NCG030465_MONITORING INFO_20190218

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT N0.
Iv U, p30ylp 5
DOC TYPE
❑HISTORICAL FILE
L� MONITORING REPORTS
DOC DATE
❑ :)bl7 Da ) "
YYYYMMDD

A SMOGREENVILLE OF NORTH CAROLINA, INC
1125 Sugg Pkwy. PHONE [phone]
GREENVILLE, NC 27834 FAX [phone]
February 7, 2019
NCDEQ- Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
f EECFN
FFe 18 �
7.019
CEN�wR �C"JL&'
rJoN
Please find attached the semi-annual storm water discharge monitoring reports and analytical
results for period 1 & 2 in 2018, for ASMO Greenville of North Carolina, Inc., COC
NCG030465.
Under our facility's general NPDES general storm water permit NCG030000, effective
December 4, 2012, we are required to submit quantitative results for two rainfall events
annually on Outfall #1. We must record and keep on file for inspection qualitative results semi-
annually.
In April 2018, we requested a meeting with DWQ to evaluate a second retention pond built for a
plant addition. The results of the meeting added a second outfall to our sampling parameters.
Included in this submittal are the results of this sampling.
Our storm water permit was re -issued and effective November 2018 and we are now sampling
to the new requirements.
If you have any questions pertaining to this submittal, please give me a call at 252-754-1765.
Sincerely,
Pam Savage
Environmental Health & Safety
Attachments

.* 1
STORMWATER DISCHARGE OUTFALL (SDO)
ANNUAL SUMMARY DATA MONITORING REPORT (DMR)1 SPPP Annual Update DATA REVIEW FORM
Calendar Year -�2- 01 R
Individual NPDES Permit No. NCSI 0II 311011011011 t)l or
Certificate of Coverage (COC) No. NCG❑D ❑3 DIP]
This monitoring report summary of the calendar year should be kept on file on -site with the facility SPPP.
Facility Name: A<- Y U 6i'.Pg,,myt f �
County: 11/7'f-
Phone Number: (o'S'D- /71oS Total no. of SDOs monitored AS�-
Outfall No. I
Is this outfall currently in Tier 2 (monitored monthly)? Yes [� No ❑
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes [ No ❑
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWO to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No [�
Parameter, (units)
Total
Rainfall,
inches
j 5
�/''��.� �
}��-7hI�
CS� r/,�Ir 10
O /W
Cm
/
Wt/l
Benchmark
N/A
/ p D
(o -
1
0.007
O.030
0, 0 (o
Date Sample
Collected,
mmlddlyy
r .;
t
,,
(A;
0.30
.00
6-
<S oo
a. a
40. 063
0.
a
l Z .00
_
L S_. dv
L
LO . oo
O .0 k
10 ! lgw
0,9-5
SIDS I/
< . Ov
0.06S
LO,a v0
0,/US
(! j 3 i kI
�2. S
Z 0.O
S7 -3
< S 00
4 o .02
< 0 , 00s-
O .
Iz zr
0,
a��
5.
LS. 00
0.0103
O- 0011ei
O. 3 7�
SWU-264 - Generic Annual DMR
Last revised 5/02/2018

Additional Outfall Attachment
Outfall No. 0-
Is this outfall currently in Tier 2 (monitored monthly)? Yes ►Q1" No ❑
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No Fo
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No D
Parameter, (units)
Total
Rainfall,
inches
�" •2)
�1�vich�{,
C� -�
U 1
Benchmark
N/A
/O 0
/SS
0 . CJJ7
0.030
0.06 17
Date Sample
Collected,
4
3 Y i
mmldd/yY
3 -
7 /8r
J
<14,
Z-sC)0
Z-D Vos-
4D.vo3
z-0 0/0
10 1?
L , (7
s-
, S• 00
I 1<0. 00.5 00
Z- D 0/00
1 G 0 0 Z-00
///3 l�r
a -
a-0
7
,00
4 p.aaS-
1 Lo. Dos
01
lza r e
0, 5-0
s. r7
S b
4 0
1 o. 002-10
140 • Dolvo
o, oS70
SWU-264 - Generic Annual DMR
Last revised 5/02/2018
4 • -'oy

"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Signature
Date ? ,4Z-V 5�
For questions, contact your local Regional Office:
DWQ Regional Office Contact Information:
EVILLE REGIONAL OF
2090 US Highway 70
Swannanoa, NC 28778
[phone]
RALEIGH REGIONAL OFFICE
3800 Barrett Drive
Raleigh, NC 27609
[phone]
WINSTON-SALEM REGIONAL OFFICE
450 Hanes Mill Rd, Suite 300
Winston-Salem, NC 27105
[phone]
FAYETTEVILLE REGIONAL OFFICE
225 Green Street
Systel Building Suite 714
Fayetteville, NC 28301-5043
[phone]
6HINGTON REGIONAL OFFI
943 Washington Square Mall
Washington, NC 27889
[phone]
1617 Mail Service Center
Raleigh, NC 27699-1617
[phone]
MOORESVILLE REGIONAL OFFICI
610 East Center Avenue/Suite 301
Mooresville, NC 28115
[phone]
LMINGTON REGIONAL OFF14
127 Cardinal Drive Extension
Wilmington, NC 28405-2845
[phone]
"To preserve, protect
and enhance
North Carolinas water._."
SWU-264 - Generic Annual DMR
Last revised W212018

�VMICROBAC'a.
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0697
ASMO Greenville of NC INC Project Name: Stormwater Sample - Mthly, Outfall
1
Ms. Pam Savage Project 1 PO Number: NIA
1125 Sugg Parkway Received: 01/25/2018
Greenville, NC 27834 Reported: 02/06/2018
Case Narrative
Field pH(by client): 6-7 by paper
Analytical Testing Parameters
Client Sample ID: OF #1, grab
Sample Matrix: Aqueous Collected By: Savage
Lab Sample ID: K8A0697-01 Collection Date: 01/23/2018 14:30
Wet Chemistry
Method: EPA 1664 Rev. B
Oil 8 Grease (SGT-HEM)
Method: SM 2540 D-2011
Total Suspended Solids
Result RL
<5.00 5.00
5.00 2.63
Units Note Prepared Analyzed Lab
mg1L 01/30/18 0930 FAY
mglL
01126/18 1356 FAY
Metals
Result
RL
Units Note
Prepared
Analyzed
Lab
Method: Metals AqueouslEPA 200.7 Rev 4.4 1994
Copper
<0.005
0.005
mglL
02 O5118 1714
02105/18 1714
FAY
Lead
<0.003
0.003
mglL
02105/18 1714
02105/18 1714
FAY
Zinc
0.487
0.010
mglL
02/05/18 1714
OV05118 1714
FAY
Laboratory
FAY. Microbac Laboratories, Inc. - Fayetteville
Definitions
RL: Reporting Limit
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
North Carolina
DENR NPDES
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By:
Bonnie K. Sanders
Senior Project Manager
[e-mail]
02J0612018 23:11
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 2

Fayetteville Division 2582 Dope Mllis Road - Fayetteville, NC 28306 (910) 864-19201 "�- ---
P 1 } K8A0697*
CHAIN OF CUSTODY RECORD
CLIENT NAME& ADDRESS:
145070 _ 016
01 93q
PDf!
PROJECT? LOCATION:
LLU
O
m
O
TYPE
OF
ANALYSIS
PRESERVATION (CODE)
iI�
�
2.
�
CODE: A = None
B = HNO3 (pH<2) + <6'0
C = H2SO4 (pH<2) + <6'C
D = NaOH + <6'C
E = ZN Acetate + <6•C
F ; }ICI
Sodium Thio
CONTACT PERSON: , f
r
f� Ajv-1 V �C�
PHONE: _ �7 r
9AMPLEO aY;Sa
OATS 1 METROO pF SHIPMENT:
LAR ID #
SAMPLE
TYPE
DATE
TIME
Camp
GRAB
PH
FLOW
TEMP -C
REs.
CHLORINE
SULFIDE
Lan
iellnqul lry j
Dase
Tlma
Aeceiv • {Signature)
Date
Time
3.30
�ht pa4d�--- 2
M 30
Rd
4111nqu
Dale .q
Time
Ree! a 6 Qnalurei
41
oila CJ
Time
d by;
Dale
Time
Received hy: (5 Qnalure)
Dale
Time
5
6
-
ph Field: ph Field:
Temp Field 1: Tamp Fleld 2:
Water Level #1
Water Level #2
InlClals—� �1�
Turnaround time: REGULAR RUSH
Comments or Special Hazards; G
kk4/", (- �.J—
IS DATA FOR REG, COMPLIANCE PURPOSE?
NO- YES _WHICH:
IQC-Go3UDd ; NCG 0 30'-((05

(VMICROBAC''
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8G0019
ASMO Greenville of NC INC Project Name: Stormwater Sample - Mthly, Outfall
1
Ms. Pam Savage Project i PO Number, NIA
1125 Sugg Parkway Received: 07/03/2018
Greenville, NC 27834 Reported: 07/18/2018
Analytical Testing Parameters
Client Sample ID: OF 41, grab
Sample Matrix: Aqueous Collected By: Savage
Lab Sample ID: K8G0019.01 Collection Date: 07/02/2018 16:30
Wet Chemistry
Result
RL
Units
Note Prepared
Analyzed
Analyst
Method: EPA 1664 Rev. B
Oil & Grease (SGT-HEM)
<5.00
5.00
mg1L
07/16/18 1252
TAB
Method: SM 2540 D-2011
Total Suspended Solids
12.0
10.0
mglL
07/06118 1021
TAB
Method: SM 4500 H+B-2011
pH at 25 °C
5.9
1.0
pH Units
H
07/05/18 0948
TAB
Metals
Result
RL
Units
Note Prepared
Analyzed
Analyst
Method: Metals AqueouslEPA 200.7 Rev 4.4 1994
Copper
<0.005
0.005
mglL
07/11/18 1224
07/11/18 1224
TAB
Lead
<0.003
0.003
mglL
07/11/18 1224
07/11118 1224
TAB
Zinc
0.038
0.010
mglL
07/11/18 1224
07/11/18 1224
TAB
Definitions
H: Analyte was prepared and/or analyzed outside of the analytical method holding time
RL: Reporting Limit
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11 North Carolina DENR NPDES
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By:
�eolLlLd- e— �f� Pi1�4 L2�-1k—
Jeanne Overstreet
Client Relationship Specialist, Environmental
[e-mail]
07/1812018 1212
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 2

Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 26306 [phone] / "
CHAIN OF CUSTODY RECORD
f]+TNAME &ADDDAEss: r
'jr
=rr, •� �[[rrtt l� ' J
.lJ(L{ �/
'cz -7Y �q!
Pp I!
PItOJECrILOCATION' n ' r\
Pvr V L
W
�
O
m
O
TYPE
OF
ANALYSIS
PRESERVATION (CODE)
�,D
Q
_
�J
��+
V !SV
� v
11;
y
�
GDOE: A = None
S = HNO3 (pH<2) + <6°C
C = H2SO4 (pH<2) + <6"C
0 = NaOH + <6'C
F = zN Acetate + <6'C
F = HCI
G = Sodium Thlo
CONTACT PERSON:
� ~' 1 L� �� `— -F xfP 1
PHONE:
�7 7
pC �• j'� C ��
MALED er:
0 , �' C
BATE I METHOD OF SENT:
/ HI gnu (-ar
'
LAS ID
SAMPLE TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
TEi.1P'O
CHLORINE
SULFIDE
L'
5 ( )Rm t. ! tin
S
.
• 7
Late
Inqul3bed by;
1
Date
7-5-4
Time
c1.'o�'
Ived by: ISIQnaly
cl �1)� 2
Dale
J. 3. k8
Time
oct.V(1
Ibqu b>e Y.
Date n
-3`rg
Tim@ /�
R vad S pnaturel
Dale
7 I
Tlma r
1ffdt3
I 1
d'
1.
inqu sdled by: /f
Dale
71me
Rees ved try. (5 g�iture]
Dale
Time
s
ph Field: L — L_ ph Field. -
Temp Fleld 1: b,4 Temp Field 2:
Q�
Water Level #1
Water Level #2
iniriats--*-
Tumaround time: REGULAR RUSH
Comments or Special Hazards:
f2P-ak.C1tS Io �� va c Q�Sr�tQ_�ic�_Ccowl
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES ;WHICH: Sr�2vt�u!��� IPr`-- ( r
Page 2 of 2

Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8G0020
ASMO Greenville of NC INC Project Name: Stormwater Sample - Mthly, Outfall
2
Ms. Pam Savage Project / PO Number: NIA
1125 Sugg Parkway Received: 07/03/2018
Greenville, NC 27834 Reported: 07/18/2018
Analytical Testing Parameters
Client Sample ID: OF 42, grab
Sample Matrix: Aqueous Collected By: Savage
Lab Sample ID: KW0020-01 Collection Date: 07/02/2018 16:25
Wet Chemistry
Method: EPA 1664 Rev. B
Oil & Grease (SGT-HEM)
Method: SM 2540 D-2011
Total Suspended Solids
Method: SM 4500 H+B-2011
pH at 25 °C
Result RL
<5.00 5.00
Units
Note
Prepared Analyzed
Analy
mg/L
Al2
07116/18 1252
TAB
<4,17 4.17 mg1L
6.2 1.0 pH Units H
07106/18 1021 TAB
07/05/18 0948 TAB
Metals
Result
RL
Units
Note Prepared
Analyzed
Analyst
Method: Metals Aqueous/EPA 200.7 Rev 4.4 1994
Copper
<0.005
0.005
mg/L
07/11/18 1228
07/11/18 1228
TAB
Lead
<0.003
0.003
mg/L
07/11/18 1228
07/11/18 1228
TAB
Zinc
<0.010
0.010
mg1L
07111/18 1228
07111/18 1228
TAB
Definitions
Al2: MSIMSD fail recovery, but the LCS passes criteria.
H: Analyte was prepared and/or analyzed outside of the analytical method holding time
RL: Reporting Limit
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11 North Carolina DENR NPDES
Report Comments
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to �y
applicable accreditation standard unless otherwise noted. ::?lL�L1c� CJL PiLdZ, -4-1-
The data and information on this, and other accompanying documents, represents Jeanne Overstreet
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included. Client Relationship Specialist, Environmental
[e-mail]
07/1812018 12:13
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com Page 1 of 2

Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 [phone] / 8C
I '� R B A � K8G0020=
CHAIN OF CUSTODY RECORD
F
:LIENTNAME 6ADDRp55:
�JYY�C�y
I (2i i tV - .,
I
T Q i�►1 v {� �]�
PO If
PROJECT 1LDCATIDN:
_3
p
Ca
O
TYPE
OF
ANALYSIS
PRESERVATION (CODE)
th1—)
i
V
�'
`
T, `
l,V
G l7pE: A= None
9 = HNO3 (pH<2) t <6eC
C = H2SO4 (pH<2) + <6°C
D = NaOH + -c6'C
E = ZN Acetate + <6'C
F = HCI
G =Sodium Thla
CON7gC7 pERSDH: -
PHON�}E: r ((� r /
'� J `"1 7 �'�
IAMPLED BY-. v 3U
T
ILfVL yr '�
DATE! METHOD OF SH]PM T:
{Jt?-A �j�L
LAB ID $
SAMPLE TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
TEMP •C
RES.
SULFIDE
,A
t_a D
ellrrqu had by:
Dale
Time
Re ed by. ISlgnslu I
Dais
Tlms
7'3`��'
q.L
y z
�.3, rS
o�:vy
ellnp ehe y'
Dale
Tlm+
R Mid : Signature)
d
13111.
3
Time '
12?"14
e lInquIshtd by: 11
Dale
Time
Recelved by: {S grlalurej
Dill
Time
5
6
ph Flald: ph Field: Water Leval 91
Tamp Field 11: Tamp Field 2: Water Level #2
r�
J`
inluats—} _
Tumaround time: G[Jl..AR RUSH `
Comments or Special Hazards:
Q' to QC,5vyl
IS DATA FOR REG. COMPLIANCE PURPOSE?
N0 ^ YES s,,�WHICH: SZP.. Wl Per''-- n i T
NC- G O 3 00 J tii LC
Page 2 of 2

VMICROBAC'
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8JO382
ASIVIO Greenville of NC INC Project Name: Stormwater Sample - Mthly, Outfall
1
Ms. Pam Savage Project 1 PO Number: NIA
1125 Sugg Parkway Received: 10/18/2018
Greenville, NC 27834 Reported: 11/06/2018
Analytical Testing Parameters
Client Sample ID: OF #1, grab
Sample Matrix: Aqueous Collected By: Savage
Lab Sample ID: K8J0382-01 Collection Date: 10/17/2018 14:40
Wet Chemistry
Method: EPA 1664 Rev. B
Oil & Grease (SGT-HEM)
Method: SM 2540 D-2011
Total Suspended Solids
Method: SM 4500 H+B-2011
pH at 25 °C
Result RL Units
<5.00 5.00 mg/L
Note Prepared Analyzed Analyst
10/23/18 0910 TAB
<10.4 10.4 mg/L
5.5 1.0 pH Units H
Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley
10/19/18 0944 MT
10119118 1404 cc
Result
RL Units Note
Prepared
Analyzed
Analyst
Method: EPA200.7
Copper, Total
0,00546
0.00500 mglL
10/25/18 0637
10/28/18 2213
KKB
Lead, Total
<0.0100
0.0100 mglL
10/25/18 0637
10/28/18 2213
KKB
Zinc, Total
0.105
0.0200 mglL
10/25/18 0637
10/28/18 2213
KKB
Definitions
H: Analyte was prepared and/or analyzed
outside of
the analytical method holding time
MDL: Minimum Detection Limit
RL: Reporting Limit
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
North Carolina DENR NPDES
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By: �� J
Jeanne Overstreet
Client Relationship Specialist, Environmental
Reported: 11/06/2018 14:18
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 1

