NCG030664_MONITORING INFO_20190315

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
N CC7 D 3 O � �y
DOC TYPE
❑HISTORICAL FILE
U,AONITORING REPORTS
DOC DATE
❑ � � 031 s--
YYYYMMDD

h
�'� Southwire�
March 15, 2019
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Permit No: NCG030000
Certificate of Coverage: NCG030664 RECEIVED
MAR 2 0 2019
Southwire
12331 Commerce Station Drive CENTRAL FILES
Huntersville, NC 28078 DWR SECTION
Dear Sir/Madam:
Enclosed is the Semi-annual Stormwater Discharge Monitoring Report and associated analytical
results for the Southwire Facility.
This report covers required sampling for 2019 January — June Semi -Annual.
Should you have any questions, please contact me at 704-379-9621 or
iamie.mc rath southwire.com. Thank you.
Regards,
Ir
Jamie McGrath
EHS Manager
Southwire I Huntersville

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03 0 6 6 4
FACILITY NAME Southwire - Huntersville
COUNTY Mecklenburg
PERSON COLLECTING SAMPLES Jamie McGrath
LABORATORY Pace Labs Lab Cert. # 12
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2019
SAMPLE PERIOD [] Jan -June ❑ July -Dec
or Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply [:]SA
Mother c-waterbody
PLEASE REMEMBER TO SIGN ON PAGES Z AND/OR 3 -i
❑ No discharge this period?'
Outfall No.
Hate Sample
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Total Suspended Solids
Standard units
prd
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total nics5
Organics
Benchmarks
_
-
100 mg/L or 50 mg/O
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
-
46529
C0530
00400
01119
01051
01094
00552
78141
Outfall #1
3/8/2019
0.16
14.4 mg1L
6.0
0.012 mg/L
<0.075 mg/L
0.10 mg/L
<5 mg/L
NA
Outfall ##2
3/8/2019
0.16
30.6 mg/L
6.8
0.037 mg/L
<0.075 mg/L
0.089 mg/L
<5 mg/L
NA
Outfall #3
3/8/2019
0.16
8.6 mg/L
4A
<0.010 mg/L
<0.075 mg/L
0.099 mg/L
<5 mg/L
NA
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
a See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General "
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report, I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Jamie McGrath
Name (Print name)
EHS Manager
Title (Print title)
641W
ature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, the must be reported in the format. "<XX me/t. where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or filer 3 responses. See General Permit text.
Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?'
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches3
New Motor Oil or
Hydraulic Oil Usage
Non -Polar 0&G/ Total
Petroleum hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
-
15 mg/L
100 mg/L or 50 mg/L4
Parameter Code
-
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 5WU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART 6 MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART li SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENC FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THk DENJLR IONAL OFFICE? YES [D NO ID
REGIONAL OFFICE CONTACT NAME: V Maine '(a235.2!•2l
Mail an oriainal cony of this DMR, including all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitorina period In the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1517 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
s 2dr9
Sign re of Permittee Da e
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 3 of 3

• ceAnalytical
wrrw.pw&tbs.mm
March 15, 2019
Jamie McGrath
Southwire
12331 Commerce Station Dr
Huntersville, NC 28078
RE: Project: 2019 SEMI ANNUAL JAN-JUNE
Pace Project No.: 92420659
Dear Jamie McGrath:
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27268
{336)623-8921
Enclosed are the analytical results for sample(s) received by the laboratory on March 08, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C.
Page 1 of 13

Pace Analytical Services, LLC
e 205 East Meadow Road - Suite A
cemalytical Eden, NC 27288
Mww.pgC"&aom [phone]
CERTIFICATIONS
Project: 2019 SEMI ANNUAL JAN-JUNE
Pace Project No,: 92420659
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: WNCO30
North Carolina Drinking Water Certification #. 37712
South Carolina Certification #: 99006001
FloridaINELAP Certification #: E87621
Kentucky UST Certification #: 84
VirginiaA(ELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification M 99030001
VirginWVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2,of 13

lcmnalytical"
W#W.Pacalabs.oam
SAMPLE ANALYTE COUNT
Project: 2019 SEMI ANNUAL JAN-JUNE
Pare Project No.: 92420659
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Lab ID
Sample ID
Method
Analysts
Analysts
Reported
Laboratory
92420659001
OUTFALL #1
EPA 1664B
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
SM 254OD-2011
CEH
1
PASI-A
EPA 9040C
ECH
1
PASI-A
92420659002
OUTFALL #2
EPA 1664B
JMS
1
PASt-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
SM 254OD-2011
CEH
1
PASI-A
EPA 9040C
ECH
1
PASI-A
92420659003
OUTFALL #3
EPA 1664B
JMS
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
SM 254OD-2011
CEH
1
PASI-A
EPA 9040C
ECH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 13

Pace Analytical Services, LLC
205 East Meadow Road - Suite A
ce, 4nalytical Eden, NC 27288
wwwpacaws.com
(336)623$921
ANALYTICAL RESULTS
Project: 2019 SEMI ANNUAL JAN-JUNE
Pace Project No.: 92420659
Sample: OUTFALL #1 Lab Ip: 92420659001 Collected: 03/08/19 14:40 Received: 03/08/19 15:50 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg1L
5.0
1
03/14/19 06:28
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
0.012 mg1L
0.0050
1
03111/1916:15
03112l1918:13 7440-50-8
Lead
ND mg/L
0.0050
1
03/11/19 16:15
03/13/19 21:22 7439-92-1
Zinc
0.10 mg1L
0.010
1
03/11/1916:15
03112l1918A3 7440-66-6
2540D TSS, Lour -Level
Analytical Method: SM 25400-2011
Total Suspended Solids
14.4 mg1L
1.0
1
03/09/19 07:07
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.0 Std. Units
0.10
1
03/10/19 12:58 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2019 01:45 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 13

Pace Analytical Services, LLC
cp "Cal
205 East Meadow Road - Suite A
• ry ru"Ca
Eden, NC 2728E
www.p amn
{335}623-8921
ANALYTICAL RESULTS
Project: 2019 SEMI ANNUAL JAN-JUNE
Pace Project No.: 92420659
Sample: OUTEALL 92
Lab iD: 92420659002 Collected: 03/08/19 15:06
Received: 03/08/19 15:50 Matrix: Water
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS Na. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mgfL 5.0 1
03/14/19 06:28
200.7 MET lCP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
0.037 mg/L 0.0050 1
0311111916:15 03/1211918:25 7440-50-8
Lead
ND mg/L 0.0050 1
03/11/19 16:15 03/13/19 21:34 7439-92-1
Zinc
0.089 mg/L 0.010 1
0311111916:15 0311211918:25 7440-66-6
2540D TSS, Low -Level
Analytical Method: SM 254OD-2011
Total Suspended Solids
30.6 mg/L 2.0 1
03/09/19 07:08 D6
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.8 Std, Units 0.10 1
03/10/19 13:15 H3
Date: 03/15/2019 01:45 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 13

Pace Analytical Services, LLC
205 East Meadow Road - Suite A
" ceAnalytir"01 Eden, NC 27288
"W.'Qom [phone]
ANALYTICAL RESULTS
Project: 2019 SEMIANNUAL JAN-JUNE
Pace Project No.: 92420659
Sample: OUTFALL03 Lab1D: 92420659003 Collected: 03108/1915:26 Received: 03/0811915:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mgfL
5.0
1
03/14/19 06:28
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
ND mg1L
0.0050
1
0311111916:15 0311211918:28 7440-50-8
Lead
ND mg1L
0.0050
1
03/11119 16:15 03/13119 21:37 7439-92-1
Zinc
0.099 mg1L
0.010
1
0311111916:15 03112/1918:28 7440-66-6
2540D TSS, Low -Level
Analytical Method: SM 254OD-2011
Total Suspended Solids
8.6 mg1L
1.0
1
03/09/19 01:08
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
4.4 Std. Units
0.10
1
03/10/19 13:21 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2019 01:45 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

ceAnalytical
wwrpwetab&corn
QUALITY CONTROL DATA
Project: 2019 SEMI ANNUAL JAN-JUNE
Pace Project No.: 92420659
QC Batch: 463221 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92420659001, 92420659002, 92420659003
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
METHOD BLANK: 2520354 Matrix: Water
Associated Lab Samples: 92420659001, 92420659002, 92420659003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L ND 4.8 03114/19 06:15
LABORATORY CONTROL SAMPLE: 2520355
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mg1L 38.5 37.6 98 78-114
MATRIX SPIKE SAMPLE: 2520356
92419835003 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
Oil and Grease mglL ND 40 39.2 98 78-114
Results pi esen an this page are In the units inrscaW by the'tfrrtm' 00hnn 1 mccept where an attamate unlit is pnnanEeQ to the right of the resutL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 03/15/2019 01,45 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13

IceAnalytical"
wwwpacelsb&mm
QUALITY CONTROL DATA
Project: 2019 SEMI ANNUAL JAN-JUNE
Pace Project No.: 92420659
QC Batch: 462549 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated tab Samples: 92420659001, 92420659002, 92420659003
METHOD BLANK: 2517596
Matrix: Water
Associated Lab Samples:
92420659001, 92420659002, 92420659003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Copper
mg/L
ND
0.0050
03/1211917:06
Lead
mg/L
ND
0.0050
0311211917:06
Zinc
mg/L
ND
0A10
03/12/1917:06
Pace AnaWcal Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE:
2517597
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Copper
mg1L
0.5
0.49 97 85-115
Lead
mg1L
0.5
0.47 93 85-115
Zinc
mg/L
0.5
0.47 94 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2517598
2517599
MS
MSD
92420617001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper
mg1L
10.6
0.5
0.5
0.50
0.49
98
97
70-130
2
ug1L
Lead
mg1L
ND
0.5
0.5
0.47
0.46
93
92
70-130
1
Zinc
mg/L
90.5
0.5
0.5
0.58
0.57
97
95
70-130
2
ug/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2517600
2517601
MS
MSD
92420659001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper
mg1L
0.012
0.5
0.5
0.52
0.51
101
101
70-130
1
Lead
mg1L
ND
0.5
0.5
0.47
0.47
94
94
70-130
0
Zinc
mg/L
0.10
0.5
0.5
0.59
0.59
97
96
70-130
0
Results presented on this page are in the unite indicated by the ZJnits" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2019 01;45 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 13

6
CMnalytrcal
www.pacebbs.com
QUALITY CONTROL DATA
Project: 2019 SEMI ANNUAL JAN-JUNE
Pace Project No.: 92420659
Pace Anatytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QC Batch: 462383
Analysis Method:
SM 2548D-2011
QC Batch Method: SM 254OD-2011
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92420659001, 92420659002, 92420659003
METHOD BLANK: 2517011
Matrix: Water
Associated Lab Samples: 92420659001, 92420659002,
92420659003
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND
1.0 03/09/19 07:05
LABORATORY CONTROL SAMPLE:
2517012
Spike LCS
LCS % Rec.
Parameter
Units
Conc. Result
% Rec. Limits Qualifiers
Total Suspended Solids
mglL
250 260
104 90-110
'
SAMPLE DUPLICATE: 2517013
92420405001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg1L
183
192 5
SAMPLE DUPLICATE: 2517014
92420659002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 30.6 34.2 11 D6
Results presented on this page are in the units indicated by the -Units' column except where an attemate unit Is presenW to the right of the result
REPORT OF LABORATORY ANALYSES
This report shall not be reproduced, except in full,
Date: 03/1512019 01:45 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

s
ceAnalytical
wwwpacelabs cam
QUALITY CONTROL DATA
ProjecL 2019 SEMI ANNUAL_ JAN-JUNE
Pace Project No.: 92420659
QC Batch: 462455 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Associated Lab Samples: 92420659001, 92420659002, 92420659003
SAMPLE DUPLICATE: 2517273
92420617001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.3 5.9 7 H3
SAMPLE DUPLICATE: 2517677
92420080001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 7.0 6.9 1 H3
Pate Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Results preS-ftd an this ~ere in the units inWcat1tl 6y the'Lnits' column except where an alternate unit Is presented to the dght of the resulL
REPORT Of LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2019 01:45 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 13

s
t ceAnalytical
rrwpnoewm0cm
QUALIFIERS
Project: 2019 SEMI ANNUAL JAN-JUNE
Pace Project No.: 92420659
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
Pace Analytical Services, LLG
205 East Meadow Road - Suite A
Eden, NC 27258
[phone]
PQL- Practical Quantitation Limit,
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a speck analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anatyle is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrytonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NE LAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
06 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
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Date: 03/15/2019 01:45 AM without the written consent of Pace Analytical Services, LLG. Page 11 of 13

a
ceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: 2019 SEMI ANNUAL JAN-JUNE
Pace Project No.: 92420659
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92420659001
OUTFALL #1
EPA 1664B
463221
92420659002
OUTFALL#2
EPA1664B
463221
92420659003
OUTFALL#3
EPA 1664B
463221
92420659001
OUTFALL#1
EPA 200.7 Rev 4.4 1994
462549
92420659002
OUTFALL#2
EPA 200.7 Rev 4.4 1994
462549
92420659003
OUTFALL#3
EPA 200.7 Rev 4.4 1994
462549
92420659001
0UTFALL#1
SM 254OD-2011
462383
92420659002
OUTFALL#2
SM 254OD-2011
462383
02420659003
OUTFALL#3
SM 2540D-2011
462383
92420659001
OUTFALL #1
EPA 9040C
462455
92420659002
OUTFALL#2
EPA9040C
462455
92420659003
OUTFALL#3
EPA9040C
462455
Date: 03/15/2019 01:45 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
EPA 200.7 Rev 4A 1994 462629
EPA 200.7 Rev 4.4 1994 462629
EPA 200.7 Rev 4.4 1994 462629
Page 12 of 13

CHAIN -OF -CUSTODY Analytical Request Document
PaceAnalytical'
Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevant fields
Company; -
Billing Information: %*1*40
MAMAPIWKXA
(Wilt clor")G)tGG/�' o,Q
ri�n��/((, 1►
Ad re s:
II►r
NLIJUG NC
Report To: a
Email Te: rt) n
U�• _
Copy To: t
Ilec 'an Info/Addres .
Customer }Project Name/Number:r j
20l `S jLrAi ` y�I�Iji'J ile�
State: County/City: Time Zone Collected:
INt / M NIII 1 PT [ 1 M7 [ 1 CT [ VT
Phone: -pt f
Site/Facillty ID N:Cv�lianco
Monitoring?
Ema'ik mla. Ali ASIA
&A
It✓f Yes [ 1 ND
Collected By (print):
Purchase Order ft:
DW PWS ID N:
70M fG M1061it&=
Quote N:
DW Location Code:
tAlected N (si;najurely
f urna round Date Required:
Immediately Pace on ice:
LAB USE ONLY- Affix Workorder w0# • 92420659
M Illlll l!I l!l I !till! Ill
ALL SHADED 1 92420659
tauriuJur,n�,, a ..
• • Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochhoric acid, (4) sodium hydroxide, IS) tine acetate,
(fi) methanol, (7) sodium bisulfate, (8) sodium thiosultate, (9) hexane, (A) ascorbic acid, in) ammonium su$late,
(C) ammonium hydroxide, (0) TSP, {U) Unpreserved, (0) Other
W km �/' (JQ('L . 1 1 Yes [KNo
m Disposal: Rush: Field Filtered (if applicable):
l Ispose as appropriate I I Return [ ] Same Day [ ] Next Day I I Yes [ )No
I I Archive: [ ] 2 Day I 13 Day [ ) 4 Day [ ] 5 Day 4
I I Hold: (Expedite Charges Applyl Analysis:
}
• Matrix Codes (Insert in Matrix box below]: Drinking Water (DW). Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SQ, Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
Comp / Collected (ar Composite End Res # of
Customer Sample ID Matrix • Grab Composite Start) CI Ctns
Date Time Date I Time
Customer Remarks / Special Conditions / Possible Hazards: Type of Ice Used: LWdt Blue Dry None
Packing Material Used:
61inquished by/Company:
eiin uished by/Company:
zu*-
Radchem sample(s) screened (<500 cpm): Y N NA'
ta[we) Date/Time: Received by/C 73 Zig
iature) Date/Time: Receive / any: (SiR ature]
ny:
Lab Semple Receipt Checklists
Custody Scale Present/Intacf
NA
Custody Signatures PresentNA
Collector Signature PresentNA
Bottles Intact NA
Corroct Bottles NA
SufficientVolume NA
Samplea Received on IceNVOA - Headepace Acceptable
USDA Regulated Soils
Samples in Holding lime NA
Residual Chlorine Proaent Y N AD
Cl Stripsr
Sample pH Acceptable N NA
pH Stripai
Sulfide Present y N
Lead Acetate Stripe:
LAB USE ONLYi
Lab Sample rK / Comments:
SHORT HOLDS PRESENT (02 hours): Y QV N/A
Lab Tracking g: 2343100
FEDEX UPS ten Courier Pa
Date/Time: MTJL LAB USE ONLY
3/q i � _� A Tablie ,
a
m
rn
a
Lab Sample Temperature Info:
Temp Blank Received: YN NA
Therm IDN: aZT Ga k
Cooler 1 Temp Upon Receipt: 3A-oc
Copier 1 Therm Corr. Factor: O oC
Cooler 1 Corrected Temp:^oC
Comments:
Template: Trip Blank Received: Y CAT NA
Prelogin: HCL McOH TSP Other
PM: Non Conform�(tce(sj: Page
PS: YES / oF:
i

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Resources General Permit No. NCG030000
Date submitted 121612018
CERTIFICATE OF COVERAGE N0. NCG03_Q JaL k I SAMPLE COLLECTION YEAR 2018
FACILITY NAME Southwire-Huntersville SAMPLE PERIOD ❑ Jan -June Q July -Dec
COUNTY Mecklenburg or ❑ Monthly' 'month)
PERSON COLLECTING SAMPLES Jamie McGrath RECEIVE 10CHARGINGTOCLASS ❑ORW ❑HQW [—]Trout ❑PNA
LABORATORY Pace Labs Lab Cert. # 12 ❑Zero -flow ❑Water Supply ❑SA
Comments on sample collection or analysis: DEC 12 2018 ■❑Other c-Waterbody
"CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
DWR SECTION
Part A: Stormwater Benchmarks and Monitoring Results
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organics
Benchmarks ==_>
_
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
12I1I18
0.10
3.9
7.6
0.016 mg/L
<0.0050 mg/L
0.036 mg/L
<5 mg1L
NIA
2
1211118
0.10
10.3
7.6
0.013 mg/L
<0.0050 mg/L
0.028 mg/L
<5 mg1L
NIA
3
1211118
0.10
11.6
6.5
0.0059 mglL
<0.0050 mglL
0.15 mg/L
<5 mg/L
NIA
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWIJ-245, last revised 10/25/2012
Page 1 of 3

FScilities4that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Jamie McGrath
Name (Print name)
EHS Manager
Title (Print title)
• & 1 2/6/2o 1 s
0/nature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX me/L where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value In excess of the benchmark, you must implement Tier .1, Tier Z or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?'
Outfall Na.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks ===s
_
-
1S mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: if you report a sample value in excess of the benchmark, you must Implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
0 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD a OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, Including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
In the case of "No Discharge" reports) to:
Division of Water Resources
Attn. DWR Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete, 1
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
121812018
Date}
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

aceAnalytiical.
w w:pacelabs.cvm
SAMPLE ACKNOWLEDGMENT
Samples Submitted By: Southwire Pace Project Manager.
Client Project ID: 2018 SEMI-ANNUAL (JULY-DEC)
Client PO#: 4500969782
Pace Analytical Project ID:
Samples Received:
Estimated Completion:
CC: Jamie McGrath
9800 Kincey Ave., Suite 100
Huntersville, NC 28078
[phone]
Taylor Ezell
Phone[phone]
[e-mail]
92409169
December 3, 2018 09:16 AM
December 10. 2018
Pace Analytical
Datemme
Customer Sample ID
Lab ID
Matrix
Collected
Method
OU7FALL#1
92409169001
Water
1210llIS 12:20
200.71CPMetals
Copper, Lead, Zinc
2540D Total Suspended Solids
9040 pH
ITEM, Oil and Grease
OUTFALL #2
92409169002
Water
12/01/19 12:46
200.71CP Metals
Copper, Lead, Zinc
2540D Total Suspended Solids
9040 pH
HEM. Oil and Grease
OUTFALL #3
92409169003
Water
12/01/18 12:56
200.7 ICP Metals
Copper, Lead Zinc
2540D Total Suspended Solids
9040 pH
HEM. Oil and Grease
Please contact your project manager if you recognize any discrepancy in this form or have any questions about your project.
Thank you for choosing Pace Analytical Services, LLC.
12/03/2018 11:14 AM Page 1 of 1

(�Ie Analytical
owalafto"
December 05, 2018
Jamie McGrath
Southwire
12331 Commerce Station Dr
Huntersville, NC 28078
RE: Project: 2018 SEMI-ANNUAL (JULY DEC)
Pace Project No.: 92409169
Dear Jamie McGrath:
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Enclosed are the analytical results for sample(s) received by the laboratory on December 03, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
taylor.ezell@pacelabs.00m
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Eden, NC 27288 '
(336J623-6921
Page 1 of 13

C8'wom/ e
wrnW'mCVkbsmm
Paco Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-B921'
Project: 2018 SEMI-ANNUAL (JULY-DEC)
Pace Project No.: 92409169
Charlotte Certification IDs
9800 Kinsey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 377DS
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99DO6001
FloridalNELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginialVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginialVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC. Page 2 of 13

•
2ceAnalyfical
1!rlww'acalabt Wrn
SAMPLE ANALYTE COUNT
Project: 2018 SEMI-ANNUAL (JULY-DEC)
Pace Project No.: 92409169
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Lab ID
Sample ID
Method
Analysts
Anatytes
Reported
Laboratory
92409169001
OUTFALL #1
EPA 1664E
LGD
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH 1
3
PASI-A
SM 2WD-2011
MVC
1
PASI-A
EPA 9D4DC
SMK
1
PASI-A
92409169002
OUTFALL #2
EPA 1664B
LGD
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH 1
3
PASI-A
SM 254OD-2011
MVC
1
PASI-A
EPA 9040C
SMK
1
PASt-A
9240,3169003
OUTFALL #3
EPA 1664B
LGD
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
SM 254OD-2011
MVC
1
PASI-A
EPA 9040C
SMK
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 13

CGAnalyfical o
rrMw.pecstabxmm
ANALYTICAL RESULTS
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden. NC 27288
[phone]
Project: 2018 SEMI-ANNUAL (JULY-DEC)
Pace Project No.: 92409169
Sample: OUTFALL #1 Lab ID: 92409169001 Collected: 12/01/18 12:20 Received: 12/03/18 09:16 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg1L
5.0
1
12/05/18 08:59
200.7 MET ICP
Analytical Method: EPA 2003 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
0.016 mg/l_
0.0050
1
12/04/18 03:00 12104l18 22:40 7440-50-8
Lead
ND mg/L
0.0050
1
12/04/18 03:00 12/04/18 22:40 7439-92-1
Zinc
0.036 mg/L
0.010
1
12/04/18 03:00 121G4/18 22:40 7440-66-6
2540D TSS, Law -Level
Analytical Method: SM 2540D-2011
Total Suspended Solids
3.9 mg1L
1.0
1
12/04/18 16:57
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
7.6 Std. Units
0A0
1
12/04/18 15:51 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/05/2018 04:48 PM without the written consent of Pace Analytical Services. LLC. Page 4 of 13

2eAnalyfical*
(�
wrv�rpecefabs.00m
ANALYTICAL RESULTS
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288 '
[phone]
Project: 2018 SEMI-ANNUAL (JULY--DEC)
Pace Project No.: 92409169
Sample: OUTFALL #2 Lab ID: 92409169002 Collected: 12101M8 12:46 Received: 12/03/18 09:16 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 16646
Oil and Grease
ND mg1L
5.0
1
12105/1808:59
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Copper
0.013 mg1L
0,0050
1
12/04/18 0100 121G4118 22:52 7440-50-8
Lead
ND mg/L
0.0050
1
12/04/18 03:00 12/04/18 22:52 7439-92-1
Zinc
0.028 mg1L
0.010
1
12/04/18 03:00 12/04/18 22:52 7440-66-6
2540D TSS, Low -Level
Analytical Method: SM 254OD-2011
Total Suspended Solids
10.3 mglL
1.0
1
121G4/18 16:57
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
7.6 Std. Units
0A0
1
12/04/18 15:59 H3
REPORT OF LABORATORY ANALYSIS
This report shall not 6e reproduced, except in full,
Dale: 12/05/2018 04:48 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13

ceArialA al
rnrrrpawfabs.ccra
ANALYTICAL RESULTS
Project: 2018 SEMI-ANNUAL (JULY-DEC)
Pace Project No.: 92409169
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 2728B
[phone]
Sample: OUTFALL #3
Lab ID: 92409169003 Collected:
12/01/18 12:56
Received: 12/03/18 09:16 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L
5.0
1
12JO5118 08:59
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Capper
0.0059 mg/L
0,0050
1
12/04/18 03:00 12/04/18 22:55 7440-50-8
Lead
ND mg/L
0.0050
1
12/04118 03700 12/04/18 22:55 7439-92-1
Zinc
0.15 mg/L
0.010
1
12/04/18 03:00 12/04/18 22:55 7440-66-6
25400 TSS, Low -Level
Analytical Method: SM 254OD-2011
Total Suspended Solids
11.6 mg/L
2.0
1
12/04/18 16:57 D6
9040 pH
Analytical Method: EPA 9040C
pH at 25 Degrees C
6.5 Std. Units
0,10
1
12/04/18 16:06 H3
Date: 12/05/2018 04748 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fell,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 13

ceAnWcal.
mrnpacelaRswm
QUALITY CONTROL DATA
Project: 2018 SEMI-ANNUAL (JULY-DEC)
Pace Project No.: 92409169
QC Batch: 445674 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92409169001, 92409169002, 92409169003
METHOD BLANK: 2442987 Matrix: Water
Associated Lab Samples: 92409169001, 92409169002, 92409169003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L ND 5.0 12/05/18 08:59
Pate Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288 '
[phone]
LABORATORY CONTROL SAMPLE:
2442988
Spike LCS
LCS
% Rec
Parameter
Units
Cone. Result
% Rec
Limits
Qualifiers
Oil and Grease
rn91L
40 36.9
92
78-114
MATRIX SPIKE SAMPLE:
2442989
92409103002 Spike
MS
MS
% Rec
Parameter
Units
Result Cone.
Result
% Rec
Limits Qualifiers
Oil and Grease
m91L
ND 40
37.1
92
78-114
Results presented on this page are in the units indicated by the "Ursa" column except where an aftemate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 1210542018 04:48 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 13

ceAnalytical *
wwW4ao6A1b&cam
QUALITY CONTROL DATA
Project: 2018 SEMI-ANNUAL (JULY-DEC)
Pace Project No.: 92409169
QC Batch: 445374 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92409169001, 92409169002, 92409169003
METHOD BLANK: 2441726
Matrix:
Water
Associated Lab Samples:
92409169001, 92409169002, 92409169003
Blank
Reporting
Parameter
Units
Resutt
Limit
Analyzed Qualifiers
Copper
mg/L
ND
0.0050
12/04/18 22:34
Lead
mg/L
ND
0.0050
12/04/18 22:34
Zinc
mg/L
ND
0,010
12/04/18 22:34
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 2441727
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Copper mg1L .5 0.51 102 85-115
Lead mg/L .5 0.49 97 85-115
Zinc mg/L .5 0.48 97 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2441728
2441729
MS
MSD
92409169001 Spike
Spike MS
MSD
MS
MSD
% Rec
Parameter Units Result Cone.
Cone. Result
Result
% Rec
% Rec
limits
RP❑ Qual
Copper mg/L 0.016 .5
.5 0,52
0.52
100
100
70-130
0
Lead mg/L ND .5
.5 0,48
0.48
95
96
70-130
1
Zinc mg/L 0.036 .5
.5 0.52
0.53
96
98
70-130
2
Results presented on this page are in the units Indicated by the "Units- column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/05/2018 04:48 PM without the wntten consent of Pace Analytical Services, LLC. Page 8 of 13

e
IekWcal
(�wrM pacefefteam
QUALITY CONTROL DATA
Project: 2018 SEMI-ANNUAL (JULY DEC)
Pace Project No.: 92409169
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
(336)62"921
QC Batch: 445558
Analysis Method:
SM 254OD-2011
QC Batch Method: SM 25400-2011
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92409169001, 92409169002, 92409169003
METHOD BLANK: 2442638
Matrix: Water
Associated Lab Samples: 92409169001, 92409169002, 92409169o03
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND 1.0 12/04/18 16:54
LABORATORY CONTROL SAMPLE:
2442639
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 234
93 9D-110
SAMPLE DUPLICATE: 2442640
92408685001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 2.2 ND
SAMPLE DUPLICATE: 2442641
Parameter
Total Suspended Solids
92409169003 Dup
Units Result Result
mg1L 11.6 14.6
RPD Qualifiers
23 D6
Results presented on this page are in the units indicated by the -Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report Sha[I not be reproduced, except in ftal.
Date: 121051201.8 04:48 PM without the wntten consent of Pace Analytical Services, LLC. Page 9 of 13

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ceArialytical
rnvw.paoe7ebi.cam
QUALITY CONTROL DATA
Project: 2018 SEMI-ANNUAL (JULY-DEC)
Pace Project No.: 92409169
QC Balch: 445419 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Associated Lab Samples: 92409169001, 92409169002, 92409169003
SAMPLE DUPLICATE: 2441845
92408930001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 7.4 7.4 0 H3
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 272a8
1336j623-8921
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/05/2018 04:48 PM without the written Consent of Pace Analytical Services, LLC.
Page 10 of 13

CBl'1Wa e
ewrrpacebbt:.cnrrr
QUALIFIERS
Project: 2018 SEMI-ANNUAL (JULY--DEC)
Pace Project No.: 92409169
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
Pace Analytical Services, LLC
205 East Meadaw Road - Suite A
Eden, NC 27288 _
[phone]
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Dipheny1hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/05/2018 04:48 PM without the written consent of Pace Analytical Services, L-C. Page 11 of 13

IeAnalAml
wwnpacaW&WW
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288.*
[phone]
Project:
Pace Project No.:
2018 SEMI-ANNUAL (JULY--DEC)
92409169
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92409169001
OUTFALL 91
EPA166413
445674
92409169002
OUTFALL #2
EPA 1664B
445674
92409169003
OUTFALL #3
EPA 1664B
445674
92409169001
OUTFALL #1
EPA 200.7 Rev 4A 1994
445374
EPA 200.7 Rev 4A 1994
445387
92409169002
OUTFALL #2
EPA 200.7 Rev 4.4 1994
445374
EPA 200.7 Rev 4.4 1994
445387
92409169003
OUTFALL #3
EPA 200.7 Rev 4.4 1994
445374
EPA 200.7 Rev 4.4 1994
445387
92409169001
OUTFALL #1
SM 2540D-2011
445558
92409169002
OUTFALL #2
SM 2WD-2011
445558
92409169003
OUTFALL #3
SM 2540D-2011
445558
92409169001
OUTFALL #1
EPA 9040C
445419
92409169002
OUTFALL #2'
EPA 9040C
445419
92409169003
OUTFALL #3
EPA 9040C
445419
Date: 12/05/2018 04:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 13

' .WQ#;92449169
CHAIN -OF -CUSTODY Analytical Request Document LAB USE ONLY•Aff.xWorkorder,
PaceAnalytrcal'
Chain-of-Custodyis a LEGAL DOCUMENT - Complete all relevant fields
Com ny: Billing Information: , 92409169 �+
I �671, l Z{1/ham ALL SHADED A, a
f'�
Ad ss; f 1 ��7/ �� 17i/�'i'k'CC� � ���'
Container Preservative T e' • Lab Project Manager:
u/; �'s, NCr] *� ail 11�C z
Repo q'{
r r L
Email TR•
6[ /%t t , MC(1 �+ f Q I, t`i� l �r1�Y C��
•• Preservative Types: ill nitric acid, (2) sulfuric acid, 13) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol,17) sodium bisulfate, (B) sodium thiosuifate, (9) hexane, JAI ascorbic acld, I ammonium sulfate,
IQ ammonium hydroxide, (DI TSP, JU) Unpreserved, (0) Other
Copy Ty' h
Si a C011e ion Info/Address:
Analyses ILat
Profile Line: r p e,
Customer Project Name/Number; % 1 �I
20i I)G! t./fl "% e7
State: Court�/City: ( Time Zone Collected:
�� / a QrBLI MUIRfYtyi{r I PT ( i MT [ [ CT ET
!
La Sump a Rece pt Chee et
Custody Seale present/Intact N NA
Custody Signatures present NA
Collector Signature Present NA
Bottles Intact N NA
Correct Bottles NA
Sufficient volume NA
Samples Roceivad on Ice
VOA - Beadspace Acceptable Y N
USDA 'Regulated SOLID'tU�'t'eSample■ in Holding Time CY is NA
Pasidual Chlorine Present Y Npilispose
Cl Stripes ^�
Sample p8 Acceptable Y NQD
pN Stripst
Sulfide Present Y N
Lead Acetato Stripat
LAB USE ONLYr
Lab Semple i 1 comments x
Phone;
Email: 1 2 1�
7� a 9
Site/Fatifity ID#:
Compliance Monitoring?
I �t Yes [ ] No
C cted.8y 1 rint):
Purchase Order N:
Quote N. I
OW PWS ID 0:
OW Location Code;
PJetted By (signatu a)*
- f• (% `,
Turnaround Date'Required:Immediately
� I - y�
ace an Ice:
[ ..'s I ] No
mpie Disposal;
as appropriate I I Return
I I archive:
I I Hold.
Rush:
[ Same ay [ ] Next Day
( ] 2 Day I yf 3 Day I 1 4 Day [a45 Day
(Expedite Charges App4yl
Field Filtered (if applicable);
[ I Yes [ ) No
Analysis:
" Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bloassay (8), Vapor IV), Other (OT)
Customer Sample ID
Matrix '
Comp /
Grab
Collected (or
Composite Start)
Composite End
Res
CI
N of
Ctns
Date
Time
Date
Time
iW,
akah
12li
13
1
L/Ut./
Jv
2 I
; J
:/
✓
V
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✓
Customer Remarks / Special Conditions / possible Haiards:
Type of Ice Used:
Slue Dry None
SHORT HOLDS PRESENT (<72 hours): Y N 1 N/A
Lab Sample Temperature Info:
Temp Blank Rec ived• Y NA
Therm IDq:
,
Packing Material Used: t�G�
t
Lab Tracking a: 2341567
Cooler 1 Temp Upon Receipt: oC
-
Radchem sample(s) screened (<500 cpm): Y N N
Samples received via:
FEDEX UPS - Clien Courier Pace Courier
i
Cooler 1 Therm Corr, Factor: 0'0 oC
Cooler 1 Corrected Temp: `r t aC
Comments:
Relinquished by/Company: (Sig at eI
Date/Time:
Received by/Com Cr
Dateppjfi��e:
C7`l/lv
MTJL LAB USE ONLY
Table q:
Atctnum:
Template:
Relinquished by/Company: (Signature)
I
Date/Time:
Received ignatur
Date/Time:
Trip clank Received: Y W NA
Prelogin:
PM;
HCL McOH TSP Other
Relinquished by/Company: (Signature)
Date/Time:
Received by/Company: (Signature)
Date/Time:
FWon-C�arformante(s):
Page:
/
of:

,
N�MR SOUflIwiw
�M
h
December 20, 2017
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Permit No: NCG0300000
Certificate of Coverage: NCG030664
Southwire
12331 Commerce Station Dr.
Huntersville, NC 28078
Dear Sir/Madam:
Please be in receipt of the Qualitative and Analytical Monitoring Data for this facility.
This report covers required sampling for Year 5 — Period 2, Sample 10 .
Thank you,
Allan Oracion
Southwire Huntersville EHS Manager

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 12/19/17
CERTIFICATE OF COVERAGE NO. NCG030664 SAMPLE COLLECTION YEAR 2017
FACILITY NAME Southwire- Huntersville SAMPLE PERIOD ❑ Jan -June ® July -Dec
COUNTY Mecklenburg or ❑ Monthly' (month)
PERSON COLLECTING SAMPLES Allan Oracion DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY Pace Labs Lab Cert. # 12 ❑Zero -flow ❑Water Supply ❑SA
Comments on sample collection or analysis: ®Other C-Waterbod
Part A: Stormwater Benchmarks and Monitoring Results
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
n No discharge this period?'
outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks
-
-
100 mg/L or 50 mg/O
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
10/16/17
.34
<2.5
5.5
<.0050
<.0050
.081
<5
ND, <1 mg/L
2
10/16/17
.34
4.9
7.0
.0099
<.0050
.044
<5
ND, <1 mg/L
3
10/16/17
.34
<2.5
7.4
.0067
<.0050
.017
<5
ND, <1 mg/L
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3
P

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Print title)
(Signature)
(Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Nan -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they, must be reported in the format, "<XX m /i. where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part_ B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?Z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
lnches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =_=>
_
-
1S mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
" See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART If SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an orJ anal and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results or at end of monitoring eriod
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
Permit Date: 11/1/2012-10/31/2017
12/20/2017
(Date)
SWU-245, last revised 10/25/2012
Page 3of3

ceAnap calm
wrwpeceraesmm
3
October 24, 2017
John Moore
Southwire
12331 Commerce Station
Huntersville, NC 28078
RE: Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Dear John Moore:
Pace Ana"ral Services, LLC
205 East Meadow Road - Suite A
Enclosed are the analytical results for sample(s) received by the laboratory on October 16, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
[phone]
Project Manager
Endosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Eden, NC 27208
[phone]
Page 1 of 45

Pace Analytical Services, LLC
® 205 East Meadow Road - Suite A
aceAnalybol Eden, NC 27288
[phone]
i
I
CERTIFICATIONS
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
LouisianalNELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
South Carolina Certification #: 99006001
Fiorida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiafVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 45

aceAnaVical
wwwpacatabs.cum
i
SAMPLE SUMMARY
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92359309001
Outfall 1
Water
10/16/17 09:01
10/16/17 12:10
92359309002
Outfall 2
Water
10/16/17 09:12
10/16/17 12:10
92359309003
Outfall 3
Water
10/16/17 09:25
10/16/17 12:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wrrtlen consent of Pace Analytical SeMces, LLC. Page 3 of 45

•
CeAnalytical
Mw wPaaetabs cam
I
SAMPLE ANALYTE COUNT
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Pace Analytical Services, LLC
205 East Meadow Road - SuiteA
Eden, NC 27288
[phone]
Anafytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92359309001
Outfall 1
EPA 1664B
JMS
1
PASI-C
EPA 608
PKS
27
PASi-C
EPA 200.7
CDF
3
PASI-A
EPA625
RES
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 25400
SLB
1
PASI-A
EPA 9040
MDW
1
PASI-A
92359309002
Outfall 2
EPA 1664B
JMS
1
PASi-C
EPA 608
PKS
27
PASI-C
EPA 200.7
CDF
3
PASI-A
EPA625
RES
58
PASI-C
EPA 624
GAW
34
PASi-C
SM 2540D
SLB
1
PASI-A
EPA 9040
MDW
1
PASI-A
92369309003
Outfall 3
EPA 1664E
JMS
1
PASI-C
EPA 608
PKS
27
PASi-C
EPA 200.7
CDF
3
PASI-A
EPA 625
RES
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
SLB
1
PASI-A
EPA 9040
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
without the written consent of PaceAnalytical Services, LLC. Page 4 of 45

Ce, niw i al
w7w!Pcarrl
l
ANALYTICAL RESULTS
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Sample: Outfall 1 Lab ID. 92369309001 Collected: 10/16/17 09:01 Received: 10/16/17 12:10 Matrix: Water
Report
Parameters Resutts Units Limit MOL DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND
mg/L
5.0
1.1
1
10/24/17 04:59
608 GCS Pesticides and PCBs
Analytical
Method: EPA 608 Preparation Method: EPA 3510
Aldrin
NO
ug/L
0.050
0.050
1
10/16/17 12:00
10=11715:05
309-00-2
alpha-BHC
NO
ug/L
0.050
0.050
1
10116/1712:00
1012011715:05
319-8"
beta-BHC
NO
ug/L
0.050
0.050
1
1011611712:00
10/2011715:05
319-85-7
delta-BHC
ND
uglL
0.050
0.050
1
10/1611712:00
10/2011715:05
319-86-8
gamma-BHC (Lindane)
NO
ug/L
0.050
0.050
1
10/16/17 12:00
10/20/17 15:05
58-89-9
Chlordane (Technical)
NO
ug/L
0.50
0.50
1
10/16/17 12:00
10/20/17 15:06
57-74-9
4,4'-DDD
ND
ug/L
0.050
0.050
1
10/1611712:00
1012011715:05
72-54-8
4,4'-DDE
NO
ug/L
0.050
0.050
1
1011611712:00
10/2011715:05
72-55-9
4,4'-DDT
ND
uglL
0.050
0.050
1
10116/1712:00
1012011715:05
50-29-3
Dieldrin
NO
ug/L
0.050
0.050
1
1011611712:00
1012011715:05
60-57-1
Endosulfan I
NO
ug/L
0.050
0.050
1
10/16/17 12:00
10/20/17 15:05
959-98-8
Endosuffan II
ND
ug/L
0.050
0.050
1
10/16/17 12:00
10/20/17 15:05
33213-65-9
Endosulfan sulfate
NO
ug1L
0.050
0.050
1
10/16/17 12:00
10/20/17 15:05
1031-07-8
Endrin
NO
u91L
0.050
0.050
1
10/16/17 12:00
1012011715:05
72-20-8
Endrin aldehyde
NO
ug/L
0.050
0.050
1
10/16/17 12:00
10/20/17 15:05
7421-93-4
Heptachlor
NO
uglL
0.050
0.050
1
1011611712:00
10120/1715:05
76-44-8
Heptachlor epoxide
NO
uglL
0.050
0.050
1
10/16/17 12:00
10/20/17 15:05
1024-57-3
PCB-1016 (Arodor 1016)
NO
ug/L
0.50
0.50
1
10/16/17 12:00
10/20/17 15:05
12674-11-2
PCB-1221 (Arodor 1221)
NO
ug/L
0.50
0.50
1
10/16/17 12:00
10/20/17 15:05
11104-28-2
PCB-1232 (Arodor 1232)
NO
ug/L
0.50
0.50
1
10/16/17 12:00
10/20/17 15:05
11141-16-5
PCB-1242 (Arodor 1242)
NO
ug/L
0.50
0.50
1
10/16/17 12:00
10/20/17 15:05
53469-21-9
PCB-1248 (Arodor 1248)
NO
ug/L
0.50
0.50
1
10/16/17 12:00
10/20/17 15:05
12672-29-0
PCB-1254 (Arodor 1254)
ND
ug/L
0.50
0.50
1
10/16/17 12:00
10/20/17 15:05
11097-69-1
PCB-1260 (Arodor 1260)
NO
ug/L
0.50
0.50
1
10/16/17 12:00
10/20/17 15:05
11096-82-5
Toxaphene
NO
ug/L
0.50
0.50
1
10/16/17 12:00
10/20/17 15:05
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
71
%
20-110
1
10/16/17 12:00
10/20/17 15:05
877-09-8
Decachlorobiphenyl (S)
26
%
20-138
1
10/16/17 12:00
10/20/17 15:05
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
NO
mg/L
0.0050
0.0025
1
10/18/17 20:15
10/19/17 18:24
7440-50-8
Lead
NO
mg/L
0.0050
0.0025
1
10/1811720A5
10/1911718:24
7439-92-1
Zinc
0.081
mg/L
0.010
0.0025
1
10/18/17 20:15
10/19/17 18:24
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method:
EPA
625
Acenaphthene
NO
ug1L
5.0
0.25
1
10/19/17 15:30
10/2?J17 0050
83-32-9
Aoenaphthyfene
NO
ug/L
5.0
0.21
1
10/19/17 15:30
10/22/17 04:50
248-96-8
Anthracene
NO
ug/L
5.0
0.14
1
10/19/17 15:30
10/22/17 04:50
120-12-7
Senzo(a)anthracene
NO
uglL
5.0
0.33
1
10/19/17 15:30
10/22/17 04:50
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
0.30
1
10/19/17 15:30
10/22/17 04:50
50-32-8
Benzo(b)fluoranthene
NO
ug/L
5.0
0.28
1
10/19/17 15:30
10/22/17 04:50
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
0.38
1
10/19/1715:30
10/2211704:50
191-24-2
Benzo(k)ftuoranthene
NO
ug/L
5.0
0.43
1
10/19/17 15:30
10/22/17 04:50
207-08-9
REPORT OF LABORATORY ANALYSIS
This report shall nat be reproduced, except in full.
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Sendces, LLC.
Page 5 of 45

