NCG060034_COMPLETE FILE - HISTORICAL_20170915

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V
DOC TYPE
HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ add 7
YYYYMMDD

Mitch
From: Ferrell, Eric (EHS) <[e-mail]>
Sent: Friday, September 15, 2017 1:13 PM
To: Hayes, Mitch
Subject: Pfizer Rocky Mount, NC - 5 Day Report - Permi : NCG060
Mitch,
G+)(c
As you requested during our conversation this week, please accept this email as a 5 day report in connection with an approximately 5 gallon diesel fuel spill at
our Pfizer Rocky Mount facility in Rocky Mount, NC.
Event Summary:
A fuel oil spill was discovered Monday, 9/11/17, on the east section of our property, in a gravel drive space, adjacent to our shipping warehouse. The
source of the spill is a 5 gallon fuel tank, used to refuel a rough terrain fork truck used by our roofing contractor. The fuel tank fell from the contractor's
pickup truck, spilling fuel in the process. There are no waterways or drains located near the spill location.
Event Response:
Upon discovery, site personnel requested service from our environmental cleanup contractor. The contractor arrived onsite, excavated the top 6 inches
(approximate) of gravel and soil, containerizing in drums for disposal. Due to the heavy compaction of gravel and soil, additional excavating equipment
is required to complete the work. Due to the need to locate utilities (the impacted area is over a fire main) and periodic rain, the completion of the work
has had to be extended to early next week. During all rain, the area has been covered with plastic sheeting, and access to the area restricted until work
is completed.
Actions Remaining:
We anticipate the work being completed early next week, including backfilling the area with new soil and gravel.
We trust you will find the foregoing satisfactory. If, however, you have any questions or require any additional information, feel free to contact me at your
convenience.
A, faro
Senior Manager, Environmental Health & Safety
Hospira, a Pfizer company
4285 N Wesleyan Blvd
Rocky Mount, NC 27804

j CG 0(00 3C5`f
Hospira
August 20, 2010
Raleigh Regional Office
Division of Water Quality
Surface Water Protection
1628 Mail Service Center
Raleigh, NC 27699-1628
Subject: Quarterly Status Report for Stormwater Outfall SW017
Reporting Period — August 2010
NPDES Stormwater Permit # NCG60034 (R 1) & NCG060035 (R2)
NPDES Wastewater Permit # NC0001589
To Whom It May Concern:
As required by our NPDES Wastewater permit, attached is a chronology of events that
outlines the actions taken to address the source of non-stormwatcr discharge from the
stormwater SWO17 outfall.
Please feel free to contact me at [phone] if you have any questions.
Sincerely,
W. Eric Ferrell
EHS Specialist
Environmental Health and Safety
Hospira, Inc.
4285 N Wesleyan Blvd
Rocky Mount, NC 27834
will [e-mail]
Enclosures
Hospira- Rocky Mount, N.C.

Outfall SWO17 Action Plan and Status Report Update Aug 2010
Date
Item Description
Action Taken
Next Ste s
12-Jan-09
The State Surface Water Quality inspectors (Ms. Autumn Hoban and Mr.
Concluded that the temperature could be
Dave Parnell) conducted an onsite inspection of our (3) cooling ponds
due to the proximity of the sewer line
related to our NPDES permit and our storm -water outfalls as identified in
located — 15-20 ft adjacent to the storm
our Storm Water Plan and permit. Samples were collected from the
drain_ Hot process water is often
cooling ponds and storm water outfalls during this inspection. The
discharged into the plant sewer system.
cooling pond samples were completed as part our upcoming NPDES
permit renewal but the storm water sample was collected due to storm
water run-off that seemed warm considering this was the fall of the year.
We discussed the temperature issue at length and walked the grounds at
R2 for possible root cause but no cross connections or potential sources
were identified.
Feb-09
The State communicated the results to the plant with indications that the
Sewer drawings were reviewed for
results seemed abnormal for storm water.
possible cross connections.
12-Feb-09
The sewer -line from the sampling station to the site discharge point was
No dye was detected in the outfall.
dye tested to see if any dye could be seen in the storm water drain leading
to outfall #17.
25-Mar-09
The City was brought onsite to conduct a visual scope inspection of our
Samples wore collected from outfall #17
storm water drain to help identify any cross connections. None were
by Hospira personnel on this date and
found, however, it appeared that the piping had a couple spots where
sent to the lab on 3-26-09. Tests were
water could infiltrate into the line.
requested for the metals identified by the
sample collected by the State.
(Sample results attached)
31-Mar-09
Another sample was collected from outfall 417 to test for the presence of
Results indicated no coliform present.
coliform to determine if a sewer leak exists. Samples were picked -up on
(Sample results attached)
April Ind
1-Apr-09
Additional samples from various sources were collected at the R2 plant to
Results indicated that the discharge from
further determine which sources might match -up with the results found at
outfall #17 is coming from groundwater
outfall #17 as well as the results for the R2 cooling pond. This was also to
since no leaks or cross connections have
help identify sources that might be affected with any new permit limits
been discovered.
being considered for our new cooling pond permit discharges. Also.
(Sample results attached)
during this time various storm drain manholes were excavated to
determine if any leaks into or from the line were occurring. An adjacent
hole was dug to groundwater level so samples could be collected and the
temperature compared to water inside the storm drain. The intent was to
determine if the ground water itself could be the source of the discharge
at outfall # 17.
2-Apr-09
A letter was sent to the State explaining all the investigative work that had
Continued to monitor outfall.
taken place and indicated that the discharge from outfall # 17 must be
coming from groundwater since no leaks or cross connections have been
discovered. However. we would continue to monitor the situation.
Page 1 of 4

Outfall SWO17 Action Plan and Status Report Update Aug 2010
Date
Item Description
Action Taken
Next Steps
9-Jun-09
The State returned to the site on a hot dry day to see if water was flowing
No root cause has been identified.
from outfall # 17. It was and additional samples were taken. At this time
(Sample results attached)
we reviewed with the State all the action items taken to identify and/or
isolate the issue.
Jun-09
Dirt was excavated around a storm water manhole near outfall 017 that
A leak was identified and sealed and the
was observed to have water leaking into it,
hole back -filled.
Jun-09
Fresh water was isolated in the building by turning it off at the meter.
No change observed at the outfall.
Jun-09
The underground fresh water line feeding the building was isolated by
No change observed at the outfall.
closing the valve inside the building and checking the meter to see if the
flow changed.
Jun-09
The fire main was checked for leaks by monitoring the line to see if the
No leaks were observed.
booster pump came to maintain pressure.
Jun-09
Spain Plumbing was brought onsite to visually scope the storm and
No leaks were found on either line.
sanitary sewer lines.
Jui-09
A second leak was noticed in the same storm water manhole that was
The area around the west side of the
The excavated area was left exposed to
repaired and excavated in June.
manhole was excavated and the leak was
monitor for water level fluctuations to
sealed.
determine if leaks were present in the area.
No specific leaks could be identified.
Jul-09
Dye test of the sanitary sewer flume was performed to check for leaks.
No leaks were observed.
Jul-09
Dye test of the sanitary sewer manholes was performed to check for leaks.
No leaks were observed in the excavated
hole adjacent to sanitary and storm sewer
(July 2009)
Jul-09
Dye test on the lift station in the basement was performed to check for
No leaks were observed.
leaks.
Aug-09
We continued to monitor the water level in the hole adjacent to storm
No specific leaks could be identified.
water manhole excavated in July. In addition we began to monitor the
water level in an indoor pit excavated to tic in a newly installed pH
neutralization system (referred to as "pH system pit") for city wastewater.
Aug-09
Met with Production staff to review water usage and sources.
Most water was used on the second floor
which goes to the lift station in the
basement. The water usage on the first
floor goes directly to the sanitary sewer.
Aug-09
A camera was used to in visually scope all indoor sanitary, pond and
No leaks were observed.
process drains on the first floor. There were some drains that were dye
tested because of not being able to get camera through traps.
Aug 09 thru
Monitoring continued on the pH system pit to sec if the water level would
Water level would fluctuate but no
Sep 09
change when doing regeneration of the De-lonization (DI) units and
specific leak could be identified.
backflushing of the Sand Filters.
Oct-09
D e test performed on the drain to neutralization pit side A
No leaks were observed.
Oct-09 IDye
test performed on the drain to neutralization pit side B I
No leaks were observed.
Page 2 of 4

