NCG030012_MONITORING INFO_20170417

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/V uc -C) 3 bbl 01'.
DOC TYPE
❑ HISTORICAL FILE
[�-- MONITORING REPORTS
DOC DATE
❑ D\0 ( -�u � I
YYYYM M DD

hcC�-o 30o
March 7, 2017 `_"
p�AR 13 201i
Laura Alexander i};d_LA l`IO QUALITY
NCDEQ �,() r,"MV14, AI ER PERNiITTING
Division of Storm Water
1612 Mail Service Center
Raleigh, North Carolina 27699-1626
Attn: Storm Water Permit Program
SUBJ: Biannual Storm Water Sampling-lst Half 2017
Dear Ms. Alexander:
APR 17 2017
CENTRAL FILES
DWR SECTION
Enclosed is a paper copy of Magneti Marelli's Storm Water Discharge Outfall (SDO) Monitoring
Report with lab analysis attached. Outfall #001 was inspected and sampling subsequent to a
qualifying rain event when there was flow from the discharge pipe (Pipe 02). Mr. James Siler
pulled the sample for TSS, pH, Metals (Copper, Lead and Zinc), and Oil & Grease. On -site
observation was also documented. The flow was a clear in color with minimum floating or
suspended solids.
Review of the analytical data indicates all parameters were below our benchmark limits as
identified in our NPDES permit with the exception of zinc which was at the benchmark limit of
0.007 mg/l.
Should you have any questions, please do not hesitate to contact me at [phone].
Sincerely,
atherine Thomas-Grazioli
Environmental Manager
Magneti Marelli PWT LLC
[phone]
Cc: File

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STORMWATER DISCHARGE OUTFALL (SDO)
QUALITATIVE MONITORING REPORT
BMP Checklist #6
NPDES PERMIT NO.
FACILITY: Am
COUNTY: L ,p
PHONE:
INSPECTOR: �Ccr•rE S to. 5 - f `�,/L-
DATE: ! 1 0t 7
OUTFALL No.
SDO-00_
OUTFALL TYPE-
"s INLET PIPE t) FLUME�-
RECE G STREAM:
4 Wet weather observation C1 Dry weather observation
+ Flow during dry weather tj No flow during dry weather tt Standing water during dry weather,
Describe the Industrial activities occurring within the outfali drainage area.
COLOR - Describe the discharge color (e.g. red, brown, green, blue) and tint (e.g., light, medium, dark).
ODOR - Describe any distinct odors (e.g. gasoline, rotten eggs, chlorine) the discharge may have.
CLARITY - Choose the number that best ranks the clarity of the discharge, where 1 is clear and 16 is very
cloudy.
1 2 � 4 b 6 7 8 9 10
FLOATING SOLIDS - Choose the number that best ranks the amount of floating solids in the discharge,
where 1 is no solids and 10 is the su a covered with floating solids.
1 2 ) 4 5 6 7 8 9 10
SUSPENDED SOLIDS - Choose the number that best ranks the amount of suspended solids in the discharge,
where 1 Is no solids and 10 is ely muddy..
1 3 4 5 6 7 8 9 10
FOAM, -
Is there any foam on or in the stormwater discharge? yes
OIL SHEEN -
Is there oil sheen visible in the stormwater discharge or at the outfall? yes
DEPOSITION AT OUTFALL -
Are there sediment or other material deposits below the outfali? yes r�
EROSION AT OUTFALL -
Is there erosion at or immediately below the outfali? yes
list and describe other obvious indicators of stormwater pollution:
By this signature, I certify that this report is accurate and co nto the best of rn no ge:
' C�A
Permittee's Signature Ins ctars Signature

219 S. Steele Str.
Sanford, NC 27330
Phone: [phone]
Cameron Testing Services, Inc.
NC WW/GW Cert. #654 NC PH14S Cert # 37799 US EPA NC01918
Chan} of Custody
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Cameron Testing Services, Inc. Laboratory Report
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Magneti-Marellio��ct January 2017 StormwaterRegalt
Sample Information
sampled x J. SilerMwDal�` 01/03/17 ReceLved
Analyses and Results
Stormwater sw cr
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J NC DENR #654
NC PHHS #37799
US EPA #NC01918
170002:
Yes
S. Bullard
02
Stormwater sw Gr
pH
6.70 S. U. 0 01/04/17
TSS
<4.17 mg/L 4.17 01/05/17
03
Stormwater sw cr
Metals
mglL 0
Metals (Cu, Zn, Pb) analyzed by FAL, Durham, NC; report attached.
4500 H B - pH
2540 D - TSS
EPA 200.8
Report
Review_
Lab Director Date
i
219 S. Steele Str. 919-208-4240
Sanford NC 27330 '[e-mail]

FIRST ANALYTICAL LABORATORIES
b""'19 PO Box 110372 - Research Triangle Park. NC 27709 �-. 9l9 942 $((i7
�0'45'n'K 4620 Industry Lane, Suite 8 -Durham, NC 27713 FAX [phone]
n1�lr.fustanal� ticallalCc cunt
FAIL Project #:
1701009.1
Report Date:';, 1/16/2017
Client:
Cameron Testing Services
Date Received: 1/5/2017
Client Project ID:
170002
Sample !Name:
170002-01 Stormwater
Concentration in Original Sample
Conc.
RL
Analyte
(mg/L)
(mg/L)
Copper (Cu)
0.007
0.001
Zinc (Zn)
0.036
0.005
Lead (Pb)
< 0.001
0.001
Approved by:
Matt Loftis, Laboratory Manager

219 S. Steele Str. Cameron Testing Services, Inc. Chalof Custody
Sanford, NC 27330 NC WW/GW Cert. #654 NC PHHS Cert # 37799 US EPA NCO1918 Page / of
Phone: [phone]_
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PPT-A
CCU RATE -RELIABLE
LABORATORIES, INC
WWW.PARLABS.COM
Attn: KURT CRANSON
TRANE CHARLOTTE
4500 MORRIS FIELD DR.
CHARLOTTE, NC 28208-
�n
REPORT OF ANALYSES
o
PROJECT NAME: NOV 15
DATE: 11/25/15
SAMPLE NUMBER-
121414
SAMPLE ID- TRC OUTFALL C
SAMPLE MATRIX- WW
DATE SAMPLED-
TIME SAMPLED- 0800
DATE RECEiV; D-
1 1 / 1 9/ 1'
SAM!-'LER- KC
RECEIVED BY- DJ
TIME RECEIVED-
1330
DELIVERED BY- TB
TYPE SAMPLE- Grab
Page I or 1
ANALYSIS
ANALYSIS
METHOD
DATE
TIME
BY
RESULT UNITS
pH VALUE
SM 450OH-B
11/19/15
0800
KC
6.62 units
OIL & GREASE
EPA 1664
11/21/15
1530
CT
< 5.4 mg/L
TOTAL SUSPENDED SOLIDS
SM 2540 D
11/23/15
0805
DJ
< 2.5 mg/L
COPPER, TOTAL
EPA 200.7
11/21/15
1028
CT
0.020 mg/L
LEAD, TOTAL
EPA 200.7
11/21/15
1521
CT
0.004 mg/L
7,TNC, TOTAT,
EPA 200.7
11/2.0/15
1839
CT
0.042 mg/L
i
LABORATORY DIRECTOR
P.O. Box 4 1483 • Charlotte, NC 28241-1483
Phone: [phone] • Fax: [phone]

SJ'O,RiYnVATU1'jz UlSCHAIa :)UTFALL (SDO)
MONITORING hol'ORT
GENERAL PERMIT NO. NCG210000 SAMPLES COLLECTED DURING CALENDAR YEAR: Z0--L-S-
CERTIFICATE OF COVERAGE NO. NCG211�11zflli]® (`Phis monitoring report is due at the Division no later than 30 dabs from
the dale the facility receives the sampling results from (lie laboratory.)
FACILITY NAME
PERSON COLLECTING SAM'I ES.—__�
CERTIFIED LABORATORY �„c� . l _ _ Lab # 33--LR
Lab #
Part A: Specific Monitoring Requirements'
UNTY
8R EI V EIVINONE NO. (0LQ--) V rt&' a633
DEC 0 2 2015PLEASE SIGN ON THE REVERSE 4
CENTRAL FILES
DWR SECTION
Outfall
No.
Date
Sample Collected;.
mo/dd/ r ..
Total Rainfall,
inches
00530
00400
00340
Total Suspended Solids,
ti ' L : ....
pH,
Standard units
Chemical Oxy�geri Demand (Cobb
ni
Benchmark*.
-
-
100
Within 6:0 = 9.0
.120
3
�.3
• o
'Monitoring is required only if the facility stores exposed piles of sawdust, wood chips, bark, mulch, or other similar material on site for longer than seven (/) days.
If the facility elects not to monitor because accumulated material is removed within seven (7) days or less, the certification below must be signed. The facility shall
also record and maintain a log in its SPPP (Stormwater Pollution Prevention Plan) of dates when material is generated and removed, how, and by whom.
*Note: If you report a value in excess of the benchmark value, or outside the benchmark range (for pH), you must implement Tier 1 or Tier 2 responses in the General Permit.
Facilities that do not store exposed (either exposed to incident precipitation or exposed to stormwater run on) piles of sawdust, wood chips, bark, mulch, or other similar material for
longer than seven (7) days on site may so certify, and the requirement for analytical monitoring may be waived. For those facilities that qualify for the analytical monitoring waiver, the
discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit requirement for
analytical monitoring, I certify that to the best of my knowledge and belief, no piles of sawdust, wood chips, bark, mulch or
other similar materials were stored exposed (either to incident precipitation or to stormwater nun on) for longer than seven (7)
days before removal since filing the last discharge monitoring report."
Name (Print name)
Title (Print title)
(Signature)
(Date)
S W U-245-072808
Page 1 of 2

('I,ONNiW/'i,l,Rk 1)� �AI1,(;I(;(')UF F,l1,1,(',1)O)
iVIONITOR N(; flKTORT
"I certify, under penalty of law, that this docuu►ent and all attachn►ents were prepared under my direction or supervision in accordance with a
system dcsigucd to assw-o that qualitled pursotu►el properly gather and evaluate the information submitted. Based on my inyuirl' of the person
or persons who mamage the system, or those persons directly responsible for gathering the information, the information submitted is, to the host
of my knowledge and belief, true, accurate, and complete, I am aware (hat there arc significant p(malties for subnutting false information,
inciudill g.thc possibility of fines and imprisonn►cnt for knowing violations,"
tI-Bo -IS
(Signature of er Iittcc) (Date)
Form SWU-254-071400
Page 2 of 2

I✓
1.
2.
4.
5.
6.
7.
8.
aol5'
EDNCG030012 (:
DIRECTIONS FOR MAKING WET WEATHER VISUAL OBSERVATIONS
Wait for a storm event that has been preceded by at least 72 hours of dry weather.
Once rainfall starts, mobilize to the outfall observation point. Wait for discharge to begin. There
will be a lag between the initial rainfall and discharge commencing. The lag is a function of the
drainage area characteristics and rainfall intensity. For example, flat sites with no pavement
respond slowly to rainfall. Pavement and slope increases the runoff rate.
Protect the observer from flash floods and lightening.
Let the discharge flow for about ten (10) to fifteen (15) minutes.
Collect some discharge flow water (about 0.5 liter) into a clear glass container.
Make the observations (see BMP Checklist #6) and record the findings. Ensure adequate
lighting.
Insert completed BMP Checklist #6 into Appendix F.
If observations indicate pollution problem, implement appropriate BMP.
STORMINATER DISCHARGE OOTFALL (SDO)
QUALITATIVE MONITORING REPORT
'8MP Checklist #6
NPDESPERdAITNO. NCt;;D3t6uG FACILITY: Nl/jCNCJ-1 /1lgr4.i '
COUNTY: �..Q.e,i
PHONE: 7174-G�{Ili
INSPECTOR: ,Sa„qj�; yv,g,' Y
DATE:
OUTFACE No. OUTFACE TYPE: " STREAM:
46
SDO-00 ( ❑INLET �PfP[ '7F7UME
Wot weather obsomtlon G Dry wcamar obsemtlon
`J Flow during dry vroatltor ii No flow during dry vmathar f; Standing vrstor during dry weather
Describe the Industrial activities occurring within the outtall drainage area.
COLOR • lhraerihe the discharge color (e.g. rod, brov!r% groan, e7uo) and tlM (o.g.. IighL medium, dark}.
ODOR • oosuitro any distinct odors (e.g. gasoline, moan eggs, chlorine) the discharge may have. _ -
Na�l4'
CLARITY - Choose the number that bast ranks the clarity. of the discharge, where 1 Is clear and 10 is very
cloudy.
12 3 4 5 6 7 8 9 10
FLOATING SOLIDS •Choose the number that hest ranks the amount of floating solids In the discharge.
wham t is no solids and /0 surface covered with floating solids.
1 2 3 4 5 8 7 8 9 70
SUSPENDED SOLIDS - Choose the number that Mast rooks the amount of suspended aaiMs In the dluMrge,
wham 1 is no aotlda and 10 Is aly muddy.
t 2_ 3 4 5 6 7 8 9 LO
FOAM.
Is them any Loam on or In the atonnwatar discharge? yes
OIL SHEEN•to them all shoan visible In the stormwatar discharge or at the oudalt7 you
DEPOSITION AT OIRiALL -
Are them sediment or other material depoalto below the outtsll7 yea
EROSION AT OUTFACE -
b tlroro erosion at or Immediately tabor the outla0? yes
LIat and describe Otl10f ODVIOUa Indicators of atOfOlwatef Po{iWOn:
BY this afgnahi'o, I certify that this report Is accurate and nte to the my e:
Perrniffee's Signature t s Sgneture
Magneti Marelli USA, Inc.
Appendix B
Storinwater Pollution Prevention Plan
Page B-5

FIRST ANALYTICAL LABORATORIES
TEL ?)19942S667
tdllnnr P;I Rae 110372 -Research Triangle Park. N(' 2770!) FXX 40 882 10)3
a1�i�nrg -i l - Precin�n Dr'ne. St utr I Ql - IZalcJt. Plc'" _'b l - 111\1C..111il�:1UU1171�aI I1LM l'MII
EPAMethod 200 Analysis Report
FAL Project #: 150825.1 Report Date: 8/18/2015
Client: Cameron Testing Services Date Received: 8/7/2015
Client Project ID: 151094
Sample Name: 151094-03 - Magneti-Stormwater
Concentration in Original Sample
Conc.
RL
Analyte
(mg/L)
(mg/L)
Lead (Pb)
0.004
0.001
Copper (Cu)
0.021
0.001
Zinc (Zn)
0.152
0.005
Approved by:
Matt Loftis, Laboratory Manager

October 27, 2015
Laura Alexander
NCDEQ
Division of Storm Water
1612 Mail Service Center
Raleigh, North Carolina 27699-1626
Attn: Storm Water Permit Program
SUBJ: Biannual Storm Water Sampling-2nd Half 2015
Dear Ms. Alexander:
Enclosed is a paper copy of Magneti Marelli's Storm Water Discharge Outfall (SDO) Monitoring
Report with lab analysis attached. Outfall #001 was checked on 8/7/2015 during a rain event
when there was flow from the discharge pipe (Pipe 02). Mr. James Siler pulled the sample for
TSS, pH, Metals (Copper, Lead and Zinc), and Oil & Grease. On -site observation was also
taken. The flow was a medium brown in color without any floating or suspended solids.
Review of the analytical data indicates all parameters were below our benchmark limits as
identified in our NPDES permit with the exception of Zinc at 0.152 mg/L and Copper at 0.021
mg/L. We have previously instituted a Tier I plan and will review our Best Management
Practices as well as historical soil samples collected to identify background Zinc and Copper
concentrations in the soil. The next scheduled Semi -Annual Storm Water Sampling event is
scheduled for the first quarter 2016. Should concentrations of Zinc and Copper continue to be
present above NPDES benchmark limits, Magneti Marelli shall institute Tier Il provisions.
This report contains carefully prepared data, as factual and accurate as possible. Should you have
any questions, please do not hesitate to contact me.
Sincerely,
Catherine Thomas-Grazioli
Environmental Manager
Magneti Marelli PWT LLC
[phone]
Magneti Marelli Powertrain USA LLC
2101 Nash Street
P,O. Box 548
Sanford. NC 27331-0548
Phone: [phone]
Fax: (9,19) 775-6332

Cameron Testing Services, Inc. Laboratory Report NC DENR WA
NC PHHS #37799
t^ US EPA #NC01918
I agneti-Marelli a 151094
j'. �.. .� n yr a �
August 2015 Stormwater�'Regu!®eaas► Yes
Sample Information
p:z spat. Z i �.
I.. Stanpled J. biter C "Date 08/07/16 I'Recetvetl` A Miller 'beta' 08/07/15
Analyses and Results
t La5',1!? ate, i s {lip Aflatyte Result s�C '�, 2a 181K td
SR
151094 01 Stormwater sw G, 08G-W < 6 matt 6 08/17/15 EPA 16W
02 Stormwater ww G, pH 6.04 s..u. 0 08/17115 4500 H B - pH
TSS 16.7 mak 2.94 D8113/15 2540 D - TSS
03 Stormwater +W G, Metals Mj#L 0 EPA 200.8
Metals (Cu, Zn, Al) analyzed by First Analytical Labs, RTP, NC; report
attached.
Report
Rwdiew
Lab Direct" Date
219 S. Steele Sir_
Sanford NC 27330
919-209 4240
c>rks@camewtefin$.wm

219 S. Steele Sir,
Sanford, NC 27330
Phone.' 919-208-4240
Cameron Testing Services, Inc.
NC WW/0W Cart. #654 NC PHH3 Cert,# 37799 US EPA NC01918
Chain of Custody
Page I_ _ - of
cont
,
Rush work will require prior approval. Additional charges will apply

4&
NEt,
0-
aA
25, 2015
Mr. David Parnell
NCDENR
Division of Energy, Mineral and Land Resources
1628 Mail Service Center
Raleigh, North Carolina 27699-1626
SUBJ: Biannual Storm Water Sampling-l" Half 2015
Dear Mr. Parnell:
NC DENR 9h Regk*W oft
Enclosed is a paper copy of Magneti Marelli's Storm Water Discharge Outfall (SDO) Monitoring
Report with lab analysis attached. Outfall #001 was checked on 2/10/2015 during a rain event
when there was flow from the discharge pipe (Pipe 02). Mr. James Siler pulled the sample for
TSS, pH, Metals (Copper, Lead and Zinc), and Oil & Grease. Onsite observation was also taken.
The flow was a medium brown in color without any floating or suspended solids.
Review of the analytical data indicates all parameters were below our permit limits.
This report contains carefully prepared data, as factual and accurate as possible. Should you have
any questions, please do not hesitate to contact me.
incerely,
r
r�
atherine Thomas-Grazioli
Environmental Manager
Magneti Marelli PWT LLC
[phone]
Magneti Marelli Powertrain USA LLC
2101 Nash Street
P.O. Box 548
SanfordNC 27331.0548
Phone:i919)776-4111
Fax: [phone]

Lin

STORMWATER DISCHARGE OUTFALL (WO)
QUALITATIVE MONITORING REPORT
BMP Checklist #B
NODES PERMIT NO. Nc . QiD000
FACILITY:
COUNTY: e�
PHONE:
INSPECTOR: 3q �,� 6S . _ . -
DATE:
QUTFALL No.
SDO-00
OUTFALL'fYPEc
0INLET �!i'IPE 11 FLUME
RECEIVING STREAM:
L � C.K :, C �QR.r
S.Aet weather obsarvatlon t7 Or waather observation
V Flow during dry weather U No flow during dry weather C1 Starting wetor during .dry wsath®r
Describe the industrial ad:"des occurring within the outfall drainage area.
COLOR - Dosci(W'the discharge color (e.g. red, brown, green, blue) and tint (o.g.; light, modlum, dlarki.
ODOR - Describe any distinct odors'(o.g. pasoiMo; rotton eggs, chlorine)'the'disd:haige may have.
CLARITY - Choose the number that boat ranks the clarhy of the discharge, where 1 Is clear and 10 is very
cloudy.
1 2 3 4. 5 6 7 8 9 10
FLOATING SOLIDS - Choose the number that best ranks the amount of floating solids in the discharge,
where 1 is no solids and 10 is surface covered with floating solids.
1 3 4 5 6 7 6 9 10 .
SUSPENDED SOLIDS - Choose the number that best ranks the amount of suspended solids In the discharge,
wham 1 Is no solids and 10 is sly muddy.
t 3 4 5 6 7 6 9 10
-
FOAM WrN
Is there any foam on or in the stormwater discharge? yes
OIL SHEEN -
to there oil sheen vtsibto in the stormwator discharge or at the outfall? yea o .
DEPOSITION AT OUTFALL - .�
Ara there sedimont or, otter material deposits below the outfali? yes
EROSION AT OUTFAL.L. -
Is there erosion at or lmmediategt below the ouftl? yes no
List and describe other obvious indicators of stormwater pQilutiem.
By this signature, I codify that this report Is accureto and complete to the best of my .owIpd
tuie Permittee's Signature lrrspectoYs igna

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Cameron Testing Services, Inc. Laboratory Report
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Client -p, Mal hertiWairelli "C MP
lr"Ojl-41 150172
rN
roject:,,-,, Feb. 2015 Stormwater "'Regulatory- Yes
Sample Inform. ation
Y.
NC DENR 9654
NC Pl:ll-!S 1/37799
US EPAPNQ01918'
'.Sarn ed,. J. Siler -at
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Analyses and Results
150172 01 Outfall sVV P, r
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'- 's-0-Me'thods
Analyte—
E>^—
"kdfCrende
TSS
M 11, 417 -`TSS
9 02110115 2540fD
pH
5.76 S. U'• 0 02/11115 450o I 18 - jpt-i
Metals
EPA 200.8
O&G-W
<5.00 mg/1- 5 02/12/15 EPA: 1664A
Metals wb, Cu, Zh) analyzed by First Analyti,C21 Laboratories, RTP, NC;
report attadhed.
Report
Review
or Lab ii6clt Date
219S. Sleek Sir.
Sanli)rd'NC 27330'

1 FIRST ANALYTICAL LABORATORIES
L,I1,nG PO Boi 11072 - Research Tningle F'ark. NC•27709
slnf,purgi 7517 Precis,�ti Drive _.St�i�e:l Ol Ralai�t NC" ;Cl �i
EPA Method 200 Analysis Report
FAL Project #: 150222.1
Client: Cameron Testing Services
Client Project ID: 150172-01
Sample Name: 150172-01 Outfall
TEL 9 f 9 9=42 3667
F. Z. 919 SS?,m-0
Report Date: 2/19/2015
Date Received: 2/10/2015
Concentration in Original Sample
RL
Analyte Conc. (mg/L) (mg/L)
Copper (Cu) 0.005 0.001
Lead (Pb) 0.002 0.001
Zinc (Zn) 0.049 0.005
Approved by:
Matt Loftis, Laboratory Manager

r YDCA..!L LABORAT ORIE S 'IWIl
440.tr-"I�i T-F�Vair&xfi iplukAll .4witVil. 14c,
-ItL-4t�P4w' RM7 T :c-HAiN-OF CUS. ODY
C 116nt: 'Caefi 60, e6j- Nitfi6Aw*.-l-
Comact: Chris,Cameron
AddeOsw2'19's.,-:SfiR41a-St. San, ford;, NC.27330
orn6. t. ri S- 99 i in e to ti 5--t I tvo.Q M--
Pur,chiasejol
N*liTolab,,,-
.Colledio:m

STORMWATER DISCHARGE OUTFALL (SDO)
QUALITATIVE MONITORING REPORT
BMP Checklist #6
NPDES PERMIT NO. CC, 6 306 / �L-•
FACILITY:. /VIO
COUNTY: L
PHONE:
INSPECTOR: _- / t
DATE:
OUTFALL No.
SD0-00_1,
OUTFALL TYPE:
I G INLET ;/PIPE 111 FLUMEisT
RECEMNG STREAM: )
_I Wet weather observation 0 Dry weather observation
-I Flow during dry weather a No flow during dry weather 1 Standing water during dry weather
Describe the Industrial activities occurring within the outfall drainage area.
COLOR - Describe the discharge color (e.g. red, brown, green, blue) and tint (e.g., light, medium, dark).
C -P-6 V-
ODOR - Describe any distinct odors (e.g. gasoline, rotten eggs, chlorine) the discharge may have.
ICI b
CLARITY - Choose the number that best ranks the clarity of the discharge, where 1 is clear and 10 is very
cloudy. 1 2 1�j) 4 5 6 7 8 9 10
FLOATING SOLIDS - Choose the number that best ranks the amount of floating solids in the discharge,
where 1 is no solids and 10 is the surface covered with floating solids.
1 T 3 4 5 6 7 8 9 10
SUSPENDED SOLIDS - Choose the number that best ranks the amount of suspended solids in the discharge,
where 1 is no solids and 10 is extremely muddy.
1 3 4 5 6 7 8 9 10
FOAM -
Is there any foam on or in tha stormwater discharge? yes no
OIL SHEEN -
Is there oil sheen visible in the stormwater discharge or at the outfall? yes CIP
DEPOSITION AT OUTFALL - _
Are there sediment or other material deposits below the outfall? yes
EROSION AT OUTFALL -
Is there erosion at or immediately below the outfall? yes no
List and describe other obvious indicators of stormwater pollution:
By this signature, I certify that this report is accurate and co plate the best my k e:
Permittee's Signature U Inspec rs Signature