Pace Analytical Services, LLC
a �+� 6 205 East Meadow Road - SuiteA
av /��} 1►►aVic I Eden, NC 27268
WwW..PWektaoom [phone]
ANALYTICAL RESULTS
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Sample: Outfall 1 Lab Id: 92359309001 Collected: 10116/17 09:01 Received: 10/16117 12:10 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No, Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
4-Bromophenylphenyt ether
ND
ug/L
5.0
0.82
1 10/19/17 15:30
10/22/17 04:50 101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
0.79
1 10/19/17 15:30
10/22/17 04:50 85-68-7
4-Chloro-3-methylphenol
NO
ug/L
5.0
3.7
1 10/19/17 15:30
10/22/17 04:50 59-50-7
bis(2-Chloroethoxy)methane
ND
uglL
10.0
0.92
1 10/19/17 15:30
10/22/17 04:50 111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1.0
1 10/19/17 15:30
10/22/17 04:50 111 44 4
2-Chloronaphthalene
NO
ug/L
5.0
0.98
1 10/19/17 15:30
10/22/17 04:50 91-58-7 L2
2-Chlorophenol
ND
ug/L
5.0
1.3
1 10/19/17 15:30
10/22/17 04:50 95-57-8
4-Chlorophenylphenyt ether
NO
ug/L
5.0
0.87
1 10/19/17 15:30
10/22/17 04:50 7005-72-3
Chrysene
NO
ug/L
5.0
0.21
1 1011911715:30
10/2211704:50 218-01-9
Dibenz(a,h)anthracene
NO
ug/L
5.0
0.55
1 10/19/17 15:30
10/22/17 04:50 53-70-3
3,3'-Dichlorobenzidine
NO
ug/L
25.0
2.1
1 1011911715:30
1012211704:50 91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1.7
1 10/19/17 15:30
10/22/17 04:50 120-83-2
Diethylphthalale
ND
ug/L
5.0
0.58
1 10/19/17 15:30
10/22/17 04:50 84-66-2
2,4-Dimethylphenol
NO
ug/L
10.0
1.2
1 10/19/17 15:30
10/22/17 04:50 105-67-9
Dimethylphthalate
NO
ug/L
5.0
0.76
1 10/19/17 15:30
10/22/17 04:50 131-11-3
Di-n-butytphthalate
ND
ug/L
5.0
0.75
1 10/19/17 15:30
10/22/17 04:50 84-74-2
4,6-Dinitro-2-rnethylphenol
ND
ug/L
20.0
2.6
1 10/19/17 15:30
10/22/17 04:50 534-52-1
2,4-Dinitrophenol
NO
ug/L
50.0
9.0
1 10/19/17 15:30
10/22/17 04:50 51-28-5
2,4-Dinitrotoluene
NO
ug/L
5.0
0.90
1 10/19/17 15:30
10/22/17 04:50 121-14-2
2,6-Dinitrotoluene
NO
ug/L
5.0
0.98
1 10/19/17 15:30
10/22/17 04:50 606-20-2
Di-n-octytphthalate
ND
ug/L
5.0
0.66
1 10/19/17 15:30
10/22/17 04:50 117-84-0
bis(2-Ethylhexyl)phthatate
ND
ug/L
5.0
0.79
1 10/19/17 15:30
10/22/17 04:50 117-81-7
Fluoranthene
NO
ug/L
5.0
0.21
1 10/19/17 15:30
10/22/17 04:50 206-44-0
Fluorene
NO
ug/L
5.0
0.21
1 10/19/17 15:30
10/22/17 04:50 86-73-7
Hexachloro-1.3-butadiene
ND
ug/L
5.0
0.94
1 10/19/17 15:30
10/22/17 04:50 87-68-3
Hexachlorobenzene
ND
ug/L
5.0
0.72
1 10/19/17 15:30
10/22/17 04:50 118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
0.88
1 10/19/17 15:30
10/22/17 04:50 77-47-4
Hexachloroethane
NO
ug/L
5.0
1.1
1 10/19/17 15:30
10/22/17 04:50 67-72-1 L2
Indeno(1,2,3-od)pyrene
NO
ug/L
5.0
0.29
1 10/1911715:30
10122/1704:50 193-39-5
Isophorone
ND
ug/L
10.0
0.89
1 10/19/17 15:30
10/22/17 04:50 78-59-1
Naphthalene
ND
ug/L
5.0
0.34
1 10/19/17 15:30
10/22/17 04:50 91-20-3
Nitrobenzene
ND
ug/L
5.0
1.1
1 10/19/17 15:30
10/22/17 04:50 98-95-3
2-Nitrophenol
ND
ug/L
5.0
0.91
1 10/19/17 15:30
10/22/17 04:50 88-75-5
4-Nitrophenol
NO
ug/L
50.0
4.1
1 10/19/17 15:30
10/22/17 04:50 100-02-7
N-Nitrosodimethylamine
NO
ug/L
5.0
0.91
1 10/19/17 15:30
10/22/17 04:50 62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
0.99
1 10/19/17 15:30
10/22/17 04:50 621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1.0
1 10/19/17 15:30
10/22/17 04:50 86-30-6
2,2'-Oxybis(l-chloropropane)
ND
ug/L
5.0
0.95
1 10/19/17 15:30
10/22/17 04:50 108-60-1
Pentachlorophenol
NO
ug/L
10.0
4.6
1 10/19/17 15:30
10/22/17 04:50 87-86-5
Phenanthrene
ND
ug/L
5.0
0.22
1 10/19/17 15:30
10/22/17 04:50 85-01-8
Phenol
NO
ug/L
5.0
1.9
1 10/19/17 15:30
10/22/17 04:50 108-95-2
Pyrene
NO
ug/L
5.0
0.19
1 10/19/17 15:30
10/22/17 04:50 129-00-0
1,2,4-Trtchlorobenzene
NO
ug/L
5.0
0.98
1 10119/1715:30
10122/1704:50 120-82-1
2,4,6-Trichlorophenol
NO
uglL
10.0
1.3
1 10/19/17 15:30
10/22/17 04:50 88-06-2
Surrogates
Nitrobenzene-d5 (S)
27
%
10-120
1 10/19/17 15:30
10/22/17 04:50 4165-60-0
REPORT
OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
Date: 10/24/2017 03:06 PM
without the written conserd of Pace Analytical
Services, LLC.
Page 6 of 45

Pace Analytical Services, LLC
® 205 East Meadow Road - Suite A
aceMafytfcai Eden, NC 27288
rnrwpscelabs.cam [phone]
ANALYTICAL RESULTS
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Sample: Outfali 1 Lab ID: 92359309001 Collected: 10/16/17 09:01 Reoeived: 10/16/17 12:10 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Surrogates
2-Fluorobiphenyl (S)
22
%
15-120
1
10/19/17 15:30
10/22/17 04:50 321-W8
Terphenyl-014 (S)
67
%
11-131
1
10/19/17 15:30
10/22/17 04:50 1718-51-0
Phenol-d6 (5)
8
%
10-120
1
10/19/17 15:30
10/22/17 04:50 13127-88-3 SO
2-Fluorophenol (S)
13
%
10-120
1
10/19/17 15:30
10122/17 04:50 367-12-4
2,4,6-Tribromophenol (S)
47
%
10-137
1
10/19/17 15:30
10122J17 04:50 118-79-6
624 Volatile Organics
Analytical
Method: EPA 624
Benzene
NO
uglL
2.0
1.7
1
10119/1703:19 71-43-2
Bromodichloromethane
ND
ug1L
2.0
1.7
1
1011911703:19 75-27-4
Bromoform
ND
ug1L
2.0
1.5
1
10/19/17 03:19 75-25-2
Bromomethane
ND
ug/L
2.0
1.0
1
10/19117 03:19 74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1.9
1
10/19/17 03:19 56-23-5
Chlorobeazene
ND
ug1L
2.0
1.7
1
10/19/17 03:19 108-90-7
Chloroethane
ND
ug/L
2.0
1.6
1
10/1911703:19 75-00-3
Chloroform
NO
ug/L
2.0
1.9
1
10/19/17 03:19 67-66-3
Chioromethane
ND
ug/L
2.0
1.5
1
10/19/17 03:19 74-87-3
Dibromochioromethane
ND
ug1L
2.0
1.8
1
10119/1703:19 124-48-1
1,2-Dichloroberzene
ND
ug1L
2.0
1.5
1
10/19/17 03:19 95-50-1
1,3-Dichlorobenzene
ND
ug&
2.0
1.5
1
10119/1703:19 541-73-1
1,4-Dichlorobenzene
ND
uglL
2.0
1.5
1
10119/1703:19 106-46-7
1,1-Dichloroethane
ND
ug1L
2.0
1.8
1
10/1911703:19 75-34-3
1,2-Dichloroethane
NO
ug1L
2.0
1.6
1
10/1911703:19 107-06-2
1,1-Dichloroethene
NO
ug1L
2.0
1.9
1
10/1911703:19 75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
1.8
1
10/1911703:19 156-59-2
trans-1,2-Dichloroethene
ND
ug1L
2.0
1.8
1
1011911703:19 156-60-5
1,2-Dichloropropane
ND
uglL
2.0
1.7
1
10/19/17 03:19 78-87-5
ds-1,3-Dichloropropene
ND
ug/L
2.0
1.6
1
1OM9/1703:19 10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
2.0
1.6
1
10/19/17 03:19 10061-02-6
Ethylbenzene
ND
ug1L
2.0
1.6
1
10/19/17 03:19 100-41-4
Methylene Chloride
ND
ug/L
2.0
1.9
1
10/19/17 03:19 75-09-2
1,1,2,2-Tetrachloroethane
NO
ug1L
2.0
1.5
1
10119/1703:19 79-34-5
Tetrachloroethene
NO
ug1L
2.0
1.8
1
10/19/17 03:19 127-18-4
Toluene
NO
ug1L
2.0
1.6
1
10/19/17 03:19 108-88-3
1,1,1-Trichloroethane
NO
ug/L
2.0
1.9
1
10/19/17 03:19 71-55-6
1,1,2-Trichloroethane
NO
ug/L
2.0
1.7
1
10/19/17 03:19 79-00-5
Trichloroethene
ND
ug/L
2.0
1.8
1
10/19/17 03:19 79-01-6
Trichlorofluoromethane
ND
ug/L
2.0
1.7
1
10/19/17 03:19 75-69-4
Vinyl chloride
ND
ug1L
2.0
1.5
1
10/19/17 03:19 75-01-4
Sumnates
4-Bromofluorobenzene (S)
110
%
7D-130
1
10/19/17 03:19 46MO-4
Toluene-d8 (S)
109
%
70-130
1
10/19/17 03:19 2037-26-5
1,2-Dichloroethane-d4(S)
84
%
70-130
1
10119/1703:19 17060-07-0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids NO mglL 2.5 2.5 1 10/17/17 11:04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:05 PM without the written consent of Pace Analytical Services, LLC, Page 7 of 45

aceAnaVical
wwwpacebblcom
i
ANALYTICAL RESULTS
Pace Analyticai Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: AMEX 2017 Jury -Dec Semi Annual
Pace Project No.: 92359309
Sample: Outfall 1 Lab ID: 92359309001 Collected: 10/16/17 09:01 Received: 10/16/17 12:10 Matrix: Water
Report
Parameters Results Units Limit MOIL DF Prepared Analyzed CAS No. Qual
9040 pH
pH
Analytical Method: EPA 9040
5.5 Std. Units 0.10 0.10 1
10/17117 00:25 H6
Sample: Outfall 2 Lab ID: 92359309002 Collected: 10116/17 09:12 Received: 10116117 12:10 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Quaff
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease
608 GCS Pesticides and PCBs
Aldrin
alpha-BHC
beta-BHC
detia-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
4,4'-DDO
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
PCB-1016 (Arodor 1016)
PCB-1221 (Arodor 1221)
PCB-1232 (Arodor 1232)
PCB-1242 (Arodor 1242)
PCB-1248 (Arodor 1248)
PCB-1254 (Arodor 1254)
PCB-1260 (Arodor 1260)
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Denachlorobiphenyl (S)
ND mg1L 5.0 1.1 1 10/24/17 04:59
Analytical Method: EPA 608 Preparation Method: EPA 3510
NO
ug/L
0,050
0.050
1
10/1611712:00
10/20/1715:55 309-00-2
NO
ug1L
0.050
0.050
1
1011611712:00
1012011715:55 319-84-0
NO
ug/L
0.050
0.050
1
10/16/1712:00
10/20/1715:55 319-85-7
NO
ug/L
0.050
0,050
1
10/16/17 12:00
10/20/17 15:55 319- "
NO
ug/L
0.050
0.050
1
10/16/17 12:00
10/20M 7 15:55 58-89-9
NO
ug/L
0.50
0.50
1
10/1611712:00
10120/1715:55 57-74-9
NO
ug/L
0.050
0.050
1
10116/1712:00
10120/1715:55 72-54-8
ND
ug/L
0.050
0.050
1
10/16/1712:00
10/20/1715:55 72-55-9
NO
ug/L
0.050
0.050
1
10116/1712:00
10/20/1715:55 50-29-3
NO
ug/L
0.050
0.050
1
10/16/1712:00
10120/1715:55 60-57-1
ND
ug/L
0.050
0.050
1
10/16/1712:00
10120/1715:55 959-98-8
NO
ug/L
0.050
0.050
1
10/16/1712:00
10120/1715:55 33213-65-9
NO
ug/L
0.050
0.050
1
10116/1712:00
10/20/1715:55 1031-07-8
NO
ug/L
0.050
0.050
1
10/1611712:00
10120/1715:55 72-20-8
NO
ug/L
0.050
0.050
1
10/16/1712:00
10120/1715:55 7421-93-4
NO
ug/L
0.050
0.050
1
10116/1712:00
10/20/1715:55 76-44-8
ND
ug/L
0.050
0.050
1
10116/1712:00
10/20/1715:55 1024-57-3
NO
uglL
0.50
0.50
1
10116/1712:00
10120/1715:55 12674-11-2
NO
ug/L
0.50
0.50
1
10/1611712:00
1012011715:55 11104-28-2
NO
ug/L
0.50
0.50
1
10116/1712:00
10/20/1715:55 11141-16-5
NO
ug/L
0.50
0.50
1
1011611712:00
10/2011715:55 53469-21-9
NO
ug/L
0.50
0.50
1
10/1611712:00
10120/1715:55 12672-29-6
NO
ug/L
0.50
0.50
1
1011611712:00
10/2011715:55 11097-69-1
NO
ug/L
0.50
0.50
1
10/16/1712:00
10/20/1715:55 11096-82-5
NO
ug1L
0.50
0.50
1
10/16/1712:00
10120/1715:55 8001-35-2
77
%
20-110
1
10116/1712:00
10/20/1715:55 877-09-8
33
%
20-138
1
1011611712:00
10/2011715:55 2051-24-3
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper 0.0099 mg1L 0.0050 0.0025 1 10/18/17 20:15 10/19/17 18:28 7440-50-8
Lead NO mg1L 0.0050 0,0025 1 10/18/17 20:15 10/19/17 18:28 7439-92-1
Zinc 0.044 mg/L 0.010 0,0025 1 ' 10118/17 20:15 10/19/17 18:28 7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of PaceAnalytical Services, LLC. Page 8 of 45

aXAnaVkail
wwwpacefaes cam
f
ANALYTICAL RESULTS
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Sample: Outfall 2 Lab ID: 92369309002 Collected: 10/16/17 09:12
Report
Parameters
625 MSSV
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,hJ)perylene
Benzo(k)fluoranthene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chiorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalale
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthatate
bis(2-Ethylhexyf)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexa hlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-0xybis(1-chloropropane)
Results Units Limit MDL DF
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Received: 1011611712:10 Matrix: Water
Analytical Method: EPA 625 Preparation Method: EPA 625
ND
ug/L
5.0
0.25
1 1
ND
ug/L
5.0
0.21
1 1
ND
ug1L
5.0
0.14
1 1
ND
ug1L
5.0
0.33
1 1
ND
ug/L
5.0
0.30
1 1
ND
ug/L
5.0
0.28
1 1
ND
ug1L
5.0
0.38
1 1
ND
ug/L
5.0
0.43
1 1
ND
ug/L
5.0
0.82
1 1
ND
UA
5.0
0.79
1 1
ND
ug/L
5.0
3.7
1 1
ND
ug/L
10.0
0.92
1 1
ND
ug/L
5.0
1.0
1 1
ND
ug/L
5.0
0.98
1 1
ND
uglL
5.0
1.3
1 1
ND
ug/L
5.0
0.87
1 1
ND
ug/L
5.0
0.21
1 1
ND
ug/L
5.0
0.55
1 1
ND
ug/L
25.0
2.1
1 1
ND
ug1L
5.0
1.7
1 1
ND
ug/L
5.0
0.58
1 1
ND
ug1L
10.0
1.2
1 1
ND
ug/L
5.0
0.76
1 1
ND
ug/L
5.0
0.75
1 1
ND
uglL
20.0
2.6
1 1
ND
ug/L
50.0
9.0
1 1
ND
ug/L
5.0
0.90
1 1
ND
ug/L
5.0
0,98
1 1
ND
ug/L
5.0
0.66
1 1
ND
ug/L
5.0
0.79
1 1
ND
ug1L
5.0
0.21
1 1
ND
uglL
5.0
0,21
1 1
ND
ug1L
5.0
0.94
1 1
ND
ug/L
5.0
0.72
1 1
ND
uglL
10.0
0.88
1 1
N❑
UA
5.0
1 A
1 1
ND
ug/L
5.0
0.29
1 1
ND
uglL
10.0
0.89
1 1
ND
ug/L
5.0
0.34
1 1
ND
ug/L
5.0
1.1
1 1
ND
ug/L
5.0
0.91
1 1
ND
ug/L
50.0
4.1
1 1
ND
ug/L
5.0
0.91
1 1
ND
ug/L
5.0
0.99
1 1
ND
ug/L
10.0
1.0
1 1
ND
ug/L
5.0
0.95
1 1
Prepared Analyzed CAS No. Qual
0/19117 15:30 10/22/17 05:17 83-32-9
0/19117 15:30 10/22/17 05:17 208-96-8
0I19117 15:30 10/22/17 05:17 120-12-7
0119117 15:30 10/22/17 05:17 56-55-3
0119117 15:30 10/22/17 05:17 50-32-8
01191171&30 1012211705:17 205-99-2
D/19I17 15:30 10/22/17 05:17 191-24-2
0119117 15:30 10/22/17 05:17 207-08-9
0119117 15:30 10/22/17 05:17 101-55-3
0119/17 15:30 10/22/17 05:17 85-68-7
0/19117 15:30 10/22/17 05:17 59-50-7
0/19/17 15:30 10/22/17 05:17 111-91-1
0119117 15:30 10/22/17 05:17 11144 4
OI19117 15:30 10/22/17 05:17 91-58-7
0119117 15:30 10/22/17 05:17 95-57-8
0l19/17 15:30 10/22/17 05:17 7005-72-3
D119117 15:30 10/22/17 05:17 218-01-9
0119117 15:30 10/22/17 05:17 53-70-3
0119117 15:30 10/22/17 05:17 91-94-1
0119117 15:30 10/22/17 05:17 120-83-2
0119117 15:30 10/22/17 05:17 84-06-2
0119117 15:30 10/22/17 05:17 105-07-9
0119117 15:30 10/22/17 05:17 131-11-3
0119117 15:30 10/22/17 05:17 84-74-2
0119117 15:30 10/22/17 05:17 534-52-1
0119/17 15:30 10/22/17 05:17 51-28-5
0119117 15:30 10/22/17 05:17 121-14-2
0/19117 15:30 10/22/17 05:17 606-20-2
0119117 15:30 10/22/17 05:17 117-84-0
0/19/17 15:30 10/22/17 05:17 117-81-7
0l19117 15:30 10/22/17 05:17 206-44-0
0119/17 15:30 10/22/17 05:17 86-73-7
0I19/17 15:30 10/22/17 05:17 87-68-3
0I19/17 15:30 10/22/17 05:17 118-74-1
0l19/17 15:30 10/22/17 05:17 77-47-4
0119117 15:30 10/22/17 05:17 67-72-1
0I1911715:30 10/22/17 05:17 193-39-5
0I1911715:30 10/22/17 05:17 78-59-1
0119117 15:30 10/22/17 05:17 91-20-3
0119/17 15:30 10/22/17 05:17 98-95-3
0119117 15:30 10/22/17 05:17 88-75-5
0/19l17 15:30 10/22/17 05:17 100-02-7
0119/17 15:30 10/22/17 05:17 62-75-9
0l19117 15:30 10/22117 05:17 621-64-7
0/19117 15:30 10/22/17 05:17 86-30-6
0I19/17 15.30 10/22/17 05:17 108-60-1
REPORT OF LABORATORY ANALYSIS
M
L2
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 45
REPORT OF LABORATORY ANALYSIS
M
L2
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 45

e
CeAnalyfical
www.p9ce1abs.c0m
ANALYTICAL RESULTS
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Outfall 2 Lab ID: 92359309002 Collected: 10/16/17 09:12 Received: 10/16/17 12:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Pentachlorophenol
ND
ug/L
10.0
4.6
1
10/19/17 15:30
10/22/17 05:17
87-86-5
Phenanthrene
ND
uglL
5.0
0.22
1
1011911715:30
10/22/17 05:17
85-01-8
Phenol
ND
ugll_
5.0
1.9
1
10/19/17 15:30
10/22/17 05:17
108-95-2
Pyrene
ND
ug/L
5.0
0.19
1
10/19/17 15,30
10/22/17 05:17
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
0.98
1
10/19/17 15:30
10/22/17 05:17
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1.3
1
10119/1715:30
10/22/17 05:17
88-06-2
Surrogates
Nitrobenzene-d5 (S)
33
%
10-120
1
10/19/17 15:30
10/22/17 05:17
4165-60-0
2-Fluorobiphenyl (S)
36
%
15-120
1
10/19/17 15:30
10/22/17 05:17
321-60-8
Terphenyl-04 (S)
87
%
11-131
1
1011911715:30
10/22/17 05:17
1718-51-0
Phenol-d6 (S)
13
%
10-120
1
10/1911715:30
10/22/17 05:17
13127-88-3
2-Fluorophenol (S)
17
%
10-120
1
10/19/17 15:30
10/22/17 05:17
367-12-4
2,4,6-Tribromophenol (S)
84
%
10-137
1
10/19/17 15:30
10/22/17 05:17
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
NO
ug/L
2.0
1.7
1
10/19/17 03:36
71-43-2
Bromodichloromethane
NO
ug/L
2.0
1.7
1
10/19117 03:36
75-27-4
Bromoform
ND
ug/L
2.0
1.5
1
10/19/17 03:36
75-25-2
Bromomethane
ND
ug/L
2.0
1.0
1
10/19/17 03:36
74-83-9
Carbon tetrachloride
ND
ug1L
2.0
1.9
1
10/19/17 03:36
56-23-5
Chlorobenzene
ND
ug/L
2.0
1.7
1
10/19/17 03:36
108-90-7
Chloroethane
ND
ug/L
2.0
1.6
1
10/19/17 03:36
75-00-3
Chloroform
ND
ug/L
2.0
1.9
1
10/19/17 03:36
67-06-3
Chloromethane
ND
ug/L
2.0
1.5
1
10/19/17 03:36
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1.8
1
10/19/17 03:36
124-48-1
1,2-Dichlorobenzene
ND
ug1L
2.0
1.5
1
10/19/17 03:36
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1.5
1
10/19/17 03:36
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1.5
1
10/19/17 03:36
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1.8
1
10/19/17 03:36
75-34-3
1,2-Dichloroethane
ND
ug1L
2.0
1.8
1
10/19/17 03:36
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1.9
1
10/19/17 03:36
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
1.8
1
10/19/17 03:36
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
1.8
1
10/19/17 03:36
156-60-5
1 Z-Dichloropropane
ND
ug/L
2.0
1.7
1
10/19/17 03:36
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1.6
1
10/19/17 03:36
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
2.0
1.6
1
10/19/17 03:36
10061-02-6
Ethylbenzene
ND
ug/L
2.0
1.6
1
10/19/17 03:36
100-41-4
Methylene Chloride
ND
ug/L
2.0
1.9
1
10/19/17 03:36
75-09-2
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1.5
1
10119/1703:36
79-34-5
Tetrachloroethene
ND
ug/L
2.0
1.8
1
10/19/17 03:36
127-18-4
Toluene
ND
ug/L
2.0
1.6
1
10/19/17 03:36
108-88-3
1,1,1-Trichloroethane
ND
ug/L
2.0
1.9
1
1011911703:36
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1.7
1
10/19/17 03:36
79-00-5
Trichloroethene
ND
ug/L
2.0
1.8
1
1011911703:36
79-01-6
Trichlorofluoromethane
ND
uglL
2.0
1.7
1
10/19/17 03:36
75-69-4
Vinyl chloride
ND
ug/L
2.0
1.5
1
10/19/17 03:36
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 45

1�?ceAnaVical*
wwwpacehab&cam
r
i
ANALYTICAL RESULTS
Pace Analytical Services, llC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: AMEX 2017 July -Dec Semi Annual
A
Pace Project No.: 92359309
Sample: Outfall 2 Lab ID: 92359309002 Collected: 10116/17 09:12 Received: 10/16/17 12:10 Matrix: Water
Report
Parameters Results Units Limit MDL DP Prepared Analyzed CAS No. Qual
624 Volatile Organics
Surrogates
4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-ii4 (S)
2540D Total Suspended Solids
Total Suspended Solids
9040 pH
pH
Analytical Method: EPA 624
98 % 70-130
1
10/19/17 03:36 460-00-4
110 % 70-130
1
10/19/17 03:36 2037-26-5
93 % 70-130
1
10/19/17 03:36 17060-07-0
Analytical Method: SM 2540D
4.9 mg1L 2.8
2.8 1
1011711711:05
Analytical Method: EPA 9040
7.0 Std. Units 0.10
0.10 1
10/17/17 00:25 H6
Sample: Outfall 3 Lab ID: 92359309003 Collected: 10116/17 09:25 Received: 10/16/17 12:10 Matrix: Water
Report
Parameters Results Units Limit MDL DP Prepared Analyzed CAS No. Qua]
HEM, Oil and Grease
Oil and Grease
608 GCS Pesticides and PCI3s
Ald rin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan 11
Endosulfan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epox]de
PCB-1016 (Arodor 1016)
PCB-1221 (Arodor 1221)
PCB-1232 (Arodor 1232)
PCB-1242 (Arodor 1242)
PCB-1248 (Arodor 1248)
PCB-1254 (Arodor 1254)
PCB-1260 (Arodor 1260)
Toxaphene
Date: 1012412017 03:06 PM
Analytical Method: EPA 1664B
ND mg1L 5.0 1 A 1 10/24/17 D4:59
Analytical Method: EPA 608 Preparation Method: EPA 3510
ND
ug/L
0.050
0.050
1
10116/1712:00
10120/1716:30 309-00-2
ND
ug/L
0.050
0.050
1
10116/1712:00
10/2011716:30 319-84-6
ND
ug/L
0.050
0.050
1
10/16/1712:00
10/2011716:30 319-85-7
ND
ug/L
0.050
0.050
1
10/16/1712:00
1012011716:30 319-86-8
ND
ug/L
0.050
0.050
1
10/16/1712:00
10/20/1716:30 58-89-9
ND
ug/L
0.50
0.50
1
10/1611712:00
1012011716:30 57-74-9
ND
ug/L
0.050
0.050
1
1011611712.00
10120/1716:30 72-54-8
ND
ug/L
0,050
0.050
1
1011611712:00
10/20/1716:30 72-55-9
ND
ug/L
0.050
0.050
1
10116/1712:00
10120/1716:30 50-29-3
ND
ug/L
0.050
0.050
1
1011611712:00
10120/1716:30 60-57-1
ND
ug1L
0.050
0.050
1
1011611712:00
10120/1716:30 959-98-8
ND
ug/L
0.050
0.050
1
1011611712:00
10120/1716:30 33213-65-9
ND
ug1L
0.050
0.050
1
10/16/1712:00
10120/1716:30 1031-07-8
ND
ugR
0.050
0.050
1
10/1611712:00
10120/1716:30 72-20-8
ND
ug/L
0.050
0.050
1
10/16/1712:00
10/2011715:30 7421-93-4
ND
ugR
0.050
0.050
1
10/1611712:00
1012011716:30 76-44-8
ND
ugR
0.050
0.050
1
10/1611712:00
10/2011716:30 1024-57-3
ND
ug1L
0.50
0.50
1
10/16/1712:00
10/20/1716:30 12674-11-2
ND
ug/L
0.50
0.50
1
10116/1712:00
10120/1716:30 11104-28-2
ND
ug/L
0.50
0.50
1
10/1611712:00
10120/1716:30 11141-16-5
ND
uglL
0.50
0.50
1
10/16/1712:00
10120/1716:30 53469-21-9
ND
ug/L
0.50
0.50
1
1011611712:00
10120/1716:30 12672-29-6
ND
ug1L
0.50
0.50
1
10/16/1712:00
1012011716:30 11097-69-1
ND
ug/L
0.50
0.50
1
1011611712:00
10120/1716:30 11096-82-5
ND
ug/L
0.50
0.50
1
10/1611712:00
10/2011716:30 8001-35-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Anal0cal Serwoes, LLC.
Page 11 of 45

aceAnalytical
www.pwdabs.com
f
ANALYTICAL RESULTS
Pace Anatytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: AMEX 2017 Juty-Dec Semi Annual
Pace Project No.: 92359309
Sample: Outfall 3
Lab ID: 92359309003
Collected:
10/16/17 09:25
Received: 10116117 12:10 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA 3510
Surrogates
Tetrachloro-m-xytene (S)
66
%
20-110
1
10/16/17 12:00
10/20/17 16:30
877-09-8
Decachlorobiphenyl (S)
36
%
20-138
1
10/16/17 12:00
10/20/17 16:30
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method:
EPA 200.7
Copper
0.0067
mg1L
0.0050
0.0025
1
10/18/17 20:15
10/19/17 18:31
7440-50-8
Lead
NO
mg/L
0.0050
0.0025
1
10/18/17 2015
10/19/17 18:31
7439-92-1
Zinc
0.017
mg/L
0.010
0.0025
1
10/18/17 20:15
10/19/17 18:31
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND
ug/L
5.0
0.25
1
10/19/17 15:30
10/22/17 05:45
83-32-9
Acenaphthylene
NO
ug/L
5.0
0.21
1
10/19/17 15:30
10/22/17 05:45
208-96-8
Anthracene
NO
ug/L
5.0
0.14
1
10/19/17 15:30
10/22/17 05:45
120-12-7
Benzo(a)anthracene
NO
ug/L
5.0
0.33
1
10/19/17 15:30
10/22/17 05:45
56-55-3
Benzo(a)pyrene
NO
ug/L
5.0
0.30
1
10/19/17 15:30
10/22/17 05:45
50-32-8
Benzo(b)fluoranthene
NO
uglL
5.0
0.28
1
10/19/17 15:30
10/22/17 05:45
205-99-2
Benzo(g,h,i)perylene
NO
ug/L
5.0
0.38
1
10/19/17 15:30
10/22/17 05:45
191-24-2
Benzo(k)fluoranthene
NO
ug/L
5.0
0.43
1
10/19/17 15:30
10/22/17 05:45
207-08-9
4-Bromophenylphenyl ether
NO
ug/L
5.0
0.82
1
10/19/17 15:30
10/22/17 05:45
101-55-3
Butylbenzylphthalate
NO
ug/L
5.0
0.79
1
10/19/17 15:30
10/22/17 05:45
85-68-7
4-Chloro-3-methylphenol
NO
ug/L
5.0
3.7
1
10/19/17 15:30
10/22/17 05:45
59-50-7
bis(2-Chloroetttioxy)methane
NO
ug/L
10.0
0.92
1
10/19/17 15:30
10/22/17 05:45
111-91-1
bis(2-Chioroethyl) ether
NO
ug/L
5.0
1.0
1
10/19/17 15:30
10/22/17 05:45
111 44 4
2-Chloronaphthalene
NO
ug/L
5.0
0.98
1
10/19/17 15:30
10/22/17 05:45
91-58-7 L2
2-Chlorophenol
ND
ug/L
5.0
1.3
1
10/19/17 15:30
10/22/17 05:45
95-57-8
4-Chlorophenylphenyl ether
NO
ug/L
5.0
0.87
1
10/19/17 15:30
10/22/17 05:45
7005-72-3
Chrysene
ND
ug/L
5.0
0.21
1
10/19/17 15:30
10/22/17 05:45
218-01-9
Dibenz(a,h)anthracene
NO
ug/L
5.0
0.55
1
10/19/17 15:30
10/22/17 05:45
53-70-3
3,3'-Dichlorobenzidine
NO
ug/L
25.0
2.1
1
10/19/17 15:30
10/22/17 05:45
91-94-1
2,4-Dichlorophenol
NO
ug/L
5.0
1.7
1
10/19/17 15:30
10/22/17 05:45
120-83-2
Diethylphthalate
NO
ug/L
5.0
0.58
1
10/19/17 15:30
10/22/17 05:45
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1.2
1
10/19/17 15:30
10/22/17 05:45
105-07-9
Dimethylphthalate
NO
uglL
5.0
0.76
1
10/19/17 15:30
10/22/17 05:45
131-11-3
Di-n-butylphthalate
NO
ug/L
5.0
0.75
1
10/19/17 15:30
10/22/17 05:45
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
2.6
1
10/19/17 15:30
10/22/17 05:45
534-52-1
2,4-Dinitrophenol
NO
ug/L
50.0
9.0
1
10/19/17 15:30
10/22/17 05:45
51-28-5
2,4-Dinitrotoluene
NO
ug/L
5.0
0.90
1
10/19/17 15:30
10/22/17 05:45
121-14-2
2,6-Dinitrotoluene
NO
ug/L
5.0
0.98
1
10/19/17 15:30
10/22/17 05:45
606-20-2
Di-n-octylphthalate
NO
ug/L
5.0
0.66
1
10/19/17 15:30
10/22/17 05:45
117-84-0
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
0.79
1
10/19/17 15:30
10/22/17 05:45
117-81-7
Fluoranthene
NO
ug1L
5.0
0.21
1
10/19/17 15:30
10/22/17 05:45
206-44-0
Fluorene
NO
ug/L
5.0
0.21
1
10/19/17 15:30
10/22/17 05:45
86-73-7
Hexachloro-1,3-butadiene
NO
uglL
5.0
0.94
1
10/19/17 15:30
10/22/17 05:45
87-68-3
Hexachlorobenzene
NO
ug/L
5.0
0.72
1
10/19/17 15:30
10/22/17 05:45
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
0.88
1
10/19/17 15:30
10/22/17 05:45
77-47-4
Hexachloroethane
NO
ug/L
5.0
1.1
1
10/19/17 15:30
10/22/17 05:45
67-72-1 L2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of PaceAnalytical 5eMces, L-C. Page 12 of 45

Pace Analytical Services, LLC
/�a /� lil ,, �.�/ 205 East Meadow Road - Suite A
l+G alyfi a Eden, NC 27288
1 www.Pxelabacam [phone]
i
ANALYTICAL RESULTS
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Sample: Outtall 3 Lab ID: 92359309003 Collected: 10/16/17 09:25 Received: 10/16/17 12:10 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Indeno(1,2,3-cd)pyrene
NO
ug/L
5.0
0.29
1
10119/17 15:30
10/22/17 05:45 193-39-5
Isophorone
NO
ug/L
10.0
0.89
1
10/19/17 15:30
10/22/17 05:45 78-59-1
Naphthalene
NO
ug/L
5.0
0.34
1
10/19/17 15:30
10/22/17 05:45 91-20-3
Nitrobenzene
NO
uglL
5.0
1.1
1
10/19/17 15:30
10/22/17 05:45 98-95-3
2-Nitrophenol
NO
ug/L
5.0
0.91
1
10/19/17 15:30
10/22/17 05:45 88-75-5
4-Nitrophenol
ND
ug/L
50.0
4.1
1
10/19/17 15:30
10/22/17 05:45 100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
0.91
1
10/19/17 15:30
10/22/17 05:45 62-75-9
N-Nitrosodi-n-propylarnme
NO
ug1L
5A
0.99
1
10/19/17 15:30
10/22117 05:45 621-64-7
N-Nitrosodiphenylamine
ND
ug1L
10.0
1.0
1
10/19/17 15:30
10/22117 05:45 86-30-6
2,2'-Oxybis(1-chloropropane)
NO
ug1L
5.0
0,95
1
10/19/17 15:30
10/22/17 05:45 108-60-1
Pentachlorophenol
NO
ug/L
10.0
4.6
1
10/19/17 15:30
10/22/17 05:45 87-86-5
Phenanthrene
NO
ug/L
5.0
0,22
1
10119/1715:30
10/22/17 05:45 85-01-8
Phenol
NO
ug/L
5.0
1.9
1
10/19/17 15:30
10/22/17 05:45 108-95-2
Pyrene
ND
ug/L
5.0
0.19
1
10/19/17 15:30
10/22/17 05:45 129-00-0
1,2,4-Trichlorobenzene
NO
ug1L
5.0
0.98
1
10/19/17 15:30
10/22/17 05:45 120-82-1
2,4,6-Trichlorophenol
NO
ug/L
10.0
1.3
1
10/19/17 15:30
10/22/17 05:45 88-0&2
Surrogates
Nitrobenzene-05 (S)
35
%
10-120
1
10/19/17 15:30
10122/17 05A5 4165-60-0
2-Fiuorobiphenyl (S)
32
%
15-120
1
10/19/17 15:30
10/22/17 05:45 321-60-8
Terphenyl-d14 (S)
81
%
11-131
1
10/19/17 15:30
10/22/17 05:45 1718-51-0
Phenol-06 (S)
12
%
10-120
1
10/19/17 15:30
10/22/17 05:45 13127-88-3
2-Fluorophenol (S)
18
%
10-120
1
10/19/17 15:30
101M17 05:45 367-12-4
2,4,6-Tribromophenol (S)
77
%
10-137
1
10/19/17 15:30
10/22117 05:45 118-7"
624 Volatile Organics
Analytical Method: EPA 624
Benzene
NO
ug1L
2.0
1.7
1
10/19/17 03:53 71-43-2
Bromodichloromethane
NO
ug/L
2.0
1.7
1
10/19/17 03:53 75-274
Bromoform
NO
ug/L
2.0
1.5
1
10/19/17 03:53 75-25-2
Bromomethane
NO
ug/L
2.0
1.0
1
10/19/17 03:53 74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1.9
1
10/19/17 03:53 56-23-5
Chlorobenzene
NO
ug/L
2.0
1.7
1
10/19/17 03:53 108-90-7
Chloroethane
NO
ug/L
2.0
1.6
1
10/19/17 03:53 75-00-3
Chloroform
NO
ug/L
2.0
1.9
1
10/19/17 03:53 67-66-3
Chloromethane
NO
ug/L
2.0
1.5
1
10/19/17 03:53 74-87-3
Dibromochloromethane
NO
ug/L
2.0
1.8
1
10/19/17 03:53 12448-1
1,2-Dichlorobenzene
NO
ug/L
2.0
1.5
1
10/19/17 03:53 95-50-1
1,3-Dichlorobenzene
NO
ug1L
2.0
1.5
1
10/19/17 03:53 541-73-1
1,4-Dichlorobenzene
NO
ug/L
2.0
1.5
1
10/19/17 03:53 106-46-7
1,1-Dichloroethane
NO
ug/L
2.0
1.8
1
10/19/17 03:53 75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1.8
1
10/19/17 03:53 1074)6-2
1,1-Dchloroethene
NO
ug/L
2.0
1.9
1
10/19/17 03:53 75-35-4
as-1,2-Dichloroethene
NO
ug/L
2.0
1.8
1
10/19/17 03:53 156-59-2
trans-1,2-Dichloroethene
NO
ug/L
2.0
1.8
1
10/19/17 03:53 156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
1.7
1
10/19A703:53 78-87-5
as-1,3-Dichloropropene
NO
ug/L
2.0
1.6
1
1011911703:53 10061-01-5
bans-1,3-Dichloropropene
NO
ug/L
2.0
1.6
1
10119/1703:53 10061-02-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 45

aceAnalytkal'
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1
ANALYTICAL RESULTS
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Outfatl 3 Lab ID: 92359309003 Collected: 10/16/17 09:25 Received: 10/16/17 12:10 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qua!
624 Volatile Organics
Analytical Method: EPA 624
Ethylbenzene
ND
ug/L
2.0
1.6
1
10/19/17 03:53
100-41-4
Methylene Chloride
ND
ug/L
2.0
1.9
1
10/19/17 03:53
75-09-2
1,1,2,2-Tetrarhleroethane
ND
ug/L
2.0
1.5
1
10/19/17 03:53
79-34-5
Tetrachloroethene
NO
ug/L
2.0
1.8
1
10/19/17 03:53
127-18-4
Toluene
ND
ug/L
2.0
1.6
1
10/19/17 03:53
10"8-3
1,1,1-Trichloroethane
ND
ug/L
2.0
1.9
1
10/19/17 03:53
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1.7
1
10119/1703:53
79-00-5
Trichloroelhene
ND
ug/L
2.0
1.8
1
10/19/17 03:53
79-01-6
Trichlorofluoromethane
ND
ug/L
2.0
1.7
1
10/19/17 03:53
75-69-4
Vinyl chloride
ND
ug1L
2.0
1.5
1
10/19/17 03:53
75-01-4
Surrogates
4-Bromofluorobenzene(S)
108
%
70-130
1
10/19/17 03:53
460-00.4
Toluene-d8 (S)
113
%
70-130
1
10/19/17 03:53
2037-26-5
1,2-Dichloroethane-d4 (S)
86
%
70-130
1
10/1911703:53
17060-07-0
2640D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids NO mg/L 2.5 2.5 1 10/17/17 11:05
9040 pH Analytical Method: EPA 9040
pH 7.4 Sid. Units 0.10 0.10 1 10/17/17 00:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 45

aceAnalyti al
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27268
[phone]
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
QC Batch: 383653 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92359309001, 92359309002, 92359309003
METHOD BLANK: 2126203 Matrix: Water
Associated Lab Samples: 92359309001, 92359309002, 92359309003
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 1.1 10/24/17 04:57
LABORATORY CONTROL SAMPLE:
2126204
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 36.3
91
78-114
MATRIX SPIKE SAMPLE:
2126205
92358742004 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
37.4
93
78-114
Results presented on this page are in the units indicated by the -Units" column except where an alternate unit Is presented to the right of the resulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/24/2017 03:06 PM without the written consent of PaceAna"Cal Services, L-C. Page 15 of45

ceAnapical
wxnvpacelabsmnt
i
QUALITY CONTROL DATA
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
QC Batch: 382919 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92359309001, 92359309002, 92359309003
Pace Ana"cal Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
METHOD BLANK: 2122101
Matrix: Water
Associated Lab Samples:
92359309001, 92359309002, 92359309003
Blank
Repotting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Copper
mg/L
ND
0.0050
0.0025
10119/1717:41
Lead
mg/L
ND
0.0050
0.0025
10119/1717:41
Zinc
mg/L
ND
0.010
0.0025
10/19/1717:41
LABORATORY CONTROL SAMPLE: 2122102
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Copper mg/L .5 0.52 104 85-115
Lead mg/L .5 0.49 98 85-115
Zinc mg1L .5 0.49 98 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2122103
2122104
MS
MSD
92358797001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Copper
mg/L
12.9 ug/L
.5
.5
0.53
0.54
104
105
70-130
1
20
Lead
mg1L
NO
.5
.5
0.46
0.47
93
94
70-130
1
20
Zinc
mg/L
37.1 ug/L
.5
.5
0.51
0.52
95
96
70-130
1
20
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2122105
2122106
MS
MSD
92359320001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Copper
mg/L
3.0J ug/L
.5
.5
0.53
0.53
105
105
70-130
0
20
Lead
mg/L
NO
.5
.5
0.49
0.48
98
96
70-130
2
20
Zinc
mg/L
NO
.5
.5
0.49
0.48
98
96
70-130
3
20
Results presented on this page are in the units Indicated dy the'UnlW column except curare an att mutt unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent or Pace Analytical Services, LLC.
Page 16 of 45

aceAnalytical e
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1
r
QUALITY CONTROL DATA
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
QC Batch: 382971 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92359309001, 92359309002, 92359309003
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 272BB
[phone]
METHOD BLANK: 2122518 Matrix: Water
Associated Lab Samples: 92359309001, 92359309002, 92359309003
Blank Reporting
Parameter Units Result Limit
MDL
Anatyzed
1,1,1-Trichloroethane
ug1L
ND
2.0
1.9
10/18/17 21:37
1,1,2,2-Tetrachloroethane
ug1L
ND
2.0
1.5
10/18/17 21:37
1.1,2-Trichloroethane
ug/L
ND
2.0
1.7
10/18/17 21:37
1,1-Dichloroethane
ug/L
ND
2.0
1.8
1011811721:37
1,1-Dichloroethene
ug/L
ND
2.0
1.9
1011811721:37
1,2-Dichlorobenzene
ug1L
ND
2.0
1.5
10/18/17 21:37
1,2-Dichloroethane
ug/L
ND
2.0
1.8
10/18/17 21:37
1,2-Dichloropropane
ug1L
ND
2.0
1.7
1 Gil8117 21:37
1.3-Dichlorobenzene
ug/L
ND
2.0
1.5
10/18/17 21:37
1,4-Dichlorobenzene
ug1L
ND
2.0
1.5
10/18/17 21:37
Benzene
ug1L
ND
2.0
1.7
10/18/17 21:37
Bromodichk)romethane
ug1L
ND
2A
1.7
10/18/17 21:37
Bromoform
ug/L
ND
2.0
1.5
10/18/17 21:37
Bromomethane
ug/L
ND
2.0
1.0
10/18/17 21:37
Carbon tetrachloride
ug1L
ND
2.0
1.9
10/16/17 21:37
Chlorobenzene
ug/L
ND
2.0
1.7
10/16/17 21:37
Chloroethane
uglL
ND
2.0
1.6
10/18/17 21:37
Chloroform
uglL
ND
2.0
1.9
10/18/17 21:37
Chloromethane
ug/L
ND
2.0
1.5
10/18/17 21:37
cis-1,2-Dichloroethene
ug/L
ND
2.0
1.8
10/18/17 21:37
cis-1, 3-Dichlorop rope ne
ug/L
ND
2.0
1.6
10/18/17 21:37
Dibromochloromethane
ug/L
ND
2.0
L8
10/18/17 21:37
Ethylbenzene
ug1L
ND
2.0
1.6
10/18/17 21:37
Methylene Chloride
ug/L
2.1
2.0
1.9
10/18/17 21:37 C9
Tetrachloroethene
ug/L
ND
2.0
1.8
10/18/17 21:37
Toluene
ug1L
ND
2.0
1.6
10/18/17 21:37
trans-1,2-Dichloroethene
ug/L
ND
2.0
1.8
1011811721:37
trans-1,3-Dichloropropene
ug/L
ND
2.0
1.6
10/18/17 21:37
Trichloroethene
ug/L
ND
2.0
1.8
10/18/17 21:37
Trichlorofluoromethane
ugR
ND
2.0
1.7
10/18/17 21:37
1lnyichloride
ug1L
ND
2.0
1.5
10/18/17 21:37
1,2-Dichloroethane-d4 (S)
%
85
70-130
10/18/17 21:37
4-Bromofluorobenzene (S)
%
101
70-130
10/18/17 21:37
Toluene-d8 (S)
%
111
70-130
10/18/17 21:37
LABORATORY CONTROL SAMPLE: 2122519
Parameter
1,1,1-Tdchloroethane
1,1,2,2-Tetrachloroethane
Spike
Units Conc.
ug/L 20
ug/L 20
LCS LCS
Result % Rec
18.0 90
17.3 87
Qualifiers
% Rec
Limits Qualifiers
52-162
46-157
Results presented on this page aye in the Unitas Indicated by the "ttnits' column except Wwre an af6sff"ft unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 10/24/2017 03:06 PM without the written consent of Pace Anatocal Services, LLC. Page 17 of 45