Outfall SW017 Action Plan and Status Report Update Aug 2010
Date
Item Description
Action Taken
Next Steps
Oct-09
Dye test performed on the acid/caustic add drain to neutralization pit side
Leak identified and repaired by installing
A
new piping. (Feb 2010)
Oct-09
Inspection performed during sand filter back wash cycle.
Water level went up and turbulence
noticed in the water located in the pH
system pit.
Oct-09
Inspection performed during DI System Regeneration
Water level went up and the pH changed
Cut concrete and excavate piping (Jan 2010)
inside the pH system pit.
Nov-09
Excavated around drains to neutralization pits A & B, found that the drain
Repaired seals, filled in and repaired
sump connected to the drain lines underground had bad seals.
concrete floor.
Nov-09
Excavated around four (4) sand filter drains.
No leaks were observed, backfilled.
tamped and repaired concrete floor.
Nov-09
Excavated piping in the north hallway (two places).
No leaks were observed, backfilled,
tamped and repaired concrete floor.
Dcc-09
Hallway excavated at the intersection of the north and cast hallways
No leaks were observed.
where the pond piping turns to the south and the process line turns to the
north.
Jan-10
Excavated around acid/caustic drain add to neutralization pit A
Repaired leak in elbow and drain funnel.
Feb-10
Although DI/RO skid drains were repaired in January. we continued to
Findings indicated a leak in piping.
Cut concrete and excavate cleanouts on east
see a fluctuation in water level and pH in pH system pit during a
wall (March 2010).
regeneration and neutralization cycle, which appeared to indicate another
leak in main piping.
Feb-10
Cooling tower evaluated for leaks by testing for TRASAR chemical used
Outfall 017 sampling results did not
only in cooling tower.
show TRASAR chemical.
Feb-10
Evaluated piping under acid/caustic under retaining dike. (outside)
Findings indicated a leak in the 10"
piping. Temporary bypass piping
installed until repairs could be made.
Mar-10
Clean outs excavated inside the building on the east wall & by air
No leaks were observed.
compressors (identified in February 2010)
Apr-10
Concern rose about leak in the sanitary sewer line. Autumn Hoban,
Sewer line was dye tested and concrete
NCDENR, was notified April 16. 2010 and made aware of the situation.
parking area was cut and excavated to
Autumn was satisfied with the actions taken and scheduled and indicated
expose sewer line and inspect all joints
further notification for sewer release/overflow requirements was
from flume to l st manhole, (approx.130
unnecessary.
ft). No leaks were observed.
May-10
Acid/caustic tanks relocated and retaining dike excavated to expose
Leak identified and construction is
Water level fluctuation has decreased in pH
piping identified in February & March.
ongoing to repair damaged 10"
system pit after bypass piping has been
acid/caustic piping. Repair scheduled to
installed. Upon completion of acidlcaustic
be completed this month.
piping construction, comprehensive
sampling of outfall SW017 is to be
completed to compare with previous data.
Page 3 of 4

Outfall SWO17 Action Plan and Status Report Update Aug 2010
Date
Item Description
Action Taken
Next Steps
Outfall 017 is being visually monitored.
Invite Autumn Romanski and Dave Parnell,
Jun-10
Construction to repair acid/caustic tanks was completed.
No flow has been observed on dry days
NCDENR Surface Water Protection group,
and the creek bed is dry.
to re-evaluate 017 and repairs.
Conditions and repairs concerning outfall
017 were satisfactory. Surface Water
Aug-10
Autumn Romanski and Dave Parnell, NCDENR Surface Water Protection
Protection group indicated they would
Awaiting State report from site visit.
group, were onsite August 12 to re-evaluate 017 and repairs.
make the recommendation to close the
issue and remove the reporting
requirement from the permit.
Page 4 of 4

u N i L v v L. i
Q
Telephone: [phone]
Fax: [phone]
iii.�a� iun v
O
VROMEST
6701 Conference Drive
Raleigh, NC 27607
Laboratory Report
--- Prepared for ---
TODD WEGENAST
HOSPIRA
4285 WESLEYAN AVENUE
ROCKY MOUNT, NC 27804
I, v I L l t ,
0& AMENDED REPORT **
Page 1 of 2
NCIWW Cert. #: 067
NCIDW Cert. #: 37731
�p�tL
rJ
Q r �.•` d Report Date: 4/1/2009
Date Received: 3/26/2009
Work Order #: 0903-01913
Project No.: Cust. Code: H05480
Project ID: STORMWATER Cust_ P_O.#:
Sample ID Date Sampled Time Sampled Matrix Sample Type Condition
a1 OUTFALL 17 3/25/2009 10:43 SW Grab 4 +/- 2 deg C
Analyzed
Test Performed
Method
Results
Date Tirne Qualifier
Aluminum
EPA 200.8
1.03 mglL
3131/09 9:25
Copper
EPA 200.8
0.007 mg1L
3127/09 17:13
Iron
EPA 200.8
2.32 mg1L
3131109 9:26
i
EPA 200.8
0.031 mglL
3127/09 1713
Sample 1D Date Sampled Time Sampled Matrix Sample Type Condition
'2 INLET TO R2 POND 3/25/2009 16:20 SW Gram 4 +1_ 2 deg C
Analyzed
Test Performed
Method
Results
pate Time Qualifier
Aluminum
EPA 200.8
0.024 mglL
M 3/27/09 17:13
Copper
EPA 200.8
<0.007 mglL
3/27/09 17:13
Iron
EPA 200.8
0.107 mg1L
3127/09 17:13
Zinc
EPA 200.8
0.012 mglL.
3/27109 17:13
Sample ID Date Sampled Time Sampled Matrix Sample Type Condition
3 HOLE 3 3/25/2009 10:33 SW Grab 4 +1- 2 deg C
—
Analyzed
Pest Performed
Method
Results
Date Time Qualifier
kluminum
EPA 200.8
2.20 mglL
3131109 9:25
;upper
EPA 200.8
0.011 mglL
3/27109 17:13
ran
EPA 200.8
4.13 mglL
3131/09 9:26
:Inc
EPA 200.8
0.072 mglL
3127/09 17:13
Sample ID Date Sampled Time Sampled Matrix Sample Type Condition
R2 POND DISCHARGE 3/25/2009 13:25 SW Grab 4 +1- 2 deg C
Analyzed
est Performed
Method
Results
Date Time Qualifier
luminum
EPA 200.8
0.601 mglL
3127/09 17:13
oppBr
EPA 200.8
0.007 mg1L
3127109 17:13
on
EPA 200.8
0.604 mg1L
3127109 17:13
PA 200.8
mg1L
3127/09 17:13

Apr.15. 2009 2.49PM Tritest fax o No.2723 P. 2/4
ME
�.' "AMENDED AMENDED REPORT
6701 Conference Drive Page 2 of 2
Raleigh, NC 27607
,'elephone: [phone] NC/WW Cert. #: D67
Fax; [phone] NC1DW Cori. #: 37731
Laboratory Report
Work Order #: 0903-01913
AMENDED REPORT: CORRECTED DETECTION LIMIT ON COPPER, 04/16/09
Reviewed by:

0
0
7 r R' 'H'T E S T
Page 1 of 1
Laboratory Report
Lob Location 'R' %i 16b 1oCa1iOn 'C' Lob Localion 'W'
JCIWW Cert.#: 067 NCIDW Cert.#: 37731 NCIWW Cert.#: 103 NC1DW Cert.#: 37733 NCNM Cert.#: 075 NCIDW Cert.#: 37721
6701 Conference Dr, Raleigh, NC 27607 6300 Ramada Dr, Suite C2, Clemmons, NC 27012 6624 Gordon Rd, Unit G, Wilmington, NC 28411
Ph: [phone] Fax: [phone]p Ph: [phone] Fax: [phone] Ph: [phone] Fax: [phone]
Project No.: Report Date: 417/2009
Project ID: FECAL-RM2 #33101 Date Received: 3/31/2009
--- Prepared for ---
TODD WEGENAST
HOSPIRA
4285 WESLEYAN AVENUE
ROCKY MOUNT, NC 27804
Work Order #: 0903-02345
Cust. Code: H05480
Cust. P.O.#:
Ito. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition
001 STORM WATER 3/31/2009 11:20 SW Grab 4 +1- 2 deg C
Test Performed Method Results Lab Loc DaZedTime Qualifier
Fecal Coliforms/MF SM 9222D <1 CFU1100mL R 3/31/09 16:36
Reviewed by:
for Tritest. Inc.

AP'r, 15: 2009 2:50PM Tr test fax o No. 2723 P. 3/4
4
" AMENDED REPORT **
Telephone: [phone]
Fax: [phone]
6701 Conference Drive
Raleigh, NC 27607
Laboratory Report
-- Prepared for ---
TODD WEGENAST
HOSPIRA
4286 WESLEYAN AVENUE
ROCKY MOUNT, NC 27804
Project No.:
Project ID: WASTEWATER AND STORM WATER
Page 1 of 2
NCNVW Cert. M 067
NCIDW Cert. #: 37731
Report Date:
4/8/2009
Date Received:
4/2/2009
Work order #:
0904-00313
Gust. Code:
H05480
Cust. P.O.#:
lo. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition
]01 BASEMENT SUMP 4/1/2009 12:20 WW Grab 4 t/- 2 deg C
Analyzed
Test Performed
Method
Results
Date Time Qualifier
Aluminum
— — EPA 200.6
0.289 mglL
413109 16:42
Copper
EPA 200.8
0.014 mg/L
413109 16:42
'--)n
EPA 200.8
0.424 mg1L
4/3109 16:42
.c
EPA 200.8
0.029 mglL
413I09 16:42
�. Sample ID Date Sampled Time Sampled Matrix Sample Type Condition
02 FRONT DITCH 4/1/2009 11.40 SW Grab 4 t/- 2 deg C
Analyzed
Test Performed
Method
Results
Date Time Qualifier
Aluminum
EPA 200.8
0.245 mg1L
417/09 10:35
Copper
EPA 200.B
<0.007 mg/L
413/09 16:42
Iron
EPA 200.8
0.685 mg/L
4/3109 16:42
Zinc
EPA 200.8
0.024 mg/L
4/3109 16:42
Sample ID Date Sampled Time Sampled Matrix Sample Type Condition
13 SAND FILTER BACKWASH 4/1/2009 12:00 WW Grab 4 fl- 2 deg C
Analyzed
Test Performed
Method
Results
date Time Qualifier
Aluminum
EPA 200.8
<0.050 mg1L
413109 16:42
Copper
EPA 200.8
<0.007 mg1L
413109 16:42
Iron
EPA 200.8
0.013 mg/L
413109 16:42
Zinc
EPA 200.8
<0.010 mglL
4/3109 16:42
Sample ID Date Sampled Time Sampled Matrix Sample Type Condition
4 RO REJECT WATER 4/1/2009 11:50 WW Grab 4 +/- 2 deg C
Analyzed
Pest Performed
Method
Results
Date Time Qualifier
%luminum
EPA 200.8
<0.050 mg/L
413/09 16:42
.opper
EPA 200.8
<0.007 mg1L
413/09 16:42
ron
EPA 200.8
0,313 m IL
l3/09 16:42
,;Ink,
EPA 200.8
0.151 mg1L
4/3109 16.42

