NCG030303_MONITORING INFO_20160205

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/v Cc,
DOC TYPE
El HISTORICAL FILE
MONITORING REPORTS
DOC DATE
El d o 1 c9 Da 05
YYYYMMDD

�rs".e Em-
SE'ED
A0
VCDFMR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
F F B 5 2016
For guidance on filling out thisform, please visit: htW://nortal.ncd r.org/web/wa/wsjsuLnndessw#tab-4
Permit No.: jV/��/�/_/_/ or Certificate of Coverage No.: j[/c
Facility Name:
County
Inspector:
Date of Inspection:
Time of inspection:
Total Event Precipitation (inches): e Q C
Phone No. --
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
wyes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" [requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A'°measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office,
6y this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of6mittA or Designee)
Paget of 2
SWU-242, bast modified 10/25/2012

1. Outfall Description: r
Outfall No. SM tl Structure (pipe, ditch, etc. ]
,. Receiving Stream: U-A T
Describe the industrial activities that occur within the outfalI drainage area:
ter-. P !!j , -"� V-r�
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: _ 1 z S'
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 1-� t-i-L
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and S is very cloudy:
2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
2 3 4 5
7. is there any foam in the stormwater discharge? Yes No
8, is there an oil sheen in the stormwater discharge? Yes
9. is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
maybe indicative of pollutant exposure. These conditions warrant further Investigation.
Page 2 of 2
swu-242, LaA modified 10/25/2012

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE No. NCG03 b 3 O
FACILITY NAME S ;))Y
COUNTY
PERSON COLLECTING SAMPLES (L-4aJ 52LL17 --]_
LABORATORY �r Lzn— iab Cert. # 46
Comments on sample collection or analysis:
Part A: Starmwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR acl:c;'
SAMPLE PERIOD ❑ Jan -June July -Dec
or ❑ Monthly"_ (month)
DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA
Zero -flaw [:]watersupply [:]SA
Other c_2*LErr'
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
�. �,{- ❑ No discharge this period?2 P�f�
:..•• ; ::::_........E3ate
.. :: O�1tfallNo
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oT
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1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date:11/1/2012-10/31/2017 .SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and bellef, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print na e)
Title (Print title)
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mgZL", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note. if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General hermit tent.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?Z
Footnotes from Part A also apply to this Part B
" See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 1i/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: if you report a sample value in excess of the benchmark, you must Implement Tier I, Tier Z, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORINQRESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mall an on inal and one copy ot this DAM including all "No Wschar e" reports within 30 days ot receipt of the lab results tar at end of monitoring erlod
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervislon in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
{Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

STORMWATER DISCHARGE OUTFALL (SDO)
ANNUAL SUMMARY DATA MONITORING REPORT (DMR)
Calendar Year 20 (S
Individual NPDES Permit No. NCSJ
Certificate of Coverage (COC) No. NCG
or
This monitoring report summary of the calendar year is due to the DWQ Regional Office no later than March a of the following year.
Facility Name: _ SQ
County:,,
Phone Number: () Total no. of SDOs monitored
Outfall No. j
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No Ij
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No V
If this outfall was in Ter 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No EF
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SWU-264-Generic-25May2010

Additional Ouffall Attachment
Ouffall No.
Is this outfall currently In Tier 2 (monitored monthly)? Yes ❑ No E]
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes 0 NoE:1
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency 7
Received approval from DWQ to reduce monitoring frequency F-1
Other 7
Was this SOO monitored because of vehicle maintenance activities? Yes ❑ No [:3
Ra
FO
C7�
Sellchmiirk
--NIA
`Date-Sa`rriple-
Collect In
I All 11M
SWU-264-Generic-25May20 1 0

I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Signature
Date _1-06 1,4
Mail Annual DMR Summary Reports to:
DWQ Regional Office Contact Information:
2090 US Highway 70 E 225 Green Street
Swannand Systel Building Suite 714
(828) : Fayetteville, NC 28301-5043
(9I0) 433-3300
3800 Ba 943 Washington Square Mall
Raleigh,; Washington, NC 27889
(gig)-, [phone]
595 Waugl 1617 Mail Service Center
Winston -Sale Raleigh, NC 27699-1617
(336) 7 ___ _ , ^(919 807-6300
610 East Center Avenue/Suite 301
Mooresville, NC 28115
[phone]
127 Cardinal Drive Extension
Wilmington, NC 28405-2845
[phone]
S W U-264-Generic-25May2010

aceAnaJyW"
e'ew.y�p0elellScarn
November 05, 2015
Mr. Johnny Baines
Eastern Environmental Management
PO Box 4030
518 S. Pearl Street
Rocky Mount, NC 27803
RE: Project: SPX 10/2015
Pace Project No.: 92273916
Dear Mr. Baines:
Pee@ Analytical Services, Inc.
9800 KinceyAve. Suite 108
HuntervAle, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 29, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have arty questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
taylor. ezell@pa celabs.com
Project Manager
Enclosures
cc: his. Cathy Baines, Eastem Environmental Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,
Page 1 of 13

aceAnalytiral`
rnOw.paodapacwm
Pace Analytical Services, Inc.
9800 Kinney Ave. 5ulte 100
Huntarsvltle, NC 26078
[phone]
CERTIFICATIONS
Project; SPX 1012015
Pace Project No.: 92273016
Charlotte Certification IDS
98W Kinwy Ave. Ste TO, Huntersvllie, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water CertiSicadon #. 37706
Kentucky UST Certification #: 84
North Carolina Field Sorvioes Certification #: 5342
West Virginia Certiflcation P 357
North Carolina Wastewater Certification #: 12
V1rgln1aNELAP CerSftcstion #: 460221
South Carolina Certification #. 99006W1
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certlftcation #: 40
FlorddalNELAP CerlNlc ition #: E87648 South Carollna Certification #: 99030001
Massachusetts Certification A M-NCO30 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 Vfrginie/VELAP Certificatron M 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be rerxoduced, except in full,
wlthcut the written consent or Pace Analytical Services. Inc.. Page 2 of 13

aceAnalytrtl"
-*?wm
SAMPLE ANALYTE COUNT
Paco AnaVlcal Servilm, Inc,
9800 KlnceyAve. Suite 100
HunterevlU9, NC 28076
[phone]
Project: SPX 1012015
Pace Project No.: 92273916
Analytts
Lab 10 Sample ID Method Analysts Reported Laboratory
92273916001 600-1
EPA 16648
JMS
1
PASI-C
EPA8082
SWB
8
PASI-C
SM 2540D
SAM
1
PASI-A
EPA 351.2
SER
1
PASI-A
EPA 353.2
DMN
3
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 13

aceAnaly ical
r eraw.paad�,cpro
I
ANALYTICAL RESULTS
Project: SPX 1012015
Pace Project No.: 92273916
Pace Analytical Services, Inc.
2800 hIncey Ave. Suite 100
Huntaisvills, NC 28078
(7D4)876-DN2
Sample: SIJO-1
Lab ID: 02273010001 Collected: 10/28/15 15:30
Received: 10/29/15 00:45 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, 0II and Grease
Analytical Method: EPA 16648
Oil and Grease
ND mg/L
5.0
1
1110511510:39
$082 GCS PCB
Analytical Method: EPA 8082 Preparation Method: EPA 3610
PCH-1016 (Aroclor 1016)
ND ug/L
0.50
1
10/30/15 09:30
10/30/15 19:06 12674-11-2
PCB-1221 (Arocior 1221)
ND ug/L
0.50
1
10130/1509:30
1M0115 19:06 11104-28-2
PCB-1232 (Aroctor 1232)
ND u911-
0.50
1
10/30/15 09:30
10130/15 19:00 11141-1"
PCB-1242 (Arodor 1242)
ND ug/L
0.60
1
10130/15 09:30
10/30/15 19:06 53469-21-0
PCB-1248 (Aroclor 1248)
ND ug/L
0.50
1
10/30/15 09:30
10/30/15 10:06 12672-29-8
' PCB-1254 (Arodor 1254)
ND ug/L
0.50
1
10/30/15 09:30
10/30/15 19:06 11097�9-1
PC13-1260 (Aroclor 1280)
ND ug/L
0.50
1
10V30/15 09:30
10/30/15 10:06 11098-82-5
Surrogates
Decachioroblphenyt (S)
35 %
10-132
1
10/30/15 09:30
10/30/15 19:06 2051 24-3
25400 Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L
5.0
1
11/01/15 16:12
351-2 Total KjeldahI Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
ND mglL
0.50
1
11/03/15 03:10 7727-37-9
3632 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
0.15 M91L
0.020
1
10/30/15 10:39
Nitrogen, Nitrite
ND mg/L
0.020
1
10/3011610:39
Nitrogen, NO2 plus NO3
0.15 mg/L
0.020
1
1MOM 510:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 11/05/2015 05:32 PM without ft written consent of Pace Analytical Services, Inc..
Page 4of13

aceAnalytical'
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QUALITY CONTROL DATA
Project: SPX 10Q015
Pace Project No.: 92273916
QC Batch: GCSVI23118 Analysts Method: EPA 1864E
QC Batch Method: EPA 1664D Analysts Description: 1664 HEM, Oil and Grease
Associated Lab Samples: =73916001
METHOD BLANK: 1599395 Mattlic Water
Associated Lab Samples: 92273916001
Blank Reporting
Parameter Units Result unlit Analyzed Qualifiers
Oil and Grease mg1L ND 5.0 11105115 10:35
Pace Analytfoal Services, Inc.
9600 KlnceyAm Suits 100
Huntersvilla, NC 28078
(7D4)67$-8082
LABORATORY CONTROL SAMPLE & LCSD: 1599396 1699307
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Cona Result Result % Rec % Rec Umlts RPD RPD Qualiters
OR and Grease mg/L 40 35.4 35.3 88 88 78-114 0 30
Results PnaerAed on less Pape are In the units Indicated 6y the'Units' column mcrapt Where an altefnate unit In presented to the right of the reeuh.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 11105l2015 05:32 PM wfthout the written consent of Pace AnaVual Services, Inc..
Page 5 of 13

aceArtalAeal
ax'w�ecetabf.�pm
QUALITY CONTROL DATA
Project SPX 1WO%
Pace Project No.: 92273916
QC Batch: OEXT138710 Analysis Method: EPA 8082
QC Hatch Method: EPA 3510 Analysis Description: 8062 GCS PCB
Associated Lab Samples: 92273916001
METHOD BLANK:. 1594382 Matrix Water
Associated Lab Samples: 92273916001
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
PCB-1016 (Arodor 1016)
ug/L
ND
0.50
10129/15 22:07
PCB-1221 (Aroclor 1221)
ug/L
ND
0.60
IM9115 22:07
PC13-1232 (Aroclor 1232)
uglL
ND
0.50
10129/15 22:07
PCB-1242 (Aroclor 1242)
ug/L
ND
0.60
10/29/15 22:07
PCB-1248 (Arodor 1248)
ug1L
NO
0.50
10/29/15 22:07
PCB-1254 (Aroclor 1254)
uglL
ND
0.50
10/29/15 22:07
PCB-1260 (Aroclor 1260)
u91L
ND
0.50
10/29/15 22:07
Decachlorobiphenyl (S)
%
83
10-132
10/29/16 22:07
Paco Analytical Services, Inc.
9800 MnceyAve. Suite 100
Huntorsvlllo, NC 28078
(7C4)875-9092
LABORATORY CONTROL SAMPLE & LCSD:
1594383
1594384
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units Cone.
Result Result
% Rae
% Rec
Llmits RPD RPD Qualifiers
PCB-1016 (Arodor 1016)
uglL 5
4.2 4.3
83
85
50-1 W 2 30
PCB-1260 (Arodor 1260)
ug1L 5
4.4 4.4
87
87
50-150 0 30
Decachlorobiphenyl (S)
%
82
83
10-132
Results presertad on thia page us in the units IrWicated by the ^Unlls' column except when en sttemate unit Is presented to the right of the resut4
REPORT OF LABORATORY ANALYSIS
Thla report shag not be reproduced, except In full,
Date: 119W2015 05:32 PM without the written consent of Pace Anotyumi Services, Inc..
Page 6 of 13

