NCG060048_MONITORING INFO_20180821

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V ucc)�i O� 1
DOC TYPE
0 HISTORICAL FILE
A MONITORING REPORTS
DOC DATE
a o Y CA a I
YYYYMMDD

0
novo nordisk
August 13, 2018
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Per the requirements of Novo Nordisk Pharmaceutical Industries' stormwater discharge General Permit
NCG060000 and Certificate of Coverage No. NCG060048, attached are the results from the qualitative
monitoring and analysis carried out on July30, 2018.
I may be reached at 919-550-2200 at extension 2217 if you have questions.
Sincer
171�-
R. Paul Moms
Novo Nordisk Pharmaceutical Industries, Inc
3612 Powhatan Rd
Clayton, NC 27527
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BMAUNIMEM % hmpo m0d
NOVO NORDISK
ATTN: PAVL MORRIS
3612 POWHATAN RD.
CLAYTON ,NC 27527
PARAMETERS
PH (not to be used for reporting)
COD, mgll
Total Suspended Residue, mgll
TPH (1664B), mg/1
Stormwater
Analysis
Method
(#1, Grab)
©ate
Analyst
Cade
6.8
08/02/18
KDS
4500HB-11
23
09/03/18
SEJ
H8000-79
6.6
08/03/18
JMT
2540D-11
<5
09/03/19
SEJ
EPA1664B
HONE
ID#: 191
DATE COLLECTED: 07/30/18
DATE REPORTED : 08/06/18
REVIEWED BY:

Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.0,j9pox,705, 114 Oakmont Dr. Page 1 of
Greenville_ NC 27858
env iron ment 1 inc.com
DISINFECTION
Phone [phone] • Fax [phone]
CHLORINE
CHLORINE NEUTRALIZED AT COLLECTION
CLIENT: 191 Week: 33
UVle�,j
pH CHECK Nam) t �--.
NOVO NORDISK
NONE
Ij
p
p
p
G
CONTAINERTYPE,PIG
ATTN: PAUL MORRIS
CHEMICAL PRESERVATION
3612 POiV ATAN Rb.
CLAYTON NC 27527
A
C
A
C
A -NONE D•NAOH
G7
[phone]
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B - HNO, E - HCL
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C- H SO F- ZINC ACETATEINAOH
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SAMPLE LOCATION
DATE
TIME
° o
a
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a
Stormwater (#I, Grab)
� d
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as
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CLASSIFICATION:
❑ WASMWATER(NPOES)
DRMNGWATER
❑ DWOtGW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
OURIN MENTNEUVERY
Y N
SAMPLES COLLECTED BY.,
{pl me Plirrtj
SAMPLES RECEIVE IN LABAT °C
ED BY (SIG.) (SAMPLER)
DATEMME
BY (SIG.)
DATEMME
COMMENTS:
:
-
b�Ai�02I
(SHED BY
DATEMME
T— (�G
M. M
ISHED (SQ
DATEMME
RECEIVEd BY ( G.
DATEMME
PLEASE READ Instructions for completing this form on the reverse side.
FORM 45
Sampler must place a "C° for composite sample or a "G^ for N 0 338343
Grab sample in the blocks above for each parameter requested.
ATI,

March 14, 2018
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
REC--JEIVED
MAR 19 2018
CENTP,AL FILEs
OWR SECTION
0
novo nordisk
Per the requirements of Novo Nordisk Pharmaceutical Industries' stormwater discharge General Permit
NCG060000 and Certificate of Coverage No. NCG060048, attached are the results from the qualitative
monitoring and analysis carried out on March 05, 2018.
I may be reached at 919-550-2200 at extension 2217 if you have questions.
Sincerely,
R. Paul Morris
Novo Nordisk Pharmaceutical Industries, Inc
3612 Powhatan Rd
Clayton, NC 27527

Emw'ummumfiq Ala bw
NOVO NORDISK
ATTN: PAUL MORRIS
3 612 POWHATAN RD .
CLAYTON ,NC 27527
v0d
Stormwater
Analysis
Method
PARAMETERS
(#1, Grab)
Date Analyst
Code
PH (not to be used for reporting)
71
03/05/18
HMM
4500HB-11
COD, mg/1
24
03/09/18
SEJ
H8000-79
Total Suspended Residue, mg/l
7.1
03/06/18
AKS
254OD-11
TPH (1664B), mgll
<6
03/08/18
SEJ
EPA1664B
ID#: 191
DATE COLLECTED: 03/01/18
DATE REPORTED : 03/09/18
REVIEWED BY:
��

Environment 1, Inc.
P.O. Box 7095, 114 Oakmont Dr.
Greenville, NC 27858
env ironmerrrf'trtt T6Tn
Phone (M) 756-6208 • Fax [phone]
DISINFECTION
—M-,
CHAIN OF CUSTODY RECORD
L
Page I of 1
CHLORINE NEUTRALIZED AT COLLECTION
I.ri LVttIIVG
CLIENT:19, Week: 7
UV
pH CHECK (UU3)
P
P
P
G
CONTAINER TYPE, PIG
40VO NORDISK
❑ NONE
kTI'N: PAUI. MORRIS
CHEMICALPRESERVATION
1612 POWHATAN RD.
'-LAYTON NC 27527
A
C
A
C
r A -NONE D-NAOH
F
919) 550-22011
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COLLECTION
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SAMPLE LOCATION
DATE
TIME
o
Stormwater QI, Grab
$
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:::{
CLASSIFICATION:
WASTEWATER(NPDES)
DRINKING WATER
DWO'GW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING
rENT/DELIVERY
N
SAMPLES COLLECTED BY:
T7
A--J
I
SAMPLES RECEIVED IN LAB AT °C
RELINQ BY (SIG,) (SAMPLER)
DATEIIIME
BY
R4CErVM
TEIfIM
COMMENTS:
RELINQUISHED BY (SIG.)
DATEIIIME
BY (SIG.)
ATEM E
RELINQUISHED BY (SIG.)
DATI_111ME
RECEIVED BY (SIG.)
DATEMME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for NO 3 4 0 9 7 8
FORM #5 Grab sample in the blocks above for each parameter requested. '"