�VMICROBAC`
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8J0383
ASMO Greenville of NC INC Project Name: Stormwater Sample - Mthly, Outfall
2
Ms. Pam Savage Project 1 PO Number: NIA
1125 Sugg Parkway Received: 10/18/2018
Greenville, NC 27834 Reported: 11/06/2018
Analytical Testing Parameters
Client Sample ID: OF #2, grab
Sample Matrix: Aqueous Collected By: Savage
Lab Sample ID: KSJ0383-01 Collection Date: 10/17/2018 14:50
Wet Chemistry
Method: EPA 1664 Rev. B
Oil & Grease (SGT-HEM)
Method: SM 2540 D-2011
Total Suspended Solids
Method: SM 4500 H+B-2011
pH at 25 "C
Method: EPA200.7
Copper, Total
Lead, Total
Zinc, Total
Result
RL
Units
Note Prepared Analyzed
Analyst
<5.00
5.00
mg/L
10/23/18 0910
TAB
<4.17
4.17
mg/L
10/19/18 0944
MT
5.5
1.0
pH Units H
10/19118 1404
DC
Analyses Subcontracted to: Microbac
Laboratories,
Inc. - Ohio Valley
Result
RL
Units Note Prepared
Analyzed
Analyst
<0.00500
0.00500
mg/L 10/25118 0637
10/28/18 2217
KKB
<0.0100
0,0100
mg/L 10/25/18 0637
10/28/18 2217
KKB
<0.0200
0,0200
mg/L J 10l25118 0637
10/28/18 2217
KKB
Definitions
H: Analyte was prepared and/or analyzed outside of the analytical method holding time
J: The analyte was positively identified, but the quantitation was below the RL
MDL: Minimum Detection Limit
RL: Reporting Limit
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11 North Carolina DENR NPDES
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By:
�,eaait.� /I()c�-�iLat�c:P�
Jeanne Overstreet
Client Relationship Specialist, Environmental
Reported: 11 /06/2018 14:38
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 Of 2

*K8JO383-
§MICROBAC
Microbac-Fayetteville SHORT HOLDS ACCEPTED MONDAY- THUI
2592 Hope Mills Rd.
Fayetteville, NC 28346
11G11I1Rf9nIYEl „`°°°
Lab Report Address
invoice Address
Tur round Time
Y MICROBAC
Client Name: U + G
Client Name:
Yid outine (5 to 7 business days)
Temp. Upon Receipt ('C) /19 Therm ID
Address: 0 r '9i
Address:
[I RUSH' (notify lab)
Holding Time
City, State, Zip: &'7fe.AxA (¢ %�3T
City, State, Zip:
{needed by)
Samples Received on Ice? Yes No WA
Contact: V vi;
Contact:
Report Type
Custody Seals intact? Yes No NIA
Telephone No.: 34( � (^
Telephone No.:
Results Only ( 'Level i [ ) Level 2
[ ] Level3 [ ] Level 4 [ ] EDD
Send Report via: [ ] Mal I ] Fax ]ti}f-mail
C-OKetSend Invoice via: [ j Mail [ ] Fax Ismail pad
a--T_mo—kid ea--n
Project: Location: UT
S PO No.; tyl�jj Compliance Monitoring? [�es [ [ No [ j4gency/Program
KY?-t
[7-0 '
Signature:
Sampler PhoneMo:_ t3�%�
�a� ��� N
Sampled by (PRINT).�T)U A n _w . w _i w .� r
Sampler
awiW } lam,
' Matrix Types: Soil/Solid (S), Sludge, Oil,
Wipe, Drinking Water (D
, Groundwater (GW), Surface Water (SW), Waste Water (WW), Other (specify)
" Preservative Types: (1) HNO3, (2) H2SO4, (3) HCI, (4) NaOH, (5) Zinc Acetate, (6) Methanol, (7) Sodium Bisulfate, (8) Sodium Thiosulfate, (8) Hexane, (U) Unpreserved
REQUESTED ANALYSIS
. r
Date
Collected
EMlffl
Preserv:itive
type
Addifional Notes
no
■r/
�Mmj
®M
■■■■■■■■■■■■■■■
ram■
ree�r�©®mm�.u.�■■■o■■■■■■■■■■■■
Possible Hazard Identificatio []Hazardous
[#<on•Hazardous [) Radioactive
Sam [t}'6ispose as appropriate [ ] Return [ ) Archive
N CG 03000 f&-ir� ' —fl- e — a v u
Reli Islt d y i e) Date1 cel ey (s nature) ate e
sac. 0 8
N CG o 3 o 14 Relinquished B3 ( nature) DatefTime Received By (signature) Daterrime
Page 2 of 2

�VMICROBAC`°'
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8K0297
ASMO Greenville of NC INC Project Name: Stormwater Sample - Mthly, Outfall
1
Ms. Pam Savage Project! PO Number: NIA
1125 Sugg Parkway Received: 11/16/2018
Greenville, NC 27834 Reported: 11/27/2018
Analytical Testing Parameters
Client Sample ID; OF #1, grab
Sample Matrix: Aqueous Collected By: Savage
Lab Sample ID: K81<0297-01 Collection Date: 11/13/2018 14:30
Wet Chemistry
Result
Method: EPA 1664 Rev. B
Oil & Grease (SGT-HEM)
<5.00
Method: SM 2540 D-2011
Total Suspended Solids
20.0
Method: SM 4500 H+B-2011
pH at 25 °C
5.3
RL
5.00
Units Note Prepared Analyzed Analyst
mg1L
6.67 mg/L
1.0 pH Units
11/20/18 0838 TAB
11/20/18 0630 MT
H 11/26118 1339 TAB
Metals
Result
RL
Units Note
Prepared
Analyzed
Analyst
Method: Metals Aqueous/EPA 200.7 Rev 4.4 1994
Copper
<0.025
0.025
mg/L
11/21/18 1446
11/21/18 1446
TAB
Lead
<0.005
0.005
mg/L
11/21/18 1446
11/21/18 1446
TAB
Zinc
0.164
0.002
mg1L
11121118 1446
11/21/18 1446
TAB
Definitions
H:
Analyse was prepared and/or analyzed outside of
the analytical method holding time
RL:
Reporting Limit
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11 North Carolina DENR NPDES
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By:
Jeanne Overstreet
Client Relationship Specialist, Environmental
Reported: 11 /27/2018 15:24
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, INC 28306 1910.864.1920 p I www.microbac.com Page 1 of 2

* K&K0297*
Microbac-Fayetteville
SHORT HOLDS ACCEPTED MONDAY- THURSDAY UNTIL 1600
6)M J C R 0 BAC 2592 Hope Mills Rd.
CHAIN OF CUSTOD'
Fayetteville, NC 28306
Number
lnstructions on back
-
Lab Report Address Invoice Address
Turround Time TO BE COMPLETED SY WROBAC'
p
Client Name: Client Name:
a
�� [� Routine (5 to 7 business days) Temp. Upon Receipt ("C) 4.O 1_ Therm ID
nC_
Address: �noZ�7 S l/.f,C ie�l Address:
[3 RUSH' (notify lab) Holding Time
City, State, Zip: G� Qu qy'�—" N C_ _.' City, State, Zip:
(needed by) Samples Received on ice? Yes No NIA
Contact: FQ-1�a-cw_ LDS Contact:
Report Type Custody Seals Intact? Yes No N/A
7
Telephone No.: Sa ' 3g l — a4t{S Telephone No.:
/
Results Only (v) Level 11 (] Level 2 j ] Level3 [ ] Level 4 [ ] EDD
Send Report via: [ ] Mail ( ] Fax Xe-mail
Send Invoice via: [ ] Mail ( ) Fax () e-mail V QS ill o — C C-vin
Project: Location:
K)vSJ �1lt�Ls� zr31
Sampled by (PRINT): Sampler Signature:
T
PO No.: k7 Compliance Monitoring? [ es I ] No (' gencyl rogram
t l..f...._._.._... BCD`--CQ
Sampler Phone No.: Y 4S
- Matrix Types: SoipSolid (S). Sludge, Oil, Wipe, Drinking Water (DVV). Groundwater (
W). Surface Water (SW), Waste Water [W, Other (specify)
Preservative Types: (1) HNO3, (2) H2SO4, (3) HCI. (4) NOON, (5) Zinc Acetate, (5) Methanol, (7) Sodium Bisulfate, (8) Sodium Thicsulfate. (9) Hexane, (U) Unpreserved
REOiI£ST£D ANAL YSIS
I!J
Client Sample 10
Date
Collected
Preservative
..
AdditionalNotes
MMENMEMM■NINE
M■
MV-
.O■EM..■M.■■.
OEM
am
MMMMMRMMMEnM
MEN
SME
NMMMIMMMMMoMMMMMMMMM
MEN
NEM
Possible Hazard Identificatio [) Hazardous Vlon-Hazardous [] Radioactive
Sam NODispose as appropriate [ ] Return [ ] Archive
Comments ���,L�
- —N -1411 L .W"
Ji ul . ed By Iure) Date/Time eIv By (' n j
DaTime
t 3 C G O W OC>0
r- r6 - 12 9 .`,� r
(!Gtel
R uis d ture) ^Ipatg ime � f�
(DatelTime I
Da i42 me
! t f�
UvCGo 3r✓y S
elinquished By ignaturej Received Fay (signature)
Daterfime
'rev.
t o
Page 2 of 2
1252 r

�VMICROBAC`
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8K0298
ASMO Greenville of NC INC Project Name: Stormwater Sample - Mthly, Outfall
2
Ms. Pam Savage Project 1 PO Number: NIA
1125 Sugg Parkway Received: 11/16/2018
Greenville, NC 27834 Reported: 11/27/2018
Analytical Testing Parameters
Client Sample ID: OF #2, grab
Sample Matrix: Aqueous Collected By: Savage
Lab Sample ID: K81<0298-01 Collection Date: 11/13/2018 14:45
Wet Chemistry
Result
RL
Units Note
Prepared
Analyzed
Analyst
Method: EPA 1664 Rev. B
Oil & Grease (SGT-HEM)
<5.00
5.00
mgiL
11/20118 OB38
TAB
Method: SM 2540 D-2011
Total Suspended Solids
22.0
5.56
mglL
11120118 0830
MT
Method: SM 4500 H+B-2011
pH at 25 °C
5.7
1.0
pH Units H
11/26118 1339
TAB
Metals
Result
RL
Units Note
Prepared
Analyzed
Analyst
Method: Metals Aqueous/EPA 200.7 Rev 4.4 1994
Copper
<0.025
O.D25
mglL
11/21/18 1450
1112108 1450
TAB
Lead
<0.005
0.005
mglL
11/21/18 1450
11121118 1450
TAB
Zinc
0.015
0.002
mglL
11/21/18 1450
11121118 1450
TAB
Definitions
H: Analyte was prepared and/or analyzed
outside of
the analytical
method holding time
RL: Reporting Limit
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
North Carolina DENR NPDES
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By: t
,::?"LX-P—
Jeanne Overstreet
Client Relationship SpeciaEist, Environmental
Reported: 11/27/2018 15:23
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com Page 1 of 2

*K8K0298*
}MICR 0 B AC Microbac-Fayetteville SHORT HOLDS ACCEPTED MONDAY- THURSDAY UNTIL 96o0
2592 Hope Mills Rd. CHAIN OF CUSTODY RECORD I
Fayetteville, NC 28306 Number
Instrtrclions on back
Lab Report Address
Invoice Address
Tur round Time TO BE COMPLETED BY MICROBAE;
p0
Client N ame: [-�
Client Name: �0.h/+'�-��
outlne (5 to 7 business days) Temp. Upon Receipt (1Cj �. p (, Thcrm 1D
Address: I a P t
Address:—�—
[I RUSH` (notify lab) Holding Time
City, State, Zip: G �BP.{ t�l x 0 C-
City, state, Zip:
(needed by) Samples Received on Ice? Yes No NIA
Contact: vL VO�Q� �'�S
Contact:
Report Type Custody Seals Intact? Yes No NIA
#
Telephone No,: oZSa� - 7j�y - o2�t�5
Telephone No.,
Results Only MILever 1 [ ) Level 2 [) Leve13 [ ] Level 4 [ ] EDD
Send Report via: ( ] Mail [ )Fax Ke-mail
Send invoice via: ( ]Mad[ )Fax [ ] e-mail V - , ram' Oyri
Project:'i'O 11�WI G i Q } Location: 0 [}
�1(il PJ
Sampled 6y (PRINT): ss�,r'�[n_F Sampler Signature:
PO No.: if t�1 _Compttance M_onitori_ng? 1 es [ ] No [Ueng�m�
Sampler phone Na.: Q2�oZ' 3 1 "c� 'r ry•J �VI. W'A`���
Matrix Types: Soll/Solid (S), Sludge, Oil, Wipe, Drinking Water (OW), Groundvmter ( W), Surface water (SW), Waste Water (VW). Other (specify)
" Preservative Types: (1) HNO3. (2) H2SO4, (3) NCI, (4) NaOH, (5) Zinc Acetate, (6) Methanol, (7) Sodium Bisullate, (8) Sodium Thiosulfate, (9) Hexane, (U) Unpreserved
REQUESTED ANALYSIS
w
Mrs
!
A%omilm�01mai
wmmwIiI�`/
MENNEEM
Uffm
Possible Hazard Identificatio [) Hazardous p on -Hazardous [ ] Radioactive
Sam k-51spose as appropriate (]Return []Archive
Comments �� ?Z.YLfVL iT
�i�-FM.Lt�+4"'it ui ed By ture) r _ rD ate ��e p � eiv By (' na )
�1CG03UGba
Cr&0,bvL R uls d s lure) 'I�^tg?ime Rea By si ature)
elinquished By ignature) Date/Time Received By (signature)
art �a- tv
DatelFime page 2 of 2

0MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8L0463
ASMO Greenville of NC INC Project Name: Stormwater Sample - Mthly, Outfall
1
Ms. Pam Savage Project 1 PO Number: NIA
1125 Sugg Parkway Received: 12/26/2018
Greenville, NC 27834 Reported: 01/07/2019
Analytical Testing Parameters
Client Sample ID: OF #1, grab
Sample Matrix: Stormwater Collected By: Savage
Lab Sample ID: K81-0463-01 Collection Date: 12/21/2018 13:30
Wet Chemistry
Method: EPA 1664 Rev. B
Oil & Grease (SGT-HEM)
Method: SM 2540 D-2011
Total Suspended Solids
Method: SM 4500 H+B-2011
pH at 25 °C
Method: EPA200.8
Copper, Total
Lead, Total
Zinc, Total
Result
<5.00
24.9
5.4
RL
Units
Note Prepared Analyzed
Analyst
5.00
mg/L
01103l19 1126
TAB
5,62 mg/L
1.0 pH Units H
Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley
12/27/18 1056 MT
01103119 1504 TAB
Result
RL
Units
Note Prepared
Analyzed
Analyst
0.0103
0.00200
mg/L
01/02/19 0828
01/02/19 1426
JYH
0.00119
0.00100
mg1L
01/02/19 0828
01/02/19 1426
JYH
0.372
0.0250
mg/L
01/02/19 0828
01/02/19 1426
JYH
Definitions
H: Analyte was prepared and/or analyzed outside of the analytical method holding time
MDL: Minimum Detection Limit
RL: Reporting Limit
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11 North Carolina DENR NPDES
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By:
,:::? 4Z&X-F— -,/--
Jeanne Overstreet
Client Retationship Specialist, Environmental
Reported: 01 /07/2019 13:21
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 2

Microbac-Fayetteville SHORT HOLDS ACCEPTED MONDAY- THURSDAY UNTIL 1600 "K8L0463"
( MICROB AC 2s92Hope MilCHAIN OFCUSTODY RECOF
�" Fayetteville, NCC 2838306 Number (I(t{ +1 j}�I kAAlllil+9Ag1�111[}I �GQAIfil�1 I)I ry!1(I
Instructions on back
Lab Report Address Invoice Address ` Turnaround Time TO BE COMPLETED By MlC, `
Client Name: {{ 1 G t Z iVt LI=C14CClient Name: ��q-W\ �outine (5 to 7 business days] Temp. Upon Receipt (°C) Therm ID
Address: Address: f [ ] RUSH" (notify tab[ Holding Time
"-
City, State, Zip: %kkF i J i LE � (
LM -� City, State, Zip: (needed by) Samples Received on Ice? Yes No N/A
Contact: �rVi 5,{ VAG E Contact: Report Type Custody Seals intact? Yes No NIA
Telephone No.: Ste- tl I ` �{t ti Sl Telephone No.: Results Only [ ] Level 1 [ ] Level 2 [ ] Leve13 [ ] Level 4 ] ] EDD
Send Report via: [ ) Mail ([ Fax X_e-mail PSGZV ry^Q 0 —'n , r_e, nd Invoice via: [ ] Mail [ )Fax Ve-mail Ej X©l C 15, ,
Project: '5TOZ..3iP%VJA1�_*Z Location: <//'
SjPO No.:� Compliance
Pt Compliae Monitoring? Yes { ] No [ ] Agency/Program
rogram
Sampled by (PRINT): Pr Eyt r VC_C'.R. Sampler Signature`x/ Sampler Phone No.: l: 02 (Y 5_
f c.
Matrix Types: SeiVSolid (S), Sludge. Oil, Wipe, Drinking Water (OW), Groundwater (GW), Surface Water (SW), Waste Water (WW), 0,her (specify)
PreServalive Types, (1) HN63, (2) H2SO4, (3) HCI, (4) NaOH, (5) Zinc Acetate, (6) Methanol, (7) Sodium Bisulfate, (8) Sodium Thiosulfate, (9) Hexare, (U) Unpreserved
REQUESTED ANALYSIS
D
Collected
Collected'
MIS
=I FA ____ ___F111A
IFA
. . . .................................................
Additional /Votes
o��r
MMMMMiMMiiia�
�WNNMWEWMWMWEMM
Possible Hazard Identificatio [ ] Hazardous
�otnmenis
STOP�v{ul��"�YL �Ci2it'i [ i
NCGo 30Uoo
J
NCa3o4(oS
Non -Hazardous [ ] Radioactive
Relinquished By (signature) Daterrime
Reliaa4is4d v isignature) Daterrime
By (signature) DateMme
t sk'22
Sam Dispose as appropriate [ ]'Return [ ] Archive
Received By (signature)
Date/Time
I Page 2 of 2 1