IeAnaOcal
m�a:pecelthtma
QUALITY CONTROL DATA
Project SPX 1(Y2015
Pace Project No.: 92273910
QC Batdt WET141157 Analysis Method: SM 25400
QC Be" Method: SM 2540D Anstyals Description: 2540D Total Suspended Solids
Associated Lab Samples: 92273916W1
METHOD BLANK: 1596407 Matrix: Water
Assodated Lab Samples: 92273916001
Blank Reporting
Parameter Units Result Umlt Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 11/01/15 15:06
Pace Analytical Ssrvicee, Inc.
9800 KlnceyAva. Butts 100
Huntefaviila, NC 28078
(704}8764092
LABORATORY CONTROL SAMPLE: 1596408
Spike LCS LCS 96 Roc
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids RKVL 250 240 96 90-110
SAMPLE DUPLICATE 1596409
92274207001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 173 179 3
SAMPLE DUPLICATE: 1596410
92273916001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mgA- ND ND
Results preserded on this paps are in the units Indicated by the "Unite' column a captwhme an alternate unit Is presented to the right at the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be repmnduced, except In Tull,
Date: 11105/2015 05:32 PM wipwut the wrliten consent or Paca Analytical SaMcm, Inc..
Page 7 of 13

I
OA17alytical
wwnpecatabs.Cam
QUALITY CONTROL DATA
Project SPX 1012015
Pace Project No.: 92273916
Pace Analytical Services, Inc.
98WKlnceyAve. SLd91D0
Huntersvlpe, NC 28076
(7041875.9092
QC Batch: WETA125207
Analysis Method: EPA 351,2
QC Batch Method. EPA 3512
Analysts Description: 351.2 TKN
Associated Lab Samples: 92273016001
METHOD BLANK, 1596242
Mairbl: Water
Associated Lab Samples: M73916001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed
Qualifiers
Nitrogen, Kjeldshl, Total mg1L
NO 0.50
11/03116 02:52
LABORATORY CONTROL SAMPLE: 1598243
Spike
LCS
LCS % Rec
Parameter Units
Conc,
Result _
% Rec Limits
Qualifiers
Nitrogen, Kjeldahl, Total rrtg(L
10
10
1100 90-110
MATRIX SPIKE 8r MATRIX SPIKE DUPLICATE: 1596244
1596245
MS
MSD
92274056001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc, Result
Result % Rec
% Rec
Limits
RPD Qual
Nitrogen, Kjakfahl, Total mg(L 0.94
10
10 11.3
10.8 104
99
W110
4
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1596246
1596247
MS
MSD
92273502001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qua]
Nitrogen, Kjaldahi, Total Mg1L 6.9
10
10 10.7
16.1 39
92
90-110
40 M1,R1
Results preeented on this page are rn the unlis indicated bythe"llnlW' Column except where an altemato unit is pres©ntod to the right of the ren tL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Data: 11/0512015 05:32 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 13

acaAnalylical
"Upimliftoxi
QUALITY CONTROL DATA
Project SPX 1=015
Pace Project No.: OM73916
QC Batch: WETA125196 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 92273916001
METHOD BLANK: ' 1696416
Associated Lab Samples: 92273916001
Parameter
Units
Nitrogen. Nitrate
mg1L
Nitrogen. Nltriba
mg1L
Nitrogen, NO2 plus NO3
mg1L
Matrix Water
Blank Reporting
Resi It Limit Analyzed Qualifiers
ND 0.020 1013011510:36
ND 0.020 10/30/1510:36
ND 0.020 10/30/1510:36
Pace Analytical Services, Inc.
9000 KlnceyAve. Suits 100
Huntersvllle, NC 29070
[phone]
LABORATORY CONTROL SAMPLE:
1595416
Spike
LCS LCS % Rec
Parameter
Units
Cone.
Result % Rec Limits Qualifiers
Nitrogen. Nitrate
mglL
2.5
2.4 96 90-110
Nitrogen, Nitrite
mg1L
1
0.97 97 90-110
Nitrogen, NO2 plus NO3
mglL
2.5
2.4 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1595417
1595418
MS
MSD
92273916001 Spike
Spike
M5
MSD
MS
MSD
% Rae
Parameter
Units
Result Cane.
Cone.
Result
Result
% Rec
% Rec
limits
RPD Qual
Nitrogen. Nitrate
mg1L
0.15 2.5
2.5
2.6
2.6
96
913
90-110
0
Nitrogen, Nitrite
mg1L
ND 1
1
1.1
1.1
104
104
90-110
0
Nitrogen, NO2 plus NO3
m91L
0.15 2.5
2.5
2.6
2.6
96
w
90-110
0
Reavlb presented on this page era In the unite Indicated by the'UnIW column axvW where en attemste unit [a presented to the right of the recall
REPORT Of LABORATORY ANALYSIS
This report shell not be reproduced, exoept In full,
Date: 11105WS 05:32 PM without tho written consent of Pace Analytical Services, Inc.. Page 9 of 13

aceAna1j&a1
wvw.yxsfaGs.atlm
QUALIFIERS
Project SPX 1012016
Pace Project No.: 92273916
DEFINITIONS
OF - Dilution Factor, If reported, represents the factor applied to the reported data due to dilution of the sample aliquoL
NO - Not Detected at or above adjusted reporting limit.
J - Estimated ooncentratlon above the adjusted method detection limit and below the adjusted reporting limit
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit
Paco Analytical Services, Inc.
8800 IQnceyyAve. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-DWheny1hydrazlne decomposes to and cannot be separated from Azabenzene using Method B270. The result for each analyte Is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Glean -Up
U - Indicates the compound was analyzed for, but not detected.
Add preservation may not be appropriate for 2 Chloroothytvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrlle by EPA
Method 8260.
N-Nitrosodiphenylam[ne decomposes and cannot be separated from Diphenylamine using Method 8270. The result raported for
each anatyle is a oombined concentration.
Pace Analytical is TNI accredited. Contact your Pace Pint for the current fist of accredited analytes.
TNI - The NELAC institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded OC limits. hatch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except In full,
Date: 1110512015 06:32 PM without the written consent of Paoe Analytical Servlcas, Inc.. Page 10 of 13

aCeAnalyiical e
wax'-0eaanr
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project SPX 1Moll 5
Pace Project No.: 92273916
Pace Analytical Sarvtces, Inc.
9800 Klnoey Ave. Suilo 100
Hurteravllle. NC 28078
(704)87&9092
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92273916001
8130.1
EPA 18048
GCSVI23118
92273916001
SDO-1
EPA3510
OEXT138710 EPA8082 GCSV123060
92.273916001
SDO.1
SM 2540D
WET141157
92273916001
S130-1
EPA351.2
WETA125207 '
92273916001
S1130-1
EPA353.2
WETA/25196
Date: 11105W15 05:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduood. excopt In full.
vdthout the wrtnn consent of Pace AnaMlcat Sery ms. Inc..
Page 11 of 13

. ;a'CLI AfMIXIC81 *
locument Name:
Sam le Condition Upon Recoil
Document Number.
F-CHR-CS-003-rev.96
LjvwulJMIL ncrweu. May IV, AV I
Palae 1 of 2"
Pace Huntersvllle Q
Client Name: • rage 2 of 2 Is for Internal Use Oniy
Courier: ❑ Fed UP❑ USP[j Cller❑ CommerdC Pace Other t l' tlotlaro-�
Custody Seal on Cooler/13ox Praaant: ❑ yes. no Seals intact: ❑ yes [f no r� i. +
Z ;.v:
Packing Material: ❑Bubble Wrap Bubble Ban None ❑ Oilier
Thermometer Used:1R Gun T1A0 Type of Ice: W�t�t31ue None oilSamples on Ice, cooling process has begun
Temo Correction Factor T1402 No Correction
r ,
Corrected Cooler Temp.:__,... `I ,�- ,_,_'C
Tamp should be above freezing to ti'C
Biological Tissue is Frozen: Yea No to
Comments:
Date and Initia arson a mining
contents
Chain of Custody Present:
DY C1No
ON/A
1.
.Chain of Custody Filled Out
ee ONO
OWA
2.
Chalri of Custody Relinquished:
os ©No
DWA
3. .
Sa ler Name & Sipnituia on COC:
as ON,
❑NIA
4.
Sani as Arrived within Hold Time,
Yes ONo
ONIA
5.
Short Hold Time Analysis <72hr :
OYes Na .
ONIA
6.
Rush Turn Around Time Requested-,
❑Y No
ONIA
7.
Sufficient Volume:
Ye ONO
❑NIA
8.
Correct Containers Used:
-Pow Containers Used:
ONO
Yes ❑Nb
ONIA
❑NIA
9.
Containers Intacx
es ONo
❑ t0A
10.
Filtered volume received for Dissolved tests
DY - C]No
N!A
11
Sample Labels match COG:
-Includes dateAlmellDlAnal sis Matrix:
Yes CINo
OWA
12.
Aff containers needing preservation have been checked.
All coMalners needing preservation are found to be In
compliance with EPA recommendatlon.
amapli=: VOA, wftr l,T0C,0&G,1M-OROtwaterl
Ye ❑No
Yes ONo
Yes ❑No
OWA
C]NIA
13.
Sainpies checked for dechlodnation:
es ONO
❑wA
14,
Headspace In VOA Vials >Bmm :
❑Yes' X0
ONIA
15,
Trip Blank Present: I
Trip Blank Custody Seals Present
Pace Trio Blank Lot # rf purchased):
OYes ONO
OYes ONo
I
_❑4
t�uA
16.
Client Notification/ Readiution: Field Oata Required? Y ! N
Person Contacted: Datefilme:
Comments/ Resolution:
SCURF Review: Date:
SRF Review; Date; j Z
Note: Whenever there is a discrepancy affecting Nodh Caro ins compliance
samples, a copy of this fort will besent to the North Carolina DEHNf1
Certification Office ( Le out of.hold, lnc mrt preservative, out of temp,
htcorrect containers)
WO#:92273936.
M���ilmiimwgi
Page 12 of 13

