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NCG060286_MONITORING INFO_20190620
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. /V (iiCo`v� O o� fi DOC TYPE ❑HISTORICAL FILE C� MONITORING REPORTS DOC DATE ❑ QOJ 5 D G d 0 YYYYMMDD June 18, 2019 CERTIFIED MAIL WITH RETURN RECEIPT ARTICLE NO: 7017 0530 0000 0188 3362 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: Reporting Year 2019 — Storm Water Discharge Monitoring Report Kellogg's Snacks —Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, r SNACKS Kellogg's Snacks Cary Bakery Operations One Quality Lane Cary, NC 27513 Ph 919.677.3200 RECEI E JUN202019 CENTRAL FILES DWR SECTION Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the May & June 2019 monitoring events for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Mark Logue (919) 677-3292 mark.logue@kellogg.com Mr. Logue is available should any questions or problems arise during the review of this DMR. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, Stev rovec Plant Manager Enclosures STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG060000 CERTIFICATE OF COVERAGE NO. NCG06 0286 FACILITY NAME Kellogg's Snacks - Cary Bakery COUNTY Wake Date submitted 06/18/2019 SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or QMonthly'_ May and June Imonthl PERSON COLLECTING SAMPLES Jeffrey 01lison &Patrick Stevens, Hart &Hickman, PC LABORATORY ENCO Laboratories Lab Cert. # 591 & 442 DISCHARGING TO CLASS RECEIVED JUN 9 0 2019 ❑ORW ❑HQW [—]Trout ❑Zero -flow ❑Water supply ❑x Other C, NSW ❑PNA ❑SA FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats ❑ use animal fats/byproducts .•EN"i iZAI_ FILES WR SECTION PLEASE kEIVIElVIi3Efi TO SIGN ON TFlE FtMktt 4 Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall' 0.67 (May), 0.29 (June) or ❑ No discharge this period Outfali No. Date Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000, Sao, Parameter Code - C0530 00400 00340 00556 31616 61212 SW01 05/31/19 220 8.12 140 <1.50 NA NA Down Spout-1 05/31/19 NA 8.01 85 NA NA NA SW01 06/5/19 26 7.83 440 <1.50 NA NA 'Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 for sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. "See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes ❑x no (ifyes, complete Part B) Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No, bate Sample Collected � (mo/dd/yr) 24-hour,rainfall amount, - Inches: New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L" Parameter Code - 46529 NCOIL 00552 COS30 Footnotes from Part A also apply to Part 8 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART it SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES 0 NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES 0 NO ❑ REGIONAL OFFICE CONTACT NAME: Thad Valentine Mail an original copy of this DMR, including -OH "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No_Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." G Ia Date Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 2 of 2 Date: 5-31-2019 Analyst: J. OHison Certification 4 5356 Facility Name: Hart & Hickman, PC Permit ##: _NCG060000 PH Analysis Reference Method: SM 4500 H+B-2000 (include veer e.¢_ SM 4-M&H+ B-20001 .Cal. Time Calibration Buffer 4.0 Calibration Buffer 10.0 *Check Buffer TO Comments 1855 4.0 10.0 7.0 Passed *pH buffer checks are to be within t 0.1 pH units of the standards true value. 4 buffer Lot0fidenlifier. 7 buffer LotH/identifier: 10 buffer Lot#lidentifter: Facility/Sample location Sample Collection Time* Sample Analysis Time* pH Result ► 1 Buffer Check value Comments/Data Qualifiers SW01 1900 1900 8.12 6.99 Down Spout -I 1920 1920 8.01 6.98 ♦ H sample is measured directly in the stream andlor on site, one time may be recorded for collection and analysis with the notation that they are measured in situ or at the immediately at the sample site. ► Calibration drift check is required when performing analyses at multiple sampling locations. (Use Buffer 7.0) Should be within t 0.1 units of the buffer's true value) *All pH results in pH units (i e., s.u.). Report all data values to the nearest 0.1 pH unit. Annual Temperature Sensor Check Date: 8/9/2018 PH Instrument ID: _Myron L Company Ultrameter Il GPFCc serial #2: 6232585 Field Personnel Notes/Equipment Maintenance 10102f1013 Certification # 5356 Date: 6-5-2019 Facility Name: Hart & Hickman, PC Analyst: _P. Stevens Permit #: _NCGt160000 pH Analysis Reference Method: SM 4500 H+B-2000 (include vear a v- SM 4500-H+ 11-2000) Cal. Time Calibration Buffer 4.0 Calibration Buffer 10.0 1 *Check Buffer 7.0 Comments 1625 4.0 10.0 7.0 Passed *pH buffer checks are to be within t 0.1 pH units of the standards true value. 4 buffer LoWlidentifier: 7 buffer Lot#lidentifier: 10 buffer Lot#lidentifier: Facility/Sample location Sample Collection Time* Sample Analysis Time* pH Result ► I Buffer Check value Comments/Data Qualifiers SW01 1635 1635 7.83 6.98 off sample is measured directly in the stream and/or on site, one time maybe recorded for collection and analysis with the notation that they are measured in situ or at the immediately at the sample site. ► Calibration drift check is required when performing analyses at multiple sampling locations. (Use Buffer 7.0) Should be within A. 0.1 units of the buffer's true value) *All pH results in pH units (i.e., s.u.). Report all data values to the nearest 0.1 pH unit. Annual Temperature Sensor Check Date: 919/2018 pH Instrument ID: _Myron L Company Ultrameter 11 GPFCr serial N. 6232-W Field Personnel Notes/Equipment Maintenance 10102/2013 ENCO Labaratartes Accurate. Timely. Responsive. Innovative. 102-A woodwinds Industrial court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, June 12, 2019 KELLOGGS SNACKS/AUSiIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (]an,3uly) ENCO Workorder(s): CC07797 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, June 3, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in - full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates (X* to the sample as raxhmd by the tabwataY, and may drily be reprnduoed in ful. page 1 of a www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SWOT Lab ID: CCO7797-01 Sampled: 05/31/19 19:00 Received: 06/03/19 11:35 Parameter Preuamdon Hold Daft/Time(s) Prep DaterrimaW AnaWsis DaWTmxgs) EPA 1664E EPA 16648 06/28/19 06/10/19 12:00 06/10/19 16:17 SM 254OD-2011 NO PREP 06/07/19 06/05/19 07:15 06/05/19 07:15 SM 522OD-2011 Same 06/28/19 06/07/19 10:15 06/07/19 15:09 Client ID: Down Spout-1 Lab ID: CC07797-02 Sampled: 05/31/19 19:20 Received: 06/03/19 11:35 Parameter Preparation H,glWDate/Time(s) Prep Date/Timefs) AnaWSis Date/Tirnefs) SM S220D-2011 Same 05/28/19 06/07/19 10:15 06/07/19 15:09 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of B w �fw www.encolabs.00m SAMPLE DETECTION SUMMARY Client ID: 5W01 Lab ID: CCo7797-01 Anallyk Chemical Oxygen Demand Total Suspended Solids Results B619 MDL ML 140 10 10 220 15 15 mum Method Notes mg/L SM 522OD-2011 mg/L SM 254OD-2011 Client ID. Down Spout-1 Lab ID: CC07797-02 9D�1]tisFtesults Chemical Oxygen Demand Flag MkL- PQL 85 10 10 blab MethodNs mg/L SM 522OD-2011 FINAL This report relates onfy to the sample as received by the laboratory, and may only be reproduced in Tull. Page 3 of 8 ��CO www.encolabs.com ANALYTICAL RESULTS Description: SW01 Lab Sample ID:CCO7797-01 Received: 06/03/19 11:35 Matrix: Surface Water Sampled:05/31/19 19:00 Work Order: CCO7797 Project: Stormwater (Jan,July) Sampled By:lefFrey 011ison Classical Chemistry Parameters ^ - SKV 6ry ca trwd ana/yre [NC 5911 Analyse FCAS Numherl Results Aga units M ND1 PQL Batch Method Analyzed §X Notes Chemical Oxygen Demand' 140 mg/L 1 10 10 9FO7004 SM 5270D-2011 06/07/19 15:09 JQC Total suspended SalidsA 220 mg/L 6.06 15 15 9FO5002 SM 254OD-2011 06/05/19 07:15 LG Classical Chemistry Parameters ^ - HKOJad6 wlk cried ark" W 4421 Analyte rCAS Numberl Results Hyg Units pE ma EM Ba Method gin ft Notes Oil & Grease (HEM) [C-0007]A < 1.50 nVL 1 1.50 5.00 9FO7013 EPA 1664B 06/10/19 16:17 SMA Description: Down Spout-1 Lab Sample I0: C007797-02 Received: 06/03/19 11:35 Matrix: Surface Water Sampled:05/31/19 19:20 Work Order: CCO7797 Project: Storrnwater (Jan,luly) Sampled By: Jeffrey 011ison Chemistry Parameters Analyt[CA5 Numbers Chemical Oxygen DemandA 13slWts Bag Multi QE KU ML Batch Method Analyzed ft N as mg/L 1 10 10 9FO7004 SM 5220D-2011 06/07/19 15:09 Jac FINAL This report relates only to the sample as removed by the laboratory, and may only be reproduced in full. Page 4 of 8 www.encolabs.com QUALITY CONTROL DATA lassical Chemistry Parameters - Quality Control Batt* 9FOS002 - NO PREP Blank (9F05002-BLK1) Prepared & Analyzed: 06/05/2019 07:15 Spike Source %REC RPD AOallde Resul Has PSZL units Level Result %REC Limits RPD Limit flotes- Total Suspended Solids 2.5 U 2.5 mg/L LCS (9F05002-BSJ) Prepared & Analyzed: 06/05/2019 07:15 Spike Source %REC RPD Ana hda: Resldt Hag P41 Unitf Level Result %REC Limits RPD Limit Notes Total Suspended Solids 96 2.5 mg/L 1w 96 80-120 Duplicate (9F05002-DUPI) Prepared & Analyzed: 06/05/2019 07:15 Source: CCO5486-01 Spike Source %REC RPD Ana Rcs% tt Hilo 1ok 311.0113 Level Result a/OREC Limits RPD LIDA Notes Total Suspended Solids 39 28 mg/L 33 15 20 Duplicate (91`05002-DUP2) Prepared & Analyzed: 06/05/2019 07:15 Source: CCOSS25-02 Analt[te Total Suspended Solids Hatt* !M7004 - Same Resul Ft= PQL 1000 190 Spike Source %REC RPD Units Level Result %FLEC Limits RPD Limit Notes mg/L 910 I4 20 Blank (9F07004-BLK3) Prepared: 06/07/2019 10: IS Analyzed: 06/07/2019 15:09 Spike Source %REC RPD Anal lds Resin ELM EQL Units Level Result o/uREC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (9F07004-651) Prepared: 06/07/2019 10:15 Analyzed: 06/07/2019 15:09 Spike Source %REC RPD ADabds Result H39 PQL units Level Result %REC Limits RPD LLUIR Notes Chemical Oxygen Demand 480 10 mg/L 500 95 90-110 Matrix Spike (9F07004-MS3) Prepared: 06/07/2019 10:15 Analyzed: 06/07/2019 15:09 Source: CC05484-01 Spike Source %REC RPD ADitlXtp Result Has E91 units Level 11=11T %REC Limi RPD Limit Notes Chemical Oxygen Demand 700 10 mg/L 526 180 99 90-110 Matrix Spike Dup (9F07004-MSD1) Prepared: 06/U7/2019 10:15 Analyzed: 06/07/2019 15:09 Source: CCO5484-01 Spike Source %REC RPD Anal ltis Rssi111 Hit9 E91 units Level Raj %REC Limits RPD LIB Notes Chemical Oxygen Demand 700 10 mg/L 526 180 98 90-110 0.9 10 lassiral Chemistry Parameters - Quality Control Dab* 9FO7013 - EPA 1"48 Blank (91`0700-BLKi) Prepared: 06/10/2019 12:00 Analyzed: 06/IW2019 16:17 Anahme Oil & Grease (HEM) Spike Source %REC RPD Rand Hba EM Units Level Result %REC Limit RPD Limit 1.50 U 5.00 mg/L FINAL This report relates only to the sample as received by the la6Orataryr and may Only 6e reproduced in Tull. Page 5 or 8 wrww.en r n b h g. rem QUALITY CONTROL DATA Iassical Chemistry Parameters - Quality Control Bait* 9FL77013 - EPA 16645 - Continued LCS (gF07013-851) Prepared: 06/10/2019 12:00 Analyzed: 06/10/2019 16:17 Spike Source %REC RPD _AeeResul FLM PQL Units Level Result %REC iimits RPD 'mi Notes Oil & Grease (HEM) 156 5.00 mg/L 159 98 78-114 LCS Dup (9F07013-BSDI) Prepared: 06/10/2019 12:00 Analyzed: 06/10/2019 16:17 Spike Sousa %REC RPD Anal lfte Reza Elag MI. Units Level B=dI %REC Umits RPD Limit Notes Oil & Grease (HEM) 149 5.00 mg/L 160 93 78-114 4 18 Matrix Spike (9F07013-MSI) Prepared: 06/10/2019 12:00 Analyzed:06110/2019 16:17 Source: ECO2426-01 Ana Oil & Grease (HEM) Spike Source %nREC Restdt Elan PQL Unim Level Resut %REC Limits RPD 197 5.00 mg/L 178 5.68 108 78-114 RPD LiMAI Now FINAL This report relates only to the sample as reomved by She laboratory, and may only be reproduced in U. Page 6 of a www.encolah--Loom FLAGS/ NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. FINAL This report relates only to the sample as received by the laboratory, and may w4 be reproduced in full. Page 7 of 8 N —l/rI11V1/t/Ir1•trIrl.r Y14V./11 •I-IIIMI•./1'IY/Vrr/`f1 40111 •.V YIINII. YI Wi1M/klN3 114,t- L,1/H I0770 Canlral Poll Dr. 4010 "ltaoullva Park Court, Suite I I 1024 YVriE3IMIRID 1:1 will eY jl♦tI4=IILVIQ1.fa.LUli1 Lrf�' Orlando, Pt.321)24 Jackeonvlllo, Iy1.92216-0000 Cary; NO QM 0 1 (401) 620.6314 Fgx (407) M(Ii N40 (004) 200•a007 Pax 1004) 200.0210 (91 u) hu7.3tu to ?••I r r./1 7l su. ,W r: Pin 0f: ± pi 1 Client Name Kf+LLOGG8 SNACKSIAUST1N FOODS (KE006) P to Numoar InOnO], fC�'L , 01 CO � U x �r�x� Hawmalton. Antitlraa4 f i i I I i I4j I I i ! Preservation ltlea Cualn / I' lk,• L6tlr - ^4•- r�:x�f - T ,-- - dljkl�Y�aHi iuniatouii Times 1l�ly rl :•z, , esi:s •.,:,,,: ii ril! 1;1• F fL: its ills .r l�l l Expedited Owl � i .w h b-1hidlltl lov. -CC07797 _...._ �- $gr) (,lu r'. ,N.t tlirt115 Addiaso ONE QUALITY LANE Pr t Nama(Clow Stormwatar (ien�) CI 78T(l.Ip 6ARY, NC 27813. PD a I olohly tft /� Te1919 677-3519 ) Pay � - pa�ONngn Contact Batsman Crrs� ko„�I►r', y Gkon 'In VA. .#ha 8a lor(g} Nnmo full eon (Pont) M4H t- ZefF/-r d1�.3�-► Ault it Contact Acaaunto Poyabls eamplarye) 6 nature :5— Bl1a Location ! Time Tana Gkt►� ,�G Item s Sample OD (Flald ldenulication) Collection Data Colleclgn III" Comp l Qmtt Matrix 1"61:049* Total N of Co"Wrtaro i`✓ � S/ 3� /��i l4at? �� � �w a ---- rw a x x x ■Boom ■ ��� ■ ■ ■ CSC W �L��- ; �1� -ICY_ �' ■��-® ■■r ■��iI NIMMESIM ■■ w--`-- EN Total # of Contalnora f al ima allnqul y alelfime nbceireld ly -�� [. n}V' ii�u: Raglrlrotnema had Ualdf ima {iecawd lsy B � 181,; Nollnqullhodl.lyDale10ne fiaeaivritl141 I1HItt lu»- r =1 N 0 amPe Cn=ipl .-�...� •,i , I F�ii I )�t'• to wjA �' r L E lttiuUl?lill�f�,} Ur�arc�platll� lalrla:OWOwundwator 00-WI 0*0rinking Water ( MOoditwil OW -Gulf wa Water .WW-Wmtawator A•Alr 0•QOMr Idwrill in Dommenlel Prdoomotian;14-A 010 t+;wN61 § i 1.14b4 1114 tl 1)1 [� r]Il :tr ilarrr,l,,:;,ir}rrl;r ll+a! Note: AN eamploa oubmtltad to CNCO !Alba era In accordwica with Me latrine and owiffflklrq fitted on the reverse e1 this lorni, Ilr MR4i IiON1 H1i110i 4WA01,01tz 4'r •;i *-Wp� EN L a � �oratoirfies, 1, Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, June 14, 2019 KELLOGGS SNACKS/AUSl-IN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE GORY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater CAS ENCO Workorder(s): CC09417 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, June 5, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sarnpie as received W the labaratay, and may only be reVrodmed in full. Page I of 8 www.en r Anti t.com SAMPLE SUMMARY/ LABORATORY CHRONICLE Client III: SWOT Lab ID: CC09417-01 Sampled: 06/05/19 16:35 Received: 06/05/19 16:53 Parameter Preuaratlan Hold Rite/Time(s) Prep Datefflme(s] Analysis Date/TFmelsl EPA 1664B EPA IWB 07/03/19 SM 25400-2011 NO PREP 06/12/19 SM 5220D-2011 Same 07/03/19 06/10/19 12:00 W10/19 16:17 06/06/19 07:19 06/06/19 07:19 06/10/19 14:32 06/10/19 17:05 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 8 CS NS �M) www.encolabs.com SAMPLE DETECTION SUMMARY went ID: 5w01 Lab ID: CGD%17-91 AnalnC Results Has 14DL EUL Units Method Notes CJernkml Oxygen Demand Total Suspended Solids 440 10 10 mg/L SM 522OD-2011 25 8.9 8.9 mg/L SM 254OD-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 8 ■ www.encolabs.com ANALYTICAL RESULTS Description: SWO1 Lab Sample I0:CCO9417-01 Received: 06/05/19 16:53 Matrix: Surface Water Sampled:06/05/19 16:35 Work Order: CCO9417 Project: Stormwater CAS Sampled By: Patrick Stevens Chemistry Parameters ^ - SWO CWY C-Ur&d ar alyte PVC s91j Analyte jCAS Numberl Results ,@gg Units DF MDL PPf L Raub McViod Ana Notes Chemical Oxygen Demand^ 440 mg/L 1 10 10 9F10032 SM 52200-2011 06/10/19 17:05 30C Total Suspended Solids^ 26 mg/L 3.57 8.9 8.9 9FO6004 SM 2540E�-2011 06/06/19 07:19 LG lassical Chemistry Parameters ^ - BVCOJacksa w& certified analyte (MC 4421 Analyte ICAS Numberl Results flag Units QF MDL EQ& Batch Metes Ana[yr N Oil 8r Grease (HEM) [C-0007]^ c 1.50 mg/L 1 1.50 5.00 9F07013 EPA 1564E 06/10/19 16:17 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 8 �� r.11 illy www.encelabs.com QUALITY CONTROL DATA lassical Chemistry Parameters - Quality Control Batdr 9FO6004 - NO PREP Blank (9F06004-BLKI) Prepared & Analyzed: OW06/2019 07:19 Spike Source %REC RPD Analift Result Bw ea1 Units Level Ret %REC Limits RPD Sjm(t Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (9F06004-BSI) Prepared & Analyzed: 06/06/2019 07:19 Spike Source %REC RPD Ana_yte Rtsdt Sim POL Units Level Rat %REC Lial"12 RPD Limit Rotes - Total Suspended Solids 100 2.5 mg/L 100 101 80-120 Duplicate (9F06004-DUP3) Prepared & Analyzed: 06/06/2019 07:19 Source: CCO6596-01 Spike Source %REC RPD Ana Resid Rao ML unib Level Result %REC Limits RPD Limit Notes Total Suspended Solids 240 50 mg/L 240 2 20 Duplicate (9F06004-DUP2) Prepared & Analyzed: 06/06/2019 07:19 Source: CCO7978-01 Spike Source %REC RPD -AT-ballft Result .Rao. PQL Milk Level Result %REC Limits RPD Limit Notes Total Suspended Solids 24 10 mg/L 23 2 20 A0110 9F10032 - Same Blank (9F30032-5LK1) Prepared: 06/10/2019 14:32 Analyzed: 06/10/2019 17.05 Spike Source %REC RPD Anal Result Elan Pal. !Unit@ Level Result a/aREC Limits RPD Limit Notes - Chemical Oxygen Demand 10 U 10 mg/L LCS (9FL0032-BS1) Prepared: 06/10/2019 14:32 Analyzed: W10/2019 17:05 Spike Source %REC RPD �nal]da R4sdt Elan POL Il1t_l14 Level Read t %REC Limits RPD limit Notes Chemical Oxygen Demand 480 10 mg/L 500 96 90-110 Matrix Spike (9FL0032-MS3) Prepared: 06/10/2019 14:32 Analyzed: 06/10/2019 17:05 Source: CC0134S-01 Spike Source °/aREC RPD Ana(1d1e ReSW Boa EEL Units Level Result °!DREG Limits RPD Limit Notes Chemical Oxygen Demand 600 10 mg/L 526 110 93 90-110 Matix Spike Dup (9FIC032-MSDI) Prepared: 06/10/2019 14:32 AnaWad: 06110/2019 17:05 Source: CCO1345-01 Spike Source %REC RPD _Anabu Result Hasa PIDL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 610 10 mg/L 526 110 95 90-110 1 10 lasMcal Chemistry Parameters - Quality Control Batch 9F07013 - EPA 1564E Biank (9F07013-BLKL) Prepared: 06/10/2019 12:00 Analyzed: 06/10/2019 16:17 Spike Source %REC RPD Anahrt Rat Ela4 2QL Units Level Result %REC Limits RPD Limit K912M Oil & Grease (HEM) 1.50 U 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be n4 roduced in fug. Page 5 of 8 CeN , _ www.encolabs.com QUALITY CONTROL DATA lassical Chemistry Parameters - Quality Control Batdr 9FO7013 - EPA 16646 - Condnued LCS (9F07013-B51) Prepared: D6110/2019 12:00 Analyzed: 06/10/2019 16:17 Spike Source %REC RPD Resul Elm PM UnAIN Level Result %REC Limits RPD Llm(t Notes 041 & Grease (HEM) 156 5.00 mg/L 159 98 78-114 LCS Dup (91`07013-15SDI) Prepared: 06/10/2019 12:00 Analyzed: 06/10/2019 16:17 Spike Source 9bREC RPD .Anahft Result Elm POL Units Level Result %REC Limits RPD Limit Notes_ Oil & Grease (HEM) 149 5.00 mg/L 160 93 78-114 4 18 Matrix Spike (9F07013-MSI) Prepared: 05/10/2019 12:D0 Analyzed: 06/10/2019 16:17 Source: BCO2426-01 Ana Oil & Grease (HEM) Spike Source Rewit BOG PQL ni Level Resu 197 5.00 mg/L 178 5.68 %REC %REC Limits RPD 108 78-114 RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in fu4. Page 6 of 8 s � www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALCI Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. FINAL This report rdates ordy bD the sample as reomW by the laboratory, and may only be reproduced in full. Pape 7 yr 8 ENVIRONMENTAL. CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD CO 10770 Central Frail Ur, 4810 (Ixaa No park Court, pulse 11 I to -A NJo«tdlrnls livid n"I 4.1 DAarldo, PL 92524 Jadworm#le, Of.922104Mg Cafy, NO 27$t t (401) 420•p914 Pax (A(I7) OZ111040 (F104) 2WW07 Per (O04) 70O•p21U (910) 46-ImWOU ho fQ I'h ,ilI l ag 14 www,@Iieofabs.com I 1 P tio6 l of .. � Client Name rO at umbai je :., 4f udotud ARdi ss§ y _ C(6li' �tJf�E7fi�:•CIrUi'liFilr�rlllU - _-I Addrese Pro)ea1 NamoMew I sfa filMf '_ • I .,' dsexytri ; CA i C4yrSTOp PO N I billing In10 oe 1ri ► IU I W7�,Sic l7d@rcl Tel lTax Fie rv7 comae I / VF ,, i r ..3z1 E:(pt'diied Safnplorte) Name, Alfilialion (Print) alfling CXL Snrrrpfar{eJ 9i0gjrturo Sits Looaton I Tlme Zama ` G-�11} W$I kBf ri 3l i 1 10- COCA`1 . • preee,velleFi See Ccxlas ff.v,r•l,us,• r iF.'f.a>s l�w� t��tt hams Sample 10(Field ldo"ficalion) Collactlon Matrix Total N 01 Cotloolon Date Tlma ICom IGIrab age codaN) ContainersTTI t)ertilil+ r"'rn�lsilin I . 111 j., • Ik yi I • 1 I a- Total 11 of MiritorfiorS 1 Sample KII IrreperMl by RON y ale/rlmn _ rdnceiv d r r I4'lei i CornmaNIUSpedol RaporIOU ROgUlfamente 111011m:fUllihiril Uy bn er•rime ar r ; • • Rollnqutahad Sy biltatTime Received IIV lluiF # e'0 er N's Tampa on140calpi "!' I' ii 4 Sidi FNF I'alf •O1� ��iiE31�I�Gfllill� Ul�acr,� I)1t�}plc: N.1r1v , nw.f1mtnr Wxtnr an• M I)Wprinf<lnn Watar 00-Sediment oWSurtaco waler WW-Waslowaler A•Ak 0.01rar (detail In comments) Prevotvetionl Vice 11-i1cl N-turo`F 6 fir) lk'(11 F 01'fhuF "' hNnelsi l Sample Preservation Verification ENCO Cary Work Orden CCO9417 Project: Stormwater CAS Clierit., KELLOGGS SNACKSIAUSTIN. FOODS. (KE006): Proj!ect.,#- [none], Ill aggedl lbv 05-Jurr,49! 17:121 Loggedigy-: Joh, ni C: King Preservation: Check, Performed By: Date/Time.- CC09417-01; ,Cant! -- - Ij !Type! Rnas+(pH)) I Requeiarreff. HICheckedl, IhiCantrdt pAlAdd justeDate/.Tme., Adiusqedt 11 ReaqpntUsed/,Comment�;: 13' 250inLA+H2504 <2 Y I N' Y 1' N. 1 A C 250mLA+H2SO4 <2 Y / N: I &�-' Y / N I 0 250rnLP+H2SO4' <2 Y / N / NA Y / Nil NA Reagent h1wirm 10 I I 1 1 21 1- F pH Strip ID- C.%ELMNTV"rir ftwkq PreservafianChe&-rpt to Remma Name ID 3 51 41 61 '- Page I May 14, 2019 CERTIFIED MAIL WITH RETURN RECEIPT ARTICLE NO: 7017 0530 0000 0188 3652 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 SNACKS Kellogg's Snacks RECEIVED rCEI fED Cary Bakery Operations MAY 21 2019 CENTRAL FILES D\pjR SECTION Re: Reporting Year 2019 —Storm Water Discharge Monitoring Report Kellogg's Snacks —Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, One Quality Lane Cary, NC 27513 Ph 919.677.3200 Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the April 2019 monitoring event fo r: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Mark Logue (919) 677-3292 mark.logue@kellogg.com Mr. Logue is available should any questions or problems arise during the review of this DMR. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, 1 Stev urove Plant Manager Enclosures STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG060000 Date submitted OS/14/2019 CERTIFICATE OF COVERAGE NO. NCG06 0286 _ FACILITY NAME _ Kello_ gg's Snacks - Cary Bakery COUNTY Wake PERSON COLLECTING SAMPLES Greg Kanellis }cart & Hickman, PC LABORATORY ENCO Laboratories - Lab Cert. # 591 & 442 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ❑x Monthlys_ April (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑Zero -flow ❑Water Supply ❑x Other C, NSW ❑PNA ❑SA FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats ❑ use animal fats/byproducts PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall z 0.2 or n No discharge this period OutfalLNo. Date Sample Collected, mo/dd/yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform, Colonies per 100 ml Enterococcl, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 120 30 1000, 500, Parameter Code C0530 00400 00340 00556 31616 61211 SW01 04/26/19 59 7.1 1200 <1.50 NA NA 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 'For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5Monthly'Sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes Eno (if yes, complete Part B) Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 1of2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, IncheS2 New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L° Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART it SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑x NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑x NO ❑ REGIONAL OFFICE CONTACT NAME: Thad Valentine Mail an original copy of this DMR, includina all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" report) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for kpowing violations." Signature of Perm SS CrcZf Date Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 2 of 2 Date: 4126/2019 Analyst: G. Kaoellis Certification tt 5356 Facility Name: Hart & Hickman, PC Permit ft: _NCC060000 PH Analysis Reference Methnd- Sht 4500 H+B-2000 (include veer e_v__ SM dr%MH+ R-2000) Cal. Time Calibration Butler 4.0 Calibration Buffer 10.0 `Check Buffer 7.0 Comments 0900 4.0 10.0 7.0 Passed 'pH buffer checks are to be within t 0.1 pH units of the standards true value. 4 buffer Lol#fidentifier: 7 buffer Lotllridentifier: 10 buffer LotMdentifler: Facility/Sample location Sample Collection Time* Sample Analysis Time• pH Result 10-1 Buffer Check value Comments/Data Qualifiers SWOT 0915 0915 7.1 7.0 ♦ If sample is measured directly in the stream and/or on site, one time may be recorded for collection and analysis with the notation that they are measured in situ or at the immediately at the sample site. ► Calibration drift check is required when performing analyses at multiple sampling locations. (Use Buffer 7.0) Should be within t 0,1 units of the buffer's true value) *All pH results in pH units (i.e., s u.). Report all data values to the nearest 0.1 pH unit. Annual Temperature Sensor Check Date: 4/19/2019 pH Instrument ID: _Horiba U-500007PBU8RLJ Field Personnel Notes/Equipment Maintenance 10/0212013 T16 Laboratondes ErNtf- t-,r Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, May 7, 2019 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater CAS ENCO Workorder(s): CC06065 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, April 26, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may onty be reproduced in fill. Page 1 of 8 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 5WU1 Lab ID: C006065-01 Sampled: 04/26/19 09:15 Received: 04/26/19 09.48 Parameter PreoarW20— Hold Date/Tmefs) Prep Date/Timg(s) Analysis Date/Time(s) EPA 1664E EPA 1664E 05/24/19 05/01/19 10:11 05/02/19 16:05 SM 254OD-2011 NO PREP 05/03/19 05/02/19 14:40 05/02/19 14:40 SM 5220D-2011 Same 05/24/19 04/30/19 13:26 04/30/19 20:20 i FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in fit. Page 2 of 8 CqNGi,..oj www.encolabs.com I SAMPLE DETECTION SUMMARY �_ Clierrt ID: 5WO1 Lab ID: 0006O65-01 ■ A1301Besu[m Elm Mal EQL unib M notes Chemical Oxygen Demand 1200 20 20 mg/L SM 5220D-2011 Total Suspended Solids 59 20 20 mg/L SM 2540D-2011 FINAL This report rekates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of a i! ANALYTICAL RESULTS Description: SWOT Matrix: Surface Water Project: Storrrtwater CAS lassical Chemistry Parameters. ^ - ENCO Cary cera r-d analyle [NC 5911 Analybe rCAS Numberl Resu linitE Chemical Oxygen Demand^ 1200 mg/L Total Suspended Solids- 59 nV/L �Iassical Chemistry Parameters ^ - Mco botsav le c"fied an*tL (NC 4421 Analyte rCAS Numberl Results )fig Units Oil & Grease (HEM) [C-0007]^ < 1.50 mg/L Lab Sample ID:CCO6065-01 Sampled:04/26/19 09:15 Sampled By:Greg Kanellis (9M 99 www.encolabs.com Received: 04/26/19 09:48 Work Order: CCO6065 DF MrL EQl. %,1&h Pled AnaJ]CSsd ft JYt�ae 2 20 20 9D30041 SM 522Oi-2011 04/30/19 20:20 JOC 8 20 20 9E02026 SM 254OD-2011 05/02/19 14:40 ASC DE FSDL EQ—L Batch Metlyod Anahmed fix D. 1 1.50 5.00 9EO1002 EPA 16646 05/02/19 16:05 SMA HNAL I This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 4 of 8 QUALITY CONTROL DATA iassical Chemistry Parameters - Quality Control Batch 9030041 - Same (e..JVLG..,0j www.encoiabs.com Blank (9D30041-BLKI) Prepared: 04/30/2019 13:26 Analyzed: 04/30/2019 20:20 Spike Source %PLEC RPD Anal lLt Result flag EQL Units Level Resu(t %REC Limits RPD Lim m2um Chemical Oxygen Demand 10 U 10 mg/L LCS (9D30041-BS1) Prepared: 04/30/2019 13:26 Analyzed: 04/30/2019 20:20 Spike Source %REC RPD _A4ah tS Result Flag 091 Units Level Resu R %REC Limits RPD Limit NMar Chemical Oxygen Demand 490 10 mg/L 500 99 90-110 Matrix Spike (9D30041-MS1) Prepared: 04/30/2019 13:26 Analyzed: 04/30/2019 20:20 Source: C607972-01 Spike Source %REC RPD Anal R9:&Ujt Elm QQL Units Level Result %REC Limits RPD l illift Notes Chemical Oxygen Demand 660 10 mg/L 526 160 95 90-110 Matrix Spike Dup (9D30041-MSD1) Prepared: 04/30/2019 13:26 Analyzed: 04/3U/2019 20:20 Source: CB07972-01 Aml Chemical Oxygen Demand Bauch OE02026 - NO PREP Rew Flag EQL 660 10 Spice Source %REC RPD Units Level Resu 0/aREC Linift RPD Limit Nliftli mg/L 526 160 96 90-110 1 10 Blank (9ED2026-BLK1) Prepared & Analyzed: 05/02/2019 14:40 Spike Source %REC RPD Anal v6e Rmutt Elm POL Units Level Result %REC iL mfts RPD Limn Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (9EO2026-BSI) Prepared & Analyzed: 05/02/2019 14:40 Spike Source %REC RPD -Anallde Resu Jt Flag ML unift Level Resuk %REC Limits RPD klinift Notes Total Suspended Solids 96 2.5 mg/L 100 96 80-120 Dupilcate (9E02026-DUPI) Prepared & Analyzed: 05/02/2019 14:40 Source: CCO1122-01 Spike Source °✓DREG RPD Alwl RteuS E109 PQL Un Level Resu 0/oREC Urnits RPD mmit Notes Total Suspended Solids 51 25 mg/L 47 8 20 lassical Chemistry Parameters - Quality Control Batch OEOIO02 - EPA 16648 Blank (9E01002-BLKI) Prepared: 05/01/2019 10:11 Analyzed: 05/02/2019 16:05 Spike Source %REC RPD Anal Y Resu Elite PM Units Level Result %REC Limits RPD Lima Notes Oil & Grease (HEM) 1.50 U 5.00 mg/L LCS (9E01002-BSI) Prepared: 05/01/2019 10:11 Analyzed: 05/02/2019 16:05 Spike Source %REC RPD AnaResult ELM pa Units Level Resu Iti %REC Limits RPD khnft pobes oil & Grease (HEM) 133 5.00 mg/L 157 85 78-114 FINAL This report relates only to the sample as received by the Laboratory, and may only be reproduced in full. Page 5 of 8 (49NCE..9) www.encolabs.com QUALITY CONTROL DATA lassical Chemistry Parameters - Quality Control Bafth 9EV1002 - EPA 16"S - Qw nived LCS Dup (9E0100Z-BSD1) Prepared: 05/01/2019 10:11 Analyzed: 05/02/2019 16:05 Spike Source %REC RPD Anal yjg Result Flag PQL llai Level Result %REC Lim RPD Limit Notes Oil & Grease (HEM) 133 5.00 mg/L 148 90 78-114 0.6 18 Matrix Spike (9E01002-MSL) Prepared: 05/01/2019 10:11 Analyzed: 05/02/2019 16:05 Source: BC01835-01 Spike Source %REC RPD _Andyte Result iw 00..L Ubitr Level Result %REC Limits RPD Limit lYobes Oil & Grease (HEM) 130 5.00 mg/L 149 1.50 U 87 78-114 FINAL This repot dates only to the sample as reoNved by the laboratory, and may only be reproduced in full. Page 6 of 8 (9 �Gm www.enculabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALL] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. FINAL This report relates o* to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 8 00rVvl$60 T7 Ti 0}],15 Canlrul Pnr1 (it 4010 Executive Park Court, Suits I I I - , • , 102•A WoDdrAnds industrial Ct, r]ringgll. N. Unpa Jacksonville, Fl- 32:f10.0060 Gary, NO 27011 (Mn 1 21i!n'III FR! Mfl7) A60,13745 (004)2P0.3007 Fax (PO4) 200-6210 (010)407.3000 Fax (010) b97.3315 ;lien! f l?