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NCG060265_COMPLETE FILE - HISTORICAL_20170120
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. DOC TYPE &(HISTORICALFILE ❑ MONITORING REPORTS DOC DATE ❑ Q 0I ^] b 14;):D YYYYMMDD SAMPLING DOCUMENTATION FORM DgrL RECEIVED JAN 2 0 Z017 Mission Foods CENTRAL FILES 401 Gateway Drive DWR SECTION Goldsboro, NC 27534 I Name of individual(s) who performed sampling: 1L /RtAk"o (-; i Date of I sample: Time of sample: Outfall sampled. 'S�FK WcW pH lev iI (std. units): Z!!!S 'T k Signat4re: -SWP? TO THE PLEASE-FILE',THIS'FORM INIHE. :ATTACH;A'COPY., .'-L'ABORATORY.,RE, OAKTON pH Meter Calibration Log kp 4 WEE) Mission Foods JAN 210 2017 401 Gateway Dr. Goldsboro, NC 27534 CENTRAL FILES DWR SECTION Instrument: OAKTON pHTestr 30 The pH meter is calibrated according to the EUTECH Instruments instruction manual. A copy of the calibration instruction manual is attached to the log. Date Calibration Reading (standard units) Person Conducting Calibration Initials l - zo 1 7,01 v�'.u'r�r�� 71 aceAnalyfical. annvpacefahs.mn December 30, 2016 Scott Shafer Mission Foods 401 Gateway Dr Goldsboro, NC 27534 RE' Project: Mission Foods 12/19 Pace Project No.: 92324482 Dear Scott Shafer: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on December 22, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures cc: Ejiri Atie, Mission Foods Rita Baeza, Mission Foods Theresa Jones, Mission Foods Kevin Miller, U.S. Compliance Corp Candace Rollins, Mission Foods Scott Shafer, Mission Foods Stephen Tingey, Mission Foods 2 r`c REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, 9 without the written consent of Pace Analytical Services, LLC. Page 1 of 14 aceAnalytical wwwpacefab&mn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: Mission Foods 12t19 Pace Project No.: 92324482 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersvi Ile. NC 28078 South Carolina Certification #: 99006001 North Carolina Drinking Water Certification #: 37706 Florida/NELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84 North Carolina Wastewater Certification #: 12 VirginiaNEtAP Certification #: 460221 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87643 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shatt not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 acmnalytrcal o wwwpacerabs c= Project: Mission Foods 12119 Pace Project No.: 92324482 Lab ID Sample ID 92324482001 001 SAMPLE SUMMARY Matrix Date Collected Date Received Water 12119/16 09:26 12122/16 11:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 14 aceAnalytrcal www.pamlabs.com SAMPLE ANALYTE COUNT Project: Mission Foods 12119 Pace Project No.: 92324482 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92324482001 001 EPA 1664B JMS 1 PASI-C SM 2540D MLS 1 PASI-A EPA 9040 ALC 1 PASI-A SM 5220D MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 14 aceAnalytical" www.peoelabs.00m ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Project: Mission Foods 12119 Pace Project No.: 92324482 Sample: 001 lab Il): 92324482001 Collected: 12/19/16 09:26 Received: 12/22116 11:35 Matrix: Water Parameters Results Units POL MDL ❑F Prepared Analyzed CAS No. 4ual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease <1.1 mg1L 5.0 1.1 1 12/30/16 07:09 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids <2.5 mg1L 2.5 2.5 1 12/23/16 10:59 9040 pH Analytical Method: EPA 9040 pH 6.0 Std. Units 0.10 0.10 1 12130/16 11:29 H6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand <12.5 mg/L 25.0 12.5 1 12/27/16 23:59 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12130/2016 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aceAnalytical wwwpsoelabs cam QUALITY CONTROL DATA Project: Mission Foods 12119 Pace Project No.: 92324482 QC Balch: 342989 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92324482001 Paco Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 1902466 Matrix: Water Associated Lab Samples: 92324482001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Oil and Grease mg1L <1.1 5.0 1.1 12/30/16 07:06 LABORATORY CONTROL SAMPLE: 1902467 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 39.2 98 78-114 MATRIX SPIKE SAMPLE: 1902468 92324190004 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 38.1 95 78-114 MATRIX SPIKE SAMPLE: 1902469 92324734004 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 38.0 95 78-114 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2016 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 s aceAnalytical wwwpacelebaaom QUALITY CONTROL DATA Project: Mission Foods 12119 Pace Project No.: 92324482 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersvilie, NC 28078 (704)875-9092 QC Balch: 342347 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92324482001 METHOD BLANK: 1899307 Matrix: Water Associated Lab Samples: 92324482001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Suspended Solids mglL <2.5 2.5 2.5 12/23/16 10:57 LABORATORY CONTROL SAMPLE: 1899308 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 242 97 90-110 SAMPLE DUPLICATE: 1899309 92324326001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 23.0 23.0 0 5 SAMPLE DUPLICATE: 1899310 92324189015 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mglL ND <5.0 5 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12130/2016 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 acmnalyticalo rvwwpatelaftcom QUALITY CONTROL DATA Project: Mission Foods 12119 Pace Project No.: 92324482 QC Batch: 343039 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92324482001 SAMPLE DUPLICATE: 1902692 Parameter PH SAMPLE DUPLICATE: 1902693 Parameter PH 92324482001 Dup Units Result Result Std. Units 6.0 6.1 92324758005 Dup Units Result Result Std. Units 6.9 6.9 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Max RPD RPD Qualifiers 2 9 D6,H6 Max RPD RPD Qualifiers 0 9 H6 Results presented on this page are In the units indicated by the "Units' column except where an alternate unit is presented to the right of the resutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, Date: 12/30/2016 04:46 PM without the written consent of Pace Analytical Services, t.l_C. Page 8 of 14 aceAna1jfta1" www.pacelabacom QUALITY CONTROL DATA Project: Mission Foods 12/19 Pace Project No.: 92324482 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 342609 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92324482001 METHOD BLANK: 1900516 Matrix: Water Associated Lab Samples: 92324482001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chemical Oxygen Demand mg/L <12.5 25.0 12,5 12/27/16 23:59 LABORATORY CONTROL SAMPLE: 1900517 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 778 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1900518 1900519 MS MSD 92324292001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand mg1L ND 750 750 801 801 106 106 90-110 D 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1900520 1900521 MS MSD 92324406001 Spike Spike MS MSD MS MSD , % Rec Max Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD RPD Qual Chemical Oxygen Demand mg/L 576 750 750 1290 1290 95 95 90-110 0 3 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2016 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 acmnalytical wwwpecelabs.com QUALIFIERS Project: Mission Foods 12119 Pace Project No.: 92324482 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260, N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. REPORT OF LABORATORY ANALYSIS This reporl shall not be reproduced, except in full, Date: 12/30/2016 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 ac,Mnalytical wwwpacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Mission Foods 12119 Pace Project No.: 92324482 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92324482001 001 EPA1664B 342989 92324482001 001 SM 2540D 342347 92324482001 001 EPA 9040 343039 92324482001 001 SM 5220D 342609 Date: 12/30/2016 04:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 / aceAlnaloical Laboratory receiving samples: Asheville ❑ Eden❑ vu,.vmenL Warne: uocument KBVISM Sept. 'Al, LUlb Sample Condition Upon Recel t SCUR Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS•033-Rev.01. t Pace Quality Office Greenwood ❑ HuntersvilleLP"" Raleigh[] Mechanicsville❑ • Client Name: W®# :92324482 0r1 PraJect #: 'Courier: E]red Ex UPS USPS []Client ❑ Commercial []Pace ❑Other: 92324482 Custody Sea[ Present? ❑Yes ❑14To Seals Intact? DY65' ❑No i!O Date/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap ❑Bubble Sags ❑None B6 Cher: Thermometer: ❑ Ili Gun ID: Type et ❑Blue ❑None amples on Ice, cooling process has sbbegun o I Correction Factor: Cooler Temp Corrected (-C): Biological', Tissue Frozen? ❑Yes [:]No,-ar+ No t/A Temp should be above free to 6-C USDA Regulated Soil (EN/A, water sample) Did samples ar ate in a quarantine tone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Intern!flonally, rives FTWO Including Hawaii and Puerto Rico)? ❑Yes ONO of Custody Present? es No N A 1. Samples Arrived within hold Time? oyes nNo r IN/A 1 1 Short Hold Time Analysis (02 hr.)1 Rush Turn Around Time Requester Sufficient Volume?' Correct Containers Used? -Pace Containers Used? Containers intact? Samples Field Filtered? Sample Labels Match COC? -includes Date ime ID Anal sls Headspace In VOA vials (>5-6mm)7 Trip Blank Present? Trio Blank CustadvSeals Present? Matrix: CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: _,,,moo N A 4. 6 o ❑N/A ❑No ❑N/A 6. s No N/A 7. 1 r fit.; ✓i\ cort—tCLAKv,A^ rS s Yes No A 8. Note If sediment is visible In the dissolved container . as ❑N/A 9. Vt' C 1J5 d w COG _ Yes ]No IINIA 2 10. — 1 5$ — V pi �_ t — (I Li ❑Yes ❑Ne 9Nl ❑Yes No N/A 11. 14, 5- et —� CI NeA.�� —ISY�(J'_'17{—f��t� ���i�4 lt+er , Field Data Required? ❑Yes []No Date/Time: 0011— y Project Manager SCURF Review: pate• I 1 ri Project Manager SRF Review: Date: Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this farm will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, Incorrect containers) Page 12 of 14 3 m a K d N 2 w_ c m x 00 in = n a b m � � 14 O m D o On a0— D' � c rD 9 fit C� N . N G3 i. 3 CI m o Q � CL d m 0 a N !+ p Lo V Cry N A w w F+ Item# BP4U-125 mL Plastic Unpreserved (N/A) (CH BP3U-250 mL Plastic Unpreserved(N/A) BP2U-500 mL Plastic Unpreserved (NIA) BP1U-1 liter Plastic Unpreserved (N/A) BP3S-250 mL Plastic H2504 (pH < 2) (Cl-) BP3N-250 mL plastic HNO3 (pH < 21 BP32-250 mL Plastic 2N Acetate & NaOH (>9) BP3C-250 mL Plastic NaOH (pH > 22) (CI-) WGFL4-Wide-mouthed Glass jar Unpreserved AG1U-1 Iker Amber Unpreserved (N/A) (Cl-) AG1H-1 liter Amber HOJpH < 2) AG3U-250 ml. Amber Unpreserved (N/A) (Cl-) AG15-1 liter Amber H2SO4 (pH < 2) AG3S-250 mL Amber H2SO4 (pH <,) xzzzA63A(DG3A)-250 mL Amber N H40 (N/A)(CI-) DG914-40 mLVOA HCI (N/A) VG9T-40 mL VOA Na2S203 (N/A) VG9U-40 mL VOA Unp (N/A) DG9P-40 mL VOA H3PO4 (N/A) ' VOAK (6 vials per kit)-5035 kit (N/A) V/GX (3 vials per kit)-VPH/Gas kit (N/A) SPST-125 mL Sterile Plastic (N/A— lab) $P2T--250 mLSterile Plastic (N/A —lab) 77 BP3A-250 mL Plastic (NH2►2SO4 (9.3-9.7) Cubitainer VS613-20 mL Scintillation vials (N/A) GN w N s O .Or t1 S si 3 7 PC- - w °0. 13 O -o = v X H O -fi o fD Cr as O rr X N A O dr 2 Crw N 3 0 1 _ Cr 94 m CL r+ o M vt O 7 LL O 3 w N i a a 0 N Q d w O r�+ O f0 1-� v n 0 0 c N O A aceAna1y ical' _-aanlael.mm CHAIN -OF -CUSTODY 1 Analytical Request Document The Cttainol-Custody is a LEGAL DOCUMENT. AD mkvant fieft must be completed a=ratcry. Scctlon A Section 8 Section C Page: of Required Clierd hkwmalim: Required PmiW InWmatiwr Ica lnlamiabon: Repon To: 2070898 Awm":L Copy To cwnye^yName: REGULATORYAGEN&,Add'•: -- - . -• t�"��;• • •' few• i" NPDES' .j— GROUNDWATER •F DRtNKING WATER i UST r RCRA r OTHER Frnti Te: ^ Pur�t� ve fRdar No.: P. Ounce rdSCt�i'N RataWrr one• ti 1Z -�lG`t az: Prajw Name: Pmii P1ol'a w.v 1,, tion �YLocation ; iLs-f-^'Siam: - ' RegtlestadDuo 0ateRAT:' - _. ProjectNumlxr.' . '- PacePratWr, - Requested Analysis Flltersd {YlNj st' - Sactlon D , Matrix Cedes — a.di.acaw nwmum� NATR", caDE a COLLECTED Preservafives Dlirtfting Waet DW water vVT Waste Wale WtM1f Product P $ $ 4 <1. ! °^t t+ U i� '• SoilfSoid SL -I '-.y-.:l3�'.=+ ,.}i- Lo t, �• -SAMPLE ID wipe � w�P Nz n 4 jAr{1'rt •:., ..AR�1 • .pt i� - ! itE{ . :/ =r(„^ s a ,? , 't • t- Sample iDs MUST BE UNIQUE Tosw TS �i•:.s;F. l i N,.s,A, t1U1or,� r,. .. ?OT_fi:.Uj O a iv: - fi ;�� F 7D '� .. o 171 ''n is U a ia' ,': �u�t: -' y';" 'rJ :: ; :0 q a.O N p �!• ZO On yy "' m t .-..G r m /7 ^7 � f+�2r-'i c{ j' e pATE•1 t :TIME . `:OutTt=if : �TIIdE is ;w: :.a Z 2 2 S Z Z i O w i T ¢ Pave Project NO 1 Lab LD. E3 'yZ F -ty 9 P' r 11 12 l:f rr^ f. •`° ADORIONAL CDYMENTSt;: zt %tau.i - - ' r. - RELINQUISNfl0 8Y l AFFILIATION }� - - - - TE ! -- - �_;TAlE . -r ACCEPTED BY I AFFtt.IATIOtt -- •, - - - :'DATE,- - TIME i r SAMPLE CONDITIONS times .� v SAMPLER "ME AND SIGNATURE'. ' `` '+ PRINT Name of SAMPLER: 1 U S! IN —1 C C�.tc f o a' °' } V SIGNATURE of SAMPLER: DATE Signed - { ' NA1r `t - i �: a—' _$ '0 E • t��. _L• !MMlDDIYYI: -arowury Nmt: By sip dv atis tam you We ameom,0 Pads NET Ja 6vy pwp-,Wre teem w o myWW+'7 le bw aNnn d 1.5% PWr mane, ter any -nuns rvl Po'e wits, 30 arf - F-ALL-4020rev,07, 15-May-=7 Q 0 v a (�t4 t4 s}k--Ip 11 1A st J'�YA t ) January 13, 2015 Regional Office Supervisor Washington LQS Regional Office 943 Washington Square Mall Washington, NC 27889 Re: NCG060000 Tier Three Written Notification Mission Foods 401 Gateway Dr. Goldsboro, NC 27534 Permit: NCG060265 To Whom It May Concern: On December 29, 2014 Mission Foods conducted a stormwater sampling event at one outfall. The facility received the results of the analysis from the laboratory, Pace Analytical, on January 8, 2015 The pH result of the sampled stormwater was 5.4 standard units. This is the sixth occasion the pH at Mission Foods has been outside the benchmark limit. The analytical results of the aforementioned sample are enclosed. Thom Edgerton of the DEMLR Washington Regional Office was notified of the exceedance via email on 1/13/215 by U.S. Compliance on behalf of Mission Foods. This letter serves as the Tier Three written notification as required by Permit No. NCG060000. If you have any questions regarding this notification I can be reached at (952) 567-5625 or by email at mpeterson@uscompliance.com please contact me at your convenience. Sincerely, Myles Peterson Environmental Specialist Enclosure: Stormwater Sample Results Cc: Omar Jimenez — Mission Foods U.S. Compliance Corporation 520 Third street • suite 100 . Excelsior, MN 55331 + Phone 952.252.3000 • Fax 952.252.3001 www.uscompliance.com aceAnalXical www,pecelabS.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704 )875-9as2 January 08, 2015 Paul Gillard Mission Foods 401 Gateway Drive Goldsboro, NC 27534 RE: Project: Stormwater 12130 Pace Project No.: 92231250 Dear Paul Gillard: Enclosed are the analytical results for sample(s) received by the laboratory on December 30, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures cc: Myles Peterson, U.S. Compliance Corp 2�SQpCCRFp���O TNI �geORA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 aceAnalytical rmw.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hurtersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: Stormwater 12/30 Pace Project No.: 92231250 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification M E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certificaton #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 UirginiafVELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 FloridalNELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 Pace Analytical Services, Inc. ace Analytical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 WWW..pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: Stormwater 12130 Pace Project No.: 92231250 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92231250001 001 EPA 16648 CLW 1 PASI-C SM 2540D MDW 1 PASI-A EPA 9040 MAB 1 PASI-A SM 5220D JTJ 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 ace Analytical wwwpacelabs.mm Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Stormwater 12130 Pace Project No.: 92231250 Sample: 001 Lab ID: 92231250001 Collected: 12/30/14 08:00 Received: 12130/14 10:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg[L 5.0 1 12/30/14 15:40 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 34.9 mgtL 4.6 1 12/31/14 10:29 9040 pH Analytical Method: EPA 9040 pH 5.4 Std. Units 0.10 1 12/31/14 12:50 H6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 60.0 mg/L 25.0 1 01/07/15 14:00 Date: 01/08/2015 03:34 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 alioMnalXical ® www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Stormwater 12130 Pace Project No.: 92231250 QC Batch: GCSV119955 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92231250001 METHOD BLANK: 1361536 Associated Lab Samples: 92231250001 Parameter Units Oil and Grease mglL LABORATORY CONTROL SAMPLE: 1361537 Parameter Units Oil and Grease mglL MATRIX SPIKE SAMPLE: 1361538 Parameter Units Oil and Grease mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 12/30/1415:38 Spike LCS LCS Conc. Result % Rec 40 37.3 93 92231292004 Spike MS Result Conc. Result ND 40 37.7 % Rec Limits Qualifiers 78-114 MS % Rec % Rec Limits Qualifiers 93 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/08/2015 03:34 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 ace Analytical wwwpacelabs.= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Fluntersville, NC 28078 (704)875-9092 Project: Stormwater 12130 Pace Project No.: 92231250 QC Batch: WET135037 QC Batch Method: SM 2540D Associated Lab Samples: 92231250001 METHOD BLANK: 1361966 Associated Lab Samples: 92231250001 Parameter Units Total Suspended Solids mglL QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit 'Analyzed Qualifiers NO 2.5 12/31/1410:24 LABORATORY CONTROL SAMPLE: 1361967 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 236 94 90-110 SAMPLE DUPLICATE: 1361968 Parameter Total Suspended Solids SAMPLE DUPLICATE: 1361969 Parameter Total Suspended Solids 92231388001 Dup Units Result Result mglL 117 133 92231390001 Dup Units Result Result mg1L 90.7 100 RPD Qualifiers 13 D6 RPD Qualifiers 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /08/2015 03:34 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aciMnalytical wm..pacelabs.c m Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 2807E (704)875-9092 Project: Stormwater 12130 Pace Project No.: 92231250 QC Batch: WET135039 QC Batch Method: EPA 9040 Associated Lab Samples: 92231250001 SAMPLE DUPLICATE: 1361974 Parameter Units pH Std. Units SAMPLE DUPLICATE: 1361975 Parameter Units pH Std. Units 1@11It1R ASIG jtall-41111AD Analysis Method: EPA9040 Analysis Description: 9040 pH 92231100003 Dup Result Result 7.1 7.1 92231250001 Dup Result Result 5.4 5.0 RPD Qualifiers 0 H6 RP❑ Qualifiers 7 H6 Results presented on this page are In the units indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/08/2015 03:34 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 aceAnalyfical wmvpscefabs.ccm Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Stormwater 12130 Pace Project No.: 92231250 QC Batch: WETA121506 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92231250001 METHOD BLANK: 1364916 Associated Lab Samples: 92231250001 Parameter Units Chemical Oxygen Demand mglL LABORATORY CONTROL SAMPLE: 1364917 Parameter Units Chemical Oxygen Demand mglL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 25.0 01/07/1514:00 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 726 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1364918 1364919 MS MSD 92231013001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mglL 30.0 750 750 729 729 93 93 90=110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1364920 1364921 MS MSD 92231423001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua) Chemical Oxygen Demand mg1L 36.0 750 750 753 753 96 96 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/08/2015 03:34 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 acmnalytical www.pacelabs.= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)B75-9092 QUALIFIERS Project: Stormwater 12130 Pace Project No.: 92231250 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA recommended holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/08/2015 03:34 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 aceAnalytical ..pacelabs.mn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)B75-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater 12/30 Pace Project No.: 92231250 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92231250001 001 EPA 1664B GCSVI19955 92231250001 001 SM 2540D WET/35037 92231250001 001 EPA 9040 WET/35039 92231250001 001 SM 5220D WETA/21506 Date: 01/08/2015 03:34 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch Page 10 of 12 weAnaloqql CHAIN -OF -CUSTODY! Analytical Request Document C%J The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed acwrat*. 3 J Page: Of • Section ASection C Section B Section -0.2 1,883 .0 Required Project lnforrnaWn: Invoice Wormation: Corr ReponT A Copy TO: fKf 11L 6�7!� 14F_ 7c-�- tz :5 o Y_? C1;1q1r1rSa11Z L f Fadla 57 RE�GULAT RY AGENCY 7��L!) A ti DRINKING R UST F-. RCRA t F. U OTHER M' T40" Order No.; Z '2M"I Quate i-A a 4 n: _7 Project N43ff*: Pace Project ,SiloL t..n Manager FT STATE: 0 29- R"vested Out DaterrAT.i --J' c Project Number. V. POW profle Requested Anatysis Filtered (YIN) Matrix Codes �%rmATRIX- I 'Cor)r' COLLECTED P4servatives - 7 Drinking Water OW Water YVT Sit Waste Water ww -Product p F Scohwo-sITECIDMPOSM L) Z soinctid SL Oil OL ,-SAMPLE-0- *-_- 11. � I ...1wt p-0 .-:;TV jAjr�_ AR '!Di'MUST.BE w LU < Z Rl; 10 IT 7 Z. :J(. Sim UNIQUE' Tisie 0, -0 (L �:, w z CD tty,Otherr • L -, X.� uj� LU '0. L) 0 IL e. •ELI LLI� 0 0 0 0 W I 1,21, 0-1' DATE.-,� TIME %DATE". 1 11ME U) Z L) a: w z z 'D M 8 < J JX'D I. —.Pace Project NoAab I.D. 7 1 6, 225 1:00 /1,2-. ,,:00 Z. 1 I I -2, -4. 16 'T. -12 —645mMEF�kS, I: ;VDMOWAI S RELINQUISHED BY I AFFILIATION DATE. TIME T AC FIF I ATION DATE TIME SAMPLE CONDITIONS 7, Ilk J4 SAMPLER NAME AND SIGNATURE PRINT T Name of SAMPLER: _39 A,,! P,01J 0oo---dA t2 Z DATE Signed �(Z_ SIGNATURE of SAMPLE "/,, "V 141-V Z3 �� 'impcfant Not .- BY signing ibis fcnn you are ameptiPace's NET 30 day payment terms and agreeing to blo charges of 1.5% per month for any imoiws' not paid Mthin'30 days. F-ALL-Q-020rev.07. 15-MRV-2f)l17 .:� at:eArl�lyflcaf' Client Name: M sstov, Document Name: Sample Condition Upon Recell Document Numbe: _. F-CHR-CSr003•rev.15 Document Revised: SepternOer 22. ZU14 r Page 1 of 2 Issuing Aut_horify: Pace Hun tersville Quality Office Courier; ed E ❑ UPS❑ USPS❑ Client❑_.� �Com_ mercial❑ Pace Other Custody Sea on Cc 6IerlBOx Present: ❑ yes G_ no Seals Intact: ❑ .yes ❑ no Packing Material: ❑ Bubble VE)p ❑ Bubble Bags R None ❑ Other Thermometer Used: IR Gun T1401 Type of Ice: (! Blue None 9-Samplos on Ice, cooling process has begun Temp Correction Factor T1401 No Correction Corrected Cooler Tern ::C I' Temp should be above freezing to 61C Biological Tissue Is Frozen: yes No Date and Inlltals f •or xaml/ v contents: Comments: Chain of Custody Present: es ONO ❑NIA 1, Chain of Custody Filled Out: es ❑NIA 2, Chain of Custodyhe Relin ulsd: O❑No ayes t�No ❑NIA 3. Sampler Name & Signature on COC: 1114as ONO ❑NIA 4. Samples Arrived within Hold Time: 19�es ONO ❑NIA 5. Short Hold Time Analysis <72hr : Oyes 1940 ❑NIA 6. Rush Turn Around Time Requested; ❑Yes go El N/A 7, Sufficient Volume: M es ONO ❑NIA 8, Correct Containers Used: -Pace Containers Used: Clyes ONO ❑Y ONO ❑NIA ❑NIA 9, Containers Intact: Yes ONO ❑NIA 10. Filtered volume received for Dissolved tests Dyes ONO 5<A 11. Sample Labels match COC: -Includes date/time/1D/Anal sis Matrix: Yes ONO ONIA 12, Ail containers needing preservation have been checked. Ail containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, coliform, TOC, 0&G, VJI.ORO (%eater) ONO Zy'aNo ❑No ❑N!A ❑NIA 13. Samples checked for dechlorinatlon: Yes ONO 0N1 4. Headspace in VOA Vlals �6mm): Dyes []No Nr 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # if purchased): ❑yes ONO ❑Yes ONO Nl 0141A 6. Client Notification/ Resolution: Field Data Requlred9 Y 1 N Person Contacted: Date/Time: Comments/ Resolution: 5CURF Reviewl Date: r SRF Revlew; Date: t J/ < Note: Whenever there Is a discrepancy affecting North Caroll a compllance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, Incorrect preservative, out of temp, Incorrect containers) t92231250;. Page 12 of 12 November 19, 2014 Regional Office Supervisor Washington LOS Regional Office 943 Washington Square Mall Washington, NC 27889 Re: NCG060000 Tier Three Written Notification Mission Foods 401 Gateway Dr. Goldsboro, NC 27534 Permit: NCG060265 To Whom It May Concern: NOV 2 5 2014 On October 15, 2014 Mission Foods conducted a stormwater sampling event at one outfall. The facility received the results of the analysis from the laboratory, Pace Analytical, on October 24, 2014, The pH result of the sampled stormwater was 4.2 standard units. This is the fifth occasion the pH at Mission Foods has been outside the benchmark limit. The analytical results of the aforementioned sample are enclosed. This letter serves as the Tier Three written notification as required by Permit No. NCG060000. If you have any questions regarding this notification I can be reached at (952) 567-5625 or by email at mpeterson@uscompliance.com please contact me at your convenience. Sincerely, /k Myles Peterson Environmental Specialist Enclosure: Stormwater Sample Results Cc: Omar Jimenez - Mission Foods NOV 2 6 2014 a 'a U.S. Compliance Corporation 520 Third Street • Suite 100 • Excelsior, MN 55331 • Phone 952.252.3000 • Fax 952,252,3001 www.uscompliance.com aceAnalytical vnvwpacefabs.com October 24, 2014 Paul Gillard Mission Foods 401 Gateway Drive Goldsboro, NC 27534 RE: Project: 001 Pace Project No.: 92221681 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Paul Gillard: Enclosed are the analytical results for sample(s) received by the laboratory on October 16, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures cc: Myles Peterson, U.S. Compliance Corp pCCR,�/��o TNI OR A.t REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 aceAnalytrtal wmv.pacelahS.cgm Pace Analytical Services, Inc, 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: 001 Pace Project No.: 92221681 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Flodcla/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 Pace Analytical Services, Inc. ace Analytical ® 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 wtm pacelabs.cam (704)875-9092 SAMPLE ANALYTE COUNT Project: 001 Pace Project No.: 92221681 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92221681001 001 EPA 1664E CLW 1 PASI-C SM 2540D MLS 1 PASI-A EPA 9040 MAB 1 PASI-A SM 5220D JTJ 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 Pace Analytical Services, Inc. aceAnalytical 9800 I<incey Ave. Suite100 Hunlersville, NC 28078078 wvwJpacalaes.com (704)875-9092 ANALYTICAL RESULTS Project: 001 Pace Project No.: 92221681 Sample: 001 Parameters Lab ID: 92221681001 Collected: 10/15/14 OR28 Results Units Report Limit DF Received: 10/16/14 08:00 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 10/17/14 13:19 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg1L 3.9 1 10/17/14 11:12 9040 pH Analytical Method: EPA 9040 pH 4.2 Std. Units 0.10 1 10/17/14 13:28 1-16 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 25.0 mg1L 25.0 1 10/23/14 12:50 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 02:42 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 aceAnalXicah wwwpacelabs.com Project: 001 Pace Project No.: 92221681 QC Batch: GCSV119215 QC Batch Method: EPA 1664B Associated Lab Samples: 92221681001 METHOD BLANK: 1309682 Associated Lab Samples: 92221681001 Parameter Units Oil and Grease mg1L LABORATORY CONTROL SAMPLE: 1309683 Parameter Units Oil and Grease mg/L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 10/17/14 13:11 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 40 37.7 94 78-114 MATRIX SPIKE SAMPLE: 1309684 35159160001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L 1 A U 41.7 34.6 83 78-114 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 02:42 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 Pace Analytical Services, Inc. aceAnalyiical 9800 Kincey Ave. Suite 100 078 Hunlersville, NC 28078 wwwpacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: 001 Pace Project No.: 92221681 QC Batch: WET133796 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 25400 Total Suspended Solids Associated Lab Samples: 92221681001 METHOD BLANK: 1309447 Matrix: Water Associated Lab Samples: 92221681001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 10/17/14 11:09 LABORATORY CONTROL SAMPLE: 1309448 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 256 102 90-110 SAMPLE DUPLICATE: 1309449 92221614001 Cup Parameter Units Result Result RPD Qualifiers Total Suspended Solids ni 5.4 ND SAMPLE DUPLICATE: 1309450 92221690002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L ND ND Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 02:42 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 acmnalytical wwwpacelabs.mm QUALITY CONTROL DATA Project: 001 Pace Project No.: 92221681 QC Batch: WET133794 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92221681001 SAMPLE DUPLICATE: 1309387 Parameter pH SAMPLE DUPLICATE: 1309388 Parameter pH 92221443001 Dup Units Result Result Sid. Units 7.8 7.8 92221843002 Dup Units Result Result Std, Units 6.6 6.5 RPD Qualifiers 1 H6 RPD Qualifiers 1 H6 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 02:42 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 • ace Analytical wwwpacefabs.eorn QUALITY CONTROL DATA Project: 001 Pace Project No.: 92221681 QC Batch: WETA120641 Analysis Method: SM 5220D QC Batch Method: SM 52200 Analysis Description: 5220D COD Associated Lab Samples: 92221681001 METHOD BLANK: 1313522 Associated Lab Samples: 92221681001 Parameter Units Chemical Oxygen Demand mg/L Matrix: Water Blank Reporting Result Limit , Analyzed Qualifiers ND 25.0 10123/1412:50 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1313523 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 757 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1313524 1313525 MS MSD 92221490005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 750 750 748 748 99 99 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1313526 1313527 MS MSD 92220339026 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 48.0 750 750 805 805 101 101 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 02:42 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 aceAnalytical o www.pacelabs.com QUALIFIERS Project: 001 Pace Project No.: 92221681 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPAguidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA recommended holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/24/2014 02A2 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 aceAnalytical www.pacelabs.ccom QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: 001 Pace Project No.: 92221681 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92221681001 001 EPA1664B GCSVl19216 92221681001 001 SM 2540D WET133796 92221681001 001 EPA 9040 WET133794 92221681001 001 SM 5220D WETN20641 Date: 10124I2014 02:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch Page 10 of 12 aceki iy icai CHAIN -OF -CUSTODY / Analytical Request.Document N 4 The Chairwf-Custody is a LEGAL DOCUMENT. M relevant fields must bo compiet" accurately. I' .......... Pago: of Section A Section B Section C _ �-' ' �• • J . IPL ' -- - _ .. Required Cfient I;"tian: . - . Required Project Information: Invoice Wormation Company: •-. • / • . ' - - • • •. .Report To: - /'` . Attention: e—, 7fCv.`a� `%rJc� i lna�ai✓ l,! Address:Lf // r t �� Copy To: f +. Company Name: . /f . v ..•<,` /.'i/' .•ice• .;q r r c• / . - - REGIJ ATORY.•AGEN& ' / ! r �_✓ �. f )�} Address: tr r r. tom, •- DRINKING WATER NPDESt -. .'GROUND ytf y- ... --WATER- s 7 - UST f ;RCRA «_ :,F r..,OTHER - Emml:To:, Purchase Order No.: Paco Quote f-;rF r)��.t _L1-:�(�r••�9'%'7�7•, .,(i>l..r:. - Roforcrwa: Phone:. Fax: P ectName: Pam Pro,= Site Location Managmr. r^j 3" .-' STATE: RequoslccQuoDatelTAT-.7r:Z; :. ..,_ '1.' - ProjedNumber.;. � .� - �.. ,. _ Pmprorio#:J. t _'t .. - .-J'1. »°rRequested AnaEysjs.Fittered'(Y/N)� •�73"': - r fA Section D -Matrix Codes Roq,AmdCrb&ite wmaawrir "- �� -!; .:J.A� TRIX�I CCIDE- — +o a - COLLECTED - Preservatives:. z i'r• " ' , _ - Drinking water OW - z'ff::'• , Water Water WT yt tj - Waste Water. YYYJ - Product P 9 a mCOW sE CF�WGPAa -• - SoNsoGd •5L ..-.. - - Q i _ yi.. i- 'r SAMPLE ID Oil OL U _ .t (A.z4.9f,.:)-• •.,•• Aires - AR.• SamplelDshSUSTBEUNIQUE )Tvssl�m� ,='s�� TSB• 'o.'.ul- 'O' :' *tr° a "wa z ' I. - y - J• - ''+: o -Uy a - oN ; g F. 'Si• �_='- '••F LL CL OoT. co ( QU) r a) — DATE - - TIME: GATE r TIME •- h = Z x Z Z O ' I fr _ 77P2ce Project No.! Lack I.D. co 3. ` .8` 9, i2 • - ADD1710NA' COMMENTS _' RELJNQUISFiE6 BY f AFFILIATION DATE TIME 'ACCEPTED BY 7 AFFILIATION. DATE TIME. SAMPLE CONDITIONS •Y SAMPLER NAME AND SIGNATURE �: �1 o Ti ,• PRINT Name of SAMPLER: r(f ni✓ $ _z i n-2 U-a Er r i DATE Signed SIGNATURE a1SAMPLER: I ram✓ • - � (MMrODNY): •Imponarri Noto: By Skpng Nos roam yoti are accepting Pace's NET 30 day payment terms ar+d agreoing to late chargesel 1.5% per month [or any iavaces not paid within 30 days. F•ALL-0-020revr.07, 15-May-Zoof Sam Ie,Canciitian Upon Receipt "SCUR '. Page 1 of 2 act7Alt<�lytfca1* � Lncument Nurribei Issuing Authority: Ft{3HR-CS-003-iev:15., Pace HUntorsv lle Qua it Office Client Name._,g,v�, Courier: ❑ 1 ed _ ❑ UPS❑ USO C,I CHentQ' Comm' Pace Other , b '�j_`':. s. s • ' Custody Seal on,Cooler[Box Present: ❑ es no ❑ t _ Y i-.;. Beals intact:. [❑ yes no � 't } r . Packing Material: &bbleNDp Bubble Bags ❑ None [; Other Thermometer Used: Ift.Gun 140 Type of Ice:. et Blue None E?6amples on ice, cooling process has begun Temp Correction Factor T1401 No Correction Corrected Cooler Temp" 3.S `C Biological Tissue is Frozen: Yes No vt Date and Initials�f person examining canfeiits: C � 1 r117 GJL�I _ Temp should be above freezing to 61C ! Comments: Chain of Custod yPresent: C s ❑No ❑NIA 1. ' �,� i Chain of CustodyFilled nut: bYes [3 o ON/A. 2. o a etc, tv 5i s ,� 1 Chain of Custody Relinquished, Dyes. fNNo ❑NIA 3, If;g6LW 0 IS N O D Sampler Name & Signature on COC: IJYes ❑No ❑NIA 4. Samples Arrived within Hold Time: Yes ❑No ❑NIA 5, t Short Hold Time Analysis <72hr : 0Yes O'No ❑NIA 6. Rush Turn Around Time Requested: QYes ONo ❑NIA 7. Sufficient Volume: es ❑No . ❑NIA 8, Correct Containers Used. i s ❑No ❑NIA 9. -Pace Containers Used: 0<(11 ❑No ❑NIA Containers Intact: &fes •11No ❑NIA 10. t! Filtered volume received for Dissolved tests E:j7ees :❑No fINIA 11. Sample Labels match COC. Y s ❑ho ❑NIA 12• F -Includes dateltime/lD/Anal sis Matrix: All containers needing preservation have been checked. t ❑No ❑NIA 13. Alt containers needing preservation are found to be In �� LJYes ❑No' Cl.N/A. compliance with EPA recommendation. , ezeeptions: VOA, celirorm, TOC, O&G, W -DRO {water} G Y—,, ❑No" Samples chocked for dechlorination: F:7Yes ❑ No, 't36A 14. Headspace in VOA Vials >6m): DYes ❑No. FKIA 15, Trip Blank Present: [,]Y©s ❑No: EJ'N)A 16. Trip Blank Custody Seals Present ❑Yes ❑No, ]NIA Pace Trip Blank Lot # (if purchased Client Notification/ Resolution: Field Data Required? - Y ! N Person Contacted: :i Date/Time: 1 Comments/ Resolution: J SCURF Revlewt Date: ".1 22.1j6t SRF Review: Date: /per r .: fflll�ilf�l�I�l���alff�llf{+ ;. Note: Whenever there is a discrepancy affecting North C rollna compliance 822216gy samples, a copy of this form will be sent to the North'Cr;rolloa DEHNR Certification Office ( Le out of hold, Incorrect preservative, out of temp, Incorrect containers) (if no label a Page 12 of 12 Compliance Inspection Report Permit: NCG060265 Effective: 12/01/12 Expiration: 10/31/17 Owner: Gruma Corporation SOC: Effective: Expiration: Facility: Mission Foods County: Wayne 401 Gateway Dr Region: Washington Goldsboro NC 27534 Contact Person: Jerry Feagley Title: Phone: 919-778-7889 Ext.237 Directions to Facility: System Classifications: Primary ORC: Secondary ORC(s): On -Site Representative(s): Related Permits: Inspection Date: 11/13/2014 Primary Inspector: Thom Edgerton Secondary Inspector(s): Certification: Phone: Entry Time: 10:00AM Exit Time: 12:OOPM Phone: 252-946-6481 Reason for Inspection: Follow-up Inspection Type: Technical Assistance Permit Inspection Type: Food/Tobacco/Soaps/CosmeticslPublic Warehousing Stormwater Discharge COC Facility Status: ❑ Compliant ❑ Not Compliant Question Areas: 0 Storm Water (See attachment summary) Page: 1 Permit: NCG060265 Owner - Facility: Gruma Corporation Inspection Date: 1111312014 Inspection Type : Technical Assistance Reason for Visit: Follow-up Inspection Summary: Met with several ranking members of the staff which were very helpful in providing information and understanding guidance. Operation will review their sampling requirements and proto-call. PH numbers will be shared and forwarded to me as necessary for further anylsis toward compliance. I can be reached by calling (252) 948-3963 or by emailing the information to thom.edgerton@ncdenr.gov. Page: 2 Edgerton, Thom From: Edgerton, Thom Sent: Friday, November 07, 2014 4:40 PM To: Impeterson@uscompliance.com' Subject: Inspection Attempt Attachments: NCG060265 - Mission Foods - Kinston - 11062014.pdf Hello, See the attached and let me know when we can meet. Thanks, Thom Thom Edgerton, Environmental Engineer North Carolina Department of Enviionment and Natural Resources (NCDENR) Division of Energy, Mineral, and Land Resources (DEMLR) Land Quality Section (LQJ Washington Regional Office (WaRO) 943 Washington Square Mall Washington, NC 27889 (252) 948-3963 Phone E-mail correspondence may be subject to the North Carolina Public Records taw and may be disclosed to third parties. .9 1\� Compliance Inspection Report Permit: NCGO60265 Effective: 12/01/12 Expiration: 10/31/17 Owner: Gruma Corporation SOC: Effective: Expiration: Facility: Mission Foods County: Wayne 401 Gateway Dr Region: Washington Goldsboro NC 27534 Contact Person: Jerry Feagley Title: Phone: 919-778-7889 Ext.237 Directions to Facility: System Classifications: Primary ORC: Secondary ORC(s): On -Site Representative(s): Related Permits: Inspection Date: 11/06/2014 Primary Inspector: Thom Edgerton Secondary Inspector(s): Certification: Phone: Entry Time: 12:30PM Exit Time: 12:35PM Phone: 252-946-6481 Reason for Inspection: Other Inspection Type: Compliance Evaluation Permit Inspection Type: FoodlTobacco/Soaps/Cosmetics/Public Warehousing Stormwater Discharge COG Facility Status: ❑ Compliant ❑ Not Compliant Question Areas: Other (See attachment summary) Page: 1 Permit: NCG060265 Owner - Facility:GrumaCorporation Inspection Date: 1110612014 Inspection Type : Compliance Evaluation Reason for Visit: Other Inspection Summary: I showed up unannounced to offer guidance toward PH compliance, but was told by the main office that no one was available to meet. I left my business card expecting to have a message when I returned to the office, to plan an inspection and offer guidance to the PH being outside benchmark again. This is unacceptable... I will resolve this issue. Page: 2 Permit: NCG060265 Owner - Facility:GrumaCorporation Inspection Date: 11/06/2014 Inspection Type: Compliance Evaluation Reason for Visit: Other Other Yes No NA NE Comment: Page: 3 r�w , Central Files: APS _ SWP �• ��;rvC Joe rn L+nS �'J t �, 718 " 7$ 817 11/4/2014 Permit Number NCG060265 a. �1Jh r 3 s S Permit Tracking Slip I,r .31 Program Category Status Project Type NPDES SW Active Renewal Permit Type Version Permit Classification FoodrTobacco/Soaps/Cosmetics/Pubiic Warehousing Stormwater Discharge COC 3.00 COC Primary Reviewer mack.wiggins Permit Contact Affiliation Jerry Feagley ( *917)9 7 -44 237 Coastal SWRule . 401 Gateway Dr Goldsboro NC 27534 Permitted Flow Facility Facility Name Major/Minor Region Mission Foods Minor Washington Location Address County 401 Gateway Dr Wayne 11 Facility Contact Affiliation Goldsboro NC 27534 S Eric Mazur 401 Gateway Dr Owner Goldsboro NC 27534 Owner Name Gruma Corporation Dates/Events Owner Type Non-Govemment Owner Affiliation e ]Z� Melissa Mendoza 1159 Cottonwood Ln Ste 200 Irving TX 75038 Scheduled Orig Issue App Received Draft Initiated Issuance Public Notice Issue Effective Expiration 4/18/2003 6/6/2012 1211 /2012 1211 /2012 10/31/2017 Regulated Activities Requested !Received Events Food and kindred products manufacture Outfall 001 3 5-. x7, 9 - �C3L �r• �z� T S �lce�• Waterbody Name Streamindex Number Current Class Subbasin Stoney Creek 27.62 C;NSW 03-04-05 G 01-n P, Z.) w OPP 0 rak'*� October 16, 2014 Regional Office Supervisor Washington LQS Regional Office 943 Washington Square Mall Washington, NC 27889 Re: NCGO60000 Tier Three Written Notification Mission Foods 401 Gateway Dr. Goldsboro, NC 27534 Permit: NCG060265 To Whom It May Concern: RECEIVED OCT ? 1 2014 On September 9, 2014 Mission Foods conducted a stormwater sampling event at one outfall. The facility received the results of the analysis from the laboratory, Pace Analytical, on September 18, 2014. The pH result of the sampled stormwater was 5.1 standard units. This is the fourth occasion the pH at Mission Foods has been outside the benchmark limit. The analytical results of the aforementioned sample are enclosed. This letter serves as the Tier Three written notification as required by Permit No. NCG060000. If you have any questions regarding this notification I can be reached at (952) 567-5625 or by email at mpeterson@uscompliance.com please contact me at your convenience. Sincerely, Myles Peterson Environmental Specialist Enclosure: Stormwater Sample Results Cc: Omar Jimenez -- Mission Foods U.S. Compliance Corporation 520 Third Street • Suite 100 • Excelsior, MN 55331 • Phone 952.252.3000 . Fax 952.252.3001 www.uscompliance.com aceAnalytical wwwpacelabs.com September 18, 2014 Brandon Woodard Mission Foods 401 Gateway Drive Goldsboro, NC 27534 RE: Project: Stormwater 001 918 Pace Project No.: 92216614 Dear Brandon Woodard: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 09, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures ccT Myles Peterson, U.S. Compliance Corp Q pCCR& `� ;IN1. 3 {9eL7AAt0�-� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytica{ Services, Inc.. Page 1 of 12 Pace Analytical Services, Inc. aceAnalytical e 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pawlabs.com (704)875-9092 CERTIFICATIONS Project: Stormwater 001 918 Pace Project No.: 92216614 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Hunlersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40 FloddalNELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shad not be reproduced, except in full, without the written Consent of Pace Analytical Services, Inc.. Page 2 of 12 Pace Analytical Services, Inc. aceAnalylical a 9800 Kincey Ave. Suite 100 HuniersvitEe, NC 28078 wwwpacefabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: Stormwater 001 918 Pace Project No.: 92216614 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92216614001 001 EPA 1664B CLW 1 PASI-C SM 2540D JTJ 1 PASI-A EPA 9040 MAB 1 PASI-A SM 5220D SMW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 Pace Analytical Services, Inc. aceAnalyrrcal 9800 KinceyAve. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Stormwater 001 918 Pace Project No.: 92216614 Sample: 001 LAID: 92216614001 Collected: 09/08/14 06:00 Received: 09/09/14 09:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua! HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 09/10/14 13:56 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg1L 4.2 1 09/15/14 15:08 9040 pH Analytical Method: EPA 9040 pH 5.1 Std. Units 0,10 1 09/10/14 14:46 H6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND mg1L 25.0 1 09/17/14 20:09 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 09/18/2014 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 acmnalytical www.pacelabs.com Project: Stormwater 001 918 Pace Project No.: 92216614 QC Batch: GCSV118838 QC Batch Method: EPA 1664B Associated Lab Samples: 92216614001 METHOD BLANK: 1282055 Associated Lab Samples: 92216614001 Parameter Units Oil and Grease mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 09/10/1413:49 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hun,ersviile, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1282056 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 37.2 93 78-114 MATRIX SPIKE SAMPLE: 1282057 92216640001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 40.6 97 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/1812014 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 aceAnalyrlcal www.pacelabs.cam QUALITY CONTROL DATA Pace Analytical Services, Inc. 98V Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater 001 918 Pace Project No.: 92216614 OC Batch: WET133170 Analysis Method: SM 2540D OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92216614001 METHOD BLANK: 1285390 Matrix: Water Associated Lab Samples: 92216614001 Blank Reporting Parameter units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 09/15/14 15:05 LABORATORY CONTROL SAMPLE: 1285391 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 256 102 90-110 SAMPLE DUPLICATE: 1285392 92216428005 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 11.4 12.4 8 SAMPLE DUPLICATE: 1285393 92216775001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 310 300 3 Results presented on this page are In the units Indicated by the "Units" column except where an atternato unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2014 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 • aceAnalytical _pacelabs.corn QUALITY CONTROL DATA Project: Stormwater 001 918 Pace Project No.: 92216614 QC Batch: WET133089 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92216614001 SAMPLE DUPLICATE: 1282092 Parameter Units PH Std. Units SAMPLE DUPLICATE: 1282093 Parameter Units PH Std. Units 92216576001 Dup Result Result 7.9 7.9 92216576002 Dup Result Result 7.9 8.0 RPD Qualifiers 0 H6 RPD Qualifiers 1 D6,H6 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Fluntersville, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/18/2014 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 aceAnalytical www.pacelabs.corrl Project: Stormwater 001 918 Pace Project No.: 92216614 QC Batch: WETA120277 QC Batch Method: SM 5220D Associated Lab Samples: 92216614001 METHOD BLANK: 1287176 Associated Lab Samples: 92216614001 Parameter Units Chemical Oxygen Demand mglL QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 09/17/14 20:09 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875.9092 LABORATORY CONTROL SAMPLE: 1287177 Spike LCS LCS % Rec Parameter Units Cone. Result % Roc Limits Qualifiers Chemical Oxygen Demand mglL 750 767 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1287178 1287179 MS MSD 92216169001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mglL 1670 1500 1500 2540 2540 58 58 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1287180 1287181 MS MSD 92216627001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mglL 674 750 750 1450 1460 103 105 90-110 1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09118/2014 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 aceAnalyfrcal wwwpacotabs.com QUALIFIERS Project: Stormwater 001 918 Pace Project No.: 92216614 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL-Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration, Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute, LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS 06 The relative percent difference (RPO) between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA recommended holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0911812014 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 i Pace Analytical Services, Inc. aceAnalytical® 9800 Kincey Ave. Suite 100 Fluntersvilte, NC 28078 www.pacafabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater 001 918 Pace Project No.: 92216614 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92216614001 001 EPA 1664B GCSVI18838 92216614001 001 SM 2540D WET133170 92216614001 001 EPA 9040 WET133089 92216614001 001 SM 5220D WETA/20277 Date: 09/18/2014 12:34 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO, NCG060000 TO DISCHARGE STORMWATER UNDER THE NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM for establishments primarily engaged in the following activities: Food and Kindred In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission and the Federal Water Pollution Control Act, as amended, this permit is hereby issued to all owners or operators, hereinafter permittees, which are covered by this permit as evidenced by receipt of a Certificate of Coverage by the Environmental Management Commission to allow the discharge of stormwater to the surface waters of North Carolina or to a separate storm sewer system conveying discharges to surface waters in accordance with the terms and conditions set forth herein. Coverage under this General Permit is applicable to: ♦ All owners or operators of stormwater point source discharges associated with activities classified as establishments primarily engaged in activities classified as: o Food and Kindred Products [standard industrial classification (SIC) 201, o Tobacco Products (SIC 21), o Soaps, Detergents and Cleaning Preparations; Perfumes, Cosmetics and Other Toilet Preparations (SIC 284), o Drugs (SIC 283), and o Public Warehousing and Storage (SIC 4221-4225), ♦ Stormwater point source discharges from like industrial activities deemed by The Division of Water Quality (DWQ) to be similar to these operations in the process, or the discharges, or the exposure of raw materials, intermediate products, by-products, products, or waste products. The General Permit shall become effective on December 1, 2012. The General Permit shall expire at midnight on October 31, 2017. Signed this day November 26, 2012. Original signed by Matt Matthews for Charles Wakild, P.E., Director Division of Water Quality By the Authority of the Environmental Management Commission t Permit No. NCG060000 TABLE OF CONTENTS PART I INTRODUCTION Section A: General Permit Coverage Section B: Permitted Activities PART II MONITORING, CONTROLS, AND LIMITATIONS FOR PERMITTED DISCHARGES Section A: Stormwater Pollution Prevention Plan Section B: Analytical Monitoring Requirements Section C: On -Site Vehicle and Equipment Maintenance Monitoring Requirements Section D: Qualitative Monitoring Requirements Section E: Assessment of Best Management Practices (BMPS) PART III STANDARD CONDITIONS FOR NPDES STORMWATER GENERAL PERMITS Section A: Compliance and Liability 1. Compliance Schedule 2. Duty to Comply 3. Duty to Mitigate 4. Civil and Criminal Liability S. Oil and Hazardous Substance Liability 6. Property Rights 7. Severability 8. Duty to Provide Information 9. Penalties for Tampering 10. Penalties for Falsification of Reports 11. Onshore or Offshore Construction 12. Duty to Reapply Section B: General Conditions 1. General Permit Expiration 2. Transfers 3. When an Individual Permit May be Required 4. When an Individual Permit May be Requested S. Signatory Requirements II Permit No. NCG060000 6. General Permit Modification, Revocation and Reissuance, or Termination 7. Certificate of Coverage Actions 8. Annual Administering and Compliance Monitoring Fee Requirements Section C: Operation and Maintenance of Pollution Controls 1. . Proper Operation and Maintenance 2. Need to Halt or Reduce not a Defense 3. Bypassing of Stormwater Control Facilities Section D: Monitoring and Records I. Representative Sampling 2. Recording Results 3. Flow Measurements 4. Test Procedures 5. Representative Outfall 6. Records Retention 7. Inspection and Entry Section E: Reporting Requirements 1. Discharge Monitoring Reports 2. Submitting Reports 3. Availability of Reports 4. Non-Stormwater Discharges 5. Planned Changes 6. Anticipated Noncompliance 7. Spills 8. Bypass R. Twenty-four Hour Reporting 10. Other Noncompliance 11. Other Information PART IV DEFINITIONS M Permit No, NCG060000 PART I - INTRODUCTION SECTION A: GENERAL PERMIT COVERAGE All persons desiring to have facilities covered by this General Permit must register with the Division of Water Quality (DWQ) by the filing of a Notice of Intent (NOI) and applicable fees. The NOI shall be submitted and a certificate of coverage issued prior to any point source discharge of stormwater associated with industrial activity to the surface waters of the state. Any owner or operator not wishing to be covered or limited by this General Permit may make application for an individual NPDES permit in accordance with NPDES procedures in 15A NCAC 2H .0100, stating the reasons supporting the request. Any application for an individual permit should be made at least 180 days prior to commencement of discharge. This General Permit does not cover activities or discharges covered by an individual NPDES permit until the individual permit has expired or has been revoked. Any person conducting an activity covered by an individual permit but which could be covered by this General Permit may request that the individual permit be revoked and coverage under this General Permit be provided. If industrial materials and activities are not exposed to precipitation or runoff as described in 40 CFR §122.26(g), the facility may qualify for a No Exposure Exclusion from NPDES stormwater discharge permit requirements. Any owner or operator wishing to obtain a No Exposure Exclusion must submit a No Exposure Certification Notice of Intent (1401) form to the Division; must receive approval by the Division; must maintain no exposure conditions unless authorized to discharge under a valid NPDES stormwater permit; and must recertify the No Exposure Exclusion annually. Any facility may apply for new or continued coverage under this permit until a Total Maximum Daily Load (TMDL) for pollutants for stormwater is established. A TMDL sets a pollutant -loading limit that affects a watershed, or portion of a watershed, draining to a specific impaired water. For discharges to watersheds affected by a TMDL, coverage under this permit may depend on the facility demonstrating it does not have reasonable potential to violate applicable water quality standards for those pollutants as a result of discharges. If DWQ determines that discharges have reasonable potential to cause water quality standard violations, the facility shall apply for an individual permit 180 days prior to the expiration date of this General Permit. Once that individual permit is effective, the facility will no longer have coverage under this General Permit. Note that the permittee must identify impaired waters (scheduled for TMDL development) and waters already subject to a TMDL in the Site Plan, as outlined in the Stormwater Pollution Prevention Plan, Part I1, Section A. During the period beginning on the effective date of the permit and lasting until expiration, the