NCG080583_MONITORING INFO_20181206

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/v O'$�S�'S
DOC TYPE
❑ HISTORICAL FILE
?�, MONITORING REPORTS
DOC DATE
❑ �ot� M
YYYYMM DD

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCG080000
CERTIFICATE OF COVERAGE NO. NCG08 O 5
FACILITY NAME in, n 4 d 0 r KI A+ 1 W (A
PERSON COLLECTING SAMPLES G(A 1 Lord+
CERTIFIED LABORATORY V/10 � ua rt c u Lab # 3 �ccL
Lab #
SAMPLES COLLECTED DURING CALENDAR YEAR: 2ol R
(This monitoring report is due at the Division no later than 30 days from
f����o the sampling results from the laboratory.)
C11/C �pr��tP�
PHONE NO. {42U) 12 �4 P
DEC a s zags
PLEASE SIGN ON THE REVERSE 4
CENTRAL FILES
Part A: Vehicle Maintenance Areas Monitoring Requirements DWR SECTION
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? )c yes ,no
(if yes, report your analytical results in the table immediately below)
Outfall
No.
Date
Sample Collected,
moldd/yr
00S30
00400
00556
Total Suspended Solids,
114LL
pH,
Standard units
Oil and Grease,
New Motor Oil Usage,
Annual averse ailmo
Benchmark
100
Within 6.0 — 9.0
30
-
S- —
bflt i
P
C
'U 1►
q
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, 'you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Part B: Oil/water Separators and Secondwy Containment Areas at Petroleum Bulk Stations and Terminals
Outfall
No.
Date _
Sample Collected,
mold r.
' 00556
, . ' 00530
00400
Oil and Grease,
Total; Suspended`Solids;
pH,
,Standard units
Permit Limit
-
30
400
6.0 — 9.0
STORM EVENT CHARACTERISTICS:
Date l0l I I (first event sampled)
Total Event Precipitation (inches):
Date (list each additional event sampled this reporting period, and rainfall amount)
Total EventPrecipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SWU-250-102107
Page I of 2

"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
�A, A J)t.AA—&-Ae-4
(Signatur f Permittee)
o ksoi ie)
(Date)
SWU-250-102107
Page 2 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCGO80000 SAMPLES COLLECTED DURING CALENDAR YEAR:
CERTIFICATE OF COVERAGE NO. NCG08 iD -s e A (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME I COUNTY 1 { 1
PERSON COLLECTING SAMPLES ln, a V, j L b t2i _ _ PHONE NO.
CERTIFIED LABORATORY }?/1 r�
Lab # PLEASE SIGN ON THE REVERSE 4
Part A: Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? I yes _no
(if yes, report your analytical results in the table immediately below)
Outfall
No.
Date
Sample Collected,
mo/dLYZ
00530,
00400
00556 -
Total Suspended Solids, '
pH,
Staadard'units
Oil 'and "Grease,
New Motor Oil Usage,
Annual ave a allmo
Benchmark
-
100
Withirf 6.'0 — 9.0..
30'
S -5
. to
10111 E3
- I I
it)
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you trust implement Tier I or Tier 2 responses.
See General Permit text.
Part B: Oil/water Separators and Secon Containment Areas at Petroleum Bulk Stations and Terminals
Outfall
No.
Date
Sample Collected,
mo/dd1yr
00556
00530
00400
Oil and Grease,
Total Suspended Solids,
pH,
Standard units
Permit Limit
30
100
6.0 — 9.0
STORM EVENT CHARACTERISTICS:
Date 00(first event sampled)
Total Event Precipitation (inches): 2 } 104,US
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SWU-250-102I07
Page 1 of 2

"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
L2L::QD,OL) 1413b116
(Signature,%f Permittee) (Date)
swu-250-102107
Page 2 of 2

laneAhalytical
www.petbla4wm
October 25, 2018
Mr. Michael DeBraske
Schneider National, Inc.
PO Box 2545
Green Bay, WI 543062545
RE: Project: SNI-Charlotte, NC
Pace Project No.: 92403089
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. DeBraske:
Enclosed are the analytical results for sample(s) received by the laboratory on October 11, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
[e-mail]
[phone]
Project Manager
Enclosures
cc: Caryssa Berg, Schneider National
Mr. Michael DeBraske, GEI Consultants, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 14

Pace Analytical Services, LLC
aceAnalytrcal® 9800 KlnCey Ave. Suite 100
Huntersvllle, NC 28078
w+w'•Pacelftcom [phone]
CERTIFICATIONS
Project: SNI-Charlotte, NC
Pace Project No.: 92403089
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
LoulsianalNELAP Certification # LA170028
Florida/NELAP Certification M E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification M 5342
VirginialVELAP Certification #: 460221
North Carolina Wastewater Certification M 12
Asheville Certification iDs
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
FlorldalNELAP Certification #: E87648 South Carolina Certification M 99030001
Massachusetts Certlflcation M M-NC030 VirginialVELAP Certification M 460222
North Carolina Drinking Water Certification M 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 14

(.�15'neAnalytical
www.paodeftcom
Project: SNI-Charlotte, NC
Pace Project No.: 92403089
Lab ID Sample ID
92403089001 SP-1
92403009002 SP-7
92403089003 SP-3
92403089004 SP-4
92403089005 SP-5
92403089006 SP-6
SAMPLE ANALYTE COUNT
Method
EPA 1664B
SM 254OD-2011
EPA 9040C
EPA 1664B
SM 254OD-2011
EPA 9040C
EPA 1664B
SM 25400-2011
EPA 9040C
EPA1664B
SM 2540D-2011
EPA 9040C
EPA1664B
SM 25400-2011
EPA 9040C
EPA1664B
SM 254OD-2011
EPA 9040C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
Analytes
Analysts Reported Laboratory
JMS
1
PASI-C
CEH
1
PASI-A
SMK
1
PASI-A
JMS
1
PASI-C
CEH
1
PASI-A
SMK
1
PASI-A
JMS
1
PASI-C
CEH
1
PASI-A
SMK
1
PASI-A
JMS
1
PASI-C
CEH
1
PASI-A
SMK
1
PASI-A
JMS
1
PASI-C
CEH
1
PASI-A
SMK
1
PASI-A
JMS
1
PASI-C
CEH
1
PASI-A
SMK
1
PASI-A
Page 3 of 14

acmnalytical o
wwwpecefabacom
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huntersville, NE 2807E
[phone]
Project: SNI-Charlotte, NC
Pace Project No.: 92403089
Sample: SP-1 Lab ID: 92403089001 Collected: 10/11118 08:35 Received: 10/11/1 B 11:25 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
2540D Total Suspended Solids
Total Suspended Solids
9040 pH
pH at 25 Degrees C
Analytical Method: EPA 1664B
NO mg1L 5.0 1 10/25/18 04:17
Analytical Method: SM 254OD-2011
8.5 mg1L 2.6 1 10/113/18 00:56
Analytical Method: EPA 9040C
6.3 Sid. Units 0.10 1 10/15/18 15:04
H3
Sample: SP-7
Lab ID: 92403089002 Collected:
10/11/18 09:35
Received: 10/11/18 11:25 Matrix: Water
Parameters
Results Units Report Limit OF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
5.0 mg1L
5.0 1
10/25/18 04:17
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
43.6 mg1L
5.0 1
10/13/1 B 00:59 D6
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
7.3 Std. Units
0,10 1
10/15/18 15:21 H3
Sample: SP-3
Lab lD: 92403089003 Collected:
10111/18 08:45
Received:
10/11/18 11:25 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
10.0 mg1L
5.0
1
10/26/18 04:17
2540D Total Suspended Solids,
Analytical Method: SM 254OD-2011
Total Suspended Solids
497 mg1L
25.0
1
10/13/18 01:00
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.3 Std. Units
0.10
1
10/15/18 15:07 H3
Sample: SP-4
Lab ID: 92403089004 Collected:
10/11/18 08:55
Received:
10/11/18 11:25 Matrix: Water
Parameters
Results Units Report Limit
OF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg1L
5.0
1
10/25/18 04:18
Date: 10/25/2018 03:07 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4of14

aceAnalyti+cal
wwwpacdabs.c6m
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92403089
Pace Analytical Services, LLC
9800 Kincey Ave. Sulte 100
Huntersville. NC 28078
[phone]
Sample: SP-4 Lab ID: 92403089004 Collected: 10/11/18 08:55 Received: 10/11/18 11:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 25400-2011
Total Suspended Solids 289 mg1L 10.0 1 10/13/18 01:00
9040 pH Analytical Method: EPA 9040C
pH at 25 Degrees C 6A Std. Units 0.10 1 10/15/18 15:10 H3
Sample: SIP-5
Lab ID: 92403089005 Collected:
10/11/18 09:05
Received: 10/11/18 11:25 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
5.6 mg1L
5.0 1
10/25/18 04:21
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
333 mglL
25.0 1
10/13/18 01:00
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
7.8 Std. Units
0.10 1
10/15/18 15:14 H3
Sample: SP-6
Parameters
Lab iD: 92403089006 Collected: 10111118 09:20
Results Units Report Limit DF
Received: 10/11/18 11:25 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 16648
Oil and Grease
ND mglL
5.0 1
10/25/18 04:21
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Total Suspended Solids
476 mglL
25.0 1
10/13/18 01:00
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
7.6 Std. Units
0.10 1
10/15/18 15:19 H3
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
Date: 10/25/2018 03:07 PM wlthout the written consent of Pace Analytical Services, LI_C. Page 5 of 14

acemalytical'
www.pacelabe.com
QUALITY CONTROL DATA
Project: 5N1-Charlotte, NC
Pace Project No.: 92403089
QC Batch: 438223 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92403089001, 92403089002, 92403089003, 92403089004, 92403089005, 92403089006
METHOD BLANK: 2409478 Matrix: Water
Associated Lab Samples: 92403089001,92403089002,92403089003,92403089004,92403089005,92403089006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L ND 4.8 10/25/18 04:13
Pace Analytical Services, LLC
9800 KlnteyAve. Suite 100
Huntersvllle, NLt 28078
[phone]
LABORATORY CONTROL SAMPLE:
2409479
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
Qualifiers
Oil and Grease
mg1L
38.5 37.2 97
78-114
MATRIX SPIKE SAMPLE:
2409480
35423532001 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Oil and Grease
mglL
1.1 U 38.5 37.1
96
78-114
Results presented on this page era In the unite Indicated by the "Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/26/2018 03:07 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 14

aceAnalytical®
www.pacelobil,com
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92403089
QC Batch: 436094 Analysis Method: SM 2540D-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92403089001
METHOD BLANK: 2399711 Matrix: Water
Associated Lab Samples: 92403089001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 10/13/18 00:51
Pace Analytical Services, LLC
9800 Klncey Aye. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2399712
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 251 242 96 90-110
SAMPLE DUPLICATE: 2399713
Parameter
Total Suspended Solids
92403108002 Dup
Units Result Result RPD Qualifiers
mglL ND ND
SAMPLE DUPLICATE: 2399714
92403275003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 179 206 14 D6
Results presented on this peps are In the units Indicated by the 'units' column except where on alternate unit Is presented to the right or the fesutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/25/2018 03:07 PM without the wrltten consent of Pace Analytical Services, I.I.C.
Page 7 of 14

aceAnaljftale
wrrecpspela6ac=
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92403089
QC Batch: 436095 Analysis Method: SM 254OD-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lacs Samples: 92403089002, 92403089003, 92403089004, 92403089005, 92403089006
METHOD BLANK: 2399715 Matrix: Water
Associated Lab Samples: 92403089002, 92403089003, 92403089004, 92403089005, 92403089006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L NO 2.5 10/13/18 00:59
Pace Analytical Services, LLC
9800 Kint:eyAve. Suite 100
Huntersville, It 28078
[phone]
LABORATORY CONTROL SAMPLE: 2399716
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 251 250 100 90-110
SAMPLE DUPLICATE: 2399717
92403089002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 43.6 51.9 17 D6
SAMPLE DUPLICATE: 2399718
92403120005 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Sollds mglL 8.8 15.0 52 06
Results presented on this page are In the units Indicated by the "Unite column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/25/2018 03:07 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 14

acMhalytical
wwwpecekbacom
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92403089
QC Batch: 436234 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Associated Lab Samples: 92403089001, 92403089002, 92403089003, 92403089004, 92403089005, 92403089006
SAMPLE DUPLICATE; 2400364
9240315B001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std, Units 6.4 6.4 0 H3
SAMPLE DUPLICATE: 2400365
92403134003 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.2 6.2 0 H3
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
Results presented on this peps are In the units Indleated by the "Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/25/2018 03:07 PM without the written consent of Pace Analytical Services, LLC,
Page 9 of 14

Pace Analytical Services, LLC
(�5aceftlyticalm 9800 KintieyAvQ. Suite 100
Huntersville, N�` 28078
•Pa�m� [phone]
QUALIFIERS
Project: SNl-Charlotte, NC
Pace Project No.: 92403089
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL = Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentralion.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values,
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW84e Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAG Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
De The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 03:07 PM without the writteri consent of Pace Analytical Services, I.L.C. Page 10 of 14

(�Iacie'Analytcal
wwwpecwoft¢om
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersvllle, NC 28078
[phone]
Project: SNI-Charlotte, NC
Pace Project No.: 92403089
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92403089001
SP-1
EPA 1664B
438223
92403089002
SP-7
EPA 1664E
438223
92403089003
SIP-3
EPA1664B
438223
92403089004
SP-4
EPA 1664B
438223
92403089005
SIP-5
EPA1664B
438223
92403089006
SP-6
EPA1664B
438223
92403089001
SP-1
SM 2540D-2011
436094
92403089002
SP-7
SM 254OD-2011
436095
92403089003
SP-3
SM 254OD-2011
436095
92403089004
SP-4
SM 2540D-2011
436095
92403089005
SP-5
SM 254OD-2011
436095
92403089006
SP-6
SM 254OD-2011
436095
92403089001
SP-1
EPA 9040C
436234
92403089002
SP-7
EPA 9040C
436234
92403089003
SP-3
EPA 9040C
436234
92403089004
SP-4
EPA 9040C
436234
92403089005
SIP-5
EPA 9040C
436234
92403089006
SP-6
EPA 9040C
436234
Date: 10/25/2018 03:07 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 14

Document Name:
-, Document -No.,
Document Revised: February 7, 2018 I
Pete 1 of 2 +
laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville 12/ Raleigh[] Mechanicsville[]
Client Nome: WO# : 92403089
Project a:
n �'�`r II1lll l �I �If 1�11l�! �l�
Courier. F d Ex CUPS U5P5 Client
❑ Commercial Upace []Other: 92403089
Custady Seal Present? ❑Yo$ M4 Seats intact? Des Dho r�r /
pate/initials Perron Examining eontenu: � - l + (-i tl
Packing Material: ❑Bubble Wrap �VBubble Bags ❑None ❑ Other Biological Tissue F ozen?
Thermometer: 92T045 Type of ice: �t ©Blue ONone Des❑No � �]N/A
QdGul ID:
Cooler Temp III: Correction factor: Add/Subtract ('C) p
Temp should be above freezing to 6'C
Cooler Temp Corrected ('C): []samples out of temp criteria, Samples an Ice, cooling process
has begun
USDA Regulated Sall e N/A, water sample)
Old samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
rlVes rlNe. lneludlns Namall end Puerto Weal? rites rlNe
Comments Dlecre en
Chain of Custody Present?
JVes
QNo
N/A
1,
Sam les Arrived within Hold Time?
Yes
No
N/A
2.
Short Hold lime Ana Le Q2 hr.?
Yes
I VrNo
ONJA
3.
Rush Turn Around Time Ra uested?
QYes.
a
N a
4.
Sufficient Volume?
tfft
No
QN1e.
S.
Correct Containers Used?
-Pace Containers Used?
—Of,
Yes
oNo
ON.
I]N/A
N A
6.
Containers Intact?
Ycs
EINLN
A
7.
01350lVed anal sis Samples Field rikered?
Y
Na
N/A
B.
Sample Labels Math COC-e
-lncludes Date(rIme/[D/Anal sis . Matrix:
Ver
❑No
I]N/A
9.
Heads ace In VOA Vials >5.6mm)?
ovel
ONO
6111.4
10.
Trip Blank Present?
TripBlank CustodySeals Present?
[]Yes
Yes
❑No
No
❑ //A
N A
11.
COMMENTS/SAMPLE DISCREPANCY
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review: 71rt�
Date/Time:
Field Date Required? ❑Yes []No
Date:
Date:
Page 12 of 14

80080! ica!`
Document Name:
Sample Conditlon Upon Recel t SCUR
Document Revised: February 7, 2018
Page 1 of 2
�.�Document.No.:
F•CAR•0-033-11ev,06
Issuing Authartt :
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Ewceptions: VOA, Collform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHS
**Bottom half of box is to list number of bottle
Project e ' WO# : 92403089
PM; RWC Due Dale. 10/25/18
CLIENT: 92-SCHNEIDER
YA00►►aV����
N
�ii°u��►u�i�t►���a�ii�ii�i�i
pH Adjustment
tog for Preserved Samples
sample t0
Type of preservative
pH upon receipt
Dote proservatlon adjusted
Time preservation
adjusted
Amount of preservative
added
Lot p
note: Wnenever Thera rf a aiscrepancy anecting mortn t.arouna compuance sampies, a copy or tors rorm wm ce sent to the inonn s amnna uttirm cercmarwn unite p.e.
Out of hold, Incorrect preservative, out of temp, Incorrect containers.
Page 13 of 14

CHAiNOF-CUSTODY 1 Analytical Request Document
o
The Chain -of -Custody is a LEGAL DOCUMENT.
All relevant
fields must be completed a=
ratety.
a_
ro
Section A
Section B
Section C
Required Client f.donnato
:
Required Protect Ltrornudion:
tmdte bdornm on:
Pa.,.
1 Of 1
tl
Repot; To
AC.etltipn'
Aaaress: 240
SuWM Rasa
Copy To
Conomw Nww
CNW10ft. NC 282$B
Address:
.ercer,mrt
Pam Quote:
.Fx
Prp(Cq Nac
SN-Ctwkme. NC
C [e-mail]
l,ocaw"Prmre: -
Regresteo DLx De'.e
Prwd a:
Pace Profile a: 2631.1
NC
!Anhds
Filtered
.
VATRIx
CME
0
COLLECTED
z
Preservatives
r-
-
$
u
mav t�
SAMPLE ID
w
�
c�
START
END
m
One Chameter per box.
ad
Ww
wP
�
�
Sample Ids must be unique
oov-
T—
orAR
is
DATE
TIME
DATE
TIME
1:..
I
/7y}
/"7�
SP-1
www®r
X
x
x
2:
+
%W
x
x
x
J
I
!
94
:- 3
SP-3
wT
x
x
x
I
.:4 _
SP4
wr
x
x
x
i
L
DDs'
SP-
v
wT
X
x
x
W1.
L
WT
x
x
UV
x
1
1
L
I
A°03 ONAL COMMENTS • - . !
�
- REINCOU13"M BYlAFFO.tATWN
F
_
'r DATE =
¢-.
`
- Ac�TI-D riY7AFFa3AT10N-;
OATE.
-
.�
r$11MPLE COIY>Arl°Irt8 '
If 12-
I
a-4 •
t
I-
Ty
'"
SAYPL M NUMAM G''.�-5�-. J ',T' •vc_ �
w-xcr•.c.e.or•.- ;..w - �'S.
�/wwx:z_.
_ �-a-3= - _ _ _
Pill U N m of SAMIP"ftCL
S >
SIGNATURE
$ ; L) v fig
I

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Resources General Permit No. NCGO80000
Date submitted y [1-711 a
CERTIFICATE OF COVERAGE NO. NCG08LL SAMPLE COLLECTION YEAR �Ly 18
FACILITY NAME f�(1�l QId fAI I �.(A S p c �+ I� f �PLE PERIOD ❑ Jan -June July -Dec
COUNTY -T� 61ECFxi or Monthlyl AA
— month
PERSON COLLECTING SAMPL APR 2 ��SCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY Lab Cert. # 5 ❑Zero -flow ❑Wa#er Supply ❑SA
r ��ES ❑Other
Comments on sample collection or analysis: CENTRAL
DWR SECTION
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?� yes Ono
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (if applicable)
ED No discharge this period'
f Date
Q4530
00400
00556
To# i Susndo ed
pN,
_
No" n Polai"�Oilrand Gr ae''�'se/TPH EPA
New Motor Oil Usage,
h111110
$Saririple Collected,
;Now'_g
� , ,
mo/tld/,yr
Solids, mg/,l
Standard units
Method 1664 (SGT.HEM}, mg/L
Mnual average gal/mo
;Benchmarks
,.. r. -
[SO.or l00see permit
Within 6.0, S! 0
15
31-7(
, 3
�-
3-7I
S 1�-.4
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfall;�
No ,f
<R�
:� 'Date
Sample +i:ollectetl,
mo/dd/yr
0055E
Non -Polar OiliandTGrea e/'fPH EPA Method
16b_4;(SG HEM}, rrrg/,L
00530
Total Suspended.5olids,
mg/L
Qg400
pH,
PtalidirdrunitMs
Permit;limit
-
15
501or 100 see permit
fi.0 - 9,0
1 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SW-250 last revised April 11, 2013
D­ } _ir'f

STORM EVENT CHARACTERISTICS:
Date 31'7118 (first event sampled)
Total Event Precipitation (inches):
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: If you report a sample value in excess of the benchmark, you must implement leer 1, Ver 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES � No ❑ fo
REGIONAL OFFICE CONTACT NAME: Z A in L d ><a h yt
Mail an original and one copy of this DM
in the case of "No Discharge" reports) to:
Division of Water Resources
Attn: DWR Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
all "No
worts, within 30 da,
f the lab results (or at end
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly
responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature c# Permittee)
�it���
(Date)
Additional copies of this form may be downloaded at: http://portal.ncdenr.org/web/wq/­ws/su/npdessw#tab-4
SWU=250 last revised April 11, 2013
Page 2 of 2

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Resources General Permit No. NCGO80000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG08_
FACILITY NAME
COUNTY
PERSON COLLECTING SAMPLES
LABORATORY Lab Cert. #
Comments on sample collection or analysis:
SAMPLE COLLECTION YEAR
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ❑ Monthly' month
DISCHARGING TO CLASS ❑ORW ❑HQW [-]Trout ❑PNA
❑Zero -flaw [—]Water Supply ❑SA
❑Other
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?[] yes Ono
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
No discharge this period'
Othfall'
No..
•. 1 ti i .
` r_ -Date
'Sample:Collected,
_a f �.. 'r
mo/dd/yr_.
' [i653D = y
0&00
Total'Suspended _;
_ � .}• r"' - Sys
Q�_5olids,�mgfl-; =
pH,
-
"Standard units
No�Polar Oiliad}Grease/TPli�'iEPA ;'jkiviiMotor0il
� `
Method 16WSGTYI�EM)„mg/L _
Usage,,
6n' � / r ♦., _ 19:5v` -'
Annual,,average:gal/mo
Benchmark
L,50'or
100:see,per>Yiil
-
within f>rOr9�0
-15z`�
-Y_ X-;
".. 'y1 - .ys
3
Z
S
3 1 -7 Iti—
'3 1
5
Part B. Oil/water Separators and Secondary Containment Areas at Petroleum Bulls Stations and Terminals (If applicable)
x
Dater
sarri re corrected
mo/da/Yr , ' '
r_i�DS30,,��
-
'Non Pplar0�l and Grease IEPA°�Method
1654;[SGT HAM),R/L
Total Sus` ended,Solitls
x;# �L:
FI ` FM
d' units
f4 Stan ard=
Permit Limn
s
-15'
S0�or200"�
r ° ay
t For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Pave 1 of 2

ac e Analytical
wwwpaoafab&WM
March 20, 2018
Mr. Michael DeBraske
Schneider National, Inc.
PO Box 2545
Green Bay, WI 543062545
RE: Project: SNI-Charlotte, NC
Pace Project No.: 92375878
Dear Mr. DeBraske:
Pace Analytical Services, LLC
9800 Kincey Ave. Sulte 100
Huntersvllle, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 07, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Caryssa Berg, Schneider National
Mr. Mlchael DeBraske, GEI Consultants, Inc,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical 5ervlces, LLC.
Page 1 of 13