RFr,Pl\/F-:D
SEP 18 7017
DWR SECTION
INF ORMAATION PROCESSING UNI , A
novo nordisk®
September 08, 2017
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Per the requirements of Novo Nordisk Pharmaceutical. Industries' stormwater discharge General Permit
NCG060000 and Certificate of Coverage No. NCG060048,.itached are the results from the qualitative
monitoring and analysis carried out on August 10, 2017.
1 may be reached at 919-550-2200 at extension 2217 if you have questions.
Since
R. Paul Morris
Novo Nordisk Pharmaceutical Industries, Inc
3612 Powhatan Rd
Clayton, NC 27527

NOVO NORDISK
ATTN: PAUL MORRIS
3612 POWHATAN RD.
CLAYTON ,NC 27527
PH (not to be used for reporting) 6.7 08/10/17 BNC 4500HB-00
COD, mg/l 28 08/18/17 SFJ H8000-79
Total Suspended Residue, mg/1 6.2 08/11/17 MAR 2540D-97
TPH (1664B), mgA <5 OW16117 SEJ EPA1664B
DATE COLLECTED:
DATE REPORTED :

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191 Week:33
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NOVONORDISK
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ATTN: PAUL MORRIS
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3612 POWHATAN RD.
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CLAYTON NC 27527
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lSltil t:ClIl11JIC t(1 Ihi? t_111f h:; �It}{J've 1'lf uoch pofdlllotT;T ,r.,''.IUI,:iII-.iC1 4 _

May 9, 2017
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
MAY 16 20V
CENTRAL FILES
DWR SECTION
0
novo nordisk
Per the requirements of Novo Nordisk Pharmaceutical Industries' stormwater discharge General Permit
NCG060000 and Certificate of Coverage No. NCG060048, attached are the results from the qualitative
monitoring and analysis carried out on April 24, 2017.
I may be reached at 919-550-2200 at extension 2217 if you have questions.
Sincere y
AL,
R. Paul Morris
Novo Nordisk Pharmaceutical Industries, Inc
3612 Powhatan Rd
Clayton, NC 27527

NOVO NORDISK
ATTN: PAUL MORRIS
3612 POWHATAN RD.
CLAYTON ,NC 27527
PARAMETERS
PH (not to be used for reporting)
COD, mg11
Total Suspended Residue, mg/1
TPH (1664B), mg/l
Stornmrater
Analysis
ilethod
(#I, Grab)
Date Analyst
Code
6.9
04/25/17
KDS
4500HB-00
44
04/27/17
SEJ
H8000-79
5.5
04/26/17
IN -TAR
254OD-97
<5
04/27/17
SEJ
EPA1664B
ID#: 191
DATE COLLECTED: 04/24/17
DATE REPORTED s 04/27/17
REVIEWED BYs /--�

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NOVO NORDISI:
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P
P
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C:ONIAVFP INFE, FW.
ATTN: PAUL MORRIS
3612 POWHATAN RD.
GHf.:l�11[;AL PFtFSL J��'A7tt J
CLAYTON NC 27527
.........-._._.._.....—
A
C
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[phone]
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RECEIVED
,�CT052016
,ENTRAL FILES
DWR sEGTION
September 29, 2016
Central files
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
0
novo nordisk
Per the requirements of Novo Nordisk Pharmaceutical Industries' stormwater discharge General Permit
NCG060000 and Certificate of Coverage No. NCG060048, attached are the results from the qualitative
monitoring and analysis carried out on September 2, 2016.
I may be reached at 919-550-2200 at extension 2217 if you have questions.
Sincerel
R. Paul Morris
Novo Nordisk Pharmaceutical Industries, Inc
3612 Powhatan Rd
Clayton, NC 27527

P.O. BOX 7085, 114 OAKMONT DRIVE
GREENVILLE N C: 27835-7085
NOVO NORDISK
ATTN: PAUL MORRIS
3612 POWHATAN RD.
CLAYTON ,NC 27527
PARAMETERS
PH (not to be used for reporting)
COD, mg/l
Total Suspended Residue, mg/l
TPH (1664B), mgll
Stormwater
Analysis
Method
(#I, Grab)
Date
Analyst
Code
6.5
09/06/16
KKM
4500HB-00
34
09/08/16
SEJ
H8000-79
6.5
09/07/16
KNF
254OD-97
c 5
09/08/16
SEJ
EPA1664B
r'PH
F
ID#: 191
DATE COLLECTED: 09/02/16
DATE REPORTED : 09/09/16
REVIEWED BY:

Environment 1,
P.O. Box 7085, 114 Oakmont Dr.
Greenville_ NC ?7RSR
CHAIN OF CUSTODY RECORD
Page I of
L
-nvironrnent 1 inc.com
DISINFECTION
CHLORINE NEUTRALlZEDATCOLLECTION
Phone [phone] • Fax [phone]
CHLORINE
CLIENT: 191 Week: 33
UV
pH CHECK (LAB)
P
P
P
G
CONTAINERTYPE, PIG
NOVO NORDISK
❑ NONE
ATTN: PAUL MORRIS
A
C
A
C
CHEMICALPRESERVATION
3612 POWHATAN RD.
CLAYTON NC 27527
❑
U' A NONE D NAOH
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[phone]
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COLLECTION
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SAMPLE LOCATION
DATE
TIME
Stormwater (f/1, Grab)
f/
P� �
4'.
�.
CLASSIFICATION:
WASTEWATER(NPDES)
DRINKINGWATER
DWQ/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING HIPMENT/DELIVERY
N
SAMPLES COLLECTED BY:
(Please Print)
SAMPLES RECEIVED IN LAB AT °C
R I (SIGZ(SAMPLER)
DATErnME
EIVED BY (SI .)
DATEMME
OMMENTS:
.)
DATEMME
RERE r1VBY(S1G.)��
DATE/iiME
t1ZNQHA,
_,
aC6/4L1,
.A
Lth;, 10.1
—
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (S .)
DATEMME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C for composite sample or a "G" for
Grab sample in the blocks above for each parameter requested. Na 3 2 3 8 5 3 `

June 14, 2016
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVED
JUN 21 2016
CENTRAL FILES
DWR SECTION
novo nordisV
Per the requirements of Novo Nordisk Pharmaceutical Industries' stormwater discharge General
NCG060000 and Certificate of Coverage No. NCG060048, attached arc the results from the qua
monitoring and analysis carried out on May 10, 2016. f
I may be reached at 919-550-2200 at extension 2217 if you have questions.
Sincercly.,
R_ Paul Morris
Novo Nordisk Pharmaceutical Industries, Inc
3612 Powhatan Rd
Clayton, NC 27527

I PAI.Onment I, Inc. CHAIN OF CUSTODY RECORD
P.D. Box ?085, i ,!I Oakmont Dr.
Greenville N(' 27R.59
Page. _1 of — I—
,gV:i
DISINFECTION
gone (252) 756-62U8 • Fax [phone]
�p
CHLORINE}VEUTR� 'EDATCCLLFCTIOiv
^EiLO fNF-
,}
_-
PH CHECK (UAB)
l l I�'+ N T: 191 N'cck: l
�I
r
I�t 4
P
P
p
G
�
CONTAINER TYPE. PIG
VOVO NORDISK
NONE
ATTN. PAUL MORRIS
3612 POWHATAN Ri).
1
CLAWON NC 27527
A
C
A
C
CFiE" iCALPFiESERVAT1DlJ
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SAN4PLELOCATI0N
DATE
TIME
(1, Graff)
-
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�
3
I
A7IQStormwater
GASSIFC
kNASTEWATER (hlf'DES)
C� DRINK OWATER
I
99
1
la
DW[�lGW
FCL}D WAM SECTION
_
I
CHAIN OF CUSTODY' SF k) FlA NTAINED
DURI`dG SHIPMENTIDELIVERY
ll
k••i
S,AVFLES COLLECTED BY;
(Pe % ref ..: C
— ....,._
SAMFLES RECEIVED IN LAB AT.SL.L °C
(@AMPLER}
DA'rErTIME
BY (51G.
DAT&INIE
CA�7MENTS:
✓RECEIVED
ref' i15
— '--
ATGTiv1E
—.._....�
OATtF11ME
RELIIV011ISHED GY(SIC.)
RECEIVED�f',]IG.j
/
RFLINbUiSHEC BY (SIG.}
DAfFJTItvJE
RECEIVED BY (SIG:,
DATE'TiME
_ Sampler must place a "C' for composite sample or a "T for ry
PLEASE READ Instructions for completing this form on the reverse side. „� „� N .W 3 2 12 4 6

NumhEi RM 1, hcoo
..0. BOX 70,'35, 114 L�PiKMC)?1 C DRIVE
GREENVILLE, N.C. 27835-7085
NOVO NORDISK
ATTN- PAUL MORRIS
3612 POWHATAN RD.
CLAYTON FNC 27527
owmNd
_ —'"�' .. � �. .•.•. - .. ,-My4fCe r'iEzr 4tDs rt m.
PHONE [phone]
FAX [phone]
Stormwater Analysis Method
PARAMETERS (#1, Grab) Date Analyst Code
PH (not to be used for reporting) Lab Error
COB, mg1l 27 05/09/16 SEJ HS000-79
Total Suspended Residue, mg/l <2.7 05/06/16 MCS 25400-97
Oil & Grease (HEM), nag/1 <5 05/10/16 SEJ 1664.E
ID#z 191
DATE COLLECTED: 05/03/16
DATE REPORTED : 06/09/16
REVIEWED BY:
r'

