NCG030429_COMPLETE FILE - HISTORICAL_20100503

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/v
DOC TYPE
HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ 0\01 0 G 5� 3
YYYYMMDD

AQrfiX-NAA
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NC®ENR
North Carolina Department of Environment and Natural Resources
Beverly Eaves Perdue
Governor
May 3, 2010
Mrs. Kimberly Killian
EHS Coordinator
GKN Driveline.
6400 Durham Road
Timberlake, NC 27583
Division of Water Quality
Coleen H. Sullins
Director
SUBJECT: Compliance Evaluation Inspection
GKN Driveline
Permit Number - NCG030429
County - Person
Dear Ms. Kimberly Killian:
Dee Freeman
Secretary
On April 1, 2010, Autumn Hoban, of the Division of Water Quality (DWQ), Raleigh Regional Office, met with
Kimberly Killian, Marty Stewart, and Zach Greenhaw to confirm NPDES SW outfalls/Representative Outfall
Status, and answer questions with regards to current updates to the Stormwater Pollution Prevention Plan. A
stormwater compliance evaluation inspection was also conducted and the assistance and cooperation of GKN
and their consultants was greatly appreciated. The facility was compliant with the permit requirements and the
inspection findings and comments are listed below.
Industry;ar d Site Descr'
GKN Driveline assembles parts for the automotive industry. Stormwater runoff generated at such facilities is
regulated by General Permit NCG030000. DWQ has therefore issued GKN Driveline, certificate of coverage,
NCG030429, this general permit became effective on November 1, 2007 and expires on October 31, 2012.
Inspection: Summary r x
The facility assembles automotive parts and conducts water and chemical based cleaning of parts. Stormwater
is from parking areas, roof drains, storage areas and loading/unloading docks. Site housekeeping was good
and spill prevention and BMP's were observed and have been implemented per the SWP3 Plan.
The facility keeps good records and was in compliance with the permit requirements.
It was determined during the site visit that the facility currently has four NPDES SW outfalls (HW9, HW7, HW5,
and HW4) and the most recent sampling event was conducted at HW4 (at the culvert) and HW5 in December
2009. It is the recommendation of the inspector that the new site plan and the updated SWP3 reflect HW9,
HW7, and HW5 as NPDES outfalls with sampling requirements, but HW 4 is sheet flow off the property to a
150 ft tree buffer, so sampling this outfall at the culvert by the plant is unnecessary and sampling should be at

r e
N j0364 0 Page 2
the property line where there is sheet flow, but this would make it difficult to sample. The day of the inspection
there was no evidence of concentrated flow at the property line or to the stream that is located beyond a (-y150
feet tree buffer). For this reason, I am recommending that the facility repair and maintain the culvert and rock
dams to ensure flow continues as sheet flow off the property at this location and visually inspect this location
along with the other NPDES SW Outfalls. HW9 currently contains a swell (-25 -30 ft from stream) that collects
SW runoff from the truck loading/unloading entrance road to the plant. A concrete pipe located at the stream
bank directs the SW flow into the stream. This stream is subject to the Neuse Buffer Rules (North Carolina
Administrative Code 15A NCAC 0213.0232 and 15A NCAC 02B.0233). Existing stormwater outfalls are exempt
from the buffer rules provided they are managed to minimize sediment, nutrients, and other pollution that convey
to waterbodies, but any new stormwater outfalls could be subject to the Neuse Buffer Rules which now require a
50 ft wide riparian buffer directly adjacent to surface waters in the Neuse River Basin, as well as, nutrient
management strategies. Discussions during this inspection included a recommendation for installation of an
appropriate BMP to ensure prevention of sediment/erosion issues or spills that could result in violations at this
location, due to the origin/location of the SW (truck loading and unloading entrance and driveway) and due to
the close proximity to the stream.
HW7 is cause for concern based on observations of this outfall and the close proximity of the culvert pipe /rip -
rap apron to the stream (-5-8 ft) making this a vulnerable outfall for violations (fill in the stream or water quality
standard violation caused by rip -rap, gravel, or sediment movement during a storm event or heavy rain). This
stream is subject to the Neuse Buffer Rules (North Carolina Administrative Code 15A NCAC 02B.0232 and 15A
NCAC 02B.0233). Existing stormwater outfalls are exempt from the buffer rules provided they are managed to
minimize sediment, nutrients, and other pollution that convey to waterbodies, but any new stormwater outfalls
could be subject to the Neuse Buffer Rules which now require a 50 ft wide riparian buffer directly adjacent to
surface waters in the Neuse River Basin, as well as, nutrient management strategies. Discussions during this
inspection included a recommendation for removal of this outfall, if possible, to eliminate possibility of stream
bank failure/erosion/turbidity - loss of rip-rap/gravel or sediment into the stream, as well as, prevent nutrients or
other pollutants (in the case of a spill) a direct route to the stream.
Petroleum/Solvents are stored on -site and meet secondary containment requirements. No spills were observed
on -site during the inspection. The site also falls under SPCC requirements and had an SPCC plan, Fifty-five
gallon drums were'stored under cover.
It is our goal to insure the quality of the surface waters of this State.
Please review the attached report. If you or your staff has any questions, do not hesitate to contact Autumn
Romanski at 919-791-4200.
Sincerely,
'oe��.
A .iumn Romanski
Enclosures
cc; Central files
RRO/DWQ Stormwater Compliance Files
Stormwater Permitting Unit
3400 Barrett Drive One
Raleigh, North Carolina 27609 NorthCarolina
Phone. [phone] Fax: [phone] ;Vaturally

Permit: NCG030429
SOC:
County: Person
Region: Raleigh
Compliance Inspection Report
Effective: 11/01/07 Expiration: 10/31/12 Owner: Gkn Driveline
Effective: Expiration: Facility: GKN Driveline
6400 Durham Rd
Contact Person: Stephen Berney
Directions to Facility:
System Classifications:
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Timberlake NC 27583
Title: Phone: [phone]
Certification: Phone:
Inspection Date: 04/01/2010 Entry Time* 09:30 AM Exit Time: 02:00 PM
Primary Inspector: Autumn H Romanski �� Phone: [phone]
Secondary Inspector(s):
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Metal Fabrication Stormwater Discharge COC
Facility Status: ■ Compliant ❑ Not Compliant
Question Areas:
0 Storm Water
(See attachment summary)
Page: 1

Permit: NCG030429
SOC:
County: Person
Region: Raleigh
Compliance Inspection Report
Effective: 11/01/07 Expiration: 10/31/12 Owner: Gkn Driveline
Effective: Expiration: Facility: GKN Driveline
6400 Durham Rd
Contact Person: Stephen Berne
Directions to Facility:
System Classifications:
Primary ORC:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Title:
Inspection Date: 04/01/2010 Entry Time: 09:30 AM
Primary Inspector: Autumn H Romanski
Secondary Inspector(s):
Timberlake NC 27583
. Phone:[phone]
Certification:
Exit Time: 02:00 PM
Phone:
Phone: [phone]
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Metal Fabrication Stormwater Discharge COC
Facility Status: ■ Compliant ❑ Not Compliant
Question Areas:
Storm Water
(See attachment summary)
Page:1

Permit: NCG030429 Owner - Facility: Gkn Driveline
Inspection Date: 04/01/2010 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
The facility outfalls were reviewed for representative outfall status and the following was determined during this site visit:
Outfall (HW9) is an NPDES SW outfall
Outfall (HW7) is an NPDES SW outfall with flow from HW6 and drainage area above (HW6) respresented in (HW7).
Discussions during the inspection included a recommendation for removal of this outfall, if possible, as it is a liability to the
stream bank and rip-rap/gravel is vunerable and at risk of becoming a violation'of fill in the stream due to its proximity to
the stream. If this outfall is removed, please inform DWQ Raleigh Regional Office and an inspector will ensure that the
SW flow is no longer able to reach the stream through outfall (HW7)and that rip-rap/gravel is stable and in no danger of
reaching the stream before removing this outfall from its current sampling requirements.
Outfall (HW5) is an NPDES SW outfall.
Outfall (HW4) is currently an NPDES SW outfall and has been sampled in the past. There is a forbay and two rock filter
dams constructed here that need repairs. There is no concentrated pathway to the stream at this location. After the last
rock filter dam, the SW spreads out over (-150 foot) tree buffer before the stream, so I recommended after repairs are
completed on the rock filter dams that this outfall be labelled sheet flow and no longer an NPDES SW outfall for the
purposes of sampling. I do recommend continued maintenance as needed on the rip -rap and rock filter dams, as well as,
visual inspections.
Outfall (HW3) - sheet flow, no sampling requirement, (50-100 ft)tree buffer after ditches, but recommend maintenance of
rip -rap in sw ditches and visual inspections.
Outfall (HW2) - sheet flow, no sampling requirement, but recommend visual inspections.
Outfall (HW1)- sheet flow, no sampling requirement, (-150ft) tree buffer from the stream, but recommend maintenance of
rock dams already in place and visual inspections.
Two DOT storm drains were identified: 1) US 501 in front of the facility in the highway easement and 2) Roby Barton Rd at
the back of the facility property line SW pipe goes under the road. At both of these locations there is sheet flow off the
facility property and the drains are clearly DOT drains and NOT designated sw outfalls for the purposes of the
NCG030429.
Page: 2

Permit: NCG030429 Owner - Facility: Gkn Driveline
Inspection Date: 04/01/2010 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
The facility outfalls were reviewed for representative outfall status and the following was determined during this site visit
Outfall (HW9) is an NPDES SW outfall
Outfall (HW7) is an NPDES SW outfall with flow from HW6 and drainage area above (HW6) respresented in (HW7).
Discussions during the inspection included a recommendation for removal of this outfall, if possible, as it is a liability to the
stream bank and rip-rap/gravel is vunerable and at risk of becoming a violation of fill in the stream due to its proximity to
the stream. If this outfall is removed, please inform DWQ Raleigh Regional Office and an inspector will ensure that the
SW flow is no longer able to reach the stream through outfall (HW7)and that rip-rap/gravel is stable and in no danger of
reaching the stream before removing this outfall from its current sampling requirements.
Outfall (HW5) is an NPDES SW outfall.
Outfall (HW4) is currently an NPDES SW outfall and has been sampled in the past. There is a forbay and two rock filter
dams constructed here that need repairs. There is no concentrated pathway to the stream at this location. After the last
rock filter dam, the SW spreads out over (-150 foot) tree buffer before the stream, so I recommended after repairs are
completed on the rock filter dams that this outfall be labelled sheet flow and no longer an NPDES SW outfall for the
purposes of sampling. I do recommend continued maintenance as needed on the rip -rap and rock filter dams, as well as,
visual inspections.
Outfall (HW3) - sheet flow, no sampling requirement, (50-100 ft)tree buffer after ditches, but recommend maintenance of
rip -rap in sw ditches and visual inspections.
Outfall (HW2) - sheet flow, no sampling requirement, but recommend visual inspections.
Outfall (HW1)- sheet flow, no sampling requirement, (-150ft) tree buffer from the stream, but recommend maintenance of
rock dams already in place and visual inspections.
Two DOT storm drains were identified: 1) US 501 in front of the facility in the highway easement and 2) Roby Barton Rd at
the back of the facility property line SW pipe goes under the road. At both of these locations there is sheet flow off the
facility property and the drains are clearly DOT drains and NOT designated sw outfalls for the purposes of the
NCG030429.
Page:2

Permit: NCG030429 Owner - Facility: Gkn Driveline
Inspection Date: 04/01/2010 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Stormwater Pollution Prevention Plan Yes No NA NE
Does the site have a Stormwater Pollution Prevention Plan?
■
n
n
❑
# Does the Plan include a General Location (USGS) map?
■
❑
❑
❑
# Does the Plan include a "Narrative Description of Practices"?
■
❑
❑
❑
# Does the Plan include at detailed site map including outfall locations and drainage areas?
■
❑
❑
❑
# Does the Plan include a list of significant spills occurring during the past 3 years?
❑
❑
■
❑
# Has the facility evaluated feasible alternatives to current practices?
■
❑
❑
❑
# Does the facility provide all necessary secondary containment?
■
❑
❑
❑
# Does the Plan include a BMP summary?
■
❑
❑
❑
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
■
❑
❑
❑
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
■
❑
n
n
# Does the facility provide and document Employee Training?
■
❑
❑
❑
# Does the Plan include a list of Responsible Party(s)?
■
❑
❑
❑
# Is the Plan reviewed and updated annually?
■
n
n
❑
# Does the Plan include a Stormwater Facility Inspection Program?
■
❑
❑
❑
Has the Stormwater Pollution Prevention Plan been implemented?
■
❑
❑
❑
Comment: SIC 3714 Assembly only- some washing of metal parts. No vehicle
maintenance done on site.
Plan is in the process of being updated.
Site map was dated 2005 and a new site map is being developed to reflect changes to
plant site.
Training was conducted October- December 2009.
Qualitative Monitoring
Yes
No
NA
NE
Has the facility conducted its Qualitative Monitoring semi-annually?
■
❑
❑
❑
Comment:
Analytical Monitoring
Yes
No
NA
NE
Has the facility conducted its Analytical monitoring?
■
❑
❑
❑
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas?
❑
❑
■
❑
Page: 3

Permit: NCG030429 Owner - Facility: Gkn Driveline
Inspection Date: 04/01/2010 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Stormwater Pollution Prevention Plan IYes No NA NE
Does the site have a Stormwater Pollution Prevention Plan?
# Does the Plan include a General Location (USGS) map?
# Does the Plan include a "Narrative Description of Practices'?
# Does the Plan include a detailed site map including outfall locations and drainage areas?
# Does the Plan include a list of significant spills occurring during the past 3 years?
# Has the facility evaluated feasible alternatives to current practices?
# Does the facility provide all necessary secondary containment?
# Does the Plan include a BMP summary?
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
# Does the facility provide and document Employee Training?
# Does the Plan include a list of Responsible Party(s)?
# Is the Plan reviewed and updated annually?
# Does the Plan include a Stormwater Facility Inspection Program?
Has the Stormwater Pollution Prevention Plan been implemented?
Comment: SIC 3714 Assembly only- some washing of metal parts. No vehicle
maintenance done on site.
Plan is in the process of being updated.
Site map was dated 2005 and a new site map is being developed to reflect changes to
plant site.
Training was conducted October- December 2009.
Qualitative Monitoring
Has the facility conducted its Qualitative Monitoring semi-annually?
Comment:
Analytical Monitoring
Has the facility conducted its Analytical monitoring?
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas?
■❑pn
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Yes
No
NA
NE
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Yes
No
NA
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Page, 3