Pace Analytical Services, LLC
6
ceAnalytr'cal 9800 KlnceyAve, Suite t00
Huntersville, NC 28078
a
W m•pacefala om (704 )875-9092
CERTIFICATIONS
Project: SNI-Charlotte, NC
Pace Project No.: 92375878
Charlotte Certification lDs
9800 Klncey Ave. Ste 100, Huntersvllle, NC 28078
Loulslana/NELAP Certification # LAII 70028
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification Ids
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
South Carolina Certification #: 99006001
Florida/NELAP Certification M E87627
Kentucky UST Certification M 84
VrginiaNELAP Certification M 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification A 99030001
VrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wrllten consent of Pace Analytical Services, LLC. Page 2 of 13

aceAnaIXical"
xavw.pecWsb&=n
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: SNI-Charlotte, NC
Pace Project No.: 92375878
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92375878001
SP-1
EPA 1664B
JMS
1
PASI-C
SM 25400
MJP
1
PAS! -A
EPA9040
KDF1
1
PASI-A
92375878002
SP-3
EPA 1664B
JMS
1
PASI-C
SM 2540D
MJP
1
PASI-A
EPA9040
KDF1
1
PASI-A
92375878003
SP-4
EPA 1664B
JMS
1
PASI-C
SM 2540D
MJP
1
PASI-A
EPA9040
KDF1
1
PASI-A
92375678004
SP-5
EPA 1664B
JMS
1
PASI-C
SM 2540D
MJP
1
PASI-A
EPA 9040
KDF1
1
PASI-A
92375878005
SP-6
EPA 1664B
JMS
1
PASI-C
SM 2540D
MJP
1
PASI-A
EPA9040
KDF1
1
PASI-A
92375876006
SP-7
EPA 1664B
JMS
1
PASI-C
SM 2540D
MJP
1
PASI-A
EPA 9040
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC,
Page 3 of 13

aceAnalytrcal e
www.peooleb&wn
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92375878
Sample: SP-1
Parameters
Lab ID: 92375878001 Collected: 03/06/18 12:00
Results Units Report Limit DF
Received: 03/07/18 10:56 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
46.9 mglL
5.0 1
03/20/18 04:36
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
1000 mg/L
100 1
03/10/18 09:27
9040 pH
Analytical Method: EPA 9040
pH
7.3 Sid. Units
0.10 1
03/08/18 02:11 H6
Sample: SP-3
Lab ID: 92375878002 Collected: 03106M8 12:15
Received: 03/07/18 10:56 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
9.0 mglL
5.0 1
03/20/18 04:37
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
606 mg/L
71.4 1
03/10/18 09:27
9040 pH
Analytical Method: EPA 9040
pH
7.1 Std. Units
0.10 1
03/08/18 02:11 H6
Sample: SP-4
Lab ID: 92375878003 Collected: 03/06/18 12:30
Received:
03/07/18 10:56 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
11.4 mglL
5.0
1
03/20/18 04:37
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
652 mg1L
62.5
1
03/10/18 09:27
9040 pH
Analytical Method: EPA 9040
pH
7.3 Sid. Units
0.10
1
03/08/18 02:11 H6
Sample: SP-5
Lab ID: 92375878004 Collected: 03/06/18 12:45
Received:
03/07/18 10:56 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
25.8 mglL
5.0
1
03/20/18 04:37
Date: 03/20/2018 01:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 13

aceAnaljftal o
%"'Pewleft nT
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92375878
Sample: SP-5 Lab ID: 92375878004 Collected: 03/06/18 12:45 Received: 03/07/18 10:56 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 1170 mg/L 71.4 1 03/10/18 09:27
9040 pH Analytical Method: EPA 9040
PH 7.1 Std, Units 0.10 1 03/08/18 02:11 H6
Sample: SP-6
Parameters
Lab ID; 92375878005 Collected: 03/06/18 13:00
Results Units Report Limit OF
Received: 03/07/18 10:56 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
15.9 mg/L
5.0 1
03/20/18 04:37
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
86.0 mg/L
12.5 1
03/10/18 09:27
9040 pH
Analytical Method: EPA 9040
PH
6.3 Std. Units
0.10 1
03/08/18 02:11 H6
Sample: SP-7
Lab ID: 92375878006 Collected: 03/0611813:15
Received: 03/07/18 10:56 Matrix: Water
Parameters
Results Units
Report Limit OF
Prepared Analyzed CAS No. Qua[
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
36.5 mg/L
5.0 1
03/20/18 04:38
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
310 mg/L
16.7 1
03/10/18 09:28
9040 pH
Analytical Method: EPA 9040
PH
6.8 Std. Units
0.10 1
03/08/18 02:11 H6
Date: 03/20/2018 01:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 13

aceAnalytical "
warmpecews.com
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 9237,9878
QC Batch: 402639 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92375878001, 92375878002, 92375878003, 92375878004, 92375878005, 92375878006
METHOD BLANK: 2233303 Matrix: Water
Associated Lab Samples: 92375878001, 92375878002, 92375878003, 92375878004, 92375878005, 9237587B00fi
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L ND 5.0 03/20/18 04:33
LABORATORY CONTROL SAMPLE: 2233304
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 40 37.2 93 78-114
MATRIX SPIKE SAMPLE: 2233305
92375928004 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mglL NO 40 38.5 95 78-114
Results presented on this page are In the units indicated by the "Units" column except where an altamale unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/20/2018 01:13 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 13

aceAna1jfta1e
wwwpeoela6sc+om
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvllle. NC Z8078
[phone]
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92375878
QC Batch: 401457 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92375878001, 92375878002, 92375878003, 92375878004, 92375878005, 92375878006
METHOD BLANK: 2226959 Matrix: Water
Associated Lab Samples: 92375878001, 92375878002, 92375878003, 92375878004, 92375878005, 92375878006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 03/10/18 09:24
LABORATORY CONTROL SAMPLE: 2226960
Spike LCS
Parameter Units Cone. Result
Total Suspended Solids mg/L 250 232
SAMPLE DUPLICATE: 2226961
92375821007 Dup
Parameter Units Result Result
Total Suspended Solids mglL 10.2 15.6
SAMPLE DUPLICATE: 2226962
92375856001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L NO NO
LCS % Rae
% Rec Limits Qualifiers
93 90-110
RPD Qualifiers
42 D6
RPD Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/20/2018 01:13 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 13

acoAnaljdical o
WWW'Dawabs.com
Pace Analytical Services, LLC
9B00 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92375878
QC Batch: 401077 Analysis Method: EPA9040
QC Batch Method: EPA9040 Analysis Description: 9040 pH
Associated Lab Samples: 92375878001, 92375878002, 92375878003, 92375878004, 92375878005, 92375878006
SAMPLE DUPLICATE: 2224580
92376862001 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 7.6 7.6 0 H6
SAMPLE DUPLICATE: 2224581 T
92376002001 Dup
Parameter Units Result Result RPD Qualifiers
pH Sld. Units 7.2 7.0 2 H6
Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/20/2018 01:13 PM without the written consent of Pace Analytical Services, Lt-C. Page 8 of 13

aceAnalytical o
mrNrpacefe M=n
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 20078
[phone]
QUALIFIERS
Project: SNI-Charlotte, NC
Pace Project No.: 92375878
DEFINITIONS
OF - Dilution Factor, If reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyle is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether,
A separate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte Is a combined concentration.
Pace Analytical Is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
06 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis Initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 03/20/2018 01:13 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

aceAnalytical
www.pacelaba.com
Pace Analytical Services, LLC
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SNI-Charlotte, NC
Pace Project No.: 92376878
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92375878001
SIP-1
EPA1664B
402639
92375878002
SP-3
EPAi664B
402639
92375878003
SP-4
EPA1664B
402639
92375878004
SP-5
EPA1664B
402639
92375878005
SP-6
EPA 1664B
402639
92375878006
SP-7
EPA 1664E
402639
92375878001
S P-1
SM 2540D
401457
92375878002
SP-3
SM 2540D
401457
92376876003
SP-4
SM 2540D
401457
92375878004
SP-5
SM 25400
401457
9237587800E
SIP-6
SM 2540D
401457
92375878006
SP-7
SM 2540D
401457
92375878001
S P-1
EPA 9040
401077
92375878002
SP-3
EPA 9040
401077
92375878003
SP-4
EPA 9040
401077
92375878004
SP-5
EPA 9040
401077
92375878005
SP-6
EPA 9040
401077
92375878006
SP-7
EPA 9040
401077
Date: 03/20/2018 01:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 10 of 13

Document Name:
Document Revlsed; February 7, 2018
aceAnal bifY
Sample Condition Upon Recel t SCUR)
Page t of 2
Document No.-.
Issuing Authority:
F-CAR•CS-033•Rev,06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ -Greenwood ❑ Huntersvlil Raleigh[] Mechanicsville❑
Client Name:
Project fi
Courier. Fe II` UPS LISPS Client
❑ Commercial ace ❑Qther:
Custody Seel Present? ❑Yes No Seals Intact? Dyes �No
Packing Material: ❑9ubble Wrap ubble Bags ❑None ❑ father
Thermometer:
T
❑ IR Gun IO: 9 6 Type of Its: Wet ❑Blue
Cooler Temp {'C]: Z ' Correction Factor: Add/Subtract ('C) p,1
Coder Temp Corrected i'C):
USDA Regulated Sol(( /A, water sample]
Old samples original a quara'ritlne tone within the United States: CA, NY, or SC {check maps)?
myes
r71, +- a
MQ 92375878
��!'�ll lflal`Il 11�11I`�'11I•_.
9237 IB7 � t,
Date/InitialsPam" Exemining Contents:
Blologlcel a Frozen?
❑Yes o ❑N/A
❑None
Temp should be above freezing to 6'C
(3Samples out of temp criteria. Samples an Ice, Cooling process
his begun
Did iimpies originate from a foreign source (Inter tonally,
ineludlne Hawall end Puarta Riml? f1Yas Nn
Comments 0lscre a
Chain of Custody Present?
171ho
N A
1.
Sam les Arrived within Hold Time?
No
N A
2.
Short Hold Time Ane Is 42 hr.)?
Yes
o
N A
3.
Rush Turn Around TimeRequested?
OVel
N/A
4.
Sufficlent Volume?
Mof
No
N A
5.
Correct Contalners Used?
-Pace Containers Used?
a
ei
(:)No
No
[]N/A
ONLA
6.
Containers Intact?
of
Na
N A
7.
Dissolved analysis: Samples Field Flltered 7
Yes
/A
8.
Sampte Labels Match COC?
-includes Date/Tlme iD Anal is Matrix:
QN/A
9. N,, G^ S j 0 C ,
Heads are In VOA Vials sS•6mm
Yes
Ohlo
A
10.
11.
Trip Blank Present? (]Yes N/A
Trip Blank Custod Seals Present? 0yes Cho A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers;
CLIENT NOTIFICATION/RESOLUTION
Person contacted; Date/rime:
Field Data Required? ❑Yes ❑No
Project Manager SCURF Review: r. Date: o
Project Manager SRF Review: a 1Ur�� Date:
.
�' Page 11of13

Document Name;
Document Revised: February 7, 2018
IceArfaly dl
Sam le Condition Upon Recel t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS•033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box If pH and/or dechlorination Is Project #
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLHS
"Bottom half of box Is to list number of bottle
WO# �.92375878 i
PM NM' Ouse-"'IDate 1 03121/itf
CLIENT:'82 SCHNEIDER
�
u�oaa��■��ao��i�i����an�
��■i���ii����iii�ii���
pH Adjustment Log for Preserved
Samples
Sample 10
Type of Preservalhre
pH upon receipt
Date preservation adjusted
Time praurvation
adjusted
Amount of Preservatlw
added
Lot p
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certlflcatlon Office (i.e.
Out of hold, Incorrect preservative, out of temp, Incorrect containers.
Page 12 of 13

V
CHAIN -OF -CUSTODY 1 Analytical Request Document o
The Chain- -Custody is a LEGAL DOCUMENT. AI{ relevant fields must he c"npieted accurately.
fi! 1Li! m
rn
__ .,--.-----
Page: of d
Section A Section B Section C
2192462
Required Client lt*wmation. Required Prpjoct Inlormabon_ Invoice lniormaltan'.
Report To:
A
Copy To:
Company Name:
REGULATORY AGENCY
F NPDES V GROUNDWATER r- DRINKING WATER
F UST r RCRA OTHER
JC
Purdwse Order No.:
Pac-a�
Fax:
Project Name:
P 7O�
Site Location
STA TE.
Q
Ale: -
Reques Mm V=eJTAT:
Project Number:
�'O° P'*ft s:
Requested
Analysis
Filtered
(YIN)
Suction D Matrix Codas
Requ:od(�cm lnlormalnn MAMlx r cooE
-
COLLECTED
Preservatives
=
Drinking Weffir OW
$
U
Water WT
Wa�teWater WW
q,
U
SC01s'03ISE
rE
ENDCRAS
z
sowsod SL
J
}
SAMPLE ID wX
y
er
>
(A-7- 0-91,-) Air AR
W
LU
C
Z
m
o
Sample IDs MUST BE UNIQUE Issue TS
O
Z
V
Other OT
X
W
0
n
2
p
m
U
j
m
a
a
U.
U.
a
N
z
c�
m
m
in
C
m
/
DATE
TIME
DATE
TIME
ED
a
M
M
x
2
z
z
z
O
.y
Ir
Pace Project Nol Lab I.D.
•
_
Z��
"i ��}1
�1�I
3
/
is
4
✓/�
5:1
1.
00
s
�,�'�.►� �' y
33
a
a
\
9
1�
10
1
`
12
ADDmt�NAL COMMENTS
RELING
DATE ,
TWE
ACCEPT BY I AFFRIA
p TE
SAMPLE comul 1ONs
/TJntE
SAWLERNAME AND .SIGNATURE
ORIGINAL
v
c �
m
m
PRINT Narno o! SAMPLER:
r
i
}
m
SIGNATURE a[ SAMPLER DATE signed /r
� V
—
j P
m
n}
E
'IrpanmY Note: By stgn" e,s (con you am accepting Pace's NET 30 day pay mmd lama ww &We"to Late Agee d 15% per month to" ir$reioes rot paitl w0m 30 flays, - F-AU-0-O20rev.07. 1 s-May-2007

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCGO80000 SAMPLES COLLECTED DURING CALENDAR YEAR: 2b ! 1
CERTIFICATE OF COVERAGE NO. NCG08 LD 59) �J (Tbis monitoring report is due at the Division no later than 30 days from
I �the date the facility receives th sam ling results from the laboratory.)
FACILITY NAME Y t U 1( * i(A � [) V1 1 10a ff l.. COUNTY
PERSON COLLECTING SAMPLES PHONE NO. O
CERTIFIED LABORATORY_]! (�l Lab # 63q Z
Lab # PLEASE SIGN ON THE REVERSE 4
Part A: Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no
(if yes, report your analytical results in the table immediately below)
Oatfall
No.
Date �� _:
Sample Collected;
mold
0053fl .::
00:400 �'"
OOSS6 r
� :'.:. . _ —
Total Suspended Sohds;
# ::
4 pH;"� " • :
.. Standardranits _
Oil,ancl Grease, r �`NewMotot
ifiVE
Otl Usage;
A nualavera e"al%ma�
Benchmark
too A.
� `` ;AWith .eAa: _s9:0
30M
-
1
21.-7
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Part B: Oillwater Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
Outfall
No:
-.Dates
Sample�Collected,
s 00556 - N `
_ _ r: O053I!
0040(1 :
Oilland�Grease,a=F_11'zW.Y.TolESuspende'd
its,
H, F 1SUNRZIs -
�Permit Limit
Z 1 I -7
'7
1 -7
21 1
.,
STORM EVENT CHARACTERISTICS:
Date I 1 _1 1!first event sampled) nn �nn
Total Event Precipitation (inches):
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
RCt,,FI V EE)
JAN 2 9-2018
DWR SECTION
INFORMATION PROCESSING UNI.
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
S WU-250-102107
Page 1 of 2

"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
Permittee
(Date)
S WU-250-102107
Page 2 of 2

aceAnalytical
www.peoebbaoarn
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersvllle, NC 28078
[phone]
January 08, 2018
Mr. Michael DeBraske
Schneider National, Inc.
PO Box 2545
Green Bay, WI 543062545
RE: Project: SNI-Charlotte, NC
Pace Project No.: 92367997
Dear Mr. DeBraske:
Enclosed are the analytical results for sample(s) received by the laboratory on December 21, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Ceryssa Berg, Schneider National
Mr. Michael DeBraske, GEI Consultants, Inc.
s
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC,
Page 1 of 14

aceAnalytical e
wmpeoelabmm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
Project: SNI-Charlotte, NC
Pace Project No.: 92367997
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersvllle, NC 28078
LouisianalNELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certiflcatlon IDs
2225 Riverside Drive, Asheville, NC 28804
Florids/NELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Vrginia/VEIAP Certification M 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
V rginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, I.I.C. Page 2 of 14

aceAnalytical e
�rwM:peoele6s.corn
Pace Analytical Services, LLC
9800 Klncey Ave. Sulte 100
Huntersville, NC U078
[phone]
SAMPLE ANALYTE COUNT
Project: SNI-Charlotte, NC
Pace Project No.: 92367997
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92367997001
SP-1
EPA 1664B
JMS
1
PASI-C
SM 2540D
SLB
1
PASi-A
EPA 9040
ECH
1
PASI-A
92357997002
SP-3
EPA 1664B
JMS
1
PASI-C
SM 2540D
SLB
1
PASI-A
EPA 9040
ECH
1
PASI-A
92367997003
SP-4
EPA 1664B
JMS
1
PASI-C
SM 2540D
SLB
1
PASI-A
EPA9040
ECH
1
PASI-A
92367997004
SP-5
EPA1664B
JMS
1
PASI-C
SM 2540D
SLB
1
PASI-A
EPA 9040
ECH
1
PASI-A
92367997005
SP-7
EPA1664B
JMS
1
PASI-C
SM 2540D
SLB
1
PASI-A
EPA 9040
ECH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 14

aceAnalytical "
wwwpeoews.mn
Pace Analytical Services, LLC
9800 KlnceyAve, Suite 100
Huntersville, NC 28078
(704 )875-9092
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92367997
Sample: SP-1
Parameters
Lab ID: 923e7997001 Collected: 12/20/17 10:30
Results Units Report Limit DF
Received: 12/21/17 14:32 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
40.8 mg/L
5.0 1
01/08/18 04:13
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
252 mg1L
12.5 1
12/27/17 08:54
9040 pH
Analytical Method: EPA 9040
pH
7.3 Std. Units
0.10 1
12/22/17 15:00 H6
Sample: SP-3
Lab ID: 92367997002 Collected: 12/20/17 10:45
Received: 12/21/17 14:32 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
13.1 mg1L
5.0 1
01/08/18 04:14
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
457 mg/L
25.0 1
12/27/17 08:54
9040 pH
Analytical Method: EPA 9040
pH
7.2 Std. Units
0.10 1
12/22/17 15:00 H6
Sample: SP-4
Lab ID: 92367997003 Collected: 12/20/17 11:00
Received:
12/21/17 14:32 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
10.3 mg/L
5.0
1
01/08/18 04:14
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
290 mg/L
31.2
1
12/27/17 08:54
9040 pH
Analytical Method: EPA9040
pH
7.3 Std. Units
0.10
1
12/22/17 15:00 H6
Sample: SP-5
Lab lD: 923e7997004 Collected: 12/20/17 11:15
Received:
12/21/17 14:32 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
9.1 mg1L
5.0
1
01/08/18 04:14
Date: 01/08/2018 02:07 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC,
Page 4 of 14

aceAnalytical.
wwwpecelaftwn
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92367997
Sample: SP-5 Lab ID: 92367997004 Collected: 12/20/17 11:15 Received: 12/21/17 14:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 25400
Total Suspended Solids 175 mg/L 25.0 1 12/27/17 09:21
9040 pH Analytical Method: EPA 9040
pH 6.9 Std, Units 0.10 1 12/22/17 15:00 H6
Sample: SP-7
Parameters
Lab ID: 92367997005 Collected: 12/20/17 11:30
Results Units Report Limit DF
Received: 12/21/17 14:32 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
21.7 mg/L
5.0 1
01/08/18 04:15
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
305 mg/L
19.2 1
12/27/17 09:21
9040 pH
Analytical Method: EPA 9040
pH
7.2 Std. Units
0.10 1
12/22/17 15:00 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 01/08/2018 02:07 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14

aceAnalytical e
ttnvtvpaoWabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92367997
QC Batch: 393437 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92367997001, 92367997002, 92367997003, 92367997004, 92367997005
METHOD BLANK: 2181380 Matrix: Water
Associated Lab Samples: 92367997001, 92367997002, 92367997003, 92367997004, 92367997005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mglL ND 5.0 01/08/18 04:12
LABORATORY CONTROL SAMPLE: 2181381
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 40 36.9 92 78-114
MATRIX SPIKE SAMPLE:
2181382
92367826004
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mglL
ND
40
39.8
96
78-114
MATRIX SPIKE SAMPLE:
2181383
92368224001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mglL
ND
40
37.3
92
78-114
MATRIX SPIKE SAMPLE:
2181384
92368612002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mglL
ND
40
37.0
92
78-114
Results presented on this papa are In the units indicated by the "Units" column except where an aRemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2018 02:07 PM without the written consent of Pace Analytical Services, LLC, Page 6 of 14

aceAnalylfical e
wwwpeC wacom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92367997
QC Batch: 392427
Analysis Method: SM 2540D
QC Batch Method: SM 2540D
Analysis Description: 25400 Total Suspended Solids
Associated Lab Samples: 92367997001, 92367997002,
92367997003
METHOD BLANK: 2176880
Matrix: Water
Associated Lab Samples: 92367997001, 92367997002, 92367997003
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Suspended Solids
mglL
ND 2.5 12/27/17 08:50
LABORATORY CONTROL SAMPLE:
2176881
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 250 100 90-110
SAMPLE DUPLICATE: 2176882
92367956001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mglL
28.4 29.0 2
SAMPLE DUPLICATE: 2176883
92367981005 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mglL
16.4 17.6 7 D6
Results presented on this page are In the units Indicated by the 'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 01/08/2018 02:07 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14

aceftlytical*
wwwpacelab&MM
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huntersvllle, NC 28078
(704)B75.9092
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92367997
QC Batch: 392428 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92367997004, 92367997005
METHOD BLANK: 2176884 Matrix: Water
Associated Lab Samples: 92367997004, 92367997005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 12/27/17 09:21
LABORATORY CONTROL SAMPLE:
2176885
Spike LCS LCS
% Rec.
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Suspended Solids
mglL
250 240 96
90-110
SAMPLE DUPLICATE: 2176886
92367997004 Dup
Parameter
Units
Result Result RPD
Qualifiers
Total Suspended Solids
mglL
175 170
3
SAMPLE DUPLICATE: 2176887
92368099003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 20.2 22.0 9 D6
Results presented on this Pepe are in the units Indicated by the units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2018 02:07 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 14

aceAnalytical
wwwpecefat amm
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92367997
QC Batch: 392108 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Descriptlon: 9040 pH
Associated Lab Samples: 92367997001, 92367997002, 92367997003, 92367997004, 92367997005
SAMPLE DUPLICATE: 2175511
92367960001 Dup
Parameter Units Result Result RPD
PH
SAMPLE DUPLICATE: 2175512
Parameter
PH
Std. Units 7.0 7.0
92367997004 Dup
Units Result Result
Std. Units 6.9 6.9
Qualiflers
1 H6
RPD Qualifiers
0 H6
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the 'Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/08/2018 02:07 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 14

Pace Analytical Services, LLC
6 98001(inceyAve. Suite 100
aceMalXical Huntersvllle, NC 28078
www.pscefaftwn [phone]
QUALIFIERS
Project: SNI-Charlotte, NC
Pace Project No.: 92367997
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantltation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazlne decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/08/2018 02:07 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

aceAnalytical e
www,PODOWs.Com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SNI-Charlotte, NC
Pace Project No.: 92367997
Lab ID
Sample ID
QC Batch Method
Analytical
QC Batch Analytical Method Batch
92361997001
SP-1
EPA1664B
393437
92367997002
SP-3
EPA 1664B
393437
92367997003
SP-4
EPA 1664E
393437
92367997004
SP-5
EPA1664B
393437
92367997005
SP-7
EPA 1664E
393437
92367997001
SP-1
SM 2540D
392427
92367997002
SP-3
SM 2540D
392427
92367997003
SP-4
SM 2540D
392427
92367997004
SP-5
SM 2540D
392428
92367997005
SP-7
SM 2540D
392428
92367997001
SP-1
EPA 9040
392108
92361997002
SP-3
EPA 9040
392108
92367997003
SP-4
EPA 9040
392108
92367997004
SP-5
EPA 9040
392108
92361997005
SP-7
EPA 9040
392108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 01/08/2018 02:07 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 14

