevention Plan been implemented?
■
n
n
n
Comment: SWPPP needs revisions regarding documentation of an evaluation of
feasible alternatives to current practices and the recent expansion of employee parking
area. Secondary containment is needed around storage areas of totes and barrels.
Qualitative Monitorin
Yes
No
NA
NE
Has the facility conducted its Qualitative Monitoring semi-annually?
■
n
❑
n
Comment:
Analytical Monitoring
Yes
No
NA
NE
Has the facility conducted its Analytical monitoring?
■
n
n
n
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? ■ n n n
Comment: Facility has identified two outfalls, one at the employee parking area (001)
and another at the stormwater retention pond (002). Outfall 002 at the pond rarely has
a discharge due to the size of the pond and personnel have submitted records
indicating No Flow. Monitoring at outfall 001 has been missed previously, which was
documented with submittal of records, but has been recently sampled. Since this outfall
only receives runoff from employee parking areas, which is not -considered an industrial
activity, monitoring at outfall 001 may be discontinued.
Permit and Outfalls Te5 NU NA N
# Is a copy of the Permit and the Certificate of Coverage available at the site? 0 n rl n
Page: 3

a
Permit: NCGO60295 Owner - Facility: Mountaire Farms Of North Carolina
inspection Date: 02/25/2009 Inspection Type: Compliance Evaluation Reason for Visit: Routine
# Were all outfalls observed during the inspection? ■ ❑ ❑ [1
# If the facility has representative outfall status, is it properly documented by the Division? ❑ 1=l p n
# Has the facility evaluated all illicit (non stormwater) discharges? ■ n in n
Comment:
Page: 4

' of WArF9
r
0 �
November 1, 2007
Tom Lee
Mountaire Farms Of North Carolina
PO Box 339
Lumber Bridge, NC 28357
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Culeen H. Sullins, Director
Division of Waler Quality
Subject: NPDES Stormwater Permit Coverage Renewal
Mountaire Farms of North Carolina
COC Number NCG060295
Robeson County
Dear Permittee:
In response to your renewal application for continued coverage under stormwater General Permit NCG060000 the Division of
Water Quality (DWO) is forwarding herewith the reissued stormwater General Permit. This permit is reissued pursuant to the
requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between the state of North
Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983.
The following information is included with your permit package:
• A new Certificate of Coverage
• A copy of stormwater General Permit NCG060000
• A copy of a Technical Bulletin for the General Permit
• Five copies of the Discharge Monitoring Report (DMR) Form
• Five copies of the Qualitative Monitoring Report Form
The General Permit authorizes discharges of stormwater only, and it specifies your obligations with respect to stormwater
discharge controls, management, monitoring, and record keeping. Please review the new permit to familiarize yourself with all
the changes in the reissued permit.
The more significant changes iri the General Permit since your last Certificate of Coverage include the following:
• Part I Section A — A new notation that the No Exposure Exclusion from permitting option may be available to the
permittee.
• Part I Section A — A new provision that facilities draining to 303(d) listed waters, or in watersheds with an approved TMDL,
may not be eligible for renewed coverage under the General Permit.
• Part II Section B Table 1 — An increased sampling frequency from once per year to twice per year.
• Part II Section B Table 3 — Benchmark concentrations now replace cutoff concentrations; the elimination of the option to
avoid sampling based on cutoff concentrations.
• Part II Section B — New provisions requiring the permittee to execute Tier One and Tier Two response actions, based on
the first benchmark exceedence (Tier One) and the second consecutive benchmark exceedence (Tier Two). Tier Two
requires that the permittee institute monthly monitoring instead of twice -per -year monitoring, until three consecutive
monitoring events show no benchmark exceedences.
• Part II Section B — A new provision that four exceedences of any particular benchmark will trigger increased DWQ
involvement in the permittee's stormwater management and control actions. DWQ may direct the permittee to apply for
an individual permit, or may direct the implementation or installation of specific stormwater control measures.
DWO received a number of comments on a series of general permits similar to this one. A full response to comments can be
found at http://ncwaterquality.org/su/industriaigpinfo.htm. Some comments resulted iri permit modifications, others are
addressed in the response document or Fact Sheet. A few specific requests for clarification are addressed below.
1. What is the deadline for having a revised SPPP that reflects the provisions of the new General Permit? DWQ will require
that the permittee have a revised, complete SPPP no later than six months after the date of issue of that permittee's new
Certificate of Coverage.
2. Must analytical results be by a certified tab? What about pH measurements? All analytical results obtained to satisfy
NPDES permit requirements must be certified, as directed in North Carolina regulations at 15A NCAC 2H .0800, and as
administered by DWQ's Laboratory Section Certification Branch. This includes field pH measurements.
. o'r1� gnu
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone [phone] Customer Service !l/
Intemet: h2o.enr.state.nc.us/sulstormwater.html 512 N. Salisbury St. Raleigh, NC 27604 FAX [phone]
An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Post Consumer Paper