FIRST ANALYWAL LABORATORIES
-e,. - RVI.:%4I ell Fl..mrse V.: L., 1,;C: F CHAIN OF CUSTODY
a Am I-0
Client:
Cameron Testing Prol. Name/No: 141464-01
Contact-,
ChrU Cameron
Address:
219 S. Steefe St. Sanford, MC 27330
Phone No.
919-208-4240 enmit: cirri gRcamerontesting.cons
Purchase Order#:
Note To Lab:
I
Collection
No. Samole ID Descriotion Date Time Matrix. Presemative
Anatysis Reauired
1464.01-
Fstarmwow
111171141
1130
SW
HNO3
Cu,Pb,Zn
2
3
'4
6
7
8
10
4
-
Page of
Received Ely[
ZIA
12a e/Time-
[EN-r—
N
R011"qVW,#Q% By: Date/Tinse-
Received Lob; DatefTime:
&SOX-F&A"JI

FIRST ANALYTICAL LABORATORIES
ro 1 b;llbig: PO Box 110372 - Research Triangle Park, NC 27709 TEL: [phone]
shipping: 7517 Precision Drive, Suite 101 - Raleigh. NC 27617 FkX: 919 882 1603
«1N'cv.tu staual}-ticallibs. com
EPA Method 200 Analysis Report
FAL Project #: 141147.1
Client: Cameron Testing Services
Client Project ID: 141464-01
Sample Name: 141464-01- Stormwater
Report Date: 12/1/2014
Date Received: 11/19/2014
Concentration in Original Sample
Conc.
RL
Analyte
(mg/L)
(mg/L)
Copper (Cu)
0.015
0.001
Lead (Pb)
0.003
0.001
Zinc (Zn)
0.175
0.005
Approved by:
Matt Loftis, Laboratory Manager

a
219 S, Steele Str. Cameron TestingServices, Inc. l `� `t 5 Chain of Custody
Sanford, NC 27330
Phone: [phone] NC WW/GW Cert. #654 NC PHHS Cert # 37799 US EPA NCO1918 Page I of I
Company: • ! Magneti-Marelli
Emaii-
CTS lab use only
Siler
Phoe
919-721-1353
Samp,empContact
C
—7:.ames pro .
Address (city,.' 2101 Nash Street
Fax
Arrive: j Z
State, Zip)'
;Sanford NC 27330
Nocesi
Due:
project Istormwater Ig0q.
ZD 1,4
Regulatory.
Rush
(YIN)
Collected:. Name: N S
Signature: C
Sample jgformation
;;,
,„,. ,Numbereof•lb ttWs
-CTS Lab
}
N Ln m E J a o o
Requested Analysis
ID'
Sample ID
m E
E m
F—
V 0
Preservatives: (U)npresery H(C)I H2(S)04
(Na)Thiosulfate Na(0)H (X)Other, indicate
Outfall
ir3a rlw
— _
1 1n 1s
_ .
pH, TSS, OG, Metals Cu,Pb,Zn
c '
� I
e i uished:}t :.
Received:
Date/Time.
Rush work will require prior approval. Additional charges will apply
P�

Cameron Testing Services, Inc. Laboratory Report
NC DEN R#654
NC PHHS #37799
US EPA #NC01918
z Client:
Magneti-Marelli CTs Proj.
141464
Project.
Nov. 2014 Stormwater Regulatory
Yes
Sample Information
:SampiiW'P
J, Siler Date 11/17/14 Received:
S. Bullard
Date
11/17/14
Analyses and Results
r
ID r
Sample ID L° Analyte Result
m E
r S_td::Methods
_Lab
rEo ..
' Reference ; .
a c7
141464 01
Outfall ww Gr pH 6.24 S. U.
0
11/17/14
4500 H B - pH
TSS 29 mg1L
5
11/18/14
2540 D - TSS
O&G-W <5.00 mg1L
5
11 /17/14
EPA 1664A
Metals mgiL
o
EPA 200.8
Metals (Cu, Pb,Zn) analyzed by First Analytical Labs, RTP, NC; report
attached.
Data
Review
Lab Technician
Report
Review
Lab Direfor
219 S. Steele Sir.
Sanford NC 27330
Date
Date
919 208-4240
chriuincamcron��si � ng.cari

IAd
EI�.�I
December 19, 2014
Mr. David Parnell
NCDENR
Division of Energy, Mineral and Land Resources
1628 Mail Service Center
Raleigh, North Carolina 27699-1626
SUBJECT: Biannual Storm Water Sampling -Fall 2014
Dear Mr. Parnell:
Enclosed is a paper copy of Magneti Marelli's Storm Water Discharge Outfall (SDO) Monitoring
Report with lab analysis attached. Outfall #001 was checked on November 17, 2014 subsequent
to a significant rainfall when there was flow from the discharge pipe (Pipe 02). Mr. James Siler
pulled the sample and onsite observation was also taken. The flow was a medium brown in color
without any floating or suspended solids. In addition, a copy of the Qualitative Storm Water
Discharge Outfall Monitoring Report is attached for your records.
A review of the November sampling event, indicate that both Copper and Zinc were above the
recommended guidelines as specified in our NPDES Permit. Currently, the State of North
Carolina, Division of Hazardous Waste has approved Magneti Marelli's RCRA Investigation
Work Plan to conduct additional soil and groundwater delineation of the Former Stoddard Tank,
overflow piping sump area, Storm Sewer Manhole and SPCC Discharge Stream. Soil and
groundwater samples will be analyzed for volatile and semi -volatile organic compounds as well
as RCRA metals. Additionally, an up -gradient soil sample will be collected and analyzed to
determine if there are any off -site contaminates potentially impacting MM Sanford site.
Magneti Marelli will conduct an additional round of samples in January 2015 for analysis for
Zinc and Copper. The soil and groundwater RCRA Investigation is scheduled for the second
week of January 2015. We anticipate a better understanding of soil and groundwater conditions
upon completion of the investigation and receipt of laboratory analysis. I will keep you informed
of the investigation and subsequent results. In the short-term interim we will review our Best
Management Practices to ensure protection of storm water.
Magneti Marelli Powertrain USA LLC
2101 Nash Street
P.O. Box 548
Sanford, NC 27331.0548
Phone: [phone]
Fax: [phone]
L L

December 19, 2014
Should you have any questions, please do not hesitate to contact me.
Sincerely,
therine Thomas-Grazioli
Environmental Manager
Magneti Marelli PWT LLC
[phone]

u
cxc:aeuxmu....
May 15, 2014
Mr. David Parnell
NCDENR
Division of Energy, Mineral and Land Resources
1628 Mail Service Center
Raleigh, North Carolina 27699-1626
SUBJ: Biannual Storm Water Sampling -Spring 2014
Dear Mr. Parnell:
MAY 19 2014
Enclosed is a paper copy of Magneti Marelli's Storm Water Discharge Outfall (SDO) Monitoring
Report with lab analysis attached. Outfall #001 was checked on 2/3/2014 during a thunderstorm
when there was flow from the discharge pipe (Pipe 02). Mr. James Siler pulled the sample and
onsite observation was also taken. The flow was a medium brown in color without any floating
or suspended solids.
This report contains carefully prepared data, as factual and accurate as possible. Should you have
any questions, please do not hesitate to contact me.
Sincerely, J�
C
Catherine Thomas-Grazioli
Environmental Manager
Magneti Marelli PWT LLC
[phone]
Magneti Marelli Powertrain USA LLC
2101 Nash Street
P.O. Box 548
Sanford, NC 27331-0548
Phone: [phone]
Fax: [phone]

STORMWATER DISCHARGE OUTFALL (SRO)
QUALITATIVE MONITORING REPORT
BMP Checklist #6
PERMIT NO. Nc G d 300/ Z-
FACILITY: JUIQ c„c �{� fylQ icll �� r
_NPDES
COUNTY: L e e-,
PHONE -
INSPECTOR:
DATE: �, Z of
OUTFALL No.
OUTFALL TYPE
RECEVING STREAM: i
SDO-00�
U INLET +, IPE f I FLUME
.✓Wet weather observation (I Dry weather observation
u Flow during dry weather CJ No flow during dry weather a Standing water during dry weather
Describe the industrial activities occurring within the outfali drainage area.
COLOR - Describe the discharge color (e.g. red, brown, green, blue) and tint (e.g., light, medium, dark).
C-1
ODOR - Describe any distinct odors (e.g. gasoline, rotten eggs, chlorine) the discharge may have.
N blYL
CLARITY - Choose the number that best ranks the clarity of the discharge, where 1 is clear and 10 is very
cloudy.
1 2 11) 4 5 6 7 8 9 10
FLOATING SOLIDS - Choose the number that best ranks the amount of floating solids In the discharge,
where 1 is no solids and 10 is the surface covered with floating solids.
1 2 �3 4 5 6 7 8 9 10
SUSPENDED SOURS - Choose the number that best ranks the amount of suspended solids in the discharge,
where i is no solids and 10 isrmely muddy.
1 3 4 5 6 7 8 9 10
FOAM -
is there any foam on or in the stormwater discharge? yes
OIL SHEEN -
Is there oil sheen visible in the stormwater discharge or at the outfall? yes l no
DEPOSITION AT OUTFALL -
Are there sediment or othor material deposits below the outfall? yes rho
EROSION AT OUTFALL -
Is there erosion at or immediately below the outfall? yes
List and describe other obvious indicators of stormwater pollution:
BY this signature 1 certify that this report is accurate a c� the of y ge:
we.) /�
Pe 's Signature Inspector's Signature

FIRST ANALYTICAL LABORATORIES
bilhiig: PO Box 110372 - Research Triangle Park, NC 27709 TEL: [phone]
shipping: 7517 Precision Drive, Suite 101 - Raleigh, NC 2761 i F.A-%: 919 882 1603
�����e.fu�stanal} ticallabs.com
EPA Method 200 Analysis Report
FAL Project #: 140221.1
Client: Cameron Testing Services
Client Project ID: 140096
Sample Name: 140096-05 - SW#1
Report Date: 2/20/2014
Date Received: 2/10/2014
Concentration in Original Sample
Conc.
RL
Analyte
(mg/L)
(mg/L)
Copper (Cu)
0.018
0.001
Lead (Pb)
0.009
0.001
Zinc (Zn)
0.142
0.005
Approved by:
Matt Loftis, Laboratory Manager

FIRST ANALYTICAL LABORATORIES rt 1"If g PC, Box 111M2-R—arch TrcuLle Park N' 777i19 TFL" 1) 1 1) 1,41 S(Mi7 CHAIN OF CUSTODYsl„li,;,,, -91 - Prrci,.- r)— , Smia 101 - Rale,yh, Ni'`_-(:I - FAX 911) SIN--16, 13
1�1\" fu.f—al\-ticallab, ,oni
Client:
Cameron Testing Proj. Name/No: 140096
Contact:
Chris Cameron
Address:
219 S. Steele St. Sanford, NC 27330
Phone No.,
919-208-4240 email: [e-mail]
Purchase Order#:
Note To Lab:
Collection
No. Sample ID Description Date Time Matrix Preservative
140221
Analysis Required
1
140096-05
SW #1
2/3/2014
1107
WW
HNO3
Cu, Pb, Zn
2
3
4
5
6
7
8
9
10
i uished By, D te/Ti
to �' ov
Page of �
aecetved By: ale/Time:
Relinquished By: Date/Time:
Received Lab: Date/Time:
5,\...4— \r0C\C0C ..r d,

219 S. Steele Str.
Sanforcl;NC 27330
Phone:. [phone]
Campron Te%ipg,$ervic"-,.,1q 9. -Chain of Custody
NC
CWW/ G 01 of
,YY.Cert-.#654'NQ PHHs Oirt 9 37796 US EPA NC619-18 Pabe.
C ompany:,
Magneti-Marelli
lEmall:
James:Silet OuMi'gnitimarelli.com
,-ft • ,`4TS0916"use'r,
�,' "C"",
,. n y, z-
dJemes,Siler
oa r Temp
.0919-721-1353
:
ciclrbss��l
7, -rd
(.City,
State; Zip) .
c
qe:
2101 Nash�'St. gFax:,%�
Sanford, NC' 27330
. Protect
zi-
Regulatory
jj Rush .1
Mme: aturo.
L
.Sample Infdriffift i6n,
TFU
lip
a)
W
0
ACTgab:,
Sample,ID
E
>
CL
2,
—
Requested,An' 'Iysis
A
is if)
CL
E Fi
_j 0
0
. - �
-0
LL
Jf.
00
G
2A 5�11
-TTO
fey
(A I
%j
R eMquished-;J�-1--,
A W;. Re"ceivecl-�'--�
v4---F4 IDaIL61-Time "Mf
gqZ)
.Rush work will require prior approval. Additional charges will apply

Cameron Testing Services, Inc. Laboratory Report
NC DENR #664
NC PHHS t37799
US EPA #NC01918
Clie fiii
Magneti-Marelli CZS a oj: '
140096
Prijecf:
2014 SW #1 Regulatory
ices
Sample Information
Samplyd
J. Sller
Date 02103/14 Rccoived
C. Cameron
Date
D2103114
Analyses and Results
LabfO'{
`ID
sample�
n o'.Q Ariaiyte Resu#
�
E
a
_T ::
b
Std 1�tethods
U-
J
—
Reference
140096 , 01
Outfall A
SVV cv PH 6.0
u
02JN.114
DPK
45G0 H B • pH
T5S 32.3 n'cyi
2.6
0210711.1
DPK
2540 0 - TSS
02
Outfall $
at t7&G-1VV <5.0 11911,
s
02J05114
DPK
EPA 1664A
03
Outfall C
sw C EPA 6241625
04
Outfall 0
sov or EPA 608
05
Outfall E
Svr Or Metals
TTO for samples -03 and -04 analyzed by ENCO; report attached.
Metals analyzed by FAL; report attached,
Meals = Cu, Pb, Zn
Data
Review
two
Lab T — niclan
Report
Review
Lab Director Rate
211) N. swek- Str. 919-20942.0
Swfofd`C 27330 cbriscecsm-rMie cing.cvm

a:CO L07 berat
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, February 21, 2014
Cameron Testing Services, Inc. (CA039)
Attn: Chris Cameron
219 South Steele Street
Sanford, NC 27330
RE: Laboratory Results for
Project Number: 140096, Project NaMe/Desc: TTO
ENCO Workorder(s): C401556
Dear Chris Cameron,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, February 7, 2014.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Link Thrower
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 21

SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 140096-03
Lab ID:
C401556-01
Sampled: 02/03/14 11:02
Received: 02/07/14 15:55
Parameter
Hold Date/Time(s)
Ps_vo Date/Time(s)
Analvsis Date/Time(s)
EPA 624
02/17/14
02/07/14
10:31 02/11/14 10:37
Client ID: 140096-04
Lab ID:
C401556-02
Sampled: 02/03/14 11:03
Received: 02/07/14 15:55
Parameter
Hold Date/Time(s)
Prep Date/Tlm
Analysis Date/Time(s)
EPA 608
02/10/14
03/21/14
02/09/14
07:54 02/14/14 13:16
EPA 608
02/03/15
03/21/14
02/09/14
08:00 02/14/14 13:16
EPA 625
02/10/14
03/20/14
02/08/14
22:53 02/11/14 18:07
Client ID: Trip Blank
Lab ID:
C401556-03
Sampled: 02/03/14 11:02
Received: 02/07/14 15:55
Parameter
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 624
02/17/14
02/07/14
10:31 02/11/14 11:07
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 21

SAMPLE DETECTION SUMMARY
Client ID: Trip Blank Lab ID: C401556-03
Analvte Results Flaa MDL QOL Units Method Notes
Chloroform 0.53 1 0.18 1.0 ug/L EPA 624
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 21

ANALYTICAL RESULTS
Description: 140096-03 Lab Sample ID:C401556-01 Received: 02/07/14 15:55
Matrix: Water Sampled:02/03/14 11:02 Work Order: C401556
Project: TTO Sampled By:)ames Siler
(Volatile Organic Compounds by GCMS
A - ENCO Cary certified anaW [NC 591]
Analyte rCAS Numberl
Results
1,1,1-Trichloroethane [71-55-6]^
< 0.12
1,1,2,2-Tetrachloroethane [79-34-5]^
< 0.28
1,1,2-Trichloroethane [79-00-5]^
< 0.14
1,1-Dichloroethane [75-34-3]A
< 0.13
1,1-Dichloroethene [75-35-4]^
< 0.21
1,2-Dichlorobenzene [95-50-1]^
< 0.19
1,2-Dichloroethane [107-06-2]^
< 0.21
1,2-Dichloropropane [78-87-5]^
< 0.10
1,3-Dichlorobepzene [541-73-1]^
< 0.15
1,4-Dichlorobenzene [106-46-7]^
< 0.19
2-Chloroethyl Vinyl Ether [110-75-8]^
< 1.1
Acrolein [107.02-8]^
< 4.0
Acrylonitrile [107-13-1]^
< 3.5
Benzene [71-43-2]A
< 0.15
Bromodichloromethane [75-27-4]A
< 0.17
Bromoforrn [75-25-2]^
< 0.22
Bromomethane [74-83-9]A
< 0.14
Carbon Tetrachloride [56-23-5]^
< 0.17
Chlorobenzene [108-90-7]^
< 0.17
Chloroethane [75-00-3]^
< 0.23
Chloroform [67-66-3]^
< 0.18
Chloromethane [74-87-3]^
< 0.13
cis-1,3-Dichloropropene [10061-01-5]^
< 0.20
Dibromochloromethane [124-48-1]^
< 0.17
Ethylbenzene [100-41-4]^
< 0.13
Methylene Chloride [75-09-2]A
< 0.23
Tetrachloroethene [127-18-4]A
< 0.17
Toluene [108-88-3]^
< 0.14
trans-1,2-Dichloroethene [156-60-5]^
< 0.21
trans-1,3-Dichloropropene [10061-02-6]A
< 0.15
Trichloroethene [79-01-6]^
< 0.15
Vinyl chloride [75-01-4]^
< 0.32
laIaq Units
DF
MQL
p,Qy
Batch
Method
Analyzed
Ay j{Qtg;:
ug/L
1
0.12
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.28
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.14
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.13
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.21
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.19
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.21
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.10
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.15
110
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.19
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
1.1
5.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
4.0
10
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
3.5
10
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.15
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.17
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.22
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.14
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.17
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.17
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.23
1.0
4610032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.18
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.13
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.20
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.17
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.13
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.23
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.17
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.14
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.21
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.15
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.15
1.0
4B10032
EPA
624
02/11/14
10:37
REF
ug/L
1
0.32
1.0
4B10032
EPA
624
02/11/14
10:37
REF
Sun ates Results DF
Spike 4 oh Ret
% Rec Limits
4at,�i Method
g
& Notes
4-8romoAuorobenzene 37 1
50.0 74 %
51-122
4B10032 EPA 624
021111141037
REF
Dlbromoffuoromethane 41 1
50.0 82 %
68-117
4810032 EPA 624
0211111410:37
REF
Toluene-d8 42 1
50.0 83 %
67-127
4810032 EPA 624
02111114 1037
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 21

v.M
Description: 140096-04
Matrix: Water
Project: TTO
ANALYTICAL RESULTS
Lab Sample ID:C401556-02
Sampled: 02/03/ 14 11:03
Sampled By:James Siler
Received: 02/07/14 15:55
Work Order: C401556
ISemivolatile Organic Compounds by GCMS
^ - ENCO Cary cerffed anaVe ANC 591]
Analvte WAS Numberl
Results fin
units
PIE
MDL
EQL
Batch
Method
Analyzed
Notes
1,2,4-Trichlorobenzene [120-82-1]^
< 1.2
ug/L
1
1.2
10
4BO8010
EPA 625
02/11/14 18:07
DFM
1,2-Dichlorobenzene [95-50-11^
< 1.1
ug/L
1
1.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
1,3-Dichlorobenzene [541-73-11^
< 1.1
ug/L
1
1.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
1,4-Dichlorobenzene [106-46-7]^
< 1.0
ug/L
1
1.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
1-Methylnaphthalene [90-12-0]^
< 1.7
ug/L
1
1.7
10
4BOB010
EPA 625
02/11/14 18:07
DFM QL-02
2,4,5-Trichlorophenol[95-95-4]^
< 1.0
ug/L
1
1.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2,4,6-Trichlorophenol[88-06-2]^
< 1.1
ug/L
1
1.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2,4-Dichlorophenol[120-83-2]^
< 1.4
ug/L
1
1.4
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2,4-Dimethylphenol[105-67-9]^
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2,4-Dinitrophenol[51-28-5]^
< 2.6
ug/L
1
2.6
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2,4-Dinitrotoluene [121-14-2]^
< 2.4
ug/L
1
2.4
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2,6-Dinitrotoluene [606-20-21^
< 1.5
ug/L
1
1.5
10
4B08010
EPA 625
02/11/14 18:07
DFM
2-Chloronaphthalene[91-58-7]^
< 1.0
ug/L
1
1.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2-Chlorophenol[95-57-8]^
< 1.2
ug/L
1
1.2
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]^
< 2.9
ug/L
1
2.9
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2-Methylnaphthalene [91-57-6]^
< 1.5
ug/L
1
1.5
10
4B08010
EPA 625
02/11/14 18:07
DFM
2-Nitrophenol[88-75-5]^
< 1.1
ug/L
1
1.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
3,3'-Dichlorobenzidine [91-94-1]^
< 3.3
ug/L
1
3.3
10
4BOB010
EPA 625
02/11/14 18:07
DFM
4-Bromophenyl-phenylether [101-55-3]^
< 1.0
ug/L
1
1.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
4-Chloro-3-methylphenol[59-50-7]^
< 1.5
ug/L
1
1.5
10
4BO8010
EPA 625
02/11/14 18:07
DFM
4-Chlorophenyl-phenylether [7005-72-3]^
< 1.6
ug/L
1
1.6
10
4BO8010
EPA 625
02/11/14 18:07
DFM
4-Nitrophenol[100-02-7]^
< 2.0
ug/L
1
2.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Acenaphthene(83-32-9]^
< 1.4
ug/L
1
1.4
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Acenaphthylene [208-96-8]^
< 1.2
ug/L
1
1.2
10
4B08010
EPA 625
02/11/14 18:07
DFM
Anthracene[120-12-7]^
< 1.6
ug/L
1
1.6
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Benzidine [92-87-5]^
< 1.6
ug/L
1
1.6
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Benzo(a)anthracene [56-55-3]^
< 1.3
ug/L
1
1.3
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Benzo(a)pyrene [50-32-8]^
< 1.3
ug/L
1
1.3
10
4B08010
EPA 625
02/11/14 18:07
DFM
Benzo(b)fluoranthene [205-99-2]^
< 1.0
ug/L
1
1.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Benzo(g,h,i)perylene [191-24-2]^
< 2.4
ug/L
1
2.4
10
4BO8010
EPA 625
02/11/14 18:07
DFM QV-01
Benzo(k)fluoranthene[207-08-9]^
< 1.3
ug/L
1
1.3
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Benzoic acid [65-85-0]^
< 1.0
ug/L
1
1.0
50
4BO8010
EPA 625
02/11/14 18:07
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
< 1.4
ug/L
1
1.4
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Bis(2-chloroethyl)ether [111 44 4]^
< 1.2
ug/L
1
1.2
10
4B08010
EPA 625
02/11A4 18:07
DFM
Bis(2-chloroisopropyl)ether[108-60-1]^
< 1.3
ug/L
1
1.3
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
< 1.7
ug/L
1
1.7
5.0
4BO8010
EPA 625
02/11/14 18:07
DFM
Butylbenzylphthalate [85-68-7]^
< 2.0
ug/L
1
2.0
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Chrysene [218-01-9]^
< 2.0
ug/L
1
2.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Dibenzo(a,h)anthracene [53-70-3]^
< 2.3
ug/L
1
2.3
10
4B08010
EPA 625
02/11/14 18:07
DFM
Diethylphthalate [84-66-2]^
< 2.1
ug/L
1
2.1
10
4B08010
EPA 625
02/11/14 18:07
DFM
Dimethylphthalate [131-11-3]^
< 1.4
ug/L
1
1.4
10
4B08010
EPA 625
02/11/14 18:07
DFM
Di-n-butylphthalate [84-74-2]^
< 1.5
ug/L
1
1.5
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Di-n-octylphthalate [117-84-0]^
< 3.1
ug/L
1
3.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
DPH (as Azobenzene)[103-33-3]^
< 1.9
ug/L
1
1.9
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Fluoranthene [206-44-0]^
< 2.1
ug/L
1
2.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Fluorene [86-73-7]^
< 1.7
ug/L
1
1.7
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Hexachlorobenzene [118-74-1]^
< 1.0
ug/L
1
1.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Hexachlorobutadiene [87-68-3]^
< 1.2.
ug/L
1
1.2
10
4BO8010
EPA 625
02/11/14 18:07
DFM
FINAL
This report relates only to the sample as received by the
laboratory,
and may only be reproduced in full.
Page 5 of 21