Document Name:
Document Revised: August 4, 2017
ZC1eAna1jNca1'
Sam le Condition U on Recei t SCUR
Pa e 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.04
Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvill Ralelgh❑ Mechanicsville❑
Client Name: Protect q: � WO#i : 92367997
c-In�c,t vw
Courier: Fe []UPS U5P5 Client it
il❑ Commercial ace Other: 8
Custody Seal Present? Dyes Na Seals Intact? Dyes
Dale/Irtltlals Person Examining Contents:
Packing Material: [-]Bubble Wrap EjBu b Bags ❑None ❑ Other Biological Tl�oe Frozen?
Thermometer: ❑Yes ;2% ❑N/A
❑ IN Gun ID: T wet []Blue []None
ype Ice:
Correction Factor: Cooler Temp Corrected (*Cl: • O Temp should be above freezing to VC
❑Samples out of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Soil NIA, water sample)
Did samples origl 4112 uarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Intern finally,
Myes includinc Hawaii and Puerto Rico)? ❑Yes [26
Comments/Dlscre an :
Chain of Custody Present?
a
Na
MNA
1.
Sam le$ Arrived within Hold Time?
QNo
N A
2.
Short Hold Time Analysis c72 hr.
Yes
N
N/A
3.
Rush Turn Around Time Requested?
Yes
o
N/A
4.
Sufficient Volume?
Yes
No
N/A
5.
Correct Containers Used?
-Pace Containers Used?r2KanlrNo
❑No
(:]N/A
N A
6,
Containers Intact?
OYU
nNo
N A
7.
Dissolved analysis: Samples Field Filtered?
a
ONJA
8.
Sample Labels Match COC?
-Includes Dale ime/iO/Anal sls Matrix:
Ityes
[]No
❑N/A
4.
Heads ace in VOA Vials >5.6mm ?
Yes
EJNo
/A-"�
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[Ives'P950
Yes
L3NO
❑N/A
QN7A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted: Date/Time:
Comments/Sample Discrepancy:
Field Dole Required? ❑Yes ❑No
Lot ID of split containers,
Project Manager SCURF Review: y'
Date: t
Project Manager SRF Review:
Date: Z[ Z
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le.
Out of hold, Incorrect preservative, out of temp, incorrect containers)
Page 12 of 14

W
0
3
a
v
K
n
9
n
a
z
0
0
w
"o
A
x
r
rL.
O
s
M
".3
R
A
ro
K
r►
�
O
ao
r,
R
ro
10
ro
.4
a
w
m
s
m
N
s
R
W �
R A
m
C
C
ir
iiri-
rrr
:,•
■■■
■■■■■
■
■■
■
i
rarr
a
it
r
rr
r
. „ ....
rri-
rriirri-
rrrr
- C-�* N-Ai=.
rrrr
rrrrarra
r
ri
UPS
rr
r
r
r
ir
■■■■■■■■■■■■
. -
■■■■■■■■■■■■
c .
C
m
a
m
3
Q.
3
S
fD
m
n
n
n
m
to
3
W
w
b
•
A
Sr
A
M,
3
m
x
S
CD
O
Cr
O
x
7
a
0
Q
eo
A
O
m
O
7
A

Q
Section A
Reputed Clierd
section B
Required Project h4wamdpn:
CHAIN -OF -CUSTODY I Analytical Request Document
The Chalm-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
sacdon C
hreaice 64ormAbow
Page : 1 Of 1
Comparrf SclrueKw Nat"W
Repw1 To: r
2420 Starga Road
Copy To:
Company Nana:
Charlode. NC 2a269
Address:
- -RamuL&I ".'I-
EmaB: �-.abm L_hf'i ": G �Y.r+i �sr . r _
Purchase Order r ..
Pam Quate:
Phone: [phone] Fax
Prq- Name: SNI-Chi. NC
pace ProFd Ub-g- rKole
-
Requested Due DWA:
propo e:
Pare Profit a: 2631-1
NC
MUM coca:
°
4
°
COLLECTED
*
Preservativesy.
a:
}
WY. Aa
3
~
U
1Nay WaMf
=
Z
e�.� crYe!
S. p
SAMPLE ID -" a
tl
a
START
EIM
'tr
l-
$
y
One Character per box. WO. WP
ry
omw Or
Sunpt ift aarst he rarigrre Taw. is
2
r•'
e
C
~
47r
4
a
n
7
cc4
i
M
D
O
Q
C
fA
f
=
a
-
DATE
ia�
DATE
TIME
x
z
2
i7
rs
s
L �/✓�t" r i
1
SP-1 Qr
W,
�:r
fr !'L
jt}3�
x
x
x
wT
x
x
x
�(yy
L—
3'L
sP-3 7:
wT
/O
0 5S
x
x
x
UI.
r`
�
�
l0�
%I
�
. 4
SPr
WT
I
I
t
I
t
t
x
X
Ix
S_
SP-5 ,
wT
J/
!�'�
x
x
x
4 •_72'i
1
_ 'AfmET10NAl C0�CB -
BY7.
oATE
TtlF>=.
A9CEF By l&-MATWN —
DATE ` .
' T11fE
e, T $AMPLE coom om '-
..a"
`�
z
S
0,h
21-17
0
3 •
N
Ll
c
$
a
PRDIT Marra of 8A1tlPlEr � has
/ c/�
m
ie i=
g $
,
d i=
SIGNATI7RE ar L• -
DATE Sigra • ,
P
rn
r

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCGO80000 SAMPLES COLLECTED DURING CALENDAR YEAR: _!]
CERTIFICATE OF COVERAGE NO. NCGOS_ n O t7(-N (This monitoring report is due at the Division no later than 30 days from
( the t the facility receives the samplingresults from the laboratory.)
FACILITY NAME C " V �. j �� COUNTY
PERSON COLLECTING SAMPLES ✓✓✓ PHONE NO. (_q70) 5q'Z -5 47,
CERTIFIED LABORATORY PAf t h u ttr h F Lab # 5547
I.ab # PLEASE SIGN ON THE REVERSE 4 R C C E I` E D
Part A: Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no
(if yes, report your analytical results in the table immediately below)
JUN 21 2017
CENTRAL FILES
R SECTION
Outran
No.
Date
Sample Collected;.
moJdd/ r
=W30•_"'
00M. -
-00556
Total Suspended Solids; '
-� -pH,-,
Standard units
Oil and'Giease, " .
MWL
New,Motor O�'1:Usage, -
Annual average mo
Benchmark
.
100 . '
-Within 6:0.=9.0
S29
IOU
7-
Co
Eg!��j
— 5
20
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
Outran
No.
Date
Sample Collected'.
mold
..00S56 " .
- - - ;00530
Oil'mW..Grease,
Total�Su inded'Solids;
y
- - ;PH,
Stanilird units.
PeridtLimiit
_
`.'_ 30
STORM EVENT CHARACTERISTICS:
Date (first event sampled)
Total Event Precipitation (inches): -
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh. North Carolina 27699-1617
SWU-250-102107
Page 1 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCG080000 SAMPLES COLLECTED DURING CALENDAR YEAR: 7011—
CERTIFICATE OF COVERAGE NO. NCG08 D D D D (This monitoring report is due at the Division no later than 30 days from
f the date the facility receives the am ling results from the laboratory.)
FACILITY NAM>w ` COUNTY ( g 13lrC l 3r�
PERSON COLLECTING SAMPLES PHONE NO. ( Zhu) )QL- 9 $
CERTIFIED LABORATORY Lab #f) 3"2
Lab # PLEASE SIGN ON THE REVERSE
Part A. Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _nn
(if yes, report your analytical results in the table immediately below)
Outfall
No.
Date
Sample Collected,'
mold r
00530
D0400
- - "00556' ; `
,
'TotW Suspended Sollds,.
- 'pH, -
- . Standard.imits
Uilaiid:q ea
."New-Moton'00'Usage,
..Annual avers al/mo'
Benchmark
-
i(10.
- .--Witt"
30r-r.--
S
1
5
Notes If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Part B: Oilfwater Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
Otttfall
No.
Date
Sample Collected,
mo/ rM91L
44556',
-00530; 1:�
Ofl aM'Grease,
i
-ToW S rd:So-lids;, 7.
Standard units
Permit Limit
-
30-=
- I00
&0 - 9.0 -
STORM EVENT CHARACTERISTICS:
Date (llrst event sampled)
Total Event Precipitation (inches): _
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SWU-250- l 02107
Page 1 of 2

CeAnalytiical"
WWW4 cubb&COM
June 06, 2017
Mr. Michael DeBraske
Schneider National, Inc.
PO Box 2545
Green Bay, WI 543062545
RE: Project: SNI-Charlotte, NC
Pace Project No.: 92341793
Pass Analytical Services, LLC
9800 Kincey Ave, Sulle 100
Huntersville, NC 28076
[phone]
Dear Mr. DeBraske:
Enclosed are'the analytical results for sample(s) received by the laboratory on May 24, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions conceming this.report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
nicole.gasio [e-mail]
[phone]
Project Manager
Enclosures
cc: Caryssa Berg, Schneider National
Mr, Michael DeBraske, GEI Consultants, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 14

Pace Analytical Services, LLC
rGI,
Y�
8800KinteyAlle, Suite100
Huntaraville, NC 26478
(�5aceAlical'
•t swm
[phone]
CERTIFICATIONS
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
Charlotte Certification IDS
98DO Kincey Ave. Ste 100, Hunlersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
FloridalNELAP Certification #: E87627
North Carolina Field Services Certification M 5342
Kentucky UST Certification M 64
North Carolina Wastewater Certification #: 12
VirginlalVELAP Certification #: 460221
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M•NC030
VlrginlaIVELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace AnsWal services, LLC,
Page 2 of 14

CeAnaljftal
eww,papMep><com
SAMPLE ANALYTE COUNT
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersvitle, NC 28078
{704}075-9092
Analyses
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92341793001
SP-1
EPA 1664B
JMS
1
PASI-C
SM 2540D
NAL
1
PASI-A
EPA 9040
KDF1
1
PASI-A
92341793002
SP-2
EPA 16646
JMS
1
PASI-C
SM 2540D
CJH1
1
PASI-A
EPA9040
KDF1
1
PASI-A
92341793003
SP-3
EPA 1664E
JMS
1
PASI-C
SM 2540D
CJH1
1
PASI-A
EPA9040
KDF1
1
PASI-A
02341793004
SP-4
EPA 1664E
JMS
1
PASI-C
SM 2540D
CJH1
1
PASI-A
EPA9040
KDF1
1
PASI-A
92341793005
SP-5
EPA 1864E
JMS
1
PASI-C
SM 25400
CJH1
1
PASI-A
EPA9040
KDF1
1
PASI-A
92341793006
SP-6
EPA 16648
JMS
1
PASI-C
SM 25400
CJH1
1
PASI-A
EPA9040
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C.
Page 3 of 14

aceAnalytica!
wsw.psos(abs oom
ANALYTICAL, RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SPA
Parameters
Lab ID: 92341793001 Collected: 05/23117 13:45
Results Units Report Limit OF
Received: 05/24/17 13:49 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grosse
Analytical Method: EPA 1664B
Oil and Grease
5.2 mglL
5.0 1
06106/17 07:06
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
108 mglL
16.2 1
05/26/17 17:27
9040 pH
Analytical Method: EPA 9040
pH
7.1 Sid. Units
0,10 1
05126/17 00:23 H6
Sample. SP-2
Lab ID: 92341793002 Collected: 05/23/17 t3:30
Received: 05/24/17 13:49 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg1L
5.0 1
0610el17 07:07
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
55.2 mglL
10.0 1
05/27117 07:44
9040 pH
Analytical Method: EPA 9040
pH
8.2 Sid. Units
0.10 1
05/26117 00:23 1-18
Sample: SP-3
Lab ID: 92341793003 Collected: 05/23117 13:10
Received: 05124M7 13:49 Matrix: Water
Parameters
Results Units
Report Limit OF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 16649
Oil and Grease
NO mg/L
5.0 1
06/06/17 07:08
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
280 mg1L
16.7 1
0527/17 07:44
9040 pH
Analytical Method, EPA 9040
pH
7A Sid. Units
0.10 1
0526117 00:23 H6
Sample: SP-4 Lab ID: 92341793004 Collected: 05123117 12A5 Received: 05/24117 13:49 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
Date: 06/062017 02:49 PM
Analytical Method: EPA 1664B
NO mg1L 5.0 1 06/06/17 07:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in NO.
without the wntien consent of Pace Analytical Services, I.L.C.
Page 4 of 14

aceAnalAcal
mrw.paoNaumn
ANALYTICAL RESULTS
Project: SNI-Charbtte, NC
Pace Project No.: 92341793
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Kuritersvll[e, NC 28078
[phone]
Sample: SP-4 Lab ID: 92341793004 Collected: 05/23/17 12:45 Received: 05/24/17 13:49 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 1060 mg1L 50.0 1 05/27/17 07A5
9040 pH Analytical Method: EPA9040
PH 7.6 Std. Units 0.10 1 05126M700:23 H6
Sample: SP-5 Lab ID: 92341793005 Collected: 05123117 12:10 Received: 05/24/17 13749 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qua[
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg1L
5.0 1
G6106117 07:08
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
386 mg1L
50.0 1
05/27117 07:45
9040 pH
Analytical Method: EPA 9040
PH
7.1 Sid, Units
0.10 1
05126/17 00:23 H6
Sample: SP-6
Lab ID: $2341793006 Collected: 05/23117 12;30
Received: 05/24/17 13:49 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg1L
5.0 1
06/06/17 07:09
25400 Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
204 mg1L
33.3 1
05127/17 07:46
9040 pH
Analytical Method: EPA 9040
pH
7.1 Sid. Units
0.10 1
05/26/17 00:23 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 06/0612017 02:49 PM without the written consent of Pace Analytical Services, I.I.C. Page 5 of 14

aceAnaly iol
www.pacefe6atttlm
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
4C Batch: 363491 Analyst Method: EPA 16640
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92341793001, 92341793002, 92341793003, 92341793004, 92341793005, 92341793006
METHOD BLANK: 2015170 Matrix: Water
Associated Leb Samples: 92341793001, 92341793002, 92341793003, 92341793004, 92341793005, 92341793006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L NO 5.0 06106l17 07:05
Pace Analytical Services, LLC
9800 Kincey Ave. Sulte 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2015171
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mg1L 40 36.5 96 76-114
MATRIX SPIKE SAMPLE: 2015172
92341793001 Spike MS MS % Rec
Parameter Units Result Cana. Result % Rec Limits Qualifiers
Oil and Grease mg1L 5.2 40 43.7 96 78.114
Results presented on trite paue are In the units indlestee by the "Units" column except where an alternate unit Is presented to the right CO the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 06/0612017 02:49 PM without the written consent o1 Pace Analytical Services, LLC. Page 6 of 14

Iac)eAnalXical(�'
www.panhbs.oam
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
OC Batch: 362513 Analysis Method: SM 2540D
OC Balch Method: SM 2640D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92341793001
METHOD BLANK: 2010010 Matrix: Water
Associated Lab Samples: 92341793001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 05/26/17 17:17
Pate Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvifle, NC 28078
(704)875-BD92
LABORATORY CONTROL SAMPLE:
2010011
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result °% Rec
Limits Qualifiers
Total Suspended Solids
mg1L
250 238 95
90.110
SAMPLE DUPLICATE: 2010012
92341670006 Dup
Parameter
Units
Result Result RPD
Qualifiers
Total Suspended Solids
mg/L
244 252
3
SAMPLE DUPLICATE: 2010013
92341754001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL ND NO
Results presented w this page are In the units indlcated by the 'units" column except when an alternate unit Is presented to the rot of Me result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 06/06/2017 02:49 PM without the written consent a1 Pace Analytical Services, LLC. Page 7 of 14

aceAnalytical
..+e-0eciall 0aoom
QUALITY CONTROL DATA
Project: SNI•Charlotte, NC
Pace Project No.: 92341793
QC Batch: 362555 Analysis Method: SM 2540D
QC Balch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92341793002, 92341793003, 92341793004, 92341793005, 9234179300E
METHOD BLANK: 2010145 Matrix: Water
Associated Lab Samples: 92341793002, 92341793D03, 92341793DD4, 92341793005, 92341793006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 05/27/17 07:42
LABORATORY CONTROL SAMPLE: 2010146
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlers011e. NC 28078
[phone]
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualities
Total Suspended Solids
mg1L
250 240 96
90-110
SAMPLE DUPLICATE: 2010147
92341644001 Dup
Parameter
Units
Result Result RPD
Qualifiers
Total Suspended Solids
mg1L
13.5 14.0
4
SAMPLE DUPLICATE: 2010148
92341819001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 5.6 6.2 10 D6
Results presented an this page are In the units Indicated by the "Units` column except where an ■rtemete unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2017 02:49 PM wilhaut the wrtttan consent of Pace Analytical Services, LLC.
Page 8 of 14

aceAnalyticale
wwwP0othbs corn
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
OC Balch: 362325 Analysis Method: EPA 9040
QC Balch Method: EPA 9040 Analysis Descriplion: 9040 pH
Associated Lab Samples7 92341793001, 92341793002, 92341793003, 92341793004, 92341793005, 92341793006
SAMPLE DUPLICATE: 2009194
92341588002 Dup
Parameter Units Result Result RPD Qualifiers
pH Slid. Units 3.5 3.5 0 H6
SAMPLE DUPLICATE: 2009195
92341638002 Dup
Parameter Units Result Result RPD Qualifiers
pH SW. Units 6.4 6.4 0 H6
Pace AneWtcal Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results praaanted on this page are In the units indicaud by the 'Units' Column except where an alternate unit Is presented to the right of We result.
REPORT OF LA130RATORY ANALYSIS
This report shall not be reproduced, except in full.
Dale: 06106/2017 02:49 PM without the written consent of Pace Analytical SerAces, LLC.
Page 9 of 14

CeAnalyt►C811
eM1►.paL1iIGS.CGm
QUALIFIERS
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
DEFINITION$
DF - Dilution Factor, If reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
POL - Practical Ouantitedon Limit.
RL - Reporting Limit.
Pace Analytical Services. LLC
9800 Klncey Ave. Suite 100
Hunloravillo, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyze is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
INC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4.5 Is recommended In SW846 Chapter 4 for the analysis of Acralein and Acrytonitrile by EPA
Method 6260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Olphenylamine using Method 8270. The result reported lot
each analyze is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
DB The precision between the sample and sample duplicate exceeded laboratory control limits.
HB Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall nol be reproduced. except In full.
Date: 06/06=17 02:49 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

CBAnalytkal
wrw.pa W0b3 eam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Paco Analytical Services, LLC
9800 Kinoay Ave. Suite 100
Huntersville. NC 28078
[phone]
Project SNI-Charlotte, NC
Pace Project No.: 92341793
Analytical
Lob ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92341793001
SP-1
EPA 1664B
363491
92341793002
SIP-2
EPA 1664B
363491
92341793003
SP-3
EPA 1664E
363491
92341793004
SP-4
EPA 1664B
363491
92341793005
SP-5
EPA 1664B
363491
92341793006
SP-6
EPA 1664B
363491
92341793001
Sp-1
SM 2540D
362513
92341793002
SP-2
SM 2540D
362555
92341793003
SIP-3
SM 2540D
362555
92341793004
SP-4
SM 2540D
362555
92341793005
SP-5
SM 2540D
362555
92341793006
SP-6
SM 2540D
362555
92341793001
SP-1
EPA 9040
362325
92341793002
SP-2
EPAS040
362325
92341793003
SP-3
EPA9040
362325
92341793004
SP-4
EPA 9040
362325
92341793005
SP-5
EPA 9040
362325
92341793006
SP-6
EPA 9040
362325
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced. except In full,
Date: 06ID612017 02:49 PM without the written consent of Pace Analytical Services, LLC, Page 11 of 14

Document Name:
Document Revised: Sept. 21, 2016
`
Sample Condition Upon Recei t SCUR
Page 1 of 2
Document No.:
issuirig Authority:
aCBAWl )Cal
F-CAR-CS-033•Rev.01
Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersvllle Raleigh❑ Mechanicsville[]
Client Name: ProjectWOE : 92341793
p:
�i .y17CliJ;?i. j J
Courier. F��d,Eir UPupS LISPS Client II I II' I II I � III III � � ill
❑ Commercial OPace ❑Other: 8234178'J 1
Custody Seal Present? ❑Yes No Sealt Intact? ❑Yes IgNo �II
Pete/Initials Person Examining Contents: ' , i' �
Packing Material: ❑Bubble Wrap Qeubble Bags []None [:]Other:Thermometer:
❑ IR Gun ID: Type o Ice: Wet ❑Blue ❑None +Simples on ice, cooling prgcess has begun
Correction Factor: Cooler temp Corrected i'Cj: Biological Tissue Frozen? ❑Yes ❑No []N/A
Temp should be above fre Ing to 6`C
USDA Regulat d Soil ( N/A, water sample)
Did samples O inate In a quarantine lone within the United States: CA, NY, or SC (check maps)?
Chain of Custody Present? QVkS ONG N A 1.
samples Arrived within Hold Time? yes ON.6 ON/A 2.
Short Hold Time Anal sia c72 hr.? Oyes C& ONIA 3.
Rush Turn Around Time Reauested? nyei Mi. i-7N/A 4.
Sutticlent Volume? EK&s ONO N/A 1 5.
Correct Containers Used? Yps [IN, ❑NIA 16.
Old samples orI5lnate from a foreign source
Including Hawaii and Puerto RICO)? ❑Yes
Containers Intact? E3tiej OING N A 7-
Samples Field Filtered? OYJNo N A S. Note if sediment Is
vlsibie in the dissolved container
Sample Labels Match COC7 m [:]No❑N1A 9. r� �+✓ l o" t ")'^" n I IZ 3 S
-includes Date/nme/10/Analvsls Matrix: t1J�
Heads ace In VOA Vials >5.6mm ? yes o NIA 10.
Trip Blank Present? ❑yeg (21410 ❑ A 11.
Trip Blank Custody Seals Present? OYes ONO NIA
CLIENt NOTIFICATION/RESOLUTION Field Date Required? []Yes ONO
Person Contacted:
Comments/Sample
Discrepancy:
Date/Time:
Project Manager scURr Review: _�17 Date:.
Project Manager SRF Review: Date: ; 25 IA -
Note: Whenever there is a discrepancy affecting North Carolina Compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect Containers)
Page 12 of 14

AA%td. CHAIN -Of -CUSTODY 1 Analytical Request Document
The Chan I-Custctiy is a LEGAL DOCUMENT. M relevant fella must be compWied aamat*.
Sordm A Secrke B Secrioa C
Requb" CBewlk/Qem.dor► RaqUhd prejou rdwrarrtiea: tsaiwica kdWON M'. Pace : Of
-
r Kwkrw ReporI To: Gen Gon
uda Roan To=
%w,28269
.Dom
Puram" Oiar N:
Pam Owra:7<13
Fa
Name: �.NC
PawPrgeaakan.oer. ricWe. .ma
erk5.__iJ.'.S+�c?
W.
Paw ProNs f. 2631.1
KC !
iJ
COLLECTED
PFCSavatW*S
�
� CODE
2
Qwmwww
VAMNwr W01
$
W
1
Z
SAMPLE ID
�
Owe ChUFUnW per OOT. YYe. wP
All
z
Samph tda aem be unique saw. TS
T,.,CTW
s3
Q
q0
a
~
a
,A
saw
a
:
i
$
i
rs
P3
fL
wr
7
f
x
x
z
oti t
SP-Y
wT
x
x
x
f-
SPA
ws
e D
x
x
x
ao a
a'
SPA
wr
x
x
x�
.�3.
vff
x
x
x
v's
SP-6
wT
1
x
x
x
aa(c
T
�
W
i
r ���j11�IIpNAI.40M7EBiA�t����A-
'Y.'."` _w.E •.....� - �,_� -:a«sc
F43
JWMASHED
BYlAFiiMlIAI
Y-.nra-ss
�
i>A�
�
�-
AOCFPiFD011/AFFR:ASIDN.
-- ���
{�
C:r-.
OATF
�,["i`4�,�.
�}: =
.�'�CLi�.�.-�
x �-Woa180011,r110Fta
..cam-. �.J3.r'�'�.' P..
.7
''t
7
1 .i
..V`JY
r'7 FfJ
f
PRIM: Mama a(
-
�
E
z
>�
Zt
i i
t : 9
SIGMA ,ATE 5 �+ y 3 — 7W
3 a
m
m
a

v
m
m
0
A
3
'v
i
a
a
M
c
a
m
=
a
m
C
M
o
w
n
3
m
ry
a
0
W
moa
n
V
ILro
N
1
�
t3i
• a
O.
N
w
A
A
4 d.
.a
O
7
�
D
C
y
n a
CL
a
yM
CIN
`n
■■■■■■■■■■■■
.■
■■.-■■■.■■
rr
RA
PA AVPAVPAV
SA
I Ar
PA AMR
m
NSA
WGVU-Wde-movthed Glass jar Unpreserved
M■■■■■■■■E■■
- • - - - •(Cl-)
MENMEMO
N�����
• - r IL
MENEM
MENEM
MENNEN
.
■■■■■■■■■■■■
'0AN
e* �
O �
3
S O
� 3
0 3 -w
c ti
O
X y
N
0
N
3
a
A
a
rt
to
AA