Permit Reissuance Letter — Permit NCG060295
Page 2
Your coverage under the General Permit is transferable gly through the specific action of DWO. The Division may require
modification and reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by DENR, nor does it relieve the
permittee from responsibility for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order,
judgment, or decree.
If you have any questions regarding this permit package please contact Kelly Johnson of the Central Office Stormwater Permitting
Unit at [phone], ext. 376.
Sincerely,
for Coleen H. Sullins
cc: DWO Central Files
Stormwater Permitting Unit Files
Fayetteville Regional Office

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG060000
CERTIFICATE OF COVERAGE No. NCG060295
STORMWATER DISCHARGES
NATIONAL POLLUTANT. DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and
the Federal Water Pollution Control Act, as amended,
Mountaire Farms Of North Carolina
is hereby authorized to discharge stormwater from a facility located at
Mountaire Farms of North Carolina
17269 NC Hwy 71 N
Lumber Bridge
Robeson County
to receiving waters designated as Big Marsh Swamp (Marsh Swamp) (Lake McNeill, Odom Pond), a Class
C;Sw water in the Lumber River Basin in accordance with the effluent limitations, monitoring requirements,
and other conditions set forth in Parts I, Il, 111, IV, V, and VI of General Permit No. NCG060000 as attached.
This certificate of coverage shall become effective November 1, 2007.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day November 1, 2007.
for Coleen H. Sullins, Director
Division of Water Quality
By Authority of the Environmental Management Commission

September 28, 2007
Ms. Colleen Sullins, Director
North Carolina Department of Environmental & Natural Resources
Division of Water Quality
Aquifer Protection Section
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
Re: Mountaire Farms of North Carolina- Lumber Bridge Processing Plant
Permit Number WQ0000484
Dear Ms. Sullins:
Due to personnel changes at the above -referenced facility, please be advised that Scott
Varner is now the Director of Processing Operations. Therefore, please direct all future
correspondence to Mr. Varner's attention at:
Mountaire Farms of North Carolina
P.O. Box 339
Lumber Bridge, North Carolina 28357
Additionally, Mr. Varner will be the responsible official for signing ,all documents and
reports.
Mountaire Farms of Delaware, Inc.
P.O. Box 1320, Millsboro, Delaware 19966
(302) 934-i 100 Tall Free [phone]
"We measure quality by how well we service our internal and external customers "

If you have any questions or need additional information, please do not hesitate to contact
me at [phone].
Sincerely,
Jeffrey Smith
Environmental Manager
Mountaire Farms Inc.
Cc: Scott Varner (Mountaire)
John Wren (Mountaire)
Halley Ondona (Mountaire)
Robert Jackson (Mountaire)