�NMICROBAC`
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8L0465
ASMO Greenville of NC INC Project Name: Stormwater Sample - Mthly, Outfall
2
Ms. Pam Savage Project/ PO Number: NIA
1125 Sugg Parkway Received: 12/26/2018
Greenville, NC 27834 Reported: 01/07/2019
Analytical Testing Parameters
Client Sample ID: OF #2, grab
Sample Matrix: Stormwater Collected By: Savage
Lab Sample ID: K81-0465.01 Collection Date: 12121/2018 13:20
Wet Chemistry
Method: EPA 1664 Rev. B
Oil 8 Grease (SGT-HEM)
Method: SM 2540 0-2011
Total Suspended Solids
Method: SM 4500 H+B-2011
pH at25°C
Method: EPA200.8
Copper, Total
Lead, Total
Zinc, Total
Result RL
<5.00 5.00
Units Note Prepared Analyzed Analyst
mglL 01/03119 1126 TAB
5.17 4.17 mglL
5.6 1.0 pH Units H
12/27/18 1056 MT
01/03/19 1504 TAB
Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley
Result RL Units Note Prepared
Analyzed
Analyst
0.00210
0.00200
mg/L 01102/19 0828
01/02119 1430
JYH
<0.00100
0.00100
mg/L 01/02/19 0828
01/02119 1430
JYH
0.0570
0.0250
mg/L 01102/19 0828
01/02119 1430
JYH
Definitions
H: Analyte was prepared and/or analyzed outside of the analytical method holding time
MDL: Minimum Detection Limit
RL: Reporting Limit
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11 North Carolina DENR NPDES
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By:
Jeanne Overstreet
Client Relationship Specialist. Environmental
I
Reported: 01 /07/2019 13:23
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com Page 1 of 2

Microbac-Fayetteville SHORT HOLDS ACCEPTED MONDAY- THURSDAY UNTIL 1600
OM 1 C R 0 B AC 2592 Hope Mills Rd. CHAIN OF CUSTODY RECOF
Fayetteville, NC 28306 Number
Instructions on back
-K8L0465-
Lab Report Address Invoice Address Turnaround Time TO BE COMPLETED 6Y MICf
Client Name: outine (5 to 7 business days) Temp, Upon Receipt (°C) TFierm 1p
Address: [ oZ5 tI,GG [<(� Address: [] RUSH' (notify lab) Holding Time C
City, State, Zip: G "LT)V [ L LE= C-a1�City, State, Zip: _ (needed by) Samples Received on Ice? Yes No NIA
Contact: P,k,vi S,q VAG E LEAS)Contact: Report Type Custody Seals Intact? Yes No NIA
Telephone No.: a2sa- 3 - a `-�-� Sy Telephone No.: Results Only [ ] Level 1 [ ] Level 2 [ ] Leve13 [ ] Level 4 [ ] EDB
Send Report via: [ ] Mail [ ) Fax e-mail Sc-,V C CZ C�Sy" 0 - C,,Sepd Invoice via: [ ] Mal [ ] Fax
Project: STat? tAAVJhT'TL Location: I)U VALI—S �[j/ ��F}^ 77- PO No., NR-ComplianceMonitoring? Yes [ ] No [ ]AgencylPragrem
P y{ 1 .Y��0.f'L Sampler X' t� i l-- -
Sampled b (PRINT); �(i{Vl plat Signature._ (r�/"�_ Sampler Phone No.:
Matrix Types: SoillSolid (S), Sludge, Oil, Wipe, Drinking Water (DW), Groundwater (GW), Surface Water (SW), Waste Water (WW), Other (specify)
" Preservative Types: (t) HNO3, (2) H2SO4. (3) MCI. (4) NaOH, (5) Zinc Acetate, (6) Methanol, 17) Sodium Bisulfate, (8) Sodium ThiosuUate, (9) Hexane, (U) Unpreserved
RE(aUESTED ANALYSIS
Client Sample 10
te
11 DaCollected
MM
©;Mmffl
■©®®®■
ONE
■ONE
■■
--■■-M■■■■■■■■■■■■■■
-__■■-■■■■■■■■■■■■■■■
�■
��■■■■■■��■�■■■�■■■■■■■■■Eiji
Possible Hazard Identificatio [] Hazardous
Comments
�M(4Nu/ATZ-12 P(--aIlel 1-r-
IL1CG 0 z0000 �
NC9a304(oS
Non -Hazardous [] Radioactive Sam Dispose as appropriate (] Return [] Archive
shed By (signature) DMOMme
tten is a y =cr-so...•Q Dv Yy a�ynaiwq
IR Ilnqurs By (signature) DateMme Received By (signature) DaterTime
Page 2 of 2 - 1

ASMO GREENVILLE OF NORTH CAROLINA, INC
1125 Sugg Pkwy. PHONE [phone]
GREENVILLE, NC 27834 FAX [phone]
October 31, 2017
NCDEQ- Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
{ EeENEE)
NOV U 7 .017
CENTL FILES
DWRS CTION
Please find attached the semi-annual storm water discharge monitoring reports and analytical
results for period I and 2 in 2017, for ASMO Greenville of North Carolina, Inc., COC
NCG030465.
Under our facility's general NPDES general storm water permit NCG030000, effective
December 4, 2012, we are required to submit quantitative results for two rainfall events
annually on Outfall #1 and record and keep on file for inspection qualitative results semi-
annually.
Sampling at our plant has resulted in zinc levels above benchmark value. We have contracted
with Matt Wallace, Principal Engineer at Amec Wheeler Foster Environment & infrastructure
in Ashville, NC to continue to evaluate the site for possible conditions that could be
contributing to these results and work on potential corrective measures to lower our zinc results.
Additionally, Bill Moore, our regional NCDEQ at the Department of Environmental Quality
Land Resources, has been contacted to review our results and assist us in obtaining a waiver
from the current total zinc benchmark.
If you have any questions pertaining to this submittal, please give me a call at 252-754-1765.
Sincerely,
Pam Savage
Environmental Health & Safety
Attachments

*MICROBAC"
Fayetteville Division
Certificate of Analysis
ASMO Greenville of NC INC Date Reported: 08/19/17
Ms. Pam Savage Project: Stormwater Sample - Mthly, Outfall 1 Date Received: 08/08/17
1125 Sugg Parkway Date Sampled: 08/07/17
Greenville NC, 27834 Sampled By: Savage
OF 01, grab
K7110302-01
Analyte
Result
Units
Analyzed
Analyzed By
Method Qualifier
Analyzed by: Microbac Laboratories, Inc. -
Fayetteville
Copper
<0.005
mg/L
08112/ 17 19:50
JAW
EPA 200.7 Rev 4.4 1994
Lead
<0.003
mg/L
08/12/17 19:50
JAW
EPA 200.7 Rev 4.4 1994
Oil & Grease (SGT-HEM)
<5.00
mg/L
08/14/17 09:45
JR
EPA 1664
pH
6.8
pH Units
08/10/17 1 O:14
ELM
SM 4500 H+B-2000 H
(Aqueous)
Total Suspended Solids
13.1
mg/L
08/09/17 10:42
TAB
SM 2540 D-1997
Zinc
0.088
mg/L
08/12/17 19:50
JAW
EPA 200.7 Rev 4.4 1994 S 1
QC Batch Run - (A?icrnbac Laboratories, Inc. - Fayelleville)
Analyte
Result
Units
Source
RPD Limit
Lead
ND
mg/L
K7140302
200
Zinc
0,079
mg/L
K7H0302
I 10
Total Suspended Solids
48.9
mg/L
K71-10350
30 5
Total Suspended Solids
15.3
mg/L
K71-10360
2 5
pH
6.8
pH Units
K71-10441
0 200
Copper
ND
mg/L
K71-10302
10
Notes and Definitions
St. Relative Percent Difference (RPD) outside accepted recovery limits
H Analyte was prepared and/or analyzed outside of the analytical method holding time
State Certifications:
NCDNR #II
NCDOH #37714
Respectfully Submitted
Jeanne Overstreet, Project Manager
Thank you for your business. We invite yourjeedbark on our level ofservice to yvou. Please cnntacr the Division Manager, Rob Dormer at 910-864-1920 with an';
questions, You ma.v ulso comuct J Trevor Boyce, President ur presidenr(amic•mbac.cont
Microbac Laboratories, Inc.
Page 1 of 2
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Fayetteville Division 2592 Hope Mills Road — Fayetteville, NIC 28306 (910) 864-19201
CHAIN OF CUSTODY RECORD
1111111111011111
-Li ENT NAME &AODFtEsS:
��o! �[� ,�1`�(ti
i _ T
IBC
PC# PROJECTILOCATION:
o F *1
Lu
`j
L
O
TYPE
OF
ANALYSIS
PRESERVATION (CODE~)
.
c�C'1
V
Q
of
ti
^l�
c`�
p
i
��
CODE: A = None
B = HNO3 (pH<2) + <6eC
C = H2SO4 (pH<2) + <6°C
E = ZN Acetate + <6'C
F = H Ci
G = Sodium Thlo
CONTACT PERSON:
PFiPNE: v
01 ~ 3 I
1AMPLED Sr �.
DATE 1 METIOO OF SHIPMENT: .
'7 I1 % CC L) 94 0(_7
LAB ID#
SAMPL£TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
TEMP
CHRES,NE
SULFIDE
Lab Initials-->
ellnq Date Tim ReeeN tl y: (Slpna } Dale Time
Turnaround time: REGULAR RUSH
8' z ?-�-17
!ellnqu y: Date Tima Received hy; 5 ynature Due Time Comments or Special Hazards:
Q 8 -Z-17 14-.27 J' tom- 4 M, (7 / 11fw.(-J� f � F>5- cclx-ec-sy l v
elln ah by: Date Tlme ees ved by: [Signature) Dale TIM,
5 6
(LC11111
�( �U_
ph Field: ph Field: Water Level #1 IJ UA I 11 t-UK K=kl. I,UN L1fllvliG I- L)M-VZIC r
Temp Field 1: Temp Field 2: Water Level #2 NO _ YES WHICH: �,p
NCB o3p� j �cGv3c�rc.�
Page 2 of 2

VMICROBAC'"'
Fayetteville Division
Certificate of Analysis
ASMO Greenville of NC INC Date Reported: 03/04/17
Ms. Pam Savage Project: Stormwater Sample - Mthly, Outfall I Date Received: 02/16/17
1125 Sugg Parkway Date Sampled: 02/15/17
Greenville NC, 27834 Sampled By: Savage
Outfall #1
K7B0592-01
Analyte
Result
Units
Analyzed
Analyzed By
Method
Qualifier
Analyzed by. Mkxobac Laboratories, Inc. -
Fayetteville
Copper
0.009
mg/L
03/01/17 11:59
AC
EPA 200.7 Rev 4.4 1994
Lead
0.014
mg/L
03/01/17 11:59
AC
EPA 200.7 Rev 4.4 1994
Oil & Grease (SGT-HEM)
<5.00
mg(L
02/27/17 20:20
JAW
EPA 1664
pH
6.1
pH Units
02/24/17 14:00
ELM
SM 4500 H+B-2000
H
(Aqueous)
Total Suspended Solids
12.0
mg/L
02/22/17 07:55
JR
SM 2540 D-1997
Zinc
0.246
mg/L
03/01/17 11:59
AC
EPA 200.7 Rev 4A 1994
QC Batch Run - (Microbee Laboratories, Inc - Fayetteville)
Analyte _ T
Result
Units
Source
RPD
LimitT
Copper
0.275
mg/L
0053550
1
200
Copper
0,231
mg/L
K7130807
7
10
Copper
1.57
mg/L
K7130644
1
10
Copper
0.265
mg/L
K7130564
4
10
Copper
0.278
mg/L
K7B0563
4
10
Copper
ND
mg/L
K7130807
10
Copper
1.24
mg/L
K7130644
7
10
Copper
0.010
mg/L
K7B0564
1
10
Copper
0.270
mg/L
0053550
2
200
Lead
0.251
mg/L
0053550
2
200
pH
5.0
pH Units
K7B0846
0
200
pH
6.6
pH Units
K7B0840
0
200
pH
6.0
pH Units
K7130599
0
200
Total Suspended Solids
360
mg/L
K7130670
5
5
Total Suspended Solids
560
mg/L
K7130669
27
5
Total Suspended Solids
53.0
mg/L
K7B0644
0.6
5
cal Suspended Solids
12.0
mg/L
K7130614
3
5
Copper
0.033
mg/L
K7B0563
3
10
Microbac Laboratories, Inc. Page 1 of 4
2592 Hope Mills Road I Fayetteville, NC 28306 1 910-864.1920 p 1910.864.8774 f I www.microbac.com

VMICROBAC'
Fayetteville Division
Certificate of Analysis
ASMO Greenville of NC INC Date Reported: 03/04/17
Ms. Pam Savage Project: Stormwater Sample - Mthly, Outfall 1 Date Received: 02/16/17
1125 Sugg Parkway Date Sampled: 02/15/17
Greenville NC, 27834 Sampled By: Savage
QC Batch Run - (Microbac Laboratories, Inc- - Fayetteville)
I Analyte
_ _ Result
Units
Source
RPD
Limit f
Zinc
0.734
mg/L
K7130563
3
10
Zinc
0.249
mg/L
0053550
0.4
200
Zinc
0.257
mg/L
0053550
2
200
Zinc
0.277
mg/L
K7B0807
6
10
Zinc
0.295
mg/L
K7B0564
2
10
Zinc
0.027
mg/L
K7B0807
6
10
Zinc
0,349
mg/L
K7130644
0.7
10
Zinc
0.068
mg/L
K7130564
23
10
Zinc
0.491
mg/L
K7130563
8
10
Lead
0.267
mg/L
K7130807
5
200
Lead
0.255
mg/L
K7B0644
2
200
Lead
0.249
mg/L
K7130564
2
200
Lead
0,264
mg/L
K7130563
4
200
Lead
0.023
mg/L
K7B0807
0
200
Lead
0.011
mg/L
K7130644
9
200
Lead
0.012
mg/L
K7130564
9
200
Lead
0.041
mg/L
K7110563
9
200
Lead
0.241
mg/L
0053550
0.8
200
Zinc
0.614
mg/L
K7130644
3
10
Notes and Definitions
H Analyte was prepared and/or analyzed outside of the analytical method holding time
State Certifications: Respectfully Submitted
NCDNR 411
NCDOH t137714
4
Jeanne Overstreet, Project Manage.
Microbac Laboratories, Inc.
Page 2 of 4
2592 Hope Mills Road I Fayetteville, NC 28306 1 910.864.1920 p 1910.864.8774 f I www.microbac.com

(�)IHICROBAC`
Fayetteville Division
Certificate of Analysis
ASMO Greenville of NC INC Date Reported: 03/04/17
Ms. Pam Savage Project: Stormwater Sample - Mthly, Outfall I Date Received: 02/16/17
1125 Sugg Parkway Date Sampled: 02/15117,
Greenville NC, 27834 Sampled By: Savage
Thank you for your business. We invite yourfeedback on our level ofservice la you. Please eontael the Division Manager, Rob Dermer at 910-864-1920 ivilh any
questions. You may also conlacl J. Trevor Boyce, President at [e-mail]
Microbac Laboratories, Inc.
Page 3 of 4
2592 Hope Mills Road I Fayetteville, NC 28306 j 910.864.1920 p 1 910.864.8774 f I www.microbac.com