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCG080000 SAMPLES COLLECTED DURING CALENDAR YEAR: ~J
CERTIFICATE OF COVERAGE NO. NCG08 (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the camp ' resu is from the laboratory.)
FACILITY NAME COUNTY
PERSON COLLECTING SAMPLES 00 PHONE NO. (alb 1
CERTIFIED LABORATORY Lab # 5 &47
Lab # PLEASE SIGN ON THE REVERSE 4
Part A: Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no
(if yes, report your analytical results in the table immediately below)
Outfall
No.
Date
Sample Collected,.
mo/dd/ r
00530:
00400 . F n?.s%00556
..� y
- Total Suspended Solids;
-
' ' p ,
r.C_cStandardiunfts
, $Oil andFGrease,;
.PAnutisl OWUsag
a aUmo
Benchmark
- Within 6!0 -
5
7.
5
5 iw
I ZO
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier i or Tier 2 responses.
See General Permit text.
Part B: Oiltwater Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
Ontfall
No.
Date
Sample Collected,
ma/d T
t , 4 00556`�- - 0
00530
;004 0 A.
Oil aad{Grease,:
s ANI , . n-
TotalCSuspendedlSoliils, ._
*
r a..
r�g1;3,`
x -i
' Standard units 3
Permit Limit
6,%-- 9.0i .a
STORM EVENT CHARACTERISTICS:
Date (first event sampled)
Total EventPrecipitation (inches): _
Date All! 17 (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SWU-250-102107
Page 1 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCGO80000 SAMPLES COLLECTED DURING CALENDAR YEAR: 7()1-1
0ERTIFICATE OF COVERAGE NO. NCG08 f) DSO (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling ults from the laboratory.)
FACILITY NAME COUNTY If . + I
PERSON COLLECTING SAMPLES PHONE NO. (A2U J. MW - ,:9$'$_,
CERTIFIED LABORATORY Lab #
Lab # EASE SIGN ON THE REVERSE
Part A: Vehicle Maintenance Areas Monitoring Requirements NC " ✓ RECEIVED
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? —yes _no
(if yes, report your analytical results in the table immediately below) JUN 2 1 1017
Outfail
No.
Date
Sample Collected,
mold
-00530-'• x
3r 4004WP
`� 1 00556: = =f
4,_ `` TRAq -
-Total Suspended'Sohds,
pH,
� Standaid units -
' ' Oil and Grease, a
r ;--
'New Mot Tl
Annuil avera e, al/ino
Benchmark
-
==100�
Wit>iin6:0='9:0
:5/7A
log
3
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Part B: Oillwater Separators and See ndary Containment Areas at Petroleum Bulk Stations and Terminals
Outfall
No.
Date .
Sample Collected,
mo/dd/yry
00556 ; '
'' ' s%00530 `.. ; .; :
:00400 -
Od and Grease, -
Total Suspended Sohds,�
r.. ��
pH;
eStandad units
Permit Limit
30
100
Ire. 6.0 _ 9 0,
STORM EVENT CHARACTERISTICS:
Date (first event sampled)
Total Event Precipitation (inches): _
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
=S
N
SWU-250-102107
Page 1 of 2

"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
OAA,4J"IJ2:3-j01I 6 1S/
(Signature f
Permittee) (Date)
SWU-250-102107
Page 2 of 2

(�15'neAnalyficalo
rra+rpatpm&oGm
June 06, 2017
Mr. Michael DeBraske
Schneider National, Inc.
PO Box 2545
Green Bay, WI 543062545
RE: Project: SNI-Charlotte, NC
Pace Project No.: 92341793
Dear Mr. DeBraske:
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntensville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 24, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Caryssa Berg, Schneider National
Mr. Michael DeBraske, GEI Consultants, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytcal Services, LLC,
Page 1 of 14

Pace Analytical Services, LLC
aceMalytical• sB00KincayAve. Suite 100
Huntersvllle, NC 2H078
7i3
www.Pmmkb&=n
[phone]
CERTIFICATIONS
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Cerfification #: 99006001
North Carolina Drinking Water Certification M 37706
FloddalNELAP Certification M E87627
North Carolina Fleld Servlces Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
VirglniaNELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certificatlon #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VrglniaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not 6e reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 14

aceAnalytical o
www.pecefebs.can
SAMPLE ANALYTE COUNT
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92341793001
SPA
EPA 1664E
JMS
1
PASI-C
SM 2540D
NAL
1
PAS I -A
EPA9040
KDF1
1
PASI-A
92341793002
SP-2
EPA 1664E
JMS
1
PASI-C
SM 2540D
CJH1
1
PASI-A
EPA9040
KDF1
1
PASI-A
92341793003
SP-3
EPA 1664E
JMS
1
PASI-C
SM 25400
CJH1
1
PASI-A
EPA9040
KDF1
1
PASI-A
92341793004
SP-4
EPA 1664E
JMS
1
PASI-C
SM 2540D
CJH1
1
PASI-A
EPA9040
KDF1
1
PASI-A
92341793005
SP-5
EPA 1664E
JMS
1
PASI-C
SM 2540D
CJH1
1
PASI-A
EPA9040
KDF1
1
PASI-A
92341793006
SP-6
EPA 1664E
JMS
1
PASI-C
SM 2540D
CJH1
1
PASI-A
EPA9040
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace AnelyHcel Services, LLC. Page 3 of 14

IceAnalytical'o
www,pacsfeba.c"
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersvllle, NC 28078
[phone]
Sample: SP-1
Lab ID: 92341793001 Collected: 05/23/17 13:45
Received:
05/24/17 13:49 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
5.2 mg/L
5.0
1
06/06/17 07:06
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
108 mg/L
16.2
1
05/26/17 17:27
9040 pH
Analytical Method: EPA 9040
pH
7.1 Std. Units
0.10
1
05/26/17 00:23 H6
Sample: SP-2
Lab lD: 92341793002 Collected: 05/23117 13:30
Received:
05/24/17 13:49 Matrix: Water
Parameters
Results Units ,
Report Limit
OF
Prepared
Analyzed CAS No, Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg1L
5.0
1
06/06/17 07:07
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
55.2 mg1L
10.0
1
05/27/17 07:44
9040 pH
Analytical Method: EPA 9040
pH
8.2 Std. Units
0.10
1
05/26/17 00:23 H6
Sample: SP-3
Lab ID: 92341793003 Collected: 05123/17 13:10
Received:
05/24/17 13:49 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg1L
5.0
1
06/06/17 07:08
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
280 mg/L
16.7
1
05/27/17 07:44
9D40 pH
Analytical Method: EPA 9040
pH
7.4 Std. Units
0,10
1
05/26/17 00:23 H6
Sample: SP-4 Lab ID: 92341793004 Collected: 05/23/17 12:45 Received: 05/24/17 13:49 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease NO mg/L 5.0 1 06/06/17 07:08
Date: 06/06/2017 02:49 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC,
Page 4 of 14

aceAnalytical
www.pecelahe.eom
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP-4
Lab ID: 92341793004 Collected: 05/23/17 12:45
Received:
05/24/17 13:49 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
1060 mg1L
50.0
1
05/27/17 07:45
9040 pH
Analytical Method: EPA 9040
pH
7.6 Std. Units
0.10
1
05/26/17 00:23 H6
Sample: SP-5
Lab ID: 9234179300E Collected: 05/23/17 12:10
Received:
05/24/17 13:49 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, 011 and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mglL
5.0
1
06/06/17 07:08
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
386 mg1L
50.0
1
05/27/17 07:45
9040 pH
Analytical Method: EPA 9040
pH
7.1 Std. Units
0.10
1
05/26/17 00:23 H6
Sample: SP-6 Lab ID: 92341793006 Collected: 05/23/17 12:30 Received: 05/24/17 13:49 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16648
Oil and Grease ND mglL 5.0 1 06/06/17 07:09
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 204 mglL 33.3 1 05/27/17 07:46
9040 pH Analytical Method: EPA 9040
pH 7.1 Std. Units 0.10 1 05/26/17 00:23 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 06/06/2017 02:49 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14

aceftlyrical'
www.pacefebs cam
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
QC Batch: 363491 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92341793001, 92341793002, 92341793003, 92341793004, 92341793005, 92341793006
METHOD BLANK: 2015170 Matrix: Water
Associated Lab Samples: 92341793001, 92341793002, 92341793003, 92341793004, 92341793005, 92341793006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L NO 5.0 06/06/17 07:05
Pace Analytical Services, LLC
9000 Kincey, Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2015171
Spike LCS
LCS
% Rae
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mglL
40 38.5
96
78-114
MATRIX SPIKE SAMPLE:
2015172
92341793001 Spike
MS
MS
% Rae
Parameter
Units
Result Conc.
Result
% Rae
Limits Qualifiers
Oil and Grease
mglL
5.2 40
43.7
96 78-114
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2017 02:49 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 14

aceAnalyrical
www.pOCOMacpm
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
QC Batch: 362513 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92341793001
METHOD BLANK: 2010010 Matrix: Water
Associated Lab Samples: 92341793001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 05/26/17 17:17
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2010011
Spike LCS LCS % Rae
Parameter Units Cone. Result % Rae Limits Qualifiers
Total Suspended Solids mglL 250 238 95 90-110
SAMPLE DUPLICATE: 2010012
92341670006 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 2" 252 3
SAMPLE DUPLICATE: 2010013
92341754001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL ND ND
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 06/06/2017 02:49 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 14

aceAnalyAca!°
waw.Ppc"toom
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
QC Batch: 362555 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92341793002, 92341793003, 92341793004, 92341793005, 92341793006
METHOD BLANK: 2010145 Matrix: Water
Associated Lab Samples: 92341793002, 92341793003, 92341793004, 92341793005, 92341793006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 05/27/17 07:42
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2010146
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 240 96 90-110
SAMPLE DUPLICATE: 2010147
92341644001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 13.5 14.0 4
SAMPLE DUPLICATE: 2010148
92341819001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 5.6 6.2 10 D6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06106/2017 02:49 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 14

(�IacI Anapical e
e wewpscelaO&Wn
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
QC Batch: 362325 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92341793001, 92341793002, 92341793003, 92341793004, 92341793005, 92341793006
SAMPLE DUPLICATE: 2009194
92341588002 Dup
Parameter Units Result Result RPD Qualifiers
pH Sid. Units 3.5 3.5 0 H6
SAMPLE DUPLICATE: 2009195
92341638002 Dup
Parameter Units Result Result RPD Qualifiers
pH Slid, Units 6.4 6.4 0 H6
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersvllle, NC 28078
[phone]
Results presented on this paps are In the units indicated by the "Unlb" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 06/06/2017 02:49 PM without the written consent of Pace Analytical Services, I.l-C.
Page 9 of 14

11�
aceArralytical
rrrmpmoepCscam
QUALIFIERS
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
DEFINITIONS
DF - Dilution Factor, it reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MD -Adjusted Method Detection Limit.
PQL - Practical Quanlitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersvi Ile. NC 28078
(704 )875.9092
S - Surrogate
1,2-Dlphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nltrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits,
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2017 02:49 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

aceAnalytical
www.paceleba.sam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SNI-Charlotte, NC
Pace Project No.: 92341793
Lab ID Sample ID QC Batch Method QC Batch
92341793001
SPA
EPA 1664E
363491
92341793002
SP-2
EPA16648
363491
92341793003
SP-3
EPA16648
363491
92341793004
SP-4
EPA16648
363491
92341793005
SP-5
EPA16648
363491
92341193006
SP-6
EPA1664B
363491
92341793001
SPA
SM 2540D
362513
92341793002
SP-2
SM 25400
362555
92341793003
SP-3
SM 2540D
362555
92341793004
SP-4
SM 2540D
362555
92341793005
SP-5
SM 25400
362555
92341793006
SP-6
SM 2540D
362555
92341793001
SP-1
EPA 9040
362325
92341793002
SP-2
EPA 9040
362325
92341793003
SP-3
EPA 9040
362325
92341793004
SP-4
EPA 9040
362325
92341793005
SP-5
EPA 9040
362325
92341793006
SP-6
EPA 9040
362325
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2017 02:49 PM without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kinrey Ave. Suge 100
Huntersville, NC 28078
[phone]
Analytical
Analytical Method Batch
Page 11 of 14

Document Name:
Document Revised: Sept. 21, 2016
8C6�ilTc�}�1C3�a
Sample Condition Upon Recei t SCUR
Page 1 of 2
F
-Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.01
Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville Raleigh[] Mechanicsville[]
Client Name:
WO# : 92341793
nn yy
Project
d:• .
'Courier:
Fx
Client
❑Commercial
'UPS
BCe
❑Other:/
1923iii4278.3I I!!! 1
Present?
Custody Seal
❑Yes No
Seal -Intact? ❑Yes
[24
Date/initials Person Examining Contents: 5-7L�--I1
Packing Material:
❑Bubble Wrap
(Bubble Bags ❑None
❑Other: /
Thermometer:
❑ IR Gun ID:
T" ^�
J_LiVV
Type o icae Wet
❑Blue
LJi ess has begun
❑None Samples on ice, cooli�ro❑N/A
Correction Factor:
Cooler temp Corrected (IQ . 0
Biological Tissue Frozen? []Yes
Temp should be above fre
)ng to VC
USDA Regulat d Soli (
N/A, water sample}
Did samples lginate in a quarantine
zone within the United States: CA, NY, or SC (check maps)?
Dld samples originate from a foreign source lint r ationally,
Yes o
including Hawaii and Puerto Rico)? []YesNo
' . rnmmanlaInle"Anannrr
Chain of Custody Present?
s
QN0
N A
1.
Samples Arrived within Hold Time?
126yes
UNif
QN/k-
2.
Short Hold Time Analysis 02 hr.)?
Yes
N A
3.
Rush Turn Around Time Requested?
Y
ED4
M N A
4.
Sufficient Volume?.
s
No
N/A
S.
Correct Containers Used?
-Pace Containers Used?
Y's
pS
[IN,
No
❑N/A
QNJA
6.
Containers Intact?
es
Cl&
N A
7.
Samples Field Filtered?
C3V
No
N A
8.
Note If sediment Is visible in the dissolved container. .
Sample Labels Match C0C7
-Includes Dat me i0/Ana sis Matrix:
lies
[:]No
❑N/A
9.
S (f S o^ G%^--`,-r ' t ►Z
7n1 ly -Sir an ttA-erf ,S 17
heads ace In VOA Vials >5-6mm
Yes
040
N A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
QYes
CYNO
No
N/A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Field Data Required? ❑Yes ❑No
Date/Time:
Project Manager SCURF Review: tav u3 Date:
Project Manager SRF Review: Date:
Note: Whenever there Is a dlscrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina OEHNR Certiflcation Office (Le,
Out of hold, incorrect preservative, out of temp, Incorrect contalners)
Page 12 of 14

Vl JO E L abed
P,
O1
LL
Z
q
`�Q
4wA1.
p
U
1's Y�
L, .�
�1n
iF an
iwA1 ��0I4� 1°nPlisN
4 q 7�
Polup
°gdw°g
5
w
js
p°less
In
0 u! MR
to'r
sfOil
�,'S
I
{}j!
i7J
a
"
i
Hd
Sal
K
x
K
%
K
K
x
X.
K
K.
%
x
•�
•.• ..:•
_
MI Aq a°sup pus nO
x
K
x
x
K
x
{
• loumn.w
. ; . � '
S
1
£ONION
HORN
to
a.
i
r
�'
#
1.
£ONH
•:
roszH
PsAjossidun
'
tt
�.
IMNIY1NO2 30I
N0110311031Ydri3131dW"
PLg
-
a
4
D
—,
fmMW.D6Mu�13any%1tllYW
(0101-2 MO-01 3d/131dW B
5
r
rz
LL
29
LU
�
millz
01

A
N
m
b
v
Z
i
R
0
3
,10y
V
IS
w
n
Q
v
H
a
�
m
w
m
G
04
m
Cn
e
M
n
M
N
M
3
�
m "
a
M
_N
m
-
CL m
-a
ro
0
a�
MM
n a
m
m_
c
m
s
A
■■■■
■■■■■■■■
1
■■■■■■■■■■■■
11 -
■■■■�Emmm=©
:.
ii
ri-
i■ri-
r
it
- • .. _ ... r :. .
■■■■■■■■■■■■
■
■■■■■■■■■■■■
1 mLVOA
■■■■■■■■■■■■
, . • 1 • • .
■■■■■■■■■■■■
F'Ar
IN
WIMMUMPIVAPIAr
EWE
■■■■■■■■■■■■
■■■■■■■■■■
■■
r�
0 In co CD
C

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCGO80000 p Q
CERTIFICATE OF COVERAGE NO. NCG08 6 A
FACILITY NAME
PERSON COLLECTING SAMPLES
CERTIFIED LABORATORY '0 C91 Lab #ter
Lab #
SAMPLES COLLECTED DURING CALENDAR YEAR: 1 i_l i-
(This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY
PHONE N6.(617(34
PLEASE SIGN ON THE REVERSE �
Part A: Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?, yes _no
(if yes, report your analytical results in the table immediately below)
Outfall
No.
Date
Sample Collected,
mo/d
00530
00400<
� 00556 v
,
Total Suspended Solids,':=
pH* =
Standard
,Oii and Grease,
"•f'NewiMot6n0il Usage;k
..
i.-,Annual ave - al/mo"te
Benchmark
Withm;6 0_-:9.0f 4
._ 30
5
is 1
3
y
32
-7•
N
-7 5
a
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier I or Tier 2 responses.
See General Permit text.
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
Ontfall
No.
Date
Sample Collected;
nwlats
00556'_ _ .
: 0053E1_ `:: = . _
� ` R 00400
Oil and Grease, x
_ Total Suspended`Sulids;, -
_ „; �.
-PH,..;
Staridard:urii
Permit Limit
_
30
I00r`�'
= < . :::::
a., . b`0= 9.0 •
STORM EVENT CHARACTERISTICS:
Date Lf IS I N (first event sampled)
Total Event Precipitation (inches): Q . Q 0
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
RECEIVED
APR 2 5 2017
CENTRAL FILES
DWR SECTION
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SWU-250-102107
Page 1 of 2

"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
A�24 L4 Zb f I-(
(Signature ff Permittee) (Date)
S WU-250-102107
Page 2 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCGO80000 SAMPLES COLLECTED DURING CALENDAR YEAR: 1J 1-
CERTIFICATE OF COVERAGE NO. NCG08 (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME i`_I(l n 1 n� COUNTY
PERSON COLLECTING SAMPLES , Q UhN_ PHONE NO. IO
CERTIFIED LABORATORY Ta C .R - Lab # 5, -
Lab # PLEASE SIGN ON THE REVERSE
Part A: Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? yes _no
(if yes, report your analytical results in the table immediately below)
Oatfall`
No.
z-
Date zr .
.Sample Collected;
mold • �a °+' i
00534) _ _
00WK IMA
Total Suspended`Sohds,;pH;�"`"�
„ i
bStandard'ts
""Oil nd[Greas ;5
New'Motor OilUs`a a
Annual�avera e, Vino
Bknchmark
= - r
_rt
100,
1 ; "Within 6 WPWT0
g
P
'-i 5 -1y
�]
P
y 3
Note: if you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
Outfall -
Date ? - 4
Sample. Corrected, s,
mold'.-
.0t1556 f
:r 0t1530
W47. 06 ri ` 4
`Oil and'Grease
�Total,SuspendedlSolids,
M
pH;
StaLndnard�l�tl+n�ltS%.Lz".'y
_.6.V 910?�-_'
STORM EVENT CHARACTERISTICS:
Date H 15 111 (first event sampled)
Total Event Precipitation (inches): AD
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
S WU-250- l 02107
Page 1 of 2

aceAnalytical•
www-PS004 tri.com
April 18, 2017
Mr. Michael DeBraske
Schneider National, Inc.
PO Box 2545
Green Bay, WI 543062545
RE: Project: SNI-Charlotte, NC
Pace Project No.: 92336168
Dear Mr. DeBraske:
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
[phone] -
Enclosed are the analytical results for sample(s) received by the laboratory on April 06, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Caryssa Berg, Schneider National
Mr. Michael DeBraske, GEI Consultants, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In Full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 14

Pace Analytical Services, LLC
Kinrey Ave.ac100
eAnalytical o 9800Huntersvlle, C1te 28078
WWW4N celab`com
[phone]
CERTIFICATIONS
Project: SNI-Charlotte, NC
Pace Project No.: 92336168
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersvitle, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification M 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
VlrglniatVELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginialVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 14

aceAnalytical
'
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: SNI-Charlotte, NC
Pace Project No.: 92336168
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92336168001
SP 1
EPA 1664B
JMS
1
PASI-C
SM 2540D
WRC
1
PASI-A
EPA 9040
ALC
1
PASI-A
92336168002
SP 2
EPA 1664E
JMS
1
PASI-C
SM 2540D
WRC
1
PASI-A
EPA 9040
ALC
1
PASI-A
92336168003
SP 3
EPA 1664E
JMS
1
PASI-C
SM 2540D
WRC
1
PASI-A
EPA 9040
ALC
1
PASI-A
92336168004
SP 4
EPA 1664E
JMS
1
PASI-C
SM 2540D
WRC
1
PASI-A
EPA 9040
ALC
1
PASI-A
92336168005
SP 5
EPA 1664B
JMS
1
PASI-C
SM 2540D
WRC
1
PASI-A
EPA 9040
ALC
1
PASI-A
92336168006
SP 6
EPA 1664B
JMS
1
PASI-C
SM 2540D
WRC
1
PASI-A
EPA 9040
ALC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 14

aceAnalytical
'
www.psoefts can
ANALYTICAL RESULTS
Project. SNI-Charlotte, NC
Pace Project No.: 92336168
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample. SP 1
Lab ID: 92336168001 Collected: 04/05/1 T 00:00
Received:
04/06/17 10:55 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
38.8 mg1L
5.0
1
04/18/17 07:28
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
323 mg1L
25.0
1
04/11/17 16:29
9040 pH
Analytical Method: EPA 9040
pH
6.7 Std, Units
0.10
1
0410T117 13:59 H6
Sample: SP 2
Lab ID: 92336168002 Collected: 04/05/17 00:00
Recelved:
04/06/17 10:55 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 16648
Oil and Grease
7.8 mglL
5.0
1
04/18/17 07:28
2540D Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
323 mglL
41.7
1
04/11/17 16:29
9040 pH
Analytical Method: EPA 9040
pH
8.6 Std. Units
0.10
1
04/07/17 13:59 H6
Sample: SP 3
Lab ID: 92336168003 Collected: 04/05/17 00:00
Received: 04/06/17 10:55 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qua[
HEM, Oil and Grease
Analytical Method: EPA 1664E
OII and Grease
7.0 mglL
5.0
1
04/18/17 07:29
2540D Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
366 mglL
50.0
1
04/11/17 16:39
9040 pH
Analytical Method: EPA 9040
pH
7.5 Std. Units
0.10
1
04/07/17 1159 H6
Sample: SP 4 Lab ID: 92336168004 Collected: 04/05/17 00:00 Received: 04/06/17 10:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16648
Oil and Grease 7.6 mglL 5.0 1 04/18/17 07:30
Date: 0411812017 03:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 14

aceAnaljdical"
www.peoelaba.cam
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92336168
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huniersville, NC 28078
[phone]
Sample: SP 4
Lab ID: 92336168004 Collected: 04/05/17 00:00
Received:
04/06/17 10:55 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared
Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
724 mg1L
50.0
1
04/11/17 16:40
9040 pH
Analytical Method: EPA 9040
pH
7.3 Std. Units
0.10
1
04/07/17 13:59 H6
Sample: SP 5
Lab ID: 92336168005 Collected: 04/05/17 00:00
Received:
0410611710:65 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
8.3 mglL
5.0
1
04/18/17 07:30
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
632 mglL
50.0
1
04/11/17 16:40
9040 pH
Analytical Method: EPA 9040
pH
7.1 Sid. Units
0.10
1
04/07/17 13:59 H6
Sample: SP 6 Lab ID: 92336168006 Collected: 04/05/17 14:10 Received: 04/06/17 10:55 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease 6.2 mg1L 5.0 1 04/18/17 07:31
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 339 mg1L 33.3 1 04/11/17 16:41
9040 pH Analytical Method: EPA 9040
pH 6.8 Std. Units 0.10 1 04/07/17 13:59 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 0411812017 03:25 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14

aceAnalytical
www.pec"acom
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92336168
QC Batch: 356972 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92336168001, 92336168002, 92336168003, 92336168004, 92336168005, 92336168006
METHOD BLANK: 1980295 Matrix: Water
Associated Lab Samples: 92336168001, 92336168002, 92336168003, 92336168004, 92336168005, 92336168006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 04/18/17 07:25
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1980296
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mg1L 40 37.0 92 78-114
MATRIX SPIKE SAMPLE: 1980297
35305736004 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 1 A U 40 38.1 95 78-114
ftevutts prevented on this page are In the units Indicated by the "UnlW column except where an alternate unit is presented to the right of the rmwtt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 04/1812017 03:25 PM without the written consent of Pace Analytical Services, I.I.C.
Page 6 of 14

aceAnalydcal
W*W.pecelaDa.WM
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92336168
QC Balch: 356186 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92336168001, 92336168002
METHOD BLANK: 1975904 Matrix: Water
Associated Lab Samples: 92336168001, 92336168002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 04/11/17 16:19
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1975905
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mglL 250 230 92 90-110
SAMPLE DUPLICATE: 1975906
92336086003
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mglL
NO
ND
SAMPLE DUPLICATE: 1975907
92336086013
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mglL
ND
NO
Results presented on this page are In the units Indicated by the "units" column except where an alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/18/2017 03:25 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 14