PaceAnalj cal
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CHAIN -OF -CUSTODY I Analytical Request Document
The Cnairt-or-Cuslody Ip a �EGALDOCUMENT. All relevant rwAds must La completed -= raNly.
Section A Section $ -' Section C
Pam■: I or
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Fulcher, Craig
From: Cathy Baines <[e-mail]>
Sent: Tuesday, January 26, 2016 2:57 PM
To: Fulcher, Craig
Subject: FW: Scanned image from MX-620ON
Attachments: [e-mail]_20160126_164159.pdf
(ATTENTION: This email was received from an external source. Please use caution when opening attachments and/or responding to this message.)
-----Original Message----- From: nre 1 eastern-environmental.com [nreply(i4eastern-environmental.com] On Behalf Of nreply@ Sent. Tuesday,
January 26, 2016 4:42 PM To: Cathy Baines Subject: Scanned image from MX-620ON
Reply to: nreply a,eastern-environmental.com <nre 1 eastern-environmental.com> Device Name: Eastern Environmental Management Device
Model: MX-620ON Location: Y9314 Rocky Mount, N.C.
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• Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030636
Date submitted 11117/2015
CERTIFICATE OF COVERAGE NO. NCG@3O363—fb C (-o30 _?1z.3
FACILITY NAME ITW Warehouse Automation
COUNTY Buncombe
PERSON COLLECTING SAMPLES Jose Gomez
LABORATORY ESC Lab Cert. # L797142
Comments on sample collection or analysis: Total rainfall event 1.0V
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2015
SAMPLE PERIOD ❑ Jan -June ® July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
[_]zero -flow []Water Supply ❑SA
®Other SDO
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?'
Outfall No.
Date Sample
Collected l
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Suspended Solids
Standard units
ard
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
OrganicsTotal
Benchmarks =_=>
_
-
100 mg/L or 50 mg1V
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
002
10/27/2015
1.00
2.94
7.73
BDL-0.010
BDL-0.005
0.131
BDL-5.7
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. unattended sites maybe eligible for a waiver of the rain gauge requirement.
a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

h. - - - - -
.� _ _
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Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics Into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Chris Bland
Name (Print name)
Plant Manager
Title (Print title)
/
/�L
(Signature)
//// 7,�
Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX rng/.L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note. if you report a sample value in excess of the benchmark, you must implement Tier 1, fer 2, or Tier 3 responses. See General Permit text.
Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
Z4-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
footnotes from Part A also apply to this Part 8
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement rer 1, rer 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART It SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ED
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal and one cape of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reportsl ta:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
11,117,1 S
[Oat
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 3

WW74Rf N0USf
AUTOMATION
November 17, 2015
Central Niles
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: ITW Warehouse Automation
Semi-annual discharge monitoring reports (DMR)
Monitoring period Year 3-Period 2
To Whom it May Concern,
)RECEIVED
NOV 302015
CENTRAL FILES
°wR SECTION
The ITW Warehouse Automation ("ITW") facility located in Arden, North Carolina is
submitting the following information to the Division of Water Quality ("Division") in regards to
the facility general industrial permit NCG030636. Please note, ITW was formerly named
Vertique, Inc.
The current monitoring period is recognized,as July 1, 2015 through December 31, 2015. The
sample analysis attached was collected from outfall 002. The results were reported within 30
days of the date of collection. In 2015, facility personnel are scheduled to be trained to the SPPP
and best management practices. Also, specific personnel were identified to properly collect
samples and report out as needed.
Attached is the discharge monitoring report required for monitoring period year 3-period 2. The
sampling requirements per Section D of the General Permit are below:
a. October 27, 2015/ITW location outfai1002/10:30 am
b. Jose Gomez/Paint Booth Operator
c. November 17, 2015
d. Environmental Science Corporation (ESC)
e. See attached analysis
f. See attached analysis
The benchmark level for zinc has been exceeded this monitoring period. This is the first
exceedance reported from the facility. ITW will review the facility perimeters to verify possible
sources of zinc and provide corrective actions where applicable.
Appalachian Environmental Resources, Inc. has been contracted to handle the water quality
program at the facility. The Stormwater Pollution Prevention Plan (SPPP) has been developed
and all information pertaining to the NPDES permit for Metal Fabrication has been completed.

WWARfHOUSf
UiOMAiION
If you have any questions or require additional information in regards to this submittal, please
contact me at (828)-654-7500 or Michael Fox at (423)-956-2900.
I certify, under penalty of law, that this document and all attachments were prepared under my
direction or supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted Based on my inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations
Sincerely,
Chris Bland
Plant Manager
ITW Warehouse Automation
Cc: File copy
Attachments

at. 1_..=_'F"..-r;.�.<E.- L'" �BKS��N6R1_.tE.l,°Flit.G."IFC:n•a""I.w�a89.fn',uu,-.e8[_: . I
BAJA
�wESQ
I
ANALYTICAL REPORT myESC
November 05, 2015
Appalachian Environmental Resources
Sample Delivery Group: L797142
Samples Received: 10/28/2015
Project Number:
Description: Stormwater (vertique)
Report To: Mike Fox
395 Steel St.
Johnson City, TN 37601
Entire Report Reviewed By: 4V��
Linda Cashman
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applkable, sampling conducted by ESC is
performeC per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304,

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
'Cp: Cover Page
2Tc: Table of Contents
3Ss: Sample Summary
4Cn: Case Narrative
5Sr: Sample Results
STORMWATER OUTFALL 001 L797142-01
r'Qc: Quality Control Summary
Gravimetric Analysis by Method 2540 D-2011
Wet Chemistry by Method 1664A
Wet Chemistry by Method 4500H+ B-2011
Metals (ICP) by Method 200.7
7GI: Glossary of Terms
$AI: Accreditations & Locations
9Sc: Chain of Custody
1
2
3
4
5
5
6
6
7
9
10
11
12
ACCOUNT: PROJECT: SDG:
Appalachian Environmental Resources L797142
DATEMME:
11/0511517:48
PAGE:
2of12

SAMPLE
SUMMARY
Collected by
STORMWATER OUTFALL 001
L797142-01 WW
Mike Fox
Method
Batch
Dilution Preparation
dateltime
Gravimetric Analysis by Method 2540 D-2011
WG825718
1 111020510:19
Metals (1CP) by Method 200.7
WG825728
1 101307i5 20:21
Wet Chemistry by Method 1664A
WG925348
1 10011512:56
Wet Chemistry by Method 4500H� B-2011
WG825397
1 1013011510:00
ONE LAB. NATIONWIDE.
Caiiecled dateltime
Received dateltime
10127A510:30
10/28/15 09:00
r C
p
Analysis
Analysis Analyst
dateltime
�z
Tc
11103/1510:09
JER
1110111516:
WBD
1012911516:56
JM
10130/1510:00
SJM
r
FSf
6
QC
7Gf
6AI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME PAGE:
Appalachian Environmental Resources L797142 11/05/1517:48 3 of 12

CASE NARRATIVE
ONE LAB. NATIONWIDE.
�Cp
All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the
dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria
except where addressed in this case narrative, a non-conformance form or properly qualified within the 2TC
sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data ❑
have been identified by the laboratory, and no information or data have been knowingly withheld that 3S5
would affect the quality of the data.
s
Sr
FQ
Linda Cashman
Technical Service Representative FAI
Sample Handling and Receiving C
Sample quantity was not sufficient to complete analysis per recommended method guidelines for the following samples.
ESC Sample ID Project Sample ID Method
L797142-01 STORMWATER OUTFALL 001 2540 D-2011
The following samples were prepared and/or analyzed past recommended holding time. Concentrations should be
considered minimum values.
ESC Sample ID Project Sam Method
Method
L797142-01 STORMWATER OUTFALL 001 4500H+ B-2011
ACCOUNT: PROJECT: SD& DATE/TIME: PAGE:
Appalachian Environmental Resources L797142 11105h517:48 4 of 12

STORMWATER OUTFALL 001
SAMPLE RESULTS - 01
ONE LAB. NATIONWIDE. �
Collected date/lime: 10127/15 10:30
L797142
Gravimetric Analysis by Method 2540 D-2011
Result Qualifier
RDL
Dilution
Analysis
Batch
FP
Analyte mg4
mg/1
date 1 tlme
�Z
Suspended Solids 2.94
2.50�
1
111031201510:09
WG825718
TC
Wet Chemistry by Method 1664A
35s
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte mgll
mgll
date I lime
rcn]
TPH - Oil & Grease ND
6.49
1
101291201516:56
WG825349
Wet Chemistry by Method 4500H+ B-2011
Result Qualifier
Dilution
Analysis
Batch
Analyte su
datellime
rQC1
pH 7.73
1—
10130/201510700
WG825397
FGI
Sample Narrative:
4500H+ B-2011 L797142-01 WG625397: 7.73 at 18.8c
IIAi
Metals (ICP) by Method 200.7
Qualifier
RDL
Dilution
Analysis
Batch
FResult
Analyte mgll
myli
dale 1 time
Copper NO
0.0100
1
111011201516:03
WG825728
Lead ND
0.00500
1
11/011201516:03
WG825728
Zinc 0.131
0.0500
1
111011201515:03
WG825728
ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
Appalachian Environmental Resources L797142 1110511517:48 5 of 12

WG825718
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE,
Gravlmetrlc Analysis l Method 2540 D-2011
L797142-01
Method Blank (MB)
(MB) 11/03/15 10:05
E
MB Result M8 Qualifier MB ROL
Analyte mgll mg11
F
Suspended Solids ND 2.50
Y
FS
L797177-01 Original Sample (OS) • Duplicate (DUP)
(OS) 11/03/15 10:08 • (DUP) 11/03A5 10:D6
FCn]
Original Result DUP Result Dilution
DUP RFD DUP Qualifier DUP RFD Limits
SSr
Analyte mgll mgll
% %
Suspended Solids 126 135 1
5.78 J3 5
Laboratory Control Sample (LCS) • Laboratory Control Sample
Duplicate (LCSD)
(LCS) 1110311510:05 • (LCSD)11103/15 10',05
FGi
Spike Amount LCS Result LCSD Result
LCS Rec. LCSD Rec, Rec. Limits LCS QualiBef LCSD Qualifier RPD RPD Limits
Analyte mg11 mgli mgli
_
% % A % % ---
BAI
Suspended Solids 773 812 800
105 103 85.0-115 1.49 5
--- --T-
FIC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Appalachian Environmental Resources L797142 11/05/1517:48 6 of 12