0� W A rFi9Q� Michael F. Easley, Governor
` William G. Ross Jr., Secretary
North Carolina Department or Environment and Natural Resources
� y
p Alan W. Klimek, P.E. Director
Division of Water Quality
September 8, 2006
Mr. Tom Lee
D�—i
Mountaire Farms of North Carolina SEP 12 2006
P.O. Box 339
Lumber Bridge, NC 28357 CG�
Subject: General Permit No. N060A0
Mountaire Farms of North Carolina
COC No. NCG060295
Robeson County
Dear Mr. Lee:
In accordance with your application for a discharge permit received on July 21, 2006 we
are forwarding herewith the subject certificate of coverage (COC) to discharge under the subject
state — NPDES general permit. This permit is issued pursuant to the requirements of North
Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina
and the US Environmental Protection Agency dated May 9, 1994 (or as subsequently amended).
If any parts, measurement frequencies, or sampling requirements contained in this permit
are unacceptable to you, you have the right to request an individual permit by submitting an
individual permit application. Unless such demand is made, this certificate of coverage shall be
final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to
the Division of Water Quality. The Division of Water Quality may require modification or
revocation and reissuance of the certificate of coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by the Division of Water Quality or
permits required by the Division of Land Resources, Coastal Area Management Act or any other
federal or local governmental permit that may be required.
If you have any questions concerning this permit please contact Aisha Lau at telephone
number [phone] ext. 578.
SincerdWINAL SIGNED BY
KEN PICKLE
Alan W. Klimek, P.E.
cc: Fayetteville Regional Office
Central Files
Stormwater Permitting Unit Files
Attachments
Na Carolina
Vhrrn!!Y
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone [phone] Customer Service
Internet: h2o.enr.state.nc.us 512 N. Salisbury St. Raleigh, NC 27604 FAX [phone]
An Equal Opportunity/Affirmative Action Employer— 50% Recycled110% Post Consumer Paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG060000
CERTIFICATE OF COVERAGE No. NCG060295
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
Mountaire Farms of North Carolina
Is hereby authorized to discharge stormwater from a facility located at
Mountaire Farms of North Carolina
17269 NC Highway 71 N
Lumber Bridge
Robeson County
to receiving waters designated as Big Marsh Swamp, Class C, Sw waters in the Lumber River Basin in accordance
with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, 11, I1I, IV, V, and VI
of General Permit No. NCG060000 as attached.
This certificate of coverage shall become effective September 8, 2006.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day September 8, 2006.
ORIGINAL SIGNED BY
KEN PICKLE
Alan W. Klimek, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

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Copyright (C)•1998, Maptech, Inc,

J :4
A74
NCDENR
r_,J .WT —C lllvllRlLL Rlbp Ef
Division of Water Quality / Water Quality Section
National Pollutant Discharge Elimination System
NCG060000
FOR AGENCY USE ONLY
Date Received
Year Munch
Da
120
Certificates orC 'era e
nt
Clie cunt
Permit Assl ned to
a�
NOTICE OF INTENT
National Pollutant Discharge Elimination System application for coverage under General Permit
NCG060000:
STORMWATER DISCHARGES associated with activities classified as:
SIG' 20
SIC' 21
Food and Kindred Products
Tobacco Products
A
t
SIC' 283
Drugs Public
,.4
`
SIC' 284
Soaps, Detergents, & Cleaning Preparations; Perfumes, Cosmetics, & Other Toilet Pr
Lions,,
t
SIC' 422
Warehousing and Storage (except 4226)
' Standard Industrial Classification Cade
g ''
(Please print or type)
1) Mailing address' of owner/operator:
Name
Street Address
City
Telephone No,
2) Location of facility producing discharge:
Facility Name
Facility Contact
Street Address
City
County
Telephone No.
910 611-A3 • -i',L%
Address to which all permit correspondence will be mailed
�)OO !a(a"1. °_a711rd Fax
3) Physical location Information:
Please provide a narrative description of how to get to the facility (use street names, state road numbers, and
distance and direction from a roadway intersection). 1-f�1l] S{�;►t1� �o i�L 4 ► h.„may ti�� Z+�
I i
(A copy of a county map or USG quad Sheol with facility cieady located on the map is required to be submitted with this application}
4) This NPDES Permit Application applies to which of the following:
❑ New or Proposed Facility Date operation is to begin
I1YIExisting
S) Standard Industrial Classification:
Provide the 4 digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial
activity at this facility
SIC Code: 1 U l 60
Page 1 of 3
SWU-221-101701