(�15'cieftlytical*
www.peceilabs.aom
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92336168
QC Batch: 356188 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92336168003, 92336168004, 92336168005, 92336168006
METHOD BLANK: 1975909 Matrix: Water
Associated Lab Samples: 92336168003, 92336188004, 92336168005, 92336168006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 04/11/17 16:38
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1975910
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 244 98 90-110
SAMPLE DUPLICATE: 1975911
92336168003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 366 358 2
SAMPLE DUPLICATE: 1975912
92336424001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL <5.0 ND
Results presented on this papa are In the units indicated by the 'Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 0411812017 03:25 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 14

leAnalAcal`
www.Pnowakcom
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92336168
QC Batch: 355720 Analysis Method: EPA 9040
QC Balch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples. 92336168001, 92336168002, 92336168003, 92336168004, 92336168005, 92336168006
SAMPLE DUPLICATE: 1973365
92336168001 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 6.7 6.7 1 H6
SAMPLE DUPLICATE: 1973366
92336050004 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 5.4 5.4 1 H6
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this pane are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/18/2017 03:25 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 14

Pace Analytical Services, LLC
�acl
Analytfcal ` 9800 Klncey Ave. Suite 100
Huntersvllle, NC 28078
sww.peCSIO ,00m
(704)8759092
QUALIFIERS
Project: SNI-Charlotte, NC
Pace Project No.: 92336168
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantltation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether,
A separate vial preserved to a pH of 4-5 Is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Dlphenylamine using Method 8270. The result reported for
each analyte Is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis Initiated outside of the 1S minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/18/2017 03:25 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

aceAnalyrlcal "
WWWPXMbb&Com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SNI-Chartotte, NC
Pace Project No.: 92336168
Lob ID Sample ID QC Batch Method QC Batch
92336168001
SP1
EPA 1664B
356972
92336168002
SP 2
EPA16648
356972
92336168003
SP 3
EPA 1664B
356972
92336168004
SP 4
EPA 1664E
356972
92336168005
SP 5
EPA 16648
356972
92336168006
SP 6
EPA1664B
356972
92336168001
SP 1
SM 2540D
356186
92336168002
SP 2
SM 2540D
356186
92336168003
SP 3
SM 2540D
356188
92336168004
SP 4
SM 25400
356188
92336168005
SP 5
SM 2540D
350188
92336168006
SP 6
SM 2540D
356188
92336168001
SP 1
EPA 9040
355720
92336168002
SP 2
EPA 9040
355720
92336168003
SP 3
EPA 9040
355720
92336168004
SP 4
EPA 9040
355720
92336168005
SP 5
EPA 9040
355720
92336168006
SP 6
EPA 9040
355720
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 04/18/2017 03:25 PM without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunteravllle, NC 28078
(704)8759092
Analytical
Analytical Method Batch
Page 11 of 14

Document Name: Document Revised: Sept. 21, 2d16
dCEARc7� lCc1�• Sam le Condition Upon Racei t SCUR Page 1 of 2
Document No.., issuing Authority:
F-CAR-CS-033-Rev-01 Pace Quali Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ HuntersvilleF�dK Raleigh[] Mechanlcsvllle❑
CIlentName: Project W0# : 92336168
�:, '
Courier: d t:x UP U5P5[]Client
❑ Commercial ZPace ❑Other: `
92336198
Custody Seal Present? Dyes ErNo Seals intact? ❑Yes []No}
Date/Initials Person Examining for n �,
Pecking Materiel; ❑Bubble Wrap bble Bags []None❑Other:
Thermometer:
❑ IR Gun ID: I 1 �p Ty Ice• et ❑Blue ❑None ❑ ample, on Ice, cooling process has begun
Correction Factor: Cooler Temp Corrected ('C): Biological Tissue Frozen? Yes [-]No N/A
Temp should be above eezing to VC
USDA Regulated S ❑ N/A, water sample)
Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {interpt"ally,
❑Yes FlNo Including Hawaii and Puerto Rlcol? []Yes UNo
Chain of Custody Present?
es
QNO
N A
1.
Samples Arrives! within Hold Time?
es
No
N A
2.
Short Hold Time Anal sls 02 hr.)?
Yes
RrNo
N A
3.
Rush Turn Around Time Re uested?
Dyes
LaWo
N A
4.
Sufficient Volume?'
UVIr
QN.
N/A
S.
Correct Containers Used?
-Pace Containers Used?
Gies
Yes
❑No
No
[IN/A'
N A
b.
Containers Intact?
flyes
No
QNLA
7.
Samples Field Filtered?
❑Yes
❑No
N/A
1 8. Note if sediment Is visible In the dissolved container
Sample Labels Match COO ❑Yes [ado ❑N/A 9.N1 I3f1I1 51 ,lni -A
Heads ace In VOA Vials >S-6mm ? QYes ONO N A 14.
Trip Blank Present? ❑Yes []NO PA 11.
Trip Blank Custody Seals Present? 13yes ❑No ❑tt/A
CLIENT NOt1FIC1kTI0N/RES0LVTlON
Person Contacted:
Comments/Sample
Discrepancy:
Project Manager SCURF Review:
Project Manager SRF Review: -
Field Date Required? ❑Yes ❑No
Date/Tlme,
Date: l�
Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le.
Out of hold, Incorrect preservative, out of temp, incorrect containers)
Page 12 of 14

43
U3
m
m
O
A
3
0
K
m
w
m
S
a
0
3
C
m
�
9
3
M
m
mo
rr
o�
co
o
u-9
16
R
M
H
.1
O.
Q 4
�
�
n
6
m
a
jD
A
0
t=
C
w
n
a -0
n m
m
K
s
a
i
iiri-
i
MMiiiir
.. .
W
M
PAMM
WAWA
MMII
BPNM
r
i
i
r
0
i
i
iri
MI
: 1
■■■E■■■■■■■■
• -
III/II/III/IIIIiIIII/M
1 •
wM%MIT
I/%I/III
/I
//
.
■■■■■■■■■■■■
=" � l MON
.. . 1 ■ . ..
I■■■1■i■■■E■■■
M■■M■■■MEM
�riiii
Mii
MM
MM
E
■i■ii■i■iii■
�
n
s
m

CHAIN -OF -CUSTODY / Analytical Request Document
•, t-Q�Pi �'1! IR �f • The i7tain-of-Custody is a LEGAL DOCUMENT. All relevant rields must be completed accurately. p
C
to
CHAIN -OF -CUSTODY I Analytical Request Document a
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately -
Section A Section B Seetien C
Repaired Client kdormatkwx Required Project Information: trnrafce Wormatierr: Pe 7 Of 5
Comparq: Srrireder Natural Report TO: Gene Gore
CnarkOne. NC 20259
Emart cum .
Purchase Order 2:
Pace Qrnte:
5�a ��"w•': s" ?5-".+tStataJlomtian:. a-li= i=.>'"
Pt+orre: f704jS99-74l3 Far
Project Name: SNI-Chxk*e. NG
Pace P"W Ma -W. rkow. .cmt
Section D Matria Cadea
Cliera k*wmabon MATRIK I CODE
Omtkp W.I. DW
-
-
2
U
COLLECTED
Water WT
$
"
U
Waite Water lNW
o
0
r[EiE
Product p
-
9
srurt
F.rtne
SOWSaitl St.
p
SAMPLE ID 011
ape WP
(A-Z. 0.9 r : l Air AR
a
w
Samae IDS MUST BE UNIQUE Tissue TS
0
a
OUrer OT
U
g
X
J
E=
T !V
DATE
TIME
DATE
Z
ro
V
rJl
0
Z
C
Z
LM 0
U
IL LL
to a
Requested Analysis FRered (YIN)
preservatives
Z
F o
to U
s z z mO _ Pace P ojett NoJ Lab I.D.
003
I ADDITIONAL COMMENTS I RELINQUISHED BY I AFFILIATION I DATE I TIME I • ACCEPTED BY l AMLIATION I DATE I TIME I SAMPLE CONDrTIONS I
4
SAMPLER NAME AND SIGNATURE
ORIGINAL
PRMTNameofSAMPLER
SIGNATURE of SAY '
'6ripon..a NWu: 1'Jy �><] trr6 tam Ya+ are aorxrptrq Pam'S NETT 70 aaT pararan rorrrr5 a.tl �$w�! la tale dtdrget d 7.SX per fd• mry
o
s o
ZV oUz wZ
DS a}
AE
DATE Signed I'y E - $ m
jMMfDDlYY): !J/ 5 I ( An rn
wdt 9DGoys. F-ALL-"20rev.07.15-May-2047

cleAnalXical
ww&pftvhftGvM
QUALITY CONTROL DATA
Project: SNl-Chartolte, NC
Pace Project No.: 92336168
QC Batch: 355720 Ana"Is Method. EPA9040
QC Batch Method: EPA 9040 Analysis Description: 9040 PH
Associated Lab Samples: 92336168001, 92336168002, 9233e168003, 92336168004, 92336168D05, 92336168006
SAMPLE DUPLICATE: 19733e5
923361e6001 Dup
Parameter UrIb Result Result RPD Qualifiers
PH Std, Units 6.7 6.7 1 HB
SAMPLE DUPLICATE: 19733M
92330050004 Dup
Parameter Units Result Resull RPD Quallfiers
PH Std. Units 5.4 5.4 1 H6
Pace Anstytkel Setvkss, LLC
98M KinceyAve. Suite 100
Huntersville, MC 28078
(704)875-O092
Rasuhs pnMrlted en tf4s papa are In IM units Indicated by the •UnW Coloaat except wrwan saamsta unit is presented to vw right at 1M matt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, exoept In full,
Date: 0411 &2017 03:25 PM without the written consent of Pace Analytical Services, LLC. Pape 9 of 14

I'WeAnalyticsl Services, LLC
9800KInceyAve. Sults100
Huntaisville, NC 28078
M 1* (704)87"092
I
QUALIFIERS
Project SNI-Charlotte, NC
Pace ProjectNo.: 92338168
DEFINITIONS
DF - Dilution Fartor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection tirnit and below the adjusted reporting limit
MDL - Adjusted Method Detection Limit,
PQL - Prac tlwl Quantkatlon Limit.
RL - Reporting Limit
S - Surrogate
1.2-Dlpherty1hydrazine decomposes to and cannot be separated from Azobenxene using Method 8270. The result for each analyte is
a combined ooncentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable,
SG - Silica reel - Ciesn-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-6 is recommended In SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8200.
N-Nitrosodlphenylamine decomposes and cannot be separated From Diphenylamine using Method 8270. The result reported for
each analyte Is a combined eoricentration.
Pace Analytical is TNt accredited. Contact your Pace PM for the current list of accredited analyies.
TNI - The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PAS I-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull,
Date: 04/1812017 03:25 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

ceAnala
aMw.paospbr.c+om
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SNI-Charlotte. NC
Paoe Project No.: 92330168
Pecs Analytical Servk", LLC
9800 Kirwey Ave. Suite 100
Huntnrsville, NC 28078
{704j8754m
Lab ID
Sample ID
QC Batch Method
Analytical
GC Batch Analytical Method Batch
92336166001
SP 1
EPA 10648
360972
92336168002
SP 2
EPA 1064E
356972
923361SH03
SP 3
EPA 1664B
358972
92336168004
SP 4
EPA1664B
356972
92336160005
SP 5
EPA16648
358972
92336169006
SP 6
EPA1664B
355972
92336166001
SP 1
SM 2540D
356186
92335168002
SP 2
SM 2540D
356186
92336168003
SP 3
SM 2540D
356188
92336168004
SP 4
SM 25QD
355188
92336166003
SP S
SM 2540❑
356188
92336168006
SP 6
SM 2540D
350188
92336168001
8P 1
EPA 9040
355720
92=160002
Bpi
EPA 0040
355720
92MI68003
SP 3
EPA 9040
355720
92336168004
SP 4
EPA 9040
355720
92338168005
SP 8
EPA 9040
355720
92336168009
SP6
EPA9040
355720
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/181201 i 03:25 PM without ttte written consent of Pace Analytical Services, LLC. Page 11 of 14

J Document Name: Document Revised: Sept. 21,2016
/Cain Sample Condition Upon Recel SCUR PaLe i of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.01 Pace Quality Offke
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersvlller-L"' Raleigh[] Mechaanlcsvllle❑
Client Name: Project tt: WO# : i
92336 � 68
Courier: Ufad Ex EluprLISPS Eklient
❑
Commercial Pace ❑Other:
Custody seal Presetlt? Dyes EJNo Seals Intact? QYes ONO
onto/initiols Parson Examining�rfMn^
Packing Material: ❑Bubble Wrap bble Bags None []Other:
Thermometer: �
❑ IR Gun iD: ��, et ❑Blue ❑Norte ❑Samples on ioe, cooling process has begun
Correction Factor: Cooler Tamp Corrected (*Cl: n1l Biological Tissue Frozen? []Yes []No N/A
Temp should be above k6e:ing to 6-C
USDA Regulated S ❑ N/A, water sample)
Did sampl!rriginate to a quarantine zone within the United States: CA, NY, or SC (check maps)? Dld samples originate from o tomign source (internauoiwttY,
I—IYes i INa Includine fiawail and Puerto Rico)? ©Yes 0No
of CustodyPresent?
e
NO
NAChain
I.
Sam es Arrived within Hold 71me7
es
2.
Shut Maid Tame Anal is 01 kr. ?
Yes
Na
3.
Rush Turn Around Time Re ed?
Yes
o
N A
4.
ff d Suent Volume?
o
ONLA
S.
Correct Containers Used?
G5es
❑No
ON/A
6.
Samples Field Filtered?
QYes
rlNq
N A
8. Note if sediment Is visible In the dissolved container
Sample labels Match COC? --
❑Yes
(moo
[]N/A
9.
-Includes Date lm 10 Ana is Matrix:
Heads ace In VOA Vials >5-6mm ?
Oval
ON, -
Trip Blank Present?
Oyes
❑No
A
12.
Trl Blank Custodyseals Present?
Yes
NO
rIZA
CLIENT NOTIFICATION/fiESOWTION
Field Data Required? []Yes ONO
Person Contacted: Date/Time:
Comments/Sample
Discrepancy:11�0.�+v1
1,
Project Manager SCURF Review: _ 1 V VVIG Date: f �U Ln
r
Project Manager SRF Review: __l�i�j4 _� Date: �Ld l �
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, Incorrect containers)
Page 12 of 14

�]
Document Name:
Document Revised: Sept. 21, 2016
j' J� oaf 4
�'d
Sam le Condition Upon Rece9 SCUtt
pa e 2 of 2
Document No.:
Issutng Authority.
f-CAR•CS-033-Rev.01
Pace Quality Office
*Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
**Bottom half of box Is to list number of bottles
Project # W08 : 92335168
PM, FIN Duo Oatel 04/20/17
CLIENTt 82-SMIDER
E
01
L
IMMEMOMMEMOL
'1000
;me
pH Adjustment log for Preserved
Samples
Sample to
Type of Preservative
pH upon receipt
pate preservation adjusted
Time pmservetlon
adjusted
Amount of Preservative
added
Lot a
Page 13 of 14

CHAIN -OF -CUSTODY 1 Analytical Request Document
pp,,,, ,,, The ChawHg-Cumoy as a LEGAL OOCUUENT. AA nA&e Am Rgku mug be mfnpicWd aeGrrarery. `p
Pace, A,l T
m
CM
CHAIN -OF -CUSTODY 1 Analytical Request Document a
The Cnah-of-Custody is a LEGAL DOGUMEW- AN relevant fleWs must be CMpIaWd ac latety.
Sset:oa A ScWon a Sea mn C
Rew bud Min kdwwratR Rew*" Projml kdurcanion: bwaKe boom zbw Pa t aS 1
Ca'i�+l� Srtxrider ttrliofui RaOaR Ta. iisne Gars
Gh ---- NC�268�
_ - -
gj .m
JpLffdhasa Orear f:
Pax Otlois:
f1hww. it AASS-7413 Ipas
IPFOPM Nair: SN4GhaMpd, NC
Iftm Pry Manager. nicwe. .cam
s.stlon o wabia cows
_
■Mgvw"Cftniv*—A o ►urinr r COr)F
a
COLLECTED
DlaMaq wx" Ow
z
yvalfs U!T
$�
u
Q
Yratr WSW wY7
C=w1YrItC
Sraai
eo�aufe
F.fOViAB
U
w
Prod,q P
CS
e
SAMPLE ID OW
u
V
�
wMe ,
a
W
IA-2.0.41.-1 Au AR
G
I
Saa�le 0% MUST BE UMIOUE Tumn TS
Odra OT
O
U
f
O
A r
t f-"
DATE
THE
DATE
TWE
s
1
.-.5
of
J14
t—
En f
Pmseroemves
i
f]
GC Pw_o Project MoJ Lab I.D.
ADDITUMAL COMMFXIS RUMMSHED BY I AFFMIAT1ON DATE TL¢ ACCEPTED BY ! AFFOAAT1OM OATS I Twe sAAv4z Cowurnam
- � • �fVV�r/ i � �1 �
-N- r err 'I 1 41 j -.%M% M Mid h iiI
SAMPLER NAME AND SIGNATURE
PRMIT WMW of SAMPLER
SIGNATURE of
+6T V wf La. l.y
r'v.3u uar.
u _
F-ALL-":!Orev.07= 154dav-20R7

STORMWATER DISCHARGE OUTFALL (SDO)
MnhrFTnRrN(- RRPnRT
NCG-ago5S3
GENERAL PERMIT NO. NCG080000
CERTIFICATE OF COVERAGE NO. NCG08 11n1)D
FACILITY NAME Z�C)ArlftdXf NQnWAa L
PERSON COLLECTING SAMPLES
CERTIFIED LABORATORY Lab #
Lab #
SAMPLES COLLECTED DURING CALENDAR YEAR: 2D 13
(This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampliN results from the laboratory.)
COUNTY
PHONE NO. (!U 0 )
PLEASE SIGN ON THE REVERSE 4
Part A: Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? X yes _.no
(if yes, report your analytical results in the table immediately below)
Outfa!!
No.
Date
Sample Collected,
maJMAj
00530. -
00400': x
005S6
Total.Snspended Solids; :
... pH, ;Y, f y _
; -Standard uitits�
s 011�arid Greases
< ,
t New Mator OB Usage,
" "Anaue! av al/mo _
Bendunark
-
100
; Wlthin' 6.0 ; `"9A
-
-
SP-
f. 1sI)I
5
it
I VL-
it
2
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier I or Tier 2 responses.
See General Permit text
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
Ontfall
No.
Date
Sample Coiledetl,
moJd
00551i . -;
l . i '. 00530 ' - ��`
00400'. 7
Offhand Grease,
ToW SuspeadedSWids, ,
_ F
yp� --
;Statidard'etteits
Permit Limit
-
'30 °
I00 _
-"6.0 = 9.0 -
STORM EVENT CHARACTERISTICS:
Date Z)101 (first event sampled)
Total Event Precipitation (inches): —D , q tp
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SWU-250-102107
Page I of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCGO80000 SAMPLES COLLECTED DURING CALENDAR YEAR:
CERTIFICATE OF COVERAGE NO. NCG08 (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME COUNTY
PERSON COLLECTING SAMPLES PHONE NO.
CERTIFIED LABORATORY Lab #
Lab # PLEASE SIGN ON THE REVERSE -�
Part A. Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes —no
(if yes, report your analytical results in the table immediately below)
Oatfali
No.
Date
Sample Collected,
mold
00530
00400,: =
s 00556
_ ,
Total Suspended Solids,
pH, "• r F _
Staailard;units ::=
Oil an&Girease,
_ �_
..N6f Motor O11 Usage; '
r.:;Anuoal ave o,
Benchmark
-
400'
Wltbin.6.0=9.0 ",
° 30�.
2
�•
D
It
. O
a
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
Outfall
No.
Date
Sample Collected,
nw/d
, 00556
Oil s_ ud Gam, =-,
Toti&Sospeaded>Sollds,
...� .
�<
pH, ,,-
Staudai d4filts
Permit Limit
-
3W.
STORM EVENT CHARACTERISTICS:
Date (first event sampled)
Total Event Precipitation (inches): -
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
S WU-250-102107
Page 1 of 2

"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
�AAA, L-JA &A 1Ze) 111
(Signaturlof Permittee) (Date)
S"-25n-102107
F 2of2

(�15'ceAnailyficalo
A* paoafaba.00m
February 28, 2017
Mr. Michael DeBraske
Schneider National, Inc.
PO Box 2545
Green Bay, WI 543062545
RE: Project: SNI-Charlotte, NC
Pace Project No.: 92330158
Dear Mr. DeBraske:
Pace Analytical Services, LI_C
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 15, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
/ -
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Caryssa Berg, Schneider National
Mr. Michael DeBraske, GEI Consultants, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

Pace Analytical Services, LLC
98dO
aceMalytical • Huntersvllle, NCi28078
www.paaalab&carn [phone]
CERTIFICATIONS
Project: SNI-Charlotte, NC
Pace Project No.: 92330158
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87027
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
VlrglnialVELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VlrginlalVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, I.I.C. Page 2 of 13

Pace Analytical Services, LLC
aceAnalytical a
9800 i<Incey Ave. 2 78
Huntersvllle, NCC 8078
m m'PowbWom
[phone]
SAMPLE ANALYTE COUNT
Project: SNI-Charlotte, NC
Pace Project No.: 92330158
Analyses
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92330158001 SP-1
EPA 1664E
JMS
1 PASI-C
SM 2540D
ALC
t PASI-A
EPA 9040
ALC
1 PASI-A
92330158002 SP-2
EPA 1664E
JMS
1 PASI-C
SM 2540D
ALC
1 PAS1-A
EPA 9040
ALC
1 PASI-A
92330158003 SP-3
EPA 1664E
JMS
1 PAS!-C
SM 2540D
ALC
1 PASI-A
EPA 9040
ALC
1 PASi-A
92330158004 SP-4
EPA 1664E
JMS
1 PASI-C
SM 2540D
ALC
1 PASI-A
EPA 9040
ALC
1 PASI-A
92330158005 SP-5
EPA 1664B
JMS
1 PASI-C
SM 2540D
ALC
1 PASI-A
EPA 9040
ALC
1 PASI-A
92330158006 SP-6
EPA 1664B
JMS
1 PASI-C
SM 2540D
ALC
1 PASI-A
EPA 9040
ALC
1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13

aceAnalytical
wrw.peceiftcom
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92330158
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP-1
Lab ID: 92330158001 Collected: 02/15/17 00:00
Received: 02/15/17 15:15 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
9.0 mg1L
5.0 1
02/28/17 07:37
25400 Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
154 mg/L
12.5 1
02/20/17 11:34
9040 pH
Analytical Method: EPA 9040
pH
6.9 Sid. Units
0.10 1
02/16/17 10:57 H6
Sample: SP-2
Lab ID: 92330158002 Collected: 02/15/17 10:35
Received: 02/15/17 15:15 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg1L
5.0 1
02128/17 07:38
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
212 mg1L
25.0 1
02120/17 11:34
9040 pH
Analytical Method: EPA 9040
pH
8.4 Std. Units
OJO 1
02/16/17 10:57 H6
Sample: SP-3
Lab ID: 92330158003 Collected: 02/15/17 10:05
Received: 02/15/17 15A5 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No, Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg1L
5.0 1
02/28/17 07:38
25400 Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
208 mg1L
13.9 1
02/20/17 11:35
9040 pH
Analytical Method: EPA 9040
pH
7.2 Std. Units
0.10 1
02/16/17 10:57 H6
Sample: SP-4 Lab ID: 92330158004 Collected: M15/17 09:55 Received: 02/15/17 15:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 02/28/17 07:39
Date: 02/28/2017 03:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 13

aceAnalytical
www.psi;Wabs=m
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92330158
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersvllle, NC 28078
[phone]
Sample: SP-4
Lab ID: 923301SBDD4 Collected: 0211511709:55
Received:
0211511715:15 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
407 mg/L
20.8
1
02/20117 11:35
904D pH
Analytical Method: EPA 9040
pH
7.4 Std, Units
0.10
1
02/16/17 10:57 H6
Sample: SIP-5
Lab ID: 92330158005 Collected: 02J15/17 09:35
Received:
02/15/17 15:15 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg1L
5.0
1
02/28/17 07:39
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
119 mg1L
11.4
1
02/20/17 11:37
9040 pH
Analytical Method: EPA 9040
pH
7.0 Std. Units
0.10
1
02/16/17 10:57 H6
Sample: SP-6
Lab ID: 92330158006 Collected: 0211511170915
Received:
02/15117 15:15 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L
5.0
1
02/28/17 07:39
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
40.3 mglL
6.9
1
02/20/17 11:37
9040 pH
Analytical Method: EPA 9040
pH
6.9 Std, Units
0.10
1
02J16117 10:57 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 02/28/2017 03:05 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13

aceAnalytical.
anrw.peixlebaixvn
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92330158
QC Batch: 350071 Analysis Method: EPA 1664E
QC Batch Method: EPA 16648 Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92330158001, 92330158002, 92330158003, 92330158004, 92330158005, 92330158006
METHOD BLANK: 1941864 Matrix: Water
Associated Lab Samples: 92330158001, 92330158002, 92330158003, 92330158004, 92330158005, 92330158006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L ND 5.0 02/28/17 07:29
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1941865
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg1L
40 36.3
91
78-114
MATRIX SPIKE SAMPLE:
1941866
92330082004 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
36.2
90
78-114
Results presented on We page are In the units Indicated by the "Units" column except where an altemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/28/2017 03:05 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

aceAnalytical
rww.peaelabacom
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92330158
QC Balch: 348957 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92330158001, 92330158002, 92330158003, 92330158004, 92330158005, 92330158006
METHOD BLANK: 1936095 Matrix: Water
Associated Lab Samples: 92330158001, 92330158002, 92330158003, 92330158004, 92330158005, 92330158006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 02/20/17 11:27
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1936096
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mglL 250 226 90 90-110
SAMPLE DUPLICATE: 1936097
92330119001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 274 318 15 D8
SAMPLE DUPLICATE: 1936098
92330156002 Dup
Parameter Units Result Result RPD Qualifier;
Total Suspended Solids mg/L 14.0 14.2 1
Results presented on this page are In the units Indicated by the'Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 02/28/2017 03:05 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 13