0
REC(�ovo nordisk
MAY 18 2015
May 13, 2015 CENTRAL FILES
DWR SECTIO,
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Per the requirements of Novo Nordisk Pharmaceutical Industries' stormwater discharge General Permit
NCG060000 and Certificate of Coverage No. NCG060048, attached are the results from the qualitative
monitoring and analysis carried out on April 21, 2015.
I may be reached at 919-550-2200 at extension 2217 if you have questions.
Since
R. Paul Morris
Novo Nordisk Pharmaceutical Industries, Inc
3612 Powhatan Rd
Clayton, NC 27527

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aceAalytical
1
_ www.pacafabs.com
May 01, 2015
Mr. Paul Morris
Novo Nordisk Pharmaceutical
3612 Powhatten Rd
Clayton, NC 27520
RE: Project: STORM WATER
Pace Project No.: 92246415
Dear Mr. Morris:
y�c6_o6�q�
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
1 [phone]
ale ✓,
Enclosed are the analytical results for sample(s) received by the laboratory on April 21, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Terri Page
[e-mail]
Project Manager
Enclosures
cc: Accounts Payable, Novo Nordisk Pharmaceutical
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 17

s
aceAnalytical
wwwPmm13b&G ro
Project: STORM WATER
Pace Project No.: 92246415
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
CERTIFICATIONS
North Carolina Bioassay Certification #: 15
North Carolina Drinking Water Certification #: 37731
FloridalNEtAP Certification # E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
Eden, NC 27288
[phone]
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Floiida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NCO30
West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712
VirginialVELAP Certification #: 460222
Eden Certification IDS
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification M 37738
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 17

aceAnalytical
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SAMPLE ANALYTE COUNT
Project: STORM WATER
Pace Project No.: 92246415
Pate Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92246415001 STORM WATER EPA 9040
JTF
1
PASI-E
EPA 1664E
CLW
1
PASI-C
SM 2540E)
RC
1
PASI-R
SM 5220D
MAB
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pate Analytical Services, Inc.. Page 3 of 17

apAnalytical
' www,paaela6s.wrrr
PROJECT NARRATIVE
Project: STORM WATER
Pace Project No.: 92246415
Method: EPA 9040
Description: 9040 pH
Client Novo Nordisk Pharmaceutical
Date: May 01. 2015
General Information:
1 sample was analyzed for EPA 9040. Ail samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
H3: Sample was received or analysis requested beyond the recognized method holding time.
• STORM WATER (Lab ID: 92246415001)
H6: Analysis initiated outside of the 15 minute EPA recommended holding time.
• STORM WATER (Lab ID: 92246415001)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
Ail surrogates were within QC limits with any exceptions noted below.
Method Blank:
All anaiytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with arty exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 17

acioMalXiml e
wnnvpecelabs.cam
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27286
[phone]
PROJECT NARRATIVE
Project: STORM WATER
Pace Project No.: 92246415
Method: EPA 1664E
Description: HEM, Oil and Grease
Client: Novo Nordisk Pharmaceutical
Date: May 01, 2015
General Information:
1 sample was analyzed for EPA 166413. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within CC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below -
Laboratory Control Spike:
All laboratory control spike compounds were within OC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 17

e
aceAnalytical
—paceiabsxorn
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Project: STORM WATER
Pace Project No.: 92246415
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Novo Nordisk Pharmaceutical
Date: May 01, 2015
General Information:
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below
Bold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All anatytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
Ail duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 17

e
acoAnalytical
snnrpecelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
PROJECT NARRATIVE
Project: STORM WATER
Pace Project No.: 92246415
Method: SM 5720D
Description: 52200 COO
Client: Novo Nordisk Pharmaceutical
Date: May 01, 2015
General Information:
1 sample was analyzed for SM 5220D. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
OC Batch: WETA/22682
A matrix spike and/or matrix spike duplicate (MS/MSD) were perforated on the following sample(s): 92246195001,92246722001
M6: Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
• MS (Lab ID: 1442596)
• Chemical Oxygen Demand
• MSD (Lab ID: 1442597)
• Chemical Oxygen Demand
Addttional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 17

e
acieAnalytical
pacdabs.aom
ANALYTICAL RESULTS
Project: STORM WATER
Pace Project No.: 92246415
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27208
[phone]
Sample: STORM WATER
Lab ID: 92246415001 Collected: 04/19115 19:00
Received: 04/21/15 16:10 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
9040 pH
Analytical Method: EPA 9040
pH
6.6 Sid. Units
0.10
1
041Y1115 16:00 H3,H6
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L
5.0
1
05101/15 06:59
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
9.5 mg/L
3.8
1
04/22/15 08:07
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
33.0 mg1L
25.0
1
04/27/15 10:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/01/2015 04:03 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 17

0
aceAnalytrcal
wrrw.pacehabs.com
QUALITY CONTROL DATA
Project: STORM WATER
Pace Project No.: 92246415
QC Batch: EDEN118209 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN
Associated Lab Samples: M46415001
SAMPLE DUPLICATE: 1440902
Parameter
pH
92246415001 Dup
Units Result Result RPD Qualifiers
Sid. Units 6.6 6.5 0 H3,H6
Pace Analytical Services, [nc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Re ft prated on this page are in the units Indicated by the 'UnW column except where an afternate unit Is presented to the right of the resutL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/0112015 04:03 PM without the written consent of Pace Analytical Services, 1 nc..
Page 9 of 17