�JceAnayicala
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E
QUALITY CONTROL DATA
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
LABORATORY CONTROL SAMPLE: 2122519
Pace Anatytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
1,1,2-Trichloroethane
ug/L
20
16.4
82
52-150
1,1-Dichloroethane
uglL
20
18.0
90
59-155
1,1-Dichloroethene
ug/L
20
20.2
101
1-234
1,2-Dichlorobenzene
ug/L
20
18.6
93
18-190
1,2-Dichloroethane
ug/L
20
17.5
87
49-155
1,2-C)ichloropropane
ug/L
20
17.8
89
1-210
1,3-Dichlorobenzene
ug/L
20
17.4
87
59-156
1,4-Dichloroberizene
ug/L
20
17.6
88
18-190
Benzene
ug/L
20
17.2
86
37-151
Bromodichloromethane
ug/L
20
16.0
80
35-155
Bromoform
uglL
20
16.1
80
45-169
Bromomethane
ug/L
20
13.8
69
1-242
Carbon tetrachloride
ug/L
20
17.4
87
70-140
Chlorobenzene
ug/L
20
16.6
83
37-160
Chloroethane
ug/L
20
31.0
155
14-230
Chloroform
ug/L
20
17.0
85
51-138
Chloromethane
uglL
20
15.6
78
1-273
cis-1,2-Dichloroethene
ug/L
20
18.5
92
68-146
cis-1,3-Dichloropropene
ug/L
20
16.0
80
1-227
Dibromochloromethane
ug/L
20
16.6
83
53-149
Ethytbenzene
uglL
20
16.0
80
37-162
Methylene Chloride
uglL
20
20.9
104
1-221
Tetrachloroethene
ug/L
20
16.0
80
64-148
Toluene
ug/L
20
15.5
77
47-150
trans-1,2-Dichloroethene
ug/L
20
19.2
96
54-156
trans-1,3-Dichloropropene
ug/L
20
15.9
80
17-183
Trichloroethene
ug1L
20
16.6
83
71-157
Trichlorofluoromethane
ug/L
20
35.7
178
17-181
Vinyl chloride
ug/L
20
19.3
97
1-251
1,2-Dichloroethane-d4 (S)
%
106
70-130
4-Bromofluorobenzene (S)
%
104
70-130
Toluene-d8 (S)
%
97
70-130
MATRIX SPIKE SAMPLE:
2122521
92358613002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
ND
20
19.7
99
46-171
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.8
99
73-159
1,1,2-Trichloroethane
ug/L
N❑
20
18.1
90
64-152
1,1-Dichloroethane
ug/L
ND
20
19.4
97
43-172
1,1-Dichloroethene
ug1L
ND
20
23.5
117
48-189
1,2-Dichlorobenzene
ug/L
ND
20
20.2
101
54-154
1,2-Dichloroethane
ug/L
ND
20
17.4
87
42-171
1,2-Dichloropropane
ug/L
ND
20
19.1
95
55-157
1,3-Dichlorobenzene
ug1L
N❑
20
19.0
95
57-148
Riwtt presented on this page 4r* In the urtft indicatsd by the "Units' colunm except wAmm an altemata unit Is prssaniad m the dgirt or the resut[.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 45

•
ceAnaVical
wwwpscelabs.Ccm
i�
QUALITY CONTROL DATA
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
MATRIX SPIKE SAMPLE:
2122521
92358613002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,4-Dichloroberizene
ug/L
ND
20
19.4
97
58-149
Benzene
ug/L
ND
20
19.3
97
54-163
Bromodichloromethane
ug/L
ND
20
19.0
95
56-152
Bromoform
ug/L
Nil
20
18.3
92
53-151
Bromomethane
ug/L
ND
20
16.0
80
10-200
Carbon tetrachloride
ug/L
ND
20
20.3
101
41-175
Chlorobenzene
ug/L
ND
20
19.4
97
67-152
Chloroethane
ug/L
ND
20
23.5
117
23-200
Chloroform
ug/L
ND
20
18.6
93
51-166
Chloromethane
ug/L
ND
20
17.6
88
40-175
as-1,2-Dichloroethene
ug/L
ND
20
20.1
100
45-174
as-1,3-Dichloropropene
ug/L
ND
20
18.1
91
38-146
Dibromochloromethane
ug/L
ND
20
17.5
88
65-144
Ethylbenzene
ug/L
ND
20
18.5
93
57-152
Methylene Chloride
ug/L
ND
20
17.2
86
40-167
Tetrachloroethene
ug/L
ND
20
17.0
85
59-155
Toluene
ug/L
ND
20
19.7
98
47-162
trans-1,2-Dichloroethene
ug/L
ND
20
20.2
101
47-178
trans- 1, 3-Dichloropropene
ug/L
ND
20
16.9
84
39-148
Trichloroethene
ug/L
ND
20
19.1
95
60-153
Trichlorofluoromethane
ug/L
ND
20
21.7
108
42-199
Vinyl chloride
ug/L
ND
20
24.5
122
46-176
1,2-Dichloroethane-d4 (S)
%
97
70-130
4-Bromofluorobenzene (S)
%
105
70-130
Toluene-d8 (S)
%
103
70-130
SAMPLE DUPLICATE: 2122520
Parameter
Units
92358613001
Result
Dup
Result RPD
Max
RPD Qualifiers
11,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichforoethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug1L
ND
ND
30
1,2-Dichloroethane
ug1L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,3-Dichlorobenzene
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Bromodichloromethane
ug/L
ND
ND
30
Bromoform
ug/L
ND
ND
30
Bromomethane
ug/L
ND
ND
30
Carbon tetrachloride
ug/L
ND
ND
30
Chlorobenzene
ug/L
NO
ND
30
Rasubs prwan. on dit page are in the umta indicated by the'tlydts' cohmm except efiere an alhematr unit is prasented to the right erthe result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC, Page 19 of 45

aceAnalyfical'
wwwpacerab&cam
I
QUALITY CONTROL DATA
Pace Artatytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
SAMPLE DUPLICATE: 2122520
92358613001
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Chloroethane
ug/L
ND
ND
30
Chloroform
ug1L
ND
NO
30
Chloromethane
ug1L
ND
ND
30
as-1,2-Dichloroethene
ug1L
ND
ND
30
cis-1,3-Dichloropropene
ug1L
ND
ND
30
Dibromochloromethane
ug1L
ND
ND
30
Ethylbenzene
ug1L
ND
ND
30
Methylene Chloride
ug/L
ND
ND
30
Tetrachloroethene
ug/L
ND
ND
30
Toluene
ug/L
ND
ND
30
trans-1,2-Dichloroethene
ug1L
ND
ND
30
trans-1,3-Dichloropmpene
ug/L
ND
ND
30
Trichloroethene
ug/L
ND
ND
30
Trichlorofluoromethane
ug/L
ND
ND
30
Vinyl chloride
ug/L
ND
ND
30
1,2-Dichloroethane-d4 (S)
%
90
87
3
4-Bromofluorobenzene (S)
%
106
106
0
Toluene-d8 (S)
%
114
114
0
Results presented on this paps are In the units Indicated by Via -Units' column except whers an alternate unit is presented to the right d the resulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 10/24/2017 03:06 PM without the written consent of Pace Anatyticai Services, LLC.
Page 20 of 45

aceAnalytrcal
wwwpacelabs.cam
QUALITY CONTROL DATA
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
QC Batch: 382695 Analysis Method: EPA 608
QC Batch Method: EPA 3510 Analysis Description: 508 GCS Pest PCB
Associated Lab Samples: 92359309001, 92359309002, 92359309003
METHOD BLANK: 2120719 Matrix: Water
Associated Lab Samples: 92359309001, 92359309002, 92359309003
Blank Reporting
Parameter Units Result Limit
4,4'-DDD
4,4'-DDE
4,4'-DDT
Aldrin
alpha-BHC
beta-BHC
Chlordane (Technical)
delta-BHC
Dieldrin
Endosulfan
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1246 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Toxaphene
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
ug/L
ND
0.050
ug/L
NO
0,050
ug/L
NO
0.050
ug/L
ND
0.050
ug/L
NO
0.050
ug1L
ND
0.050
ug1L
ND
0.50
ug1L
ND
0.050
ug/L
ND
0.050
ug/L
ND
0.050
ug/L
ND
0,050
ug/L
ND
0,050
ug/L
ND
0A50
ug/L
ND
0.050
ug/L
ND
0.050
ug1L
ND
0.050
ug1L
ND
0.050
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
ug/L
ND
0.50
%
59
2D-138
%
40
20-110
MDL
0.050
0.050
0.050
0.050
0.050
0.050
0.50
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
Analyzed
10/18/17 12:41
10/18/17 12:41
10/18/17 12:41
10118/17 12:41
10/18/17 12:41
10/18/17 12:41
10/18117 12:41
10/18/17 12:41
10/18117 12:41
10118/17 12:41
10/18/17 12:41
10118/17 12:41
10/18/17 12:41
10/18/17 12:41
10/18/17 12:41
10118117 12:41
10/18/17 12:41
10/18/17 12:41
10/18/17 12:41
10/18/17 12:41
10/18/17 12:41
10/18/17 12:41
10/18/17 12:41
10/18/17 12:41
10/18/17 12:41
10/18/17 12:41
10118/17 12:41
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 272BB
(336)623-B921
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2120720
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
.25
0.22
89
31-141
4,4'-DDE
ug1L
.25
0.19
75
30-145
4,4'-DDT
ug/L
.25
0.25
101
25-160
Aldrin
ug/L
.25
0.14
55
42-122
alpha-BHC
ug/L
.25
0.19
76
37-134
beta-BHC
ug/L
.25
0.17
67
17-147
delta-BHC
ug/L
.25
0.21
83
19-140
Dieldrin
ug1L
.25
0.20
83
36-146
Endosulfan I
ug/L
.25
0.20
80
45-153
Results presenmd on Uft paps are in the curies intllated by the "UnW cohamr except whore an atbrmaie Unit is preser d to the right of tto resent.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date, 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 45

_ ;a'ceAnalytical@
! WwW..pacBf3b&cam
QUALITY CONTROL DATA
Project AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
LABORATORY CONTROL SAMPLE: 2120720
PaceAn*Wcal Services, LLC
205 East Meadow Road • Suite A
Eden, NC 27288
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Endosulfan II
ug/L
.25
0.21
83
1-202
Endosultan sulfate
ug/L
.25
0.21
86
26-144
Endrin
ug/L
.25
0.24
95
30-147
Endrin aldehyde
ug/L
.25
0.19
76
50-150
gamma-BHC (Lindane)
ug/L
.25
0.19
78
32-127
Heptachlor
ug/L
25
0.19
78
34-111
Heptachlor epoxide
ug/L
.25
0.20
82
41-126
Decachlorobiphenyl (S)
%
71
20-138
Tetrachloro-m-xylene (S)
%
83
20-110
MATRIX SPIKE SAMPLE:
2120721
92359309001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
NO
.25
0.24
98
31-141
4,4'-DOE
ug/L
ND
.25
0.19
76
30-145
4,4'-DDT
ug/L
NO
.25
0.24
98
25-160
Aldrin
ug/L
NO
.25
0.11
46
42-122
alpha-BHC
ug/L
NO
.25
0.15
61
37-134
beta-BHC
ug/L
NO
.25
0,18
73
17-147
delta-BHC
ug/L
NO
.25
0.23
91
19-140
Dieldrin
ug/L
NO
.25
0.23
92
36-146
Endosulfan I
ug/L
ND
.25
0.23
95
45-153
Endosulfan II
ug/L
NO
.25
0.24
96
1-202
Endosulfan sulfate
uglL
NO
.25
0.24
98
26-144
Endrin
ug/L
ND
.25
0.26
104
30-147
Endrin aldehyde
ug/L
NO
.25
0.23
93
50-150
gamma-BHC (Lindane)
ug/L
NO
.25
0.18
72
32-127
Heptachlor
ug/L
NO
.25
0.16
65
34-111
Heptachlor epoxide
ug/L
NO
.25
0.21
86
41-126
Decachlorobiphenyl (S)
%
34
20-138
Tetrachioro-m-xylene (S)
%
64
20-110
SAMPLE DUPLICATE: 2120722
92359309002 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
4,4'-DDD
ug/L
ND NO
30
4,4'-DDE
ug/L
NO ND
30
4,4'-DDT
ug/L
NO ND
30
Aldrin
ug1L
NO ND
30
alpha-BHC
ug/L
NO NO
30
beta-BHC
ug/L
ND NO
30
Chlordane (Technical)
ug/L
ND NO
30
delta-BHC
ug/L
NO NO
30
Dieldrin
ug/L
NO NO
30
Reautts presented on this page are in the
untie indicated by the "tlntta" column except where an alternate unitis
presented to the right of the msulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM
without the written consent of Pace analytical Services, LLC.
Page 22 of 45

ace,Malytical
wwwpaceiab&COM
1
QUALITY CONTROL DATA
Project AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
SAMPLE DUPLICATE: 2120722
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 272BB
[phone]
Parameter
Units
92359309002
Result
Dup
Result RPD
Max
RPD Qualifiers
Endosulfan I
ug1L
NO
NO
30
Endosulfan II
ug/L
NO
NO
30
Endosulfan sulfate
ug1L
NO
ND
30
Endrin
ug/L
ND
ND
30
Endrin aldehyde
ug/L
ND
ND
30
gamma-BHC (Lindane)
ug/L
ND
ND
30
Heptachlor
ug/L
NO
NO
30
Heptachlor epoxide
ug/L
ND
ND
30
PCB-1016 (Aroclor 1016)
ug1L
ND
ND
30
PCB-12221 (AroGor 1221)
ug/L
ND
ND
30
PCB-1232 (AroGor 1232)
ug1L
ND
ND
30
PCB-1242 (AroGor 1242)
ug/L
NO
ND
30
PCB-1248 (AroGor 1248)
ug/L
NO
ND
30
PCB-1254 (AroGor 1254)
ug/L
NO
ND
30
PCB-1260 (AroGor 1260)
ug/L
NO
ND
30
Toxaphene
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "tarts" column except where an alternate unit is presented W the right of the resutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduoed, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pala Analytical Services, LLC.
Page 23 of 45

1�26Analytical
wwwpacskb&oom
i
i
QUALITY CONTROL DATA
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Pace Analytical Services, LLG
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QC Batch: 383124 Analysis Method:
QC Batch Method: EPA 625 Analysis Description:
Associated Lab Samples: 92359309001, 92359309002, 92359309003
EPA 625
625 MSS
METHOD BLANK: 2123336
Matrix: Water
Associated Lab Samples: 92359309001, 92359309002, 92359309003
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed Qualifiers
1,2,4-Trichlorebenzene
ug/L
NO
5.0
0.98
10121/1721:50
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
0.95
10/21/17 21:50
2,4,6-Trichlorophenot
ug/L
NO
10.0
1.3
10/21/17 21:50
2,4-Dichlorophenol
ug/L
NO
5.0
1.7
10/21/17 21:50
2,4-Dimethylphenot
ug/L
NO
10.0
1.2
10121/1721:50
2,4-Dinitrophenol
ug1L
NO
50.0
9.0
10/21/17 21:50
2,4-Dinitrotaluene
ug/L
ND
5.0
0.90
10/21/17 21:50
2,6-Dinitrotoiuene
ug/L
NO
5.0
0.98
10/21/17 21:50
2-Chloronaphthalene
ug/L
NO
5.0
0.98
10/21/17 21:50
2-Chlarophenol
ug/L
NO
5.0
1.3
10/21/17 21:50
2-Nitrophenol
ug/L
ND
5.0
0.91
10/21/17 21:50
3,3'-Dichtorobenzidine
ug/L
NO
25.0
2.1
10/21/17 21:50
4,6-Dinitro-2-methytphenol
ug/L
ND
20.0
2.6
10/21/17 21:50
4-Bromophenylphenyl ether
ug/L
ND
5.0
0.82
10/21/17 21:50
4-Chloro-3-methyiphenol
ug/L
ND
5.0
3.7
10/21/17 21:50
4-Chlorophenylphenyi ether
ug/L
NO
5.0
0.87
10/21/17 21:50
4-Nitrophenol
ug/L
NO
50.0
4.1
10/21/17 21:50
Acenaphthene
ug/L
ND
5.0
0.25
10/21/17 21:50
Acenaphthylene
ug/L
ND
5.0
0.21
10/21/17 21:50
Anthracene
ug/L
ND
5.0
0.14
10121/1721:50
Benzo(a)anthracene
ug/L
ND
5.0
0,33
10/21/17 21:50
Benzo(a)pyrene
ug/L
ND
5.0
0.30
10/21/17 21:50
Benzo(b)fluoranthene
ug/L
ND
5.0
0.28
10/21/17 21:50
Benzo(g,h,i)perylene
ug/L
ND
5.0
0.38
10121/1721:50
Benzo(k)fluoranthene
ug/L
NO
5.0
0.43
10/21/17 21:50
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
0.92
10/21/17 21:50
bis(2-Chloroethyl) ether
ug/L
ND
5.0
1.0
10/21/17 21:50
bis(2-Ethythexyl)phthalate
ug/L
ND
5.0
0.79
10/21/17 21:50
Butylbenzylphthalate
ug/L
ND
5.0
0.79
10/21/17 21:50
Chrysene
ug/L
NO
5.0
0.21
10/21/17 21:50
Di-n-butylphthalate
ug/L
NO
5.0
0.75
10/21/17 21:50
Di-n-octylphthalate
ug/L
NO
5.0
0.66
10/21/17 21:50
Dibenz(a,h)anthracene
ug/L
ND
5.0
0.55
10/21/17 21:50
Diethylphthalate
ug/L
ND
5.0
0.58
10121/1721:50
Dimethylphthalate
ug/L
NO
5.0
0.76
10/21/17 21:50
Fluoranthene
ug/L
NO
5.0
0.21
10/21/17 21:50
Fluorene
ug/L
NO
5.0
0.21
10/21/17 21:50
Hexachloro-1,3-butadiene
ug/L
NO
5.0
0.94
10121/1721:50
Hexachlorobenzene
ug/L
ND
5.0
0.72
10/21/1721:50
Hexachlorocydopentadiene
ug/L
NO
10.0
0.88
10/21I17 21:50
Hexachloroethane
ug/L
NO
5.0
1.1
10/21/17 21:50
Results presented on this page am in the units indicated by Ow -Units' column ezcept where an Marvin unn is prow tod to the right of the msulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 01..06 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 45

Pace Analytical Services, LLC
ceAnalytrcal •
205 East Meadow Road - Suite A
Eden, NC 27288
'"ww'com
(336)6238921
QUALITY CONTROL DATA
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
METHOD BLANK: 2123336
Matrix:
Water
Associated Lab Samples: 92359309001, 92359309002, 92359309003
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
Qualifiers
Indeno(1,2,3-cd)pyrene
ug1L
ND
5.0
0.29
10/21/17 21:50
lsophorone
ug1L
ND
10.0
0.89
10/21/17 21:50
N-Nitroso-di-n-propylamine
ug1L
ND
5.0
0.99
10/21/17 21:50
N-Nitrosodimethylamine
ug1L
ND
5.0
0.91
10/21/17 21:50
N-Nitrosodiphenylamine
ug/L
ND
10.0
1.0
10/21/17 21:50
Naphthalene
ug/L
ND
5.0
0.34
10/21/17 21:50
Nitrobenzene
ug/L
ND
5.0
1.1
10/21/17 21:50
Pentachlorophenol
ug/L
ND
10.0
4.6
10/21/17 21,50
Phenanthrene
ug/L
ND
5.0
0.22
10/21/17 21:50
Phenol
WL
ND
5.0
1.9
10/21/17 21:50
Pyrene
ug/L
ND
5.0
0,19
10/21/17 21 :50
2,4,6-Tribromophenol (S)
%
72
10-137
10/21/17 21:50
2-Fluorobiphenyl (S)
%
32
15-120
10121/17 21 :50
2-Fluorophenol (S)
%
18
10-120
10/21/17 21:50
Nitrobenzene-d5 (S)
%
34
10-120
10/21/17 21:50
Phenol -dB (S)
%
12
10-120
10/21/17 21:50
Terphenyl-d14 (S)
%
73
11-131
10/21/17 21:50
LABORATORY CONTROL SAMPLE:
Parameter
2123337
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
21.9
44
44-142
2.2'-Oxybis(1-chloropropane)
uglL
50
24.0
48
36-166
2,4.6-Trichlorophenol
ug/L
50
32.0
64
37-144
2.4-Dichlorophenol
ug/L
50
28.2
56
1-191
2,4-Dimethylphenol
ug/L
50
34.6
69
32-119
2,4-Dinitrophenol
ug1L
250
237
95
1-181
2,4-Oindrotoluene
ug/L
50
45.4
91
39-139
2,6-Dinitrotoluene
ug/L
50
41.7
83
50-158
2-Chloronaphthalene
ug1L
50
28.7
57
60-118 L2
2-Chlorophenol
ug/L
50
25.2
50
23-134
2-Nitrophenol
ug/L
50
28.3
57
29-182
3,X-Dichlorobenzidine
ug/L
100
89.1
89
1-262
4,6-Diri tro-2-methylphenol
ug/L
100
103
103
1-181
4-Bromophenytphenyl ether
ug/L
50
37.4
75
53-127
4-Chloro-3-methylphenol
ug/L
100
65.1
65
22-147
4-Chlorophenytphenyl ether
ug1L
5o
32.9
66
25-158
4-Nitrophenol
ug1L
250
94.9
38
1-132
Acenaphthene
ug/L
50
31.8
64
47-145
Acenaphthylene
ug1L
50
32.0
64
33-145
Anthracene
ug1L
50
44.9
90
1-166
Benzo(a)anthracene
ug/L
50
47.5
95
33-143
Benzo(a)pyrene
ug/L
50
47.0
94
17-163
Benzo(b)tuoranthene
ug1L
50
45.3
91
24-159
ftvwft presenmd on this page are in the units mdkated by the Rfntts' eoGmin except when an attarrraft unit is preierftd to the rigffi or the nmuR.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 45

aceAnaVical
www.pecelabsoom
t
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2115 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
LABORATORY CONTROL SAMPLE:
2123337
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Benzo(g,h,i)perylene
ug&
50
45.5
91
1-219
Benzo(k)fluoranthene
ug/L
50
47.1
94
11-162
bis(2-Chioroethoxy)methane
ug/L
50
30.9
62
33-184
bfs(2-Chloroethyl) ether
ug/L
50
28.5
57
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
45.9
92
8-158
Butylbenzytphthalate
ug/L
50
45.9
92
1-152
Chrysene
ug/L
50
48.3
97
17-168
Di-n-butylphthalate
ug/L
50
47.5
95
1-118
Di-n-octylphthalate
ug/L
50
43.5
87
4-146
Dibenz(a,h)anthracene
ug/L
50
46.6
93
1-227
Diethylphthalate
ug/L
50
42.9
86
1-114
Dimethylphthalate
ug/L
50
40.1
80
1-112
Fluoranthene
ug/L
50
49.7
99
26-137
Fluorene
ug/L
50
37.0
74
59-121
Hexachloro-1,3-butadiene
ug/L
50
18.1
36
24-116
Hexachlorobenzene
ug/L
50
40.6
81
1-152
Hexachlorocyctopentadiene
ug/L
50
23.8
48
25-150
Hexachloroethane
ug/L
50
18.3
37
40-113 L2
lndeno(1,2,3-cd)pyrene
ug/L
50
46.9
94
1-171
Isophorone
ug/L
50
31.9
64
21-196
N-Nitroso-di-n-propytamine
ug/L
50
30.8
62
1-230
N-Nitrosodimethylamine
ug/L
50
16.9
34
25-150
N-Nitrosodiphenylamine
ug/L
50
39.7
79
25-150
Naphthalene
ug/L
50
25.2
50
21-133
Nitrobenzene
ug/L
50
29.4
59
35-180
Pentachlorophenol
ug/L
100
92.4
92
14-176
Phenanthrene
ug/L
50
44.3
89
54-120
Phenol
ug/L
50
11.8
24
5-112
Pyrene
ug1L
50
49.2
98
52-115
2,4,6-Tribromophenol (S)
%
87
10-137
2-Fluorobiphenyl (S)
%
57
15-120
2-Fluorophenol (S)
%
30
10-120
Nitrobenzene-d5 (S)
%
56
10-120
Phenol-d6 (S)
%
21
10-120
Terphenyl-c114 (S)
%
85
11-131
MATRIX SPIKE SAMPLE:
2123338
35340529002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
0.981.1
50
11.1
22
44-142 M1
2,2'-Oxybis(1-chforopropane)
ug/L
0.95U
50
8.9
18
36-166 M1
2,4,6-Trichlorophenol
ug/L
1.3U
50
24A
49
37-144
2,4-Dichlorophenol
ug/L
1.7U
50
15.8
32
1-191
2,4-Dimethytpttenol
ug/L
1.2U
50
17.8
36
32-119
2,4-Dinitrophenol
ug/L
9.OU
250
176
71
1-181
Rasutts presented on this Pape are in the unita indicated by the "Units' column except where an ait nuft unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in ILA,
Date: 10/24/2017 03'.06 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 45

•
acmnalytical
nvwpacelabs.mm
I
QUALITY CONTROL DATA
PaceAnalydcal Services, LLG
205 East Meadow Road - Suite A
Eden, NC 27280
[phone]
Project: AMEX 2017 Juty-Dec Semi Annual
Pace Project No_: 92359309
MATRIX SPIKE SAMPLE:
2123338
35340529002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec.
Limits Qualifiers
2,4-Dinitrotoluene
ug/L
0.901.1
50
40.3
81
39-139
2,6-Dinitrotoluene
ug/L
0.981.1
50
31.4
63
50-158
2-Chloronaphthalene
ug/L
0.981.1
50
14.9
30
60-118 MO
2-Chlorophenol
ug/L
1.31-1
50
11.5
23
23-134
2-Nitrophenol
ug/L
0.91U
50
12.9
26
29-182 M1
3,3'-Dichlorobenzidine
ug/L
2.1U
100
79.3
79
1-262
4,6-Dinitro-2-methylphenol
ug/L
2.6U
100
94.8
95
1-181
4-6romophenylphenyl ether
ug/L
0.82U
50
30.9
62
53-127
4-Chloro-3-methylphenol
ug/L
3.7U
100
57.2
57
22-147
4-Chlorophenylphenyl ether
uglL
0.87U
50
22.1
44
25-158
4-Nitrophenol
ug/L
4.1U
250
79.2
32
1-132
Aoenaphthene
uglL
0.25U
50
18.0
36
47-145 M1
Aoenaphthylene
uglL
0.21U
50
18.2
36
33-145
Anthracene
ug1L
0.14U
50
41.5
83
1-166
Senzo(a)anthracene
ug/L
0.33U
50
45.1
90
33-143
Benzo(a)pyrene
ug/L
1.1J
50
43.9
86
17-163
Senzo(b)fluorantherle
ug/L
0.28U
50
42.7
85
24-159
Benzo(g,h,i)perylene
ug/L
2.6J
50
43.3
82
1-219
Benzo(k)fluoranthene
ug/L
0.431_1
50
43.8
88
11-162
bis(2-Chloroethoxy)methane
ug/L
0.92U
50
13.6
27
33-184 M1
bis(2-Chloroethyl) ether
uglL
1.01-1
50
12.7
25
12-158
bis(2-Ethylhexyl)phthalate
ug/L
0.791-1
50
44.8
90
8-158
Butylbenzylphthalate
ug/L
0.791.1
50
45.8
92
1-152
Chrysene
ug/L
0.21 U
50
46.4
93
17-168
Di-n-butylphthalate
ug/L
0.75U
50
45.4
91
1-118
Di-n-octylphthalate
ug/L
0.66U
50
41.7
83
4-146
Dibenz(a,h)anthraoene
ug/L
2.4J
50
43.0
81
1-227
Diethyfphthalate
ug/L
0.58U
50
36.2
72
1-114
Dimethylphthalate
ug/L
0.76U
50
29.2
58
1-112
Fluoranthene
ug/L
0.21 U
50
46.9
94
26-137
Fluorene
ug/L
0,21 U
50
25.9
52
59-121 M1
Hexachloro-1,3-butadiene
ug/L
0.94U
50
9.6
19
24-116 M1
Hexachlorobenzene
ug/L
0.72U
50
34.7
69
1-152
Hexachlorocyclopentadiene
ug/L
0.881.1
50
10.2
20
25-150 M1
Hexachloroethane
ug/L
1.1 U
50
9.5
19
40-113 MO
Indeno(1,2,3-cd)pyrene
ug/L
2.7J
50
44.4
83
1-171
isophorone
ug/L
0.89U
50
14.2
28
21-196
N-Nitroso-di-n-propytamine
ug/L
0.9911
50
13.4
27
1-230
N-Nitrosodimethylamine
ug1L
0.91 U
50
7.9
16
25-150 Mt
N-Nitrosodiphenylamine
ug/L
1.01J
50
36.6
73
25-150
Naphthalene
ug/L
0.34U
50
13.0
26
21-133
Nitrobenzene
ug/L
1.1U
50
15.1
30
35-180 M1
Pentachlorophenol
ug/L
4.6U
100
84.8
85
14-176
Phenanthrene
ug/L
0.221-1
50
40.7
81
54-120
Phenol
ug/L
1.91-1
50
5A
10
5-112
Pyrene
ug/L
0.19U
50
49.0
98
52A15
2,4,6-Tribromophenol (S)
%
83
10-137
Results pnserded on this page are in the erdls irrdicatod dY the -Urfa' cotrann estept when an attrmata unit Is ixe:ent W to the r%ft of the rasrra.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduoed, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 45

CeAnalyiical.
wwwpaoekbaaam
QUALITY CONTROL DATA
Project: AMEX 2017 Juty-Dec Semi Annual
Pace Project No.: 92359309
MATRIX SPIKE SAMPLE:
Parameter
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-dl4 (S)
SAMPLE DUPLICATE: 2123339
Parameter
1,2,4-Trichlorobenzene
2,2'-0xybis(1-chtoropropane)
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenot
2-Nitrophenol
3,3'-Oichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenytphenyi ether
4-Chloro-3-methylphenol
4-Chlorophenylphenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)ftuoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-Chioroethoxy)methane
bis(2-Chloroethyt) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octytphthalate
Dibenz(a,h)anthracene
Diethylphthalate
Dimethylphthalate
Fluoranthene
2123338
35340529002 Spike
Units Result Conc.
MS MS
Result % Rec
28
13
27
9
74
Units
35340529004
Result
Dup
Result RPD
Max
RPD
ug/L
0.98U
NO
30
ug1L
0.95U
NO
30
ug/L
1.3U
NO
30
ug/L
1.7U
NO
30
ug/L
1.2U
NO
30
ug/L
9.OU
NO
30
ug/L
O.90U
ND
30
ug/L
0.98U
NO
30
ug/L
0.98U
NO
30
ug/L
1.3U
ND
30
ug/L
0.91 U
NO
30
ug/L
2.1U
NO
30
ug1L
2.6U
ND
30
ug/L
0.82U
NO
30
ug/L
3.7U
ND
30
ug/L
0.87U
ND
30
ug/L
4.1 U
NO
30
ug/L
0.25U
NO
30
ug/L
O.21U
NO
30
ug/L
0.14U
NO
30
ug/L
0.33U
NO
30
uglL
0.3OU
NO
30
ug/L
0.28U
NO
30
ug/L
2.OJ
1.51
30
ug/L
0.43U
NO
30
ug/L
0.921J
NO
30
ug/L
1.0U
NO
30
ug/L
0.79U
NO
30
ug/L
0.79U
NO
30
ug/L
0.21 U
NO
30
ug/L
0.75U
NO
30
ug1L
0.66U
NO
30
ug/L
1.61
1.3J
30
ug/L
0.58U
NO
30
ug/L
O.76U
ND
30
ug/L
0.21 U
NO
30
PaceAna"cal Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
% Rec
Limits Qualifiers
15-120
10-120
10-120
10-120 SO
11-131
Qualifiers
Results presentetl on this page are In tM units Indicated by the 'Un ts' column except wlnre an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10124/2017 03:06 PM without the written consent of Pace Anatytical Services, LLC. Page 28 of 45

aceAnalytical•
QUALITY CONTROL DATA
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
SAMPLE DUPLICATE: 2123339
Parameter
Units
35340529004
Result
Dup
Result
Fluorene
uglL
0.21U
ND
Hexachloro-1,3-butadiene
uglL
0.94U
ND
Hexachlorobenzene
uglL
0.72U
ND
Hexactilorocyclopentadiene
uglL
0.88U
ND
Hexachloroethane
ug/L
1.1 U
ND
Indeno(1,2,3-cd)pyrene
ug/L
2.0J
1.4J
Isophorone
uglL
0.891.1
ND
N-Nitroso-di-n-propylamine
uglL
0.991J
ND
N-Nitrosodimethylamine
uglL
0.91U
ND
N-Nitrosodiphenylamine
uglL
1.ou
ND
Naphthalene
uglL
0.34L!
ND
Nitrobenzene
uglL
1AU
ND
Pentac hlorophenol
uglL
4.6U
ND
Phenanthrene
uglL
0.22U
ND
Phenol
ug/L
1.9U
ND
Pyrene
uglL
0.19U
ND
2,4,6-Tribromophenol (S)
%
63
83
2-Fluorobiphenyl (S)
%
34
33
2-Fluorophenol (S)
%
18
17
Nitrobenzene-d5 (S)
%
38
34
PhenoW6(S)
%
11
11
Terphenyl-dl4 (S)
%
75
55
RPD
26
3
7
13
2
30
Max
RPD
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Qualifiers
Results pstawdud on this Page are in the units brdkatod by Ma "Units' column except where an aeamata unit is presented to She rigid of the nwh.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytic Ed Services, LLC.
Page 29 of 45

?cemaocjlg
Pace Analytical Services, LLC
205 East Meadow Road - Surte A
Eden, NC 27288
anrwPscetaesrnrn
[phone]
i
I
QUALITY CONTROL DATA
Project: AMEX 2017 July -Dec
Semi Annual
Pace Project No.: 92359309
QC Batch: 382671
Analysis Method: SM 2540D
QC Batch Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92359309001, 92359309002, 92359309003
METHOD BLANK: 2120577
Matrix: Water
Associated Lab Samples: 92359309001, 92359309002, 92359309003
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed
Qualifiers
Total Suspended Solids
m91L
NO 2.5
2.5 10/17/17 11:00
LABORATORY CONTROL SAMPLE:
2120578
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Suspended Solids
mglL
250 238 95
90-110
SAMPLE DUPLICATE: 2120579
92359210016 Dup
Max
Parameter
Units
Result Result RPD
RPD
Qualifiers
Total Suspended Solids
mg1L
NO NO
5
SAMPLE DUPLICATE: 2120580
92359236001 Dup
Max
Parameter
Units
Result Result RPD
RPD
Qualifiers
Total Suspended Solids
mg/L
9.2 9.2
0 5
premed an itua page an in ttw units ittditaled by" Unfts" C0kn l e:eept win an alLemah unit is praenmd to the right otaw result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 45

Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden. NC 27288
WWwPW8k1b&oont [phone]
QUALITY CONTROL DATA
Project: AMEX 2017 .July -Dec Semi Annual
Pace Project No.: 92359309
QC Bate_ 382641 Analysis Method: EPA 9040
QC Bate Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92359309001, 92359309002, 92359309003
SAMPLE DUPLICATE: 2120467
92359226001 Dup Max
Parameter Units Result Result RPD RPD Quaiiflers
pH Std. Units 7.0 6.9 2 9 D6,H6
Results presertlatl on this page are in the unit indicated by the 'Umt' column except where an alternate unit Is presented to the right ar the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 45

Pace Analytical Services, LLC
aceAnalytical 205 East Meadow Road - Suite A
Eden, NC 27288
Nnvwpacdabsoom [phone]
QUALIFIERS
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit,
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1.2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD valves.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SVV846 Chapter 4 for the analysis of Ac rolein and Acrylonitrile by EPA
Method 8260,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
C9 Common Laboratory Contaminant.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
so Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2017 03:06 PM without the written consent or Pace Analytical Services, LLC. Page 32 of 45

aceAnalytical
wWWpMX&b$=n
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: AMEX 2017 July -Dec Semi Annual
Pace Project No.: 92359309
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92359309001
Outfall 1
EPA 1664B
383653
92359309002
Outfall2
EPA 1664E
383653
92359309003
Outfall 3
EPA 1664B
383653
92359309001
Outfall 1
EPA 3510
382695
92359309002
Outfall 2
EPA 3510
382695
92359309003
Outtall 3
EPA 3510
382695
92359309001
Outfall 1
EPA 200.7
382919
923SS309002
Outtall 2
EPA 200.7
382919
92359309003
Outfall 3
EPA 200.7
382919
92359309001
Outfall 1
EPA 625
383124
92359309002
Outfall 2
EPA 625
383124
92359309003
Outtall 3
EPA 625
383124
92359309001
Outtall 1
EPA 624
382971
92359309002
Outfall 2
EPA 624
382971
92359309003
Outfall 3
EPA 624
382971
92369309001
Outfall 1
SM 2540D
382671
92359309002
Outfall 2
SM 2540D
382671
92359309003
Outfall 3
SM 2540D
382671
92359309001
Outfall 1
EPA 9040
382641
92359309002
Outfall 2
EPA 9040
382641
923593D9003
Outfall 3
EPA 9040
382641
Date: 10/24/2017 03:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.L.C.
EPA 608
382875
EPA 608
382875
EPA 608
382875
EPA 200.7
383127
EPA 200.7
383127
EPA 200.7
383127
EPA 625 383447
EPA 625 383447
EPA 625 383447
Page 33 of 45

Document Name: Document Revised: August 4, 2017
/�Sample
2ceAnafyUut"
Condition Upon RecelptlSCUR) ' Pa e 1 of 2
Document No.: issuing Authority:
F-CAR•CS-033-Rev.O4 t Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville Raleigh[] Mechanicsvillen
Sample Condition ! Client Name:Upors Receipt Projet WQ# : 92359309
Courier: CFe0Xx CUPS CUSPS []Client
❑ Commercial ace ❑Other: ti 1 11
92339309
Custody Seat Present? ❑Yes Na Seals Intact? Dyes �
Date/Initials Person Examining Contents: t
Packing Material: ❑Bubble wrap ubble Bags ❑None ❑ Other Biological Ti ue Frozen?
Thermometer. ❑Yes�O ❑N/A
❑ 1A Gun ID: �' Twet ❑Blue ❑Bone
Type
o1Ice:
Correction Factor: Cooler Temp Corrected ('C): l�r 2 Temp should be above freezing to VC
❑Samples out of remp criteria. Samples an ice, Coaling process
has begun
USDA Regulated Sail [ /A, water sample)
Did samples originatet a quarantine zone within the United States: CA, NY, or SC (check maps I? Did samples originate from a foreign source linter anally,
my.. [ NC indudine Hawaii and Puerto Fiml7 FlYes
Comments/Oistae ancy:
Chain of Custody Present?
es
ONG
NIA
1.
Samples Arrived within Hold Time?
J21e,
CINO
N/A
2.
Short Hold Time Anal sis J<72 hr.?
Elves
2C
❑N/A
3.
Rush Turn Around Time Requested?
Qyes
a
NJA
4.
Sufficient Volume?
es
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
es
❑No
LIZ
❑N/A
ON/.,
6.
Containers Intact?
es
ONO
N/A
7,
Dissolved analysis: Samples Field Filtered?
❑Yes
o
CINIA
g.
Sample Labels Match COC?
-Includes Date/Time/10/Analysis Matrix:
es
❑No
❑N/A
9.
Heads ace in VOA Vials (>5.6mm)?
❑Yes
o
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
Yes
J2116
ONa
['NJA
NJA
11,
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Lot ID of split containers:
Date/Time:
Field Data Required? ❑Yes ONO
Project Manager SCURF Review: Date -
Project Manager SRF Review: 6b Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 34 of 45

Document Name: Document Revised: August 4, 2017
Sample Condition Upon Receipt(SCUR) Page 2 of 2
�' °�2��f�a� Document No.: Issuing Authority:
F-CAR-CS-033-Rev.04 Pace Quality Office
'Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
"Bottom half of box is to list number of bottles 3
Project - WO# : 92359309
tPM: PTE Due bats: 10/23/17
CL I ENT : 93—Sout htr i,e
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Page 35 of 45

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8PZU-500 mL Plastic Unpreserved (N/A)
8PZU-1 liter Plastic Unpreserved (N/A)
SP45.125 mL Plastic H2SO4 (pH < 2) (CI-)
SPIN-ZS0 m1 Plastic HNO3 (pH < 2)
SP4Z-12S mL Plastic ZN Acetate & NaOH (>91
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aGIN-1 titer Amber HCI (pH c 21
AG3U-250 ml.Amber Unpreserved (N/A) (CI-)
AGIS- 1 Iiter Amber H2504 (pH c 2)
AG35-250 mL Amber H2504 (pH < 2)
AG3A(DG3A)-250 mL Amber NH4CI (N/A)(CI-)
DG9H-40 mL VQA Hp (N/A)
VG9T-40 mL VOA Na2S203 (N/A)
VG9U-40 mL VOA Unp tN/A)
DG9P-40 mL VOA 113PO4 (N/A)
VOAK (6 vials per kit)-S035 kit (N/A)
V/GK 13 vials per kit)-VPH/Gas kit IN/A)
SP5T-125 mL Sterile Plastic IN/A — lab)
SPZT-250 mL Sterile Plastic (N/A — lab)
BP3A-250 mL Plastic jNH2I2SO4 (9.3.9.7)
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Document Name:
Document Revised: August 4, 2017
Y
Sample Condition Upon Receipt{SCUR)
Page 2 of 2
i ceAnr?picdl
Document No.:
Issuing Authority:
~
F-CAR-CS-033•Rev.04
Pace Quality Office
*Check mark top half of box if pH and/or dechiorination
is verified and within the acceptance range for
preservation samples.
"Bottom half of box is to list number of bottles
S
Project WQ# : 92359309
PM: PTE Due Date: 10/25/17
CLIENT: 95—Southulre
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Page 37 of 45