{niR f'0003 (KE(7 ) (#IjlJrrt§o OW" QUAl,.ITY �ANR f,IPy;Gfr?'�II RY tit r,tr (9jT)0J 0.19 fi — §,im iIA06) l!ii.-.in fl lfiplllr, . JPNMr .. �'lmF,tt�y-k'>.! b ;pplRrl { ;+indfltrn. r — — f+i gJPGI f+I;nlhar [none} I!m{art flnmelllesq Stormwater CAS lin lorlinq �'anferc[ Rodney Bateman WWI Qflrgnrr �GqutllntB Payewe Ode LPrR4an 1 Time Zone ilArn N .rr,l;, ffv wRkl IQgnlilir.p1lonl f nllrlr,tlnn ifnl" C01#no?ipn Tin;h comp f OW) it i1{�rltlfilnrr i�a4iriiiemRrlls Total 0 of ConWnora s.l n as I Rmpa oo VJKPIPI r Ink Ci�i-t7•H;li{}:"n:at So-Eioll Owztlli.01rtfl YJafw §Ld§5!1'MFvrl W0411,90 WORt WIN-Wa4IeWRlet A -Air Q,Qhgr (daUIII In Comments) Wesorwallrml I-Ico WHO N-HNO3 p.H2004 NO'NaOH 0,01hor I-tg1e All mmpine swfmiVeli ra f;NCO Inks ore in acosn)nnoe wllh IN tarms and conditions listed on Ilia ravorso of this form, untm prier wrltlon agreements exist wwwattincoiaos.com Page,--L of Roqueatod Turnaround T'Imos Note : Rush requests subject to ac-coptanco by the facility Standard Expedited Due 1�1_ Lab Workordor cco6as5 Sample Comments commonla) P Sample Preservation Verification G ENCO Cary 9 C Work Order. CCO6065 Project: Stormwater CAS Client: KELLOGGS SNACKSIAUSTIN FOODS (KE006) Project #: [none] Logged Ira: 26-Apr-1910:04 Logged By: John C King _ Preservation Check Performed By: DatelTirne: AZ6 C( 5-M C t T -- p�3B �, c .. i� '. •y���c1Presl yl? � �`^ g_ (11 eliGe7 • _ fi"�aa ......�. mod, 1 t��iae B 250mLA+H2SO4 <2 Y► N 1& Y I N I C 25D aLA+H2SO4 t2 YIN ► YIN116 D <2 V / N ► MA Y ( ► NA e IRea ent 1Name II.D 1 7 ,PH Strip MI r '; )rC'�"=1 IRea entiName IID 3 4 Rea ent?Name IID 5 0 1C'CELMNTIPrintkwko IPreservationCheck!rpt ,page 1 E March 22, 2019 CERTIFIED MAIL WITH RETURN RECEIPT ARTICLE NO: 7017 0530 0000 0199 3249 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED MAR 2 8 2019 CEN 1 iuAL FILE: OWR SECTJO; l Re: Reporting Year 2019 — Storm Water Discharge Monitoring Report Kellogg's Snacks — Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, �A s Kellogg's Snacks Cary Bakery Operations One Quality Lane Cary, NC 27513 Ph 919.677,3200 Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the March 2019 monitoring event for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General hermit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Mark Logue (919) 677-3292 mark.logue@kellogg.com Mr. Logue is available should any questions or problems arise during the review of this DMR. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate 'the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, Steve Surovec Plant Manager Enclosures STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG060000 Date submitted 03/21/2019 CERTIFICATE OF COVERAGE NO. NCG06 0286 FACILITY NAME Kellogg's Snacks - Ca Baker COUNTY Wake PERSON COLLECTING SAMPLES Greg Kanellis J art & Hickman, PC LABORATORY ENCO Laboratories Lab Cert. # 591 & 442 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or QMonthlys_ March (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero -flow ❑Water Supply ❑SA ❑x Other C, NSW FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats ❑ use animal fats/byproducts PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Total event rainfall' 0.1 or ❑ No discharge this period' Outfall No. Date Sample Collected, mo/dd/Yr TSS, mg/L pH, Standard units COD, mg/L Oil and Grease, mg/L Fecal Coliform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark - 100 or 50' Within 6.0-9.0 120 30 1000, 500' Parameter Code - C0530 00400 00340 00556 31616 61221 SW01 03/8/19 4.1 6.9 85 <1.50 NA NA 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 4See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes EO no (if ves, complete Part B) Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, IncheS2 New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - 15 mg/L 100 mg/L or 50 mg/L° Pammeter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES 0 NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES Q NO ❑ REGIONAL OFFICE CONTACT NAME: Thad Valentine Mail an original copy of this DMR including all "No Discharge" re orts within 30 days of receipt of the lab results or at end of monitoringperiod in the case Pf "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." lcw� _-_1 Signature of Per-mittee zs Date Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 2 of 2 Date: 3X2019 Analyst: G. KaneI6 Certification # 5356 Facility Name: Hart & Hickman, PC Permit #: _NCG060000 pH Analysis Reference Method: SM 45M H+B-2000 (include vear e_g_ W 45011-H+ B-20001 Cal. Time Calibration Buffer 4.0 Calibration Buffer 10.0 *Check Buffer 7.0 Comments 10:30 4.0 10.0 TO Passed 'pH buffer checks are to be within t 0.1 pH units of the standards true value. 4 buffer Lot#lidentifier: 7 buffer Lot#hdentifier: 10 buffer Lot#rdentifier: Facility/Sample location Sample Collection Time* Sample Analysis Time* pH Result 10-1 Buffer Check value Comments/Data Qualifiers Sw01 1715 1715 6.90 7.0 ♦If sample is measured directly in the stream and/or on site, one time may be recorded for collection and analysis with the notation that they are measured in sim or at the immediately at the sample site. ► Calibration drift check is required when performing analyses at multiple sampling locations. (Use Buffer 7.0) Should be within f 0.1 units of the buffer's true value) *All pH results in pH units (i.e., s.u.). Report all data values to the nearest 0.1 pH unit. Annual Temperature Sensor Check Date: 8/9/2018 pH Instrument ID: _Myron L Company Ultrameter 11 GPFC serial H. 6232585 Field Personnel Notes/Equipment Maintenance 1010212013 4 Eli CO Laboraton'c*s Accurate. Timely. Responsivc Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, March 20, 2019 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/best: Stormwater (Jan,July) ENCO Workorder(s): CC03597 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, March 8, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FDM This report relates only to the sample as received by the laboratory, and may only be reproduced in ful. Gage i of a www.encolahs.com SAMPLE SUMMARY/LABORATORY CHRONICLE GierrtID: SWOT LabIO: CC03597-01 Sampled: 03/08/19 17.15 Received: 03/08/19 17:35 Parameter ratio Bold WC111mefs1 Prep Daw/TiMSfsl badpis 0ate/Time(s) EPA 1664E EPA 1664B 04/05/19 03/13/19 17:25 03/19/19 15:53 SM 2540D-2011 NO PREP 03/15/19 03/14/19 12:45 03/14/19 12:45 SM 522OD-2011 Same 04/05/19 03/15/19 07:47 03/15/19 10:30 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in M. Pape 2 of 8 www.ancolabs.com SAMPLE DETECTION SUMMARY Chem M; SWOT Lab I0. CC03597-01 Analyte RSs4lt:c Eiw HQL P91 Units Metfiod N Chemical Oxygen Demand 85 10 10 mg/L SM 5220D-2011 Total Suspended Solids 4.1 2.5 2.5 mg/L SM 2540D-2011 FLNAL This report mate anly to the sample as received by the laboratory, and may only be reproduced in Nfl. Page 3 of a ANALYTICAL RESULTS Description: SWOT Lab Sample ID:CC03597-01 Matrix, Surface Water Sampled:03/08/19 17:15 Project: Stormwater (3an,July) Sampled By:Timothy 10otz lassical Chemistry Parameters .lNeW www.encolabs.com Received: 03/08/19 17:35 Work Order: CC03597 ^ - SIKU C-y c-tfied dnaiyh: (NC 5911 Anatvte fCAS Numher] Results -$fig Units IE MMDIL PQL Batch Method Analyzed !<]I Notes Chemical Oxygen Demand' 85 mg/L 1 10 10 9C15003 SM 522OD-2011 03/15/19 10:30 30C Total Suspended Soilds^ 4.1 mg/L 1 2.5 2.5 9C14015 SM 254OD-2011 03/14/19 12:45 ASC lassical Chemistry Parameters ^ - GVW Jades Wffe c"JW"W[A'C 4421 Analyte rCAS Numberl Results lilm 11u1.t, 1LE KU PQL Batch Method AnaboW III NMS Oil & Grease (HEM) [C-"71^ < 1.50 mg/L 1 1.50 5.00 9C13014 EPA 1664E 03/19/19 15:53 SMA FINAL This repot relates ady to the sample as received try the laboratory, and may only be reproduced in ful. Pape 4 of 8 w � www.encGlabs.com QUALITY CONTROL DATA lassical Chemistry Parameters - Quality Control Batch 9C24015 - NO PREP Blank (9C14015-BLK1) Prepared & Analyzed: 03/14/2019 12:45 Spike source %REC RPD Amhde Resift film POL units Level Resul %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (9C14015-BS1) Prepared & Anaiyaed: 03/14/2019 12:45 Spike Source 4/e14.EC RPD Ana1ift Renit Elan f'4L 1lnfu Level Result %REC Limits RPD Lia i Notes Total Suspended Solids 100 2.5 rnWL 100 101 80-120 Duplicate (9C14015-DUP3) Prepared & Analyzed: 03/14/2019 12:45 Source: CBLSS42-D1 Spike Source %REC RPD Resin Flag PAL Uniu Level Reno %REC Limits RPD Limit Notes Total Suspended Solids 17000 1200 mg/L 21000 20 20 Duplicate (9C14015-DUP2) Prepared & Analyzed: 03/14/2019 12:45 Source: CCO2186-01 AnWytc Total Suspended Solids Batch 9C15003 - Same 900 500 Spike Source %REC RPD Units Level Riffs 016REC Limits RPO Limit Notes mg/L 900 0 20 Blank (9C1S003-81.1(1) Prepared: 03/15/2019 07:47 Analyzed; 03/15/2019 10:30 Spike Source %REC RPD Ana 11dE Result Hag eel. Units Level ResLdt 0/aREC limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (9C3S003-851) Prepared: 03/15/2019 07;47 Analyzed: 03/15/2019 10:30 Spike Source %REC RPD A[ldhme Result Flag P91 unfits Level RSS311L %REC Limits RPD Limit Notes Chemical Oxygen Demand 500 10 mg/L 500 99 90-110 Matrix Spike (9C1S003-M51) Prepared: 03/15/2019 07:47 Analyzed: 03/15/2019 10:30 Source: CCO1617-01 Spike Source %REC RPD Ana Result ELM Mi. 11,1111 Level %REC Lim] RPD Limit Notes_ Chemical Oxygen Demand 700 10 mg/L 526 180 99 90-110 Matrix Spike Dup (9C15003-M501) Prepared: 03/15/2019 07:47 Analyzed: 03/15/2019 10:30 Source: CC01617-01 Spike Source %REC RPD Anal w3e Resul flag P91 Units Level Re I %REC Uneits RPD Limit Notes Chemical Oxygen Demand 700 10 mg/L 526 180 99 90-110 0.3 10 lassical Chemistry Parameters - Quality Control Batch 9C13014 - EPA 1G640 Blank (9C33014-BLK1) Prepared: 03/13/2019 17:25 Analyzed: 03/14/2019 14:40 Anal Oil & Grease (HEM) Spike Source LiREC RPD Resul t iRag pQL Slait4 Level Result %REC 6_mii4 RPD lIm1I 1.50 U 5.00 mg/L 4 FINAL This report relate; 0* to the sample as reeerved by the laboratory, and may only be reproduced In full. Page 5 of 8 J 4w www.encolabs-com QUALITY CONTROL DATA lassical Chemistry Parameters - Quality Control Batch 9C13014 - EPA 1664E - Continued LCS (9C13014-B51) Prepared: 03/13/2019 17:25 Maiyzed: 03/14/2019 14:40 Spike source %REC RPD Ana hde ReWt flaa EM U-ndb Level Refit %REC LIM RPD umj Notes_ Oil & Grease (HEM) 151 5.00 mg/L 163 92 78-114 LCS Dup (9C13014-BSDI) Prepared: 03/13/2019 17:25 Analyzed: 03j14/2019 14:40 Spike Source °/aREC RPD And1vto Result Boo 021. units Level Result %REC Limits RPD Limit Notes_ Oil & Grease (HEM) 131 5.00 mg/L 160 82 78-114 14 18 Matrix Spike (9C13014-MS1) Prepared: 03/13/2019 17:25 AroWed: 03/14/2019 14:40 Source: SC01066-03 Area ift Oil & Grease (HEM) Spike Source %REC Result B" —PGL- Units Level Result %REC Limill RPD 162 5.00 mg/L 167 1.50 U 97 78-114 RPD Limit Notes FINAL This report relates only to the sample as received by ttre laboratory, and may only be reproduced in full. Pape 6 of 8 Ce! ! www.enoolabs.com 11 FLAGS/NOTES AND DEFINMONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. ECALC] Calculated analyte - MDLIMRL reported to the highest reporting limit of the component analyses. FINAL This report relates onlY to the sample as received by the laboratory. and may only be repraduced in U. Page 7 of a I NVIHUNMENTAL CONSURVATION LAWORATORIES CHAIN•OF-CUSTOOY RECORD www,oricolnba.cem CO 10170 Cenlrol Ppn Or, 41M Q1to AVO Park Coufi, aullo I I I M-A 1lyawMiuds 1114uslnol Of. , Orlando, FL 32024 Jockaonvllla, PL 922 10. 0000 Caws, NC 0611 1407) 02e•e314 Pml (40T)050,0110 (004MO-3007 Fart {0041200.0210 (010) 4o7�3atio Flux JOW 407mMill Ptiyp � __, (if _ Client Namo "Ki Number Ilrgtalows l Motilysian .. r)tllJ�a Fjf t' lJf l itl fplJfld KELLOGGS SNACKS.rAUSTIN FOODS (KE00e) [none] `i 11ilod Addroaa pfojw NaMOM400 Ntila : !1IM1 Nfluesle atiNbcl to ONE QUALITY LANE Stormwater (Jen,July) lice'�1610m)by lliarruily r Cityr8T21 PO a ! pile Into �r CAAY, NC 27513- 48M 4634 �p �/l �f€iIl[i�irCi T01 Ppr[ Reporting Cow"I m (919) 677-3519 () - Rodney Betemen GGGVVV Sam larla) Nama, AflItla110n (Prinlj p131in Com I SO ►xaunts Payeble Samplar(s) Slgnaturo 81to Location l Tuna Zono $ kAO VYOf ICU ddr CC03597 Proaarvtillari Sae CodeIComhina ae nncussnr ' Colloatlon Mntna oIlvltongo Tmo Complprnb aenp0del Total of gl3lill)Ii� Uflfil41i18itemSam[" Conlalnere sw 4 x x- x -1 I --T 11 0- MMM a pemple WI Pfepafad By alnflIme cllaqubh y 7e X Dal I VI y !1 60111. NofingWahe py Da sliktal Rocalvad � �� fi4lr?Illfilrj Commenlalppeebl Heponlrp Roqulremerna TIIN/Iiflii alIntiWahotl by )allYilma r acoirn1113y O&I A e 6 Inge on 1=11A 0 ;?. Grrrlih Igll IWn la1'Tio �Il�ui -- oil H00Limulo Iaatrta ; Ga ,%JratlnaWalef DW-UOIr tJR,UMa1nii Yvaier aR'u901M9n1 YRHiarq= 1'Ye1af, nt!•7RaaWNalef p•Por V,Vg1er tVa4al in GammenE/l /•rfeervanunr 111up r—W li'1'1r•ru:l 1J•r1v!i31J'-i-aWlf w- /.nngr Irrglall I!I CgllrtngrllaJ Nora All aampkb auhmltlnd to UNCO Lath ato In a000rddnao with Ilia lewmll and COndlllona Noted an Iha faMse of Ihla talm, urilana pilot Millali adt001041106 60101 Sample Preservation Verification a � Utl'OA. of -der: CCO359- Pr)jact Stvrmwater (•Dank July,•): siriirKEII I GGGS SN;4CKSl'�IN FWEIS (KEaGS� Rt ezt =ej if male. �� r M F a C 25DM A-4 F c 1f I, Nt !` ksi lY /I x !1 I -e2 le !F 15 NA Flea ent Name ID 1 2 pH Strip ID: �U Reawnt Name ID 3 4 Reagent Name ID 5 6 C:IELMNTIPrintlwko PreservationCheck.rpt page 1 , March 1, 2019 CERTIFIED MAIL WITH RETURN RECEIPT ARTICLE NO: 7017 0530 0000 0188 3256 Central Files RECEIVED Division of Water Quality MAR 18 2019 1617 Mail Service Center CENTRAL FILES Raleigh, North Carolina 27699-1617 Dt"M SECT10,NI Re: Reporting Year 2019 — Storm Water Discharge Monitoring Report Kellogg's Snacks — Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, Kellogg's Snacks Cary Bakery Operations One Quality Lane Cary, NC 27513 Ph 919.677.3200 Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the February 2019 monitoring event for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Mark Logue (919) 677-3292 mark.logue@kellogg.com Mr. Logue is available should any questions or problems arise during the review of this DMR. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted_ Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, -�4 Steve Surovec Plant Manager Enclosures STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCGO60000 Date submitted 02/27/2019 CERTIFICATE OF COVERAGE NO. NCG06 0286 _ FACILITY NAME Kellogg's Snacks - CaryBakery_ COUNTY Wake PERSON COLLECTING SAMPLES _Haley Randolph, Hart & Hickman, PC LABORATORY ENCO Laboratories Lab Cert. # 591 & 442 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2019 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ❑x Monthly' February (month) DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA ❑Zero -flow [:]watersupply ❑SA ❑x Other C, NSW FACILITY ACTIVITIES INCLUDE (check all that apply): ❑ use/process meats ❑ use animal fats/byproducts PLEASE REMEMBER TO SIGN ON THE REVERSE � Total event rainfall' 0.15 or ❑ No discharge this period' Outfall°No.: UateSample Collected; mo/dd/yr TSS, mg/L. pH, Standard units, COD, mg/L Oil and Grease, mg/L Fecal Collform, Colonies per 100 ml Enterococci, Colonies per 100 ml Benchmark 100 or 504 Within 6.0 — 9.0 120 30 10001 5001 Parameter Code - C0530 00400 00340 00556 31616. 61211 SW01 02/11/19 32 7.0 54 1.89 J NA NA 021119 4.8 7.2 28 <1.50 NA NA 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. "See General Permit text, Table 1, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new oil per month? ❑ yes 2 no (if M, complete Part B) Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. 0utfall No.. Date Sample Collected [mo/dd/yr) 24-hour rainfall amount, Inches New Motor 011 or Hydraulic oil Usage Non -Polar O&G/Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L° Parameter Code. - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑X NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES 0 NO ❑ REGIONAL OFFICE CONTACT NAME: Thad Valentine Mail an original copy of this MR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case g f "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonm;z7r: " 3 l Signature of Pe Date Permit Date: 11/1/2018-05/31/2021 SWU-249, Last Revised 11/5/2018 Page 2 of 2 Date: _f/1112019 Analyst: _H. Randolph Certification # S356 Facility Name: Hart & Hickman, PC Permit N: _NCG060000 pH Analysis Reference Method: S1114500 H+B-2000 (include veer e.e_ SM 4500-H+ B-2000) Cal. Time Calibration Buffer 4.0 Calibration Buffer 10.0 *Check Buffer 7.0 Comments 10:15 4.0 10.0 7.0 Passed *pH buffer checks are to be within i 0.1 pH units of the standards true value. 4 buffer LotWidentifier: 7 buffer LetWidentitier: 10 buffer Lot#lidentifier: Facility/Sample location Sample Collection Time* Sample Analvsis Time* pH Result i Ji-1 Buffer Check value Comments'DataQualifiiers SWOT 11:35 1I:35 6.95 7.0 5WO2 11:45 11:45 7,16 7.0 ♦ If sample is measured directly in the stream and/or on site, one time may be recorded for collection and analysis with the notation that they are measured in situ or at the immediately at the sample site. ► Calibration drift check is required when performing analyses at multiple sampling locations. (Use Buffer 7.0) Should be within t 0.1 units of the buffer's true value) *All pH results in pH units (i.e., s u.). Report all data values to the nearest 0.1 pH unit. Annual Temperature Sensor Check Date: 819l2018 pH Instrument ID: _Myron L Company Ultrameter II GPFCE serial M. 6232M5 Field Personnel Notes/Equipment Maintenance 10/02/2013 - CO Laboratories Accurate. T itnelya Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, February 21, 2019 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater CAS ENCO Workorder(s): CCO2164 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, February 11, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report slates a* to the sample as received by dw laboratory, and may only be reproduced in U1. pow 1 of a www.emmiabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE QFentID: SWOS Lab ID: C002164-01 Sampled: 02/11/19 11:35 Received: 02/11/19 12:13 Parameter pnwaratlaa Prep DatcMIro fs3 Anglysis DatefT-lV3e(s1 EPA 1664B EPA 16640 03/11/19 02/20/19 10:37 02/21/19 14:40 SM 2540o-2011 NO PREP 02/18/19 02/14/19 16:15 02/14/19 16:15 SM 5220D-2011 Same 03/11/19 02/14/19 10:10 02/14/19 14:30 Client ID: SW02 Lab ID: CCO2164.02 Sampled: 02/11/19 11:45 Received: 02/11/19 12:13 Parameter Preparation Hold Data/Timefs} - Date/Trmefs] Analvsls Date/Time(s) EPA 166413 EPA 1664E 03/11/19 02/20/19 10:37 02/21/19 14:40 SM 254OD-2011 NO PREP 02V18/19 02/14/19 16:15 02/14/19 16:15 SM 522UD-2011 Same 03/11/19 02/14/19 10:10 02/14/19 14:30 lientID: SW01 Roof Downspout Lab ID: CCO2164-03 Sampled: 02/11/19 11:20 Received: 02/11/19 12.13 Parameter SM 522OD-2011 Preparation Same 03/11/19 Prep Date/Timefs] 02/14/19 10:10 Analysis Date/Tlmefsl 02114/19 14:30 (7ientID: SW IFtoofUpsteam Lab ID: CCO2164-04 Sampled: 02/11/19 13:50 Received: 02/11/19 12:13 Parameter Preparation Hold DatelTime(sl Prep Date/Time[s� Analysis DatelTFmefsl SM 522OD-2011 Same 03/11/19 02/14/19 10:10 02/14/19 14:30 FINAL This report motes only m the sanpre as mcdved by the laboratxy, and may ony be reproduced In fill. Page 2 of 8 www.encotabs.com SAMPLE DETECRON SUMMARY Client In: SW01 Lab 11): CCO216"1 An_a4 Chemical Oxygen Demand Oil & Grease (HEM) Total Suspended Solids Results BAR ma EQL 54 10 10 1.89 3 1.50 5.00 32 7.6 7.6 MD& Method Notes mg/L SM 522OD-2011 mg/L EPA 1664E mg/L SM 254OD-2011 Client ID: SW02 Lab ID: CCO2164-02 Ana Hag MDL Em Natm Chemical Oxygen Demand 28 10 10 mg1L SM 522OD-2011 Total Suspended Solids 4.8 4.2 4.2 mg/L SM 254OD-2011 Client ID: SW01 Roof Downspout lab ID: C002164-03 AI10I1d0 Results Plan MM PRL UntNs Method Notes Chemical Oxygen Demand 52 10 10 mg/L SM 5220D-2011 Client ID: SW01 Roof Upstream Lab ID: COD2164-04 AOa Results 11g Na Ea Units mcftd Notes Chemical Oxygen Demand 180 10 10 mg/L SM 5220D-2011 FINAL This report relates only to the sample as received by the labmatmy, and may only be reproduced in fup. Page 3 of 8 www.encolabs.com ANALYTICAL RESULTS Description: SWOT Lab Sample ID:CCO2164-01 Received: 02/11/19 12:13 Matrix: Surface Water Sampled:02/11/19 11:35 Work Order: CCO2164 Project: Stormwater CAS Sampled By: Haley Randolph assical Chemistry Parameters Analyte rC4S Number] Results !bg Units [IE FJL EQL Batch MCM0 Analyzed By Emotes Chemical Oxygen Demand- 54 mg/L 1 10 10 9B14004 SM 522OD-2011 02/14/19 14:30 JOC Total Suspended Solids- 32 mg/L 3.03 7.6 7.6 9814010 SM 2540D-2011 02/14/19 16:15 ASC assical Chemistry Parameters ^-ENCOaaot,,ry C*J#Waaaty�[NC 4421 Anahrte rCAS Numberl Results Elin V171ri 2E MU ML 110= Method wed fk= Oil & Grease (HEM) [C-0007]^ 1.89 l mg/L 1 1.50 5.ou 9132OW7 EPA 16648 02/21/19 14:40 SMA Description: SW02 Lab Sample ID:CCO2164-02 Received: 02/11/19 12:13 Matrix: Surface Water Sampled: 02/11/19 11:45 Work Order: CCO2164 Project: Stormwater CAS Sampled By:Haley Randolph assical Chemistry Parameters Anahrbe rCAS Numbers Results 099 Units PE KU ML Batch Method Ana AX Notes Chemical Oxygen Demand^ 28 mg/L 1 10 to 9B14004 SM 5220D-2011 02/14/19 14:30 3OC Total Suspended Solids^ 4.8 mg/L 1.67 4.2 4.2 9014010 SM 254OD-2011 02/14/19 16:15 AK assical Chemistry Parameters ^ - ENCO.Iacbo Ve CfftbW aralytr (NC 4421 Anahrte rCAS Numberl Results lIM Units )f mal. pQj Alkh Mtn Anahmed @y Nstt� Oil & Crease (HEM) [C-0007]^ c 1.50 mg/L 1 1.50 5.00 9620007 EPA 16646 02/21/19 14:40 SMA Description: SW01 Roof Downspout Lab Sample ID:CCO2164-03 Received: 02/11/19 12:13 Matrix: Surface Water Sampled: 02/11/19 11:20 Work Order: CCO2164 Project, Stormwater CAS Sampled By: Haley Randolph assical Chemistry Parameters ^ - ENCO Carr ceti W w aW (NC 591) Ahrhe KAS Numberl Results an y„I&g 2E MU EM 51=11 Meths Ana RX notes Chemical Oxygen Demand^ 52 mg/L 1 10 10 9814004 SM 522OD-2011 02/14/19 14:30 30C Description: SW01 Roof Upstream Lab Sample ID:CCO2164-04 Received: 02/11/19 12i13 Matrix: Surface Water Sampled:02111/19 13:50 Work Order: CCO2164 Project: Stormwater CAS Sampled By: Haley Randolph assical Chemistry Parameters ^ - ENCO CaryC&br9l analytePVC 5911 13essllit 1a Mau 2E 11" E21 Batrh Mtn AnabUmd Ax Notes Chemical Oxygen Demand^ 180 mg/L 1 10 10 9814004 SM 522OD-2011 02/14/19 14:3D 30C FINAL This report relates only to the sampk as receivW by the laboratory, and may o* be reproduced is fill. Page 4 of 8 www.enoDiabs.com QUALITY CONTROL DATA ssical Chemistry Parameters - Quality Control Batch 9814004 - .Same Blank (9B14004-BLKI) Prepared: 02/14/2019 10:10 Analyzed: 02/14/2019 14:30 Spike Source %REC RPD 9Qaltde Resu IL Elan PQL Units Level gas ', %FLEC wMits RPD Limit Notes_ Chemical Oxygen Demand 10 U 10 mg/L LCS (9B14W4-BS1) Prepared: OV1412019 10:10 Analyzed: 02/14/2019 14:30 Spike Source WORK RPD AnalYte Resu IL Ella P91 Units Level RCiult %REC Urrift RPD lima NQbas Chemical Oxygen Demand 430 10 mg/L 500 95 90.110 Matrix Spike (9614004-MS3) Prepared: 02/14/2019 10:10 Analyzed: 02/14/2019 14:30 Source: CB17023-01 Spike Source 4/9REC RPD ArWvte Resin[ Elm 241. unLtx Level Resuh %REC Limits RPD iftnA n2= Chemical Oxygen Demand 540 10 mg/L 526 34 96 90-110 Matrix Spike Dup (9B14004-MSDI) Prepared: 02/14/2019 10:10 Analyzed: 02/14/2019 14:30 Source: C017023-01 Spike Source %REC RPD Ana11tSE Resu Elm MI. uelts Level Rem %REC Limits RPD iL ems' Nggg Chemical Oxygen Demand 550 10 mg/L 526 34 98 90-110 2 10 Batch 9814010 - NO PREP Blank (9B34010-BLK1) Prepared B Analyzed: 02/14/2019 16:15 Spike Source %REC RPD Analyte Resu Elm MI. units Level RC51rit %REC Limits RPD Limit pis"s Total Suspended Solids 2.5 U 2.5 mg/L LC5 (9814010-BSI) Prepared &Analyzed: 02/14/2019 16:15 Spike Source %REC RPD Anal rte Result ELaR RQL Un1Ys Level Resu t %REC )lift RPD 1laft Natm Total Suspended Solids 100 2.5 mg/L 100 too 80-120 Duplicate (9B14010-DUPI) Prepared & Analyzed: 02/14/2019 16:15 Source CCD0102-01 Spike Source 9roREC RPD Anal Y1& Besuit ELM E!QL Units Level Resu 0i6REC Limits RPD Limit Rots Total Suspended Solids 110 25 mg/L 110 2 20 Duplicate (9514010-DUP2) Prepared & Analyzed: 02/14/2019 16:15 Source: CCO0139-01 Spike Source %REC RPD Anallde Rmsult ELM ffi. Units Level Res %REC Limits RPD Lu11it Bobas Total Suspended Solids 140 100 mg/L 170 18 20 k1assical Chemistry Parameters - Quality Control Batch 9520MI - EPA 1664E Blank (9B20007-BLKI) Prepared: 02/20/2019 10:37 Analyzed: 02/21/2019 14:40 Analyte Oil & Grease (HEM) Spike Source %REC RPD Be&& Elm P91 Units Level Resuft %REC Limb RPD jj@g 1.50 U 5.00 mg/L FINAL This report relates only tD the sample as received by the Laboratory, and may onh' be reproduced in full. Page 5 of a www.eocolabs.com 11 QUALITY CONTROL DATA ssical Chemistry Parameters - Quality Control Batdb 9520907 - EPA 1664E - Confinmed LCS (9820007-11SI) Prepared: 02/20/2019 10:37 Analyzed: 02/21/2019 14:40 Spike Source %REC RPD Analft Result f1m E" Units Level Res %REC 'omits RPD Limit Notes Oil & Grease (HEM) 144 5.00 mg/L 161 89 78-114 LCS Dup (91120007-11SD1) Prepared: 02/20/2019 10:37 Analyzed: 02/21/2019 14:40 Spike Source %REC RPD Analviz Resin Ela9 ML Units Level Resu 0/@REC Limits RPD Limit Mom Oil & Grease (HEM) 127 5.00 mg/t 154 82 78-114 12 18 Matrix Spike (91320007-MSL) Prepared: 02/20/2019 10:37 Analyzed: 02/21/2019 14:40 Source: BM697-01 ImIRft i Oil & Grease (HEM) Spike Source %REC Reau flora P9L Units Level Resuk %REC Limits RPD 202 5.00 mg/L 165 20.0 110 78-114 RPD LLMA dotes_ FINAL This report relates cx* tD the sample as reoeved by the laboratory, and may only be reproduced m full, Page 6 of 8 www.encolabs.com 11 FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank, D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. Mi2L Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL, N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. (CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. FINAL This report relates ordy to the sample as received by the laboraiwy, and may o* be nepndumd in M. Page 7 of 8 h.+••u.vr+nryr•rr•r. Vvr�wy�. trr7r rYrr• rnMYrrrnr vrrrr�r vlrgp• yr MVMryMr rr4vvrslrr ee et YY�Q/ItrV/YMJtr�V/1/ 10115 Central l+Qrt Ur, 4810 f ecullva nark U1.011, 61,141111111 102•A Woodwinds Induetrlat CI, 00onno, H. =124 JacksorWllle, FL 327104Mg Cary, NC 27511 CA) (401) 0805314 Fox 007) n5n,0g45 (M) 2n0.0067 Fox (004) 2W,0210 (019) 467.3000 Pex (414) 467,3516 Page Comm Nnhi (' }ry/ (VI. Address �^ �/' ' ,t I � 1 �,.yA pU CNyf$Trlip - r 'i7T� T•J►//- ,... ff / ____i C" �Z� �Q� Tel Pax LI f) y �— Proloct �1unlaor I 1 H uested Ane aes oquoctod turnaround TImos Na1e I l;U4h (epUesak /ubJgtl to "woptnmen by 1ha faclltty — Standard _ Expoditod DUO �+ 777Prose 1,101 t 4 emel0esc r5 �� �•y PO 011.114iinng Into J lev.