acaAnalyticale
wwwpacelatrs.cam
QUALITY CONTROL DATA
Project: STORM WATER
Pace Project No.: 92246415
QC Batch: GCSV/21144 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92246415001
METHOD BLANK: 1448049 Matrix: Water
Associated Lab Samples: 92246415001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 05/01/15 06:50
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE:
1448050
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oii and Grease
mg/L
40 38.4
96
78-114
MATRIX SPIKE SAMPLE:
1448051
92246402001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
35.9
90
78-114
Resuhs presented on this page are in the untts indicated by the "Units' column except where an aitsrnate unit Is prese"M to the right of the MUM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/01/2015 04:03 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 17

ace.Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: STORM WATER
Pace Project No.: 92246415
QC Batch: RWETI8252 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92246415001
METHOD BLANK: 1440349
Associated Lab Samples: 92246415001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE:
1440350
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 1440351
Parameter
Units
Total Suspended Solids
mg1L
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 04i12l15 08:06
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 242 97 90-110
92245286001 Dup
Result Result RPD Qualifiers
58.7 58A 1
Resuhs presented on this page are In the units Indicated by the -Units* column except where an ahernate unit is presented to the right of the resulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05/01/2015 04:03 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 17

ro
aceAnalyticai
anvw.pacela6s.com
QUALITY CONTROL DATA
Project: STORM WATER
Pace Project No.: 92246415
QC Batch: WETA122682 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92246415001
METHOD BLANK: 1442592
Associated Lab Samples: 92246415001
Parameter Units
Chemical Oxygen Demand mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 0412711510:55
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1442593
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand rnglL 750 797 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1442594 1442595
MS MSD
92246722001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cane. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mgfL 84.0 750 750 846 846 102 102 90-110 0
MATRIX SPIKE & MATRV SPIKE DUPLICATE: 1442596 1442597
MS MSD
92246195001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mglL 4010 6000 6000 7460 7460 58 58 90-110 0 M6
0
Results presented on this page are in the units indicated by the "Unite" column except wham an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in MI,
Date: 05/01/2015 04:03 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 17

aceAnalytical
wwwcpaca(abs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Project: STORM WATER
Pace Project No.: 92246415
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit"
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values"
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethyivinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonilrile by EPA
Method 8260"
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analylical is TNI accredited. Contact your Pace PM for the current list of accredited anatytes.
TNI - The NELAC Institute.
1!1=IaI,7_'t to] :71*1
PASI-A
Pace Analytical Services - Asheville
PASI-C
Pace Analytical Services - Charlotte
PASI-E
Pace Analytical Services - Eden
PASI-R
Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: M0112015 04.03 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 17

e
aceAnalytical
wmpacebbs.can
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: STORM WATER
Pace Project No.: 92246415
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92248415001
STORM WATER
EPA 9040
EDEN118209
92246415001
STORM WATER
EPA 1664B
GCSVl21144
92246415001
STORM WATER
SM 2540D
RWET18252
92246415001
STORM WATER
SM 5220D
WETA122682
Date: 05/01/2015 04:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 17

i
0
novo nordisk
September 12, 2014
Central Files
Division of Water Quality
1617 Mail Service Center c •b
Raleigh, NC 27699-1617 }�]_
Per the requirements of Novo Nordisk Pharmaceutical Industries' stormwater discharge General Permit
NCG060000 and Certificate of Coverage No. NCG060048, attached are the results from the qualitative
monitoring and analysis carried out on August 13, 2014.
I may be reached at 919-550-2200 at extension 2217 if you have questions.
Sincerely,
r
R. Paul Morris
Novo Nordisk Pharmaceutical Industries, Inc RECEIVED
3612 Powhatan Rd
Clayton, NC 27527
SEP $ 6 2014
CENTRAL FILES
DWR SECTION

cLi
I
BAnalyfibal
wwwpeceiabs.cvm
August 28, 2014
Mr. Paul Morris
Novo Nordisk Pharmaceutical
3612 Powhatten Rd
Clayton, NC 27520
RE: Project: SSW -ANNUAL SW
Pace Project No.: 92213287
Dear Mr. Morris:
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on August 13, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Terri Page
[e-mail]
Project Manager
Enclosures
oc: Accounts Payable, Novo Nordisk Pharmaceutical
REPORT OF LABORATORY ANALYSIS
. This report shall not be reproduced, except in MR,
without the written consent of Pace Analytical Services, Inc._
Page 1 of 17

ceAnalytical
wrnxRmcebbs.00m
I -
Project: SSW -ANNUAL SW
Pace Project No.: 92213287
Raleigh Certification IDs
6701 Conference Drive Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersviile, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida[NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(3W)623-8921
CERTIFICATIONS
North Carolina Bioassay Certification M 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627
Georgia Certification: VirginiaNELAP ID# 46022
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 17

aceAnalytrcal
.Paoelabs.cum
SAMPLE ANALYTE COUNT
Project: SSW -ANNUAL SW
Pace Project No-: 92213287
Pate Anatytltal Services, Inc.
205 East Meadow Road - Suits A
Eden, NC 27288
(3W)623-8921
Lab ID Sample ID Method
. Analysts
Analytes
Reported
Laboratory
92213287001 SW-1 EPA 1664B
AM1
1
PASI-C
SM 2540D
MBG
1
PASI-R
EPA 9040
MDW
1
PASI-A
SM 5220D
MAB
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc.. Page 3 of 17

e
ceAnalytical
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PROJECT NARRATIVE
Project: SSW -ANNUAL SW
Pace Project No.: 92213287
Method: EPA 1664B
Description: HEM, Oil and Grease
Client: Novo Nordisk Pharmaceutical
Date: August 28, 2014
General Information:
1 sample was analyzed for EPA 168413. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
Ali surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within OC limits with any exceptions noted below.
Pace Analytical Services, Inc.
295 East Meadow Road - Sutte A
Eden, NC 27288
[phone]
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 17