A r, 15. 2009 2:50FM Tr i test fax o No 2723 F. 4/4
� FE) T E5 " AMENDED REPORT
6701 Conference Drive Page 2 of 2
Raleigh, NC 27607
felephone: [phone] NCIWW Cert. #; 067
Fax: [phone] NCIDW Cert. #; 37731
Laboratory Report
Work Order k 0904-00313
Jo. Sample ID
Date Sampled
Time Sampled Matrix
Sample Type Condition
005' CONDENSATE WATER
411/2009
11:66 WW
Grab 4 +/- 2 deg C
Analyzed
Test Performed
Method
Results
Date Time Qualifier
Aluminum
EPA 200.8
<0.050 mg1L
413/09 16:42
Copper
EPA 200.8
<0.007 mg/L
413109 16:42
Iron
EPA 200.8
0.080 mg/L
413109 16:42
Zinc
EPA 200.6
<0.010 mg/L
413/09 16:42
AMENDED REPORT: CORRECTED DETECTION LIMIT ON COPPER. 04/15/09
Reviewed by, -
for

A�D`W Laboraton Section Wesutts
County:
NASH
Sample 10:
A1345417
River gas in
TAR
JJA
PO Number #
BW4994
Report To
RROSP
_r'.C'
O • v4
Date Received:
06/1012009
Time Received:
13:50
Coflector:
A HOB N
cr. ;rscr
LabworksLoginl0
HPARKER
Region:
RRO
�r
Y%
Date Reported:
711D109
Sample Matrix:
WASTEWATER
Loc. Type:
EFF� LET
Report Generated'.
07/1012009
Emergency Yes/No
COC Yes1No
VisitlD
Loc,Descr,: HOSPIRA01TSW
9/(Lp_
r
Location ID:
HOSPIRA017SW2
Collect Date: 06109/2009 Collect Time:: 12:45
Sample Depth
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to wtwv,dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-Estimated concentration is < PQL and >MDL
81-Countable membranes with �20 colonies; Estimated
NE -No established PQL
B2- Counts from all filters were zero.
P-Efevaled PQL due to matrix interference and/or sample dilution
83- Countable membranes with more than 6D or 80 colonies; Estimated
01-Holding time exceeded prior 10 receipt at lab,
84-Filters have Counts of both >BO or BD and c 20; EsGmaled
02- Holding time exceeded following receipt by lab
135-Tao many colortitis were present; too numerous to count (TNTC)
pQL-Practical Quantifation Limit -subject to change due to instrument sensitivity
J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated
U-Samples analyzed for this compound but not detected
J3-The sample matrix interfered with the abihly to make any accurate determination; Estimated
X 1-Semple not analyzed for this compound
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
WI -The component has been tentatively identified based on mass spectral library search and has an estimated value
LAB
Laboratory Section>> 1623 Malt Service Center, Raleigh, NC 27699.1623 [phone] Page 1 of 3
11

L
NC (DWQ La6oratory'Section 1Resufts sample ID A845417
Location ID: HOSPIRA017SW2 Collect Daia: 0610912039
Loc. Descr,: HOSPIRA 0i 7 SW Collect Time:: 12:45
visit ID
CAS x Analyte Name PQL Result ❑uallfipr Units Analyst/Dale Appraved By!Date
Sample temperature at recelpt by lab 2.9 'C DSAUNDFRS SMATHIS
!Atthod Reference W10109 Hn IM9
MET
7440-224
AQbyfCPMS
5
5.0
U
Up1L.
PGAUTHIER
ESTAFFORD
MelhodRefarance
EPA200.8
Wi8109
6r301D9
7429-90.5
At by ICP
50
120
ug1L
SGOSS
ESTAFFORD
Method Reference
EPA200.7
6118M
6l30mg
7440-38-2
As by ICPMS
2
2.0
U
uglL
PGAUTHIER
ESTAFFORD
Mothod Reference
EPA200.8
6/11109
6130f09
7440-38-3
Ida by tCP _
._..,
10
10
U
_ ug1L
SGOSS
.... ESTAFFORD
Method Reference
EPA 200.7
&17109
6130109
7440-41-7
Be by ICP
5
5.0
U
ua
SGOSS
ESTAFFORD
Method Reference
EPA 200.7
W1&09
6130109
7440-70-2
Ca by ICP
0.1
021
mg1L
SGOSS
ESTAFFORD
Method Reference
EPA 200.7
6117M
613W09
7440,43-9
Cd by ICPMS
-
T 1
1,0
U
LtWL
PGAUTHIER
ESTAFFORO
Method Reference
EPA200.8
6/1&09
6130/09
744048A Cobalt by ICP 50 50 U Ug1L SGOSS ESTAFFORD
Meuiod Reference EPA 200.7 6118r09 613=9
7440-47-3
or try ICPMS
10
10 U
UO&
PGAUTHIER
ESTAFFORD
Method Reference EPA 2MA
&ISM9
6130109
7440-50-8
Cu by ICPMS
2
2.0 U
UO&
PGAUTHIER
ESTAFFORD
Malhod Reference EPA 200.8
6118f09
6130109
7439-8S-6
Fe by ICP
50
420
ug/L
SGOSS
ESTAFFORD
Method Reference FPA20D.7
W78109
6r30f09
7439-97-6
Hg 245.1
0.2
020 U
ugfL
SGOSS
ESTAFFORO
Method Reference EPA 245.1 &11/09 W0106
7440-09-7 K by ICP 0.1 0.10 U mg/L. SGOSS ESTAFFORD
Method Reference EPA 2D0.7 &17M9 6130109
7439-93-2
1J ICP
25
25 U
ug&
SGOSS
ESTAFFORD
Method Reference
EPA 20D.7
W77109
6130AD9
7439-95-4
Mg by ICP
011
0.10 U
1119ti
SGOSS
ESTAFFORD
Method Reference
EPA 200.7
6/0M
1560109
7439-96-5
MnbyICP
10
15
uglL
SGOSS
ESTAFFORD
Method Reference
EPA 200.7
6118109
6130109
7439-98-7
Mo by ICPMS
10
10 U
ug1L
PGAUTHIER
ESTAFFORD
Mefd Reference
EPA 2008
6118109
6130109
Laboratory Section>> 1623 Maif Service Center. Raleigh, NC 27699-1623 1919) 733.3908 Page 2 of 3

NC tDWQ Laboratory Section Results Sample ID A645417
Location ID: HOSPIRA017SW2 Collect Date: 06l09=09
Loc. Descr.: HOSPIRA 017 SW Collect Time:: 12!45
Visit ID
CAS ff
Analyte Name
PQL
Result
Qualifier
Units
Analyst/Date
Approved By7Date
7440-23-5
Neby1CP
0.1
0.10
U
mipt
SGOSS
ESTAFFORD
Method Reference
EPA 200.7
6/17109
6/30109
7440-02-0
NI by ICPMS
10
10
U
ugfL
PGAUTHIER
ESTAFFORD
Method Reference
EPA 200,8
6119109
6130109
7439-92-1
Pb by ICPUS
10
10
U
1191L
PGAUTHIER
ESTAFFORD
Method Reference
EPA 200.8
6118109
6130109
7440-3E-0
Sb by ICPMS
10
10
U
uQ&
PGAUTHIER
ESTAFFORD
Method Reference
EPA 200.8
61t8109
6/30109
7782-49-2
Se by ICPMS
5
5.0
U
ug1L
PGAUTHIER
ESTAFFORD
Method Reference
EPA 200.E
611=9
6130109
7440-31-5
Sn by ICPMS
10
10
U
ug1L
PGAUTHIER
ESTAFFORD
Method Reference
EPA 2W0 8
6118109
613af09
7440-26-0
Thalllum (TO ICPMS
10
10
U
ug1L
PGAUTHIER
ESTAFFORD
Method Reference
EmA 200,8
8ri8109
W30/09
7440-32-6 TI (Titanium) by ICP 10 10 U LJWL SGOSS ESTAFFORD
Method Reference EPA 2C0.7 6r17109 613=9
744M2-2 VbyICP 25 25 U ug1L SGOSS ESTAFFORD
Method Reference EPA 200.7 6/18109 6130W
7440-66-6 ZnbyICPMS 10 10 U ug)L PGAUTHIER ESTAFFORO
Method Reference EPA 200,8 611 V09 6/30109
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone] Page 3 of 3