Pace -na icaI'
CHAIN -OF -CUSTODY 1 Analytical Request Document
the Chain-of•Cuslody is a LEGAL DOCUMENT. All relevant fields must he completed nccuralely.
Page: of
Section A Section B Section C
f
2177090
Required Clinnt Information: Required Project Intormallon: Invnice Inlormallor.
Company: Report To: Ansnlfont
S �1
rJLt�'!wrll[ LAC Y� a q VJ^��
Address: q •+�� j S4. pi a Copy
To:
Company mo:
REGULATORY AGENCY
r� r,
AdQrgs ' ? t.4 �r l ('J • �)r
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NPDES F GROUND WATER DRINKING WATER
(' UST I— RCRA i OTHER
PUrchaso
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loon: ` FEIx: Project
G �(� %lk
Name:, �-
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Site Location
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Requested Due DotorTAT: Prajaet
Numlw
Paces Prnrtle e:
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes
a
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Required Clienl Inrnrrtmhort MATRIX ! CODF.
8
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r
Document Name: Document Revised: August 4, 2017
' aCeRnafY Cal .
Sample Condition Upon Recei tISCUR) I Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.04 Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ HuntersvilRaleigh[] Mechanicsville[]
ConditionSample Client Name:Upon Receipt Projer Yu WO# : 923593®9
Courier: ❑Fe K ❑UPS ❑USPS ❑Client��
❑ Commercial Pace ❑Other: It 1
92359309
Custody Seal Present? ❑Yes EIN, Seats Intact? ❑Yes i I SA
Date/[nitlals Person Examining Cornents:1 �}"l b''I i
Packing Material: ❑Bubble Wrap rubble Sags ❑None ❑ Other Biological Tf ue Frozen?
Thermometer.— ❑Yes []N/A
IR Gun 10: `} �et []Blue ❑,tone
❑ Too � Type of Ice:
Correction Factor: Cooler Temp Corrected ('C): r Z Temp should be above freezing to 6'C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Sail ( /A, water sample)
Did samples originate quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (inte DnaIIV,
IlYes I—Iincladine Hawaii and Puerto Iticot? (—IYes PINO
Comments/Disc mpancy:
Chain of Custody Present?
es
ON.
N/A
1.
Samples Arrived within Hold Time?
es
niv.
nNJA
2,
Short Hold Time Analysis 02 hr.)?
Yes
0
❑N/A
3.
Rush Turn Around Time Requested.?
Yes
o
QNJA
4.
Sufficient Volume?
121es
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
es
es
❑Na
No
❑NJA
N/A
6.
Containers Intact?
es
Na
NJA
7.
Dissolved analysis: Samples Field Filtered?
Oyes
o
N/A
9.
Sample Labels Match CW.
-Includes Date/Time/ID/Analysis Matrix:
es
[]No
❑N/A
9.
Headspace In VOA Vials (>5-6mm)?
❑Yes
a
NJA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
Fives
Qyes
o
No
❑NJA
N/A
11,
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Lot tO of split Containers:
Date/Time:
Field Data Required? []Yes ❑No
Project Manager SCURF Review: Date -
Project Manager SRF Review: Date:
Note: Whenever there is a discrepancy affecting North Catalina compliance Samples, a copy of this form will be sent to the North Carolina i)EHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 39 of 45

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692U4 liter Plastic Unpreserved (N/A)
SP4S-125 mL Plastic H25O4 (pH < 21(CI-(
BP3N-250 mL plastic HNO3 (pH < 2)
BP4Y-125 mL Plastic 2N Acetate & NaOH 1>91
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8P4C-125 mL Plastic NaOH (pH > 12) (Cl-)
WGFU-Wide-mouthed Glass l%u Unpreserved
AGIU-1 liter Amber Unpreserved (NIA) (CI-)
AG1H-1 liter Amber NO (PH < 2)
AG3U-250 ml, Amber Unpreserved IN/A1 (CI-)
AG1S-1 liter Amber H25O4 (pH r 21
AG35-250 mL Amber H2SO4 (PH < 2)
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D69H-40 mL VOA I (N/A)
VG9T-40 ml. VOA Na2S2O3 (N/Al
VG9U-40 ml VOA Unp (N/A1
OG9P-40 mL VOA 113PO4 IN/A)
VOAK 16 vials per kit(-5035 kit (N/Al
V/GK (3 vials per kitl-VPH/Gas kit (N/A)
SPST-175 mL Sterile Plastic IN/A — tab)
SP2T-250 mL Sterile Plastic (N/A — labl
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Semi-annual Stormwater Discharee Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted -Sune- 30 2411_+
CERTIFICATE OF COVERAGE NO. NCG03 O % (0
FACILITY NAME sei�`hw' fQ
COUNTY riieC►t (bc,rg
PERSON COLLECTING SAMPLES `iOda( CA7,*W*O1fof" -
LABORATORY Pce ce_ Lab Cert. # 12
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR ZU1_7
SAMPLE PERIOD E Jan -June ❑ July -Dec
or' ❑ Monthly' tmonth)
DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA
❑Zero -flow []WaterSupply []SA
RECEIVED ❑Other
JUL U 7 2WEASE REMEMBERTO SIGN ON PAGES 2 AND/OR 3 4
CENTRAL FILES
DWR SECTION
[❑ No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
P H,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organ&
Benchmarks =__>
_
-
100//�mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
6e,127-/17
2.04
0.9
(o.I
0.00Q>1
0.00S
0,005
S.D
4/01
2
sly /12
2.0
15.(0
(0.(
O.00S3
0 ,dos
0,010
5,0
3
S(zvjr
Z.pzf
IZ,G
&-1�
0,60Si
a,005
o,oto
5.10
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites maybe eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained In the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor'
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

` Facilities that incorporate a solvent management plan into the Stormwater Polll t n PreventiomPlan may so certify, and the requirement for TTO monif`orin
q g
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included In the stormwater Pollution Prevention Plan."
_-5-g ►1I0s P. R4,A v .e.
Name (Print name)
Title (Print title) - ^�
-30-- 7
Si ature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX malt.". where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L,
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inchess
Non -polar O&G/TPH by
EPA 2664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks ===>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 —9.0 SU
t
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must Implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B_
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an oriainal and one copy of this DIVIR including all "'No Discharae'reports. within 30 &ys of recelQt of the lab results tor at end of monitorin2Aeriod
Lli the case of "No Discharae"renortsl to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MST SIGN THISC-EBIJMTION FOR 8EIY INFORMATION REPORTED.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed ro
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations."
of Permittee)
Permit Date: 11/1/2012-10/31/2017
4, —Fd / -7
(Date)
SWU-245, last revised 10/25/2012
Page 3 of 3

NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: hU://I?ortal.ncdear.ore./weblwq/ws/su/ni2dessw#tab-4
Permit No.: or Certificate of Coverage No.:
Facility Name: S00-91t% Pe- ttfr-1Pfrsc,fl1e-
County: I'1' <041-e� b& r j - - Phone No. �oY 3 -;�9 %06
Inspector: 100
to
Date of Inspection: 2 2 o I ?L
Time of Inspection: c;qn l - 1IN-41
Total Event Precipitation (inches): 2.69
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
0 Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
} and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
ac�q► � lj.�G!
(Signature of Permittee or Designee) T
Page 1 of 2
SWU-242, last modified 10/25/2012

1. Outfall Description:
Outfall No. I Structure (pipe, ditch, etc.) PiK
Receiving Stream: 6ef1 nomeof a, ff-'19uf&ry Ya Cie_ CP-fAx
Describe the industrial activities that occur within the outfall drainage area:
-&n to grki o7 /lor i S,'ote c,(- Greif: /Dri
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: grey * c e-ct r
3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 170nQ-
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
= - 5. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
0 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes Na
10. Other Obvious Indicators of Stormwater Pollution:
List and describe 40 r12
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: hMp://portal.ncdenr.org/webl!gq/w.s/su/npdessw#tab-4
Permit No.: or Certificate of Coverage No.:
Facility Name: S00-hLji'rC th ntrrsv1ll e-
County: AfCk I -e-1 b&, rq _ Phone No. 20'/ 3 ;�9 61&06
inspector: 7Z44 C4 ✓cao(fa Ff
Date of Inspection: il% jr 2 2 2 a 1 _R _
Time of Inspection: apM - //A -,*I
Total Event Precipitation (inches): 2 .at/
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
[9Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
/ Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement Please refer to these definitions, if applicable.
`,.J
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
owe► - ��,�/�
(Signature of Permittee or Designee)
Page 1 of 2
SWU-242, Last modified 10/25/2012

1. Outfall Description:
Outfall No. 'k Structure (pipe, ditch, etc.) Di�2
Receiving Stream: Vn / t?0704 C&,-1 M (,1z7U la Ca h 2 Cte-e-K _
Describe the industrial activities that occur within the outfall drainage area:
0 wice- anal VI'sf�� 02100 h c ,/,N qLaoi
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: _SCIPa,r fir, l!2oLL kY _
3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 4e o4or
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
11 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes o�
9. Is there evidence of erosion or deposition at the outfall? Yes CNo)
10. Other Obvious Indicators of Stormwater Pollution:
List and describe &o'leJ
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
J may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, last modified 10/25/2012

IKW
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visithtWallpgrtal,ncdenr.org./web/wQ/ws/su/npdessw#tab-4
Permit No.: �/�/_/ o/����� or Certificate of Coverage No.:
Facility Name: 5001-hk,.,i r�2. tfL,11ttrSLsU1e.
County: A<0411� b&,rq Phone No. '�'09 379 61&00
Inspector: 7Mcf C ti,✓✓o o[ to ff
Date of Inspection: ^ 2-2- 2 o I� _
Time of Inspection: qt=?M - IlAtr+1—__-_--
Total Event Precipitation (inches): 2.69
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
13 Yes ❑ No
Please verify whether Qualitative Monitoring must be per during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event" However,
some permits do not have this requirement Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
aa� ,1.,.
(Signature of Permittee or Designee)
Page 1 of 2
SWU-242, Last modMed 10/25/2012

1. Outfall Description:
Outfall Na. 3 Structure (pipe, ditch, etc.) -p-1pp— wr 004(,S pono�
Receiving Stream: —ter?#?g4yd C'c",H;�n' _
Describe the industrial activities that occur within the outfall drainage area:
2. Color. Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: an C4 lr'g
3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): i?zg o ola r
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 0 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 11i�is no solids and 5 is the surface covered with floating solids:
elf 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
© 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes (o� -
9. Is there evidence of erosion or deposition at the outfall? Yes
/ ¢Vo J
10. Other Obvious Indicators of Stormwater Pollution:
List and describe ILZ
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

•
1c,
Analyiical
wwrmm
May 31, 2017
Steven Bollinger
Cardno MMA
1700 Kraft Dr
Suite 2050
Blacksburg, VA 24060
RE: Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Dear Steven Bollinger:
Pace Analytical Services, LLC
205 East Meadow Road - Suite A. -
Eden, NC 272BB
(336)623$921
Enclosed are the analytical results for sample(s) received by the laboratory on May 22, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
���
Taylor Ezell
[e-mail]
[phone]
Project Manager
Enclosures
cc: Don Chevy, Southwire
Rory Mullennex, Cardno MMBA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent or Pace Analytical Services, LLC.
Page 1 of 40

Pane Analytical Services, LLC
205 East Meadow Road - Suite A.
ceftlytical Eden, NC 27288
[phone]
CERTIFICATIONS
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Charlotte Certification 113s.
9800 Kinney Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification M 84
VirginWVELAP Certification #: 4&0221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiafVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shalt not 6e reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 40

CLAnalyilcal
rwW..paCml@b&0"
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
205 East Meadow Road - SuiWA,"
Eden, NC 27288
[phone]
Project:
2017 ,IAN-JUNE SEMI ANNUAL
Pace Project No.:
92341420
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92341420001
OF 01
EPA 1664B
JMS
1
PASI-C
EPA 608
RES
27
PASI-C
EPA200.7
SER
7
PASI-A
EPA625
RES
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
MDW
1
PASI-A
EPA 9040
MJSi
1
PASI-A
92341420002
OF #2
EPA 1664E
JMS
1
PAS1-C
EPA 608
RES
27
PASI-C
EPA 200.7
SER
7
PASI-A
EPA 625
RES
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
MDW
1
PASI-A
EPA 9040
MJS1
1
PASI-A
92341420003
OF 03
EPA 1664E
JMS
1
PASI-C
EPA608
RES
27
PASI-C
EPA 200.7
SER
7
PASI-A
EPA625
RES
58
PASI-C
EPA 624
GAW
34
PASt-C
SM 2540D
MDW
1
PASI-A
EPA 9040
MJS1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the mitten consent of Pace Analytical Services, LLC. Page 3 of 40

ceA y i al s
ewr¢pee C"
ANALYTICAL RESULTS
Project: 2017 JAN-JUNE SEMI ANNUAL
Pare Project No.: 92341420
Pate Analytical Services, LLC
205 East Meadow Road - Suite A,
Eden, NC 27288
[phone]
Sample: OF #1
Parameters
Lab ID: 92341420001 Collected: 05/22/17 10:00
Results Units Report Limit DF
Received: 05f22117 14:55 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND
mg1L
5.0
1
05/26/17 05:29
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA
3510
Aldrin
NO
ug/L
0.10
1
05123/1715:54 05/2511718:33
309-00-2
alpha-BHC
ND
ug1L
0.10
1
05123/1715:54 05/25/17 18:33
319-84-6
beta-BHC
ND
ug/L
0.10
1
05123/1715:54 05125/17 18:33
319-85-7
delta-BHC
ND
ug1L
0.10
1
0512311715:54 05/25/1718:33
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.10
1
0523117 15:54 05125/17 18:33
58-89-9
Chlordane (Technical)
ND
ug1L
1.0
1
05/23/17 15:54 05/25117 18:33
57-74-9
4,4'-DDD
ND
ug/L
0.10
1
0512311715:54 05f25/1718:33
72-54-8
4,4'-DDE
ND
ug1L
0.10
1
05123/1715:54 05125/1718:33
72-55-9
4,4'-DDT
ND
ug/L
0.10
1
05/23/1715:54 05125/17 18:33
50-29-3
Dieldrin
ND
ug/L
0.10
1
05/23/1715:54 05125M718:33
60-57-1
Endosulfan I
ND
ug/L
0.10
1
05/23/17 15:54 05/25/17 18:33
959-98-8
Endosulfan II
ND
ug/L
0.10
1
05/23/17 15:54 05/25/17 18:33
33213-65-9
Endosuffan sulfate
ND
ugfL
0A0
1
05/23/17 15:54 05/25/17 18:33
1031-07-8
Endrin
ND
ug1L
0.10
1
0512311715:54 0512511718:33
72-20-8
Endrin aldehyde
ND
ugfL
0.10
1
05/23/17 15:54 0525/17 18:33
7421-93-4
Heptachlor
ND
ugfL
0.10
1
0512311715:54 05125/17 18:33
76-44-8
Heptachlor epoxide
ND
ug/L
0.10
1
05/23117 15:54 05/25/17 18:33
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug1L
1.0
1
05/23/17 15:54 05/25/17 18:33
12674-11-2
PCB-1221 (AroGor 1221)
ND
ug/L
1.0
1
05/23/17 15:54 05/25/17 18:33
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug1L
1.0
1
05/23117 15:54 05/25/17 18:33
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug1L
1.0
1
05/23/17 15:54 05/25/17 18:33
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ugfL
1.0
1
05/23/17 15:54 05/25/17 18:33
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug1L
1.0
1
05/23/17 15:54 05/25/17 18:33
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/L
1.0
1
05/23/17 15:54 05/25/17 18:33
11096-82-5
Toxaphene
ND
ugfL
1.0
1
05/2311715:54 051251171833
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
76
%
20-110
1
05/23/17 15:54 05125/17 18:33
877-09-8
Decachlorolrphenyl (S)
28
%
20-138
1
05/23/17 15:54 05125M7 18:33
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND
ug1L
1.0
1
05/25/17 16:50 05/28/17 01:09
7440-43-9
Chromium
ND
ug/L
5.0
1
05/25/17 16:50 OSQ8117 01:09
7440-47-3
Copper
6.1
ug/L
5.0
1
05/25/17 16:50 05/28/17 01:09
7440-50-8
Lead
ND
ugfL
5.0
1
05/25/17 16:50 05/28/17 01:09
7439-92-1
Nickel
ND
ugfL
5.0
1
0525/17 16:50 0528117 01:09
7440-02-0
Silver
ND
ugfL
5.0
1
0525/17 16:50 05/28117 01:09
7440-22-4
Zinc
ND
ug/L
10.0
1
0525/17 16:50 0528117 01:09
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND
ug1L
5.0
1
0526117 09:00 05/30/17 21:25
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
0526/17 09:00 05/30/17 21:25
208-96-8
Anthracene
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
120-12-7
Benzo(a)anthracene
ND
ug(L
5.0
1
05/26/17 09:00 05/30/17 21:25
56-55-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/312017 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 40

Pace Analytical Services, LLC
n ©� t+� • 205 East Meadow Road - SLMeA.-
G/V Caly cal Eden, NC 27268
wwwP corn [phone]
ANALYTICAL RESULTS
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Sample: OF #1 Lab ID: 92341420001 Collected: 05/22/17 10:00 Received: 05/22/17 14:55 Matra: Water
Parameters
Resutts
Units
Report Limit
OF
Prepared Analyzed
625 MSSV
Analytical Method: EPA625
Preparation Method: EPA625
Benzo(a)pyrene
NO
ug1L
5.0
1
05/26/17 09:00 W30/17 21:25
Benzo(b)fluoranthene
NO
ug(L
5.0
1
05/26/17 09:00 M30/17 21:25
Benzo(g,h,i)perylene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
Benzo(k)ftuoranthene
NO
ug/L
5.0
1
M26/17 09:00 05/30/17 21:25
4-Bromophenylphenyl ether
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 21:25
Butylbenzylphthalate
NO
ug/L
5.0
1
05/26/17 09:00 OW30/17 21:25
4-Chloro-3-methytphenol
NO
ug/L
5.0
1
05/26/17 09:00 05130M7 21:25
bis(2-Chloroethoxy)methane
NO
uglL
10.0
1
05/26/17 09:00 05/30/17 21:25
bis(2-Chloroethyl) ether
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 21:25
2-Chtoronaphthatene
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 21:25
2-Chlorophenol
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
4-Chlorophenylpheno ether
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 2115
Chrysene
NO
ug/L
5.0
1
05I26117 09:00 05/30/17 21:25
Dibenz(a,h)arithracene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
05/26/17 09:00 05/30/17 21:25
2,4-Dichlomphenol
NO
ug/L
5.0
1
05/26/17 09:00 05130/17 21:25
Diethylphthatate
NO
ug/L
5.0
1
OW6117 09:00 05/30/17 21:25
2,4-Dimethytphenol
NO
uglL
10.0
1
05/26/17 09:00 05/30/17 21:25
Dimethylphthatate
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
Di-n-butylphthalate
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
4,6-Dinitro-2-methytphenol
NO
ug/L
20.0
1
05/26117 09:00 05/30/17 21:25
2,4-Dinitrophenot
NO
ug1L
50.0
1
05/26/17 09:00 05/30/17 21:25
2,4-Dindrotoluene
NO
ug/L
5.0
1
05/26/17 09:00 06/30/17 21:25
2,6-Dinitrotoluene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
Di-n-octylphthafate
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
Fluoranthene
NO
ug/L
- 5.0
1
05/26/17 09:00 05/30/17 21:25
Fluorene
NO
ug/L
5.0
1
05126/17 09:00 05/30/17 21:25
Hexachloro-1,3-butadiene
NO
ugIL
5.0
1
05/26/17 09:00 05/30/17 21:25
Hexachlorobenzene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
Hexachlorocyclopentadiene
NO
ug/L
10.0
1
05/26/17 09:00 05/30/17 21:25
Hexachloroethane
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
Indeno(1,2,3cd)pyrene
NO
ug/L
5.0
1
05126/17 09:00 05/30/17 21:25
lsophorone
ND
ug/L
10.0
1
05/26/17 09:00 05/30/17 21:25
Naphthalene
ND
uglL
5.0
1
05/26/17 09:00 05/30/17 21:25
Nitrobenzene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
2-Nitrophenol
NO
ug1L
5.0
1
05/26/17 09.00 05/30/17 21:25
4-Nitrophenol
NO
ug/L
50'0
1
05/26/17 09:00 05/30/17 21:25
N-Nitrosodimethylamine
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 21:25
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
05/26/17 09:00 05/30/17 21:25
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
Pentachlomphenol
ND
uglL
10.0
1
05/26/17 09:00 05/30/17 21:25
Phenanthrene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 21:25
Phenol
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 21:25
Pyrene
NO
uglL
5.0
1
05/26/17 09:00 05/30/17 21:25
1,2,4-Trichlombenzene
NO
ug/L
5.0
1
05)26117 09:00 W30117 21:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2017 05:04 PM without the wriieen consent of Pace Anatocal Services, LLC.
CAS No, Qual
50-32-8
205-99-2
191-24-2
207-08-9
101-55-3
85-08-7
59-50-7
111-91-1
111 44 4
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
91-94-1
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-20-3
98-95-3
88-75-5
100-02-7
62-75-9
621-64-7
86-30-6
108-00-1
87-86-5
85-01-8
108-95-2
129-00-0
120-82-1
M1
Page 5 of 40

Pace Anslytcal Services, LLC
n �e� l/+� f 205 East Meadow Road - Suite A.
C`/'7nalytica Eden, NC 27288
1!• w.P wM [phone]
ANALYTICAL RESULTS
Project. 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Sample: OF #1 Lab ID: 92341420001 Collected: 05122/17 10:00 Received: 05/22/17 14:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4,6-Trichlorophenol
ND
ug1L
10.0
1
05/26/17 09:00 05/30/17 21:25 88-06-2
Surrogates
Nitrobenzene-d5 (S)
52
%
10-120
1
05/26/17 09:00 05/30/17 21:25 4165-60-0
2-Fluarobiphenyl (S)
59
%
15-120
1
05/26/17 09:00 05/30/17 21:25 321-60-8
Terphenyl-d14 (S)
66
%
11-131
1
05/26/17 09:00 05/30/17 21:25 1718-51-0
Phenol-06 (S)
18
%
10-120
1
05/26/17 09:00 05/30/17 21:25 13127-88-3
2-Fluorophenol (S)
30
%
1D-120
1
05/26/17 09:00 05/30/17 21:25 367-12-4
24,6-Tribromophenol (S)
59
%
10-137
1
05/26/17 09:00 05/30/17 21:25 118-79-6
624 Volatile Organics Analytical Method: EPA 624
Benzene
ND
ug1L
2.0
1
05/23/17 20:28 71-43-2
Bromodichloramethane
ND
ug/L
2.0
1
05/23/17 20:28 75-27-4
Bromoform
ND
ug1L
2.0
1
05/23/17 20:28 75-25-2
Bromomethane
ND
ug/L
2.0
1
05/23/17 20:28 74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
05/23/17 20:28 56-23-5
Chlorobenzene
ND
ug/L
2.0
1
05/23/17 20:28 108-90-7
Chloroethane
ND
ug/L
2.0
1
05/23/17 20:28 75-00-3
Chloroform
ND
ug1L
2.0
1
05/23/17 20:28 67-66-3
Chloromethane
ND
ug1L
2.0
1
05/23/17 20:28 74-87-3
Dibromochloromethane
ND
ug1L
2.0
1
05/23/17 20:28 124-48-1
1,2-Dichlorobenzette
ND
ug1L
2.0
1
05/2311720:28 95-50-1
1,3-Dichlorobenzene
ND
ug1L
2.0
1
0512311720:28 541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
0512311720:28 106-46-7
1, 1 -Dichloroethane
ND
ug/L
2.0
1
0512311720:28 75-34-3
1,2-Dichioroethane
ND
ug1L
2.0
1
0512311720:28 107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
05123/1720:28 75-35-4
cis-1,2-Dichloroethene
ND
ug1L
2.0
1
05/23/17 20:28 156-59-2
trans-1,2-Dichlaroethene
ND
ug/L
2.0
1
05/23/17 20:28 156-60-5
1,2-Dichloropropane
ND
ug1L
2.0
1
05/23/17 20:28 78-87-5
cis-1,3-Dichloropropene
ND
ug1L
2.0
1
05/23/17 20:28 10061-01-5
trans-1,3-Dichloropropene
ND
ug[L
2.0
1
0512311720:28 10061-02-6
Ethylbenzene
ND
ugtL
2.0
1
05/23/17 20:28 100-41-4
Methylene Chloride
ND
ug/L
2.0
1
05/23/17 20:28 75-09-2
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
0512311720:28 79-34-5
Tetrachloroethene
ND
ug/L
2.0
1
05/23/17 20:28 127-18-4
Toluene
ND
ug1L
2.0
1
05/23/17 20:28 108-88-3
1,1,1-Trichioroethane
ND
ug/L
2.0
1
0512311720:28 71-55-6
1,1,2-Trichloroethane
ND
ug1L
2.0
1
05123/1720:28 79-00-5
Trichloroethene
ND
ug/L
2.0
1
05/23/17 20:28 79-01-6
Trichlomfluoromethane
ND
ugfL
2.0
1
05/23/17 20:28 75-69-4
Vinyl chloride
ND
ug/L
2.0
1
05123/1720:28 75-01-4
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
05/23/17 20:28 460-00-4
Toluene -dB (S)
104
%
70-130
1
05/23/17 20:28 2037-26-5
1,2-Dichioroethane-d4 (S)
93
%
70-130
1
05/23/17 2028 17060-07-0
REPORT OF LABORATORY ANALYSIS
This report snarl not be reproduced. except in full,
Date: 05/31/2017 05:04 PM witfmut the written consent of Pace Analytical Services, LLC. Page 6 of 40

IC
emalytica!
www4ecefab&="
ANALYTICAL RESULTS
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Pace Analytical Services, LLC
205 East Meadow Road - Suite A.
Eden, NC 27288
[phone]
Sample: OF 91 Lab ID: 92341420001 Collected: 05/22/17 10:00 Received: 05/22/17 14:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Anafyzed CAS No. Qual
2540D TSS, Low -Level Analytical Method: SM 2540D
Total Suspended Solids 14.8 mg1L 1.2 1 05/23/17 00:42
9040 pH Analytical Method: EPA 9040
pH 6.1 Std. Units 0.10 1 05/23/17 20:30 H6
Date: 05/31/2017 05:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written Consent of Pace Analytical Services, LLC.
Page 7 of 40

Pace Analytcal Services, LLC
CeQ h/�«205 East Meadow Road - Suite A.
p v+����J �' Eden, NC 27288
"°'"' Acom [phone]
ANALYTICAL RESULTS
Project: 2017 JAN4UNE SEMI ANNUAL
Pace Project No.: 92341420
Sample: OF #2 Lab ID: 92341420002 Collected: 05/22/17 10:20 Received: 05122/17 14:55 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease NO mg/L 5.0 1 05/26/17 05:30
608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosuffan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
PCB-1016 (Arodor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Arodor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCS-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlombiphenyl (S)
200.7 MET ICP
NO
ugfL
0.050
1
05123/1715:54 05/2511718:51
309-00-2
NO
ug/L
0.050
1
0512311715:54 0512511718:51
319454-6
NO
ug1L
0.050
1
0512311715:54 0512511718:51
319435-7
NO
ugfL
0.050
1
05/2311715:54 0512511718:51
319-86-8
NO
ug1L
0.050
1
05/23/1715:54 0512511718:51
58-89-9
NO
ug/L
0.50
1
0512311715:54 05125/1718:51
57-74-9
ND
ug/L
0.050
1
0512311715:54 05125/1718:51
72-54-8
ND
ug/L
0.050
1
05/2311715:54 05/2511718:51
72-55-9
NO
ug/L
0.050
1
05/2311715:54 0512511718:51
50-29-3
ND
ug/L
0.050
1
0512311715:54 05/2511718:51
60.57-1
NO
ug/L
0.050
1
05123/1715:54 05/2511718:51
959-98-8
ND
ug/L
0.050
1
05123/1715:54 05/2511718:51
33213-65-9
NO
ug/L
0.050
1
0512311715:54 05/25/1718:51
1031-07-8
NO
ug/L
0.050
1
05/23/17 15:54 051251W 18:51
72-20-8
NO
ug/L
0.050
1
05/2311715:54 05/25/1718:51
7421-93-4
NO
ug/L
0.050
1
0512311715:54 05/2511718:51
76A4-8
NO
ug/L
0.050
1
0512311715:54 05/2511718:51
1024-57-3
NO
ug/L
0.50
1
0512311715:54 05/2511718:51
12674-11-2
NO
ug1L
0.50
1
0512311715:54 05/2511718:51
1110428-2
NO
ug1L
0.50
1
051231W 15:54 05/25/17 18:51
11141-16-5
NO
ug1L
0.50
1
0512311715:54 0512511718:51
53469-21-9
NO
ug1L
0.50
1
0512311715:54 0512511718:51
12672-29.6
NO
ug/L
0.50
1
0512311715:54 0512511718:51
11097-69-1
NO
ug1L
0,50
1
0512311715:54 0512511718:51
11096-82-5
NO
ug1L
0.50
1
0512311715:54 05/2511718:51
8001-35-2
70
%
20-110
1
05/2311715:54 0512511718:51
877-09-8
33
%
20-138
1
0512311715:54 05/25/1718:51
2051-24-3
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
NO
ug/L
1.0
1
05/25/17 W50 05/28/17 01:12
744n 43-9
Chromium
NO
ug/L
5.0
1
05/25/17 1&50 05/28/17 01:12
7440-47-3
Copper
5.3
ug1L
5.0
1
05/25/17 16:50 05128/17 0112
7440-50-8
Lead
NO
ug/L
5.0
1
05/25/17 16:50 05/28/17 01:12
7439-92-1
Nickel
NO
ug/L
5.0
1
05/25/17 16:50 W28117 01:12
7440-02-0
Silver
ND
ug/L
5.0
1
05/25/17 16:50 05/28/17 01:12
7440-22-4
Zinc
10.1
ug/L
10.0
1
05/25/17 16:50 05/28/17 01:12
7440-66-6
625 MSSV
Analytical Method: EPA625 Preparation Method: EPA625
Acenaphthene
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:22
83-32-9
Acenaphthylene
NO
ugfL
5.0
1
05/26/17 09:00 05/30/17 22:22
208-96-8
Anthracene
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:22
120-12-7
Benzo(a)anthracene
ND
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:22
56-55-3
REPORT OF LABORATORY ANALYSIS
This report shed not be reproduced, except in full.
Date: 05/31 /2017 05:04 PM without the written consent of race Analytical Services, LI-C. Page 8 of 40

C2/''11 alyti QI •
WWePacatabs.cun
ANALYTICAL RESULTS
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Pace Analytical Services, LLG
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: OF #2 Lab ID: 92341420002 Collected: 05/22/17 10:20 Received: 05/22/17 14:55 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Benzo(a)pyrene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 50-32-8
Benzo(b)tluoranthene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 205-99-2
Benzo(g,hJ)perylene
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:22 191-24-2
Benzo(k) luoranthene
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:22 2074)8-9
4-Bromophenylphenyl ether
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 101-55-3
Butylbenzylphthalate
NO
ug/L
5.0
1
05126/17 09:00 05130/17 22:22 85-68-7
4-Chloro-3-methylphenol
NO
ug/L
5.0
1
05126/17 09:00 05/30/17 22:22 59-50-7
bis(2-Chloroethoxy)methane
NO
ug/L
10.0
1
05/26/17 09:00 05/30/17 22:22 111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 11144 4
2-Chloronaphthalene
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 91-58-7
2-Chlorophenol
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 95-57-8
4-Chlorophenylphenyl ether
ND
uglL
5.0
1
05/26/17 09:00 05/30/17 22:22 7005-72-3
Chrysene
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 218-01-9
Dibenz(a,h)anthracene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 53-70-3
3,3'-Dichlorobenzidine
NO
ug/L
25.0
1
05/26/17 09:00 05/30/17 22:22 91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
05/26117 09:00 05/30/17 22:22 120-83-2
Diethylphthalate
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 84-66-2
2,4-Dimethylphenol
NO
ug/L
10.0
1
05/26/17 09:00 05/30/17 22:22 105-67-9
Dimethyfphthatate
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 131-11-3
Di-n-butylphthalale
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 84-74-2
4,6-Dinitro-2-methylphenol
NO
ug/L
20.0
1
05/26/17 09:00 05/30/17 22:22 534-52-1
2,4-Dinitrophenol
NO
ug/L
50.0
1
05/26/17 09:00 05/30/17 22:22 51-215-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 606-20-2
Di-n-octylphthalate
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 117-84-0
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 117-81-7
Fluoranthene
NO,
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 206-44-0
Fluorene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 86-73-7
Hexachloro-11,3-buta6ene
NO
ug1L
5.0
1
05126/1709:00 0513011722:22 87-68-3
Hexachlorobenzene
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:22 118-74-1
Hexachlorocyclopentadiene
NO
ug/L
10.0
1
05/26/17 09:00 05/30/17 22:22 77-47-4
Hexachloroethane
NO
ug/L
5.0
1
05/26/17 09:00 05130/17 22:22 67-72-1
fndeno(1,2,3-cd)pyrene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 193-39-5
Isophorone
NO
ug1L
10.0
1
05/26/17 09:00 05/30/17 22.22 78-59-1
Naphthalene
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:22 91-20-3
Nitrobenzene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 W75-5
4-Nitrophenol
ND
ug/L
50.0
1
05/26/17 09:00 05/30/17 22:22 100-02-7
N-Nitrosodimethylamine
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 62-75-9
N-Nitroso-di-n-propytamine
ND
ug/L
5.0
1
05126/1109:00 05/30/17 22:22 621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
05/26/17 09:00 05/30/17 22.22 86-30-0
2,2'-0xybis0-chloropmpane)
NO
uglL
5.0
1
05/26117 09:00 05/30/17 22:22 108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
05/26/17 09:00 05/30/17 22:22 87-86-5
Phenanthrene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 85-01-8
Phenol
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 108-95-2
Pyrene
ND
ug/L
5.0
1
05/26/17 09700 05/30/17 22:22 129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:22 120-82-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2017 05:04 PM wldmut the written consent of Pace Analytical Services, LLC. Page 9 of 40

Pace Analytical Services, LLC,
205 East Meadow Road - Suite A
,ftyimleEden. NC 27288
I!
wwwP acorn [phone]
ANALYTICAL RESULTS
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Sample: OF #2 Lab ID: 92341420002 Collected: 05I22117 10:20 Received: 05/22/17 14:55 Matrix: Water
Parameters
Results
Units
Report Limit
OF
Prepared Analyzed
CAS No. Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
05/26/17 09:00 05/30/17 22:22
88-06-2
Surrogates
Nitrobenzene-d5 (S)
49
%
10-120
1
05/26/17 09:00 05/30/17 22:22
4165-60-0
2-Fluorobiphenyl (S)
57
%
15-120
1
05/26/17 09:00 05/30/17 22:22
321-60-8
Terphenyt-d14 (S)
83
%
11-131
1
05/26/17 09:00 05/30/17 22:22
1718-51-0
Phenol-d6 (S)
13
%
10-120
1
05/26/17 09:00 05/30/17 22:22
13127-88-3
2-Fluorophenol (S)
14
%
10-120
1
05/26/17 09:00 05/30/17 22:22
367-12-4
2,4,6-Tribromophenol (S)
38
%
10-137
1
05/26/17 09:00 05/30/17 22:22
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
NO
ug/L
2.0
1
05/23/17 20:46
71-43-2
Bromodichloromethane
NO
ug/L
2.0
1
05/23/17 20:46
75-27-4
Bromoform
NO
ug/L
2.0
1
05/23/17 20:46
75-25-2
Bromomethane
NO
ug/L
2.0
1
05/23/17 20:46
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1
05/23/17 20:46
56-23-5
Chiorabenzene
NO
uglL
2.0
1
05/23/17 20:46
108-90-7
Chtoroethane
NO
ug/L
2.0
1
05123/17 20:46
75-00-3
Chloroform
NO
ug/L
2.0
1
05/23/17 20:46
67-66-3
Chloromelhane
NO
ug/L
2.0
1
05/23/17 20:46
74-87-3
Dibromochloromethane
NO
ug/L
2.0
1
05/23/17 20:46
124-48-1
1,2-Dichlorobenzene
NO
ug/L
2.0
1
05/2311720:46
95-50-1
1,3-Dichlorobenzene
NO
ug1L
2.0
1
05/23/1720:46
541-73-1
1,4-Dichlorobenzene
NO
ug/L
2.0
1
05/2311720:46
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1
05/2311720:46
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1
05/23/17 20:46
107-06-2
1,1-Dichloroethene
NO
ugll.
2.0
1
0512311720:46
75-35-4
cis-1,2-Dichloroethene
NO
ug/L
2.0
1
0512311720:46
156-59-2
trans-1,2-Dichioroethene
NO
ug/L
2.0
1
05/2311720:46
156-60-5
1,2-Diehloropropane
NO
ug/L
2.0
1
05/2311720:46
78-87-5
cis-1,3-Dichloropropene
NO
ug/L
2.0
1
0512311720:46
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
05123/17 20:48
1OD61-02-6
Ethylbenzene
ND
ug1L
2.0
1
05123/17 20:46
100-414
Methylene Chloride
ND
ug/L
2.0
1
05/23/17 20:46
75-09-2
1,1,2,2-Tetrachloroethane
NO
uglL
2.0
1
0512311720:46
79-34-5
Tetrachloroethene
NO
ug/L
2.0
1
05/23/17 20:46
127-18-4
Toluene
NO
ug/L
2.0
1
05123/17 20:46
108-88-3
1, 1, 1 -Trichloroethane
NO
ug/L
2.0
1
0512311720:46
71-5"
1,1,2-Trichloroethane
NO
ug/L
2.0
1
05/2311720:46
79-00-5
Trichloroethene
NO
ug1L
2.0
1
05/23/17 20:46
79-01.6
Trichlorofluoromethane
ND
ug/L
2.0
1
05/23/17 20:46
75-69-4
Vinyl chloride
NO
ug/L
2.0
1
05123/17 20:46
75-01 4
Surrogates
4-Bromofluorobenzene (S)
104
%
70-130
1
05/23/17 20:46
460-00-4
Toluene-d8 (S)
110
%
70-130
1
05/23/17 20:46
2037-26-5
1,2-Dichloroethane-d4 (S)
90
%
70-130
1
05/23/17 20:46
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall nut be reproduced, except in full,
Date: 05/31/2017 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 40

ceAnaly wl e
erwP*Cehab&=n
ANALYTICAL RESULTS
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Pace Ana"cal Services, LLC,'
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: OF #2 Lab ID: 92341420002 Collected: 05/22/17 10:20 Received: 05/22/17 14:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D TSS, Low -Level Analytical Method: SM 2540D
Total Suspended Solids 15.6 mg/L 1.6 1 05/23/17 00:42
9040 pH Analytical Method: EPA 9D40
pH 6.1 Std. Units 0.10 1 05/23/17 20:30 H6
Dale: 05/31/2017 05:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 40

wwwpwaws.com
ANALYTICAL RESULTS
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Pace Analytical Services, LLC. '
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: OF 93 Lab ID: 92341420003 Collected: 05R2117 11:00 Received: 05/22/17 14:55 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No.
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND
mg/L
5.0
1
05/26/17 05:30
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
ND
ug/L
0.050
1
05/2311715:54 05/25/1719:26
309-00-2
alpha-BHC
ND
ug/L
0.050
1
0512311715:54 05/25/1719.26
319-84-6
beta-13HC
ND
ug/L
0,050
1
05/2311715:54 0512511719:26
319-85-7
delta-BHC
ND
ug/L
0.050
1
05/23/1715:54 05/2511719:26
319-8"
gamma-BHC (Lindane)
ND
ug/L
0.050
1
05/23/17 15:54 05/25/17 19-26
58-89-9
Chlordane (Technical)
ND
ug/L
0,50
1
05/23/17 15:54 05/25/17 19:26
57-74-9
4,4'-DDD
ND
ug/L
0.050
1
0512311715:54 0512511719:26
72-54-8
4,4'-DDE
ND
ug/L
0.050
1
05/2311715:54 0512511719:26
72-55-9
4,4'-DDT
ND
ug/L
0.050
1
05/2311715:54 05/2511719:26
50-29-3
Dieldrin
ND
ug/L
0.050
1
05123/1715:54 05/2511719:26
60-57-1
Endosulfan I
ND
ug/L
0.050
1
05/23/17 15:54 05/25/17 19:26
959-98-8
Endosutfan II
ND
ug/L
0.050
1
05/23/17 15:54 05/25/17 19:26
33213-65-9
Endosutfan sulfate
ND
ug1L
0.050
1
05/23/17 15:54 05i25t17 19:26
1031-07-8
Endrin
ND
ug/L
0.050
1
0512311715:54 05/2511719:26
72-20-8
Endrin aldehyde
ND
ug/L
0.050
1
05/23/17 15:54 05/25/17 19:26
7421-93-4
Heptachlor
ND
ug/L
0.050
1
05/23/1715:54 05125/1719:26
76-44-8
Heptachlor epoxide
ND
ug/L
0.050
1
05/23/17 15:54 05/25/17 19:26
1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
1
05/23/17 1554 05/25/17 19:26
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
1
05/23/17 15:54 05/25/17 19:26
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
1
05Q3/17 1554 05/25/17 19:26
11141-16-5
PCB-1242 (Aro for 1242)
ND
ug/L
0.50
1
05/23/17 15:54 05/25/17 1926
53469-21-9
PCB-1248 (Aroclor 1248)
ND
u9/L
0.50
1
05/23/17 15:54 05/25/17 1926
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
1
05/23/17 15:54 05/25/17 19:26
11097-69-1
PCB-1260 (Arodor 1260)
ND
ug/L
0.50
1
05/23/17 15:54 05/25/17 1926
11096-82-5
Toxaphene
ND
ug1L
0.50
1
05123/17 15:54 05/25/17 19:26
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
67
%
20-110
1
05/23/17 15:54 05/25/17 19:26
877-09-8
Decachlorobiphenyl (S)
44
%
20-138
1
05/23/17 15:54 05/25/17 19:26
2051-24-3
200.7 MET ICP
Analytical Method:
EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND
ug/L
1.0
1
05125/17 16:50 05/28/17 01:25
7440-43-9
Chromium
ND
u91L
5.0
1
05/25/17 16:50 05/28/17 01:25
7440-47-3
Copper
5.1
ug/L
5.0
1
05/25/17 16:50 05/28/17 01:25
7440-50-8
Lead
ND
uglL
5.0
1
05/25/17 16:50 05/28/17 01-25
7439-92-1
Nickel
ND
ug/L
5.0
1
05/25/17 16:50 05/28/17 01:25
7440-02-0
Silver
ND
ug1L
5.0
1
05/25/17 16:50 05/28/17 01:25
7440-22-4
Zinc
ND
ug1L
10.0
1
05/25/17 16:50 05/2B117 01:25
7440-66-6
625 MSSV
Anatytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
83-32-9
Acenaphthylene
ND
ug1L
5.0
1
05126/17 09:00 05/30/17 22:51
208-98-8
Anthracene
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
56-55-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05/31/2017 05:04 PM without the written consent of Pace Analytical Services, LLC.
Qual
Page 12 of 40

Pace Analytical Services, LLQ.
/+205 East Meadow Road - Suite A
V"c l/ekv+�/ Eden, NC 27288
wrw.pecnfabscam [phone]
ANALYTICAL RESULTS
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Sample: OF #3 Lab ID: 92341420003 Collected: 05/22/17 11:00 Received: 05/22/17 14:55 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Benzo(a)pyrene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
50-32-8
Benzo(b)fluoranthene
NO
ug1L
5.0
1
05/26/17 09:00 0513(Y17 22:51
205-99-2
Benzo(g,hJ)perylene
NO
uglL
5.0
1
05/26/17 09:00 05/30/17 22:51
191-24-2
Benzo(k)fluoranthene
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
207-08-9
4-Bromophenylphenyl ether
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
101-55-3
Butytbenzylphthalate
NO
ug/L
5.0
1
05/26/17 09:00 05130/17 22:51
85-68-7
4-Chloro-3-methylphenol
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
59-50-7
bis(2-Chloroethoxy)methane
NO
ug1L
10.0
1
05/26/17 09:00 05/30/17 22:51
111-91-1
b is(2-Chloroethyl) ether
NO
ug/L
5.0
1
05/26/17 09:00 05130117 22:51
Ill 44 4
2-Chloronaphthalene
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
91-58-7
2-Chlorophenol
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
95-57-8
4-Chlorophenylphenyl ether
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
7005-72-3
Chrysene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
218-01-9
Dibenz(a,h)anthracene
NO
ug/L
5.0
1
05/26/17 09:00 05130/17 22:51
53-70-3
3,3'-Dichlorobenzidine
NO
ug1L
25.0
1
05/26/1709:D0 05/3011722:51
91-94-1
2,4-DicNorophenol
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
120-83-2
Diethylphthalate
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
84-66-2
2,4-Dimethytphenol
NO
uglL
10.0
1
05/26/17 09:00 05130/17 22:51
105-67-9
Dimethylphthalate
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
131-11-3
Di-n-butylphthalate
NO
ug1L
5.0
1
05/26/17 09:DO 05/30/17 22:51
84-74-2
4,6-Dinitro-2-methylphenol
NO
ug1L
20.0
1
05/26/17 09:00 05/30/17 22:51
534-52-1
2,4-Dinitrophenol
NO
ug/L
50.0
1
05/26/17 09:00 05/30/17 22:51
51-28-5
2,4-Dinitrotoluene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
606-20-2
Di-n-octyiphthalate
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
117-8"
I.is(2-Ethylhexyl)phthalate
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
117-81-7
Fluoranthene
NO
ug/L
5.0
1
05/26/17 09:00 05130/l7 22:51
20644-0
Fluorene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
86-73-7
Hexachloro-1,3-butadiene
NO
ug/L
5.0
1
05/26/17 09:00 05130/17 22:51
87-68-3
Hexachlorobenzene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
118-74-1
Hexachlorocyclopentadiene
ND
uglL
10.0
1
05/26/17 09:00 05/30/17 22:51
77-474
Hexachloroethane
ND
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
67-72-1
Indeno(1,2,3-cd)pyrene
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
193-39-5
Isophorone
ND
ug/L
10.0
1
05/26/17 09:00 05/30/17 22:51
78-59-1
Naphthalene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
91-20-3
Nitrobenzene
ND
uglL
5.0
1
05/26/17 09:00 05r"17 22:51
98-95-3
2-Nitrophenol
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
88-75-5
4-Nitrophenol
ND
uglL
50.0
1
05/26/17 09:00 05/30/17 22:51
100-02-7
N-Nitrosodimethylamine
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
62-75-9
N-Nitroso-di n-propylamine
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
621-64-7
N-Nitrosodiphenylamine
NO
ug1L
10.0
1
05/26/17 09:00 05/30/17 22:51
86-30-6
2,2'-Oxybis(i-chloropmpane)
NO
ug1L
5.0
1
05/26/17 09:00 05/30/17 22:51
10"D-1
Pentachlorophenol
NO
ug1L
.10.0
1
05/26/17 09:00 05/30/17 22:51
87-86-5
Phenanthrene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
85-01-8
Phenol
NO
uglL
5.0
1
05/26/17 D9:00 05/30/17 22:51
108-95-2
Pyrene
NO
ug/L
5.0
1
05/26/17 09:00 05/30/17 22:51
129-00-0
1,2,4-Trichlorobenzene
NO
ug/L
5.0
1
05/26/17 09:00 M30117 22:51
120-62-1
REPORT OF LABORATORY ANALYSIS
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Date: 05/31 /2017 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 40