Permit: NCG030429
Inspection Date: 04/01/2010
Owner - Facility: Gkn Driveline
Inspection Type: Compliance Evaluation
Comment: Conducted analytical monitoring at outfalls 004 and 005 in June and
December of 2009. Results from Meritech lab were reviewed during the inspection.
Reason for Visit: Routine
I reviewed the TTO sampling results and we discussed the development of a Solvent.
Management Plan. Since the SWP3 is being updated, the facility has the option to
develop and add a solvent management plan and submit to DWQ for approval. Once
approved, and as we discussed during the inspection, the SMP can be used in leu of
sampling to meet permit requirements. I collected MSDS information on the solvents
on -site during the inspection and discussed secondary containment and spill
prevention.
Permit and Outfalls Yes No NA NE
# Is a copy of the Permit and the Certificate of Coverage available at the site? ■ ❑ ❑ ❑
# Were all outfalls observed during the inspection? ■ ❑ ❑ ❑
# If the facility has representative outfall status, is it properly documented by the Division? ■ ❑ ❑ fl
# Has the facility evaluated all illicit (non stormwater) discharges? ■ ❑ ❑ ❑
Comment: The facility outfalls were reviewed for representative outfall status. Please
see summary for details.
It is recommended that the facility send a letter requesting respresentative outfall status
for approval by the Raleigh Regional Office. Please include a site map for referencing
the location of the outfalls with updates that show changes or changes planned to the
site.
Page:4

Permit: NCG030429 Owner - Facility: Gkn Driveline
Inspection Date: 04/01/2010 Inspection Type: Compliance Evaluation
Comment: Conducted analytical monitoring at outfalls 004 and 005 in June and
December of 2009. Results from Meritech lab were reviewed during the inspection.
Reason for Visit: Routine
I reviewed the TTO sampling results and we discussed the development of a Solvent
Management Plan. Since the SWP3 is being updated, the facility has the option to
develop and add a solvent management plan and submit to DWQ for approval. Once
approved, and as we discussed during the inspection, the SMP can be used in leu of
sampling to meet permit requirements. I collected MSDS information on the solvents
on -site during the inspection and discussed secondary containment and spill
prevention.
Permit and Outfalls
# Is a copy of the Permit and the Certificate of Coverage available at the site?
# Were all outfalls observed during the inspection?
# If the facility has representative outfall status, is it properly documented by the Division?
# Has the facility evaluated all illicit (non stormwater) discharges?
Comment: The facility outfalls were reviewed for representative outfall status. Please
see summary for details.
It is recommended that the facility send a letter requesting respresentative outfall status
for approval by the Raleigh Regional Office. Please include a site map for referencing
the location of the outfalls with updates that show changes or changes planned to the
site.
Yes No NA NE
■❑❑❑
■ ❑ ❑ ❑
■❑❑Q
■❑❑❑
Page:4

Material Safety Data Sheet
1. Chemical product and company identification
Product name
RUSTILO 4135 HF
Code
09016-AE
Product use
Corrosion inhibitor.
Manufacturer
Castrol Industrial North America, Inc.
150 W. Warrenville Road
Naperville, IL 60563
Supplier
Castrol Industrial North America, Inc.
150 W. Warrenville Road
Naperville, IL 60563
Product Information: 1-800-621-2661
EMERGENCY SPILL
1 [phone] CHEMTREC (USA)
INFORMATION:
2. Composition/information on ingredients
Ingredient name
CAS # % by weight
Distillates (petroleum), hydrotreated light paraffinic (Hydrocarbon solvent) 64742-47-8 85 - 90
Refined paraffin wax
8002-74-2 1-5
3. Hazards identification
Physical state
Liquid.
Color
Clear. Amber.
Emergency overview
WARNING!
ASPIRATION HAZARD.
Harmful or fatal if liquid is aspirated into lungs.
MAY CAUSE EYE IRRITATION.
MAY CAUSE SKIN IRRITATION..
MAY CAUSE RESPIRATORY TRACT IRRITATION.
Do not ingest. Do not get in eyes, on skin or clothing. In accordance with good industrial hygiene
and safety work practices, airborne exposures should be controlled to the lowest extent
practicable. Keep container closed. Use only with adequate ventilation. Wash thoroughly after
handling.
Routes of entry
Dermal contact. Eye contact. Inhalation. Ingestion.
Potential health effects
Eyes
May cause eye irritation.
Skin
May cause skin irritation. Prolonged or repeated contact can defat the skin and lead to irritation
and/or dermatitis.
Inhalation
May cause respiratory tract irritation.
Ingestion
Ingestion may cause gastrointestinal irritation and diarrhea.
Aspiration hazard if swallowed -- harmful or fatal if liquid is aspirated into lungs.
Medical conditions
None identified.
aggravated by over-
exposure
Product RUSTILO 4135 HF MSDS # 09016-AE Page: 1/5
name
Version 4 Date of issue 12/13/2005. Format US Language ENGLISH.
Build 4.2.6 ( ENGLISH )

See toxicological information (section 11)
4. First aid measures
Eye contact
In case of contact, immediately flush eyes with plenty of water for at least 15 minutes. Get medical
attention if irritation develops.
Skin contact
Immediately wash exposed skin with soap and water. Remove contaminated clothing and shoes.
Wash clothing before reuse. Thoroughly clean shoes before reuse. Get medical attention if
irritation develops.
Inhalation
If inhaled, remove to fresh air. If not breathing, give artificial respiration. If breathing is difficult,
give oxygen. Get medical attention if irritation develops.
Ingestion
If swallowed, do NOT induce vomiting. Never give anything by mouth to an unconscious person.
Aspiration hazard if swallowed- can enter lungs and cause damage. Get medical attention.
5. Fire -fighting measures
Flammability of the product
May be combustible at high temperature.
Flash point
112.78 °C (Open cup) Cleveland.
112 °C (Closed cup)
Products of combustion
These products are carbon oxides (CO, CO2).
Unusual fire/explosion
This material is not explosive as defined by established regulatory criteria.
hazards
Fire -fighting media and
In case of fire, use water fog, foam, dry chemicals, or carbon dioxide.
instructions
Protective clothing (fire)
Fire-fighters should wear positive pressure self-contained breathing apparatus (SCBA) and full
turnout gear.
6. Accidental release measures
Personal precautions Immediately contact emergency personnel. Keep unnecessary personnel away. Use suitable
protective equipment (See Section: "Exposure controls/personal protection"). Follow all fire
fighting procedures (See Section: "Fire -fighting measures").
Environmental If emergency personnel are unavailable, contain spilled material. For small spills add absorbent
precautions and clean-up (soil may be used in the absence of other suitable materials) scoop up material and place in a
methods sealed, liquid -proof container for disposal. For large spills dike spilled material or otherwise
contain material to ensure runoff does not reach a waterway. Place spilled material in an
appropriate container for disposal. Avoid contact of spilled material with soil and prevent runoff
entering surface waterways. See Section 13 for Waste Disposal Information.
Personal protection in Splash goggles. Full suit. Boots. Gloves. Suggested protective clothing might not be sufficient, -
case of a large spill consult a specialist BEFORE handling this product.
7. Handling and storage
Handling Do not ingest. Do not get in eyes, on skin or on clothing. Avoid contact with skin and clothing. In
accordance with good industrial hygiene and safety work practices, airborne exposures should be
controlled to the lowest extent practicable. Use only with adequate ventilation. Wash thoroughly
after handling.
Storage Keep container tightly closed. Keep container in a cool, well -ventilated area. Empty containers
may contain harmful, flammable/combustible or explosive residue or vapors. Do not cut, grind, drill,
weld, reuse or dispose of containers unless adequate precautions are taken against these
hazards.
Product RUSTILO 4135 HF MSDS # 09016-AE Page: 2/5
name
Version 4 Date of issue 12/13/2005. Format US Language ENGLISH.
Build 4.2.6 ( ENGLISH )

8. Exposure controls/personal protection
Occupational exposure
limits
Ingredient name Occupational exposure limits
Distillates (petroleum), hydrotreated light ACGIH TLV (United States, 1/2004). Skin
paraffinic (Hydrocarbon solvent) TWA: 200 mg/m3 8 hour(s).
Refined paraffin wax ACGIH TLV (United States, 112005).
TWA: 2 mg/m3 8 hour(s). Form: Fume
Control Measures Provide exhaust ventilation or other engineering controls to keep the airborne concentrations of
vapors below their respective occupational exposure limits.
Hygiene measures Wash hands, forearms and face thoroughly after handling chemical products, before eating,
smoking and using the lavatory and at the end of the working period.
Personal protection
Eyes Avoid contact with eyes. Safety glasses with side shields.
Skin and body Avoid contact with skin and clothing. Wear suitable protective clothing.
Respiratory Use only with adequate ventilation. In accordance with good industrial hygiene and safety work
practices, airborne exposures should be controlled to the lowest extent practicable.
Hands Wear suitable gloves.
Not available.
V V
Consult local authorities for acceptable exposure limits.
9. Physical and chemical properties
Physical state Liquid.
Odor Mild.
Color Clear. Amber.
Specific gravity 0.8 to 0.85
Solubility Insoluble in cold water.
Viscosity Kinematic: <7 mmZ/s (<7 cSt) at 40°C
SUS: 35 to 38 SUS at 37.778°C
10. Stability and reactivity
Stability and reactivity
The product is stable.
Conditions to avoid
Not available.
Incompatibility with various
Not available.
substances
Hazardous decomposition
Not available.
products
Hazardous polymerization
Will not occur.
Product RUSTILO 4135 HF MSDS # 09016-AE Page: 3/5
name
Version 4 Date of issue 12/13/2005. Format US Language ENGLISH.
Build 4.2.6 ( ENGLISH )

11. Toxicological information
Chronic toxicity
Carcinogenic No component of this product at levels greater than 0.1% is identified as a carcinogen by ACGIH
effects or the International Agency for Research on Cancer (IARC). No component of this product
present at levels greater than 0.1 % is identified as a carcinogen by the U.S. National Toxicology
Program (NTP) or the U.S. Occupational Safety and Health Act (OSHA).
Mutagenic No component of this product at levels greater than 0.1 % is classified by established regulatory
effects criteria as a mutagen.
Reproductive No component of this product at levels greater than 0.1 % is classified by established regulatory
effects criteria as a reproductive toxin.
Teratogenic No component of this product at levels greater than 0.1% is classified by established regulatory
effects criteria as teratogenic or embryotoxic.
12. Ecological information
Ecotoxicity No testing has been performed by the manufacturer.
13. Disposal considerations
Waste information Avoid contact of spilled material and runoff with soil and surface waterways. Consult an
environmental professional to determine if local, regional or national regulations would classify
spilled or contaminated materials as hazardous waste. Use only approved transporters, recyclers,
treatment, storage or disposal facilities. Dispose of in accordance with all applicable local and
national regulations.
Consult your local or regional authorities.
14. Transport information
Not classified as hazardous for transport (DOT, TDG, IMO/IMDG, IATA/ICAO)
15. Regulatory information
U.S. Federal regulations US INVENTORY (TSCA): In compliance
TSCA 12(b) one-time export notification:: dipropylene glycol methyl ether
This product is not regulated under Section 302 of SARA and 40 CFR Part 355.
SARA 311/312 MSDS distribution - chemical inventory - hazard identification: RUSTILO 4135 HF:
Immediate (Acute) Health Hazard
SARA 313
Form R - Reporting
This product does not contain any hazardous ingredients at or above regulated thresholds.
requirements
Supplier notification
This product does not contain any hazardous ingredients at or above regulated thresholds.
CERCLA Sections 102a/103 Hazardous Substances (40 CFR Part 302.4):: Methanol: 5000 lbs.
(2268 kg);
State regulations
Massachusetts RTK:Refined paraffin wax; dipropylene glycol methyl ether
New Jersey:dipropylene glycol methyl ether
Pennsylvania RTK:Refined paraffin wax (generic environmental hazard); dipropylene glycol methyl
ether (generic environmental hazard)
California prop. 65: No products were found.
Product RUSTILO 4135 HF MSDS # 09016-AE Page: 4/5
name
Version 4 Date of issue 12/13/2005. Format US Language ENGLISH.
Build 4.2.6 ( ENGLISH )

Inventories AUSTRALIAN INVENTORY (AICS): In compliance.
CANADA INVENTORY (DSL): In compliance.
CHINA INVENTORY (IECS): In compliance.
EC INVENTORY (EINECS/ELINCS): In compliance.
JAPAN INVENTORY (ENCS): In compliance.
KOREA INVENTORY (ECL): In compliance.
PHILIPPINE INVENTORY (PICCS): In compliance.
16.Other information
Label requirements
HMIS® Rating :
Other special
considerations
History
Date of issue
Date of previous issue
Prepared by
Notice to reader
WARNING!
ASPIRATION HAZARD.
Harmful or fatal if liquid is aspirated into lungs.
MAY CAUSE EYE IRRITATION.
MAY CAUSE SKIN IRRITATION.
MAY CAUSE RESPIRATORY TRACT IRRITATION.
Health 1 - National Fire Fire hazard
Flammability 1 Protection
Physical 0 Association Health Instability
Hazard (U.S.A.) Specific hazard
Personal B
protection
PETROLEUM OIL: STEL = 10 mg/M3. Using terminology of the International Agency for
Research on Cancer (IARC), the petroleum distillates listed in Section 11 are classified by the
supplier as severely processed. Not all those listed in Section II may be present. The supplier has
stated that these distillates do not require a carcinogen label as defined by OSHA 29 CFR
1910.1200.
12/13/2005.
03/31 /2005.
Product Stewardship
All reasonably practicable steps have been taken to ensure this data sheet and the health, safety and environmental information
contained in it is accurate as of the date specified below. No warranty or representation, express or implied is made as to the
accuracy or completeness of the data and information in this data sheet.
The data and advice given apply when the product is sold for the stated application or applications. You should not use the
product other than for the stated application or applications without seeking advice from us.
It is the user's obligation to evaluate and use this product safely and to comply with all applicable laws and regulations. The BP
Group shall not be responsible for any damage or injury resulting from use, other than the stated product use of the material, from
any failure to adhere to recommendations, or from any hazards inherent in the nature of the material. Purchasers of the product
for supply to a third party for use at work, have a duty to take all necessary steps to ensure that any person handling or using the
product is provided with the information in this sheet. Employers have a duty to tell employees and others who may be affected of
any hazards described in this sheet and of any precautions that should be taken.
Product RUSTILO 4135 HF MSDS # 09016-AE Page: 5/5
name
Version Date of issue 12/13/2005. Format US Language ENGLISH.
Build 4.2.6 ( ENGLISH )