Fayetteville Division 2592 Hope Mills Road Fayetteville, NC 28305 [phone] 1854-87"
CHAIN OF CUSTODY RECORD
PAGE
'-NTNAMt&ADDRES5:
v�[
a76
PO PROJECTILOCATION;
CONTACT PERSON'
PAID sAVf' P-r
0_
Q
TYPE
OF ANALYSIS
PRESERVATION (CODE)
;,�
-
.',
¢
-
:�.�
-1
,..�
mot.
�:
"-�
GORE: A = None
B = HNO3 (pH<2) + <6'C
C = H2SO4 (pH<2) + <6'C
D = NaOH * <6'0
E = ZN Acetate + <6'C
F = HCI
G = Sodium Thio
PHONE:
34 � �tS
AMPLE BY:a
r
i Q
DATEEMETHOD OFSHIPMENT: t C_PLO A'r
CO JP--(L' -- r
LAB ID $
SAMPLE
TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
TEMPO
RES
CHLORINE
N E
SULFIDE
Z s r
I o
i
a
L.d t)
9nqu1 had 6y;
pile
Time
ReFe tl Ey: [Slaneto
2,
Date
Time
oun. q eha y:
Die
Tlslt
G . s gnstutej
Data
Tlme
e In had by-..
Dale
Time
Rece ad nY: (S gnuuraj
Date
Time
5
B
ph Field: ph Field; Water Level #1
temp Field 1: Temp Field 2: Water Level 92
initials-*-
Turnaround time: REGULAR RUSH
Comments or Special hazards:
IS DATA FOR iREG, CO PLIANCE PURPOSE?
NO � YES WHICH: -jo
N C-C, O 3 of�o } IJCC v 30'-{�CS
�e4of4

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality eneral Permit No. NCG030000
Date submitted lol3i /
CERTIFICATE OF COVERAGE NO. NCG03 d q (_S SAMPLE COLLECTION YEAR odd l I
FACILITY NAME ASMO !UC . --a1C._ SAMPLE PERIOD R'Jan-June El _uly-Dec
COUNTY or ❑ Monthly" (month"
PERSON COLLECTING SAMPLES VU DISCHARGING TO CLASS ❑ORW ❑HQW [:]Trout❑PNA
LABORATORY 7:0- t I Lab Cert. # 3? % ! ❑Zero -flow ❑Water Supply ❑SA
Comments on sample collection or analysis: DOther C , j\J SUJ _
Part A: Stormwater Benchmarks and Monitoring Results
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics5
Benchmarks ===>
-
-
100 mg/L or 50 mg/L4
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
O-(
/ 7
I Z , 0 Y-1 c
t
d - 009
0.0('4 ''
e
)F#r'
��' U 1
3.J N'`g2
lv ��
�0.()Us
�a.UD3'
.0ffn
t LSOv
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for.the.same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title) `�
(Signature) — (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, theymust be reported in the format "<XX mgLLL where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil Per month.
n No discharge this period?z
Qutfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches'
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks ===a
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES 0'NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑'NO ❑
REGIONAL OFFICE CONTACT NAME: P5, !l Acjoru—
Mail an original and one copy of this DMR, intluding all "No Discharge" reports._within 30 days of receipt of the lab results (or at end of_monitori�cn _period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Permit Date: 11/1/2012-10/31/2017
(Date)
SWU-245, last revised 10/25/2012
Page 3 of 3

0
ASMO GREENVILLE OF NORTH CAROLINA, INC
1125 Sugg Pkwy. PHONE [phone]
GREENVILLE, NC 27834 FAX [phone]
August 5, 2017
NCDEQ- Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVED
AUG 15 2017
CENTRAL FILES
DVVR sEC'rION
After reviewing my storm water files, I could not find a record of issuing 2016 sampling to
NCDENR. Please find attached the semi-annual storm water discharge monitoring reports and
analytical results for period 1 & 2 in 2016, for ASMO Greenville of North Carolina, Inc., COC
NCG030465.
Under our facility's general NPDES general storm water permit NCG030000, effective
December 4, 2012, we are required to submit quantitative results for two rainfall events
annually on Outfall #1 and record and keep on file for inspection qualitative results semi-
annually.
Sampling at our plant has resulted in zinc levels above benchmark value. We have contracted
with Matt Wallace, Principal Engineer at Amec Wheeler Foster Environment & Infrastructure
in Ashville, NC to continue to evaluate the site for possible conditions that could be
contributing to these results and work on potential corrective measures to lower our zinc results.
If you have any questions pertaining to this submittal, please give me a call at 252-754-1765.
Sincerely,
am Sav
Environmental Health & Safety
Attachments
tCEIVED
.A96 ][5 2917
CENTRAL FILES
DWR JECTION

C It.;.
Fayetteville Division
Certificate of Analysis
ASMO Greenville of NC INC Date Reported: 03/04/17
Ms. Pam Savage Project: Stormwater Sample - Mthly, Outfall 1 Date Received: 02/16/17
1125 Sugg Parkway Date Sampled: 02/15/17
Greenville NC, 27834 Sampled By: Savage
Outfall #1
K7B0592-01
I Analyte
Result
Units
Analyzed
Analyzed By
Method
Qualifier J
Analyzed by: Microbac Laboratories, Inc. -
Fayetteville
Copper
0.009
mg/L
03/01/17 11:59
AC
EPA 200.7 Rev4.4 1994
Lead
0.014
mg/L
03/01/17 11:59
AC
EPA 200.7 Rev4.4 1994
Gil & Grease (SGT-HEM)
<5.00
mg/L
02/27/17 20.20
JAW
EPA 1664
PH
6.1
pH Units
02/24/17 14:00
ELM
SM 4500 H+B-2000
H
(Aqueous)
Total Suspended Solids
12.0
mg/L,
02/22/17 07:55
JR
SM 2540 D-1997
Zinc
0,246
mg/L
03/01/17 11:59
AC
EPA 200.7 Rev 4.41994
1
QC Batch Run - (Microbac Laboratories. Inc - Fayetteville)
IAnalyte
Result
Units
Source
RPD
Limit
Copper
0.275
mg/L
0053550
1
200
Copper
0.231
mg/L
K7B0807
7
10
Copper
1.57
mg/L
K7B0644
I
t0
Copper
0.265
mg/L,
K7130564
4
10
Copper
0.278
mg/L
K7B0563
4
10
Copper
ND
mg/L
K7130807
10
Copper
1.24
mg/L
K7130644
7
10
Copper
0.010
mg/L
K7130564
1
10
Copper
0.270
mg/L
0053550
2
200
Lead
0,251
mg/L
0053550
2
200
PH
5.0
pH Units
K7130846
0
200
PH
6.6
pH Units
K7130840
0
200
PH
6.0
pH Units
K7B0599
0
200
Total Suspended Solids
360
mg/L
K7B0670
5
5
Total Suspended Solids
560
mg/L
K7130669
27
5
Total Suspended Solids
53.0
mg/L
K7130644
0.6
5
\� al Suspended Solids
12.0
mg/L
K7B0614
3
5
Copper
0.033
mg1L
K7B0563
3
10
Microbac Laboratories, Inc.
Page 1 of 4
2592 Hope Mills Road I Fayetteville, NC 283061910.864.1920 p 1910,864.8774 f I www.microbac.com

1A 1 CROBAC
Fayetteville Division
Certificate of Analysis
ASMO Greenville ofNC INC
Date Reported: 03/04/17
Ms. Pam Savage
Project: Stormwater Sample - Mthly, Outfall 1
Date Received: 02/16/17
1125 Sugg Parkway
Date Sampled: 02/15/17
Greenville NC, 27834
Sampled By: Savage
QC Batch Run - (Microbac Laboratories, Inc. - Fayetteville)
Analyte
Result
Units
Source
RPD Limit
Zinc
0.734
mg/L
K7130563
3
10
Zinc
0.249
mg/L
0053550
0.4
200
Zinc
0.257
mg/L
0053550
2
200
Zinc
0.277
mg/L
K7B0807
6
10
Zinc
0.295
mg/L
K7B0564
2
10
Zinc
0,027
mg/L
K7B0807
6
10
Zinc
0.349
mg/L
K7130644
0.7
10
Zinc
0.068
mg/L
K7130564
23
t0
Zinc
0.491.
mg/L
K7130563
8
t0
Lead
0.267
mg/L
K7130807
5
200
Lead
0.255
mg/L
K7130644
2
200
Lead
0.249
mg/L
K7130564
2
200
Lead
0.264
mg/L
K7130563
4
200
Lead
0.023
mg/L
K7B0807
0
200
Lead
0.011
mg/L
K7130644
9
200
Lead
0,0I2
mglt,
K7130564
9
200
Lead
0.041
mg/L
K7B0563
9
200
Lead
0,241
mg/L
0053550
0.8
200
Zinc
0.614
mg/L
K7130644
3
10
Notes and Definitions
H Analyte was prepared and/or analyzed outside of the analytical method holding time
State Certifications: Respectfully Submitted
NCDNR #11
NCDOH #37714 �� L�u•r.La�i�_P
Jeanne Overstreet, Project Manage.
Microbac Laboratories, Inc.
Page 2 of 4
2592 Hope Mills Road I Fayetteville, NC 283061910.864.1920 p 1910.864.8774 f I www.rnicrobac.com

Fayetteville Division
Certificate of Analysis
ASMO Greenville of NC INC
Ms, Pam Savage Project: Storinwater Sample - Mthly, Outfall 1
1125 Sugg Parkway
Greenville NC, 27834
Date Reported: 03/04/17
Date Received: 02/16/ 17
Date Sampled: 02/15/17
Sampled By: Savage
Thank you for your business. We invite your feedback on our level ofservice to you. Please contact the Division Manager, Rob Dermer at 910-864-1920 with any
questions, You may also contact J. Trevor Boyce, President [e-mail]
Microbac Laboratories, Inc.
Page 3 of 4
2592 hope Mills Road I Fayetteville, NC 283061910.864.1920 p 1910.864.8774 f I www.microbac.com

Fayetteville: Division 2592- Hope Nils Road Fayettevi€ie, IBC 25306 (910) 864-19201854-87'
CHAINOF CUSTODY RECORD
PAGE,
*K7i3D592*
WENTNAMSAAO0R �
1 -z-jG
(� f/
ia7 3 Pieourw.
P❑X.
PR0280TILOCATION: �
�,
o
.0
TYPE
OF
ANALYSIS
PRESERVATION! (CCDE)
. 4
CODE: A = None
B = HNO3 (pH +
C = H2SO4 H<2+ <6°C
D = NaOH + <B'C
E = zN Acetate + <s•C
F = HCI
G = Sodium Thlo
=RTACT'PERSOM:: a
1AMPLEO 6Y:
0A*Mf
METHOn OF'SHfPMEMT:
co
LAB td -9
.SAMPLE
TYPE
DATE
T1ME
COMP
GRAB
PH
FLOW
TEMP •C
RES.
CNL6RIME
SULRDE
lG #
�4t4-�►2
r
( c�
a.
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e In fader:-
Me
Time:
Race, edny: (5 Qnature)
5
B
ph Field: ph Field: Water Level 01
Temp Fled 1 Tamp Field 2: Water_ Laval 02
Initials�
Tumaround time: REGULAR RUSH
Comments or Special Hazards:
c_s vv l C.; C G
IS DATA FOR REG, CO PLIANCE PURPOSE?
NO YES WHICH:
lv C-C' 0 3 o0c) v 3 C,'-I
C;4of,l

Semi-annual Stormwater Dis%.nar a Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 11 Z I'7
CERTIFICATE OF COVERAGE NO. NCG 3 O��
FACILITY NAME A5MQ (2Q6W) ill L-LG- DF t� C, TNC .
COUNTY P ITT'
PERSON COLLECTING SAMPLES P A-►V1 S/A 11
LABORATORY M [G(LQ MC_ (�� Lab Cert. # 3' 7 `T
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR -Z0 ( ry
SAMPLE PERIOD ❑ Jan -June Duly -Dec
or ❑ Moni
DISCHARGING TO CLASS
RECEIVED
FEB 0 I Z017
CENTRAL FILES
DWR SECTION
PLEASE REMEMBER TO S
❑ No discharge this��riod?'
4
outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics5
Benchmarks =__>
_
-
100 mg/L or 50 mg/L ..
- 6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
i mg/L
z- ►
0. 3g
a. 00 '"31 L_
to • 5
0.00rilc
4 o. aQ
0, z.g-a
L
/V A
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/l/201Z-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities thi , ,icorpo rate a solvent management plan into the 5tormwater PoIL_ on Prevention Plan may so certify, and the requirement for TTO m, ..coring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For thwse facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title
z-r
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH:by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
/dO"T
LCC469 LO
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If yot: _port a sample value in excess of the benchmark, you must imple,-ant Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES LINO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO Q
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal and one copv of this DMR. includina off "No Discharge" reports. within 30 dovs of receipt of the lab results (or at end of monitorina period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
i
(Signature of Permittee)
Permit Date:11/1/2012-10/31/2017
Z S T. -., Z--1 4
(Date)
SWU-245, last revised 10/25/2012
Page 3 of 3

� 1
Semi-annual Stormwater ML;narge Monitoring Resort
for North Carolina Division of Water Quality General Permit No. NCG030000
D -submitted
CERTIFICATE OF COVERAGE NO. NCG03Q Q Q D SAMPLE COLLECTION YEAR 2-41
FACILITY NAME -A5rn'0 G261a_� V J L L OF tJ C-� TNC - SAMPLE PERIOD Jan -June ❑July -Dec
COUNTY P I-rT or []monthly' month
PERSON COLLECTING SAMPLES SAVAGE DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout - ❑PNA
LABORATORY M J C-A0 6AC, #rf Lab Cert. # 32 21 ❑Zero -flow [:]Water Supply ❑SA
�
Comments on sample collection or analysis: EFCEf V 0-
[Other
C
I\1�
,r
FEB 01 26,j�PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
Part A: Stormwater Benchmarks and Monitoring Results 0vvj3, F/CJE�S
6C710A❑ No discharge this period:
Non -Polar O&G/
Outfall No.
Date Sample
24-hour rainfall
Total. Suspended: Solids'
pH;.
Copper
Lead
tint
Total Petroleum
Total Toxic
Collected'
amount,
Standar&units
hydrocarbons
Organics5
(mo/dd/yr)
inches
Benchmarks =_=>
—
-
100 mg/L or 50 mg/O.-
'6.0 - 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
Z z
r o
l �{ . 3 [-
- o
o- �'�
4 0,(%) �
o .)s o
� zScb
A
uU
IL
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameterat the same outfa`tt"
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkm' ark here. '
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge require
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark appli_�s.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductorsanufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition"cbitted in the'EPA' -
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; fo!ssemtconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/2S/2012
Page 1 of 3

1
Facilities thF_ ,.icorporate a solvent management plan into the Stormwater Poll, --.ten Prevention Plan may so certify, and the requirement for TTO m, ..Loring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Basedrupon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature) ( Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format "<XX m L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inchee
Non -polar O&G/TPH.by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks ===>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
-No--r--
Footnotes from Part A also apply to this Part 8
" See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: l 1, f yoe: _port a sample value in excess of the benchmark, you must imple,..ent Tier 1, Tier Z, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lob results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Z3 U� zaI�-
(Date)
Permit Date:11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Disc:narge Monitoring~ Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 2-�`l 1 11
o3 0
CERTIFICATE OF COVERAGE NO. NCG03� 2 Q Q
FACILITY NAME A5MO C�� L_t✓ pF C, LrvC .
COUNTY P I-rT
PERSON COLLECTING SAMPLES A-vyi S.A�IA f�
SAMPLE COLLECTION YEAR 2_0 1 5
SAMPLE PERIOD ❑ Jan -June E July -Dec
or ❑ Monthly( (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY __ K tC-909 (_ fl Lab Cert. # 3_ q'1 [_� �� ❑Zero -flow ❑Water Supply ❑SA
Comments on sample collection or analysis: ysis: � [v�]ther C S i� CIO PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
Part A: Stormwater Benchmarks and Monitoring Results
No discharge this period?
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
U
Total Suspended Solids
pH,.
Standard units
Copper
_
Lead
Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
s
Organics
Benchmorks ===>
_
-
100 mg/L or 50 mg/L . ,
6.0 — 9.0
0.007 mg/L
0.03-mg/L
0.067 mg/L
15 mg/L
1 mg/L
DF P4
12-(o l5-
(o
1? D
6 S
o.00 ,3
<D.0031
0,zSa
.4S-,0n"9
NA
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities 1k., ..icorporate a solvent management plan into the Stormwater PolL.-m Prevention Plan may so certify, and the requirement for TTO m- .coring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
;'Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(Tf0), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
C7eye-t 4
Title (Print title
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L" , where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?'
Outfall No.
Date Sample
Collected"
(mo/dd/yr)
24-hour rainfall
amount,
Inches;
Non -polar O&G/TPH.by
EPA 1664'(SGT-HEM)
Total Suspended Solids
pH
Benchmarks =_->
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
L�
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

c
Note: if yaz port a sample value in excess of the benchmark, you must imple,..ant Tier 1, Tier Z or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• ,A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES 1N A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an orioinal and one copy of this DW including all "No Discharge" reports, within 30 days of receipt of the lab results or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Permit Date:11/1/2012-10/31/2017
(Date)
SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater awarge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted — 011A -f I , �Z-o I S!
CERTIFICATE OF COVERAGE NO. NCG03 0 L4 (a 5 SAMPLE COLLECTION YEAR
FACILITY NAME ASM0 T ZT)AC.A(LoL(iJA)SIC'. SAMPLE PERIOD �n-June ❑July -Dec
COUNTY fE 'T` or ❑ Monthly' (month)
PERSON COLLECTING SAMPLES vv`_ S JA G DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY M fC 1 P�-AC#-f l� Lab Cert. # 3 ��f `-(__ RFC
t _-�V� ❑2ero-flow [-]water Supply [:]SA
Comments on sample collection or analysis: M17-I..+o. � I V ® I , � f4 � � aOtherC Ili S (A� C=
!.0 E� i;i+_e��-==� PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 rC
�.7a+w'v I PW EL' ` 1 V
CENTRAL FILES 0%19f
Part A: Stormwater Benchmarks and Monitoring ResultsSEOTICN
❑ No discharge this period?z
outfall No.
Date Sample
Collected 1
(mo/dd/yr)
24-hour rainfall
amount,
inches
Total Suspended Solids
pH,
Standard units
Copper
Vx" jL
Lead
,,���
f L_
Zinc
�
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks =__>
_
-
100 mg/L or 50 mg/0
6.0 - 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
U 3 Zo &;
3. -5
O
<0. vK-00
Lc . 006-0
D . i io `i
-e_5_.0D A
f�
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance"for•the same -parameter at the same outfall.
3 For sampling periods with no discharge at any single outfall, you must still submit this discharge mooring -repo rt with a checkmark here.
The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible fora waiver of the rain gauge requirement.
' See General Permit, Table 3 identifying the especially sensitive'r'ecei�ing'water classifications where rpcye��tective benchmark applies.
S Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For,, purposes of this permit the definition o Jvotal Z.Qtganics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement'to,sampie (for metal finishing use the definition asfbund in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31.).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Pri lea
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
CPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
-
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 4
Permit Dat 1/2012-10/31/2017 SWU-245, last revised 5/2012
l
• Page 2of3