permittee is authorized to discharge stormwater associated with industrial activity. Such discharges shall be controlled, limited and monitored as specified in this permit. Part 1 Page 1 of 2 Permit No. NCG060000 SECTION B: PERMITTED ACTIVITIES Until coverage under this permit expires or is modified or revoked, the permittee is authorized to discharge stormwater to the surface waters of North Carolina, or to a separate storm sewer system, which has been adequately treated and managed in accordance with the terms and conditions of this General Permit. Any other point source discharge to surface waters of the state is prohibited unless it is an allowable non-stormwater discharge or is covered by another permit, authorization, or approval. The discharges allowed by this General Permit shall not cause or contribute to violations of Water Quality Standards. This permit does not relieve the permittee's responsibility for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, or decree. Part I Page 2 of 2 Permit No. NCG060000 PART 11— MONITORING, CONTROLS, AND LIMITATIONS FOR PERMITTED DISCHARGES SECTION A: STORMWATER POLLUTION PREVENTION PLAN The permittee shall develop and implement a Stormwater Pollution Prevention Plan (SPPP). The SPPP shall be maintained on site unless exempted from this requirement by the Division. The SPPP is public information in accordance with Part 111, Standard Conditions, Section E, paragraph 3 of this permit. The SPPP shall include, at a minimum, the following items: 1. Site Overview. The Site Overview shall provide a description of the physical facility and the potential pollutant sources that may be expected to contribute to contamination of stormwater discharges. The Site Overview shall contain the following: (a) A general location map (USGS quadrangle map or appropriately drafted equivalent map), showing the facility's location in relation to transportation routes and surface waters; the name of the receiving waters to which the stormwater outfalls discharge, or if the discharge is to a municipal separate storm sewer system, the name of the municipality and the ultimate receiving waters; and accurate latitude and longitude of the points of stormwater discharge associated with industrial activity. The general location map (or alternatively the site map) shall identify whether any receiving waters are impaired (on the state's 303(d) list of impaired waters) or if the site is located in a watershed for which a TMDL has been established, and what the parameters of concern are. (b) A narrative description of storage practices, loading and unloading activities, outdoor process areas, dust or particulate generating or control processes, and waste disposal practices. A narrative description of the potential pollutants that could be expected to be present in the stormwater discharge from each outfall. (c) A site map drawn at a scale sufficient to clearly depict: the site property boundary; the stormwater discharge outfalls; all on -site and adjacent surface waters and wetlands; industrial activity areas (including storage of materials, disposal areas, process areas, loading and unloading areas, and haul roads); site topography and finished grade; all drainage features and structures; drainage area boundaries and total contributing area for each outfall; direction of flow in each drainage area; industrial activities occurring in each drainage area; buildings; stormwater Best Management Practices (BMPs); and impervious surfaces. The site map must indicate the percentage of each drainage area that is impervious, and the site map must include a graphic scale indication and north arrow. (d) A list of significant spills or leaks of pollutants during the previous three (3) years and any corrective actions taken to mitigate spill impacts. (e) Certification that the stormwater outfalls have been evaluated for the presence of non- stormwater discharges. The permittee shall re -certify annually that the stormwater outfalls have been evaluated for the presence of non-stormwater discharges. The certification statement will be signed in accordance with the requirements found in Part I11, Standard Conditions, Section B, Paragraph 3. Part 11 Page 1 of 12 Permit No. NCG060000 2. Stormwater Management Strategy. The Stormwater Management Strategy shall contain a narrative description of the materials management practices employed which control or minimize the stormwater exposure of significant materials, including structural and nonstructural measures. The Stormwater Management Strategy, at a minimum, shall incorporate the following: (a) Feasibility Study,' A review of the technical and economic feasibility of changing the methods of operations and/or storage practices to eliminate or reduce exposure of materials and processes to rainfall and run-on flows. Wherever practical, the permittee shall prevent exposure of all storage areas, material handling operations, and manufacturing or fueling operations. In areas where elimination of exposure is not practical, this review shall document the feasibility of diverting the stormwater run-on. away from areas of potential- contamination. (b) Secondary Containment Requirements and Records. Secondary containment is required for: bulk storage of liquid materials including petroleum products; storage in any amount of Section 313 of Title III of the Superfund Amendments and Reauthorization Act (SARA) water priority chemicals: and storage in any amount of hazardous substancesin order to prevent leaks and spills from contaminating stormwater runoff. A table or summary of all such tanks and stored materials and their associated secondary containment areas shall be maintained. If the secondary containment devices are connected to stormwater conveyance systems, the connection shall be controlled by manually activated valves or other similar devices (which shall be secured closed with a locking mechanism). Any stormwater that accumulates in the containment area shall be at a minimum visually observed for color; foam, outfall staining, visible sheens and dry weather flow, prior to release of the accumulated stormwater. Accumulated stormwater shall be released if found to be uncontaminated by any material. Records documenting the individual making the observation, the description of the accumulated stormwater, and the date and time of the release shall be kept for a period of five (5) years. For facilities subject to a federal oil Spill Prevention, Control, and Countermeasure Plan (SPCC), any portion of the SPCC plan fully compliant with the requirements of this permit may be used to demonstrate compliance with this permit. (c) BMP Summary. A listing of site structural and non-structural Best Management Practices (BMPs) shall be provided. The installation and implementation of BMPs shall be based on the assessment of the potential for sources to contribute significant quantities of pollutants to stormwater discharges and on data collected through monitoring of stormwater discharges. The BMP Summary shall include a written record of the specific rationale for installation and implementation of the selected site BMPs. The BMP Summary shall be reviewed and updated annually. 3. Spill Prevention and Response Procedures. The Spill Prevention and Response Procedures (SPRP) shall incorporate an assessment of potential pollutant sources based on a materials inventory of the facility. Facility personnel responsible for implementing the SPRP shall be identified in a written list incorporated into the SPRP and signed and dated by each individual acknowledging their responsibilities for the plan. A responsible person shall be on -site at all times during facility operations that have the potential to contaminate stormwater runoff through spills or exposure of materials associated with the facility operations. The SPRP must be site stormwater specific. Therefore, an oil -Spill Prevention Control and Countermeasure plan (SPCC) may be a component of the SPRP, but may not be sufficient to completely address the stormwater aspects of the SPRP. The common elements of the SPCC with the SPRP may be incorporated by reference into the SPRP. Part II Page 2 of 12 Permit No. NCG060000 4. Preventative Maintenance and Good Housekeeping Program. A preventative maintenance and good housekeeping program shall be developed and implemented. The program shall address all stormwater control systems (if applicable), stormwater discharge outfalls, all on -site and adjacent surface waters and wetlands, industrial activity areas (including material storage areas, material handling areas, disposal areas, process areas, loading and unloading areas, and haul roads), all drainage features and structures, and existing structural BMPs. The program shall establish schedules of inspections, maintenance, and housekeeping activities of stormwater control systems, as well as facility equipment, facility areas, and facility systems that present a potential for stormwater exposure or stormwater pollution where not already addressed under another element of the SPPP. Inspection of material handling areas and regular cleaning schedules of these areas shall be incorporated into the program. Timely compliance with the established schedules for inspections, maintenance, and housekeeping shall be recorded and maintained in the SPPP. 5. Facility Inspections. Inspections of the facility and all stormwater systems shall occur as part of the Preventative Maintenance and Goad Housekeeping Program at a minimum on a semi- annual schedule, once during the first half of the year (January to June), and once during the second half (July to December), with at least 60 days separating inspection dates (unless performed more frequently than semi-annually). These facility inspections are different from, and in addition to, the stormwater discharge characteristic monitoring at the outfalls required in Part II B, C, and D of this permit. 6. Employee Training. Training programs shall be developed and training provided at a minimum on an annual basis for facility personnel with responsibilities for: spill response and cleanup, preventative maintenance activities, and for any of the facility's operations that have the potential to contaminate stormwater runoff. The facility personnel responsible for implementing the training shall be identified, and their annual training shall be documented by the signature of each employee trained. 7. Responsible Party. The SPPP shall identify a specific position or positions responsible for the overall coordination, development, implementation, and revision of the SPPP. Responsibilities for all components of the SPPP shall be documented and position assignments provided. 8. SPPP Amendment and Annual Update. The permittee shall amend the SPPP whenever there is a change in design, construction, operation, site drainage, maintenance, or configuration of the physical features which may have a significant effect on the potential for the discharge of pollutants to surface waters. All aspects of the SPPP shall be reviewed and updated on an annual basis. The annual update shall include: (a) an updated list of significant spills or leaks of pollutants for the previous three (3) years, or the notation that no spills have occurred (element of the Site Overview); (b) a written re -certification that the stormwater outfalls have been evaluated for the presence of non-stormwater discharges (element of the Site Overview); (c) a documented re-evaluation of the effectiveness of the on -site stormwater BMPs (BMPSummary element of the Stormwater Management Strategy). (d) ' a review and comparison of sample analytical data to benchmark values (if applicable) over the past year, including a discussion about Tiered Response status, The permittee shall use the Division's Annual Summary Data Monitoring Report (DMR) form, available from the Stormwater Permitting Unit's website (See 'Monitoring Forms' here: http: /112ortal.ncdenr.orjzlweblwq/ws./su/npdessw.). Part 11 Page.3 of 12 Permit No. NCG060000 The Director may notify the permittee when the SPPP does not meet one or more of the minimum requirements of the permit. Within 30 days of such notice, the permittee shall submit a time schedule to the Director for modifying the SPPP to meet minimum requirements. The permittee shall provide certification in writing (in accordance with Part III, Standard Conditions, Section B, Paragraph 3) to the Director that the changes have been made. SPPP Implementation. The permittee shall implement the Stormwater Pollution Prevention Plan and all appropriate BMPs to prevent contaminants from entering surface waters via Stormwater. Implementation of the SPPP shall include documentation of all monitoring, measurements, inspections, maintenance activities, and training provided to employees, including the log of the sampling data and of actions taken to implement BMPs associated with the industrial activities, including vehicle maintenance activities. Such documentation shall be kept on -site for a period of five (S) years and made available to the Director or the Director's authorized representative immediately upon request. Part 11 Page 4 of 12 Permit No. NCG060000 SECTION B: ANALYTICAL MONITORING REQUIREMENTS Analytical monitoring of stormwater discharges shall be performed as specified in Table 1. All analytical monitoring shall be performed during a measureable storm event at each stormwater discharge outfall (SDO). Only SDOs discharging stormwater associated with industrial activity must be sampled (See Definitions). ,A measurable storm event is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. (See Definitions.? Table 1. Analytical Monitoring Requirements Discharge Characteristics Units Measurement Fre uenc 1 Sample TypeZ Sample Location3 H standard semi-annual Grab SDO Total Suspended Solids m L semi-annual Grab SDO Oil & Grease m L semi-annual Grab SDO Fecal Coliform4 per 100 ml of freshwater semi-annual Grab SDO Enterococci 4 per 100 ml of saltwater semi-annual Grab SDO Chemical Oxygen Demand m L semi-annual Grab SDO Total Rainfalls inches semi-annual Rain Gauge - Footnotes: 1 Measurement Frequency: Twice per year during a measureable storm event 2 Grab samples shall be collected within the first 30 minutes of discharge. 3 Sample Location: Samples shall be collected at each stormwater discharge outfall (00) unless representative outfall status (ROS) has been granted. A copy of the letter granting ROS shall be kept on site. DWQ's ROS letter remains in effect through subsequent reissuance of this permit and as long as the pertinent site conditions and operations remain unchanged, unless the ROS letter provides for other conditions or duration. 4 'Fecal colifor,n sampling applicable only to facilities discharging to fresinvaters ihat process meats. Enterococci sampling applicable only to facilities discharging to saltwaters that p" r e s meats. 5 For each sampled measureable storm event, the total precipitation must be recorded. An on -site rain gauge or local rain gauge reading must be recorded. Where isolated sites are unmanned for extended periods of time, a local rain gauge reading may be substituted for an on -site reading. The permittee shall complete the analytical samplings in accordance with the schedule specified below in Table 2, unless adverse weather conditions prevent sample collection (see Adverse Weather in Definitions). A minimum of 60 days must separate Period 1 and Period 2 sample dates, unless monthly monitoring has been instituted as part of other requirements of this permit. Inability to sample because of adverse weather conditions must be documented in the SPPP and recorded on the DMR. The permittee must report the results from each sample taken within the Part 11 Page 5 of 12 Permit No. NCG060000 monitoring period (see Part III, Section E). Sampling-is_not;required:outside,of-the'.facilitys:normal Loperating t3ours3 Table 2. Monitoring Schedule Monitoring period1.2 Sample Number Start End Year 1- Period 1 1 tJanuary;1, 2013' June 30, 2013 Year 1- Period 2 2 July 1, 2013 December 31, 2013 Year 2 - Period 1 3 January 1, 2014 June 30, 2014 Year 2 - Period 2 4 July 1, 2014 December 31, 2014 Year 3 - Period 1 5 January 1, 2015 June 30, 2015 Year 3 - Period 2 6 July 1, 2015 December 31, 2015 Year 4 - Period 1 7 January 1, 2016 June 30, 2016 Year 4 -- Period 2 S July 1, 2016 December 31, 2016 Year 5 - Period 1 9 January 1, 2017 June 30, 2017 Year 5 - Period 2 10 Juty_1,201-7) October 31, 2017 Footnotes: 1 Maintain semi-annual analytical monitoring throughout the permit renewal process (unless other provisions of this permit prompt monthly sampling). 2 If.no discharge occurs duringthe;sampling:period?the:permittee'must-submit a'monitoring report indicating "No Flow" or "No Discharge" within-30 days ofthe end-ofthe sampling period. Failure to monitor semi-annually per permit terms may result in the Division requiring monthly monitoring for all parameters for a specified time period. "No discharge" from an outfall or inability to collect a sample because of adverse weather conditions during a monitoring period, for example, does not constitute failure to monitor, as long as it is properly reported. The permittee shall compare monitoring results to the benchmark values in Table 3. The:benchmark values :in-Taible.3-are-not permit-Iiinits`,but should-be-used-asguidelines for-ttie permittee's:Stormwater. P.olluti"on Prevention -Plan (SPPP)! Exceedances of benchmark values require the permittee to increase monitoring, increase management actions, increase record keeping, and/or install stormwater Best Management Practices (BM Ps) in a tiered program. See below the descriptions of Tier One, Tier Two, and Tier Three response actions below. In the event that the Division releases the permittee from continued monthly monitoring under Tier Three, DWQ's release letter remains in effect through subsequent reissuance of this permit, unless the release letter provides for other conditions or duration. Part 11 Page 6 of 12 Permit No. NCG060000 Table 3. Benchmark Values for Analvtical Monitorine Discharge Characteristics Benchmark Values pH1 6 - 9 standard unitsl Total Suspended Solids (TSS) 100 mg/L TSS (ORW, HWQ Trout & PNA waters) 50 mg/L Oil & Grease 30 mg/L Fecal Coliform 1,000 per 100 ml Enterococci 500 per 100 ml Chemical Oxygen Demand 120 mg/L Footnotes: 1 9fpH751ues outside'this:range are recorded'in`sampled.stormwater-'discharges, but ambient, precipitatiompMevels are: lower,%then•.the:tower_thr.esifold�6f.this'•benchmark•ringe is tlie.pHtof--A the precipitation (within instrument accuracy) instead of 6 S.U. Readings from an on=site or-local'.rain gauge (or-'local:precipitation data) rriusfbe:documented•to demonstrate.background•concentration!i�were, ,,below.ttie'benctimarlc pH: a-nge of 6-9.iA Part 11 Page 7 of 12 Permit No. NCG060000 Tier One If: The first valid sampling results are above a benchmark value, or outside of the benchmark range, for any at anv outfall; Then: The permittee shall: 1. Conduct a stormwater management inspection of the facility within two weeks of receiving sampling results. 