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Page 5 of 31
SAFETY DATA SHEET
MINERAL SPIRITS NON EXEMPT
20078
Page: 1
Revision Date: 06/21/2007
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
L. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE
�OMPANY/UNDERTAKING
Ashland Regulatory Information Number 1-800-325-3751
P.O. Box 2219 Telephone [phone]
Columbus, OH 43216 Emergency telephone number 1-800-ASHLAND
(1-800-274-5263)
Product name MINERAL SPIRITS NON EXEMPT
Product code 20078
Product Use Description No data
2. HAZARDS IDENTIFICATION
Emergency Overview
Appearance: liquid„ colourless
CAUTION! COMBUSTIBLE LIQUID AND VAPOR. MAY AFFECT THE CENTRAL
NERVOUS SYSTEM CAUSING DIZZINESS, HEADACHE OR NAUSEA. MAY
CAUSE EYE, SKIN AND RESPIRATORY TRACT IRRITATION. PROLONGED OR
REPEATED CONTACT MAY DRY SKIN, CAUSE IRRITATION AND BURNS.
MAY BE HARMFUL IF INHALED. MAY CAUSE RESPIRATORY TRACT
IRRITATION. PROLONGED OR REPEATED CONTACT MAY DRY THE SKIN
AND CAUSE IRRITATION AND BURNS.
Potential Health Effects
Routes of Exposure
Inhalation, Skin absorption, Skin contact, Eye Contact, Ingestion
Eye Contact
Can cause eye irritation. Symptoms include stinging, tearing, redness, and
swelling of eyes. May cause mild eye irritation. Symptoms include stinging, tearing, and
redness. Additional symptoms of eye exposure may include: blurred vision
Shin Contact
Can cause skin irritation. Prolonged or repeated contact may dry the skin.
Symptoms may include redness, burning, and drying and cracking of skin, burns and
other skin damage. Additional symptoms of skin contact may include: skin blistering
Page 1 / 12

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YVSHLANEX
SAFETY DATA SHEET
MINERAL SPIRITS NON EXEMPT
20078
Page: 2
Revision Date: 06/21/2007
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
Passage of this material into the body through the skin is possible, but it is unlikely that
this would result in harmful effects during safe handling and use.
Ingestion
Swallowing small amounts of this material during normal handling is not likely to
cause harmful effects. Swallowing large amounts may be harmful. This material can get
into the lungs during swallowing or vomiting. This results in lung inflammation and
other lung injury.
Inhalation
Breathing of vapor or mist is possible. Breathing small amounts of this material
during normal handling is not likely to cause harmful effects. Breathing large amounts
may be harmful. Symptoms are not expected at air concentrations below the
recommended exposure limits, if applicable (see Section 8.).
Aggravated Medical Condition
Preexisting disorders of the following organs (or organ systems) may be
aggravated by exposure to this material:, skin, lung (for example, asthma -like
conditions), kidney, immune system, auditory system, Individuals with preexisting heart
disorders maybe more susceptible to arrhythmias (irregular heartbeats) if exposed to high
concentrations of this material.
Symptoms
Signs and symptoms of exposure to this material through breathing, swallowing,
and/or passage of the material through the skin may include:, redness of the face and
neck, stomach or intestinal upset (nausea, vomiting, diarrhea), irritation (nose, throat,
airways), central nervous system excitation (giddiness, liveliness, light-headed feeling)
followed by central nervous system depression (dizziness, drowsiness, weakness, fatigue,
nausea, headache, unconsciousness) and other central nervous system effects, effects on
memory, respiratory depression (slowing of the breathing rate), shortness of breath, loss
of coordination, confusion, irregular heartbeat, respiratory failure, coma
Target Organs
This material (or a component) has been shown to lower activity of certain
immune system cells in experimental animals. The significance of this effect with
respect to human health is uncertain., Exposure to this material (or a component) has
been found to cause kidney damage in male rats. The mechanism by which this toxicity
occurs is specific to the male rat and the kidney effects are not expected to occur in
humans., Overexposure to this material (or its components) has been suggested as a cause
of the following effects in laboratory animals:, mild, reversible liver effects, kidney
damage, effects on hearing
Page 2 / 12

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A .. Page:3
SAFETY DATA SHEET Revision Date: 06/21/2007
MINERAL SPIRITS NON EXEMPT
20078
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
Carcinogenicity
Based on the available information, this material cannot be classified with regard
to carcinogenicity. This material is not listed as a carcinogen by the International Agency
for Research on Cancer (IARC), the National Toxicology Program (NTP), or the
Occupational Safety and Health Administration (OSHA).
Reproductive Hazard
This material (or a component) may be harmful to the human fetus based on
positive test results with laboratory animals.
Other Information
No data
3. COMPOSITIONIINFORMATION ON INGREDIENTS
Components CAS -No. Concentration
MINERAL SPIRITS REGULAR (BASE 8052-41-3 >=80-<90%
DATA)
TRIMETHYLBENZENE 1,2,4- 95-63-6 >=5-<10%
TRRVIETHYLBENZENE, 1,3,5- 108-67-8 >=5-<10%
XYLF.NE 1330-20-7 >=1.5-<5%
ETHYL BENZENE 100-41-4 >=0.5-<I%
4. FIRST AID MEASURES
Eyes
If symptoms develop, move individual away from exposure and into fresh air.
Flush eyes gently with water while holding eyelids apart. If symptoms persist or there is
any visual difficulty, seek medical attention.
Skin
Remove contaminated clothing. Flush exposed area with large amounts of water.
If skin is damaged, seek immediate medical attention. If skin is not damaged and
symptoms persist, seek medical attention. Launder clothing before reuse.
Ingestion
Seek medical attention. If individual is drowsy or unconscious, do not give
anything by mouth; place individual on the left side with the head down. Contact a
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Page 8 of 31
JASHLANEI
SAFETY DATA SHEET
MINERAL SPIRITS NON EXEMPT
20078
Page; 4
Revision Date: 06/21/2007
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
physician, medical facility, or poison control center for advice about whether to induce
vomiting. If possible, do not leave individual unattended.
Inhalation
If symptoms develop, immediately move individual away from exposure and into
fresh air. Seek immediate medical attention; keep person warm and quiet. If person is
not breathing, begin artificial respiration. If breathing is difficult, administer oxygen. If
symptoms develop, move individual away from exposure and into fresh air. If symptoms
persist, seek medical attention. If breathing is difficult, administer oxygen. Keep person
warm and quiet; seek immediate medical attention. .
Notes to Physician
Hazards-, Inhalation of high concentrations of this material, as could occur in
enclosed spaces or during deliberate abuse, may be associated with cardiac arrhythmias.
Sympathomimetic drugs may initiate cardiac arrhythmias in persons exposed to this
material. This material is an aspiration hazard. Potential danger from aspiration must be
weighed against possible oral toxicity (See Section 2 - Swallowing) when deciding
whether to induce vomiting.
Treatment: No information available.
5. FIRE -FIGHTING MEASURES
Suitable Extinguishing Media
dry chemical, foam, carbon dioxide (CO2)
Hazardous Combustion Products
May form:, carbon dioxide and carbon monoxide, various hydrocarbons
Precautions for Fire -Fighting
If product is heated above its flash point it will produce vapors sufficient to
support combustion. Vapors are heavier than air and may travel along the ground and be
ignited by heat, pilot lights, other flames and ignition sources at locations near the point
of release. Wear full firefighting turn -out gear (full Bunker gear), and respiratory
protection (SCBA).
Flammability Class for Flammable Liquids
Combustible Liquid Class IICombustible Liquid Class II
6. ACCIDENTAL RELEASE MEASURES
Page 4 / 12

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Page 9 of 31
SAFETY DATA SHEET
MINERAL SPIRITS NON EXEMPT
20078
Page: 5
Revision Date: 06/21/2007
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
Personal Precautions
For personal protection see section 8. Eliminate all ignition sources (flares,
flames including pilot lights, electrical sparks). Persons not wearing protective equipment
should be excluded from area of spill until clean-up has been completed. Stop spill at
source. Prevent from entering drains, sewers, streams or other bodies of water. Prevent
from spreading. If runoff occurs, notify authorities as required. Pump or vacuum
transfer spilled product to clean containers for recovery. Absorb unrecoverable product.
Transfer contaminated absorbent, soil and other materials to containers for disposal.
Environmental Precautions
Prevent run-off to sewers, streams or other bodies of water. If run-off occurs,
notify proper authorities as required, that a spill has occurred.
Methods for Cleaning Up
Absorb liquid on vermiculite, floor absorbent or other absorbent material.
7. HANDLING AND STORAGE
Handling
Containers of this material may be hazardous when emptied. Since emptied
containers retain product residues (vapor, liquid, and/or solid), all hazard precautions
given in the data sheet must be observed. Static ignition hazard can result from handling
and use. Electrically bond and ground all containers, personnel and equipment before
transfer or use of material. Special precautions may be necessary to dissipate static
electricity for non-conductive containers. Use proper bonding and grounding during
product transfer as described in National Fire Protection Association document NFPA 77.
Storage
Keep containers closed when not in use. Store in a cool, dry, ventilated area, away
from incompatible substances. Do not store near extreme heat, open flame, or sources of
ignition.
8. EXPOSURE CONTROLS / PERSONAL PROTECTION
Exposure Guidelines
MINERAL SPIRITS REGULAR (BASE 8052-41-3
DATA)
ACGIH time weighted average 100 ppm
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Page 10 of 31
YNSHLANO.
SAFETY DATA SHEET
MINERAL SPIRITS NON EXEMPT
20078
Page: 6
Revision Date: 06/21/2007
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
NIOSH
Recommended exposure limit
350 mg/m3
(REL):
NIOSH
Ceiling Limit Value and Time
1,800 mg/m3
Period (if specified):
OSHA Zl
Permissible exposure limit
500 ppm
OSHA Zl
Permissible exposure limit
2,900 mg/m3
OSHA ZIA
time weighted average
100 ppm
OSHA ZIA
time weighted average
525 mg/m3
US CA OEL
Time Weighted Average (TWA)
100 ppm
Permissible Exposure Limit (PEL):
US CA OEL
Time Weighted Average (TWA)
525 mg/m3
Permissible Exposure Limit (PEL):
TRIMETHYLBENZENE 14,4- 95-63-6
NIOSH
Recommended exposure limit
25 ppm
(REL):
NIOSH
Recommended exposure limit
125 mg/m3
(REL):
ACGIH
time weighted average
25 ppm
OSHA ZIA
time weighted average
25 ppm
OSHA ZIA
time weighted average
125 mg/m3
US CA OEL
Time Weighted Average (TWA)
25 ppm
Permissible Exposure Limit (PEL):
US CA OEL
Time Weighted Average (TWA)
125 mg/m3
Permissible Exposure Limit (PEL):
TRIMETHYLBENZENE,1,3,5- 108-67-8
NIOSH
Recommended exposure limit
25 ppm
(RE.,):
NIOSH
Recommended exposure limit
125 mg/m3
(REL):
ACGIH
time weighted average
25 ppm
OSHA ZIA
time weighted average
25 ppm
OSHA ZIA
time weighted average
125 mg/m3
XYLENE
1330-20-7
ACGIH
time weighted average
100 ppm
ACGIH
Short term exposure limit
150 ppm
OSHA Zl
Permissible exposure limit
100 ppm
OSHA Zl
Permissible exposure limit
435 mg/m3
NIOSH
Recommended exposure limit
100 ppm
(REQ:
NIOSH
Recommended exposure limit
435 mg/m3
(REL):
NIOSH
Short term exposure limit
150 ppm
NIOSH
Short term exposure limit
655 mg/zn3
NIOSH
Recommended exposure limit
100 ppm
(P=):
NIOSH
Recommended exposure limit
435 mg/m3
(RFI.):
NIOSH
Short term exposure limit
150 ppm
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Page 11 of 31
ASHLJOVqU
SAFETY DATA SHEET
MINERAL SPIRITS NON EXEMPT
20078
NIOSH
Short term exposure limit
NIOSH
Recommended exposure limit
(REL):
NIOSH
Recommended exposure limit
(REL):
NIOSH
Short term exposure limit
NIOSH
Short term exposure limit
655 mg/m3
100 ppm
435 mg/m3
150 ppm
655 mg/m3
Page: 7
Revision Date: 06/21/2007
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
General Advice
These recommendations provide general guidance for handling this product.
Personal protective equipment should be selected for individual applications and should
consider factors which affect exposure potential, such as handling practices, chemical
concentrations and ventilation. It is ultimately the responsibility of the employer to
follow regulatory guidelines established by local authorities.
Exposure Controls
Provide sufficient mechanical (general and/or local exhaust) ventilation to
maintain exposure below TLV(s).
Eye Protection
Chemical splash goggles in compliance with OSHA regulations are advised;
however, OSHA regulations also permit other type safety glasses. Consult your safety
representative.
Skin and Body Protection
Wear resistant gloves (consult your safety equipment supplier). To prevent
repeated or prolonged skin contact, wear impervious clothing and boots.
Respiratory Protection
If workplace exposure limit(s) of product or any component is exceeded (see
exposure guidelines), a NIOSH-approved air supplied respirator is advised in absence of
proper environmental control. OSHA regulations also permit other NIOSH respirators
(negative pressure type) under specified conditions (see your industrial hygienist).
Engineering or administrative controls should be implemented to reduce exposure.
9. PHYSICAL AND CHENUCAL PROPERTIES
Physical state
Form
Colour
Odour
Page 7 / 12
liquid
Liquid, liquid,
colourless
hydrocarbon -like