—Om Heperling Conlacr u 14A �, ,�".' k� r1111irgt Contact II„ �xlY 9,10 Location, Tfine Zona I '•�/ftj/ SampWrfa) N qQ)mn, Pmlirriwn rant � _ J (l,►,rj� �? samplor(s) s,wo m --/ - Lobt WOrkordnr � allon t8co Codas Camb{no nit nomilia items A Baas{ n 11, W.Ia d rrlanlilw0on) CnifeCtien Date jj Cvllnclion Tine Comp Grab Meldx (goo codes► Val s of a Cenlelrlert - gate 10 Comments <•• Total N of Contalnoro Sempio M P're{iareif {ly Gemmel tntspecini 1p{rsnung Flegnir3mn to Hegngi sued fly nntin�uishad 11r / nnto/tlms Pocal y ad y nt imn pnfrrlrlmn Fialirnluir:had Hy Oe1n/Tlmn r flaesivad ay pnfalTlmn Cooler b'e A tar"ps 604oceipi Conditlort U mocelpi Acco labla unacca taut- Mrilthbi aw-afamsawafr,r 00,4011 pyy ,irihirig Wafpr 611-Gadtrn901 DW-9 riots Writer Wyy.Wontowaler A•Air 0,01hor0e1101 In cammontsl Preserwallon: race H44C1 N-HNO3 &H2804 NO•NaOH 0.0ther (dololl In comments) We � All aempleo submitted to CNCO Labe are In aeeordsnca vAth Iho Isms and condillans lAted on Ihs reverie of Ihis form, unless prior wrllten agreements exisl Via Certified Mail October 18, 2018 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 REOFIVED NOV 2 0 2018 CENTRAL FILES DWR SECTION Re: Reporting Year 2018 — Storm Water Discharge Monitoring Report Kellogg's Snacks — Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the October 2018 monitoring event for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Rodney Bateman (919) 677-3348 rodney.bateman@kellogg.com Mr. Bateman is available should any questions or problems arise during the review of this DMR. SRAM -Muter Pmjec W-5Dgg\KEL011 Cary 2G1H S10rnrwater10dober 2018 Event\Storalwater Cover letter 20181019.doc DWQ — Central Files October 18, 2018 Page 2 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. i am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, Steve Surovec Plant Manager Enclosures S4AAA-Master Projects\KelbggWEL-01 I Cary 2018\Swrmwatar Onaber 2018 EverttlStornnwiter Cover letter 2018101 B,dnc SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted _October 18, 2018 CERTIFICATE OF COVERAGE NO. NCGO60286_ _ _ _ SAMPLE COLLECTION YEAR 2018 FACILITY NAME —Kellogg Company — Cary, NC Facility FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Wake ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Gregory Kanellis DISCHARGING TO SALTWATERS? ❑YES ®NO LABORATORY ENCO Labs Lab Cert. 8 591 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Result Total event rainfall 10.1 in (10106118) or ❑ No discharge this period' y Outfall No. aSample:Collected, ' mo/dd/yr TSS, mg/L pH, Standard:units COD,• mg/L Oil and Grease, mg/L Fecal Coliform1; Colonies per 100 ml Enterococcil, Colonies per 100,ml Benchmark _ : - . •.. 100 or 504. Within 6.6 - 9.0 120 30 1000 500 SW01 10/06/18 20 6.37 390 <1.50 NA NA SW02 10/06/18 7.3 6.42 77 1.55) NA NA 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at ate, outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ®no (ifyes, complete Part B) Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. :Outfall No. Sample Collected, m6/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual average gal/mo Benchmark. - 30 100 or 504. 6.0 — 9.0 - 1 Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 45ee General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: * A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: Thad Valentine Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results !or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 01 ! l� (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wa/ws/su/npdessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 Sample, Preservation Verification OEM ENCQ Cary Work Order: CB10447 Project: Stormwater (Jan,July) Client: KELLOGGS SNACKSIAUSTIN FOODS (KE006) Project #: [none] Logged In: 08-Oct-18 09:51 I Logged By: Rachel Ann Yo is{h/ c' Preservation Check Performed By: ! Date/Time: 0� s l i �5 - CB10447-01 Cqn hype Press Fly g Hequwerrient p,,CheGc In•Contro wPH Ad1usted;q<��ate<Tme a � r. Adjusted men R gentUsedlGtss t ;^ B 250mLA+H2SO4 <2 Y/ N.NA Y I N! A C 250mLA+H2SO4 <2 Y ! N / NA Y ! N ! NA D 250mLP+H2SO4 <2 Y) N I NA Y N NA C B 10447-02 Conti T ' Fres (pH) PHICheecckeed l �� DateRme - ed'Reagent se s� , f,. Req�irernent In ControE�u„p'AiitustedAdju is B 250mLA+H2SO4 �Q Y! N/ NA Y/ N 1 NA C ' 250mLA+H2SO4 �Q Y ! N / NA Y I N / NA D 250mLP+H2SO4 <2 i YJ! N / NA Y N / NA Reagent Name ID _1 2 pH Strip ID: PH Strips C710820 C:lelmntlPrint\wxo r- reservduunt.,i it:u r..i pt Rea ent Name ID 3 4 Readent Name ID 5 6 - Page 1 of 1 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN-OP-CUSTftY RECORD www.encolabs.com C� 10776 Central Port Dr. 4810 Execotiae Park Court, Suite 111 102•A Woodwinds Industrial Ct. Odanda, FL 32824 Jacksonville, FL 32216-6069 Cary, NC 27511. (407) 82&6314 Fax (4b7) 8%6945 (904) 2W3007 Fax (904) 296.6210 (919) 467.3090 Fax (919) 467.3515 Page Of Client Name KELLOGGS SNACKWAUSTIN FOODS (KEQOB) Proled Number [none) Requested Analyses Requested Turnaround Times Note : Rush requests subjoM to aieeptancobythe tacillty 4F Expedited Due o CV � 0 O m L�f 08 a o--le/Standard c rn CO ~ Address ONE QUALITY LANE Project NamaMasc r Stormwater (Jah,July) City1STMp. CARY, NG 27513- PO 41 Billing Into Tel (9,19) 677-3519 TO Reporting Contact Rodney Bateman Sampler(s) Niimo. A91Elatlon (Print) } Billin Contact Accounts Payable Sampler(e) Signature Sita Location/ Time Zono Lab Workorder GB 10447 Preservation (Son Codosj (Combing as nocpssary) Item M Sample it)If=laid fdantilicalion) Collection Date Collection - �Tima Comp / Gmb Matrix (sae codes,) ' 7a1a1 op of Containers Sample Comments sv't) lo' 6' r Lj?;o G, sW 4' X X X Swop. la 1� y 1S G Sw 4 X x X r . i i. r <--Total # of Containers sample Iri red By jDaleMme a110'AG 1 Relinquished By Datamme FI9car ByV `D W 1V A un Ck 1. 4+1 Commons epoftft Requirements Ralinquish By DeteJTme Received By Dale/rune Relinquished By Datefnme Received By DalwTune rooloro's E m s on Receipl O� Condition Upon Receipt "'� 3 V�Acce ta61e _ Unacceptable Matrix:OW-Groundwater SO -Soil DW-Drinking Water SE•Sedimenl OW -Surface Water WW-Wnsliwaler A•Air 0.0ther (detail in comments) Preservation: I -Ice H.HCI N-HNO3 S•H2SO4 NO•Na0H O.Other (detail In comments) Note; Athsarriplas submitted to ENCO Labs are In accordance with the terms and condtions listed on the reverse of this term, unless prior written agreements exist 000 www.encolabs.com FLAGS/NOTES AND DEFINITIONS iB The analyte was detected in the associated method blank. D The sample was analyzed at dilution. 7 The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates OF* to the sample as received by the labond , and may only be rePmduoad in rub. Page 7 of 8 CS0 www.enculabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Bahah BJ11017 - EPA 1664B - Conl7nued LCS (8711017-651) Prepared: 10/11/2018 17:38 Analyzed: 10/16/2018 16:23 Spike Source %REC RPD Ana htlg wit 039 ML Wks Level ill! %REC Limits RPD UMA Notes Oil & Grease (HEM) 139 5.00 mg/L 160 87 78-114 !CS Dup (8J31017-BSDI) Prepared: 10/11/2018 17:38 Arteiyzed: 10/16/2018 16:23 Spike Source %REC RPD Anahrte RCMU Elm POL Unib Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 140 5.00 mg/L 160 87 78-114 0.6 18 Matrix Spike (8711017-MSI) Prepared: 10/11/2018 17:38 Analyzed: 10/16/2018 16:23 Source: B604497-07 Spike Source %REC RPD Anal rte Result Rao PPQL Units Level Re %REC Limits RPD Limit Notes Oil & Grease (HEM) 144 5.00 mg/L 160 3.11 138 78-114 FINAL This report relatm only to the sem* as received by the laboratory, and may wy be reproduced in U. Page 5 of 8 www.encelabsl.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Bauch SJIIO17 - NO PREP Blank (8111017-BLKS) Prepared & Analyzed: 10/11/2018 11:27 Spike Source %REC RPD .90alift Rem& Hag 1201. Units Level Rik %REC Limi RPD LIMA Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (8]11017-BS1) Prepared S:Analyzed: 10/11/2018 11:27 Spike Source WORK RPD Anal Result Elm P.41 units Level %REC Limits RPD u1nit Notes Total Suspended Solids 100 2.5 mg/L 100 104 80-120 Duplicate (8311017-DU123) Prepared & Analyzed: 10/11/2018 11:27 Source:CB13786-07 Spike Source o/uREC RPD Af3a Result fin RQL Units Level Result %REC Ur"iRPD Limit Notes Total Suspended Solids 230 25 mg/L 240 4 20 Duplicate (8111017-DUP2) Prepared & Analyzed: 10/11/2018 1127 Source: CB13796-08 AAa� Total Suspended Solids 8a" 8J120OS - Same ICII 021 ilq 210 25 Spike Source %REC RPD Units Level Res %REC LIMA A RPD 11:111ft Notes mg/L 210 2 20 Blank (8312005-BLK1) Prepared: 10/12/2018 11:2x Analyzed: 10/12/2018 15:25 Spike Source %REC RPD Anal Result gas M1 ikdts Level Result %REC LFMIts RPD Li14(t Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (8]12005-BS1) Prepared: 10/12/2018 11:27 Analyzed: 10/12/2018 15:25 Spike Source %REC RPD ADDivle Resul Has FOL Units Level Result %REC Limits RPD Lima Motes Chemical Oxygen Demand 480 10 mg/L 500 97 90.110 Matrix Spike (8312005-MSI) Prepared: 10/12/2018 11:27 Analyzed: 10/12/2018 15:25 Source: CR07177-01 Spike Source %REC RPD Alzatf[ta Result Ball M Unite Level R=d %REC Limits RPD Limit Notes Chemical Oxygen Demand 670 10 mg/L 526 170 96 90-110 Matrix Spike Dup (8]120 S-MSDI) Prepared: 10/12/2018 11:27 Analyzed: 10/12/2018 15:25 Source: CB07177-01 Spike Source %REC RPD Ana 6ttg Result Elm P91. units Level Result %REC Limits RPD Limit Ngw Chemical Oxygen Demand 700 10 mg/L 526 170 101 90-110 3 10 Classical Chemistry Parameters - Quality Control $af* 8J11017 - EPA 1664E Blank (8111017-BLK1) Prepared: 10111/2018 17:38 Analyzed: iD/1612018 16:73 Spike Source %REC RPD Aria hds Ruud Ban FU Units Level ReW %REC Limits RPD Lllait lY+i o Oil & G(HEM) 1.50 U 5.00 mg/L FINAL This report mates only to the sampie as received by the laboratory, and may only be reproduced in lull. Page 5 of 8 www.encolabs.com ANALYTICAL RESULTS Description: SW01 Lab Sample ID:CB10447-01 Received: 10/08/18 09:01 Matrix: Surface Water Sampled:10/06118 14:30 Work Order: CB10447 Project: Stormwater (Jan,July) Sampled By: Greg Kanellis Chemistry Parameters ^ - swo cwy C"&d arralyte [AC 5911 . Analyte FCAS Numberl Results fia9 units 2f MOL -PQL- B t ti Method Anafrzed 91 Not se Chemical Oxygen Demand^ 390 mg/L 1 10 10 8112005 SM 522OD-2011 10/12/18 15:25 ]OC Total Suspended Solids^ 20 mg/L 7.69 19 19 SJ11017 SM 254OD-2011 10/11/18 11:27 OMR Classical Chemistry Parameters ^ - &KC-Lelcstnrille catfied analyte[AC 4421 Analrte FCAS Number] Resin .4 fiat units PE MDL IL Babcli Method AnalvAed gy Oil & Grease (HEM) [C-M7]^ < 1.50 m9/L 1 1.50 5.00 8J11017 EPA 1664E 10/16/18 16:23 SMA Description., SW02 Lab Sample ID:CB10447-02 Received: 10/08/18 09:01 Matrix: Surface Water Sampled:l0/06118 14:15 Work Order: [810447 Project: Stormwater (Jan,July) Sampled By: Greg Kanel[is lClassical Chemistry Parameters ^ - SKV C-Y C"A d analyw [MC 5911 Analyte fQW Numberl Bnul EIim RJR& PE NU MIL Btom meow Aria ft Notes Chemical Oxygen Demand^ 77 mg/L 1 10 10 8312005 SM 522OD-2011 10/12/18 15:25 JOC Total Suspended Solids^ 7.3 mg/L 1.43 3.6 3.6 8111017 SM 2540D-2011 10/11/18 11:27 OMR Classical Chemistry Parameters ^ - 9 C'O Jacicscvrwlle o"Agd anafyte [AC 4421 &WIM FCAS Number! Resul fide Units RE KU EU Batch MUM Anal1nd ft (Votes oil At Grease (HEM) [C-D007]^ 1.55 3 mg/L 1 1.50 5.00 8311017 EPA 1664B 10/16/18 16:23 SMA FINAL This report rdates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 8 �uco www.encolabs.com SAMPLE DETECTION SUMMARY alern ID: swot Lab ID: CS1o447-01 Areal tte Resul 909 iu R" maid Homo l= Chemical Oxygen Demand 390 10 10 mg/L SM 522OD-2011 Total Suspended Solids 20 19 19 mg/L SM 254OD-2011 plant ID; Sw02 Lab 1D; Cs10447-02 Anall Besultf El49 "a E9L uniu MeaW N0tm Chemical Oxygen Demand 77 10 10 mg/L SM 522OD-2011 Oil & Grease (HEM) 1.55 ] 1.50 5.00 mg/L EPA 16640 Total Suspended Solids 7.3 3.6 3.6 mg/L SM 254OD-2011 FINAL This report relates only to the sample as. ecem by the Iaboimtory, and may only be reproduced in fu 1. Page 3 of 8 9�eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE clientID: SW01 Lab ID: CB10447-01 Sampled: 10/06/18 14:30 Received: 10/08/18 09:01 Parameter Preparation Bold Date/TlmefsA Prep Date/Timefs) Analvsls DateITimefsl EPA 1664E EPA 1664B 11/03/18 10/11/18 17:38 10/16/18 16:23 SM 254OD-2011 NO PREP 10/13/18 10/11/18 11:27 10/11/18 11:27 SM 522OD-2011 Same 11/03/18 10/12/18 11:27 10/12/18 15:25 client ID: SW02 Lab ID: C1510447-02 Sampled: 10/06/18 14:15 Received: 10/08/18 09.01 ftrame ft=arau4m ld - oamefs) Pro RWathmefs) 19w EPA 16648 EPA 1664E 11/03/18 10/11/18 17:38 10/16/18 16:23 SM 254OD-2011 NO PREP 10/13/18 10/11/18 11:27 10/11/18 11:27 SM 522OD-2011 Same 11/03/18 10/12/18 11:27 10/12/18 15:25 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Tull. Page 2 of 8 kENCO Laboraton"es Accurate. Timely. Responsive. Innovative. 102-A woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, October 17, 2018 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (]an,]uly) ENCO Workorder(s): CB10447 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, October 8, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) F WL This report relates only to the sample as received by tre laboratory, and may only be reproduced In lull. Pape 1 of 8 Date: 10/612018 Analyst: G. Kanellis Certification # 5356 Facility Name: Hart & Hickman, PC Permit #: _NCC060000 pH Analysis Reference Nfethnd- CM 4500 H+P-20M finrlude vearr4_ SM 4gM-H+ R-20MI Cal. Time Calibration Buffer 4.0 Calibration Buffer 10.0 `Check Buffer 7.0 Comments 1400 4.0 10.0 7.0 Passed *pH buffer checks are to be within f QI pH units of the standards true value. 4 buffer LoWidentifier: 7 buffer LotWidentifier: 10 buffer LoWidentifier: Facility/Sample location Sample Collection Time* Sample Analysis Time • pH Result ► Buffer Check value CommentsData Qualifiers SW01 1430 1430 6.37 7.0 SW02 1415 1415 6.42 TO ♦If sample is measured directly in the stream and/or on site. one time may be recorded for collection and analysis with the notation that they are measured in situ or at the immediately at the sample site. ► Calibration drift check is required when performing analyses at multiple sampling locations. (Use Buffer 7.0) Should be within f 0.1 units of the buffer's true Value) *All pH results in pH units (i e., s.u.). Report all data values to the nearest QI pH unit. Annual Temperature Sensor Check Date: M/2018 pH Instrument ID: _Myron L Company Ultrameter If GPFC serial M 6232585 Field Personnel Notes/Equipment Maintenance 10102f2013 Via Certified Mail April 12, 2018 PkPePi\JD AVR 19 2018 CENRAL FILES DWR SECTION Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: Reporting Year 2018 — Storm Water Discharge Monitoring Report Kellogg's Snacks — Cary Bakery One Quality Lane Cary. North Carolina Dear Sir/Madam, f• SNACKS Cary Bak° 1 Opera7<.ra Ore OuaY.y Lan Oay. NC 27553 Ph 919 5713200 Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the March 2018 monitoring event for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Anthony DePietro (919) 677-3292 anthony.depietro cr,kel to g.com Mr. DePietro is available should any questions or problems arise during the review of this DMR. S `AiAALl Ier ProjectsNKello4KEL-01 I Cep 2018'Stor AeO.%Iarch 2018 Exmt'Storm ester Coves Imer 20180412 doc DWQ — Central Files April 12, 2018 Page 2 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information. the information submitted is, to the best of my knowledge and belief; true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, Steve Surovec Plant Manager Enclosures S V%AA-\faster Projeas}KeilogjkEL-011 Can 2019'Stormxwe'M. ch 2m Eve rStorm ater Cofer letter 20180412 &c SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted _April 16, 2018 CERTIFICATE OF COVERAGE NO. NCG060286_ — — T SAMPLE COLLECTION YEAR �2018 FACILITY NAME -Kellogg Company - Cary, NC Facility FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Wake ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Gregory Kanellis DISCHARGING TO SALTWATERS? [-]YES ®NO LABORATORY ENCO Labs Lab Cert. # 591 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Result Total event rainfall 1 0.09 in (02107118) or U No discharge this period' �Autfali,Na:Sample;Collected, TSSI. pH, CODOIFFecai:Coliformnnteracoccil, Standard` mo/dd/yr, mg/L; units .mg/L 3.mg/L %. :Colonies per.:100 m1 ;Colonies•per:100 m1` ;BenharkA 0cWithin:6.0=.0 120.30 1000r500' SW01 03/06/18 68 6.44 21 <2.40 NA NA 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at Any outfalls. You must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no (if yes, complete Part B) Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. TSS, H, :;,New Motor.'OII,Llsa e;,: Ou.tfall No tSamplo,Collected, P g Qil,and Grease, 4h , /ddLYr mg/L :. m L, . Standard unifs4 Annual average gal/ma Benchmark'° - 30 l00 or 50° 6 0`•9.0,.: ," 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. SWU-244 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Thad Valentine Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of recei t of the lab results or at end o monitoring period in the case of ""No Discharge" reports to. Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature ofPermittee) lL (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wg/ws/`su/`npdessw#tab-4 5 W U-249 Last Revised: October 18, 2012 Page 2 of Certification # 5356 Date: 3/612018 Analyst: G. Kanellis Facility Name: Hart & Hickman, Permit # NCGO60000 pll Analysis Reference ►lethualr C%f 4-M H+IL2000 (include year e.g.. C\S 4S(t H+ B-2(0111 Cal. Time Calibration Buffer 4.0 Calibration Buffer 10.0 *Check Buffer 7.0 Comments 1330 4.O 10.0 7.0 Passed *pH buffer checks are to be n ithin t 0.1 pH units of the standards true value. 4 buffer LoWidentifrer: 7 buffer Lot#/identifier: 10 buffer Luthlidentifier: FacilityiSample location Sample Collection Time* Sample Analysis Time* pH Result ► Buffer Check value Comments+Data Qualifiers S1rw'Oi 1415 1415 6A4 7.0 • If sample is measured directly in the stream and/or on site, one time may be recorded for collection and analysis n ith the notation that they are measured in situ or at the immediately at the sample site. ► Calibration drift check is required when performing analyses at multiple sampling locations. (Use Buffer 7.0) Should be nithin t 0.1 units of the buffer's true value) *All pH results in pH units (i.e., s.u.). Report all data values to the nearest 0.1 pH unit. Annual Temperature Sensor Check Date: 611412017 pll Instrument ID: _Myron 1. Company Ultrameter 11 GPFCE serial #: 6232585 Field Personnel NoteslEquipment Maintenance 10'02 CM 21641 ENCO Laborato ries Accurate. Timely. .Responsive, Innovative. 102-A woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, March 19, 2018 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE. Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (]an,7uly) ENCO Workorder(s): CB03172 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, March 6, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, (LL-. C�-A Chuck Smith Project Manager Enclosure(s) F3NAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 8 w w www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE client ID: SW01 Lab ID: 0003172-01 Sampled: 03/06/18 14:15 Received: 03/06/18 15:15 parameter Preparation Hold 4atcMme(s) Preu Date/Time[si Analysis Date/Time(s) EPA 1664E EPA 1664E 04/03/18 03/14/1B 12:00 03/16/18 11:36 SM 254OD-1997 NO PREP 03/13/18 03/12/18 10:44 03/12/18 10:44 SM 522OD-1997 Same 04/03/18 03/12/18 12:21 03/12/18 15:06 FINAL This report relates only to the sample as received by the laboratory, and may only, be reproduced in full. Page 2 of 8 Ce VCO www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: SWOS tab Ip: C803172-01 AnalM Results FFl- MDL eQl units Met od Nnt _s Chemical Oxygen Demand Total Suspended Solids 21 68 mg/L SM 522OD-1997 mg/L SM 2540D-1997 FINAL This report relates only to the sample a5 received i7y the laboratory, and may only be reproduced in full. Page 3 of 8 00) �u www.encolabs.com ANALYTICAL RESULTS Description: SW01 Lab Sample ID:CB03172-01 Received: 03/06/18 15:15 Matrix: Surface Water Sampled:03/06118 14:15 Work Order: CB03172 Project: Stormwater (Jan,)uly) Sampled By: Greg Kanellis Chemistry Parameters ^ - ENCO Cary certdmd anaVe CNC 5911 Analyte rCAS Numberl Results Flag units DF MDL POLL AgE- Method nal ed By Not Chemical Oxygen Demand, 21 mg/L 1 10 10 8C12006 SM 522OD-1997 03/12/18 15:06 10C Total Suspended Solids^ 6$ mg/L 5 12 12 8CO9023 SM 254OD-1997 03/12/18 10:44 MKS Classical Chemistry Parameters ^ - ENCO Jaoksmn7le certified analyze [NC 442) Analvte rCAS Numberl Itesill BM Units ¢F MPL pa etch Method Analyzed gj[ Note Oil & Grease (HEM) [C-0007]^ c 2.40 mg/L 1 2.40 5.00 BC13007 EPA 16648 03/16/18 11:36 SMA FINAL This report relates only to the sample as received try the:aWratory, and may only be reproduced in lull- Page 4 of 8 ��Go www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 8C09023 - NO PREP Blank (8C09023-BLKL) Prepared & Analyzed: 03/12/2018 10:44 Spike Source %REC RPD Ar3alyt9 Res1Zt H-M PQL Units Level Result a/aREC Limits RPD _ Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (SC09023-BSI) Prepared & Analyzed: 03/12/2018 10:44 Spike Source %REC RPD .Lnatyte ReWlt Elar3 POL Units Level Result %REC LimijA RPD Limit Notes Total Suspended Solids 95 2.5 mg/L 100 95 80-120 Duplicate (SC09023-DUPl) Prepared & Analyzed: 03/12/2018 10:44 Source:CA,15909-01 Spike Source %REC RPD Analrte Result Flak FQL Unit; Level Besut5 a/aREC Limits RPD Limit Notes Total Suspended Solids 200 100 mg/L 190 6 20 Duplicate (SC09023-DUP2) Prepared & Analyzed: 03/12/2018 10:44 Source: M0156-01 Spike Source %REC RPD Analyte Remelt Elan POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 43 33 mg/L 40 6 20 Batch 8C12006 - Same Blank (SC12006-BLKI) Prepared: 03/12/2018 12:21 Analyzed: 03/12/2018 15:06 Spike Source %REC RPD Anal vte Re5111i flag PQL Units Level Result %REC Urnita RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (SC12006-BSI) Prepared: 03/12/2018 12:21 Analyzed: 03/12/2018 15:06 Spike Source %REC RPD Anah3e Result Flag l!" Ulaits Level Result %REC Limits RPD Eimit Notes Chemical Oxygen Demand 500 10 mg/L S00 101 90-110 Matrix Spike (SC12006-MS1) Prepared: 03/12/2018 12:21 Analyzed: 03/12/2018 15-06 Source: C002160-02 Spike Source a/oREC RPD Anal Yte R€ ul E1419 P01 Units Level Result a/aREC Limits RPD Limit Notes Chemical Oxygen Demand 590 10 mg/L 526 59 100 90-110 Matrix Spike Dup (SC12006-MSDL) Prepared: 03/12/201B 12:21 Analyzed: 03/12/2019 15:06 Source: CB02160-02 Spike Source %REC RPD Analyte Result Elan POL Units Level Result a/aREC Limits RPD Limit Notes Chemical Oxygen Demand 590 10 mg/L 526 59 101 90-110 0.8 10 Classical Chemistry Parameters - Quality Control Batch SC13007 - EPA 1664B Blank (SC33007-BLKS) Prepared: 03/14/2018 12:00 Analyzed: 03/15/2018 17:32 Spike Source a/aREC RPD Ana Result FIm POL Units Level Result %REC yLyf 'tli RPD Urnit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may aNy be reproduced in full. Page 5 of 8 (��Go www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch SC13007 - EPA 16"S - Continued LCS (BC13007-BSI) Prepared: 03/14/2018 12:00 Analyzed: 03/15/2018 17:32 Spike Source CYoREC RPD A alyte Ruujt Elaq P91 WKS Level Result 0/6REC Lim! RPD i it Nglos Oil & Grease (HEM) 171 5.00 mg/L 161 106 78-114 LCS Dup (SC13007-8SD1) Prepared: 03/14/2018 12:00 Analyzed: 03/15/2018 17:32 Spike Source %REC RPD 1Analyte Result Ela9 ROL units Level RCIYI 9/oREC Limit& RPD UM4 Notes Oil & Grease (HEM) 183 5.00 mg/L 160 114 78-114 7 18 Matrix Spike (BC13007-MS1) Prepared: 03/14/2010 12:00 Analyzed: 03/15/2018 17:32 Source: 8801102-01 Spike Source %REC RPD [nalyte R-ew-t Flag PQL Units Level Result %REC Limits RPD Limit Notes Oil & Grease (HEM) 292 5.00 mg/L 156 54.3 152 78-114 QM-07 FINAL This report relates orgy to the Sample as received by the laboratory, and may only be reproduced in full. Page 6 of 8 �co www.enoDlabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank_ D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitabon Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to Uv sample as received by the laboratory, and may only be reproduced in full, Page 7 of 8 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com cerlike 5. I'IlIN!QWkII'i Pane I D Ti ONE C. �I-.,A�J FY i.ArJF; It lyi f4111,111 its Standard CAWY NC 2151Z.- r9i ff) 67 I n. A4',COL '11:.; Out! elf, :;R" I De l crI ICB03'.1,72 Uq-1 1,klm fill., I:IIII'Ijij1'.1dJ X 0�0 ',?I' j.q„Illn my JT.I 1114} '4 willw mill llr ..j A, Wl ltl"U:L' V. A,*rvr.q; hh,� 1, lIruIqc'%I1,lj Nil t (� \ 2� 2 ƒ: ) @2 (' /f &9 /« [ Uk2 � ..._ \$ . I k�e v / , f\ . . \ / / } \ \ f 2 T } ƒ . § \ \ \ G SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCGO60000 Date submitted _February 20, 2018 CERTIFICATE OF COVERAGE NO. NCGO60286_ _ _ _ SAMPLE COLLECTION YEAR _2018 FACILITY NAME _Kellogg Company — Cary, NC Facility FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Wake REM,seA s meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Gregory Kanellis DISCHARGING T SALTWATERS? ❑YES ®NO LABORATORY ENCO Labs Lab Cert. # 591 MAR 0 9 24 CCNT1ils+k-L EREMEMBER TO SIGN ON THE REVERSE 4 POIR s �(02 TI N Part A: Stormwater Benchmarks and Monitoring Result Total event rainfai 0.09 m07118) or ❑ No discharge this period' Outfalt No. SampleCollected, mo/,dd/yr . TSS, mg/L pH, Standard units COD, mg/L oil and Grease, mg/L Fecal Collform1, Colonies per 100 ml Enterococcil, Colonies per 100 ml Benchmark - 100 or 504 Within 6.0 — 9.0 <_ 120 30 1000 5o0 SW01 02/07/18 130 7.35 100 <2.40 NA NA sW02 02/07/19 13 7.62 29 <2.40 NA NA 1 Only applies to facilities that use/process meats, 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. "See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ®no (if g& complete Part B) Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Outfall No. Sample. Collected, mo%dd/yr. Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil.Usage, Annual average gal/mo Benchmark 30 100 or SW 6.0 — 9.0 - ' Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. °See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. SWU-249 Last Revised: October 18, 2012 Page I of 2 *FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Thad Valentine Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitorina period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 3 5` Z?- (Date) Additional copies of this form may be downloaded at: http://Portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 SWU-249 Last Revised: October 18, 2012 Page 2 of 2 Date: 2f711$ Analyst: _H. Randolph Certification # 5356 Facility Name: Hart & Hickman, PC Permit #: _NCG060000 PH Analysis Reference Method: SM 4500 H+P-2000 (include vear e.e.. SNI 45110-H+ R-20001 Cal. Time Calibration Buffer 4.0 Calibration Buffer 10.0 `Check Buffer 7.0 — Comments 1400 4.0 10.0 7.0 Passed *pH buffer checks are to be within t 0.1 pH units of the standards true value. 4 buffer LoWiidentifier: 7 buffer Lot#fidentifier: 10 buffer Lot#lidentifier: Facility/Sample location Sample Collection Time* Sample Analysis Time* pH Result 104 Buffer Check value Comments/Data Qualifiers SW01 1520 1520 7.35 7.0 S W02 1500 1500 7.62 7.0 ♦If sample is measured directly in the stream and/or on site, one time may be recorded for collection and analysis with the notation that they are measured in situ or at the immediately at the sample site. ► Calibration drift check is required when performing analyses at multiple sampling locations. (Use Buffer 7.0) Should be within f 0.1 units of the buffer's true value) `All pH results in pH units (i.e., s.u.). Report all data values to the nearest 0.1 pH unit Annual Ternperaiure Sensor Check Date: 6l14/2017 PH Instrument ID: _Myron L Company Ultrameter 11 GPFCE serial #: 6232_585 Field Personnel Notes/Equipment Maintenance 10/02/2013 (0 ENCO Laboraton'es Accurate. Timely. Responsive. Innovative. 102-A woodwinds industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, February 19, 2018 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (]an,]uly) ENCO Workorder(s): CA17001 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, February 7, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the Wboratory, and may only be reproduced In full. Page 1 of 8 Ce WS1 00) www.ertcolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE dientlD: SWOT Lab ID: CA17OO1-01 Sampled: 02/07/18 15:20 Received: 02/07/18 16:00 Parameter Preparation Hold Date/Time(s) F Analysis Date/rjmefs! EPA 1664B EPA 1664E 03/07/18 02/14/18 14:24 02/16/18 15:23 SM 2549D-1997 NO PREP 02/14/18 02/14/18 15,45 02/14/18 15:45 SM 522OD-1997 Same 03/07/18 02/09/18 10:13 02/09/18 15:00 Client ID: SW02 Lab ID: CA17001-02 Sampled: 02/07/18 15:00 ReceWed: 02/07/18 i6:00 Parameter Preparation Hold D=Mmdsl Prep DateMnWs] Analysis Date/Time(sl EPA 1664E EPA 1664B 03/07/18 02/14/18 14:24 02/16/18 1523 SM 254OD-1997 NO PREP 02/14/18 02/14/18 15:45 02/14/18 15:45 SM 522OD-1997 Same 03/07/18 02/09/18 10:13 02/09/18 15:00 RNAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. Page 2 of 8 FJVCO www.encolabs.com SAMPLE DETECTION SUMMARY dient it): SWOI Lab ID: CA17001-01 AnaWte Results Elm IWID6 E9-L- UnitsHeUMI Chemical Oxygen Demand 100 10 10 mg/L SM 52200-1997 Total Suspended Solids 130 36 36 mg/L SM 2540D-1997 Client ID: SW02 Lab ID: CA17001-02 Anahrte Results BM MDL PQL Notes Chemical Oxygen Demand 29 10 10 mg/L SM 5220D-1997 Total Suspended Solids 13 2.5 2.5 mg/L SM 2540D-1997 FlOL This report relates only to the sample as received by the laboratory, and may oily be reproduced In full. Page 3 of 8 r.11 ww G www.encolabs.com ANALYTICAL RESULTS Description: SWOT Lab Sample ID:CA17001-01 Received: 02/07/18 16:00 Matrix: Surface Water Sampled: 02/07/18 15:20 Work Order: CA17001 Project: Stormwater ()an,]uly) Sampled By: Haley Randolph Classical Chemistry Parameters ^ - ENCO Cary ar&W aw6 to Pvc 5911 Anahrte r AS Numberl ResultsI�qa Units RF MDL PL e3" Method Analyzed -By Notes Chemical Oxygen Demand^ 100 mg/L 1 10 10 SB09013 SM 522OD-1997 02/D9/18 15:00 30C Total Suspended Solids^ 130 mg/L 14.3 36 36 8B14D06 SM 254OD-1997 02/14/18 15:45 OMR Classical Chemistry Parameters ^ - EA11W Jack* nV7'* c—fied acolyte (NC --?] Anahft [CAS Ntgrtberl Resu Elm Units PF M L LQL Mg—h Method Anal Notes Oil & Grease (HEM) (C-0007j^ J < 2.40 mg/L 1 2.40 5.00 8B14010 EPA 1664E 02/16/18 15:23 SMA Description: SW02 Lab Sample ID:CA17001-02 Received: 02/07/18 16:00 Matrix: Surface Water Sampled: 02/07/18 15:00 Work Order: CA17001 Project: Stormwater (]an,luly) Sampled By: Haley Randolph Chemistry Parameters ^ - ENQ7 Cdly cetifJCd anafytC (NC 591] Anahrte FCAS Numberl Results fin YMAS Df MIL pit Batch Mgt Analyzed ft Note, Chemical Oxygen Demand^ 29 mg/L 1 10 10 8BO9013 SM 522OD-1997 02/09/1815:D0 30C Total Suspended Solids^ 13 mg/L 1 2.5 2.5 8814006 SM 254OD-1997 02/14/18 15:45 OMR Classical Chemistry Parameters ^ - EMU Awbunvd4v cavf ed a,wryfe [NC 442J Analyte rCAS Number] Results flog Units Rf MRL EQL —Ba1t Method Anah edz ft Notes oil & Grease (HEM) [C-0007j^ < 2.40 mg/L 1 2.40 5,00 8814010 EPA 1664B 02/16/18 15:23 SMA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 8 www.encolahs-Cam QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 9809013 - Same Blank (SB09013-BLKI) Prepared: 02/09/2018 10:13 Analyzed: 02/09/2018 15.00 Spike Source %REC RPD Anal vte Result Ela4 P-01. Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (8B09013-BSI) Prepared: 02/09/2018 10:13 Analyzed: 02/09/2018 15:00 Spike Source %REC RPD Ana h Result Flag IM Units Level Result %REC Limits RPD unit Notes Chemical Oxygen Demand 490 10 mg/L 500 98 90.110 Matrix Spike (BB09013-MS!) Prepared: 02/09/2018 10:13 Analyzed: 02/09/2018 15:00 Source: CA17001-01 Spike Source %REC RPD Aaallde R sit+ tl Elag f!QL- Units Level Result %REC Limits RPD Limit Now Chemical Oxygen Demand 630 10 mg/L 526 100 100 90-110 Matrix Spike Dup (BB09013-MSD3) Prepared: 02/09/2018 10:13 Analyzed: 02/09/2018 15:00 Source: CA17001-01 Spike Source %REC RPD Allah Result EMQ RQL units Level Result %REC Limns RPD Lima Notes Chemical Oxygen Demand 610 10 mg/L 526 100 97 WHO 3 10 Batch 8014006 - NO PREP Blank (8614006-BLK3) Prepared & Analyzed: 02/14/2018 15:45 Spike Source %REC RPD Ana hd& Result Ela9 201. U11111 Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (SB14006-BSI) Prepared & Analyzed: 02/14/2018 15:45 Spike Source %REC RPD Anal YtB Rewlt Elba Ill Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 96 2.5 mg/L 100 96 80-120 Duplicate (BB14005-DUPI) Prepared & Analyzed: 02/14/2018 15:45 Source: CA18884-01 Spike Source %REC RPD Ana hde Resu Elan POL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 40 2S mg/L 43 7 20 Duplkate (8B34006-DUP2) Prepared & Analyzed: 02/14/2018 15:45 Source: CB01420-01 Spike Source %REC RPD Ana l& RMI Boa PQL units Level Result %REC Lim(( RPD Limit Notes Total Suspended Solids 160 50 mg/L 150 1 20 Classical Chemistry Parameters - Quality Control Batch 8014910 - EPA 1664E Blank (BB14010-BLK3) Prepared: 02/14/2018 14:24 Analyzed: 02/15/2018 15:30 Spike Source %REC RPD AnaResult RM PQL Units Level Result %REC Lim RPD limit Notes CAI & Grease (HEM) 2.40 U 5.00 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. page 5 of 8 r�co www.encolabs.cDm QUALITY CONTROL DATA Classical Chemistry parameters - Quality Control Sate* 0814010 - EPA I6645 - Continued LCS (8B34010-BSI) Prepared: 02/14/2018 14:24 Analyzed: 02/15/2018 15:30 Spike Source %REC RPD Ana hcte am Ew POL Units Level Result %REC limits RPD Limit Notes Oil & Grease (HEM) 147 5.00 mg/L 157 93 78-114 LCS Dup (BB14010-BSD3) Prepared: 02/14/2018 14:24 Analyzed: 02/15/2018 15:30 Spike Source . %REC RPD Ana Result 500 POi Units Level ResuK %REC Limits RPD Limit He= Oil & Grease (HEM) 156 5.00 mg/L 158 98 78-114 6 18 Matrix Spike (BB14010-MSi) Prepared: 02/14/2018 14:24 Analyzed: 02/15/2018 15:30 Source: BB00668-01 Spike Source %REC RPD Ana Restrlt 59 POLL Units Level Result %REC Limits RPD Limit Notes - Oil & Grease (HEM) 190 5.00 mgJL 157 15.6 111 78-I14 FINAL This report relates only to the sample aS received by the laboratory, and may only be reproduced in full. Page 6 of B www.enwla6s.com FLAGS/NOTES AND DEFINMONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRQ, adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 8 1ENV,�-iRONM.ENTAL.CONSERVATION"Lg1BORATORIESj CHAIN OF;CUSTODYiREC-ORD. tA/,1N,lAl: 11[a� s:toml +iroilPaltbit 1 ANA�tuM,r lryulmi+,iq%. } Cijlhrtc�-�li'tCu31� kisacxoursY'IiAeIRLY>BCt�ter 1, QerytN4p7�r`�, _ 4 ! Cllaltlt{SfnAk' S � a }Frii�p!�'!� irlybr :1#3 nDlpwcs KR+c�+LI F! i �f�p1YLlIJMt�I § , �r , r +krlfiasi ' - F+N Nnnrn, �, '•r r � I k ; � F I rrinM6i{r�,nroln,sraxuyxty 'll�' W�`h�r�l:l,lirlli'f r LAN E 1 r a.LA►i2Y�'[uC�27�13=: � ' ;, � ; ._._;tSt�rid�rd'� �. s �y ry�ry 1 �� D }�' tl: •i �t F 'I� lm ri } ; a 8 � LBst8 f1 + t - ' e �,I " - ' t b _ �_ .e-@ted7f r � I ITff1'+t ty ,.. i. I� It i dr 46 rl� It" ira I ,k�,i' rb,MrrrAi,. 09 -A .71001 :IP4eor+lpnisl,lra: aY'cv,eir,+:�, ,71 v'snli .+mrrllp' , Isii:ialmi _ , i�aira,zz�t. Mai , pr�„ir. oa�s�luR urlatalll! �/Ir�es k SsGIjCi�ilfr�nrlts. 1h kk 71 FT I, IT � � ill I � � � I: � �� I �� � •�° i7- 41 t U w•'`ti�tiil.,t++fsf,CorSlt�inets.: ... .. k� �ir!'mqIlll.!b4�[ .� Dalo3Im T IA_.�oR�hMF,04rtiidlmnmll rigl q�lil�ua.4hf I t r+1A 16>,a � fMlllw'''t. oun,:rll,ll� Is ? t� ii�IrtlNii,1111d UV' k l}II dT�M VUti _ r 7Wil,�tq.4 � v •�-�' '4, �c�ii�itabl6� F 1 „�.;lJh�a�Btint llurrir�AwlQrMwtctyufriR80�?I,PlY:4!r{tbmq.Wulnr i arllrcfmrc S}Y&a(�iljVr txW1YYfY7gI�Rwilrgi`AfpIIY(}.Orl+midrsAll,m{pr}imnul; riPle�avpdn�li4gtulli�igl+;N9e;prFl:i3t]aa�4ifnOH.04tiIRrr(13UWIlIVCNOI nq�il ►�np� v IPQ iu��smdfU r 411,11E„i,aniYitdim6FrinlyTrltr,rijw,uu�uu4.1fla rI laitrin"amwumaorntiu'am?ri;Inwrispl�ar.,.mrrt. mnTn�+chin Sample, P`r"eser►afion Verification F =. ENCO�Cary.KIM uai,JU- eite�t= :KE�tat;cs N�c c 1e�s FOODS (KE006) pmpactlq [ 1= Lag din Q'r.-F6?24' 7- Lagged By: Rachel'Ahn.YQnis-- P Yvaton Check P.erf nhiea-.By; 6 Zt11; j t- _ JAA5 t' --- _ CA17�01-0t ftH Ad��s�sti " 0 : - - =9r � m#1�#1�1254 •2= 'Y .1 pA .1 CA Y % N 1 �►a - Lo +H2SO4 4 Y 1 N 1' N Y Z`i�+. HZSSO� N j 1V,4_- ciai7iio�-viz Cant Tye - _- st R ,'#E IJs tCar ►r�rit9, -- - l wfomi f�iF+zr A{#WSI B S��tASO4 I'Y 1F N / !n YC 256i A+H2SO4 .t.2f 1 y ?� t f� l� T -14 '% 4 sue 1-r i..RTr�ttr+Si <2 i hiiz R ent t�anee id pH 5trip;ID; r =- - Pik C710810 *Imrif[grir�t%wK6_P�� and�Cii�ck in F .;Re asi Name -A _ --=_i� - RFa eni [dai-- _.iD:- 4 6 Via Certified Mail February 26, 2018 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: Reporting Year 2018 — Storm Water Discharge Monitoring Report Kellogg's Snacks — Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the February 2018 monitoring event for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Anthony DePietro (919) 677-3292 anthony.depietro&kellogg.com Mr. DePietro is available should any questions or problems arise during the review of this DMR. Uhhk0l,FsaRhick�.�an.bcallsn%uafilesSAAA-Mate* ProjectsSlGNbgglEiFl_-01 I Cary 2018)StormwffierS a' ry 2018 EvcmlStormw=a Caver loner 20180219.&c DWQ —Central Files February 26, 2018 Page 2 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, Steve Surovec Plant Manager Enclosures \Mfso I.hardrickm .locaPt msterfile %AAA -Master Prgects}KeUoggT,EL-011 Cary 201 "tornr%wer\Febrwry 2018 EvcmXStom—ucr Corer letter 20180219.doc Via Certified Mail December 6, 2017 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: Reporting Year 2017 — Storm Water Discharge Monitoring Report Kellogg's Snacks — Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, RECEIVED DEC I.-) --,, I / CENTRJtL FILES DWR SECTIO; - Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the second half of 2017 for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: RECEIVED Mr. Anthony DePietro DEC 13 Z017 (919) 677-3292 anthony.depietro a,kellog�� com rENZr,Al- FILES E VVR SECTION Mr. DePietro is available should any questions or problems arise during the review of this DMR. CaUsersWskajd05VAppData\Loca[\MicrosoNSwndows\Temporary Internet FitesSCornent.outlook11Q9llIDOA5tormwataCover letter 112220t7.doc DWQ — Central Files December 6, 2017 Page 2 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, Steve Surovec Plant Manager Enclosures c,W4i rruskajd051appdatalocspnucrosoAlwindowsltemporary intemet fileskontem.outlook\ig9didojlstormwater coe'cr letter 11222017 doc SEMI-ANNUAL STORMWATER DISCHARGE MONITORING REPORT for North Carolina Division of Water Quality General Permit No. NCG060000 Date submitted _November 22, 2017 CERTIFICATE OF COVERAGE NO. NCGO60286— _ — -,_, SAMPLE COLLECTION YEAR _2017 FACILITY NAME _Kellogg Company — Cary, NC Facility FACILITY ACTIVITIES INCLUDE (check all that apply): COUNTY Wake ❑ use/process meats ❑ use animal fats/byproducts PERSON COLLECTING SAMPLES Gregory Kanellis DISCHARGING TO SALTWATERS? ❑YES ®NO LABORATORY ENCO Labs Lab Cert. # _591 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 Part A: Stormwater Benchmarks and Monitoring Result Total event rainfall a 0.09 in (1019117) 0.10 in (11/7/17)or ❑ No discharge this period Outfall No. Sample. Collected, mo/dd/.yr TSS, mg/L pH, Standard units. COD, mg/L Oil and Grease, mg/L Fecal Collforml, Colonies per 100 ml Enterococci1, Colonies per 100 ml Benchmark - 100 or 504 With 6.0 — 9.0 120 30 1000 Soo SWOT 10/09/17 <12 6.8 300 <2.40 NA NA SW02 10/09/17 6.0 7.2 90 <2.40 NA NA SWOT 11/7/17 NA NA 3100 NA NA NA 1 Only applies to facilities that use/process meats. 2The total precipitation must be recorded using data from an on -site rain gauge. 3 For sampling periods with no discharge at any outfalls. You must still submit this discharge monitoring report with a checkmark here. 'See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ❑ yes ® no Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. autfall No. :-Sample Collected, -mo/dd/yr Oil and Grease, mg/L TSS, mg/L pH, Standard units New Motor Oil Usage, Annual averse al/mo Benchmark - 30 100 or 504 6.0 — 9.0 - ' Only applies to facilities that use/process meats. 'The total precipitation must be recorded using data from an on -site rain gauge. ' For sampling periods with no discharge at any outfalls, you must still submit this discharge monitoring report with a checkmark here. "See General Permit text, Table 3, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. (if yes, complete Part B) SWU-249 Last Revised: October 18, 2012 Page 1 of 2 *FOR PART A AND PART B MONITORING RESULTS: 0 A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: Thad Valentine Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm (Z z (Date) Additional copies of this form may be downloaded at: http://portal.ncdenr.orglweb/wq/ws/su/npdessw#tab-4 S W U-249 Last Revised: October 18, 2012 Page 2 of 2 Date: 101912017 Analyst: G. Kanellis Certification # 5356 Facility Name: Hart & Hickman, PC Permit #: NCG060000 pH Analysis Reference Method: SM 45M H+B-2000 (include year e.¢_ SM 4500-H+ B-20001 Cal. Time Calibration Buffer 4.0 Calibration Buffer 10.0 "Check Buffer 7.0 Comments 1830 4.0 10.0 7.0 Passed *pH buffer checks are to be within t 0.1 pH units of the standards true value. 4 buffer Lot#lidentifier: 7 buffer Lot#lidentifier: 10 buffer UWAdentifier: FacilkylSample location Sample Collection Time* Sample Analysis Time♦ pH Result 1011 Buffer Check value Comments'Data Qualifiers SWOT 1900 1900 6.77 7.0 S W02 1845 1845 7.17 TO • If sample is measured directly in the stream and/or on site, one lime may be recorded for collection and analysis with the notation that they are measured in situ or at the immediately at the sample site. ► Calibration drift check is required when performing analyses at multiple sampling locations. (Use Buffer 7.0) Should be within +0.1 units of the buffer's true value) *All pH results in pH units (i.e., s_u.). Report all data values to the nearest 0.1 pH unit Annual Temperature Sensor Check Date: 6/14/2017 pH Instrument ID: _Myron L Company Ultrameter 11 GPFCE serial N. 6232585 Field Personnel Notes/Equipment Maintenance 10102f2013 FJ.VCO Laboratories Accurate. Timer. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, October 18, 2017 KELLOGGS SNACKS/AUS IN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater CAS ENCO Workorder(s): CA12883 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, October 9, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 8 CeNhk' www.encelabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SW01 Lab ID: CA32883-01 Sampled: 10/07/27 19:00 Received: I0/09/17 12:42 Parallold_Date/limefs] EPA 1664B 11/04/17 10/11/17 Analysis DateMnWsl 15:44 10/12/17 15:30 SM 2540D-1997 10/14/17 10/13/17 13:40 10/13/17 13:40 SM 5220D•1997 11/04/17 10/09/17 14:54 , 10/09/27 17:45 Qient ID: SW02 Lab ID: CA124W-02 Sampled: 10/07/17 18:45 Received: 10/09/17 12:42 Parameter tloldDate/Time(sl AnaWs Date/itmetsl EPA 1664E 11/04/17 10/11/17 15744 10/12/17 15:30 SM 2540D-1997 10/14/17 10/11/17 16:20 10/11/17 16:20 SM 5220D-1997 11/04/17 10/09/17 14:54 10/09/17 17:45 FINAL ih6 report relates only to the sample as received by to IaboratarY, and may oMy be reproduced in ful. Page 2 of a www.encDlabs.com SAMPLE DETECTIDN SUMMARY Client iD: SWO1 Lab ID: CA12883-01 AnMyte BM f1m ffiL VDIts Method N= Chemical Oxygen Demand 300 10 10 mg/L SM 5220D-1997 Client ]ED: SW02 Lab ID: CA12883-02 Anal Results flag K" ML Units Method N Chemical Oxygen Demand 90 10 10 mg/L SM 522OD-1997 Total Suspended weds 6.0 3.3 3.3 mg/L SM 254OD-1997 FINAL This report relates ordy to the sample as received try the laboratory, and may poly be reproduced in full. Page 3 of 8 Ce Nk" 0 0) www.encolabs.com ANALYTICAL RESULTS Description: SW01 Lab Sample ID:CA12883-01 Received: 10/09/17 12:42 Matrix: Surface Water Sampled:10107/17 19:00 Work Order: CA12883 Project: Storrnwater CAS Sampled By: Greg Kanellis lClassical Chemistry Parameters ^ - swo Cary'C"fiied arralyre /RC 5911 Anafvte fCAS Numbed Results am m DF MOL pL Ba + Kauko An hmed By Notes Chemical Oxygen Demand^ 300 mg/L 1 10 10 7109044 SM 5220o-1997 10/09/17 17:45 JOC Total Suspended Solids^ < 12 mg/L 5 12 12 7313005 SM 2540o-1997 10/13/17 13:40 OMR Classical Chemistry Parameters ^ - FKV1wftmvd1e c&Vfiet! mv1kte /AC 442j Analyte rCAS Numberl 90111 f fin Units DF NU E" 11atigh Method Anahgad am N Oil & Grease (HEM) (C-0007]^ < 2.40 mg/L 1 2.40 5.00 7111010 EPA 1664B 10/12/17 15:30 SMA Description: SW02 Lab Sample ID:CA12883-02 Received: 10/09/17 12:42 Matrix: Surface Water Sampled:10/07/17 18:45 Work Order: CA12883 Project: Stormwater GAS Sampled By.- Greg Kanellis 10assical Chemistry Parameters I ^-9VC0Qjyc,,hned&n WlNr591j Analyte rCAS Numbed Results Rag Va[tli DF MU ML AW&h Method Anahzed ICY MUM Chemical Oxygen Demand ^ 90 mg/L 1 10 10 7109044 SM 52200-1997 10/09/17 17:45 Jac Total Suspended Solids- 6.0 mg/L 1.33 3.3 3.3 7111024 SM 25QD-1997 10/11/17 16:20 OMR Classical Chemistry Parameters ^ - 6/C0 Ja0kYX r7le certfied analrre fAC 4421 Analyte rCAS Numberl Resul Flag Units M Ka f% 1= Metes Ana MCI= Oil & Grease (HEM) [C-"7]^ < 2.40 mg/L 1 2.40 5.00 7111010 EPA 1664E 10/12/17 15:30 SMA FINAL This reportrelates only to the sample as received by the lady, and may only be reproduced in ful. Page 4 of 8 CS N' 0 0) www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7J04044 - Same Blank (7309044-BLKI) Prepared: LO/09/2017 14:54 Analyzed: 10/09/2017 17:45 Spike Source %REC RPD Argil di Result flag PQL Units Level BMW %REC Limits RPD Limit Lion Chemical Oxygen Demand 10 U 10 mg/L LCS (7309044-BSI) Prepared: 10/09/2017 14:54 Analyzed: 10/09/2017 17AS Spike Sauce %REC RPD Anands Result Sag PQL Uni15 Lend Result "/aREC Limit& RPD Limit moo Chemical Oxygen Demand 490 10 mg/L 500 97 90-110 Matrix Spike (7309044-MSI) Prepared: 10/09/2017 14:54 Analyzed: 10/09/2017 17:45 Source: CA12883-01 Spike Source %REC RPD Anilb s Re & Haig PQL Units Level Result %REC Lim iL4 RPD Limit Notes Chemical Oxygen Demand 830 10 mg/L 526 300 101 90-110 Matrix Spike Dup (7309044-MSD1) Prepared: 10/09/2017 14:54 Analyzed: 10/09/2017 17:45 Source: CAL2883-01 Spike Source %REC RPD An Result Him PQL Units Level Result %REC Limits RPD Limit Rgua Chemical Oxygen Demand 840 10 mg/L 526 300 103 90-110 1 10 Batch 7J11024 - NO PREP Blank (7]11024-BLK1) Prepaned & Analyzed: 10/11/2017 16:20 Spike Source 9/6REC RPD A Re1ul1 flag PQL Units Level Result %REC Limits RPD Limit [! abes Total Suspended Solids i 2.5 U 2.5 mg/L LCS (7311024-BS1) Prepared & Analyzed: 10/11/2017 16:20 Spike Source %REC RPD A1+�i1de Result Flag PQL knits Level Raw %REC Limits RPD Limit notes_ Total Suspended Solids 89 2.5 mg/L 100 89 80-120 Duplicate (7311024-DUP3) Prepared & Analyre : 10/11/2017 16:20 Source: CAL3171-01 Spike Source %REC RPD Ana hr3e Resul ELM eel. lh]ii4 Level Result %REC Limits RPD Limit Notes Total Suspended Solids 21 17 mg/L 23 9 20 Duplicate (7311024-DUP2) Prepared & Analyzed: 10/11/2017 16:20 Source: CA14948-01 Spike Source %REC RPD Aria Result E102 E4L Units Level Result %REC Limits RPD Limill Notes Total Suspended Solids 290 50 mg/L 270 6 20 Batch 7JI300S - NO PREP Blank (7313005-BLK3) Prepared & Analyzed: 10/13/2017 13:40 Spike Source %REC RPD ALra Resin Elm EQL Units Level Rewl %REC Limits RPD Limit slates Total Suspended Solids 2.5 U 2.5 mg/L FINAL This report relates Only m the sample as receiyed by the laboratory, and may only be reproduced in ful. Page 5 of 8 (9 �69 www.encDlabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Balch 7J130D5 - NO PREP - Continued LCS (7313O05-80) Prepared & Analyzed: 10/13/2017 13:40 Spike Source %REC RPD -Andbft Rssdt ELIO POL Units Level Result %REC Limits RPD Lim- Notes Total Suspended Solids 90 2,5 mg/L 100 90 80-120 Duplicate (7313005-DUPI) Prepared & Analyzed: 10/13/2017 13:40 Source: CAIL3549-01 Spike Source %JtEC RPD Ana lrSa Result Ela9 e01 Uni Level Resul %REC Limits RPD Mini Notes Total Suspended Solids 1600 100 mg/L 16M 2 20 Duplicate (7]13005-DUP2) Prepared & Analyzed: 10/13/2017 13:40 Source: CA14944-01 Spike Source a/aREC RPD Ana hrte Rc5w Z fag SQL units Level Result %REC Limits RPD Limi Notes Total Suspended Solids 320 50 mg/L 320 2 20 Classical Chemistry Parameters - Quality Control Balch 7JI1010 - EPA 1664E Blank (7311010-OLKI) Prepared: 10/11/2017 15:44 Analyzed: 10/12/2017 15:30 Spike Source %REC RPD Anahme Result llag e¢L ni Level Result %REC Limits RPD MWR Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (7311010-BSI) Prepared: 10/11/2017 15:44 Analyzed: 10/12/2017 15:30 Spike Source %REC RPD Ana lkts Resldt Oda e91 Units Level %REC Limits RPD Limitl� Oil & Grease (HEM) 158 5.00 mg/L 163 97 78-114 LCS Dup (7311O1O-BSOI) Prepared: 10/11/2017 15:44 Analyzed: 10/12/2017 15:30 Spike Source a/aREC RPD AnaL1[t0 Result flag QOL Units Level gesu(Z a/aREC LomlRPD kimk dote Oil & Grease (HEM) 147 5.00 mg/L 159 92 78.114 7 18 Matrix Spike (7311010-MS3) Prepared: 10/11/2017 15:44 Analyzed: 10/12/2017 15:30 Source: BAO433S-01 Spike Source a/oREC RPD AnallSe Rssdt Elaa M. Units Level gam( %REC Lim RPD kilnft Notes_ Oil & Grease (HEM) 144 5.00 mg/L 150 2.40 U 96 78-114 FINAL This report relates only to the sample as recewed by the laboratory, and may only be reproduced in full. Page 6 of 8 CS Nk" 0 0) www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This mpaR relate a* to the sample as received by the laboratDry, and may only be reproduced in full. Page 7 of 6 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com CCU t0775 Carlral Pori dr. Oaf D Exuaa<fvo Paris court suits i t l . 162d Wootlwfntls Industrial Cl. Orlando, FL 32824 Ja6aonvi la, FL 32216.6069 Cary, NC 27511 1 (407) 826.6314 :Fax (407)1L5 4"S, • (90/) 296.3007 •Fax (904) 290.62l0 ; k (919) 467.3090 Fax (919) 4M.3515 Page I of I Cllenl Name e p y Protect Number n Requssled Ans Requested Turnaround r A t Times Addlau r y M _' Peoj NemeJDase . / + Note: Rush rKussta subj e, to 'ONE' UAL T�' . S Wate CA A1 Ill.; ., a , �1 aocep.Iaretabytheta by .. PO 07 Billing Into CARP NC 27513- >- r _ . .O . "' 'yam, � Standard 1a; . d Fox s Roporarg"tea g� g °877.35i9`° =' ' `� . '.. `Rodne Bateman �'. :� s v,l m� 4 F f; i . Expedited Samptar(r) Nanlo - Atfilfat on (Print] • _ ) . ,lr . BI11ing CAntett i - . - .. �. ' i.. i'+�..-t 1. -Acoounts'Payable N 'Due���. Site Location! Time Zona © _ v • - b a W rk orde r - o o .. Preservauan (See Coon) (Cm!"birer now . y) CA 12883 Ilem r .- .-Semple ' Ili (Fold 6d trfleation j CoeelIon Gala " ' CoeiW t �' • I Grab Matrix - Total , , �, » ,1'S•_ l t ( 1 • �!nP (sou cotle>'I ' contsalan Y � . r~ • a_ .. Sample Comments • .F L, t.a }•.r r . '.•!. •� !+ T rt k. k _ .. . ��� 1r. , w ,Yt .. .. .r „ M -5 c,,. a •r: ,f , r,i -.r. •1 r � -T6lel # OfCOnt&InOre . ,..t �'... �. t .. mpla KII Prepared Sy-: . ° ,. r� r . Dai !time- -, Reif uishad B * , r �� - ti - . Datenlma ' �^ ... iorgl�-r Recafvotl B- G&mMqSpHpeael Reporting Requirements Relirquished By . , ,.". DntoFl7ime • „ :' ivrd y' ,, r '; Dalarrana ' t Ralinquisired By '3 t' DateMme Roca 8y . - Daloalmo - r� •: r'r Tampa o1 Recelpl ., Condition V Recalpi VAC69 iHb10 Unacceptable Mautx : GW.Gtoundwater SO -SON Dw•Ddniting Watar BE -Sediment sw-Stirtacewatei ww-wastewater A -Air 0-00w (dotailin comments) Prsaarvatlon: Llta H•HCI N•HNO3 S-H2SO4 NO-NaOH Odthet (detail in ccmmonts) Note : A9 samples subinitted to ENCO Late* are In aceordanea with the loans and conditions honed an We reverse d this form, unless pdw wrinan agreements exW r .. Sample Preservation Verifi8ation ENCQ Cary . Work Order: CA12883 Project: Stormwater CAS Client: KELLOGGS SNACKSIAUST IN FOODS (KE006) Project #: [none] Logged In: 09-Oct-17 13:29 Logged By: John C King CA12883-01 C nt Type a �aPs (pH};t Requiremen pH Checked / efn Control 'PH Adjusted :UatelTime 4, d '.AdWsted Reagent ElsedlComments ,-- B 250mLA+H2SO4 <2 if / N I NA Y 16Ll NA C 250mLA+H2SO4 <2 lVr 1 N 1 NA Y I ! NA D 250mLP+H2SO4 <2 'I I N 1 NA Y ! / NA CA12883-02 Carsti :k...An Type i Pres .(pH)J pH Checked l Control., pH Adjusted Date�me Adjusted r Reagent UsikV mments : , B 250mLA+H2SO4 <2 I 1 N/ NA Y I 1 NA C 250mLA+H2SO4 <2 11 N/ NA Y I �, 1 NA D 250mLP+H2SO4 <2 Y I N/ NA Y/ I NA Reagent Name ID 1 2 l� Rea ent Name ID f i Rea ent Name ID 5 6 Page 1 of 1 ENCO Laboratories Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, November 17, 2017 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater CAS ENCO Workorder(s): CA17106 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, November 7, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Endosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in MI. Page £ of 7 OF man www.encolabs.com SAMPLE SUMMARY/ LABORATORY CHRONICLE Client ID: Sw01 Lab ID: CA17106-01 Sampled: 11/07/17 14:45 Received: 11/07/17 IS:20 Parameter PreuaratiQn Hold DatefTrme(s) Peep, Date/Trme(s) Analysis Date/Time(s) SM 5220D-1997 Same 12JO5117 11/14/17 17:10 11/14/17 19:45 FINAL This report relates cdy to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 7 C, F " I www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 5Wg1 Lab ID: CA17106-01 Chemiel Oxygen Demand 3100 100 100 mg/L SM 522OD-1997 FINAL This report relates ordy to the sample as naxtved by the laboratory, and may only be reproduced in fu0. Page 3 of 7 M�- www.encolabs.com ANALYTICAL RESULTS Description: SW01 Lab Sample ID: CA17106-01 Received: 11/07/17 15:20 Matrix: Surface Water Sampled:11/07/17 14:45 Work Order: CA17106 Project: Stormwater CAS Sampled By: Greg Kanellis Classical Chemistry Parameters ^ - EXV Cary certlAed ana" [W 5911 AAn hrte ICAS Numbed Restrl flig Units DF MDL POLL Batch Method Analrud ax Notes Chemical Oxygen DemandA 3100 mg/L 10 100 100 7K14031 SM 5220o-1997 11/14/17 19:45 30C FINAL This report relates or* to the sample as received by the labaratorY, and may only be reproduced in full. Pape 4 of 7 FJVCa www,encola6s.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batd6 7K14031- Same Blank (7K14031-BLKl) Prepared: 11/14/2017 17:10 Analyzed: 11/14/2017 19:45 Spike Source 0/aREC RPD An hde Result HWq EQL UniL4 level get %REC, Limifs RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (7K14031-BSL) Prepared: 11/14/2017 17:10 Analyzed: 11/14/2017 19A5 Spike Source %REC RPD r iltf& Result Elm POL Uhiti Level Resul %REC Limits RPD LimK Notes Chemical Oxygen Demand 500 10 mg/L 500 100 90-110 Matrix Spike (7K14031-MS1) Prepared: 11/14/2017 17:10 Analyzed: 11/14/2017 19:45 Source: CA09070-01 Spike Source %REC RPD Ana Resul Flag POL Units . Level Rat %REC Limits RPO 'mi Notes Chemical Oxygen Demand 560 10 mg(L 526 42 99 90-110 Matrix Spike Dup (7K14031-MSD1) Prepared: 11/14/2017 17:10 Analyzed: 11/14/2017 19:45 Source: CA09070-01 Spike Source a/*REC RPD Ana Refit Elm PGL Units Level Resin 0/*REC LimRPD limit Notes Chemical Oxygen Demand 580 10 mg/L 526 42 102 90-110 2 10 FINAL This report relates 0* to the sample as received by the laboratory, and may only be repi Lived in foil. Page 5 of 7 www.encol!a6s.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting limit. The MRL is roughly equivalent to the practical quantitatian limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (65% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINK. This report relates only to the sample as received by the laboratory, and may only be reproduced in fuB. Page 6 of 7 t "",-- -- GI\YrnVtfTYt GI\ IML" VVI\.7clrltMl tV17,LMCJVI"{!41 VntC�7 - 4nMll+a'{:/r"4V�7 fVYf-nG\sVnd - - 1ir71tlw1C11�I1101l1.4V11� C� 107175 Orlando Lrs32E 4 Or. 481w FI. 3�221CS-Mg uite 211 7CO2•A Coodwlnds Induslrisl d. ' 27511 (407) 826.5314 Rix (407) 850-Mi' (804) 296-3007 Fax (0o4) 2f}8-62l0 (9iM 67.301)0 Fax (91 B) as7-3515 Page J of p; Ci(ani Name z, Project Number Requested Analyses I Requested Turnaround - Times ' - Address - ` ' - .- Project NamdDosc.. Note : Rush requests eublocE to y acceptance by the, t"Wry e ; r ' ,.. City/STOP `, PO rt! ailing Info Standard I. Tai Fax Reporlinp COn%ct Expedited. Due Samplers) Name. ARilimion (Print),_. - - Billing Contact Q f 3eriipler(s 1(plahlre site Location r zone Lab Workorder r •k r G� t 01 � .. Presarvetlon (Soo Coded (Combin6 as nerlasary} , Samoa ID (geld Identification) Co eclion Dais- Collection Time Comp I Wab Mah9x {see codes) Total t+ a] Containers ' Sample Comments F 1 r`r <-- Total R of Containers sample Kit Propar0d sly � ;,- ,. Dateyrima , •. � Relinquished By - - F - - , Dat - - '15 Race y - Datayr - l� ConvtierLLef3peeial Raporfinp Requirements a rie By r DatelTkrle n Roos By pateyrime' . . l F �' rt F Fix• t . F v I ln' . .. o, - �• 1 I _ Rolintalished By. Datalrime Receive_ d By Datdrime ,.,_?. i ';(.; - Cooler e's 8 Temps on ROCWpi - .. .. t - . -. Condition Ypbn Receipt Acceptable 'Unacceptable Matrix:PW-UrowWwaler 50-508Aw•onnanpWelor SE•Sodiment SWSurfaceWater WW.Wastawator A -Air 0-01her(detailin0ommanis) Presatvallon,.yleo H•HCI H-HNO3 S-H2SO4 NO-M80H 0.Othoi(detail incomments) Note : Aft 5arrtdes submitted to ENCO labs are In accordance with iho terms and condition hated on the reverse of this form. unteeia prlor "an agrasmenb exist . ' Ito H� 6 uiftontit � s Sample Preservation Verification - \ ENCO Cary s Work Order. CA17106 Project: Stormwater CAS Client: KELLOGGS SNACKSIAUSTIN FOODS (KE006) Project #: [none] Logged in: 08-Nov-17 10:34 Logged By: John C King Preservation Check Performed By: Daterrime: CA17106-01 i Cont Type .1_ Pres,(pH) = epH Adjusted ReagentUsed/Comments.equirement kpqecked) ontrol Adjusted A 250mLP+H2SO4 �2 N/ NA Y I 1 NA Rea ent Name ID Rea ent Name ID Reagent Name ID 1 .3 5 2 4 6 pH Strip ID: C:IELMNT1Printlwko_PreservationCheck.rpt Page 1 c t Via Certified Mail DECEIVED July 13, 2017 JUL 2 Q 201� CENTRAL FILES Central Files DWR SECTION Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: Reporting Year 2017 — Storm Water Discharge Monitoring Report Kellogg's Snacks — Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, z RECEIVED JUL 2 0 20q C&N7-R,4L FILES DINR SECr1ON Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the first half of 2017 for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Anthony DePietro (919) 677-3292 anthony.a(zipietro@kellogp,.com cam Mr. DePietro is available should any questions or problems arise during the review of this DMR. C:V[lsers�t s dOSkAppDataV,oas NlicrowftNWutdowslTemponry Internet FdesVComent,Outlook\NOS11 AOU1S1omwater Cover letter O623261T,doc DWQ — Central Files July 13, 2017 Page 2 I certify, under penalty of Iaw, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Steve Surovec Plant Manager c:4nsersluskejdoSWpdauUoWa nicrosoflYwindowsltcmporaryntemet fikeskontent.wtlook4As3ldOtAslor:nater over letter 06232017.doc STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCG060000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017 CERTIFICATE OF COVERAGE NO. NCG06 0286 (This monitoring report is due at the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Kellogg Company - Cary, NC Facility COUNTY Wake PERSON COLLECTING SAMPLES Gregory Kanel is PHONE NO. (919) 677-3292 CERTIFIED LABORATORY ENCO Las Lab # 591 .. Lab # PLEASE SIGN ON THE REVERSE Part A: Specific Monitoring Requirements `Outfall tllate. .00530 00400 00340 00556 31616 `� No � :!