2. Identify and evaluate possible causes of the benchmark value exceedance. 3. Identify potential and select the specific: source controls, operational controls, or physical improvements to reduce concentrations of the parameters of concern, and/or to bring concentrations within the benchmark range. 4. Implement the selected actions within two months of the inspection. S. Record each instance of a Tier One response in the SPPP, include the date and value of the benchmark exceedence, the inspection date, the personnel conducting the inspection, the selected actions, and the date the selected actions were implemented. Tier Two If: During the term of this permit, the first valid sampling results from two consecutive monitoring periods are above the benchmark values, or outside of the benchmark range, for any specific parameter at a specific discharge o Then: The permittee shall: 1. Repeat all the required actions outlined above in Tier One. 2. Immediately institute monthly monitoring for all parameters. The permittee shall conduct monthly monitoring at every outfall where a sampling result exceeded the benchmark value for two consecutive Y samples. Monthly (analytical and qualitative) monitoring shall continue until three consecutive sample results are below the benchmark values or within benchmark range. 3. If no discharge occurs during the sampling period, the permittee is required to submit a monthly monitoring report indicating "No Flow" to comply with reporting requirements. 4. Benchmark exceedances for a different parameter separately trigger a tiered response. S. Maintain a record of the Tier Two response in the SPPP. Tier Three. During the term of this permit, if the valid sampling results required for the permit monitoring periods exceed the benchmark value, or are outside the benchmark range, for any specific parameter at anytspecific outfaINn'four_occasions, the permittee sWI7nbtify.the.DWQ.Regiona1 Office Supervisor.in_writing within 3904ys_of receipt of;the:fourtti 5nalytical'results.1 DWQ may but is not limited to: • require that the permittee revise, increase, or decrease monitoring frequency for some or all parameters; • rescind coverage under the General Permit, and require that the permittee apply for an individual stormwater discharge permit; • require the permittee to install structural stormwater controls; • require the permittee to implement other stormwater control measures; • require the permittee to perform -upstream -and downstream monitoring to characterize impacts ons receiving waters; br • require the permittee implement site modifications to qualify for a No Exposure Exclusion. Part 11 Page 8 of 12 Permit No. NCG060000 SECTION C: STORMWATER DISCHARGES: ON -SITE VEHICLE AND EQUIPMENT MAINTENANCE MONITORING REQUIREMENTS Facilities that have any vehicle maintenance activity occurring on -site which uses more than SS gallons of new motor oil and/or hydraulic oil per month when averaged over the calendar year shall perform analytical monitoring as specified below in Table 4. All analytical monitoring shall be performed during a measureable storm event at all stormwater discharge outfalls (SDOs) that discharge stormwater runoff from vehicle maintenance areas, and in accordance with the schedule presented in Table 2 (Section B). Sampiingis not required outside of the facility's normah operating hours. Table 4. Analytical Monitoring Requirements for On -Site Vehicle Maintenance Discharge Characteristics Units Measurement Fre uenc 1 Sample ___Type2 Sample Location3 H standard semi-annual Grab SDO Non -Polar Oil & Grease / TPH EPA Method 1664 SGT-HEM mg/L semi-annual Grab SDO Total Suspended Solids m L semi-annual Grab SDO Total Rainfal14 inches semi-annual Rain gauge - New Motor Oil Usage gallons/month semi-annual Estimate - Footnotes: 1 Measurement Frequency: Twice per year, during;a'tn easureable:storm:event,, until either another permit is issued for this facility or until this permit is revoked or rescinded. See Table 2 for schedule of monitoring periods through the end of this permitting cycle. 2 Grab samples'sha]the-collected'.within'.the:first'30:minutes:of discharge.3 3 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) that discharges stormwater runoff from area(s) where vehicle maintenance activities occur. 4 For each sampled measureable storm event the total precipitation must be recorded. An on -site or local rain gauge reading must be recorded. Where isolated sites are unmanned for extended periods of time, a local rain gauge reading may be substituted for an on -site reading. Failure to monitor semi-annually per permit terms may result in the Division requiring monthly monitoring for all parameters for a specified time period, as provided in Part 11 Section B. Monitoring results shall be compared to the benchmark values in Table S. The benchmark values in Table 5 are not permit limits but should be used as guidelines for the permittee's Stormwater Pollution Prevention Plan (SPPP). Exceedances of benchmark values require the permittee to increase monitoring, increase management actions, increase record keeping, and/or install stormwater Best Management Practices (BMPs), as provided in Part 11 Section B. In the event that the Division releases the permittee from continued monthly monitoring under Tier Three, DWQ's release letter remains in effect through subsequent reissuance of this permit, unless the release letter provides for other conditions or duration. Part II Page 9 of 12 Permit No. NCG060000 Table S. Benchmark Values for On -Site Vehicle and Equipment Maintenance Activities Discharge Characteristics Benchmark Values H 6 — 9 standard units Non -Polar Oil & Grease / TPH EPA Method 1664 SGT-HEM 1S mg/L Total suspended solids 100 m L TSS ORW, H W, Trout & PNA waters 50 m L v-5tAa1 SECTION D: STORMWATER DISCHARGES: QUALITATIVE MONITORING REQUIREMENTS The purpose of qualitative monitoring is to evaluate the effectiveness of the Stormwater Pollution Prevention Plan (SPPP) and assess new sources of stormwater pollution. Qualitative monitoring of stormwater outfalls must be performed during a measurable storm event. Qualitative monitoring requires a visual inspection of each stormwater outfall regardless of representative outfall status. Qualitative monitoring shall be performed semi-annually as specified in Table 6, and during required analytical monitoring events (unless the permittee is required to perform further qualitative sampling per the Qualitative Monitoring Response, below). Inability to sample because of adverse weather conditions must be documented in the SPPP and recorded on the DMR (see Adverse Weather in Definitions). Only SDOs discharging stormwater associated with industrial activity must be monitored (See Definitions). In the event an atypical condition is noted at a stormwater discharge outfall, the permittee shall document the suspected cause of the condition and any actions taken in response to the discovery. This documentation will be maintained with the SPPP. Part 11 Page 10 of 12 Permit No. NCG060000 Table 6. Qualitative Monitoring Requirements Discharge Characteristics Frequencyl Monitoring Location2 Color semi-annual SDO Odor semi-annual SDO Clarity semi-annual SOO Floating Solids semi-annual SDO Suspended Solids semi-annual SDO Foam semi-annual SDO Oil Sheen semi-annual SDO Erosion or deposition at the outfall semi-annual SDO Other obvious indicators of stormwater pollution semi-annual SDO Footnotes: 1 Measurement Frequency: Twice per year during a measureable storm event. See Table 2 for schedule of monitoring periods through the end of this permitting cycle. The permittee must continue qualitative monitoring throughout the permit renewal process. 2 Monitoring Location: Qualitative monitoring shall be performed at each stormwater discharge outfall (SDO) regardless of representative outfall status. A minimum of 60 days must separate monitoring dates, unless additional sampling has been instituted as part of other analytical monitoring requirements in this permit. If the permittee's qualitative monitoring indicates that existing stormwater BMPs are ineffective, or that significant stormwater contamination is present, the permittee shall investigate potential causes, evaluate the feasibility of corrective actions, and implement those corrective actions within 60 days, per the Qualitative Monitoring Response, below. A written record of the permittee's investigation, evaluation, and response actions shall be kept in the Stormwater Pollution Prevention Plan. itative Mon Qualitative monitoring is for the purposes of evaluating SPPP effectiveness, assessing new sources of stormwater pollution, and prompting the permittee's response to pollution. if the permittee repeatedly fails to respond effectively to correct problems identified by qualitative monitoring, or if the discharge causes or contributes to a water quality standard violation, DWQ may but is not limited to: • require that the permittee revise, increase, or decrease monitoring frequency for some or all parameters (analytical or qualitative); • require the permittee to install structural stormwater controls; • require the permittee to implement other stormwater control measures; • require the permittee to perform upstream and downstream monitoring to characterize impacts on receiving waters; or • require the permittee implement site modifications to qualify for a No Exposure Exclusion. Part If Page 11 of 12 Permit No. NCG060000 SECTION E: ASSESSMENT -OF BEST MANAGEMENT PRACTICES (BMPS) Forfacilities that use or process anima! fats/ byproducts: Within twelve (12) months of the issuance of coverage under this General Permit, the permittee shall complete an assessment of best management practices associated with off loading, handling and spill prevention of rendered fats and oils that are stored and used at the facility. Following the completion of this assessment, the permittee shall submit a report of findings and proposed corrective measures to be taken to both the local DWQ Regional Office and Stormwater Permitting Unit. DWQ will review the report, and either approve the proposed corrective action measures plan, direct changes be made to it, or possibly require further assessment of best management practices. Failure,to,submit this -repo Mis, a".violationof•permit conditions: The assessment report shall include, but not be limited to, the following: 1. A narrative description of all the material handling activities (not just fats and oils handling) that are outside, or that otherwise expose materials to incidental rainfall or run-on. 2. A feasibility evaluation as to whether reduced exposure can be achieved at the site, and rank the potential management measures as to feasibility. Emphasize the evaluation of on -site conditions with respect to incidental, accidental, fugitive materials, and spills, whether solid or liquid. 3. �An evaluation of the presence, and volume of, or absence of animals/wildlife on -site and whether fecal coliform concentrations might be correlated to the presence or absence of those animals/wildlife. 4. A proposed corrective action measures -plan with milestones and proposed schedule for implementation. Part 11 Page 12 of 12 Permit No. NCG060000 PART III STANDARD CONDITIONS FOR NPDES STORMWATER GENERAL PERMITS SECTION A: COMPLIANCE AND LIABILITY 1. Compliance Schedule The permittee shall comply with Limitations and Controls specified for stormwater discharges in accordance with the following schedule: Existing Facilities already operating but applying for permit coverage for the first time: The Stormwater Pollution Prevention Plan shall be developed and implemented within 12 months of the effective date of the Certificate of Coverage and updated thereafter on an annual basis. Secondary containment, as specified in Part 11, Section A, Paragraph 2(b) of this general permit, shall be accomplished within 12 months of the effective date of the issuance of the Certificate of Coverage. New Facilities applying for coverage for the first time: The Stormwater Pollution Prevention Plan shall be developed and implemented prior to the beginning of discharges from the operation of the industrial activity and be updated thereafter on an annual basis. Secondary containment, as specified in Part II, Section A, Paragraph 2(b) of this general permit shall be accomplished prior to the beginning of discharges from the operation of the industrial activity. Existing facilities previously permitted and applying for renewal under this General Permit: All requirements, conditions, limitations, and controls contained in this permit (except new SPPP elements in this permit renewal) shall become effective immediately upon issuance of the Certificate of Coverage. New elements of the Stormwater Pollution Prevention Plan for this permit renewal shall be developed and implemented within 6 months of the effective date of this general permit and updated thereafter on an annual basis. Secondary containment, as specified in Part Ili, Paragraph 2(b) of this general permit shall be accomplished prior to the beginning of discharges from the operation of the industrial activity. 2. Duty to Comply The permittee must comply with all conditions of this general permit. Any permit noncompliance constitutes a violation of the Clean Water Act (CWA) and is grounds for enforcement action; for permit termination, revocation and reissuance, or modification; or denial of a permit upon renewal application [40 CFR 122.411. a. The permittee shall comply with standards or prohibitions established under section 307(a) of the CWA for toxic pollutants within the time provided in the regulations that establish these standards or prohibitions, even if the general permit has not yet been modified to incorporate the requirement. b. The CWA provides that any person who violates section[s] 301, 302, 306, 307, 308, 318 or 405 of the Act, or any permit condition or limitation implementing any such sections in a permit issued under section 402, or any requirement imposed in a pretreatment program approved under sections 402(a)(3) or 402 (b)(8) of the Act, is subject to a civil penalty not to exceed $37,500 per day for each violation. [33 USC 1314(d) and 40 CFR 122.41(a)(2)] c. The CWA provides that any person who negligently violates sections 301, 302, 306, 307, 308, 318, or 405 of the Act, or any condition or limitation implementing any of such sections in a permit issued under section 402 of the Act, or any requirement imposed in a pretreatment program approved under section 402(a)(3) or 402(b)(8) of the Act, is subject to criminal penalties of $2,500 to $25,000 per day of violation, or imprisonment of not more than 1 year, or both, In the case of a second or subsequent conviction for a negligent violation, a person shall be Part Ill Pagel of 10 Permit No. NCG060000 subject to criminal penalties of not more than $50,000 per day of violation, or by imprisonment of not more than 2 years, or both. [33 USC 1319(c)(1) and 40 CFR 122.41(a)(2)] d. Any person who knowingly violates such sections, or such conditions or limitations is subject to criminal penalties of $5,000 to $50,000 per day of violation, or imprisonment for not more than 3 years, or both. In the case of a second or subsequent conviction for a knowing violation, a person shall be subject to criminal penalties of not more than $100,000 per day of violation, or imprisonment of not more than 6 years, or both. [33 USC 1319(c)(2) and 40 CFR 122.41(a)(2)] e. Any person who knowingly violates section 301, 302, 303, 306, 307, 308, 318 or 405 of the Act, or any permit condition or limitation implementing any of such sections in a permit issued under section 402 of the Act, and who knows at that time that he thereby places another person in imminent danger of death or serious bodily injury, shall, upon conviction, be subject to a fine of not more than $250,000 or imprisonment of not more than 15 years, or both. In the case of a second or subsequent conviction for a knowing endangerment violation, a person shall be subject to a fine of not more than $500,000 or by imprisonment of not more than 30 years, or both. An organization, as defined in section 309(c)(3)(B)(iii) of the CWA, shall, upon conviction of violating the imminent danger provision, be subject to a fine of not more than $1,000,000 and can be fined up to $2,000,000 for second or subsequent convictions. [40 CFR 122.41(a)(2)] f. Under state law, a civil penalty of not more than $25,000 per violation may be assessed against any person who violates or fails to act in accordance with the terms, conditions, or requirements of a permit. [North Carolina General Statutes § 143-215.6A] g. Any person may be assessed an administrative penalty by the Administrator for violating section 301, 302, 306, 307, 308, 318 or 405 of this Act, or any permit condition or limitation implementing any of such sections in a permit issued under section 402 of this Act. Administrative penalties for Class I violations are not to exceed $16,000 per violation, with the maximum amount of any Class I penalty assessed not to exceed $37,500. Penalties for Class 11 violations are not to exceed $16,000 per day for each day during which the violation continues, with the maximum amount of any Class Il penalty not to exceed $177,500. [33 USC 1319(g)(2) and 40 CFR 122.41(a)(3)] 4.Du1y toMti ate Th permittee shall`take'al]`reas6nable steps.to minimize:or_prevenhany--discharge-in:violation,of thisi tgeneral;permit}which has a reasonable likelihood of adversely affecting human health or the environment [40 CFR 122.41(d)]. 