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Page 12 of 31
A
SAFETY DATA SHEET
MINERAL SPIRITS NON EXEMPT
20078
Boiling point/range
Melting point/range
PH
Flash point
Evaporation rate
Explosion limits
Vapour pressure
Vapour density
Density
Solubility
Partition coefficient (n-
octanolAvater)
Autoignition temperature
10. STABILITY AND REACTIVITY
Stability
S table.
Conditions to Avoid
Avoid contact with:
Page: 8
Revision Date: 06/21/2007
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
315.00 OF 1157.22 °C
-94 °F / -70 °C
No data
104.99 °F / 40.55 °C Tag closed cup
0.11 (N-Butyl Acetate)
1.0 %(V) 6.0 %(V)
2 mmHg @ 68.00 OF / 20.00 °C
4.9
0.7720 g/cm3 @ 60.00 OF / 15.56 °C
6.65 lb/gal @ 61 OF / 16 °C
negligible in water
No data
450 OF / 232 °C
Incompatible Products
Avoid contact with:, strong oxidizing agents
Hazardous Decomposition Products
May form:, carbon dioxide and carbon monoxide, various hydrocarbons
Hazardous Reactions
Product will not undergo hazardous polymerization.
Thermal Decomposition
No data
11. TOXICOLOGICAL INFORMATION
Acute Oral Toxicity
Page 9 / 12

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Page 13 of 31
SAFETY DATA SHEET
MINERAL SPIRITS NON EXEMPT
20078
Page: 9
Revision Date: 06/21/2007
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
MINERAL SPIRITS REGULAR (BASE LD 50 Rat: 5 g/kg
DATA)
TRZMETHYLBENZENE 1,2,4- LD 50 Rat: 6 g/kg
TRIMETHYLBENZENE, 1,3,5- LD 50 Rat: 5,000 mg/kg
XYLENE LD 50 Rat: 4,300 mg/kg
ETHYL BENZENE LD 50 Rat: 3,500 mg/kg
Acute Inhalation Toxicity
TRDAF-THYLBENZENE 1,2,4- LC 50 Rat: 18 g/m3, 4 h
ETHYL BENZENE,
LC Lo Rat: 4000 ppm 4 h
Acute Dermal Toxicity
MINERAL SPRUTS REGULAR (BASE LD 50 Rabbit: 3 g/kg
DATA)
XYLENE LD 50 Rabbit: 2,000 mg/kg
ETHYL BENZENE
LD 50 Rabbit: 15,433 mg/kg
12. ECOLOGICAL INFORMATION
Aquatic Toxicity
Acute and Prolonged Toxicity to Fish
No data
Acute Toxicity to Aquatic Invertebrates
No data
Environmental Fate and Pathways
No data
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ASHUN-1WID0
SAFETY DATA SHEET
MINERAL SPIRITS NON EXEMPT
20078
13. DISPOSAL CONSIDERATIONS
Page: 10
Revision Date: 06/21/2007
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
Waste Disposal Methods Dispose of in accordance with all applicable local, state and
federal regulations. For assistance with your waste management needs - including
disposal, recycling and waste stream reduction, contact Ashland Distribution's
Environmental Services Group at 800-637-7922.For assistance with your waste
management needs - including disposal, recycling and waste stream reduction, contact
Ashland Distribution's Environmental Services Group at 800-637-7922.
14. TRANSPORT INFORMATION
IMDG:
UN1268, PETROLEUM DISTILLATES, N.O.S. 3, III
IATA_P:
UN1268, Petroleum distillates, n.o.s. 3, Ill
IATA_C:
UN1268, Petroleum distillates, n.o.s. 3, III
CFR_ROAD:
UN1268, Petroleum distillates, n.o.s. (Aliphatic Petroleum Distillates, ) 3, III
CFR_RAIL:
UN1268, Petroleum distillates, n.o.s. (Aliphatic Petroleum Distillates, ) 3, III
CFR_INWTR:
UN1268, Petroleum distillates, n.o.s. (Aliphatic Petroleum Distillates, ) 3, 111
IMDG_INWTR:
UN1268, PETROLEUM DISTILLATES, N.O.S. 3, 111
1MDG_ROAD:
UN1268, PETROLEUM DISTILLATES, N.O.S. 3, III
I M DG_RAI L:
UN1268, PETROLEUM DISTILLATES, N.O.S. 3, 111
Dangerous goods descriptions (if indicated above) may not reflect package size, quantity,
end -use or region -specific exceptions that can be applied. Consult shipping documents
for descriptions that are specific to the shipment.
15. REGULATORY INFORMATION
California Prop. 65
WARNING! This product contains a chemical known in the State of California to cause
cancer.
Page 10 112

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Page 15 of 31
SAFETY DATA SHEET
MINERAL SPIRITS NON EXEMPT
20078
BENZENE
ETHYL BENZENE
Page: 11
Revision Date: 06/21/2007
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
WARNING! This product contains a chemical known in the State of California to cause
birth defects or other reproductive harm.
BENZENE
TOLUENE
Additional Regulations
US. OSHA Hazard Communication Standard: On One of the Floor Lists of the OSHA
HCS (29 CFR 1910.1200).
US. High Production Volume Chemicals
US. TSCA IUR 2006, Partially Exempt Petroleum Process Streams (40 CFR 710.46(b)(1))
OECD. Program to investigate the potential hazards of high production volume further
work.
SARA Hazard Classification Fire Hazard
Acute Health Hazard
Chronic Health Hazard
SARA 313 Component(s)
TRMETHYLBENZENE
1,2,4-
XYLENE
ETHYL BENZENE
OSHA Hazards
Health
HMIS 1
NFPA 0
6. OTHER INFORMATION
Page 11 / 12
95-63-6 6%
1330-20-7 2.31 %
100-41-4 0.66%
Combustible Liquid
Mild skin
Mild eye
Flammability Reactivity
2 0
2 0
Other

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Page 16 of 31
. ,.
SAFETY DATA SHEET
MINERAL SPIRITS NON EXEMPT
20078
Page: 12
Revision Date: 06/21/2007
Print Date: 6/23/2007
MSDS Number: R0000589
Version: 2.0
The information accumulated herein is believed to be accurate but is not warranted to be
whether originating with the company or not. Recipients are advised to confirm in advance
of need that the information is current, applicable, and suitable to their circumstances. This
MSDS has been prepared by Ashland's Environmental Health and Safety Department (1-
800-325-3751).
Page 12 / 12

MATERIAL SAFETY DATA SHEET Page 1
SECTION 1 - PRODUCT AND COMPANY IDENTIFICATION.
NOBLE OIL SERVICES, INC.
5617 Clyde Rhyne Drive
Loretta Accts. Payable
Sanford, NC 27330
800/662-5364 129
MEDICAL EMERGENCY 1-800-246-2890
PRODUCT NAME: Noble 10OZ 40# pail
PRODUCT DESCRIPTION:WHITE FREE FLOWING POWDER, LITTLE ODOR.
CHEMICAL FAMILY: ALKALINE DETERGENT.
REVISION DATE: 03/07/06 PRINT DATE: 01/12/07 PRINT TIME: 09:58
SECTION 2 - COMPOSITION, INFORMATION ON INGREDIENTS.
Hazard
CAS #
WT/Wt % Less Than
SODIUM METASILICATE
6834-92-0
<50
ACGIH TLV: N-E.
(TWA);
OSHA PEL: N.E.
(TWA);
DIETHYLENE GLYCOL BUTYL ETHER
112-34-5
1.4
ACGIH TLV: N.E.
(TWA);
OSHA PEL: N.E.
(TWA);
TRIETHANOLAMINE
102-71-6
<5
ACGIH TLV: 5 MG/M3
(TWA);
OSHA PEL: N.E.
(TWA);
NOTE 1 - Section 313 Supplier
Notification: "1" identifies chemical ingredients subject
to reporting requirements
of Section 313
of the Emergency
Planning and Community
Right -To -Know Act of 1986.
This information should be included in all MSDS's that are
copied and distributed for
this material.
SECTION 3 - HAZARDS IDENTIFICATION.
HEALTH------------------- 2
INSTABILITY-------------- 0
FIRE--------------------- 0
OTHER-------------------- x
(0=insignificant; 1=slight; 2=moderate; 3=high; 4=extreme)
THRESHOLD LIMIT VALUE: N.E., blended product. See Section 2 for information on listed
ingredients.
PRIMATY ROUTES OF ENTRY: Eye contact, Skin contact.
EFFECTS OF ACUTE OVEREXPOSURE:
Eyes - Severe irritation, or burns possible.
Skin - Irritation, or burns possible with prolonged contact.
Swallowing - Irritation or burns of mouth, throat and stomach. Stomach upset.
EFFECTS OF CHRONIC OVEREXPOSURE: Unknown; none expected beyond acute effects.
CARCINOGENICITY: This product or its ingredients have not been identified as a carcinogen
or probable carcinogen by NTP, IARC monographs, or OSHA.
MEDICAL CONDITIONS AGGRAVATED BY EXPOSURE: Dermatitis and similar skin disorders.
SECTION 4 - FIRST AID MEASURES.

(Continued)
Page 2
PRODUCT NAME: Noble 10OZ 40# pail
REVISION DATE: 03/07/06 PRINT DATE: 01/12/07 PRINT TIME: 09:58
EYES - Immediately flush with cool.running water holding eye lids apart. Remove contact
lenses if present, and continue flushing for 15 minnutes. Get medical assistance.
SKIN - Immediately flush with cool running water for 15 minutes. Remove contaminated
clothing and wash before reuse. If irritation or burn develops and persists, get medical
advice or assistance.
INHALED - Remove to fresh air. Immediately call for medical advice or assistance if
breathing difficulty or irritation is severe or continues.
SWALLOWED - Rinse mouth with large amounts of water. Drink water, milk or other fluids to
dilute. Do not induce vomiting unless directed by medical personnel. Immediately call
for medical advice or assistance.
SECTION 5 - FIRE FIGHTING MEASURES.
Extinguishing media: As needed for surrounding fire.
Special Fire Fighting Procedures: For any chemical fire wear self contained breathing
apparatus, and protective clothing to prevent contact.
Unusual Fire and Explosion Hazards: None.
Hazardous Combustion Products: Oxides of carbon and phosphorous.
SECTION 6 - ACCIDENTAL RELEASE MEASURES.
Small Spills, less than 2 pounds: Recover as practical. Flush spill area to drain with
excess water.
Large Spills: Only knowledgeable and properly protected people should work with a large
spill. Get professional assistance if necessary.
Stop source of discharge if safe to do so. Evacuate unprotected personnel from the
immediate area. Keep material dry. Contain spilled material, and keep from discharging
to surface waters. Recover to drum for later use, treatment or disposal.
Flush residual to drain.
Notify local, state, or national authorities if required.
Disposal: Product and un-neutralized solutions are alkaline. Normally sewer disposable
in dilute solutions. Check with local authorities about any possible restrictions.
SECTION 7 - HANDLING AND STORAGE.
Handling: Avoid unnecessary contact with product. Avoid breathing product dust, or mists
of solution of product.
Wash immediately after contact. Wash after use.
Clean up spills promptly to prevent accidental contact.
Prevent contact with incompatable materials; see Section 10.
Storage: Keep containers tightly closed. Keep product dry to prevent caking.
SECTION 8 - EXPOSURE CONTROLS, PERSONAL PROTECTION.

(Continued)
Page 3
PRODUCT NAME: Noble 10OZ 40# pail
REVISION DATE: 03/07/06 PRINT DATE: 01/12/07 PRINT TIME: 09:58
Ventilation: General or local to avoid exposure to irritating product mists of solutions.
Respirator: None normally required. NIOSH/MSHA approved respirator where conditions may
cause exposure limits to be exceeded from dust of product or mists of solutions.
Eye Protection: Glasses, goggles, or face shield to prevent eye exposure.
Protective Clothing: Chemical resistant, impermeable gloves as needed to prevent
excessive contact. Full body covering covering and shoes as needed to prevent excessive
contact.
Other Protective Equipment or Measures: Eye wash stations in the work area.
SECTION 9 - PHYSICAL AND CHEMICAL PROPERTIES.
Boiling Point: N.E. Vapor Pressure: N.E.
Specific Gravity: N.E.
Percent Volitile: Less than 215
Solubility in Water: Complete.
Vapor Density: N.E.
Evaporation Rate: N.A.
pH: 12 ± .5 (2% solution)
Appearance and Odor: See Section 1. V.O.C. : Nil.
SECTION 10 - STABILITY AND REACTIVITY.
Stable: Yes. Hazardous Polymerization will not occur.
Conditions to Avoid: Contact with incompatable materials (see below).
Incompatable Materials: Strong oxidizing agents, strong acids.
SECTION 11 TOXICOLOGICAL INFORMATION
no data
SECTION 12 - ECOLOGICAL INFORMATION
no data
SECTION 13 DISPOSAL INFORMATION
WASTE MANAGEMENT INFOMATION:
If this product becomes a waste, it does not meet the criteria of a hazardous waste as
defined under the Resorce Conservation and Recovery act (RCRA) 40 CFR 261.
But still check and dispose of in accordance with all applicable local, state and federal
regulations.
SECTION 14 - TRANSPORT INFORMATION
DOT Information- 49 CFR 172.101
DOT Description: NON -REGULATED BY D.O.T.
CONTAINER/MODE: (POWDER) DRUM
SECTION 15 - REGULATORY INFORMATION

(Continued) Page 4
PRODUCT NAME: Noble 10OZ 40# pail
REVISION DATE: 03/07/06 PRINT DATE: 01/12/07 PRINT TIME: 09:58
US FEDERAL Regulations: (TSCA Toxic Substances Control Act)Status
TSCA (United States) The intentional ingredients of this product are listed.
CERCLA RQ-40 CFR 302.4 (a): none listed
SARA 302 COMPONENTS-40 CFR 355 APPENDIX A: NONE
SECTION 311/312 HAZARD CLASS - 40 CFR 370.2
SARA 313 COMPONENTS - 40 CFR 372.65: Diethylene Glycol butyl ether
cas# 112-34-5 -- 1.41;
International Regulations Inventory Status: not determined
State and Local Regulations: California Proposition 65: none
1
SECTION 16 - OTHER INFORMATION
DISCLAIMER:
The above information is, to the best of our knowledge, current, accurate, and complete
based on information reasonably availabe to us as of the date of preparation of this form.
However, it is the users's reponsibility to determine the safety, toxicity and suitability
for his or her own use of the product described herein. Since the actual use by others is
beyond our control, no guarantee, expressed or implied, is made by us as to the effects of
such use or on the safety or toxicity of this product. Nor do we assume any liability
arising out of use by others of the product. Nor is the information herein to be
construed as absolutely complete, since additional information may be necessary or
desirable when exceptional conditions or circumstances exist or because of applicable laws
or regulations.
NE = NOT ESTABLISHED / NA = NOT APPLICABLE
END OF DOCUMENT