Pace Analytical Services, Inc.
aceAnaiyficaie 205 East Meadow Road - Suite A205
Eden, NC 27288
ww p com (336)623$921
PROJECT NARRATIVE
Project: SSW -ANNUAL SW
Pace Project No.: 92213287
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: Novo Nordisk Pharmaceutical
Date: August 28, 2014
General Information-
1 sample was analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc.. Page 5 of 17

aceAnalytical.
www.PacsA3bs.wm
PROJECT NARRATIVE
Project- SSW -ANNUAL SW
Pace Project No.: 92213287
Method: EPA 9t>4l1
Description: 9040 pH
Client: Novo Nordisk Pharmaceutical
Date: August 28, 2014
General Information:
1 sample was analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below.
Hold Time.
The samples were analyzed within the method required hold times with any exceptions noted below.
1-16: Analysis initiated outside of the 15 minute EPA recommended holding time.
• SW-1 (Lab ID: 92213287001)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NG 27288
[phone]
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.- Page 6 of 17

Pace Analytical Services, Inc.
aceAnalytical a 205 East Meadow Road - Suite A
Eden, NC 27288
wrw.paceJabs.00m [phone]
PROJECT NARRATIVE
Project: SSW -ANNUAL SW
Pace Project No.: 92213287
Method: SM 5220D
Description: 5220D COD
Client: Novo Nordisk Pharmaceutical
Data: August 28, 2014
General Information:
1 sample was analyzed for SM 5220D. All samples were received in acceptable condition with any exceptions noted below_
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: WETA120057
A matrix spike and/or matrix spike duplicate (MSIMSD) were performed on the following sample(s): 92213962001,92214028001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based an laboratory oontroi sample (LOS) recovery.
• MS (Lab ID: 1272881)
• Chemical Oxygen Demand
• MSD (lab ID: 1272882)
• Chemical Oxygen Demand
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 17

aMAnalytical.
www.par�bsaom
ANALYTICAL RESULTS
Project: SSW -ANNUAL SW
Pace Project No.: 92213287
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: SWA
tab ID: 92213287001 Collected: 08112l14 22:27
Received: 08/13/14 17:03 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L
5.0
1
08/18/14 13:37
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
31.4 mg/L
3.8
1
08/14/14 11:14
9040 pH
Analytical Method: EPA 9040
pH
6.8 Sid. Units
0.10
1
08/15/14 11:06 H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
26.0 mg/L
25.0
1
08/28/14 15:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2014 04:20 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 17

aceAnalytical
wwMp8oeJ3bs.mrn
Project: SSW -ANNUAL SW
Pace Project No.: 92213287
QC Batch: GGSW18593
QC Batch Method: EPA 1664E
Associated Lab Samples: 92213287001
METHOD BLANK: 1266228
Associated Lab Samples: 92213287001
Parameter Units
Oil and Grease mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 1664E
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 08/1811413:30
Pace Analytial Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE:
1266229
Spike LCS
LCS
% Rec
Parameter
Units
Cane. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 38.5
96
78-114
MATRIX SPIKE SAMPLE:
1266230
92213414001 Spike
MS
MS
% Rec
Parameter
Units
Result Cone.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
39.3
96
78-114
Results presented on th6 page are in the urdts indicated by the -Units' rd ran except where an albowds unit Is prsaantad to Ms 119M of the result.
REPORT OF LABORATORY ANALYSIS
This mart shall not be reproduced, axoept in full,
Date: 08/2812014 04:20 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 17

aceAnalytical
eW W..paGvA1bs.com
Project: SSW -ANNUAL SW
Pace Project No.: 92213287
QC Batch: RWETl6907
QC Batch Method: SM 2540D
Associated Lab Samples: 92213287001
METHOD BLANK: 1263898
Associated Lab Samples: 92213287001
Parameter Units
Total Suspended Solids mg1L
LABORATORY CONTROL SAMPLE: 1263899
Parameter Units
Total Suspended Solids mg/L
SAMPLE DUPLICATE: 1263900
Parameter Units
Total Suspended Solids mg1L
Pace Analyttcal Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 08/14/14 11:11
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 270 108 90-110
92213286MI Dup
Result Result RPD Qualifiers
1660 1570 5
ResWta preseffrtDd wr this PMG are in the units Indicated by !fie "Units' catumn except Where an alternate unit Is preseread to the dWd of the "mutt
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2014 04:20 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 17

e
aceAnalytica!
wwwpacelalmmm
Project: SSW -ANNUAL SW
Pace Project No.: 92213287
QC Batch: WET/32673
QC Batch Method: EPA 9040
Associated Lab Samples: 92213287001
SAMPLE DUPLICATE. 1264906
Parameter Units
pH
Std. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description: 9040 pH
92213287001 Dup
Result Result RPD
6.8 6.8
Qualifiers
0 H6
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Results presented on this page are In the units indicated by the 'Unita' column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 08/28/2014 04:20 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 17