ffl�q-u -, 0em w
www.encolabs.com
ANALYTICAL RESULTS
Description: 140096-04 Lab Sample ID:C401556-02 Received: 02/07/14 15:55
Matrix: Water Sampled:02/03/14 11:03 Work Order: C401556
Project: TTO Sampled By:James Siler
ISemivolatile Organic Compounds by GCMS
^ - ENCO Cary certified anaW [NC 591J
Analyte fCAS Numberl
Results Flag
Units
DF
MQL
POL
Batch
Method
Analyzed
Ay Notes
Hexachlorocyclopentadiene [77-47-4]^
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Hexachloroethane [67-72-1]^
< 1.1
ug/L
1
1.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
< 2.2
ug/L
1
2.2
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Isophorone [78-59-1]^
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Naphthalene [91-20-3]^
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Nitrobenzene [98-95-3]^
< 1.2
ug/L
1
1.2
10
4BO8010
EPA 625
02/11/14 18:07
DFM
N-Nitrosodimethylamine[62-75-9]^
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
< 1.5
ug/L
1
1.5
10
4BO8010
EPA 625
02/11/14 18:07
DFM
N-Nitrosodiphenylamine/Diphenylamine
< 2.1
ug/L
1
2.1
10
4BOB010
EPA 625
02/11/14 18:07
DFM
[86-30-6/122-39-4]^
Pentachlorophenol[87-86-5]^
< 1.8
ug/L
1
1.8
10
4B08010
EPA 625
02/11/14 18:07
DFM
Phenanthrene [85-01-8]^
< 1.4
ug/L
1
1.4
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Phenol[108-95-2]^
< 1.4
ug/L
1
1.4
10
4B08010
EPA 625
02/11/14 18:07
DFM
Pyrene [129-00-O]^
< 2.1
ug/L
1
2.1
10
4B08010
EPA 625
02/11/14 18:07
DFM
Surrogates
Results
DP
Spike L vl
% Rec
% Rec Limits
a
Method
Ana/rzed
By Notes
2,4,6-Tribromophenol
82
1
100
82 %
18-157
4BO8010
EPA 625
02111114 18:07
DFM
2-Huorobiphenyl
33
1
50.0
67 %
15-139
4BO8010
EPA 625
02111114 18:07
DFM
2-Fluorophenol
46
1
100
46 %
10-104
4308010
EPA 625
02111114 18:07
DFM
Nitrobenzene-d5
30
1
50.0
60 %
16-140
4808010
EPA 625
02/11/14 18:07
DFM
Phenol-d5
36
1
100
36 %
10-83
4608010
EPA 625
02111114 18:07
DFM
Terphenyl-d14
45
1
50.0
91 %
23-164
4BO8010
EPA 625
02111114 18:07
DFM
Semivolatile Organic Compounds by GC
^ - ENCO Cary certified analyze [NC 591]
Analvte ICAS Numberl
Results
fin
Units
OF
MD
M
Batch
Method
Analyzed
)¢jI Notes
4,4'-DDD [72-54-8]^
< 0.044
ug/L
1
0.044
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
4,4'-DDE [72-55-9]^
< 0.048
ug/L
1
0.048
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
4,4'-DDT [50-29-3]^
< 0.049
ug/L
1
0.049
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Aldrin [309-00-2]^
< 0.041
ug/L
1
0.041
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
alpha-BHC [319-84-6]^
< 0.036
ug/L
1
0.036
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
beta-BHC [319-85-7]^
< 0.036
ug/L
1
0.036
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Chlordane (n.o.s.)[57-74-9]^
< 0.020
ug/L
1
0.020
1.0
4BO9003
EPA 608
02/14/14 13:16
MWC
Chlordane (tech) [12789-03-6]^
< 0.20
ug/L
1
0.20
0.50
4BO9003
EPA 608
02/14/14 13:16
MWC
delta-BHC [319-86-8]^
< 0.048
ug/L
1
0.048
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Dieldrin [60-57-1]^
< 0.045
ug/L
1
0.045
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Endosulfan I [959-98-8]
< 0.045
ug/L
1
0.045
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Endosulfan II [33213-65-9]^
< 0.036
ug/L
1
0.036
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Endosulfan sulfate [1031-07-8]^
< 0.032
ug/L
1
0.032
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Endrin [72-20-8]^
< 0.041
ug/L
1
0.041
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Endrin aldehyde [7421-93-4]^
< 0.042
ug/L
1
0.042
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
gamma-BHC [58-89-91^
< 0.034
ug/L
1
0.034
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Heptachlor [76-44-8]^
< 0.030
ug/L
1
0.030
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Heptachlor epoxide [1024-57-3]^
< 0.037
ug/L
1
0.037
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
PCB-1016/1242[12674-11-2/53469-21-9]^
< 0.43
ug/L
1
0.43
0.50
4BO9004
EPA 608
02/14/14 13:16
MWC
PCB-1221[11104-28-2]^
< 0.37
ug/L
1
0.37
0.50
4809004
EPA 608
02/14/14 13:16
MWC
PCB-1232[11141-16-5]^
< 0.45
ug/L
1
0.45
0.50
4BO9004
EPA 608
02/14/14 13:16
MWC
PCB-1248 [12672-29-6]^
< 0.014
ug/L
1
0.014
0.50
4BO9004
EPA 608
02/14/14 13:16
MWC
PCB-1254 [11097-69-1]^
< 0.37
ug/L
1
0.37
0.50
4BO9004
EPA 608
02/14/14 13:16
MWC
FINAL
This report relates only to the
sample as received by the
laboratory,
and may only be reproduced in full.
Page 6 of 21

t5
N
ANALYTICAL RESULTS
www.encolabs.com
Description: 140096-04
Lab Sample ID:C401556-02
Received: 02/07/14 15:55
Matrix: Water
Sampled:02/03/14 11:03
Work Order: C401556
Project: TTO
Sampled By:James Siler
Semivolatile Organic Compounds by GC
^ - ENCO Cary cued analyze [NC 591]
Analyte (CAS Numbed
Results
Flag
Units
DE ]ADS P L
Batch
Method
Analyzed
Ay Notes
PCB-1260 [11096-82-5]A
< 0.45
ug/L
1 0.45 0.50
4BO9004
EPA 608
02/14/14 13:16
MWC
Toxaphene [8001-35-2]A
< 0.22
ug/L
1 0.22 1.0
4BO9003
EPA 608
02/14/14 13:16
MWC
Surrogates
R u
OF
Spike Lv/
% Rec % Rec Limits
Batch
Method
An /
,By Notes
1,4,5,6-TCMX
0.99
1
1.00
99 % 44-134
4BO9003
EPA 608
0211411413:16
MWC
2,4,5,E-TCMX
0.99
1
1.00
99 % 45-151
4BO9004
EPA 608
0211411413:16
MWC
oecachlorobiphenyl
0.96
1
1.00
96 % 37-149
4BO9003
EPA 608
0211411413:16
MWC
aemchloroblphenyl
0.96
1
1.00
96 % 42-159
4BO9004
EPA 608
0211411413:16
MWC
FINAL This report relates orgy to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 21

ANALYTICAL RESULTS
Description: Trip Blank Lab Sample ID:C401556-03 Received: 02/07/14 15:55
Matrix: Water Sampled:02/03/14 11:02 Work Order: C401556
Project: TTO Sampled By:Cameron Testing
(Volatile
Organic Compounds by GCMS
^ - ENCO Cary certified anaW [NC 591]
Analyte rCAS Numberl
Results Flaa
Units
gF
MQL
E_QL
Batch
Method
Analyzed
Ay Notes
1,1,1-Trichloroethane [71-55-6]^
< 0.12
ug/L
1
0.12
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,1,2,2-Tetrachloroethane [79-34-5)^
< 0.28
ug/L
1
0.28
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,1,2-Trichloroethane [79-00-5]^
< 0.14
ug/L
1
0.14
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,1-Dichloroethane [75-34-3]^
< 0.13
ug/L
1
0.13
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,1-Dichloroethene [75-35-4]^
< 0.21
ug/L
1
0.21
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,2-Dichlorobenzene [95-50-1]^
< 0.19
ug/L
1
0.19
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,2-Dichloroethane [107-06-2]^
< 0.21
ug/L
1
0.21
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,2-Dichloropropane [78-87-5]^
< 0.10
ug/L
1
0.10
1.0
4B10032
EPA 624
02/11/14 11:07
REF '
1,3-Dichlorobenzene [541-73-1]^
< 0.15
ug/L
1
0.15
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,4-Dichlorobenzene [106-46-7]^
< 0.19
ug/L
1
0.19
1.0
4B10032
EPA 624
02/11/14 11:07
REF
2-Chloroethyl Vinyl Ether [110-75-8]^
< 1.1
ug/L
1
1.1
5.0
4B10032
EPA 624
02/11/14 11:07
REF
Acrolein [107-02-8]^
< 4.0
ug/L
1
4.0
10
4B10032
EPA 624
02/11/14 11:07
REF
Acrylonitrile [107-13-1]^
< 3.5
ug/L
1
3.5
10
4B10032
EPA 624
02/11/14 11:07
REF
Benzene [71-43-2]^
< 0.15
ug/L
1
0.15
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Bromodichloromethane [75-27-4]^
< 0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Bromoform [75-25-2]^
< 0.22
ug/L
1
0.22
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Bromomethane [74-83-9]^
< 0.14
ug/L
1
0.14
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Carbon Tetrachloride [56-23-5]^
< 0.17
ug/L
1
0.17
1.0
4610032
EPA 624
02/11/14 11:07
REF
Chlorobenzene[108-90-7]^
< 0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Chloroethane [75-00-3]^
< 0.23
ug/L
1
0.23
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Chloroform [67-66-3]^
0.53 1
ug/L
1
0.18
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Chloromethane [74-87-3]^
< 0.13
ug/L
1
0.13
1.0
4B10032
EPA 624
02/11/14 11:07
REF
cis-1,3-Dichloropropene [10061-01-5]^
< 0.20
ug/L
1
0.20
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Dibromochloromethane [124-48-1]^
< 0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Ethylbenzene [100-41-4]^
< 0.13
ug/L
1
0.13
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Methylene Chloride [75-09-2]^
< 0.23
ug/L
1
0.23
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Tetrachloroethene[127-18-4)^
< 0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Toluene[108-88-3]^
< 0.14
ug/L
1
0.14
1.0
4B10032
EPA 624
02/11/14 11:07
REF
trans-1,2-Dichloroethene [156-60-5]^
< 0.21
ug/L
1
0.21
1.0
4B10032
EPA 624
02/11/14 11:07
REF
trans-1,3-Dichloropropene [10061-02-6]^
< 0.15
ug/L
1
0.15
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Trichloroethene [79-01-6]^
< 0.15
ug/L
1
0.15
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Vinyl chloride [75-01-4]^
< 0.32
ug/L
1
0.32
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Surrogates Resu
QF
Spike Lv/
'/o Rec
a/o Rec Limits
Batch
Meth
Ana/vzed
ly Notes
4-Bromofluorobenzene 38
1
50.0
76 %
51-122
4810032
EPA 624
02111114 11:07
REF
Dibromofluoromethane 43
1
50.0
85 %
68-117
4B10032
EPA 624
02111114 11:07
REF
Toluene-d8 43
1
50.0
86 %
67-127
4810032
EPA 624
02111114 11:07
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 21

Spike
Source
%REC
RPD
Anal a
Raul
Flag
PQL
Units
Level
Result %REC
Limift RPD
Limi Notes
1, 1, 1-Trich loroethane
0.12
U
1.0
ug/L
1, 1, 2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,3-Dichlorobenzene
0.15
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Chloroethyl Vinyl Ether
1.1
U
5.0
ug/L
Acrolein
4.0
U
10
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon Tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis-1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Methylene Chloride
0.23
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
4-Bromofluorobenzene
39
u9/L
50,0
78
51-122
Dibromofluoromethane
42
u9/L
50.0
84
68-117
Toluene-&
43
ug/L
50.0
86
67-127
LCS (41310032-BS3)
Prepared: 02/10/2014 17:53 Analyzed: 02/11/2014 00:16
Spike
Source
%REC
RPD
Anal 1(te
Result
l]a9
E4L
Units
Level
Result %REC
Limits RPD
l:11615 Notes
1,1,1-Trichloroethane
20
1.0
ug/L
20.0
99
52-162
1,1,2,2-Tetrachloroethane
20
1.0
ug/L
20.0
101
46-157
1,1,2-Trichloroethane
21
1.0
ug/L
20.0
103
.52-150
1,1-Dichloroethane
20
1.0
ug/L
20.0
100
59-155
1,1-Dichloroethene
21
1.0
ug/L
20.0
103
10-234
1,2-Dichlorobenzene
20
1.0
ug/L
20.0
100
18-190
1,2-Dichloroethane
21
1.0
ug/L
20.0
105
49-155
1,2-Dichloropropane
20
1.0
ug/L
20.0
98
10-210
1,3-Dichlorobenzene
20
1.0
ug/L
20.0
100
59-156
1,4-Dichlorobenzene
18
1.0
ug/L
20.0
92
18-190
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in
full.
Page 9 of 21

QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 4B10032 - EPA 5030B MS - Continued
LCS (4B10032-BS3) Continued Prepared: 02/10/2014 17:53 Analyzed: 02/11/2014 00:16
Spike
Source
%REC
RPD
Analvte
Result
Flaa
POL
Vnits_
Level
Result
%REC
Limits RPD
Limit Notes
2-Chloroethyl Vinyl Ether
38
5.0
ug/L
40.0
96
10-305
Acrolein
9.1
3
10
ug/L
40.0
23
10-200
Acrylonithle
56
10
ug/L
60.0
94
10-200
Benzene
20
1.0
ug/L
20.0
98
37-151
Bromodichloromethane
21
1.0
ug/L
20.0
105
35-155
Bromoform
17
1.0
ug/L
20.0
86
45-169
Bromomethane
16
1.0
ug/L
20.0
81
10-242
Carbon Tetrachloride
20
1.0
ug/L
20.0
100
17-140
Chlorobenzene
21
1.0
ug/L
20.0
105
37-160
Chloroethane
18
1.0
ug/L
20.0
89
14-230
Chloroform
20
1.0
ug/L
20.0
100
51-138
Chloromethane
15
1.0
ug/L
20.0
74
10-273
cis-1,3-Dichloropropene
19
1.0
ug/L
20.0
94
10-227
Dibromochloromethane
21
1.0
ug/L
20.0
106
53-149
Ethylbenzene
18
1.0
ug/L
20.0
89
37-162
Methylene Chloride
21
1.0
ug/L
20.0
106
10-221
Tetrachloroethene
19
1.0
ug/L
20.0
95
64-148
Toluene
18
1.0
ug/L
20.0
92
47-150
trans-1,2-Dichloroethene
19
1.0
ug/L
20.0
97
54-156
trans-1,3-Dichloropropene
21
1.0
ug/L
20.0
104
17-183
Trichloroethene
19
1.0
ug/L
20.0
97
71-157
Vinyl chloride
14
1.0
ug/L
20.0
68
10-251
4-Bromofluorobenzene
39
u91L
50.0
79
51-122
Dibromofluoromethane
42
u91L
50.0
84
68-117
Toluene-d8
43
u91L
50.0
85
67-127
Matrix Spike (4B10032-MS1)
Prepared: 02/10/2014 17:53 Analyzed: 02/11/2014 00:45
Source: C401302-09
Spike
Source
%REC
RPD
Anal vte
Result
Flao
ML
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1,1-Trichloroethane
20
1.0
ug/L
20.0
0.12 U
101
52-162
1,1,2,2-Tebadtloroethane
19
1.0
ug/L
20.0
0.28 U
94
46-157
1,1,2-Trichloroethane
19
1.0
ug/L
20.0
0.14 U
97
52-150
1,1-Dichloroethane
20
1.0
ug/L
20.0
0.13 U
102
59-155
1,1-Dichloroethene
22
1.0
ug/L
20.0
0.21 U
108
10-234
1,2-Dichlorobenzene
20
1.0
ug/L
20.0
0.19 U
102
18-190
1,2-Dichloroethane
21
1.0
ug/L
20.0
0.21 U
106
49-155
1,2-Dichloropropane
20
1.0
ug/L
20.0
0.10 U
99
10-210
1,3-Dichlorobenzene
21
1.0
ug/L
20.0
0.15 U
103
59-156
1,4-Dichlorobenzene
19
1.0
ug/L
20.0
0.19 U
96
18-190
2-Chloroethyl Vinyl Ether
35
5.0
ug/L
40.0
1.1 U
87
10-305
Acrolein
8.3
3
10
ug/L
40.0
4.0 U
21
10-200
Acrylonitrile
49
10
ug/L
60.0
3.5 U
82
10-200
Benzene
20
1.0
ug/L
20.0
0.15 U
101
37-151
Bromodichloromethane
22
1.0
ug/L
20.0
0.17 U
108
35-155
Bromoforrn
16
1.0
ug/L
20.0
0.22 U
82
45-169
Bromomethane
20
1.0
ug/L
20.0
0.14 U
100
10-242
Carbon Tetrachloride
21
1.0
ug/L
20.0
0.17 U
106
70-140
Chlorobenzene
22
1.0
ug/L
20.0
0.17 U
108
37-160
Chloroethane
23
1.0
ug/L
20.0
0.23 U
113
14-230
FINAL
This report relates only to the sample as received by the laboratory, and may only be
reproduced in
full.
Page 10 of 21

QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 4810032 - EPA 50306 MS - Continued
Matrix Spike (4B10032-MS4) Continued Prepared: 02/10/2014 17:53 Analyzed: 02/11/2014 00:45
Source: C401302-09
Spike
Source
%REC RPD
Anala
Result E149
PQL
Units
Level
Result
%REC
Limits RPD Li ft Notes
Chloroform
20
1.0
ug/L
20.0
0.18 U
101
51-138
Chloromethane
23
1.0
ug/L
20.0
0.13 U
116
10-273
cis-1,3-Dichloropropene
19
1.0
ug/L
20.0
0.20 U
95
10-227
Dibromochloromethane
20
1.0
ug/L
20.0
0.17 U
101
53-149
Ethylbenzene
19
1.0
ug/L
20.0
0.13 U
94
37-162
Methylene Chloride
21
1.0
ug/L
20.0
0.23 U
107
10-221
Tetrachlorcethene
20
1.0
ug/L
20.0
0.17 U
98
64-148
Toluene
19
1.0
ug/L
20.0
0.14 U
95
47-150
trans-1,2-Dichloroethene
20
1.0
ug/L
20.0
0.21 U
100
54-156
trans-1,3-Dichloropropene
20
1.0
ug/L
20.0
0.15 U
100
17-183
Trichloroethene
21
1.0
ug/L
20.0
0.15 U
104
71-157
Vinyl chloride
19
1.0
ug/L
20.0
0.32 U
95
10-251
4-Bromofluorobenzene
Dibromoflucromethane
Toluene-&
40
41
43
ug/L
ug/L
ug/L
50.0
50.0
50.0
80
83
.86
51-122
68-117
67-127
Matrix Spike Dup (4630032-MSD1)
Prepared: 02/10/2014 17:53 Analyzed: 02/11/2014 01:15
Source: C401302-09
Spike
Source
%REC
RPD
Analvte
Resu1L
F1a9 QQL
Units
Level
Result
%REC
Limits
RPD
kimit Notes
1, 1, 1-Trichloroethane
20
1.0
ug/L
20.0
0.12 U
98
52-162
3
25
1,1,2,2-Tetrachloroethane
21
1.0
ug/L
20.0
0.28 U
105
46-157
11
25
1, 1, 2-Trichloroethane
21
1.0
ug/L
20.0
0.14 U
103
52-150
6
25
1,1-Dichloroethane
20
1.0
ug/L
20.0
0.13 U
100
59-155
3
25
1,1-Dichloroethene
21
1.0
ug/L
20.0
0.21 U
103
10-234
5
25
1,2-Dichlorobenzerie
20
1.0
ug/L
20.0
0.19 U
100
18-190
1
25
1,2-Dichloroethane
21
1.0
ug/L
20.0
0.21 U
103
49-155
2
25
1,2-Dichloropropane
19
1.0
ug/L
20.0
0.10 U
97
10-210
2
25
1,3-Dichlorobenzene
20
1.0
ug/L
20.0
0.15 U
99
59-156
4
25
1,4-Dichlorobenzene
18
1.0
ug/L
20.0
0.19 U
91
18-190
5
25
2-Chloroethyl Vinyl Ether
39
5.0
u9/L
40.0
1.1 U
98
10-305
12
25.9
Acrolein
10
10
ug/L
40.0
4.0 U
26
10-200
23
36
Acrylonitrile
60
10
ug/L
60.0
3.5 U
100
10-200
19
50
Benzene
19
1.0
ug/L
20.0
0.15 U
97
37-151
4
25
Bromodichloromethane
21
1.0
ug/L
20.0
0.17 U
103
35-155
5
25
Bromoform
18
1.0
ug/L
20.0
0.22 U
92
45-169
12
25
Bromomethane
18
1.0
ug/L
20.0
0.14 U
92
10-242
B
25
Carbon Tetrachloride
20
1.0
ug/L
20.0
0.17 U
99
70-140
7
25
Chlorobenzene
21
1.0
ug/L
20.0
0.17 U
103
37-160
5
25
Chloroethane
22
1.0
ug/L
20.0
0.23 U
109
14-230
4
25
Chloroform
19
1.0
ug/L
20.0
0.18 U
97
51-138
3
25
Chloromethane
22
1.0
ug/L
20.0
0.13 U
108
10-273
7
25
cis-1,3-Dichloropropene
19
1.0
ug/L
20.0
0.20 U
94
10-227
1
25
Dibromochloromethane
21
1.0
ug/L
20.0
0.17 U
106
53-149
5
25
Ethylbenzene
18
1.0
ug/L
20.0
0.13 U
90
37-162
5
25
Methylene Chloride
20
1.0
ug/L
20.0
0.23 U
102
10-221
5
25
Tetrachloroethene
19
1.0
ug/L
20.0
0.17 U
95
64-148
3
25
Toluene
18
1.0
ug/L
20.0
0.14 U
90
47-150
5
25
trans-1,2-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
96
54-156
4
25
trans-1,3-Dichloropropene
21
1.0
ug/L
20.0
0.15 U
105
17-183
4
25
FINAL This repot relates orgy to.the sample as
received by the laboratory, and may only be
reproduced in
full.
Page 11 of 21