=: Sample Total Suspended pH; Chemical Oxygen. ygen : Oil and Grease, Fecal Coliform,- s .Collected, _.. Solids; Standard units Demand, . mg/L Colonies per 100 nil 01i&dd/ r" m Benchmark 100 Within 6.0 — 9.0 120 30 1000 SW01 6/23/17 <8.3 6.0 660 8.59 NA SW02 6/23/17 2.8 6.2 28 2.40 J NA Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X_no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements .Outfall • No. F:. �, Date7 ?5amplerCollected, rioldd/ r ; 00556 00530 00400 Oil and Grease, :. m Total Suspended Solids, . m pH, Standard:units New Motor Oil Usage, Annual averse Sallino Benchmark - 30 100 6.0 -- 9.0 Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier i or Tier 2 responses. See General Permit text. STORM EVENT CHARACTERISTICS: Date 6/23/17 (first event sampled) 0.04 Total Event Precipitation (inches): Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Mail Original and one copy to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 S WU-249-102107 Page 1 of 2 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted: Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." - _75: . _V - zC l (Signature of Per ittee) (Date) S WU-249-102107 Page 2 of 2 Date: G "'j Analyst: r. Certification # 5356 Facility Name: dart & Hickman, PC Permit 0: _NCG060000 PH Analysis Reference klethnd: SM d50011+11-2000 (include veer & v_ W d56a.11+ 11_24[101 Cal, Time Calibration Bul&r4.0 Calibration Buffer ID.0 *Check Buffer 7.0 Comments •pII baffercheeks are to be yrfolu t 0.1 pH units of the standards true Val � 4 buffer U1#11dentifier. J'Al OX 7 buffer L Wfidentffler: 42Z 10 buffer l.00lidentlfkr. Facility/Satnpic location Sample Collcnion Time* Sample Analysis Time* pH Result Rol Buffer Check value CommentslDats Quaiiriers swa l b - v53d C, a'), -7. 0 Swu2 Osq S o5 6. -7. a • 1f sample Is measured directly in the stream and/or on site, one time may be recorded for collection and analysis with the natation that they are measured in situ or at the bmardlately at the sample site. ► Calibration drift check is required when performing analyses at multiple sampling locations. (Use Buffer 7A) Should be within t 0.1 units or the buffer's true value) *All PH results In pH units (Le., s.u.). Report all data values to the o mmt 0.1 p1I unit. Annual Temperature Sensor Check Date: 6IM017 plf Instrument ID: —Myron L Company Uitrameter 11 GPFC serial M 6232511S Field Personnel Notes/Equipment. Mainteanace I0/0'Jt013 ENCO Laboratones Accurate. Timely, Responsive. Innovative. 102-A woodwinds Industrial Court Cary NC, 27511 Phone: 919A67.3090 FAX: 919.467.3515 Wednesday, July 5, 2017 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (Jan,]uly) ENCO Workorder(s): CA02153 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, June 23, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This repot relates only to the sample as medyed by the laboratory, and may only be neproduDed In fLill. Page 1 of 8 0 F. m Nkq � M r www.enculabr.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SW-01 LabIO: CA02153-01 Sampled: 06/23/17 05:30 Received: 06/23/17 11:40 Parameter Kold Dabe/Trme(s) Prep Date/Time(s) Analysis DatelTrmg(s) EPA 1664B 07/21/17 06/28/17 15:46 06/29/17 13:23 SM 2540D-1997 06/30/17 06/28/17 11:50 06/28/17 11:50 SM 5220D-1997 07/21/17 06/27/17 14:41 06/27/17 17:20 CierttID: SW-02 Lab ID: CA02153-02 Sampled: 06/23/17 05:45 Received: 06/23/17 12:40 Parameter Hold DaftMmg(s) Prep Date/Time(s) Analysis DatelTime(s) EPA 1664B 07/21/17 06/28/17 15:46 06/29/17 13:23 SM 2540D-1997 06/30/17 06/28/17 11:50 06/28/17 11:50 SM 5220D-1997 07/21/17 06/27/17 14:41 06/27/17 17:20 FINAL This report relates only tD the sample as received try the laboratory, and may ony be reproduced in full. Page 2 of 8 f �uco www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: ' SW-01 Lab ID: CA02153-01 Anal 1d?C Resufts EL MDL I L 9 ) w4f�4 Chemical Oxygen Demand 660 10 10 mg/L SM 5220D-1997 Oil & Grease (HEM) 8.59 2.40 5.00 mg/L EPA 1664E CIieM ID: SW-02 Lab ID: CA02153-02 Ana Resu E N MIL Pa units Method Notea Chemical Oxygen Demand 28 10 10 mg/L SM 5220D-1997 Oil & Grease (HEM) 2.40 1 2.40 5.00 mg/L EPA 1664B Total Suspended Solids 2.8 2.8 2.8 mg/L SM 254OD-1997 FINAL This report relates cny to the sample as reoeived by the laboratory, and may only be reproduced in full. Page 3 of 8 CqNLG..0'j www.encwlabs.com ANALYTICAL RESULTS Description: SW-01 Lab Sample ID:CA02153-01 Received: 06/23/17 11:40 Matrix: Surface Water Sampled:06/23/17 05:30 Work Order: CA02153 Project Stormwater (Jan,July) Sampled By: Greg Kanellis Classical Chemistry Parameters ^ - FNCO Cary cerhfitti7 a—W [NC 591] Analitte ICAS Numberl Results Flag Units QE MDL f2L Batch Method Anal A Notes Chemical Oxygen Demand^ 660 mg/L. 1 10 10 7F27017 SM 522OD-1997 06/27/17 1720 30C Total Suspended Solids- < 8.3 mg/L 3.33 8.3 8.3 7F28W7 SM 254OD-1997 06/28/17 11:50 OMR Classical Chemistry Parameters ^ - ENCOJa�anville cer0fied anatyte [NC 442] Anabft IFCAS NumhK1 13esu flag Unns 1f Hu E91 Batch Meth Analyzed am N Oil & Grease (HEM) [C-M7]^ 8.59 mg/L 1 2.40 5.00 7FZ8013 EPA 1664E 06/29/17 13:23 SMA Description: SW-02 Lab Sample ID:CA02153-02 Received: 06/23/17 11:40 Matrix: Surface Water Sampled: 06/23/17 05:45 Work Order: CA02153 Project Stonnwater (Jan,3uly) Sampled By:Greg Kanellis Classical Chemistry Parameters ^ - ENCO ary cerMed analyte [NC 5911 Anak de fCAS Numberl Resutts Ma units 2E HU E2L !cal Method Am AY N Chemical Oxygen Demand 28 mg/L. 1 10 10 7F27017 SM 5220D-1997 06/27/17 17:20 30C Total Suspended Solids^ 2.8 mg/L 1.14 2.8 2.8 7F28007 SM 254OD-1997 06/28/17 11:50 OMR Classical Chemistry Parameters ^ - ENCOaaoksp—Re certlried analyle [NC 4421 . Analvbe [CAS Numbers Resu E61!2 Units gF MDL EQL Batch Method Anatned ft N Oil & Grease (HEM) [C-0007]^ 2.40 3 mg/L. 1 2.40 5.00 7F28013 EPA 1664E 06/29/17 13:23 SMA FINAL This report reLdes only b the sample as received 6r the laboratory, and may only be reproduced in ful Page 4 of 8 9 �Ge) www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7F27017 - Some Blank (7F27017-BLKi) Prepared: 06/27/2017 14:41 Analyzed: 06/27/2017 17:20 Spike Source o/aREC RPD Anal Resu 1S Ebg IML Units Level Resu K %REC Lim RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (7F27017-BSI) Prepared: 06/27/2017 14:41 Analyzed: 06/27/2017 17:20 Spike Source %REC RPD Ana Result am POL Units Level Bmu o/aREC Limits RPD Limit Notes Chemical Oxygen Demand 500 10 mg/L 500 101 90-110 Matrix Spike (7F27017-MSI) Prepared. 06/27/2017 14:41 Analyzed: 06/27/2017 17:20 Source: CA0741B-02 Spike Source %REC RPD Anal rte Resu }t Flag POL Units Level Resu %REC Limits RPD Limit lye Chemical Oxygen Demand 520 10 mg/L 526 24 94 90-110 Matrix Spike Oup (7F27017-MSDI) Prepared: 06/27/2017 14:41 Analyzed: 06/27/2017 17:20 Source: CA07418-02 Spike Source %REC RPD Anal Resu R F1a0 EQ.L Units Level ResK %FLEC Limits RPD Limit Chemical Oxygen Demand 520 10 mg/L 526 24 94 90-110 0.4 10 Batch 7F28007 - NO PREP Blank (7F28007-BLK1) Prepared & Analyzed: 06/28/2017 11:50 Spike Source %REC RPD Anal ldg Rewft am £UL Units Level Rig %REC Limots RPD Limit dabes Total Suspended Solids 2.5 U 2.5 mg/L LCS (7F28007-BSI) Prepared & Analyzed: 06/28/2017 11:50 Spike Source %REC RPD AnalResu Ela9 EOL Un is Level Result %REC LlmltS RPD Limit Nates Total Suspended Solids 96 2.5 mg/L 100 96 ' 80.120 Duplicate (7F2$007-DUPI) Prepared & Analyzed: 06/28/2017 11:50 Source: CAD8152-01 Spike Source %REC RPD Anal tde Resu Flau eal. .Una Level Resu R %REC Limits RPD Limit Notes Total Suspended Solids 74 20 mg/L 81 8 20 Duplicate (7F28007-DUP2) Prepared & Analyzed: 06/28/2017 11:50 Source: CADS190-01 Spike Source %REC RPD Anab tg Resu Ela4 RQL Units Level Res utti %REC Limits RPD Limit Mates Total Suspended Solids 200 50 mg/L 190 6 20 Classical Chemistry Parameters - Quality Control Batch 7F28013 - EPA 1664E Blank (7F28013-BLK1) Prepared: 06/28/2017 15:46 Analyzed: 06/29/2017 13:23 Spike Source %REC RPD Anal Y4e Resu Elm MI. U iJ> t Level Resu R %REC Limits RPb Limit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L FINAL This report -Dales only to the sample as received by the laboratorY, and may only be reproduced in full. Page 5 of 8 (� �eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Satiate 7F28013 - EPA 1664B - Conrtrnived LCS (7F28013-BSI) Prepared: 06/28/2017 15:46 Analyzed: 06/29/2017 13:23 Spike Source %REC RPD Anal Y3e Bwult Elac 241. Units Level Resuk %REC Lim RPD Lim' Names Oil & Grease (HEM) 123 5.00 mg/L 144 86 78-114 LCS Dup (7F2B013-BSDI) Prepared: 06/28/2017 15:46 Analyzed: 06/29/201713:23 Spike Source %REC RPD Anal tde l3esuft Elm e4L m its Level Result %REC Limits RPD LLMA dotes Oil & Grease (HEM) 131 5.00 mg/L 143 91 78-114 6 18 Matrix Spike (7F28013-MS3) Prepared: 06/28/2017 15:46 Analyzed: 06/29/2017 13:23 Source: BA02798-01 Spike Source %REC RPD Anal vte RessIR Elag ML Units Level Resuk %REC Limits RPD Limit Notes Oil & Grease (HEM) 134 5.00 mg/L 149 3.36 87 78-114 FINAL This report relates only to the sanoe as received by the laboratory, and may only be reproduced in full. Page 6 of 8 E�Ge) www.encolabs.com FLAGS/NOTES AND DEFINITIONS a The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (859/o or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 8 ENVIRO I NMENTALtoNgERvAnoN'L-ASORATORIES- icHAIN-'OF-PUSTODY:'-'ReCORD Owl =W,"d*t �A �-Jjl I rid 0 N Ej2UAUIL, LLAN C) ' mil —SttindArdL At, oev- i eman M _lEvedifed, L# �bj! i m zm1h .6 C', A 021,r,5 3 upp"'Im rmoaei��;j t Al tj Je 4ad %ITI Wxavl� S;ainpie ' Preservation Verif cation - ENCO Cary r►nrork'046r..: ,cAo2`l53: Project: SfgrmuaWr°(:lan,.lufyy Cl nt KtLLOGGS SNACkC !AUS lk FbOI7S (tC�O6) Proms � (nvnej Logged In: 23-Jun-#f l2,45 Logged 5jr- PWWwAn Yon h %ice K v YP+��I•. ':.F- "G '.,?' j' B,r, 2MmtA+H2SO4 c�" y'l N; :YTf' Iwo - C Mrit:A-�H25Q4. 22 Y! N "' 'Y I N D 2*LP+H2.SO4 cZ Y N I NA CAQ2l53;Oj Rle 7 B 25QmLAt�-12S�4 .42 Y l_ N 1! ! N l C` 2 LA+H2Sa4 <2, Y `/ 'N ! N,4 -Y I..N"1 D2LP+ti2SE3? - <2 Y N/ fVA Y I N t ,NA -- Rea'eirt 2 Idea ent Name ID 4 F U.- :•Red P��e 1 ai t C�o�aa� IV Certification # 5356 ,hate; 0 1 L Facility name: Hart & llkkma% PC Analyst: Permit #; NCG060000 pit Analysh Reference Illetbod: SM 459011+B-2000 (Include scar ems., S%14500-11+ 8-2000) Cal. Time Calibration Buffer 4.0 Calibration Buffer 10.0 `Check Buffer 7.0 Comments d 'pit buffer checks are to be within * 0.1 pit units of the standards true value. 4 buffer Lot#/ideadner. 7 buffer Lot#/ideatlBer. fr 10 buffer Lotli.'Identliier. G� � /�a to 11L D Facility'Sample location Sample Collection Tim* Sample Analysis Time* pli Result 0-1 Buffer Check value Comments0ata Qualifiers SWGI �D Na 1 •5 7.c7 trw c SWO2 13S ti35 1.7 . o • If sample is measured directly in the stream and/or on site, one time may be recorded for eoIlectlon and analysis with the notation that they are measured in sine or at the immediately at the sample site. ► Calibration drift check is required when performing analyses at multiple sampling locations. (Use Buffer 7.0) Should he within t 0.1 units of the bafrer's true value) 'All pil results In pill units (Ix., La.). Report aB a values to the nearest 0.1 pit unit. Annual Temperature Sea or Check Date: l pit Instrument ID: _ r Field Personnel \otes/Fquipnent 5lafntenanee 10/0_'/'_Ol3 RECEIVED DEC 2 S 2016 CENTRAL FILES DWR SECTION ra ENCO Labo tories Accurate. 'Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, December 9, 2016 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (]an,]uly) ENCO Workorder(s): CZ12923 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, November 29, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may ony be reproduced in fun. Page 1 of 8 ((J�Ei www.enoDlabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE ClierttID: SW01 LabiD: CZ12923-01 Sampled: 11/29/16 14:15 Received: LI/29/16 16:37 Parameter Hold Die/Timers] Prep Date/Timers) Analysis Date/Time(s) EPA 1664E 12/27/16 12/06/16 13:29 12/07/16 14:42 SM 2540D-1997 12/06/16 12/01/16 1330 12/01/16 13:30 SM 5220D-1997 12/27/16 12/05/16 13:27 12/05/16 16:31 CderitID: SW02 Lab ID: CZ12923-02 Sampled: ii/29/16 14:30 Received: 11/29/16 16:37 PaTamebe Hold DatelTime(s) Prep Date/Time(s) Analysis DatelTime(s) EPA 1664E 12/27/16 12/06/16 13:29 12/07/16 14:42 SM 2540D-1997 12/06/16 12/01/16 13:30 12/01/16 13:30 SM 5220D-1997 12/27/16 12/05/16 13:27 12/05/16 16:31 FINAL This report relates only b0 the sample as received by the laboratory, and may only be reproduced in fill. Page 2 of 8 0F.=Nk9 www.enoolabs.com SAMPLE DETECTION SUMMARY:J Client ID: SWOT Lab ID: CZ12923-01 A1�.aElite MDR ML Units Method Notes Chemical Oxygen Demand 24 10 10 mgjL SM 522OD-1997 Total Suspended Solids 5.5 3.0 3.0 mg/L SM 254OD-1997 Client ID: SW02 Lab Ib: CZ12923-02 AIl;t11d& Ss lti Ewn MDL EQL Mob mcund Nates Chemical Oxygen Demand 160 10 10 mg/L SM 522OD-1997 Total Suspended Solids 24 12 12 mg/L SM 254OD-1997 FINAL. This remW relates only to the sample as received by the laboratory, and may only be reproduced in U. Page 3 of 8 (��ao www.encolabs.com ANALYTICAL RESULT'S =1 Description: SW01 Lab Sample ID:CZ12923-01 Received: 11/29/16 16:37 Matrix: Surface Water Sampled: 11/29/16 14:15 Work Order: CZ12923 Project: Storrnwater (Jan,July) Sampled By:Greg Kanellis Chemistry Parameters ^ - ENCO Cary cad`ffmf m&yIe [NC 5911 Anahrbe rCAS Number] Results $ag Units 2E rjLL ML aakh t(gffipd Ana lned §1 Notes Chemical Oxygen Demand' 24 mg/L 1 10 10 6LO5022 SM 522OD-1997 12/05/16 16:31 ]OC Total Suspended Solids^ 5.5 mg/L 1.19 3.0 3.0 6LO1002 SM 2540D-1997 12/01/16 13:30 MMR Classical Chemistry Parameters ^ - ENC0-L-C swW1e [notified arlalyte [NC 4421 Anailte]CASNumberl Results fin YMM OE Hu EQL l=b Method AnAvzW By Notes Oil & Grease (HEM) [C-0007]^ < 2.40 mg/L 1 2.40 5.00 6LO6009 EPA 1664E 12/07/16 14:42 SMA Description: SWO2 Lab Sample ID: CZ12923-02 Received: 11/29/16 16:37 Matrix: Surface Water Sampled-11/29/16 14:30 Work Order: CZ12923 Project: Stormwater (Jan,July) Sampled By: Greg Kaneilis Classical Chemistry Parameters ^ - ENCO Cary cw071ed analyte INC 591J Anahrte rCAS Number] Results 099 mam PE H—Ph ML patch Methad Analyzed Ay N Chemical Oxygen Demand^ 260 mg/L 1 10 10 6L05022 SM 5220D-1997 12/05/16 16:31 30C Total Suspended Solids^ 24 mg/L 5 12 12 6L01002 SM 254OD-1997 12/01/16 13:30 MMR Classical Chemistry Parameters ^ - ENCO Jadsannrie Ceafied aneyte [NC 442] Analyte rCAS Numberl Rou EW9 Mp,b PE ML P9L Batch Method Analysed ft Irir� Oil & Grease (HEM) [C-0007]^ < 2.40 mg/L 1 2.40 5.00 6L06009 EPA 1664E 12/07/16 14:42 SMA FINAL This report relates only to the Sample as received by the laboratory, and may only be reproduced in full. Page 4 of 8 CeNk'00) www.encolabs-corn QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6LO1OO2 - NO PREP Blank (61.01002-BLKl) Prepared & Analyzed: 12/01/2016 13:30 Spike Source %REC RPD Anal lde Result Elm PQL Units Level Resu R %REC IL mite RPD limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (GL01002-Bso Prepared & Analyzed: 12/01/2016 13:30 Spike Source %REC RPD Anal Result Elag QQL Units Level Result %REC Limits RPb Limit Notes Total Suspended Solids 95 2.5 mg/L 100 95 8t1-120 Duplicate (6L01002-DUPl) Prepared & Analyzed: 12/01/2016 13:30 Source: CZ16973-01 Spike Source %REC RPD Anal Result FIM MI. SLICE Level Resu %REC Limits RPD Limit Notes Total Suspended Solids 330 100 mg/L 340 4 20 Duplicate (6L01002-DUP2) Prepared & Analyzed: 12/01/2016 13:30 Source:CZ07890-01 Analld� Total Suspended Solids Batch 6LO5O22 - .Same Resu lC Elag EQL 62 25 Spike Source 9/aREC RPD Units Level Result %REC Urnib RPD Limit Notes mg/L 57 8 . 20 Blank (61.05022-BLKi) Prepared: W05/2016 13:27 Analyzed: 12/05/2016 16:31 Spike Source %REC RPD Anal Re;r11R ON PQL UAf14 Level Result 9/oREC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 1D mg/L LCS (6LOS022-BS1) Prepared: 12/05/2016 13:27 Analyzed: 12/05/2016 16:31 Spike Source %REC RPD Ana hd& Be.4Nlt an SQL Uns Level Resu R %REC Limits RPD Limit Notes Chemical Oxygen Demand 510 10 mg/L 500 101 90-110 Matrbi Spike (6LOS022-MSl) Prepared: 12/05/2016 1127 Analyzed: 12/05/2016 16:31 Source: CZ12923-01 Spike Source %REC RPD Anal lr3i: Result Elam POL Units Level Resu R a✓oREC Limits RPD Limit Notes Chemical Oxygen Demand 550 10 mg/L 526 24 100 90-110 Matrix Spike Dup (6LOS022-MSD1) Prepared: 12/05/2016 13:27 Analyzed: 17/05/2016 16:31 Source: CZ12923-01 Spike Source %REC RPD Ana tYbe Resu Elm eal. UnItS Level Resu k %REC Umi RPD Limit Notes Chemical Oxygen Demand 550 10 mg/L 526 24 100 90-110 0.4 10 Classical Chemistry Parameters - Quality Control Batch 6106OO9 - EPA 16648 Blank (61.06009-BLKl) Prepared: 12/06/2016 13:11 Analyzed: IV07/2016 14:42 Spike Source %REC RPD Anal ld?i: Result Ela9 Pal Udb Level Remelt %REC Limits RPD Limit t(Qbes Oil & Grease (HEM) 2.40 U 5.00 mg/L FINAL This report relates only roc the sample as received by the laboratory, and may only be reproduced in ft& Page 5 of 8 @ Fmm = NS � s ll� www.encolabs.com QUALM CONTROL DATA LD Classical Chemistry Parameters - Quality Control Batch 6LO6009 - EPA 16648 - Coni fnued LCS (61.06009-13SI) Prepared: 1VO612016 13:11 Analyzed: 12/07/2016 14:42 Spike Source %REC RPD A[a11de RKwu IE� Pal. Units Level Resuk %REC Limits RPD kaid Dotes Oil & Grease (HEM) 150 5.00 mg/L 159 94 78-114 LCS Dup (6L06009-BSDi) Prepared: 12/06/2016 13:11 Analyzed: 12/07/2016 14:42 Spike Source 9/oREC RPD _Analtde Rewlt EIM m Units Level Result 9/oREC Limits RPD Limit Notes Oil & Grease (HEM) 106 5.00 mg/L 161 66 78-114 34 18 QM-12 Matrix Spike (61.06009-MSIL) Prepared: 12/06/2016 13:11 Analyzed: 12/07/2016 14:42 Source: BZ05262-01 Spike Source %REC RPD Anal Result "m PPL Units Level Resuk °/DREG Lim RPD Limit Notes Oil & Grease (HEM) 168 5.00 mg/L 179 5.46 91 78-114 FINAL This report relates ony to the sample as received by the laboratory, and may only be reproduced in hAL Page 6 of 8 ENCO www.encelabs.corn FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. 3 The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-12 Precision between duplicate samples was outside acceptance. limits. FINAL This report reliYeas only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 8 EN c., ' NF rL S'OEO) -CUSTODY,'RECORD, VIRONMENTAL CONSERVATION LABORATORIESi CHAIN-OF- -(Ju I &ROD ctlrv� Nc 7P 11 !��T Fdm j�i,jj2Jjfj&!j I]'. in ln} 46-351h %Www4nitbkibsicom Non .91 • Mules, Eicp6dlt4d 0 u a 19 1 Im 0 pl�jm17 , ktail, aw 11MIULfla".0111Y) Wtll'dc M p toA 877-3.519 A=UNWROYLIble CZ - 1, -2 92 3 rye shmm it) Fl- .!�ws I tzlm-m pitl -W616 c6frmant9-i AN t1i I ie, yj v NA 310 <-- 1 2 --J �m', ?1116 IV RNMisi-hial nwrontm lli)vnhmwov% ACCOMWO' kwilb! awcwtaidoilifi6itso;a4l iootii t Ali gum wiltivWiftilu"i ill wqbpdL)1iJU W01 116jillil'1111 41U clYT11mmilill d i"Wo-i 01 NylltLn. Illivits . mvv�r, llikuu� - 701 - Z . .. Z- -1— ! . _ - .. .1. Sarole,Preservatian Verifcaton ,ENCO Cary 4*1. M k , *r;' CZ; 2923 Stasrmyat&� (jan,Juty) - Ctidnt KEL GdS SNACKSIAUS-nN FDt7I]S'(KEOIPP) Prujectl; [66ne} Logged In: 29-Nov-15 16.t2 Logge�_By; Ar�reuv S;C664 CZ12923-01 t.n✓ylii � -4 8 2.5OmLA+t42SE)�#' {2 ti' '1 h1A 1l ! Y NA — 250.'riLA+MZgQd :2• Y /C&,!'NA Y .N-/ NA D 2-5iOm P H2SQ4- _ 4 I NA Y (-,q)► NA CZ12S23 02- ��, pH lce7� _serst VN: ti�artttune B 2mlA+.kiZS0�4 _Z. — Y j{ NA 'Y NA C, 2WMLA+k2S64 -<2 Y 611 NA Y N - NA a rnLP+}i2 o4 Q.-,_ - YF) N. 1 NA Y ! NA Rea erit.Narrie _ID 4 2 _.. R e:M-Na-I. me- iD =4- Rea ent. Name .10 - 6 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCG060000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2016 CERTIFICATE OF COVERAGE NO. NCG06 0286 (This monitoring report is due at the Division no later than 30 days from EfV�d ty receives the sampling results from the laboratory.) FACILITY NAME _KelloggCom art - Cary, NC Faciii ��+ OUNTY Wake PERSON COLLECTING SAMPLES GregoryGr'egory Kane is DEC Z $ ZOi6 PHONE NO.( 919 ) 677-3292 CERTIFIED LABORATORY ENCO Las Lab # 591 Lab # CENTRAL FILES PLEASE SIGN ON THE REVERSE Part A: Specific Monitoring Requirements DWR SECTION Outfall No. Date ' Sarnple Collected, mo/dd/ r 00530 00400 00340 00556. 31616 Total Suspended Solids, inm pH,. Standard units Chemical Oxygen Demand, Oil and Grease,.. mg/L Fecal Coliform, Colonies per 1004&'>;' Benchmark - 100 Within 6.0 _ 9.0 120 30 1000 S WO 1 11 /29/ 16 5.5 1 7.5 24 <2.40 NA S W02 1 129 16 24 7.7 160 <2.40 NA Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected, moldd/ r 00556 00530 00400 Oil and Grease, Total Suspended Solids, pH, Standard units New Motor Oil Usage'; ;,, Annual avers a-, al/mo= ' Benchmark - 30 100 6.0 — 9.0 F-- Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses. See General Permit text. STORM EVENT CHARACTERISTICS: Mail Original and one copy to: Division of Water Quality Date 1 1/29/16(first event sampled) 0.06 Attn: DWQ Central Files Total Event Precipitation (inches): 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): S WU-249-102107 Page 1 of 2 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature M Permittee) (Date) S WU-249-102107 Page 2 of 2 "r . STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCG060000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2016 CERTIFICATE OF COVERAGE NO. NCG06 0286 (This monitoring report is due at the Division no later than 30 days the date the facility receives the sampling results from the laboratoi FACILITY NAME Kellogg Company -Cary, NC Facility COUNTY Wake PERSON COLLECTING SAMPLES Gregory Kane is Jeffre - O�tson PHONE NO. ( 919 ) 677-3292 CERTIFIED LABORATORY ENCO Las Lab # 591 Lab # PLEASE SIGN ON THE REVERSE Part A: Specific Monitoring Requirements F;M Outfall No. Date.: Sample Collected, mo/dd/ r 00530 00400. 00340 ::', 00556. 31616:. Total'Suspended- Solids, m pH; ` Standard units Chemical Oxygen Demand,--- t, ' Oil and Grease, _ mglL ;Fecal Cohfarm; .. Colonies per'160,nily; 'Benchmark' - 100 Within 6.0 — 9.0 120 30 1000.. . SW01 04/28/16 2$ 6.5 210 2,69 J NA o SW 1 05/12/16 NA NA 1,000 NA NA SW 5/29/16 NA 90 NA NA SW02 04/28/16 7.8 91 73 <2.40 Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements NA RECEIVED JUN 14 2016 CENTRAL. FILES MR SECTION Outfall No. Date Sample Collected, mo/dd/ r 00556 00530 00400 Oil and Grease, Total Suspended Solids,. pH, Standard units New Motor Oil Usage, Annual averse galtmo Benchmark - 30 100 6.0 — 9.0 - Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses. See General Permit text. Mail Original and one copy to: STORM EVENT CHARACTERISTICS: Division of Water Quality 04/29/16 Attn: DWQ Central Files Date (first event sampled) 0 68 1617 Mail Service Center Total Event Precipitation (inches): Raleigh, North Carolina 27699-1617 Datc05/12/16&05/29/16 (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): 0.56&1.95 SWU-249-102107 Page 1 of 2 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility o fines and imprisonment for knowing violations." Ll (Signat a of Per ittee) (Date) SWU-249-102107 Page 2 of 2 Via Certified Mail June 9, 2016 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 SNa Kellogg's Snacks Cary Bakery Operations One Quality Lane Cary, NC 27513 Ph 919.677.3200 Re: Reporting Year 2016 — Storm Water Discharge Monitoring Report Kellogg's Snacks — Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the first half of 2016 for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Anthony DePietro (919) 677-3292 anthony.depietro@kellogg.com Mr. DePietro is available should any questions or problems arise during the review of this DMR. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, Steve Surovec Plant Manager Enclosures r ENCO. . .. Laboratones - Agate. Timely. Responsive. Irmovative. 102-A Woodwinds Iindustrial Court Cary NC, 27511 v ,�1 O Phone: 919.467.3090 FAX: 919.467.3515 (� Tuesday, May 10, 2016'��] KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn. Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (]an,]uly) ENCO Workorder(s): CZ05296 Dear Rodney Bateman, JUA(14 zoi6 CENTF�4L FlL CwR SECTION Endosed is a copy of your laboratory report for test samples received by our laboratory on Friday, April 29, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as reo*ed by the tabmabwy, and may only be reproduced in M. Page L of S E�Ee) www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SW-01 Lab ID: CZ05296-01 Sampled. 04/28/16 18:20 Received: 04/29/16 08:30 pprameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Tiimc(s) EPA 1664E 05/26/16 05/04/16 10:51 05/04/16 16:39 SM 2540D-1997 05/05/16 05/02/16 10:20 05/02/16 10:20 SM 5220D-1997 05/26/16 05/03/16 10:21 05/03/16 13:36 diets ID: SW-02 Lab ID: CZ05296-02 Sampled: C14128/16 18:05 Received: 04/29/16 08:30 Parameter Hgjd Dabe m Prep Date/ Ime(s) Analysis Date/Time(s) EPA 1664E 05/26/16 05/04/16 10:51 05/04/16 16:40 SM 2590E-1997 05/05/16 05102V16 10:20 05/02/16 10:20 SM 52201-1997 05/26/16 05/03/16 10:21 05/03/16 13:36 HNAL ThIs report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 8 v _ �co www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: SW-01 Lab ID: CZ05296-01 Analy Results flag MDL ERL Units Method Ij Chemical Oxygen Demand 210 10 10 mg/L SM 522OD-1997 Oil & Grease (HEM) 2.69 3 2.40 5.00 mg/L EPA 16640 Total Suspended Solids 28 10 10 mg/L SM 254OD-1997 Client ID: SW-02 Lab ID: CZ05296-02 Ana h+te Results flag MDL M YBAR MeUpod r!4ffi4 Chemical Oxygen Demand 73 10 10 mg/L SM 522OD-1997 Total Suspended Solids 7.8 4.2 4.2 mg/L SM 254OD-1997 FINAL This report mates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 8 www.encolabs.com ANALYTICAL RESULTS Description: SW-01 Lab Sample IDCZ05296-01 Received: 04/29/16 08:30 Matrix: Surface Water Sampled:04/28/16 18:20 Work Order: CZ05296 Project: 5tormwater (Jan,July) Sampled By:7lmothy Klotz l aassical Chemistry Parameters ----11.—Y.---mm7—"" a»1 Analyte fCAS Numberl Results Fig units gf MDL PQL Babc.h MethadAnal 001:1 Chemical Oxygen Demand^ 210 mg/L 1 10 10 6E03009 SM 522OD-1997 05/03/15 13:36 JOC Total Suspended Solids^ 28 mg/L 4 10 10 6EO2003 SM 2540D-1997 05/02/16 10:20 MMR Classical Chemistry Parameters ^ - £NCO A7d rnire cfeGaraaW INC 4421 Anahrte FCAS Numberl $ate f6g units Df MDL EQL Batch Method Anahr"W Ay M2= Oil 8. Grease (HEM) [C-00071A 2.69 3 mg/L 1 2.40 5.00 6EO4008 EPA 1664E 05/04/16 16:39 SMA Description: SW-02 Lab Sample ID:CZ05296-02 Received: 04/29/16 08:30 Matrix: Surface Water Sampled: 04/2811618:05 Work Orden.CZ05296 Project: Stormwater (Jan,July) Sampled By:Greg Kanellis lClassical Chemistry Parameters ^ - ENCO Cary —bAe analyte (NC 5971 Analyte rCAS Numberl Results INS YAM L)f MDL p2L Batch Method Analyzed 9z N Chemical Oxygen Demand^ 73 mg/L 1 10 10 6EO3009 SM 5220D-1997 05/03/16 13:36 30C Total Suspended Solids^ 7.8 mg/L 1.67 4.2 4.2 6EO2003 SM 254OD-1997 05/02/16 10:20 MMR (Classical Chemistry Parameters ^ - ENCOJadQsaMB a cartAaal ar *te [NC 4421 Artayie rCAS Numberl Resuis Flag YAMS PE lu P46 Batch Method Anahrzed �y � Oil & Grease (HEM) [C-0007]^ < 2.40 mg/L 1 2.40 5.00 6ED4008 EPA 16646 05/04/16 16:40 SMA FINAL This report relabes only to the sample as received by the iaboratay, and may only be reproduced in full. Page 4 of 8 3 CSNSco www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6EO2003 - NO PREP Blank (6E02003-BLKl) Prepared & Analyzed: 05/02/2016 10:20 Spike Source %REC RPD Anal l(4C Result Elm IML Units Level Resu %REC Limtb RPb Limit Note$ Total Suspended Solids 2.5 U 2.5 mg/L LCS (6E02003-851) Prepared & Analyzed: 05/02/2016 10:20 Spike Source %REC RPD Anal i;esult Elm EQL Units Level Resu R %REC Limits RPD Limit Notes Total Suspended Solids 100 2.5 mg/L 100 100 80-120 Duplicate (6E02003-13UP1) Prepared & Analyzed: 05/02/2016 10:20 Source: CZ04512-01 Spike Source %REC RPD Anal Result Fla9 Pal tlnits Level Bog %REC Lirnlb RPD Limit Notes Total Suspended Solids 340 100 mg/L 350 3 20 Duplicate (6E07A03-DUP2) Prepared & Analyzed: 05/02/2016 10:20 Source: CZ01647-05 Anal Total Suspended Solids Batch 6EO3009 - Same IE WU 6w ML 500 100 Spike Source %REC RPD Units Level Resu cYcREC Limits RPD Limit Kom mg/L 590 16 20 Blank (6E03009-BLK1) Prepared: 05/03/2016 10:21 Analyzed: 05/03/2016 13:36 Spike Source %REC RPD Anal Resu Elm P4L units Level Resu %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (GE03009-BSL) Prepared: 05/03/2016 10:21 Analyzed: 05/03/2016 13:36 Spike Source %REC RPD Anal Resu F109 E41 Units Level Result %REC Limits RPD Limit Nogg Chemical Oxygen Demand 490 10 mg/L 500 98 90-110 Matrix Spike (6E03009-MS1) Prepared: 05/03/2016 10:21 Analyzed: 05/03/2016 13:36 Source: CZ01647-01 Spike Source %REC RPD Anal 1ltg RRIU Elm EQL Units Level Resu %REC Lim ils RPD Limit Wgift, Chemical Oxygen Demand 550 10 mg/L 526 25 100 90-110 Matrix Spike Dup (6E03009-MS01) Prepared: 05/03/2016 10:21 Analyzed: 05/03/2016 13:36 Source: CZ01647-01 Spike Source %REC RPD Anal Yle moult Fba EM Units Level Resu k %REC Limjt RPD Lim�i Notes Chemical Oxygen Demand 550 10 mg/L 526 25 99 90-110 0.4 10 Classical Chemistry Parameters - Quality Control Batch 6E04008 - EPA 1664A Blank (6E04008-BLK1) Prepared: 05/04/2016 10:51 Analyzed: 05/04/2016 16:40 Spike Source %REC RPD AealYte Result FINI eal. UJIUS Level Resu %REC Lim RPD Limit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L FiNAi This report relates only to the sarrrple as received by the labcratury, and may only be reproduced in full. Page 5 of 8 (o�Go www.encolabr.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Bauch 6EO4008 - EPA I664A - Conirnued LCS (6E04008-BSI) Prepared: 05/04/2016 10:51 Analyzed: 05/04/2016 16:40 Spike Source %REC RPb Anal vte Resuk E1a9 E111. Units Level Resu 9/6REC Limits RPD Limit Notes Oil & Grease (HEM) 136 5.00 mg/L 150 90 78-114 LCS bup (6E04008-BSD1) Prepared: 05/04/2016 10:51 Analyzed: 05/04/2016 16:40 Spike Source %REC RPD Anal Result am WL WHIZ Level ResuR %REC Limits RPD Limit Notes Oil & Grease (HEM) 157 5.00 mg/L 174 90 79-114 14 18 Matrix Spike (6E04008-MSI) Prepared: 05/04/2016 10:51 Analyzed: 05/04/2016 16:40 Source: CZ05296-01 Spike Source %REC RPD Anal Besu@ Flag MLL Units Level Resu(L %REC Limits RPD Lh= Notes Oil & Grease (HEM) 137 5.00 mg/L 154 2.69 87 78-114 RNAL This report relates only to the sample as received by the taboratory, and may only be rWrod-ed in U. Page 6 of 8 CS uco www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. 