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ANALYTICAL RESULTS
Pace Analytical Services, LLC.
205 East Meadow Road - Su<te A
Eden, NC 27268
[phone]
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Sample: OF #3 Lab ID: 92341420003 Collected: 05/22/17 11:00 Received: 05/22/17 14:55 Matrix: Water
Parameters
625 MSSV
2,4,6-Trichlorophenol
surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluomphenol (S)
2,4,6-Tribromophenol (S)
624 Votatile Organics
Benzene
Bromodichloromethane
Brornofonn
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane
1,2-Dichlorobenzene
1, 3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-DiChloroethene
cis-1,2-Dichloroethene
trans-1 ,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- l ,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1. 1. 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene -dB (S)
1,2-Dichloroethane-d4 (S)
Date: 05/31/2017 05:04 PM
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 625 Preparation Method: EPA 625
ND ug/L 10.0 1 05/26/17 09:00 05/30/17 22:51 68-06-2
63
%
70
%
83
%
23
%
36
%
77'
%
Analytical Method: EPA 624
ND
ug/L
ND
ug1L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
NO
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
uglL
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100 %
103 %
92 %
10-120
1
05/26/17 09:00 05/30/17 22:51
4165-60-0
15-120
1
05/26/17 09:00 05/30/17 22:51
321-60-8
11-131
1
05/26/17 09700 05/30/17 22:51
1718-51-0
10-120
1
05/26/17 09:00 05/30/17 22:51
13127-88-3
1 D-120
1
05/26/17 09:00 05/30/17 22:51
367-12-4
1 D-137
1
05/26/17 09:00 05/30/17 22:51
118-79-6
2.0
1
05/23/17 21:21
71-43-2
2.0
1
05/23/17 21:21
75-274
2.0
1
05/23/17 21:21
75-25-2
2.0
1
05/23/17 21:21
74-83-9
2.0
1
05/23/17 21:21
56-23-5
2.0
1
05/23/17 21:21
108-90-7
2.0
1
05/23/17 21721
75-00-3
2.0
1
05/23/17 21:21
67-06-3
2.0
1
05/23/17 21:21
74-87-3
2.0
1
05/23/17 21:21
124-48-1
2.0
1
05/23/17 21:21
95-50-1
2.0
1
05/23/17 21:21
541-73-1
2.0
1
05/23/17 21:21
106-46-7
2.0
1
05/23/17 21:21
75-34-3
2.0
1
05/23/17 21:21
107-06-2
2.0
1
05/23/17 21:21
75-35-4
2.0
1
05123M 7 21:21
156-59-2
2.0
1
05/23/17 21:21
156-60-5
2.0
1
05/23/17 21:21
78-87-5
2.0
1
05/23/17 21:21
10061-01-5
2.0
1
05/23/17 21:21
10061-02-6
2.0
1
05/23/17 21:21
100414
2.0
1
05/23/17 2121
75-09-2
2.0
1
05/23/17 21:21
79-34-5
2.0
1
05/23/17 21:21
127-184
2.0
1
05/23/17 21:21
108-88-3
2.0
1
05/23/17 21:21
71-55-6
2.0
1
05/23/17 21:21
79-00-5
2.0
1
05/23/17 21:21
79-01-6
2.0
1
05/23/17 21:21
75-694
2.0
1
05/23/17 21:21
75-014
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in toll,
wttfiout the written consent of Pace Anatyfi al Services, LLC,
05/23/17 21:21 460-00-4
05/23/17 21:21 2037-26-5
05/23/17 21:21 17060-07-0
Page 14 of 40

•
ceARalytiCal
WWW..p8c%hbs.Cam
ANALYTICAL RESULTS
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Pace Analytical Services, LLC ,'
205 East Meador Road - Srate A
Eden, NC 27288
[phone]
Sample: OF #3 Lab ID: 92341420003 Collected: OSQ2/17 11:00 Received: 05/22/17 14:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
2540D TSS, Low -Level Analytical Method: SM 2540D
Total Suspended Solids 12.6 mg11- 1.0 1 05/23/17 00:42
9040 pH Analytical Method: EPA W40
PH 6.4 Std. Units 0.10 1 05/23/17 20:30 H6
Date: 05/31/2017 05:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 40

ceAI78 cal
www-pacewscom
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
QC Batch: 362361 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 9234142DOG1, 92341420002, 92341420003
METHOD BLANK: 2DO9348 Matrix: Water
Associated Lab Samples: 9234142000i, 92341420002, 92341420003
Blank Reporting
Parameter Units Result Limit Analyzed Qualfiers
Oil and Grease mg/L ND 5.0 05/26/17 05:28
Pace Analytical Services, LLC,
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE:
2009349
Spike LCS
LGS
% Rec
Parameter
Units
Conc, Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 37.9
95
78-114
MATRIX SPIKE SAMPLE:
2009350
92340923004 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
38.6
96
78-114
Ra ftz pneernsd an this papa are in the radb Inmeatad by the "thd " oWurrpr exeept e*ure an attereate urAt is preaen. to un npHt of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Lull,
Date: 05/3l /2017 05:04 PM wifhaut the written consent of Pace Analytical Services, LLG. Page 16 of 40

IeAIIc7ifjflC,al
Wawpacwabsaom
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
QC Batch: 362143 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92341420001, 92341420002, 92341420003
METHOD BLANK_ 2008213
Matrix:
Water
Associated Lab Samples:
92341420001, 92341420002, 92341420003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug1L
ND
1.0
05/28117 00:07
Chromium
uglL
ND
5.0
05/28/17 00:07
Capper
ug1L
ND
5.0
05/28/17 00:07
Lead
uglL
NO
5.0
05/28/17 00:07
Nickel
uglL
NO
5.0
05/28/17 00:07
Silver
uglL
ND
5.0
05/28/17 00:07
Zinc
ug1L
NO
10.0
05/28/17 00:07
LABORATORY CONTROL SAMPLE: 2008214
Pace Analytical Services, LLC,
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
ug1L
500
498
100
85-115
Chromium
ug1L
500
495
99
85-115
Copper
uglL
500
505
101
85-115
Lead
uglL
500
494
99
85-115
Nickel
ug1L
500
486
97
85-115
Silver
ug1L
250
248
99
85-115
Zinc
uglL
500
506
101
85-115
MATRIX SPICE & MATRIX SPIKE DUPLICATE:
2008215
2008216
MS
MSD
92341484001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug1L
<0.50
500
500
511
491
102
98
70-130
4
Chromium
ug/L
<2.5
500
500
506
484
101
97
70-130
4
Copper
ug1L
<2.5
500
500
519
500
104
100
70-130
4
Lead
ug1L
<2.5
500
500
503
482
100
96
70-130
4
Nickel
uglL
<2.5
S00
500
493
474
99
95
70-130
4
Silver
ugfL
<2.5
250
250
253
243
101
97
70-130
4
Zinc
ug(L
<2.5
500
500
519
499
104
100
70-130
4
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
20D8217
2008218
MS
MSD
92341310001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Cori.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug1L
NO
500
500
496
489
99
98
70-130
1
Chromium
ug1L
7.8
500
S00
493
493
97
97
70-130
0
Pmdhr pr - rdW en Mio papa an In
She urtfa iedicaW by dm
"UnW ooMu m exV Mre an utrn 2W wQ is Waaented So the rW or the resort
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31 /2017 05:04 PM witlwut the written consent of Pace Analytical Services, LLC. Page 17 of 40

Pace Analytical Services, LLC .
��7g
CBAnalyfical
205 East
Meadow Road - Suite A
Eden, NG 27288
ae►w.pWWab& vn
(3M)623-8921
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2008217
2008218
MS
MSD
92341310001
Spike
Spike
MS
MSD
MS
MSD
% Rec '
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper
ug/L
27.6
500
500
542
533
103
101
70-130
2
Lead
ug/L
ND
500
500
469
462
94
92
70-130
2
Nickel
ug/L
9.5
500
500
472
467
93
91
70-130
1
Silver
ug/L
ND
250
250
249
245
99
98
70-130
1
Zinc
ug/L
13.2
500
500
507
505
99
98
70-130
0
Rawris prsssndd on this paps we In On units ugiaafed by Ow "U tW aWwM sxospt vow& sn rdbnnta urd is prswrdsd to the rWd of the rwAt
REPORT OF LABORATORY ANALYSIS
This reporl shall not be reproduced, except in foil,
Date: 05/3112017 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 40

a
CeAnalytical
www.peoereba.00m
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
QC Batch: 361854 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92341420001, 92341420002, 92341420003
METHOD BLANK: 2006656 Matrix: Water
Associated Lab Samples: 92341420001, 92341420002, 92341420003
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1-Trichloroethane
ug1L
NO
2.0
05123/1715:26
1,1,2,2-Tetrachloroethane
ug1L
ND
2.0
0512311715:26
1,1,2-Trichloroethane
ug1L
NO
2.0
05/23/1715:26
1,1-Dichloroethane
ug1L
ND
2.0
M23/1715:26
1,1-Dichloroethene
ug1L
NO
2.0
05123/1715:26
1,2-Dichlorobenzene
ug1L
NO
2.0
05123/1715:26
1,2-Dichloroethane
ug1L
NO
2.0
05/2311715:26
1,2-Dichloropropane
ug1L
ND
2.0
0512311715:26
1,3-Dichlorobenzene
ug1L
ND
2.0
05123/1715:26
1,4-Dichlorobenzene
ug1L
NO
2.0
0512311715:26
Benzene
ug1L
NO
2.0
0512311715:26
Bromodichloromethane
ug1L
ND
2.0
0512311715:26
Bromoform
ug1L
ND
2.0
0512311715:26
Bromomethane
ug1L
ND
2.0
0512311715:26
Carbon tetrachloride
ug1L
ND
2.0
05/23/17 15:26
Chlorobenzene
ug/L
ND
2.0
05/23/1715:26
Chloroethane
uglL
ND
2.0
05123/1715:26
Chloroform
ug1L
ND
2.0
05/2311715:26
Chloromethane
ug1L
ND
2.0
05/2311715:26
cis-1,2-Dichloroethene
uglL
ND
2.0
05/2311715:26
cis-1,3-Dichloropropene
ug1L
ND
2.0
D512311715:26
Dibromochloromethane
ug1L
ND
2.0
05/2311715:26
Ethylbenzene
ug1L
ND
2.0
W23M715:26
Methylene Chloride
ug1L
NO
2.0
05/23/17 15:26
Tetrachloroethene
ug1L
NO
2.0
M23/1715:26
Toluene
ug1L
NO
2.0
05123/1715:26
trans-1,2-Dichloroethene
ug1L
NO
2.0
05/23/1715:26
trans-1,3-Dichloropropene
ug1L
NO
2.0
05/23/1715:26
Trichlomethene
ug1L
NO
2.0
05/23/1715:26
Trichlorofluoromelhane
ug1L
NO
2.0
0512V1715:26
Vinyl chloride
ugfL
NO
2.0
05/23/17 15:26
1,2-Dichloroethane-d4 (S)
%
87
70-130
05/23/17 15:26
4-Bromofluorobenzene (S)
%
100
70-130
05123M7 15:26
Toluene-d8 (S)
%
1D6
70`130
05/23/17 15:26
Qualifiers
Pace Analytical Services, LLC .
205 East Meadow Road - Suite A'
Eden, NC 27268
[phone]
LABORATORY CONTROL SAMPLE: 2006657
Spike LCS LCS % Rec
Parameter Units Conc. Resutt % Rec Limits Qualifiers
1, 1, 1 -Trichloroethane ug1L 20 18.7 93 52-162
1,1,2,2-Tetrachioroethane uglL 20 20.4 102 46-157
Rosuft prpae. an tents paps as in the units hcOMW by the "Un ' eorumn axupt rArsrr an sttatab umtt is prsfa I to tens riper of ter revAL
REPORT OF LABORATORY ANALYSIS
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Date: 05/31/2017 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 40

Ceft1 jl [!i{ al
WWW..pecelatrscom
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
Pace Anatydcal Services, LLC
205 East Meadow Road - Suite A'
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE:
2006657
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
1,1,2-Trichloroethane
uglL
20
19.7
99
52-150
1,1-Dichloroethane
uglL
20
18.8
94
59-155
1,1-Dichloroethene
uglL
20
19.5
98
1-234
1,2-Dichlorobenzene
uglL
20
19.5
97
18-190
1,2-Dichloroethane
uglL
20
19.2
96
49-155
1,2-Dichloropropane
uglL
20
19.9
99
1-210
1,3-Dichlorobenzene
uglL
20
20.1
100
59-156
1,4-Dichlorobenzene
ugfL
20
19.9
100
18-190
Benzene
uglL
20
20.3
102
37-151
Bromodichloromethane
uglL
20
20.2
101
35-155
Bromoform
ug1L
20
19.5
97
45-169
Bromomethane
uglL
20
15.7
78
1-242
Carbon tetrachloride
ug1L
20
20.0
100
70-140
Chlorobenzene
uglL
20
20.0
100
37-160
Chloroethane
uglL
20
17.6
88
14-230
Chloroform
uglL
20
19.6
98
51-138
Chloromethane
uglL
20
17.1
86
1-273
cis-1,2-Dichloroethene
ug/L
20
19.3
97
68-146
cis-1,3-Dichlompropene
uglL
20
21.1
106
1-227
Dibromochloromethane
uglL
20
22.0
110
53-149
Ethylbenzene
uglL
20
19.5
97
37-162
Methylene Chloride
uglL
20
17.6
88
1-221
Tetrachloroethene
uglL
20
19.2
96
64-148
Toluene
u91L
20
19.3
97
47-150
trans-1,2-Dichloroethene
uglL
20
19.6
98
54-156
trans- 1, 3-Dichloropropene
uglL
20
20.7
103
17-183
Trichloroethene
uglL
20
19.4
97
71-157
Trictilorofluoromethane
uglL
20
19.7
98
17-181
Vinyl chloride
uglL
20
17-4
87
1-251
1,2-Dichloroethane-c!4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
99
70-130
MATRIX SPIKE SAMPLE:
2006659
92341420003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits
1,1,1-Trichloroethane
uglL
NO
20
21.3
107
46-171
1,1,22-Tetrachloroethane
uglL
NO
20
21.0
105
73-159
1.1,2-Trichloroethane
ug1L
ND
20
20.8
104
64-152
1,1-Dichloroethane
uglL
NO
20
20.6
103
43-172
1,1-Dichloroethene
uglL
NO
20
22.5
113
48-189
1,2-Dichlorobenzene
uglL
NO
20
21.8
109
54-154
1,2-Dichloroethane
ug/L
NO
20
20.5
103
42-171
1,2-Dichloropropane
uglL
NO
20
21.8
109
55-157
1,3-Dichlorobenzene
uglL
ND
20
22.4
112
57-148
Resuft t0 on mft page am In Ow wrib wKftstee by thr'Lk%W oDimm esaept vA me a, ananaW writ Ia pream . to the riprri or the nnudt
REPORT OF LABORATORY ANALYSIS
Qualifiers
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Date: 05/31/2017 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 40

ceAnalytkal
wwwipacakbLcom
QUALITY CONTROL DATA
Pane Analytical Services, LLC
205 East Meadow Road - Suite A -
Eden, NC 27288
[phone]
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
MATRIX SPIKE SAMPLE:
2006659
92341420003
Spike
MS
M5
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
NO
20
22.2
111
58-149
Benzene
ug/L
NO
20
21.7
109
54-163
Bromodichloromethane
ug/L
NO
20
21.9
110
56-152
Bromoform
ug(L
NO
20
21.6
108
53-151
Bromomethane
ug/L
NO
20
17.8
89
10-200
Carbon tetrachloride
ug(L
NO
20
22.3
111
41-175
Chlorobenzene
ug/L
NO
20
21.8
109
67-152
Chloroethane
ug/L
NO
20
20.1
101
23-200
Chloroform
uglL
ND
20
20.9
104
51-166
Chloromethane
ug/L
NO
20
20.3
101
40-175
cis-1,2-Dichloroethene
ug/L
NO
20
21.0
105
45-174
cis-1,3-Dichlaropropene
ug1L
NO
20
22.4
112
38-146
Dibromochloromethane
ug/L
NO
20
23.2
116
65-144
Ethylbenzene
ug/L
NO
20
22.0
110
57-152
Methylene Chloride
ug/L
NO
20
18.0
84
40-167
Tetrachloroethene
ug/L
ND
20
21.9
109
59-155
Toluene
ug/L
NO
20
21.6
108
47-162
trans-1,2-Dichloroethene
ug/L
NO
20
21A
110
47-178
trans-1,3-Dichloropropene
ug/L
NO
20
22.0
110
39-148
Trichloroethene
ug/L
NO
20
22.6
113
60-153
Trichlorofluoromethane
ug/L
NO
20
21.7
108
42-199
Vinyl chloride
ug/L
NO
20
19.8
99
46-176
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bmmofluorobenzene (S)
%
96
70-130
Toluene-d8 (S)
%
98
70-130
SAMPLE DUPLICATE: 2006658
Parameter
Units
92341420002
Result
Dup
Resutf RPD Qualifiers
1,1,1-Trichlorcethane
ug/L
NO
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
NO
1,1,2-Trichloroethane
ug/L
NO
NO
1,1-Dichloroethane
ug/L
NO
NO
1,i-Dichloroethene
ug/L
NO
NO
1,2-Dichlorobenzene
ug/L
NO
NO
1,2-Dichloroethane
ug/L
NO
NO
1,2-Dichloropropane
ug/L
NO
NO
1,3-Dichlorobenzene
ug/L
ND
NO
1,4-Dichiorobenzene
ug/L
NO
NO
Benzene
ug/L
NO
NO
Bromodichloromethane
ug/L
NO
NO
Bromoform
ug/L
NO
NO
Bromomethane
ug/L
NO
NO
Carbon tetrachloride
ug/L
NO
NO
Chlorobenzene
ug/L
NO
NO
Raautta preaer 0 an tlda page are M en untta hrdhsnd try the-Urdrs" whom tswpt ntnn " 2amm a wW Is preaen- to On rWd of the reardl
REPORT OF LABORATORY ANALYSIS
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Date: 05/31/2017 05:04 PM vAdxxrt the written consent of Pace Analocal Services, LLC. Page 21 of 40

•
,ClekWcaf
(--!mrwmm
QUALITY CONTROL DATA
Project: 2017 JAN- JUNE SEMI ANNUAL
Pace Project No.: 92341420
SAMPLE DUPLICATE: 20W658
Parameter
Units
92341420002
Result
Dup
Result
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis- 1,3-Dichioropropene
ug/L
ND
ND
Dibromochloromethane
ug1L
ND
ND
Ethylbenzene
ug/L
ND
ND
Methylene Chloride
ug[L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug(L
AND
ND
trans-1.3-Dichloropropene
ug1L
ND
ND
TriChloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
90
91
4-Bromofluorobenzene (S)
%
104
103
Toluene-d8 (S)
%
110
104
RPD Qualifiers
1
0
5
Pace Analytical Services, LLC
205 East Meador Road - State A•
Eden, NC 272W
[phone]
Resuft p on this pate sn in On units irrdioand by the -UNq- acturrw a WhWe ■rr Atrnate rout is presented to the right of the resuiL
REPORT OF LABORATORY ANALYSIS
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Date: 05/31/2017 05:04 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 40

ceMajoml
Wffrpeoebb&00m
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMIANNUAL
Pace Project No.: 92341420
QC Batch: 361807 Analysis Method: EPA608
OC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB
Associated Lab Samples: 92341420001, 92341420002, 92341420003
METHOD BLANK: 2006521 Matrix: Water
Associated Lab Samples: 92341420001, 92341420002, 92341420003
Blank Reporting
Parameter Units Result Limit
Analyzed
4,4'-DDD
ug/L
NO
0.050
0512511714:34
4,4'-DDE
ug/L
ND
0.050
05125/1714:34
4,4'-DDT
ug/L
NO
0.050
05125/171434
Aldrin
ug/L
NO
0.050
05125/1714:34
alpha-BHC
ug/L
ND
0.050
05/2511714:34
beta-BHC
ugfL
ND
0.050
05/2511714:34
Chlordane (Technical)
ug/L
ND
0.50
05/25/17 14:34
detta-BHC
ug1L
ND
0.050
05/2511714:34
Dieldrin
ug/L
ND
0.050
05/25/17 14:34
Endosulfan I
ug/L
NO
0.050
05/25/17 14:34
Endosutfan II
ug/L
NO
0.050
05/25/17 14:34
Endosulfan sulfate
ug/L
ND
0.050
05/25117 14:34
Endrin
ug/L
NO
0.050
05125/1714:34
Endrin aldehyde
ug/L
NO
0.050
05/25/17 14:34
gamma-BHC (Lindane)
ug/L
NO
0.050
05/25/17 14:34
Heptachlor
ug/L
NO
0.050
05/25/17 14:34
Heptachlor epoxide
ug/L
NO
0.050
05/25/17 14:34
PCB-1016 (Aroclor 1016)
ug/L
ND
0.50
05/25117 14:34
PCB-1221 (Aroclor 1221)
ug/L
NO
0.50
05/25/17 14:34
PCB-1232 (Aroclor 1232)
ug/L
ND
0.50
05/25/17 14:34
PCB-1242 (Aroclor 1242)
ug1L
NO
0.50
05/25/17 14:34
PCB-1248 (Aroclor 1248)
ug/L
ND
0.50
05/25/17 14:34
PCB-1254 (Aroclor 1254)
ug/L
ND
0.50
05/25/17 14:34
PCB-1260 (Aroclor 1260)
ug/L
ND
0.50
05/25/17 14:34
Toxaphene
ugfL
ND
0.50
05/2511714:34
Decachlorobiphenyl (S)
%
64
20-138
05/25/17 14:34
Tetiachloro-m-xylene (S)
%
91
20-110
05/25/17 14:34
Qualifiers
Pace Analytical Services, LLC
205 East Meadow Road - Suite A•
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE:
2006522
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
.25
0.26
104
31-141
4,4'-DDE
ug/L
.25
0.25
99
30-145
4,4'-DDT
ug/L
.25
0.26
107
25-160
Aldrin
ug/L
.25
0.23
91
42-122
alpha-BHC
ugfL
.25
0.24
98
37-134
beta-BHC
ug/L
.25
0.21
86
17-147
delta-BHC
ug/L
.25
0.26
106
19-140
Dieldrin
ug/L
.25
0,25
100
36-146
Endosulfan I
ug/L
.25
0.26
104
45-153
Rou tta p on ttds papa an in tM enea rhdicated by the 'UrdW ooka m except whms m aRmntte uMis praamdad to the dgm orthe reaLa
REPORT OF LABORATORY ANALYSIS
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Date: 05/31/2017 05:04 PM wdmxA the written consent of Pace Analytical Services, LLC. Page 23 of 40

CeA ([local•
www.pacelabscam
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMIANNUAL
Pace Project No.: 92341420
LABORATORY CONTROL SAMPLE: 2006522
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Endosulfan II
ug/L
.25
0.26
106
1-202
Endosulfan sulfate
ug/L
.25
0.27
109
26-144
Endrin
ug/L
.25
0.26
104
30-147
Endrin aldehyde
ug/L
.25
0.22
91
50-150
gamma-BHC (Lindane)
ug/L
.25
0.25
100
32-127
Heptachlor
ug/L
.25
0.23
95
34-111
Heptachlor epoxide
ug/L
.25
0,25
102
41-126
Decachlombiphenyl (S)
%
79
20-138
Tetrachloro-m-xylene (S)
%
101
20-110
MATRIX SPIKE SAMPLE:
2006523
92341420002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
ND
.25
0.21
84
31-141
4,4'-DDE
ug/L
ND
.25
0.20
81
30-145
4,4'-DDT
ug/L
ND
.25
0.22
91
25-160
Aldrin
ug/L
ND
.25
0.17
70
42-122
alpha-BHC
ug/L
ND
.25
0.18
72
37-134
beta-BHC
ug/L
ND
.25
0.16
66
17-147
detta-BHC
ug/L
ND
.25
0.20
80
19-140
Dieldrin
ug/L
ND
.25
0.20
80
36-146
Endosulfan I
ug/L
NO
.25
0.21
84
45-153
Endosulfan II
ug/L
NO
.25
0.21
85
1-202
Endosulfan sulfate
ug/L
NO
.25
0.22
89
26-144
Endrin
ug/L
ND
.25
0.22
91
30-147
Endrin aldehyde
ug/L
ND
.25
0.19
77
50-150
gamma-BHC (Lindane)
ug/L
ND
.25
0.19
79
32-127
Heptachlor
ugtL
ND
.25
0,18
75
34-111
Heptachlor epoxide
ug/L
ND
.25
0.20
79
41-126
Decachlombiphenyl (S)
%
35
20-138
Tetrachloro-m-xylerte (S)
%
78
20.110
SAMPLE DUPLICATE: 2006524
92341420003 Dup
Parameter
Units
Result
Result RPD Qualifiers
4,4'-DDD
ug/L
NO
ND
4,4'-DDE
ug/L
ND
ND
4,4'-DDT
ug/L
NO
ND
Aldrin
ug/L
ND
ND
alpha-BHC
ug/L
ND
ND
beta-BHC
ug/L
ND
ND
Chlordane (Technical)
ug1L
ND
ND
delta-BHC
u911-
ND
ND
Dieldrin
ug1L
ND
ND
Raerdte presufted an tide pap. are In dw urdte Infested by the -tkftC aotr, be 1 5, VAWS an aIEwnate silt Is p ar. to tiw e4 ft M the nwdL
REPORT OF LABORATORY ANALYSIS
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Date: 05/31/2017 05:04 PM without the written Consent of Pace Analytical Services, LLC. Page 24 of 40

CeAnalyfica!
www.pacda4smm
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
SAMPLE DUPLICATE: 2006524
Parameter
Units
92341420003
Result
Dup
Result
Endosulfan I
ug1L
NO
NO
Endosutfan 11
ug/L
NO
NO
Endosulfan sulfate
ug1L
NO
NO
Endrin
ugfL
NO
NO
Endrin aldehyde
ug1L
NO
NO
gamma-BHC (Lindane)
ug[L
NO
NO
Heptachlor
ug1L
NO
NO
Heptachlor epoxide
ug1L
NO
NO
PCB-1016 (Aroctor 1016)
ug1L
NO
NO
PCB-1221 (Arocior 1221)
ugLfL
ND
NO
PCB-1232 (Aroclor 1232)
ug1L
NO
NO
PCB-1242 (Aroclor 1242)
ug1L
NO
NO
PCB-1248 (Arodor 1248)
ug1L
NO
ND
PCB-1254 (Aroclor 1254)
ug1L
NO
NO
PCB-1260 (Aroclor 1260)
ug1L
NO
NO
Toxaphene
ug1L
NO
NO
RPD Qualifiers
Pace Anafytical Services, LLC
205 East Meadow Road - Suite A-
Eden, NC 27288
[phone]
Resift P I on this pope am in the unfts indtos ed M the "onus- w haiw swap! Wvm an a-- - unit is Wmwdsd to tM d9M or the mod!
REPORT OF LABORATORY ANALYSIS
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Date: 05/31/2017 05:04 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 40

Pace Analytical Services, LLC
e
205 East Meadow Road - Suite Ar
Eden, NC 27288
(336)62"921
QUALITY CONTROL DATA
JAN-JUNE SEMI ANNUAL
420
377
Analysis Method:
EPA625
625
Analysis Description:
625 MSS
92341420001,92341420002,92341420003.
2
Matrix: Water
92341420001,92341420002,92341420003
Blank Reporting
Units
Result Limit
Analyzed
Qualifiers
ug/L
NO
5.0
05/3011710:21
e)
ug/L
NO
5.0
05/30/17 10:21
ug1L
NO
10.0
0&3011710:21
ug/L
NO
5.0
05/3011710:21
ug/L
NO
10.0
O5/30/1710:21
ug/L
NO
50.0
05130/1710:21
ug/L
NO
5.0
0513011710:21
ug/L
NO
5.0
0513011710:21
ug/L
NO
5.0
0513011710:21
ug/L
NO
5.0
0513011710:21
ug/L
NO
5.0
0513011710:21
ug/L
NO
25.0
0513(W1710:21
I
ug/L
NO
20.0
0513011710:21
r
ug/L
NO
5.0
05130/1710:21
ug/L
NO
5.0
05/3011710:21
r
ug/L
NO
5.0
05130/1710:21
ug/L
NO
50.0
OW30/1710:21
ug/L
NO
5.0
0513011710:21
ug/L
NO
5.0
05/30/1710:21
ug/L
NO
5.0
05/30/1710:21
ug/L
ND
5.0
05130/1710:21
u91L
ND
5.0
05/30/1710:21
ug1L
NO
5.0
05130/1710:21
ug1L
NO
5.0
05130/1710:21
ug/L
NO
5.0
05130/1710:21
ceAnalyhcal
www Carr
Project: 2017
Pace Project No.: 92341
QC Batch: 362
QC Batch Method: EPA
Associated Lab Samples:
METHOD BLANK: 200936
Associated Lab Samples:
Parameter
1,2,4-Trichlorobenzene
-0xry 2,2'bis(1-chloropropan
2,4,6-Trichiorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Nitrophenol
3,3'-Dichloroberaidine
4,6-Dinitro-2-methylpheno
4-Bromophenylphenyl ethe
4-Chlom-3-methylphenol
4-Chlorophenylphenyl ethe
4-Nitrophenol
Acenaphthene
Acenaphthy[ene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g, h,i )perylene
Senzo(k)fluoranthene
bis(2-Chloroethoxy)metha
bis(2-Chloroethyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h )anthracene
Diethylphthalale
Dimethyfphthalate
Fluoranthene
Ffuorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
t� preemnI d on eds papw an In the units hid by d w'Ihdb' *edam %*Wm an altwrnatw writ Is F . to the r� of the MOWL
Date: 05/31/2017 05:04 PM
n
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
wahatt the written consent of Pace Analytical Services. U.C.
Page 28 of 40

CeAna00/
arrw.paoaiabs.00m
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMIANNUAL
Pace Project No.: 92341420
METHOD BLANK: 2009362 Matrix:
Associated Lab Samples: 92341420001, 92341420002, 92341420003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
05130/1710:21
Isophorone
ug/L
ND
10.0
0513011710:21
N-Nitraso-di-n-propylamine
uglL
ND
5.0
05/3W1710:21
N-Nitrosodimethylamine
ug/L
ND
5.0
05130/1710:21
N-Nitrosodiphenylamine
ug/L
ND
10.0
05/30/17 10:21
Naphthalene
ug/L
ND
5.0
05/30/17 10:21
Nitrobenzene
ug/L
ND
5.0
05/30/1710:21
Pentachlorophenol
ug/L
NO
10.0
05/3011710:21
Phenanthrene
ug/L
ND
5.0
0513011710:21
Phenol
ug/L
ND
5.0
05130/17 110:21
Pyrene
ug/L
NO
5.0
05/30/17 10:21
2,4,6-Tribromophenol (S)
%
83
10-137
05/30/17 10:21
2-Fluorobiphenyl (S)
%
73
15-120
05/30/17 10:21
2-Fluorophenal (S)
%
41
10-120
05/30117 10:21
Nitrobenzene-65 (S)
%
69
10-120
05/30/17 10:21
Phenol-d6 (S)
%
26
10-120
05/30/17 10:21
Terphenyl-d14 (S)
%
112
11-131
05/30/17 10:21
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
20M363
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
28.6
57
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
41.3
83
36-166
2,4,6-Trichlorophenol
ug/L
50
46.6
93
37-144
2,4-Dichlorophenol
ug/L
50
41.5
83
1-191
2,4-Dimethylphenol
ug/L
50
40.8
62
32-119
2,4-Dinitrophenol
ug/L
250
190
76
1-181
2,4-Dinitrotoluene
ug/L
50
43.3
87
39-139
2,6-Dinitrotoluene
ug/L
50
43.3
87
50-158
2-Chloronaphthalene
ug/L
50
37.5
75
60-119
2-Chlorophenol
ug/L
50
39.2
78
23-134
2-Nitrophenol
ug/L
50
39.6
79
29-182
3,3'-Dichlorobenzidine
ug/L
100
80.3
80
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
76.3
76
1-181
4-Bromophenylphenyl ether
ug1L
50
40.5
81
53-127
4-Chloro-3-methylphenol
ug(L
100
81.2
81
22-147
4-Chlorophenylphenyl ether
ugfL
50
42.2
84
25-158
4-Nitrophenol
ug/L
250
83A
33
1-132
Acenaphthene
ug/L
50
42.0
84
47-145
Acenaphthylene
ug/L
50
40.9
82
33-145
Anthracene
ug/L
50
40.0
80
1-166
Benzo(a)anthracene
ug/L
5o
38.3
77
33-143
Benzo(a)pyrene
ug/L
5o
37.6
75
17-163
Benzo(b)fluoranthene
ug/L
50
37.9
76
24-159
Pace Ana"cal Services, LLC
205 East Meadow Road - Suite A'
Eden, NC 27288
[phone]
Qualifiers
Mauft praprr- on etch papa m in tha unit irtdkmted by dw -ukft!* eekrrrm W me an aJlsrrr-0 vrde is prsasrrbd tv e w r4ft of do resrdt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2017 05:04 PM without the wrttten consent of Pace Analytical Services, LLC. Page 27 of 40

ceArIa cal
trr w.PWGbbscom
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Proiect No.: 92341420
LABORATORY CONTROL SAMPLE: 20D9363
Pace Analytical Services, LLC
205 East Meadow Road - Suite X
Eden, NC 27288
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits
Qualifiers
Benzo(g,h,i)perylene
ug/L
50
41.0
82
1-219
Benzo(k)fluoranthene
uglL
50
37.6
75
11-162
bis(2-Chtoroethoxy)methane
ugfL
50
39.3
79
33-184
bis(2-Chloroethyl) ether
ug/L
50
42.6
85
12-158
bis(2-Ethythexyl)phthalate
ugfL
50
47.5
95
B-158
Butylbenzylphthalate
ugfL
50
46.8
94
1-152
Chrysene
ug/L
50
38.8
78
17-168
Di-n-butylphthalate
ug/L
50
43.4
87
1-118
Di-n-0ctylphthalate
ug/L
50
48.8
98
4-146
Dibenz(a,h)anthracene
ug/L
50
37.4
75
1-227
Diethylphthalate
ug/L
50
45.0
90
1-114
Dimethylphthalate
ug/L
50
45.0
90
1-112
Fluoranthene
ug/L
50
38.7
77
26-137
Fluorene
ug/L
50
42.8
86
59-121
Hexachloro-1,3-butadiene
ugfL
50
23.0
46
24-116
Hexachlorobenzene
ug[L
50
38.7
77
1-152
Hexachlorocyclopentadiene
ug/L
50
24.3
49
25-150
Hexachloroethane
ug/L
50
24.1
48
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
40.1
80
1-171
Isophorone
ugfL
50
39.0
78
21-196
N-Nitroso-di-n-propylamine
uglL
50
42.6
85
1-230
N-Nitrosodimethylamine
ugfL
50
28.6
57
25-150
N-Nitrosodiphenylamine
ug/L
50
40.6
81
25-150
Naphthalene
ug/L
50
34.1
68
21-133
Nitrobenzene
ug/L
50
36.2
72
35-180
Pentachlorophenol
ug/L
100
77.7
78
14-176
Phenanthrene
uglL
50
39.4
79
54-120
Phenol
ugfL
50
19.8
40
5-112
Pyrene
ug/L
50
42.8
86
52-115
2,4,6-Tribromophenol (S)
%
87
10-137
2-Fluombiphenyt (S)
%
86
15-120
2-Fluorophenol (S)
%
49
10-120
Nitrobenzene-d5 (S)
%
78
10-120
Phenol-d6 (S)
%
33
10-120
Terphenyl-dl4 (S)
%
99
11-131
MATRIX SPIKE SAMPLE:
2009364
92341420001
Spike
MS
MS
% Rec
Parameter
Units
Result
Cane.
Result
% Re,
Limits Qualifiers
1,24-Trichlorobertzene
ug/L
NO
50
24.6
50
44-142
2,2'-Oxybis(1-chloropropane)
ugfL
NO
50
31.9
64
36-166
2,4,6 Trichlorophenol
ugfL
NO
50
38.0
76
37-144
2,4-Dichlorophenol
ug/L
NO
50
33.0
66
1-191
2,4-Dimethylphenol
ugfL
ND
50
30.2
60
32-119
2,4-Dinitrophenol
ug/L
NO
250
69.8
28
1-181
Rm" prvndsd on this peps srs in etc units Irked by the -unit- ootuosr exceo rdrere an zownrts unit is prsssrrled to the rlpM of ttn rssrdt
REPORT OF LABORATORY ANALYSIS
This report shag not be reproduced, except in full,
Date: 05/31/2017 05:04 PM without the written consent of Pace Analytical Services. LLC. Page 28 of 40

to
ceAna"cal
WWW pocaubs.coM
Project: 2017 JAN-JUNF SEMIANNUAL
Pace Project No.: 92341420
MATRIX SPIKE SAMPLE: 2009364
Parameter
Units
2,4-Dinitrotoluene
ug/L
2,6-Dinitrotoluene
ug/L
2-Chloronaphthalene
ug/L
2-Chlorophenol
ug/L
2-Nitrophenol
ug/L
3,3'-Dichlorobenzidine
ug/L
4,6-Dinitro-2-methylphenol
ug/L
4-Bromophenyiphenyl ether
ug/L
4-Chloro-3-methylphenol
ug/L
4-Chlorophenylphenyl ether
ug/L
4-Nitrophenot
ug/L
Acenaphthene
uglL
Acenaphthytene
ug/L
Anthracene
ug/L
Benzo(a)anthracene
ug/L
Benzo(a)pyrene
ug/L
Benzo(b)fluoranthene
ug/L
Benzo(g,h,i)perylene
ug/L
Benzo(k)fluoranthene
ug/L
bis(2-Chloroethoxy)methane
ug/L
bis(2-Chloroethyl) ether
ug/L
bis(2-Ethythexyl)phthatate
ug/L
Butyibenzylphthalate
ug/L
Chrysene
ug/L
Di-n-butylphthalale
ug/L
Di-n-actylphthalate
ug/L
Dibenz(a,h)anthracene
ug/L
Diethyiphlhalate
ug/L
Dimethytphthalate
ug/L
Fluoranthene
ug/L
Fluorene
ug/L
Hexachloro-1 ,3-butadiene
ug/L
Hexachlorobenzene
ug/L
Hexachlorocyclopentadiene
ug/L
Hexachloroethane
ug/L
Indeno(1,2,3-cd)pyrene
u9/L
Isophoro ne
ug/L
N-Nitroso-di n-propytamine
uglL
N-Nitrosodimethylamine
ug/L
N-Nitrosodiphenylamine
ug/L
Naphthalene
ug/L
Nitrobenzene
ug/L
Pentachlorophenol
ug/L
Phenanthrene
ug/L
Phenol
ug/L
Pyrene
ug/L
2,4,6-Tribromophenol (S)
%
QUALITY CONTROL DATA
9234142000i Spike
Result Conc.
NO
ND
NO
NO
ND
NO
NO
ND
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
ND
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
50
50
50
50
50
100
100
50
100
50
250
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
50
50
MS
Result
37.1
36.6
31.5
30.8
26.7
61.2
34.1
35.8
68.4
37.7
72.8
36.4
34.7
35.4
34.5
33.4
33.4
34.4
33.5
31.4
33.3
41.9
41.2
34.9
38.6
44.5
34.9
40.4
39.9
36.0
38.5
19.6
34.3
14.4
19.1
35.1
29.8
33A
21.8
36.3
28.3
28.6
67.5
35.7
12.9
36.5
Pace Analytical Services, L LC
205 East Meadow Road - Suite A'
Eden, NC 2728E
[phone]
MS
% Rec
% Rec
Limits Qualifiers
74
39-139
73
50-158
63
60-118
62
23-134
53
29-182
59
1-262
34
1-181
72
53-127
68
22-147
75
25-158
29
1-132
73
47-145
69
33-145
71
1-166
64
33-143
63
17-163
63
24-159
69
1-219
63
11-162
63
33-184
67
12-158
78
8-158
78
1-152
65
17-168
77
1-118
83
4-146
70
1-227
81
1-114
80
1-112
72
26-137
77
59-121
39
24-116
69
1-152
29
25-150
38
40-113 Mt
70
1-171
60
21-196
67
1-230
44
25-150
73
25-150
57
21-133
57
35-180
67
14-176
71
54-120
26
5-112
73
52-115
76
10-137
t1Nrlte preeeerte I on ads pays we in nr -nift indieated by On "urns" a Wu a:wpt od me sn sEarra. ure is preewded to the riod of the resat
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2017 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 40

ceAnapeal e
wtrw.peae�nom
QUALITY CONTROL DATA
Pace Analytical Services, L.LC .
205 East Meadow Road - Suite Pi
Eden, NC 27288
[phone]
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
MATRIX SPIKE SAMPLE: 2009364
92341420001 Spike MS
MS
% Rec
Parameter Units Result Conc. Result
% Rec
Limits Qualifiers
2-Fluorobiphenyl (S) %
66
15-120
2-Fluorophenol (S) %
34
10-120
Nitrobenzene-d5 (S) %
62
10-120
Phenol-d6 (S) %
23
10-120
Terphenyt-d14 (S) %
76
11-131
SAMPLE DUPLICATE: 2009365
92341935001
Dup
Parameter
Units
Result
Result RPD Qualifiers
1,2,4-Trichlorobenzene
ug1L
NO
NO
2,2'-Ozybis(I-chloropropane)
uglL
NO
ND
2,4,6-Trichlorophenol
ug1L
ND
ND
2,4-Dichlorophenol
uglL
ND
NO
2,4-Dimethylphenol
uglL
ND
3.1J
2,4-Dinitrophenal
ug/L
ND
NO
2,4-Dinitrotoluene
uglL
ND
NO
2,6-Dinitrotoluene
uglL
ND
NO
2-Chloronaphthalene
uglL
NO
NO
2-Chlorophenol
uglL
NO
NO
2-Nitrophenol
uglL
NO
NO
3,3'-Dichlorobenzidine
uglL
NO
ND
4,5-Dinibm-2-methylphenol
uglL
NO
ND
4-Bromophenylphenyl ether
uglL
NO
ND
4-Chloro-3-methylphenol
uglL
NO
ND
4-Chlorophenylphenyt ether
ug1L
NO
NO
4-Nitrophenol
uglL
ND
NO
Acenaphthene
uglL
ND
ND
Acenaphthytene
UglL
ND
NO
Anthracene
uglL
ND
NO
Benzo(a)anthracene
UgIL
NO
1.1J
Benzo(a)pyrene
ug1L
NO
II AJ
Benzo(b)ffuoranthene
uglL
ND
1.51
Benzo(g,h,i)perytene
uglL
NO
ND
Benzo(k)fluoranthene
uglL
ND
1.1J
bis(2-Chloroethoxy)mefhane
uglL
ND
NO
bis(2-Chloroethyl) ether
uglL
ND
NO
bis(2-Ethylhexyl)phthalate
uglL
9.3
5.6 50 D6
Butylbenzylphthatate
ug(L
NO
NO
Chrysene
u91L
ND
1.1i
Di-n-butylphthalate
uglL
ND
NO
Di-n-octylphthalate
uglL
NO
NO
Dibenz(a,h)anthracene
uglL
NO
NO
Diethylphthalate
uglL
NO
NO
Dimethylphthalate
uglL
ND
ND
Fluoranthene
uglL
ND
2J
pnpanhd on this papa an in ttw -a** inmeatad by the -UrtW salaam exwp! whwe an attarrraea w* is I itatmrWaafffam"K
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05131 /2017 05:04 PM without the written consent of Pace Analytical Services, LLC.
Page 30 of 40

CeAnaocal e
aw�vpecelatrs.00m
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
SAMPLE DUPLICATE: 2009365
Parameter
Units
92341935001
Result
Dup
Result
Fluorene
ugfL
ND
ND
Hexachloro-1,3-butadiene
ugfL
ND
ND
Hexachlorobenzene
ugfL
ND
ND
Hexachlorocyclopentadiene
ug1L
ND
ND
Hexachloroethane
ug/L
ND
ND
lndeno(1,2,3-cd)pyrene
ugfL
ND
1J
lsophorone
ug/L
ND
ND
N-Nitroso-di-n-propylamine
ug[L
NO
ND
N-Nitrosodimethylamine
ug1L
ND
ND
N-Nitrosodiphenylamine
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
Nitrobenzene
ug/L
ND
ND
Pentachlorophenol
ug/L
ND
ND
Phenanthrene
ugfL
ND
ND
Phenol
ug/L
ND
ND
Pyrene
ug1L
ND
1.51
2,4,6-Tribromophenol (S)
%
68
89
2-Fluorobiphenyl (S)
%
44
65
2-Fluorophenol (S)
%
19
32
Nitrobenzene-d5 (S)
%
35
52
Phenol-d6 (S)
%
12
18
Tefphenyl-dl4 (S)
%
63
55
RPD Qualifiers
27
40
51
39
42
14
Pace Ana"cat Services, t.LC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
iftm r p.sd on nds paps an In the wdta bidimatod by the 'Urdu' whmm dwe an athnsa. wdt is prmwftd to the riyrt of the rswh
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fi.dl,
Date: 05131120W 05:04 PM wittwut the written consent of Pace Analytical Services, LLC.
Page 31 of 40