(� aceAnalytical
www.pecMeb&cum
QUALITY CONTROL DATA
Project: SNI-Chatiotte, NC
Pace Project No.: 92330158
QC Batch: 348512 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated lab Samples: 92330158001, 92330158002, 92330158003, 92330158004, 92330158005, 92330158008
SAMPLE DUPLICATE: 1933512
92329838002 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 5.8 5.9 1 H8
SAMPLE DUPLICATE: 1933513
92330155003 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 8.5 8.5 1 H6
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the resuh.
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except In full,
Date: 02128/2017 03:05 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

aceAnalytical®
*W..pacele6a.wm
QUALIFIERS
Project SNI-Charlotte, NC
Pace Project No.: 92330158
DEFINITIONS
DF - Dilution Factor, If reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyi ether.
A separate vial preserved to a pH of 4-5 Is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute..
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis Initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/28/2017 03:05 PM without the written consent of Pare Analytical Services, LLC. Page 9 of 13

(�Ia'cmnalytical*
www.pscefab&=
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SNI-Charlotte, NC
Pace Project No.: 92330158
Pace Analydcal Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28070
[phone]
Lab ID
Sample ID
QC Batch Method
Analytical
QC Batch Analytical Method Batch
92330158001
SP-1
EPA166413
350071
92330158002
SP-2
EPA 1664B
350071
92330158003
SP-3
EPA 1664B
350071
92330158004
SP4
EPA 1664B
350071
92330158005
SP-5
EPA 1664B
350071
92330158006
SP-6
EPA 1664B
350071
92330158001
SP-1
SM 2540D
348957
92330158002
SP-2
SM 2540D
348957
92330150003
SP-3
SM 2540D
348957
92330158004
SP-4
SM 2540D
348957
92330158005
SP-5
SM 2540D
348957
92330158006
SP-6
SM 2540D
348957
92330158001
SP-1
EPA 9040
348512
92330158002
SP-2
EPA 9040
348512
92330158003
SP-3
EPA 9040
348512
92330158004
SP-4
EPA 9040
348512
92330158005
SP-5
EPA 9040
348512
92330158006
SP-6
EPA 9040
348512
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 02/28/2017 03:05 PM without the written consent of Pace Analytical Services, LLC. Page 10 Of 13

Document Name:
Document Revised: Sept. 21, 2016
lCal
Sample Condition Upon Recei t SCUR
Page 1 of 2
Document No.:
Issuing Authority:
aCeAIIaI
F-CAR-CS-033-Rev.01
Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville 0� Raleigh[] Mechanicsville[]
Client Name: � Wp#� 92330158
� Project#:` � ji
Fx Client
Commercial Qace UPS ❑0 her; 0
�� 7330188 1
Custody Seal Present? ❑Yes [2Na Seals Intact? ElYes [:]No i
� Data/Initials Person Examining Contents: kJ
Packing Material: []Bubble Wrap Bags ❑None ❑Other:
Thermometer:
❑ IR Gun 10: M_ Type o Ica: Qw t ❑Blue ❑None ©6 mples on Ice, cooling process has begun
Correction Factor: Cooler temp Corrected ('CI: Biological. Tissue Frozen? ❑Yes ❑NO [IN/1(
Temp should be above free Trig to 6'C
USDA Regulated Soil ( 7/A, water sample)
Did samples or ginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Int©p_olonaliy,
❑Yes ❑ o IncludlnR Hawaii and Puerto Rico)? ❑Yes o
Chain of
Samples
Rue) Turn Around Time Requested?
Oyes
N6'�
N A
4,
SuffidentVolume?'
DY9
QNo
N/A
S.
Correct Containers Used?
ess
❑No
❑N/A
6.
-Pace Containers Used?
Yes
QN.
N A
Containers Intact?
Yes
QN.
N/A
7.
Samples -Field Filtered?
Dyes
nNa
H' a
S. Note if sediment Is visible In the dissolved container • --
j Sample Labels Match COC?
❑Yes
❑Na
❑N/A
0Aoe_ p =5=7 Qo TSKc e A r
-Includes DateMme/ID Anal sis Matrix:
Heads ace In VOA Vials >5-6mm)?
Dyes
J3No
43QA
10.
Trip Blank Present?
❑Yes
©No
(]N/A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Date/Time:
Field Data Required? ❑Yes ❑No
Project Manager SCURF Review-,u! i Date: _ IL5_1%_1"
Project Manager SRF Review: Date,. 2 7
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, Incorrect preservative, out of temp, Incorrect containers)
Page 11 of 13

m
m
N
O
■■■■■■■■■■■■■
R . . r
MMMMMPV
■■■■■■■■■■■■
i ■
4l
W

M
CHAIN -OF -CUSTODY I Analytical Request Document
" The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section a Sectierl C
Required Client Irdorrrunkirv. Requavd Project htlonllatlon: hrraice kdorrnatiorc patie
C—pary. SarleiCer Nat=ml Report To- Tana Case Auer==
Address: 2420 Slarna Roan Copy To: Canpmy Name:
Ctarlaue. NC 211269
'
Email' .cprrl
Purchase Orders.
Pace Owe:
Phone, (764►599.7433 IF.
Prop=Nana: SNI.Cherlotte.NC
paw Prgera mwkvw nimte. paeelabs.0wsk
StateILocation _
Requgted Due Data:
P""a a.
Pace Prae9e a: 2631.1
NC
Fherrd
,
in
�Tj
MTs>x CODE
-'
COLLECTED
Z
Preservatives
-
M'
0'" wad ow
u
°
was wr
8
"r
wb� was w w
SAMPLE ID � P
<
o
s
U
ti
v
g
04 a
One Character per fibx ws. wP
._.
w
START
END
n
a
a
R
t_A-7, 0-9 1. _} o�a�r AR
o
S`
F
o
in
W
C�' idsmust heWugrp T_ TS
rc
W
W
O
S
c
.d
v
�tZ�301 g
�
a
o
w
z
�
a
t
`a
W
DATE
TDdE
DATE
TIME
a
r
,
s
x
x
z
X
O
_� .
O
i-
o
11
sP.t
r
In
,�
x
x
x
00 k
r
.- 2 L
SP•2 l i
WT
t✓r
r '' j
i0 `il
x
x
x
oo z
34�
S" lc�
NIT
o.
x
x
x
003
'
P a
I
C(D
4i
SPA
a
VVT
! J
x
x
x
I
5:
SP,S
VVY
t3
x
x
x
m57
6
SPA
WT
1
1
x
x
x
i
I
I
ago
S �'S
9H*1
10.
=:11.
12 .
LL
- 'BYI AF'fYI�:ION! �4�
OASE. u
+ter 7nrE
"='- ACG�iI�rIY IAFF:JADOFI t =
•-DATE.'
T:EE
�S�IiPLE Ol11m17i0N0
T.5 .Y
�...�.
L3
L
T\---)
v
i
SAYPLERNAMImANGSICaNATURE-;�'i'sr'�`u-
-('iiO!'6i.$I♦JIPL♦riF:
C
c
w
: z
a
+ $ _ZA
SIGMTURE of SAMPLER DATE SiyneA: `
s
r
C.
w U}

la'ceAnalyfical
www.peafebacae
December 19, 2016
Mr. Michael DeBraske
Schneider National, Inc.
PO Box 2545
Green Bay, WI 543062545
RE: Project: SNI-Charlotte, NC
Pace Project No.: 92322177
1� C' Q � � �� Pace Analytical Services, LLC
1 L Y / 9800 KinceyAve. Suite 100
Hunteraville, NC 2BG78
(704)8759092
RECEIVED
��N. 17 Z017
CENTRAL
WRR ECTION
Dear Mr. DeBraske:
Enclosed are the analytical results for sample(s) received by the laboratory on December 06, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
Enclosures
cc: Mr. Michael DeBraske, GEI Consultants, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 14

aceAnalytical`
Wmiommucom
Project: SNI-Charlotte, NC
Pace Project No.: 92322177
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kinsey Ave. Ste 100, Huntersvil le, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FloridafNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification M 84
Vlrginia/VEIAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Vlrginia/VEIAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 14

laceAnalyticalo
WWWpaceotcom
SAMPLE ANALYTE COUNT
Project: SNI-Charlotte, NC
Pace Project No.: 92322177
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Semple ID
Method
Analysts
Analysts
Reported
Laboratory
92322177001
SP-1
EPA 1664B
JMS
1
PASI-C
SM 2540D
MLS
1
PASI-A
EPA 9040
MLS
1
PASi-A
92322177002
SP-2 '
EPA 1664B
JMS
1
PASI-C
SM 2540D
MLS
1
PASI-A
EPA 9040
MLS
1
PASI-A
92322177003
SP-3
EPA 1664E
JMS
1
PASI-C
SM 2540D
MLS
1
PASI-A
EPA 9040
MLS
1
PASI-A
923221770"
SP-4
EPA 1664B
JMS
1
PASI-C
SM 2540D
MLS
1
PASI-A
EPA 9040
MLS
1
PASI-A
92322177005
SP-5
EPA 1664E
JMS
1
PASI-C
SM 2540D
MLS
1
PASI-A
EPA 9040
MLS
1
PASI-A
92322177006
SP-6
EPA 1664E
JMS
1
PASI-C
SM 2540D
MLS
1
PASI-A
EPA 9040
MLS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 3 of 14

la'c ie A na /y fical
www.pac*b&CcM
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92322177
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Sample: SP-1
Parameters
Lab ID: 92322177001 Collected: 12/06/16 10:00
Results Units Report Limit DF
Received: 12106/1614:10 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mglL
5.0 1
12/19/16 07:42
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
259 mg1L
16.7 1
12/12/16 11:11
9040 pH
Analytical Method: EPA 9040
pH
7.1 Std. Units
0.10 1
12/12/16 12:23 H6
Sample: SP-2
Lab ID: 92322177002 Collected: 12/06/16 10:00
Received:
12/06/16 14:10 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg1L
5.0
1
12/19/16 0TA2
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
155 mg1L
16.7
1
12/12/16 11:11
9040 pH
Analytical Method: EPA 9040
pH
6.9 Std, Units
0.10
1
12/12116 12:23 H6
Sample: SP-3
Lab ID: 92322177003 Collected: 12/06/16 10:00
Received:
12/06/16 14:10 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L
5.0
1
12119M6 07:43
25400 Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
248 mg1L
16.7
1
12/12/16 11:12
9040 pH
Analytical Method: EPA 9040
pH
6.9 Std. Units
0.10
1
12/12/16 12:23 H6
Sample: SP-4 Lab ID: 9232217TO04 Collected: 12/06/16 10:00 Received: 12/06/16 14:10 Matrix; Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16648
Oil and Grease ND mg1L 5.0 1 12/19/16 07:44
Dale: 112/19/2016 03:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 14

aceArralytical e
wwr.POGWD&Corn
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92322177
Pace Analytical Services, LLC
9800 Klncey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
Sample: SP-4
Lab ID: 92322177004 Collected: 12/06/16 10:00
Received:
12/06/16 14:10 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared
Analyzed CAS No.
Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
245 mg1L
16.7
1
12/12/16 11:12
9040 pH
Analytical Method: EPA 9040
PH
6.9 Std. Units
0.10
1
12/12/16 12:23
H6
Sample: SP-5
Lab ID: 92322177005 Collected: 12/06/10 10:00
Received:
12/06116 14: 10 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared
Analyzed GAS No.
Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg1L
5.0
1
12/19/16 07:44
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
74.6 mg/L
14.8
1
12/12/16 13:05
06
9040 pH
Analytical Method: EPA 9040
PH
6.7 Std. Units
0.10
1
12/12/16 12:23
H6
Sample: SP•6
Lab ID: 92322177006 Collected: 12/0611610:00
Received:
12/06/16 14:10 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared
Analyzed CAS No.
Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mg1L
5.0
1
12/19/16 07:45
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
159 mg1L
25.0
1
12/12/16 13:06
9040 pH
Analytical Method: EPA 9040
PH
7.2 Std. Units
0.10
1
12/12/16 12:23
H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/19/2016 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 14

aceAnalytical.
rrrm.Paoefebscom
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92322177
QC Batch: 341435 Analysis Method: EPA 16648
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92322177001, 92322177002, 92322177003, 92322177004, 92322177005, 92322177006
METHOD BLANK: 1894518 Matrix: Water
Associated Lab Samples: 92322177001, 92322177002, 92322177003, 92322177004, 92322177005, 92322177006
Blank Reporting
Parameter Units Result limit Analyzed Qualifiers
Oil and Grease mg1L ND 5.0 12/19/16 07:33
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersvllle, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 1894519 1894520
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Oil and Grease mglL 40 35.8 35.7 90 89 78-114 0 30
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 12/19/2016 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 14

aceAnalytical to
www.pagela6s.com
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92322177
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
QC Batch: 340332
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92322177001, 92322177002, 92322177003, 92322177004
METHOD BLANK: 1887729
Matrix: Water
Associated Lab Samples: 92322177001, 92322177002, 92322177003, 92322177004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 12/12/16 11:00
LABORATORY CONTROL SAMPLE:
1887730
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
- mg/L
250 248
99 90-110
SAMPLE DUPLICATE: 1887731
92322027001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L ND ND
SAMPLE DUPLICATE: 1887732
92322075002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 22.2 14.2 44 D6
Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 12119/2016 03:04 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14

laceAnalytical
www.psowftcom
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92322177
QC Batch: 340333 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92322177005, 92322177006
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1887733
Matrix: Water
Associated Lab Samples: 92322177005,
92322177006
Blank Reporting
Parameter
Units
Result Llmit
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND 2.5
12/12/16 12:59
LABORATORY CONTROL SAMPLE:
1887734
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 252
101 90-110
SAMPLE DUPLICATE: 1887735
92322177005
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg1L
74.6
88.8 17 D6
SAMPLE DUPLICATE: 1887736
92322225003
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Sollds
mg/L
ND
ND
Resufts presented on this paps are In the unit Indicated by the "Units' column except where an alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except In full,
Date: 12/19/2016 03:04 PM without the written consent of Pace Analytical Services, I.I.C.
Page 8 of 14

aceAnalytical "
www.Pece OUcom
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92322177
QC Batch: 340391 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92322177001, 92322177002, 92322177003, 92322177004, 92322177005, 92322177006
SAMPLE DUPLICATE: 1887921
92322039001 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 7.3 7.3 0 H6
SAMPLE DUPLICATE: 1887922
92322097001 Dup
Parameter Units Result Result RPD Qualifiers
pH Sid. Units 6.3 6.3 0 H6
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an altemats unit Is presented to the right of the resuiL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/19/2016 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 14

aceAnaiyiical
aww.peaetabicom
QUALIFIERS
Project: SNI-Charlotte, NC
Pace Project No.: 92322177
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersvilie, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyle is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether,
A separate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis of Acroleln and Acrylonitrile by EPA
Method 8260.
N-Nitrosodlphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/19/2016 03:04 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

aceAnalytical e
%WWp80W8b8.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suke 100
Huntersville, NC 28078
[phone]
Project: SNI-Charlotte, NC
Pace Project No.: 92322177
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92322177001
SIP-1
EPA1664B
341435
92322177002
SP-2
EPA1664B
341435
92322177003
SP-3
EPA 1664B
341435
92322177004
SP-4
EPA1664B
341435
92322177005
SP-5
EPA1664B
341435
92322177006
SP-6
EPA1664B
341435
92322177001
Sp-1
SM 2540D
340332
92322177002
SP-2
SM 2540D
340332
92322177003
SP-3
SM 2540D
340332
92322177004
SP-4
SM 2540D
340332
92322177005
SP-5
SM 2540D
340333
92322177006
SP-6
SM 2540D
340333
92322177001
SPA
EPA 9040
340391
92322177002
SP-2
EPA 9040
340391
92322177003
SP-3
EPA 9040
340391
92322177004
SP-4
EPA 9040
340391
92322177005
513-5
EPA 9040
340391
92322177006
SP-6
EPA 9040
340391
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 12/19/2016 03:04 PM without the written consent of Pace Analytical Services, LLC.
Page t i of 14

'
Document Name:
Document Revised: Sept. 21, 2016
Sample Condition Upon Recei t SCUR
Page 1 of 2
Document No.:
Issuing Authority:
��aceAnaljft,71
F-CAR-CS-033-Rev.41
Pace Quallq Office -
Laboratory receiving samples;
Asheville ❑ Eden[:] Greenwood ❑ Huntersville Raleigh[] Mechanicsville[]
Client Name: Project W0# : 92322177
II
'Courier: Fed Ex OUPS OUSK LiClientIN I'��I 111111
❑ Commercial Q c ❑Other: 92322177
Custody Seal Present? Dyes �00 Seals intact? Dyes %lo
�j Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap c aubble Bags ❑None ❑Other:
Thermomete
Gun ID: �_ pe f Ice: et ❑Blue []None-�amples orrice, cooling process has begun
Correction Factor: Cooler Temp Corrected (•C): Biological Tissue Frozen? Dyes �& []N/A
Temp should be above &fApzlng to 6'C
USDA Regulated Soil ( I/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
r 1Yes,o indudinrr Hawaii and Puerto Rico)? ❑Yes t❑fQjf
I Chain of Custodv Present? of nVn f 'INo 11NYA 1 1. 1
Short Hold Time Analysis 1<72 hi.)?
Dyes
o
N A
3.
Rush Turn Around Time Requested?
Dyes
N A
4.
5.
Sufficient Volume?' Subs QNO N A
Correct Containers Used?
-Pace Containers Used?
.4es
es
❑No
ONO
❑N/A
N A
6.
7.
Containers Intact? rs No N A
Samples Field Filtered?
Yea
Q No .
A
8. Note If sediment is visible in the dissolved container • .
Sample labels Match COC?
-Includes Date/Time/lD/Anal sis Matrix:
I&s
❑Na
❑N/A
9.
Heads ace in VOA Vials >5.6mm ?
QYes
ONo
IQ A
10.
Trip Blank Present?
❑Yes
A o
❑N/A 1
11. _ - .
CLIENT NOTIFICATION/RESOLUTION Field Data Required? []Yes []No
Person Contacted: Dategime:
Comments/Sample
Discrepancy:
Project Manager SCURF Review: t; Date:
Project Manager SRF Review: _ r v{z� _ Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office the.
Out of hold, Incorrect preservative, out of temp, Incorrect Containers)
Page 12 of 14

Document Name:
- a Sam le Condition Upon Recel
aceAnalytical Document No.:
F-CAR-CS-033-Rev.01
*Check mark top half of box if pH and/or dechlorination
Is verified and within the acceptance range for
preservation samples.
"Bottom half of box is to list number of bottles
Document Revised: Sept. 21, 2016
)t SCUR Page 2 of 2-
issuing Authority:
Pace Quality Office
Project; Wp# : 92322177
PM: NMG - Due Date: 12/20/16
CLIENT: 82-SCHNEIVER
pH Adjustment
Log for Preserved Samples
Sample iD
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Page 13 of 14

I
�=- CHAIN -OF -CUSTODY I Analytical Request Document a
f The Chain -of -Custody is a LEGAL DOCUMENT. AD relevant fps must be.completed accurately.
Section A - Section B Section C I{I J
RegWnd Cuenn Irdormatian: Requited Project imormadw: Invoice Wonnatioru I - Page : ( t Of 1
Cw4-V Sduneider Nabmiat
Report To: Cene Cara
l
2420 Stw" Rand
Copy To:
Campamy Name: j
CAarioft NC2t12t6
r:_ 'ti•: cti ;; i. :•!�
- - -
Entail .cam
Purdlaw Order N:
Pace Chow �
704j599-7413 Far
prdea Name SNi-CharkMe. NC
P— Prci- lanape< Hire.. .mm•
Requested Due Date:
Pmjnct 0.
Para PraCde a; 2631-1 i
NC
I:-
'Requested
Filtered
rM,,,'
Wreec CODE
8
c0i
COLLECTED
s
Presefvalives
- -
0." wear 06V
p
iL
a
9
wMe WT
wsa.w.a, VVW
.2
0
SAMPLE ID od
a
START
END
4
a
t71Y t.11ifaGrer par t101L A. wP
tA'Zr 0-9 t
r
W
g0— or
6e �
" iK.f rPrlSt Mh Te
8
Y
m
w
c
r
A
7
.p
O
=
c
n
2
[7
0
c
-
A
DATE
TPAE
DATE
Tp1E
.
r
x
x
z
z
O
i
O
r
n
x
SP-t Q r V
wT
/,
x
x
x
Q
2 �;
SP-2 p 1 40
-T
x
x
x
oa
v
rp
SP-3 TI
wT
a b
x
x
x
wT
ra-
x
x
x
' s
SP-s tLf�
wT
i�'
x
x
x
5
_� �
>fi�'
sPa
wr
1a_
x
x
x
e
� _9
�7:�V::;.`r�^�.•AOt7r11Pa11tL'GO?tl1�rTS'� y., �:.k
-��. � •
CS
".�'•� �:OY./AF'FiL.IAiION +T`.'i�`
`
�"74AE �•
,4 •.: Tom;,
�}'` AGt
$TI
%J�.IA71oliF-`�"�
-
-•-.
4
r�_6� 1E
:�,w��,-
7�,.y
w '{'SAMPLE
-
cOKCIrio0t6
��•• -v-�
�viYT ;�cr
'-+.a:�z"r1:e_.=k �. r'=.,r.:. �xa�=-.+r-r-ss,�.c n.
i;'_»� �»�A*--.:-vi:R•'L:.-�cD�:.�,Fc"'-r�C..
F
Hx7'a%E<.-
-�:r�r-r_•�
:s�Lrw-' �,
.4.'�4��'�7•z-�.���.i�ax^r7aL�.3��',.`�'�-_
.4.t_ -.�
�
T_=-L:c.�.�
.#`1...X�..ac_�.aSat=r.�r,..isl+=�•r�'
r
1
z ,ZT. z..�
.
PRW Napa W
I
a
rL 1.
U t
:
SM"TURE of SWPLFR: DATE Signed:2
Go S
��

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCGO80000 t] b 9 SAMPLES COLLECTED DURING CALENDAR YEAR: 7r.�l Lo
CERTIFICATE OF COVERAGE NO. NCG08 0060Ck (This monitoring report is due at the Division no later than 30 days from
th�t Mg&�es the s ling results from the laboratory.)
FACILITY NAME SC
PERSON COLLECTING SAMPLES C- QU UnQQ T PHONE NO. Cg2Q 1 5q 0 -
CERTIFIEED LABORATORY Lab # DEC 0 5 2016
Lab # PLEASE SIGN ON THE REVERSE 4
CENTRAL FILES
Part A: Vehicle Maintenance Areas Monitoring Requirements DWR SECTION
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? X yes _no
(if yes, report your analytical results in the table immediately below)
Outfall
No.
Date�,
Sample CoQected,
mold
I10556� r s; "s
Total: Suspended S6LdspH,
xt
;Standard=units. . ,s
90d and'Grease,
„ . :. Yr... _,.
New MotorOilUsage,
Annua4avera e, allino. ,
Benchmark
-
100
Within 610 29:0.
Note: if you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
Outfall
No.
Date
Sample`Collected,
mo/ddlYe
'.: o055b*'f
0.00530.. _.s. _SA'
�`00400 :x
Oil and.Grease,
%T6611SuspendedlSolids,
t.5 +" '
pH, _
�5tanda dunitsr�'
Permit Limit
_ 30_=
to°s100ck'
abAr=9'0.
STORM EVENT CHARACTERISTICS:
Date « i30 (first event sampled)
Total Event Precipitation (inches): 11D LO
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
SWU-250-102107
Page 1 of 2