Note: If yaport a sample value in excess of the benchmark, you must impent Tier 1, Tier 2, or Tier 3 responses. See General Permit text.. 1
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO Q�
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case o "No Discharge' re orts to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED -
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
(Date)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 3

0
IN
*MICROBAC b
Fayetteville Division
Certificate of Analysis
ASMO Greenville of NC INC Date Reported: 04/13/15
Ms. Pam Savage Project: Stormwater Sample - Mthly, Outfall 1 Date Received: 03/24/15
1125 Sugg Parkway Date Sampled: 03/20/15
Greenville NC, 27834 Sampled By: Savage
Outfall #1, grab
K5C0889-01
Analyte
Result
Units
Analyzed
Analyzed By
Method
Qualifier
Analyzed by: Microbac Laboratories, Inc.
- Fayetteville
Copper
<0.00500
mg/L
04/03/15 06:59
JAW
EPA 200.7 Rev 4.4 1994
Lead
<0.00150
mg/L
04/03/15 06:59
JAW
EPA 200.7 Rev 4.4 1994
Oil & Grease (SGT HEM)
<5,00
mg/L
04/05/15 21:00
MLW
EPA 1664
pH
6.0
pH Units
03/27/15 14:00
DSK
SM 4500 H+B-2000
H
(Aqueous)
Total Suspended Solids
3.33
mg/L
03/27/15 11:00
MLW
SM 2540 D-1997
Zinc
0.164
mg/L
04/03/15 06:59
JAW
EPA 200.7 Rev 4.4 1994
QC Batch Run - (Microbac Laboratories, Inc. - Fayetteville)
Analyte
Result
Units
Source
RPD
Limit
Copper
0.0335
mg/L
K5C0707
18
200
Copper
0.268
mg/L
K5C0707
8
200
Copper
0,271
mg/L
K5C0520
1
200
Lead
ND
mg/L
K5C0520
200
Copper
0.0200
mg/L
K5C0754
2
200
Lead
0.00150
mg/L
K5C0707
40
200
Copper
0.0260
mg/L
K5C0520
51
200
Total Suspended Solids
1.50
mg/L
K5C0882
6
5
Total Suspended Solids
2.00
mg/L
K5C0935
0
5
Zinc
0.330
mg/L
K5C0707
2
200
Zinc
0.428
mg/L
K5C0520
0
200
Zinc
0.142
mg/L
K5C0754
66
15
Zinc
0.182
mg/L
K5C0520
4
15
Lead
0,264
mg/L
K5C0707
5
200
Lead
0,243
mg/L
K5C0520
0.8
200
Lead
ND
mg/L
K5C0754
200
Zinc
0.0645
mg/L
K5C0707
6
15
Microbac Laboratories, Inc.
Page 1 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 G 910.864.1920 p 1910.864.8774 f I www.microbac.com

ASMO Greenville of NC INC
Ms, Pam Savage
1125 Sugg Parkway
Greenville NC, 27934
Notes and Definitions
*MICROBAC"
Fayetteville Division
Certificate of Analysis
Project: Stormwater Sample - Mthly, Outfall 1
H Analyle was prepared and/or analyzed outside of the analytical method holding time
Date Reported: 04/13/15
Date Received: 03/24/15
Date Sampled: 03/20/15
Sampled By: Savage
State Certifications: Respectfully Submitted
NCDNR #11
NCDOH #37714
Bonnie K. Sanders, Senior Project Manager
Thank you for your business. We invite pour feedback on our level ofservice to you. Please euntaet the Division Manager. Rnh Derrner at 910-864-1920 with any
questions. Knr may also contact ,1. Trevor Snyce. President at hrecident a micrahuc.cum
Microbac Laboratories, Inc.
Page 2 of 3
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1 910-864.8774 f I www.microbac.com

Fayetteville Division 2592 Hope Mills Road - Fay ettevilfe, NC 28306 [phone] 1 8
CHAIN OF CUSTODY RECORD
*K5C0889*
1111111 [II �Illi [ll III II IIIII Il!!1 I[� 1111
CLIENT NAME& ADDRESS: (PO
7'^►rmo lGr- U`laL
�L
�,{ �ea-7
+
PROJECTILOCATION:
v� } � � -�--
co
Oco
LL
0
TYPE
O NALYSIS
PRESERVATION (CODE)
�.f
°'
J
O
CODE: A = None
B = HNO3 (pH<2) + <6°C
C = H2SO4 (pH<2) + <15T
D = NaOH + <g°C
E = ZN Acetate + <b°C
F' = HCl
G =Sodium Thfa
CONTACT PERSON:
PA-Vv\ SAVA CSC � _ 4 s � V--A T
PHONE: jj �/ (r
Z�� _ 1 Z[�"{ `C a
SAMPLED BY:
P}r� /
`�lC� C
DATE! METHOD OF SHIPMENT:
coJ,u u-m- Sirs
LAB ID #
SAMPLE TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
TEMP •C
RES.
CHLORINE
SULFIDE
tom, ,4c1'Gn
A Lab
Inftials—►
Yelinquished by:
Dale
Time
RefIved by: {Sle rel
Date
3y5
Tiq�
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2
ieil quls a y:
Date
a ignat raj
Date
Ime
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Ime
Rocclyed by: (Slgnatijre
Date
Time
5
6
ph Field: ph Field:
Temp Field 1: Temp Field 2:
Water Level #1
i
�I
01
Turnaround time: REGULA /'fiU.��1�j�,/�
Comments or Special Haz rds: h�"J �.�✓`` /
$5t3 fLwt wpr�' �---n-Yk. t T
NG�o3cDLo Coc-I.3C-Go30Lf(PS
IS DATA FOR REG, COMPLIANCE PURPOSE?
Page 3 of 3

_GREENVILLE OF NORTH CAROLINA, INC
1125 _
Su9� PkwY• PHONE [phone]
GREENVILLE, NC 27834 FAX [phone]
May 1, 2015
NCDENR- Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Please find attached the semi-annual storm water discharge monitoring report and analytical
results for period 1 in 2015, for ASMO Greenville of North Carolina, Inc., COC NCG030465.
Under our facility's general NPDES general storm water permit NCG030000, effective
December 4, 2012, we are required to submit quantitative results for two rainfall events
annually on Outfall 41 and record qualitative results semi-annually for inspection.
Our zinc levels show we are above benchmark value, so we have started monthly sampling to
monitor, reviewed the site for possible conditions that could be contributing to this result and
have started activities to potentially lower our zinc results.
If you have any questions pertaining to this submittal, please give me a call at 252-754-1765.
Sincerely,
/ , ?_1A dc�-
Pam Savage
Environmental Health & Safety
Attachments

ASMO GREENVILLE OF NORTH CAROLINA.,� INC
1125 Sugg Pkwy, PHONE [phone]
GREENVILLE, NC 27834 FAX [phone]
February 23, 2015 RECEIVED
NCDENR- Division of Water Quality MAR 0 2 2015
Central Files CENTRAL FILES
1617 Mail Service Center DWR SECTION
Raleigh, NC 27699-1617
Please find attached the semi-annual storm water discharge monitoring report and analytical
results for period 2 in 2014, for ASMO Greenville of North Carolina, Inc., COC NCG030465. }
Under our facility's general NPDES general storm water permit NCG030000, effective
December 4, 2012, we are required to submit quantitative results for two rainfall events
annually on Outfall #1 and record qualitative results semi-annually for inspection.
Our zinc levels have remained below benchmark value, so we have discontinued monthly
sampling but we will continue to monitor our activities to ensure sources of zinc in our storm
water in order maintain below benchmark values.
If you have any questions pertaining to this submittal, please give me a call at 252-754-1765.
Sincerely,
Pam Savage
Environmental Health & Safety
Attachments

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted E/3,r?c�Af �3,.zU15
CERTIFICATE OF COVERAGE NO. NCG0312 q & S
FACILITY NAME AS410 61.ee-,1 0(6, ,Of N&zy- l
COUNTY Z., r
PERSON COLLECTING SAMPLES slit Gt U
LABORATORY /Yf &LoAaC 1 / Lab Cert. # 3 7'7l `-1
Comments on sample collection or analysis: ,
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR °w/ ef
SAMPLE PERIOD ❑ Ian -June [D-J`uly-Dec
or []monthly' (month]
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply [:]SA
[ Ether ef- • /t.i 5&J
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?z
Outfall No.
Date Sample
Collected"
(mo/dd/yr)
24-rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non-Polar O&G/hoar
Total Petroleum
Hydrocarbons
Total Toxic
Organics5
Benchmarks =__>
09 0� /
100 mg/L or 50 mg/0
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
/
d LST
I . 0
z
0 OOSO
Lp. oo/ O
0.06&
A.73
N ,A-
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with'a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive_receiving water classifications where,the more;protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities Which perform metal finishing opdrations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject,to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31). o
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included,in the Stormwater Pollution Prevention Plan."
Name (Print name)
26,;J
Title (Print ti
(Signature) (Da(e)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX me/C where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Ikon -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
+ TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one co2y of this DMR including all "No Discharge" reports, within 30 days of receipt of the lob results (or at end of monitoring period
in the case o "No Discharge" reports) to: -
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

ASMO Greenville of NC INC
Ms. Pam Savage
1125 Sugg Parkway
Greenville NC, 27834
VMICROBAC@
Fayetteville Division
Certificate of Analysis
Project: Stormwater Sample - Mthly, Outfall
Outfall ##l, grab
K410329-01
Date Reported: 10/07/14
Date Received: 09/10/14
Date Sampled: 09/08/14
Sampled By: Savage
Analyte Result
Units
Analyzed
Analyzed By
Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Copper 0.0050
mg/L
10/02/ l4 16:1 l
SA
EPA 200.8 Rev 5.4
Lead <0,0010
mg/L
10/02/14 16:11
SA
EPA 200.8 Rev 5.4
Zinc 0.066
mg/L
10/02/14 16: l 1
SA
EPA 200.8 Rev 5.4
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Oil & Grease (SGT-HEM)
2.73
mg/L
09/16/14 07:30
JAO
EPA 1664
B
pH
6.2
pH Units
09/23/14 10:15
DSK
SM 4500 H+B-2000
H
*uspended Solids
11.0
mg/L
09/12/14 10:18
SW
(Aqueous)
SM 2540 D-1997
Zinc
0,0116
mg/L
09/29/14 21:45
JAW
SM 3111 B-1999
QC Batch Run - (MicrabacLaboratories, Inc-Chicagoland)
Analyte
Result
Units
Source
RPD
Limit
Copper
0,0213
mg/L
1410741
0.478
20
Zinc
0.201
mg/L
1410741
0.496
20
Copper
0.0252
mg/L
1410712
1.88
20
Zinc
0.218
mg/L
1410712
IA l $
20
QC Batch Run - (A icwbac Laboratories, Inc. - Fayetteville)
1_ Analyte
Result
Units
Source
RPD
Limit
Total Suspended Solids
19900
mg/L
K410324
64
5
Total Suspended Solids
5.00
mg/L
K410257
96
5
Total Suspended Solids
137
mg/L
K410375
5
5
Zinc
0.0650
mg/L
K410169
12
10
Notes and Definitions
• Analyte was prepared and/or analyzed outside of the analytical method holding time
B Detected in the associated Method Blank
Microbac Laboratories, Inc.
Page 1 of 3
9Sa9 14— Mille 0-1 1 Ca..ol+nville k1r, 9wina I ain AAA ia9fl - I ain RAA P77A f 1 un.n.r m�nrnhar rr.m

ASMO Greenville of NC INC
Ms, Pam Savage
1125 Sugg Parkway
Greenville NC, 27834
State Certifications:
NCDNR 9l l
NCDOH 437714
�VMICROBACt
Fayetteville Division
•
Certificate of Analysis
Date Reported: 10/07/14
Projecl: Stormwater Sample - Mthly, Outfall 1 Date Received: 09/10/14
Date Sampled: 09/08/14
Sampled By: Savage
•
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Thank you for your business. We invire,vour feedback wr our levy! ofser vier ro yos. !'Ieasr r:annrcr nc� Uivisiorr Manager, Roh Derrner ar 910-864-1920 with anV
quevions. You may alse) canlacr J. Trevor Bovice, President at presideirf@,mirmbac.com
Microbac Laboratories, Inc.
Page 2 of 3
IrOl W--- 6rti11& 0-. e1 I P�t*^44n 111n Kir' 9RZflA 1 01A RAA i07fl r I ain AAA R77A f I u .n —inr k - —

L'
i
Fayetteville Division 2592 Hope Mills Road •- Fayetteville, NC 28306 (910) 864-19201864-877,6
0
CHAIN o.CUSTODY RECORD o.AE I'�l�dV�l4�G�111�IV'�,
::LIEN7NAME aADDRESS:
iasmo G +wtc
i
V F IC j "-Z$JC •
G roRn,, cce Ca7�
PO
PROJECT ILOCAT}ON: r�'�2M{lJ'4'—tL
QJ-rFat�L
0
m
0
TYPE
OCLANALYSIS
PRESERVATION (CODE)
V '
1
�i
I
�i
{
CODE: A = None
B = HNO3 (pH<2) + <6°C
C = H2SO4 (pH<2) + <13T
D = NaOH + <6°C
E = ZN Acetate + <6°C
F = HCl
G = Sodium Thio
CONTACT PERSON:LLI
�L�T
PHONE.,
0`3141 ` a—y 4 S
;AM PLED BY;
PA"vl &VAG
DATE METHOD OF SHIPMENT:
LAB ID #
SAMPLE TY E
DATE
TIME
COMP
GRAB
PH
FLOW
TEMP -C
R€S'
CHLORINE
SULFIDE
V
L4
"/'/14,-./
VIA
1
Lap
Letlny
Datteee
io
TTkno p
% 7iJ�
Rae ed by: (Sign re)
2
Data
Tlme
tell q hed
//an�te
TI a
=
Ign■ re)
ma
3
7' /U' j
.'d
Vy— 4
641�-
LILL
LI, pp
tell shad by;
Date
Time
Reeelva by; Signature]
Date
Time
5
fi
ph Flaid: ph Field:
Temp Field 1: Temp Field 2:
Water Level #1
Water Level #2
inmais—o.
Turnaround time: EGULAR RUSH
Comments or Special Hazards:
S�i3K 8� WA—CEYL, F CYz-01 (
NC.Gg3c)op�C0C_ NCG%?30<;'S-
IS DATA FOR REG. C PLIANCE PURPOSE?
NO YES WHICH:
Page 3 of 3

J
ASMO GREENVILLE OF NORTH CAROLINA, INC
1125 Sugg Pkwy. PHONE [phone]
GREENVILLE, NC 27834 FAX [phone]
August 29, 2014
RECEIVED
SEP 0 3 2014
CENTRAL FILES
DWOJBOG
NCDENR- Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVED
SEP 0 `; ?n'
CENTRE,. F)LF
Mr,r1� — -
Please find attached the semi-annual storm water discharge monitoring report and analytical
results for period 1 in 2014, for ASMO Greenville of North Carolina, Inc., COC NCG030465.
Under our facility's general NPDES general storm water permit NCG030000, effective
December 4, 2012, we are required to submit quantitative results for two rainfall events
annually on Outfall #1 and record qualitative results semi-annually for inspection.
As a result of two consecutive results over benchmark values for total recoverable zinc, we
increased our sampling to monitor total recoverable zinc levels. Results from the sampling
events at our facility's designated outfall, show a steady decrease in zinc levels. Our July
sampling event shows below benchmark levels. Per our permit requirements we will continue
monthly monitoring and continue with our activities to further reduce sources of zinc in our
storm water in order to maintain below benchmark values.
If you have any questions pertaining to this submittal, please give me a call at 252-754-1765.
Sincerely,
Pam Savage
Environmental Health & Safety
Attachments