COUNTY J lJ 1. ✓ } I
RLVEA BASIN: -- !
e
REPORT TO G&I Regional Office
Other
COLLECTOR(S)
Estimated SOD Range:
qw H qq
DIVISION OF WATER QUALITY
Chemistry Laharatory Report! Water Quality
❑ SAMPLE TYPE
PRJOR
❑yAMSiENT ❑ QA ❑ S['RE.AA, EFFLUENT = �'�i
I�tT COMPLIANCE ❑ CHAIN OF CUSTODY ❑ LAKE ❑ I'NFLUEN T Iwi��
❑ EMERGENCY VfS�rfT R1� ESTUARY ^�
1� Station Lscatiar7
a: rQ �� /Std
Lab Number
Date Received
_ E 0
Tune Rcceiled
��
Receit,ed By
Date Released
Date Reported
Seed: Chlorinated: Remarks-. =7
P-WAf, -4-o 5 R 1 fv
Station rllLocation Code Date Begin (yylm dd) Dane End (yylmmld�y. Time Segln Time End Depth . DM. Do, DBM Value Type- M H, t- Camposile•T, S. D Sample Type
>� b�Oi� 0111 /)a 1 nca to no. (IZ6 1 �54 1-7-vi 1 v' lnll a2
BCD 310 mttlL
COD High 340 mg1L
COD Low 335 tn,'L.
Cohfornr MF Fecal31616 1100m)
Colifo=r MF Total 31504 1100ml
Colifor t: tube Fecal 31615 /100M
Colifarm: Fecai Strap 31673 f100m1
Residue: Total 500 mg/L
Volatile 505 mg/L
Fixed 510 mgtL
Residue: Suspended 530 mg/L
Volatile 535 mg/L
Fixed 540 mVL
pH 403 units
Acidity to p1f 4.5 436 mgfL
AtHiry to pH 8 3 435 mg/L
Alkalinity to pH 9.3 415 _81L.
Alkalinity to pH 4.5 410 mg/L
TOC 620 mgtL.
Turbidity 76 NTU
Caliform Total Tube 1100 ml
i
i
(1a4$PM 1
CMaride 940 mg/L
Chlorophyll a EPA445A modified option ug1L
Color: True 80 C.U.
Col PH) 83 PH. cu.
Color: pH 7.6 82 au,
Cyanide 720 mg/L
Fleofide 951 mg/L
Formaldehydc71880 m2/L
Grease and Oils 556 mg/L
Hardness Total 900 m81L,
Spmific Cond. 95 utnhostcrn
MBAS 39260 mg/L
rhenoLs 32730 ug/L
gulfete 945 mgfL
Sulfide 745 mg/L
Baron
Tannin & Ligtin up'L
Hcxavalenr Chromium ug/L
Bicarbonate mg/L
Carbonate mp/1.
Total Dissolved Solids mWL
n
NHS as N 610 milli,
TKN an N 625 mg/L
NO2 pl.. NO3 as N 63C n4vL
P; Total as P 665 m&IL
PO4 m r 70501 m8/1.
P� Dila01\rd as P 66 mgfL
-Potassium mgfL
Cd-Cadmium 1027 ug/L.
Cr.Ch romium:To lal 1034 u sIL
u- Capper 1042 u011.
Ni Nickel 1067 u#L
-pb- Lead 1051 up/L
Zn- Zinc 1092 u&IL
V_Vanadium ug/L
Ag= Silver 1077 uyrJL
AI -Aluminum 1105 uWL
Be- Beryllium 1012 vg1L
Ca- Calcium 916 mg/L
Co -Cobalt 1037 ugfL
25
Pe- Iron 1045 ur%L
Iv,a-F,al hdenum ug�L
Sb-Anlimony vi/i L
Sn-Tin ug/L
11-Thallium ug1L
Ti-Titanium ug1L
Hg• 1631 ng/L
COMMENTS:
— — _ —
Li -Lithium 1132 uwL
Mg- Magnesium 927 ing/L.
Mn-Mnlpnew 1055 ug/L.
Na. Sodium 920 mg/L
Arxnir.Toea11002 uglL
Se Selenium 1147 uglL
Hg• Mercury 71900 uWL
Sa-Barium up/L.
Organochlorine Pesticides
gp 0rnophosphoru s Pesticidra
Organonitrogen Pesticides
Acid Herbicides
Besd/itfeutrai&Acid Egractable Organics
TPH Diesel Range
Purgeable Orgattics (VOA bottle mq'd)
TPH Gasoline Range
TPH/BTEX Gasa1 ine Range
Phytoplankton
Temperature on arrival (n f

County:
NASH
River Basin
im
Report To
RROSP
Collector.
A HOBAN
Region-
RRO
Sample Matrix:
WASTEWATER
Loc. Type:
ELF IJEMT
Emergency YeslNo
COC Yes/No
Location ID: HOSPlRA017SW1
(C DW Laboraton Section &sults
Sample ID:
A845416
(?� 11A7-`F
PO Number
9W4993
Q
Date Received:
0611012009
Time Received:
13.50
Labworks LoginlD
HPARKER
`^t
Dale Reporled:
7110/09
Report Generated:
07110/2009
VesiUD
Loc. Descr.: HOSPIRA 017 5W
O a
Collect Date: 0610912009 I Colloct Time: 11:50 1Sample Depth
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab-org under Staff Access
A -Value reported is the average of two or more determinations
143-Estimated concentration is < POL and >MDL
B1-Counts ble membranes with Q0 colonies: Estimated
NE -No established POL
82. Counts from all fillers were zero.
83- Countable membranes with more than 60 or 60 colonies; Estimated P-Elevated POL due to matrix intederenca and/orsample dilution
Ba-Filters have counts of both �60 or 80 and c 20; Estimated 02- Holding Q7-Ho di g Utime
exceeded prior to
exceeded following
receipt at lab.
ng ing receipt by lab
BS-Too many colonies were present; too numerous to count (TNTC)
J2- Reported value failed to meet OC criteria for either precision or accuracy; Estimated POL- Practical analyzOuariled
f r this
Limit subject to change due to instrument tens tiviry
U-Samples analyzed for this compound but not detected
J3-The sample matrix interfered with the ability to make any accurate detennina0on; Estimated
XI- Sample not analyzed for this compound
J&The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
NI -The component has been tentatively identified based on mass spectral library search and has an estimated value
UAB
Laboratory Section>> 1623 Mail Service Center, Ralelgh, NC 27699-1623 [phone] Page 1 of 3

f
.NC OWQ Laboratory Section Kesults Sample ID A845416
Location tD: HOSPIRA017SW1 Collect Date: 0610912009
Loc. Descr.: HOSPIRA 017 SW Collect Time:: 11.50
Visit ID
CAS it Analyte Name PQL Result Qualifier Units Anelyst/Date Approved By 10ate
Sernpletemper=re at receipt by lab --�� — — 2.9 +� "C DSAUNDERS ^ SMATHIS — —
Mcihod Reference U10109 9111109
MIC
Gollfonh, MF Fecal In nquld t 3 01 CFUMOOmi NDEO CGRFEN
Method Reference APHA92220-20th G11=9 811mg
WET
Ion Chromatography
_TITL>=_
rng1L
AWILLIAMS
CGREEN
Method Reference
EPA 300.0
6123109
6nme
Ta1al DL%Wlvad Solids In liquid
12
492
Q2
mwL
ADEXTER
CGREEN
Method Reference
APHA2540C.18TH
5117109
6124139
Chlonde
1
16
mgR.
AWILLIAMS
CGREEN
Melhad Referencd
EPA 300.0
6123109
E126109
Fluoride
0.4
2.0
UP
mg/L
AWILLIAMS
CGREEN
Method Reference
EPA 300.0
N23109
W26MO
Sultate
2
190
mQIL
AWILLIAMS
CGREEN
Method Reference
EPA 300.0
6123109
6126M9
MET
7440-22.4 A8 by ICPMS
5
5.0
U
uglL
PGAUTHIER
ESTAFFORD
%whodReference
EPA200.8
6l18109
Sr3DM9
7429-g0-5 AI by ICP
50
1400
ug1L
SGOSS
ESTAFFORD
Method Reference
EPA 200.7
6718109
6730109
7440-38-2 As by ICPMS
2
2.0
U
ug1L
PGAUTHIER
ESTAFFORD
Melhad Relerence
EPA 200.E
Ulam9
6MM9
7440-38-3 6a by ICP 1n 65 VVI- SGOSS ESTAFFORD
Method Reference EPA 200.7 rdl7109 U30M
7440-41-7
Be by ICP
5
5.0 L!
ugA-
SGOSS
ESTAFFORD
McDtod Reference
EPA 200.7
3"18109
66c(
7440.70-2
Ca by ICP
0.1
20
mgh.
SGOSS
ESTAFFORD
Method Reference
EPA 2f10,7
6117M9
613=9
7440-43-9
Cd by ICPMS
1
1.0 U
UG&
PGAUTHIER
ESTAFFORD
Melhod Reference
EPA200.8
6113M
6rjw9
7440-48-4
Cobalt by ICP
50
50 U
U91L
SGOSS
ESTAFFORD
Method Reference
EPA 200,7
6118109
6103Ltl09
7440.47-3 Cr by ICPMS 10 10 U uv- PGAUTHIER ESTAFFORD
Method Reference EPA 200,8 6178109 efde7109
7440-SO-8 Cu by ICPMS 2 11 ug1L PGAUTHIER ESTAFFORC
Mothod Refarome EPA 200.8 6116109 6130/09
Laboratory Sectione> 1623 Mall Service Center, Raleigh, NC 27899.1623 [phone] Page 2 of 3