Cemalool
iwrcFacateDsmm
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
QC Batch: 361660 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 25400 Total Suspended Solids
Associated Lab Samples: 92341420001, 92341420002, 92341420003
METHOD BLANK: 2005743 Matrix: Water
Associated Lab Samples: 92341420001, 92341420002, 92341420003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L NO 1.0 05/23117 00:39
Pace Anatytical Services, LLC ,
205 East Meadow Road - Suite A
Eden, NC 2728E
[phone]
LABORATORY CONTROL SAMPLE: 2005744
Spike LCS LCS % Rex
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 242 97 90-110
SAMPLE DUPLICATE: 2005745
92341014001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg[L ND 3.4
Revift pry ee nut pav sn Ie tha radls ir,memd M tAe'Lkd ' eoirorrr wh t m attemata Lu* is presrrrbd to the rW* of an reerdt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31 /2017 05:04 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 40

CeAnalytical•
rrrnp�ahimm
QUALITY CONTROL DATA
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
QC Batch: 361866 Analysis Method: EPA 9040
QC Batch Method: EPA W40 Analysis Description: 9040 pH
Associated Lab Samples: 92341420001, 92341420002, 92341420003
SAMPLE DUPLICATE: 2006677
92340893001
Dup
Parameter
Units
Result
Result RPD Qualifiers
pH
Std_ Units
7.9
7.9 0 H6
SAMPLE DUPLICATE: 2006678
92341552002
Dup
Parameter
Units
Result
Result RPD Qualifiers
PH
Std. Units
7.8
7.8 1 H6
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Recant prosw0d on Was papa am in to un to huftW d by dw -UrdW ootu= a:owt Wwre an aldnrr - radt is ptiawibd to ttN r%td orUu raardL
REPORT OF LABORATORY ANALYSIS
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Date: M3112017 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 40

Pace Ar►atydcal Services, LLG
205 East Meadow Road - Suite A
I,C
Analytical • Eden, NC 27288
W!PDOM [phone]
QUALIFIERS
Project: 2017 JAN-JUNE SEMI ANNUAL
Pace Project No.: 92341420
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit,
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration_
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D).- Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable_
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chbroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NEtAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/31/2017 05:04 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 40

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inrw.pacafabs.Cam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: 2017 JAN-JUNE SEMIANNUAL
Pace Project No.: 92341420
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92341420001
OF #1
EPA 1664B
362361
92341420002
OF #2
EPA 1664E
362361
92341420003
OF #3
EPA 1664E
362361
92341420001
OF #1
EPA 3510
351807
92341420002
OF #2
EPA 3510
361807
92341420003
OF #3
EPA 3510
361807
92341420001
OF #1
EPA 200.7
362143
92341420002
OF #2
EPA 200.7
362143
92341420003
OF 93
EPA 2D0.7
302143
92341420001
OF 91
EPA 625
362377
92341420002
OF #2
EPA625
362377
92341420003
OF #3
EPA 625
362377
92341420001
OF #1
EPA 624
361854
92341420002
OF #2
EPA 624
361854
92341420003
OF #3
EPA 624
361854
92341420001
OF #1
SM 25400
361660
92341420002
OF #2
SM 2540D
361660
92341420003
OF #3
SM 2540D
361660
92341420001
OF #1
EPA 9040
361866
92341420002
OF #2
EPA 9040
361866
92341420003
OF #3
EPA 9040
381866
Date: 05/31/2017 05:04 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in W,
without the written consent of Pace Anafybral Services, LLC.
EPA 608
EPA 608
EPA 608
EPA 200.7
EPA 200.7
EPA 200.7
EPA 625
EPA 625
EPA 625
362272
362272
362272
362366
362366
362366
362667
362667
362667
Page 35 of 40

74ecal.
Condition Upon Recei SCURj Pa e 1 of 2
Document Na.' issuing Authority:
F-CAR43-033-Rev.01 Pace RuaiityOffice
Laboratory receiving samples-
Asheville ❑ Eden[:] Greenwood ❑ Huntersvillezi Raleigh❑ Mechanicsville[:]
.Receipt
... Client Name: WQ# : 9234142D
S C zAtlk project tl:
Courier: ❑Fed Ex ❑UPS ❑USPS 4CJient��'
❑ Commercial ❑Pace ❑Other 92341420 1 1
Custody Seal Present? []Yes A No Seals Intact? ❑Yes PIN
Date/Initials Person Examining Caatents:
Packing Material: ❑Bubble Wrap Bubble Bags []None [—]Other:
Thermometer IRGuniD: -nuc)?) Typelee: ❑Niue ❑Nana Owet A g process has begun
samples on Ice, cooling
�
Correction Factor: Cooler Temp Corrected ('Cj: �� _ _ _ Blalogical Tissue Frozen? []Yes ZNo []N/A
Temp should be above freezing to 6'C
USDA Regulated SoB (,] N/A, water sample)
Did samples yiginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (intemationaliy,
]Yes LAo including Hawall and Puerto Rico)? []Yes (moo
Chain of Custody Present?
Yes
No
❑N/A
1.
Samples Arrived within Hold Time?
Yes
ONG
❑N/A
2.
Short Hold Time Analysis <72 hr.)?
[]Yes
No
N/A
3.
Rush Turn Around Time Requested?
❑Yes
[dmo
[]N/A
4.
Sufficient Volume?
Yes
[]No
❑N/A
S.
Correct Containers Used?
,nYes
[]No
❑N/A
6.
Containers Intact?
Samples Feld filtered?
Sample labels Match COC?
-Includes Date/nme/ID/Analysis Matrix: P
Headspace in VOA Vials (>5-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Project Manager SCURF Review:
Project Manager SRF Review:
Oyes J3No N A S. Note if sediment li visible in the dissolved container
❑Yes J6No ❑N/A 9.
❑Yes [6No ❑N/A lui1.1 *0 's/z Z- (1+
❑Yes V!4o ❑N/A 11:IJt =�� zl�/ fitC+-OIN
Field Data Required? []Yes ❑No
Date/Time:
Date:
Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 36 of 40

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�. Semi-annual Stormwater L.har a Monitoring Report ..�
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted ZD 1
CERTIFICATE OF COVERAGE NO. NCG03k (Q
FACILITY NAME
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COUNTY Arc_ ,4_V1�jOVA_1
'3 PERSON COLLECTING SAMPLES 0 E. NIzroF,
LABORATORY rXe J0.6 5 Lab Cert. # 12
Comments on sample collection or analysis:
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SAMPLE COLLECTION YEAR 2 01
SAMPLE PERIOD ❑ Jan -June 0"July-Dec
or ❑ Monthly" (month)
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C RGING 70 CLASS ❑ORW ❑HQW ❑Trout ❑PNA
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CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
DWR SECTION
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1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving•water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes.. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11;.for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the T70 monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(Tf0), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
/C&,CA� PA& P-Oco'l
Title (Print title)
91
(Sig t re) . (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX meL" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Nate: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
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�. d '[4j� .: 5i'rY`+•t
r 4 ��
F'i'�i�} -tP1 o-dr:
t {_5
�µq�f��: i�`�
x `".
47
.,w," r
. , Outfall-No.. e' I
,
� Iry.. 1't . i
�' ��Collettedl'
"�%"Ilk
a amount, `.
;�. Nka w3� 9,
jFVon;;polar0$.G%TPM b�"
. ;. r.. .,,, ,
�����,�tM
�,, f,.
'v4', w�,
t' :Total Suspended
Inches r«t�:�
:ai�P,.A1664i(SGTRHEM1i
s.;'
s,
1'Samg/L� °:.'° "
M 1mg/L or 54Xmg/L* i
00
6 4L�".9 4 SU
I�Mm_.*l .1 »fti J-+3-..,.ti­.Ynr
Footnotes from Part A also apply to this Part B
t
* See General Permit text, Table 5, identifying the especially sensitive receiving water, classifications where the more protective benchmark applies.
Permit De '%1/1/2012-10/31/2017 SWU-245, last revised ' '25/2012
` Page 2 of 3

- Note: if k- report a sample value in excess of the benchmark, you must imi,.—Ijent Tier 1, Tier 1, or Tier 3 responses. See General Permit text. -)
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reporsllo:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
of Permittee)
Permit Date: 11/1/2012-10/31/2017
l
(Date)
SWU-245, last revised 10/25/2012
Page 3 of 3

Ili
WINVA
ANN 3R
Stormwater Discharge OutfalI (SDO)
Qualitative Monitoring Report
Forguidance on falling out this form, please visit httn:!/nortal.ncdenr.orgr/we Jw—g lwstsu Jnndessw#taL�-.4
Permit No.: �CJ�/3 QJP/�LO/ or -Certificate of Coverage No.:
Facility Name: —*9tL-4t;kwiIM1A= Ov/kkeSV t f I
county:
Inspector: -
Date of Inspection: e i
Time of Inspection: ! !r!ZD --
Total Event Precipitation (inches): C, tf a
Phone No. 7 0 Y - 37 't " 9G a 0
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Recis
es ❑ No� 1�1)
J4N � 8
201?
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the H—h wL AIL S
r 4 ry� P 9 c7 N
s Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event" However,
some permits do not have this requirement Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no 3
precipitation.
r ;
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office. I
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
of Permittee or Designee)
Page 1 of 2
SWU-242, Last modified 10/25/2012

1. Outfall Description: '
outfall No. -9�_ Structure (pipe, ditc , etc.) IPV
Receiving Stream: kC R5 ua
Describe the industrial activities that occur within th }outfall drainage area:
3 us 5, n T
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:1
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 4
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 42] 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1
2 3 4 5
h. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
a 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes d95?
8. Is there an oil sheen in the stormwater discharge? Yes dEl
9. Is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious Indicators of Stormwater Pollution:
List and describe tLdL 1==
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

OR 7,j
Nam.
AN X
WNW
Stormwater Discharge.0utfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: http[/Zgrtal.ncdenr.orE f web jwq jws jku nndessw#ta6-4
Permit No.: RXM�9-3191 o/o-�, or Certificate of Coverage No.: N/C/.G1V/ 310Ak1 11/
Facility Name: 5 u t 1
County: 4.,ti Phone No. _"740
Inspector: Lw 4e.
Date of Inspection: 4
Time of Inspection: / `Jr v —
Total Event Precipitation (inches): dO • 410•
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.) REcEN ED
Yes ❑ No SAS 1$ 201?
=r-rrRA1 FILES
Please verify whether Qualitative Monitoring must be performed n9 aep ie ntative storm
v ,
event" or "measureablestorm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm events or during a "measureable storm event" However,
some permits do not have this requirement Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
1
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
1 obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
of Permittee or Designee)
Page 1 of 2
SM-242, Last modified 10/25/2012

1. Outfall Description: ,
Outfall No. P— . Structure (pipe, ditch, etc.) _ p1d_
Receiving Stream: LM rlcwvk c01'� , -1d -L-, (IU C'fkLk
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, -medium, dark) as descriptors: _
3. Odor: Describe any distinct odors that the discharge may have (i.e:, smells strongly of oil,
weak chlorine odor, etc.): r7 crL&—
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 3 4 5
S. Floating Solids:. Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
® 2 3 4 5
5. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
0 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes Q
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes R
10. Other Obvious Indicators of Stormwater Pollution:
List and describe-� _
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, bast modified 10/25/2012

Ili
MDE
Stormwater Discharge Outfall (SDO).
Qualitative Monitoring Report
Forguidance on filling out this form, please visit. http:/./po.qal.ncde-nr.org/web/wq/wslsu/npdessw#tab-4
/npdessw#tab-4
Permit No.: N/C/b/12/
Facility Name: .SO (AJ
County: Ae?,OWA
Inspector:
Date of Inspection:
Time of Inspection:
O_/O/ 'or Certificate of Coverage No.:
Phone No. ZO q37 - Q OO
rim35
Total Event Precipitation (inches): a
Was this a "Representative Storm Event" or "Measureable.Storm Event" as defined by the permit?
fSee information below.)
�es ❑ No
RECEIVED
JAN 18 ZOi7
Please verify whether Qualitative Monitoring must be performed during a "presentctve sum
event"or'measureable storm event" (requirements vary, depending on the�'rrM-t}?ECTION
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
of Permittee or Designee)
Paget of 2
SWU-242, Wtmodified 10/25/2012

1. Outfall Description: 11
Outfall No. 3 Structure (pipe, ditch, etc.) ' w V -%tX
Receiving Stream: c
Describe the industrial activities that occur within t e outfalI drainage area:
S'i tne.e . �20�+1 � �dFiiNll.Zcl/rf id I/a�il f�[ vt
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: T,7 J{
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): -,I--e,
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 �p 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
® 2 3 • 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
LD 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes 0
B. Is there an oil sheen in the stormwater discharge? Yes 0
9. Is there evidence of erosion or deposition at the outfail? Yes
10. Other Obvious Indicators of Stormwater pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

lo
r JN M*ii ca
WWW4MC&Akh&G=
Pecs Arudyticai Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
December 09, 2016
John Moore
Southwire
12331 Commerce Station
Huntersville, NC 28078
RE: Project: 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Dear John Moore:
kC 6- o 30 6 6a��
RECEIVED
JAN 18 2017
CENTRAL FILES
DWR SECTION
Enclosed are the analytical results for sample(s) received by the laboratory on November 29, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
�57�
Taylor Ezell
[e-mail]
Project Manager
Endosures
REPORT OF LABORATORY ANALYSIS
This report Wmil not be reproduced, except in MD.
wdmxA the written consent of Pace Ana"caf Services. LLC.
Page 1 of 40

Pace Analytical Services, LLC
�4�1V Kl�fliC4! 205 East Meadow Rp�d - Suite A
Eden, NC 27'ZBB
w mpacglabscom (336 )623-8921
CERTIFICATIONS
Project: 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Charlotte Certification E179
9800 IGncey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Florida/NEt.AP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Virginia/VEIAP Certification #: 460221
Asheville Certification IN
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NCO30 Virginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduoed, except in full,
wdKKd the written consent of Pace Analytical Services, LLC. Page 2 of 40

MAna"cal
• f wwr!Pcom
Pace Anslybod Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE SUMMARY
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92321165001
OUTFALL 1
Water
11/29M614:10
11/29/1616:30
92321165002
OUTFALL 2
Water
11 /29/16 14:35
11/29/16 16:30
92321165003
OUTFALL 3
Water
11/29/16 14:45
11/29/16 16:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in fun,
without the written commm of Pace Arra"cal Services. LLC. Page 3 of 40

/�al
ceAr�alytical
wweaarelab&=n
Pace Analytical Services, LLC
205 East Meadow Rnyd - Suite A
Eden, NC 27238
(336)62341921
SAMPLE ANALYTE COUNT
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Analysts
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92321165001
OUTFALL 1
EPA 1664B
JM5
i
PASI-C
EPA608
SWB
27
PASI-C
EPA200.7
SH1
7
PASI-A
EPA 625
Bpi
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
MJS1
1
PASI-A
EPA 9040
ALC
1
PASI-A
92321165002
OUTFALL 2
EPA 1664E
JMS
1
PASI-C
EPA 608
SWB
27
PASI-C
EPA200.7
SH1
7
PASI-A
EPA 625
Bpi
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
MJS1
1
PASI-A
EPA 9040
ALC
1
PASI-A
92321165003
OUTFALL 3
EPA 1664E
JMS
1
PASI-C
EPA608
SWB
27
PASI-C
EPA 200.7
SH 1
7
PASI-A
EPA 625
BPJ
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
MJS1
1
PASI-A
EPA 9040
ALC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall riot he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 40

�+�7 Ana"cal"
Pace Analytical Services, LLC
A IU a 205 East Meadow Road - Sure A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Sample: OUTFALL 1 Lab 10: 92321165001 Collected: 11/29/16 14:10 Received: llrM1616:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
OF
Prepared
Analyzed
CAS No. Qua]
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO
mg1L
5.0
1.1
1
12/05/16 08:33
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation Method: EPA
3510
Aldrin
NO
ug/L
0.050
0.050
1
1210111613:51
12/08/1618:17
3094)0-2
alpha43HC
NO
ug1L
0.050
0.050
1
12/0111613:51
12/0811618:17
319-81-6
beta-BHC
ND
ug/L
0.050
0.050
1
1210111613:51
12/08/1618:17
3194&7
delta-BHC
NO
ug/L
0.050
0.050
1
12101/1613:51
12108/1618:17
319-86-8
gamma-BHC (Lindane)
NO
ug/L
0.050
0.050
1
12/0111613:51
12/08/16 18:17
58-89-9
Chlordane (Technical)
NO
ug1L
0.50
0.50
1
12/01/16 13:51
12/08/16 18:17
57-74-9
4X-DDD
NO
ug/L
0.050
0.050
1
12101h613:51
1210811618:17
72-54-8
4X-DDE
NO
ug/L
0.050
0.050
1
1210111613:51
12108/1618:17
72-55-9
4X-DDT
NO
ug1L
0.050
0.050
1
12101/1613:51
12108/1618:17
50-29-3
Dieldrin
NO
ug/L
0.050
0.050
1
12101/1613:51
12/0&1618:17
60-57-1
Endosuffan I
NO
ug1L
0.050
0.050
1
12/01/16 13:51
12/08/16 18:17
959-98-8
Endosulfan 11
NO
ug/L
0,050
0.050
1
12/01/16 13:51
12108/1618:17
33213-65-9-
Endosulfan sulfate
NO
ug1L
0.050
0.050
1
12101/16 13:51
121=16 1817
1031-07-8
Endrin
NO
ug1L
0.050
0.050
1
12101/1613:51
12108/1618:17
72-20-8
Endrin aldehyde
NO
uglL
0.050
0.050
1
12/01/16 13:51
12108/16 18:17
7421-934
Heptachlor
NO
ug/L
0.050
0.050
1
12/01/16 13:51
12108/1618:17
764"
Heptachlor epopde
NO
uglL
0.050
0.050
1
12/01/16 13:51
12/08/16 18:17
1024-57-3
PCB-1016 (Arodor 1016)
NO
ug1L
0.50
0.50
1
12/01/16 13:51
12/08/16 18:17
12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug/L
0.50
0.50
1
12101/1613:51
12/0811618:17
11104-28-2
PCB-1232 (Arodor 1232)
NO
ug1L
0.50
0.50
1
12/01/16 13:51
12/08/16 18:17
11141-16-5
PCB-1242 (Arodor 1242)
NO
U911-
0.50
0.50
1
12/01/16 13:51
12108/16 18:17
53469-21-9
PCB-1248 (Arodor 1248)
NO
ug/L
0.50
0.50
1
12/01/16 13:51
12 O8116 18:17
12672-29-6
PCB-1254 (Arodor 1254)
NO
ug/L
0.50
0,50
1
12/01/16 13:51
12108/16 18:17
11097-69-1
PCB-1260 (Arodor 1260)
NO
u91L
0.50
0.50
1
12/01/16 1151
12108/16 18:17
11096-82-5
Toxaphene
ND
ug1L
0.50
0.50
1
1210111613:51
12108/1618:17
8001-35-2
Surragafts
Tetrachbro-rn-xylene (S)
83
%
20-110
1
12/01/16 13:51
12/08/16 18:17
877-09-8
Decachlorobiphenyl (S)
38
%
20-138
1
12/01/16 13:51
12/08/16 18:17
2051-24-3
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND
mg/L
0.0010
0.00050
1
11/30/16 21:30
12/02/16 06:50
7440-43-9
Chromium
ND
mg1L
0.0050
0.0025
1
11/30/16 21:30
12/02/16 06:50
7440-47-3
Copper
NO
mg1L
0.0050
0.0025
1
111=16 21:30
12/02/16 06:50
7440-50-8
Lead
NO
mg/L
0.0050
0.0025
1
11/30/16 21:30
12/02116 06:50
7439-92-1
Nickel
NO
mg1L
0.0050
0.0025
1
11/30/16 21:30
12/02/16 06:50
7440-02-0
Sihrer
NO
mg1L
0.0050
0.0025
1
11/30/16 21:30
12/02/16 06:50
7440-22-4 '
Zinc
0.026
mg/L
0.010
0.0025
1
11/30/16 21:30
12/02/16 06:50
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method:
EPA
625
Aoenaphthene
NO
ug/L
5.0
0.25
1
11/29/1616:40
11/30/16 22:49
83-32-9
Acenaphthylene
NO
ug/L
5.0
0.21
1
11/29/1616:40
11/30/16 22:49
208-.96-8
Anthracene
NO
ug/L
5.0
0.14
1
11/29/1616:40
11/30/16 22:49
120-12-7
Benzo(a)anthracene
NO
ug/L
5.0
0.33
1
11/29/16 16:40
11/30/16 22:49
56-55-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/092016 03:39 PM without the written consent of Pace Analytical Services, L LC. Page 5 of 40

C6AllalX al �
wwwcam
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27298
[phone]
ANALYTICAL RESULTS
Project: 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Sample: OUTFALL 1 Lab ID: 92321165001 Collected: 11/29/16 14:10 Received: 11129/16 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Benzo(a)pyrene
ND
ug/L
5.0
0.30
1
11/29/16 16:40
11/30/16 22:49
50-32-8
Senzo(b)fluoranthene
ND
uglL
5.0
0.28
1
11/29/16 16:40
11/30/16 22:49
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
0.38
1
11/29/16 16:40
11/30/16 22:49
191-24-2
i anzo(icruoranthene
ND
ug/L
5:0
0:43---1-11/29/16.16:40--1'1f30/16�22:49-207-08-9
4-Bromophenylphenyi ether
-ND
ug/L
5A
0.82
1
11129/1616:40
11/30/16 22:49
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
0.79
1
11/29/16 16:40
11/30/16 22:49
85-68-7
4-Chloro-3-methy(phenol
ND
uglL
5.0
3.7
1
11/29/1616:40
11/30/16 22:49
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10"0
0.92
1
11/29/16 16:40
11/30/16 22:49
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1.0
1
11/29/16 16:40
11/30/16 22:49
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
0.98
1
11/29/16 16:40
11/30/16 22:49
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1.3
1
11/29/16 16:40
11/30/16 22:49
95-57-8
4-Chtorophenytphenyl ether
ND
uglL
5.0
0.87
1
11/29/16 16:40
11/30/16 22:49
7005-72-3
Chrysene
ND
u9/L
5.0
0.21
1
11/2911616:40
11/30/16 22:49
218-01-9
Dibenz(a,h)anthrecene
ND
uglL
5.0
0.55
1
11/29/16 16:40
11/30/16 22:49
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
2.1
1
11/29/16 16:40
11/30/16 22.49
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1.7
1
11/29/16 16:40
11/30/16 22:49
120-83-2
Diethylphthalate
ND
ug1L
5.0
0.58
1
11/29/16 16:40
11/30/16 22:49
84-06-2
2,4-Dimethylphenol
ND
uglL
10.0
1.2
1
11129/1616:40
11/30/16 22:49
105-67-9
Dimethylphthalate
ND
ug/L
5.0
0.76
1
11/29/16 16:40
11/30/16 22:49
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
0.75
1
11/29/16 16:40
11/30/16 22:49
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
2.6
1
11/29/16 16:40
11/30/16 22:49
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
9.0
1
11/29/16 16:40
11/30/16 22:49
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
0.90
1
11/2911616:40
11/30/16 22:49
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
0.98
1
11/29/16 16:40
11/30/16 22:49
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
0.66
1
11/29/16 16:40
11/30/16 22:49
1174M-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
0.79
1
11/29/16 16:40
11/30/16 22:49
117-81-7
Ftuoranthene
ND
ug/L
5.0
0.21
1
11/29/16 16:40
11/30/16 22:49
206-44-0
Fluorene
ND
ug/L
5.0
0.21
1
1112911616:40
11/30/16 22:49
86-73-7
Hexachloro-1,3-butadiene
ND
u9/1-
5.0
0.94
1
11/29/16 16:40
11/30/16 22:49
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
0.72
1
11/29/16 16:40
11/30/16 22:49
118-74-1
Hexachlorocydopentadiene
ND
ug/L
10.0
0,88
1
11129/16 16:40
11/30/16 22:49
77-47-4
Hexachloroethane
ND
ug/L
5.0
1.1
1
11/29/16 16:40
11/3011622:49
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
0.29
1
11/29/16 16:40
11/30/1622AQ
193-39-5
Isophorone
ND
ug/L
10.0
0.89
1
11/29/16 16:40
11/30/16 22:49
78-59-1
Naphthalene
ND
u91L
5.0
0.34
1
11/29/16 16:40
11/30/16 22:49
91-20-3
Nitrobenzene
ND
ug/L
5.0
1.1
1
11/29/16 16:40
11/30/16 22:49
98-95-3
2-Nitrophenol
ND
ug/L
5.0
0.91
1
11/29/1616:40
11/30/16 22:49
88-75-5
4-Nitrophenol
ND
ug/L
50.0
4.1
1
11/29/16 16:40
11130/16 22:49
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
0.91
1
11/29/16 16:40
11/30/16 22:49
62-75-9
N-Nitmso-di-n-propytamine
ND
ug/L
5.0
0.99
1
11/29/16 16:40
11/30/16 22:49
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1.0
1
11/29/16 16:40
11/30/16 22:49
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
0.95
1
11/29/16 16:40
11/30/16 22:49
108-60-1
Pentachlorophenol
ND
u911-
10.0
4.6
1
11/29/16 16:40
11/30/16 22:49
87486-5
Phenanthrene
ND
ug/L
5.0
0.22
1
11/29/16 16:40
11/30/16 22,49
85-01-8
Phenol
ND
ug/L
5.0
1.9
1
11/29/16 16:40
11/30/16 22:49
Pyrene
ND
ug1L
5.0
0.19
1
11/29/16 16:40
11/30/16 22:49
129-00-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in NO,
Date: 12/09/2016 03:39 PM without the written consent of Pace Anaytirai Services, LLC. Page 6 of 40

Pace Anatybmai Services, LLC
�+
2115 Fast Meadow Road - Suite A
ceAna cal Eden, NC 27288
e Nwwp s opm (336)623-W21
ANALYTICAL RESULTS
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Sample: OUTFALL i Lab 1D: 92321165001 Collected: 11/29/16 14:10 Received: 11/29/1616:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No_ Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
I.2,4-Trichlorobenzene
ND
ug/L
5.0
0.98
1
11/29/1616:40
11/30/16 22:49
120-82-1
2,4,6-Trichlorophenol
ND
uglL
10.0
1.3
1
11/29/1616:40
11/3011622:49
88-06-2
Surrogates
Nitrobenzene-d5 (S)
63
%
10-120
1
11IM1616:40
11/30/16 22:49
4165-60-0
2-Fluorobiphenyl (S)
77
%
15-120
1
11/2911616:40
11/3011622:49
321-60-8
Terphenyl-dl4 (S)
68
%
11-131
1
11/2911616:40
11/30/16 22:49
1718-51-0
Phenol-06 (S)
25
%
10-120
1'
11/29/1616:40
11/30/16 22:49
13127-88-3
2-Fluorophenol (S)
37
%
10-120
1
11/29/1616:40
11/30/16 22:49
367-124
2,4,6-Tribromophenol (S)
73
%
10-137
1
11/29/1616:40
11/30/16 22:49
118-79.6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND
ug/L
2.0
1.7
1
1210111618:58
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1.7
1
12101/1618:58
75-27-4
Bromoform
ND
u91L
2.0
1.5
1
12101/1618:58
75-25-2
Bromomethane
ND
ug/L
2.0
1.0
1
12101/1618:58
74433-9
Carbon tetrachloride
ND
u91L
2.0
1.9
1
12/01/16 18:58
W23-5
Chlorobenzene
ND
ug1L
2.0
1.7
1
12101/1618:58
108-90-7
Chloroethane
ND
ug/L
2.0
1.6
1
12101/1618:58
75-00-3
Chloroform
ND
ug/L
2.0
1.9
1
1210111618:58
67-66-3
Chloromethane
ND
ug/L
2.0
1.5
1
12/01/16 18:58
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1.8
1
1210111618:58
124-48-1
1,2-Didtlorobenzene
ND
u91L
2.0
1.5
1
1210111618:58
95-50-1
1,3-Dichlonobenzene
ND
u91L
2.0
1.5
1
12101/1618:58
541-73-1
1,4-0idtlorobenzene
ND
u91L
2.0
1.5
1
12101/1618:58
1064&7
1,1-Dichloroethane
ND
uglL
2.0
1.8
1
12/0111618:58
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1.8
1
12/0111618:58
107-06-2
1,1-Qichloroethene
ND
ug1L
2.0
1.9
1
12/0111618:58
75-35-4
ds-1,2-Dichloroethene
ND
u91L
2.0
1.8
1
12/01/16 18:58
156-59-2
trans-1,2-Dichbroethene
ND
u911-
2.0
1.8
1
12/01/16 18:58
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1.7
1
12/01/16 18:58
7M7-5
cis-1,3-Dichioropropene
ND
u91L
2.0
1.6
1
12101/1618:58
10061-01-5
trans-1,3-Dichloropropene
ND
u9/L
2.0
1.6
1
1210111618:58
10061-02-6
Ethylbenzene
ND
ug/L
2.0
1.6
1
12/01/1618:50
10041-4
Methylene Chloride
ND
ug1L
2.0
1.9
1
12101/16 18:58
75-09-2
1.1,2,2-Tetrachloroethane
ND
uglL
2.0
1.5
1
12/01/16 18:58
79-34-5
Tetrachloroethene
ND
ug/L
2.0
1.8
1
12101/1618:58
127-18-4
Toluene
ND
ug/L
2.0
1.6
1
12101/1618:58
108-88-3
1,1,1 Trichloroetttane
ND
ug/L
2.0
1.9
1
1210111618:58
71-55-6
1,1,2-Trichloroethane
ND
uglL
2.0
1.7
1
12/01/16 18:58
79-00-5
Trirhloroethene
ND
ug/L
2.0
1.8
1
12/01/16 18:58
79-01-6
Trichlorofluommethane
ND
ug/L
2.0
1.7
1
12101/1618:58
75-69-4
Vinyl chloride
ND
ug/L
2.0
1.5
1
12/01/16 18:58
75-014
Surrogates
4-Bromofluorobenzene (S)
104
%
70-130
1
12/01/16 18:58
4604004
Toluene-d8 (S)
107
%
70-130
1
12/01116 18:58
2037-26-5
1.2-Qichloroethane-04 (S)
97
%
70-130
1
12/01/16 18:58
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in fug.
Date: 12/09/2016 03:39 PM without the written consent of Pace Anafyticai Services. LLC. _ .__ ___ Page 7 of 40

Pace AnatyticcW Serriees, LLC
ceAnalytical'
r ww!pscahbs.cam
i
ANALYTICAL RESULTS
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
205 East Meadow Road - Suite A
Eden, NC 27268
[phone]
Sample: OUTFALL 1 Lab ID: 0232116MI Collected: 11MI16 14:10 Received: 11/29/16 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids
9040 pH
8-2 • mgA-
Analytical Method: EPA 9040
2.5 2.5 1
11/30/16 18:10
0fi 3:5-Std7Units 0:iO 0N0--i 1r30/16'12:03 Flo'
Sample: OUTFALL 2 Lab ID: 92321ISM02 Collected: 11/29/1614:35 Received: 11/29/1616:30 Matrix: Water
Report
Parameters Resutts Units Limit MDL DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
608 GCS Pesticides and PCBs
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Undane)
Chlordane (Technical)
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosuffanl
Endosulfen Il
Endosulfan suffate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
PCB-1016 (Arodor 1016)
PCB-1221 (Arodor 1221)
PCB-1232 (Arodor 1232)
PCB-1242 (Arodor 1242)
PCB-1248 (Arodor 1248)
PCB-1254 (Arodor 1254)
PCB-1260 (Arodor 1260)
Toxaphene
Sum gates
Tetrachbro-m-xylene (S)
Decachlorobiphenyl (S)
200.7 MET ICP
Cadmium
Analytical Method: EPA 1664E
NO mg/L 5.0 1.1 1 12/05/16 08:34
Analytical Method: EPA 608 Preparation Method: EPA 3510
NO
ug/L'
0.050
0.050
1
12/01/1613:51
1210811618:35
30940-2
NO
ug/L
0.050
0.050
1
12/01/1613:51
1210811618.35
319-84-6
ND
ug/L
0.050
0.050
1
1210111613:51
12/0811618:35
3194L5-7
ND
ug/L
0.050
0.050
1
12/01/1613:51
1210811618:35
319-86-8
NO
ug/L
0.050
0.050
1
12/01/1613:51
1210811618:35
58-89.9
NO
ug/L
0.50
0.50
1
12/01/1613:51
12108/1618:35
57-74-9
NO
ug/L
0.050
0.050
1
12/01/1613:51
12108/1618:35
72-54-8
NO
ug/L
0.050
0.050
1
1210111613:51
12/08/1618:35
72-55-9
NO
uglL
0.050
0.050
1
12101/1613:51
12/0811618:35
50-29-3
NO
ug/L
0.050
0.050
1
12/01/1613:51
1210811618:35
60-57-1
NO
u9/1-
0.050
0.050
1
12/01/1613:51
12108/1618:35
959-98-8
NO
ug/L
0.050
0.050
1
12/01/1613:51
12108/1618:35
33213-65-9
NO
uglL
0.050
0.050
1
1210111613:51
12108/1618:35
1031-07-8
NO
ug/L
0.050
0.050
1
1210111613-51
1210811618:35
72-20-8
NO
ug/L
0.050
0.050
1
12101/1613:51
12/08/1618:35
7421-93-4
NO
ug/L
0.050
0.050
1
12101/1613:51
1210811618:35
76-44-6
NO
ug/L
0.050
0.050
1
12101/1613:51
12108/1618:35
1024-57-3
NO
ug/L
0.50
0.50
1
12101/1613:51
12/08/1618:35
12674-11-2
NO
ug/L
0.50
0.50
1
12101/1613:51
12/08/1618:35
11104-28-2
NO
ug/L
0.50
0.50
1
12JO111613:51
12/0811618:35
11141-16-5
NO
ug/L
0.50
0,50
1
1210111613:51
12/0811618:35
53469-21-9
NO
ug/L
0.50
0,50
1
12/0111613:51
12/08/1618:35
12672-29-6
NO
ug/L
0.50
0.50
1
12/01/1613:51
12/08/1618:35
11097-69-1
NO
ug/L
0.50
0.50
1
12/01/1613:51
12108/1618:35
11096-82-5
NO
ug/L
0,50
0.50
1
12101/1613:51
12/0811618:35
8001-35-2
75
%
20-110
1
1210111613:51
12/08/1618:35
877-09-8
26
%
20-138
1
12/01/16 13:51
12/08/16 18:35
2051-24-3
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
NO mg/L 0.0010 0.00050 1 1IM16 21:30 12/02/16 06.68 7440-43-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 12/09/2016 03:39 PM without the written consent of Pace Ana*bcal Services, LLC. Page 8 of 40

Peke Anaiyticat Services, LLC
CA2 /� �„ x 205 East Meadow Road - Suite A
A JLiJ�/[fcar Eden, NC 27288
r wwr pmlabsa= [phone]
ANALYTICAL RESULTS
Project: 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Sample: OLrrFALL 2 Lab ID: 92321165002 Collected: 11/29/16 14:35 Received: 11/29/16 16:30 Matrix Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua]
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Chromium
ND
mg/L
0.0050
0.0025
1
11/30/16 21:30
12/02/16 06:58 7440-47-3
Copper
0.00S6
mg/L
0.0050
0.0025
1
11/30/16 21:30
12102/16 06:58
7440-50-8
Lead
NO
mg/L
0.0050
0.0025
1
11/80/16 21:30
12/02/16 06:50
7439-92-1
Nickel
NO
mg/1-
0.0050
0.0025
1
11/30/16 21:30
12/02/16 06:58
7440-02-0
Silver
NO
mg/L
0.0050
0.0025
1
11/30/16 21:30
12/02/16 06:58
7440-22-4
Zinc
NO
mglL
0,010
0.0025
1
11/30/16 21:30
12IO2/16 06:58
7440-66-6
025 MSSV
Analytical
Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
NO
ug/L
5.0
0.25
1
11/29/16 16:40
11/30/16 23:17
83-32-9
Aoenaphthylene
ND
ug/L
5.0
0.21
1
11129/1616:40
11/30/16 23:17
208-96-8
Anthraoane
NO
ug/L
5.0
0.14
1
11/2911616:40
11/30116 23:17
120-12-7
Benzo(a)anthraoene
NO
ug/L
5.0
0.33
1
1112916 16:40
11/30/16 23:17
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
0.30
1
11/29/16 16:40
11/30/1623:17
50-32-8
Benzo(b) luoranthene
ND
uglL
5.0
0.28
1
11/29/16 16:40
11/30116 23:17
205-99-2
Senzo(g,h.i)perylene
ND
ug/L
5.0
0.38
1
11/29/1616.40
11/30/16 23:17
191-24-2
Benzo(k)fluoranthene
NO
uglL
5.0
0.43
1
11/29116 16:40
11/30/16 23:17
207-08-9
4-Bromophenylphenylether
NO
uglL
5.0
0.82
1
11129/1616:40
11/30116 23:17
101-55-3
Butylbenzylphthalate
NO
ug/L
5.0
0.79
1
IM911616:40
11/30116 23:17
85-68-7
4-Chloro-3-methylphenol
NO
ug/L
5.0
3.7
1
1M911616:40
11/30/16 23:17
59-60-7
bis(2-Chloroethoxy)metI=e
NO
ug/L
10.0
0.92
1
11/29/1616:40
11/30/1623:17
111-91-1
bis(2-Chlomethyl) ether
ND
ug/L
5.0
1:0
1
11/29/16 16:40
11/30116 23:17
111 44-4
2-Chloronaphthalene
NO
ug/L
5.0
0.98
1
11129/1616:40
11/30/16 23:17
91-58-7
2-Chlorophenol
NO
uglL
5.0
1.3
1
11/29/16 16:40
11/30/16 23:17
95-57-8
4-Chlorophenylphenyl ether
NO
ug/L
5.0
0.87
1
11/29/16 16:40
11/30/16 23:17
7005-72-3
Chrysene
NO
ug/L
5.0
0.21
1
11/2911616:40
11/30/16 23:17
218-01-9
Dibenz(a,h)anthracene
NO
ug/L
5.0
0.55
1
11/29/1616:40
11/30/16 23:17
53-70-3
3,3'-Dichlorobenzidine
NO
ug/L
25.0
2.1
1
11129/1616:40
11/30/16 23:17
91-94-1
2,4-Dichiorophenol
NO
ug/L
5.0
1.7
1
11/29/16 16:40
11/30116 23:17
120-83-2
Diethylphthalate
NO
ug/L
5.0
0.58
1
11/2911616:40
11/30/16 23:17
84-0Fr2
2,4-Dimethylphenol
ND
ug/L
10.0
1.2
1
11/29/16 16:40
11/30/16 23:17
105.67-9
Dimethylphthalate
NO
ug/L
5.0
0.76
1
11129/1616:40
1113011623:17
131-11-3
Di-"utylphthalate
NO
ug/L
5.0
0.75
1
11/29/16 16.40
11/30/16 23:17
84-74-2
4,6- initro-2-methylphenol
NO
uglL
20.0
2.6
1
11/29/1616.40
11/30/16 23:17
534-52-1
2,4-Dinitrophenol
NO
ug1L
50.0
9.0
1
11/29/16 16:40
11/30/16 23:17
51-28-5
2,4-Dindrotoluene
NO
ug/L
5.0
0.90
1
11/29/1616:40
11/30/16 23:17
121-14-2
25-Dinitrotoluene
ND
ug/L
5.0
0.98
1
11129/1616:40
11/30/16 23:17
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
0.66
1
11/2W16 16:40
11/30/16 23:17
1174M-0
bis(2-Ethylhexyl)phthalate
NO
uglL
5.0
0.79
1
11/29/16 16:40
.11/30/1623:17
117-81-7
Fluoranthene
NO
ug/L
5.0
0.21
1
11/29/16 16:40
11/30116 23:17
20644-0
Fluorene
ND
ug/L
5.0
0.21
1
11/29/16 16:40
11/30/16 23:17
86-73-7
Hexachloro-1,3-butadiene
ND
uglL
5.0
0.94
1
11129/1616:40
11/30116 23:17
87-68-3
Hexac hlorobenzene
NO
ug/L
5.0
0.72
1
11/29/16 16:40
11/30/16 23:17
118-74-1
Hexachlorocyclopentadiene
NO
uglL
10.0
0.88
1
11/29/16 16:40
11/30/16 23:17
77-47-4
I•• lexachloroethans
NO
ug/L
5.0
1.1
1
11/29/16 16:40
11/30/16 23:17
67-72-1
lndeno(1,2,3-cd)pyrene
ND
ug/L
5.0
0.29
1
11/2911616:40
11/30/16 23:17
193-39-5
Isophorone
ND
ug/L
10.0
0.89
1
11/29/16 16:40
11/30/16 23:17
78-59-1
REPORT OF LABORATORY ANALYSIS
'M1
M1
MI
M1
This report shall not be mproduced, except in fW,
Date: 12/09/2016 03:39 PM without the written oonsent of Pace Analytical Services, LLC. Page 9 of 40

aceAralytical
WWWpsodabxcVm
Pace Ana"cai Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623.892 i
ANALYTICAL RESULTS
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Sample: OUTFALL 2 Lab ID: 92321165002 Collected: 11/29/1614:35 Received: 11/29/16 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Naphthalene
ND
ug/L
5.0
0.34
1
11/29/16 16:40
11/30/16 23:17
91-20-3
Nitrobenzene
NO
ug/L
5.0
1.1
1
11/29/16 16:40
11/30/16 23:17
98-95-3
2-Nitrophenol
ND
ug/L
5.0
0.91
1
11/29/16 16:40
11/30/16 23:17
88-75-5
itrophanol --
ND
ug(1
50-0
4:1-----1--11/MI6.16:40-11/30116-28-1.7-100-02-7
N-Nitrosodimethylamine
NO
ug/L
5.0
0.91
1
11/29/16 16:40
11/30/16 23:17
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
0.99
1
11/29/16 16:40
11/30/16 23:17
621-04-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1.0
1
11/29/16 16:40
11/3011623:17
86-30-6
2,2'4)xyb1s(1-chloropropane)
ND
ug/L
5.0
0.95
1
11/29/16 16:40
11/30/16 23:17
108-60-1
Pentachlorophenol
NO
ug/L
10.0
4.6
1
11/29/16 16:40
11/30/16 23:17
87-86-5
Phenanthrene
NO
ug/L
5.0
0.22
1
11/29/16 16:40
111=1623:17
85-01-8 M1
Phenol
NO
ug/L
5.0
1.9
1
11/29/16 16:40
11/30/16 23:17
Pyrene
NO
u9/L
5.0
0.19
1
11/29/16 16.40
11/30/16 23:17
129-00-0 MI
1,2,4-Trichlorobenzene
NO
u91L
5.0
0.98
1
11/29/16 1&40
11/30/16 23:17
120-82-1 M1
2,4,6-Trichlorophenol
NO
ug/L
10.0
1.3
1
11/29116 16:40
11/30/16 23:17
88-06-2
Surrogates
Nitrobenzened5 (S)
37
%
10-120
1
11/29/16 16:40
11/30/16 2317
4165-60-0
2-Fluorobiphenyl (S)
43
%
15-120
1
11/29/16 16:40
11/30/16 23:17
321-60-8
Terphenyl-dl4 (S)
43
%
11-131
1
11/29/16 16:40
11/30/16 23:17
1718-51-0
Phenold6 (S)
15
%
10-120
1
11/29/16 16:40
11/30/16 23:17
13127488-3
2-Fluorophenol (S)
23
%
10-120
1
11/29/16 16:40
11/30/16 23:17
367-12-4
2,4,6-Tribromophenol(S)
48
%
10-137
1
11/29/1616:40
11/30/16 23:17
118-79-6
624 Volatile Organics Analytical Method: EPA 624
Benzene
NO
ug/L
2.0
1.7
1
12101/1619:15
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1.7
1
12/01/1619:15
75-27-4
Bromoform
ND
ug/L
2.0
1.5
1
12/01/1619:15
75-25-2
Bromomethane
NO
ug/L
2.0
1.0
1
12/0111619:15
74483-9
Carbon tetrachloride
NO
ug/L
2.0
1.9
1
12/01/1619:15
56-23-5
Chlorobenzene
NO
u91L
2.0
1.7
1
12101/1619.15
108-90-7
Chloroethane
NO
u91
2A
1.6
1
12/01/1619:15
75-00-3
Chloroform
NO
ug/L
2.0
1.9
1
12101/1619:15
67-6&3
Chloromethane
NO
ug/L
2.0
1.5
1
12/01/1619:15
74-87-3
Dibromochloromethane
NO
ug/L
2.0
1.8
1
12/01/1619:15
124-48-1
1,2-Dichlorobenzene
NO
u91L
2.0
1.5
1
12101/1619:15
95-50-1
1,3-Dictdorobenzene
ND
ug/L
2.0
1.5
1
1210111619:15
541-73-1
1,4-Dichlorobenzene
NO
ug/L
2.0
1.5
1
12101/1619:15
106-46-7
1,1-Diahloroethane
NO
ug/L
2.0
1.8
1
12/01/1619:15
75-34-3
1,2-Dichlaroethane
ND
ug/L
2.0
1.8
1
12101/1619:15
107-06-2
1,1-Dichloroethene
NO
ug/L
2.0
1.9
1
12101/1619:15
75-35-4
cis-1,2-Dichloroethene
NO
ug/L
2.0
1.8
1
12/01/1619.15
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
2.0
1.8
1
12/01/1619:15
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1.7
1
12/01/1619:15
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1.6
1
12101/1619:15
10061-01-5
trans-1,3-Dichloropropene
NO
uglL
2.0
1.6
1
12101/1619:15
10061-02-6
Ethylbenzene
NO
ug/L
2.0
1.6
1
12/0111619:15
100-41-4
Methylene Chloride
NO
ug/L
2.0
1.9
1
12/01/16 19:15
75-09-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fu 1,
Date: 1210=016 03:39 PM without the written ooruent of Pace Analytical Services, LLC. Page 10 of 40