Spike
Source
%REC
RPD
Anal rte
Result
Flag
PPL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Trichloroethene
20
1.0
ug/L
20.0
0.15 U
98
71-157
6
25
Vinyl chloride
17
1.0
ug/L
20.0
0.32 U
87
10-251
8
25
9 Bromofluorobenzene
39
ug/L
50.0
78
51-122
DibromoNucromethane
42
u91L
50.0
84
68-117
Toluene-d8
42
u91L
50.0
84
67-127
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 4508010 - EPA 351OC MS
Blank (41308010-BLKl) h
Prepared: 02/08/2014 22:53 Analyzed: 02/11/2014 14:18
Spike
Source
%REC
RPD
AnaLlttQ
Result
Flag
PQL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,2,4-Trichlorobenzene
1.2
U
10
ug/L
1,2-Dichlorobenzene
1.1
U
10
ug/L
1,3-Dichkxobenzene
1.1
U
10
ug/L
1,4-Dichlorobenzene
1.0
U
10
ug/L
1-Methylnaphthalene
1.7
U
10
ug/L
2,4,5-Trichlorophenol
1.0
U
10
ug/L
2,4,6-Trichlorophenol
1.1
U
10
ug/L
2,4-Dichkxophenol
1.4
U
10
ug/L
2,4-Dimethylphenol
1.3
U
10
ug/L
2,4-Dinitrophenol
2.6
U
10
ug/L
2,4-Dinitrotoluene
2.4
U
10
ug/L
2,6-Dinitrotoluene
1.5
U
10
ug/L
2-Chloronaphthalene
1.0
U
10
ug/L
2-Chlorophenol
1.2
U
10
ug/L
2-Methyl-0,6-dinitrophenol
2.9
U
10
ug/L
2-Methylnaphthalene
1.5
U
10
ug/L
2-Nitrophenol
1.1
U
10
ug/L
3,3'-Dichlorobenzidine
3.3
U
10
ug/L
4-13ro nophenyl-phenylether
1.0
U
10
ug/L
4-Chloro-3-methylphenol
1.5
U
10
ug/L
4-Mlorophenyl-pherrylether
1.6
U
10
ug/L
4-Nitrophenol
2.0
U
10
ug/L
Acenaphthene
1.4
U
10
ug/L
Acenaphthylene
1.2
U
10
ug/L
Anthracene
1.6
U
10
ug/L
Benzidine
1.6
U
10
ug/L
Benzo(a)anthracene
1.3
U
10
ug/L
Benzo(a)pyrene
1.3
U
10
ug/L
Benzo(b)fluoranthene
1.0
U
10
ug/L
Benzo(g,h,i)perylene
2.4
U
10
ug/L
QV-01
Benzo(k)fluoranthene
1.3
U
10
ug/L
Benzoic acid
1.0
U
50
ug/L
Bis(2-chkxoethoxy)methane
1.4
U
10
ug/L
Bis(2-chloroethyl)ether
1.2
U
10
ug/L
Bis(2-chloroisopropyl)ether
1.3
U
10
ug/L
Bis(2-ethylhexyl)phthalate
1.7
U
5.0
ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 21

a�.>.we..u•
Spike
Anala
Result
Flaa
lQ
Units Level
Butylbenzylphlhalate
2.0
U
10
ug/L
Chrysene
2.0
U
10
ug/L
Dibenzo(a,h)anthracene
2.3
U
10
ug/L
Diethylphthalate
2.1
U
10
ug/L
Dimethylphthalate
1.4
U
10
ug/L
Di-n-butylphthalate
1.5
U
10
ug/L
Di-n-octylphthalate
3.1
U
10
ug/L
DPH (as Azobenzene)
1.9
U
10
ug/L
Fluoranthene
2.1
U
10
ug/L
Fluorene
1.7
U
10
ug/L
Hexachlorobenzene
1.0
U
10
ug/L
Hexachlorobutadiene
1.2
U
10
ug/L
Hexachlorocyclopentadiene
1.3
U
10
ug/L
Hexachloroethane
1.1
U
10
ug/L
Indeno(1,2,3-cd)pyrene
2.2
U
10
ug/L
Isophorone
1.3
U
10
ug/L
Naphthalene
1.3
U
10
ug/L
Nitrobenzene
1.2
U
10
ug/L
N-Nitrosodimethylamine
1.3
U
10
ug/L
N-Nitroso-di-n-propylamine
1.5
U
10
ug/L
N-Nitrosodiphenylamine/Diphenylamine
2.1
U
10
ug/L
Pentachlorophenol
1.8
U
10
ug/L
Phenanthrene
1.4
U
10
ug/L
Phenol
1.4
U
10
ug/L
Pyrene
2.1
U
10
ug/L
Source %REC RPD
Result %REC Limits RPD Limi Notes
2,4,6-Tribromophenol
64
u9/L
100 64 18-157
2-Fluorobiphenyl
43
u9/L
50.0 87 15-139
1-Fluorophenol
55
u9/L
100 55 10-104
Nitrobenzene-d5
39
u9/L
50.0 78 16-140
Phenol-d5
38
u9/L
100 38 10-83
Terphen"14
44
u91L
50.0 88 23-164
LCS (4BOB010-BSI)
Prepared: 02/08/2014 22:53 Analyzed: 02/11/2014 14:51
Spike
Source
%REC RPD
Analvte
Result
Flag M
Units
Level
Result %REC
limits RPD Limit Notes
1,2,4-Trichlorobenzene
41
10
ug/L
50.0
82
44-142
1,2-Dichlorobenzene
36
10
ug/L
50.0
72
32-129
1,3-Dichlorobenzene
36
10
ug/L
50.0
71
10-172
1,4-Dichlorobenzene
36
10
ug/L
50.0
71
20-124
1-Methylnaphthalene
41
10
ug/L
50.0
83
46-80 QL-02
2,4,5-Trichlorophenol
45
10
ug/L
50.0
90
59-121
2,4,6-Trichlorophenol
46
10
ug/L
50.0
91
61-119
2,4-Dichlorophenol
43
10
ug/L
50.0
86
49-118
2,4-Dimethylphenol
39
10
ug/L
50.0
78
42-111
2,4-Dinitrophenol
41
10
ug/L
50.0
83
1-149
2,4-Dinitrotoluene
43
10
ug/L
50.0
87
39-139
2,6-Dinitrotoluene
46
10
ug/L
50.0
92
50-158
2-Chloronaphthalene
45
10
ug/L
50.0
89
60-118
2-Chlorophenol
40
10
ug/L
50.0
80
23-134
-FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in
full. Page 13 of 21

www.enccdabs.com
QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 4508010 - EPA 3510C MS - Continued
I LCS (4B08010-BS1) Continued
Prepared: 02/08/2014 22:53 Analyzed: 02/11/2014 14:51
Spike
Source
%REC RPD
Anal (te
Res"I Rag
PQL
Units
Level
Result %REC
Limits RPD Limit Notes
2-Methyl-4,6-dinitrophenol
44
10
ug/L
50.0
89
33-160
2-Methyinaphthalene
42
10
ug/L
50.0
84
33-111
2-Nitrophenol
43
10
ug/L
50.0
87
36-113
3,3'-Dichlorobenzidine
66
10
ug/L
50.0
132
10-262
4-Bromophenyl-phenylether
45
10
ug/L
50.0
90
53-127
4-Chloro-3-methylphenol
42
10
ug/L
50.0
84
25-147
4-Chlorophenyl-phenylether
45
10
u9/L
50.0
90
25-158
4-Nitrophenol
30
10
ug/L
50.0
60
33-105
Acenaphthene
42
10
ug/L
50.0
84
47-145
Acenaphthylene
44
110
ug/L
50.0
88
33-145 r
Anthracene
42
10
ug/L
50.0
85
27-133
Benzidine
12
10
ug/L
50.0
24
10-136
Benzo(a)anthracene
45
10
ug/L
50.0
91
33-143
Benzo(a)pyrene
51
10
ug/L
50.0
103
17-163
Benzo(b)fluoranthene
48
10
ug/L
50.0
97
24-159
Benzo(g,h,i)perylene
58
10
ug/L
50.0
117
10-219
Benzo(k)fluoranthene
49
10
ug/L
50.0
99
11-162
Benzoic acid
15 1
50
ug/L
50.0
30
10-120
Bis(2-chloroethoxy)methane
41
10
ug/L
50.0
82
33-184
Bis(2-chloroethyl)ether
42
10
ug/L
50.0
84
12-158
Bis(2-chloroisopropyl)ether
43
10
ug/L
50.0
86
36-166
Bis(2-ethylhexyl)phthalate
49
5.0
ug/L
50.0
98
10-158
Butylbenzylphthalate
54
10
ug/L
50.0
108
64-152
Chrysene
46
10
ug/L
50.0
92
17-168
Dibenzo(a,h)anthracene
62
10
ug/L
50.0
124
10-227
Diethylphthalate
46
10
ug/L
50.0
91
62-127
Dimethylphthalate
47
10
ug/L
50.0
93
.10-114
Di-n-butylphthalate
48
10
ug/L
50.0
96
10-118
Di-n-octylphthalate
55
10
ug/L
50.0
110
10-146
DPH (as Azobenzene)
44
10
ug/L
50.0
88
69-108
Fluoranthene
45
10
ug/L
50.0
90
26-137
Fluorene
42
10
ug/L
50.0
84
59-121
Hexacilorobenzene
47
10
ug/L
50.0
93
10-152
Hexachlorobutadiene
41
10
ug/L
50.0
83
24-116
Hexachlorocyclopentadiene
43
10
ug/L
50.0
85
10-99
Hexachloroethane
33
10
ug/L
50.0
66
12-82
Indeno(1,2,3<d)pyrene
61
10
ug/L
50.0
123
10-171
Isophorone
44
10
ug/L
50.0
88
21-196
Naphthalene
40
10
ug/L
50.0
80
21-133
Nitrobenzene
42
10
ug/L
50.0
84
35-180
N-Nitrosodimethylamine
34
10
ug/L
50.0
69
24-94
N-Nitroso-di-n-propylamine
38
10
ug/L
50.0
76
10-230
Pentachlorophenol
45
10
ug/L
50.0
90
51-135
Phenanthrene
44
10
ug/L
50.0
88
54-120
Phenol
25
10
ug/L
50.0
50
19-78
Pyrene
46
10
ug/L
50.0
92
65-134
2, 4, 6-Thbromophenol
89
u91L
100
89
18-157
2-Fluorobiphenyl
45
u91L
50.0
89
15-139
2-Fluorophenol
60
u91L
100
60
10-104
This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 21

Spike
Source
°/oREC
RPD
Analyte
Rfs"A
Flag
PQL-
Units
Level
Result
9/oREC
Limits RPD
Umik Notes
N10robenze17e-d5
44
u9/L
50.0
87
16-140
Phenol-d5
48
u9/L
100
48
10-83
Terphenyl-d14
48
u9/L
50.0
97
23-164
Matrix Spike (4B08030-MS3)
Prepared: 02/08/2014 22:53 Analyzed: 02/11/2014 15:23
Source: C400990-03
Spike
Source
9/oREC
RPD
Anal [�
Resul
RM
RQL
Units
Level
Result
°/oREC
Limi RPD
Limit Notes
1,2,4-Trichlorobenzene
35
10
ug/L
50.0
1.2 U
70
44-142
1,2-Dichlorobenzene
31
10
uq/L
50.0
1.1 U
63
32-129
1,3-Dichlorobenzene
30
10
ug/L
50.0
1.1 U
61
10-172
1,4-Dichlorobenzene
31
10
ug/L
50.0
1.0 U
62
20-124
1-Methylnaphthalene
36
10
ug/L
50.0
1.7 U
72
46-80
2,4,5-Trichlorophenol
42
10
ug/L
50.0
1.0 U
84
59-121
2,4,6-Trichlorophenol
40
10
ug/L
50.0
1.1 U
79
61-119
2,4-Dichlorophenol
38
10
ug/L
50.0
1.4 U
77
49-118
2,4-Dimethylphenol
36
10
ug/L
50.0
1.3 U
72
42-111
2,4-Dinitrophenol
37
10
ug/L
50.0
2.6 U
74
11-149
2,4-Dinitrotoluene
39
10
ug/L
50.0
2.4 U
78
39-139
2,6-Dinitrotoluene
38
10
ug/L
50.0
1.5 U
77
50-158
2-Chloronaphthalene
37
10
ug/L
50.0
1.0 U
75
60-118
2-0lorophenol
32
10
ug/L
50.0
1.2 U
64
23-134
2-Methyl4,6-dinitrophenol
39
10
ug/L
50.0
2.9 U
78
33-160
2-Methylnaphthalene
36
10
ug/L
50.0
1.5 U
72
33-111
2-Nitrophenol
35
10
ug/L
50.0
1.1 U
71
36-113
3,T-Dichlorobenzidine
59
10
ug/L
50.0
3.3 U
118
10-262
4-Bromophenyl-phenylether
39
10
ug/L
50.0
1.0 U
78
53-127
4-Chloro-3-methylphenol
40
10
ug/L
50.0
1.5 U
80
25-147
4{hlorophenyl-phenylether
40
10
ug/L
50.0
1.6 U
79
25-158
4-Nitrophenol
27
10
ug/L
50.0
2.0 U
53
33-105
Acenaphthene
37
10
ug/L
50.0
1.4 U
74
47-145
Acenaphthylene
38
10
ug/L
50.0
1.2 U
77
33-145
Anthracene
37
10
ug/L
50.0
1.6 U
75
27-133
Benzidine
3.6
J
10
ug/L
50.0
1.6 U
7
10-136
Benzo(a)anthracene
40
10
ug/L
50.0
13 U
80
33-143
Benzo(a)pyrene
45
10
ug/L
50.0
1.3 U
91
17-163
Benzo(b)fluoranthene
43
10
ug/L
50.0
1.0 U
86
24-159
Benzo(g,h,i)perylene
54
10
ug/L
50.0
2.4 U
108
10-219
Benzo(k)fluoranthene
43
10
ug/L
50.0
1.3 U
86
11-162
Benzoic acid
6.4
1
50
ug/L
50.0
1.0 U
13
10-120
Bis(2-chloroethoxy)methane
33
10
ug/L
50.0
1.4 U
66
33-184
Bis(2-chloroethyl)ether
34
10
ug/L
50.0
1.2 U
67
12-158
Bis(2-chloroisopropyl)ether
34
10
ug/L
50.0
1.3 U
68
36-166
Bis(2-ethylhexyl)phthalate
42
5.0
ug/L
50.0
1.7 U
85
10-158
Butylbenzylphthalate
50
10
ug/L
50.0
2.0 U
100
10-152
Chrysene
41
10
ug/L
50.0
2.0 U
81
17-168
Dibenzo(a,h)anthracene
52
10
ug/L
50.0
2.3 U
105
10-227
Diethylphthalate
40
10
ug/L
50.0
2.1 U
79
62-127
Dimethylphthalate
38
10
ug/L
50.0
1.4 U
77
10-114
Di-n-butylphthalate
44
10
ug/L
50.0
1.5 U
88
10-118
FINAL
This report relates only to
the sample as received by the laboratory, and
may only be
reproduced in
full.
Page 15 of 21

a1�4
Spike
Source
%REC
Anand
Result Flag
PQL
Units
Level
Result
%REC
Limits RPD
Di-n-octylphthalate
48
10
ug/L
50.0
3.1 U
96
10-146
DPH (as Azobenzene)
39
10
ug/L
50.0
1.9 U
78
69-108
Fluoranthene
41
10
ug/L
50.0
2.1 U
81
26-137
Fluorene
37
10
ug/L
50.0
1.7 U
73
59-121
Hexachlorobenzene
40
10
ug/L
50.0
1.0 U
81
10-152
Hexachlorobutadiene
36
10
ug/L
50.0
1.2 U
71
24-116
Hexachlorocydopentadiene
34
10
ug/L
50.0
1.3 U
68
10-99
Hexachloroethane
28
10
ug/L
50.0
1.1 U
56
12-82
Indeno(1,2,3td)pyrene
52
10
ug/L
50.0
2.2 U
104
10471
Isophorone
35
10
ug/L
50.0'
1.3 U
70
21-196
Naphthalene
35
10
ug/L
50.0
1.3 U
70
21-133
Nitrobenzene
34
10
ug/L
50.0
1.2 U
67
35-180
N-Nitrosodimethylamine
28
10
ug/L
50.0
1.3 U
57
24-94
N-Nitroso-di-n-propylamine
31
10
ug/L
50.0
1.5 U
61
10-230
Pentachlorophenol
42
10
ug/L
50.0
1.8 U
84
51-135
Phenanthrene
38
10
ug/L
50.0
1.4 U
77
54-120
Phenol
22
10
ug/L
50.0
1.4 U
44
19-78
Pyrene
42
10
ug/L
50.0
2.1 U
83
52-115
RPD
U-it Notes
2,4,6-Tribromophenol
80
u9/L
100
80
I8-157
2-Ruorobiphenyl
36
u9/L
50.0
73
15-139
2-Fluorophenol
52
u9/L
100
52
10-104
Nitrobenzene-d5
33
u9/L
50.0
66
16-140
Phenol-d5
41
u91L
100
41
10-83
Terphenyl-d14
42
u91L
50.0
84
23-164
Matrix Spike Dup (4B08010-MSD1)
Prepared: 02/08/2014 22:53 Analyzed: 02/11/2014 15:55
Source: C400990-03
Spike
Source
%REC
RPD
Analvte
Result
Flan ML
UQJU
Level
get
%REC
Limits
RPD
Limit Notes
1,2,4-Trichlorobenzene
35
10
ug/L
50.0
1.2 U
71
44-142
2
28.1
1,2-Dichlorobenzene
31
10
ug/L
50.0
1.1 U
63
32-129
0.3
30.9
1,3-Dichlorobenzene
31
10
ug/L
50.0
.1A U
62
10-172
1
41.7
1,4-Dichlorobenzene
31
10
ug/L
50.0
1.0 U
61
20-124
0.5
32.1
1-Methylnaphthalene
35
10
ug/L
50.0
1.7 U
71
46-80
1
25
2,4,5-Trlchlorophenol
42
10
ug/L
50.0
1.0 U
84
59-121
0.5
25
2,4,6-Trichlorophenol
40
10
ug/L
50.0
1.1 U
80
61-119
1
25
2,4-Dichlorophenol
38
10
ug/L
50.0
1.4 U
76
49-118
2
25
2,4-Dimethylphenol
34
10
ug/L
50.0
1.3 U
68
42111
6
26
2,4-Dinitrophenol
39
10
ug/L
50.0
2.6 U
78
11-149
4
50
2,4-Dinitrotoluene
39
10
ug/L
50.0
2.4 U
79
39-139
1
25
2,6-Dinitroto4uene
41
10
ug/L
50.0
1.5 U
82
50-158
7
29.6
2-Mloronaphthalene
38
10
ug/L
50.0
1.0 U
76
60-118
2
25
2-(hlorophenol
32
10
ug/L
50.0
1.2 U
64
23-134
1
28.7
2-Methyl-4,6-dinitropherrol
42
10
ug/L
50.0
2.9 U
83
33-160
6
25
2-Methylnaphthalene
35
10
ug/L
50.0
1.5 U
70
33-111
2
27
2-Nitrophenol
35
10
ug/L
50.0
1.1 U
71
36-113
0.3
50
3,T-Dichlorobenzidine
47
10
ug/L
50.0
3.3 U
94
10-262
23
71.4
4-Bromophenyl-phenylether
39
10
ug/L
50.0
1.0 U
77
53-127
1
25
4-Chloro-3-methylphenol
38
10
ug/L
50.0
1.5 U
77
25-147
4
37.2
4-Chlorophenyl-phenylether
39
10
ug/L
50.0
1.6 U
79
25-158
0.4
33.4
FINAL
This report relates
only to the sample as received by the
laboratory, and may only be
reproduced in
full.
Page 16 of 21

QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 4BO8010 - EPA 3510C MS - Continued
Matrix Spike Dup (4608030-MSD3) Continued Prepared: 02/08/2014 22:53 Analyzed: 02/11/2014 15:55
Source: C400990-03
Spike
Source
°/uREC
RPD
Anal
Result Flaa
PPL
Units
Level
Result
%REC
Limits
RPD
Li i
4-Nitrophenol
27
10
ug/L
50.0
2.0 U
55
33-105
3
27
Acenaphthene
36
10
ug/L
50.0
1.4 U
73
47-145
2
27.6
Acenaphthylene
38
10
ug/L
50.0
1.2 U
76
33-145
0.3
40.2
Anthracene
37
10
ug/L
50.0
1.6 U
73
27-133
2
32
Benzidine
4.0 ]
10
ug/L
50.0
1.6 U
8
10-136
11
50
Benzo(a)anthracene
40
10
ug/L
50.0
1.3 U
80
33-143
03
27.6
Benzo(a)pyrene
45
10
ug/L
50.0
1.3 U
90
17-163
0.6
39
Benzo(b)fluoranthene
43
10
ug/L
50.0
1.0 U
86
24-159
0.3
38.8
Benzo(g,h,i)perylene
54
10
ug/L
50.0
2.4 U
108
10-219
0.4
58.9
Benzo(k)fluoranthene'
43
10
ug/L
50.0
1.3 U '
87
11-162
1
32.3
Benzoic acid
23 1
5o
ug/L
50.0
1.0 U
46
10-120
113
41
Bis(2-chloroethoxy)methane
33
10
ug/L
50.0
1.4 U
66
33-184
0.3
34.5
Bis(2-chloroethyl)ether
34
10
ug/L
50.0
1.2 U
67
12-158
0.1
55
Bis(2-chloroisopropyl)ether
35
10
ug/L
50.0
1.3 U
70
36-166
2
46.3
Bis(2-ethylhexyl)phthalate
41
5.0
ug/L
50.0
1.7 U
82
10-158
3
41.1
Butylbenzylphthalate
49
10
ug/L
50.0
2.0 U
97
10-152
2
25
Chrysene
40
10
ug/L
50.0
2.0 U
81
17-168
0.9
48.3
Dibenzo(a,h)anthracene
53
10
ug/L
50.0
2.3 U
106
10-227
1
70
Diethylphthalate
41
10
ug/L
50.0
2.1 U
82
62-127
4
11
Dimethylphthalate
41
10
ug/L
50.0
1.4 U
81
10-114
6
26.5
Di-n-butylphthalate
42
10
ug/L
50.0
1.5 U
83
10-118
6
25
Di-n-octylphthalate
45
10
ug/L
50.0
3.1 U
90
10-146
6
31.4
DPH (as Azobenzene)
39
10
ug/L
50.0
1.9 U
78
69-108
0.5
36
Fluoranthene
40
10
ug/L
50.0
2.1 U
80
26-137
0.8
32.8
Fluorene
37
10
ug/L
50.0
1.7 U
74
59-121
1
25
Hexachlorobenzene
40
10
ug/L
50.0
1.0 U
79
10-152
2
25
Hexachlorobutadiene
36
10
ug/L
50.0
1.2 U
73
24-116
2
26.3
Hexachlorocyclopentadiene
35
10
ug/L
50.0
1.3 U
71
10-99
5
50
Hexachloroethane
29
10
ug/L
50.0
1.1 U
57
12-82
3
50,
Indeno(1,2,3-cd)pyrene
52
10
ug/L
50.0
2.2 U
105
10-171
0.6
44.6
Isophorone
34
10
ug/L
50.0
1.3 U
69
21-196
1
63.3
Naphthalene
34
10
ug/L
50.0
1.3 U
69
21-133
1
30.1
Nitrobenzene
34
10
ug/L
50.0
1.2 U
68
35-180
2
39.3
N-Nitrosodimethylamine
27
10
ug/L
50.0
1.3 U
55
24-94
4
36
N-Nitroso-di-n-propylamine
36
10
ug/L
50.0
1.5 U
61
10-230
0.9
55.4
Pentachlorophenol
42
10
ug/L
50.0
1.8 U
84
51-135
0.2
25
Phenanthrene
39
10
ug/L
50.0
1.4 U
78
54-120
0.9
25
Phenol
21
10
ug/L
50.0
1.4 U
41
19-78
7
25
Pyrene
42
10
ug/L
50.0
2.1 U
83
52-115
0.2
25
Notes
QM-07
QM-11
2,4,6-Tribromophenol 81
u91L
100
81
18-157
2-Fluorobiphenyl 38
u91L
50.0
76
15-139
2-Fluorophenol 50
u91L
100
50
10-104
Nitrobenzene-d5 34
u91L
50.0
68
16-140
Phenol-d5 38
u91L
100
38
10-83
Terphenyl-d14 43
u91L
50.0
86
23-164
Semivolatile Organic Compounds by GC - Quality Control
Batch 4MY003 - EPA 3510C
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 21

QUALITY CONTROL DATA
Semivolatile Organic Compounds by GC - Quality Control
Batch 4BO9003 - EPA 3510C - Continued
Blank (4B09003-BLK3) Prepared: 02/09/2014 07:54 Analyzed: 02/14/2014 11:44
Spike
Source %REC RPD
Analyt
Result
Flaa
Q
Units
Level
Result %REC Limits RPD Limit Notes
4,4'-DDD
0.044
U
0.050
ug/L
4,4'-DDE
0.048
U
0.050
ug/L
4,4'-DDT
0.049
U
0:050
ug/L
Aldrin
0.041
U
0.050
ug/L
alpha-BHC
0.036
U
0.050
ug/L
beta-BHC
0.036
U
0.050
ug/L
Chlordane (n.o.s.)
0.020
U
1.0
ug/L
Chlordane (tech)
0.20
U
0.50
ug/L
delta-BHC
0.048
U
0.050
ug/L
Dieldrin
0.045
U
0.050
ug/L
Endosulfan I
0.045
U
0.050
ug/L
Endosulfan II
0.036
U
0.050
ug/L
Endosulfan sulfate
0.032
U
0.050
ug/L
Endrin
0.041
U
0.050
ug/L
Endrin aldehyde
0.042
U
0.050
ug/L
gamma-BHC
0.034
U
0.050
ug/L
Heptachlor
0.030
U
0.050
ug/L
Heptachlor epoxide
0.037
U
0.050
ug/L
Toxaphene
0.22
U
1.0
ug/L
2,4,5,E-TCMX
1.1
u91L
1.00
108 44-134
Derachlorobiphenyl
0.70
u91L
1.00
70 37-149
LCS (4B09003-BSI)
Prepared: 02/09/2014 07:54 Analyzed: 02/14/2014 11:57
Spike
Source
%REC
RPD
Anayte
Result Elan
PQL
Units
Level
Result
"/DREG
Limits RPD
Unift Notes
4,4'-DDT
1.1
0.050
ug/L
1.00
110
37-160
Aldrin
1.1
0.050
ug/L
1.00
106
42-122
Dieldrin
1.0
0.050
ug/L
1.00
105
36-146
Endrin
1.0
0.050
ug/L
1.00
105
30-147
gamma-BHC
1.0
0.050
ug/L
1.00
104
19-140
Heptachlor
0.98
0.050
ug/L
1.00
98
45-122
2,4,5,E-TCMX
0.94
u91L
1.00
94
44-134
Dsrarhlorab1phenyl
0.93
u91L
1.00
93
37-149
Matrix Spike (4B09003-MS1)
Prepared: 02/09/2014 07:54 Analyzed: 02/14/2014 12:10
Source: C400990-03
Spike
Source
%REC
RPD
_Analvte
Result Flag
P-M
Unib
Level
Result
%REC
Limits RPD
Limit Notes
4,4'-DDT
1.2
0.050
ug/L
1.00
0.049 U
121
35-160
Aldrin
1.1
0.050
ug/L
1.00
0.041 U
106
42-122
Dieldrin
1.1
0.050
ug/L
1.00
0.045 U
107
36.146
Endrin
1.1
0.050
ug/L
1.00
0.041 U
107
30-147
gamma-BHC
1.1
0.050
ug/L
1.00
0.034 U
108
19-140
Heptachlor
1.0
0.050
ug/L
1.00
0.030 U
103
45-122
2, 4, 5, 6-TCMX
1.0
u91L
1.00
100
44-134
Decachlorobiphenyl
1.1
u91L
1.00
109
37-149
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 21