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No, NCG030000
Date submitted A-LA-GLt.ST Za, Zp I t-
CERTIFICATE OF COVERAGE NO. NCG03�1 �i(o _ C:;_ SAMPLE COLLECTION YEAR O 1
FACILITY NAME PiSLIAQ 6_; LLB OF NU2� (fA7e0L(t A J .1�. SAMPLE PERIOD v Jan -June ❑July -Dec
f
COUNTY Pi rr
PERSON COLLECTING SAMPLES ! .A-n4 SA -SAG C _
LABORATORY WI 1C "8AC_ C * Z �) Lab Cert. # 3 717I y
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
or ❑ Monthly (month]
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply [:]SA
Other C rQ Sub
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics5
Benchmarks =__>
_
-
100 mg/L or 50 mg/L°
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
C6 1 2-zc)1
r � . f�
S. �
0. 005l
4 o. 0W O
o • v(o (
�-r- 3
N {�
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance.for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
a See General Permit, Table 3 identifying the especially sensitive receivirig wa'ter'cli ssifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample {fo(metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
/)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Storm water Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
D2,.""4 L.X,.W %A-_e
Name (Print name)
6,e,44 e.Y�QALI
Title (Print titl
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date:11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 2 of 3 jr

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO EP--"
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 dovs_o�rece�t of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
l� Tsai
(Date)
Permit Date:11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 3

a
MICROBAC"°
Fayetteville Division
Certificate of Analysis
ASMO Greenville of NC INC Date Reported: 07/05/14
Ms. Pam Savage Project; Stormwater Sample - Mthly, Outfall 1 Date Received: 06/13/14
1125 Sugg Parkway Date Sampled: 06/12/14
Greenville NC, 27834 Sampled By: Client
OF#1
1406450-01
I Analyte Result
Units
Analyzed
Analyzed By _
Method Qualifier
Analyzed by: Microbac laboratories, Inc. - Ghicagoland
Copper 0.0058
mg/L
06/22/14 13:30
SA
EPA 200.8 Rev 5.4
Lead <0.0010
mg/L
06/22/14 13:30
SA
EPA 200.8 Rev 5.4
Zinc 0.066
mg/L
06/22/14 13:30
SA
EPA 200.8 Rev 5.4 B
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Oil & Grease (HEM)
8.37 mg/L 06/26/14 16:53 MSL
EPA 1664 Rev. B
pH
5.7 pH Units 06/16/14 15:20 DSK
SM 4500 H+13-2000 H
(Aqueous)
41 Suspended Solids
16.6 mg/L 06/17/1[4 07:45 JAO
SM 2540D-1997
QC Batch Run - (Microbac Laboratories, Inc. - Chicagoland)
Analyte
Result
Units
Source
RPD
Limit
Zinc
0.164
mg/L
14F 1088
0.0563
20
Copper
0.0203
mg/L
14F1088
2.42
20
Lead
0.181
mg/L
14FI088
1.75
20
Zinc
0.218
mg/L
14171032
2.56
20
Lead 0.193 mg/L 14F1032 2.95 20
Copper 0.0270 mg/L 14F1032 3.68 20
QC Batch Run - (Microbac Laboratories, Inc. - Fayetteville)
I Analyte
Result
Units
Source
RPD
Limit
Total Suspended Solids
3.00
mg/L
1406452
9
5
Total Suspended Solids
5.50
mg/L
1406436
26
5
Total Suspended Solids
16.0
mg/L
1406396
6
5
Notes and Definitions
1. Analyte was prepared and/or analyzed outside of the analytical method holding time
B Blank Contamination
Microbac Laboratories, Inc. � P: ae�1i;nf.Y277- 7

Fayetteville Division 2592 Hope Mills Road -- Fa, aville, NC 28306 (910) 864-19201 864-8774 fax
�VICOBA�
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
ENT NAME& ADDRESS:
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TYPE
OF ANALYSIS
PRESERVATION (CODE)
l,�
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►►►''
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CODE.-' A =None
B = HNO3 (pH<2) + <6"C
C = H2SO4 (pH<2) + <6'C
❑ = NaOH + <6°C
E = ZN Acetate + <6`C
F = NCI
G = Sodium Thio
CONTACT PERSO`N�
/ ''Q�%� '"'4 (iAC E
PHONE:
�Ja Y 7 —7 S L Y 11 �S
RPLEO BY:
DATE! METHOD OF SHIPMENT:
LAB ID #
SAMPLE TYPE
DATE
GRAB
PH
FLOW
TEMP•C
RES.
CHLORINE
SULFIDE
qTIMEECOMP
✓
Lab
Inqu sh b
Date
71ms
Receive d y: i51 natunj
Date
Time
{nqulahed by
to
Tlme
Rece vrd by: (Signature)
Date
Time
3
4
knqulshed by;
oste
Reee —d by: Slgnatura)
DataFirn.
5
iyl--
6
ph Field: ph Field: Water Level #1
Temp Field 9: Temp Field 2: Water Level #2
initiais--►
Turnaround time: REGULAR RUSH
Comments or Special Hazards:
/�6r�f�P rr AICG 0300Ce
o C Al Gf O-Z 4{+/v ,5—
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICH:
0

ASMO GREENVILLE OF NORTH CAROLINA, INC
1125 Sugg Pkwy. PHONE [phone]
GREENVILLE, NC 27834 FAX [phone]
December 21, 2011
NCDENR- Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVED
MAR - 8 2012
DWQ-WARO
Please find attached the semi-annual storm water discharge monitoring report and analytical
results for period 2 in 2011, for ASMO Greenville of North Carolina, Inc., COC NCG030465.
Under our facility's general NPDES general storm water permit NCG030000; effective
November 1, 2007, we are required to submit quantitative results for two rainfall events
annually on Outfall 41 and record qualitative results semi-annually for inspection.
Results from the sampling event at our facility's designated outfall, completed on 11/4/11, show
compliance with applicable parameters. Due to the location of our certified lab and the time it
takes to reach the lab, testing for pH was completed at the time of sampling on -site.
If you have any questions pertaining to this submittal, please give me a call at 252-754-1765.
Sincerely,
Pam Savage
hnvironmental Health & Safety
Attachments
�-
6,
is u.
DV�
Li

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCG030000 SAMPLES COLLECTED DURING CALENDAR YEAR: .20 f 1
CERTIFICATE OF COVERAGE NO. NCG03� t b �(This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME A5-�" o E2 � us L-Uti Op N c �.,c . COUNTY
PERSON COLLECTING SAMPLES ,q �,.t 5.� G L -PHONE NO. (c ) -75L4- 4 oa O
CERTIFIED LABORATORY [ ( Lab # -�-t-
Lab # PLEASE SIGN ON THE REVERSE 4
Part A: Specific Monitoring Requirements
Ot
'16s3
0;.:.'t'
Saa
aSuspe
9.4�
Q
'd"'IL E
Oil ana'Gr
Toe
arEY
-
�
'
d
rol:ut
1
0
tlilaBencnark'
0 433i
I
.
OF' I
4l 04if
5 ,`-1
l,S
{SFO
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Trier or Tier 2 res` �'d
See General Permit text.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes ✓o
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
h Outf$U �..
Date tY
r
'y5 r wa4556.s ,
TI. Crease,
-
�as12...... ,>s
c Total Snspeiided Solids,
r `. ';r
iS pH,�
yam_ 1.,
; NewMotar..0il ilsa e,
ci
.},
Sample Goilecteii,,ti
, k,'r
.. ,.'-- M+4w, 7rY.
.;:•a µ
i
1 "e allmo
,^:,::Standardtunits . r
.:Atiniial av:.e a
Beo�hnnarli
r:i
k i I k
i7i
y
rrw
..o..:.9:0
Y w s=
,:06l
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
STORM EVENT CHARACTERISTICS:
Date (first event sampled)
Total v nt Precipitation (inches): 0 • Z.
Date I I f r (List each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches): 0 , d
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SWU-245-102107
Pagel of 2

1 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or
manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject
to the requirement to sample (for metal finishing use the definition as found' in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for
electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent
management plain shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the
discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I
certify that to the best of my knowledge and belief, no dumping of concentrated toxic,organics into the stormwater or areas which are exposed to rainfall or stormwater
runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management
plan included in the Stormwater Pollution Prevention Plan."
L.4-- she
Name (Print name) ...
Title (Print title)
(Signature) (Date)
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is,' to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
z/ ,e. a./I
(Date)
S WU-245-102107

N
Fayetteville Division
2592 hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
mum
ASMO Greenville of NC INC Date Reported: November 30, 2011
Ms. Pam Savage Project: Stormwater Sample - Outfall !
1125 Sugg Parkway Date Received: November 04, 201
Greenville NC, 27834 Sampled By: Pam Savage Date Sampled: November 04, 2011
1111089-01
Outfall #11
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Fayetteville Division
Lead
1.51
ug/L
11/10/11
18:16
JAW
SM 3113 B
Oil & Grease (HEM)
<5.00
mg/L
1 1/9/1 1
18:00
JAW
EPA 1664
PH
5.55
pH Units
11/7/11
16:08
DSK
SM 4500 H+B
1'I
Total Suspended Solids
19.2
mg/L
1119/1 1
16:30
JAW
SM 20th Ed. 2540 D
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Surrogale: DecachlorohiphenjI
40,0 %
26% -
116%
1111112011
18:OKP
EPA 608 Rev 7195
Surrogate: Tetrachloro-in-v3,lene
70, 0 %
40% -
130%
1111112011
18: OKP
EPA 608 Rev 7195
4,4'-DDD
<0.00099
mg/L
11/11/1 1
18:08
EP
EPA 608 Rev 7/95
U
4,4'-DDE
<0.00099
mg/L
11/11/1 1
18:08
EP
EPA 608 Rev 7/95
U
4,4'-DDT
<0.00099
mg/L
11/11/11
18:08
EP
EPA 608 Rev 7/95
Ua
Aldrin
<0.00099
mg/L
11/11/11
18:08
EP
EPA 608 Rev 7/95
U
alpha-BFIC
<0.00099
mg/L
1 I/11/11
18:08
EP
EPA 608 Rev 7/95
Ua
Aroclor 1016
<0.00099
mg/L
1I/12/11
0:13
clr
EPA 608 Rev 7/95
Ua
Aroclor 1221
<0.00099
mg/L
1 I/12/1 1
0:13
clr
EPA 608 Rev 7/95
Ua
Aroclor 1232
<0.00099
mg/L
11/12/11
0:13
clr
EPA 608 Rev 7/95
Ua
Aroclor 1242
<0.00099
mg/L
11/12/11
0:13
clr
EPA 609 Rev 7/95
Ua
Aroclor 1249
<0.00099
rn&,/L
11/12/11
0:13
clr
EPA 608 Rev 7/95
Ua
Aroclor 1254
<0.00099
mg/L
11/12/11
0:13
clr
EPA 608 Rev 7/95
Un
Aroclor 1260
<0.00099
mg/L
11/12/11
0:13
clr
EPA 608 Rev 7/95
U,l
Aroclor 1262
<0.00099
mg/L
11/12/11
0:13
clr
EPA 608 Rev 7/95
Ua
Aroclor 1268
<0.00099
mg/L
11/12/11
0:13
clr
EPA 608 Rev 7/95
Ua
beta-BHC
<0.00099
mg/L
1 1/1 Ill 1
18:08
EP
EPA 608 Rev 7/95
U
Chlordane
<0.0099
mg/L
11/1 1/11
18:08
EP
EPA 608 Rev 7/95
U
delta-BHC
<0.00099
mg/1-
1 1/1 Ill 1
18:08
EP
EPA 608 Rev 7/95
Un
Dieldrin
<0 00099
mg/L
11/11/1 1
18:08
EP
EPA 608 Rev 7/95
U
Endosulfan 1
<0.00099
mg/L
1 Ili 1/11
18:08
EP
EPA 608 Rev 7/95
U
Endosulfan 11
<0.00099
mg/L
11/11/11
i8:08
EP
EPA 608 Rev 7/95
Ua
Endosulfan sulfate
<0.00099
mg/L
11/11/1 1
18:08
EP
EPA 608 Rev 7/95
U
Endrin
<0.00099
mg/L
11/1 1/1 1
18:08
EP
EPA 608 Rev 7/95
U
State Certifications:
Respectfully Submitted
NCDNR #11
(�l
NCDOH #37714
&Iffl R
USDA #3787
Robert Dermer, Division Manager
Thank you for your business. We incite urur Jreclhuck urr nrrr lercl
oJ'srrvic'c[ rn yuu. I7r<ne
c'rrurucr rhr
!)iri.vorr blurr r�er,
Hrnc�rl Ik+rrncral
rJlfl-N(�-!J2(l, .lunres Arok�+, 1'rccculrnr,
u1
janecc nukc.r(ifbnic'rnhuc, cnm ctr "1're+'ur Rnl'c'r.
('F, r), ur rrCt'ur, hnl cr
u:ruicmhac•. rnn+ a irJr ura Y cnnrmcrrrs or
su,[;};rsrioux,
Page
I of_ 7

(31
Fayetteville Division
2592 Flope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
ASMO Greenville of NC INC
Ms. Pam Savage Project: Stormwater Sample - Outfall 1 Date Reported: November , 2011
04201 i
1125 Sugg Parkway Date Received: November
Greenville NC, 27834 Sampled By: Pam Savage Date Sampled: November 04, 2011
1111089-01
Outfall #1
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Endrin aldehyde
<0.00099
mg/L
1l/l 1/11
18:08
EP
EPA 608 Rev 7/95
Ua
Endrin Ketone
<0.00099
mg/L
1 Ill 1/11
18:08
EP
EPA 608 Rev 7/95
U
gamma-BHC
<0.00099
mg/L
1 Ill 1/11
18:08
EP
EPA 608 Rev 7/95
Ua
Heptachlor
<0.00099
mg/L
1 Ill1/1l
18:08
EP
EPA 608 Rev 7/95
Ua
Heptachlor epoxide
<0.00099
mg/L
1 Ill 1/11
18:08
EP
EPA 608 Rev 7/95
U
Methoxychlor
<0.0050
mg/L
11/11/11
18:08
EP
EPA 608 Rev 7/95
U
Total PCB's
<0.00099
mg/L
1 1/12/11
0:13
clr
EPA 608 Rev 7/95
Ua
Toxaphene
<0.0099
mg/L
11/1 I/11
18:08
EP
EPA 608 Rev 7/95
U
Surrogate: 1, 2-DOrloroerhane-D4
101 %
80% -
132%
1111712011
15:3Rn
EPA 624 Rev 7195
Surrogate; 4-Bromofluorobenzene
99.9 %
80% -
120%
1111712011
15:3A'n
EPA 624 Rev 7195
Surrogate: Dibranofluoromethmre
100 %
80% -
120%
1111712011
15: 3gn
EPA 624 Rev 7195
Surrogate: Toluene-D8
103 %
80% -
120%
1111712011
15:3)'n
EPA 624 Rev 7195
1, 1, 1 -Trichloroethane
<0.0010
mg/L
11/17/11
15:39
jIn
EPA 624 Rev 7/95
U
1,1,2,2-Tetrachloroethane
<0.0010
mo-
11/17/11
15:39
jIn
EPA 624 Rev 7/95
U
1,1,2-Trichloroethane
<0.0010
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95
U
1, 1 -Dichloroethane
<0.0010
ing/L
11/17/11
15:39
jIn
EPA 624 Rev 7/95
U
1, l-Dichloroethene
<0.0010
mg/L
11/17/11
15:39
jIn
EPA 624 Rev 7/95
U
1,2-Dichlorobenzene
<0.0020
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95
U
1,2-Dichloroethane
<0,0010
Mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95
U
1,2-Dichloropropane
<0.0010
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95
U
1,3-Dichlorobenzene
<0.0020
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95
U
1,4-Dichlorobenzene
<0.0020
mg/L
11/17/11
15:39
jIn
EPA 624 Rev 7/95
U
2-Chloroethyl vinyl ether
<0.0020
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95
U
2-Hexanone
<0.0050
mg/L
11/17/I1
15:39
jIn
EPA 624 Rev 7/95
U
Acetone
0.015,
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95
Benzene
<0.0010
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95
U
Bromodichloromethane
<0.0010
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95
U
Bromoform
<0.0010
mg/L
11/17/11
15:39
jIn
EPA 624 Rev 7/95
U
Bromomethane
<0.0020
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95
U
State Certifications:
Respect Submitted
NCDNR #11
NCDOH #37714
f/JiG]
�� Q �'
USDA #3787
Robert Dermer, Division Manager
Thank you for your business. iNc inrirc roar lcrdhrrck our our lrrrl o):+rn icr Nr
you. Ylrur.a+ runrurr rhr 1)iei.rrun A4crrr«} cr,
Ruhcrr !)rrrarr ar )f U-N(,d-lJ20, Jmrrec Mokr.+, f'residcnr, W
jumcs.rxrkcw a ruicruhrrc.cnnr ur '1'rcvrrr Ruycc,
('h,Y1, ur rruvur•, hnyce
n rrricrr>buc•. coot
H'irlt rntr
cununrrtl.v or +'tr��afinna,
Page 2 o F 7