NC DWQ La6oratory Section R-esufts Sample ID gB4541 g
.Location ID: HOSP1RA017SL411 Collect Data: 0N0912009
Lot. Descr,: HOSP1RA 017 SIN Collect Time:: 11:50
Visit t0
CA5 # Anatyte Name PQL Result Qualifier Units AAalysVDate Approved By Cate
7439-89.6 Fe by ICP 50 6700 ug1L SGOSS ESTAFFORD
Method Reference EPA 200.7 6118f09 813=9
7439-97-6 Hg 245.1 0.2 0.20 U uOk SGOSS ESTAFFORD
Method Reference EPA 265.1 6111@9 6130109
7440-09-7 KbyICP 0.1 62 rhg/L SGOSS ESTAFFORD
Method Reference EPA 200.7 6117109 6130109
7439-93-2 LI ICP 25 25 U uglL SGOSS ESTAFFORD
WAlhod Relerence EPA 200.7 6117r89 6f30fa9
743E-95-4
Mg by ICP
0.1
5.2
MOL
SGOSS
ESTAFFORD
Metflod Relerence
EPA 200.7
6l17109
6130109
7439-96-5
Mn by ICP
10
170
ug7l.
SGOSS
ESTAFFORD
Method Reference
EPA 200,7
6118109
6130109
7439-98-7
MobyICPMS
10
10 U
uglt
PGAUTHIER
ESTAFFORD
Method Reference
EPA200.8
6118109
WOW
7440-23-5
NebyICP
0.1
100
m41L
SGOSS
ESTAFFORD
Method Reference
EPA 200,7
6117109
8r30I09
7440-02-0
NI by ICPMS
10
i0 U
uglL
PGAUTHIER
ESTAFFORD
Method Reference
EPA 200.8
61181139
5130109
7439-92-1 Pb by ICPMS 10 10 U ug1L PGAUTHIER ESTAFFORC
Melhod Reference EPA 200.8 6118109 6130109
7440-36-0
Sb by ICPMS
10
10
U
uglL
PGAUTHIER
ESTAFFORD
Method Reference
EPA 200.8
6f18f09
6130f09
7782-49-2
Se by ICPMS
5
5.0
U
uyL
PGAUTHIER
ESTAFFORD
Melhud Reference
EPA 200.8
6l18/09
6f10ro9
7440-31.5
Sn by ICPMS
10
10
U
u91
PGAUTHIER
ESTAFFORD
MethodReferenca
EPA 200.8
6118109
6l30f09
7440-28-0
Themum (q ICPMS
10
10
U
ugfL
PGAUTHIER
ESTAFFORD
Method Reference
EPA 200.8
6118M
6r30f09
7440-32-6
TI (%ntuln) by ICP
10
10
U
U91L
SGOSS
ESTAFFORD
Method Reference
EPA 200.7
6117109
Bf30109
7440-62-2
V by ICP
25
25
U
uglL
SGOSS
ESTAFFORD
Method Reference
EPA200.7
611&09
6130109
7440-66.6 Z 3 by ICPMS 10 48 ugR- PGAUTHIER ESTAFFORD
Method Reference EPA 20C.8 611 BM 8I30f09
Laboratory Section>> 1623 Mall Servlce Center, Raleigh, NC 27699-1623 [phone] Page 3 of 3

�wtlq`93
• ,
DIVISION OF WATER QUALITY
water
Number
NS f
Chesaistry Labaratary
Report ! Quality
11 Smpl& TYPE
Lb :
Due Rccei-d ;
}
- J D -09
COUNTY
RIVER OASIN :
MQ Y mac,
AMBIENT QA STR.EAM S M 'EFFLUENT L 7y !�
Time Recoiled:
Recciwd By
_ 2 SD
tj
aj
I!T
REPORT TO Re®ondOffice
�COMPLLSNCE C14ASNOFCUSTODY El LAKE � NFLUEhT
Othrr
EMERGENCY
V151T lD ESTUARY
Data Released :
COLLECTOR(S) : ne-f I
❑
Date Reported:
Estimated BUD Range:
Station Location:
Seed: Chlorinated:
Rem arlu.• +aRur,
D OIrJ�
_
�
S1a11a NAAcatioo Code
W6s5,0;hrq
Date Be �}^ (7y!
Idd)
'q
Dale End (rlmmldd)
Time Begin
Time End
ss
Depth - DM, DB, DBM
Value Type - A, H, L
CampositnT, S, B
Sample Type
O1?_5j/)1
P)gTl r
o9 Jo cc 10 4
I,11 0
1E=
e,ey w
BOD 3IU m911-
COD Fbgh 340 mr/L
COD Law 335 mnJL
Col iforro: MF Feeal 31616 f I DQmI
Caiifarm MFTotal 31504 1100m]
Coliform: tube Fecal 31615 1100m)
Colifarm: Fecal Strop 31673 AMani
Residue Total 500 mg/L
Volatile 505 MAIL
Fixed 510 mg1L
Rosiduc: Suspended 530 mg/L
Volatile 535 mg/L
Fixed 540 mRIL
pH 403 units
Acidity to pH 4.5 436 mafL..
Acidity io pH 8, 3 435 mWL
Ai'ralinity to pH 4.3 415 mg/L
Alka]inity to pH 4.5 410 mg/L
TOC 680 mg/L
Turbidity 76 NHJ
Colifornr Total Tube 11 10 ml
Chloride 940 MAIL
Chlarophylla EPA 445,0 modified option ug(L
Color: True 80 C.U. -
Calar.(pH) 83 pH• c.u_
Color: pH 7.6 82 (i-u.
Cyanide 72D MWL
Fluoride 951 mg/L
Farmaldchyde 71880 mr)I.
Grease and Oils S56 mg/L
Hardncas Total 900 mg/L.
Specific Cond. 95 umhoVcm
MBAs 38260 mgrL
Phenols 32730 ug/L
Sulfate 945 mg/L.
Sulfide 745 mg/L
Boron
Tannin & Lignin uj;rL,
HeXRWjCnt Chromium vg/L
Bicarbonate mg(L
Carbonate mglL
otal Dissolwd Solids mgfL
NH3 as N 610 -GIL
TKN an N 625 mg/L
NO2 plus NO3 as N 630 m9(L
P: Total as P 66S mgn-
PO4 as P 70507 oip/L
P: Dissolved as P 666 mgfL
K-potassium mrjl-
Cd-Cadmium 1027 ug/L
Cr-Chrornium.Toial 1034 ug/L
Cu. Copper 1042 og/L
Ni-Nick.] 1067 ug/1-
Pb-1,ead 1051 uWL
Zn-Zinc 1092 ug1L
V-Vanadium ua1L
A Silva 1077 uglL.
AI- Aluminum 1 105 ug/L
Be- BcgLlium 1012 vg/L
Ca- Cakium 916 mg/L
Co- Cobalt 1037 ugJ3-
Fe- Iran 1045 ugfl.
Mo-blolybdcnum ug'L
Sb-Antimony, ug/L
Sn-Tin ug/L
SZ
Tl-Thallium ug/L
Ti-Titanium ug/L
14g-1631 nFJL
Li -lithium 1132 ug/L
Mg Magpesium 927 m9/1-
Mis-Manpnese 1055 uy/L
Na- Sodium 929 mglL
AVseniv.Tozx[ 1002 ug1L
Se -Selenium 1147 UOLL
Hg- Mercury 71900 uSfL.
Ba-Barisvn u91L
Orlpnuchlorine Pesticides
Orpnophosphorus Pesticides
Organonilragen Pesticides
Acid Herbicides
Bwe/Neut:al&Acid Earactable Otpnics
TPH Diesel Range
Purg sble Organics (VOA battle r"'d)
TPH Gasoline Ran
TPWUT'ESL Gasalinc Ra ge
PhytaplanAton
Temperature an artival (°C): r

Report to: _KRO
NC DENRIDWQ I,aboratory
Sample Anomaly Report (SAR)
ab Number: AB45416 Sample ID: _Hospira 017SWI
•ation Location: Hospira 017 SW County: Nash Region: Raleigh
Sample Type: Effluent Priority: Compliance Collector: A,Hoban/D.Parnell
Date collected: 619109 Date received: 6/10/09 Date analyzed: 6/17/09
Affected Parameter(s)., TDS
Analytical Area (check one):
Mwat ❑METALS ❑VOA ❑SVOA
❑NUT ❑MICRO ❑PEST
The following anomalies occurred (check all that apply):
®Samples
❑improper container used
❑VOA vials with headspace
❑Sulfide samples with headspace
❑Samples not received, but listed on fieidshect
❑Samples received, but not listed on fieldshect
❑ abeled as to tests, preservatives, etc.
olding time expired
❑Prior to receipt in lab
®After receipt in lab
❑Insufficient quantity for analysis
[]Sample exhibits gross non -homogeneity
❑Sample not chemically preserved properly
❑pH out of range (record pVl):
❑Improper chemical
❑Residual chlorine present in sample
❑Color interference
❑Heavy emulsion formed during extraction
❑Sample bottle broken in lab - no reportable results
❑Other (specify):
❑Quality Control
❑Instrument failure— no reportable results
❑Analyst error— no reportable results
❑Surrogates
❑None added
❑Recovery outside acceptance limits
❑Spike recovery
❑None added
❑Recovery outside acceptance lirnits
❑Failed to meet criteria for precision
❑Internal standards
❑Blank contamination
❑QC data reported outside of controls (e.g., QCS, LCS)
❑Incorrect procedure used
❑SOP intentionally modified with QA and Branch Head
approval
❑Invalid instrument calibration
[]Elevated detection limits due to:
❑Insufficient sample volume
Comments: The sample was originally analyzed on 6-15-09 at 200m1. The found mg/L exceeded the acceptable limits. The result
was 2812mg/L, The sample needed to be rerun at a lower dilution. The sample was rerun at 50ml on 6-17-09 which was I day past
the holding time. The result on the second run was 492mg/L. Due to the large difference in results there was a possible contamination
during the initial run. The result found on 6-17-09 is the one being reported.
Corrective Action: Precautions will be taken to ensure there are no issues with contamination.
❑Samples were rejected by DWQ Lab. Authorized by: Date:
❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured.
❑Sample(s) on hold until
(V MSample reported with qualification. Data qualification code used:Q2
❑Other (explain):
Notification Required'? ❑ Yes ❑ No
Person Contacted: Date:
Form completed by: JAn ela Dexter{ JI 1"� W y Date: 6/23/2009
Lead Chemist Rev1 rnitia!}:
❑BIOCHEM ❑PEST [ISVOA
❑METALS ❑VOA
ich Head Review (init
JQC Review (I lial): ��R f�Cr togged into database by (initial): I z,//of
oA Forms'LaboraiorytiAR 10�73,01 dha