Material Safety Data Sheet
1. Product and company identification
Product name
Rustilo DWX 30
MSDS #
451261
Historic MSDS #:
09107-AE
Code
451261-US03
Product use
Rust preventive
For specific application advice see appropriate Technical Data Sheet or consult our company
representative.
Manufacturer
Castrol Industrial North America, Inc.
150 W. Warrenville Road
Naperville, IL 60563
Supplier
Castrol Industrial North America, Inc.
150 W. Warrenville Road
Naperville, IL 60563
Product Information: 1-800-621-2661
EMERGENCY SPILL
1 [phone] CHEMTREC (USA)
INFORMATION:
2. Hazards identification
Physical state Liquid.
Color Brown. [Light]
Emergency overview WARNING!
COMBUSTIBLE LIQUID AND VAPOR.
INHALATION CAUSES HEADACHES, DIZZINESS, DROWSINESS AND NAUSEA AND MAY
LEAD TO UNCONSCIOUSNESS.
CAUSES EYE AND SKIN IRRITATION.
MAY CAUSE RESPIRATORY TRACT IRRITATION.
ASPIRATION HAZARD.
HARMFUL OR FATAL IF SWALLOWED.
CAN ENTER LUNGS AND CAUSE DAMAGE.
Combustible liquid. Prolonged or repeated contact can defat the skin and lead to irritation and/or
dermatitis. Aspiration hazard if swallowed. Can enter lungs and cause damage. Keep away from
heat, sparks and flame. Do not breathe vapor or mist. Do not ingest. If ingested, do not induce
vomiting. Avoid contact with eyes, skin and clothing. Use only with adequate ventilation. Keep
container tightly closed and sealed until ready for use. Wash thoroughly after handling.
Routes of entry Dermal contact. Eye contact. Inhalation. Ingestion.
Potential health effects
Eyes Causes eye irritation.
Skin Causes skin irritation. Prolonged or repeated contact can defat the skin and lead to irritation
and/or dermatitis.
Inhalation Vapors may cause drowsiness and dizziness. Can cause central nervous system (CNS)
depression. May cause respiratory tract irritation.
Ingestion Aspiration hazard if swallowed. Can enter lungs and cause damage. Ingestion may cause
gastrointestinal irritation and diarrhea.
See toxicological information (section 11)
Product name Rustilo DWX 30 Product code 451261-US03 Page: 1/7
Version 1.01 Date of issue 12/17/2009. Format US Language ENGLISH.
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3. Composition/information on ingredients
Ingredient name
CAS #
%
Petroleum naphtha
64742-88-7
80 - 85
Low boiling point naphtha - unspecified
64742-95-6
5 - 10
2-(2-butoxyethoxy)ethanol
112-34-5
1 - 5
1,2,4-Trimethylbenzene
95-63-6
1 - 5
Paraffin waxes, petroleum, clay -treated
64742-43-4
1 - 5
Mesitylene
108-67-8
1 - 5
4. First aid measures
Eye contact In case of contact, immediately flush eyes with plenty of water for at least 15 minutes. Get medical
attention.
Skin contact Immediately wash exposed skin with soap and water. Remove contaminated clothing and shoes.
Wash clothing before reuse. Clean shoes thoroughly before reuse. Get medical attention.
Inhalation If inhaled, remove to fresh air. If it is suspected that fumes are still present, the rescuer should
wear an appropriate mask or self-contained breathing apparatus. If not breathing, give artificial
respiration. If breathing is difficult, give oxygen. Get medical attention immediately.
Ingestion Aspiration hazard if swallowed. Can enter lungs and cause damage. Do not induce vomiting.
Never give anything by mouth to an unconscious person. Get medical attention immediately. .
5. Fire -fighting measures
Flammability of the
Combustible liquid.
product
Flash point
Open cup: 48.333°C (119°F) [Cleveland.]
Fire/explosion hazards
In a fire or if heated, a pressure increase will occur and the container may burst, with the risk of a
subsequent explosion.
Extinguishing media
Suitable
Use dry chemical, COz, water spray (fog) or foam.
Not suitable
Do not use water jet.
Fire -fighting procedures
Promptly isolate the scene by removing all persons from the vicinity of the incident if there is a fire.
No action shall be taken involving any personal risk or without suitable training. Move containers
from fire area if this can be done without risk. Use water spray to keep fire -exposed containers
cool.
Hazardous combustion
Combustion products may include the following:
products
metal oxide/oxides
carbon oxides (CO, COz) (carbon monoxide, carbon dioxide)
sulfur oxides (S02, SO3 etc.)
Protective clothing (fire)
Fire-fighters should wear appropriate protective equipment and self-contained breathing apparatus
(SCBA) with a full face -piece operated in positive pressure mode.
6. Accidental release measures
Personal precautions
No action shall be taken involving any personal risk or without suitable training. Keep unnecessary
and unprotected personnel from entering. Do not touch or walk through spilled material. Shut off
all ignition sources. No flares, smoking or flames in hazard area. Do not breathe vapor or mist.
Provide adequate ventilation. Wear appropriate respirator when ventilation is inadequate. Put on
appropriate personal protective equipment (see section 8).
Environmental
Avoid dispersal of spilled material and runoff and contact with soil, waterways, drains and sewers.
precautions
Inform the relevant authorities if the product has caused environmental pollution (sewers,
waterways, soil or air).
Methods for cleaning up
Product name Rustilo DWX 30 Product code 451261-US03 Page: 2/7
Version 1.01 Date of issue 12/17/2009, Format US Language ENGLISH.
(US) (ENGLISH)

Large spill
Stop leak if without risk. Move containers from spill area. Approach release from upwind. Prevent
entry into sewers, water courses, basements or confined areas. Wash spillages into an effluent
treatment plant or proceed as follows. Contain and collect spillage with non-combustible,
absorbent material e.g. sand, earth, vermiculite or diatomaceous earth and place in container for
disposal according to local regulations (see section 13). Use spark -proof tools and explosion -proof
equipment. Dispose of via a licensed waste disposal contractor. Contaminated absorbent
material may pose the same hazard as the spilled product. Note: see section 1 for emergency
contact information and section 13 for waste disposal.
Small spill
Stop leak if without risk. Move containers from spill area. Dilute with water and mop up if water-
soluble or absorb with an inert dry material and place in an appropriate waste disposal container.
Use spark -proof tools and explosion -proof equipment. Dispose of via a licensed waste disposal
contractor.
7. Handling and storage
Handling
Put on appropriate personal protective equipment (see section 8). Workers should wash hands
and face before eating, drinking and smoking. Do not breathe vapor or mist. Do not ingest. Avoid
contact with eyes, skin and clothing. Use only with adequate ventilation. Wear appropriate
respirator when ventilation is inadequate. Do not enter storage areas and confined spaces unless
adequately ventilated. Store and use away from heat, sparks, open flame or any other ignition
source. Use explosion -proof electrical (ventilating, lighting and material handling) equipment. Use
non -sparking tools. Take precautionary measures against electrostatic discharges. To avoid fire
or explosion, dissipate static electricity during transfer by grounding and bonding containers and
equipment before transferring material.
Storage
Store in accordance with local regulations. Store in a segregated and approved area. Store away
from direct sunlight in a dry, cool and well -ventilated area, away from incompatible materials (see
section 10). Eliminate all ignition sources. Separate from oxidizing materials. Keep container
tightly closed and sealed until ready for use. Containers that have been opened must be carefully
resealed and kept upright to prevent leakage. Do not store in unlabeled containers. Use
appropriate containment to avoid environmental contamination.
8. Exposure controls/personal protection
Occupational exposure limits
Ingredient name Occupational exposure limits
1,2,4-Trimethylbenzene ACGIH TLV (United States).
TWA: 123 mg/m' 8 hour(s). Issued/Revised: 9/1994
TWA: 25 ppm 8 hour(s). Issued/Revised: 9/1994
Paraffin waxes, petroleum, clay -treated ACGIH TLV (United States).
TWA: 2 mg/m' 8 hour(s). Form: Fume
Mesitylene ACGIH TLV (United States).
TWA: 123 mg/m' 8 hour(s). Issued/Revised: 9/1994
TWA: 25 ppm 8 hour(s). Issued/Revised: 9/1994
While specific OELs for certain components may be shown in this section, other components may be present in any mist, vapor or
dust produced. Therefore, the specific OELs may not be applicable to the product as a whole and are provided for guidance only.
Some states may enforce more stringent exposure limits.
Control Measures Use only with adequate ventilation. Use process enclosures, local exhaust ventilation or other
engineering controls to keep worker exposure to airborne contaminants below any recommended
or statutory limits. The engineering controls also need to keep gas, vapor or dust concentrations
below any lower explosive limits. Use explosion -proof ventilation equipment.
Hygiene measures Wash hands, forearms and face thoroughly after handling chemical products, before eating,
smoking and using the lavatory and at the end of the working period. Appropriate techniques
should be used to remove potentially contaminated clothing. Wash contaminated clothing before
reusing.
Personal protection
Eyes Avoid contact with eyes. Safety glasses with side shields or chemical goggles.
Skin and body Do not get on skin or clothing. Wear suitable protective clothing.
Respiratory Use adequate ventilation. Do not breathe vapor or mist.
Product name Rustilo DWX 30 Product code 451261-US03 Page: 317
Version 1.01 Date of issue 12/17/2009. Format US Language ENGLISH.
(US) (ENGLISH)

Hands The correct choice of protective gloves depends upon the chemicals being handled, the conditions
of work and use, and the condition of the gloves (even the best chemically resistant glove will
break down after repeated chemical exposures). Most gloves provide only a short time of
protection before they must be discarded and replaced. Because specific work environments and
material handling practices vary, safety procedures should be developed for each intended
application. Gloves should therefore be chosen in consultation with the supplier/manufacturer and
with a full assessment of the working conditions.
9. Physical and chemical properties
Physical state
Liquid.
Color
Brown. [Light]
Odor
Mild.
Flash point
Open cup: 48.333°C (119°F) [Cleveland.]
Density
785 kg/m' (0.785 g/cm') at 15.6°C
Viscosity
Kinematic: <2 mmZ/s (<2 cSt) at 40°C
Solubility
insoluble in water.
10. Stability and reactivity
Stability and reactivity
The product is stable.
Possibility of hazardous
Under normal conditions of storage and use, hazardous reactions will not occur.
reactions
Conditions to avoid
Avoid all possible sources of ignition (spark or flame).
Incompatibility with
Reactive or incompatible with the following materials: oxidizing materials.
various substances
Hazardous decomposition
Under normal conditions of storage and use, hazardous decomposition products should not be
products
produced.
Hazardous polymerization
Under normal conditions of storage and use, hazardous polymerization will not occur.
11. Toxicological information
Acute toxicity
'
Other Toxicity Data
Can cause central nervous system (CNS) depression.
Contains material that may cause target organ damage, based on animal data. Target Organs:
kidneys.
Long term studies have shown that some of the base oils contained in this product may cause
tumor promotion in laboratory animals. The mechanism of this promotion effect appears to be
related to repetitive skin irritation from chronic exposure conditions. With the normal safety and
personal hygiene work practices, it is believed that this promotion mechanism has little or no
relevance to humans. None of the oils are classified as carcinogens.
Other information
Potential chronic health effects
Carcinogenicity
No known significant effects or critical hazards.
12. Ecological information
Ecotoxicity
No testing has been performed by the manufacturer
Product name Rustilo DWX 30 Product code 451261-US03 Page: 4/7
Version 1.01 Date of issue 12/17/2009. Format US Language ENGLISH.
(US) (ENGLISH)

13. Disposal considerations
Waste information The generation of waste should be avoided or minimized wherever possible. Empty containers or
liners may retain some product residues. This material and its container must be disposed of in a
safe way. Dispose of surplus and non -recyclable products via a licensed waste disposal
contractor. Disposal of this product, solutions and any by-products should at all times comply with
the requirements of environmental protection and waste disposal legislation and any regional local
authority requirements. Avoid dispersal of spilled material and runoff and contact with soil,
waterways, drains and sewers.
NOTE: The generator of waste has the responsibility for proper waste identification (based on characteristic(s) or listing),
transportation and disposal
14. Transport information
International transport regulations
Regulatory
UN
Proper shipping name
Class
Packing group
Additional information
information
number
DOT
UN 1993
FLAMMABLE LIQUID, N.O.S.
3
III
-
Classification
(Petroleum naphtha)
TDG
UN 1993
FLAMMABLE LIQUID, N.O.S.
3
III
-
Classification
(Petroleum naphtha)
IMDG
UN 1993
FLAMMABLE LIQUID, N.O.S.
3
III
-
Classification
(Petroleum naphtha)
IATA/ICAO
UN 1993
FLAMMABLE LIQUIDS,
3
III
-
Classification
N.O.S. (Petroleum naphtha)
15. Regulatory information
U.S. Federal Regulations
United States inventory
All components are listed or exempted.
(TSCA 8b)
TSCA 12(b) one-time export: Naphthalene; propylbenzene
SARA 302/304/3111312 extremely hazardous substances: No products were found.
SARA 302/304 emergency planning and notification: No products were found.
SARA 302/304/311/312 hazardous chemicals: 1,2,4-Trimethylbenzene; Mesitylene; 2-(2-
butoxyethoxy)ethanol
SARA 311/312 MSDS distribution - chemical inventory - hazard identification: Rustilo DWX
30: Fire hazard, Immediate (acute) health hazard, Delayed (chronic) health hazard
SARA 313
Product name CAS number Concentration
Form R - Reporting
Barium sulfonate 93820-55-4 1.53 - 2.2874
requirements
2-(2-butoxyethoxy)ethanol 112-34-5 2.12
1,2,4-Trimethylbenzene 95-63-6 1.4437
Supplier notification
2-(2-butoxyethoxy)ethanol 112-34-5 2.12
1,2,4-Trimethyl benzene 95-63-6 1.4437
CERCLA Sections
CERCLA: Hazardous substances.: Naphthalene: 100 lbs. (45.4 kg); Ethylbenzene: 1000 lbs. (454
102a/103 Hazardous
kg); Cumene: 5000 lbs. (2270 kg); xylene: 100 lbs. (45.4 kg); Benzene: 10 lbs. (4.54 kg); 2-(2-
Substances (40 CFR
butoxyethoxy)ethanol;
Part 302.4):
State regulations
Product name Rustilo DWX 30 Product code 451261-US03 Page: 5/7
Version 1.01 Date of issue 12/17/2009. Format US Language ENGLISH.
(US) (ENGLISH)