L
Fayetteville Division
2592 Mope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
ASMO Greenville of NC INC Date Reported: November 30, 2011
Ms. Pam Savage Project: Stormwater Sample - Outfall 1
1 125 Sugg Parkway Date Received :November 04, 2011
Greenville NC, 27834 Sampled By: Pam Savage Date Sampled: November 04, 2011
lll1089-01
Outfall #1
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac laboratories, Inc. - Chicagoland
Carbon Disulfide
<0.0020
Carbon tetrachloride
<0.0010
Chlorobenzene
<0.0010
Chloroethane
<0.0020
Chloroform
<0.0010
Chloromethane
<0.0020
cis-1,3-Dichloropropene
<0.0010
Dibromochloromethane
<0.0010
Ethylbenzene
<0.0010
Methylene chloride
<0.0020
Methyl-t-Butyl Ether
<0.0020
Tetrachloroethene
<0.0010
Toluene
<0.0010
trans-1,2-Dichloroethene
<0.0010
trans-1,3-Dichloropropene
<0.0010
Trichloroethene
<0.0010
Trichlorofluoromethane
<0,0010
Vinyl Acetate
<0.0010
Vinyl chloride
<0.0020
Total 1,2-Dichloroethene
<0.0010
Total Xvlenes
<0.0010
Surrogate: 2,4,6-Trrhromophenol
101 °/0
Surrogate: 2-Fl uorobrphen),l
44,8 Yo
Surrogate: 2-Flrrorophenol
31.7 Yo
Surrogate: Afarohen_ene-d5
40.8 Yo
Surrogate: Phenol -di
265 %
Surrogate: Terphen),1414
59.0 YO
l ,2,4-'I'richlorobenzene
<9.9
1,2-Dichlorobenzene
<9.9
State Certifications:
NCDNR #11
NCDCH #37714
USDA #3787
mg/L
11/17/11
15:39
itn
EPA 624 Rev 7/95 U
mg/L
1 I/17/1 1
15:39
iln
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
iln
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
iln
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
iln
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
iln
EPA 624 Rev 7/95 U
mg1L
11/17/11
15:39
iln
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
jln
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
iln
EPA 624 Rev 7/95 U
mg/L
11 / 17/ 1 1
15:39
On
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
i in
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
iln
EPA 624 Rev 7/95 U
mg/L
11 / 17/ 1 1
15:39
On
EPA 624 Rev 7/95 U
mg/L
11 /17/1 1
15:39
On
EPA 624 Rev 7/95 U
mg/L
1 I/17/1 1
15:39
On
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
On
EPA 624 Rev 7/95 U
mg/L
1 1/17/1 1
15:39
iln
EPA 624 Rev 7/95 U
mg/L
1 1/17/1 1
15:39
iln
EPA 624 Rev 7/95 U
mg/L
11/17/11
15:39
iln '
EPA 624 Rev 7/95 U
47.8%
- 138%
11/1112011
14:2BR
EPA 625 Rev 7/95
100/0-
110%
1111112011
14:2BR
EPA 625 Rev 7/95
10% -
110%
1111112011
14: 2BR
EPA 625 Rev 7/95
10% -
110'%
1111112011
14: 2BR
EPA 625 Rev 7/95
10% -
60.8%
1111112011
14. 2BR
EPA 625 Rev 7/95
16.8%
- 110%
1111112011
14:2BR
EPA 625 Rev 7/95
µg/L
11 / 11 / 1 l
14:23
BR
EPA 625 Rev 7/95
µre L
11/I 1/11
14:23
BR
EPA 625 Rev 7/95
Respectfully Submitted
X '
Robes termer, Division Manager
Thank you for your business. We iuvirc yvrrr.jecdhurk a,r uur ka el n/: rrvfe¢ iu ymc !'Ira.cc cnr,rucl the Di+isin,v Alurrcrgcr, ltr,herr 1)ern,er rri J10-,Y(1-1)2(1, .Irrrncc Nnkc.+, Pru.r;denr, rer
jrw,e.+.rrnk�.v(r�nricrnhuc.cvne nr 1'rcrnrNgpc'c. C!s(i, u, rr¢'+•ur.hurx'r(r�rnkv-rdrur.cur+, H'irh rnrVcumntrrrr.v ursrrs;�;C.vrings.
Page 3 of 7

Fayetteville Division
2592 I -lope Mills Rd
Fayetteville, NC: 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
ASMO Greenville of NC INC
Ms. Pam Savage Project: Stormwater Sample - Outfail I Date Reported: November 30, 2011
1125 Sugg Parkway Date Received: November 04, 2011
Greenville NC, 27834 Sampled By: Pam Savage Date Sampled: November 04, 2011
1111089-01
Outran #1
Analyte Result Units Analvzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc.
1,2-Diphenylhydrazine
l,3-Dichlorobenzene
1,4-Dichlorobenzene
2,2'-oxybis(1-chloropropane)
2,4,5-Trichlorophenol
2,4,6-'rri c h to ropheno I
2,4-Dichlorophenoi
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluenc
2,6-Dichlorophenol
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methy1naphthalene
2-Methylphenol
2-Nitroaniline
2-N itrophenol
3,3'-Dichlorobenzidine
3/4-Methyl phenol
3-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenyl phenyl ether
4-ChToro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
State Certifications:
NCDNR #11
NCDOH #37714
USDA #3787
Chicagoland
<9.9
pg/L
1l/11/11
14:23
BR
EPA 625 Rev 7/95
<9.9
µglL
1 1/1 Ill 1
14:23
BR
EPA 625 Rev 7/95
<9.9
µg/L
1 l/11/11
14:23
BR
EPA625 Rev 7/95
<9.9
pg/L
1 1/1 I/11
14:23
BR
EPA 625 Rev 7/95
<9.9
µg/L
11/11/1 1
14:23
BR
EPA 625 Rev 7/95
<9.9
µg/L
11/l 111 1
14:23
BR
EPA 625 Rev 7/95
<9.9
}tg/L
11/11/1 1
14:23
BR
EPA 625 Rev 7/95
<9.9
pg/L
11/1 1/1 1
14:23
BR
EPA 625 Rev 7/95
<50
ug/L
11/1 l/11
14:23
BR
EPA 625 Rev 7/95
<9.9
Ag/L
11/11/1 1
14:23
BR
EPA 625 Rev 7/95
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
<9.9
1tg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
<9.9
ug/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
<9.9
pg/L
11/1 1/1 1
14:23
BR
EPA 625 Rev 7/95
<99
µg/L
I1/11/11
14:23
BR
EPA 625 Rev 7/95
<99
dug/l,
11/1 l/11
14:23
BR
EPA 625 Rev 7/95
<9.9
pg/L
I1/1 l/11
14:23
BR
EPA 625 Rev 7/95
<9.9
µg/l_
11/1 1/1 1
14:23
BR
EPA 625 Rev 7/95
<50
µg/L
11/1 l/11
14:23
BR
EPA 625 Rev 7/95
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7195
<9,9
µg/L
11/1 1/1 l
14:23
BR
EPA 625 Rev 7/95
<25
µg/L
11/1 111 1
14:23
BR
EPA 625 Rev 7/95
<9.9
µg/L
11/1 1/1 1
14:23
BR
EPA 625 Rev 7/95
<20
µg/L
11/11/1 l
14:23
BR
EPA 625 Rev 7/95
<9.9
µg/L
11/11/1l
14:23
BR
EPA 625 Rev 7/95
<9.9
µg/L
11/11/1 l
14:23
BR
EPA 625 Rev 7/95
<9.9
pg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
<50
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
<9.9
pg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
<9.9
pg/L
11/11/1 l
14:23
BR
EPA 625 Rev 7195
ReSpeCtfLlIlY Sub_ntitte�etl
Robert Denver, Division Manager
Thank you for your business. We unwe voter feedback on nur ler•el of scrrlce to Pnu. Plena• comacr the Owimon hlanager. Roherf !)caner a7 910-H64-1920, ,famo Mikes, Precidenr, of
yiwc.Y.rwkes R wicrohac.com or Dvvor Nopce.(31'0,al Irerur.hO)cv0Poncrohac.coin with anY connnenek or 4ggemon.c.
Page 4 01.7

Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910,864.8774 Fax
Certificate of Analysis
ASMO Greenville of NC INC Date Reported: November 30, 2011
Ms. Pam Savage Project: Stormwater Sample - Outfall 1
1 125 Sugg Parkway Date Received: November 04 2011
Greenville NC, 27834 Sampled By: Pam Savage Date Sampled :November 04, 2011
I111089-01
Outfall #1
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Acetophenone
<9.9
µg/L
1 1/1 Ill 1
14:23
BR
EPA 625 Rev 7/95
Aniline
<9.9
µg/L
1 1/1 Ill 1
14:23
BR
EPA 625 Rev 7/95
Anthracene
<9.9
µglL
11/11/11
14:23
BR
EPA 625 Rev 7/95
Benzidine
<50
µg/L
11/14/11
8:59
BR
EPA 625 Rev 7/95
Benzo[a]anthracene
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Benzo[a]pyrene
<9.9
µr= L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Benzo[b]fluoranthene
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Benzo[g,hj]perylene
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Benzo[k]fluoranthene
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Benzoic acid
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Benzyl alcohol
<9.9
µg/L
WWII
14:23
BR
EPA 625 Rev 7/95
Bis(2-chloroethoxy)methane
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Bis(2-chloroethyl)ether
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Bis(2-ethylhexyl)phthalate
<9.9
µg/L
1 Ill 1/11
14:23
BR
EPA 625 Rev 7/95
Butyl benzy] phthalate
<9.9
µg/L
1 Ill 1/i 1
14:23
BR
EPA 625 Rev 7/95
Carbazole
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Chrysene
<9,9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Dibenz[a,h]anthracene
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Dibenzofuran
<9.9
µr= L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Diethyl phthalate
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Dimethyl phthalate
<9.9
µg/L
11/1 1/1 1
14:23
BR
EPA 625 Rev 7/95
Di-n-butyl phthalate
<9.9
µg/L
1 ]/1 1/H
14:23
BR
EPA 625 Rev 7/95
Di-n-octyl phthalate
<9.9
µg/L
11/1 1/1 1
14:23
BR
EPA 625 Rev 7/95
Fluoranthene
<99
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Fluorene
<9.9
µg/L
i l/11/11
14:23
BR
EPA 625 Rev 7/95
Hexachlorobenzene
<9,9
µg/L
11/1 1/1 l
14:23
BR
EPA 625 Rev 7/95
Flexaehlorobutadiene
<9,9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
llexachlorocyclopentadiene
<9.9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Hexachloroethane
<9,9
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
Indeno[1,2,3cd]pyrene
<9.9
µg/L
11/11/11
1423
BR
EPA 625 Rev 7/95
State Certifications:
Respect Submitte
NCDNR #11
NCDQH #37714
i/liG]��
'
USDA #3787
Robert Dermer, Division Manager
Thank you for your business. We
inrire yurrr, fi crlhack ux
urrr lercl oJ'ren ice rn yvu, /Yerue
contact dre DWI., lot) dlunrrl er,
knhcrl Ucrmer ❑r rJl b-Nfia-1 rJ211, ,lunrr.r Nake: 14x cir/enr, ar
rrnmac.noker a nucrvrhuc•.crnn or 7ivvor
Bruce, (J:U, at rrevor.bovice(ynricrobac.com with on),
-
corrrnrerrr.= or su��esrinrrs.
Page Saf7

J
Fayetteville Division
2592 1 lope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phonc
910.864.8774 Fax
Certificate of Analysis
ASMO Greenville of NC INC Date Reported: November 30, 2011
Ms. Pam Savage Project: Stormwater Sample - Outfall
1125 Sugg Parkway Date Received: November 64 2011
Greenville NC, 27834 Sampled By: Pam Savage Date Sampled: November 04. 2011
ll11089-01
Outfall #1
Analyte _ - Result Units Analvzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Isophorone
<99
Naphthalene
<9.9
Nitrobenzene
<99
N-Nitrosodimethylamine
<9.9
N-Nitrosodi-n-propylamine
<9.9
N-NitrosodiphenyIamiIte
<9.9
Pentachlorophenol
<50
Phenanthrene
<9.9
Phenol
<9.9
Pyrene
<9.9
Pyridine
<9.9
2,3,7,8-Tetrachlorodibenzo-p-dioxin Negative
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
µg/L
11/11/1 1
14:23
BR
EPA 625 Rev 7/95
µg/L
11/11/1 1
14:23
BR
EPA 625 Rev 7/95
µg/L
11/1 1/1 l
14:23
BR
EPA 625 Rev 7/95
µg1L
1l/11/11
14:23
BR
EPA 625 Rev 7/95
µg/L
11/11/11
14:23
BR
EPA 625 Rev 7/95
µg/L
11/1 I/11
14:23
BR
EPA 625 Rev 7/95
µg/1_
1 1111 / l 1
14:23
BR
EPA 625 Rev 7/95
µg1L
1 1/1 Ill 1
14:23
BR
EPA 625 Rev 7/95
Ng/1-
1 1/1 Ill 1
14:23
BR
EPA 625 Rev 7/95
µg/L
11/1I111
14:23
BR
EPA 625 Rev 7/95
Pos/Neg
1 1/1 I / l 1
14:23
BR
EPA 613
1111089-01 REl
Outfall #1
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Chicagoland
Surrogale: DeccichlorobipheRYl .50.0 % 26% - 116% 1111212011 0:1-Or EPA 608 Rev 7195
Surrogate: 7M-tichloro-m-xylene 75.0 % 40% - 130% 1111212011 0:11•Ir EPA 608 Rev 7195
State Certifications:
NCDNR #11
NCDOH #37714
USDA 93787
RespflGmUtft`Ily Submitted
h
Robert Deerr`m++err, Division Manager
Thank you for your business. We mow k ouo- Jcedhack on our level q/survic(, in t'ou. Heme comaci the Uividon Manager, Robert 0(!rux,r n 91 U-M4-1'91U, ,lamesNoke.,, Premdem, al
rames.nokva a nricrrrhac.com or ')-evor linvice. 0" ). of rrrrur. hn�� recayuct'( daeXon? xiih airY cummunA nr supwemiotm
Page 6 r)l 7

Fayetteville Division
2592 Elope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
9110.864.8774 Fax
Certificate of Analysis
ASMO Greenville of NC INC
Ms. Pain Savage Project: Stormwater Sample - Outfall 1 Date Reported: November 30, 201 1
1 125 Sugg Parkway 'Date Received: November 04, 2011
Greenville NC, 27834 Sampled By: Pam Savage Date Sampled: November 04, 2011
Notes and Definitions
Ua Undetected
U Analyle included in the analysis. but not dciected
Analyte was prepared and/or analyzed outside ofthe analytical method holding lime
State Certifications:
NCDNR #11
NCDOH #37714
USDA #3787
Respectfully
olSubmitted
IRhe_rrtt�Dermer, Division Manager
Thank you for your business. We o vrrc yvnrr Jeedhock on orrr level uf.svmce ro ron. Plea,w conku7 the Division Manager. Roherr Uernrer ar 910-864-1920, ,$mrec Nokrs, Pre'drlenr, al
jonvea.rrokerrrrnricrohoc,corn or Trevor Boyce, Ch"O, w rry ror.IrorceGAnrhr nhrrc.conr with onv ronumgat orAugg Arians,
h:1gL'7rt-7

QD
CASE NARRATIVE Date: Tuesday, November 22, 2011
Client: Microbac - Fayetteville Division
Project: 1111089 - General
Lab Order: 11K0452
The Laboratory Control Spike Duplicate associated with the 1111089-01 sample failed the precision criteria
for Dibenz[ah]antracene. The accuracy criteria were met by both the LCS and LCSD.
The Laboratory Control Sample and Laboratory Control Sample Duplicate associated with the 1111089-01
sample failed the acceptance criteria for Bromomethane. This is considered insignificant, as the bias was
high yet the sample concentration was below the reporting limit.
250 West 84th Drive, Merrillville, IN 46410 TE1,.800.536.8379 TEI.,.219.769.8378 FAX.[phone]
Page 3 of 10