��77 ��}} NC DENRIDWQ Chemistry Laboratory
rt to: RR O 5P Sample Condition Uoon Receint Anomaly Reflort
I Lab Number: C
rmple M. T Station Location:
County: N q _ _ Region: 990
Collector: 0 Date collected: —1_! Qq Date received: T�IO 1 Q�
Priority: —jgue Sample Type: t? 4—'fuehi-
Affected Parameter(s):
The condition of these samples were not acceptable because (check all th apply):
a Coolers Samples (affected Samples are described below)
❑ Samples were not received on wet ice ❑ Samples not received, but listed on fieldsheet
❑ No temperature blank submitted (see comments): ❑ Samples received; but not listed on fieldsheet
❑ Sample To reading: _ °C O Samples not received, but listed on COC
❑ Cooler T° reading: 0C ❑ Samples received, but not listed on COC
❑ Temperature>b°C. T° reading: °C ❑ islabeled as to tests, preservatives, etc.
❑ Samples frozen H
Holding time expired Fad,A'
❑ Improper container used
❑ Containers ❑ Insufficient quantity for analysis
❑
Leaking
CI
Broken
❑ Chain of Custody
❑
Without labels
❑ No custody seals
o
VOA vials with headspacc
❑ Custody seals not intact
❑
Sulfide samples with headspace
❑ Not relinquished.
❑ No datehime relinquished
0 Container
Labels
❑ No signature
❑
Not the same IDlinfo. as on COC
❑ Incomplete information
❑
Not the same ID/info. as on fieldsheet
❑
Incomplete. Missing the following:
Ct Documentation
❑ .Station #/Sample ID
❑ Fieldsheet wet/illegible
Cl Collection date
❑ Fieldsheet incomplete:
• Collector
❑ Records not written in indelible ink
❑ Analysis
❑ Sample(s) submitted without fieldsheet
❑ Preservative
O Other:
❑ Other (specify):
O
Markings smeared or illegible
❑
Torn
Comments: A O '`
}�SPL'f,f- >r P e4"V : > -C I I'*"' c F4 g q5 y! CJ J.{.-f+/lr . /+L3 q
Corrective Action: ` fS Pt DEL)
`
❑ Samples were rejected by DWQ Lab. Authorized by: �`7
,% Accepted and analyzed per collector's request after notifying the collector. ✓
❑ Accepted and analyzed after notifying the client and determining that another sample could not be secured.
_ fl Sample(s) on hold until.
❑ Sample(s) accepted and analyzed. No notification required.
G Other (explain): II
Person Contacted: J Date: W l) a 1 a
Forth completed by:
Chemist Review (initial):
BIOCHEM ❑ VOA O PEST
❑ MET ❑ SVOA
Branch Head Review (initial):
QAlQC Review (initia 9 Logged into database by (initial): /1 % U
QANFnnnRSarrVIe Rcteivine\SCUR . ��t l ( V l Ian lmdl i

County
NASH
River Basin
j-5
Report To
RROSP
Collector:
A HOBAN
Region:
RAO
Sample Maulx.
WASTEWATER
Loc. Type:
EFFLUENT
Emergency YerdNo
COC YesINo
1 Location ID: HOSPIRASSW4
VisiBD
Loc. Descr.: HOSPIRA SSW
Collect Date: D6l091200 I Collect Time:: 14:35
Sample Qualifiers and Comments
Sample Ia:
A1345418
PO Number 0
9W4995
Date Recelved:
06/1012009
Time Received:
13160
Labworks LoginlD
HPARKER
Date Reported:
7f10lD9
Report Generated:
D711012009
�
� �
�09
Sample Depth
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-Estimated concentration is < POL and >MDL
61-Countable membranes with <20 colonies; Estimated
NE -No established POL
B2- Counts from all filters were zero,
P-Elevated POL due to matrix interference andlor sample dilution
83- Countable membranes with more than 6tl or 80 colonies; Estimated
B4-Filters have counts of both >60 or 80 and < 20: Estimated 01-Holding time exceeded prior to receipt at lab.
02- Holding time exceeded following receipt oy lab
95-Too many colonies were present; too numerous to taunt (TNTG)
POL- Practical Quantitation Limit-sub)ecl to change due to instrument sensitivity
J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated
J3-The sample matrix interfered with the ability to make any accurate tletemtination; Estimated W. Samples analyzed for this compound but not detected
.16-The lab analysis was from an unpreservtd or improperly them+tally preserved samplo} Estimated X1- Sample not analyzed for this compound
N 1-The component has been tentatively identified based on mass spectral library search and has al estimated value
LAB
Laboratory Snctlon>> 1623 Mall Service Center, Raleigh, NC 27699.1623 (919] 733-3900 Page t of 3

.i1r�' �`�f�Q La6arcctory Se,.:con 12esufts Sample lD Aga$4,,
location 10: HQSPIRASSWI Collect Date: 06109t2009
Loc. Descr.; HOSPIRA SSW Collect Time:: 14:35
Visi, ID
GAS it Analyte Name PQL Result Qualifier Units AnalysUDate Approved By 1Date
Semple tetnpiarwWre at to mipt by tab 2.13 D5AUNDEHS SMATHIS
Method Reference 61101p9 6111109
MIC
Conform, MF Fecal to Ilquld t 2000 B601 CFU1100ml NDEO CGREEN
Monad Referenca APHA9222D-20rh ru10+09 6116IN
MET
744D-22-4
AU by ICPMS
S
5.0
U
up1L
PGAUTHIER
ESTAFFORD
Method Reference
EPA200.8
608109
61=9
7429-90-5
AI by ICP
50
50
U
ug1L
SGOSS
ESTAFFORD
Method Reference
EPA260.7
U18109
6130109
7440-38-2
As by ICPMS
2
2.0
U
%IWL
PGAUTHIER
ESTAFFORD
Method Reference
EPA200.9
Ulm
6r30109
7440-38.3
Ba by ICP
10
25
uglL
SGOSS
ESTAFFORD
Method Refefence
EPA 200.7
6117109
W30109
7440-41-7
Be by ICP
5
5.0
U
ugR
SGOSS
ESTAFFORD
Meowd Relefence
EPA200.7
8r18109
W30109
7440-70-2
Ca by ICP
D.1
5.6
-9&
SGOSS
ESTAFFORO
Method Relereme
EPA 200.7
6117M
6r30fD9
7440 43.9
Cd by ICPMS
1
1.0
U
ug} l-
PGAUTHIER
ESTAFFORD
Method Reference
EPA200.8
6118f09
6rS0109
7440-48-4
Cobalt bylCP
50
50
U
uyL
SGOSS
ESTAFFORD
Method Relefence
EFA 200.7
611em
6130109
7440A7-3
Cr by ICPMS
10
10
U
LJO&
PGAUTHIER
ESTAFFORD
Method Reference
EPA 2W.8
611&t1S
613=9
7440-50-8
Cu by ICPMS
2
8.9
ugrL
PGAUTHIER
ESTAFFORD
Method Reference
EPA 2MA
vie=
613D109
7439-89-E
Fe by ICP
50
210
up1L
SGOSS
ESTAFFORO
MethodR9tetence
EPA200.7
611ef09
fitvw9
7439-97-6
Hg 245.1
0.2
020
U
U01L
SGOSS
ESTAFFORD
Method Re:efence
EPA 24S.1
U11109
6l301C9
7440-09-7
KbyICP
0.1
2.6
m91L
SGOSS
ESTAFFORD
Method Relerence
EPA200.7
U17,14
6130109
7439-93.2
11 ICP
25
25
U
u01t
SGOSS
ESTAFFORD
Method Reference
EPA 200.7
6117109
6014109
7439-95-4
Mg by ICP
0.1
2.0
m911-
SGOSS
ESTAFFORD
Method Reverence
EPA 200.7
6117109
6130109
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 {9191 733.3908 Page 2 of 3