QUALITY CONTROL DATA
Semivolatile Organic Compounds by GC - Quality Control
Batch 4BO9003 - EPA 3510C - Continued
Matrix Spike Dup (4809003-MSD3)
Prepared: 02/09/2014 07:54 Analyzed: 02/14/2014 12:24
Source: C400990-03
Spike
Source
%REC
RPD
Anal vte
Resul Fleg
P L
ni
Level
Result
%REC
Lim'
RPD
i i Notes
4,4'-DDT
1.2
0.050
ug/L
1.00
0.049 U
122
35-160
1
25
Aldrin
1.1
0.050
ug/L
1.00
0.041 U
107
42-122
0.5
25
Dieldrin
1.1
0.050
ug/L
1.00
0.045 U
108
36-146
1
25
Endrin
1.1
0.050
ug/L
1.00
0.041 U
108
30-147
1
25
gamma-BHC
1.1
0.050
ug/L
1.00
0.034 U
110
19-140
1
25
Heptachlor
1.0
0.050
ug/L
1.00
0.030 U
105
45-122
2
32
2,4,5,E-TCMX
Decachl-v&phenyl
Batch 4809004 - EPA 3510C
a98
1.0
u91L
u91L
1.00 98 44-134
1.00 104 37-149
Blank (4B09004-BLKI)
Prepared: 02/09/2014 08:00 Analyzed: 02/14/2014 11:44
Spike Source %REC RPD
Ana
Result
Elan
POL
Units
Level Result %REC Urni RPD Limit Notes
PCB-1016/1242
0.43
U
0.50
ug/L
PCB-1221
0.37
U
0.50
ug/L
PCB-1232
0.45
U
0.50
ug/L
PCB-1248
0.014
U
0,50
ug/L
PCB-1254
0.37
U
0.50
ug/L
PCB-1260
0.45
U
0.50
ug/L
2,4,5,E-TCMX
1.0
u91L
1.00 103 45-151
Decachloru&phenyl
0.67
tg/L
1.00 67 42-159
LCS (4B09004-BSI)
Prepared: 02/09/2014 08:00 Analyzed: 02/14/2014 12:37
Spike Source %REC RPD
Analyt
Result Flan P9l.
Units
Level Result %REC Limits RPD Limit Nis
PCB-1016/1242
11 0.50
ug/L
10.0 107 50-114
PCB-1260
11 0.50
ug/L
10.0 106 8-127
2,4,5,E-TCMX
0.99
u91L
1.00 99 45-151
Decachlorobiphenyl
0.98
u91L
1.00 98 42-159
Matrix Spike (4809004-MSi)
Prepared: 02/09/2014 08:00 Analyzed: 02/14/2014 12:50
Source: C400990-03
Spike Source %REC RPD
-Anallde
Result Ela9 PQL
Units
Level Result %REC Limits RPD Limit Notes
PCB-1016/1242
11 0.50
ug/L
10.0 0.43 U 107 50-114
PCB-1260
11 0.50
ug/L
10.0 0.45 U 112 8-127
2,4,5,E-TCMX
1.1
LVA
1.00
108
45-151
Decachlorobiphenyl
1.0
u91L
1.00
104
41-159
Matrix Spike Dup (4B09004-MSDI)
Prepared: 02/09/2014 08:00 Analyzed: 02/14/2014 13:03
Source: C400990-03
Spike
Source
%REC
RPD
Anal vte
Rewlt Mau P9l.
-Unib
Level
Result %REC
Limits RPD
Limit Notes
PCB-1016/1242
11 0.50
ug/L
10.0
0.43 U 108
50-114 0.5
25
PCB-1260
11 0.50
ug/L
10.0
0.45 U 113
8-127 0.8
25
2,4,5,E-TC74X
1.0
u91L
1.00
101
45-151
Decachlorobiphenyl
1.1
u91L
1.00
110
42-159
FINAL Tt�s report relates only to the sample as received by the laboratory, and may only be reproduced (n full. Page 19 of 21

FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
7 The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, the impact
on data quality is minimal.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable LCS recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is
ND, the impact on data quality is minimal.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 21

�
'
LL
PER
MM-
DIWF
P�210i"

STORMWATER DISCHARGE OUTFALL (SDO)
QUALITATIVE MONITORING REPORT
BMP Checklist #6
NPDES PERMIT NO. /UC G 03001 z-
FACILITY: M a ew eA- /vld,-
COUNTY: L e e-,
PHONE7'74,-
INSPECTOR:
DATE: Z 0 j
OUTFALL No.
OUTFALL TYPE:
RECEIVING STREAfd:
SDO-00
0 INLET :►'PIPE 1) FLUME
✓Wet weather observation n Dry weather observation
1:1 Flow during dry weather u No flow during dry weather a Standing water during dry weather
Describe the industrial activities occurring within the outfall drainage area.
COLOR - Describe the discharge color (e.g. red, brown, green, blue) and tint (e.g., light, medium, dark).
C-i t,,/
ODOR - Describe any distinct odors (e.g. gasoline, rotten eggs, chlorine) the discharge may have.
N V'N
CLARITY - Choose the number that best ranks the clarity of the discharge, where 1 is clear and 10 is very
cloudy.
1 2 b 4 5 6 7 8 9 10
FLOATING SOLIDS - Choose the number that best ranks the amount of floating solids in the discharge,
where 1 is no solids and 10 Is the surface covered with floating solids.
1 2 /Jt) 4 5 6 7 8 9 10
SUSPENDED SOLIDS - Choose the number that best ranks the amount of suspended solids in the discharge,
where 1 is no solids and 10 is xtrenrely. muddy.
1 V 3 4 5 6 7 8 9 10
FOAM -
Is there any foam on or in the stormwater discharge? yes
OIL SHEEN -
is there oil sheen visible in the stonnwatw discharge or at the outran? yes
DEPOSITION AT OUTFALL -
Are there sediment or other inaLerial deposits below the outfall? yes re
EROSION AT OUTFALL -
Is there erosion at or immediately below the outfall? yes
List and describe otter obvious indicators of storrnwater pollution:
By this signature, ) certify OW this report is accurate a cornpkpte
�AZt r
4 K &-& 1+ crw"
-
Pig 's Signature nspedors Signature

FIRST ANALYTICAL LABORATORIES
biu,ng PO Box 110372 -Research Triangle Park. NC 27709 TEL: [phone]
.dipping -31- Precision Drive. Suite 101 - Raleigh. NC '2761 % F bLX: 919 882 1603
«-%rn.firstanalpticallabs.cau
EPA Method 200 Analysis Report
FAL Project #: 140221.1 Report Date: 2/20/2014
Client: Cameron Testing Services Date Received: 2/10/2014
Client Project ID: 140096
Sample Name: 140096-05 - SW#1
Concentration in Original Sample
Conc.
RL
Analyte
(mg/L)
(mg/L)
Copper (Cu)
0.018
0.001
Lead (Pb)
0.009
0.001
Zinc (Zn)
0.142
0.005
Approved by:
Matt Loftis, Laboratory Manager

®FIRST ANALYTICAL; LABORATORIES
1 KEm,I111!7.e,w
.,_ Rech Tn.urcle Fart' NC27709 TEL")I'('�r7 $aU CHAINOe CUSTODY
'?IR.I, JL Nr' 7'(•1 - F.i\ '11•> 3�'_ Ih, �3
x�ne fuvanal�yru�llahr a•m
Client:
Cameron Testing Proj. Name/No: 140096
Contact:
Chris Cameron
Address:
219 S. Steele St. Sanford, NC 27330
Phone No.,
919-208-4240 email: chrisCcDcamerontestina.com
Purchase Order#:
Note To Lab:
140221
Collection
No. Samole ID Description Date Time Matrix Preservative Analysis Reauired
1
140096-05
SW #1
2/3/2014
1107
WW
HNO3
Cu, Pb, Zn
2
3
4
5
6
7
8
9
10
Pdftulshed By, D teegp g:
/ 00
Page _L at
Received By: ote/Time:
Relinquished By: Date/Time:
Received Lab: Date/Time-
/.041

s steels Str. Cameron Testing Services, Inc. Chain of Custody
Sanford. NC 27330 g r , t / y Page _� of
Phone: [phone] NC WW/GW Can. i/654 NC PHHS Cert !! 37799 US EPA NC01918 ��T t? , 5
Company: Magneti-Marelli
—
E118!
James.Selerd(JMagneliMarelli.com
BT&lab use Only
"GOntaCt: James Siler Phono
ir'
919.721-1353
_
SemrpC, emp , 5 oG Prof.
Jib Oper}6
vAdd�esS i yFax:
r- : �� 2101 Nash St.
T`Blank Arnve
, �(YlN1NA)
(City, State;
�t Zip) Sanford, NC 27330 'Notes:
tt`' Due
1
Project: 2D%L1 S0 1*-)
p
, Regulatory Rush
'; 1N) g (YIN)
Colloctod: Name:
Signafuro:
Sample Information
E;.
,Number df,,bdfflds
Sample ID
`
N a� x
M E a
Z
_
}
m
N
U N "
O m
V E J a:N
H
m
o
Requested Analysis
�'CTS Lab
ID
a
s $ -
ULL
a �GQc
a�3\l �uoo
Y
wl
04 I; - 0
o Z
3
14
C
�431if I ,
1'
0¢
(A'
e uished:
Received:
Date Ime
Rush work will require prior approval. Additional charges will apply

Cameron Testing Services, Inc. Laboratory Report
Client, Magneti-Marelli CTS Pr0j.
Project: 2014 SW i#1 Regulatory
Sample Information
Sampled J. Sher Date 02/03/14 Received
Analyses and Results
NC DENR N664
WC PHHS #37799
Us EPA #NC01918
140096
Yes
C. Cameron Date 02103114
Lab I0 Sample'ID m o. `2 Analyte Result c A16 Std. Mathods
g V O ¢ c a ° Reference
' d
140096, 01 Outfall A sw c. pi i 60 s u a 02/04114 DPK 4500 H B • pH
TSS 32.3 ro''L 26 02107/14 DPK 2540 0 - TSS
02 Outfall B SW Or O&C-W c5.0 M3,1 5 02105114 OPK EPA 1664A
03 Outfall C sv r1 EPA 6241625
04 Outfall D SW Or EPA608
05 Outfall E s:V Q h4cfals
TTO for samples -03 and -04 analyzed by ENCO; report attached.
Metals analyzed by FAL; report attached.
Metals = Cu, Pb, Zn
Data r I
RevWw
I
Lab T lan
+
Report
Review O/
Lab Director
3 i 9 S. SteeU: Su'.
Sa fo(d NC 273 30
Oil, zi?
Date
919-1094240
clxisQ`,7ca��rmteuir�.mm

C-'O Laboratories
v, o
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Friday, February 21, 2014
Cameron Testing Services, Inc. (CA039)
Attn: Chris Cameron
219 South Steele Street
Sanford, NC 27330
RE: Laboratory Results for
Project Number: 140096, Project Nakne/Desc: TTO
ENCO Workorder(s): C401556
Dear Chris Cameron,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, February 7, 2014.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative. This report shall not be reproduced except in full, without
the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
Link Thrower
Project Manager
Enclosure(s)
FINAL TNs report relates orgy to the sample as received by the laboratory, and may oNy be reproduced In full. Page 1 of 21

-i•
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: 140D96-03
Lab ID:
C403556-01
Sampled: 02/03/14 11:02 Received: 02/07/14 15:55
Parameter
EPA 624
Hold Date/Time(s)
02/17/14
preo Date/Time(s)
02/07/14
analysis Date/Time(s)
10:31 02/11/14 10:37
Client ID: 140096-04
Lab ID:
C401556-02
Sampled: 02/03/1411:03 Received: 02/07/14 IS:
Parameter
EPA 608
Hold Date/Time(s)
02/10/14
03/21/14
prep Date/rime(s)
02/09/14
AnaWs bate/Time(s)
07:54 02/14/14 13:16
EPA 608
02/03/15
03/21/14
02/09/14
08:00 02/14/14 13:16
EPA 625
02/10/14
03/20/14
02/08/14
22:53 02/11/14 18:07
Client ID: Trip Blank Lab ID: C401556-03 Sampled: 02/03/14 12:02 Received: 02/07/14 15:55
Parameter Hold Date/Time(s) $sp Date/Timefs) Analvsis Date/Time(s)
EPA 624 02/17/14 02/07/14 10:31 02/11/14 11:07
FINAL This report relates oriy to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 21

SAMPLE DETECTION SUMMARY
I Client ID: Trip Blank Lab M: C401556-03
AB.alyte Results on WL E" Units 1'9.eClled H=
Chloroform 0.53 1 0.18 1.0 ug/L EPA 624
FINAL This report relates orJy to the sample as received by the laboratory, and may ally be reproduced In full. Page 3 of 21

www.encolabs.com
ANALYTICAL RESULTS
Description: 140096-03 Lab Sample ID:C401556-01
Received: 02/07/1415:55
Matrix: Water Sampled:02/03/14 11:02
Work Order: C401556
Project: TTO Sampled By:3ames Siler
Volatile Organic Compounds by GCMS
^ - EAY'O Cxy mr ed a-W [ABC 5911
Analvte FCAS Numberl
Results
Elan
Units
gE
M"
M
@Auft
Method
Analyzed
Ax MCI
1,1,1-Trichloroethane [71-55-6]^
< 0.12
ug/L
1
0.12
1.0
4B10032
EPA 624
02/11/14 10:37
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
< 0.28
ug/L
1
0.28
1.0
4B10032
EPA 624
02/11/14 10:37
REF
1,1,2-Trichloroethane [79-00-5]^
< 0.14
ug/L
1
0.14
1.0
4B10032
EPA 624
02/11/14 10:37
REF
1,1-Didhloroethane [75-343]^
< 0.13
ug/L
1
0.13
1.0
4B10032
EPA 624
02/11/14 10:37
REF
1,1-Dichloroethem [75-354]^
< 0.21
ug/L
1
0.21
1.0
4B10032
EPA 624
02/11/14 10:37
REF
1,2-Dichlorobenzene [95-50-1]^
< 0.19
ug/L
1
0.19
1.0
4B10032
EPA 624
02/11/14 10:37
REF
1,2-Dichloroethane[107-06.2]^
< 0.21
ug/L
1
0.21
1.0
4810032
EPA 624
02/11/14 10:37
REF
1,2-Dithloropropane [78-87-5]^
< 0.10
ug/L
1
0.10
1.0
4B10D32
EPA 624
02/11/14 10:37
REF
1,3-Dichlorobepme [541-73-1]^
< 0.15
ug/L
1
0.15
1r0
4B10032
EPA 624
02/11/14 10:37
REF
1,4-Dkhlorobenzene [106-46-7]^
< 0.19
ug/L
1
0.19
1.0
4810032
EPA 624
02/11/14 10:37
REF
2-Chloroethyl Vinyl Ether [110-75-8]^
< 1.1
ug/L
1
1.1
5.0
4B10032
EPA 624
02/11/14 10:37
REF
Acrolein [107-02-8]^
< 4.0
ug/L
1
4.0
10
4B10032
EPA 624
02/11/14 10:37
REF
Acrylonraile [107-13-1]^
< 3.5
ug/L
1
3.5
10
4810032
EPA 624
02/11/14 10:37
REF
Benzene [7143-2]^
< 0.15
ug/L
1
0.15
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Bromodichloromethane [75-27-4]^
< 0.17
ug/L
1
0.17
1.0
4810032
EPA 624
02/11/14 10:37
REF
Bromoform [75-25-2]^
< 0.2.2
ug/L
1
0.22
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Bromomethane [74-83-9]^
< 0.14
ug/L
1
0.14
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Carbon Tetrachloride [56-23-5]^
< 0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Chlorobenzene [108-9D-7]^
< 0.17
ug/L
1
0.17
1.0
4BID032
EPA 624
02/11/14 10:37
REF
Chloroethane [75-00-3]^
< 0.23
ug/L
1
0.23
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Chloroform [67-66-3]^
< 0.18
ug/L
1
0.18
1.0
4810032
EPA 624
02/11/14 10:37
REF
Chloromethane [74-87-3]^
< 0.13
ug/L
1
0.13
1.0
4810032
EPA 624
02/11/14 10:37
REF
cis-1,3-Dichloropropene [10061-M-5]^
< 0.20
ug/L
1
0.20
1.0
4810032
EPA 624
02/11/14 10:37
REF
Dibromochloromethane [124-48-1]^
< 0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Ethylbenzene [100414]^
< 0.13
ug/L
1
0.13
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Methylene Chloride [75-09-2]^
< 0.23
ug/L
1
0.23
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Tetradhloroedme [127-184]^
< 0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Toluene [108-88.3]^
< 0.14
ug/L
1
0.14
1.0
4B10032
EPA 624
02/11/14 10:37
REF
trans-1,2-Dichloroetlnene [156-60-5]^
< 0.21
ug/L
1
0.21
1.0
4B10032
EPA 624
01/11/14 10:37
REF
trans-1,3-Dkhloropropene [10061-02-6]^
< 0.15
ug/L
1
0.15
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Tridrloroethene [79-01-6]^
< 0.15
ug/L
1
0.15
1.0
4B10032
EPA 624
02/11/14 10:37
REF
Vinyl chloride [75-014]^
< 0.32
ug/L
1
032
1.0
4B10032
EPA 624
02/11/14 10:37
REF
suffaaaftsBaSaSflSF
RE
spift 6Y!
% Rec
% Rec
umltc
Ldffh
lIC
9
Notes
40ronroAuavbemerre
37
1
Mo
74 %
51-122
Mow
EPA 624
0211111410.37
REF
00romo0uoromerhane
41
I
50.0
82 %
58-117
4610032
EPA 624
0211411410:37
REF
Toluene-d8
41
1
50.0
83 %
67-127
4810032
EPA 624
0211111410.37
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in fun. Page 4 of 21

www.encolabs.com
ANALYTICAL RESULTS
Description: 140096-04 Lab Sample ID:C401556-02
Received: 02/07/14 15:55
Matrix: Water Sampled: 02/03/14 11:03
Work Order. C401556
Project: TTO Sampled By:7ames Siler
ISemivolaiile Organic Compounds by GCMS
^-EAKVUrycerbiwanayle/NC591]
.
Anahft rCAS Numbed
Results E619
Units
2E
Kb
1L
fiai♦h
Method
Analyzed
g11 E21M
1,2,4-Trirhlorobenzene [120-82-1]^
< 1.2
ug/L
1
1.2
10
4BO8010
EPA 625
02/11/14 18:07
DFM
1,2-Dichlorobenzene[95-50-1]^
< 1.1
ug/L
1
1.1
10
4808010
EPA 625
02/11/14 18:07
DFM
1,3-Dichlorobenzene [541-73-1]^
< 1.1
ug/L
1
1.1
10
4008010
EPA 625
02/11/14 18:07
DFM
1,4-Dichlorobenzene [106-46-7]^
< 1.0
ug/L
1
1.0
10
4BOB010
EPA 625
02/11/14 18:07
DFM
1-Methylnaphthalene [90-12-0]^
< 1.7
ug/L
1
1.7
10
4BOB010
EPA 625
02/11/14 18:07
DFM QL-02
2,4,5-Tridllorophenol[95.95.4]^
< 1.0
ug/L
1
1.0
10
4808DIO
EPA 625
02/11/14 18:07
DFM
2,4,6-Tridtlorophenol[88-06-2]^
< 1.1
ug/L
1
1.1
10
4808010
EPA 625
02/11/14 18:07
DFM
2,4-Dichlorophenol1120-83-2]^
< 1.4
ug/L
1
1.4
10
4B08010
EPA 625
02/11/14 18:07
DFM
2,4-Dimethy1phenol[105.67-9]^
< 1.3
ug/L
1
1.3
10
4BOB019
EPA 625
02/11/14 18:07
DFM
2,4-Dinitrophenol[51-28-5]^
< 2.6
ug/L
1
2.6
10
4BO8010
EPA 625
02/11/14 18:07
DFM
2,4-Dinitrotoluene [121-14-2]^
< 2.4
ug/L
1
2.4
10
4BOB010
EPA 625
02/11/14 1B:07
DFM
2,6-Dinitrotoluene [606-20-2]^
< 1.5
ug/L
1
1.5
10
4BOB010
EPA 625
02/11/14 18:07
DFM
2-Chloronaphthalene [91-58-7]^
< 1.0
ug/L
1
1.0
10
4SO8010
EPA 625
02/11/14 18:07
DFM
2{hlorophenol[95.57-8]^
< 1.2
ug/L
1
1.2
10
4808010
EPA 625
02/11/14 18:07
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
< 2.9
ug/L
1
2.9
10
4808010
EPA 625
02/11/14 18:07
DFM
2-Methylnaphthalene [91.57-6]^
< 1.5
ug/L
1
1.5
10
4BOB010
EPA 625
02/11/14 18:07
DFM
2-Nitrophenol[88-75-5]^
< 1.1
ug/L
1
1.1
10
48GW10
EPA 625
02/11/14 18:07
DFM
3,3'-Dichlorobenzidine [91-94-1]^
< 3.3
ug/L
1
3.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
4-Bromophenyl-phenylether [101-55-3]^
< 1.0
ug/L
1
1.0
10
4B08010
EPA 625
02/11/14 18:07
DFM
4-Oloro-3-methylphenol [59-50-7]^
< 1.5
ug/L
1
1.5
10
4808010
EPA 625
02/11/14 18:07
DFM
4-Mlorophenyl-phenylether(7005-72-3]^
< 1.6
ug/L
1
1.6
10
4BOB010
EPA 625
02/11/14 18:07
DFM
4-Nitrophenol[10D-02-7]^
< 2.0
ug/L
1
2.0
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Acenaphthene [83-32-9]^
< 1.4
ug/L
1
1.4
10
4B00010
EPA 625
02/11/14 18:07
DFM
Acenaphthylem [208-96-8)^
< 1.2
ug/L
1
1.2
10
4808010
EPA 625
02/11/14 18:07
DFM
Anthracene [120-12-7]^
< 1.6
ug/L
1
1.6
10
4BOB010
EPA 625
OZ/11/14 18:07
DFM
Benzidine [92-87-5]^
< 1.6
ug/L
1
1.6
10
4B08010
EPA 625
OZ/11/14 18:07
DFM
Benzo(a),Tnthracene [56-55-3]^
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Benzo(a)pyrene [5D-32-8]^
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Benzo(b)fluorandwe [205-99-2]^
< 1.0
ug/L
1
1.0
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Benzo(g,h,i)perylene [191-24-2]^
< 2.4
ug/L
1
2.4
10
4BOB010
EPA 625
02/11/14 18:07
DFM QV-01
Benzo(k)Ruorantfiene [207-08-9]^
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Benzoic add [65-85-0]^
< 1.0
ug/L
1
1.0
50
4BO8010
EPA 625
02/11/14 18:07
DFM
Bis(2-ch1oroethozy)mMhane[111-91-1]^
< 1.4
ug/L
1
1.4
10
4BOB010
EPA 625
02/11/14 18:07
DFM
ais(2thloroethyl)ether [111-44-4]1
< 1.2
ug/L
1
1.2
10
4SO8010
EPA 625
02/11/14 18:07
DFM
9is(2-ddoroisopropyl)ether [108-00-1]^
< 1.3
ug/L
1
1.3
10
4BOB010
EPA 625
02/11/14 18:07
DFM
Bis(2-ethylhexyl)phthatate [I17-81-7]^
< 1.7
ug/L
1
1.7
5.0
4BO8010
EPA 625
02/11/14 18:07
DFM
Butylbenzylphthalate [85.68-7]^
< 2.0
ug/L
1
2.0
10
4508010
EPA 625
02/11/14 18:07
DFM
Chrysene [218-01-9]^
< 2.0
ug/L
1
2.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Dibenw(a,h)antfvacene (53.7D-3]^
< 2.3
ug/L
1
2.3
10
4SO8010
EPA 625
02/11/14 18:07
DFM
Diethylphthalate [84-66-2)^
< 2.1
ug/L
1
2.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Dimethylphthalate [131-11-3]^
< 1.4
ug/L
1
1.4
10
4808010
EPA 6Z5
02/12/14 18:07
DFM
Di-n-butylphthalate [84-74-2]^
< 1.5
ug/L
1
1.5
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Di-n-cctylphthalate [117-84-0]^
< 3.1
ug/L
1
3.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
DPH (as Azobenzene)[103-33-3]^
< 1.9
ug/L
1
1.9
10
4808010
EPA 625
02/11/14 18:07
DFM
Ftuorandwe [20644-0]^
< 2.1
ug/L
1
2.1
10
4SO8010
EPA 625
02/11/14 18:07
DFM
Fluorene [86-73-7]^
< 1.7
ug/L
1
1.7
10
4808010
EPA 625
02/11/14 18:07
DFM
Hexadelorohenzene [118-74-1]^
< 1.0
ug/L
1
1.0
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Hexaddorobutadiene[87-68-3]^
< 1.2
ug/L
1
1.2
10
4B08010
EPA 625
02/11/14 18:07
DFM
FINAL
This report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 5 of 21