Analvtieal Results Date: Tuesday, November22, 2011
Client: Microbac - Fayetteville Division
Client Project: 1111089 - General
Client Sample ID: 1111089-01 Work Order/ID: 11 K0452-01
Sample Description: Sampled: 11/04/2011 0:00
Matrix: Aaueous Received: 11/10/2011 9:30
Analyses AT Result RL Qual Units DF Analyzed
Method: EPA 608 Rev 7105 Analyst: EP
Pesticides/PCBs Prep Method: SW846 35108 Prep Daterrime: 1 Ill 112011 09:57
4,4.-DDD
A
<0.00099
0.00099
U
mg1L
1
11/11/2011 18:08
4,4'-DDE
A
< 0.00099
0.00099
U
mg1L
1
1111112011 18:08
4,4'-DDT
A
<0.00099
0.00099
mglL
1
11/11/2011 16:08
Aldrin
A
c 0.00099
0.00099
U
mg1L
1
11/11/2011 18:08
alpha-BHC
A
<0.00099
0,00099
mglL
1
11/11/2011 18:08
Aroclor1016
A
<0,00099
0,00099
U
mg1L
1
11/12/2011 0:13
Arodor 1221
A
<0,00099
0.00099
U
mglL
1
11/12/2011 0:13
Aroclor 1232
A
<0.00099
0.00099
U
mglL
1
11/12/2011 0:13
Aroclor1242
A
<o.00099
0,00099
U
mg1L
1
11/12/2011 0:13
Arodor 1248
A
<0.00099
0.00099
U
mg1L
1
11/12/2011 0:13
Arodor 1264
A
<0.00099
0.00099
U
mg1L
1
11/12/2011 0:13
Aroclor1260
A
<0.00099
0,00099
mg/L
1
11/12/2011 0:13
Arodor 1262
A
<0,00099
0,00099
U
mg1L
1
11/12/2011 0:13
Arodor 1268
A
< 0.00099
0.00099
U
mg1L
1
11112/2011 0:13
beta-BHC
A
<0.00099
0.00099
U
mg1L
1
11/1112011 18:08
Chlordane
A
<0.0099
0.0099
U
mg1L
1
11/11/2011 18:OB
delta-BHC
A
<0,00099
0.00099
mg1L
1
11/11/2011 18:08
Dieldrin
A
<0.00099
0.00099
U
m91L
1
1 1111112011 18:08
Endosulfan I
A
<0.00099
0.00099
U
mg1L
1
1111112011 18:08
Endosulfan Il
A
< 0,00099
0.00099
mg1L
1
11/11/2011 18:08
Endosulfan sulfate
A
<0.00099
0.00099
U
mg1L
1
11/11/2011 18:08
Endrin
A
<0.00099
0.00099
U
mglL
1 -
11/11/2011 18:08
Endrin aldehyde
A
<0.00099
0.00099
mglL
1
11/11/2011 18:08
Endrin Ketone
A
<0,00099
0.00099
U
mglL
1
11/11/2011 18:08
gamma-BHC
A
c0.00099
0.00099
mg1L
1
11/11/2011 18:08
Heptachlor
A
<0.00099
0.00099
mglL
1
11/111201t 18.08
Heptachlor epoxide
A
< 0.00099
0.00099
U
mg1L
1
11/11/2011 18:08
Methoxyehlor
A
< 0.0050
0.0050
U
mglL
1
t 1 /1112011 18:08
Total PCB's
A
< 0,00099
0.00099
mglL
1
11112/2011 0:13
Toxaphene
A
<0.0099
0.0099
U
mglL
1
11/11/2011 18.08
Surr: Decachlorobipheny1
1
50.00
26.116
%REC
1
11/12/2011 0:13
Surr: Decachlorobiphenyl
1
40.00
26-116
%REC
1
1 11/11/2011 18:08
Sum- Tetrachloro-m-xylene
1
70.00
40-130
%REC
1
11/11/2011 18:08
Surr. Tetrachloro-m-xylene
1
75.00
40-1.30
%REC
1
11/12/2011 0:13
Semivolatile Organic Comuounds
Method: EPA 625 Rev 7195
Prep Method: SW846 3510
Analyst: BR
Prep DaterTime:1 Ill112011 07:35
1,2,4-Trichlorobenzene
A
<9.9
9.9
NgIL
1
1V1112011 14:23
1,2-Dichlorobenzene
A
<9.9
9.9
pg1L
1
11/11/2011 14:23
1,2-Diphenylhydrazine
A
< 9,9
9.9
pg1L
1
1111112011 14:23
1,3-Dichlorobenzene
A
<9.9
9.9
NgIL
1
11/11/2011 14:23
1,4-Dichlorobenzene
A
<9.9
9.9
NgIL
1
11/11/2011 14:23
250 West 84th Drive, Merrillville, 1N 46410 TEL.800.536,8379 T171-219.769.8378 FAX.[phone]
Page 4 of 10

Analytical Results Date: Tuesday, November22, 2011
Client:
Microbac - Fayetteville Division
Client Project:
1111089 - General
Client Sample ID:
1111089-01
Work Order/ID:
11K0452-01
Sample Description:
Sampled:
11/04/2011 0:00
Matrix:
Aqueous
Received:
11/10/2011 9:30
Analyses
AT Result
RL Qual Units DF
Analyzed
Method:EPA 625 Rev 7195 Analyst:BR
Semivolatile Organic Comaounds Prep Method: SW846 3510 Prep DaterTime: 111111201107:35
2,2'- _ is(i-chloropropane)--
2,4,5-Trichlorophenol
A
<9.9
9.9
pg/L
1
11/11/2011 14:23
A
<9.9
9.9
p91L
1
1111112011 14:23
2,4,6-Trichlor2phenol
A
< 9.9
9.91
IP91L
1
1111/12011 14,23
2,4-Dichlorophenol
A
<9.9
9.9
NgIL
1
1111112011 14:23
2,4-Dimethylphenol
A
<9.9
9.9
NgIL
1
11/11/2011 14:23
2,4-Dinitrophenol
A
<50
N 50
p91L
1
11/11/2011 14:23
2,4-Dinitrotoluene
A
< 9.9
9.9
pg/L
1
1111112D11 14:23
2,6-Dichlorophenol_
A
<9.9
9.9
pg1L
1
11/11/2011 14:23
2,6-Dinitrotoluene
A
<9.9
9.9
p91L
1
11/11/2011 14:23
2-Chloronaphthalene
A
<9.9
9.9
pg1L
1
11/11/2011 14:23
2-Chlorophenol
A
<9.9
9.9
pg1L
1
11/11/2011 14:23
2-Methylnaphthalone
A
<9.9
9.9
pg1L
1
1ill 1/2011 14:23
2-Methylphenol
A
< 9.9
9.9
p91L
1
11/11/2011 14:23
2-Nitroaniline
A
<9.9
9.9
pg/L
1
11/11/2011 14:23
2-Nitrophenol
A
<9.9
9.9
JP9IL
1
11/11/2011 14:23
3,3'-Dichlorobenzidine
A
<So
50
pg1L
1
1111112011 14:23
314-Methylphenol
A
<9.9
9.9
pg/L
1
11111/2011 14:23
3-Nitroaniline
A
<9,9
9.9
pg/L
1
11/11/2011 14:23
4,6-Dinitro-2-methylphenol
4-13romophenyl phenyl ether
4-Chloro-3-methy_Iphenol
4-Chloroaniline
A
<25
25
pgrL
1
1 11/11/2011 14:23
A
<9.9
9.9
jP91L
1
11/11/2011 14:23
A
<20
20
pglL
1
1111112011 14:23
A
<9.9
9.9
pg1L
1
1111112011 14',23
4-Chlorophenyl phenyl ether
4-Nitroaniline
A
<9.9
9.9
pg1L
1
11/11/2011 14:23
A
<9.9
9.9
pg1L
1
11/11/2011 14:23
4-Nitrophenol
A
<50
50
pg1L
1
1 11/11/2011 14.23
Acenaphthene
A
<9.9
9.9
pg/L
1
11/11/2011 14:23
Acenaphthylene
A
<9.9
9.9
pg/L y
1
11/1112D11 14:23_
Acetophenone
A
< 9.9
9.9
pg1L
1
11/11/2011 14:23
Aniline
A
<9.9
9.9
pg1L
1
11/11/2011 14:23
Anthracene
A
<9.9
9.9
pg/L
1
11/11/2011 14:23
Benzidine
A
< 50
50
pg1L
1
11/14/2011 8:59
Benzo[a]anthracene
A
I <9.9
9,9
pg11-
1
11/1112011 14:23
Benzo[a]pyrene
A
<9.9
9.9
pg/L
1
1Ill 112D11 14:23
Benzo[b]fluoranthene
A
<9.9
9.9
pg1L
1
11/11/2011 14:23
Benzo[g,h,i]perylene _
Benzo[k]fluoranthene
A
< 9.9
9.9
pg/L
1
11111/2011 14:23
A
<9.9
9.9
pg/L
1
11/11/2011 14:23
Benzoic acid
A
<9.9
9.9
pg1L
1
1111112011 14:23
Benzylalcohol
A
<9.9
9.9
pg/L
1
11/11/2011 14:23
Bis(2-chloraethoxy)methane
Bis(2-chloroethyl)ether _
Bis(22thylhexyl)phthatate
A
<9.9
9.9
pg1L
1
11/11/2011 14:23
A
<9.9
9.9
pglL
1
11111/2011 14:23
A
< 9.9
9.9
pg/L
1
1111112/111 14:23
250 West 84th thrive, Merrillville. IN 46410 TEL.[phone] TEL,.219.769.8378 FAX.[phone]
Page 5 of 10

u
Analytical Results Date: Tuesday, November 22, 2011
Client: Microbac - Fayetteville Division
Client Project: 1111089 - General
Client Sample ID: 1111089-01 Work Order/ID: 11 K0452-01
Sample Description: Sampled: 11/04/2011 0:00
Matrix: Aqueous Received: 11/10/2011 9:30
Analyses AT Result RL Qual Units DF Analyzed
Method: EPA 625 Rev 7195 Analyst: BR
Semivolatiie Organic Compounds Prep Method: SW846 3510 Prep Daterrime;1Ill 112011 07:35
Butyl benzyl phthalate
A
< 9.9
9.9
µg1L
1
11/11/2011 14:23
Carbazole
A
< 9.9
9.9
µg1L
1
11/1112011 14:23
Chrysene
A
< 9.9
9.9
µg1L
1
11/11/2011 14:23
Dibenz[a,h]anthracene
A
<9.9
9.9
µg1L
1
11111/2011 14:23
Dibenzofuran
A
<9.9
9.9
µg1L
1
11/11/2011 14:23
Diethyl phthalate
A
< 9.9
9.9
µg1L
1
11/11/2011 14:23
Dirrlethyl phthalate
A
< 9.9
9.9
µg1L
1
11/11/2011 14:23
Di-n-butyl phthalate
A
< 9.9
9.9
µg1L
1
1 i/l V2011 14:23
Di-n-octyl phthalate
A
< 9.9
9.9
µglL
1
1111112011 14:23
Fluoranthene
A
<9.9
9.9
µg1L
1
11/11/2011 14:23
Fiuorene
A
<9.9
9.9
µg1L
1
11/11/2011 14:23
Hexachlorobenzene
A
<9.9
9.9
µglL
1
1111112011 14:23
Hexachlorobutadiene
A
<9.9
9.9
µg1L
1
1111112011 14:23
HexachlorocyclDpentadiene
A
<9.9
9.9
µglL
1
1111112011 14:23
Hexachloroethane
A
<9.9
9.9
µg1L
1
1111112011 14:23
Indeno[1,2,3cd]py. ne
Isophorone
A
<9.9
9.9
µglL
1
1111112011 14:23
A
<9.9
9.9
µglL
1
11111/2411 14:23
Naphthalene
A
< 9.9
9.9
µglL
1
1111112011 14:23
Nitrobenzene
A
< 9.9
9.9
µg1L
1
1 ill V2011 14:23
N-N itrosodimethyla mine _
A
<9,9
9.9
µg1L
1
11/11/2011 14:23
N-Nitrosodi-n-propylamine �
N-Nitrosodiphenylamine
A
<9.9
9.9
µglL
1
11/11/2011 14:23
A
< 9.9
9.9
µg1L
1
11/11/2011 14:23
Pentachlorophenol
A
<50
50
µglL
1
11111/2011 14:23
Phenanthrene
A
< 9.9
9.9
µglL
1
11/11/2011 14:23
Phenol
A
< 9.9
a9
µ91L
1
11/11/2011 14:23
Pyrene
A
<9.9
9.9
µg1L
1
11111/2011 14:23
Pyridine
< 9.9_
-� 9.9
µg1L
1
11/11/2011 14:23
Surr.' 2,4,6-Tnbro2ophenol
S
101.00
47.8-138
%REC
t J
11/1112011 14:23
Surr 2-Fluorob' henyl
S
44.80
10-110
%REC
1
11/11/2011 14: 23
Surr.' 2-Fluarophenol
5
31,70
10-110
%REC
1
11/11/2011 14:23
Surr: Nitrobenzene-d5
S
40.80
10-110
%REC
1
11/11/2011 14:23
5urr.• Phenol-0
S
I
26.50
159.00
10-60.8
%REC
1
11/11/2011 14:23
Burn- Terpheny6d14
5
16.8-110
%REC
1
11111/2011 14:23
Method: EPA 613
Analyst: BR
Dioxin Prep
Method: SW046 3510
Prep DatelTime:1ill 112011 07:35
2,3,7,8-TetrachlDrodibenzo-p-dioxin A
I Negative
0.0 PoslNeg
1 11111/2011 14:23
Method: EPA 624 Rev 7195
Analyst:pn
Volatile Organic Compounds, 25ml Purge
Prep DatelTime:1111712011 15:38
1,11-Trichloroethane A
<0.0010 1
0.0010 U mg/L
J 1 1 lll17/2011 15:39
1,1,2,2-Tetrachloroethane
A
<0,0010
0.0610
U
mg1L
1 1
1 11/1712011 15:39
1,1,2-Trichloroethane
A
<0.0010
O.D010
U
mg1L
1
11/1712011 15:39
250 West 84th Drive, Merrillville, IN 46410
TEL.[phone]
TEL.[phone]
FAX.219.769,1664
Page 6 of 10

1�
Analytical Results Date: Tuesday, November22, 2011
Client: Microbac - Fayetteville Division
Client Project: 1111089 - General
Client Sample ID: 1111089-01 Work Order/ID: 11 K0452-01
Sample Description: Sampled: 11/04/2011 &00
Matrix: Aqueous Received: 11/10/2011 9:30
Analyses AT Result RL Qual Units DF Analyzed
Method: EPA 624 Rev 7195 Analyst:jln
Volatile Organic Compounds, 25ml Purge Prep Datelrime:1111712011 15:38
1,1-Dichloroethene
A
<o.00fo
0.0010
U
mg11-
1
1111712011 15;39
1,1-Dichloroethene
A
<0.0010
0.0010
U
mg1L
1
11/17/2011 15:39
1,2-Dichlorobenzene
A
<0.0020
0.0020
U
mglL
1
11/17/2011 15:39
1,2-Dichloroethane
A
< 0.0010
0.0010
U
mg1L
1
11/17/2011 15:39
1,2-Dichloropropane
A
< 0.0010
0.0010
U
mg1L
1
11/17/2011 15:39
1,3-Dichlorobenzene
A
<0,0020
0.0020
U
mg1L
1
11/17/2011 15:39
1,4-Dichlorobenzene
A
< 0.0020
0.0020
U
mg1L
1
1111712011 15:39
2-Chloroethyl vinyl ether
A
< 0.0020
0.0020
U
mg1L
1
11/17/2011 15:39
2-Hexanone
A
<0.0050
0.0050
U
mg1L
1
1111712011 15:39
Acetone
A
o.015
0.0050
mg1L
1
11/1712011 15:39
Benzene
A
< 0.0010
0.0010
U
mg1L
1
11117/2011 15:39
Bromodichloromethane
A
<p,00f0
0.0010
U
mg1L
1
11/17/2011 15:39
Bromoform
A
<0.0010
0.0010
U
mglL
1
11/17/2011 15:39
Bromomethane
A
<0.0020
0.0020
U
mg/1-
1
11/17/2011 15:39
Carbon Disulfide
A
<0.0020
0.0020
U
mglL
1
11/17/2011 15:39
Carbon tetrachloride
A
< 0.0010
0.0010
U
mg1L
1
11/17/2011 15:39
Chlorobenzene -�
A
< 0.001 o
0.0010
UJ
mglL
1
1111712011 15;39
Chloroethane
A
<0,0020
0.0020
U
mg1L
1
11/17/2011 15:39
Chloroform
A
<0.0010
0.0010
U
mg1L
1
11/1712011 15:39
Chloromethane
A
<0.002o
0,0020
U
mg1L
1
11/17/2011 15:39
cis-1,3 Dichloropropene
A
<0.0010
0.0010
U
mg1L
1
11/1712011 15:39
Dibromochloromethane
A
<0.0010
0.0010
U
mg1L
1
11/17/2011 15:39
Ethylbenzene
A
< 0.0010
0.0010
U
mglL
1
11/1712011 15:39
Methylene chloride
A
< 0,0020
0.0020
U
mg1L
1
11/17/2011 15:39
Methyl-t-Butyl Ether
A
< 0.0020
0.0020
U
mg1L
1
11/17/2011 15:39
Tetrachloroethene
A
<0.0010
0.0010
U
mg/L
1
11/17/2011 15:39
Toluene
trans-1,2-Dichloroethene
A
<0.0010
0,0010
U
mglL_
1
1111712011 1539
A
<0.0010
0.0010
U
mglL
1
1111712011 15:39
trans- 1,3-Dichloropropene
A
<0.0010
0,0010
U
mg1L
1
1VlV2011 15:39
Trichloroethene
A
<0,00f0
0.0010
U
mg1L
1
11/17/2011 15:39
Trichlorofluoromethane
A
< 0.0010
0.0010
U
mg1L
1
11117/2011 15:39
Vinyl Acetate
A
<0,00f0
0.0010
U
mg1L
1
1111V2011 15:39
Vinyl chloride
A
<0.0020
0.0020
U
mg1L
1
11/17/2011 15:39
Totall,2-Dichloroethene
M
<0.0010
0.0010
U
mglL
1
11/17/2011 15:39
Total Xylenes
M
< 0.0010
0.0010
U
mglL
1
11/17/2011 15:39
Surr: 1,2-Dichloroethane-D4
S
101.00
Y M132
%REC
1
11/17/2011 15:39
Surr; 4-Sromoiluorobenzene
s
99.90
80-120
%REC
1
11/17/2011 15:39
Surr. Dibromofluoromethane
S
1100.00
80-120
%REC
1
11/17/2011 15:39
Surr: Toluene-D8
5
103.OD
80-120
%REC
1
11/17/2011 15:39
250 West 84th Drive, Merrillville, IN 46410 TEL.[phone] TEL.[phone] FAX.[phone]
Page 7 of 10

Fayettevllis Dlvlslon 25 2 Hope MON Road - Fayenew"u, l-,r--75 P
CHAIN OF CUSTODY RECORD
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mmmmm:mmmmm
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mom
nomm
mmmm
;WO
mmmMM'N:
um
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Comments or Social Hazstds:
lS DATA FOR REG. COMPW4NCE PURPOSP-7
NO YES X UHlOH: DWQ-NPOES