WG825348 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE.
Wet Chemistry by Method 1664A L797142-01
Method Blank (MB) RP(MB) 10I2911516;54
MB Result MB Qualifier MB RDL
F
Analyrte mg11 mgf!
TPH - Oil & Grease ND 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 10/29115 16:54 • (LCSD) 10/29115 16:54
Spike Amount
LCS Result
LCSD Result
LCS Rec. LCSD Rec, Rec. Limits LCS Qualifier
LCSD Qualifier RPD RPD Limits
Anatyte mgll
mgll
mg11
% % %
a %
TPH - Oil & Grease 20.0
20.1
19.8
101 99.0 78.0-114
1.50 18
ACCOUNT:
PROJECT: SDG:
DAT671ME: PAGE:
Appalachian Environmental Resources
L797142
4110511517:48 7 of 12

WG825397
Wet Chemistry by Method 4500H+ B-2011
L797109-01 Original Sample (OS) • Duplicate (DUP)
(OS)10130/15 10:00 • (DUP)10/30/15 10:00
Original Result DUP Result Dilution
Analyse su 5u
PH 7.53 7.52 1
L797403-02 Original Sample (05) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L797142-01
DUP RPD DUP Qualifier DUP RPD Limits
0.133 1
(OS) 10/30/15 10:00 • (DUP)10/30/15 10:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits
Analyte Su su % %
PH 7,00 7.02 — -- 1 - ---0.285 1
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 10/30/15 10:00 • (LCSD)10130/15 10:00
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier
Analyse Su Su sL % % %
PH --_ - -- -_ 6.72 6,71 6.70 99.9 99.7 98.5-102
LCSD Qualifier RPD RPD Limits
0,149 1
ONE LAB. NATIONWIDE.
ACCOUNT:
PROJECT: SDG:
DATEITIME:
PAGE:
Appalachian Environmental Resources
L797142
=5/1517AS
9 of 12

WG825728
QUALITY
CONTROL SUMMARY
ONE t_AB,NATIONWIDE,
Metals (ICP) by Method 200.7
1.797142-01
Method Blank (MB)
, Cp
(MB) 11/01/15 17:55
❑
ME Result M8 Qualifier
ME RDL
Analyte mgll
mg/1
TC
Copper ND
0,0100
Lead ND
0.00500
rq
Zinc ND
0.0500
FC
Laboratory Control Sample (LCS) - Laboratory
Control Sample
Duplicate (LCSD)
(LCS)11101/15 15:14 • (LCSD) 11/01/3 17:03
S r
Spike Amount LCS Result
LCSD Result
LCS Rec.
LCSD Rec. Rec, Limits LCS Qualifier
LCSD Qualifer
RPD
RPD Limits
Analyte mgll mgll
mg/I
%
% %
%
%
Copper 1.00 1.06
1.03
106
103 85-115
2
20
Lead 1.00 1.07
Zinc 1.00 1.03
1.04
1.00
107
103
104 85-115
100 85-115
3
3
20
20
FG1
L797067-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
FAI]
(OS) 11/01/15 15:20 • (MS) 11/01/15 15:26 • (MSD) 11/01/15 15:29
Spike Amount Original Result
MS Result
MSD Result
MS Rec. MSD Rec. Dilution
Rec. Limits MS Qualifier
MSD Qualifler
RPDRPD Limits
rq
Analyte mg/I mgll
mg11
mgll
% %
%
%
Copper 1.00 ND
1.03
1.04
103 104 1
75-125
1 20
Lead 1.00 0.00324
1.06
1.07
105 107 1
75-125
1 20
Zinc 1.00 0.0352
1.04
1.06
100 102 1
75-125
2 20
L7972O9-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) 1VOW 516:28 • (MS)11/01/15 16:31 • (MSD)11/01115 16:34
Spike Amount Original Result
MS Result
MSD Result
MS Rec.
MSD Rec. Dilution
Rec. Limits MS Qualifier
MSD Qualifier RPD
RPD Limits
Analyte mgll mg11
mg/I
mgll
%
%
%
%
%
Copper 1.00 0.0220
1.09
1,07
106
104 1
75-125
2
20
Lead 1.00 0.00268
1.07
1.05
107
105 1
75-125
1
20
Zinc 1.00 0,191
1.07
1.05
86
86 1
75-125
2
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Appalachian Environmental Resources L797142 11/05/15 17:48 9 of 12

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. 0
Abbreviations and Definitions
SDG
Sample Delivery Group,
rqp
MDL
RDL
Method Detection Limit.
Reported Detection Limit.
�Tc
ND,U
Not detected at the Reporting Limit (or MDL where applicable).
RPD
Relative Percent Difference.
(dry)
Results are reported based on the dry weight of the sample. [this will only be present on a dry
RS
Original Sample
report basis for soils].
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
rC n
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring
Sr
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.
Recovery.
SDL
Sample Detection Limit.
FC1
MOL
Unadj. MOL
Method Quantitation Limit.
Unadjusted Method Quantitation Limit.
Qualifier
Description
aAl
J3
The associated batch QC was outside the established quality control range for precision.
Sc
ACCOUNT:
PROJECT: SDG: DATE171ME:
PAGE:
Appalachian Environmental Resources
L797142 11105/1517:48
10 of 12

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
ESC Lab Sciences is the ontyenvironmental laboratory accreditedlcertified to support your work nationwide hom one location. One phone call, one point of contact, one laboratory. No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capabllity from our single location laboratory is comparable to the collI totals of the
network fahoratories in our Industry. The most significant benefit to our 'one location' design is the design of our laboratory campus. The model Is conducive to accelerated producllvrty,
decreasing turnaround time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CFil
State Accreditations
Alabama
40660
Nevada
TN-03-2002-34
Alaska
UST-080
New Hampshire
2975
Arizona
AZ0612
New Jersey—NELAP
TNO02
Arkansas
88-0469
New Mexico
TN00003
California
01157CA
New York
11742
Colorado
TN00003
North Carolina
Env375
Conneticut
PH-0197
North Carolina
DW21704
Florida
E87487
North Carolina 1
41
Georgia
NELAP
North Dakota
R-140
Georgia'
923
Ohio—VAP
CLOO69
Idaho
TN00003
Oklahoma
9915
Illinois
200008
Oregon
TN200002
Indiana
C-TN-01
Pennsylvania
68-02979
Iowa
364
Rhode Island
221
Kansas
E-10277
South Carolina
84004
Kentucky'
90010
South Dakota
nla
Kentucky'
16
Tennessee"
2006
Louisiana
A130792
Texas
T104704245-07-TX
Maine
TNO002
Texas'
LA80152
Maryland
324
Utah
6157585858
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
109
Minnesota
047-999-395
Washington
C1915
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
9980939910
Montana
CERT0086
Wyoming
A2LA
Nebraska
NE-OS-15-05
Drinking Water z Underground
Storage Tanks 1 Aquatic Toxicity ' Lhemical,iMicrolo ologlcal
x Mold m Accreditation not applicable
Third Party & Federal
Accreditations
A2LA — $SO 17025
1461.01
AIHA 100789
Canada
1461.01
DOD 1461,01
EPA—Crypto
TNO0003
USDA S-67674
Our Locations
ESC lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at our central laboratory.
ACCOUNT: PROJECT: SDG: DATEIrIME: PAGE:
Appa$achlan Environmental Resources L797142 11/05/1517:48 11 of 72

Ccmpanv Name/Address:
OWIMS Information;
Analysis
Ccnlal ner
J Preservative
Chem of Custody Page — of
OESC
L-A-8 O-C.I-C-N-C-95
12065 Ltbanoh Ad
C 9
'A
'J�—
Report to:
Ice- Fow
Email TO:
Project
Description:
Collected:
156
Phone:
Fax:
Client Project A 1
tab Project $1
Coll t by JpYinti:
FdIc, F-�
Sitt!/Facility to a
P.O'
Acctiitum:
Temp t9e.'
Orelo6w � I
� .
ITSR:
iB:
ColJeCJJd by (signaluire):
immediately
Packed on Ice N Y
Rush? ILab MUST Be Notified)
Same Day ....... 100%
Newt Day ........ 10D%
J TWO DSY .................... S(Y%
Three Day. .............. —15,%
Date Results Needed
Email? —No Ye!,
FAX? No Yes IND.99
of
Shlpped.Via;
Sample 10
Camp/Grab
Matfi)L •
Depth
Date
lime
-ntrs
L/ Li
o hi J i f
3 oPQ,.—
a
Matrix: 55 - Sol] GW - Groundwater VrW - WasteWater OW - DrIni,ingWatef Ot - Other ph Temp O d2 ELI) 0
Remarks: How Othet Hi3ld 4'
Relinquished by: (Signature]
Date:
Time:
Rec ived Signa* r LI)
Samples r turned via: 0 UPS
0 courier 0—
COnd;tlor . i: (lab usepptyj
COC Seal In I _N NA,
Relinquished try ililgrialsire)
DAN
Time:
ReceiViVeAt4rel
Te;7 aCBottles Received
Relinquished by: JSIgn ature)f
Date:
Time;
11,
�Relelv' 0 d for 13b Ibly: JrYg !ZnalkkTe)
Date; Tlmd:
pH Chec'kctdi

Snap:an Tools
12195 State Line Road
Eiizabethton,TN37643
Billing Information:
Ja,Yt:e Estep
219S State Line Rd
Elizabe.hton, TN 37643
Analysis
/
Container
/ Preservative
iChain of Custody Page _ of —
*ESC
L•A•8 G-C•I•E•ee•C•f;:•a
&A
. O..
p
Z
I:
uy
L]
= ca
`
a
C
>++
p-
a-
2
O
tL
fs
_
E
S
In
cn
-�
f�
0
N
o
F�
t"
n
p
E
01
V1
in
Z
rC)
a
Z. ,
•= i
c
w P
G7
d
z
UJ
VT
O
^�
"�
C' i
as
- ;r
O.
t�
Moue1tMe% TN 37122
vfa„e:alsasft-snse
phone: 8DO—M7-Sass
ru:6ts isa•ses9
Report to:
Mike Fox
Email Tx
Brian.:rwiaesnapon.com;mfox4baenn.com
Project
Description: discharge monitof> ng-monthly
Oty/State
Codected:
L N ? 941
Phone: 423-543-S771
Fax:
Client Project
Mcnthly Monitoring
Lab Project p
SNAPONETN-MONTHLY
D188
Collected by {print),
v
Sitc/Facility ID p
P.O. ff
14NO17976
Acctnum: SNAPONETN
Template:T63159
Prelogln:. P523158
TSB 650 -Linda ashman
PBi ` L
eoflecte by signature):
Im t
Parke on Ice N Y
Rush? (Lai) MUST Be ka:ii.ed)
Same Div .... ......._........... 20L%
_NextDay.._.-........_.._-.......100fL
T Two D2Y..............................SO%
. _Three Oay ........ ................. 2Sx
Date Results Needed
Email? Na X Yes
FAX? —No Yes
of
Shipped Vfa- Corp Exp -
Sample ID
Carrp/Grab
Matrix •
Depti,
Date
Time
ntrs
f�61LIr�1YY11iNRi
�11AOt1 I�J� 0��,1
COMPOSITE
G,
W1N
t7 i— Z
�q ZO
5
X
X
X
X
X
GRAB
ww
p 3 a
X
X-OIL
_
Matrix: SS - Soil GW • Groundwater WW - WasteWater Df'W -- Drl iking Water OT - Other �7
Remarks: pH Temp
Flow Other Hold if
Relingaishe b &ISignature)
Date:
(� 5
Time:
f
deceived by: {Sign turel
Samples returned via: ❑ UPS
0 FedEx 0 Courier
Condition: (lab use only)
COC Seal Intact. Y T N _NA
Relinq h y : (Signature). �a,
Date:
Time:
Received by: {Sig OWTJ
mp C. bottles Received:
Relinquished by. IS$nature
Date:
Time.,
Received for lab by: ISl,naturel
Date; Time:
- ate
pH Checked:
NCF:

A
RECEIVED
RC—DENR FEB o 5 zIb
Stormwater Discharge Outfall (SDO) CENTRAL FILES
Qualitative Monitoring Report oWR SECTION
For guidance on filling out this form, please visit:
Permit No.: ZI/C �_/_/� j or Certificate of Coverage No.: jj/-C/-G/()/3W) 2 i 3
Facility Name:
County:
Inspector:
Date of Inspection:
Time of Inspection:
Total f'svent Precipitation (inches): r Q C
Phone No.
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
9Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm '
event" or `measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement Please refer to these definitions, If applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation
A'"measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify thgthis report is accurate and complete to the best of my knowledge:
(Signature of6!e:mittA or Designee)
Page 1 of 2
sWU-242, last modified 10/25/2022

0
1. Outfall Description: y
Outfall No. :� L Structure [pipe, ditch, etc (` rk
Receiving Stream: U T
Describe the industrial activities that occur within the outfall drainage area:
r-.<-, 1e 21 - AME--, t� Q - ..
2. Color: Describe the color of the discharge using basic c lors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: _ �u e 1+5
3. odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): r� �� ._ ... _. _
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where i is no solids and 5 is extremely muddy:
2 3 4 5
7. Is there any foam in the stormwater discharge? Yes N
8. is there an oil sheen in the stormwater discharge? Yes
9. is there evidence of erosion or deposition at the outfall? Yes No
10. other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be Indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
$WU-242. East modified 10/25/2012

aceAnaly�l
tnhcpaveleba�n
November 05, 2015
Mr. Johnny Baines
Eastern Environmental Management
PO Box 4030
518 S. Pearl Street
Rocky Mount, NC 27803
RE: Project: SPX 10/2015
Pace Project No.: 92273916
Dear Mr. Baines:
Pace Analytical Services, Inc.
980D KIncey Ave. Suite 100
Huntersvf6e, NC 2OD78
(704)8759092
Enclosed are the analytical results for sample(s) received by the laboratory on October 29, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
cc M5. Cathy Bah m Eastem Environmental Management
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In lull,
wftut the wrtlten consent of Pace Analytical Services, Inc.,
Page 1 of 13

I,C
AlI I0
CERTIFICATIONS
Project: SPX 10/2015
Pace Project No.: 92273M
Charlotte CertIfication IDs
9800 Klnc ey Ave. Ste 100, Huntersvllle, NC 28078
Florida/NELAP CerOficatlon M E87627
North Carolina Ddnldng Water Certltfratlon M 37706
Kentucky UST Certif+catbn M 84
North Carolina Field Servioes CerNflcation #: 6342
West Virginia Cerdfloadon #, 367
North Carolina Wastewater Certification #. 12
Vhgln1Wr=LAP CertMcatlon #: 460221
South Carolina Certification M 99006001
Asheville CerdfkeatlOn ms
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certlftcation #: 40
Flodda/NELAP Certlfication #: E87648 South Carolina Certiflcation #. 99030001
Massachusetts Certlflcation #: U-NC030 West Virginia Certlflcation M 356
North Caroline Drinking Wader Certification M 37712 VirginieNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in U,
whhout the written Consent of Pace Analytical Services, tnc,.
Pace Analytical 39rAces, Inc.
9800 KInaey Ave, Suite t00 ,
l4unionMIM, NC 28 078
(704)875$062
Page 2 of 13

-4
n
n �
aceAnaocal
won
SAMPLE ANALYTE COUNT
Project SPX 1012015
Pace Project No.: 92273916
Pace Analytical Sarvlces, Ine.
MW KinoeyAve. Suite 100
Hunbaravnle, NC 2807a
(704)87H•9092
Analysts
Lab ID Sampte ID Method
Analysts
Reported
Laboratory
92273916001 WO-1 EPA 1664B
JMS
1
PASS-C
EPA8082
SWB
8
PASi-C
SM 2540D
SAM
1
PASI-A
EPA 351.2
SER
1
PASI-A
EPA 353.2
DMN
3
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shag not he reproduced, except In full.
without the written torment of Pace Analytical Services. Inc..
Page 3 of 13

aceAnabtr'caie
ANALYTICAL RESULTS
Project: SPX 1012015
Pace Project No.: M73916
Pace Analytical Services, Im.
9800 KlnceyAwe. Sulfa 100
HuntemAls. NC 28078
(704)B7548092
Sample: SDO.1
Parameters
Lab ID: 02273916001 Collected: 10/20/1516:30
Results Units Report Limit OF
Received: 10/29/15 09:45 Matrix: Water
Prepared Analyzed CAS No. Quell
HEM, Oil and Grease
Analy9cal Method: EPA 16848
Oil and Grease
ND
mg/L
5.0
1
1110511510:39
$002 GCS PCB
Analytical Method: EPA 8082 Preparation Method: EPA 3510
PCB-1016 (Aroctor 1016)
NO
ug(L
0.50
1
10130/15 09:30 1W30115 19:06 12074-11-2
PCB-1221 (Arodor 1221)
NO
ug/L
0.50
1
10/30/15 09:30 10/30/15 19:06 11104-28-2
PCB-1232 (Arodor 1232)
ND
ug1L
0.50
1
10130/1 S 09:30 10tf30/15 19:08 11141-18-6
PCB-1242 (Arodor 1242)
ND
ug/L
0.50
1
10/30/15 09:30 10/30/15 19:06 53469-21-9
PCB-1248 (Aroclor 1248)
Nil
ug&
0.50
1
10130/16 09.30 10/30/1519*06 12672-29-8
' PCB-1254 (Amdor 1254)
ND
ug/L
0.50
1
10/30/15 09:30 10/3011519:06 11007.89-1
PCB-1 260 (Arodor 1280)
NO
ug/L
0.50
1
10130/1509:30 10MOMS19:06 11098-82-5
Surrogates
Decachioro6lpherryl (S)
25M Total Suspended Solids
Total Suspended Solids
351.2 Total IQeldahl N"on
Nitrogen, l9aidahl, Total
353.2 Nitrogen, NO2JN03 unpres
Nitrogen, Nitrate
Nitrogen. Nitrite
Nitrogen, NO2 plus NO3
Date: 1VOW015 05:32 PM
35 %
Analytical Method: SM 25400
NO mg/L
Analytical Method: EPA 351.2
ND mg/L
Analytical Method: EPA 353.2
0.15 mg1L
NO mg/L
0.15 mg/L
10-132 1 10/30/15 09:30 110/30115 19-.00 2051-24-3
5.0
1
1110111515:12
0.50
1
11/03/15 03:10 7727-37-9
0,020
1
10/30/15 10.39
0.020
1
1013011510:39
0.020
1
10f3011610:39
REPORT OF LABORATORY ANALYSIS
This report aha9 not be reproduced, wept In full.
without the writlan cansent of Pars Analytical SerA ces. Inc.•
Page 4 of 13

aecAnalyticW e
QUALITY CONTROL DATA
Project SPX 10r2015
Pace Project No.. =73916
QC Batch: GCSYl23118 Analysts Method: EPA 1684B
QC Batch Method: EPA 16648 Analysis Description: 1664 HEM, Oil and Grasse
Assodaled Lab Samples: W73918001
METHOD BLANK: 1599395 Matrbr Water
Assodated Lab Samples: 02273916001
Blank ReporOng
Parameter units Result Limit Analyzed Qualifiers
Oil and Grease mg1L ND 5.0 1110511510:35
PaceArtalyttcal Sarvleea, Inr-
ONO KinceyAm Suite WO
Hurbreville, NC 20078
(704)8754=
LABORATORY CONTROL SAMPLER LCSD: 1599396 1599397
Spike LCS LCSD LCS LCSD % Rac Max
Parameter Units Conc, Result Result % Rec % Rec Limits RPD RPD Qualifiers
DIl and Grease mg/L 40 35.4 35.3 88 88 78-114 0 30
Pastdfe presenbd on Oft papa ere In the units Indicated by ths'Units' column satapt where an alternate unit to praeented to the right of ate result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in hill.
Date: 11IM015 05:32 PM vrithout the written cwrlseni of Pace Analytical Services, Inc...
Page 6 of 13

ceAnalyticxl'
QUALITY CONTROL DATA
Project: SPX 10/2016
Pace Project No.: 92273916
Pace Analytical Services, Inc.
M I(InoeyAve, Suft 100
HuntersvlAe, NC 28078
(704)8759092
QC Batch: OEXT/38710
Analysts Method: EPA SOU
OC Batch Method: EPA 3510
Analyals Description: W82 GCS PCB
AssocWed Lab Samples: 92273916001
METHOD BLANK: , 1504382
Matrix: Water
Associated Laic Samples: %273916001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
PCB-1016 (Amcor 1016)
ug/L
ND 0.50
10/29/15 22:07
PCB-1221 (Arodor 1221)
ug/L
ND 0.60
10/29/15 22:07
PCB-1232 (Amcor 1232)
u01L
ND 0.50
10/29/15 22 07
PCB-1242 (Arodor 1242)
uglL
ND 0.50
10/29/16 22:07
PCB-1248 (Aroclor 1248)
ug/L
ND 0.50
10129115 22.07
PCB-1254 (Aroc or 1264)
ug/L
ND 0.60
10129/16 22:07
PCB-1280 (Arodor 1260)
ug/L
ND 0.60
1 =911 5 22:07
Decachlorobiplu" (S)
%
83 10-132
10/29/16 22:07
LABORATORY CONTROL SAMPLE 8 LCSD:
1594383
1594384
Spike LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc. Result Result
% Rec % Rec
Llmlls RPD RPD Qualifiers
PCB-1016 (Arodor 1016)
u91L
5 4.2 4.3
83 86
60-150 2 30
PCB-1260 (Arodor 1260)
uglL
5 4.4 4.4
87 87
50-150 0 30
Decachloroblphenyl (S)
%
82 83
10-132
b Reaulla prevented on this a an In the unite Indicated Vm tJnity^ cWumn mme when an altemate unit le peg by pt prevented to the Hot of tiu reealL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In fun,
Date: 11105/2015 05:32 PM without the written consent of Pace ArtaKlcel Servioes, Inc..
Page 6 of 13