ANALYTICAL RESULTS
Description: 140096-04 Lab Sample ID:C401556-02 Received: 02/07/1415:55
Matrix: Water Sampled:02/03/14 11:03 Work Order. C401556
Project: TTO Sampled By:lames Siler
ISemivolatile Organic Compounds by GCMS
^ - ENCO Cary cw&kd -41e /AC 5911
..
.
Analyte IcAS Numberl
JResultr 8M
Mab
RE
MX
EM
fiatsh
Method
Anali wil
01 Notes
Hexachlorocydopentadiene [77-47-4]^
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Hexachloroethane[67-72-1]^
< 1.1
ug/L
1
1.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
< 2.2
ug/L
1
2.2
10
4B08010
EPA 625
02/11/14 18:07
DFM
Isophorone [78-S9-I]^
< 1.3
ug/L
1
1.3
10
4B08010
EPA 625
02/11/14 18:07
DFM
Naphthalene [91-20.3]^
< 1.3
ug/L
1
1.3
10
4B08010
EPA 625
02/11/14 18:07
DFM
Nitrobenzene [98-95-3]^
< 1.2
ug/L
1
1.2
10
4B08010
EPA 625
02/11/14 18:07
DFM
N-Nltrosodimethylamine [62-75.9]^
< 1.3
ug/L
1
1.3
10
4BO8010
EPA 625
02/11/14 18:07
DFM
N-Nitroso-di-n-propylamine [621-64-7]1
< 1.5
ug/L
1
1.5
10
4BO8010
EPA 625
02/11/14 18:07
DFM
N-Nihnsodiphenylamine/Diphenylamine
< 2.1
ug/L
1
2.1
10
4B08010
EPA 625
02/11/14 18:07
DFM
(86-3D-6/122-39-4]^
Pentachlorophenal[87-86-5]^
< 1.8
ug/L
1
1.8
10
4BO8010
EPA 625
02/11/14 18:07
DFM
Phenanthrene[85-01-8]^
< 1.4
ug/L
1
1.4
10
4B08D10
EPA 625
02/11/14 18:07
DFM
Phenol[108-95-2]^
< 1.4
ug/L
1
1.4
10
4B08010
EPA 625
02/11/14 18:07
DFM
Pyrene [129-00.0]^
< 2.1
ug/L
1
2.1
10
4BO8010
EPA 625
02/11/14 18:07
DFM
SUMM&E
1,4,6-7nbn-gpheno1
1-R-robipheny/
2-Rrarophenol
N&obenrene-dS
Phenol-d5
Terpheny4-d14
82
33
46
30
36
45
RE
1
1
1
1
1
1
SA fire
100
50.0
100
50.0
100
50.0
% Ret
82%
67 %
46 %
6096
36 %
91 %
46 RetUmlt r
18-157
15-139
10-104
16-140
10-83
23-164
ApM&
4BO8010
4BU8010
4BO8010
4BO8010
4BO8010
4B08010
EPA 625
EPA 625
EPA 625
EPA 625
EPA 615
EPA 625
B
0211111418.07
01/11/1418.07
0211111418:07
01/Il/1418:07
OW1/1418:07
01111/1418:07
By N.4tle4
DRN
DRN
DFM
DFM
DFM
DFM
Semivolatile Organic Compounds by GC
^ - EM17 Cary avtlhed aa*te [AC 5911
.
Analvte IcAS Numberl
1iesulb
fin
1to[m
PE
1!1!?L
EQL
AlUh
Method
Analyzed
4,4'-DDD [72-54-B]^
< 0.044
ug/L
1
0.044
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
4,4'-DDE [72-55-9]^
< 0.048
ug/L
1
0.046
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
4,4'-DDT [50-29.3]^
< 0.049
ug/L
1
0.049
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Aldrin [309-0D-2]^
< 0.041
ug/L
1
0.041
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
alpha-BHC [319-84-6]^
< 0.036
ug/L .
1
0.036
0.050
4BO9003
EPA 608
02/14/14 13:26
MWC
beta-BHC (319-85-7]^
< 0.036
ug/L
1
0.036
0.050
4SO9003
EPA 608
02/14/14 13:16
MWC
Chlordane (n.os.)[57-74-91^
< 0.020
ug/L
1
0.020
1.0
4BO9003
EPA 608
02/14/14 13:16
MWC
Chlordane (tech) [12789-03-6]^
< 0.20
ug/L
1
0.20
0.50
4BO9003
EPA 608
02/14/14 13:16
MWC
delta-BHC [319-86-8]^
< 0.048
ug/L
1
0.048
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Dieldrin [60-57-1]^
< 0.045
ug/L
1
0.045
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Endowlfan I [959-98-8]
< 0.045
ug/L
1
0.045
0.050
4BD9003 _
EPA 608
02/14/14 13:16
MWC
Endosulfan II [33213-65-9]^
< 0.036
ug/L
1
0.036
0.050
4SO9003
EPA 608
02/14/14 13:16
MWC
Endosulfan sulfate [1031-07-8]^
< 0.032
ug/L
1
0.032
0.050
4SO9003
EPA 608
02/14/14 13:16
MWC
Endrin [72-2D-B]^
< 0.041
ug/L
1
0.041
0.050
4BO9003
EPA 608
02/14/14 13:16
MWC
Endrin aldehyde [7421-93-4]^
< 0.042
ug/L
1
0.042
0.050
4BD9003
EPA 608
OZ114/14 13:16
MWC
gamma-BHC [58-89-9]^
< 0.034
ug/L
1
0.034
0.050
4BD9003
EPA 608
0Zt14/14 13:16
MWC
Heptachlor V6-44-8]^
< 0.030
ug/L
1
0.030
0.050
41309003
EPA 608
02/14/14 13:16
MWC
Heptachlor epoxide [1024-57-3]^
< D.037
ug/L
1
0.637
0.050
4SM03
EPA 608
02/14/14 13:16
MWC
PCB-1016/1242 [12674-11-2/53469-21-9]^
< 0.43
ug/L
1
0.43
0.50
4BO9004
EPA 608
02/14/14 13:16
MWC
PCB-1221 [11104-28-2]^
< 0.37
ug/L
1
0.37
0.50
4BO9004
EPA 608
02/14/14 13:16
MWC
PCB-1232 [11141-16-5]^
< 0.45
ug/L
1
0.45
0.50
4SO9004
EPA 608
02/14/14 13:16
MWC
PCB-1248 [12672-29-6]^
< 0.014.
ug/L
1
0.014
0.50
4SM04
EPA 608
02/14/14 13:16
MWC
PCB-1254 [11097-69-1]^
< 0.37
ug/L
1
0.37
0.50
4BO9004
EPA 608
02/14/14 13:16
MWC
FINAL
Ms report relates only to the sample as received by the
laboratory, and may only be reproduced in full.
Page 6 of 21

ANALYTICAL RESULTS
Description: 140096-04 Lab Sample ID: C401556-02 Received: 02/07/14 15:55
Matrix: Water Sampled: 02/03/14 11:03 Work Order: C401556
Project: TTO Sampled ByJames Siier
JSemivolatile Organic Compounds by GC
^-ENCOCary ceGK[dan 6*(AC 5911
Anahtte lcAS Numberl
Results
E[Ag
MORE
QE
MU EQL
patch
Method
Analyzed
Sy !lobes
PCB-1260 [11096-82-5]^
< 0.45
ug/L
1
0.45 030
4609004
EPA 608
02/14/14 13:16
MWC
Toxaphene [8001-35-2]^
< 0.22
ug/L
1
0.22 1.0
4BO9003
EPA 608
02/14/14 13:16
MWC
Sunwimtes
PF
Apike 4
% Rec
% Rec
00
AY Notes
2,4,5,E-TCMX
0.99
1
1.00
9996
44-134
4809003
EPA 608
a?114/1413.16
MWC
2,4,5,E-70a
0.99
1
1.00
99 %
45-151
4BU9004
EPA 608
0211411413.16
MWC
Decachlwvbipheny/
a96
I
1.00
96 %
37-149
4BU9003
EPA 608
0211411413:16
MWC
0eachl—bipheiry/
0.96
1
1.00
96 %
42459
4809004
EPA 608
0211411413:16
MWC
KNAL This report relates oNy to the sample as reoeived by d,e laboratory, and may w4 be reproduced in full. Page 7 of 21

www.encolabs.com
ANALYTICAL RESULTS
Description: Trip Blank Lab Sample ID:C401556-03 Received: 02/07/14 15:55
Matrix: Water Sampled:02/03/14 11:02 Work Order: C401556
Project: TTO Sampled By: Cameron Testing
lVofati[e Organic Compounds by GCMS
^ - ERm ally wt warww /NC 5911
Analyte MAS Numberl
Results
fin
mom
2E
MU
PU
Batch
memod
Anahized
gy 11�
1,1,1-Trichlomethane [71-55-6]^
< 0.12
ug/L
1
0.12
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,1,2,2-Tetradtbroethane[79-34-51^
< 0.28
ug/L
1
0.28
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,1,2-Trichbroethane (79-00-5]^
< 0.14
ug/L
1
0.14
1.0
4610032
EPA 624
02/11/14 11:07
REF
1,1-Didtiaroethane [75-34-3]^
< 0.13
ug/L
1
0.13
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,1-Didtloroethene [75-35.4]^
< 0.21
ug/L
1
0.21
1.0
4810032
EPA 624
02/11/14 11:07
REF
1,2-Dichlorobenzene [95-50-1]^
< 0.19.
ug/L
1
0.19
1.0
4B10032
EPA 624
02/11/14 11:07
REF
1,2-Didtloroethane[107-06.21^
< 0.21
ug/L
1
0.21
1.0
4810032
EPA 624
02/11/14 11:07
REF
1,2-Dichloropropane[78-87-5]^
< 0.10
ug/L
1
0.10
1.0
4810032
EPA 624
02/11/14 11:07
REF
1,3-Didrlorobenzene [541-73-1]^
< 0.15
ug/L
1
0.15
1.0
4810032
EPA 624
02/11/14 11:07
W
1,4-Diddorobenzwe[106.46-7]^
< 0.19
ug/L
1
0.19
1.0
4B10032
EPA 624
02/11/14 11:07
REF
2-Chloroethyl Vinyl Ether [110-75-8]^
< 1.1
ug/L
1
1.1
5.0
4810032
EPA 624
02/11/14 11:07
REF
Acrolein [107-02-8]^
< 4.0
ug/L
1
4.0
10
4010032
EPA 624
02/11/14 11:07
REF
Acrylonitrile 1107-13-11^
< 3.5
ug/L
1
3.5
10
4BID032
EPA 624
02/11/14 11:07
REF
Benzene(71-43-2]^
< 0.15
ug/L
1
0.15
1.0
4810032
EPA 624
02/11/14 11:07
REF
Brornodidtloromethane 175.27-4]^
< 0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Bromoform (75-25-2]^
< 0.22
ug/L
1
0.22
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Bromomethane (74-83-9]^
< 0.14
ug/L
1
0.14
1.0
4810032
EPA 624
02/11/14 11:07
REF
Carbon Tetrachloride(56-23-5]^
< 0.17
ug/L
1
0.17
1.0
4810032
EPA 624
02/11/14 11:07
REF
Chlorobenzene [108-90-7]^
< 0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Chloroelhane [75-W-3]^
< 0.23
ug/L
1
0.23
1.0
4310032
EPA 624
02/11/14 11:07
REF
Chloroform [67-66-3]^
0.53
3
ug/L
1
0.18
1.0
41310032
EPA 624
02/11/14 11:07
REF
Chloromethane [74-87-3]1
< 0.13
ug/L
1
0.13
1.0
4810032
EPA 624
02/11/14 11:07
REF
ds-1,3-Dichloropropene [10061-01-5]^
< 0.20
ug/L
1
0.20
1.0
481OD32
EPA 624
02/11/14 11:07
REF
Dibromochloromethane [124.48-1]^
< 0.17
ug/L
1
0.17
1.0
4B10032
EPA 624
02/11/14 11:07
REF
Ethylbenzene [100.41-4]^
< 0.13
ug/L
1
0.13
1.0
4610032
EPA 624
02/11/14 11:07
REF
Methylene Chloride [75-09-2]^
< 0.23
ug/L
1
0.23
1.0
4B10D32
EPA 624
02/11/14 11:07
REF
Tetraddoroethene [127-18-4]^
< 0.17
ug/L
1
0.17
1.0
4810032
EPA 624
02/11/14 11:07
REF
Toluene [108-88-3]^
< 0.14
ug/L
1
0.14
1.0
4B10032
EPA 624
02/11/14 11:07
REF
trans-1,2-1Xchloroethene [156-N-5]^
< 0.21
ug/L
1
0.21
1.0
4810032
EPA 624
02/11/14 11:07.
REF
trans-1,3-D'idtloropropene [10061-02-0]^
< 0.15
ug/L
1
0.15
1.0
4010032
EPA 624
02/11/14 11:07
REF
Trichloroethene [79-01-6]^
< 0.15
ug/L
1
0.15
1.0
4510032
EPA 624
02/11/14 11:07
REF
Vinyl chloride [75-01r4]1
< 0.32
ug/L
1
0.32
1.0
4B10032
EPA 624
02/11/14 11:07
REF
sw7cwtes
Bi
2E
%Rev
`%5 Rec
Units
Al he
9Q3I1
lY Notes
4-BromoflLam5en2ene
38
1
50.0
76 %
51-122
4B10032
EPA 624
0211111411:07
REF
Dibrtmlafluaromeffiane
43
1
50.0
8596
68-117
48IW32
EPA 624
0211111411:07
REF
To/ume-dB
43
1
50.0
86 %
67-127
4BI0032
EPA 624
02111114 11:07
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in hdl- Page 8 of 21

QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Balch 4B10032 - EPA 5030E MS
Blank (4B10032-BU(1) Prepared: 02/10/2014 17:53 Analyzed: 02/10/2014 23:46
Spike
Source
%REC
RPD
Anal
Resin
E109
E L
Yalu
Level
Resul.S %REC
Limits RPD
Limit Notes_
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1, 1, 2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dic hloroethane
0.21
U
1.0
ug/L
1,2-Dichloroproparhe
0.10
U
1.0
ug/L
1,3-Dichlorobenzene
0.15
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/Lr
2-Chloroethyl Vinyl Ether
1.1
U
5.0
ug/L
Acrolein
4.0
U
10
ug/L
Aaylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon Tetrachloride
0.17
U
1.0
ug/L
Chloroberizere
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.16
U
1.0
ug/L
C hloromethane
0.13
U
1.0
ug/L
cis-1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Methylene Chloride
0.23
U
1.0
ug/L
Tetrachlaroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichlormthene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
OAS
U
1.0
ug/L
Trichlorcethene
0.15
U
1.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
4-Lim w&vrcb&wene
39
u91L
50.0
78
51-122
LNbmm fluoromethane
41
U91L
50.0
84
68-117
Tahrene-&
43
u9A
50.0
86
67-127
LCS (4B30032-BS3)
Prepared: 02/10/2014 17:53 Analyzed: 02/11/2014 00:16
Spike
Source
%REC
RPD
Anal lttf:
Result
13a4
POL
lfnib
Level
Result %REC
LIM RPD
Lind Notes
1,1,1-Tridhloroethane
20
1.0
ug/L
20.0
99
52-162
1,1,2,2-Tebadhlaroethane
20
1.0
ug/L
20.0
101
46-157
1,1,2-Trichloroethane
21
1.0
ug/L
20.0
103
52-150
1,1-Dichloroethane
20
1.0
ug/L
20.0
100
59-155
1,1-Dichloroethene
21
1.0
ug/L
20.0
103
10-234
1,2-Dichiorobenzene
20
1.0
ug/L
20.0
100
18-190
1,2-Diddoroethane
21
1.0
ug/L
20.0
105
49-155
1,2-Dichloropropane
20
1.0
ug/L
20.0
98
10-210
1,3-Dic hlo of a ene
20
1.0
ug/L
20.0
100
59.156
1,4-Dlchlorobenzene
18
1.0
ug/L
20.0
92
18-190
FINAL
This report relates only to
the sample as recdvea by the laboratory, and may only be reproduced In
M.
Page 9 of 21

J
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 4810032 - EPA 50308_MS - COMinued
LCS (4B30032-BS1) Continued Prepared: 02/10/2014 17:53 Analyzed: 02/11/2014 00:16
Spike
Source
%REC
RPD
Anal
Result
PM
PQL
Units
Level
get
%REC
Limits RPD
Limit Notes
2- hloroethyl Vinyl Ether
38
5.0
ug/L
40.0
96
10.305
Acrolein
9.1.
1
10
ug/L
40.0
23
10-200
Anylonitrile
56
10
ug/L
60.0
94
10-200
Benzene
20
1.0
ug/L
20.0
98
37-151
Bromodichloromefhane
21
1.0
ug/L
20.0
105
35.155
Bromoform
17
1.0
ug/L
20.0
86
45-169
Bromomethane
16
1.0
ug/L
20.0
81
10-242
Carton Tetrdchloride
20
1.0
ug/L
20.0
100
17-140
Chloroberaene
21
1.0
ug/L
20.0
105
37-160
Chlor d;,e
18
1.0
ug/L
20.0
89
14-230
Chloroform
20
1.0
ug/L
20.0
100
51-138
Chloromefhane
15
1.0
ug/L
20.0
74
10-273
ds-1,3-Dichloropropene
19
1.0
ug/L
20.0
94
10-227
Dibroraddoromefhane
21
1.0
ug/L
20.0
106
53-149
Ethylbenzene
18
1.0
ug/L
20.0
89
37-162
Methylene Chloride
21
1.0
ug/L
20.0
106
10.221
Tetrachloroethene
19
1.0
ug/L
20.0
95
64-148
Toluene
18
1.0
ug/L
20.0
92
47-150
trans-1,2-Dichloroetltene
19
1.0
ug/L
20.0
97
54-156
trans-1,3-Dichloropropene
21
1.0
ug/L
20.0
104
17-183
Trichkuoethene
19
1.0
ug/L
20.0
97
71-157
Vinyl chloride
14
1.0
ug/L
20.0
68
10-251
4-8nwnoflLwrvbenz&w
39
u91L
50.0
79
51-122
MAN"o0uoromelharre
41
WA
S0.0
84
68-117
Tdumed8
43
WA
50.0
85
57--127
Matrix Spike (4810032-MS1)
Prepared: 02/10/2014 17:53 Analyzed. 02/11/2014 00:45
Source: C401302-09
Spike
Source
%REC
RPD
Ana
Result
Elm
PD1.
.tlnall
Level
Belt
%REC
Limits RPD
LM Notes
1,1,1-Trichloroethane
20
1.0
ug/L
20.0
0.12 U
101
52-162
1,1,2,2-Tehachloroethane
19
1.0
ug/L
20.0
0.28 U
94
46.157
1,1,2-TrichkKoethane
19
1.0
ug/L
20.0
0.14 U
97
52-150
1,1-Dichloroethane
20
1.0
ug/L
20.0
0.13 U
102
59-155
1,1-Didtioroethene
22
1.0
ug/L
20.0
0.21 U
108
10-234
1,2-Didhlombenzene
20
1.0
ug/L
20.0
0.19 U
102
18-190
1,2-Dichl methane
21
1.0
ug/L
20.0
0.21 U
106
49.155
1,2-Dirhkxopropane
20
1.0
ug/L
20.0
0.10 U
99
10-210
1,3-Dktilorobertzene
21
1.0
ug/L
20.0
0.15 U
103
59-156
1,4-Dichlorobenzene
19
1.0
ug/L
20.0
0.19 U
96
18-190
2-Chloroethyl Vinyl Ether
35
5.0
ug/L
40.0
1.1 U
87
1D•305
Aaolein
8.3
3
10
ug/L
40.0
4.0 U
21
10-200
Aaylonibile
49
10
U91L
60.0
3S U
82
1D-200
Benzene
20
1.0
u9/L
20.0
0.15 U
101
37-151
Bromodidilormet ane
22
1.0
ug/L
20.0
0.17 U
108
35-155
Bromoform
16
1.0
ug/L
20.0
0.22 U
82
45-169
Brornomethane
20
1.0
ug/L
20.0
0.14 U
100
10-242
Carbon Tetrachloride
21
1.0
ug/L
20.0
0.17 U
106
70-140
Chloroberuene
22
1.0
U9/1-
20.0
0.17 U
108
37-160
Chloroethane
23
1.0
ug/L
20.0
0.23 U
113
14-230
FINAL
This report relates only to
the sample as,eoei by the laboratory, and mey arty be
reprodumd in
full.
Page 10 of 21
r'

QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 4020032 - EPA 5030E MS - Confined
Matrix Spike (4830032-MSI) Continued Prepared: 02/10/2014 17:53 Analyzed: 02/11/2014 00:45
Source: C401302-09
Spike
Source
%REC
RPD
Anal vte
Result
Rao P"
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Chloroform
20
1.0
ug/L
20.0
0.18 U
101
51-138
Qdoromethane
23
1.0
ug/L
20.0
0.13 U
116
10-273
ds-1,3-Dichloropropene
19
1.0
ug/L
20.0
0.20 U
95
10-227
Dibromochloromethane
20
1.0
ug/L
20.0
0.17 U
101
53-149
Ethylbenzene
19
1.0
ug/L
20.0
0.13 U
94
37-162
Methylene Chloride
21
1.0
ug/L
20.0
0.23 U
107
10-221
Tetrachloroethene
20
1.0
ug/L
20.0
0.17 U
98
64-148
Toluene
19
1.0
ug/L
20.0
0.14 U
95
47-150
trans-1,2-Dichloroefhene
20
1.0
ug/L
20.0
0.21 U
100
5+156
trans-1,3-Dichloropropene
20
1.0
ug/L
20.0
0.15 U
100
17-183
Trichloroethene
21
1.0
ug/L
20.0
0.15 U
104
71-157
Vinyl chloride
19
1.0
ug/L
20.0
0.32 U
95
10-251
4-8r0moAuor2benzene
40
ugA
50.0
80
51-122
D/bromoNuornmeMane
41
1 f9A
50.0
83
68-117
Toluene &
43
ug/L
50.0
86
67-127
Matrix Spike Dup (4B10032-MSDi)
Prepared: 02/10/2014 17:53 Analyzed: 02/11/2014 01:15
Source: C401302-09
Spike
Source
%REC
RPD
Anal
Resul
E1a9 P_QL
!!nits
Level
Result
%REC
units
RPD
Limit Notes
1,1,1-Trichloroethane
20
1.0
ug/L
20.0
0.12 U
98
52-162
3
25
1,1,2,2-Tetrachloroethane
21
1.0
ug/L
20.0
0.28 U
105
46.157
11
25
1,1,2-Trichloroedme
21
1.0
ug/L
20.0
0.14 U
103
52-150
6
25
1,1-Dichloroethane
20
1.0
ug/L
20.0
0.13 U
100
59-155
3
25
1,1-Dichloroethene
21
1.0
ug/L
20.0
0.21 U
103
10-234
5
25
1,2-Dichlorobenzene
20
1.0
ug/L
20.0
0.19 U
100
18-190
1
25
1,2-Dichloroethane
21
1.0
ug/L
20.0
0.21 U
103
49-155
2
25
1,2-Dichloropropene
19
1.0
ug/L
20.0
0.10 U
97
10-210
2
25
1,3-Dalorobenzene
20
1.0
ug/L
20.0
0.15 U
99
59-156
4
25
1,4-Dichlorobenzene
18
1.0
ug/L
20.0
0.19 U
91
18-190
5
25
2-Chloroethyl Vinyl Ether
39
5.0
ug/L
40.0
1.1 U
98
10-305
12
25.9
Acrolein
10
10
ug/L
40.0
4.0 U
26
1D-200
23
36
Acrylonitrile
60
10
ug/L
60.0
3.5 U
100
10-200
19
50
Benzene
19
1.0
ug/L
20.0
0.15 U
97
37-151
4
25
Bromodichlorornethane
21
1.0
ug/L
20.0
0.17 U
103
35-155
5
25
Bromoform
18
1.0
ug/L
20.0
0.22 U
92
45-169
12
25
Bromomethane
18
1.0
ug/L
20.0
0.14 U
92
10-242
8
25
Carbon Tetrachloride
20
1.0
ug/L
20.0
0.17 U
99
70.140
7
25
Chlcrobenzene
21
1.0
ug/L
20.0
0.17 U
103
37-160
5
25
Chloroethane
22
1.0
ug/L
20.0
0.23 U
109
1+230
4
25
Chloroform
19
1.0
ug/L
20.0
0.18 U
97
51-138
3
25
Chloromethane
22
1.0
ug/L
20.0
0.13 U
108
10-273
7
25
ds-1,3-Dichloropropene
19
1.0
ug/L
20.0
0.200
94
10-227
1
25
Dibromochloromethane
21
1.0
ug/L
20.0
0.17 U
106
53-149
5
25
Ethylbenzene
18
1.0
ug/L
20.0
0.13 U
90
37-162
5
25
Methylene Chloride
20
1.0
ug/L
20.0
0.23 U
102
10-221
5
25
Tetrachloroethate
19
1.0
ug/L
20.0
0.17 U
95
64-148
3
25
Toluene
18
1.0
ug/L
20.0
0.14 U
90
47-150
5
25
trans-1,2-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
96
5+156
4
25
trans-1,3-0ichloropropene
21
1.0
ug/L
20.0
0.15 U
105
17-183
4
25
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in
full. '
Page 11 of 21

QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Bahch 4010032 - EPA 5030E MS - Continued
Matrix Spike Dup (4B10032-114SD1) Continued Prepared: 02/10/2014 17:53 Analyzed: 02/11/2014 01:15
Source: C401302-09
Spike Source %REC RPD
Anal ld9 Resin Elm P" Units Level gesujt %REC Umfts RPD Limit )y2ie
Trichbroethene 20 1.0 ug/L 20.0 0.15 U 98 71-157 6 25
Vinyl chloride 17 1.0 ug/L 20.0 032 U 87 1D-251 8 25
39 U91L 50.0 78 51.122
D/hvnmofluaonwWne 42 U91L 50.0 84 68-117
Toluene-& 42 ug/L 50.0 84 67-127
Semivolatile Organic Compounds by GCMS -Quality Control
Batch 4B0B010 - EPA 3510C MS
Blank (4608010-11ILKI) Prepared: 02/08/2014 22:53 Analyzed: 02/11/201414:18
Anal lde
Rem
Elm
PQL
Units
1,2,4-Trichlarobenzene
1.2
U
10
ug/L
1,2-131dilorobenzene
1.1
U
10
ug/L
1,3-Dichkrobenzene
1.1
U
10
ug/L
1,4-Diddorobenzene
1.0
U
10
ug/L
1-Methylnaphthalene
1.7
U
10
ug/L
2,4,5-Trichlorophenol
1.0
U
10
ug/L
2,4,6-Trichlorophenol
1.1
U
10
ug/L
2,4-0khlaropherwl
1.4
U
10
ug/L
2,4-Dimethylphenol
13
U
to
ug/L
2,4-Dinitrophenol
2.6
U
10
ug/L
2,4-Dinilrotoluene
2.4
U
10
ug/L
2,6-Un'drotoluene
15
U
10
ug/L
2{h1omriaphthaierte
1.0
U
10
ug/L
2-ChImpheral
12
U
10
ug/L
2-Methyl-4,6dmltrophenol
2.9
U
10
ug/L
2-Me"riaphthalene
1.5
U
10
ug/L
2-Nitrophenol
1.1
U
10
ug/L
3,3'-Dichlorobenzidine
33
U
10
ug/L
4-8romophenyl-phenyk9her
1.0
U
10
ug/L
4-0lloro-3-methylphenol
1.5
U
10
ug/L
4-Chlrophenyl-pherrylether
1.6
U
10
ug/L
4-Nbvphenol
2.0
U
10
ug/L
Acemphthene
1.4
U
10
ug/L
Atenaphthylene
1.2
U
10
ug/L
Anthracene
1.6
U
10
ug/L
Benzidine
1.6
U
10
ug/L
Bertzo(a)anthracem
13
U
10
ug/L
Benzo(a)pyrene
1.3
U
10
ug/L
Benzc(b)fluoranthene
1.0
U
10
ug/L
Bmzo(g,h,i)perylene
2.4
U
10
ug/L
Betzo(k)fkroranthene
13
U
10
ug/L
Benzoic acid
1.0
U
50
ug/L
Bis(2-chloroeth )mettwne
1.4
U
10
ug/L
Bis(2-chkroethyhether
1.2
U
10
ug/L
Bis(2-ddoroisopropyl)ether
1.3
U
10
ug/L
Bis(2-e"1he#)phthalate
1.7
U
5.0
ug/L
Spike Source %REC
Level Result %REC Limits RPD
RPD
M IR Notes
QV-01
FINAL This report relates only to the sample as reached by the laboratory, and may My be rep u&Ked in full. Page 12 of 21

QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Satrh 4808010 - EPA 351OI MS - Cont/nued
Blank (4608010-ELK1) Continued Prepared: 02/08/2014 22:53 Analyzed: 02/11/2014 14:18
Spike
Anal vte
Result
f189
E%
Units Level
Butylbenzylphthalate
2.0
U
10
ug/L
Chrysene
2.0
U
to
ug/L
Dibenzo(a,h),inthracene
2.3
U
10
ug/L
Died*phthalate
2.1
U
10
ug/L
Dimethylphthalate
1.4
U
10
ug/L
Di-n-butylphthalate
1.5
U
10
ug/L
Di-n-octylphthalate
3.1
U
10
ug/L
OPH (as Azobenzene)
1.9
U
10
ug/L
Fluoranthene
2.1
U
10
ug/L
Fluorene
1.7
U
10
ug/L
Hexachlorobenzene
1.0
U
10
ug/L
Hexachlorobutadiene
1.2
U
10
ug/L
Hexachlorocyclopentadiene
1.3
U
10
ug/L
Hexachloroethane
1.1
U
10
ug/L
Indeno(1,2,3-cd)pyrene
2.2
U
10
ug/L
Isophorone
1.3
U
10
ug/L
Naphthalene
1.3
U
10
ug/L
Nitrobenzene
1.2
U
10
ug/L
N-Nitrosodimethylamine
1.3
U
10
ug/L
N-Nitroso-di-n-propylamine
1.5
U
10
ug/L
N-Nitrosodiphenylamine/Diphenylamine
2.1
U
10
ug/L
Pentachlorophenol
1.8
U
10
ug/L
Phenanthrene
1.4
U
10
ug/L
Phenol
1.4
U
10
ug/L
Pyrene
2.1
U
10
ug/L
Source %REC RPD
Result %REC Urnits RPD Llmit Notes
Z4,6-Trib-nWI eno/
64
WA
100 64 18-157
244-oWpheny/
43
u9/L
50.0 87 15-139
2-R-ophenol
55
U91L
100 55 10-104
Nftbenzene-d5
39
U91L
50.0 78 16-140
Phenol-d5
38
U91L
100 38 10-83
Terphenyfd14
44
U91L
50.0 88 23-164
LCS (4B08010-BS1)
Prepared: 02/08/2014 22:53 Analyzed: 02/11/2014 14:51
Spike
Source
%REC
Ana
Resin
Flag - PQL
lILILe
Level
gesul %REC
Units RPD
1,2,4-Trichlorobenzene
41
10
ug/L
50.0
82
44-142
1,2-Dichlorobenzene
36
10
ug/L
50.0
72
32-129
1,3-Dichlorobenzene
36
10
ug/L
50.0
71
1D-172
1,4-Dichlorobenzene
36
10
ug/L
50.0
71
20-124
1-Methylnaphthalene
41
10
ug/L
50.0
83
46-80
2,4,5-Trirhlorophenol
45
10
ug/L
50.0
90
59-121
2,4,6-Trichlorophenol
46
10
ug/L
50.0
91
61-119
2,4-Dichlorophenol
43
10
ug/L
50.0
B6
49-118
2,4-Dimethylphenol
39
10
ug/L
50.0
78
42-111
2,4-Dinitrophenol
41
10
ug/L
50.0
83
1-149
2,4-Dinitmtoluene
43
10
ug/L
50.0
87
39-139
2,6-Dinftrotoluene
46
10
ug/L
50.0
92
50-158
2-(hloronaphthalene
45
10
ug/L
50.0
89
60-118
2-Chlorophenol
40
10
ug/L
50.0
80
23-134
FINAL
This report relates only to the sample as receKed by the laboratory, and may only be reproduced in
full.
RPD
11110 mows
QL-02
Page 13 of 21

QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Ba&h 4008010 - EPA 3510C_MS - Continued
LCS (4808010-BSI) Continued Prepared: 02/08/2014 22:53 Analyzed: 02/11/2014 14:51
Spike
Source
%REC RPD
Ana6LLl1
Result Elm
J!"
Units
Level
Result %REC
Liml3s RPD wit Notes
2-Methy",6-dinitrophenol
44
10
ug/L
50.0
89
33-160
2-Methylnaphthalene
42
10
ug/L
50.0
84
33-111
244ltrophend
43
10
ug/L
50.0
87
36-113
IT-Dichlorobenzidine
66
10
ug/L
50.0
132
10-262
4-Bromphenyl-phenyledw
45
10
ug/L
50.0
90
53-127
4-Mloro-3-methylphend
42
10
ug/L
50.0
84
25-147
4-Chlorophenyl-phenylether
45
10
ug/L
50.0
90
25-158
4-Nirophenol
30
10
ug/L
50.0
60
33-105
Acenaphthene
42
10
ug/L
50.0
84
47-145
Atenaphthylene
44
110
ug/L
50.0
88
33-145
Anthracerve
42
10
ug/L
50.0
85
27-133
Benzidine
12
10
ug/L
50.0
24
10-136
Benzo(a)anthraoene
45
10
ug/L
50.0
91
33-143
Benzo(a)pyrene
51
10
ug/L
50.0
103
17-163
Benzo(b)fluoranthem
48
10
ug/L
50.0
97
2+159
Berao(g,h,i)perylene
58
10
ug/L
50.0
117
10-219
Benzo(k)fluoranthene
49
10
ug/L
50.0
99
11-162
Benzoic acid
15 J
50
ug/L
50.0
30
1D-120
Bis(2-ddoroethoxy)methane
41
10
ug/L
50.0
82
33-184
Bis(2-chbroethyl)ether
42
10
ug/L
50.0
84
12-158
Bis(2-chloroisopropyl)ether
43
10
ug/L
50.0
86
36-166
Bls(2-ethy0wxyl)phthalate
49
5.0
ug/L
50.0
98
10-158
Butylbenzylphthaiate
54
10
ug/L
50.0
108
64-152
Chrysene
46
10
ug/L
50.0
92
17-168
Dibenzo(a,h)anthracene
62
10
ug/L
50.0
124
10-227
Diethylphthalate
46
10
ug/L
50.0
91
62-127
Mnethyiphthalate
47
10
ug/L
50.0
93
.10-114
Di-n4x"phthalate
48
10
ug/L
50.0
96
10.118
Di-n-odylphthalate
55
10
ug/L
50.0
110
10-146
DPH (as Azobenzene)
44
10
ug/L
50.0
88
69-108
Ruoranthow
45
10
ug/L
50.0
90
26-137
Ruorene
42
10
ug/L
50.0
84
59-121
Hexaddorobenzene
47
10
ug/L
50.0
93
10-152
HexachbVautadiene
41
10
ug/L
50.0
83
24-116
Hexachkxocyclopentadiene
43
10
ug/L
50.0
85
10-99
Hexachlomethane
33
10
ug/L
50.0
66
12-82
Indeno(1,2,3td)pyrene
61
10
ug/L
50.0
123
10-171
Lsophorone
44
10
ug/L
50.0
88
21-196
Naphthalene
40
10
ug/L
50.0
80
21-133
Nitrobenzene
42
10
ug/L
50.0
84
35-180
N-Nitrosodimethylamine
34
10
ug/L
50.0
69
24-94
N-Nitroso-di-n-propylamine
38
10
ug/L
50.0
76
1D-230
Pentachloroptmol
45
10
ug/L
50.0
90
51-135
Phenanthrene
44
10
ug/L
50.0
88
54-120
Phenol
25
10
ug/L
50.0
50
19-78
Pyrene
46
10
ug/L
50.0
92
65-134
1,4,6-Tnbromoph W
89
u94
100
89
18-157
1-RWrvNpbenyl
45
U94
50.0
89
15.139
24*A qm*-w/
60
U91L
100
60
19-104
This report relates o* to the sample as recetved by the laboratory, and may orgy be reproduced in U. Page 14 of 21

QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 4808010 - EPA 3510C MS - Canbinaed
LCS (4808010-asi) Continued Prepared: 02/08/2014 22:53 Analyzed: 02/11/2014 14:51
Spike Source %REC RPD
Analvte
Result EIOg M
UAlb
Level gesui %REC Limits RPD Limit Notes
N&obrnzene-d5
44
u91L
50.0 87 16-140
Phenol-dS
48
u91L
100 48 10-83
Terphe7y1-d14
48
u9/L
50.0 97 23-164
Matrix Spike (4608030-MS1)
Prepared: 02/06/2014 22:53 Analyzed: 02/11/2014 15:23
Source:C400990-03
Spike
Source
%REC RPD
Anal Yte
ReSuli
Elm ' P91
Units
Level
gwul
%REC
Limits RPD Limit Notes
1,2,4-Trichlorobenzene
35
10
ug/L
50.0
1.2 U
70
4+142
1,2-Didilorobenzene
31
10
urq/L
50.0
1.1 U
63
32-129
1,3-Dicillorobenzene
30
10
ug/L
50.0
1.1 U
61
10-172
1,4-Dichlorobenzene
31
10
ug/L
50.0
1.0 U
62
20-124
1-Methylnaphthalene
36
10
ug/L
50.0
1.7 U
72
46-80
2,4,5-Trichlorophenol
42
10
ug/L
50.0
1.0 U
84
59.121
2,4,6-Tridtlorophenol
40
10
ug/L
50.0
1.1 U
79
61-119
2,4-Dlchlorophenol
38
10
ug/L
50.0
1.4 U
77
49-118
2,4-Dimethylphenol
36
10
ug/L
50.0
13 U
72
42-111
2,4-Dinilrophenol
37
10
ug/L
50.0
2.6 U
74
11-149
2,4-Dinitrotoluene
39
10
ug/L
50.0
2.4 U
78
39-139
2,6-Dir itrotoluene
38
10
ug/L
50.0
1.5 U
77
50-158
2-Chloronaphthalene
37
10
ug/L
50.0
1.0 U
75
60-118
2-Chlorophencl
32
10
ug/L
50.0
1.2 U
64
23-134
2-Methyl-4,6-dinitrophenol
39
10
ug/L
50.0
2.9 U
78
33-160
2-Methylnaphthalene
36
10
ug/L
50.0
1.5 U
72
33-111
2-Nitrophenol
35
10
ug/L
50.0
1.1 U
71
36-113
3,3'-DichloroberWdine
59
10
ug/L
50.0
3.3 U
118
10-262
4-Bromophenyl-phenylether
39
10.
ug/L
50.0
1.0 U
78
53-127
4-Chloro-3-methylphenol
40
10
ug/L
50.0
1.5 U
80
25-147
4-Ch"henyl-phenylether
40
10
ug/L
50.0
1.6 U
79
25-158
4-Nitrophenol
27
10
ug/L
50.0
2.0 U
53
33-105
Acenaphthene
37
10
ug/L
50.0
1.4 U
74
47-145
Acenaphthylene
36
10
ug/L
50.0
1.2 U
77
33-145
Anthracene
37
10
ug/L
50.0
1.6 U
75
27-133
Benzidine
3.6
3 10
ug/L
50.0
1.6 U
7
10-136
Benzo(a)anthracene
40
10
ug/L
50.0
13 U
80
33-143
Benzo(a)pyrene
45
10
ug/L
50.0
13 U
91
17-163
Benzo(b)Ruoranthene
43
10
ug/L
50.0
1.0 U
86
24-159
Benzo(g,h,i)perylene
54
10
ug/L
50.0
2.4 U
108
10-219
Benzo(k)fluoranthene
43
10
ug/L
50.0
1.3 U
86
11-162
Benzoic acid
6.4
3 50
ug/L
50.0
1.0 U
13
10-120
Bis(2-(hkxoethoxy)methane
33
10
ug/L
50.0
1.4 U
66
33-184
Bis(2-chloroethyl)ether
34
10
ug/L
50.0
1.2 U
67
12-158
Bis(2-chloroisopropyl)edw
34
10
ug/L
50.0
1.3 U
68
36-166
B'ts(2-ethylhexyl)phthalate
42
5.0
ug/L
50.0
1.7 U
85
10-158
Butylbenzylphthalate
50
10
ug/L
50.0
2.0 U
100
10-152
Chrysene
41
10
ug/L
50.0
2.0 U
81
17-168
Dtbenzo(a,h)anlhracene
52
to
ug/L
50.0
23 U
105
10-227
Diethylphthalate
40
10
ug/L
50.0
2.1 U
79
62-127
Dimethylphthalate
38
10
ug/L
50.0
1.4 U
77
10-114
Di-n-butylphihalate
44
10
ug/L
50.0
1.5 U
88
10.118
This repot rela6S only to the sample as received by the laboratory, and may only be reproduced In lull. Page 15 of 21

QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 4OW010 - EPA 3510C MS - Continued
Matritt spike (4B08010-MSl) Continued Prepared: 02/08/2014 22:S3 Analyzed: 02/11/2014 15:23
Source: C400990-03
Spike
Source
%REC
RPD
Analiris
BeSul
flag MI.
VW&
Level
Result
%REC
!Limits
RPD
Limit Notes
Di-nodylphthalale
48
10
ug/L
50.0
3.1 U
96
ID-146
DPH (as Azobenzene)
39
10
ug/L
50.0
1.9 U
78
69-108
Fluorangu ne
41
10
ug/L
50.0
2.1 U
81
26-137
Ruorene .
37
10
ug/L
50.0
1.7 U
73
59-121
Hexachlombenzene
40
10
ug/L
50.0
1.0 U
81
10-1S2
Hexachlorobutadiene
36
10
ug/L
Solo
1.2 U
71
24-116
HexachlorMclopentadiene
34
10
ug/L
50.0
13 U
68
10-99
Hexadtloroethane
28
10
ug/L
S0.0
1.1 U
56
12-82
Indeno(1,2,3-ad)pyrene
52
10
ug/L
50.0
2.2 U
104
10.171
Isophorone
35
10
ug/L
50.0'
1.3 U
70
21-196
Naphthalene
35
10
ug/L
50.0
1.3 U
70
21-133
Nitrobenzene
34
10
ug/L
50.0
1.2 U
67
35-180
N-Nftsodimethylamine
28
10
ug/L
50.0
13 U
57
24-94
N-Nitroso-di-n-propylamine
31
10
ug/L
SD.0
1.5 U
61
10-230
Pentadilorophernl
42
10
trg/L
50.0
1.8 U
84
51-135
Phenanthrene
38
10
ug/L
50.0
1.4 U
77
54-120
Phenol
22
10
ug/L
50.0
1.4 U
44
19.78
Pyrene
42
to
ug/L
50.0
2.1 U
83
52-115
Z4,6-Tdb n wherwol
80
ugA
700
8D
18-157
1-Ruorobipheny4
36
ug/L
50.0
73
15-139
1,F7uoraprhenal
51
tg/L
10I0
52
10.104
Nilrrh#M en s
33
ugA
50.0
66
16-140
Pheno%d5
41
WA
100
41
10-83
Tefpheny4-dl4
41
L91L
50.0
84
13-164
Matrix Spike Dup (408010-MSD1)
Prepared: 02/08/2014 22:53 Analyzed: 02/11/201415:55
Source: C400990-03
Spike
Source
%REC
RPD
Ana11t1ffi
R esu
Elm Mi.
!lO115
Level
%REC
U,i1
RPD
LM Notes
1,2,4-Trkhkwobenaene
35
10
ug/L
50.0
1.2 U
71
44-142
2
28.1
1,2-Dkhkwobenzene
31
10
ug/L
50.0
1.1 U
63
32-129
03
30.9 .
1,3-Dichlombenaene
31
10
ug/L
50.0
1.1 U
62
10-172
1
41.7
1,4-Di hbDbmzene
31
10
ug/L
50.0
1.0 U
61
20424
0.5
32.1
1-Methylnaphthalene
35
10
ug/L
50.0
1.7 U
71
46-80
1
25
2,4,5-Trkhlorophenol
42
10
ug/L
50.0
1.0 U
84
59-121
0.5
25
2,4,6-Trldtloropheral
40
10
ug/L
50.0
1.1 U
80
61-119
1
25
2,4-DithhWhenol
38
10
ug/L
50.0
1.4 U
76
49-118
2
25
2,4-Dimethyiptlenol
34
10
ug/L
50.0
13 U
68
42-111
6
26
2,4-Din"henol
39
10
ug/L
50.0
2.6 U
78
11-149
4
50
2,4-0in'drotoluene
39
10
ug/L
50.0
2.4 U
79
39-139
1
25
2,6-Dimbotoluene
41
10
ug/L
50.0
1.5 U
82
5D-158
7
29.6
2-hlonmphthalene
38
10
ug/L
50.0
1.0 U
76
60-118
2
25
2-0rlorophenol
32
10
ug/L
50.0
1.2 U
64
23-134
1
28.7
2401ethy14,6-dmtrophenol
42
10
ug/L
50.0
2.9U
83
33-160
6
25
2-Methylnaphthalene
35
10
ug/L
50.0
1.5 U
70
33-111
2
27
2-Nitrophenol
35
10
ug/L
50.0
1.1 U
71
36-113
0.3
50
3,T-D'Kdrlaobenzidine
47
10
ug/L
50.0
33 U
94
10-262
23
71.4
4-Wonaphenyl-phenyMher
39
10
ug/L
50.0
1.0 U
77
53-127
1
25
4-0rloro-3-methylphend
38
10
ug/L
50.0
1.5 U
77
25-147
4
37.2
4-l]doropfxnyl-phertylether
39
10
ug/L
50.0
1.6 U
79
25158
0.4
33.4
FINAL This report relates only to the sample as received by the laboratory, and may orty be
reproduced In
hdl.
Page 16 of 21

QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch 4808010 - EPA 3510C MS - Continued
Matrix Spike Dup (4808010-MSD3) Continued Prepared: 02/08/2014 22:53 Analyzed: 02/11/2014 15:55
Source: C400990-03
Spike
Source
%REC
RPD
Anal lde
Resul!
Dag Eal.
Mwb
Level
gesug
%REC
MMb
RPD
LIMA
4-Nitrophenol
27
10
ug/L
50.0
2.0 U
55
33-105
3
27
Acenaphthene
36
10
ug/L
50.0
1.4 U
73
47-145
2
27.6
Acenaphthylene
38
10
ug/L
50.0
1.2 U
76
33-145
03
40.2
Anthracene
37
10
ug/L
50.0
1.6 U
73
27-133
2
32
Benzidine 1
4.0
3 10
ug/L
50.0
1.6 U
8
10-136
11
50
Benzo(a)anthracene
40
10
ug/L
50.0
1.3 U
8o
33-143
0.7
27.6
Benzo(a)pyrene
45
10
ug/L
50.0
13 U
90
17-163
0.6
39
Benzo(b)Fluoranthene
43
10
ug/L
50.0
1.0 U
86
2+159
0.3
38.8
Benzo(g,h,i)perylene
54
10
ug/L
50.0
2.4 U
108
10-219
0.4
58.9
Benzo(k)fluoranthene'
43
10
ug/L
50.0
1.3 U '
87
11-162
1
32.3
Benzoic add
23
3 So
ug/L
50.0
1.0 U
46
10-120
113
41
Bis(Z-chloroethoxy)methane
33
10
ug/L
50.0
1.4 U
66
33-184
0.3
34.5
Bis(2-chIoroethyl)ether
34
10
ug/L
50.0
1.2 U
67
12-158
0.1
55
Bis(2-chloroisopropyl)ether
35
10
ug/L
50.0
1.3 U
70
36-166
2
46.3
B-is(Z-ethylhexyl)phthalate
41
5.0
ug/L
50.0
1.7 U
82
10-158
3
41.1
eutylbenzyfphthafate
49
10
ug/L
50.0
2.0 U
97
10-152
2
25
Chrysene
40
10
ug/L
50.0
2.0 U
81
17-168
0.9
48.3
Dibenzo(a,h)anthracene
53
10
ug/L
50.0
2.3 U
106
10-227
1
70
Diethylphthalate
41
10
ug/L
50.0
2.1 U
82
62-127
4
11
Dimethylphthalate
41
10
ug/L
S0.0
1.4 U
81
10-114
6
26.5
Di-n-butyfphthalate
42
10
ug/L
50.0
1.5 U
83
10-118
6
25
Di-n-octylphthalate
45
10
ug/L
50.0
3.1 U
90
1D-146
6
31.4
DPH (as Azobenzene)
39
30
ug/L
50.0
1.9 U
78
69-108
0.5
36
19uoranthene
40
10
ug/L
50.0
2.1 U
80
26-137
0.8
32.8
Fluorene
37
10
ug/L
50.0
1.7 U
74
59-121
1
25
Hexachlorobenzene
40
10
ug/L
50.0
1.0 U
79
10-152
2
25
Hetmdilorobutadiene
36
10
ug/L
S0.0
1.2 U
73
24-116
2
263
Hexachlorocydopentadiene
35
10
ug/L
50.0
1.3 U
71
10.99
5
50
Hexachloroethane
29
10
ug/L
50.0
1.1 U
57
12-82
3
50.
Indeno(1,2,3-cd)pyrene
52
10
ug/L
50.0
2.2 U
105
10-171
0.6
44.5
Isophorone
34
10
ug/L
50.0
13 U
69
21-196
1
633
Naphthalene
34
10
ug/L
50.0
1.3 U
69
21-133
1
30.1
Nitrobenzene
34
10
ug/L
50.0
1.2 U
68
35-180
2
393
N-Nitrosodimethylamine
27
10
ug/L
50.0
1.3 U
55
24-94
4
36
N-Nitroso-di-n-propylamine
30
10
ug/L
50.0
1.5 U
61
10-230
0.9
55.4
Pentarhforophenol
42
30
ug/L
50.0
1.8 U
84
51-135
0.2
25
Phenanthrene
39
10
ug/L
50.0
1.4 U
78
54-120
0.9
25
Phenol
21
10
ug/L
50.0
1.4 U
41
19-78
7
25
Pyrene
42
10
ug/L
50.0
2.1 U
83
52-115
0.2
25
QM-07
QM-11
2,4,6-Trfbrvmophenol 61
u9/1
100
81
18-157
2-Huorabiphenyl 38
u9/L
50.0
76
15-139
2-Huaopherro/ 50
ug/L
100
50
10-104
ftobenzeoe-d5 34
u9/1
50.0
68
16-140
Phenol -OS 38
ug/L
100
38
10-83
Terphenyddl4 43
ug/L
50.0
86
23164
Semivolatile Organic Compounds by GC - Quality Control
Batch 4W0003 - EPA 3510C
FINAL TNs report relates orgy to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 21