7 The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. F NAL This report relates only to the sample as received by Mre lab=bory, and may only be reproduced in tali. Page 7 or 8 I0775 Contial Port Dr. Orlando, FL 32824' (407) 826-5314 Fax (407) 650.6945 4810 EKaCuWa Park Court, suits 111 JacksorMile, FL 32216.8069 (904) 296.3007 Fax i9W) 29G-9210 102•A Woodwinds Industrial Cl, Cary, NC 27511 (919)167-3090 Fox(919)467.3515 Paae 1 ' O, I 1 Client Narita' " ' ' } KELLOGGS SNAG PM*l Number Requested' Analyses Requested Turnaround Times Note :push requests subject to a000Mr" by the lKIhty % Standard — Expedited Due—�— ..❑ a «CVV4 � � 0' O to (f} (fi � _ Address E QUALITY Pro)ed NamolDaso City/ST/Zip NC 7513- PO 0 / BillIng Into Tel' 919 6774619 Fuii Reporting Contacl Rodney Bateman Sampler(s) Nanw., Alliliallon (Print) BRt ng ConlaM Accounts Payable Sampier(a) Signatura^ rl-L5�lionITino_ Zone Lab Workorder ' 'Preservation (See Cadesf (Combine as'nocossary) Ilam 0 c Semple ID (Field Identill"i6n) . • Cclloc'tion Data' Coilaction Time Comp! Grab Matrix (see codes) . Total 11 of . Contalners Sample Comr1'Ients u alb 1 1°�4 fib < Total # of Containers r Semple Kit Prepared By Datofrima ; RoHnquishod By Dal Roco3_vod By, Deleirri I ma CammonislSpeolai Re In 9 ilequlromsnta R@linqulshod By DatoRme Rviceivod By Dat�ma Ralinquishoci By Date/Tima Homived By . Dato/nma J Coobr e's & Temps on Rocpipt Cardtlon Receipt nnri • `"1 (,. Acceptable Unacceptable +emmr: [itr ureunewater uu.uorr OWunn" Waier"Stt-tml 11en1 row.,gurfaCa Water w w-waaiawator A•Alr O-Other (astae rn Comments) Preservation: (•Ice, WHO N•HNO3 S•H2$04 NO-NaOH O-Olhor (UeW N ConVnent!) l Note; All samplas submitted to ENCO Labe are in ecMdrince with the forms and conditions Usled on the reverse of this lorm, unless prior written agreements exist Sample Preservation Verification ENCO Cary Work Order: CZ05296 Project: Stormwater (Jan,July) Client KELLOGGS SNACKS/AUSTIN FOODS (KE006) Project #: [none] Logged In: 29-Apr-16 09:49 Logged By: John C King CZ05296-01 Ct�ni ype � � Requlr�rn6141GP" VH Adtusted r := Date1,T► 1e iEi€ r AL�U�aCU Reagent U§FXUC...amr4 i�dM B 250mLA+H2SO4 <2 VV, Y'/` 1 NA EC 250mLA+H2SO4 <2 Y/ 1 NA D 250mLP+H2SO4 <2 1 N 1 NA I Y/ ! NA CZ05296-02 i3ant TypepROw&eid wmRe�nt 1) not f_ Adjusted m� B 250mLA+H2SO4 <2 I N I NA Y/ / NA C 250mLA+H2SO4 <2 l N I NA Y/ 1 NA D 250mLP+H2SO4 c2 / N/ NA Y 1 I NA Reagent Name ID 1 2 R eacient Name ID 3 4 Rea ent Name ID 5 6 Page 1 00� FN.CO Laboratones Aeearwie 'Trincly. Responsive. Imerxiaative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, May 24, 2016 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater CAS ENCO Workorder(s): CZ06903 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, May 13, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report reMes only to the sample as m"e yed by the laboratory, and may only be reproduced in full. Page 1 of 7 SIM41no 1111111111� - I ) www.encolabs.com SAMPLE SUMMARY/ LABORATORY CHRONICLE Client ID: SW-01 Lab ID: CZ06903-01 Sampled: 05/12/16 20:20 Received: 05/13/16 09:SS Parameter b m PrrenDate/Trme(sl Analysis DaielTimefsl SM 522OD-1997 06/09/16 05/23/16 15:52 05/24/16 10:17 FINAL This report relates only to the sample as reodved by the laboratory, and may only be reproduced in full. Page 2 of 7 �uco www.enaola b&com SAMPLE DETECTION SUMMARY Client 10: SW-01 Lab ID: CZ06903-01 J Ana hrte Results Elm M ERL unb Method Notes Chemical Oxygen Demand 1000 20 20 mg/L SM 522OD-1997 FINAL This report nelabEs only to the sample as received by the laboratory, and may only be repradi in fun. Page 3 of 7 0 F.�VCO www.encolabs.com ANALYTICAL RESULTS Description: SW-01 Lab Sample I D: CZ06903-01 Received: 05/13/16 09:55 Matrix: Surface Water Sampled:05/12/16 20:20 Worts Order: CZ06903 Project: Stormwater CAS Sampled By:Greg Kanellis Classical Chemistry Parameters ^ - MCO Cary ceoMmd a-W [NC 5911 Analyte [CAS Numbers Rgs fwg MORE Pf MDL EQJ DA=h Method AnaOX N Cynical Oxygen Demand- 1000 mg/L. 2 20 20 6EZ3030 SM 52200-1997 05/24/16 10:17 10C FINAL This report relates arty bD the sample as received by the laboratory, and may only be reyradwed in fLA. Page 4 of 7 (� �Go www.encolahs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batt* 6E23O3O - Same Blank (6E23030-BLKl) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Spike Source %REC RPD Anal ResuR Sao POL Was Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (6E23030-BSJ) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Spike Source %REC RPD Anal lde Result Elm PQL Units Level ResuR %REC Limits RPD Limit Notes Chemical Oxygen Demand 490 10 mg/L 500 96 90-110 Matrix Spike (6E23030-MS1) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 Source. C512441-01 Spike Source %REC RPD Analvte Result Flag —PQL Units Level Resuk '/oREC )Limits RPD Lkaft god Chemical Oxygen Demand 550 10 mg/L 526 35 97 90-110 Matrix Spike Dup (6E23030-MSD3) Prepared: 05/23/2016 15:52 Analyzed: 05/24/2016 10:17 11 Source: C512441-01 Anand& Chemical Oxygen Demand Spike Source %REC Result Eli= EQL MD& Level gig %REC Limits RPD 560 10 mg/L 526 35 100 90-110 3 RPD Limit Notes 10 FINAL This report relates only fo the sanjoe as repeived by the laboratory, and may only be reproduced In fuR. Page 5 of 7 (��Ee) www.encolabs.com FLAGS/ NOTES AND DEFINMONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. RN& This report miates only to the sample as received try the laboratory, and may only be reproduced in NO. Page 6 of 7 ENVIRONMENTAL<CONSERVATION.LABORATORIES, CHAIN-OF-CUSTODY'RECORD' www.encolabs.com 10775 Cornrbl part 0;- N 481D Ewcuuw Part cuud, Suito 111 102-A Woodwioft 111d„sliiad Cl.' Brlundu, FL3:.+B+i', lackoanaillo F1.31:r10OD69 Car tIC27611 - f40ria28-531 1 'Fni {40r1050 6946 (004),276.30D7'- Fa1t (90.11x96,G210 IgI91 467.3090 FBI1919) 467.31,15 "!:* — Q(; Srrmpla Ril prols,7rad i3y, U sla'1 iC., lWinrulshad ey I ,� - Oaleflim0: Recalvad By. Da ll-w CorryranlalIl5.p}ncol_Ra�oftrlyR1Wuilunlunls Rrliniriibh6dDy -. .. p,ilu 1rno Ro1oivnd9 Y• . at . ima f� 11 `! h• f Ralad inquishHy, Dalenime FlacoWd 8y Ua7a/Timc "lnr n'q g Trtmpa an Rrx ipl 6� Cann tirxl U an pwMIp1 Unacce tahl© Nlnttix:6W;GraurWwalor,SD•SoIIDW;DrinkingWnlor-SE•Sodmpnt,SMl•Su4iro tor,WWWmtowslor A•+Ur;p•01ha/;dDlNimcommwtaf ProWtvatlon:Waa:H•HCI-N•.HND3.8•H23UA;NONoOH,,O.Othartdolal*ncommonis) N01e Ati 5arl>plt-Y au4rrtiIInl to CNCO L'8tys ero In aor:uitl9rton,w:lh 11ic toms arid�curirliliuru.li.lvif wt Ilw rmvrn;o of tldti io�m, unlo� a prior wrglcn :rgmvmrnts oi'r.7 I SAMple.-Preservatldh Veriftcaition VjC W&WOrder Order:' CZ06903 v Project: ol Stormwater'CAS .Gliiafit- KELLOGGS SNACKS/AUS-tiN FOODS (KEOG Pfopic"t fn6hej Logged In. 13-May�.16 13*12 CZ06903.61 , Lagged By:' Andr6W S.C66ns M NA Reagent Name ID. 2 Aeagent Name' ID 41 Reagent Name ID 5 6 Pape- 1. of FW.-CO Laboratones AcewAte. Timer. Responsive. Innovative. 102-A woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, June 9, 2016 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE GORY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater CAS ENCO Workorder(s): CZ07915 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, May 31, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in fup. Page 1 of 7 (96M.P.) www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE alent ID: SW-01 Lab ID: 1207915-01 Sampled: 05/29/16 88:55 Received: 05/32/16 10:03 Parameter }cold Date/Trmefs) P s AfWIYSiS DaLc�Time(s) SM 5220D-1997 06/26/16 06/07/16 11:57 06/07/16 14:30 FINAL Thus report relates only to the sanoe as received by the laboratory, and may only be reproduced In f AL Page 2 of 7 (E.�Go www.enoolabs.com SAMPLE DETECTION SUMMARY Menc m: sw-01 Lab ID: (Z07915-01 Ana Results E619 MID& ML VD-ft � Chemical Oxygen Demand SD 10 10 mWL SM 522OD-1997 FINAL 1hs report relates only to the sample as received by the laboratory, and may any be reproduced to U. Page 3 of 7 (FJ�Ge) www.encolabs.com ANALYTICAL RESULTS Description: SW-01 Lab Sample ID:CZ07915-01 Received: 05/31/16 10:03 Matrix: Surface Water Sampled: 05/29/16 08:55 Work Order: CZ07915 Project: Stormwater CAS Sampled By-; Jeffrey OlEison Classical Chemistry Parameters - ENCO Cary -r6'W anaW (NC 5911 Analvte rCA5 Numberl Resu gag unite U MDL ML Batch Ry Chemical Oxygen Demand^ 8o mg/L. 1 10 10 6FO7018 SM 5220D-1997 06/07/16 14:30 30C FINAL Thm report rdaaes any to the sample as received by the laboratory, and may ony be reproduced in U. Page 4 of 7 9�Go www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Ba11d1 6FO7O18 - Same Blank (6FO7018-BLKI) Prepared: 06/07/2016 11:57 Analyzed: 06/07/2016 14:30 Spike Source %REC RPD Anal E Result Flag POL Unhs Level Result MoREC Llmft RPD Limit Nis Chemical Oxygen Demand 10 U 10 mg/L LCS (6F07018-BS1) Prepared: 06/07/2016 11:57 Analyzed: 06/07/2016 14:30 Spike Source %REC RPD Anal Result ELM i OL units Level ResuR 9/aREC Limits RPD Limit Notes Chemical Oxygen Demandt 490 10 mg/L 500 99 90-110 Matrix Spike (6FU7018-MS1) Prepared: 06/07/2016 11:57 Analyzed: 06/07/2016 14:30 Source: CZ01299-01 Spike Source %REC RPD AL+aIILt& Result EIM PQ—LL Units Level sesu %REC Limits RPD Limit Notes Chemical Oxygen Demand 1500 20 mg/L 1000 590 95 90-110 Matrix Spike Dup (6FO7018-MSD1) Prepared: 06/07/2016 11:57 Analyzed: 06/07/2016 14:30 Source: CZ012B8-01 Spike Source %REC RPD Anal Resu Elm ML 1l11lL4 Level gesu %REC Limits RPD U -tt Nis Chemical Oxygen Demand 1500 20 mg/L 1000 590 94 90-110 0.3 10 FINAL ih6 report relates only to the sample as recoved by the laboratory, and may argy be reprvduoed in M. Page 5 of 7 (E�0 www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL. This report relates only to the sample as received by the laboratory, and may only be reproduced in U. Page 6 of 7 — - r•••f••v••ofr •••r•r'VV••VrPf•rf r rvf rfrrfw•Vrrr••f f,vfrrrV.� vffrfu\^Vr vVvr vfrr- rxY%f%fvl r - - '• - ARef•CI�LV�Qi:�7•�ylfl - i• N I �� •~ 110775 Contral Port Dr, r . 4610 Executive Park Court. Suite 111 _ .. 102-A woodwinds Industrial CL Orlando; FL 32824 ,faprspnvllle, FL 32218.6089 Cary, NC 27511-e ,, i (407) 926.5914 Fax (40p 85D-G945 {9N) 296,IW7 Fax (ON) 296.6210 1919f 467-3t)90 Fax (919) 467.3515 Page j Of 1 Mont Noma �!f Pro)oq Number Requested analyzes Requested Turnaround, Times Note: Hush requests subian 10 apesptarrcabythe Gacfliry _X'Standard _Expedited Due � r° �) (�" `�► ' Q. v _ - Address ' rr' '��" t%/)t?. �yr�i LaKe Prc4w NamalDesc S j'tiP1►114+rrlQ, �/Q,� Ciry/sTiziip PO e 1 Billing info , Tat: s h. tg'} 7?-3'Siq Fax RoportingContact 60d+�e �rr{enlan Samplers) -Name, Anitiatlon (Prim) _ Ming Conran n45, Yoke sampler Ignatu Silo LOM604iITimezorle LabWorkorder Preservation )Sao Codes) (Combine ns necessary) llomp t' "sampl0ID{FiotdtdeAlifloatlon)' ColleationWite Colfdction Tiro ComplGrab Matrix (see codes) Total v of Containers Sample Comments SS &t,7 b 5 tv 1. X V. i . i.. t �i•I��®i•■■tit�®®® MM®M®M®®®M MMMMIMPI 5wnpl0 Hlt Prepared By 7Dat MMMMMM��� ofnmo ROfinquIshed ey DatoMmo Received B Dale l GOmmOntslSpacial Reporting RequirpmpnLt - Relinquished By, DataMmo Rocelvad By D tpR Ctnai t 4.0 4 ..9: A ccm RalEnquishad By DaldT me !Ikelvpd By Dold lime' Cooler Cr. d Temps on Receipt Cond lion RDcaipt Acceptable ' Unacceptable i; •Matrix;GWGrrsurKl-Amlof So•Soi1DW.Vdnk)ngWaler SE•SedImoni 5w..Surtacowator WM-Waslowatar AWr0-00ior{duta9inc#rnmorvs)' Praserimtion:I-Ito,M,HCI N•HNO3'S•HZSO4 ND-NifOH DOthar(detalllncommorls) "ale: All,sampl©s submitted to ENCO Labs are in accordance wish the terms and =W,iims Gsiod on the (worse of this lofm, onloss prior writlon agree mama exist lam- i; •Matrix;GWGrrsurKl-Amlof So•Soi1DW.Vdnk)ngWaler SE•SedImoni 5w..Surtacowator WM-Waslowatar AWr0-00ior{duta9inc#rnmorvs)' Praserimtion:I-Ito,M,HCI N•HNO3'S•HZSO4 ND-NifOH DOthar(detalllncommorls) "ale: All,sampl©s submitted to ENCO Labs are in accordance wish the terms and =W,iims Gsiod on the (worse of this lofm, onloss prior writlon agree mama exist lam- Sample Preservation Verification ENCD Cary CMWQ. Work Order: CZ07915 Project: Storrimwater CAS Client: KELLOGGS SNACKWAUSTIN FOODS (KE006) Project M [none] Logged In: 31-May-1611:06 Logged By: John C King CZ07915-01 !qt PreSF =Checked ,aaQffiel�ltil� in,Controi,usted `*q�d;' t - 1 ,F�teagensedlCornmer�ts 250mLP+H2SO4 <2 Y' 1 N / NA Y 1 / NA Reagent Name ID 1 2 R eacient Name ID 3 4 Rea ent Name ID 5 6 Page 1 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCG060000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 CERTIFICATE OF COVERAGE NO. NCG06 0286 (This monitoring report is due at the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME _ Kellogg Company - Cary, NC Facility COUNTY Wake PERSON COLLECTING SAMPLES KiU Hiortdahl PHONE NO. 9( 19 ) 677-3292 CERTIFIED LABORATORY ENCO Las Lab # 591 Lab # PLEASE SIGN ON THE REVERSF—>.., Part A: Specific Monitoring Requirements 11 NOv � % 10 „•Outfall Date Sample Collected, mo/dd/ r 00530 00400 00340 00556 31616: Total Suspended Solids, pH, Standard units Chemical Oxygen Demand, m Oil and�GLrease,. m Fecal p� ;SF . Colonies ` mj Benchmark 100 Within 6.0 — 9.0 120 30 1000 S W01 10/27/ 15 6.9 6.4 110 4.12 NA SW02 10 27115 3.7 6.8 2.9 <2.40 NA Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier I or Tier 2 responses. See General Permit text. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —yes Xno (if yes, complete Part B) Part B: Vehicle Maintenance Activitv MonitorinE Requirements fit, Outfali No: Date -Sample Collected, mo/dd/ r 00556 00530 00400 Oil and Grease, m Total Suspended Solids, pH9 Standard units New Motor Oil Usage, Annual average al/mo _Benchmark 30 100 6.0 -- 9.0 Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier I or Tier 2 responses. See General Permit text. STORM EVENT CHARACTERISTICS: Date 10/27/15(first event sampled) 0.15 Total Event Precipitation (inches): Date (list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): Mail Original and one copy to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 'ILES TION '4 0"4C S W U-249-10210� Page l,of "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." t (Signature of Pe ittee) (Date) S W U-249-102 t 07 Page 2 of 2 November 17, 2015 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED NOV 2 3 2015 CENTRAL FILES DWR SECTIOr" Re: Reporting Year 2015 — Storm Water Discharge Monitoring Report Kellogg's Snacks — Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, SNACKS Kellogg's Snacks Cary Bakery Operations One Quality Lane Cary, NC 27513 Ph 919,677.3200 Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the second half of 2015 for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No, NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is Mr. Joseph Atkinson (919) 677-3292 joseph.atkinson@kellogg.com Mr. Atkinson is available should any questions or problems arise during the review of this DMR. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, Steve Surovec Plant Manager Enclosures 0 ENCO Laboraton"es Accurate. Timely. Respmesive. Irmpvatiue. 102-A woodwinds Industrial Court Cary NC, 27511 Prone: 919.467.3090 FAX: 919.467.3515 Thursday, November 5, 2015 KELLOGGS SNACKS/AUSiIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (Jan,3uly) ENCO Workorder(s): C505328 Dear Rodney Bateman, Endosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, October 27, 2015. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 19,M N- N. %� Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as reoetved by the laboratory, and may only be reproGuced in U. Page 1 or 8 OR WS - e 0) www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SW-01 Lab10, C505328-01 Sampled: 10/27/15 08:20 Received: 10/27/15 09:3E1 Parameter EPA 1664B Hotd bate/Time(s) 11/24/15 11/03/15 ] Anahrsis Date/Timels] 15:32 11/05/15 17:23 SM 2540D-1997 11/03/15 10/29/15 13:40 10/29/15 13:40 SM 4500H+B-2000 10/27/15 08:34 10/28/15 08:50 10/28/15 08:50 SM 5220D-1997 1IJ24115 10/30/15 12:15 10/30/15 18:10 Clie tID: SW-02 Lab ID: CS05328-02 Sampled: 10/27/15 08:30 Received: 10/27/15 09:30 ftra Hold Date/Time(s) Preo DatcMme(sl Analysis Date/Time[sl EPA 1664E 11/24/15 11/03/15 15:32 11/OS/15 17:23 SM 2540D-1997 11/03/15 10/2SV15 13:40 10/29/15 13:40 SM 4500H+B-2000 10/27/15 08:44 SM 5220D-1997 11/24/15 10/28/15 08:50 10/28/15 08:50 10/30/15 12:15 10/30/15 18:10 FINAL This report relates oc* to the sample as received by the laboratory, and may only be reproduced in fug. Page 2 of a CAr C www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: s wai Lab ID: CSOS328-01 Anylltte Results 9n Nu EQL !wu Method Nglin Chemical Oxygen Demand 110 10 10 mg/L SM 5220D-1997 Oil & Grease (HEM) 4.12 J 2.40 5.00 mg/L EPA 1664B PH 6.4 1.0 1.0 PH SM 4500H+B-2000 Q-01 Total Suspended Solids 6.9 2.5 2.5 mg/L SM 2540D-1997 Client ID: SW-02 Lab ID: C5O5328-02 Awdft Results tin MDL PQS mat Mr Notes Chemical Oxygen Demand 29 10 10 mg/L SM 5220D-1997 PH 6.8 1.0 1.0 PH SM 45DOH+6-2000 Q-01 Total Suspended Solids 3.7 3.3 3.3 mg/L SM 2540D-1997 FINAL This report relates (rely to the sample as received by the laboratory, and may only be reproduced in full. Page 3 or 8 0 F. ... NS, www.en—dabs.com ANALYTICAL RESULTS Description: SW-01 Lab Sample ID:C505328-01 Received: 10/27/15 09:30 Matrix: Surface Water Sampled:10/27115 08:20 Work Order: C505328 Project: Stvrmwater ()an July) Sampled By: Kitty H. (Classical Chemistry Parameters ^ - SCO wry cerdhed amyl' [AC 5Yi] Analyte rCAS Number? Results i36w units DF MOL ML patch Method Analyzed 111 N Chemical Oxygen Demand 110 mg/L 1 10 10 5130015 SM 522OD-1997 10/30/15 18:10 JOC PH- 6A prH 1 1.0 1.0 532BW5 5M 4500H+B-200C 10/28/15 08:50 AEB Q-01 Total Suspended 5olidsA 6.9 mg/L 1 2.5 2.5 5129005 5M 254OD-1997 10/29/15 13:40 MMR Classical Chemistry Parameters ^ . FJIrCOJarksnnx!!e Cer6fiBd analyfr /AC- 4421 Aoalyte rCAS Numbed Ftesw In Units 12E 91A PStL Rauh Method Ana !}1[ 1 Oil & Grease (HEM) [C-M7]A 4.12 l mg/L 1 2.40 5.00 SK03012 EPA 1664B 11/05/15 17:23 SMA Description: SW-02 Lab Sample ID:C505328-02 Received: 10/27/15 09:30 Matrix: Surface Water Sampled:10/27/15 08.30 Work Order: C505328 Project: Stonnwater (Jan,July) Sampled By. Kitty H. lClassical Chemistry Parameters ^-6vcaOvyceVWa 4 e[NC 5911 AMalyte 1CA5 Number] Resu f EIN kiln RE MDL ERL Rauh lam+ Anal3zed lilt tlffia Chemical Oxygen DemandA 29 mg/L 1 10 10 5330015 SM 5220o-1997 10/30/15 18:10 JOC PHA 6.8 pH 1 1.0 1.0 5J28005 iM 4500H+B-200C 10/28/15 08:50 AE9 Q-01 Total Suspended Solids^ 3.7 mWL 1.33 3.3 3.3 5JZ9005 SM 25QD-1997 10129/15 13:40 MMR Classical Chemistry Parameters ^-&%COJadsanx7lemtlrredamlrre[NC 442] Rend am mom 12E MM EQL !Ih Wthod Analyzed ft 11Q= Oil & Grease (HEM) [C-0007]A < 2.40 mg/L 1 2.40 5.00 5K03012 EPA 1664E 11/05/15 17:23 SMA FIMA.L This report relates orJy to the sample as received by the laboratory, and may only be reproduced in cur. Page 4 of 8 www.enColahe cam QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Ba5d15J28005 - NO PREP LCS (5328005-B$1) Prepared & Analyzed: 10/28/2015 08:50 Spike source %REC RPD Anallft Result Bag P4L Units Level Result %REC Limlts RPD Limit Notes pH 6.9 1.0 PH 7.00 99 99-101 Duplicate (532800S-DUPI) Prepared & Analyzed: 10/28/2015 08:50 Source: C505328-01 Spike Source %REC RPD Ana hBs Result Bag EQL Units Level Result %REC Limits RPD Limit Notw pH 6.3 1.0 pH 6.4 0.5 25 Bak* 5J2900.5 - NO PREP Blank (532900S-BLK1) Prepared &Analyzed: 10/29/2015 13:40 Spike Source %REC RPD Ana ltde Re51dt flag PQL units Level RespAt %REC LIMI RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (5129005-B51) Prepared & Anaiyced: 10/29/2015 13:40 Spike source %REC RPD Andhds Result Bag POL Unit& Level Result %REC Limits RPD Limit Notes Total Suspended Solids 97 2.5 mg/L 100 97 80-120 Duplicate (5329005-DUP3) Prepared & Analyzed: 10/29/2015 13:40 Source: C511167-01 Spike Source 9yoREC RPD Anal *rte Result Hag RQL Units Level gesul %REC Limits RPD Limit Notes Total Suspended Solids 88 50 mg/L 94 7 20 Duplicate (5329005-DUP2) Prepared & Analyzed: 10/29/2015 13:40 Source: C511948-01 Spike Source %REC RPD ABande Result Hag QQL Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 240 100 mg/L 260 6 20 Bahalr 57301015 - Same Blank (SI30015-BLKI) Prepared: 10/30/2015 12:15 Analyzed: 10/30/2015 18:10 Spike Source %REC RPD Anal ttte Result 13sig ffiL UAiif Level Resul 4/6REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (5330015-BS1) Prepared: 10/30/2015 12:15 Analyzed: 10/30/2015 18:10 Spike Source %REC RPD Ana ht4e Res3dt Bag ML Units Level Result %REC Llltliss RPD limit NQ&w Chemical Oxygen Demand 490 10 mg/L 500 98 90-110 Matrix Spike (5130015-14151) Prepared: 10/30/2015 12:15 Analyzed: 10/30/2015 18:10 Source: CSWS49-01 Spike source %REC RPD AAai>� Rend Bag FUL units Level %REC Limits RPD Limit Notes Chemical Oxygen Demand 770 10 mg/L 500 310 93 90-110 FINAL This report relates only to the sample as received by die lahaatory, and may only be reprod- in lull. page 5 of 8 4ti 4r www-encolahr-com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch SJ30015 - Same - COnd=red Matrix Spike Dup (5730015-MSDl) Prepared: 10/30/2015 12:15 Am": 10/30/2015 18:10 Source: C500548-01 Spike Source %REC RPD Anal ReSW Flag PQL Units Level Result %REC Limits RPD Limit lYOW& Chemical Oxygen Demand 760 10 rtrg/L 500 310 90 90.110 1 10 Classical Chemistry Parameters - Quality Control Batdt SK93012 - EPA 16641A Blank (SK03012-BLK1) Prepared: 11/03/2015 15:32 Analyzed: 11/05/2015 17:23 Spike Source %REC RPD Ana h0S Rexu1L Elam E01. Units Level lid! %REC Limits RPD mi& Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (SK03012-651) Prepared: 11/03/2015 15:32 Analyzed: 11/05/2015 17:23 Spike Source %REC RPD 8na Boult FIM P9.6 Units Level R %REC Limi RPD l i! al n4te& Oil & Grease (HEM) 40.9 5.00 mg/L 42.1 97 78-114 LCS Dup (SK03012-BSDl) Prepared: 11/03/2015 15:32 Analyzed: 11/05/2015 17:23 Spike Source %REC RPD Ana hfte Result Big PGL Unitf Level Bl5 d %REC Limits RPD Limit Notes Oil >1 Grease (HEM) 35.6 5.00 mg/L 41.9 85 78-114 14 18 Matrix Spike (SK0301244S3) Prepared: 11/03/2015 15:32 Anayzed: 11/OS/2015 17:23 Source: B504527-01 Spike Source %REC RPD A Resin 1922 PQL units Level gt ldt %REC Limits RPD mit Notes Oil & Grease (HEM) 755 5.00 mg/L 155 521 151 78-114 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 8 www.enculabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. Q-01 Analysis performed outside of method - specified holding time. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LC5 recovery. FINAL This report relates only to the sample as received by the laborarory, and may only be reProdvoad in U. Rage 7 of $ �- 10775 Central Pon Dr. 4810 Exeaniva Park Court, Suite 111 102•A Woodwinds Industrial Ct. - - . r Le ..N: Dtlaedo, FL 32824 Jacksorwlne, FL 32216-8084 Cary, NC 27511 - (407) 826-5314 Fax (407) 85"945 (904) 296-3007 Fax (904) 298-8210 (919) 467.3090 Fax (919) 467.3515 Page of Client Name Project Number Requested Anstys" Requested Turnaround Times Note :Rush requests subject to acceptame, by the lacinty . Standard , _ Expedited Due 0 I CNI N O 01 - m r 06 o - CIO . _ g � a (n .. Address - - • ` —ONE , LANE- -._Stormwater Project amoluesc Jan J U! CityfSULP CARY .NC 75 3- PO # f Bitting Into 4200294236 Tel 919 677-3519 Fax Reporling Contact RodneV Bateman Sampler(s) Name. Allihutlan (Print) 'PFRat#y-Klein— B ng Contact Accounts Payable Sampler(s) Signature Site Location f Time zone Lab Workorder C505328 ' Pr4laarvftlon (Sea Codes) (Combine as necessa ) Ile- # Samoa IID) (Fiell�d� Identification) Cotleetoom Bate Cdloclicn Time Comp / Grab Matrix (see codes) Total f of Containers - Sample Comments Sw-0•Z 2� 5�30 14 'Z. 1 n 7 Total # of Containers Semple Kit Prepared By _ m D alome li R gnquiehad f_ Daterimo Roc ' B (•� pat o a z7 f.�: 9�a Comments/Spoelal Raporting Roquirotnera —{-�� Rennqutahod By Datef ime Received By Datemmo tt1111 C!1 1" Relinquished By Datoffine Received By DaterNmo 1�n �'y ` c-LA %w-L . C��;vcr,�.3 10E . Caofar 4'a mps an R pt a - �U .z r- Catdition U RawlPt �! Acceptable ..,_,_ Unacceptable Matrix: GW-Groundwater S0Sa_ d DWDrkWng Water sE•Sadimmtt SW-Surlace water WW-ftstawatar A•Alr O.Other (detail 16 comments)-PI'aaar"Uon: I•Ica H•HCI N•HNO3 S•H2SO4 ND•NaOH-O.Olher (datall In comments) Note: All samples submitted to ENCO Labs are in accordance with the terms and conditions listed on Itw reverse of ibis form, unless prior written agreements exist - Sample Preservation Verification ENCO Cary Work Order: C505328 Project: Stonmvater (Jan,July) Client: KELLOGGS SNACKS/AUSTIN FOODS (KE006) Project M [none] Logged In: 07-Oct-15 09:31 Logged By: John C King C50S328-01 ype -- - - ttr - - sted l,lsedlCommersts A 1 L.A+H2SO4 <2 Y/ N l 9 Y/ N I B 1 LA+H2SO4 <2 Y/ N/ W Y/ N/ E 250mLP+H2SO4 <2 / N/NA1Y/6 I NA - C505328-02 Cant ype Ltequinam �tn Co MME p OEM — i�sedlCansmerrls, " A A 1 LA+H2SO4 <2 Y/ N I& Y/ N I B 1LA+H2SO4 <2 Y/ N I Y/ N/ 10 E 250mLP+H2SO42 1 N/ NA Y! (N) / NA Reagent Name ID 1 2 Rea ent Name ID 3 4 Rea ent Name ID 5 6 Page 1 r STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCG060000 CERTIFICATE OF COVERAGE NO. NCG06 0296 FACILITY NAME Kellogg Company - Cary, NC Facility PERSON COLLECTING SAMPLES KittX Hiortdahl CERTIFIED LABORATORY ENCO Las Lab # 591 Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2015 (This monitoring report is due at the Division no later than 30 days from the date the �fac' i�receives the sampling results from the laboratory.) �� vUNTY PHONE NO. Wake 677-3292 Za15PLEASE SIGN ON THE REVERSE 4 CEN-rJRAL FILES DWR SECTION Outfall Date ,;:. :. 00530 .. , ;00400 00340 " 00SS6 31616 Not ;Sample =Total.Suspended' r° ', pH,.:- Chemical,Oxygen Oil and Grease, Fecal Coliform,_ Collected, _ Solids, StandardLunits ' Demand, .��' mglI, �.Colonies.per 100 ml ' moldd/ in` m r -Beiichmark'AA ;� _ T ;100 = 'Within'6.0=9.0 120 ` 130 1000 SW01 04/30/15 NA 6.7 54 <2.40 NA 6.1 Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses. See General Permit text. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —yes Xno (if yes, complete Part B) Outfall Date' ''" 00556 00530 00400 No Sample, Collected; Oil;and'Grease, Total Suspended Solids, . pH, New Motor Oil Usage, mo7ddl r ` m m Standard unitsAnnual 'average gaUmo°. Benchmark. x , 30 100 ' , 6A -- 9.0 . Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses. See General Permit text. STORM EVENT CHARACTERISTICS: Mail Original and one copy to: Division of Water Quality Date 04/30/15(first event sampled) 0.58 Attn: DWQ Central Files Total Event Precipitation (inches): 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date 06/01/1 list each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): 0.34 C2 090 .me. S W U-249-102107 Page 1 of 2 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 6/8/15 (Date) S W U-249-102107 Page 2 of 2 ENCO Laboratories Accurate_ Timer Responsive ]mrarastive. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Thursday, May 28, 2015 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Starmwater (Jan,July) ENCO Workorder(s): C502865 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, May 1, 2015. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as reo0fi d by the laboratory, and may only be reproduced in full. Page 1 Of 8 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SW01 Lab ID: C502865-01 Sampled: 04/30/15 19:00 Received: 05/01/15 09:39 Parameter Sri j Analysis DaWTiimefs] EPA 16648 05/28/15 05/12/15 09:56 05/13/15 14:15 SM 4500H+B-2000 04/30/15 19:14 05/04/15 14:03 05/04/15 IC03 SM 5220D-1997 05/28/15 05/05/15 12:54 05/05/15 16:13 ClientI0: SW02 Lab ID: C502865-02 Sampled: 04/30/15 19:15 Received: 05/01/15 09:39 Parameter Prep DabefiUme(s) Analysis DatelTime[s] EPA 1664B 05/2B/15 05/12/15 09:56 05/13/15 14:15 SM 2540D-1997 05/07/15 05/04/15 08:45 05/04/15 08:45 5M 4500H+B-2000 04/30/15 19:29 05/04/15 14:03 05/04/15 14:03 SM 5220D-1997 05/28/15 05/05/15 12:54 05/05/15 16:13 FINAL This report relates only to the sample as reeved by the laboratory, and may only be reproduced In full. Page 2 of 8 ) . 