ceAnalythx!'
Pace Anslyttcal Savicas, Inc.
MOO KlnceyAvo. Suite 100
Hurkhmadle. NC 28M
(704)B764082
QUALITY CONTROL DATA
Project: SPX 1002015
Pace Project No.: 92273916
QC Batch: . WETI41157 Analysts Method: SM 2540D
QC Batch Method: SM 2540D Analysts Description: 2640D Total Suspended Solids
Assodated lab Samples: M73916001
METHOD BLANK: 1596407
Assodated Lab Samples: 92273916001
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE: 1596408
Parameter units
Total Suspended Solids mglL
SAMPLE DUPLICATE: 1596409
Matrbt: Water
Blank Reporting
Result •Limp Analyzed Qualifiers
ND 2.5 11f01115 15:06
Spike LCS LCS % Rec
Conc. Result % Rec Limas Qualifiers
250 240 96 90-110
92274207001
Dup
Parameter
Units
Result
Result RPO Qualifiers
Total Suspended Solids
mg/L
173
179 3
SAMPLE DUPLICATE: 1596410
92273916001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
NO
ND
Rmuld presented an this papa an In to anita rndlcated by the 'UnWedumn except when m altanuto unit Is pnaented to thsdght of the result.
REPORT OF LABORATORY ANALYSIS
This report shot not be repraduced, except In full,
Data: 11/05f2015 05:32 PM tviihout the written mnmM of Pace Analytical Service®, Inr,. Page 7 of 13

li,
laeAnaOcal'
QUALITY CONTROL DATA
Project SPX 1012015
Pace Project No.: =73916
QC Batch: WETA125207 Analysis Method: EPA 351.2
QC Batch Method: EPA 3512 Analysis Description: 351.2 TKN
Associated Lab Samples: 92273916001
METHOD BLANK: 1696242 Matrix: Water
Associated Lab Samples: 92273916001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeidahl, Total mgfL NO 0.50 11l03115 02:52
Pace Analytical Services, Inc.
N00 Klnsay Are. Sults 100
Huntersvile, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 15913243
Spike LCS LCS % Rec
Parameter Units Conc. Result _ % Rec Limits Qualifiers
Nitrogen, Kleldahl, Total mg!L 10 10 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE 1696244 1596245
MS MSD
92274056001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, KJeldahl, Total mg&- 0.94 10 10 11.3 10.8 104 99 90-110 4
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1596246 1596247
MS MSD
92273502001 Spike Spike MS MSD MS MSD % Rac
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qua!
Nitrogen, Kjeidahl, Total mgfL 6.9 10 10 10.7 16.1 39 92 90-110 40 M1,R1
Rasurts pressated on ale page are In the unite lnftated by ths'UnW column except where an altemsto unrt b presented to ere right of the reault.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Data: 11/0512015 05:32 PM without the written consent of Pace Analytical Services, Inc,.
Page 8 of 13

Paco Analylicai Saalces, Inc.
0800 KlnaeyAve. $We 100
Huntamvl4e, NC 28070
(704)8754092
QUALITY CONTROL DATA
Protect SPX 10/2015
Pace Protect No.: =73918
QC Batch: WE-fiA125198 Analysis Method:. EPA353.2
QC Batch Method: EPA 3532 Armlysls Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 92273916001
METHOD BLANK ' 1595416 Matrix Water
Associated Lab Samples: 92273916001
Blank Reporting
Parameter Units Result Lh tt Analyzed Qualifiers
Nitrogen, Nfrate mg/L ND 0.020 10134f15 10:36
Nitrogen, Nitrite mg/L ND 0.020 10f30116 10:36
Nitrogen, NO2 plus M03 mg1L ND 0.020 1 OW1610:38
LABORATORY CONTROL SAMPLE:
1595416
Spike
LCS LCS % Rec
Parameter
Units
Cone.
Result % Rec Limits Qualifiers
Nitrogen, Nitrafie
mg/L
2.5
2A 96 90-110
Nitrogen, NIM
mg/L
1
0.97 97 90-110
ftogeri, NO2 plus NO3
mg1L
2.5
2.4 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1595417
150541 B
MS
MSD
92273916001 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc,
Conc,
Result
Result
% Rec
% Rec
Limits
RFD Quel
Nitrogen, Nitrate
nV&
0.15 2.5
2.5
2.6
2.6
96
96
90-110
0
Nitrogen, Nitrtts
MQ&
ND 1
1
1.1
1.1
104
104
90-110
0
Nitrogen, NO2 plus M03
mglL
GAS 2.5
2.5
2.6
2.6
96
96
90-110
0
Rwultspresaeted an this page Armin the unit todiested by the Zhdls- ealumn except where am atternete ueit Is prssseted to the right of Me raven
REPORT OF LABORATORY ANALYSIS
Ttds report shall not be reproduced, except in full,
Date: 11/0& 2015 05:32 PM without the watten consent of Pace Analytical Services, Inc..
Page 9 of 13

aceAnaocal'
rvwcpacub"b rrr
QUALIFIERS
Project. SPX 10/2015
Pace Project No.: 92273916
DEFINITIONS
DF - Dilution Factor, If reported, represents the factor applied to the reported data due to dilution of the sample aliquot
ND - Not Detected at or above adjusted reporting limit.
J - Fgtirnat>sd concentration above the adjusted method detection limit and below the adjusted reporting fimit
MDL-Adjuated Method Detection UmIL
PQL - Practice[ Quantltation Limit
RL - Reporting Limit
Paco Analytleal Sw vlcra, Inc.
0800 KlnceyAm Sulfa 100
HuntorsAle, NC 2807a
(704)8754002
S - Surrogate
1,2-Diphenylhydrazlne decomposes to and cannot be separated from Azobenzene using Method B270. The result for each anaiyte Is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Semple (Duplicate)
MS(D) - Metric Spike (Duplicate)
DUP - Sampio DupikNta
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Gean-Up
U - Indicates the compound was analyzed far, but not detected.
Add preservation may not be appropriate for 2 Chlomethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 Is recommended in SW846 Chapter a for the analysis of Acrolain and Acryionitrile by EPA
Meftrod 8260.
I4-Nitrosodiphenylamine decomposes and cannot be separated from bipher yiamine using Method 8270. The result reported for
each analyte Is a combined concentration.
Paco Analytical is TNI accredited. Contact your Pao& PM for the current Est of accredited ana[ytes.
TM - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical SeFvfces -Asheville
PASI-C Paco Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spice recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not bo roproduoad. except to lull,
Date: 11/0512015 D5:32 PM without the wrkttett consent of Pace Analytical SorAws, Inc- Page 10 of 13

ceAnaYical
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project SPX 1012015
Pace Project No.: 02273916
Pace Anatytical SaMces, Inc.
0890 K]noeyAve. Suite f00
Nuntersvile, NC 28078
poa)e7n-sc>ss
Lab [D
Sample ID
QC Batch Method
QC Bauch Analytical Method
92273916001
8DO-1
EPA 16545
OCSVl23118
92273918001
SDI?-1
EPA3610
OEXT138710 EPA8082
92273916001
SDO.1
SM 25400
WET141157
02273916001
SDO-1
EPA 351.2
WETA125207 '
92273915001
SDO-1
EPA 353.2
WETA125196
REPORT OF LABORATORY ANALYSIS
Thfs report shall not be reproduced, except In full.
Date: 11105W15 05.32 PM without the written consent of Pace Anayt&:at Senfces, Inc..
Analytical
Batch
GCSV123060
Page 11 of 13

uOcument-Name., uVku1?1V11lrwvrmu,limy iv,sWl%r
`✓ kW Sam ie Condition Upon Recel t ($CUR) Pagel 1 of 2"
Document Number. Issuing Authority:
F-CHR-CS-003-rev.16 Pace Huntersvllle Quallty Office
Client Name:, l .,r„ • Page 2 oi2 is for Internal Use o„<y
Courier: ❑ FedPO"' UP❑ USP[] CllerCl CommereiLl Peoe Other
Custody Beal on Coo[erlRwc Present: ❑ yee. `no Seals intact: ❑ ye�,no �^�Q, ME
Packing Mabarlal: ❑ Subbfe Wrap Bubble Be None ❑ Other
Thermometer Used: IR Gun T74P Type of Ice: �Bl
ue None Samples ott ice, coonng process has begun
"0
Temo Correction Factor T1402 No Correction l I
CorrectedCoolerTelnp.: 'C
Temp shouki be stave freezing to M
Blologlcal Tissue Is Frozen: Yee No t�iA
Comments: /
Date and INtla arson OMmining.
contents•'oi
Chain of Custody Present:
DY ❑No
❑NIA
1.
Chain of Cus . Filled Out
eo ONa
❑NIA
2.
Chelri of Custody Relinquished:
es ONO
pNIA
3. .
Sa lei Name & sl ature on Coe:
ides 13Na
❑NIA
4.
Sam les Arrived within Hold Time,
Yes ONO
EINIA
6.
Short Hold Time Ana 42iir :
❑Yes No
❑NIA
B.
Rush'Tum Around Time Requested.
E)Yqp.dNo
13MA
7.
Sufflclent Volume:
A'ysj, on.
ONIA
8.
Correct Containers Used.
-Pace Containers Used:
©No
Yes ❑Na
❑NIA
❑NIA
9.
Containers Intact
es ON,
[JtPA.
10.
Filleted volume received for Dissolved tests
❑Yes-1]No
NI,a
11.
Sample Labels match COC:
-includes dateAime/1D/Anal sts Matrix:
Yes CINo
OWA
12.
,
tl contatners needktg preservattan haws been checked.
All cohlainem ii 4ng preservatlon are found to be In
compliance with EPA recommendation.
ems: VQA a dorm,'r0C.OaQ,W-AR0
Y ❑No
Yee ONO
Ea ONo
❑NIA
❑NIA
13,
Sam checked for dechlodnation:
V41 ONo
©wIA
14,
Headspace in VOA Vials :--i3mm :
Ciyes. J34
❑WA'
15.
Trip Blank Present: 1
Trip Blank Custody Seals Present
'
Paco Trip Blank Lot# if purchased).
OYes ❑No
Dyes ❑No
l
i
Q
l IiA
Ia.
Client Notifleationl'Reeolution: Fteid Data Rewired? Y I N
Person Contacted: Datelitme:
Comments/ Resolution:
SCURF Review: - Date: ro � ��lf : 76L747� 1
SRF Review: Date:
Nasample, Whenever CVY ofthisthis Imm will Is a be Bad tcy o he North Carolina QEH R�
Cerllftcation Oftice ( Le out of.itoid, incorrect.preservathre, out of temp, 92273916
bcorrect containers}
Page 12 of 13