4. Civil and Criminal Liability Except as provided in Part 111, Section C of this general permit regarding bypassing of stormwater control facilities, nothing in this permit shall be construed to relieve the permittee from any responsibilities, liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3,143-215.6, or Section 309 of the Federal Act, 33 USC 1319, Furthermore, the permittee is responsible for consequential damages, such as Fish kills, even though the responsibility for effective compliance may be temporarily suspended. S. Oil and Hazardous Substal3ce Liability_ Nothing inthis:generaLpermit shall :be•con struedlo:preclude the institution:of.anyaegal:action.or; relieve thepermittee:from any: responsibilities, liabilities•orlpenaltiesvo.which;the:permittee is or maybe subject:to,under:NCGS-143-215:75 et seq. or, Section 311.of.the.Federal•Act, 33_USC,1321. 6. Property Rights The issuance of this general permit does not convey any property rights in either real or personal property, or any exclusive privileges, nor does it authorize any injury to private property or any Part III Page 2 of 10 Permit No. NCG060000 invasion of personal rights, nor any infringement of Federal, State or local laws or regulations [40 CFR 122.41(g)]. Severability The provisions of this general permit are severable, and if any provision of this general permit, or the application of any provision of this general permit to any circumstances, is held invalid, the application of such provision to other circumstances, and the remainder of this general permit, shall not be affected thereby [NCGS 15013-23]. 8. Duty to Provide Information The .permittee sEilCfurni`sh to the Permit Issuing Authority, within a reasonable time, any, information -whic_h,the:Permit•]ssuing Autherity may request to -determine. —whether cause;exists=for modifying, revoking and reissuing, or terminating the general permit issued pursuant to thisigeneral pi rmit or to determine compliance with�this general permit:,Jhe permittee shall also furnish to the Permit Issuing Authority upon request, copies of records required to be kept by this general permit [40 CFR 122.41(h)]. Penaltigs for TaMpering The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders inaccurate, any monitoring device or method required to be maintained under this general permit shall, upon conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for not more than two years per violation, or by both. If a conviction of a person is for a violation committed after a first conviction of such person under this paragraph, punishment is a fine of not more than $20,000 per day of violation, or by imprisonment of not more than 4 years, or both [40 CFR 122,411. 10. Penalties for Falsification of Reports The Clean Water Act provides that any person who knowingly makes any false statement, representation, or certification in any record or other document submitted or required to be maintained under this general permit, including monitoring reports or reports of compliance or noncompliance shall, upon conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for not more than two years per violation, or by both [40 CFR 122.41]. 11. Onsho[or Offsh Lg Construction This general permit does not authorize or approve the construction of any onshore or offshore physical structures or facilities or the undertaking of any work in any navigable waters. 12. {_Duty to Reapply. Dischargers covered by this general permit;need-nobsubmita new Notice of Intent (NO]) or renewal request unless so directed by the Division. If the Division chooses not to renew this general permit, the permittee will be notified to submit an application for an individual permit [15A NCAC 02H .0127(e)]. SECTION B: GENERAL CONDITIONS 1. General Permit Expiration General permits will be effective for a term not to exceed five years, at the end of which the Division may renew them after all public notice requirements have been satisfied. If a general permit is renewed, existing'permiftees:do not:need tosubinit a r`— ewal request -or pay a renewal fee unless directed by the Division. New applicants seeking coverage under a renewed general permit must submit a Notice of Intent to be covered and obtain a Certificate of Coverage under the renewed general permit [15A NCAC 02H .0127(e)]. Part III Page 3 of 10 Permit No. NCG060000 2. Tran(ers This general permit is not transferable to any person without prior written notice to and approval from the Director in accordance with 40 CFR 122.61_ The Director may condition approval in accordance with NCGS 143-215.1, in particular NCGS 143-215.1(b)(4)b.2., and may require modification or revocation and reissuance of the Certificate of Coverage, or a minor modification, to identify the new permittee and incorporate such other requirements as may be necessary under the CWA [40 CFR 122.41(I)(3), 122.611 or state statute. The.Permittee is required to notify the Division4n writing in the event the permitted facility.is sold or,closed.; 3. When an Individual Permit May be Required—, The Director may require any owner/operator authorized to discharge under a certificate of coverage issued pursuant to this general permit to apply for and obtain an individual permit or an alternative general permit. Any interested person may petition the Director to take action under this paragraph. Cases where an individual permit may be required include, but are not limited to, the following: a. The discharger -is a significant contributor of pollutants; b. Conditions at the permitted site change, altering the constituents and/or characteristics of the discharge such that the discharge no longer qualifies for a general permit; C. The discharge.violates the terms or conditions of this general permit; d. A change has occurred in the availability of demonstrated technology or practices for the control or abatement of pollutants applicable to the point source; e. Effluent limitations are promulgated for the point sources covered by this general permit; f. A water quality management plan containing requirements applicable to such point sources is approved after the issuance of this general permit; g. The Director determines at his or her own discretion that an individual permit is required. 4. When an Individual Permit May be Requested Any_permittee,operating under this general permit may request -to be excluded from the coverage of this general permit by,applying for -an individua! permit. When an individual permit is issued to an owner/operator the applicability of this general permit is automatically terminated on the effective date of the individual permit. 5. Signatory Requirements All applications, reports, or information submitted to the Permitting Issuing Authority shall be signed and certified [40 CFR 122.41(k)]. a. All Notices of Intent to be covered under this general permit shall be signed as follows: (1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a responsible corporate officer means: (a) a president, secretary, treasurer or vice president of the corporation in charge of a principal business function, or any other person who performs similar policy or decision making functions for the corporation, or (b) the manager of one or more manufacturing, production, or operating facilities, provided, the manager is authorized to make management decisions which govern the operation of the regulated facility including having the explicit or implicit duty of making major capital investment recommendations, and initiating and directing other comprehensive measures to assure long term environmental compliance with environmental laws and regulations; the manager can ensure that the necessary systems are established or actions taken to gather complete and accurate information for permit application requirements; and where authority to sign documents has been assigned or delegated to the manager in accordance with corporate procedures. Part III Page 4 of 10 Permit No. NCG060000 (2) For a partnership or sole proprietorship: by a general partner or the proprietor, respectively; or (3) For a municipality, State, Federal, or other public agency: by either a principal executive officer or ranking elected official [40 CFR 122.22]. b. All reports required by the general permit and other information requested by the Permit Issuing Authority shall be signed by a person described in paragraph a. above or by a duly authorized representative of that person. A person is a duly authorized representative only if: (1) The authorization is made in writing by a person described above; (2) The authorization specified either an individual or a position having responsibility for the overall operation of the regulated facility or activity, such as the position of plant manager, operator of a well or well field, superintendent, a position of equivalent responsibility, or an individual or position having overall responsibility for environmental matters for the company. (A duly authorized representative may thus be either a named individual or any individual occupying a named position.); and (3) The written authorization is submitted to the Permit Issuing Authority [40 CFR 122.22) c. Changes to authorization: If an authorization under paragraph (b) of this section is no longer accurate because a different individual or position has responsibility for the overall operation of the facility, a new authorization satisfying the requirements of paragraph (b) of this section must be submitted to the Director prior to or together with any reports, information, or applications to be signed by an authorized representative [40 CFR 122.221 d. Certification. Any person signing a document under paragraphs a. or b. of this section shall make the following certification [40 CFR 122.221. NO OTHER STATEMENTS OF CERTIFICATION WILL BE ACCEPTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properlygother and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible forgathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penaltiesfor submitting false information, including the possibility of fines and imprisonment for knowing violations." 6. General Permit Modification. Revocation and Beissuaallce., or Termination The issuance of this general permit does not prohibit the Permit Issuing Authority from reopening and modifying the general permit, revoking and reissuing the general permit, or terminating the general permit as allowed by the laws, rules, and regulations contained in Title 40, Code of Federal Regulations, Parts 122 and 123; Title 15A of the North Carolina Administrative Code, Subchapter 2H .0100; and North Carolina General Statute 143-215.1 et al. After public notice and opportunity for a hearing, the general permit may be terminated for cause. The filing of a request for a general permit modification, revocation and reissuance, or termination does not stay any general permit condition. The Certificate of Coverage shall expire when the general permit is terminated. 7. Certificate of Coverage Actions The general permit may be modified, revoked and reissued, or terminated for cause. The notification of planned changes or anticipated noncompliance does not stay any general permit condition [40 CFR 122.41(f)]. Part HI Page 5 of 10 Permit No. NCG060000 8. Annual Ad,Minister��nd Compliance Monitoring Fee Requirements The permittee must pay the administering and compliance monitoring fee within 30 (thirty) days after being billed by the Division. Failure to pay the fee in timely manner in accordance with 15A NCAC 2H .0105(b)(2) may cause this Division to initiate action to revoke coverage under the general permit. SECTION C: OPERATION AND MAINTENANCE OF POLLUTION CONTROLS 1. Proper Operation and Maintenance The-permittee shall at-all.times properly operate and maintain all facilities and systems of treatment and control (and -related appurtenances) which are installed or used by the permittee to achieve compliance with the conditions of this permit. Proper operation and maintenance also includes adequate laboratory controls and appropriate quality assurance procedures. This provision requires the operation of back-up or auxiliary facilities or similar systems which are installed by a permittee only -when the -operation is necessary to achieve compliance with the conditions of this permit [40 CFR 122.41(e)]. 2. Need to Halt or Reduce Not' a Defense it shall not be a defense for a permittee in an enforcement action that it would have been necessary to halt or reduce the permitted activity,in order to maintain compliance with the condition of this general permit [40 CFR 122.41(c)]. 3. Bypassing of Stormwater Control Facilities Bypass is prohibited and the Director may take enforcement action against a permittee for bypass unless: a. Bypass was unavoidable to prevent loss of life, personal injury or severe property damage; and b. There were no feasible alternatives to the bypass, such as the use of auxiliary control facilities, retention of stormwater or maintenance during normal periods of equipment downtime or dry weather. This condition is not satisfied if adequate backup controls should have been installed in the exercise of reasonable engineering judgment to prevent a bypass which occurred during normal periods of equipment downtime or preventive maintenance; and c. The permittee submitted notices as required under, Part III, Section E of this general permit. If the Director determines that it will meet the three conditions listed above, the Director may approve an anticipated bypass after considering its adverse effects. SECTION D: MONITORING AND RECORDS Representative Sampling Samples collected and measurements taken, as required herein, shall be characteristic of the volume and nature of the permitted discharge. Analytical sampling shall be performed during a measureable storm event. Samples shall betaken on a day and time that is characteristic of the discharge. All samples shall be taken before the discharge joins or is diluted by any other waste stream, body of water, or substance. Monitoring points as specified in this general permit shall not be changed without notification to and approval of the Permit Issuing Authority [40 CFR 122.41(j)]. 2. Recording Results For each measurement or sample taken pursuant to the requirements of this general permit, the permittee shall record the following information [40 CFR 122.411: a. The date, exact place, and time of sampling or measurements; Part III Page 6 of 10 Permit No. NCG060000 b. The individual(s) who performed the sampling or measurements; c. The date(s) analyses were performed; d. The individual(s) who performed the analyses; e. The analytical techniques or methods used; and f. The results of such analyses. 3. Flow Measurements Where required, appropriate Flow measurement devices and methods consistent with accepted scientific practices shall be selected and used to ensure the accuracy and reliability of measurements of the volume of monitored discharges. 4. Test Procedures Test procedures for the analysis of pollutants shall conform to the EMC regulations published pursuant to NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to regulations published pursuant to Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act, as Amended, and Regulation 40 CFR 136, To meet the intent of the monitoring required by this general permit, all test procedures must produce minimum detection and reporting levels and all data generated must be reported down to the minimum detection or lower reporting level of the procedure. If no approved methods are determined capable of achieving minimum detection and reporting levels below general permit discharge requirements, then the most sensitive (method with the lowest possible detection and reporting level) approved method must be used. S. Representative Outfall If a facility has multiple discharge locations with substantially identical stormwater discharges that are required to be sampled, the permittee may petition the Director for representative outfall status. If it is established that the stormwater discharges are substantially identical and the permittee is granted representative outfall status, then sampling requirements may be performed at a reduced number of outfalls. 6. Records Retention Qualitative monitoring shall be documented and records maintained at the facility along with the Stormwater Pollution Prevention Plan (SPPP). Copies of analytical monitoring results shall also be maintained on -site. The permittee shall retain records of all monitoring information, including o all calibration and maintenance records, o all original strip chart recordings for continuous monitoring instrumentation, o copies of all reports required by this general permit, o copies of all data used to complete the Notice of Intent to be covered by this general permit. These records or copies shall be maintained for a period of at least 5 years from the date of the sample, measurement, report or Notice of Intent application. This period may be extended by request of the Director at any time [40 CFR 122.41]. If this volume of records cannot be maintained on -site, the documents must be made available to an inspector upon request as immediately as possible. Inspection and Entry The permittee shall allow the Director, or an authorized representative (including an authorized contractor acting as a representative of the Director), or in the case of a facility which discharges through a municipal separate storm sewer system, an authorized representative of a municipal operator or the separate storm sewer system receiving the discharge, upon the presentation of credentials and other documents as may be required by law, to: Partill Page 7 of 10 Permit No. NCG060000 a. Enter upon the permittee's premises where a regulated facility or activity is located or conducted, or where records must be kept under the conditions of this general permit; b, Have access to and copy, at reasonable times, any records that must be kept under the conditions of this general permit; c. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment), practices, or operations regulated or required under this general permit; and d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as otherwise authorized by the Clean Water Act, any substances or parameters at any location [40 CFR 122.41(i)]. SECTION E: REPORTING REQUIREMENTS rG Discharge Monitoring Reportsl Samples analyzed in accordance with the terms of this general permit shall be submitted to the Division on Discharge Monitoring Report (DMR) forms provided by the Director. DMR forms are available on the Division's website(http://portal.ncdenr.orp-Zwcblwg/ws/su/npdeaswl. Submittals: shall be delivered to the Division no later than 30 days from the date the facility receives the sampling results from the laboratory. When no discharge has occurred from the facility during the report period; the permittee is required' to submit a discharge monitoring report„within 30 days of the end of the specified sampling period, giving all required information and indicating "NO FLOW" as per NCAC T1SA 0213.0506. If the permittee monitors any pollutant more frequently than required by this general permit using test procedures approved under 40 CFR Part 136 and at a sampling location specified in this general permit or other appropriate instrument governing the discharge, the results of such monitoring shall be included in the data submitted on the DMR. The permittee shall record the required qualitative monitoring observations on the SDO Qualitative Monitoring Report form provided by the Division and shall retain the completed forms on site. Qualitative monitoring results should'not be submitted to the Division, except upon DWQ's specific requirement to do so. Qualitative Monitoring Report forms are available at the website above. ReportsSubmitting a. Two signed copies of Discharge Monitoring Reports (DMRs) shall be submitted to: i Central Files Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 b. One copy of the Best Management Practices Assessment Report (refer to Part 11., Section E.) shall be submitted to each the local DWQ Regional Office (RO) and the Stormwater Permitting Unit (SPU). Addresses for each RO and the counties covered by each RO can be found here http://portal.ncdenr.org/weblwq/home%. The address for the SPU is shown below. The permittee shall retain a copy of the report on site. Stormwater Permitting Unit Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Part Ill Page 8 of 10 Permit No. NCG060000 Availability of Reports Except for data determined to be confidential under NCGS 143-215.3(a)(2) or Section 308 of the Federal Act, 33 USC 1318, all reports prepared in accordance with the terms shall be available for public inspection at the offices of the Division. As required by the Act, analytical data shall not be considered confidential. Knowingly making any false statement on any such report may result in the imposition of criminal penalties as provided for in NCGS 143-215.68 or in Section 309 of the Federal Act. 4, Non-Stormwater Discharges If the storm event monitored in accordance with this general permit coincides with a non- stormwater discharge, the permittee shall separately monitor all parameters as required under all other applicable discharge permits and provide this information with the stormwater discharge monitoring report. S. Planned Changes The permittee shall give notice to the Director as soon as possible of any planned changes at the permitted facility which could significantly alter the nature or quantity of pollutants discharged [40 CFR 122.41(1)]. This notification requirement includes pollutants which are not specifically listed in the general permit or subject to notification requirements under 40 CFR Part 122.42 (a). 6. Anticipated Noncompliance The permittee shall give advance notice to the Director of any planned changes at the permitted facility which may result in noncompliance with the general permit [40 CFR 122.41(1)(2)]. 7. Saills The permittee shall report to the local DWQ Regional Office, within 24 hours, all significant spills as defined in Part IV of this general permit. Additionally, the permittee shall report spills including: any oil spill of 25 gallons or more, any spill regardless of amount that causes a sheen on surface waters, any oil spill regardless of amount occurring within 100 feet'ofsurface waters, and any oil spill less than 25 gallons that cannot be cleaned up within 24 hours. 8. Bypass Notice [40 CFR 122.41(m)(3)]: a. Anticipated bypass. If the permittee knows in advance of the need for a bypass, it shall submit prior notice, if possible at least ten days before the date of the bypass; including an evaluation of the anticipated quality and affect of the bypass. b. Unanticipated bypass. The permittee shall submit notice within 24 hours of becoming aware of an unanticipated bypass. 9. lwenjy-fogr Hour Reporting a. The permittee shall report to the central office or the appropriate regional office any noncompliance which may endanger health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be provided within S days of the time the permittee becomes aware of the circumstances. The written submission shall contain a description of the noncompliance, and its causes; the period of noncompliance, including exact dates and times, and if the noncompliance has not been corrected, the anticipated time compliance is expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence of the noncompliance [40 CFR 122.41(1) (6)]. b. The Director may waive the written report on a case -by -case basis for reports under this section if the oral report has been received within 24 hours. Part III Page 9 of 10 Permit No. NCG060000 c. Occurrences outside normal business hours may also be reported to the Division's Emergency Response personnel at (800) 662-7956, (800) 858-0368 or (919) 733-3300. 10. Other Noncompliance The permittee shall report A instances of noncompliance not reported under 24 hour reporting at the time monitoring reports are submitted [40 CFR 122.41(1)(7)], 11. Other information Where the Permittee becomes aware that it failed to submit any relevant facts in a Notice of Intent to be covered under this general permit, or submitted incorrect information in that Notice of Intent application or in any report to the Director, it shall promptly submit such facts or information [40 CFR 122.41(1)(8)], Part III Page 10 of 10 PART IV DEFINITIONS Act See Clean Water Act. Permit No. NCG060000 2. Adverse Weather Adverse conditions are those that are dangerous or create inaccessibility for personnel, such as local flooding, high winds, or electrical storms, or situations that otherwise make sampling impractical. When adverse weather conditions prevent the collection of samples during the sample period, the permittee must take a substitute sample or perform a visual assessment during the next qualifying storm event. Documentation of an adverse event (with date, time and written narrative) and the rationale must be included with your SPPP records. Adverse weather does not exempt the permittee from having to file a monitoring report in accordance with the sampling schedule. Adverse events and failures to monitor must also be explained and reported on the relevant DMR. 3. Allowable Non-Stormwater Discharges This general permit regulates stormwater discharges. Non-stormwater discharges which shall be allowed in the stormwater conveyance system are: a. All other discharges that are authorized by a non-stormwater NPDES permit. b. Uncontaminated groundwater, foundation drains, air -conditioner condensate without added chemicals, springs, discharges of uncontaminated potable water, waterline and fire hydrant flushings, water from footing drains, irrigation waters, flows from riparian habitats and wetlands. c. Discharges resulting from Fire -fighting or fire -fighting training, or emergency shower or eye wash as a result of use in the event of an emergency. 4. Best Management Practices CBM .sj Measures or practices used to reduce the amount of pollution entering surface waters. BMPs may take the form of a process, activity, or physical structure. More information on BMPs can be found at: http-./Ictpub.epa.gov/npdes/stormwilter/menuotbmps/index,c 5. Bypass A bypass is the known diversion of stormwater from any portion of a stormwater control facility including the collection system, which is not a designed or established operating mode for the facility. 6. Bulk Storage of Liquid Products Liquid raw materials, manufactured products, waste materials or by-products with a single above ground storage container having a capacity of greater than 660 gallons or with multiple above ground storage containers located in close proximity to each other having a total combined storage capacity of greater than 1,320 gallons. 7. Certificate of Coverage The Certificate of Coverage (COC) is the cover sheet which accompanies a general permit upon issuance and lists the facility name, location, receiving stream, river basin, effective date of coverage under the general permit and is signed by the Director. 8. Clean Water Act The Federal Water Pollution Control Act, also known as the Clean Water Act (CWA), as amended, 33 USC 1251, et. seq. 9. Division or DWQ The Division of Water Quality, Department of Environment and Natural Resources. Part 1V Page 1 of 4 Permit No, NCG060000 10, Director The Director of the Division of Water Quality, the permit issuing authority. 11. EMC The North Carolina Environmental Management Commission. 12. Grab Sample An individual sample collected instantaneously. Grab samples that will be analyzed (quantitatively or qualitatively) must be taken within the first 30 minutes of discharge. 13. Hazardous Substance Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the Clean Water Act. 14. Landfill A disposal facility or part of a disposal facility where waste is placed in or on land and which is not a land treatment facility, a surface impoundment, an injection well, a hazardous waste long-term storage facility or a surface storage facility. 15. Measureable Storm Event A storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval may not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and obtains approval from the local DWQ Regional Office. Two copies of this information and a written request letter shall be sent to the local DWQ Regional Office. After authorization by the DWQ Regional Office, a written approval letter must be kept on site in the permittee's SPPP. 16. Municipal Separate Storm Sewer System [MS41 A stormwater collection system within an incorporated area of local self-government such as a city or town. 17. No Exposure A condition of no exposure means that all industrial materials and activities are protected by a storm resistant shelter or acceptable storage containers to prevent exposure to rain, snow, snowmelt, or runoff. Industrial materials or activities include, but are not limited to, material handling equipment or activities, industrial machinery, raw materials, intermediate products, by-products, final products, or waste products. DWQ may grant a No Exposure Exclusion from NPDES stormwater permitting requirements only if a facility complies with the terms and conditions described in 40 CFR §122.26(g). 18. Notice of Intent The state application form which, when submitted to the Division, officially indicates the facility's notice of intent to seek coverage under a general permit. 19. Permit Issuing Authority The Director of the Division of Water Quality (see "Director" above). 20. Permittee The owner or operator issued a Certificate of Coverage pursuant to this general permit. 21. Point Source Discharge of Stormwater Any discernible, confined and discrete conveyance including, but not specifically limited to, any pipe, ditch, channel, tunnel, conduit, well, or discrete fissure from which stormwater is or may be discharged to waters of the state. Part 1V Page 2 of 4 Permit No. NCG060000 22. Representative Outfall Status When it is established that the discharge of stormwater runoff from a single outfall is representative of the discharges at multiple outfalls, the DWQ may grant representative outfall status. Representative outfall status allows the permittee to perform analytical monitoring at a reduced number of outfalls. 23. Secondary Containment Spill containment for the contents of the single largest tank within the containment structure plus sufficient freeboard to allow for the 25-year, 24-hour storm event. 24. Section 313 Water Priority Chemical A chemical or chemical category which: b, Is listed in 40 CFR 372.65 pursuant to Section 313 of Title [I] of the Superfund Amendments and Reauthorization Act (SARA) of 1986, also titled the Emergency Planning and Community Right - to -Know Act of 1986; c. Is present at or above threshold levels at a facility subject to SARA title II1, Section 313 reporting requirements; and d. Meets at least one of the following criteria: i. Is listed in appendix D of 40 CFR part 122 on Table II (organic priority pollutants), Table III (certain metals, cyanides, and phenols) or Table IV (certain toxic pollutants and hazardous substances); ii. Is listed as a hazardous substance pursuant to section 311(b)(2)(A) of the CWA at 40 CFR 116.4; or iii. Is a pollutant for which EPA has published acute or chronic water quality criteria. 25. Severe Property„ Damage Substantial physical damage to property, damage to the control facilities which causes them to become inoperable, or substantial and permanent loss of natural resources which can reasonably be expected to occur in the absence of a bypass. Severe property damage does not mean economic loss caused by delays in production. 26. Significant Materials Includes, but is not limited to: raw materials; fuels; materials such as solvents, detergents, and plastic pellets; finished materials such as metallic products; raw materials used in food processing or production; hazardous substances designated under section 101(14) of CERCLA; any chemical the facility is required to report pursuant to section 313 of Title III of SARA; fertilizers; pesticides; and waste products such as ashes, slag and sludge that have the potential to be released with stormwater discharges. 27. Significant Spills Includes, but is not limited to: releases of oil or hazardous substances in excess of reportable quantities under section 311 of the Clean Water Act (Ref: 40 CFR 110.3and 40 CFR 117.3) or section 102 of CERCLA (Ref: 40 CFR 302.4). 28. StormwatenDischarge Out(a11_(SDO) The point of departure of stormwater from a discernible, confined, or discrete conveyance, including but not limited to, storm sewer pipes, drainage ditches, channels, spillways, or channelized collection areas, from which stormwater flows directly or indirectly into waters of the State of North Carolina, 29. Storallyater The flow of water which results from precipitation and which occurs immediately following rainfall or as a result of snowmelt. Part IV Page 3 of 4 Permit No. NCG060000 30. Stormwater Associated with Industrial Activity The discharge from any point source which is used for collecting and conveying Stormwater and which is directly related to manufacturing, processing or raw material storage areas at an industrial site. Facilities considered to be engaged in "industrial activities" include those activities defined in 40 CFR 122.26(b)(14), The term does not include discharges from facilities or activities excluded from the NPDES program. 31. Stormwater Pollution Prevention Plan (SPPP) A comprehensive site -specific plan which details measures and practices to reduce stormwater pollution and is based on an evaluation of the pollution potential of the site. 32. Total Maximum Daily Load (TMDL) TMDLs are written plans for attaining and maintaining water quality standards, in all seasons, for a specific water body and pollutant. A list of approved TMDLs for the state of North Carolina can be found at htt»;1,(portal.ncdenr.ore/web/wg/ns/mtu/tmdI 33. Toxic Pollutant Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act. 34. Vehicle MaintenancgAcl:iyitX Vehicle rehabilitation, mechanical repairs, painting, fueling, lubrication, vehicle cleaning operations, or airport deicing operations. 35. Visible Sedimentation Solid particulate matter, both mineral and organic, that has been or is being transported by water, air, gravity, or ice from its site of origin which can be seen with the unaided eye. 36. 25-year. 24 hour Storm Event The maximum 24-hour precipitation event expected to be equaled or exceeded, on the average, once in 25 years. Part IV Page 4 of 4 I) 0 aceAnalytical www.peoelebaaam January 08, 2015 Paul Gillard Mission Foods 401 Gateway Drive Goldsboro, NC 27534 RE: Project: Stormwater 12130 Pace Project No.: 92231250 Dear Paul Gillard: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 Enclosed are the analytical results for samples) received by the laboratory on December 30, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sam ple analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures cc: Myles Peterson, U.S. Compliance Corp REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. (704)875-9092 Page 1 of 12 aceAnalytical wn►w.pecelabsm n Project: Stormwater 12l30 Pace Project No.: 92231250 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #; 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification M E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS FioridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 10C Huntersville, NC 28078 (704)875-9092 Page 2 of 12 Pace Analytical Services, Inc. aceAmlXical a 9800 KinceyAve. Suite Huntersville, NC 28078078 wwwpacefabs com t704>875-9092 SAMPLE ANALYTE COUNT Project: Stormwater 12/30 Pace Project No.: 92231250 Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92231260001 001 EPA1664B CLW 1 PASI-C SM 2540D MDW 1 PASI-A EPA 9040 MAB 1 PASI-A SM 5220D JTJ 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 aceMalytical Huntersville, NC 28078 "wwPace'ab'wM (704)875-9092 ANALYTICAL RESULTS Project: Stormwater 12/30 Pace Project No.: 92231250 Sample: 001 Parameters Lab ID: 92231250001 Collected: 12/30/14 08:00 Results Units Report Limit DF Received: 12/30/14 10:20 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 12/30/14 15A0 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 34.9 mg/L 4.6 1 12/31114 10:29 9040 pH Analytical Method: EPA 9040 pH 5.4 Std. Units 0.10 1 12/31/14 12:50 H6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 60.0 mg1L 25.0 1 01/07/15 14:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/08/2015 03:34 PM without the written consent of Pace Analytical Services, Inc,. Page 4 of 12 aceAnalytical wwwpeoelabs.00m QUALITY CONTROL DATA Project: Stormwater 12130 Pace Project No.: 92231250 QC Batch: GCSW19955 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92231250001 METHOD BLANK: 1361536 Associated Lab Samples: 92231250001 Parameter Units Oil and Grease mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 12/30/14 15:38 Pace Analytical Services, Inc, 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1361537 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 37.3 93 78-114 MATRIX SPIKE SAMPLE: 1361538 92231292004 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 37.7 93 78-114 Results presented on this page am In the units Indicated by fie "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 01/08/2015 03:34 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 aceAnalytical wwwpecelaba.com Project: Stormwater 12I30 Pace Project No.: 92231250 QC Batch: WET135037 QC Batch Method: SM 2540D Associated Lab Samples: 92231250001 METHOD BLANK: 1361966 Associated Lab Samples: 92231250001 Parameter Units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: 1361967 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 1361968 Parameter Units Total Suspended Solids mgIL SAMPLE DUPLICATE: 1361969 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 12/31/14 10:24 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 236 94 90-110 92231388001 Dup Result Result RPD Qualifiers 117 133 13 D6 92231390001 Dup Result Result RPD Qualifiers 90.7 100 10 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /0812015 03:34 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aceAnalytical wwwpacelabacom Project: Stormwater 12130 Pace Project No.: 92231250 QC Batch: WETl35039 QC Batch Method: EPA 9040 Associated Lab Samples: 92231250001 SAMPLE DUPLICATE: 1361974 Parameter Units Std. Units pH SAMPLE DUPLICATE: 1361975 Parameter pH Units Std. Units QUALITY CONTROL DATA Analysis Method: EPA 9040 Analysis Description: 9040 pH 92231100003 Dup Result Result RPD 7.1 7.1 92231250001 Dup Result Result 5.4 5.0 Qualifiers 0 H6 RPD Qualifiers 7 H6 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvitte, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the "units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 01 /08/2015 03:34 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 e aceAnalytical www.pecefabu.