NCG060000 N.O.I.
6) Provide a brief parrative description of the types of industrial activities and products manufactured at
this facility: rrJ 0r• 't " k
7) Discharge points ! Receiving waters:
How many discharge points (ditches, pipes, channels, etc.) convey stormwater from the property? 2
What is the name of the body or bodies of water (creek, stream, river, lake, etc.) that the facility stormwater
discharges end up in? Pyj c M a//-'j ' ."'2rt."'e _
If the site stormwater discharg to a separate storm se+n er system, name the operator of the separate storm
sewer system (e.g. City of Raleigh municipal storm sewer).
8) Does this facility have any other NPDES permits?
12'No
❑ Yes
If yes, list the permit numbers for all current NPDES permits for this facility:
9) Does this facility have any Non -Discharge permits (ex: recycle permits)?
Cl No
2'Yes
If yes, list the permit numbers far all current Non -Discharge permits for this facility: OUQ U' 9)4
10) Does this facility employ any best management practices for stormwater control?
❑ No
des !! t
If yes, please briefly describe: _ ��+� �. k,2o t,,t, ti4.vti �- '7�n .. rs.t.t.n� ►��;t Tt _
nr _ - --
11) Does this facility have a stormwater Pollution Prevention Plan?
l2'No
❑ Yes
If yes, when was it implemented?
12) Are vehicle maintenance activities occurring at this facility?
❑ No Yes
13) Hazardous Waste:
a) Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility?
G2''No Cl Yes
b) Is this facility a Small Quantity Generator (less than 1000 kg, of hazardous waste generated per month) of
hazardous waste?
{3'No ❑ Yes
c) Is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste generated per month) of
hazardous waste?
O'No ❑ Yes
d) If you answered yes to questions b. or c., please provide the following information:
Type(s) of waste:
Page 2 of 3
SWU-221-101701

NCG060000 N.O.I.
How is material stored:
Where is material stored:
How many disposal shipments per year:
Name of transport / disposal vendor:_
Vendor address:
14) Certification:
North Carolina General Statute 143.215.6 b (i) provides that:
Any person who knowingly makes any false statement, representation, or certification in any application, record, report,
plan or other document filed or required to be maintained under Article 21 or regulations of the Environmental
Management Commission Implementing that Article, or who falsifies, tampers with or knowingly renders inaccurate any
recording or monitoring device or method required to be operated or maintained under Article 21 or regulations of the
Environmental Management Commission implementing that Article, shall be guilty of a misdemeanor punishable by a
fine not to exceed $10,000, of by imprisonment not to exceed six months, or by both. (18 U.S.C. Section 1001 provides
a punishment by a fine of not more than $10.000 or imprisonment not more than 5 years, or both, fora similar offense,)
hereby request coverage under the referenced General Permit. I understand that coverage under this permit
will constitute the permit requirements -for the discharge(s) and is enforceable in the same manner as an
individual permit.
I certify that I am familiar with the information contained in this application and that to the best of my knowledge
and belief such information is true, complete, and accurate.
Printed Name of Person Signing: —Co m Let,
Title: Otrv.e­�VUr v,( t'g't7cP .5 itc,, L?P..e4,a sG-q-�
7- 17.06
(Signature of Applicant) (Date Signed)
Notice of Intent must be accompanied by a check or money order for $80.00 made payable to:
NCDENR
Final Checklist
This application will be returned as Incomplete unless all of the following items have been included:
Check for $80 made payable to NCDENR
12" This completed application and all supporting documents
lam' Copy of county map or USGS quad sheet with location of facility clearly marked on map
Mail the entire package to:
Stormwater and General Permits Unit
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Note
The submission of this document does not guarantee the issuance of an NPDES permit.
Page 3 of 3
SW tJ-221-101701