PaceArralytical
.rw.oaialrsran
CHAIR -OF -CUSTODY ! Analytical Request Document
fie ChaiR•o6r,ul.Fgdy ¢ a i EGAt OC•CUMENT- An ml4mu FWft mast 6. o=s)leiad accyreWy.
-
REGU TORYAGENCY
i
Ptc- •
..
12
SAMPLE >f OZ.
COW OT
r
Y�
a
VWtWN�ft��gforomVW=C* WUP-.9%NU=daypaY+�+oMklRsum7¢OtirlpbC�S.p4roQec011S;�'Dal.P.n,raicio yraQw'n30Arya' — F-►UJ.-Q-a2QleV.ai,453'

Fulcher, Craig
From: Cathy Baines <[e-mail]>
Sent: Tuesday, January 26, 2016 2:57 PM
To: Fulcher, Craig
Subject: FW: Scanned image from MX-620ON
Attachments: [e-mail]_20160126_164159.pdf
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Original Message From: nreply ,eastern-env�ronmental.com nre ]yna,eastern-environmental.com] On Behalf Of nreply@ Sent: Tuesday,
January 26, 2016 4:42 PM To: Cathy Baines Subject: Scanned image from MX-620ON
Reply to: nre lyReastem-environmental.corn <nre 1 dastern-environmental.com> Device Name: Eastern Environmental Management Device
Model: MX-620ON Location: Y9314 Rocky Mount, N.C.
File Format: PDF MMR(G4) Resolution: 200dpi x 200dpi
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Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted _ _L 3 r /.S
CERTIFICATE OF COVERAGE NO. NCG03L _a a 3
FACILITY NAME S_QX
COUNTY
PERSON COLLES'II G SAMPLES An
LABORATORY CLC-f_— Lab Cert. # q6
Comments on sample collection or analysis:
SAMPLE COLLECTION YEAR _ ao15
SAMPLE PERIOD R Jan -June ❑ July -Dec
or []Monthly' month]
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
[]Zero -flow [_]Water Supply [:]SA
❑Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
Part A. Starmwater Benchmarks and Monitoring Results
❑ No discharge this period?
P�
Date Sample
24-hour rainfall
pH,
To oxic
Outfall No
:_.. 1:
Collected
amount
Total Suspended Solids .
Standard units
Cop{�er' :.
Zinc
Total Petraleu`rn .
qr a s 5
:
ino dd
inch3'
es
i
Hydrocarbons
Benchmarks >;
_
:100 mg/L ar 50 mgJL "-
6 0 — 9 0
0 007 mg/C
0 03 mg/L € ,
O'.067. mgJL .
15, mg/L :
1 mg/L ::::;
m
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
ZFor sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
s The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
-'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR,469.22- and for -cathode ray
tube manufacture use the definition found in 40 CFR 469.31). R C F, ! V L U
JUK 08 2015
DIJVR SECTON
INF0Rh1ATl0td PROCESS! VG UNIT
Permit Date_ 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3
—C:

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TrO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics Into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print nam )
Title (Print title)
0/- 3
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format "<XX m L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
LJ No discharge this period?`
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or,
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief; true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Permit Date: 11/1/2012-10/31/2017
_'?- —
jDate)
SWU-245, last revised 10/25/2012
Page 3 of 3

k*4 n
CDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit; httn://nortal,ncdenr.org(web/wq/wsIsulnndessw#ttaL-4
Permit No.: or Certificate of Coverage No.. Nf/L/LI-1—/—/_/—/_/
Facility Name:
County:
Inspector:
Date of Inspection:
Time of Inspection:
Phone No,
Total Event Precipitation (inches):--.,. 3 F _
Was this a "Representative Storm Event' or "Measureable Storm Event" as defined by the permit?
(See information below.)
0 Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event roust have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
Page 1 of 2
54VI1-242, bast modified 10/25/2012

1. Outfall Description: r
Outfall No. 5P4-t Structure (pipe, ditch, etc.) _s.�l Gam_
Receiving Stream: 4 r' r
Describe the industrial ac ivities that occur within the outfall drainage area: d
Clrrs rrn r-5
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: El L& - - ( t S
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 1-4 1 D
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
'10 2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
� 22 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
2 3 4 5
7. Is there any foam in the stormwater discharge? Yeso
8. is there an oil sheen in the stormwater discharge? Yes
9. is there evidence of erosion or deposition at the outfall? Yes
10. other Obvious Indicators of Stormwater Pollution:
List and describe
Note. Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant farther investigation.
Pagc 2 of 2
SWU-242, Last modified 10/25/2012

aceAnaiXical o
www.pacelabs.com
May 13, 2015
Mr. Johnny Baines
Eastern Environmental Management
PO Box 4030
518 S. Pearl Street
Rocky Mount, NC 27803
RE: Project: SPX SEMIANNUAL
Pace Project No.: 92247861
Dear Mr. Baines:
Pace Analytical Services, Inc.
9800 Kincey Ave. suite ioo
Huniersvifle, NC 28070
Enclosed are the analytical results for sample(s) received by the laboratory on May 01, 2015. The
results relate only to the samples included in this report, Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring for
Angela Baioni
[e-mail]
Project Manager
Endosures
cc: Ms. Cathy Baines, Eastern Environmental Management
REPORT OF LABORATORY ANALYSIS
This report shall not be teproduced, except In tub,
without the written consent of Pace Analytical Services, Inc.
[phone]
Page 1 of 13

aceAnalytical
WmPaceraes.wm
Project: SPX SEMI ANNUAL
Pace Project No.: 92247861
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
HunlsrsviRe, NC 28078
[phone]
Charlotto Cartlffcation IDs
9800 Kincoy Ava. Ste 100, Huntersvllle, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certificatfon IDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina Dtinking Water Certification #: 37712
CERTIFICATIONS
FlorldalNEIAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Vlrginia[VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VrginiaNELAP Certification k 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent or Pace Analytical Services, Inc.. Page 2 of 13

leAnalytical
wnttpecermu m
SAMPLE ANALYTE COUNT
Project: SPX SEMI ANNUAL
Pace Project No.: 92247861
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytts
. Roportod
Laboratory
92247861001 SDD1 EPA 16646
CLW
1
PASI-C
EPA 8082
SWB
8
PASI-C
SM 2540❑
WRC
1
PASI-A
TKN+NO3+NO2 Calculallon
EWS
1
PASI-A
EPA351.2
JDA
1
PASI-A
EPA353.2
DMN
3
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be repiuduced, except in lull,
without the written consent of Pnce Analytical Services, Inc.. Page 3 of 13

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28070
[phone]
Project: SPXSEMIANNUAL
Pace Project No.: 92247861
Sample: SD01 Lab ID: 92247861001 Collected: 04/30/15 08:15 Received: 05/01/15 10:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
HEM, 011 and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND m911-
5,0
1 05105/15 12:30
8082 GCS PCB
Analytical Method: EPA 8082 Preparation Method: EPA 3510
PCB-1018 (Aroclor 1016)
ND ug/L
0150
1 05/09/15 14:33 06/12/15 10:37
12674-11-2 tit
PCB-1221 (Aroetor 1221)
ND ug/L
0.50
1 05/09/15 14:33 0511211510:3T
11104-28-2 H2
PCB-1232 (Aroclor 1232)
NO uglL_
0,50
1 05109/15 14:33 05/12115 10:37
11141-16-5 H2
PCB-1242 (Aroclor 1242)
ND ug/L
0.50
1 05/09/16 14:33 05/12/15 10:37
53469-21-9 H2
PCB-1248 (Arocior 1248)
ND uglL
0.50
1 05/09/15 14;33 05/12/15 10:37
12672-29.6 H2
PCB-1254 (Afadar 1254)
ND uglL
0.50
1 05/09/15 14;33 05/12/15 10:37
11097-69-1 H2
PCB-1260 (Aroclor 1260)
ND uglL
0,50
1 05/09115 14:33 05/12/15 10:37
11096-82-5 H2
Surrogates
Decachloroblphenyl (5)
58 %
10-132
1 05109/15 14:33 05/12/15 10,37
2051-24-3
2540D Total Suspended Solids
Analytical Method: 5M 2540D
Total Suspended Solids
15.7 mg1L
4.2
1 05/04115 21:56
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Total Nitrogen
0.41 mg/L
0.12
1 05111/15 16:46
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
ND mglL
0,50
1 05/10/15 11;23
7727-37-9
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: CPA 353.2
Nitrogen, Nitrate
0.41 mg/L
0.020
1 05/01/15 23:47
Nitrogen, Nlldle
ND mglL
M020
1 05/01/15 23:47
Nitrogen, NO2 plus NO3
0.41 mg1L
0.020
1 05/01/15 23:47
Date: 05/1312015 08:05 AM
REPORT OF LABORATORY ANALYSIS
This report shatl not be reproduced, except in full,
without the written consent of Pace Analytical Servlccs, Inc..
Page 4 of 13

aceAnalytical"
+t+vwpectdabscom
QUALITY CONTROL DATA
Project: SPX SEMI ANNUAL
Pace Project No.: 92247861
QC Batch: GCSV/21189 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92247861001
METHOD BLANK: 1450156
Associated Lab Samples: 92247861001
Parameter Units
Oil and Grease mglL
LABORATORY CONTROL SAMPLE: 1450157
Parameter Units
Oil and Gresso mg/L
Pace Analytical Services, Inc.
9800 KinceyAve, Suite too
Huntersville, NC 20078
(704)B75-9092
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 0510511512:18
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 33.4 84 78-114
MATRIX SPIKE SAMPLE: 1450158
92247532004 Spike MS MS e% Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mglL ND 40 37.2 93 78-114
Results presented oa this page ere In the units Inarcaled by the'I1nNs" column except where on alternate unit Is presented to ttle right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fu8,
Dale: 05/13/2015 08:05 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 13