Massachusetts
Substances
New Jersey Hazardous
Substances
Pennsylvania RTK
Hazardous Substances
California Prop. 65
Inventories
Canada inventory
Europe inventory
Australia inventory (AICS)
China inventory (IECSC)
Japan inventory (ENCS)
Korea inventory (KECI)
Philippines inventory
(PICCS)
16.Other information
Label requirements
HMIS® Rating :
History
Date of issue
Date of previous issue
Prepared by
Notice to reader
The following components are listed: MESITYLENE; PSEUDOCUMENE
The following components are listed: MINERAL SPIRITS; SOLVENT NAPHTHA (PETROLEUM)
medium aliphatic; TRIMETHYL BENZENE (mixed isomers); BENZENE, TRIMETHYL-;
PSEUDOCUMENE; 1,2,4-TRIMETHYL BENZENE; Barium; GLYCOL ETHERS
The following components are listed: BENZENE, TRIMETHYL-; PSEUDOCUMENE; Barium;
GLYCOL ETHERS
WARNING: This product contains a chemical known to the State of California to cause cancer.
Naphthalene; Ethylbenzene
WARNING: This product contains a chemical known to the State of California to cause cancer and
birth defects or other reproductive harm.
Benzene
All components are listed or exempted.
All components are listed or exempted.
All components are listed or exempted.
All components are listed or exempted.
Not determined.
All components are listed or exempted.
At least one component is not listed.
WARNING!
COMBUSTIBLE LIQUID AND VAPOR.
INHALATION CAUSES HEADACHES, DIZZINESS, DROWSINESS AND NAUSEA AND MAY
LEAD TO UNCONSCIOUSNESS.
CAUSES EYE AND SKIN IRRITATION.
MAY CAUSE RESPIRATORY TRACT IRRITATION.
ASPIRATION HAZARD.
HARMFUL OR FATAL IF SWALLOWED.
CAN ENTER LUNGS AND CAUSE DAMAGE.
Health " 2
Flammability 2
Physical 0
Hazard
Personal B
protection
12/17/2009
11 /20/2009.
Product Stewardship
National Fire
Protection
Association (U.S.A.)
Fire hazard
Health U Instability
Specific hazard
Product name Rustilo DWX 30 Product code 451261-US03 Page: 6/7
Version 1.01 Date of issue 12/17/2009. Format US Language ENGLISH.
(US) (ENGLISH)

All reasonably practicable steps have been taken to ensure this data sheet and the health, safety and environmental information
contained in it is accurate as of the date specified below. No warranty or representation, express or implied is made as to the
accuracy or completeness of the data and information in this data sheet.
The data and advice given apply when the product is sold for the stated application or applications. You should not use the product
other than for the stated application or applications without seeking advice from us.
It is the user's obligation to evaluate and use this product safely and to comply with all applicable laws and regulations. The BP
Group shall not be responsible for any damage or injury resulting from use, other than the stated product use of the material, from
any failure to adhere to recommendations, or from any hazards inherent in the nature of the material. Purchasers of the product for
supply to a third party for use at work, have a duty to take all necessary steps to ensure that any person handling or using the
product is provided with the information in this sheet. Employers have a duty to tell employees and others who may be affected of
any hazards described in this sheet and of any precautions that should be taken.
Product name Rustilo DWX 30 Product code 451261-US03 Page: 7/7
Version 1.01 Date of issue 12/17/2009. Format US Language ENGLISH.
(US) (ENGLISH)

Romanski, Autumn
From: Marty Stewart [[e-mail]]
Sent: Tuesday, March 30, 2010 9:22 PM
To: Romanski, Autumn
Subject: RE: GKN Stormwater
Autumn,
Yes we are still on for Thursday, but can it be 10:00am? I believe that is what I got from
the staff at GKN. The address you have is correct.
See you Thursday at 10am.
Marty Stewart
Staff Professional II
Kleinfelder
3500 Gateway Centre Blvd., Suite 200
Morrisville, NC 27560
mstewart(@kleinfelder.com
919.755.5011 ext. 108 (o)
336.263.6864 (c)
919.861.7777(f)
>>> "Romanski, Autumn" 03/30/10 1:54 PM >>>
Marty,
Just wanted to confirm we are still meeting at GKN Thurs April 1st at 09:30AM.
I have the address as 6400 Durham Rd Timberlake, NC. (Can see from hwy 501 going into
Roxboro).
Look forward to meeting you then.
Autumn
From: Marty Stewart[mailto:[e-mail]]
Sent: Tuesday, February 16, 2010 2:27 PM
To: Romanski, Autumn
Subject: RE: GKN Stormwater
Autumn,
Thursday April 1 will be fine. Let's pencil that date in for a site visit.
Marty R. Stewart
Staff Professional II
3500 Gateway Centre B1vd,Suite 200
Morrisville, NC 27560
ol,919.755.5011 ext. 108
1

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>>> "Romanski, Autumn" 2/16/2010 1:27 PM >>>
Marty,
Sorry, but I am booked on March 18th and I have office emergency phone duty the following
week and will not be able to schedule field work that week. I have open Wednesday March 10th
and Wednesday March 17. The next Thursday I have available is April 1st. Just let me know
which of these options will work for you.
Autumn
From: Marty Stewart [[e-mail]]
Sent: Monday, February 15, 2010 9:34 AM
To: Romanski, Autumn
Cc: Nisely, Myrl
Subject: RE: GKN Stormwater
How about Thursday March 18th? Conflicts prevent me from attending a 3/11 meeting. Let me
know.
Marty R. Stewart
Staff Professional II
3500 Gateway Centre B1vd,Suite 200
Morrisville, NC 27560
of 919.755.5011 ext. 108
cl 336.263.6864
f 1 919.861.7777
rcid:image001.png(@01CAD029.A584A2901
>>> "Romanski, Autumn" 2/12/2010 2:14 PM >>>
Marty,
I can plan to meet at the site on Thursday March 11th @10 AM.
Can you confirm this date and time will work?
Look forwarding to seeing you.
Sincerely,
Autumn
-----Original Message -----
From: Marty Stewart[mailto:[e-mail]]
Sent: Wednesday, February 10, 2010 10:50 PM
To: Romanski, Autumn; Nisely, Myrl
Subject: GKN Stormwater
Myrl,
0)

v
We spoke about meeting at the GKN site with Autumn and the EHS staff at GKN. I spoke with Kim
Killian at GKN and it would be best for the GKN staff for a site visit to occur on a Thursday
in the coming weeks (when they are working at that location). I propose a Thursday in the
first or second week of March for all of us to meet and walk the site and discuss the
outfalls.
Let me know you thoughts.
Have a good day,
Marty Stewart
Staff Professional II
Kleinfelder
3500 Gateway Centre Blvd., Suite 200
Morrisville, NC 27560
mstewart(@kleinfelder.com
919.755.5011 ext. 108 (o)
336.263.6864 (c)
919.861.7777(f)
Warning: Information provided via electronic media is not guaranteed against defects
including translation and transmission errors.
If the reader is not the intended recipient, you are hereby notified that any dissemination,
distribution or copying of this communication is strictly prohibited. If you have received
this information in error, please notify the sender immediately.
Warning: Information provided via electronic media is not guaranteed against
defects including translation and transmission errors.
If the reader is not the intended recipient, you are hereby notified that any
dissemination, distribution or copying of this communication is strictly
prohibited. If you have received this information in error, please notify the
sender immediately.
9

Warning: Information provided via electronic media is not guaranteed against
defects including translation and transmission errors.
If the reader is not the intended recipient, you are hereby notified that any
dissemination, distribution or copying of this communication is strictly
prohibited. If you have received this information in error, please notify the
sender immediately.
Warning: Information provided via electronic media is not guaranteed against defects
including translation and transmission errors.
If the reader is not the intended recipient, you are hereby notified that any dissemination,
distribution or copying of this communication is strictly prohibited. If you have received
this information in error, please notify the sender immediately.
4

Romanski, Autumn
From: Nisely, Myrl
Sent: Tuesday, January 26, 2010 11:18 AM
To: Romanski, Autumn
Subject: FW: Your Question About Outfalls
Attachments: ATT00001.bmp
FYI. This site will likely need to be viewed to fully understand what is needed.
Myrl
From: Marty Stewart [mailto:[e-mail]]
Sent: Tuesday, January 26, 2010 11:16 AM
To: Nisely, Myrl
Cc: Smith, Danny
Subject: Re: Your Question About Outfalls
Mr. Nisely,
Sorry we have been unable to connect. My schedule has been crazy lately, with working out of the office, field work and
a new child at home.
I will be able to call you in the morning to discuss this more, which I think we should do. Just to give you some
information of what I would like clarification on:
1- How many outfalls do you have that the facility possesses? They say they have 9 headwalls and have been treating
them like outfalls, although I am not sure they all are outfalls.
2-I am aware that all the industrial affected outfalls need to be sampled... not questioning that. But why are non-
industrial impacted outfalls required to be sampled at all? Is it solely because there are more than one? Again this will
also lead back to my issue on headwalls/outfalls.
Again sorry for not connecting with earlier. I hope to connect tomorrow.
Marty R. Stewart
Staff Professional II
3500 Gateway Centre Blvd,Suite 200
Morrisville, NC 27560
of 919.755.5011 ext. 108
cl 336.263.6864
f 1919.861.7777
r DHR
Bright People. Right Solutions.
>>> "Nisely, Myrl" <[e-mail]> 1/26/2010 10:52 AM >>>
Dear Mr. Stewart,
In spite of repeated attempts to reach you by phone, we still have not communicated about the outfalls at GKN. Here
is what I can tell you.
DWQ policy will not allow Representative Outfall Status for the industrial ones. Each will require sampling per the
permit. Any "purely stormwater" outfalls not impacted by industrial activity may be granted that status, meaning that

if there are two or more, it may be possible to sample only one to cover the others. Even so, ALL outfalls are to be
judged for the Qualitative parameters twice a year.
If you have further questions, please contact me.
Myrl A. Nisely <°))))><
Environmental Chemist
NC.DENR - Div. Water Quality
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Telephone: [phone] or x4255
Fax: [phone]
myrl.nisely(@ncdenr.gov ><((((°>
E-mail correspondence to and from this address may be subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Warning: Information provided via electronic media is not guaranteed against
defects including translation and transmission errors.
If the reader is not the intended recipient, you are hereby notified that any
dissemination, distribution or copying of this communication is strictly
prohibited. If you have received this information in error, please notify the
sender immediately.
`]

Romanski, Autumn
From: Nisely, Myrl
Sent: Tuesday, January 26, 2010 11:18 AM
To: Romanski, Autumn
Subject: FW: Your Question About Outfalls
FYI. This site will likely need to be viewed to fully understand what is needed.
Myrl
From: Marty Stewart [mailto:[e-mail]]
Sent: Tuesday, January 26, 2010 11:16 AM
To: Nisely, Myrl
Cc: Smith, Danny
Subject: Re: Your Question About Outfalls
Mr. Nisely,
Sorry we have been unable to connect. My schedule has been crazy lately, with working out of the office, field work and
a new child at home.
I will be able to call you in the morning to discuss this more, which I think we should do. Just to give you some
information of what I would like clarification on:
1- How many outfalls do you have that the facility possesses? They say they have 9 headwalls and have been treating
them like outfalls, although I am not sure they all are outfalls.
2-I am aware that all the industrial affected outfalls need to be sampled... not questioning that. But why are non-
industrial impacted outfalls required to be sampled at all? Is it solely because there are more than one? Again this will
also lead back to my issue on headwalls/outfalls.
Again sorry for not connecting with earlier. I hope to connect tomorrow.
Marty R. Stewart
Staff Professional II
3500 Gateway Centre Blvd,Suite 200
Morrisville, NC 27560
of 919.755.5011 ext. 108
cl 336.263.6864
f 1919.861.7777
KL EfNF,EL L3,�R
Bright People. Right Solutions.
>>> "Nisely, Myrl" <[e-mail]> 1/26/2010 10:52 AM >>>
Dear Mr. Stewart,
In spite of repeated attempts to reach you by phone, we still have not communicated about the outfalls at GKN. Here
is what I can tell you.
DWQ policy will not allow Representative Outfall Status for the industrial ones. Each will require sampling per the
permit. Any "purely stormwater" outfalls not impacted by industrial activity may be granted that status, meaning that

if there are two or more, it may be possible to sample only one to cover the others. Even so, ALL outfalls are to be
judged for the Qualitative parameters twice a year.
If you have further questions, please contact me.
Myrl A. Nisely <°))))><
Environmental Chemist
NC DENR - Div. Water Quality
Raleigh Regional Office
1628 Mail Service Center
Raleigh, NC 27699-1628
Telephone: [phone] or x4255
Fax: [phone]
myrl.nisely(@ncdenr.gov ><((((°>
E-mail correspondence to and from this address may be subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Warning: Information provided via electronic media is not guaranteed against
defects including translation and transmission errors.
If the reader is not the intended recipient, you are hereby notified that any
dissemination, distribution or copying of this communication is strictly
prohibited. If you have received this information in error, please notify the
sender immediately.
2

i2E: Analytical Monitoring Requirements (TTO)
Subject: RE: Analytical Monitoring Requirements (TTO)
From: "Delores Green -Epps" <Delores.Green [e-mail]>
Date: Fri, 18 Nov 2005 17:01:37 -0500
To: <[e-mail]>
Ms. Atkins,
Per our discussion on Thursday, November 17, 2005, GKN Driveline Roxboro Facility is not required to conduct a TTO sampling per
the Stormwater Permit requirements. All test results were provided during the site visit.
Sincerely,
Delores Green -Epps
EHS Coordinator
GKN Driveline Roxboro Facility
336-364-6326
From: Delores Green -Epps
Sent: Tuesday, November 15, 2005 4:15 PM
To: '[e-mail]'
Cc: Philip Kinney
Subject: Analytical Monitoring Requirements (TTO)
Ms. Atkins,
I am writing to request clarification of your Compliance Evaluation Inspection. During your site visit you requested to see the results of
the TTO sampling. Upon further review of GKN's permit (NCG030000), Part II Page 5 of 7, Analytical Monitoring Requirements,
Footnotes: 5 states, "Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations,
manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes.....
Based upon my interpretation of the permit, GKN is not required to complete a TTO sampling analysis because the facility's process
does not consist of metal finishing, manufacture semiconductors,... Please provide me with your interpretation.
Thanks in advance for your assistance.
Delores Green -Epps
EHS Coordinator
GKN Driveline Roxboro Facility
336-364-6326
DISCLAIMER:
This E-Mail is strictly confidential and intended solely for the addressee. It may contain information which is covered by
legal profession or other privilege. If you are not the intended addressee you must not use, disclose or copy this
transmission.
This E-Mail is not intended to impose nor shall it be construed as imposing any legally binding obligation upon GKN plc
and/or any of its subsidiaries or associated companies.
Neither GKN plc nor any of its subsidiaries or associated companies gives any representation or warranty as the
accuracy or completeness of the contents of this E-Mail. GKN shall not be held liable to any person resulting from the
use of any information contained in this E-Mail and shall not be liable to any person who acts or omits to do anything in
reliance upon it.
1 of 1 11/21/2005 8:23 AM