I
eAnalyfcal •
waM!paczla6swm
Project: SSW -ANNUAL SW
Pace Project No.: 92213287
QC Batch: WETA/20057
QC Batch Method: SM 5220D
Associated Lab Samples: 92213287001
METHOD BLANK: 1272879
Associated Lab Samples: 92213287001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 1272880
Parameter Units
Chemical Oxygen Demand mg/L
QUALITY CONTROL DATA
Analysis Method:
Analysis Description
Matrix: Water
SM 5220D
5220D COD
Pace Analytical 5errioes, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 0812811415:15
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750 740 99 90-110 -
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1272881 1272882
NIS MSD
92214028001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conn Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 2570 3000 3000 4500 4500 64 64 90-110 0 M1
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1272883 1272884
MS MSD
92213962001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Cone. Result Resutt % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 26.0 750 750 752 760 97 98 90-110 1
Results presented on this page we in the units indicated by the 'Units" rolumn except when an alter na unftjsprosefftdtatherigMoftheresutL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: OS/2812014 04:20 PM without the written consent of Pace Analytical Services, Inc -
Page 12 of 17

Pace Analytical Services, Inc.
ceAnalytical • 205 East Meadow Road - Suite A
Eden, NC 27298
WWW.P &Co1n (336)623$921
QUALIFIERS
Project: SSW -ANNUAL SW
Pace Project No.: 92213287
DEFfNMONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit-
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit_
RL - Reporting Limit_
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration_
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2014 04:20 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 17

Pace Analytical Services, Inc.
ceAnalytrcal0 205 East Meadow Road - Suite A
Eden, NC 27288
swr pacelehtmm (33"23-8921
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SSW -ANNUAL SW
Pace Project No.: 92213287
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92213287001
SW-1
EPA 1664B
GCSV118593
92213287001
SW-1
SM 2540D
RWET16907
92213287001
SW-1
EPA 9040
WET132673
92213287001
SW-1
SM 5220D
WETAI20057
Date: 08/28/2014 04:20 PM
REPORT OF LABORATORY ANALYSIS
This report sham not be reproduced, except in full,
without the written consent at Pace Analytical Services, Inc._
Page 14 of 17

Instructions for completing Chain of Custody (COC)
I. Sect.ioii to and B: Complutc all Cli,:nt information at top of sleet: eompam name. addrv;ss, phun.;, lax. contact (the person to c:untaet ifthcre art
questions. in(] who xvill r uciv'c the final report.). c-m�►i l address (if avadahle t. 11,04. Prolcet' Name :uld!tu' Pro ed Number as you would like to sec it
appear (m the: rclx)rt.
2. Section t.,: invoice Information: !tilling inro 7 iation is inlettidud in this sMion. ']'his intl'mmition should include the music and nddre:ss clt tilt: pen -on
ruceivint: Illy invoice,
3, (dote Itetimncc should he completed if a cluotution r►n4 prnvided by face An:tivliu:d. '1'ha Prgject Mtin,, gger, and I'mfile No. tvill he compivted by
1"acc Analytical Servivos,
4Site Location: r1 sopartite C OC must he filled oul tilt mull day or sampic c olhxtion ltccord the tm, lutt,:.r postal axle tiirthc 111, mate in which the
sanll+les twat eclllcetecl.
�. RePpOntory AUney: Li -It the priegriilii tli.tt iy guiding file ►work tci cnslt p►<Ip+ r r.,Tul ititins i►ru f'cillcnv.d.
6. Section D: Unnpll:le a tiamplc lksciiption in the "SAMPI 1: iD' section :ir you lvouid like it t► aplicaron tliv (aborotory rupmi. The following
info ntatimi should also hc,• illOi-OtA thu sampIv mviirix, .,�tunplc: type ((; (gr h) or C. (c ompositel. 'Whin coltccting it aempm ilu. lice strut time and end
teal; should be do utimented in the respective boxes. I'lie collection time fora grab fG i should he Lntercd in the; hOWS nu►rked '('omfuisitc,
End;(;rahA Sample; temp at cx,llection lit mquiwd by,,;tltc). the total mtniticr ofe►intairivr:, and pmervati►•e used.
7. Mark iftlie sainplu was #illcrud in the field by marking Y or N ill '1,iltered' row by tlr.: Analvsns mqucsted
9. Rv(4ttV,tud .Attalvsi4: list the. requiiO analysis and rtuAliods ,it the liiw�, prtevielud and platx a uhcck in tllc colunio tclr file ,imiple, rucluiring the
altalysis. Additic,nal comincm, -should he icferencal in flit hrttorri left hand comer or hicludc Yitacilmclity liar extended list, of l aratncttm..
Q. The saniplcrshtluld print flivirilanic ill tilt sl)t1iC pl-ovidcd and sign Ihcir iiamc liillcltvxl by tht date tit'IIYe samli ing :v.`nl ai the huttom ofthc C•OC ill
IIle spacers de,igrirllcd tier •NAN-11'l.l•:It NAN-fI:.ANU SIGN,ATI 4F.
it) V4`licn relineµiishmps eu Aotl% of the sample% to ,t i1:prewwativc of the tahnnitory ter tether e,rf;ailir_(tir$il, tnthu:de. the Item :VunihcrK of fhosu samples
buina, trans1enrcd: si'an iv inquishcd hv, date altd til v, and inlelllelc %imr aftilialion.
'clinportant plate:
Standard Turnaround Tinte Is Z Weeks/10 business clays. lt.v%ith-, will hu delivei—ed by end of husinevs on the daft• t1m; unlcss other arf-anaements
hav;: hct'ti made xvith vour Pm.1 ~ct manager,
Special Project Requirements .such tis Low I .Cvul I etueli"n l.inlity ur te;vvl of QC mpo ucf nturt he utcltidW on the chaise ofcustod) in the Additinnal
Corlinecntr• secti►titl.
N
0
LO
W
.a