I
eAnalytical
rw:pe.cam
Pace Analytical Services, LLC
205 East Meadow Road - Suits A
Eden, NC 27258
[phone]
r ANALYTICAL RESULTS
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Sample: OUTFALL 2
Lab ID: 92321165002
Collected:
11/29/16 14:35
Received: 11129/1616:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
624 VoWle Organics
Analytical Method: EPA 624
1,1,2,2-Tetrachloroethane
NO
ug/L
2.0
1.5
1
12101/1619:15
79-34-5
Tetrachloroethene
NO
u91L
2.0
1.8
1
12/0111619:15
127-18-4
Toluene
NO
ug(L
2.0
1.6
1
12/0111619:15
108-88-3
1,1,1-Trichloroethane
NO
ug/L
2.0
1.9
1
12/01/1619:15
71-55-6
1,12-Trichloroethane
NO
ug/L
2.0
1.7
1
12/01/1619:15
79-00-5
TridMoroed ene
NO
ug/L
2.0
1.8
1
12101/1619:15
79-01-6
Trichlomfluoromethane
ND
WA
2.0
1.7
1
12/01/1619:15
75-69-4
Vinyl chloride
NO
ug/L
2.0
1.5
1
12/0111619:15
75-01-4
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
12JO1116 19:15
460-004
Toluene-d8 (S)
103
%
70-130
1
12/01/16 19:15
2037-26-5
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
12/01/16 19:15
17060-07-0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 5.4 mg/L 2.6 2.6 1 11/30/16 18:10
9040 pH Analytical Method: EPA 9040
pH 6.7 Std. Units 0.10 0.10 1 11/30/1612:03 H6
Sample: OUTFALL 3 Lab ID: 9=1165003 Collected: 11129/1614.45 Received: 11/29/16 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No.- ' Quat
HEIR, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1.1 1 12105/16 08:34
608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510
Aldrin
NO
ug/L
0.050
0.050
1
12101/1613:51
12108/1618:52
309-00-2
alpha-BHC
NO
ug/L
0.050
0.050
1
12/01/1613:51
12/08J1618:52
3194"
beta-BHC
NO
ug/L
0.050
0.050
1
12/01/1613:51
12/081l618:52
319-85-7
delta-BHC
NO
ug/L
0.050
0.050
1
12101/1613:51
12108/1618:52
319-86-8
gamma-BHC (Lindane)
ND
ug/L
0.050
0.050
1
12/01/1613:51
12/08/1618:52
58-89-9
Chlordane (Technical)
ND
ug/L
0.50
0.50
1
12/01/1613:51
12/08/1618:52
57-74-9
4,4'-DDD
NO
ug/L •
0.050
0.050
1
12/01/1613:51
12/08/1618:52
72-54-8
4,4'-DDE
NO
ug/L
0.050
0.050
1
12101/1613:51
12/0811618:52
72-55-9
4,4 DDT
NO
ug/L
0.050
0.050
1
12101/1613:51
12108/1618:52
50-29.3
Dieldrin
NO
ug/L
0.050
0.050
1
12/0111613:51
1210811618:52
60-57-1
Endosutfan I
NO
ug/L
0.050
0.050
1
12/01/1613:51
12/08/16 18:52
959-98-8
Endosulfan tl
NO
ug1L
0.050
0.050
1
12/01/16 13:51
12/08/1618:52
33213-65-9
Endosutfan sulfate
ND
ug/L
0.050
0.050
1
12/01/1613:51
12/0811618:52
1031-07-8
Endrin
NO
ug/L
0.050
0.050
1
12/01/1$13:51
12ID811618:52
72-20-8
Endrin aldehyde
NO
ug1L
0.050
0.050
1
12101/1613:51
121=16 18:52
7421-93-4
Heptachlor
NO
ug/L
0.050
0.050
1
12101/1613:51
12/08/16 18:52
76A 4.8
Heptachlor epoxide
NO
ug/L
0.050
0.050
1
12101/16 13:51
12/08/16 18:52
1024-57-3
REPORT OF LABORATORY ANALYSIS
This n°pmt shall not be repmduced. except in fell.
Date: 12/09/2016 03:39 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 40

Mnapcal'
www.pacatbacom
Pace Anaydcel Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-892t
ANALYTICAL RESULTS
Project: 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Sample: OUTFALL 3 Lab ID: 92321165003 Collected: 11/29/16 14:45 Received: 11/29/16 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510
PCB-1016 (Arodor 1016)
ND
ug/L
0.50
0.50
1
12/01/16 13:51
12/08/1618:52
12674-11-2
PCB-1221 (Amclor 1221)
ND
ug/L
0.50
0.50
1
12/01/16 13:51
12/08/16 18.52
11104-28-2
PCB-1232 (Arocor 1232)
ND
uglL
0.50
0.50
1
1210111613:51
12/08/16 18:52
11141-16-5
PCB-1242•(r roclor-1242)
ND
ugA:
0.50
0 50-1-
l2101/i6-13:51-12108/16-i"e"-'5346'^ 2l=9
PCB-1248 (Arodor 1248)
ND
uglL
0.50
0.50
1
12/01116 13:51
12/08/16 18:52
12672-29-6
PCB-1254 (Arodor 1254)
ND
uglL
0.50
0.50
1
12/01/16 13:51
12/08116 18:52
1M74WI
PCB-1260 (Ardor 1260)
ND
ug/L
0.50
0.50
1
12/01/16 13:51
121=16 18:52
11096-82-5
Toxaphene
ND
ug/L
0.50
0.50
1
12/01/16 13:51
12108/1618:52
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
72
%
20-110
1
12/01/16 13:51
12/08/16 18:52
877-09-8
Decachlorobiphenyl (S)
39
%
20-138
1
12/01/16 13.51
12/0811618:52
2051-24-3
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND
mg/L
0,0010
0.00050
1
11/30/16 21:30
12/02/16 07:02
7440-43-9
Chromium
ND
mg/L
0,0050
0.0025
1
11/30/16 21:30
12/02/16 07:02
7440-47-3
Copper
0.0058
mg1L
0.0050
0.0025
1
11/30/16 2130
12102/16 07:02
7440-50-8
Lead
ND
mg/L
0.0050
0.0025
1
11/30/16 21:30
12102/16 07:02
7439-92-1
Nickel
ND
mg/L
0.0050
0.0025
1
11/30/16 21:30
12/02/16 07:02
7440-02-0
Silver
ND
mg/L
0.0050
0.0025
1
11/30/16 21:30
12/02/16 07:02
7440-22-4
Zinc
ND
mg/L
0.010
0.0025
1
11/30/16 21:30
12/02/16 07:02
7440-66-6
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND
ug/L
5.0
0.25
1
11/29/16 16:40
12/01/16 00:13
83-32-9
Acenaphthylene
ND
ug1L
5.0
0.21
1
11/29/16 16:40
12/01/16 00:13
208-96-8
Anthracene
ND
ug/L
5.0
0.14
1
11129/1616:40
12/01/16 00:13
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
0.33
1
11/29/16 16:40
12/01/16 00:13
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
0.30
1
IM9116 16:40
12/01/16 00:13
50-32-8
Senzo(b)fluoranthene
ND
ug/L
5.0
0.28
1
11129/1616:40
12/01/16 00:13
205-99-2
Benzo(g,h,i)perylene
ND
u91L
5.0
0.38
1
11/2911616:40
12101/1600:13
191-24-2
Benzo(k)fiuoranthene
ND
ug/L
5.0
0.43
1
11/29/16 16:40
12/01/16 00:13
207-08-9
4-Bromophenylphenyl ether
ND
ug1L
5.0
0.82
1
11/29/16 16:40
12/01/16 00:13
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
0.79
1
11/29/16 16:40
12/01/16 00:13
85-68-7
4-CMoro-3-methylphenol
ND
ug1L
5.0
3.7
1
11/29/16 16:40
12/01/16 00:13
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
0.92
1
11/29/1616:40
1210111600:13
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1.0
1
11/29/16 16:40
12/01/16 00:13
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
0.98
1
11/29/16 16:40
12/01/16 00:13
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1.3
1
11/29/16 16:40
12101/16 00:13
95-57-8
4-Chlorophenyiphenyl ether
ND
ug/L
5.0
0.87
1
11/29/16 16:40
12/01/16 00:13
7005-72-3
Chrysene
ND
ug/L
5.0
0.21
1
11/29/16 16:40
12101/1600:13
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
0.55
1
11/29/16 16:40
12/01/16 00:13
53-70-3
3,3'-Dichlorobenzidine
ND
ug1L
25.0
2.1
1
11/29/16 16:40
12/01/16 00:13
91-94-1
2,4-Dichlomphenal
ND
ug/L
5.0
1.7
1
11/29/16 16:40
12/01/16 00:13
120483-2
Diethylphthalate
ND
ug/L
5.0
0.58
1
11W1616:40
12/01/16 00:13
84-66.2
2,4-Dimethylphenol
ND
ug/L
10.0
1.2
1
11/29/16 16:40
12/01/16 00:13
105-67-9
Dimethylphthaiate
ND
u9/L
5.0
0.76
1
11/29/16 16:40
12/01/16 00:13
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
0.75
1
11/29/16 16:40
12/01/16 00:13
84-74-2
REPORT OF LABORATORY ANALYSIS
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Date: 12/09/2016 03:39 PM without the written consent of Pace Anaykaf Services, LLC. Page 12 of 40

aCaAnalytical'
WWWP3D0AJbS=n
Pace Analydcal Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
(336)62"921
ANALYTICAL RESULTS
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Sample: OUTFALL 3 Lab ID: 92321165003 Collected: 11/29/16 14:45 Received: 11/29/16 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
625 NSSV Analytical Method: EPA 625 Preparation Method: EPA 625
4,6-Dindm-2-rnethytphenol
ND
ug/L
20.0
2.6
1
11129/1616:40
12/01/16 00:13
534-52-1
2,4-Mnitrophenol
ND
ug/L
50.0
9.0
1
11/29/16 16:40
12/01/16 00:13
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
0.90
1
11/29/16 16:40
12/01/16 00:13
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
0.98
1
11/2911616:40
12/01/16 00:13
606-20-2
Di-n-ociylphthalate
ND
ug/L
5.0
0.66
1
11/29/1616:40
12/01/16 00:13
11744-0
bis(2-Ethylhexyt)phthalate
ND
ug/L
5.0
0.79
1
11/29/1616:40
12/01/16 00:13
117-81-7
Fluoranthene
ND
ug/L
5.0
0.21
1
11/29/1616:40
12/01/16 00:13
206- 4-0
Fluorene
ND
ugiL
5.0
0.21
1
11/29/16 16:40
12/01/16 00:13
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
0.94
1
11/2911616:40
12/01/16 00:13
87-68-3
Hexachlorobenzene
ND
ug1L
5.0
0.72
1
11/29/16 16:40
12JO1116 00:13
118-74-1
Hexachlorocydopentadiene
ND
ug1L
10.0
0.88
1
11/29/16 16:40
12/01/16 00:13
77-474
Hexarhloroethane -
ND
ug/L
5.0
1.1
1
11/29/16 16:40
12/01/16 00:13
67-72-1
Indeno(1,2,3-cd)pyrene
ND
uglL
5.0
0.29
1
1112911616:40
12101/16 00:13
193-39-5
Isophorone
ND
U9&
10.0
0.89
1
11/29/16 16:40
12/01/16 00:13
78-59-1
Naphthalene
ND
uglL
5.0
0.34
1
11/29/1616:40
12/01/16 00:13
91-20-3
Nitrobenzene
ND
ug/L
5.0
1.1
1
11129/1616:40
12/01/16 00:13
98-95-3
2-Nitrophenol
ND
ug/L
5.0
0.91
1
1112911616:40
12101/1600:13
88-75-5
4-Nitrophenol
ND
ug/L
50.0
4.1
1
11/2911616:40
12101/16 00:13
100-02-7
N-Nitrosodimethylamine
ND
ug1L
5.0
0.91
1
11/2911616:40
12/01/16 00:13
62-75-9
N-NitrDso-di-n-propylamine
ND
uglL
5.0
0.99
1
11/29/1616:40
12101/16 00:13
621-64-7
N-Nitrosodiphenytamine
ND
ug/L
10.0
1.0
1
11/29/1616:40
12/01/16 00:13
86-30-6
2,2'-Oxybis(1-chiaropropane)
ND
ug/L
5.0
0.95
1
11/2911616:40
12/01/16 00:13
108-60-1
Pentachlomphenol
ND
ug/L
10.0
4.6
1
11/2W1616:40
12101/16 00:13
8746-5
Phenanthrene
ND
ug/L
5.0
0.22
1
11/2911616:40
12/01/16 00:13
85-01-8
Phenol
ND
ug/L
5.0
1.9
1
11129/1616:40
12/01/16 00:13
Pyrene
ND
ug/L
5.0
0.19
1
11/29/16 16:40
12/01/16 00:13
129-00-0
1,2,4-Tdchlorobenzene
ND
ug/L
5.0
0.98
1
11/29/1616:40
12101/16 00:13
120-82-1
2,4,6-Tdchlorophenol
ND
ug/L
10.0
1.3
1
11/2911616:40
12101/16 00:13'
884)6.2
Surrogates
4
Nitrobenzene-c!5 (S)
35
%
10-120
1
11/29/16 16:40
12/01/16 00:13
4165-60-0
2-Fluorobiphenyl (S)
42
%
15-120
1
11 /29/16 16:40
•12101/16 00:13
321-60-8
Terphenyl-d14 (S)
51
%
11-131
1
11/29/16 16:40
12/01/16 00:13
1718-51-0
Phenol-d6 (S)
14
%
10-120
1
11/29/16 16:40
12/01/16 00:13
1312743&3
2-Fluorophenol(S)
21
%
10-120
1
11/2911616:40
12/01/16 00:13
367-12-4
2,4,6-Tribromophenol (S)
46
%
10-137
1
11/29/1616:40
12/01/16 00:13
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND
ug/L
2.0
1.7
1
12/01/1619:33
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1.7
1
12/0111619:33
75-27-4
Bromoform
ND
ug1L
2.0
1.5
1
12101/1619:33
75-25-2
Bromomethane
ND
ug1L
2.0
1.0
1
1210111619:33
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1.9
1
12101/1619:33
56-23-5
Chlorobenzene
ND
ug/L
2.0
1.7
1
12/01/1619:33
108-90-7
Chloroethane
ND
ug/L
2.0
1.6
1
12/01/1619:33
75-00-3
Chloroform
ND
uglL
2.0
1.9
1
12/01/1619:33
67-66-3
Chloromethane
ND
ug/L
2.0
1.5
1
12/0111619:33
74-87-3
REPORT OF LABORATORY ANALYSIS
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Date: 12/09/2016 03:39 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 40

,�aneAnalytical*
www.Fa0ffA =M
ANALYTICAL RESULTS
Project 2016 SEMI-ANNUAL
Paco Analytical serokas, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]-
Pace Project No.: 92321165
Sample: OUTFALL 3 Lab ID: 9=1165003 Collected: 11/29/1614:45 Received: 11/29/16 16:30 Matrix: Water
Report
Parameters Results Units Limit MDL Dl` Prepared Analyzed CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624
Dibromochloromethane
ND
ug/L
2.0
1.8
1
12101/1619:33
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1.5
1
12/01/16 19:33
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1.5
1
12/01/16 19:33
541-73-1
1;-Dichlorobanzano
rD
ug/L
2:0
1:5 1
12r'J1116-'.8:33--105-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1.8
1
12101/1619:33
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1.8
1
12/01/16 19:33
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1.9
1
12/01/16 19:33
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
1.8
1
12/01/1619.33
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
1.8
1
12101/1619:33
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
1.7
1
12101/1619:33
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1.6
1
12/01/16 19:33
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
2.0
1.6
1
12101/1619:33
10061-02-6
Ethylbenzene
ND
ug/L
2.0
1.6
1
12/01/16 19:33
100-41-4
Methylene Chloride
ND
ug/L
2.0
1.9
1
12/01/16 19:33
754)9-2
1,1,2,2-Tetrachioroethane
ND
ug/L
2.0
1.5
1
12/01/16 19:33
79-34-5
Tetrachloroethene
ND
ug/L
2.0
1.8
1
12101/1619:33
127-184
Toluene
ND
ug/L
2.0
1.6
1
12101/1619:33
1084M-3
1,1,1-Trichloroethane
ND
ug/L
2.0
1.9
1
12/01/16 19:33
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1.7
1
12/0111619:33
79-00-5
Trichloroethene
ND
ug/L
2.0
1.8
1
12101/1619:33
79-01-6
Tdchloroi3uoromethane
ND
u911-
2.0
1.7
1
12101/1619:33
75-69-4
Vinyl chloride
ND
ug/L
2.0
1.5
1
12/01/16 19:33
75-01-4
Surrog""
4-Bromofluorobenzene (S)
102 % 70-130
1
12/01/16 19:33 460-00-4
Toluene-d8 (S)
104 % 70-130
1
12/01/16 19:33 2037-26-5
1,2-Dichloroethane-d4 (S)
95 % 70-130
1
12/01/16 19:33 17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
13.0 mg/L 5.0
5.0 1
11/30/16 18:10
9040 pH
Analytical Method: EPA 9040
pH
6.5 Std. Units 0,10
0.10 1
11/3011612:03 H6
REPORT Of LABORATORY ANALYSIS
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Date: 12/0912016 03:39 PM without the written consent of Pace Anaytml Services, LLC. Page 14 of 40

aceAnalytal `
wwr'-Aa�tadscmm
Pace An*Ucal Services, LLC
2D5 East Meadow Road - Suite A
Eden, NC 27268
[phone]
QUALITY CONTROL DATA
Project: 2016 SEMI-ANNUAL
Paoe Project No.: 92321165
QC Batch: 339287 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92321165001, 92321165002, 92321165003
METHOD BLANK: 1881467 Matrix: Water
Associated Lab Samples: 92321165001, 92321165002, 92321165003
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 1.1 12/05/16 08:31
LABORATORY CONTROL SAMPLE: 1881468
Spine LCS LOS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 40 35.3 88 78-114
MATRIX SPIKE SAMPLE: 1881469
92321114001 Spike MS MS % Rec
Parameter Units Result Conn result % Rec Limits Qualifiers
Oil and Grease mg/L ND 40 37.7 91 78-114
Results presenisd on this page we in the units indicated by the `Unita' cohmm except wha an aleersurte unk Is presented to the right at the result
REPORT OF LABORATORY ANALYSIS
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Date: 12/09/2016 03.39 PM wittrout the written consent of Pace Analy6 Services. LLC,
Page 15 of 40

,�aceAna*al*
www pacelabsoom
QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
QC Batch: 338679 Analysis Method: EPA 200.7
QC Batch Method: EPA200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92321166001, 92321165002, 92321165003
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]'
METHOD BLANK: 1877885
Matrix: Water
Associated Lab Samples:
92321165001, 92321165G02, 92321165003
Blank
Reporting
Parameter
Units
Result
limit
MDL
Analyzed Qualifiers
Cadmium
mg/L
ND
0.0010
0.00050
12/02f1611:36
Chromium
mg/L
ND
0.0050
0.0025
1210211611:36
Capper
mg/L
ND
0.0050
0.0025
12102/1611:36
Lead
mg/L
ND
0.0050
0.0025
12102/1611:36
Nickel
mg/L
ND
0.0050
0.0025
12/02/1611.36
Silver
mg/L
ND
0.0050
0.0025
12/02/1611:36
Zinc
mg1L
ND
0.010
0.0025
12/02/16 07:38
LABORATORY CONTROL SAMPLE:
Parameter
1877886
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Cadmium
mg/L
.5
0.49
99
85-115
Chromium
mg/L
.5
0.49
98
85-115
Capper
mg/L
.5
0.53
106
85-115
Lead
mgA.
.5
0.48
97
85-115
Nickel
mg/L
.5
0.48
97
85-115
Silver
mg/L
.25
0.26
102
85-115
Zinc
mg/L
.5
0.51
101
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1877887
1877888
MS
MSD
92321046001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qua]
Cadmium
mg/L
<0.50 ug/L
.5
.5
0.49
0.49
98
99
70-130
1
20
Chromium
mg/L
<2.5 ug/L
.5
.5
0.49
0.49
98
99
70-130
1
20
Copper
mg/L
<2.5 ug/L
.5
.5
0.52
0.53
105
106
70-130
1
20
Lead
mg/L
<2.5 ug/L
.5
.5
0.40
0.48
96
97
70-130
0
20
Nickel
mg/L
<2.5 ug/L
.5
.5
0.48
0.48
95
96
70-130
0
20
Silver
mg/L
<2.5 ug/L
.25
.25
0.26
0.26
102
103
70-130
1
20
Zinc
mg/L
<2.5 ug/L
.5
.5
0.50
0.50
99
100
70-130
1
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1877889
1877890
MS
MSD
92321165001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Cadmium mg1L ND .5 .5 0.50 0.50 99 99 70-130 0 20
Chromium mg/L ND .5 .5 0.49 0.49 98 98 70-130 0 20
Rasrdb presented an thia pqa are maw units kMicaed by the'tJ&W column except wtrars an atternata unit la preserted to the right ar ttw rmutL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 12/0912016 03:39 PM without the written consent of Pace Analytical Services, L.LC. Page 16 of 40

cgAnalyUcal e
.-% P30612ba.am
Pace Analytical Services, LLC
2D5 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1877889
MS
92321165001
Spike
Parameter
Units
Result
Conc.
Copper
mg/L
ND
.5
Lead
mg/L
ND
.5
Nickel
mg/L
ND
.5
Silver
mgtL
ND
.25
Zinc
mglL
0,026
.5
1877890
MSD
Spike
MS
MSD
MS
MSD
% Rec
Max
Cones
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
.5
0.52
0.53
104
105
70-130
1
20
.5
0.49
0.50
99
99
70-130
0
20
.5
0.49
0.49
98
98
70-130
0
20
.25
0.26
0.26
102
102
70-130
0
20
.5
0.54
0.54
103
103
70-130
0
20
Resudb presented on aft page am In dre units indleatad by ttr "Unite' odu m ammW where an etwnate unit is pFeserftd to the right of the rwjIt.
REPORT OF LABORATORY ANALYSIS
7hiss report shall not be reproduced, except in full,
Date: 12/09/2016 03:39 PM without the written consent of Pace Ana"cal Services, L-C.
Page 17 of 40

aceAnalyiical'
rrkW Peoela MMM
Pace Analytical Servkm* LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]-
QUALITY CONTROL DATA
Project: 2016 SEMI-ANNUAL
Pace Project No.: 92321165
QC Batch: 338976 Anatysis-Method: EPA624
QC Batch Method: EPA624 Analysis Description: 624 MSV
Associated Lab Samples- 92321165001, 92321165002, 92321165003
METHOD BLANK: 1879658
Matrix: Mter
Associated Lab Samples: 92321165001, 92321165002, 92321165003
Blank
Reporting
Parameter
Units
Result
Limit
MOIL
Analyzed Qualifiers
IIAl-Trichloruethane
ug/L
NO
2.0
1.9
12/01/16 13:22
IIA2,2-Tetrachloroethane
ug/L
NO
2.0
1.5
12101/1613:22
1,1,2-Trichloroethane
ug/L
NO
2.0
1.7
12101/1613.22
1,1-Dichloroethane
ug/L
ND
2.0
1-8
12101116IT22
1,1-Dichloroethene
ug/L
ND
2.0
1.9
12101/1613:22
1,2-Dichlombenzene
ug/L
NO
2.0
1.5
12101/1613:22
1,2-Dichloroethane
ug/L
ND
2.0
1-8
12/01/16 13:22
1,2-Dichloropropane
ug/L
ND
2.0
1-7
12/01/16 13:22
1,3-Dichlorobenzene
ug/L
NO
2.0
1.5
12101/1613:22
1,4-DicJhlorobenzene
ug/L
NO
2.0
1.5
12101/1613:22
Benzene
ug/L
ND
2-0
1.7
12/01/16 13:22
Bromodichloromethane
ug/L
ND
2.0
1.7
1210111613:22
Bromoform
ug/L
NO
2.0
1.5
12/01/16 13:22
Bromomethane
ug/L
NO
2.0
1.0
12/01/16 13:22
Carbon tetrachloride
uglL
ND
2.0
1.9
12/01/16 13:22
Chlorobenzene
ug/L
ND
2.0
1.7
12101/1613:22
Chloroethane
ug/L
NO
2.0
1.6
12/0111613:22
Chloroform
ug/L
ND
2.0
1.9
12/01/16 13:22
Chloromethane
ug/L
ND
2.0
1.5
1210111613:22
cis-1,2-Dichloroed ene
ug/L
ND
2.0
1.8
12/01/16 13:22
cis-1,3-Dichioropropene
ug/L
NO
2.0
1.6
12/01/1613:22
Dibromochlorornethane
ug/L
NO
2.0
1.8
12/01/16 13:22
Ethylbenzene
ug/L
NO
2.0
1.6
12/0111613:22
Methylene Chloride
ug/L
ND
2.0
1.9
12/01/16 13:22
Tettachloroethene
ug/L
NO
2.0
1.8
12/01/16 13:22
Toluene
ug/L
NO
2.0
1.6
12/01/16 13:22
trans-1,2-Dichloroethene
U91L
NO
2.0
1.8
12101/1613:22
trans-1,3-Dichtoropropene
ug[L
ND
2.0
1.6
12101/1613:22
Trichloroethene
ugll_
NO
2.0
1.8
12101/1613:22
Tdchlorofluoromethane
ug/L
NO
2.0
1.7
12/01/16 13:22
Vinyl chloride
U91L
NO
2.0
1.5
12/01/16 13:22
1,2-Dichkwoethane-d4 (S)
%
93
70-130
12/01/16 13:22
4-Bromofluorobenzene (S)
%
99
70-130
12101116 13:22
Toluene-d8 (S)
°%
106
70-130
12/01/16 13:22
LABORATORY CONTROL SAMPLE: 1879659
Spike LCS LCS % Rec
Parameter Units Cone. Result % Roe Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 19.7 98 52-162
1,1,2,2-Tetrachloroethane ug/L 20 18.6 93 46-157
Resuft praeerrted on Crd page am in the unit indicated by the 'Unit' COUMa where an altnnte unit is prssentad to the right of the result
REPORT OF LABORATORY ANALYSIS
T -ds report Shall not be reproduced, except in full,
Date: 12109Q016 03:39 PM without the written Consent of Pace Analytical Services, LLC. Page 18 of 40

ce",,�Wa*
IM paceiaftsam
Pace An*tIcal services, LLC
205 Fast Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
LABORATORY CONTROL SAMPLE: 1879659
Spike
LOS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits
Qualifiers
1,1,2 Trichloroethane
ug/L
20
19.1
95
52-150
11-Dirhlorcethane
ug/L
20
17.8
89
59-155
1,1-Dichloroethene
ug/L
20
19.5
97
1-234
1.2-Dichlorobenzene
ug/L
20
19.0
95
18-190
1,2-Dichloroethane
ug/L
20
19.4
97
49-155
1,2-Dichloropropane
ug/L
20
17.5
88
1-210
1,3-Dichiarobenzene
ug/L
20
18.7
93
59-156
1,4-Dichlorobenzene
ug/L
20
18.6
93
18-190
Benzene
ug/L
20
19.6
98
37-151
Bromodichloromettwe
uglL
20
19.7
99
35-155
Bromoform
ug/L
20
18.1
91
45-169
Bromomethane
ug/L
20
16.6
83
1-242
Carbon tetrachloride
ug/L
20
21.9
109
70-140
Chlorobenzene
ug/L
20
-18.0
90
37-160
Chloroethane
ug/L
20
17.6
88
14-230
Chloroform
ug/L
20
19.8
99
51-138
Chloromethane
ug/L
20
14.1
70
1-273
cis-12-Dichloroethene
ug/L
20
18.4
92
68-146
cis-1,3-Dichloropropene
ug/L
20
18.6
93
1-227
Dibromochloromethane
ug/L
20
19.9
99
53-149
Ethylbenzene
ug/L
20
18.4
92
37-162
Methylene Chloride
ug/L
20
17.9
90
1-221
Tetrachloroethene
ug/L
20
17.5
87
64-148
Toluene
ug/L
20
19.0
95
47-150
trans-1,2-Dichloroethene
ug/L
20
18.8
94
54-156
trans-1,3-Dichloropropene
ugA-
20
18.5
93
17-183
Trichloroethene
ug/L
20
19.7
99
71-157
Trichlorofluoromethane
ug/L
20
21.6
108
17-181
Vinyl chloride
ug/L
20
16.5
83
1-251
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobehzene (S)
%
102
70-130
Toluene-48 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
1879661
923213MM1
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
NO
20
23.3
116
46-171
1,1,2.2-Tetrachloroefhane
ug1L
NO
20
19.9
99
73-159
1,1,2-Trichloroethane
ug/L
NO
20
21.4
107
64-152
1,1-Dichloroethane
ug/L
NO
20
20.2
101
43-172
11-Dichloroed ene
ug/L
NO
20
23.0
115
48-189
1,2-Dichlorobenzene
ug/L
NO
20
19.7
99
54-154
1,2-0ichloroethane
ug/L
NO
20
21.7
108
42-171
1,2-Dichloropropane
ug/L
NO
20
19.3
97
55-157
1,3-Dichlorobenzene
ug/L
NO
20
19.4
97
57-148
Resuft preser I on thts p pa are in the units hrdxabd by the -!nits' cahemn eroxpt where an altenuft unit is paasarded to tto right of the noulL
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
Date: 12/09/2016 03:39 PM without the wnftn consent of Pace Analytical Services, LLC. Page 19 of 40

aceAnalytical s
wwwpscela &wM
Pace AnalyCcal Services, LLC
205 Fast Meadow Road - Suits A
Eden, k 27288
(336)6238921-
QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
MATRIX SPIKE SAMPLE: 1879661
92321369001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
limits Qualifiers
1,4-Didtlorobenzene
ug/L
ND
20
19.6
98
58-149
Benzene
ug/L
ND
20
22.9
114
54-163
Bromodichloromethane
ug/L
ND
20
22.3
112
56-152
Bromoform
ug/L
ND
20
17.9
89
53-151
Bromomethane
ug/L
NO
20
21.2
106
10-200
varbon-t-trachiorde
U91L
r:D
20
26:2
131
41-175
Chlorobenzene
ug/L
ND
20
20.8
104
67-152
Chtoroethane
ug/L
ND
20
21.8
109
23-200
Chloroform
u9/1-
ND
20
22.5
113
51-166
Chloromethane
ug/L
NO
20
17.9
90
40-175
cis-1,2-Dichloroethene
ug/L
ND
20
20.8
104
45-174
cis-1,3-Dichloropropene
ug/L
ND
20
20.9
104
38-146
Dibromochloromethane
ug/L
ND
20
20.2
101
65-144
Ethylbenzene
ug/L
ND
20
21.1
105
57-152
Methylene Chloride
ug/L
ND
20
17.9
90
40-167
Tetrachloroethene
ug/L
NO
20
19.7
98
59-155
Toluene
ug/L
ND
20
23.0
115
47-162
trans-1,2-Dichloroethene
ug/L
ND
20
21.8
109
47-178
trans-1,3-Dichloropropene
ug/L
ND
20
20.0
100
39-M
Trichloroethene
ug/L
NO
20
23.9
120
W153
Trichlorofluoromethane
ug/L
ND
20
27.1
136
42-199
Vinyl chloride
ug/L
ND
20
20.3
102
46-176
1,2-Didtloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 1879660
Parameter
Units
92321318001
Result
Oup
Result RPD
Max
RPD Qualifiers
1.1,1-Trichknmthane
ug/L
ND
NO
30
1.1,22-Tetradtloroethane
ug/L
ND
NO
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
NO
ND
30
1,1-Dichloroethene
ug/L
ND
NO -
30
1,2-Dirhlorobenzene
ug/L
ND
NO
30
1.2-Didtloroethane
ug/L
ND
NO
30
1,2-Dichloropropane
ug/L
NO
ND
30
1,3-Dichlorobenzene
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Bromodichloromethane
ug/L
NO
ND
30
Bromoform
ug/L
NO
ND
30
Bromomethane
u91L
ND
ND
30
Carbon tetrachloride
ug/L
ND
ND
30
Chlorobenzene
ug/L
NO
ND
30
Rosugs presented on this papa ore in the units Indicated by the -UrdW cdemm except wharf an alternate unit is praserdsd to the right otthe result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 03:39 PM without the written concert of Pace Analytical Services, LLC. Page 20 of 40

�aceMa/yh'cal
QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
SAMPLE DUPLICATE: 1879660
Pace Andy0cmd Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Parameter
Units
92321318001
Result
Dup
Result
Maas
RPD RPD Qualifiers
Chloroethane
ug/L
ND
ND
30
Chloroform
U91L
ND
ND
30
Chloromethane
U91L
ND
ND
30
cis-12-Dichloroethene
ug/L
ND
ND
30
ds-1,3-Dichloropropene
ug/L
ND
ND
30
Dibromochloromethane
ug/L
ND
ND
30
Ethylbenzene
U911-
ND
ND
30
Methylene Chloride
ug/L
ND
ND
30
Tetrachloroethene
ug/L
ND
ND
30
Toluene
ug/L
ND
ND
30
trans-1,2-Dichloroethene _
U91L
ND
ND
30
trans-1,3-Dichioropropene
ug/L
ND
ND
30
Trichloroethene
U91L
ND
ND
30
Trichlorofluoromethane
U91L "
ND
ND
30
Vinyl chloride
ug/L
ND
ND
30
1,2-Dichlonsethane-d4 (S)
%
98
96
3
4-Bromofluorobenzene (S)
%
102
100
2
Toiuene-d8 (S)
%
105
102
3
itesulls pn=r ted an this page are in the units indicaW by the'unW column eYoept where an alternate unit is v 1 - Psd to the right of the n sutt
REPORT OF LABORATORY ANALYSIS
This report shwa not be reproduced, except in fuu,
Date: 12109/2016 03:39 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 40

Ice
Analyical
www,09cr/abscam
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 2M8
(336)62348921
QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
QC Batch: 338979 Analysis Method: EPA608
QC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB
Associated Lab Samples: 92321165001, 92321165002, 92321165003
METHOD BLANK: 1879679 Matrix: Water
Associated Lab Samples, 92321165001, 92321165002, 92321165003
Blank Reporting
Parameter Units Result Limit MDL Analyzed Quafifiers
4,4'-DDD
ug/L
ND
0.050
0.050
1210711613:26
4,4'-ODE
ug/L
NO
0.050
0.050
12/07/16 13:26
4,4'-DDT
ug/L
ND
0.050
0.050
1210711613:26
Aldrin
u91L
NO
0.050
0.050
12107/1613:26
alpha-BHC
ug/L
ND
0.050
0.050
12107/1613:26
beta-BHC
ug/L
ND
0.050
0.050
12/07/16 13:26
Chlordane (Technical)
ug/L
ND
0.50
0.50
12/07/16 13:26
delta-BHC
ug/L
NO
0.050
0.050
12107/1613:26
Dieldrin
ug/L
NO
0.050
0.050
12/07/16 13:26
Endosulfan I
ug/L
NO
0.050
0.050
12/07/16 13:26
Endosullan II
ug/L
ND
0.050
0.050
12/07/16 13.26
Endosulfan sulfate
ug1L
ND
0.050
0.050
12/07/16 13:26
Endrin
ug1L
NO
0.050
0.050
12107/1613:26
Endrin aldehyde
ug/L
NO
0.050
0.050
12/07/16 13:26
gamma-BHC (Undane)
ug/L
NO
0.050
0.050
12/07/16 13:26
Heptachlor
ug/L
ND
0.050
0.050
12/07/1613:26
Heptachlor epoxide
ug/L
NO
0.050
0,050
12/07/16 13:26
PCB-1016 (Arodor 1016)
ug/L
NO
0.50
0.50
12/07/16 13:26
PCB-1221 (Arodor 1221)
ug/L
ND
0.50
0.50
12/07/16 13:26
PCB-1232 (Arodor 1232)
ug/L
N❑
0.50
0.50
12/07/16 13:26
PCB-1242 (Arodor 1242)
ug/L
ND
0.50
0.50
12/07/16 13:26
PCB-1248 (Aroclor 1248)
ug1L
NO
0.50
0.50
12/07/16 13:26
PCB-1254 (Arodor 1254)
ug/L
ND
0.50
0.50
12/07/16 13:26
PCB-1260 (Arodor 1260)
ug/L
ND
0.50
0.50
12/07/16 13:26
Toxaphene
ug/L
NO
0.50
0.50
12107/1613:26
Decachlorobiphenyl (S)
%
94
20-138
12107/1613:26
Tetrachloro-m-xylene (S)
%
93
20-110
12/0711613:26
LABORATORY CONTROL SAMPLE:
1879NO
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
4,4'-DDD
ug/L
.25
0.22
90
31-141
4,4'-DDE
ug/L
.25
0.20
82
30-145
4,4'-DDT
ug/L
.25
0.19
79
25-160
Aldrin
ug/L
.25
0.18
73
42-122
alpha-BHC
ug1L
.25
0.24
97
37-134
beta-BHC
ug/L
.25
0.23
95
17-147
delta-BHC
uglL
.25
0.24
98
19-140
Dieldrin
ug/L
.25
0.21
85
36-146
Endosulfan I
ug/L
.25
0.23
92
45-153
auufti prparUd an itch papp are in do un to inCicaad by the 'UrdW cahnm v=W where an of erne unh is pnnarRad to the right of the rem%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced: except in fuB,
Date: 12/09/2016 03:39 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 40