NC (DWQ Laboratory Section Resufts Sample ID p8454 1 BB
Location ID: HOSPIRASSWI Collect Dew 0610912009
Lac. Descf.. HOSPIRA SSW Collect Time:: 14:35
Visit ID
GAS #
Analyto Name
PQL
Result
Quallfier
Units
Analyst/Date
Approved By Wate
7439-96-5
MnbyICP
10
17
uglL
SGOSS
ESTAFFORD
Method Reference
EPA200.7
NIM9
813C109
7439-9B-7
MobyICPMS
10
10
U
UWL
PGAUTHIER
ESTAFFORD
Method Reference
ERA200.8
6nW09
61=9
7440-23-5
Ne by ICP
0.1
33
UWL
SGOSS
ESTAFFORD
Melhod Reference
EPA 200.7
U17109
6130109
7440-02-0
NI by ICPMS
10
10
U
ug/L
PGAUTHIER
ESTAFFORD
McModReference
EPA MA
Sf19M9
%n0109
7439-92-1
Pb by ICPMS
10
10
U
ug/L
PGAUTHIER
ESTAFFORD
Method Reference
EPA 200.8
U18l09
W30109
7440-36-0
Sb by ICPMS
10
10
U
ugl L
PGAUTHIER
ESTAFFORD
Method Relerencee
£PA20u.e
wiew
W30109
7782-49-2
Se by ICPMS
5
5.0
U
u®IL
PGAUTHIER
ESTAFFORD
MethodRefarence
EPP,200.8
61181D9
Bf30109
7440-31-5
Sn by ICPMS
10
10
U
uglL
PGAUTHIER
ESTAFFOR❑
Method Reference
EPA 200.8
6118r09
6130109
7440-28-0
Thenlum (r� ICPMS
10
10
U
uglL
PGAUTHIER
ESTAFFORD
Metnnd Reference
EPA 200.8
WIV09
618o100
7440-32-6
71(Titanium) by ICP
10
10
U
uglL
SGOSS
ESTAFFORD
Method Reference
EPA 200.7
61171rj9
a0=9
7440-62-2
V by ICP
25
25
U
ugA-
SGOSS
ESTAFFORD
Method Reference
EPA200.7
6118109
6f90/09
7440-66-6
Zn by ICPMS
10
29
uglL
PGAUTHIER
ESTAFFORD
Method Reference
EPA 200.8
611n9
613C109
Laboratory Sectlon>> 1623 Mall Service Center, Raleigh, NC 27699-1623 1919) 733-3908 Page 3 of 3

4
DIVISION OF WATER QUALITY
1 ( 1
q w
AV,1
Chemistry 1-4b.-Wy Report I Wei— Qwllty
El SAMPLE TYPE
Lob
Date Received :
COUNTY JIr1�
I ✓��
rRM [mil'
��/
rune Received '
+
RIVER BASH;
AMS�NT
QA
STREAM
f ( EFFLUENT
Rcce'ned By
1
Hf
REPORTTO
Regional Office CO PLIANCE
CHAIN OF CUSTODY
LAKF
❑ iNFLUENT
Other
❑ EMERGENCY
VISIT ID
ESTIMARY
Data Rciczmd
COLLECTORS)t r
0
Dale Reported;
Ss!AEstimated
BOD Range:
Sutiea Location:
i`-C•6 O
Seed:
Cblarinarrd:
Remarks:
Staria`,a �r/Lecalion Code
Dat■ Rw�n ("mid
Dale End �` 7�mm1
Time Bgle
Tlme End Depth - DM, DB, DBAT
Value Type - A, 11, L
Composite-T, S• D
Sample Type
`lfil.s�, 2¢ $ S iJf 1
fM001.0.9 _
� ILUa 99
0 _3 S
: �o
-- _--
_
_--- -
HOD 3 10 mSIL
COD High 340 inpJL
COD Low 335 ngfL
Coliform: )dF Feea131616 /1 OOrrtl
Coliform: MF Total 31504 /100m1
Colifarm: tube Fecal 3 16 15 1100m1
Coliform: Fecal Strcp 31613 1100ml
Residue'.Tolet 500 mg1L
Volatile SOS mg1L
Fued 510 0`91.
Residue 5uspmded 530 m8/L
Volatirt 535 mg/L
Fixed 540 rn,JL
pH 403 units
Acidity to pH 4,5 436 mg/L
Acidity to pH 8.9 435 mglL
Allralin;rfw pH 8.3 415 mWL
Alkalinity to PH 4.5 410 mWL.
TOC 630 mSIL.
Turbidity 76 XT U
Colifarm Tora1 Tube /1 oo mr
Chloride 940 mpIL
Chlorophyll a EPA445.0modiSed option ug/L
Color: True 80 e.u.
Caror.(pH) 83 PH. C.U.
Color: pH T6 82 C.U.
Cyanide 720 mp/L
Fluoride 951 mg1L
Fnnt Wl hydc7188o mg/L
Grease and Oils 556 mg/L
Hardness Total 900 1,1911
Specific Card. 95 umhos/rrrt
MBAS 38260 mg/L
Phenols 32730 u�I.
Sulfate 945 mg l
Sulfide 745
Boron
Tannin & Ligtin uy/l,
Hexavwcnt Chromium ug/L
picarbonme mg/L
Carbonate mg+L
otal Dis:solvcd Solid. m8/L
NW as N 610 m8/L
TKN ein N 625 mg/L
1402 plus NOI as N 630 rlv%
P: TUia1 a P 665 rMA
PO4 w P 70507 mg/L
P: Dissolved as P 666 nig/L
K-Palris.ivm mR/l-
Cd- Cadmium 1027 ug/L
Cr-Chromium-Toid 1034 ug/L
Cu. Capper !042 ug/L•
Ni-Nickel 1067 ug/L
Pb- Lead 1051 ug/L
Za-Zinc 1092 up/L
V-Vanadium u11/L
Ag• Silver 1077 uS/L
AI -Aluminum 1105 ug1L
Be- 11tu.T 1012 aSi
Ca- Calcium 916 mg/L
ly
Cc -Cabals 1037 up/L
Fe tron 1045 ug/L
Mo-Molybdcnum uWL
Sh-Antimorry ug/L
Sn-Tin uSfL
TI•Thallium ug/L
re Titaniurn ug/L
lig-1631 ag/L
Li-Lilhium 1132 uS/L
MR.M esitint 927 mpfL
Mn-Manganese 1055 ug/L
Na- Sodium 929 mg/L
Arsenic Tota11002 ug/L•
Se Sefenium 1 N7 vefL
Hg-.Mercury 71900 uE/L
Do -Barium u81L
Organochlerine Pesticides
Organophosphorus Festicidn
Organonitrom Pesticides
Acid Herbicides
Raso/Neutral&Acid F-rdractahle Organics
TPH Diesel Range
Purgeable Organics ( VOA battle re 'd)
TPH Gasoline Raagc
TPH/BTEX Gasoline Range
Phytoplanlcton
TemrieratureonenivalCi°C)- cJ
COklh1ENT5: �1Y1" -' 0357

� NC DENRIDWQ Chemistry Laboratory
R s
to: Sample Condition Unon Receint Anomaly Renort
Lab Number: i <
ample ID: 3— — Station Location: I ]�i� i J
County: NQ�C y _ Region: — p _ — ---
ColIector: A+J Data ca]Eected:l i ! Oq Date received:01
Priority: [}�1 �iQi_C' Fi _ Sample Type: L
Affected Parameter(s):
The condition of these samples were not acceptable because (check 7k=reccived,
0 Coolers d samples are described below)
❑ Samples were not received on wet ice but listed on fieldshect
❑ No temperature blank submitted (see comments): ❑ Samples received, but not listed on fieldsheet
❑ Sample T° reading: °C ❑ Samples not received, but listed on COG
❑ Cooler T° reading: °C ❑ Samples received, but not listed on COC
❑ Temperature >6°C. T° reading: °C O islabeled as to tests, preservatives, etc,
❑ Samples frozen Holding time expired f et�A �
❑ Improper container used
❑ Containers 0 Insufficient quantity for analysis
❑
Leaking
❑
Broken
❑ Chain of Custody
❑
Without labels
❑ No custody seals
❑
VOA vials with headspace
U Custody seals not intact
❑
Sulfide samples with headspace
❑ Not relinquished.
❑ No date/time relinquished
❑ Container
Labels
❑ No signature
❑
Not the same ID/info. as on COC
❑ Incomplete information
❑
Not the same ID/info. as on fieldsheet
❑
Incomplete. Missing the following:
❑ Documentation
d ,Station #/Sample ID
D Fieldsheet wet/illegible
a Collection date
❑ Fieldsheet incomplete:
p Collector
❑ Records not written in indelible ink
❑ Analysis
❑ Sample(s) submitted without fteldsheet
O Preservative
❑ Other:
❑ Other (specify):
❑
Markings smeared or illegible
❑
Torn
Comments: # f jale -_tic r lA& Vehp al:� lA-1;TL tJ a- —1 W
(rye (r (=AV d r`d i 60-)& —Cc e , alp I .t•��m de Uy Ar 4i44,t-t k aAA,
F-- Agg5-�-11G rum �2t:�.�.�—� /+
Corrective Acfion�Q�� tit��iCX�__ty4t- �
Cl
0
Samples were rejected by DWQ Lab, Authorized by:
Accepted and analyzed per collector's request after notifying the collector. f
Accepted and analyzed after notifying the client and determining that another sample could not be secured.
Sample(s) on hold until:
Sample(s) accepted and analyzed. No notification required.
Other (explain):
Person Contacted; 1 Date: l� _ / t)
Form completed by: aji— Date:
L Chemist Review (initial):
BfOCHEtvI 0 VOA ❑ PEST
❑ MET U SVOA
Branch Head Rcview (initial}:
QPJQC Acvinv (inilis Logged into database by (initial):
QA%Fon \Sample Her Mrg\SCUrt �. (/U f 101J T10l dd