cu
Document Name: Sample Condition Llpoa
Document Rev#sed: Apn104.2[)13
;�p1181yj�'
Receipt SCUT
e 1 of 2
Document No.:
Issulrig Authorli9aa
F-RAi-CS
Pace Asheville Qua Otte
Client Name:_ Y,90
�1
11-14
Where Received: ] Huntersyilie ❑ Asheville
Eden Raleigh
Courier (Cirdey - Fed Ex UPS LISPS Client -
Cornmerclai
. Other
Custody Seal on Cooler/Box Present i1 yes ,� { no
/Bag`s
Seals
irlact yes
0 no
Packing Matedul: ❑ Bubble Wrap ❑ Bubble y�j Mona
Circle Thermometer Used: IR Gran 3N:122066?; x Of ice:
Other
Blue None
ri Samples on ice. 000ltrrg process has begun
tR nun RaekLaSN,12206S2711
Tam p Correction Factor: Add ! Su&et 19, % C
Biological
Corrected Cooler Ternp.: C 9ical Tissge is Fran: Yea aro
Temp dwtM be above freezing to 6•C Commenter
Date and InMWs of ponce ;g
1 arrati
f�
ChdIn of COs Present: E IW
❑WA
1.
Chain of C Filled Out
as tuo
OWA
2.
CCr�/
Chain of CustDdy Refl (shed:
Yes Onro
OWA
3.
Sampler Name & Si mature on COC:
Yee ❑r4o
❑WA
4.
Sam las Arrived withlit Hold Time:
Yes ONo
OWA
6.
Short hold Time Mal [72hr :
OYes [IN.
WA
6.
a �el r
Rush Tum Around Time R uested:
❑Yes &NO
OWA
7.
Suff clerlt Volume:
gfY. ON.
EIWA
8.
Correct Containers LPmd
-Pace Containers Used:
res ONO
/ Yes ❑No
QNA
ONIA
9
Containers intact
9yes ONO
OWA
10.
Filtered volume •recetved for Dissolved tests
❑Yea ENO
ETWA
11.
Sample Labels match COG:
.Includes dateRlmefEDlAnaf is Nlsubc
/IlYes I�rro.
.�
❑WA
12.
All =Wrrers rawfi g p wove hn have been dredged.
.
Ali oontakiers nmdlrig preservation we found to be In
compIletva with EPA recommendation.
WMPW= VOA. 9olAn+in, TM O&G, WI-DRO {water}
21- ©No
/ ONO
Yes 0?40
OWA,
OWA
13.
samples checked for dechlwnatlorr
❑Yes ONO
NtA
.14.
Head ce in VOA Vials ;-Ornm :
❑Yes ❑No
Trip Blank Present;
Trip Blank Custody Seals Present
Pace Trip Blank Lot # Cf urrhased):
OYa9 ONO CAA
[Yes ONO QkA
16.
Client Nodfleatlonf Resolution: Field 0ata RagTiued7 Y / N
Person Contacted: Date rne:
Comments/ Resoludw:
SCURF /SRF
Review-::
Date:
Note-. Whenever there is a pancy aftecilng Nash Carolfna crompEw
samples, a copy of this ram wM be rant to Me North Carorms OEHNR
Certificedon Ofcroe (1.e actor hold, i =nvd pr'eservaiive, out of temp,
Inwrad cantainem)
Moe label here
OR
Handwdle project number
of no label evafleble)
Page 16 of 17

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�;err■!!rr■!■rrr■�■!■■iii�i
!■ e!lrer■rrle■!■�
■
■a
Client Sample Ins
Sample Discre anc
PH Adjustment Loq for Preserved Sam
!es
Sample ID
Type of
Preservatve
PH up-
receipt
Bate presarva Solt
A(O sWd
Tune Preservation
,4cfueted
Amourd of
Pressrvabe added
LotR or
Preservative
Bottle Code Key
125 ml Plastic Unp: 13P4U
250 ml Plastic Unp: BP31J
500 mi Plastic Unp- BF2U
I Liter Plastic Unp: 8PIU
250 ml Plastic H2SO4: BP3S
250 ml Plastic HNO3: RMN
250 ml Plastic ZN Acetate: BP3Z
250 ml Plastic NaOH: BP3C
Wide mouthed glass jar unp: WGFU
i Liter Amber Unp: AG1 U
i Liter Amber HCl.- AG1H
500 ml Amber Unp: AG2U
1 Liter Amber H2SO4: AG IS
250 ml Amber H2SO4: AMS
250 ml Amber NH4CL: AGM
40 mi VOA HCl: DG9H
40 ml VOA Na2S2O3: VG9T
40 ml VOA Unp: VG9U
40 mi VOA H2SO4: DG9S
5035 IGG VOAK
VPH ! Gas Kit : VlGK
125 rn1 Sterile Plasflc: SPST
250 ml Sterns Plastic: SP2T
Page 17 of 17