"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
(5ignatu of Permittee) 0
W 61 /Ito
(Date)
SWU-250-1021 a7
Page 2 of 2

0. ­�- �- 0
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCGO80000
Date submitted
CERTIFICATE OF COVERAGE NO. N0008 5 1 V
FACILITY NAME i 1�'�e —
COUNTY
PERSON COLLECTING SAMPLES
LABORATORY Lab Cert. #
Comments on sample collection or analysis:
Part A: Vehicle Maintenance Areas Monitoring Requirements
SAMPLE COLLECTION YEAR
SAMPLE PERIOD ❑ Jan June ❑ July -Dec
or ❑ Monthly' month
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
RECEIVED ero-flow Water Supply []SA
RECEIVED Cp[]water
JAN 3 0 2017
CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE 4
DVVR SECTION W ivo discharge this period'
Outfall
No:a_­�
Lj ' j'_: .
Date
=iSarnple Collected,
�i'&r, r o/cld7yr.
'00SW
00400
00556
Total Suspended
Solids„rrtg/l,
pH,
Standard units
Non -Polar Oil and Grease/TPH EPA
Method:1664:(SGT_HE1VI), mg%L
New Motor Oil Usage,
Annual average gal/ma
Benciirnarki
_-.
SOor100 see permit
Within 6:0 - 9.0
15
-
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no
(if yes, report your analytical results in the table immediately below)
Part S. Oil/water Separators and Secondary Containment Areas at Petroleum Sulk Stations and Terminals
. "Outfal! . _
No.
k �_.Z-�'.
Mate.'_ -
Sarriple [ollidbd,l�
_mojdT%yr z- �l
'-- 00556
00530
00400
. Non=Polar Oil and.Giease/TPH'EPA Method
_ � 165�r{kG HEiVi);�fk%Li-R`' �1'
Total Suspended Solids,
pH,
5tandardguttits
Per€rtii L'irhlt
._ i
- - , �
=�_ ' ;1�5,
50"or 100 seeio efiit..
6.0 - 9.0
For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised October 25, 2012

STORM EVENT CHARACTERISTICS:
Date (first event sampled)
Total Event Precipitation (inches): _
Date (list each additional event sampled this reporting period, and rainfall amount)
R Total Event Precipitation (inches):
Note: If *u report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
0 A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION e.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an orl inal and one copy -of this DM1R lnclud n all "No Discharge' reports,within 30 days of r cei t o the lab results or at end a mQnitorin period in
the case of "No Disrhgrcre"_reports�to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
t Raleigh, North Carolina 27699-1617
'YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
CAP '7
r-
(Signature of Permittee) (bate)
Additional copies of this form may be downloaded at:.httR://portaLncdenr.org/webLwq/wsLsu/npdessw#tab4
SWU-250 last revised October 25, 2012
Pam 2 of 2

(�Ia'cmnalytical*
wrwwooft oom
October 19, 2016
Mr. Michael DeBraske
Schneider National, Inc.
PO Box 2545
Green Bay, WI 543062545
RE: Project: SNI-Charlotte, NC
Pace Project No.: 92315307
REC'EI VED
OCT 3 r 2016
CENTRAL FILES
DWR SEC7.10N
Pace Analytical Services, LLC
9600 KlnceyAve, Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. DeBraske:
Enclosed are the analytical results for sample(s) received by the laboratory on October 07, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
Enclosures
cc: Mr. Michael DeBraske, GEI Consultants, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 14

(�aneAnalyticalo
rwvw.pewl4�bi com
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: SNI-Charlotte, NC
Pace Project No.: 92315307
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification M 37706
FloddalNELAP Certification #: E87627
North Carolina Field Services Certlfication #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Mrglnia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification M 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 14

aceAnaly ical e
wwwpeafaba.oxn
SAMPLE ANALYTE COUNT
Project: SNI-Charlotte, NC
Pace Project No.: 92315307
Pace Analytical Services, LLC
9800 Kincey Ave, Sulte 100
Hunlersville, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92315307001
#1 Outfall
EPA1664B
JMS
1
PASI-C
SM 2540D
MLS
1
PASI-A
EPA 9040
ALC
1
PASI-A
92315307002
#2 Outfall
EPA 1664B
JMS
1
PASI-C
SM 2540D
MLS
1
PASI-A
EPA 9040
ALC
1
PASI-A
92315307003
03 Outfall
EPA 1664B
JMS
1
PASI-C
SM 2540D
MJ51
1
PASI-A
EPA 9040
ALC
1
PASI-A
92315307004
04 Outfall
EPA 1664E
JMS
1
PASI-C
SM 2540D
MJS1
1
PASI-A
EPA 9040
ALC
1
PASI-A
92315307005
#5 Outfall
EPA 1664B
.iM3
1
PASI-C
SM 2540D
MJ31
1
PASI-A
EPA 9040
ALC
1
PASI-A
92315307006
#6 Outfall
EPA1664B
JMS
1
PASI-C
SM 2540D
MJS1
1
PASI-A
EPA9040
ALC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 14

(�IaceAnalyfical*
www.pecalebtcom
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92315307
Pace Analytical services, I_LC
9800 Kincey Ave. Suite 100
Hunterevllle, NC 28078
[phone]
Sample: #1 Outfall
Lab ID: 92315307001 Collected: 10/07/16 10:10
Received: 10/07/16 13:00 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
8.3 mg1L
5.0
1
10/19/16 08:30
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
423 mg1L
16.7
1
10/12/16 13:28
9040 pH
Analytical Method: EPA 9040
pH
7.7 Std. Units
0.10
1
10/17/16 15:13 H6
Sample: #2 Outfall Lab ID: 92315307002 Collected: 10/07/16 10:20 Received: 10/07/16 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
12.8 mglL
5.0
1
10/19/16 08:30
2540D Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
894 mglL
50.0
1
10/12/16 13:28
9040 pH
Analytical Method: EPA 9040
pH
7.6 Std, Units
0.10
1
10/17/16 15:13 H6
Sample: #3 Outfall
Lab ID: 92315307003 Collected: 10107M6 10:35
Received: 10/07/16 13:00 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Clual
HEM, Oil and Grease
Analytical Method: EPA 16048
Oil and Grease
15.2 mglL
5.0
1
10/19/16 08:30
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
519 mglL
33.3
1
10/12116 18:05
9040 pH
Analytical Method: EPA 9040
pH
7.5 Std, Units
0.10
1
10/17/16 15:13 H6
Sample: #4 Outfall Lab ID: 92315307004 Collected: 10/07/16 10:50 Received: 10/07/16 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease 9.7 mglL 5.0 1 10/19/16 08:30
Date: 10/19/2016 03:35 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Ll-C.
Page 4 of 14

(�Ia'aeAnalyfical*
wwwpeWMbamm
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92315307
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
(704)875r9092
Sample: #4 Outfall Lab ID: 92315307004 Collected: 10/07/16 10:50 Received: 10/07/16 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 542 mg1L 25.0 1 10/12/16 18:05
9040 pH Analytical Method: EPA 9040
pH 7.7 Sid. Units 0.10 1 10/17/16 15:13 H6
Sample: #5 Outfall Lab ID: 92315307005 Collected: 10/07/16 10:50 Received: 10107116 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease 13.6 mg/L 5.0 1 10/19/16 08:30
25400 Total Suspended Solids Analytical Method: SM 25400
Total Suspended Solids 944 mg1L 25.0 1 10/12/16 18:06
9040 pH Analytical Method: EPA 9040
pH 7.6 - Sid. Units 0.10 1 10/17/16 15:13 H6
Sample: #6 Outfall
Lab 1D: 92315307006 Collected: 10/07/16 11:10
Received: 10/07116 13:00 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
18.1 mg1L
5.0
1
10/19/16 08:30
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
660 'mg1L
25.0
1
10/12/16 18:06
9040 pH
Analytical Method: EPA 9640
pH
6.9 Sid. Units
0.10
1
10/17/16 15:13 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1011912016 03:35 PM without the written consent of Pace Analytical Services, LLC,
Page 5 of 14

(�Ia'oeAnalyficale
wwwPaceAtbacom
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92315307
QC Batch: 333689 Analysis Method: EPA 1664E
OC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92315307001, 92315307002, 92315307003, 92315307004, 92315307005, 92315307006
ME THOD BLANK: 1849195 Matrix: Water
Associated Lab Samples: 92315307001, 92315307002, 92315307003, 92315307004, 92315307005, 92315307006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mglL ND 5.0 10/19/16 08:30
LABORATORY CONTROL SAMPLE: 1849196
Parameter Units
Oil and Grease mg1L
Pace Analytical Services, LLC
9000 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec '
Conc. Result % Rec • Limits Qualifiers
40 37.5 94 . 78-114
MATRIX SPIKE SAMPLE: 1849197
92315432002 Spike MS MS % Rec
Parameter Units Result Conc• Result % Rec Limits Qualifiers
Oil and Grease mg1L ND 40 36.1 90 78-114
Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/19/2016 03:35 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 14

'eAnalXical*c
rnvw.paoefeUMM
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92315307
QC Batch: 332687 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92315307001, 92315307002
METHOD BLANK: 1843631 Matrix: Water
Associated Lab Samples: 92315307001, 92315307002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 10/12/16 13:21
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1843632
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 246 98 90-110
SAMPLE DUPLICATE: 1843633
92315396001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL 262 258 2
SAMPLE DUPLICATE: 1843634
92315393005 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mglL ND ND
Results presented on this page are in the units Indicated by the'UnitC Column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2010 03:35 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 14

,IRCalytical "
www.pacefaCs.com
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92315307
QC Batch: 332888 Analysis Method: SM 25400
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92315307003, 92315307004, 92315307005, 92315307006
METHOD BLANK: 1844772 Matrix: Water
Associated Lab Samples: 92315307003, 92315307004, 92315307005, 92315307006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mglL NO 2.5 10l12118 18:04
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 2907E
[phone]
LABORATORY CONTROL SAMPLE: 1844773
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 228 91 9D-110
SAMPLE DUPLICATE: 1844774
92315307003 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 519 512 1
SAMPLE DUPLICATE: 1844775
92315341004 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L NO NO
Results presented on this page are In the units Indicated by the "Units" column except where an aitemato unit is presented to the right of the resutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2016 03:35 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 14

(�Ia'cieAnalydcale`
wew.pacakos.mm
QUALITY CONTROL DATA
Project: 5NI-Charlotte, NG
Pace Project No.: 92315307
QC Batch: 333423 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92315307001, 92315307002, 92315307003, 92315307004, 92315307005, 92315307006
SAMPLE DUPLICATE: 1847788
92315235001 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 7.1 7.2 1 H6
SAMPLE DUPLICATE: 1847789
Parameter
pH
92315307006 Dup
Units Result Result
Std. Units 6.9 7.0
RPD Qualifiers
0 H6
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Hunteraville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except whore an ilteroats unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2016 03:35 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
aceAnalXical Huntersvllle, NC 28078
www.pet labsoom [phone]
QUALIFIERS
Project: SNI-Charlotte, NC
Pace Project No.: 92315307
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estlmated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 Is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodlphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
HIS Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/19/2016 03:35 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

aceAnaljftal
welr.Pacefaftcom
Project: SNI-Charlotte, NC
Pace Project No.: 92315307
Lab ID Sample ID
92315307001
#10utfall
92315307002
#2
Outfall
92315307003
#3
Outfall
92315307004
44
Outfall
92315307005
#5
Outfall
92315307006
#6
Outfall
92315307001
#10utfall
92315307002
#2
Outfall
92315307003
#3
Outfall
92315307004
#4
Outfall
92315307005
#5
Outfall
92315307006
#6
Outfall
92315307001
#1Outfall
92315307002
#2
Outfall
92315307003
#3
Outfall
92315307004
#4
Outfall
92315307005
#5
Outfall
92315307006
#6
Outfall
Date: 10/19/2016 03:35 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
QC Batch Method QC Batch Analytical Method
EPA1664B
333889
EPA1664B
333689
EPA1004B
333689
EPA1664B
333689
EPA 1664E
333889
EPA 1664B
333689
SM 2540D
332687
SM 2540D
332687
SM 2540D
332888
SM 2540D
332688
SM 2540D
332888
SM 2540D
332888
EPA 9040
333423
EPA 9040
333423
EPA 9040
333423
EPA 9040
333423
EPA 9040
333423
EPA 9040
333423
REPORT OF LABORATORY ANALYSIS
This report small not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 11 of 14

Document Name:
Document Revised: Sept. 21, 2016
a����,11�.
r'
Sample Condition Upon Recei t SCUR
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.00
Pace Quall Office
W®# . ��� Page 2 of 2 for Internal Use ONLY
Cllen ame: 1530?
Project #.
Courier: F dEx UPS- LISPS -[]Client 1 11111 111111111111111
i 0231 1
❑ commercial [ace ❑Other. @7
Custody Seal Present? Dyes I23No Seals Intact? ❑Yes []No ��
Date/initials Peron Examining Cont�htli11ba „_,
Packing Material: []Bubble Wrap [Rubble Sags []None []Other:
Thermometer:
124et ❑Blue ❑None PSarrfples on ice, cooling process has begun
❑ IR Gun ID: `T15d5 a of Ice:
Correction Factor: Cooler Temp Corrected 1'C): nj Biological Tissue Frozen? ❑Yes El No E2K/A
Temp should be above freezing to 6'C J
USDA Regulated Soil ( Q N/A, water sample)
Did samples originate! a quarantine tone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
1711rac rlNn Indudlna Hawall and Puerto ilral? 171Yes r INo
Comments Discre an :
Chain of Custody Present?
f7l<ex
CINO
N A
1.
Samples Arrived within Hold Time?
QNo
omlA
2.
Short Bold Time Analysis s72 hr.)?
Dyes
No
N A
3.
Rush Turn Around Time Requested?
Yes
QKa
N A
4.
Sufficient Volume?
es
No
N A
S.
Correct Containers Used?
jdfes
[:]NO
❑N/A
6.
-Pace Containers Used?
Yes
nNo
N/A
Containers Intact?
eyes
No
N A
.7.
Samples Field Filtered?
QYes
No
A
B. Note If sediment Is visible In the dissolved co taine
Sample Labels Match COC?
©Yes
Mdo
❑N/A
9. 0 >Oj
-includes Date/nme/ID/Anal sis Matrix:
' C
All containers needing acid/base have been
documented SCURF?
Checked and on page two of
QYes
❑No
/A
I�
111D
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015�
(water) DOC, LLHg
11.
Samples checked for dechlorination? MYes QN0 A
Heads ace in VOA Vials >5.6mm 7
OYes
Q No
A
12.
Trip Blank Present?
[]Yes
ONO
13.
Trip Blank Custody Seals Present?
Dyes
❑No
/�/A
❑N/A
Pace Trip Blank Lot p if purchased):
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Date/Time:
Field Data Required? []Yes []No
Project Manager SCURF Review: 14 MU Date: (i71�\0
Project Manager SRF Review: Vac, Date: lo
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, Incorrect preservative, out of temp, Incorrect containers)
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Ralelgh❑ Mechanicsville[]
Page 12 of 14

CBAl1c'1lyhCai
Section A
RmpArad Client 6rfornwU m:
e r—
T fpa /1a.c. r.
Section B
Required Rojas tr k-na>wL
Report To:
% Copt, To: �J
(D9
Pradrase 0rdw No.:
Rdied Name: c . % -
CHAIN -OF -CUSTODY I Analytical Request Document
The Chwi of -Custody is a LEGAL DOCUMENT. AN relevwd melds must be mrpleted amuraWy.
Section C Page. at
� : 2069485
Kowa" Name: �
secow D Mai: codes
a
urm*,eson e�AT�lx r coos
Dm*uv Warr Dw
COLLECTED
o
water wT
waste wow ww
Prodtas P
s
Compeam
w
SaYSCGd SL
SAMPLE ID Co C
5
�
U
(A-Z M I.-) Air AR
a
G
0
W
SMVIO IDS M UST aE UNIQUE rasue TS
Outer OT
o
U
�:
a
z
>t
F
X
Iu
w
U
DATE
I TIME
DATE
TIME
a
2
4i4
10-7M/o,-716;
5
c I '7:
!o'7
0
n
REGULATORY AGEN
r KPDES r- GROUNDWATER F DRINKING WATER
I- UST r RCRA r OTHER
14C4 G 1 .Q Sits Location
STATE:
ftqumWd Anaysis I:Lfered (YIN)
z
Preservatives
y
m
n
U
m
Q r1-3 ! 5 3d`l
a
w Pace Proiect Nor Lab L.D.
AODITIWIAL G3011E31T5 RELOCA2 SHIM BY r AFFnAATION DATE TIME ACCEPTED BY r AFMIATM DATE THEE SAMPLE CONDn 10"
b-7 13a�1 - a 7 3uv
A -7 I I3Sy t4-VIY1, —,rnAA In17(!<< 1-�Stl S.9
SAMPLER NAILS AND SJGNATIM
ORIGINAL
PRIM Name of SAMPLE
SIGNATURE of SAhWtFJ :
n
U
`o
Z
n a
m
z
E
"4aporLmi NoW ay .Fna era A" yw Pam NET 3a Cap peymml lenm wW ag� m Ins dmges d l.M pm at O for my IrrUtIeCD ndl paid wClfin 30 OUM
F-ALL-O-020rev.R7. tS•May2W7

.°� CHAIN -OF -CUSTODY I Analytical Request Document
The Chah-of-Custody is a LEGAL DOCUMENT. All relevant fields must be Completed accurately.
5ec4on A Sacbon a 5ectkm C
Requites Cbeot hdoaw.,roo: Requited Project Inrorrttrtlon- 6troice effermatio2 Pa 1 Of 1
�• � Sdreicler Natiohsl Report To. Gar (`we JAU&tM
Address: 2420 Starita Roan Copy To: Campary Name:
CKaAo.te. NC 28269
AdWess
-
rT+ail: 90r0cftscS c,ditr,Com
Pw=hwe Order a;
Pace Quote:
Phtxn: 17C )SW7a13 Jr.
ProR'ci Nam: SNKhartotle• NC
P-- Fs P n00W pas' mm.
- - .. state l Localkm .
P.equested Ole Dale;
Projecto
IPam Pm6b& a: 2631-1
NC
-
RaMms
Filtered
wtau C=
3
u
COLLECTED
z
Preservatives
Y
C
a-W ml« ow
WT
1f
W.W
Watts W, Ww
v
m
U
x
Z
SAMPLE ID a °'° a
r
I
sTMT
END
U
w
Doe Character per box. Ww rota
w
w
a
i
n
.00
{AZA.
W,O.9l,-j cu AR
0
r
i
z
n
5
�2�
em
ty.
V
m Saple Ids must be unique I- Ts
�
�
~
x
i
i
f
O
O
n
¢
DATE
TOWE
DATE
TWIE:
A-
sP-1
WT
X
x
x
SP-2
VVT
X
X
X
SP3
WT
x
X
X
az'
SPA
WY
x
x
x
:5
SP-s
WT
x
x
x
SPA
WT
X
X
x
. A811"
9r�
r-`
-i0i!
ra12�9
! = '"` '' '= °'a' -. ". .wqun`_ e`YJiiFFAliiitt7ei+
°r1
ialE
�.T
•t
^�
a:-Ac�iEnoirrAFFIIJRTu71il:,n"'�
'^".'
-
aATE.
L
}role
bk
SA&LL CO1�1isO�8£t
,n�'
,.-L �:i �.sa:aa`Y^ �+= 1C_ k'-.?4-� L,.`�.+3. .SH- +w. - 4i A!klYitif�`ACF
rr'!
d-•
Q R
��r
�t• rs4
.n.
1
l'3.r�`Y '-`Y�Q
i�fCll: ...- --ra y
i
PRINT Name of SAMPLM
S
w
2 _
$
e z
SIGNATURE of SAMPLER DATE Sf
f
cc
Iu—
re`c�
0
a
In
m
a-

ceAnalyrical
October 19, 2016
Mr. Chris Ray
Town of Zebulon
450 East Horton
Zebulon, NC 27597
NCG-og6696
6'
RE: Project: STORMWATER
Pace Project No.: 92315301
RECEIVED
OCT 2 5 2016
CENTRAL FILES
DWR SECTION
Pace AnaWical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilla, NC 28078
[phone]
Dear Mr. Ray:
Enclosed are the analytical results for sample(s) received by the laboratory on October 07, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc: Ms. Robyn Snow, Town of Zebulon
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 10

aceAnaliftal e
WWW.Psook.com
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersvllle, NC 28078
[phone]
CERTIFICATIONS
Project: STORMWATER
Pace Project No.: 92315301
Charlotte CertlFlcatlon IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Mrginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiafVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except In full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 10

Pace Analytical Services, LLC
5aneAmlyticale 9800 KinceyAve. Suite 100
Muntersvllle, NC 28078
WWW.PWW&kc" [phone]
SAMPLE ANALYTE COUNT
Project: STORMWATER
Pace Project No.: 92315301
Ana lytes
Lab ID Sample ID Method Analysts Reported Laboratory
92315301001 #11#2 STORMWATER EPA 1664E JMS 1 PASI-C
SM 2540D MLS 1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 10

Pace Analytical Services, LLC
9B06
ceAnalytrcal * Huntersvllle, NC328078
enre .ire
[phone]
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92315301
Sample: #11#2 STORMWATER Lab ID: 92315301001 Collected: 10/07116 06:34 Received: 10/07/16 12:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mglL 5.0 1 10/19/16 08:30
2540D Total Suspended Solids Analytical Method: SM 25400
Total Suspended Solids 68.5 mglL 12.5 1 10/12/16 13:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2016 03:34 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 10

aceAnalytical
wrrw.paoNei*cUrn
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92315301
QC Batch: 333689 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92315301001
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1849195
Matrix: Water
Associated Lab Samples: 92315301001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Oil and Grease
mg1L
NO 5.0
10/19/16 08:30
LABORATORY CONTROL SAMPLE:
1849196
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
40 37.5
94
78-114
MATRIX SPIKE SAMPLE:
1849197
92315432002 Spike
MS
MS % Rec
Parameter
Units
Result Conc.
Result
% Rec Limits Qualifiers
Oil and Grease
mg/L
NO 40
36.1
90 78-114
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/19/2016 03:34 PM without the written consent of Pace Analytical Services, LLC,
Page 5 of 10

('1a'veAnalyfical
wmrpactiArDs.carr
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92315301
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
HuntersAile, NC 28078
[phone]
QC Batch: 332687
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92315301001
METHOD BLANK: 1843631
Matrix: Water
Associated Lab Samples: 92315301001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg1L
NO
2.5 10/12/16 13:21
LABORATORY CONTROL SAMPLE: 1843632
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 246
98 90-110
SAMPLE DUPLICATE: 1843633
92315396001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
262
258 2
SAMPLE DUPLICATE: 1843634
92315393005 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg1L
NO
NO
Results presented on this page are In the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/19/2016 03:34 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 10

IeAnalytical
trww.peor�b>.cam
QUALIFIERS
Project: STORMWATER
Pace Project No.: 92315301
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitatlon Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylam ins decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte Is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/19/2016 03:34 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 110

(�'aceAnalytical
w".psafaDs.sem
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: STORMWATER
Pace Project No.: 92315301
Lab ID
Sample ID
QC Batch Method
QC Batch
92315301001
92315301001
#11#2 STORMWATER
#11#2 STORMWATER
EPA 1664B
SM 2540D
333689
332687
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/19/2016 03:34 PM without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersvllle, NC 28078
[phone]
Analytical
Analytical Method Batch
Page 8 of 10