aceAna46cal
www pacelehs.cam
QUALITY CONTROL DATA
Project: SPX SEMIANNUAL
Pace Project No.: 92247861
QC Batch: OEXT134937 Analysis Method: EPA 8082
QC Batch Method: EPA 3510 Analysis Description: 8082 GCS PCB
Associated Lab Samples: 92247861001
METHOD BLANK: 1455119
Associated Lab Samples: 92247861001
Parameter
Units
PCB-1016 (Aroclor 1016)
u91L
PCB-1221 (Aroclor 1221)
ug1L
PCB-1232 (Aroclor 1232)
ug/L
PCB-1242 (Aroclor 1242)
ud/L
PCB-1248 (Aroclor 1248)
ug1L
PCB-1254 (Aroclor 1254)
ug1L
PCB-1260 (Aroclor 1260)
ug1L
Decachlorobiphenyl (S)
%
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
0.50
05/12115 04:46
ND
0.50
05112/15 04:46
ND
0.50
05/12115 04:46
ND
0.50
05/12115 04:46
ND
0.50
05/12115 04:46
ND
0.50
05/12/15 04:46
ND
0.50
05M2115 04A6
70
10-132
05112115 04:46
LABORATORY CONTROL SAMPLE & LCSD:
1455120
1455121
Spike
LCS LCSD
t-CS
LCSD
e% Rec Max
Parameter
Units Conc.
Result Result
e% Rec
% Rec
Ltmlts RPD RPD Qualifiers
PCB-1016 (Aroclor 1016)
ug/L 5
4.2 4.2
85
84
50-150 2 30
PCB-1260 (Arocior 1260)
ug1L 5
3.4 37
68
74
50-150 8 30
Decachtorobiphenyl (S)
%
62
68
10-132
Results preaented on this page an In the units indicated by the 'units" column except where an alternate unit Is presented to the right of the reauit.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/13/2015 08:05AM without the written consent of Pace Analytical Services, Inc..
Page 6 o1 13

aceAnalytical
rowwpacefabs.com
Project: SPX SEMI ANNUAL
Pace Project Na.: 92247861
QC Batch: WET137226
OC Batch Method: SM 2540D
Associated Lab Samples: 92247861001
METHOD BLANK: 1449805
Associated Lab Samples: 92247861001
Parameter
Units
Total Suspended Solids
mglL
LABORATORY CONTROL SAMPLE: 1449806
Parameter
Units
Total Suspended Solids
my1L
SAMPLE DUPLICATE: 1449807
Parameter
Units
Total Suspended Solids
mg1L
SAMPLE DUPLICATE: 1449608
Parameter
Units
Total Suspended Solids
mglL
Pace Analytical Sorvlcos, Inc.
9800 Klncey Avo. Suite 100
Huntersvllle, NC 28076
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 051D4/15 21:51
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 226 90 90-110
92247797001 Dup
Result Result RPD Qualifiers
ND ND
92247760001 Dup.
Result Result RPD Qualifiers
53.D 59.0 11 06
Results presented on this page are In the unlls Indlealed by the "Units" column ezt:apt where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 06113/2015 08:05 AM without the written consent cf Page Analylical Services, Ina.. Page 7 of 13

aceAnalXical.
www.pssefabs.com
QUALITY CONTROL DATA
Project: SPX SEMI ANNUAL
Pace Project No.: 92247861
QC Batch: WETA122848 Analysis Method: EPA 351.2
QC Batch Method: EPA 351.2 Analysis Description: 351,2 TKN
Associated Lab Samples: 92247861001
METHOD BLANK: 1453909 Matrix: Water
Associated Lab Samples: 92247861001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg1L NO 0.50 05/10/15 11:16
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
liuntersville, NO 2a078
[phone]
LABORATORY CONTROL. SAMPLE: 1453910
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg[L 10 10A 101 90-110
MATRIX SPIKE & MATRIX SPIKE OUPLICATF: 1453911 1453912
MS MSD
92248338002 Spike Spike MS MSD MS MSD % Rec
Parameter Units - Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mglL 1.8 10 10 11.5 11.2 97 94 90-110 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1453913 1453914
MS MSD
92248586001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Oual
Nitrogen, Kjeldahl, Total mg1L 15.9 10 10 27.3 26.9 114 110 9D-110 1 M1
Results presented on this page are In the unite Indicated by the "Units" column except where an alternate unit Is presented to the right of the resen,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 0511312015 08:05 AM without the wriften consent of Pace Analytical Services, Inc.. Page 8 of 13

aceAnalytical
rmw.ptroelahaoom
QUALITY CONTROL DATA
Project: SPX SEMI ANNUAL
Pace Project No.: 92247861
Pace Analytical Servtcas, Inc.
9800 KlnceyAve. Suite 100
Hunleri;Wle, NC 28078
(704)e75-9092
QC Batch: WETA/22781
Analysis Method: EPA 353.2
QC Balch Method: EPA 353.2
Analysis Description: 353.2
Nitrate + Nitrite, Unpres.
Associated Lab Samples: 92247861001
METHOD BLANK: 1448938
Matrix: Water
Associated Lab Samples: 92247861001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg1L
ND 0,020
05/01/15 23:44
Nitrogen, Nitrite
mglL
ND 0.020
05101/15 23:44
Nitrogen, NO2 plus NO3
mgfL
ND 0,020
05/01/15 23:44
LABORATORY CONTROL SAMPLE: 1448939
Spike LCS
LCS % Rec
Parameter
Units
Conn, Result
% Rec Limits Qualifem
Nitrogen, Nitrate
mglL
2.5 2.5
100 90-110
Nitrogen, Nitrite
rng1L
1 1.0
101 90-110
Nitrogen, NO2 plus NO3
mg1L
2.5 2.5
100 90-110
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1448940 1448941
MS MSD
92247861001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units
Result
Conc. Conc. Result
Result e% Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate mg1L
0.41
2.5 2.5 2.9
2.9 101 100
90-110 0
Nitrogen, Nitrite mg1L
ND
1 1 1.0
1.1 104 105
90-110 1
Nitrogen, NO2 plus NO3 mg/L
0,41
2.5 2.5 2.9
2.9 101 100
90-110 0
ResLdta presented on this page are In the units Indicated try the 'Unite' column except where an alternate unit Is presented to the right at the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05113/2015 08:05 AM Without the written consent or Pnce Arinlytical Services, Inc.. Page 9 of 13

aceAnalytical o
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QUALIFIERS
Project: SPX SEMI ANNUAL
Pace Project No.: 92247881
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusled Method Detection Limit.
PQL - Practical Quantitalion Limit.
RL - Reporting Limit.
Pace Analytical Sarvices, Inc.
9800 Kincey Ave. Suite 100
Hunterswlte, NC 28070
[phone]
S - Surrogate
1,2-Dlphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concontration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gal - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, end Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acroleln and Acrylonitrile by EPA
Method 8260.
N-Nitrosodtphonylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical Is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN - The NEI.AC Institute.
LABORATOWES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
112 Extraction or preparation conducted outside EPA method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/1312015 08:05 AM without the written consent 0 Pace Analytical Services, Inc„ Page 10 of 13

aceAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SPX SEMIANNUAL
Pace Project No.: 92247861
PareAnelyticel Services, Inc.
9800 Kincey Ave. Svlte 100
Huntersvills, NC 28078
[phone]
Lab 10
Sample lD
QC Batch Method
QC Batch Analytical Method
92247861001
8D01
EPA 1664B
GCSVl21189
92247861001
SD01
EPAS510
OEXT134937 EPA8082
92247861001
SD01
SM 2540❑
WET137226
92247861001
S1301
TKN+NO3+NO2
WET137383
Calculation
97247861001
8001
EPA351.2
WETAl22848
92247B61001
S001
EPA 353.2
VVETA122781
•Date; 05113/2015 08:D5 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In Tull,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
GCSV121267
Page 11 of 13

� '=Analyflcar"
Document Name:
Condition Upon Roo
R-CS-003-rev.15
Document Revised: Septemuer 11. zui4
Pace 1 of 2
Client Name:�t:V eofth �-iy,,j 2
Courier: ❑ Fod- x ❑ UPS❑ USPS❑ Client��no
rnmerctal❑ Pace Other
Custody Seal on Cooler/Box Present: ❑ yes Seals intact: ❑ yes ❑ no
ace Huntersvllle Quality Office
Packing Material: ❑ Bubble V[kp E2fu I ags ❑ None ❑ Other
Thermometer Used: IR Gun T1401 Typo of too:, doe[ Blue None Samples on Ice, cooling process has begun
Temn Cerractinn Factor T1401 No Corrantlnn
Corrected Cooler Temp.: 'C
Tamp should be above freezing to WC
Biological Tissue is Frozen; Yes No
g
Comments.
Date and Initials p rs r e Wining
contents: '
Chain of Custody Present;
Y ONO
❑NIA
1.
Chain of Custody Filled Out:
ZVI ONO,,
❑N/A
2.
Chain of Custody Relinquished:
Yas o
❑NIA
3.
Sampler flame & Signature on COG:
—Zye a ONO
❑NIA
4.
Sam les Arrived within Hold Time:
VfyX LINo
L1NIA
6,
Short Hold Tlme Analysis a72hr :
dyes'OtW
❑NIA
6.
Rush Turn Around Time Requested:
❑Y a 141,10
ONIA
7.
Sufficient Volume;
Y ❑No
❑NIA
8.
Correct Containers Used,
-Pace Containers Used:
s ❑No
ZyaC1No
❑NIA
❑NIA
9,
Containers Intact:
Yea ❑No
EIN/6
10,
Filtered volume received for Dissolved tests
fay, ©No
UfNIA
11.
Sample Labels match COC:
-Includes date/tlmellD/Anal sis Matrix;
Yca []No
DWA
12.
All containers needing preservaton have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendatlon.
exeo !Ions: VOA,celiforrn. TOC, O&G, Wf-DRO (water)
EI/Yea ❑No
a ❑No
Zee❑ No
❑NIA
11NIA
13.
Samples checked for dechlorinaVon:
11Y83 ONO
ljw
14,
Heads ace in VOA Vials ;�6mm :
DYes ❑No
NI
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # if urchase
❑Yaa ❑No
[]Yes ONO
N
16,
Ghent Notification/ Resolution: Field Data Required? Y 1 N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF RevleW; Date:
SRF RBview: Date:
Note; Whenever there Is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( Le out of hold, Incorrect preservative, out of tomp,
Incorrect containers)
woe: ezza7aei
li�ip�p im mmu
-Tage 12 or 13

�.f'3CE'Af131yt1C31'
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chaim-of-Crss" is a LEGAL DOCUMENT. All rei&=l fields must be ewn* d a— a%4y.
Section A Section B Section C
Page: � of
f
Requimd CFent tnfarmWow Required Prged InfamO&G lnvO= lnfvrrtSY
RePcd TD:��y�
14 4 95
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REGU RY AGENCY
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Putd+asc Order No:
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ProjEGt Nsme;
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Para
�*
Si Location
Requested Due Date/TAT-
Project Number.
oca Froua ;
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STATE:
RegUested
AnalysiS
Filtered
(YIN)
Seeson II Matrix Codes
x
Rwuki dCk" Womayon r.fAMIX r CODE
COLLECT D
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Waste Water %%W
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Prod U P
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SAMPLE ID wpe OL
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(A-Z. 0-9 ! Air AR
Sample IDs MUST 8E UNIQUE
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Tissue TS
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