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 HuAtersville, NC 28078 (704)875-9092 Project: Stormwater 12130 Pace Project No.: 92231250 QC Batch: WETA121506 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92231250001 METHOD BLANK: 1364916 Associated Lab Samples: 92231250001 Parameter Units Chemical Oxygen Demand mglL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 0110711514:00 LABORATORY CONTROL SAMPLE: 1364917 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 726 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1364918 1364919 MS MSD 92231013001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qua] Chemical Oxygen Demand mg1L 30.0 750 750 729 729 93 93 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1364920 1364921 MS MSD 92231423001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone, Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 36.0 750 750 753 753 96 96 90-110 0 Results presorted on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 01/0812015 03:34 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 axAmlyfical WW..pacWa6acam QUALIFIERS Project: Stormwater 12130 Pace Project No.: 92231250 DEFINITIONS Pace Analytical Services, Inc, 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 (704)8759092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroothylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute, LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA recommended holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /08/2015 03:34 PM without the written consent of Pace Analytical Services, Inc„ Page 9 of 12 le Analytrcal www.pacebbs com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater 12130 Pace Project No.: 92231250 Paco Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92231250001 001 EPA 1664B GCSVI19955 92231260001 001 SM 25401) WET135037 92231250001 001 EPA 9040 WET135039 92231250001 001 SM 52201) WETA121506 Date: 01/08/2015 03:34 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch Page 10 of 12 CHAIN -OF -CUSTODY/ Analytical Request Document N ZAnafylical- wwwThe Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. —celabs o m ' • •? • _ o Of �6 Section A . Section B Section G 'n Requlrvd CTeent Infametion: - . Ragrdred Project trdorrnabon: Imroite Information: `° SIGH !—UdfJs ReportTe t�� C�ic�r? z l*cA %�1A {;�-�f?a�c.z r� Copy To: LDS Ae77.=L50x? Co partyNa:rtie: ,T _SSZ, 1�CGLS REGULATORY AGENCY SQ�i CC.'fi�r 1Z7S_ +Y-' 7rlPri,�5-or.JC-V:5Cis34, I1A,fn .CC;,kl - - l_::�iii��:,V <'�'��; tz:. NPDES.. r, -,GROUNDWATER•_:—_ DRINKING WATER . '� UST = RCRA _ , i OTHER Entail 7a: :P.vec _G1cc}v��i�!/sSic�✓r" Oro- No.: Poarom Reterenoa: Y/Y. i 7,0- 79 : 7 -7St - L 3 i Name: Pacer r Site Location ; :G:_:. `- �- STATE: _ ; a . _ " .:., ... . Requested Due DatdTAT: f v Project Ntsmher: _ . , _ Pace Progb a:.. - .. ,Requested Analysis Filtered (YIN) - — - _' 'a``__• •_ Section Matrix Codes It.yvz,.dtneravt htoTltix r CODE - ' e �• COLLECTED Preservafiv i_ 'z- }, '• _ Drinking Water DW g VO Water WT $ Lj W to Water WW m C CO�OStiE N Z _ .. SoigSo6d SL- ; SAMPLE ID 00 Wipe , VP lAZ Air..- i AR LLJ 0- .w �. _ o- Q' , F jc- i . Sample IDs MUST BE UN16US ' Tssue TS O e• : m ++ -- Other _ OT_ -7- .�,. ._.J• •� � Jr, _ .F�. ra •_oArE' .'.OATE.. ,TIME TIME t -�. 2 = T Z Z I O �' W ,Pace Project NOJ Lab I.D. t. cot { 6, 25 �F.. 3 4 - - rt 6 7. 8 -777 zE 9 10. 1i 12 ADDITe"i:e6MMicNTi' REIHOUISHEDt3YlAFRuATION .DATE - TBIIE, +' A BY TION • - DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE _. i } ` c .. . PRINT Name of SAMPLER: A}i _�•I J L)60 / IZ elf J �• $ a SIGNATURE of sN pmL / i /, i' 1 / DATE Signed ZG ¢ `-4 U a a �� — rz- co Important Note: By slgmq 0us tam you are aCCaprbq Pace's NET 3D day P tears and agr--In q to taro charps of 1.5% per me nM for arty i woken na paid Mft 30 deye. F-ALL-"20tev.07. 1 S-May-2007 Document Name: Document Revised: September 22. IU114 27ceAnaVlml' Sample Condition Upon Receipt SCUR page 1 of 2 Document Number: Issuing Authority: F-CHR-CS-003-rev.16 Pace Huntersville Quality Office Client Name: Ass-ov, Courier: ad ElUPC]uSPS❑ Client❑Commercial❑ Pace Other a" Custody S on CcolerlBox Present: Elyes E9 no Seala inlact: ❑ ❑ no ea Y i Packing Material: ❑ 8ubble V❑p ❑ Bubble Bags (None ❑ Other ,I i Thermometer Used: IR Gun T1401 Type of Ice: eye . Blue None 9--wmpies on Ice, cooling process has begun iI Temp Correction Factor T1401 No Correction i Corrected Cooler Tom p•' � •C Temp should be above freezing to 6°C Biological Tissue Is Frozen: Yes No V v Comments: Date and fnilia contents: Chain of Custody Present: es ONO ❑NIA 1. Chain of Custody Filled Out: ea CINo ❑NrA 2, Chain of Custod Rglin uished: Dyes i<to ❑WA 3. Sampler Name & Signature on COC: es ON. ❑NIA 4. Samples Arrived within Hold Time: Tres ONO ❑NiA 5. Short Hold Time Anal sis <72hr : Oyes [Rif. ❑NIA 6. Rush Turn Around Time Requested: ❑Yes IMNo ❑NIA 7. Sufficient Volume: 8Ye8 ONO ONIA 8. Correct Containers Used: -Pace Containers Used: Eyes ❑No I6ONO ❑NIA ❑NIA g, Containers intact. 14yes ONO ❑NIA i0. Filtered volume received for Dissolved tests ❑Yea ONO E61A 11. Sample Labels match COC: -Includes date/timeAD/Anal sis Matrix: EIyes ONO ❑NIA 12. All containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. exceptions: VOA, coliloim, TOC, 080, Vu1.0110 vales) ONO Zy",No Ye ❑No ©NiA ❑NIA 13. Samples checked for dechlorination; Yea ONO ❑Ni 4, Heads ace in VOA Vials >8mm : ❑Yea ONO NI 15. Trip Blank Present; Trip Blank Custody Seals Present Pace Trip Blank Lot # if urchased ❑Yoa ONO Dyes ❑No NI NiA 8. Client Notification/ Resolution: Field Date Required? Y I N Person Contacted: Daterrlme: Comments/ Resolution: SCURF kevlew: Date: WOU92231250 SRF Review: Date: 3 r Note: Whenever there Is a discrepancy affecting North Caroli a compliance le t I samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office( 1.0 out of hold, Incorrect preservative, nut of Comp, i 92231250 Incorrect contalners) Page 12 of 12 Alj�A NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Charles Wakild, P. E. Governor Director December 4, 2012 Melissa Mendoza Gruma Corporation 1159 Cottonwood Ln Ste 200 Irving, TX 75038 Dee Freeman Secretary Subject: NPDES Stormwater Permit Coverage Renewal Mission Foods COC Number NCG060265 Wayne County Dear Permittee: In response to your renewal application for continued coverage under stormwater General Permit NCG060000 the Division of Water Quality (DWQ) is forwarding herewith the reissued General Permit. This permit is reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated October 15, 2007 (or as subsequently amended). The following information is included with your permit package: • A new Certificate of Coverage (COC) • A copy of General Permit NCG060000 • A copy of the Technical Bulletin for the General Permit • Two copies of the Discharge Monitoring Report (DMR) Form • Two copies of the Qualitative Monitoring Report Form The General Permit authorizes discharges of stormwater, and it specifies your obligations for discharge controls, management, monitoring, and record keeping. Please review the new permit to familiarize yourself with all the changes in the reissued permit. Your facility has six (6) months from the time of receipt of the permit to update your current SPPP to reflect all new permit requirements, The first sample period of your permit begins January 1, 2013. Your facility must sample a "measureable storm event" beginning during the periods beginning January 1 and July 1 of every year (or, if applicable, report "No Flow," as outlined in Part III, Section E). Also, please note that Tier 3 Actions in Part II of your permit are triggered by benchmark exceedances on four occasions beginning on the effective date of this permit and do not count prior exceedances. The more significant changes in the General Permit since your last COC was issued are noted either in the Draft Permit Fact Sheet that accompanied the public notice (http://pdrtai.ncdenr.org/web/wq/ws/su/current- notices), or in the Response to Comments / Summary of Changes and Technical Bulletin documents that are posted on the Stormwater Permitting Unit's website with the new General Permit. Please visit http:/Jportal.ncdenr.org/web/wq/ws/su/npdessw (Click on 'General Permits' tab) to review that information for your specific General Permit carefully. 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Location: 512 N. Salisbury St. Raleigh, North Caroi;na 27604 Phone:919-807-6300' FAX:919-807-6492 Internet: www.ncwatc, uaI!tv.orq o An Equal Opportunity k 0 .r._'rreAe!;Dn Employer Nne oahCarolina ,A7aturally Melissa Mendoza Deceml7Pr 4, 2012 Page 2 of 2 Some of the changes include: • Part II: • Section A: The Stormwater Pollution Prevention Plan (SPPP) section, if applicable, has been updated to the most current language of our permits. Additional conditions for specific industry sectors have been added to the SPPP requirements in some cases. • Sections B, C: Failure to perform analytical stormwater monitoring may result in the Division requiring that the permittee begin a monthly sampling scheme. • Sections B, C: A lower TSS benchmark of 50 mg/I for HQW, ORW, PNA and Tr Waters applies to these more sensitive waters. • Sections B, C: The monitoring parameter Oil & Grease (O&G) has been replaced by the parameter Total Petroleum Hydrocarbons (TPH) for vehicle maintenance areas, and in some cases, other analytical monitoring requirements. • Sections B, C, D: Inability to sample due to adverse weather must be recorded in the SPPP, or in separate on -site records if your General Permit does not require an SPPP. Adverse weather is defined in the "Definitions" section of the permit. • Sections B, C. The term "Representative Storm Event" has been replaced by "Measurable Storm Event." A measurable storm event is defined in the permit. • Section D: If the permittee fails to respond effectively to problems identified by qualitative monitoring, DWQ may require the permittee to perform corrective action. Please review Parts III and IV to understand the Standard Conditions of your new NPDES General Permit, including Compliance and Liability, Reporting, Monitoring and Records requirements; Operation and Maintenance obligations; and Definitions. Please note that all samples analyzed in accordance with the terms of this permit must be submitted to the Division on Discharge Monitoring Report (DMR) forms available on the Stormwater Permitting Unit's website above. DMR forms must be delivered to the Division no later than 30 days from the date the facility receives the sampling results from the laboratory. Also note that existing permittees do not need to submit a renewal request prior to expiration unless directed by the Division. Your coverage under the General Permit is transferable only through the specific action of DWQ. This permit does not affect the legal requirements to obtain other permits which may be required by DENR, nor does it relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit package, please contact the Division's Stormwater Permitting Unit at (919) 807-6300. Sincerely, �L f/+ ci��/�',� tom' G4 for Charles Wakild, P.E. cc: DWQ Central Files Stormwater Permitting Unit Files Washington Regional Office STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG060000 CERTIFICATE OF COVERAGE No. NCG060265 STORM WATER NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations, promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Gruma Corporation is hereby authorized to discharge stormwater from a facility located at: Mission Foods 401 Gateway Dr Goldsboro Wayne County to receiving waters designated as Stoney Creek, a class C;NSW waterbody in the Neuse River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, II, II1, and IV of General Permit No. NCG060000 as attached. This certificate of coverage shall become effective December 4, 2012. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this 41h day of December, 2012. for Charles Wakild, P.E., Director Division of Water Quality By Authority of the Environmental Management Commission -f WATF Michael F. Easley Governor ..,� 7 William G. Ross Jr., Secretary. -H Department of Environment and Natural Resources Q Alan W. Klimek, P.E., Director Division of Water Quality April 18, 2003 Mr. Gabriel Gutierrez, Plant Manager Mission Foods 1 159 Cottonwood Lane I rving,TX 75038 Subject: General Permit No. NCG060000 Mission Foods COC NCG060265 Wayne County Dear Mr. Gutierrez: In accordance with your application for discharge permit received on February 3, 2003, we are forwarding herewith the subject certificate of coverage to discharge under the subject state - NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated December 6, 1983_ If any parts, measurement frequencies or sampling requirements contained in this pen -nit are unacceptable to you, you have the right to request an individual permit by submitting an individual permit application. Unless such demand is made, this certificate of coverage shall be final and binding. .Please take notice that this certificate of coverage is not transferable except after notice to the Division of Water Quality. The Division of Water Quality may require modification or revocation and reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local governmental permit that may be required. If you have any questions concerning this permit, please contact Mack Wiggins at telephone number 919/733- 5083 ext. 542. Sincerely, -r: •i_.TI ,,,,,,,,,,,Ban W. Klimek, P.E. cc: Washington Regional Office Central Files Stormwater and General Permits Unit Files NC05N:C Customer Service 1 800 623-7748 Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 733-7015 AW STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG060000 CERTIFICATE OF COVERAGE No. NCG060265 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Gruma Corporation is hereby authorized to discharge stormwater from a facility located at Mission Foods 401 Gateway Drive east of Adamsville at Millers Crossing Wayne County to receiving waters designated as an unnamed tributary to Stoney Creek in the Neuse River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, 1I, I11, IV, V, and VI of General Permit No. NCG060000 as attached. This certificate of coverage shall become effective April 18, 2003 This Certificate of Coverage shall remain in effectTfor the duration of the General Permit. Signed this day April 18, 2003 for Alan W. Klimek, P.E., Director Division of Water Quality By Authority of the Environmental Management Commission �:a;',j Wayne -.N- r jr ! x3Y I f o 78 lAr,tOQ1'� JS511 37.5 -5111 \Trai r \f-� r• pineWOOdis �`�� �!• f' .�� '� * r,..-, /}� Fork ;+� '� '••�;' � �//'" _bi .r• . r�#;+•�, ✓'i"'r••��jII��I �."tr.."3 �� �f 3�I '� �"i � �..t�'. � ' �"� it „++°A"" �� „�,�.i�"� '�,_.��v�,,,�t_. y.. �P __�-�--'_ a 'ail New H, kg _ Ali F � \Y. '\ .G�� � �� ` a '� - a •'•• I\ • � :{_. • !'"�. , �C' i� i1 q '=�'= f:�f E r'�/��� 'tl .,,•-� lrjR �., ....;,":�•� #.; ! 1 a✓� .� •F irrtf+i'txx� • F��p� •} • �. • ( �� ��' �. jTye� �'I P ._�_: �` Jot J = Yt' aa_` .� °� ♦ a� L�j, j �! --�_•_ OCld emp s �s Park E.Ur ayne- ` ` rrr ` TrEr Jer ��HI . h • (Il yyT\. •' 16 C .,. »I e. (".�__`1.�-,� •/ - � Q R� Y } •4 0 �! 1 c < Wvv Q7U9 I _ Park e tt rli ,f r i ! r Pare »... $ i mllEr7i ' 1 li ail. SUbSta 5 %'r �' � .A 1�" t � `t i ✓ :PSI � '�.. JB's1�� � 3. � \ i� �k - " � �. L AshleyR;.�_a. \13rM• , s ' s . o' ,` �''. •'a •� I� �. Eit 70j �1i11 r,'��iscnawite Ac OQrtrt1 2••G t;'Br ' rs 4 t Peace 17/ _'.._� s}; ri`=—,r^_,.'r,�.......—t._ ��'• i�;-.1..'�}�r''"-.�..�U�� � �\./ f•T ' � � 35.'� ^I% •• • ���, Fir ^� I ,, � � � ..., n «• • Adaki 'file • � ' �' • i :'5; :• s'�->. • . .�! - �,.i:"1\ �. , .,j yr. `�, B 4;Z4 Substa xl • y . ,. ! • 3S5 ��. ���.,.� f ..� .. �....— Trailer,, Park ,�-^' �.:-._34 Adamavllk%'t' ✓ r :S ' • Ch jfill . ,riArkins0 �.,r � �....�.� 1� '1� • ••• �:� �uttoia • � /j""^-^-../.`�•�. /� • r , Chapel Tra0er e Park - Cem'• / 5 ilxE Ll Meis - • }1. �� � � •) 'r:: �1 : 'S. �s..,.�-"''�� `Radio ,'. * lii3� A "/ �Cerr3l- A �. Facility ti • j»' 91 W Copyright (C) 1997, Maptech, Inc "7% Markers Name: Discharge Site-NCG060265 Short Name: Dschrg Coordinates: 0350 22' 28.5" N, 0770 55' 31.5" W Comment: Mission Foods, Subbasin 030405, Neuse River Basin, Wayne County, unnamed tributary to Stoney Creek, Class C NSW, Quad F27SW