Document Nemq: .: :+;1 pot ument Revised; way 24, 2016
CBAItr?r lCdl� Sample Coridh36n U 'ui, rfja a i'o�"
Document No.: Issuing Authority:
1 y P-RA4CS-W1 R@v.04 Pace Raleigh QUIRIV Office
Client Name- p:W�� oII� yl�9� 2I 3I I1 # �5I`I
3®1
UA?LIftject
courier. Ci
❑ Commercial da []Other: 8Z31'3301 "
Custody Seal PnMent? ❑Yes Seats intact? []Yes kao
Oate/tnitlah Person Examining Cant" �!d (y
ParadrlgMaterial: ❑Bubble Wrap ❑6ubbie Bags Oon�eQOtiter:
41
Tharmometer: T1505 TM d toar R+ Wet []Blue ❑Nome ❑5amplm on Ice, cooling process has begun
Correction Factor: 0A'G Gooier Temp Corrected ('C}: Je \ Blofoglal Tissue Frozen? []Yes []NO JrN A
-- -__
Temp should be above fre 17 to VC
USDA Regulated Soil (ZA, water sample)
Did sampi j orlglnate in a quarantine zone within the United States: CA, NY, or SC (check maps)? rid samples originate from a foreign source (internationally,
I-'ires n Irm"ine Hawaii and Puerto Ricoh ayes rim;
CammetttaJDlser
Chain of Custody Present?
No
N A
1.
samples Arrived within Hold Time?
e'S
ONO
ONJA
2.
3.
Short HoW Time Anafols 102 hr.)? N A
Rush Turn Around Thna vested?
Elyes
MKI
A
4.
Suff1clent Voltane?
as
ONO
A
S.
Correct Containers Used?
9a
❑No
❑WA
6.
-PaceContalners Uaedi
No
ONJA
Containers Intact?
as
QNo
N/A
7.
Samples Field Filtered?
Yes
QNo
R<A
a,
Note if sediment is visible In the dissolved oontalner
Sample labels Match COC?
es
ON.
❑N/A
9.
-Indudes Date/TIw*AY±!wIysIs Matrix.,
All containers needing add/base preservation have been
10. woo"
crocked?
of
[:]No
❑WA
All containers needing preservation are found to be In
"tlra°
complianc4 with EPA recommendation?
wIMM04
(HMOs, H2SO4, HCk2; Na0H 4 Sulfide, NeOH>12 Cyanide)
a
ONO
❑N/A
Exceptions: VOA, Collforrn, TOC, Oil and Grosse,
DRO 8015 w DorPN
CjYes
QNo
&NIA
Samples clacked for dechlorination?
es
QNo
11,
Head ate In VOA Vlals >5-6mm 7
es
No
12.
Trip Blank Present?
❑Yes
❑No
fN
11
Trip Blank Custody Seals Present?
❑Yes
©No
Pace Trip Blank lot # Jif purchased):
CLIENT NOTBFICATIOWRESDLI11ION FkAd Data Required? []Yes []NO
Person Contacted:
Comments/Sempte
Discrepancy:
Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: ffily]�> _ Date:
Nwa: Whenever there is a discrepancy affecting North Csrotlno compliance samples, a copy of this form wit be sent to the North Carolina DEHNR Certification Offioe (i.e.
Owl of told, incorrect preservative, out of temp, Incorrect containers)
Page 9of10

CHAIWOF-CUSTODY 1 Analytical Request Document
FdL�214f1a1}! l • "a Chain cPCL*Ddy In a LEGAL DOCUMExr.,w rakwwA fiaMs mull be wroalad acomaldy.
?� n n
F
0
I-MMM. sun
.. _.
'
• i
e
--
[�l��
MO■■■ME■■■
"■■■■■M■■■■■■
•
e
.,
r�r�r�■■■■�;■■■■
■M■■■■■■■■■■■
®
■■■■■■■■■■■■■
e
■■�■■■�■■�■�■■�■■■■�■■■■
■■■■■■■■■■■■■
-wylws•t Nu4: By �iV�! tIs �o.w yw a,a+m�P�9 P�oY! MEi 70 a7y pt}at� NNW aw aQvg 10 tMM wta M 14% oo GKCdh+w aft � W p: 44 .k. W don F-ALL-Q-WOMVv T. lb-May-Z Mr

.INKS
Review your project
results through
Have a Question?
Ask -
The
Ex ert
Visit+us at:
www.testa mericainc.com'
tV C (,- v S v 75-y
TestAmenca
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-130885-1
Client Project/Site: CA RR
For:
Genesee & Wyoming, Inc. tCEIV D
Railroad Company, Inc
200 Meridian Centre NDV 14 Z016
Suite 300
RAL FILES
Rochester, New York 14618 D\NR SECTION
Attn: Mr. William Ross
�r
Authorized for release by:
1012012016 2:04:38 PM
Lisa Harvey, Project Manager II
[phone] e.3221
[e-mail]
The test results in this report meet all 2003 NECAC and 2009 TNl requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the a -mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Definitions/Glossary
Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
Qualifiers
General Chemistry
Qualifier Quatitier Description
H F Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Abbreviation These commonly used abbreviations may or may not be present In this report.
o Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Oil Fac Dilution Factor
DL, RA, RE, IN indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
MIL Minimum Level (Dioxin)
NC Not Calculated
NO Not detected at the reporting limit (or MOIL or EDL if shown)
PQL Practical Quantitabon Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Job ID: 680-130885-1
TestAmerica Savannah
Page 2 of 12 10/20/2016

Client: Genesee & Wyoming, Inc.
Project/SiW CA RR
Lab Sample ID Client Sample ID
680-130885-1 Waste Water Holding Tank
Sample Summary
Matrix
Water
TestAmerica Job ID: 680-130885-1
Collected Received
10113116 14:00 10/14/16 09:50
TestAmerica Savannah
Page 3 of 12
10/20/2016

Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
Job ID: 680-130885-1
Laboratory: TestAmerica Savannah
Narrative
Case Narrative
Client: Genesee & Wyoming, Inc.
Project: CA RR
Report Number: 680-130885-1
TestAmerica Job ID: 680-130885-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method, In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 10/14/2016; the samples arrived in good condition, properly preserved and on ice. The temperature of the
cooler at receipt was 0.3 C.
HEM AND SGT-HEM
Sample Waste Water Holding Tank (680-130885-1) was analyzed for HEM and SGT-HEM in accordance with EPA Method 1664B. The
samples were prepared and analyzed on 10/18/2016,
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL SUSPENDED SOLIDS
Sample Waste Water Holding Tank (680-130885-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples
were analyzed on 10/17/2016.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH}
Sample Waste Water Holding Tank (680-130885-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples
were analyzed on 10/1812016.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample was analyzed in the
laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definition slGlossa ry page.
TestAmerica Savannah
Page 4 of 12 10/20/2016

Client Sample Results
Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
Client Sample ID: Waste Water Holding Tank
Date Collected: 10113/1614:00
Date Received: 10/14110 09:50
General Chemistry
Analyte Result Qualifier
HEM (Oil & Grease) 2.8
Total Suspended Solids 18
pH 7.9 HF
RL MUL Unit
2.6 0.73 mg1L
7.1 7.1 mg/L
SU
TestAmerica Job ID: 680-130885-1
Lab Sample ID: 680-130886-1
t
Matrix: Water
D Prepared Analyzed Dil Fac
10118116 08:41 10/18116 12:04
10117116 12:04 1
10/18/16 09:59 1
_i
TestAmerica Savannah
Page 5 of 12
10/20/2016

Client: Genesee & Wyoming, Inc.
Project/Site: CA RR
QC Sample Results
TestAmerica Job ID: 680-130885-1
Method: 1664E - HEM and SGT-HEM
a
Lab Sample ID: MB 680-45365411-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 453730
Prep Batch: 453654
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
HEM (Oil & Grease) <5.0
5.0 1.4 mg1L
1ail ail 6 08;41 10/16/16 12:04 1
Lab Sample ID: LCS 680-453664/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 453730
Prep Batch: 453654
L °�
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
HEM (Oil & Grease)
40,0
32.20
mg1L _ 80 78. 114
Lab Sample ID: LCSD 680.453654/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 453730
Prep Hatch: 453654
Spike
LCSD LCSD
%Rec. RPD
;
Analyte
Added
Result Qualifier
Unit D %Rec Llmfts RPD Limit
HEM fOil & Gressel
40.0
31.80
mall- 79 78 - 114 1 18
Method: 2540 D-2011 - Total Suspended Solids (Dried at 103-105°C)
Lab Sample ID: MB 680-45353211 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 453532
MI9 MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DII Fac
Total Suspended Solids <1.0 1.0 1.0 mg1L 10117116 12:04 1
Lab Sample ID: LCS 680-453532/2
Matrix: Water
Analysis Batch: 453532
Analyte
Total Suspended Solids
Lab Sample ID: LCSD 68045353213
Matrix: Water
Analysis Batch: 453532
Analyte
Total Suspended Solids
Spike LCS LCS
Added Result Qualifier Unit
20.0 16.0 mg1L
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
%Rec.
D %Rec Limits
80 80-120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
20.0 17.5 mg1L 88 80. 120 8 25
Method: 4500 H+ B-2011 - pH
Lab Sample ID: LCS 680-45373815 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 453738
Spike LCS LCS %Rec.
Anatyte Added Result Qualifier Unit D %Rec Limits
pH 7.00 7.1 SU 102 63 _ 158
TestAmerica Savannah
Page 6 of 12
10/20/2016

QC Association Summary
Client: Genesee & Wyoming, Inc.
ProyecVSite: CA RR
General Chemistry
Analysis Batch: 453532
Lab Sample ID
Client Sample ID
Prop Type
680-130885-1
Waste Water Holding Tank
TotalINA
MB 680-45353211
Method Blank
TotalINA
LCS 680-453532/2
Lab Control Sample
TotallNA
LCSD 680-453532/3
Lab Control Sample Dup
TotalINA
Prep Batch: 453654
FLab Sample ID
Client Sample ID
Prep Type
TestAmerica Job ID: 680-130885-1
i,
Matrix
Method
Water
2540 D-2011
Water
2540 D-201I
Water
2540 D-2011
Water
2540 D-2011
Matrix Method
680-130885-1
Waste Water Holding Tank
Total/NA
Water
1664E
MB 680453654/1-A
Method Blank
Total/NA
Water
1664B
LCS 680453654I2-A
Lab Control Sample
Total/NA
Water
1664E
LCSD 680453654/3-A
Lab Control Sample Dup
Total/NA
Water
1664E
Analysis Batch: 453730
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
680-130885-1
Waste Water Holding Tank
Total/NA
Water
1664E
MB 680-453654/1-A
Method Blank
TotalINA
Water
1664E
LCS 680-453654/2-A
Lab Control Sample
TotalINA
Water
1664E
LCSD 68045365413-A
Lab Control Sample Dup
TotalINA
Water
1664E
Analysis Batch: 463738
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
680-130885-1
Waste Water Holding Tank
Total/NA
Water
4500 H+ B-2011
LCS 660-45373815
Lab Control Sample
Total/NA
Water
4500 H+ B-2011
Prop Batch L _`
t 4
Prep Batch
ik o I
Prep Batch
453654
453654
453654
453654
Prop Batch
TestAmerica Savannah
Page 7 of 12 10/20/2016

Lab Chronicle E
Client: Genesee & Wyoming, Inc. TestAmerica Job ID: 680-130885-1
Project/Site: CA RR
Client Sample ID: Waste Water Holding Tank
Date Collected: 10113116 14:00
Date Received:10114116 09:50
Batch Batch
Prep Type
Type Method Run
Total/NA
Prep 1664B
Total/NA
Analysis 1664B
Instrument ID: NOEQUIP
Total/NA
Analysis 2540 0-2011
Instrument ID: NoEquip
Total/NA
Analysis 4500 H+ 6-2011
lnstrument ID: MANTECH
Lan Sample ID: buu-930585-1
Matrix: Water
ail
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
959 mL
500 mL
453654
10118116 08:41
JNN
TAL SAV
1
453730
10/18/16 12:04
JNN
TAL SAV
1
140 mL
1000 mL
453532
10117M6 12:04
JCM
TAL SAV
©_
1
453738
10118M6 09:59
LAF
TAL SAV
Laboratory References:
TAL SAV = TestAmerice Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
Page 8 of 12
10/20/2016

Certification Summary
Client: Genesee & Wyoming, Inc.
Project]Site: CA RR
Laboratory: TestAmerica Savannah
The certifications listed below are applicable to this report.
F
TestAmerica Job ID: 680-130885-1
Authority
Program
EPA Region
Certification ID
Expiration Date
A2LA
DoD ELAP
399.01
02-28-17
A2LA
ISOtIEC 17025
399.01
02-28-17
Alabama
State Program
4
41450
06-30-17
Arkansas DEQ
State Program
6
88-0692
01-31-17
California
State Program
9
2939
07-31-16 `
Colorado
State Program
B
NIA
12-31-16
Connecticut
State Program
1
PH-0161
03-31-17
Florida
NELAP
4
E87052
06-30-17
GA Dept. of Agriculture
State Program
4
NIA
06-12-17
Georgia
State Program
4
NIA
06-30-17
Georgia
State Program
4
803
06-30-17
Guam
State Program
9
15-005r
04-16-17
Hawaii
State Program
9
NIA
06-30-17
Illinois
NELAP
5
200022
11-30-16
Indiana
State Program
5
NIA
06-30-17
Iowa
State Program
7
353
06-30-17
Kentucky (DW)
State Program
4
90084
12-31-16
Kentucky (UST)
State Program
4
18
06-30-17
Kentucky (IN1h!)
State Program
4
90084
12-31-16
Louisiana
NELAP
6
30690
06-30-17
Louisiana (DW)
NELAP
6
LA160019
12-31-16
Maine
State Program
1
GA00006
09-24-18
Maryland
State Program
3
250
12-31-16
Massachusetts
State Program
1
M-GA006
06-30-17
Michigan
State Program
5
9925
06-30-17
Mississippi
State Program
4
NIA
06-30-16 `
Nebraska
State Program
7
TestAmerica-Savannah
06-30-17
New Jersey
NELAP
2
GA769
06-30-17
New Mexico
State Program
6
NIA
06-30-17
New York
NELAP
2
10842
03-31-17
North Carolina (DW)
State Program
4
13701
07-31-17
North Carolina "IS"
State Program
4
269
12-31-16
Oklahoma
State Program
6
9984
08-31-17
Pennsylvania
NELAP
3
68-00474
06-30-17
Puerto Rica
State Program
2
GA00006
12-31-16
South Carolina
State Program
4
98001
06-30-17
Tennessee
State Program
4
TN02961
06-30-17
Texas
NELAP
6
T104704185-15-8
11.30-16
USDA
Federal
SAV 3-04
06-11-17
Virginia
NELAP
3
460161
06.14-17
Washington
State Program
10
C805
06-10-17
West Virginia (DWy
State Program
3
9950C
12-31-16
West Virginia DEP
State Program
3
094
08-31-16 '
Wisconsin
State Program
5
999819810
08-31-17
Wyoming
State Program
8
8TMS-L
06-30-16 `
` Certification renewal pending - certification considered valid.
TestAmerica Savannah
Page 9 of 12 10/20/2016

Method Summary
Client: Genesee & Wyoming, Inc.
TestArnerica Job ID: 680-130885-1
Project/Site! CA RR
Method Method Descrtptlon
Protocol
Laboratory
16648 HEM and SGT-HEM
16648
TAL SAV
2540 D-2011 Total Suspended Solids (dried at 103-105°C)
SM
TAL SAV
4500 H+ B-2011 pH
SM
TAL SAV
Protocol References:
1664E = 166413
SM = "Standard Methods For The Examination Of Water And Wastewater',
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestAmerica Savannah
U]
;,N
i �.
Page 10 of 12 10/20/2016

Gs
Serial Number 95349
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
TestAmeCicaSavannah.
THE LEADER IN ENVIRONMENTAL TESTING
TeslAmerlca Savannah Website: www.testamericainc.com
T 5102 LaRoche Avenue Phone: [phone]
GA 314D4 Fax: [phone]
0 Alternate Laboratory Name/Location
Phone:
Fax:
PRGL<T RUMEN
CA A4��
PR9=T NO,
PROJECT LOCATION
(STATE) /(� G
MATRIX
TYPE
REQUIRED ANALYSIS
PAGE
OF
TAL (LAB) PROJECT MANAGER
4 is'yj y VB
P.O. NUMBER
CONTRACT NO.
�
m
0
0
q
a
O
a
a
o
,„
v.
o
0
rn
a
_
r
y
-�
`n
o
o
a
O
0
a
0
z
Vj
�
STA14DARD REPORT
DELIVERY D
DATE DUE
EXPEDITED REPORT
DELIVERY
(SURCHARGE)
OATEDUE _
CLIENT (SITE) PM
�3e c�
CLIENT PHONE
�ZI.69S'_S
CLIENT FAXZ52
332-322
CLIENT NAME
�f
Cr`� A 4,
CLIENT E-MAIL
CLIENT ADDRESS l�
G C
NUMBER OF GOOLERS SUBMITTED
PER SHIPMENT -
COMPANY
COMPA Y CONTRACTING THIS WORK (il applicable)
SAldPL F
SAMPLE IDENTIFICATION
�ufn
0
v
NUMBER
OF
CONTAINERS
SUBMITTED
REMARKS
DATE
TIME
(
FI
III
I
I
I
l
I
I
C
II
I
I
680-1,30885
Chaon of Custocl
I
RELI LSHE BY: ISZMTUREI
DATE
�3 r�
TIME
Z rdf
RELINQUISHED BY: f%NATUREI
DATE
TIME RELINQUISHED BY: (SWATURE)
DATE
TIME
W�WED BY;(SlGNATunn
DATE
TIME
RECEIVED BY: IS1Gr ATUAE1
DATE
I TIME
RECEIVED BY. isEG0TURE)
DATE
TIME
LABORATORY USE ONLY
RECEIVED FOR RATORY BY: DATE
(5�(SMTUTsE)10
TIME
CUSTODY INTACT
YES Q
CUSTODY
SEAL NO.
SAVANNAH
LOG NO.
CA$ORATpRY REMARKS
TALS240.8ao (IWO)

Login Sample Receipt Checklist
Client: Genesee & Wyoming, Inc.
Login Number: 130885
List Number: 1
Creator: Flanagan, Naomi V
Question
Radioactivity wasn't checked or is <1= background as measured by a survey
meter.
The cooler's custody seal, If present, is Intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice,
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in Ink and legible.
COC Is filled out with all pertinent information.
Is the Field Samplers name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time (excluding tests with immediate
HTs)
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, incl. any requested
MSlMSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (114").
Mulliphasic samples are not present.
Samples do not require splitting or conipositing.
Residual Chlorine Checked.
Answer Comment
N/A
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
NIA
True
True
NIA
Job Number: 680-130886-1 }
List Source: TestAmerica Savannah -
f
F-12
TestAmerica Savannah
Page 12 of 12 10/20/2016

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCGO80000 SAMPLES COLLECTED DURING CALENDAR YEAR: 71) I Lo
CERTIFICATE OF COVERAGE NO. NCG08QS$ 9 (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Schyw cfi f K )a 0 I & I COUNTY M,tC Vag-Q bu r
PERSON COLLECTING SAMPLES PHONE NO.
CERTIFIED LABORATORY P Lab #]�
Lab # PLEASE SIGN ON THE REVERSE
Part A: Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? A yes _no
(if yes, report your analytical results in the table immediately below)
Oitfall
Na. `'
-
Date
Sample Collected;,
mold
00530'.
` .:00400
>r'00556"K
' Total Suspended Solids, ,
_ - ` t`'
5tandard�units .=r,
Oil a"nd'GreM.ase F ~
`New Ma , - sage, H s
!�Annualiavera e
Benchmark
.100.
. ° within 6:a,='9.0N,'NMM
uv I
121ov ll.►-
Uu2
$1
55
. �'
0013
at
-5
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 respons �� �, VrE D
See General Permit text.
Part B: On/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
-..Outran
No
-Date ` . '
Sample :Collected ,
:OOSS6 =
. ,� 00530 ..
s`�0040tli• *__
Od and Grease;
Total Suspended+Solids,
Pe�mit Limit
STORM EVENT CHARACTERISTICS:
Date IZd(Xe 4(first event sampled)
Total Event Precipitation (inches): D . V
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
JAN 17 Z017
CENTRAL FILES
DWR SECTION
SWU-250-102107
Page 1 of 2

"I certify, under penalty of law, that this document and all.attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
(SIgnatuh of Permittee) CT (Date)
SWU-250-102107
Page 2 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCGO80000 SAMPLES COLLECTED DURING CALENDAR YEAR: IN kp
CERTIFICATE OF COVERAGE NO. NCGOS 65 $ - (This monitoring report is due at the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME StSh"jQW_NUrIOM i COUNTY
PERSON COLLECTING SAMPLES 81{" e1off- PHONE NO. (C� 1
CERTIFIED LABORATORY_ pry l►rt-tfa% Lab #�Q(�
�— Lab # PLEASE SIGN ON THE REVERSE 4
Part A: Vehicle Maintenance Areas Monitoring Requirements
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ^ yes no
(if yes, report your analytical results in the table immediately below)
Outfall
No.
Date
Sample Collected,
mold
00530
00400
00556
Total Suspended Solids,
pH;_
Standard units
Oil and`Grease,
'• New?Motor Oil Usage',
Annual ave e' mo
Benchmark
-
100
Within 6.0 — 9.0
30'
12 D(A 11LO
ZL4
v
u
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals
Outfall
No.
Date
Sample Collected,
mo/ddl
00556
00400 ,4
Oil and Grease,
Total Suspended Solids, ,
x :._ ,.. :E
pH, . _
_ Standasd,units
Permit Limit
-
_ 30 ..
100 -• . -
6:0. - 9:0
STORM EVENT CHARACTERISTICS: ' Mail Original and one copy to:
f Division of Water Quality
Date IQI 14fi st event sampled) Attn: DWQ Central Files
Total Event Precipitation (inches): 1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
SWU-250-102107
Page 1 of 2

"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
� �� � W If PFJ . J.W)-�ry
. W6-
111-511`1 _
(Date)
SWU-250-102107
Page 2 of 2

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG080000
pS S—SrDaatte submitted I0 JZ U ( 1 b
CERTIFICATE OF COVERAGE NO. NCG08_L k 0 O SAMPLE COLLECTION YEAR DLO I LP
FACILITY NAME S SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
COUNTY or ®Month�J��' Lmonth]
PERSON COLLECTING SAMPLEV ri I On M& DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY Lab Cert. # 3`} �n i . RECEIVED ❑Zero -flow ❑Water Supply ❑SA
[:]OtherComments on sample col lectio or analysis: 0 C r 31
2016
CENTRAL FILES PLEASE REMEMBER TO SIGN ON THE REVERSE
�n
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons ofnrAcirr month? yes _no
(if yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
❑ No discharge this period;
Outfall
No.
Date;005303x.
Sam le CollectedTota!
p
00400
wY._� , Im55f:��<:y
Sus ' nded<
Pe
SOIEtls; mg/�L�
PH
Standard units_
Non -Polar Oil a dG` rea a-
/TPIi EPA ..N�yew
Method 16" (SGT;HEM), mg/,L
sMotor0il U�s�agemo/dil/yl'
Annual average,l/,mod
Benchmark.
11]04e penfiit
INit1iE'rt6�0 0
15
1
u
•5
1 5 2
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
Outfall
No:
Date:
Sample Collected, °
yra
g 00556 .� -EN019dWRO0530
0040Q
Nan=Polar'OEland�Grease%TPH�EPAMetfiod
-1fi64 (EMj, rrtg/Lmg/L
Total�Suspended Sofids,
�IIad/ units
Pernniturhi ':
3 � 15;
50(or 100 see n
fi.0 9
I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SWU-250 last revised April 11, 2013
Page 1 of 2

Semi-annual Stormwater Discharee MonitoringReRort
for North Carolina Division of Water Quality General Permit No. NCG080000
Date submitted ''
CERTIFICATE OF COVERAGE NO. N0008 0 _(�U !�L
FACILITY NAME !'
COUNTY
PERSON COLLECTING SAMPLES
LABORATORY If Lab Cert. # '
Comments on sample collection or analysis:
SAMPLE COLLECTION YEAR
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ® Monthly( ' ' (month)
DISCHARGING TO CLASS ❑ORW ❑HCIW ❑Trout ❑PNA
[]Zero -flow ❑Water Supply [—]SA
❑Other
PLEASE REMEMBER TO SIGN ON THE REVERSE 4
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no
Of yes, report your analytical results in the table immediately below)
Part A: Vehicle Maintenance Areas Monitoring Requirements (If applicable)
No discharge this period
WNJ—al-i
No.
Date
Sample Collected,
m_o/,dtlyr
00530
Total SuspendedM
5olid5, mg/L
00400
Standats
IpHP
00556
Non -Polar Oil and Grease/TPH EPA
Method 16G4 (SGT KELKI mg/L
INe—w Motor Oil Usage,
Annual average gal/1no
(3Benchmark
® -
50,or 100isee permit
W_ _ithin 5.0M 0
-
1-I
IDIL9
5 Z
q- -1
S
0 017 H U
A i4q
-I . LP
I - Cp
I
0
Part B: Oil/water Separators and Secondary Containment Areas at Petroleum Bulk Stations and Terminals (If applicable)
0utfa11
No.
Date
Sample Collected,
m%dd/,yr
00556
Non -Polar Oil and Grease/TPH EPA Method
1664 (SGTY-HEM), mg/1L
00530
Total Suspended Solids,
mg/L
00400
p�uoits
Standa
Permit Limit
15
5Qo7r100,see permit
6.0�9.0
I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
SA U-250 last revised April 11, 2013
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date O� (first event sampled)
Total Event Precipitation (inches): 0 - L �
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES El NO Vx
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one cony of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in
the case o f "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, thatthis document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Permittee)
2 Ib
(Date)
Additional copies of this form may be downloaded at:.http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
SW-250
last revised April 11, 2013
Page 2 of 2