/ 0��� W A
O `C
October 28, 2005
Delores Green -Epps
GKN Automotive
6400 Durham Road
Timberlake, NC 27583
Subject: Compliance Evaluation Inspection
GKN Automotive - Timberlake Plant
COC Number NCG030429
Person County
Dear Ms. Green- Epps:
Michael F. Easley, Governor
William G. Ross, Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
I conducted a compliance evaluation inspection of the GKN Automotive Timberlake plant on October 25, 2005..
You and Russ Comer represented the facility during the inspection. Your assistance was greatly appreciated.
The GKN Automotive Timberlake plant is located on Durham Road (Hwy 501) in Timberlake, NC. The site
contains nine stormwater outfalls that discharge into an unnamed tributary of the North Flat River in the Neuse
River basin.
The stormwater management and the spill prevention and response plans were reviewed during the inspection and
found to be sufficient. The plans are revised annually by GKN officials and were last revised by you in October
2005. The site map did not contain all of the outfalls and should be updated.
HAZWOP team members undergo annual training in spill response. All other employees are informed to contact
team members in the event of a spill.
The plant met the cut-off concentrations for analytical monitoring during the first year of the permit. Additional
analytical monitoring is not required until the last year. Laboratory records were available for all parameters
except total toxic organics (TTO). Please send documentation of TTO analysis to the Raleigh regional office by
November 18, 2005.
During the last monitoring event, pH was measured using strips. DWQ regulations require pH to be measured by
meters which, in turn, necessitates the plant to obtain field certification. I have enclosed a field laboratory
certification application and information sheet. More information can be obtained by contacting the lab
certification branch at [phone] or by visiting their website at http://h2o.enr.state.nc.us/lab/cert.htm.
A visual review was made of the site and the stormwater outfalls. Wooden pallets and cardboard were stored
outside at the time of the inspection. No outside chemical storage was seen. Spill kits were located throughout
the site. Overall the outfalls were in good condition. Only two areas appeared to need attention. Outfall 3b
required additional riprap to control erosion and the drainage pipe behind the training house was damaged. Mr.
Comer stated that these areas would be attended to as soon as possible.
Noe Carolina
Naturally
North Carolina Division of Water Quality Raleigh Regional Office Surface Water Protection Phone [phone] Customer Service
Intemet: h2o.enr.state.nc.us 1628 Mail Service Center Raleigh, NC 27699-1628 FAX [phone]
An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Post Consumer Paper

GKN Automotive Plant
NCG030429
Enclosed is the inspection checklist for your review. If you have any questions or comments, please contact me
either by phone at [phone] or by email at i [e-mail].
Sincerely,
7
i(� cw�-'
ennie R. Atkins, Ph.D.
Environmental Chemist
Cc: EPA
Person County Health Department
Central Files

United States Environmental Protection Agency
Form Approved\
EPA Washington, D.C. 20460
OMB No. 2040-0057
Water Compliance Inspection Report
Approval expires 8-31-98
Section A:. National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1 1 Lj1 2 1 51 31 NCGo30429 111 121 05/10/25 117 181 ;;I 191SI 201
Remarks
211111111111111111111111111111111111111111 11111116
Inspection Work Days Facility Self -Monitoring Evaluation Rating 61 QA --------------------------- Reserved ----------------------
67I 169 701 1 711 1 721 NJ 73I I 174 751 I I I I I I 180
I_u
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
3KD; Ata�;r::�..�ve _ncoro�r-ated
Exit Time/Date
Permit Expiration Date
6,1, Q ;;,,;_chap,; hci
^imY r_>rt r; cF.,. NC 27582
.,)5:03 PIM 05/30/::5
Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s)
Other Facility Data
Name, Address of Responsible Official/Title/Phone and Fax Number
Contacted
. , .
,.�n -�_e:•:<.:,..,��too iiui.�,a�r- _
; .;r..�r.:t.>>;r.: tic ,.�:�t�.� �._y...5r.,3...,000
No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit Operations & Maintenance E Records/Reports Self -Monitoring Program
Storm Water
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
Jennie .-_kris RRO WQ///
Signature of Manage t Q A Re er Agency/Office/Phone and Fax Numbers . Date
EPA Form 3560-3 (Rev 9( ) Previeditions are obsolete.

NPDES yr/mo/day Inspection Type
3 11 12 17 18
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)

Permit: NCG030429
Inspection Date: 10/25/2005
Owner - Facility: GKN Automotive Incorporated
Inspection Type: Stormwater
Permit
Yes
No
NA
NE
(If the present permit expires in 6 months or less). Has the permittee submitted a new application?
1=l
[I
■
is the facility as described in the permit?
■
n
n
n
Are there any special conditions for the permit?
n
■
n
n
Is access to the plant site restricted to the general public?
■
n
n
n
Is the inspector granted access to all areas for inspection?
■
n
n
n
Comment:
Operations & Maintenance
Yes
No
NA
NE
Is the plant generally clean with acceptable housekeeping?
■
I I
0
[I
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge
n
n
■
n
Judge, and other that are applicable?
Comment:
Record Keeping
Yes
No
NA
NE
Are records kept and maintained as required by the permit?
■
n
n
n
Is all required information readily available, complete and current?
■
n
n
n
Are all records maintained for 3 years (lab. reg. required 5 years)?
■
n
n
n
Are analytical results consistent with data reported on DMRs?
■
n
n .
n
Is the chain -of -custody complete?
■
n
n
n
Dates, times and location of sampling
Name of individual performing the sampling
Results of analysis and calibration
[1
Dates of analysis
Name of person performing analyses
Transported COCs
rl
Are DMRs complete: do they include all permit parameters?
■
n
n
n
Has the facility submitted its annual compliance report to users and DWO?
n
n
®
n
(If the facility is = or> 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift?
n
n
■
n
Is the ORC visitation log available and current?
[I
Q
■
[I
Is the ORC certified at grade equal to or higher than the facility classification?
n
n
■
n
Is the backup operator certified at one grade less or greater than the facility classification?
n
n
■
n
Is a copy of the current NPDES permit available on site?
■
[I
Facility has copy of previous year's Annual Report on file for review?
n
n
■
n
Comment: Facility met analytical cut-off concentrations during the first year of the permit. Analytical monitoring not
required until the last year.

STATE OF NORTH CAROLINA Application for Field Parameter
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES Environmental Laboratory Certification
DIVISION OF WATER QUALITY
LABORATORY CERTIFICATION Form #200- field application October 2001
INSTRUCTIONS: This application is only one part of the certification process; completing and submitting an application does not
constitute certification. Please complete all applicable parts of this form using a typewriter, computer, or print legibly in ink.
To apply for Field Parameter Laboratory Certification, return the original and one copy of this application to:
Mr. James W. Meyer
ENR/DWQ Laboratory Section
1623 Mail Service Center
Raleigh, NC 27699-1623
For additional information, contact the Laboratory Certification program office:
Telephone: [phone] X 207
Fax: [phone]
E-Mail: [e-mail]
Program Homepage: http://h2o.enr.s-tate.nc.us/lab/cert.htm or www.dwglab.or_q
Municipal, Industrial and Other Facilities should fill out only Sections A, C and provide a signature in Section D.
Commercial Facilities must supply all applicable information in Section A, additional identification of all regulated
facilities in Section B, and signatures required in Section D.
Section A: Facility and Contact Information
Facility Name or Commercial Management Company Name
Contact Person Telephone #, ext.
EPA Laboratory Code FAX #
Laboratory Supervisor
Laboratory Supervisor/Operator's Certificate Number Grade/Type of Certificate(s)
If not a Certified Operator, please provide Education level and/or Laboratory experience
Laboratory Supervisor E-Mail Address: Telephone #, ext.
Facility Address
Mailing Address
City State Zip
For a municipal/industrial facility certification only, please list NPDES permit number (s) and county location below.
Additional sheets may be attached if necessary. Commercial applicants please fill out Section B.
NPDES #
- COUNTY
NPDES #
COUNTY
NPDES #
COUNTY

Section B Commercial Client Contact Information
(Municipal/Industrial applicants - proceed to Section C)
Please list below information regarding current clients serviced by your company's management program:
Facility Name NPDES # Type/Grade of Plant
Facility
Street Address
City/State
Zip
Facility
Name
NPDES #
Type/Grade
of Plant
Facility
Street Address
City/State
Zip
Facility
Name
NPDES #
Type/Grade
of Plant
Facility
Street Address
City/State
Zip
Facility
Name
NPDES #
Type/Grade
of Plant
Facility
Street Address
City/State
Zip
Facility
Name
NPDES #
Type/Grade
of Plant
Facility
Street Address
City/State
Zip
Facility
Name
NPDES #
Type/Grade
of Plant
Facility
Street Address
City/State
Zip
Facility
-------------------
Name
NPDES #
Type/Grade
of Plant
Facility
Street Address
City/State
Zip
Facility
Name
NPDES #
Type/Grade
of Plant
Facility
Street Address
City/State
Zip
Facility
Name
NPDES #
Type/Grade
of Plant
Facility
Street Address
City/State
Zip
THIS SECTION MAYBE COPIED AS NECESSARY. PLEASE NUMBER THIS AND ADDITIONAL PHOTOCOPIED PAGES
PAGE ------- OF-------

Section C Laboratory Information
(1) Types of Samples Processed (Check all that apply)
❑ Wastewater Effluent (Domestic) ❑ Storm Water
❑ Wastewater Effluent (Industrial) ❑ Reclaimed Water
❑ Groundwater ❑ Pretreatment
❑ Surface Water ❑ Other (please specify)
❑ Public Water Supply
(2) Circle, or write in, the method used for each requested analytical parameter, and indicate the laboratory's lower reporting
limit with units of measure.
Analytical Parameter
EPA
Methods
Standard Methods
18th, 19th, 20th Edition
Other
Methods
Lower Reporting
Limit
Concentration
include units
OFFICE
USE
ONLY
Specific Conductance
120.1
2510 B
Dissolved Oxygen
360.2
4500-0 C
360.1
4500-0 G
pH
150.1
4500H+ B
Residue, Settleable .
160.5
2540 F
Chlorine, Total Residual
330.1
4500CI B
330.2
4500CI C
330.3
4500CI D
330.4
4500CI F
330.5
4500CI G
HACH 8167
10014 ULR
Temperature
170.1
2550 B
(3) Equipment: Please list equipment available to perform the selected analyses:
Analytical Parameter Equipment office use
(4) Quality Control Program - the following must be available upon request.
(a) Data pertinent to each analysis must be maintained for five years. Certified data must consist of date collected,
time collected, sample site, sample collector, and sample analysis time. The field benchsheets must provide a
space for the signature or initials of the analyst, and proper units of measure for all analyses.
(b) A record of instrument calibration where applicable, must be filed in an orderly manner so as to be readily
available for inspection upon request.
(c) A copy of each approved analytical procedure must be available to each analyst.
(d) Each facility must have glassware, chemicals, supplies, equipment, and a source of distilled or deionized water
that will meet the minimum criteria of the approved methodologies.
(e) Evidence of participation in an annual quality assurance study.