S`
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
August 23, 2002
RUSSELL A GALL
ABBOTT LABORATORII S - RM l
PO BOX 2226
ROCKY MOUNT, NC 27802
Alan W. Klimek, P.E., Director
Division of Water Quality
N CCU—o6p "
Subject: NPDES Stormwater Permit Renewal
Abbott Laboratories - RM 1
COC Number NCG0600 4343 -
Nash County L--
Dear Permittee:
In response to your renewal application for continued coverage under general permit NCG060000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued
pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1993.
The following information is included with your permit package:
A new Certificate of Coverage
A copy of General Stormwater Permit NCG060000
A copy of a Technical Bulletin for the general permit
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or
decree.
If you have any questions regarding this permit package please contact Aisha Lau of the Central Office Stormwater
and General Permits Unit at [phone], ext. 578
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Stormwater & General Permits Unit Files
Raleigh Regional Office
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699.1617 [phone]
MA`
CD NENR
Customer Service
1-800.623-7748

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Gregory J. Thorpe, Phil.
Acting Director
Division of Water Quality
December 27.2001
RUSS GALL
A1313O7F LA13ORA'1'OR1i'S
PO 13OX 2220
ROCKY MOUNT, NC 27502
Subject: Nli Stor'nlwatcr Permit Rcnewad
ABI30-1-I' I_A13ORA'F(-.)RfhS
CC)C Number NCG060034
Nash County,
Dour Pcrnlillcc:
Your Facility is currently covered kW Slor'nlwater dischar�1'c under Gcncral Permit NCG060001l. This Iper11111 expires
on August 31, 2002. The Division stall is Cur'rCnlly in the process oFrewriting this permit and is tichcolulcc] tut have
the pClnlit [CISSUCd by ]ale sununcr of 2002. Once the permit is I-CISSUCd. your' kIcility would he Uligfhlc lilt
C(lrlllnUed CQVCragC Underthe rCiSsued perillrl.
In order to assure your continued Cove;ratIC under the «Cncral per-1110, YOU must apply to the Division of Water
Quality (DWQ) for 1-elicw,11 ol, your I)CI-nlit cnvcrM1a TO imtkc (his renewal process easier, We arC infurnrinkl Y01.1 in
advance Ii Ynur permit Will he expiring. 1 nclosed you Will Find a (:eneral Permit Coverage Renewal
Application Form. The application nitsst he cnnlplCled and rcturncd by March 4, 2002 in order to assur-C Continued
CrnTrage under the gencral permit.
Failure to reyuCst rcncW,tl Within this tinlC period may result in a Civil assessment of al lutist $250.00. Larger
pUWIltics Inay he asSCSscd dcpcnding nn the dclinyucncy ol'the recluest. Dischar,gc of slormw,itcr li'onl your facility
Witlloul coverage under a valid stormwater NPDES permit Would conslitute a violation of NCGS 143-215.1 and
could result in USSCssnlcntS oFCivil penalties nF up to $10.000 per day.
['lease note that reccnl Fcdcnd legislation has extended the ,no exposure Cxclusinn" to all nperators ol' industrial
Facilities in any o1 the I I calcgories of "Sloan water discharges associates] With industrial activity." (cxccpl
constl'uclion activities). Il'you I-CCI your Facility c,ul CUrtily a condition of "no expOSUre", i.e. 111c Facilly industrial
Materials and operatinlls arc not C'Xi to sulrnlwater, you can apply For the r1n CxposurC Cxclusion. For aildilionol
inCornuuion Contact the Ccnlral Office Slornlwater StaFF nlcnlhcr I15ICd below or Check the StormwatCr & Gcncral
Permits Unit NVch Site at httpa/h2o.enrstatU.nc.ushu/slornn+,nCrJltml
11'the subject slurnlwater discharte to Waters o1-the slale has been terminated. please corllploc [Ile enclosed
Rescission Reoluest Form. Ivlailin-T instructions tiro liStcd or1 the bottom o l'the Form- You will he notilied when the
rescission pr0CCSS IRIS peen corllpletcd.
ll you have any questions regarding the permit renewal procedures please contact Joe Alhiston of the Raleigh
Regional 011icc,it r)19-571-4700 or Aisha [.,till oFthe Central OlYlue Storrnwatcr Unit at (919) 733-5W3, ext. 575
Sincerely.
131-arllcy 13C1111cu. Supervisor
Strn-111wa1Ur and Gcncral PCI-IrlitS Unit
cc: Central Files
Raleigh Rektiorlal Office
e�A
NCDENR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

State of North'Carolina
!.. Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Jerry Leedy
Abbott Laboratories
One Abbott Park
Abbott Park, IL 60064
Dear Mr. Leedy:
May 14, 1993 R � C Vti";� D
AIRY 1 8 1993
DERNR-RAL IUD
Subject: General Permit No. NCG060000
Abbott Laboratories-RM1
COC NCGO60034
Nash County
In accordance with your application for discharge permit received on September 29, 1992, we are
forwarding herewith the subject certificate of coverage to discharge under the subject state - NPDES general
permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the
Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated
December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please. take. notice. that this certificate. of coverage is. not transferable. except after notice. to the. Division
of Environmental Management. The Division of Environmental Management may require modification or
revocation and reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area
Management Act or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Mr. Bill Mills at telephone number 919/733-
5083.
cc:
Sincerely,
Original Signed By
Coleen H. Sullins
A. Preston Howard, Jr„ P. E.
Raleigh Regional Office
Pollution Prevention Pap
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
STORMWATER DISCHARGES
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
Abbott Laboratories
is hereby authorized to discharge stormwater from a facility located at
Abbott Laboratories - RM 1
6.2 miles north of Rocky Mount, US Hwy 301
Rocky Mount
Nash County
to receiving waters designated as Beech Branch in the Tar -Pamlico River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III
and IV of General Permit No. NCGO60000 as attached.
This certificate of coverage shall become effective May 14, 1993.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day May 14, 1993.
Original Signed By
Coleen M. Sullins
A. Preston Howard, Jr., P.E., Director
Division of Environmental Management
By Authority of the Environmental Management Commission

VABBOTT
`C LABORATORLES-RM1
3992
2'30rI
• 4�� ri 1 � ,:�- � `�� Davis- Cem
0 _Ij
3991
',
if
Cem
130- 1! 1lrf 0
127
Z" 1" /J11
NORTH CAROLINA % ^ .tiiE'i 3989
ESLEYAN COLLEG -_��/
1 n i1.3s�Iro (zl
�O-\ I
' f - ' �� M r �I r 3988DOOm.N.
130
/01
\/,�• �`' `\ /off Slat\ vPatrOl e tr f ^120
i /
7'3011 ,,.{-' ,•IJ JD . r' 250 4 iITMOR—GEOLOGICAL SURVEY vrASFrrrvGTdrv,o C-196'e• 6 00'
l7
N N / '4J
251000m E.
I MILE ROAD CLASSIFICATION °per
a
Heavy-duty ___. _ Light -duty..
Medium-duty—��__ Unimproved dirt
00
U. S. Route State Route
N C
r' DRAKE, N. C.

NC®ENR
North Carolina Department of Environment and Natural Resources
Pat McCrory
Governor
Mr. W. Eric Ferrell
EHS Specialist
Hospira, Inc.
4285 N Wesleyan Blvd
Rocky Mount, NC 27804
Dear Mr. Ferrell:
Division of Water Quality
Charles Wakild, P.E.
Director
March 8, 2013
John Skvarla, III
--Secretary
2013
Subject: Rescission of Stormwater Permit NCG060035
Clarification of Coverage for Permit NCG060034
Hospira, Inc. -- Rocky Mount
Nash County
On 2/8/2013, the Division of Water Quality received your request to rescind your organization's
stormwater permit coverage under Certificate of Coverage Number NCG020774. In accordance with your
request, Certificate of Coverage Number NCG060035 is rescinded effective immediately.
In your letter of April 20, you also requested that your certificate of coverage for NCG060034 be
renewed. NCG060034 was renewed as noted in our letter to Marty Nealey on December 4, 2012.
Unfortunately, the renewal was in a routinely -scheduled renewal process and was not coordinated with
your request to cover plants R I and R2 under the same permit. Therefore, I have attached a revised
"Certificate of Coverage" for your facility that makes it clear that plants R I and R2 are both covered
under the same permit. We appreciate the efforts you have made to cover both facilities under one
Stormwater Pollution Prevention Plan.
If you have questions about this matter, please contact Boyd DeVane at 919 807-6373, or the Water
Quality staff in our Raleigh Regional Office at 919-791-4200.
Sincerely,
0.
for Charles Wakild, P.E., Director
cc: Raleigh Regional Office
Stormwater Permitting Unit
DWQ Central Files - w/attachments
Fran McPherson, DWQ Budget Office
Wetlands and Stormwater Branch
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Rafeigh, North Carolina 27604
Phono: 919-807-63001 FAX: [phone]
latemet: www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Acfion Employer
One
NorthCarolina

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG060000
CERTIFICATE OF COVERAGE No. NCG060034
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Hospira, Inc
is hereby authorized to discharge stormwater from a facility located at
Hospira — Plants RI & R2
4285 N. Wesleyan Blvd.
Rocky Mount
Nash County
to receiving waters designated as Beech Branch, a class B; NSW water in the Tar -Pamlico Basin,
in accordance with the effluent limitations, monitoring requirements, and other conditions set
forth in Parts I, 11, III, IV, V, and VI of General Permit No. NCG060000 as attached.
This certificate of coverage became effective December 4, 2012 but modified to include both
plants in NCG060034 on March 8, 2013.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day March 8, 2013
for Charles Wakild, P.E., Director
Division of Water Quality
By the Authority of the Environmental Management Commission