QUALITY CONTROL DATA
Semivolatile Organic Compounds by GC - Quality Control
Batch 4809003 - EPA 3510C - Continued
Blank (4809003-11M) Prepared: 02/09/2014 07:54 Analyzed: 02/14/2014 11:44
Spike Source %REC RPD
Anal )de
Result
ELM
M
VDIt9
Level Resin %REC Limits RPD j Notu
4,4'-DDD
0.044
U
0.050
ug/L
4,4'-DDE
0.048
U
0.050
ug/L
4,4'-DDT
0.049
U
0.050
ug/L
Aldrin
0.041
U
0.050
ug/L
alpha-BHC
0.036
U
0.050
ug/L
beta-BHC
0.036
U
0.050
ug/L
Chlordane (n.os.)
0.020
U
1.0
ug/L
Chlordane (tech)
0.20
U
0.50
ug/L
delta-BHC
0.048
U
0.050
ug/L
Dieldrin
0.045
U
0.050
ug/L
Endosulfan I
0.045
U
0.050
ug/L
Endosulfan II
0.036
U
0.050
ug/L
Endosulfan sulfate
0.032
U
0.050
ug/L
Endrin
0.041
U
D.050
ug/L
Endrin aldehyde
0.042
U
0.050
ug/L
gamma-BHC
0.034
U
0.050
ug/L
Heplactdor
0.030
U
0.050
ug/L
Heptachlor epoxide
0.037
U
0.050
ug/L
Toxaphene•
0.22
U
1.0
ug/L
2,4,5,6-TCMX
1.1
ug/L
1.00 108 44-134
DecachbraNpheny/
0.70
119/7
1.00 70 37-149
LCS (4809003-BS3)
Prepared: 02/09/2014 07:54 Analyzed: 02/14/2014 11:57
Spike
Source
%REC
RPD
AOaIvt
Resul! Elm
EM
units
Level
Raj
%REC
Umfts RPD
limit Notes
4,4'-DDT
1.1
0.050
ug/L
1.00
110
37-160
Aldrin
1.1
0.050
ug/L
1.00
106
42-122
Dieldrin
1.0
0.050
ug/L
1.00
105
36-146
Endrin
1.0
0.050
ug/L
1.00
105
30-147
gamma-BHC
1.0
0.050
ug/L
1.00
104
19.140
Heptachlor
--
0.98
-
0.050
ug/L
1.00
98
45-122
2,4,5,6-TG4X
094
ug/L
1.00
94
44134
L1-dr/aroblpherry/
0.93
ug/L
1.00
93
.37-149
Matrix Spike (4B09003-MSl)
Prepared: 02/09/2014 07:54 Analyzed: 02/14/201412:10
Source:C400990-03
Spike
Source
%REC
RPD
_Anabde
Result Ba0
PQL
Units
Level
Rewl
%REC
Limits RPD
UMA Notes
4,4'-DDT
1.2
0.050
ug/L
1.00
0.049 U
121
3S-160
Aldrin
1.1
0.050
ug/L
1.00
C.D41 U
106
42-122
Dieldrin
1.1
0.050
ug/L
1.00
0.045 U
107
36-146
Endrin
1.1
0.050
ug/L
1.00
0.041 U
107
30-147
gamma-BHC
1.1
0.050
ug/L
1.00
0.034 U
108
19-140
Heptachlor
1.0
0.050
ug/L
1.00
0.030 U
103
45-122
2,4,5,6-TCMX
1.0
ug/L
1.00
IA7
44-134
Dawdrlaob% )h-y/
1.1
u91L
1.00
109
37-149
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Pape 18 of 21

QUALITY CONTROL DATA
Semivolatile Organic Compounds by GC - Quality Control
Balch 4B09003 - EPA 3510C - Continued
Matrix Spike Dup (4B09003-MSD1)
Prepared: 02/09/2014 07:54 Analyzed: 02114/201412:24
Source: C400990-03
Spike
Source
%REC
RPD,
Anal vte
Result Elm
ML
Units
Level
Result
%REC
Limits
RPD
Man Notes
4,4'-DDT
1.2
0.050
ug/L
1.00
0.049 U
122
35-160
1
25
Aldrin
1.1
0.050
ug/L
1.00
0.041 U
107
42-122
0.5
25
Dieldrin
1.1
0.050
ug/L
1.00
0.045 U
108
36-146
1
25
Endrin
1.1
0.050
ug/L
1.00
0.041 U
108
30-147
1
25
gamma-BHC
1.1
0.050
ug/L
1.00
0.034 U
110
19-140
1
25
Heptachlor
1.0
0.050
ug/L
1.00
0.030 U
105
45-122
2
32
2,4,5C-TCMX
a98
Lg4
1.00
98
44-134
Ll-6bobiplreayl
1.0
W4
IAO
104
37-149
Balkh 4BO9004 - EPA 3510C
I
,
Blank (4609004-BUCt)
Prepared: 02/09/2014 08:00 Analyzed: 02/14/2014 11:44
Spike Source %REC RPD
Ana
Result
Elan
ML
Units
Level Resu %REC limits RPD LIMR Notes
PCB-1016/1242
0.43
U
0.50
ug/L
PCB-1221
037
U
0.50
ug/L
PCB-1232
0.45
U
050
ug/L
PCB-1248
0.014
U
0.50
ug/L
PCB-1254
0.37
U
0.50
ug/L
PCB-1260
0.45
U
0.50
ug/L
Z4,56-TCMX
1.0
WIL
1.00 103 45-151
Diecadrhrobipheny!
a67
U94
!AO 67 42-M
LCS (4B09004-BS1)
Prepared: 02/09/2014 08:00 Analyzed: 02/14/2014 12:37
Spike Source %REC
RPD
Anailrle
Result
Elm ML
Unim
Level Result %REC Umfts RPD
)M Notes
PCB-1016/1242
11
0.50
ug/L
10.0 107 50-114
PCB-1260
11
0.50
ug/L
10.0 106 8-127
2,4,5,6-Taa
a99
tg4
1.00 99 45-151
Decacftbrnbpbevyl
0.98
u91L
1.00 98 42-159
Matrix Spike (4609004-MS1)
Prepared: 02/09/2014 08:00 Analyzed: 02/14/201412:50
Source: C400990-03
Spike Source %REC
RPD
Anebft
Resu
Ela9 e4L
Unite
Level Resin %REC !1ID[ts RPD
Limit Notes
PCB-1016/1242
11
0.50
ug/L
10.0 0.43 U 107 50-114
PCB-1260
11
0.50
ug/L
10.0 0.45 U 112 8-127
1,4,56-TCMX
1.1
U91L
1.00 108 45-151
Decaohbrabi -h 4
1.0
u¢L
1.00 104 42-159
Matrix Spike Dup (4BO9004-MSD1)
Prepared: .02/09/2014 08:00 Analyzed: 02/14/201413:03
Spike
Source
%REC
RPD
Anal ltlae
Result Flag E91
Unib
Level
Resul %REC
Limits RPD
Limit Notes
PCB-1016/1242
11 050
ug/L
10.0
0.43 U 108
50.114 0.5
25
PCB-1260
11 0.50
ug/L
10.0
0.45 U 113
8-127 0.8
25
Z4,56-7a4X
1.0
u91L
1.00
101
45-151
D-chbrob#*enyl
1.1
MIL
1.00
110
42-159
FINAL
TNs report relates only to the sample as received by the laboratory, and may only be reproduced In
full.
Page 19 of 21

FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
7 The reported value is between the laboratory method detection limit(MDQ and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL Is roughly equivalent to the practical quantitation limit (PQQ and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content
QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, the impact
on data quality is minimal.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was
accepted based on acceptable L(S recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is
ND, the impact on data quality is minimal.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 21

m
CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD
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P",21of21

i
AGNEr
ARE���
January 5, 2012
Ms. Vicki Weber
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SLrTBJ: Biannual stormwater sampling
Dear Ms Webb:
E
MAR - 6 2012 ;?
I
Ral^inh .-i Office
Enclosed is a paper copy of Magneti Marelli's Stormwater Discharge Outfall (SDO) Quantitatvie
Monitoring Report with lab analysis attached. Outfall #001 was checked on 11/04/11 during a
thunderstorm when there was flow from the discharge pipe (Pipe 02). I pulled the sample and
onsite observation was also taken. The flow was a light brown in color without any floating or
suspended solids.
A separate test on process water (referred to as vibrator spray) was included in this report, but is
completely unrelated to the stormwater runoff test results. The lab should have separated these
samples but included them in the same report. I apologize for any confusion or inconvenience.
This report contains carefully prepared data, as factual and accurate as possible. Should you have
any questions I can be contacted at [phone] or [phone] cell.
Sincerely,
�G
Eric Gislason
Environmental Consultant
Magneti Marelli Powertrain USA LLC
2101 Nash Street
P.O. Box 548
Sanford, NC 27331.0548
Phone: [phone]
Fax: [phone]
''ti

STORMWATER DISCHARGE OUTFALL (SDO)
QUALITATIVE MONITORING REPORT
BMP Checklist #6
-IPDES PERMIT No. NCG030012
FACILITY: Magneti Marelli USA, Inc.
COUNTY: Lee
PHONE: [phone]
INSPECTOR: :Z , Al zn 'IDATE:
Z1, Y` /l
OUTFALL No.
OUTFALL TYPE
RECEIVING STREAM:
SDO-
❑ DITCH PIPE ❑ CATCH BASIN
UT to Lick Creek
❑ Dry weather observation Wet weather observation
❑ No flow during dry weather ❑ Flow during dry weather ❑ Standing water during dry weather
Describe the industrial activities occurring within the outfall drainage area.
COLOR - Describe the tint (e.g., light, medium, dark) and color (e.g. red, brown, green, blue).
JJdischarge
�!
G D
ODORd Describe any distinct odors (e.g. gasoline, rotten eggs, chlorine) the discharge may have.
/V©/e
C.I_ARITY - Choose the number that best ranks the clarity of the discharge, where 1 is clear and 10 is very
cloudy.
1 2 04 5 6 7 8 9 10
FLOATING SOLIDS - Choose the number that best ranks the amount of floating solids in the discharge,
where 1 is no solids and 10 is the surface covered with floating solids.
1 0 3 4 5 6 7 8 9 10
SUSPENDED SOLIDS - Choose the number that best ranks the amount of suspended solids in the discharge,
where 1 is no solids and 10,,is extremely muddy.
1 2 3 4 5 6 7 8 9 10
FOAM -
Is there any foam on or in the stormwater discharge? yes no
OIL SHEEN -
Is the discharge the
there oil sheen visible on stormwater or at outfall? yes no
DEPOSITION -
Are there deposits of sediment or other material at the outfall? yes no
EROSION -
Is there erosion at or immediately below the outfall? yes no
List and describe other obvious indicators of stormwater pollution:
Has a signifpicagt spill occurred within this outfall's drainage area since previous inspection?
Yes N (If Yes, attach copy of spill report)
By this signature, I certify that his report is accurate and complet .. o the best of m knowledge:
Permittee' Signature Inspectors Signature
Magneti ,Vfarelli USA, Inc. Stormwater Pollution Prevention Plan
Appendix A BMP Checklist #6

0
iT'EST
Q 6701 Conference Drive, Raleigh, NC 27607
ph�
-(91g) 83-4,4984. tax: '(919),834-6497
NCWW Cert#57, NCDW Cerl#37731
J 6624 Gordon Road. Unit G, Wilmington, NC 28411
P6: (910) ' 63.091 tax: [phone]
NCWW Cort#'75, NCDW Cert#37721
6300 Ramada Dr., Suite C2, Clemmons, NC 27012
ph: (336) 766-78 1 46. tax; (3W'M672514
NCWW Cert#103, NCDW Cert#37733
Report Results To:
Company: ( IM41� e,_
Address:
Attn:
Phone:
Fax:
Sampled by (signature):
Chain of Custody
Bill To-
Tritest W.O.# 011'W'717
Project Reference: I*
Project Number. lilt -001-7
Purchase Order #:
50 Standard Report Delivery
0 Rush Report Delivery (w/surcharge)
—Rush projects are subject to prior approval by
the 1660ratory.
Requested,Due Date:
Sample Description
giart Date
`�—E"---D'
ho� Date
4tr,
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14-
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Start
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lure)
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Received te (signature)
Date
11/1(
Time
/b�7
§-elinquished by (signature)
Received by (signature)
Date
Time
Relinquished by (signature)
Received by (signature)
Date
Time
Receipt Conditions (Lab Use Only)
4±2'C 0 Temp: C
Res. Chlorine:
0 Absent 0 Present 0 n/a
Acid preserv. <2?
[I Yes 0 No 0 n/a
Base preserv, > 12?
0 Yes 0 No 0 n/a
I'A ( 11/lc

o Page 1 of 1
7Ra TIE ST
Laboratory Report
Lob tocotion :R' lab Cocofion 'C' Lob [ctilroti `tW'
NCNYW Cert.#: 067 NC/DW Cert.#: 37731 NCMiW Cert.# 103 NC/D1N Cert# J33 NC/INW Cert # 075 tVC/DUV Ceri # 36701 Conference C>r, Raleigh, Nc 27607 6300 Ramada Dr, Suite C2 Clemmons, NG6624 Gordon Rd Unit G; Wilmington NC 28411ph: [phone] Fax: [phone] Ph: (336) 766-784fi Fax(336} 7&6-25Ph: (910) Z63-9793. Fair. [phone]
Project No.:01 Report pate: 11/117/9011
ProjectID: 1111-007 Date Received: 11111/2011
— Prepared for --
CHRiS S. CAMERON
CAMERON TESTING SERVICES
219 S. STEELE STREET
SANFORD, NC 27330
Nb. Sample 1t)
001 1111-007-005 STORMWATER
Test Performed
Reviewed by:
-�2 4- .r 4- .—,-
for Tritest, Inc.
Work Order #: 1111-00767
Cust.- Code: CA4240
Cust.�P:O:#:

1.
NC, DENR #645
NC PHHS #37799
US EPA #NC01918
Cameron Testing -Services, Inc:_
Nov. 2Q11 Stormwater
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Magneb, 'M Celli
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Sample Information
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•MAT
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11/04711TYpe:
Grab
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Yes
Data
Review t
L echnlcian Date
Report
Review
La hector Date
219 S. Steele Str.
Sanford NC 27330
919-208-4240
chris a carn=ntestin&corn

NC DENR #645
NC PHHS #37799 Cameron Testing Services, Inc.
US EPA #NC01 918
For —q— 6'002-O&G'c6ridehfnA6n' so high,
Nov. 2011 O&G CheckOM
y2 sofsampawasused.
"
Magneltl-Mirelli
Sample Infortnaflon
CSC/DP
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Analyses and R
04w
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/
L-db Technician
Date
Report
Review
Lab Director
Daft
219 S. Steele
Str.
Sanford NC 27330
919-208-1240
chfis@carnerontesting,corn

A
�1qR ea
March 23, 2011
Ms. Vicki Weber
NCDENR
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SUBJ: Biannual stormwater sampling
Dear Ms Webb:
Enclosed is a paper copy of Magneti Marelli's Stormwater Discharge Outfall (SDO) Quantitatvie
Monitoring Report with lab analysis attached. Outfall #001 was checked on 10/14/10 during a
thunderstorm when there was flow from the discharge pipe. I pulled the sample and onsite
observation was also taken. The flow was a light grey in color without any floating or suspended
solids. The temperature was ambient or 20.1 degree Celcius.
I apologize in the delay of sending you this report. This was simply an oversight on my part. This
report contains carefully prepared data, as factual and accurate as possible. Should you have any
questions I can be contacted at [phone] or [phone] cell.
Sincerely,
Eric Gislason
Environmental Consultant
Magneti Marelli Powertraln USA LLC
2101 Nh5h Street
PO. Box 548
Sanford, NC 27331.0548
Phone: [phone]
Fax: [phone]

or-"�
Sut'y
STORMWATER DISCHARGE OUTFALL (SDO)
QUALITATIVE MONITORING REPORT
BMP Checklist #6
RECEiVE,D
44AR28201,
RaleighRegio a10., e
NPDES PERMIT No. NCG030012
FACILITY: Magneti Marelli USA, Inc.
COUNTY: Lee
PHONE: [phone]
INSPECTOR: 6'f/G
DATE: c;Z N D
OUTFALL No.
OUTFALL TYPE: /
RECEIVING STREAM:
SDO-
❑ DITCH PIPE ❑ CATCH BASIN
UT to Lick Creek
❑ Dry weather observation Wet weather observation
❑ No flow during dry weather ❑ Flow during dry weather ❑ Standing water during dry weather
Describe the industrial activities occurring within the outfall drainage area.
COLOR - Describe the discharge tint (e.g ligh , medium, dark) and color (e.g. red, brown, green, blue).
it I k / rt° •
ODOR - Describe any distinct odors (e.g. gasoline, rotten eggs, chlorine) the discharge may have.
CLARITY - Choose the number that best ranks the clarity of the discharge, where 1 is clear and 10 is very
cloudy.
1 2 3 4 5 6 7 8 9 10
FLOATING SOLIDS - Choose the number that best ranks the amount of floating solids in the discharge,
where 1 is no solids and 10 is the surface covered with floating solids.
1 2 3 4 5 6 7 8 9 10
SUSPENDED SOLIDS - Choose the number that best ranks the amount of suspended solids in the discharge,
where 1 is no solids and 10 is remely muddy.
1 2 3 4 5 6 7 8 9 10
FOAM -
Is there any foam on or in the stormwater discharge? yes no
OIL SHEEN -
Is there oil sheen visible on the stormwater discharge or at the outfall? yes no
DEPOSITION -
Are there deposits of sediment or other material at the outfall? yes no
EROSION -
Is there erosion at or immediately below the outfall? yes no
List and describe other obviou indicators of stormwater pollution:
oone- o
Has a sign i ' t spill occurred within this outfall's drainage area since previous inspection?
Yes 22 (If Yes, attach copy of spill report)
By this signature, 1 ce . !Ttthis report is accurate and comp) "eto.thebl my �owiedge:
/V)'\+� I Cc
Permittee's Signature Inspector's Signature
Magneti Marelli USA, Inc.
Appendix A
Stormwater Pollution Prevention Plan
BMP Checklist #6

RESEARCh & ANA[yTICA[
LABORATORIES, INC.
Analytical / Process Consultations
Phone [phone]
CHAIN OF CUSTODY RECORD
WATER / WASTEWATER MISC.
,COMPANY
ja
•: •
— —
•
•
•
• • • i
•
STREET ADD-
•-•
CONTACT •
717
.•
NRECEIVED
.:I
i
BY

RESEARCh & ANAtyTICA[
I.AbORAT®RIES� INC. ,,C,,,
Analytical/Process Consultations "
November 3, 2010
Magneti Marelli
P.O. Box 548
Sanford, NC 27331
Attention: Michael Stowe
Chemical Analysis for Sampling identi ked as Stormwaterl collected 14 October 2010
L• Project Number: N/A
C is (mBlL C r 0-
53.0 <5.0 <0.005 7.49 YJ, AA, JC
mg/L = milligrams per Liter = parts per million (ppm)
SU = Standard Units
< = less than or Below Quantitation Limit (BQL)

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
August 23, 2002
CHARLES JEFFERY
MAGNETI MARELLI USA INCORPORATED
2101 NASH ST
SANFORD, NC 27330
Subject: NPDES Stormwater Permit Renewal
MAGNETI MARELLI USA INCORPORATED
COC Number NCG030012
Lee County
Dear Permittee:
In response to your renewal application for continued coverage under general permit NCG030000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued
pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983.
The following information is included with your permit package:
A new Certificate of Coverage
* A copy of General Stormwater Permit NCG030000
* A copy of the Analytical Monitoring Form (DMR)
* A copy of a Technical Bulletin for the general permit
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or
decree.
If you have any questions regarding this permit package please contact Bill Mills of the Central Office Stormwater
and General Permits Unit at [phone], ext. 548
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Stormwater & General Permits Unit Files
Raleigh Regional Office
e�ACD NENR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

4,
�O� N1AT9Q Michael F. Easley, Governor
William G. Ross Jr., Secretary
tea
G North Carolina Department of Environment and Natural Resources
Gregory J. Thorpe, Ph.D.
"1 Acting Director
4 Division of Water Quality
December 27, 2001
CHARLES JEFFERY
MAGNETI MARELLI USA INCORPORATED
2101 NASH ST
SANFORD, NC 27330
Subject: NPDES Stormwater Permit Renewal
MAGNETI MARELLI USA INCORPORATED
COC Number NCG030012
Lee County
Dear Permittee:
Your facility is currently covered for stormwater discharge under General Permit NCG030000. This permit expires
on August 31, 2002. The Division staff is currently in the process of rewriting this permit and is scheduled to have
the permit reissued by late summer of 2002. Once the permit is reissued, your facility would be eligible for
continued coverage under the reissued permit.
In order to assure your continued coverage under the general permit, you must apply to the Division of Water
Quality (DWQ) for renewal of your permit coverage. To make this renewal process easier, we are informing you in
advance that your permit will be expiring. Enclosed you will find a General Permit Coverage Renewal
Application Form. The application must be completed and returned by March 4, 2002 in order to assure continued
coverage under the general permit.
Failure to request renewal within this time period may result in a civil assessment of at least $250.00. Larger
penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility
without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and
could result in assessments of civil penalties of up to $10,000 per day.
Please note that recent federal legislation has extended the "no exposure exclusion" to all operators of industrial
facilities in any of the I 1 categories of "storm water discharges associated with industrial activity," (except
construction activities). If you feel your facility can certify a condition of "no exposure", i.e. the facilty industrial
materials and operations are not exposed to stormwater, you can apply for the no exposure exclusion. For additional
information contact the Central Office Stormwater Staff member listed below or check the Stormwater & General
Permits Unit Web Site at http://h2o.enr.state.nc.us/su/stormwater.htmi
If the subject stormwater discharge to waters of the state has been terminated, please complete the enclosed
Rescission Request Form. Mailing instructions are listed on the bottom of the form. You will be notified when the
rescission process has been completed.
If you have any questions regarding the permit renewal procedures please contact Joe Albiston of the Raleigh
Regional Office at 919-571-4700 or Bill Mills of the Central Office Stormwater Unit at [phone], ext. 548
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Raleigh Regional Office
e�A
NCDENR
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

V � RECEIVED
i
State of North Carolina ®EH N R- RAL RO
Department of Environment, Health and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27604
James B. Hunt, Jr., Governor A. Preston Howard, Jr., P. E.
Jonathan B. Howes, Secretary, Director
April 23, 1993
Fred Gopal
Weber, USA Inc.
2101 Nash Street
Sanford, NC 27330
Subject: General Permit No. NCG030000
Weber, USA Inc.
COC NCG030012
Lee County
Dear Mr. Gopal:
In accordance with your application for discharge permit received on September 16, 1992, we are
forwarding herewith the subject certificate of coverage to discharge under the subject state - NPDES general
permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215 .1 and the
Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated
December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the Division
of Environmental Management. The Division of Environmental Management may require modification or
revocation and reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Environmental Management or permits required by the Division of Land Resources, Coastal Area
Management Act or any other Federal or Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Mr. Bill Mills at telephone number 919/733-
5083.
cc:
Sincerely, .
Original Signed By
Coleen H. Sullins
A. Preston Howard, Jr., P.E.
Raleigh Regional Office
Pollution Prevention Pays
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
1.
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE NO, NCG030012
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
Weber, USA Inc.
is hereby authorized to discharge stormwater from a facility located at
Weber, USA Inc.
2101 Nash Street
Sanford
Lee County
to receiving waters designated as an unnamed tributary to San Lee Park Lake in the Cape Fear River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III
and IV of General Permit No. NCG030000 as attached.
This Certificate of Coverage shall become effective April 23, 1993
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day April 23, 1993.
Original Signed ay
Coleen H. Sullin
A. Preston Howard, Jr., P.E., Director
Division of Environmental Management
By Authority of the Environmental Management Commission

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f
State of North Carolina S
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
William G. Ross Jr., Secretary
Gregory J. Thrope, Ph.D., Acting Director
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Charles Jeffery
Magneti Marelli Powertrain USA Inc
2101 Nash St
Sanford NC 27330
:7�
•
.NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOUR EC s
5/30/2002
SUBJECT: NOTICE OF VIOLATION AND REVOCATION FOR NON PAYMENT
PERMIT NUMBER NCG030012
Magneti Marelli USA Incorporated
Lee COUNTY
Dear Permittee:
TV
« oW2�
Payment of the required annual administering and compliance monitoring fee of $80.00 for this year has not
been received for the subject permit. This fee is required by Title 15 North Carolina Administrative Code 2H.0105, under
the authority of North Carolina General Statutes 143-215.3(a)(1), (1 a) and (1 b). Because this fee was not fully paid within
30 days after being billed, this letter initiates action to revoke the subject permit, pursuant to 15 ncac 2H.0105(b) (2) (k)
(4), and G.S. 143-215.1 (b) (3).
Effective 60 days from receipt of this notice, subject permit is hereby revoked unless the required Annual .
Administering and Compliance Monitoring Fee is received within that time. Discharges without a permit are subject to the
enforcement authority of the Division of Water Quality. Your payment should be sent to:
N.C. Department of Environment and Natural Resources
Division of Water Quality
Budget Office
1617 Mail Service Center
Raleigh, NC 27699-1617
If you are dissatisfied with this decision, you have the right to request an administrative hearing within Thirty (30)
days following recipt of this notice, identifying the specific issues to be contended. This request must be in the form of a
written petition conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative
Hearings, Post Office Drawer 27447, Raleigh, North Carolina, 27611-7447. Unless such request for hearing is made or
payments received, revocation shall be final and binding. If you have any questions, please contact:
Mr. Ken Schuster, Raleigh Water Quality Regional Supervisor, [phone].
Sincerely,
r
PO�F�6gor�y
rpe,�Ph.D.
cc: Supevisor, Water Quality Permits and Engineering Unit
Raleigh Regional Office
County Health Department
` P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled / 10% post -consumer paper

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