1ll�9 o www.encolabs.com SAMPLE DETECTION SUMMARY I Client ID: SWOT Lab ID: C5028bS-01 Anahrbe Results Fli2g -MA )SZ Units Method Notes Chemical Oxygen Demand 54 10 10 mglL SM 5220o-1997 pH 6.7 1.0 1.0 pH SM 4500H+B-2000 Q Client ID: SW02 Lab ID: C502e6"2 Anahrte Results H—K Euu-niptE Method Notes Chemical Oxygen Demand 90 10 10 mg/L SM 522OD-1997 PH 6.1 1.0 1.0 pH SM 4500H+B-2000 Q Total Suspended Solids 25 12 12 mg/L SM 2540D-1997 ANAL This report relates only to the sample as received by the laborainry, and may o* be reproduced in full. age 3 of 8 ENCC—] www.encolabs.corn ANALYTICAL RESULTS Description: SW01 Lab Sample ID:C502865-01 Received: 05/01/15 09:39 Matrix: Surface Water Sampled:04/30115 19:00 Work Order: C502865 Project: Stormwater (lan,luly) Sampled By: Kitty H. (Classical Chemistry Parameters ' ^-EWValyC"Agdana"[AC 591] Anahrte rCAS Numberl Results mg units OF R1 PQl Bad Method Analyzed IhE Notes Chemical oxygen DemandA 54 mg/L 1 10 10 5E05018 SM 52200-1997 05/05/15 16:13 30C PH. 6.7 pH 1 1.0 1.0 5EM27 SM 4500H+B-2MK 05/04/15 14:03 MKS Q Classical Chemistry Parameters ^ - D%CD Jado mL— r&Lredana+l'[e (AU 442] Anatvte rCAS Numberl Results HP9 units P—F p},py P L Batch Method Anabged By Notes oil & Grease (HEM) [C-00071A < 2.40 mg/L 1 2.40 5.00 5E12004 EPA 1664E 05/13/15 14:15 SMA Description: SW02 Lab Sample ID: C502865-02 Received: 05/01/15 09:39 Matrix: Surface Water Sampled:04/30/15 19:15 Work Order: C502865 Project: Stormwater (lan,luly) Sampled By: Kitty H. (Classical Chemistry Parameters ^ - EACO Cary c .ed a-W (At= 5911 Anahrte [CAS Numberl Results MAR U,]s4 AE M13L POL Batch Method Artalyz Ax N Chemical Oxygen aDemand^ 90 mg/L 1 10 10 5E05018 SM 5220a1997 05/05/15 16:13 3CIC pH^ 6.1 pH 1 1.0 1.0 SE04027 3M 4500H+B-200C 05/04/15 14:03 MILS Q Total Suspended Solids^ 25 mg/L 1 12 12 5E04002 SM 2540D-1997 05/04/15 08:45 MMR Classical Chemistry Parameters ^ - EAC0.bn rawr7le cn Ailed anaW [A' 442] Anahrte iCAS Numberl Rewlts Jig units 2E 1U ML, _BAtl;h Method A .ahrzea ft Notes oil & Grease (HEM) [C-0007]^ < 2.40 mg/L 1 2.40 5.00 5E12004 EPA 1664B 05/13/15 14:15 SMA FINAL This report relates only to the sample as received by the laboratory, and may a* be reproduced in full. Page 4 of 8 CeNk, gg. www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch SEL74002 - NO PREP Blank (SED4002-BLKI) Prepared & Analyzed: 05/04/2015 08:45 Spike Source %REC RPD Ana llde Result Rita POL Un"tts Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (5E04002-8S1) Prepared & Analyzed: 05/04/2015 08:45 Spike Source %REC RPD Ana ReSlilt Hag £2L Units Lewd Result %REC Limits RPD LFnrit Notes Total Suspended Solids 97 2.5 mg/L 100 97 80-120 Duplicate (SE04002-DUP3) Prepared & Analyzed: 05/04/2015 08:45 Source: C504955-01 Spike Source %REC RPD Ana llds Result flag kOL units Level Result %REC Umots RPD umlit t(Q= Total Suspended Solids 67 56 mg/L 69 3 20 Duplicate (SE04002-DUP2) Prepared & Analyzed: 05/04/2015 08:45 Source: C502863-01 Spike Source %REC RPD Ana Result Flag PQL units Level Restitt %REC limits RPD Lirnit Notes Total Suspended Solids 130 25 mg/L 140 8 20 Bath 5E04027 - NO PREP LCS (SE04027-BS1) Prepared & Analyzed: 05/04/2015 14:03 Spike Source %REC RPD Atlas RsadL Hag POL Units Level Result %REC Urnits RPD Limit Notes pH 7.0 1.0 pH 6.99 101 99-101 Duplicate (SE04027-DUP1) Prepared & Analyzed: 05/04/2015 14:03 Source., C502865-01 Spike Source %REC RPD Ana Rena Hag PQL units Level get %REC Limits RPD Limit Notes pH 6.9 1.0 pH 6.7 2 25 Bak* SE0501B - Same Blank (5E05018-81.1(l) Prepared: 05/05/2015 12:54 Analyzed: 05/05/2015 16:13 Spike Source %REC RPD Anairle Result Him PQl Units Level Result %REC Limits RPD limit fates Chemical oxygen Demand 10 U 10 mg/L LCS (5E0S01B-BS1) Prepared: 05/05/2015 12:54 Analyzed: 05/05/2015 16:13 Spike Source -- %REC RPD Mande Result Hag PQL Units level RM ( %REC Limits RPD Limit Notes Chemical Oxygen Demand 500 10 mg/L 500 101 90-110 Matrix Spike (SE05018-MS3) Prepared: 05/05/2015 12:54 Analyzed: 05/05M15 16:13 Source: C502865-01 Spike Source %REC RPD Ana Result Bay PQL units Level Rev %REC Umits RPD Lfiglt Notes Chemical Oxygen Demand 580 10 mg/L 526 54 100 W110 FINAL This report relates only to the sample as reoe;, ed try the laboratory, and may only be reproduced in ttdL Page 5 of 8 �co www.enc01abs.00m QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch SE05018 - Same - Coehiaued Matrix Spike Dup (5E05018-MSD1) Prepared: 05/05/2015 1154 Analyzed: 05/05/2015 16:13 Source: C502865-01 Spike Source %REC RPD 9nandg Result Etag P91 un$s Level Rwul %REC Limits RPD Limit Notes Chemical Oxygen Demand 580 10 mg/L 526 54 100 90-110 0 10 Classical Chemistry Parameters - Quality Control Batch 5E12004 - EPA 1664A Blank (SE12004-BLKl) Prepared: 05/12/2015 09:56 Anah/zed: 05/13/2015 14:15 Spike Source %REC RPD Ana lyte Result $a9 P_QL Units Level Result %REC Limits RPD urnit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (5E12004-BSl) Prepared: 05/12/2015 09:56 Analyzed: 05/13/2015 14:15 Spike Source %REC RPD Anahtte Rc5ult Elm PQL Units Level R=9 %REC Limits RPD Limit Notes Oil & Grease (HEM) 39.5 5.00 mg/L 45.1 88 78-114 LCS Dup (SE12004-BSD1) Prepared: 05/12/2015 09.56 Ana{yzed: 05/13/2015 14:15 Spike Source %REC RPD Ana Rat #3a9 PQL units Level RJR %REC Limits RPD Limit Notes Oil & Crease (HEM) 37.9 5.00 mg/L 45.2 84 78-114 4 18 Matrix Spike (SE12004-MS1) Prepared: 05/12/2015 09:56 Analyzed: 05/13/2015 14:15 Source: B502041-04 Spike Source %REC RPD Ana htte Result Etag ROL units Level Result %REC Limi?i RPD Limit Ngug Oil & Grease (HEM) 52.2 5.00 mg/L 43.2 23.7 66 78-114 QM-07 PINAL This report relates only to the sample as rerehred by the laboratory, and may only be reproduced in fLAL Page 6 of 8 C4 am� Nco www.enoolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. Q Analysis performed outside of method - specified holding time. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as reoekvej try the laboratory, and may only be reproduced in full. Page 7 of 8 �-' -QI .. , .•. vrr,r _ rl,•r•„v,••„•, y„a•. v nrr, v err-v•rv.vri. ,a,ry . . tARtlt.CttLVtitMi.LVMt■ T 1R n 10775 Caned Port Dr AB10 Execuliva Perk Chun' Suta 1I 1 _ 4r , 102•A Woodwinds IndLg9Uw CL 6Aa1da FL 32624 r - Jads3atv911a FL 32218.606f1'�' . NC 27513 • s r (a07) t)28.6314 •Fax (407) 850 694s (904J 295 9007; Fat (tiOiJ 2ti6�21 ay ? (9 a ae7 �000. 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Yi:.:. �?. r,{ �- f. , /"rss +::_. ..yr. .'` .F.rt .� 5 Accepiableri`•�r �_�.Unacceptable r.•"Idatrl: GwAtoundyratec+&4S�Dw-DchhdlipWWei;sE-seeim®nt!sw-SO+f� star:WYi;We9l9wAlar A•Alr oOthOr[tble�incoi[unenu}lf,T,`.,,.ProimvvUon:14c*:H4lCIrN-HNO3st'rH2SN no-NaDH'04)her(dotaAktca s} ( F F - .. 7 ' R a v 1 _.a,. h"' . ' { - Nato' AU samples MO kt YII}11 dra t011rla Cend•,t101q lten apreomo s .. *... eui>mdletl M EN60 LeW eeaeromo and Atiad en the rwame of thtt form. uFtJorstldOr wri adst'.r' - F }.. ..rid,, y W • . r N � 3 e .r a ? - +- tv } •,.. ^� of A- +i -.I/S+F `•.'?+MiY.`YrR""SL''F ��I_:`a3,.3 yy!1ra'F.i irL� {'��5 _, ,,• • , ..[.k ,� T - Y�..r EY :. .. -a Jyr -a " ..r . l .pia' . i. ... �. _ .. .. a ... •' - - � 'r. a1. . i ''... �r` i, ., , L ..F ENCO Laboraton-*es Accircrie Tr►nehy. RespAnswe. Imeo-vstive . 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, June 8, 2015 KELLOGGS SNACKSIAUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater CAS ENCO Workorder(s): C506623 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, June 2, 2015. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory, This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may onty be reproduced in full. Page 1 of 7 June 19, 2015 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Kellogg's Snacks Cary Bakery Operations One Quality Lane Cary, NC 27513 Re: Reporting Year 2015 - Storm Water Discharge Monitoring Report Ph 919.677.3200 Kellogg's Snacks -Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the first half of 2015 for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Joseph Atkinson (919) 677-3292 'ose h.atkinson kello .com Mr. Atkinson is available should any questions or problems arise during the review of this DMR. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,. including the possibility of fines and imprisonment for knowing violations. Sincerely, Steve Surovec Plant Manager Enclosures www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SWOT Lab ID: C506623-01 Sampled: 06/01/15 19:10 Received: 06/02/15 O8:15 Para Hold atEb (ram Preo Date/Timels) Analysis Datemme(s) SM 2590D-1997 06/08/15 06/03/15 09:10 06/03/15 09:10 FINAL This report mates only to the sample as reoeivW by the laborawry, and may only be npWuoed In full. Page 2 of 7 www.encolabs.com SAMPLE DETECTION SUMMARY Qlent ID: swol Lab ID: CS"623-01 Ana hrte Results MDL POIL Units method N Total Suspended Solids 48 12 12 mg/L. SM 254OD-1997 FINAL This report relate, only to the sample as reCeked by the laboratory, and may only be reproduced in ftdl. Page 3 of 7 www.encolabs.com ANALYTICAL RESULTS Description: SW01 Lab Sample ID: C506623-01 Received: 06/02/15 08:15 Matrix: Surface Water Sampled:06/01/15 19:10 Work Order: C506623 Project: Stormwater CAS Sampled By: Kitty N. Passical Chemistry Parameters ^ - EACt7 6ry a*ats,Ryanarytn (AC 591] Analvte ICAS Number] Results Elm units DF I)w DL P91 Batch Method Ar ed B�f !Notes Total Suspended Solids' 48 mg/L 1 12 12 5FO3005 SM 2540o-1997 06/03/15 09:10 MMR FINAL This report relates only to the sample as reo#wd by the laboratory, and may only be reproduced in full. Page 4 of 7 www.encolabs.00m QUALITY CONTROL DATA Classical Chemistry Parameters -Quality Control i A&h SF03005 - NO PREP Blank (SF03005-BLK1) Prepared & Analyzed:06/03/2015 09:10 Spike Source %REC RPD Jkhlb1: Result flag PQL MA5 Level Result %REC Limits RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L LCS (SF03005-BSI) Prepared & Analyzed:06/03/2015 09:10 Spike Source %REC RPD Arnahrte ReSDlt flag EM ll & Level Resul[ %REC Lifnits RPD Limit Notes Total Suspended Solids 95 2.5 mg/L 100 95 80-129 Duplicate (5F03005-DUPI) Prepared & Analyzed: 06/03/2015 09:10 Source. CSD6333-01 Spike Source %REC RPD Anal Result flag ML 6l111.ts Level Result %REC Limits RPD Limit Notes Total Suspended Solids 26 17 mg/L 23 14 20 Duplicate (5F03005-DUP2) Prepared & Analyzed: 06/03/2015 09:10 ' 11 Source:C506667-01 Anahft Result Flag l!QL Total Suspended Solids 190 So Spike Source %REC Llnits Level Result %REC Limits RPD mg/L 240 22 I RPD Limit Notes 20 QM-12 FINAL This report relates only to the sample as revived by the laboratory, and may only be reproduced In full. Page 5 of 7 www.enaolabs.coln FLAGsS/NOTES AND DEFINMONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85e1A or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 6 of 7 '�' - --w-,Fr,t�nr+w..n r�r!'{V rIVrwVraf/"a. a,Vai LTawvlt ae'♦a Vr.ItiY Va17�lra'V."�VMM.Mvr'-Ia�VM1aM„ k `� �- R1tl 11/♦Cllaf.V�Olii.7aLVal1 l 10775 Cenual Port ➢r � � '4810 E.osGrOre Park Caum Sta10 111 _ a1➢2-A Wwdwhft IT9k1SUtal Ci. � � ` - „E .. - r - 0.80d R r OdandO,-FL 92824 .IadrsomAle, F'iZ 3221 $' � � Cast, NC 27511 D307 ,Fa ! g T 9j487.99: Fox (919) A8735t5L407)82"314isFax(407)850.55 M i N. : 1 �iT�CaM mPclNu r Requested TUmelotr,a p IBSV� ' .d a,r.. .,r,- ,,� ., EQM Al AtlydYoeap k P Narsse!➢eee r Fgr 1q J . Note: Rush i oasts uM oCl -a''i 7'I 1.'�rv, ..J tlJ .\ {�r•'E S. t, 1-y.J F','•l 5 y, ,�. �1 11�'�..M EgAr �I 'l� ..,, y i r MCMIY ...+LM*dytN�t f.1 r +iww t. i rr * $�+r•# � I . 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S: , N _t• y, •'-. 11 -i J'- y a '.i �` Pi"1`,�' ti F r., p i%1'� M',fia -'�I'y'`�,'•.0 .s'i+'e: Y .'� o� L IS'i �'. - r .T q,A 1""- lJ!r•xlSYa. l�.,:1,. .J .I ♦ f`i i' i W 1i� p` sA_- %' a'R Y_,e J'♦44G t�ler Vna,W table . - Y JWW Wastawator>A Atra r�-00sor(defog in rmmrnanla) Prsaaivaiion: l ice H•HCI N HND3.3•H2504=N0 Ne0HI0 OWai (detail Cncortursa[stsl- z�' i i" J Matrlx ¢-GmndaatarFSO Soil ➢WDfsskUsp Water vSE Setllmant.SW.SuAoca Water a" k , Note : IU1 submpwd to EhIGD tabs am in nowedanm w tM 8m la m and oandMons fisted on the rmvme of thle form unless prlw wiipen dgreelnenl8 extsi ' 3'- ,« V. ; ;�.. 'l - - r �.. �• v. ,- - „{ s a' l v ` rr • SSr ,� d. r ,w ',�, stir, _ S'4'' J'n 4 , �',t„fl*L+:z , ,., ,:'.�nr'L- .a.+'s.. n,a {s - .,7.:'r'+'ti'`` j i•rr•"•`"`.H «., y. r,:1:•ti'? H . d.' 7'r�':�'ir` ,,�1 •yB':,F ^-rt,.� sxti; r 'f a� ' r ..der• 4',,;a:r. Sh i":.:.�IiiR�w'dp .r� . •dam' 'i',-.5+73. �ec1G§,:.r:.r. - .r" - • , s � rt , 1. hC6�7�0 aS(a �� I Via Certified Mail January 7, 2015' Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 CEJqN DWR R4 eS /6N . Re: Reporting Year 2014 - Storm Water Discharge Monitoring Report Kellogg's Snacks -Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, SNACKS Cary Bakery One Quality Lane Cary, NC 27513 ph 919.677.3400 fx 919.677.0015 Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the second half of 2014 for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Joseph Atkinson (919) 677-3292 joseph.atkinson@kellogg.com Mr. Atkinson is available should any questions or problems arise during the review of this DMR. C71Usas4LskjmO3\4pEW&V,oca1 M msoft% indows%Temporery Internet FdestContart.Outlook\OWSOKHUOLStormwater Cover lettrr.doc DWQ — Central Files January 2, 2015 Page 2 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, Steve Surovec Plant Manager Enclosures ciasen\u*jra03WPdataVuaaiVricrowftlwindowsVenWrary intemet 6lakordeM.auilookl0wsokhuO\sto mwater cover letter.doc a''boraton%os. . .CO L Accurate.Timely. Responsive. I»nava#ve.. 102-A woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, January 2, 2015 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: 5tormwater (]an,July) ENCO Workorder(s): C410568 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Monday, November 24, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only W the sample as receloed by the laboramry, and may only be reproduced in ftdL pays 1 of 8 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE alent ID: SWOT Lab ID: C410568-01 Sampled: 11/23/14 28:25 Received: 11/24/14 12:22 Parameter Hold Date/TiMefsjl Prep Date/Timds] Anahrsis batelTimefsl EPA 1664B 12/21/14 12/03/14 14:05 12/04/14 13:06 SM 2540U-1997 11/30/14 11/25/14 10:37 11/25/14 10:37 SM 4500H+B-2000 11/23/14 18:39 11/25/14 16:01 11/25/14 16:01 Client ID: Sw02 Lab ID: C410568-02 Sampled: 11/23/14 18:15 Received: 11/24/14 12:22 Parameter Hold Date/31nydsl Prey DatelTrme(s] Anahrsis Datel lmelsl EPA 1664E 12/21/14 12/03/14 14:05 12/04/14 13:06 SM 2540D-1997 11/30/14 11/25/14 10:37 11/25/14 1037 SM 4500H+B-2000 11/23/14 18:29 11/25/14 16:01 11/25/14 16:01 SM 5220D-1997 12/21/14 12/02/14 11:13 12/02/14 16:19 FINAL 11115 report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 8 eWq C www.enoolabs.pom SAMPLE DETECTION SUMMARY Client ro: Swol Lab ID: C41O5fi"l Results In "AL E" units !iceNotes Oil & Grease (HEM) 2.83 1 2.40 5.00 mg/L EPA 16648 pH 7.0 1.0 1.0 pH SM 4500H+B-2000 Q Total Suspended Solids 13 1.0 1.0 mg/L, SM 2540D-1997 Client ID: Sw02 Lab ID: C41056"2 Ana hrte fin IQ4 PAZ4 v itlii Me Chemical Oxygen Demand 58 10 10 mg/L SM 5220D-1997 pH 6.4 1.0 1.0 pH SM 450OH+B-2000 Q Total Suspended Solids 6.0 1.0 1.0 mg/L SM 2540D-1997 FINAL This report relates anly to the sample as received by the laboratory, and may only be reproduced in TLM. Page 3 or 8 ........... . err Q �N www.encotabs.com ANALYTICAL RESULTS Description: SWOT Lab Sample ID:C410568-01 Received: 11/24/14 12:22 Matrix: Surface Water Sampled:11/23/14 18:25 Work Order: C410568 Project: Stormwater (]an,luly) Sampled By:Tlmothy Klotz ]Classical Chemistry Parameters ^ - EWO G y m-nAred--6* [AV 5911 Anahte CCU tiumberl mil no MUM RE !L EQL BASSh Method Anahrzed li]I 1Vofg pH^ 7.0 pH 1 1.0 1.0 4K25003 3M 4500H+B-20K 11/25/14 16:01 MKS Q Total Suspended SolidsA 13 mg/L 1 1.0 1.0 4K25002 SM 25QD-1997 11/25/1410:37 MMR Classical Chemistry Parameters ^ - EAm JackwnWk mtrvd"A& [AC 442) Analyte rCAS Numbed Results flag Units PFF HU ML Batch Method Analvzad Oil & Grease (HEN) [C-0007]A 2.83 3 mg/L 1 2.40 5.00 4LO31105 EPA 1664B 12/04/14 13:06 M1F Description: SW02 Lab Sample ID:C410568-02 Received: 11/24/14 12:22 Matrix: Surface Water Sampled:11/23/14 18:15 Work Order: C410568 Project: Stormwater (]an,]uly) Sampled By:Timothy Klotz Chemistry Parameters ^ - EACi7 Cat--Mrkd ana4t-, [AC 591] . Analyte rCAS Numberl gesd(ts Elag u"it3 pf MOL E!Qy AdUh Llemo Anahmed ft Notes Chemical Oxygen Demand- 58 ng/L 1 10 10 4LO2009 SM 522OD-1997 1210211416:19 ]OC PHA 6.4 pH 1 1.0 1.0 41<25003 SM 4500H+5-200C 11/25/14 16:01 MKS Q Total Suspowled Solids- 6.0 mg/L 1 1.0 1.0 4K25002 SM 2540D-1997 11125/1410:37 MMR Classical Chemistry Parameters ^ --CTJ fld—Wle a-*te[AC -21 Analyte rCAS Number] $esu Fig ni Q,E WDL E41 Raub Meld Anatyred Oil & Grease (HEM) [C-OW7]^ < 2.40 mg fL 1 2.40 5.00 41-03005 EPA 1664B 12/04/14 13:06 MY FIMAL This report relates only to Vie sample as reobN ed by the laboratory, and may ody be reproduced in full. Pape 4 of 3 co www.encolabs.aom QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Barrie 4K25OO2 - NO PREP Blank (4K25002-131LKI) Prepared & Analyzed: 11/25/2014 10:37 Spike Source %REC RPD Aflandg ReSWA Ha QQL Volts Level Rat %REC Limits RPD Limit Notes Total Suspended Solids 1.0 U . 1.0 tng/L LCS (4K25002-8Si) Prepared & Analyzed: 11/25/2014 10:37 Spike Source %REC RPD Ana hrte Result Has PQL Units Level Result %RECLim! RPD limit Notes Total Suspended Solids 100 1.0 mg/L 100 100 OD-120 Duplicate (4K25002-DUPL) Prepared & Analyzed: 11/25/2014 10:37 Source: C324967-01 Spike Source %REC RPD pila Result Haft PQL U AS Level Resort %REC Limits RPD Limit Notes Total Suspended Solids 10 1.0 mg/L 10 0 10 Batch 40125003 - NO PREP LCS (4K25003-BS3) Prepared & Analyzed: I JM/2014 08:41 Spike Source %REC RPD Ana lyee Resift Rau PQL units Level Result %REC Limits RPD Limit Motes PH 7.0 1.0 pH 6.99 99 99-101 Duplicate (4K25003-DUPl) Prepared & Analyzed: 11/25/2014 16:01 Source: C410568-01 Spike Source %REC RPD -Anallde Resent Hill Mi. UDlls Level I t %REC Limits RPD Limit Notes PH 7.0 1.0 pH 7.0 0 25 Batch 4LO2OO9 - Same Blank (4L02009-ELK1) Prepared: 12/02/2014 11:13 Analyzed: 121021201416:19 Spike Source %REC RPD Anahttg ResUl fin PQL units Level Result %REC Limits RPD Limit ii4tRk Chemical Oxygen Demand 10 U 10 mg/ LCS (41-02009-13S1) Prepared: 12/02/2014 11:13 Analyzed: 12/02/2014 16:19 Spike Source %REC RPD , AAnande Result Hag PQL Units Level Result %REC Limits RPD limit Notes Chemical Oxygen Demand 510 10 mg/L 500 101 90-110 Matrix Spike (41.02O09-MS3) Prepared: 12/02/2014 11:13 Analyzed: 12/02/2014 16:19 Source: C314967-01 Spike Source %REC RPD Anande, Result an POL units Level RgSu %REC Limits RPD UMA Notes Chemical Oxygen Demand 540 10 mg/L 500 46 % 90-110 Matrix Spike Dup (4LO2009-MSD1) Prepared: 12/021201411:13 Analyzed: 12/0212014 16: 19 Source: C314967-01 Spike Source %REC RPD Ana hde Result Hag PQL Units Level Resin %REC Limits RPD Limit Motes Chemical Oxygen Demand 540 10 mg/L 500 46 98 90-110 OA 10 Classical Chemistry Parameters - Quality Control Batch 4LO3OO5 - EPA 1664A FINAL This report relates only to the sample as received by the laboratory, and may ordy be reproduced in full. Page 5 of a lcsim,m www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Blank (4L03005-BLK3) Prepared: 12/03/201414:05 Analyzed: 12/04/2014 13:06 Spike Source %REC RPD .9Dahite Resin lbs PQL Units Level Result '/DREG Limi RPD )fit Notes Oil & Grease (HEM) 2.40 U 5.00 mg/L LCS (4L03005-BS1) Prepared: 12/03/201414:05 Analyzed: 12/04/2014 13:06 Spike Source %REC RPD Ana llde Resul flau Pal. Units Level RCMAt %REC Limits RPD )fitNotes Oil & Grease (HEM) 35.3 5.00 mg/L 41.4 85 78-114 LCS Dup (4L03005-BSOl) Prepared: 12/03/2014 14:05 Analyzed: 12/04/2014 13:06 Spike Source %REC RPD Anallde ResEd Hag CQL U9tli Level Res %REC MMjjigii RPD L[Mjt Notes Oil & Grease (HEM) 38.7 5.00 mg/L 41.3 94 78-114 9 18 Matrix Spike (4L03005-MS1) Prepared: 12/03/2014 14:05 Analyzed: 12/04/2014 13:06 Source: B405230-01 Spike Source %REC RPD Ana11Et4 Result E1aA ML Units Level $Saidt %REC Limits RPD Umit NoW Oil & Grease (HEM) 69.3 5.00 mg/L 44.4 21.8 107 78-114 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduces in hill. Page 6 of 8 s www.encolabs.c ixi FLAGS/NOTES AND DEFINMON5 B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. Q Analysis performed outside of method - specified holding time. FINAL This report relates only to the sample as received by the laboratory, and may onty be reproduced in rull. . Page 7 of 8 `—' ENVIRONMENTAL. CONSERVATION ° LABORATORIES, CHAIN -OF -CUSTODY. RECORD Www.encola bs.com 4810 Executive Park uite,441; 102-A Woodwinds Indus Idaf Ct. Orlarldq F< 32824.Or- Jddcsrnwd a, FL 32216 069 • Cary, NC 275i 1 . _ 4f77} 825 5314� FaYt 467) 850-8945. 96-6210 ' (919) 4G7.3090 Fpx (919) 467.3515 Pages,. _L Q+ _•_ . ( -(_, (904).298.3d07' Fax (9o4 2 Client Name Project Number Requested Analyses Requested iilrilarDtlr?d, - 'Times FOODS y Address -' Project Npmelbesc - Nele: Rush requests sutijlscl to - •'_QUALrY IAli er-.. r Aceeptan6dy.uielncilily, aty/sTrzlli PO p,! Billing Intl] . QARY'. lJ627513-: 42002942:3f ❑ � Standard , ,0.Tql � � ` _ Fa- Reporting Contact . 1, 6T-7.3a13 RodreSteriG � '' a � _ Expedited. IX) Due 1 / Sampler(s)_Name. AtWakn (Prfnl)'r, Tn othy'Klotz Acci�unts,Pay-lb1t *- f _ _ 0 0 U:10. Samplers) Signalure', Sito.Loeatlon'Y Time 7.one Valli Workorder • c f ti Preservation (Sea Codes) (Combine as, necessnry). - Cole6on .. MstrW Total A at lrem q •'- Sample ID (Field IderttlGcation) Cnllerifon Date :Time :,Camp/Grab' '(sea codes) ' ;Canlnlners ..,.Sample Comrment5 �p - Yam' {,r 7 w ' o . `"t" a '"I''iit'-",!� nd, 1�`.Z3=1'{ I iglu G . .r t i I •.. : . : fie,.. .Y. .. '' � •- +. ' -. ,. 'a � e . a' . - • i 4 rt: y.,+ k .J - �'. r•a' .. S L i >f.� kx , '* }k�F Ur q f.1"ee�r 4t�� ' --..:r ..,:.-• .. .,..sue •.... J-:r 5- .aJ. .. ; ,� ,'kY•.r ..ate .k s: 'r.:r9d"@ a+,n+. w8.•" ,{. .:'n i ' r• I t •Y,.- • r 3- ' � i . ti � .' u �tr-. Ivt ILr,���� '�I 1 � •p ': thy- n ,' �`� Y '. '1 "' a •k; I � .�' b ,:;�. .. e^k • r II .� 9 d d'•� $a 9... dE•. I t�.i_t< v+l .:_ 1 e�:,�JYak�"1u.a+'lY+�'IiYYrk�rQ�n' Y�. .. (tk �y t •°Y M�9" "�:"k _�i• ,�_ ei a r '.Y l- Y ' r �f� oar" r .-°a °'jtl'". r``= ,lµ` G ,,. •va i i - Yl � � � k �,• trl � �� , � ti I. � - ]Y .y Ix'w A,LX rt It •k-,.. - h s —Total # of Containers Sample Kit Prepared By Pal / 17 Rafinquished By Date1 me'' - Reoelvo By - Datarr, a CommanlslSpecial Reporting Requirements ' - Relinquished By Datemmo., Re wed 13 Dal(g ima Relinquished By Date/Time- ece By '- DaleMme Cooler s d Temps,on R Ipl •,� Y �- Gvndldm pan Racslpt., -- - ' .. •-Acceptabta; lJRacc 1l Matrix: GW-Groundwater'SO.Sof10WDdnkingWster,SE-SedimartSW-SurlacaWatefWFI :;WWastewalerA=Air 0:01har.(dalallincomments) ,Preservation:-ce;H•HCIrWHNO3;S•H2SO4;�RD•NaDH-O.Other(delaitlncomments)r. k Nato All samples svbrmtted to ENCO Labs are in accordanCe:With the terms and conditions listed 0the raysrsa-ol this form, unless prier written agreements exist eptable e :rL ENCO'Laboratories. Accurate..' Timer. 'Responsive Imeovsliue 102-A Woodwinds Industrial Court Gary NC, 27511 Phone: 919."7.3090 FAX: 919.467.3515 Tuesday, December 30, 2014 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (]an,3uty) ENCO Workorder(s): C416671 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, December 16, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This repot relates only to the sample as rea9vee by the laboratory, and may only be reproduced in full. Pape 1 of 7 www.encotabs.anm SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SW-01 Lab ID: C416671-01 Sampled: 12/16/14 11:20 Received: 12/16/14 12:40 Paratneber Hold Datefrittte(s1 Prep Date/Timefsl Analysis DateMnwfs) SM 522OD-1997 01113/15 12/26/14 11:2.5 12/26/14 15:37 FINAL This report retates only to the sample as reoe ved by the laboramry, and may only be reproduced in MI. Page 2 of 7 OF. ON www.enaalabs.00m SAMPLE DETECTION SUMMARY Client ID: SW-01 Lab ID: C416671-01 AnahrUe Results Rao HM POLM Notes Chemical oxygen Demand 88 to 10 mg/L SM 5220D-1997 FINAL This report rn�ates only to the sample as received by the laboratory, and may only be reproduced In full- Page 3 of 7 www.encolabs.com ANALYTICAL RESULTS Description: SW-01 Lab Sample ID:C416671-01 Received: 12/16/14 12:40 Matrix: Surface Water Sampled:12/16/14 11:20 Work Order: C416671 Project: Stormwater (lan,luly) Sampled By:TIMOTHY KLOTZ Classical Chemistry Parameters ^ - EACO C2Wy-Vried an*te (AC 5911 AnalyU FCAS Numbed Chemical Oxygen DernandA Bewlts Flag m0m Of LL PQL Batch Method Anal Ef Lr4tso4 as mg/L 1 10 10 4L26012 SM 522OD-1997 12/26/14 15:37 JOC FINAL This report relates only to the sample as recehoed by the laboratory, and may only be reproduced In full. Page 4 of 7 QeNkl www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 4L26012 -Same Blank (41-26012-BLKI) Prepared: 12/26/2014 11:25 Analyzed: 12/26/2014 15:37 Spike Source %REC RPb Anande Resul 1ba PQL units Level Result %REC Limils RPD limit Chemical Oxygen Demand 10 U 10 mg/L LCS (41_26012-BSI) Prepared: 121261201411:25 Analyzed: 12/26/2014 15:37 Spike Source %REC RPD Ana 6d& Rss1rEt Hag PQL Unim Level Result %REC Limits RPb J MA Notes Chemical Oxygen Demand 500 10 mg/L 500 99 90-110 Matrix Spike (4L26012-MS3) Prepared: 12126/201411:25 Analyzed: 12/26/2014 15:37 Source: C414993-03 Spike Source %REC RPD -Artatvte $esul Flag PQL UBlts Level Result %REC Limits RPD Limit 1Y4tes. Chemical Oxygen Demand 500 10 mg/L 500 10 U 100 90-110 Matrix Spike Dup (41.26012-1015Dl) Prepared: 12/26/2014 11:25 Analyzed: 14261201415:37 Source: C414993-03 Spike Source %REC RPD Anal RISLIt lido PQL !!nks Level Result %REC Limits RPD Limit Notes Chemical oxygen Demand 490 10 mg/L 500 10 U 99 90-110 2 10 FINAL This report relates only to the sample as rimed by the laboratory, and may only be reproduced in t'rdL Page 5 of 7 www.encolabs.com FLAGS/NOTES AND DERNMON5 B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. FINAL This report relates only to the sample as reoeived by the laboratory, and may orJy be reprodu®d In U. Pape 6 of 7 T777 777 - + 1140- 74L.�"vKIv7*i ENVIR0mmEAIME�46isrRvAndN NKRAMBIES IJS MPVMEC ORC xWjNwnq a #[Ornt ik % sWri 5i14U1l,�a."Tr LI Any Al t IIFiNtli2nS FP f f 1.4 ,s,*' �11 RIM, Mill J71 zw Ilk 1 L tot Now U4 j'&j . M. 3r ,T, I _77 _1 W. .17: 17 Ali eV Ik 1A, 1 nor 1 "®rMs STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCG060000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 CERTIFICATE OF COVERAGE NO. NCG06 0286 (This monitoring report is due at the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Kellogg Company- Cary, NC Facility COUNTY Wake PERSON COLLECTING SAMPLES Timothy Klotz PHONE NU-(- 919 } 677-3292 CERTIFIED LABORATORY ENCO Las Lab # 591 Lab # PLEASE SIGN ON THE REVERSE 4 Part A: Specific Monitoring Requirements Outfall :Date 00530 00400 ..,00340 , .... 00556 31616 No. Simple. -Total Suspended pH, "` ChemicalOzygen " " 'Oil and Grease;" Fecal Coliform;: Collected, . Solids, Standard units Demand, :; mgl Colonies per 100 ml ' mo/ddlyY m L . m L Benchmark 100", <�. Within 6.0 — 9.0' 120 = 30:1000 SW02 05/27/14 NA NA 120 NA Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes Xno (if yes, complete Part B) Part 13: Vehicle Maintenance Activitv Monitorine Requirements NA - Outfali: > Date::...' ,,: �00555 a 00S3D > =00400 No: Sample.Collected, k Oil -and Grease, Total Suspended Solids, pH, New. Motor OilUsage, mo/ddl r " m a m' Standard units Annual average; at/mo Benchmark 30 :100 �6 0 = 9.0. Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses. See General Permit text. STORM EVENT CHARACTERISTICS: Mail Original and one copy to: Division of Water Quality Date04/25/14 (first event sampled) Attn: DWQ Central Files Total Event Precipitation (inches): 0.47 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date05/27/1 q ist each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): 0.22 S W U-249-102107 Page I of 2 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility pf fines and imprisonment for knowing violations." (Signature of Permittee) (Date) S W U-249-102107 Page 2 of 2 ENCO Laboratories Accurate. 'Tamely. Responsive. Innovative. 102-A woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Wednesday, July 2, 2014 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (]an,]uly) ENCO Workorder(s): C404081 Rear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, April 25, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as reoejue M the laboratory, and may any be reprodumd in full. Page i of a a � www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SWOT Lab ID: C404081-01 Sampled: 04/25/14 13:40 Received: 04/25/14 16:25 Paran3ete> EPA 16648 Hold Datemme(sl 05/23/14 Pren DatelTime 05/01/14 Al Analysis Date/7ime(sl 11:21 05/02/14 10:00 SM 2540D-1997 05/02/14 G4128/14 09:05 04/28/14 09:05 SM 4500H+B-2000 04/25/14 13:54 04/28/14 14:39 04/28114 14:39 client ID: SW02 Lab ID: C404081-02 Sampled: 04/25/14 13:30 Received: 04/25/14 16:25 Para metgt Hold Date/Time(s) PrenDatelTime[sl Analysis Date/Time(sl EPA 16646 05/23/14 05/01/14 11:21 05/02/14 10:00 SM 2540D-1997 05/02/14 04/28/14 09:05 04/28/14 09:05 SM 4500H+B-2000 04/25/14 13:44 04/28/14 14:39 04/28/14 14:39 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 8 ce-JVgr www.enoolabs.mm SAMPLE DETECTION SUMMARY Client ID: SWOT Lab ID: C404081-01 8".Results 1g mu EQ_L m1fim HAth N PH 6.8 1.0 1.0 PH SM 4500H+B-2000 Q Total Suspended Solids 33 1.0 1.0 m4/L SM 2540D-1997 Client ID: SW02 Lab I0: C404081-02 Ana Result fim km PAL Units Method Motes Oil & Grease (HEM) 2.97 1 2.60 5.00 mg/L EPA 1664E PH 6.0 1.0 1.0 PH SM 4500H+&2000 Q Total Suspended Solids 76 1.0 1.0 mg/L SM 2S40L-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 8 CeN www.encotabs.com ANALYTICAL RESULTS Description: SW01 Lab Sample ID:C404081-01 Received: 04/25/14 16:25 Matrix: Surface Water Sampled:04/25/14 13:40 Work Order: C404081 Project: Stormwater (]an July) Sampled By:Timothy Motz Chemistry Parameters .