Section D Authorized Signature
This statement certifies that the information in this application is truthful and accurate, and that the applicant is aware of
all regulations regarding the Quality Assurance requirements of Laboratory Certification.
Signature of Laboratory Supervisor: Date:
Office Use Only:
Date Application Received:
Invoice #
Check #
Application Process Completed:
NC Lab. Certification Number
Date Certification Issued
Revised 2/4/05

Instruction Guidance for Completing a Field Parameter Certification Application
1) Supervisory Requirements:
The supervisor of a field parameter certified laboratory must meet at least one of the following requirements: 1) an Operator's
Certification equivalent to the type or grade of the regulated facility (ies). These Operators Certificates are issued by the Water
Pollution Control Systems Operators Certification Commission. 2) a minimum of a B.S. or A.B. degree in chemistry or closely related
science curriculum from an accredited college or university plus a minimum of six months laboratory experience in analytical
chemistry; 3) a two year associate degree from an accredited college, university, or technical institute in chemistry technology,
environmental sciences, or closely related science curriculum plus a minimum of two years experience in analytical chemistry; or 4)
non -degree supervisors may have at least six years laboratory experience in analytical chemistry.
2) Fees:
Do not submit annual fees until you are issued an invoice. Application fees do not apply to Field Parameter Certification.
An applicant for Field Parameter certification is not charged by the Department of Environment and Natural Resources, Laboratory
Section for the evaluation and processing of the application. Invoices for annual Certification fees will be mailed after the evaluation
has been completed. Your facility may continue to analyze samples until the State Laboratory has issued or denied certification.
Annual Certification Fees will be calculated in accordance with 15A NCAC 2H .0800. An annual minimum fee of $100.00 will be
assessed to all Municipal,/ Industrial Field Parameter certified labs and a fee of $200.00 will be assessed to all Commercial Field
Parameter certified laboratories.
3) Methods:
In accordance with DWQ policy, a facility is expected to use approved methods for the collection, preservation and analysis of
samples following program requirements. All test procedures must produce detection and reporting levels below the permit
discharge requirements and all data generated must be reported to the approved detection level or lower reporting level of the
procedure. Indicate the lowest quality control check standard value in the box labeled "lower reporting limit concentration". For
example, if you currently analyze standards of 100 µg/L, 125 µg/L and 150 µg/L for Total Residual Chlorine, you would enter the 100
µg/L value as your current lower reporting limit.
4) EPA Lab Code:
To obtain an EPA Lab Code, contact Mr. Charles Feldmann at 513 - 569 - 7671, or e-mail her at Feld [e-mail] . If
your laboratory has been issued a US EPA lab code in the past, it can be located on any report issued by the EPA. It is the 7 digit
alphanumeric code beginning with the postal code for the state (NC), followed by 5 numbers. (Example: NC11111)
5) Proficiency Testing:
Once certified, this office must receive acceptable proficiency test sample results from an accredited provider. The following
parameters require annual proficiency testing of blind or "unknown" value: pH, Total Residual Chlorine, Settleable
Residue, and Conductivity. Applicants for 2002 Field Parameter Laboratory Certification must supply acceptable results no
later than December 31, 2002. We encourage all applicants to complete this requirement as soon as possible to prevent
decertification of their facility or company. Ampuls must be obtained from any of the following accredited providers:
Absolute Standards, Inc.,
Hamden, CT
Stephen Arpie,M.S.
203 - 281 -2917
AccuStandard, Inc.
New Haven, CT [
William McClain
203 - 786 -5290 X 102
Analytical Products Group, Inc.,
Belpre, OH
Thomas Coyner
740 - 423 -4200
Chrisope Technologies
Lake Charles, LA
Theresa Stokeld
800 - 256 -4376 X 203
Environmental Resource Associates (ERA)
Arvada, CO
Curtis Wood
303 - 431 -8454
Microcheck, Inc.
Northfield, VT
Michael Sinclair
802 - 485 -6600 X 22
NSI Environmental, Solutions; Inc.
RTP, NC
Mark Hammersla
919 - 957 -9672
NYS DOH Environmental Laboratory
Approval Program,
Albany, NY
Kenneth Jackson
518 - 485 -5570
Protocol Analytical Supplies, Inc.
Middlesex, NJ
William Hahn
732 - 627 -0500
Resource Technology Corporation (RTC)
Laramie, WY
Robert Rucinski
307 - 742 -5452
Spex Certiprep Inc.
Metuchen, NJ
Vanaja Sivakumar
732 - 549 -7144 X 418
Ultra Scientific; Inc.
North Kingstown, RI
Edward Martz
401 - 294 -9400
Analytical Standards, Inc. (AS[
Parkersburg, WV
Fred Anderson
800-283-4844
The list of NIST Accredited Providers is accurate as of publication of this notice. Additions to the list can be obtained from the
NIST web site: hftp://ts.nist.gov/ts/htdocs/210/214/scopes/calchem.htm
March 2003

t0� WATF
�O 61
bA W-U —i
EMMA DELGADO
GKN AUTOMOTIVE INCORPORATED
6400 DURHAM ROAD
TIMBERLAKE, NC 27583
Dear Permittee:
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
August 23, 2002
Subject: NPDES Stormwater Permit Renewal
GKN AUTOMOTIVE INCORPORATED
COC Number NCG030429
Person County
In response to your renewal application for continued coverage under general permit NCG030000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued
pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983.
The following information is included with your permit package:
* A new Certificate of Coverage
* A copy of General Stormwater Permit NCG030000
* A copy of the Analytical Monitoring Form (DMR)
* A copy of a Technical Bulletin for the general permit
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or
decree.
If you have any questions regarding this permit package please contact Bill Mills of the Central Office Stormwater
and General Permits Unit at [phone], ext. 548
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Stormwater & General Permits Unit Files
Raleigh Regional Office
e��
NCDENR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

r�p�-.W AT�R p
�O
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
BETH PALMA
GKN AUTOMOTIVE INCORPORATED
6400 DURHAM ROAD
TIMBERLAKE, NC 27583
Dear Permittee:
Gregory J. Thorpe, Ph.D.
Acting Director
Division of Water Quality
December 27, 2001
Subject: NPDES Stormwater Permit Renewal
GKN AUTOMOTIVE INCORPORATED
COC Number NCG030429
Person County
Your facility is currently covered for stormwater discharge under General Permit NCG030000. This permit expires
on August 31, 2002. The Division staff is currently in the process of rewriting this permit and is scheduled to have
the permit reissued by late summer of 2002. Once the permit is reissued, your facility would be eligible for
continued coverage under the reissued permit.
In order to assure your continued coverage under the general permit, you must apply to the Division of Water
Quality (DWQ) for renewal of your permit coverage. To make this renewal process easier, we are informing you in
advance that your permit will be expiring. Enclosed you will find a General Permit Coverage Renewal
Application Form. The application must be completed and returned by March 4, 2002 in order to assure continued
coverage under the general permit.
Failure to request renewal within this time period may result in a civil assessment of at least $250.00. Larger
penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility
without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and
could result in assessments of civil penalties of up to $10,000 per day.
Please note that recent federal legislation has extended the "no exposure exclusion" to all operators of industrial
facilities in any of the I I categories of "storm water discharges associated with industrial activity," (except
construction activities). If you feel your facility can certify a condition of "no exposure", i.e. the facilty industrial
materials and operations are not exposed to stormwater, you can apply for the no exposure exclusion. For additional
information contact the Central Office Stormwater Staff member listed below or check the Stormwater & General
Permits Unit Web Site at http://h2o.enr.state.nc.us/su/stormwater.htmI
If the subject stormwater discharge to waters of the state has been terminated, please complete the enclosed
Rescission Request Form. Mailing instructions are listed on the bottom of the form. You will be notified when the
rescission process has been completed.
If you have any questions regarding the permit renewal procedures please contact Joe Albiston of the Raleigh
Regional Office at 919-571-4700 or Bill Mills of the Central Office Stormwater Unit at [phone], ext. 548
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Raleigh Regional Office
®��
NCDENR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
- 1- 800-623-7748

GKN Automotive, Inc.
June 7, 2001
NC Department of Environment and Natural
Division of Water Quality
Budget Office
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: GKN Automotive, Inc. - Roxboro Facility
Timberlake, NC, Person County
Permit No. NCG030429
Dear Sirs:
Roxboro Facility
6400 Durham Road
Timberlake -,NC 27583, USA
Telephone: �(.336) 364-6200
Telefax`a(336)\364-6309
Enclosed please find Check No. 5621 in the amount of $80.00 to cover the required annual
administering and compliance monitoring fee for Permit No. NCG030429 for the GKN
Automotive, Inc. - Roxboro Facility. This check is submitted in accordance with Title 15 North
Carolina Administrative Code 21-1.0105 under the authority of NCGS 143-215.3(a)(1), (la) and
(lb). Please note that submission of this fee is late as the most recent request for payment letter
(dated May 30, 2001) was received at our facility on June 2, 2001. Previous correspondence from
your office was not processed as the facility was without an Environmental, Health and Safety
representative until recently. Please change contact information for our site from Mr. Chris
Herrmann to myself, Beth W. Palma. If you have any questions, please do not hesitate to call me
at 336-364-6324.
Sincerely,
Beth W. Palma
Environmental, Health and Safety Engineer
Enclosure
cc: Mr. Ken S61n fer;-Water-QualitySupervisor;-RRO-(w/o enclosufc)

5621
~ GKN AUTOMOTIVE INC.
PH 919-563-7000
P. O. BOX 220 6649/531
MEBANE, NC 27302
DAT S 2 QQl
PAY
TO THE n /��
ORDER OF NC W�p ISM, 21YI !' 601 +-trrw '4 / y0.(,�OJ QSO$ Op
O.QQ
a�
1 I Oo DOLLARS
p D-.11 o°cx_
ACHOVIA
Wachovin Bank, N.A.
Wi ton-Salcm, NC 27102
li
FOR No. NCG030 429 - -G- - - - 4 _ NP
-
118000056

Z.
I

State of North Carolina
Depadment, of Environment
and Natural Resources
Division.of Water Quality
Michael F. Easley, Governor
William G. Ross Jr., Secretary
Kerr T. Stevens, Director
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
CHRIS HERRMANN
GKN AUTOMOTIVE, INC.
6400 DURHAM ROAD
TIMBERLAKE NC 27583
1 � •
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
5/30/2001
SUBJECT: NOTICE OF VIOLATION AND REVOCATION FOR NON PAYMENT',
PERMIT NUMBER NCG030429. _
'•GKN AUTOMOTIVE, INC.. v
PERSONi COUNTY
Dear Permittee:
Payment of the required annual administering and compliance monitoring fee of $80.00 for this year has not
been received for the subject permit. This fee is required by Title 15 North Carolina Administrative Code 2H.0105, under
the authority of North Carolina General Statutes 143-215.3(a)(1),,(1 a) and (1 b). Because this fee was not fully paid -within
30 days after being billed, this letter initiates action to revoke the subject permit, pursuant to 15 ncac 2H.0105(b) (2) (k)
(4), and G.S. 143-215.1 (b) (3).
Effective 60 days from receipt of this notice, subject permit is hereby revoked unless the required Annual
Administering and Compliance Monitoring Fee is received within that time. Discharges without a permit are subject to the
enforcement authority of the Division of Water Quality. Your payment should be sent to:
N.C. Department of Environment and Natural Resources
Division of Water Quality
Budget Office
1617 Mail Service Center
Raleigh, NC 27699-1617
If you are dissatisfied with this decision, you have the right to request an administrative hearing within Thirty (30)
days following recipt of this notice, identifying the specific issues to be contended. This request must be in the form of a
written petition conforming to Chapter 1508 of the North Carolina General Statutes, and filed with the Office of Administrative
Hearings, Post Office Drawer 27447, Raleigh, North Carolina, 27611-7447. Unless such request for hearing is made or
payments received, revocation shall be final and binding. If you have any questions, please contact:
Mr. Ken Schuster, Raleigh Water Quality Regional Supervisor, [phone].
Sincerely,
Kerr T. Stevens
cc: Supevisor, Water Quality Permits and Engineering Unit
Raleigh Regional Office
County Health Department
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer. 50% recycled / 10% post -consumer paper

State of North Carolina
Department of Environment
and Natural Resources
Division'of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
Kerr T: Stevens, Director
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
1�•
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
5/21 /99
CHRIS HERRMANN
GKN AUTOMOTIVE, INC.
6400 DURHAM ROAD
TIMBERLAKE NC 27583
SUBJECT: NOTICE OF VIOLATION AND REVOCATION FOR NON PAYMENT
PERMIT NUMBER NCG030429
GKN AUTOMOTIVE, INC.
PERSON COUNTY
Dear Permittee:
Payment of the required annual administering and compliance monitoring fee of $80.00 for this year has not
been received for the subject permit. This fee is required by Title 15 North Carolina Administrative Code 2H.0105, under
the authority of North Carolina General Statutes 143-215.3(a)(1), (1a) and (1b). Because this fee was not fully paid within
30 days after being billed, this letter initiates action to revoke the subject permit, pursuant to 15 ncac 2H.0105(b) (2) (k)
(4), and G.S. 143-215.1 (b) (3).
Effective 60 days from receipt of this notice, subject permit is hereby revoked unless the required Annual
Administering and Compliance Monitoring Fee is received within that time. Discharges without a permit are subject to the
enforcement authority of the Division of Water Quality. Your payment should be sent to:
N.C. Department of Environment and Natural Resources
Division of Water Quality
Budget Office
P.O. Box 29535
Raleigh, NC 27626-0535
If you are dissatisfied with this decision, you have the right to request an administrative hearing within Thirty (30)
days following recipt of this notice, identifying the specific issues to be contended. This request must be in the form of a
written petition conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative
Hearings, Post Office Drawer 27447, Raleigh, North Carolina, 27611-7447. Unless such request for hearing is made or
payments received, revocation shall be final and binding. If you have any questions, please contact:
Mr._Ken-Schuster,-Raleigh_Water Quality Regional -Supervisor, [phone].
cc: Supevisor, Water Quality Permits and Engineering Unit
Raleigh Regional Office
County Health Department
Sincerely,
Z ` .'
Kerr T. Stevens
MAYAL
P.O. Box 29535, Raleigh, North Carolina 27626-0535
An Equal Opportunity Affirmative Action Employer
Telephone [phone] FAX [phone]
50% recycled / 10% post -consumer paper

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
Mr. Chris Herrmann
GKN Automotive, Inc.
6400 Durham Road
Timberake, North Carolina 27583
Dear Mr. Chris Herrmann:
�EHNF=1
January 23, 1998 JNN 21 G99
Subject: General Permit No. NCG030000
GKN Automotive, Inc.
COC NCG030429
Person County
In accordance with your application for discharge permit received on November 25, 1997, we are
forwarding herewith the subject certificate of coverage to discharge under the subject state - NPDES general
permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .l and the
Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated
December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the Division
of Water Quality. The Division of Water Quality may require modification or revocation and reissuance of the
certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management
Act or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Tony Evans at telephone number 919/733-5083
ext. 584.
Sincerely,
ORIGINAL SIGNED BY
BRADLEY BENNETT
A. Preston Howard, Jr., P. E.
cc: Raleig1TEegional'O__ffice
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030429
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
GKN Automotive, Inc.
is hereby authorized to discharge stormwater from a facility located at
GKN Automotive, Inc.
6400 Durham Road
Timberlake, NC
Person County
to receiving waters designated as an unnamed tributary to North Flat River, Class WS III NSW in the Neuse River
Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III
and IV of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective January 23, 1998.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day January 23, 1998.
ORIGINAL SIGNED BY
BRADLEY BENNETT
A. Preston Howard, Jr., P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

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