-y M i'.ed a-ANxc (AC 5911 AnaMe FCAS Numberl Remits Fla9 1]I1115 of MDL P9L Batch 1 AnatyE.ld the 1t4i� PH [ECL-0062]A 6.8 pH 1 1.0 1.0 4D28036 SM 4500H+6-200( 04/28/14 14:39 MMR Q Total Suspended Solids [ECL-0169]^ 33 mg/L 1 1.0 1.0 4D28001 SM 2540D-1997 04/28/14 09:05 MMR Classical Chemistry Parameters ^ - EACO Jac6onv41fe cr.0red an"fNC 4421 AnaHte rCAS Numberl Results Rau unim LDf MDL EQy Batch Meewd rA ralvzed fix No Oil & Grease (HEM) [C-0007]^ < 2.60 mg/L 1 2.60 5.00 4EO1006 EPA 1664B 05/02/14 10:00 RIF Description: SW02 Lab Sample ID: C404081-02 Received: 04/25/14 16:25 Matrix: Surface Water Sampled:04/25/14 13:30 Work Order: C404081 Project: Stormwater (]an,luly) Sampled By:Timothy Klotz (Classical Chemistry Parameters ^ - EACO Cary ctaaVAed anaW IAC 591J Analyte IM Numberl Results flag M9131 PE M dl Q9L AdW1 Mediod Anahrzed RxNo PH [ECL-0062]^ 6.0 PH 1 1.0 1.0 4D2W36 SM 4500H+B-2000 04/28/14 14:39 MMR Q Total Suspended Solids [ECL-0169]1 76 mg/L 1 1.0 1.0 41328001 SM 2540D-1997 04/28/14 09:05 MMR Classical Chemistry Parameters ^ - EAW _bd"L Le a bfAAed aW" [AC 4421 Anahrte rCAS Number] Results Fkg Units DF L pI Batch pgtbod Analyzed ft now Oil & Grease (HEM) [C-0007]^ L97 ] mg/L 1 2.60 5.00 4EO1006 EPA 1664E 05/02/14 10:00 M]F FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 8 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 4D28001 - NO PREP Blank (4D28001-BLKL) Prepared & Analyzed: 04/28/2014 09:05 Spike Source %REC RPD Ana hdg Result Hag PQL Units Level Resin %REC Limits RPD Limit Notes Total Suspended Solids 1.0 U 1.0 mg/L LCS (4D28001-asl) Prepared & Analyzed: 04/28/2014 09:05 Spike Source %REC RPD Ana bde Res t[lt Flag 1291 Units Level lit %REC Limits RPD Limmill Notes Total Suspended Solids 100 1.0 mg/L 100 100 W120 Duplicate (4D28001-DUP3) Prepared & Analyzed: 04/28/201409:05 Source:C405283-01 Spike Source %REC RPD Ana11[te Result flag PQL units Level Rnculh %REC Limits RPD Limit Notes Total Suspended Solids 69 1.0 mg/L 46 40 10 QM-12 Duplicate (4D28001-DUP2) Prepared Be Analyzed: 04/28/2014 09:05 Source: C405283-02 Spike Source %REC RPb Ana 4tte Result Flag M Units Level Result %REC Limits RPD Limit Notes Total Suspended Solids 14 1.0 mg/L 12 18 10 QM-12 Batch 4028035 - NO PREP LCS (4D28036-BS1) Prepared & Analyzed: 04/281201413:36 Spike Source %REC RPD Ana hd& Result Flag ROL Units Level Result %REC Limits RPD Limit Notes PH 7.0 1.0 PH 7.01 99 99-101 Duplicate (4D28036-DUP2) Prepared & Analyzed: 04/28/2014 14:39 Source: C404081-01 Spike Source %REC RPD AnaandC Result Flag PQL Units Levee RM %REC Limits RPD Limi Notes PH 6.7 1.0 pH 6.8 1 25 Classical Chemistry Parameters - Quality Control Satdr 4EO1006 - EPA 1664A Blank (4ED1006-BLKI) Prepared: 05/01/2014 11:21 Analyzed: 05/02/201410:00 Spike Source a/oREC RPD Ana l7de Result Flag PAL Units Level Result %REC Limi RPD Merit dotes Oil & Crease (HEM) 2.60 U 5.00 mg/L LCS (4E01006-BSI) Prepared: 05/Ol/2014 11:21 Analyzed: 05/02/2014 10:00 Spike Source a/aREC RPD -Anahfts Resin flag POLL Units level ReSul %REC Limits RPD 9m t Notes Oil & Grease (HEM) 38.7 5.00 mg/L 41.3 94 7&114 LCS Dup (4E01006-9SD3) Prepared: 05/01/2014 11:21 Analyzed: 05/02/2014 10:00 Spike Source %REC RPD Anahi'tE Result Flag RQL Units Level get %REC i} "Its RPD Lifnit Note Oil & Grease (HEM) 38.9 5.00 mg/L 41.3 94 78-114 0.5 18 FINAL This report relates only to the sample as reoei eed by the laboratory, and may only be reproduced in full. Page 5 of 8 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 4E01006 - EPA 1664A - Continued Matrix Spike (4E01006-MSl) Prepared: 05/01/2014 11:21 Analyzed: 05/02/2G14 10:00 Source: B402019-03 Spike Source %REC RPD _A0ahte Result lin P91 l,lnit.s level Result %REC Limi RPD mi Nates Oil & Grease (HEM) 41.1 5.00 mg/L 44.7 3.77 85 78-114 FINAL This reW relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 8 www.enmiabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitabon limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". Q Analysis performed outside of method - specified holding time. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only to the sample as rec6ved by the laboratory, and may orgy be reproduced in full. Page 7 of 8 CHAI-1diAT66 ,'.AtCPRD, -L�'. 'W 0 ',F.; ENVIRONIVIENTAL:;!CONSERVATIONA6okkfbAlts: 107n eonlf'd�l P—om'6, I i -A, Yefaadatada bt&.'t& 61" 69r�tid 2751 g�F !,32216 40 4i(0194 ?;:15115 wwW'-AmcolJbsXo'M-- 0119017 1 :.df I I Oiotq Mum R!�c(uPstodTui naround, F�mi Ndrti ormwderljanLju 'CAR'�� Y.AC276 Tol, 1, Smt�9 L, 13 5 1! l-"'.o �` , . od .,RVI... - : "An! 't,Am*, Affil alloo We lnTh� k "bco 19 ti �V`4 1 unts PY941e, j7-4041 'C Gal Een C6daiz) (Cnmbine mn nmmwryl Itdrnk rwnpi6 it) jF� io'i' 1,6.y. �,COW4M Untu ,Toni Walfix, fatal v 0 'Cont'llrierv, a mments -swat, V.. — 5 X— L • iS L--j A JjyL 19 "iyndfl Dawning" mps "Lla lo 'A A lo'conwn 51, FX In wmi I uti%$id 10 ENCO 6La are, am rAumbil66 vjd c"I iw lvmr�o at ENC.0 Laboratories Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, June 10, 2014 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (Jan,]uly) ENCO Workorder(s): C406506 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, May 28, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This repot relates only to the sample as reoeved by the laboratory, and may only be reproduced In full. Page 1 of 7 cii rrir www.encolabs.cOm SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SWOT Lab ID: C406506-01 Sampled: 05/27/14 15:10 Received: 05/28/14 07:45 Parameter Hold Date/Time(s) Pren Date/Timefs] Analysis Date/TomeW '94 5220D-1997 06/24/14 05/30/14 11:58 05/30/14 14:47 Client ID: Sw02 Lab ID: C406506-02 Sampled: 05/27/14 15:15 Received: 05/20/14 D7.45 Parameter Hold Date/7imefsl Eren pa Analysis Date/Timefs] SM 522OD-1997 06/24/14 05/30/14 11:58 05/30/14 14:47 FINAL This repGa retates only to the sample as recelvW by the laborainry, and may onty be reprodmcd in (Wl. Page 2 of 7 ce. NkYgg www.encolabs.com SAMPLE DETECTION SUMMARY Client In, SWOI Lab ID: C406506-01 Analvte Results MDL P2 Units H Natca Chemical oxygen Demand 180 10 10 mg/L SM 5220D-1997 Client ID: Sw02 Lab ID: C406506-02 Anahtte Results Ela9 Hu PQ llnits Method Notes Chemical oxygen Demand 120 10 10 mg/L SM 5220D-1997 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduorl in toll. Page 3 of 7 www.enoolahs.00m ANALYTICAL RESULTS Description: SW01 Lab Sample ID:C406506-01 Received: 05/28/14 07:45 Matrix: Surface Water Sampled:05/27/14 15:10 Work Order: C406506 Project: Stormwater (lan,luly) Sampled By:Timothy Klotz IC[assicat Chemistry Parameters ^ - EACO Cary a:yVA! d an3lyte INC 5911 Analyte rCAS Numberl Results On Units 2E HU ML Batch Method AnaIy NN Chemical Oxygen Demand 180 mg/L 1 10 10 4F30016 SM 5220o-1997 OS/30/14 14:47 CV rECL-003511 Description: SW02 Lab Sample ID:C406506-02 Received: 05/28/14 07:45 Matrix: Surface Water Sampled:05/27/14 15:15 Work Order: C406506 Project: Stormwater (lan July) Sampled By:Ttmothy Klotz Chemistry Parameters Analyte rCAS Number] Results FlaH Units PE NDL E2L Batch Met Nadi Analyzed ft [ilQS� Chemical Oxygen Demand 120 mg/L 1 10 10 4E30016 SM 5220D-1997 05/30/14 14:47 CV [ECL-00351A FINAL This report relates only to the sample as receKted by the laboratory, and may only be reproduced In full. Page 4 of 7 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control 13aWh 4E30016 - Same Blank (4E30016-BLNl) Prepared: 05/30/2014 11:58 Analyzed: 05/30/2014 14:47 Spike Source %REC RFD Anahft Result Rag EQL Unite level Result %REC Lirrift RFD Lim9t Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (4E30016-BSI) Prepared: 05/30/2014 11:58 Analyzed: 05/30/201414:47 Spike Source %REC RPD AnaResult flan P_QL Units Level Result %REC Limm RPD limm Notes Chemical Oxygen Demand 490 10 mg/L 500 98 90-110 Matrix Spike (4E30016-MSI) Prepared: 05/30/2014 11:58 Analyzed: O5/30/2014 14.47 Source: C405380-01 Spike Source %REC RPD Anahrte Resuif flag E L Units Level ResuR */aREC Limits RPD Lima Notes Chemical Oxygen Demand 540 10 mg/L 500 55 97 90-110 Matrix Spike Dup (4E30016-MSD1) Prepared: 05/30/2014 11:58 Analyzed: 05/30/2014 14:47 Source. C405380-01 Anahtte Chemical Oxygen Demand Spike Source °/aREC Result flag EKIL UnFts level Result %REC Limits RPD 550 10 mg/L 500 55 99 90-110 2 RPD Urnit Notes 10 FINAL This report relates only to the sample as receKed by the laboratory, and may only be reproduced in full. Page 5 of 7 www.enoolabs.00m FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MILL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification", FINAL This report relates only to the sample as reoaKied by the laboratory, and may only be reproduced in full. Page 6 of 7 ENVIRONMENTAL CONSERVATION LABORATORIES' CHAIN -OF -CUSTODY RECORD -• - tO775 Central Port Dr.. 4010 Exewive Park Court; Suite 111 102d1 Uroodwinds tndusinat Court Orlarwo, FL 32824 .JadwwIle, FL 322SB 6069 Cary,. NC 27511 J4071826-5314 Fox (407) 850-8945 (9t9)467-3090 Fax (919)467-3515 Page -I of Client Name HartA.Hickman Prgecl Numbw RequestedAnstysee I RequestedTumaround 'times ject to "awe cebytRush he;,`�lity -'Standard _ Expedited Due I 1 Q O ass 3334 Hillsborough St Protect NamerDesc Kellogg CnyrST2p Raleigh; NC 27.fiO7 PO 01 Biilnq Into Tel .. Faxi 9,19-8474241 in;'Contact - Timothy Klotz Sampler(s) Name, Affiliation (Print) - - - Timothy Klotz. `(H&H) Billing Contact Rodney Bateman (Kellogg) EmpWis) signetur Facilityp(ifrequired) Lob Workorder .' e �,0 Pro"mat on l er CWosl ( cmt>rne as necessa y Items . Sample ID (FWd lderdelc ;6n - - Colledion Date Collection Time CompI Grob Matrix lsee md") Ca tatnora 54 Sample Comments SWV o1 s•� Z >c Sw o2 5-21-4H I1515' 7 k• <.. Total tt o ontairtefs ale ka Prepred 0 IDatafTime DistalTims Rocerved By 0all6florne Comments R.0TmJ t �--, r;�i4 Dala;Time Recervad By Datefrme Mier We , emps on Receipt Q .• onAtronACCRecmpt eptable Unsweptabie Matrix:GW-Grourdwaler SO•Scil SE -Sediment SW -Surface Water.WW-Wastewater A -Air O.Other(deladincomments) Prewnatlon:I-lea H•HCI N-HNO3 S-H3SO4 NO-NaOH O-Other(detaOincammente) Note: All samples submitted to ENCO Labs are In accordance with the tens and conditions listed on the reverse of this form; unless prior wiittem agreements exist J STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCG060000 CERTIFICATE OF COVERAGE NO. NCG06 0286 FACILITY NAME Kellogg Company- Cary, NC Facility PERSON COLLECTING SAMPLES Timothy Klotz CERTIFIED LABORATORY ENCO La F Lab # 591 Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 (This monitoring report is due at the Division no later than 30 days from the date the facility receives the sampling results from the Iaboratory.) COUNTY Wake PHONE NO. (7F9) 677-3292 PLEASE SIGN ON THE REVERSE 4 OutfAl, Date 00530. 00400 x 00340 00556 31616 Total",Suspended_> rpIl, Chemical Oxygen Oil and Grease, : _ Fecal Coliform, No. w ry Sample `' Collected, Solids, S.tanda'rd units Demand, .; m&L Colonies per 100 �r iriolddl x . m L =m L Benchmark ' `" - . -. ��,�. z100 Within 6:0 ="9A 120.. 30 - .:1000'. SWO1 1 04/25/14 33 6.8 1 NA <2.60 NA swol 1 05/27/14 1 NA I NA 1 180 1 NA I NA SW02 05/27/14 NA NA 120 NA Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes Xno (if yes, complete Part B) NA rart is: vemcie iviamtenance activity onitoring xe uirements Outfall. Date.. -AS.,".'- , � 00556 '; b00530 00400 No mo/ddl r , pleiCoilectedOiland Grease; „ Total,Suspended Solids, pH, New Motor Oil Usage, Sani� m Standard units Annualavera a allmo Benchmark, _ �__ 30� „ . 100,6:0-9.0;=.. Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses. See General Permit text. STORM EVENT CHARACTERISTICS: Mail Original and one copy to: Division of Water Quality Date 04/25/14 (first event sampled) Attn: DWQ Central Files Total Event Precipitation (inches): 0.47 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Date05/27/1 Jlist each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): 0.22 S W U-249-102107 Page 1 of 2 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) S W U-249-102107 Page 2 of 2 E.NCO Laboratories Accurate. Timer. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3315 Wednesday, July 2, 2014 KELLOGGS SNACKS/AUSUN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE. Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (Jan,]uly) ENCO Workorcler(s): C404081 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, April 25, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to M sample as received by the laboratory, and may only be reproduced in MI. Page 1 or 8 (0 NIS www.encolabs.eom SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Sw02 Lab ID: C404081-01 Sampled: 04/25/14 13:40 Received: 04/25/24 16:25 Parameter Hold DatelTimefsl PrepDateLrimefsl Analysis Date/Time(s) EPA 1664B 05/23/14 05/01/14 11:21 05/02/14 10:00 SM 2WD-1997 05/02/14 04/28/14 09:05 04/28/14 09:05 SM 4500H+B-2000 04/25/14 13:54 04/28/14 14:39 04/28/14 14:39 Client ID: Sw02 Lab ID: C404081-02 Sampled: 04/Z5J14 13:30 Recefyed: 04/25/14 16:25 Parameter Hold Date/Titnefsl Prep DatelTime(sl Analysis Date/Timefsl EPA 1664E 05/23/14 05/01/14 11:21 05/02/14 10:00 SM 2540D-1997 05/02/14 G4128/14 09:05 04/28/14 09:05 SM 4500H+B-2000 04/25/14 13:44 04/28/14 14:39 04/28/14 14:39 FINAL This report relates only to the sample as reoeihAd by the laboratory, and may ordy be reproduced in fun, Page 2 of 8 11EM, w a www.encolabs.com SAMPLE DETECTION SUMMARY Client IP: swol Lab I13: C4O4081-01 Ana HOL ML llnl !3 N pH 6.8 1.0 1.0 pH SM 4500H+8-2000 Q Total Suspended Solids 33 1.0 1.0 mg/L SM 2540D-1997 aient Io: SW02 lab I6: C4O4O81-02 Oil & Grease (HEM) pH Total Suspended Solids molts lug H61 2.97 1 160 6.0 1.0 76 1.0 B" mum Method 5.00 mg/L EPA 16648 1.0 pH SM 4500H+H-2000 1.0 mg/L SM 254OD•1997 '•1 FINAL This report relates only to the sample as relived by the laboratory, and may only be reproduced in full. Page 3 of 8 i i www.enmiabs.com ANALYTICAL RESULTS Description: SW01 Lab Sample ID:C404081-01 Received: 04/25/14 16:25 Matrix: Surface Water Sampled:04/25/14 13:40 Work Order: C404081 Project: Stormwater (Jan July) Sampled By:Timothy Klotz Classical Chemistry Parameters ^ - EACO Cagy ¢rtlfled anaW (AC 5911 Anatdc FCAS Numberl Results jig units PH [ECL-0062]1 6.8 pH Total Suspended Solids [ECL-0169]^ 33 mg/L Classical Chemistry Parameters ^ - EAW -WL O/1C mt;rlied aw4lh? [AC 4421 PF HOL POL %itch Mdhod Analyzed 1bt Noi� 1 1.0 1.0 4D26036 SM 4500H+B-200C 04/28/1414:39 MMR Q 1 1.0 1.0 4D28001 SM 25MD-1997 04/28/14 09:05 MMR Results EhV Units PF BRI P12< Batch Method 6rla& Notes oil & Grease (HEM) [C-0007]A < 2.60 mg/L 1 2.60 5.00 4EO1006 EPA 1664B 05/02/14 10:00 RIF Description: SW02 Lab Sample ID: C404081-02 Received: 04/25/14 16:25 Matrix: Surface Water Sampled:04/25/14 13:30 Work Order: C404081 Project: Stormwater (Jan July) Sampled BV:Timothy Klotz Classical Chemistry Parameters ^-EWVCaryab0fieda»ly,(AC 5911 Anabft FCAS Numberl Results fig MR& PH [ECL-0062]1 6.0 pH Total Suspended Solids [ECL-0169]1 76 mg/L Classical Chemistry Parameters ^-EAMbcASMvilk?cerr/fed""INC 4421 AnalAe fCAS Nuo]berl ResuF>s f19 Unirs Oil & Grease (HEM) [C-0007]^ 2.97 J mg/L. DF MDL P41 Batch Method Anahaad AM l 1 1.0 1.0 4D28036 iM 4500H+B-200C 04/28/14 14:39 MMR . Q 1 1.0 1.0 4D28001 SM 2WD-1997 04/28/14 09:05 MMR PF MOL P4L hatch !Method Analyzed B1 Notes 1 2.60 5.00 4E01D06 EPA 1664E 05/02/14 10:00 MIF FINAL This report relates only to the sample as received py the kaboratory, and may only be reproduted bn f dL Page 4 of 8 �i Us! _ www.encolabs.com QUALITY CONTROL 13ATA Classical Chemistry Parameters - Quality Control Batch 4D28001 - NO PREP Blank (41328001-BLKI) Prepared & Analyzed: 04/28/2014 09:05 Spike Source %REC RPD _Anabft Resell FW PUL U11113 Level Result %REC Limift RPD Umlt Notes - Total Suspended Solids 1.0 U 1.0 mg/L LCS (4D28001-BSI) Prepared & Analyzed: 04/28/2014 09:05 Spike Source %REC RPD Ana hda Result flag PQL Units Level Result %REC Limift RPD Limit Notes Total Suspended Solids 100 1.0 mg/L 100 100 W120 Duplicate (4D28001-DUP1) Prepared & Analyzed: 04/28/2014 09:05 Source: C405283-01 Spike Source %REC RPD 11de Rml! flag PQL mwu Level Result %REC limits RPD !fit Notes Total Suspended Solids 69 1.0 mg/L 46 40 10 QM-12 Duplicate (4D28001-DUP2) Prepared & Analyzed: 04/28/2014 09:05 Source: C405283-02 Spike Source %REC RPD Ana. Res Wt Bag PQL Units Level Result */bPEC limits RPD U111I.t Notes Total Suspended Solids _ 14 1.0 mg/L 12 i8 10 OM-12 Batch 4D28036 - NO PREP LCS (4D28036-BSL) Prepared & Analyzed: 04/28/2014 13:36 Spike Source %REC RPD Ana Result Hag PQL UnfU Level Result %REC Limits RPD limit Notes PH 7.0 1.0 pH 7.01 99 99.101 Duplicate (4D28036-DUPI) Prepared & Analyzed: 04/28/2014 14:39 Source: C404081-01 Spike Source %REC RPD Ana iYle Result Hag PQL Units Level Result %REC Limi RPD Limit Notes PH 6.7 i.0 PH 6.8 1 25 Classical Chemistry Parameters - Quality Control Batch 4EO1006 - EPA 1664A Blank (4E01006-BLKI) Prepared: OS/Ol/2014 11:21 Analyzed: 05/02/2014 10:00 Spike Source %REC RPD Ana Result Bag POLL Units Level Result %REC Urnits RPD Limit Notes Oil & Grease (HEM) 2.60 U 5.00 mg/L LCS (4EO1006-BSI) Prepared: 05/01/2014 11:21 Analyzed: 05/0212014 10:00 Spike Source %REC RPD Ana hde Result Hag RU tlnits Level Result %REC Limi RPD t_jlat Notes Oil & Grease (HEM) 38.7 5.00 mg/L 41.3 94 78-114 LCS Dup (4EO1006-BSDI) Prepared: 051011201411:21 Analyzed: 05/02/2014 10:00 Spike Source %REC RPD Ana lldg Result Hag POL Yalu Level Result %REC Liml RPD Li i Notes Oil & Grease (HEM) 38.9 5.00 mg/L 41.3 94 78-114 0.5 18 FINAL This report redtes only to the sample as remyery by the laboratory, and may only be reproduced in fun. Page 5 of 8 (9 �ew www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batt* 4E01D06 - EPA 1664A - Canlinered Matrix Spike (4E01006-MS3) Prepared: 05/01/2014 11:21 Analyzed: 05/02/2014 10:00 Source: M201"31 Spike Source %REC RPD -Anal Result ftag PQL Units Level Result %REC Umift RPD Umft Notes Oil& Grease(HEM) 41.1 5.00 tng/L 44.7 3.27 85 78-114 FINAL This report relates only, to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 8 www.encolabs.com FLAGSJNOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. I The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (850/a or greater confidence) to make a "tentative identification". Q Analysis performed outside of method - specified holding time. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 8 -- a..aw.il3 4'�'rn�..-..+i.+w +�K „ 'Yl6"bY�f �'M"�.+q r-,�� ,,.,�,...m✓!, ant•'°�"'wY.r.r.Y`4�,R+.r-:�u:r+nM�-W».'p�.'Fw' :ua �':-w"'+tly-- -SY-v-."-^a; -rY :cry r ^,^+wu .'i'f ;va'>:n. .4t^x'.-"'-�%^r;a W: +F"�1'YnFius,av ,,::+f4.1: 'Fw�... rX•. .. .�-,_y: -dr .,. ' MI=NTR•L CONSERVATION LABQRATORIES,� :CHAIN'OF-CUSTDDY RECORD: ullNiiil.en ;• � • ENVIRaN - colabs�Cbit,'r�� ' •�� IU776 Conlial 'arl pr 4010 GIrxr,Ilw P,rA Cosa l Strife 111 t{1Q A YInPdainds tnrkushial Ct,. . ptlarrrlP,>-I,`'lPH24 Jarksvivrlln FL3221fFGDGi1- r Cttiry;i4C27511`� r 1 A•D7102Q{3(4p71 tM1-F'N►1350;fi'JAS'';.. 1-0JrIA}2�1i tOtF7"Ptizt4tlAf-2411G�tO { s:'(Ut.D{4GiJOfiit•�FrtctEllptaG7•;IS15 '.{�A�Q'�_ •1 iOt —:� _ �iR�x I. ' ',,AequrNad AnAlyua ROqupstpd•Tumuroundt. KELLOGS ShAC>t51AUSTrN F�OI?S' KEB Arldrnrs• - • - .. pw�oc! N,mnR}otir:' i ` x _ I ; fipn PlatrOd by ilw (pill, =A:©NE,QLfALITYfI.ANEz Stormw ker Jan Jul )- _ _ --- _ f. ? l' CIty/51p PO,i!{Slllirr}, Ilsw r 'CARY�yNO27513 �50638127(}: ;gyp. m �j� an.dard iirparlfnQ Cr>trtnct - !Z QF. -'^7i5 �1919i7'351�, Radne` Btem'an: �; i!< Expedited: Sn+nplof(el f ttriu'Rrtdinikrr tRrmtl f]llllri� Canlocl l' t r �L7 Nf n Timothy Klotz: Arcaunts PayableDine1�.;1- &,�Isr(aj 91ph[�tura �'. r y a S1ta Wrn11dn l:limn roan` Y 0•' � � ,!� i�!//� I:ab,W,�f�t?TlClt£N��_ 1 , fs�'{-i i "hqt: fir,^0�• sp I V/-% +Y : x FYR- eys i _... _ - _. _. �- i-• iPiaaervdliarrlSenGo�cd6tGnmbino.nnnocr�asuYl � T��lTi�{.R��i� -� y _ s vr' r i1 s ZIltl[tlOri I ', . ¢ A1Altist 141d1 0,14 5arnp�o1lEgAo1r wrttih' lionj paddCiurilir+lc, ":rirw ' , %Cmp�,Gi.b lseovafa'}: Genidlnars S�rrlplg.Comfn@ltl8 ( L I S ! t I s } r .r " I• i• L ' 4 - L I _ au 1 y ", '1 n ...:_ `: .; ..a �-..';''s...,�... __:... _..� � •--.'Y I e 1 r_ it L _ _ i P e, I. . i'. M <•-Tatrsl N`gt,Coi�f�tfnt� SerngaKll-Prdputurl6y . Ptfle!!ilme; Fl>�nrj R � R.i� noorvo4fly'. Oatar7ima.. • T CAriimantN5lsddalRrgloiliitgRm#lrlrMi111nIR :_ Ru�r�rid y, .- ilnsn{tima' RlrooivdEE3y,: pvtarrlms; _ r Ro4ngWahMBy; - 1}dlNimm• Racwiv+wfpY' [1yi Imn' � nmrr� 1aDP10rA3IL1 Mp1,; :.- ,'' CcndNrrn trhrl > s� �Acctaptable' - •' • - =:Unacao lalila fdglrix;GWCua�ma++a!iirE:&O:soeow�rtnkl;ipwd:nr, sE.srrmm6nr:swsurfnoow,ro"r,VJVJW�te++i�,nr'A�ASt60•Utttnr(Ontailin'mnunplltsi'. ProsonotYont!•ko�fi�HCl'ti•}fNpJ"S•iRSDt;Np;No0iE�0-0Vra[dafai7erairrrr>enla}. Noln X11 damgllod r ahmilrtrf la ENCO Leslie ore' in ncrcord.e no wilft llw tuinzg surd ndmJ[iicrte litfod vii the rnvei o of thin fntin; unldm pear w ilti,n apmomunks nmli ENCO Laboratories. Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, June 10, 2014 KELLOGGS SNACKS/AUSTIN FOODS (KE006) Attn: Rodney Bateman ONE QUALITY LANE CARY, NC 27513- RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater (Jan,July) ENCO Workorder(s): C406506 Dear Rodney Bateman, Enclosed is a copy of your laboratory report for best samples received by our laboratory on Wednesday, May 28, 2014. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL I tus report relates only to the sample as rec ivcl by the taboratory, and may only be reprodu®d In full. Page 1 or 7 OF � � www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: SWOT Lab ID: C406506-01 Sampled: 05/27/14 15:10 Received: 05/28/14 07:45 Parameter Hdd Date/Time(LI Prep Date/Timelsl Analysis Date/Timelsl SM 5220D-1997 06/24/14 05/30/14 I1:58 05/30/14 14:47 Client ID: SW02 Lab ID: C406506-02 Sampled: 05/27/14 15:15 Received: 05/28/14 07:45 pmutl a Hold Date/Timelsl Prep Date/Trmelsl Analysis Date/TMCW SM 522AD-1997 06/24/14 05/30/14 11:58 05/30/14 14:47 FINAL This report relates only to the sample as received by the laborawry, and may only be reproduced in full. Page 2 of 7 CEN www.encolabs.com SAMPLE DETECTION SUMMARY Analytr Results BA9 MDL POL vbdM MetbQd Notes Chemical Oxygen Demand 180 10 10 mg/L SM 5220D-1997 Client ID: SW02 Lab ID: C406506-02 Ana Rcsutts"—D—L EQE units lid Chemical Oxygen Demand 120 10 10 mg/L SM 5220EI-1997 FINAL This report relates onty to the sampte as received by the laboratory, and may only be reproduced In fnlL Page 3 of 7 www.enoolabs.com ANALYTICAL RESULTS Description: SW01 Lab Sample ID:C406506-01 Received: 05/28/14 07:45 Matrix: Surface Water Sampled.05/27/14 15:10 Work Order: C406506 Project: Stormwater (lan,luly) Sampled By:Timothy Klotz Classical Chemistry Parameters - EACO Cary ccVW —4tL (AC 5911 Analyte fCAS Numlg_r_Z Resul fim Units PF Jji)L ML Batch Method Analvzed my N r Chemical Oxygen Demand 180 mg/L 1 10 10 4E30016 SM 5220o-1997 05/30/1414:47 Cv ECL-0035 A Description: SW02 Lab Sample ID:C406506-02 Received: 05/28/14 07:45 Matrix: Surface Water Sampled:05/27/14 15:15 Work Order: C406506 Project: Stormwater (lan,luly) Sampled By: Timothy Klotz Classical Chemistry Parameters ^ - EAACD Cary crrtf Aed anayte W 591] Analvte ICAS Numbdl Results Fim 22M PF MOL EL Batch methad Analyzed B� Notes Chemical Oxygen Demand 120 mg/L 1 10 10 4E30016 SM 52200-1997 05/30/14 14:47 CV [ECL-0035] FINAL This report relates only to the sample as received by the laboratory, and Cray only W reproduced in feel. Page 4 of 7 u � � www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 4E30016 - Same Blank (4E30016-BLK1) Prepared: 05/30/2014 11:58 Analyzed: 05/30/2014 14:47 Spike Source %REC RPD Ana Result ►lag PQL Unit4 Level Result %REC mmillm RPD Unlit Notes Chemical Oxygen Demand 10 U 10 mg/L l.CS (4E30016-651) Prepared: 05/30/2014 11:58 Analyzed: 05/30/2014 14:47 Spike Source %REC RPD AL►dbde Res"I Elm ML uniu Level Result %REC Lirnift RPD unlit Notes Chemical Oxygen Demand 490 10 mg/L 500 98 90-110 Matrix Spike (4E30016-MSI) Prepared: 05/30/2014 11:58 Analyzed: 05/30/2014 14:47 Source:C405380-01 Spike Source %REC RPD Ana hdg Result flag eQL Llnib Level Rem %REC Limits RPD Limit Notes Chemical Oxygen Demand 540 10 mg/L 5D0 55 97 90-110 Matrix Spike Dup (4E30D16-MSD1) Prepared: 05/30/2014 11:58 Analyzed: 05/30/2014 14:47 Source: C405380-01 Anal]de Chemical Oxygen Demand Spike Source %REC Res sdS fhm e4L Units Level Rat %REC Limits RPD 550 10 mg/L 500 55 99 90-110 2 RPD Lima Notes 10 FINAL This report relates o* to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 7 www.encolabs.00m FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. 14RL Method Reporting Limit The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". FINAL This report relates only to the sample as rewKed by the laboratory, and may only be reproduced In full. Page 6 of 7 ENVIRONMENTAL CONSERVATION LABORATORIES: CHAIN -OE -CUSTODY RECORD t0775 Central Port Dr., 4810 Exeeutkn Park Court; Suit* 111 102a W*6&rrrds Industrial Court =Ee) Orlando, FL 32624 :JaGtsonvitte, FL 3220-6mg Cary.. NC 27511R, 9 , {407) WO-5314 Fax 1407) 850-5645 (904129113-W. Fax (9D4) 296-6210 -(919) 4673090 Fax (919) 467.3515. Page ) of Iievamame- Hart`& Hickman Projecl Number - RequesWAnalyses Requested Tumaroun Times Note : Rush requests sLky;ew to acceptance bylhetacirrty Standard � Expedited Due ! i Q O Address 3334 Hillsborough St Project Nomi Kellogg City1STrbp Raleigh; NC,27.607 PO N f Bijkg Irdo Tat Fax: 919-8474241 Reporting Coraact Timothy Klotz Sampler(sl Name, AKhalion (Prins) Timothy Klotz'(H&H) Billing Contact Rodney'Bateman (Kellogg) samplerlsl5}gnatur - A-L Facility a (d requiredl t Lab WofiCl7rder {� g �. V l r U 14v Preservation (Sao Goi (Combine as necessary) tt.m N Soml le 10 (Field ldentificstionj . � ,Collection Date Collection Time Comp I Grab. mi(I" codes)' . lot" 1101 contaii Sample Comments Sw o1 Svi Z �C sw-02 5_71-11i 11515 5•r-) Z -x <-- Total # of Containers Sample Kit Prepared By, DaWTime atar ane" Dataffne Comments - • • Deli Rocs' (! B oat ✓J �a }(,jJI (� l�f?' 1 DateJ1'Nrse Received By, Dese/Tane 17as S, amps on Receipt Q �r orwit'gn% Receipt V Acceptable Uneoceptable Malrlx:OW-Groundwater .So -Soil SE-Sedinwt SWSurfaiMWater .WWWastewater A•Air.O-other.(delailincdmmantsl I'raservanon:F" H-11U N•nNUJ 3-1125u4 Na•Navn o-umerOaelailincornmei NOW: All samples all' itled to ENCO Labs are 6 accardanm with the terms and eondWiare Bated on the foverse of tt1la form, unless prior written agreemems exist 1 SN�St Via Certified Mail July 2, 2014 Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED JUL 0 8 2014 CENTRAL FILES DWQIBOG Re: Reporting Year 2014 - Storm Water Discharge Monitoring Report Kellogg's Snacks -Cary Bakery One Quality Lane Cary, North Carolina Dear Sir/Madam, Enclosed please find a copy of the Storm Water Discharge Monitoring Report (DMR) for the first half of 2014 for: Kellogg's Snacks Cary Bakery One Quality Lane in Cary, NC This information is submitted as required under North Carolina Storm. Water General Permit No. NCG060000, Certificate of Coverage NCG060286. Our technical point of contact is: Mr. Tony DePietro (919) 677-3292 anthony.depietro@kellogg.com Mr. DePietro is available should any questions or problems arise during the review of this DMR. Please note that an exceedance of the benchmark value for chemical oxygen demand (COD) was noted at one of the sampling locations. Kellogg's is initiating Tier I response actions. C%wsktskazd73WppataULocaL'%Gcromfil mdows\Temporary ]ntenxt F3ks\Conimt.Outlo k43G)GDD244Storm ater Corry Idter.doc DWQ — Central Files July 2, 2014 Page 2 I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on any inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Sincerely, Steve Surovec Plant Manager Enclosures c:}users5uskud73WppdaiaUocaftmicrosoftluindowsltempormy inte et fiWconlmt_putIaW4gSdd--4\9Omn ater cover 1et[tt.doc ;•y;' STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT GENERAL PERMIT NO. NCGO60000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2014 CERTIFICATE OF COVERAGE NO. NCG06 0296 (This monitoring report is due at the Division no later than 30 days from FACILITY NAME Kellogg Company - Cary, NC Facility the date the facility receives the sampling results from the laboratory.) COUNTY Wake PERSON COLLECTING SAMPLES Timoth Klotz PHONE NO. 91 677-3292 CERTIFIED LABORATORY ENCO Las Lab # 591 Lab # PLEASE SIGN ON THE REVERSE 4 Part A: Specific Monitoring Requirements Y. Outfalla' :Date ! x.� 0053U �00400 , x 00340 . ' ::,:. 0055 3161 Na Sampled ._ Total Suspended :* pH, Chemical Oxygen Oil and Grease Fecal Coliform, Coilected, Salids, "Standard umts Demand,. rr g/ Colonies per 100 nil molddl r.'. a° �' m ,r i x Benchmark; „ 100 WithinT6:0 _ 9.0 .. HP r120 30 i• 1 Y11000: 8 Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark ranee for pH, you must implement Tier 1 or Tier 2 responses. See General Permit text. Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —yes Xno (if yes, complete Part B) Part IS: Vehicle Maintenance Acttvtty Monttorm Keouirements Outfall y s NoY "''' Date 498 ple Collected; 1 olddl'r IX00556 ss00530 r 00400Ilk ::. �I' ' i ��°011rcand;Crease :' " > m" �1 3."�' ,.TataliSuspended',Solids; v din „ti, s:.,a." ;, �. ^"'pH, s � ,',� w,.:. R� Standard"units', NewiMotor Od'=Usag"e Annual'avers► a allmo Benchmark' �,. �*30 °: ° ° 100 r :V 6ff 9.O t- Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses. See General Permit text. STORM EVENT CHARACTERISTICS: Mail Original and one copy to: Division of Water Quality Date I 1/23/14 (first event sampled) Attn: DWQ Ceniral Files Total Event Precipitation (inches): 0.64 1617 Mail Service Center Raleigh, North Carolina 27699-1617' Date 12116/1Alist each additional event sampled this reporting period, and rainfall amount) Total Event Precipitation (inches): 0.32 S W U-249-102107 Page 1 of 2 A- "I certify, under penalty of law,'that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) SWU-249-102107 Page 2 of 2