I
A IQf ca
www.pacpfafrscom
Pace A wb'bcal Services, LLC
205 East Meadow Road - Suite A
Eden, NC 272BS
[phone]
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
LABORATORY CONTROL SAMPLE: 1879680
Parameter
Units
Endosulfan II
ug/L
Endosulfan sulfate
ug/L
Endrin
ug/L
Endrin aldehyde
ug/L
gamma-BHC (Undane)
ug/L
Heptachlor
u91L
Heptachlor epoxide
ug/L
Decachlon26iphenyl (S)
%
Tetrachkxo-m-xylene (S)
%
QUALITY CONTROL DATA
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
.25
0.23
93
1-202
.25
0.23
93
26-144
.25
0.23
93
30-147
.25
0.19
76
50-150
.25
0.24
96
32-127
.25
0.20
83
34-111
.25
0.23
91
41-126
74
20-138
95
20-110
Qualifiers
Resufts pr-d on ads pqe are in the urdts hvDcaWd by the "%JrdM columm axapt where an a4e nwo urdt is tuesarrted to tir rW a4f the result
REPORT OF LABORATORY ANALYSIS
This report shall not the reproduced, except in full.
Date: 12/09/2016 03:39 PM mumtrt the written Consent of Pace Anatocal Services, LLC.
Page 23 of 40

e
aceAnalyh'cal
wwpecalabacan
Pace AnalyHeal Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]-
QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
QC Batch: 338743 Analysis Method: EPA 625
QC Batch Method: EPA625 Analysis Description: 625 MSS
Associated Lab Samples: 92321165001, 92321165002, 92321165003
METHOD BLANK: 1878200 Matrix: Water
Associated Lab Samples: 92321165001, 92321165002, 92321165003
Blank Reporting
Parameter Units Result Limit MDL
1,2,4-Trichlorobe.nzene
2,2'-Oxybis(1-chloropropane)
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-DinIVotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Nitrophenol
3,T-Dichlorobenzidine
4,6-Dinitro-2-methylphenol
4-Bromophenylphenyl ether
4-Chiaro-3-methylphenol
4-Chlorophenylphenyl ether
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)peryiene
Benzo(k)ffuoranthene
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di n octylphthalate
Dibenz(a,h )anthracene
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1 ,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
uglL
U91L
ug/L
ug/L
uglL
ug/L
ug/L
ug/L
ug1L
uglL
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug1L
ug1L
uglL
ug/L
ug/L
ug/L
ug1L
ug/L
ug1L
ug/L
uglL
ug1L
ug/L
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
ND
NO
ND
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
-6-.6
5.0
10.0
5.0
10.0
50.0
5.0
5.0
5.0
5.0
5.0
25.0
20.0
5.0
5.0
5.0
50.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
5.0
0.98
0.95
1.3
1.7
1.2
9.0
0.90
0.98
0.98
1.3
0.91
2.1
2.6
0.82
3.7
0.87
4.1
025
0.21
0.14
0.33
0.30
0.28
0.38
0.43
0.92
1.0
0.79
0.79
0.21
0,75
0,66
0.55
0.58
0.76
0.21
0.21
0.94
0.72
0.88
1.1
Analyzed Qualifiers
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30Y16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11 /30116 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11 /30116 20:57
11/30/16 20.57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11/30/16 20:57
11130116 20:57
11/30/16 20:57
Rawlrs pr i on this page am In the emks indicated by the "Urdu" odumn wwqA where an s wdt is presented to the right of the rosuM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12IM016 03:39 PM without the written comae of Pace Analytical Services, LLC, Page 24 of 40

aceAna"cal -
e++W4%xeiebs.am
Pace AnefytEcal Servk:gm LLC
205 last Meadow Road - Sulta A
Eden. NC 27288
[phone]
QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
METHOD BLANK 1878200 Matrix: Water
Associated Lab Samples: 92321165001, 92321165002, 92321165003
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
Indeno(1,2,3-cd)pyrene
ug/L
NO
5.0
0.29
11/30/16 20:57
Isophorone
ug/L
ND
10.0
0.89
11/30/16 20:57
N-Nitroso-di-n-propylamine
ug/L
NO
5.0
0.99
11/30/16 200:57
N-Nilrosodimethylamine
11911-
NO
5.0
0.91
11/30/16 20:57
N-NibxmWiphenylamine
ug/L
NO
10.0
1.0
11/30/16 20:57
Naphthalene
ug/L
NO
5.0
0.34
11/30/16 20:57
Nitrobenzene
ug/L
NO
5.0
1.1
111=16 20:57
Pentachlorophenol
ug/L
NO
10.0
4.6
11/30/16 20:57
Phenanthrene
ug/L
ND
5.0
0.22
11/30/16 20:57
Phenol
11911-
NO
5.0
1.9
11/30/16 20:57
Pyrene
ug/L
NO
5.0
0.19
11/30/16 20:57
2,4.6-Tribromophenol (S)
%
79
10-137
11/30/16 20:57
2-Fluorobiphenyl (S)
%
63
15-120
11/30/16 20:57
2-Fluorophenol (S)
%
42
10-120
11/30/16 20:57
Nitrobenzene-d5 (S)
%
70
10-120
11 /30116 20:57
Phenol-d6 (S)
%
32
10-120
11/30/16 20:57
Terphenyl- d14 (S)
%
85
11-131
11/30/16 20:57
Qualifiers
LABORATORY CONTROL SAMPLE:
1878201
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Roe
Limits Qualifiers
1,2.4-Trichlorobenzene
ug/L
50
28.8
58
44-142
2,2'-Oxybis(i-chloropropane)
ug1L
50
34.2
68
36-166
2,4,6-Trichlorophenol
ug/L
50
46.4
93
37-144
2,4-Mchlorophenol
ug/L
50
38.9
78
1-191
2,4-Dimethylphenol
ug/L
50
36.4
73
32-119
2,4-Dinitrophenol
ug/L
250
125
50
1-181
2,4-Dinhrotoluene
ug/L
50
42.9
86
39-139
2,6-Dinitrotoluene
ug/L
50
43.2
86
50-158
2-Ctdoronaphthalene
ug/L
50
39.9
80
60-118
2-Chlorophenol
ug/L
50
35.7
71
•23-134
2-Nftphenol
ug/L
50
34.4
69
29-182
3,3'-DicNorobenzidine
ug/L
100
74.2
74
1-262
4,6-Dinitro-2-methyiphenol
ug/L
100
70.8
71
1-181
4-Bromophenylphenyl ether
ug/L
50
36.0
72
53-127
4-Chioro-3-methylphenol
ug/L
100
75.8
76
22-147
4-Chlorophenylphenyl ether
u911-
50
41.4
83
25-158
4-Nitrophenol
ug1L
250
105
42
1-132
Acenaphthene
ug/L
50
42.0
84
47-M
Acenaphthylene
ug/L
50
41.0
82
33-145
Anthracene
ug/L
50
37.1
74
1-166
Benzo(a)anthracene
ug/L
50
37.3
75
33-143
Benzo(a)pyrene
ug/L
50
39.3
79
17-163
Benzo(b)tluoranthene
ug/L
50
39.2
78
24-159
Results presented on tMa page are In thr uru"is Indicated by the 'Units" coharm except where an atterrrata unit is to the right or hire result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 03:39 PM without the written consent of Pace Anatybeal Services, LLC, Page 25 of 40

aceAnalytical,
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Pecs Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, I4C 27288
[phone]
QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
LABORATORY CONTROL SAMPLE: 1878201
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Benzo(g,h J)perylene
ug/L
50
38.7
77
1-219
Benzo(k)fluoranthene
ug/L
50
40.2
80
11-162
bis(2-Chioroethoxy)methane
ugfL
50
34.0
68
33-184
bis(2-Chloroethyl) ether
ug/L
50
33.8
68
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
34.9
70
8-158
8uc, banzylphthalate
ug;'L
50---------
W.-5
73
1-152
Chrysene
ug/L
50
38.0
76
17-168
Di-n-butylphtitalate
ug/L
50
40.8
82
1-118
Di{t-0c.-tylphthalate
ug/L
50
37.0
74
4-146
Dibenz(a,h)anthracene
uy/L
50
40.5
81
1-227
Diethylphthalate
ug/L
50
47.4
95
1-114
Dimethylphthalate
ug/L
50
45.1
90
1-112
Fluoranthene
ug/L
50
39.9
80
26-137
Fluorene
ug/L
50
42.3
85
59-121
Hexachloro-1,3�utadiene
ug/L
50
25.1
50
24-116
Hexachlorobenzene
ug1L
50
38.1
76
1-152
Hexachlorocyciopentodiene
ug1L
50
26.4
53
25-150
Hexachloroethane
ug/L
50
24.3
49
40-113
Indeno(1,2,3-od)pyrene
ug/L
50
39.9
80
1-171
Isophorone
ug/L
50
35.7
71
21-196
N-Nftso-di n-propylamine
ug/L
50
40.8
82
1-230
N-titrosodirnethylamine
ug1L
50
22.4
45
25-150
N-Nitrosodiphenylamine
ug1L
50
39.6
79
25-150
Naphthalene
ug/L
50
30.7
61
21-133
Nitrobenzene
ug/L
50
33.1
66
35-180
Pentachlorophenol
ug/L
100
81.1
81
14-176
Phenanthrene
ug/L
50
37.2
74
54-120
Phenol
ug/L
50
18.3
37
5-112
Pyrene
ug/L
50
35.2
70
52-115
2,4,6-Tribmmophenol (S)
%
79
10-137
2-Fluorobiphenyl (S)
%
82
15-120
2-Fluorophenoi (S)
%
43
10-120
Nib-obanzene-d5 (S)
%
69
10-120
Phenol-d6 (S)
%
33
10-120
Terphenyl-dl4 (S)
%
76
11-131
MATRIX SPIKE SAMPLE:
1878202
92321165002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
12,4-Trichlorobenzene
ug/L
ND
50
17.9
36
44-142 M1
2,2'-Oxybis(1-chloropropane)
ug/L
ND
50
21.1
42
36-166
2,4,6-Trichlorophenol
ug/L
ND
50
26.4
53
37-144
2,4-Dichlorophenol
ug/L
ND
50
22A
45
1-191
2,4-Dimethylphenoi
ug/L
ND
50
22.6
45
32-119
2,4-Dinitrophenol
ug/L
ND
250
85.2
34
1-181
Results presented on Cris page are In the units Eradicated by the 'UNrs' cakunn I where an afternate unit is presented to the right of On resutt
REPORT OF LABORATORY ANALYSIS
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Date: 12/0912016 03:39 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 40

aceAnalyb►cal'
Pace Anatytiaat Services, LLC
205 Fast Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
MATRIX SPIKE SAMPLE:
Parameter
1878202
Units
92321165002
Result
Spike
Conn
MS
Result
MS
% Rec
% Rec
Limits Clualifiers
2,4-Dinitrotoluene
ug1L
ND
50
26.5
53
39-139
2,6-Dinitrotoluene
ug1L
ND
50
26.0
52
50-158
2-Chkrronaphthalene
uglL
NO
50
24.0
48
60-118 MS
2-Ghlorophenol
ug/L
ND
50
22.1
44
23-134
2-Nitrophenol
ugfL
ND
50
20.5
41
29-182
3,3'-Dichlorobenzidine
ug1L
ND
100
36.9
37
1-262
4,6-Dinitro-2-methylphenol
ug/L
NO
100
48.0
48
1-181
4-Bromophenylphenyl ether
uglL
NO
50
22.6
45
53-127 M1
4-Chloro-3-methytphenol
ugfL
NO
100
46.9
47
22-147
4-Chlorophenylphenyl ether
ug .
NO
50
24.7
49
25-158
4-Nitrophenol
uglL
ND
250
70.2
28
1-132
Acenaphthene
ug1L
NO
50
25.6
51
47-145
Acenaphthylene
ug/L
NO
50
24.8
50
33-145
Anthracene
ug1L
NO
50
24.9
50
1-166
Benzo(a)anthracene
ug/L
ND
50
24.5
49
33-143
Benzo(a)pyrene
ug/L
NO
50
25.4
51
17-163
Benzo(b)fluoranthene
ug/L
NO
50
24.8
50
24-159
Benzo(g,hj)perylene
ug/L
NO
50
24.6
49
1-219
Benzo(k)tluoranthene
ugA-
NO
50
26.2
52
11-162
bis(2-Chloroethoxy)methane
ug/L
NO
50
19.8
40
33-184
bis(2-Chlaroethyl) ether
ug/L
NO
50
20.9
42
12-158
bis(2-Ethylhexyl)phthalate
ug/L
NO
50
22.4
45
8-158
Butylbenzylphthalate
ug1L
NO
50
23.5
47
1-152
Chrysene
uglL
NO
50
25.4
51
17-168
Dk"utylphthalate
ug1L
NO
50
27.0
54
1-118
Di-n-0ctylphthatate
ug/L
NO
50
23.4
47
4-146
Dibenz(a,h)anthraoene
uglL
ND
50
26.0
52
1-227
Diethylphthalate
u911-
NO
50
29.9
60
1-114
Dimethylphthalate
ugfL
NO
50
27.5
55
1-112
Fluoranthene
ugfL
NO
50
26.4
53
26-137
Fluorene
u91L
NO
50
25.6
51
59-121 M1
Hexachlonr1,3-butodiene
ugfL
NO
50
16.0
32
24-116
Hexachkxobenzene
ugfL
NO
50
25.6
51
1-152
Hexachlorocyciopentadiene
ug/L
NO
50
17.0
34
25-150
Hexachloroethane
u91L
NO
50
15.2
30
40-113 M1
Indeno(1,2,3-od)pyrene
u91L
ND
50
25.9
52
1-171
lsophorone
ugfL
ND
50
20.7
41
21-196
N-Nitroso-dki-propytamine
ug/L
NO
50
26.3
53
1-230
N-Nitrosodimethylamine
ug/L
NO
50
14.2
28
25-150
N-Nitrosodiphenylamine
ug/L
ND
50
26.2
52
25-150
Naphthalene
ug/L
ND
50
19.5
39
21-133
Nitrobenzene
ug/L
NO
50
20.2
40
35-180
Pentachlo ophenol
ug/L
NO
100
52.7
53
14-176
Phenanthrene
uglL
NO
50
25.4
51
54-120 M1
Phenol
ug/L
NO
50
11.7
23
5-112
Pyrene
ug/L
NO
50
22.8
46
52-115 M1
2,4,6-Tribromophenol (S)
%
50
10-137
Rasuf s prasarKad on
this paps am in the units Endicabrd by tM'UnW eabarm rooeeI *trors an ab '. unit Is
praserrted to dw right of ilia result
REPORT OF LABORATORY ANALYSIS
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,�aceAnalyfical
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QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
MATRIX SPIKE SAMPLE: 1878202
92321165002 Spike MS MS
Parameter Units Result Conc. Result % Rec
Pace Anafytical Servlcsa, LLC
205 East Meadow Road - Suite A
Eden, AC 27288
[phone]-
% Rec
Limits Qualifiers
2-Fluorobiphenyl (S)
%
49
15-120
2-Fluorophenol (S)
%
26
10-120
Nitrobenzene-d5 (S)
%
40
10-120
Phenol-d6 (S)
%
21
10-120
Terphenyl-d14 (S)
%
47
11-131
SAMPLE DUPLICATE: 1878203
92321165003
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
1,2,4-Trichforobenzene
ug/L
ND
NO
30
2,2'-Oxybis(1-chloropropane)
ug/L
NO
NO
30
2,4,6-Trichlorophenol
ug/L
NO
NO
30
2,4-Dichlorophenol
ug/L
NO
NO
30
2,4-Dimethylphenol
ug/L
NO
NO
30
2,4-Dinitrophenol
ug/L
NO
NO
30
2,4-Dinitratoluene
ug/L
NO
NO
30
2,6-Dinitrotofuene
ug/L
NO
NO
30
2-Chloronaphthalene
ug/L
NO
NO
30
2-Chlorophenol
ug/L
NO
ND
30
2-Nitrophenol
ug/L
NO
NO
30
3,3'-Dichlombenzidine
ug/L
NO
ND
30
4,6-Diniiro-2-methylphenol
ug/L
NO
NO
30
4-Bromophenyfphenyl ether
ug/L
NO
NO
30
4-Chloro-3-methylphenol
ug1L
ND
NO
30
4-Chiorophenylphenyl ether
ug[L
NO
NO
30
4-Nitrophenol
ug/L
NO
NO
30
Acenaphthene
ug/L
NO
NO
30
Acenaphthylene
ug/L
NO
NO
30
Anthraoene
ug/L
ND
NO
30
Benzo(a)anthraoene
ug/L
ND
NO
30
Benzo(a)pyrene
ug/L
NO
NO
30
Benzo(b)fluoranthene
ug/L
NO
NO
30
Benzo(g.h,i)perylene
ug/L
NO
NO
30
Benzo(b)fluoranthene
ug/L
NO
NO
30
bis(2-Chloroethoxy)methane
ug/L
NO
NO
30
bis(2-Chloroethyl) ether
UPI
NO
ND
30
bis(2-Ethylhexyl)phthalate
ug/L
ND
NO
30
Butyfbenzylphthalate
ug/L
NO
NO
30
Chrysene
ug/L
NO
NO
30
Di-n-butylphthalate
ug/L
NO
ND
30
Di-n-oc tylphthalate
ug/L
NO
NO
30
Diberiz(a,h)anthracene
ug/L
NO
NO
30
Diethylphthalate
ug/L
NO
NO
30
Dimethylphthalate
ug1L
NO
NO
30
Fluoranthene
ug/L
NO
NO
30
Rssu is prsseon tha pWe am In the unift Indicated by ttw -UnW eA, I1.1m an afternaea unit is pres•rdad to the rigtrt of the rawtL
REPORT OF LABORATORY ANALYSIS
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Date: _12/09/2016 03:39 PM wittmut the written consent of Pace Analytical Services, LLC. Page 28 of 40

QUALITY CONTROL DATA
Project: 2016 SEMI-ANNUAL
Pace ProjectNo.: 92321 M
SAMPLE DUPLICATE: 1878203
Parameter
Units
92321165003
Result
Dup
Result
RPD
Fluorene
ug/L
ND
ND
Hexadtloro-1,34utadiene
ug/L
ND
ND
Hexachlorobenzene
ug/L
ND
ND
Hexachlor+ocydopentadiene
ug/L
ND
ND
Hexachloroethane
ug/L
ND
ND
Indeno(1,2,3--W)pyrene
ug/L
ND
ND
Isophorone
ug/L
ND
ND
N-Nitroso-di n-propylamine
uglL
ND
ND
N-Nitrosodimethylamine
ug/L
ND
ND
N-Nibusodiphenylamine
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
Nitrobenzene
ug/L
ND
ND
Pentachlorophenol
uglL
ND
ND
Phenanthrene
ug/L
ND
ND
Phenol
ug/L
ND
ND
Pyrene
ug/L
ND
ND
2,4,6-Tribrornophenol (S)
%
46
50
9
2-Fluorobiphenyl (S)
%
42
51
19
2-Muorophenol (S)
%
21
25 •
21
Nitrobenzene-d5 (S)
%
35
44
24
Phenol-d6 (S)
%
14
18
23
Terphenyl-dl4 (S)
%
51
47
9
Paco Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
(336)6238921
Max
RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Resuas preser I on ads pap. am to a,a un is tndicalad by the vats' calurrm ecospt -Im in e0 1 urdt is pre nI to the Agra of the resulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 03:39 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 40

,�aceAnalyticai.
ewwwCOlabscaM
QUALITY CONTROL DATA
Project: 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Pace Anatyacal Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone] .
OC Batch: 338855 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92321165001, 92321165002, 92321165003
METHOD BLANK: 1879024 Matrix: Water
Associated Lab Samples: 92321165001, 92321165002, 92321165003
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 2.5 11/30/1618:03
LABORATORY CONTROL SAMPLE: 1879025
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 228 91 90-110
SAMPLE DUPLICATE: 1879026
92321256001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 350 283 21 5 D6
SAMPLE DUPLICATE: 1879027
92321149001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 55.5 56.0 1 5
Results prase»fad on tidy page are In the un is he hurled by the 'Units" cahuae except whoa an sheerest urdf Is presented to the right ofthe result
REPORT OF LABORATORY ANALYSIS
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Date: 12109/2016 03:39 PM without the written consent of Pace Analytical Services, LLC.
Page 30 of 40

aceAr�afyi�icale
Pace Analydeal SetrWM LLC
205 East Meadow Road - Suite A
Eden, NC 272a8
[phone]
QUALITY CONTROL DATA
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
QC Batch: 338719 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92321165001; 92321165002. 92321165003
SAMPLE DUPLICATE: 1878033
92321071001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
PH Std. Units 6.4 6.5 0 9 H6
SAMPLE DUPLICATE: 1878034
92321114001 Dup
Parameter Units Result Result
PH Std. Units 7.3 7.3
Max
RPD RPD Qualifiers
0 9 H6
7
Results pntsers'on this page am in the un is t WkWed by the "thdls' Cohn= 11w1we an alternate unit is preswftd to the rigtd of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/09/2016 03:39 PM without the written oonsent of Pace Analytical Services, LLC_
Page 31 of 40

,�aneAtWcal*
wwwps_com
r
QUALIFIERS
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot
ND - Not Detected at or above adjusted reporting limit
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL - Adjusted Method Detection Limit
PQL - Practical Quantitation Limit
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, AC 27288
[phone]-
RL - Reporting Limit
S - Surrogate
1,2-Dipheny1hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anew is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethytvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Aaylonitriie by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each anaiyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anatytes.
TNI - The NELAC Institute_
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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CEAnalytical
wwnpxtpn
Pace Ana"cal Services, LLC
21i5 East Meadow Road - Suite A
Eden, NC 27288
(336)62343921
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project 2016 SEMI-ANNUAL
Pace Project No.: 92321165
Analytical
Lab 10 -
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92321165001
OUTFALL 1
EPA 1664B
339287
92321165002
OUTFALL 2
EPA 1664E
339287
92321165003
OUTFALL 3
EPA 1664E
339287
9232116SO01
OUTFALL 1
EPA 3510
338979
EPA 608
339163
92321165002
OUTFALL 2
EPA 3510
338979
EPA 608
339163
92321165003
OUTFALL 3
EPA 3510
338979
EPA 608
339163
92321165001
OUTFALL 1
EPA 200.7
338679
EPA 200.7
338879
92321165002
OUTFALL 2
EPA 200.7
338679
EPA 200.7
338879
92321165003
OUTFALL 3
EPA 200.7
338679
EPA 200.7
338879
9232116=11.
OUTFALL 1
EPA 625
338743
EPA 625
338907
92321165002
OUTFALL•2
EPA 625
338743
EPA 625
338907
92321165003
OUTFALL 3
EPA 625
338743
EPA 625
338907
92321165001
OUTFALLi
EPA 624
338976
92321165002
OUTFALL 2
EPA 624
338976
92321165003
OUTFALL3
EPA 624
338976
92321165001
OUTFALL1
SM 2540D
338855
92321165002
OUTFALL2
SM 2540D
338855
92321165003
OUTFALL 3
SM 2540D
338855
92321165001
OUTFALL 1
EPA 9040
338719
92321165002
OUTFALL 2
EPA 9040
338719
92321165G03
OUTFALL 3
EPA 9040
338719
REPORT OF LABORATORY ANALYSIS
This reW shall not be reproduced. except in full,
Date: 12/09QO16 03:39 PM without the written consent of Pace Analytical Services, LLC.
Page 33 of 40

�eeArjal cal'
Laboratory receiving samples:
Asheville ❑ EdenO
twcument Name: Document Revised: Sept. 21, 2016
-Sample Condition Upon Receipt(SOUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.01 Pace Quality Office
Greenwood ❑ Huntersvilleo- Raleigh❑ Mechanicsville[]
Sample... .. Ghent Name: . Wp# : 9234165
ReceiptProject.
Courier. Fed Ex UPS ❑LISPS [flied -
❑ Commercial ❑Pace E]Other: L9232116S
Custody Seal Present? ❑Yes Q Seals Intact? E]Yes ❑No -
DaWlydtials Person Examining Contentx: F 1 '
Packing Material: ❑Bubble Wrap Qe6bble Bags []None ❑Other:
Thermometer.
❑ IR Gun 10-. Type otk Q�ClBfue ❑None des on ice, coding process has begun
�—
._Corcectson.l estora-�----[^�'�s Tc.: ::rra�ed (•.1-- T. BioiogicaiTmsUd Frroien7 ' Ll
Temp should be above freezijig to 61C
USDA Regulated Soil ( UN%A, water sample)
Did samples origlngfe in a quarantine zone within the United States. CA, NY, or SC (check maps)? Did samples originate from a foreign source (Intematfonaf
_C_ Ye_s ONO including Hawaii and Puerto Rico)? ❑Yes
' r•Ie.f.•MORt6JnitKeMR�/•
Chain of Custody Present?
NO
❑N/A
1.
Samples Arrived within Hold Time?
/
04,
No
[]N/A
2.
Short Hold Time 8gad
Isis <72 hr.)?
❑Yes
o
❑N/A
3.
Rush Turn Around Time Requested?
QYes
a
❑N/A
4.
Sufficient Volume?
No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
We'
fi7fns
[]No
rINa
❑N/A
FIN/A
6.
Containers Intact?
No
❑N/A
7.
Samples Field Filtered?
❑Yes
QNo
S. Note if sediment is visible in the dissolved container -
Sample Labels Match CDC?
OV6_,'
❑No
❑N/A
9.
-Includes Date/ ime/lo/Analysis Matrix: L' i
Headspace in VOA Vials (>5-6mm)?
❑Yes
o
❑N/A
10.
Trip Blank Present?
❑Yes
❑No
©K/R
11.
Trip Blank C Seals Present?
❑Yes
ONO
01"A
CLIENT NOTIRCATIONJRESOLUTION
Reid Data Required? ❑Yes []No
Person Contacted:
Comments/Sampie
Dlscrepa ncy:
Date/Time:
!!!
Project Manager SCURF Review: pate:
Project Manager SRF Review: Date: 1)j2�j
dote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina OEHNR Certification Office (i.e.
)ut of hold, Incorrect preservative, out of temp, Incorrect containers)
Page 34 of 40

Item#
SP4U-12S mL Plastic Unpreserved (N/A)(CI-)
BP3U-250 mL Plastic Unpreserved (N/A)
I BIRM-500 mL Plastic Unpreserved (N/A)
BP1U-1 liter Plastic Unpreserved IN/A)
BP3S-250 mL Plastic H2504 (pH < 2} (Cl-)
BP3N-LW mL plastic HNO3 (pH < 2)
BPSZ-250 mL Plastk ZN Acetate & NaOH (>9)
zz BP3t-250 mi. Plastic NaOH (pH > 12) (Cl-)
WGFU-Wide-mouthed Glass Jar Unpreserved
AGIU-1 liter Amber Unpreserved (N/A) (Cl-)
AG1H-1 liter Amber HCl (pH < 2)
A63U-250 mi. Amber Unpreserved (N/A) (Cl-)
AG15-1 liter Amber H2504 (pH < 2)
AG3S-250 ml. Amber H2SO4 (pH < 2)
zz. z A63A(DG3A)-250 mL Amber NH4CI (N/A)(CI-)
i M9H-40 mLVOA HCI (N/A)
VGBT-40 mL VOA Na2S203 (N/A)
V69U-40 mL VOA Unp (N/A)
DG9P-40 mi. VOA H3PO4 (N/A)
VOAK (B vials per klt)-503S kit (N/A)
V/GK (3 vials per kityVPH/Gas kit (N/A)
5PST-1ZS mL Sterile PlastiE(N/A — lab)
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BP3U-250 nI* Plastic Unpreserved (N/A)
BPZU-500 r L Plastic Unpreserved (N/A)
BP1U-1 liter Plastic Unpreserved (N/A)
BP33-250 nil. Plastic H2SO4 IpH < 2) (CI-)
BP3N-250 riIL plastic HNO3 (pH < 2)
BP3t-250 rill. Plastic 2N Acetate & NaOH (>9)
/X Ix IZ z z z z 8P3C-250 IL Plastic NaOH (pH > 12) ICI-)
WGFU-Wid II mouthed Glass jar Unpreserved
AG1U-11ite; Amber Unpreserved (N/A) (Cl-)
.-. AGIN-1 Iiteil Amber HCI (pH < 2)
A63U-250 TLAmber Unpreserved (N/A) (Cl-)
AG15-1 IlteriAmber H2SO4 (pH < 2)
A63s-250 n1l Amber H2SO4 (pH < 2)
zzzAGM(DG3 )-250 mL Amber NH4C1(N/A)(Ci-)
LtJ DG9H40 m i VOA HCI (N/A)
VG9T40 ml1 VOA Na2S203 (N/A)
V69U-40 m VOA Unp INN
DG9P-4p m VOA H3PO4 (N/A)
VOAK (6 vla s per kit)-5035 kit IN/A)
V/GK (3 Vial? per kit)-VPH/Gas kit IN/A)
SPST 125 m Sterile Plastic (N/A — lab)
SP2T-250 PIL Sterile Plastic (N/A— lab)
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BPSU-1 liter Plastic Unpreserved (N/A)
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WGFU-Wide-mouthed Glass jar Unpreserved
AG1U-1 IiterAmber Unpreserved (N/A) (CI-)
O„
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AGIR-1 liter Amber HCl (pH < 2)
S
AG3U-250 mL Amber Unpreserved (N/A) (CI-)
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A
V69T-40 rnL VOA Na25203 (N/A)
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VG91J-40 mLVOA Unp (N/A)
DGSP-40 ml VOA H3PO4 (N/A)
VOAK (5 vials per Mt)-5035 kit (N/A)
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n
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CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
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Charlo te, NC A
Charlotte -Douglas International
Weather History for KCLT - November, 2016
November
29
2016
View
Tuesday, November 29, 2016
Daily Weekly Monthly Custom
Temperature
Mean Temperature
Max Temperature
Min Temperature
Degree Days
Heating Degree Days
Month to date heating degree days
Since 1 July heating degree days
Cooling Degree Days
Actual
64 OF
68 OF
60 OF
1
343
418
0
e 9:46 AM EST on December 05, 2016 [GMT -0500'
Average
46 OF
58 OF
35 OF
19
412
618
0
Record
76 OF [20011
20 OF (19551

Month to dateChling degree days
Year to date cooling degree days
Growing Degree Days
Moisture
Dew Point
Average Humidity
Maximum Humidity
Minimum Humidity
Precipitation
Precipitation
Month to date precipitation
Year to date precipitation
Snow
Snow
Month to date snowfall
Since 1 July snowfall
Since 1 September snowfall
Snow Depth
Sea Level Pressure
Sea Level Pressure
Wind
Wind Speed
Max Wind Speed
Mav Al Oct Cnaarl
1
2190
12 (Base 50)
61°F
80
93
67
ifpq
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0.40 in
0.45
30.21
0.00 in
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0.0
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0.0
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14 mph (South)
30 mph
Q7 mnh
n
1513
0.12 in
3.03
38.27
0.00 in
Average
0.1
0.1
0.1
1.37 in [1963)
T in [1963)
Record

CHAIN-OF-C,—,,fODY I Analytical Request Document
The Chairs-ofCuslody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
VIM ElSimllrk-1
12331 Cownerce Station
Ll�-,TTTT �M 77TIPT-11 �1�
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CHAIN-OF-6, ODY ! Analytical Request Document
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CHAIN OF-&tODY I Analytical Request Document
The Chaln-of-Cuslody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
SOCUM A Section 8 Swab" C
RaqWmd CII@M hdonnation: — RequIred on: kwalce kdonottlon: Page: of
COMPW Soufiwro - tMIn AaB Report P S011,1122O.—V Aftedort tig"W 11ALLWES 2AZI 1-577 Zrz,
Addn=7 12331 Commerce Station Copy To: Comp" Name:
HuntersvItle, NC 28078
Address:
Email: W.g.mo0r&@wudwAm.wM
Pumhoso Ow" Al:
Pow Quote:
Phase; 704-370-OM Fax
Prof Nam: 2016 Semi -Annual
P— Project Manager: taylor.oullOpmaleba.cocn,
,Requested Duo Dow
propcit
POW PMRIS 6110-1
NC
MATRLX CODE
COLLECTED
FSresBTvatives
WSWodnMV Wow
YftK WY
WNW W" ww
Pnwud p
SAMPLE ID 6WO&M IL
START
END
09 M
Om chwacw per box. wpe AR WP
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Sample Ift he
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DATE
TIME
DATE
TIME
X
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PRINT Nam of aAMPLEFL'
$GNATURE of SAMPLER:
MATE Signed:

�Q
AIL 2 5 ZU16
CEWRDWR EC7lLES
ON
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG0300M
Date submittedyzlzzog,
CERTIFICATE OF COVERAG-Er O. NCG0,309 40 (P
FACILITY NAME S CV�M�It�lrNrl/lj 1/r f jib --
COUNTY
PERSON COLLECTING SAMPLES M
LABORATORY Lab Cert- it I? —
Comments on sa ple collection or analysis:
Mee .,vAetoltnY TAwmkors%wern
AC40 A61 CR adift4 fa 41, B10poi 06 4/3o/zIgo
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR Zto 1 '
SAMPLE PERIOD 07an-June ❑ July -Dec
or ❑ Manthlyl (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water supply ❑m
❑Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
n No discharge this period?"
_ Outfall No.
Date Sample
Collected r
(mo/dd/yr)
244hour rainfall
amount,
inches'
Total Suspended Solids
PH,
Standard units
Copper
Lead
Zinc
Non-Polar 08G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics 5
'Benchmmks --= >
_
100 6WL or 50 mg/0
6.0 — 9.0 _
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 nWL _
i riWL
Z
T s 6
o.
CA
0.011
0,do
0,037
0, Z3
PiM
k
is
/O• fy
5 • g7
6• OW&1
T, ably
99-657,
Y
'Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an On -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
`See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11;'for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit date: 11/1/2012-10/31/2017
0
swU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since Filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
_122,n es P . low
Name
/(Print name)
Tal Print title)
YO
ign ure) ate}
Note: Results must be reported in numerical format. Po not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L". where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note. if you report a sample value in excess of the benchmark you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. .
Part B: Vehicle Maintenance Area Monitoring Results: only forfacil'rties averaging > 55 gal of new oil per month.
❑ No discharge this periodiz
OutFall No.
pate Sample
Coed
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Non -polar O&G/TPH 1by'.
• .EPA MtA (SGT-HEM
Total Suspended Solids
pH
Benchmarks
15 mg/L
100 mg/L or 50 mg/L*
&0 — 9.0 SU ,
Footnotes from Part A also apply to this Part B
• See General Permit text, Table 5, Identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date:11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 2 of 3
0

Note: if you report a sample value in ercess of the benchmarlk, you must Implement Tier 1, Tler Z or Tkr 3 responses. See General permit text -
FOR PART A AND PART B MONITORING RESULTS: V`— I'
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.( �� P"T'T0�C"
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER PER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Moil an original and one copy of thisDM& in udinall "No D! in 30 dolff-of receint of the lob resuft tot n of wortitaring mriod
in the case of 'No Discharge"reaortsl to
Division of water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnet property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
• am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations'
aeZt=e2 10
(S' not re of Permittee( (Date)
Permit Date-11/1/2012-10/31/2017
0
SWU-24S, last revised 10/25/2012
Page 3 of 3

Routine Inspection Form
f t,e j ?n s fJecf���
711afzolF nc�wl S
•
Inspector Name:
Inspector Signature:
Weather Condition:
Description of any
Discharges:
Description of Control
Measures Needing
Repairs:
Stormwater Pollution Prevention Plan
SOUTHWIRE US Medium/High Voltage Cable
Huntersville, North Carolina
`. Inspection Nate
p1� and Time:
r C/fe-4 M2 r
Description of any Failed
Control Measures that
Need Replacement:
R 9S!
Description of Incidents
fi RQl� i
of Noncompliance
observed:
1 Jeie & C
16 Description of
Additional Control
Measures Needed to
Comply with Permit:
le55ew 91,v4f ci orea%�-S
."ir
L_ 4- -
Z✓aG
2�11 2. d.1 r
Indicate the conditions present in the following areas of concern by circling "Yes" or "No" in
response to each question. Explain all "No" responses and specify corrective action taken in the
space provided at the end of this checklist. if a particular question does not apply to your
facility, respond by circling "N/A".
rp �N �Iac.� �/rka•e
filet r rl-9-trc.w-e /zjefrrj NMerJS.
eayse c� do Se-&,Gt'
fnA d(a (L2lpas rn510j m4d3 twr!, A:�
L r `-
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C•�/��i/ %� [� �p So-v�rvrltG. I'�o �'i'i�L'12/IG�Kf�JDSvR-LS
�j fl�7c�c`QCc9fftQl/K qr1/� -i0 4

•
11
0
• Area of Concern
Inspection Questions
Response
Is area free of spills, leaks and debris?
YJA
No
N/A
Material Handling Area
Loading/Unloading
Have overall housekeeping measures
been checked?
�
No
N/A
Is area free of spills, leaks and debris?
No
N/A
Material Storage Area
Reel with Cable Staging
Have overall housekeeping measures
been checked?
llj�'
No
N/A
Is area free of spills, leaks and debris?
1W
No
N/A
Material Storage Area
Empty Reel Staging
Have overall housekeeping measures
been checked?
Xj�'
No
N/A
Is area free of spills, leaks and debris?
dr&§
No
N/A
Have overall housekeeping measures
been checked?
UR
No
N/A
Has the integrity been visually checked?
M
No
N/A
Material Storage Area
Is double walled tank shell in good
(1) — 2,000 gallon diesel tank
condition? (i.e. no gaps, cracks, or.
)ffiit
Noy
N/A
deterioration) _
..
Are spill response materials available?
OR
No
N/A
Is area free of spills, leaks and debris?
No
N/A
Have overall housekeeping measures
been checked?
f&m
No
N/A
Material Storage Area
Has the integrity been visually checked?
I+s
No
N/A
Fire Pump Building (1) — 300 gallon
diesel tank
Is double walled tank shell in good
condition? (i.e. no gaps, cracks, or
No
N/A
deterioration)
Are spill response materials available?
YQ
No
N/A
Is area free of spills, leaks and debris?
No
N/A
Material Storage Area
Have the integrity of the containers been
visually checked?
No
N/A
Is flooring of Lube Room in good
Lube Room (6) — 70 gallon
containers of oil
condition? (i.e. no gaps, cracks, or
No
N/A
deterioration)
Are spill response materials available?
)FA
No
N/A
Waste Handling/Storage Area
Wood Pallets
Qom/ � ,e Qt1Ow
is area free of spills, leaks and debris?
No
N/A
Have overall housekeeping measures
been checked?
�
No
N/A

Area of Concern
Inspection Questions
Response
Is area free of spills, leaks and debris?
Yes
No
N/A
Have overall housekeeping measures
Yes
No
N/A
Waste Handling/Storage Area
Dumpsteri>>
been checked?
2sCFu.E
Is the cover closed?
Yes
No
Is area free of spills, leaks and debris?
<M
No
N/A
Waste Handling/Storage Area
Have overall housekeeping measures
Open Tap Roil Offs
been checked?
Yap
No
N/A
Outfalls
Is area free of spills, leaks'and deb6?
VM
No
N/A
Are there signs of any erosion?
M�
1W
N/A
r">>
In the space provided below, explain all "No" responses and indicate specific corrective -
actions taken.
Source = .
�>G art f:
sua t Act�tlii_�tsgs;F
P02
+ vve-A
Ott Sc
7 /4 It .0
Signature of Spill Coordinator D to
W9
11
•

Ir
�, II I� 1114 Sidi'
"
J

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quali - General Permit No. NCG030000
Date submitted '2 z'0 /}
CERTIFICATE OF COVERAG No. NCG03f I 4.�-q -t SAMPLE COLLECTION YEAR E U 1 '�> —
FACILTTY NAME U - (A-4- SAMPLE PERIOD ❑ San -June Wuly-Dec
COUNTY e t V 1 4n- or ❑ Monthly' month
PERSON COLLECTING SAM.PL-I►J la7T`4- DLSCKARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY d&& LA- b5 Lab Cert. p 1 � _-1�11 f�ps� �� ❑Zero -flow []Water Supply m
) `R rY7"4,.�p
Comments on sample collection or analysis E36iherlow c e-/2z'P-/t CA-J N V"
PLEASE REMEMBER TO SIGN . PAGX2 AND/OR 3 4
Pan A: Stormwater Benchmarks and Monitoring Results
7 No dischorge this period??
Dutfall No.
Dal; Sample
Collertedr
.imol�/vri'
24-taut rainfall
anaum,
.1
Total Siapeaded Solids
PH.
Standard units.
COPP"
Lead
Tmt
Non -Polar D&G/
Total Petroleum
.4fydromrbons
TOWToxic
DrRnics
Bendrmorks = >
-
-
10o mg/L or 50 fiW ''
- 6 o = 9.o `
O.W7 mg/L
" 0.033 mg/L
0.057 mg/L
1s mg/L
1 mg/L
r,
,Q
10
A
rr
�I
-- �r
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfail.
] For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3 The total precipitation must be recorded using data from an on -site rain gauge. unattended sites may be eligible for a waiver of the rain gauge requirement.
`See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date:11/1/2012-10/31/2017
SWU-245, last reV[sed 10/25/2012
Page 1 of 3
A a-gsJ

AW
Facilities that incorporate a solvent management plan into the 5tormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived, The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this fadl'ity is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
I/-i(s LyIa-yi'-�
Title (Print title)
z z��
[ g ature) 7 ( ate}
Note: Results must be reported in numerical format. -Da not report Below Detection limit, BDL, <PRt, Nan -detect, ND, or other similar non -numerical
format. when results are below the applicable limits, they must be reported in -the format. "<XX mPJV where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L
Note: if you report a sample value in excess of the benchmark you must implement Tier 1, 77er 2, or nier 3 responses. See General permit tend.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
n No dischorae this period?'
Outfan No.
Date Sample
Collected'
(mo/dd/yr)
244hour rainfall
amount,
Inches
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Susperded Solids
pH
eenthmmks =>
-
15 mg/L
100 mg/L or 50 mg/L'
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
' See General Permit tent, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10125/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark you must implement Tler 1, TTer 2, or Tier 3 responses. See General Permft text
FOR PART A AND PART B MONITORING RESU
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIRIEMENTS. SEE PERMIT PART It SECTION B.
• 2 EKCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ Noff
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ f��
REGIONAL OFFICE CONTACT NAME:
Moil an oriaino and one uopv of this AMR including all 'No IDistharae' reports within 30 don of mcelpt of the lab results for of end of monftodna period
in the 2= of, Oft Discharae'reogrtsl to:
Division of Water quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
ajpawarg-that there areEignificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
re of Permittee) {Date)
Permit Date:11/1/2012-10/31/2D17
SWU-245, last revised 10/25/2012
Page 3 of 3

-1 r North Carolina Department of Environmental Quality
Pat McCrory Donald R. van der Vaart
Governor Secretary
Mr. Paul Ingle
Meritor Heavy Vehicle Systems, LLC
105 Wamsutta Mill Road
Morganton, NC 28655
Dear Mr. Ingle:
October 6, 2015
RECEIVED
OCT 0-8 2015
CENTRAL FILES
DWR SECTION
Subject: NPDES General Permit NCG030644
Meritor Heavy Vehicle Systems, LLC
Formerly Sypris Technologies, Inc.
Certificate of Coverage NCG030644
Burke County
Division personnel received your request to revise your stormwater permit Certificate of Coverage to
accurately reflect your new company and/or facility name.
Please find enclosed the revised Certificate of Coverage. The terms and conditions contained in the
General Permit remain unchanged and in full effect. This revised Certificate of Coverage is issued
under the requirements of North Carolina General Statutes 143-215.1 and the Memorandum of
Agreement between North Carolina and the U.S. Environmental Protection Agency.
If you have any questions or need further information, please contact the Stormwater Permitting
Program at [phone].
cc: Asheville Regional Office
Stormwater Permitting Program Files
Central Files
Sincerely,
P�
for Tracy E. Davis, P.E., CPM, Director
Division of Energy, Mineral and Land Resources
Division of Energy, Mineral, and Land Resources
Energy Section • Geological Survey Section • Land Quality Section
1612 Mail Service Center, Raleigh, North Carolina 27699-1612.919-707-9200 / FAX: [phone]
512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: http://portal.nodenr.o[gtw
An Equal Opportunity 1 Affirmative Action Employer — 50% Recycled 110% Post Consumer Paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030644
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Meritor Heavy Vehicle Systems, LLC
is hereby authorized to discharge stormwater from a facility located at:
Meritor Heavy Vehicle Systems, LLC
105 Wamsutta Mill Road
Morganton
Burke County
to receiving waters designated as Catawba River, a class WS-IV water in the Catawba River
Basin, in accordance with the effluent limitations, monitoring requirements, and other conditions
set forth in Parts I, II, III, and IV of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective October 6, 2015.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day October 6, 2015.
for Tracy E. Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission

I-
A&4�
*A
NCDENR
Erm11WMEM uio 1'iRYi/1L FKJaL t[e3
Division of Energy, Mineral & Land Resources
Land Quality SectionlStormwater Permitting
National Pollutant Discharge Elimination System
PERMIT NAMEIOWNERSHIP CHANGE FORM
FOR AGENCY USE ONLY
Date Received
Year
Month I
Day
1. Please enter the permit number for which the change is requested.
NPDES Permit (or) Certificate of Coverage
3 0 0 0 0 t 1 0 13 10 6 4 4
11. Permit status prior to requested change.
a. Permit issued to (company name): _ _ Sypris Technologies, Inc. _
b. Person legally responsible for permit: John A Rhyne
First Ml Last
Ehs Director
Title
101 Bullitt Lane, Suite 450
Permit Holder Mailing Address
Louisville KY 40222
City State Zip
[phone] 828439-8463
Phone Fax
c. Facility name (discharge): Sypris Technologies, Inc.
d. Facility address: 105 Wamsutta Mill Road
Address
Morganton NC 28655
y� City State ' Zip
e. Facility contact person: .,) t ,.� (� ) oZo2 19
First / Ml / Last Phone
IIl. Please provide the following for the requested change (revised permit).
a. Request for change is a result of: ® Change in ownership of the facility
❑ Name change of the facility or owner
If other please explain: Purchase of operations and lease of real estate
b. Permit issued to (company name): Meritor Heavy Vehicle Systems, LLC
c. Person legally responsible for permit: t7 V L _ Ingle
First MI Last
RECEIVED
SEE 2 3 2015
DENR-LAND QUALITY
STORMWNATER PERMITTING
d. Facility name (discharge):
e. Facility address:
f. Facility contact person:
Title
105 Wamsutta Mill Road
Permit Holder Mailing Address
Morganton NC 28655
City State Zip
8Z8) - 4 7 B9 L-'*t 1F A0al W • C00%
Phone E-mail Address
Meritor Heavy Vehicle Systems, LLC
105 Wamsutta Mill Road
Address
Morganton
NC 28655
City
State Zip
Robinson
First
Ml Last
(61S ) 7LY - g1,'44
c�ydt . 4d,+�Sr� a 44GO ib z •Colw%
Phone
E-mail Address
W. Permit contact information (if different from the person legally responsible for the permit)
Revised Jan. 27. 2014

NPDES PERMIT NAME/OWNERSHIP CHANGE FORM
Page 2 of 2
Permit contact: Robinson
First Nit Last
fAcl y 1~-d&"4e2
Title
105 Wamsutta Mill Road
Mailing Address
Morganton NC 28655
City State "Lip
(628 ) 7bV-1(1,Vq U-0K. Rol6w^�sa� I�x+r .cvM
Phone E-mail Address
V. Will the permitted facility -continue to conduct the same industrial activities conducted prior
to this ownership or name change?
® Yes
❑ No (please explain)
V1 Required Items: THIS APPLICATION WILL BE RETURNED UNPROCESSED IF ITEMS
ARE INCOMPLETE OR MISSING:
❑ This completed application is required for both name change and/or ownership change
requests.
❑ Legal documentation of the transfer of ownership (such as relevant pages of a contract deed,
or a bill of sale) is rewired for an ownership change request. Articles of incorporation are
not sufficient for an ownership change.
The certifications below must be completed and signed by both the permit holder prior to the change, and
the new applicant in the case of an ownership change request. For a name change request, the signed
Applicant's Certification is sufficient.
PERMITTEE CERTIFICATION (Permit holder prior to ownership change):
1, John A. Rh ne, attest that this application for a name/ownership change has been reviewed and is
accurate Ad complete to the best of my knowledge. I understand that if all required parts of this
applikati r� are not completed and that if all required supporting information is not included, this application
returned �A incomplete.
Signature
CERTIFICATION
2 ao
ate
1, o.- y attest that this application for a name/ownership change has been reviewed and is accurate and
comple to the best of my knowledge. I understand that if all required parts of this application are not
complet d and that if all required supporting information is not included, this application package will be
returned as incomplete.
T Q•
Signature
9- 1G-1S
Date
PLEASE SEND THE COMPLETE APPLICATION PACKAGE TO:
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
Revised Jan. 27, 2014

i,
�l.
BILL OF SALE AND ASSIGNMENT AND ASSUMPTION AGREEMENT
BILL OF SALE AND ASSIGNMENT AND ASSUMPTION AGREEMENT, made and
entered into as of July 9, 2015 (this "Bill of Sale"), by and between Meritor Heavy Vehicle
Systems, LLC, a Delaware limited liability company ("Buyer"), and Sypris Solutions, Inc., a
Delaware corporation ("Sypris"), Sypris Technologies, Inc., a Delaware corporation ("Sypris
Technologies"), and Sypris Technologies Kenton, Inc., a Delaware corporation ("Sypris
Kenton") (each of Sypris, Sypris Technologies and Sypris Kenton are sometimes herein referred
to individually as a "Seller" and collectively as "Sellers").
RECITALS
A. Sypris and Buyer have entered into an Asset Purchase Agreement dated as of July 9,
2015 (the "Asset Purchase Agreement") pursuant to which Sypris agreed to sell, and to cause the
other Sellers to sell, the Assets, and Buyer agreed to assume the Assumed Liabilities.
Capitalized terms used herein but not defined herein shall have the meanings given to such terms
in the Asset Purchase Agreement.
B. Sellers desire to sell, assign, transfer, convey and deliver the Assets to Buyer, and Buyer
desires to purchase and acquire the Assets.
C. Buyer desires to assume and Sellers desire to transfer to Buyer the Assumed Liabilities.
NOW, THEREFORE, in consideration of the premises and for other good and valuable
consideration, the receipt and sufficiency of which are hereby acknowledged by each of the
parties hereto, Sellers and Buyer hereby agree as follows:
1. Sellers hereby sell, assign, transfer, convey and deliver to Buyer, free and clear of
all Liens other than Permitted Liens, and Buyer hereby purchases, acquires and accepts from
Sellers, all of the right, title and interest of Sellers in and to the Assets.
2. Buyer hereby assumes and undertakes to pay, perform and discharge, the
Assumed Liabilities.
3. The provisions of Section 2.2 of the Asset Purchase Agreement are incorporated
herein by reference; provided, however, that upon receipt of a consent to the assignment of any
Contracts or Permits of a Seller included in the Assets after the date hereof, this Bill of Sale shall
automatically sell, assign, transfer, convey and deliver such Contract or Permit to Buyer without
the requirement of any further instrument executed by or action taken by any Seller.
4. Nothing in this Bill of Sale, express or implied, is intended or shall be intended to
confer upon or give to any person, firm, entity or corporation other than Sellers, Buyer and their
respective successors and permitted assigns, any remedy or claim under or by reason of this Bill
of Sale or any term, covenant or condition hereof, and all of the terms, covenants and conditions,
promises and agreements in this Bill of Sale contained shall be for the sole and exclusive benefit
of the parties hereto and their successors and permitted assigns.

5. To the extent any provisions of this Bill of Sale are inconsistent with the Asset
Purchase Agreement, the provisions of the Asset Purchase Agreement shall control.
6. This Bill of Sale shall be construed and interpreted according to the laws of the
State of Michigan, excluding any choice of law rules that may direct the application of the Laws
of another jurisdiction.
7_ This Bill of Sale shall be binding upon and inure to the benefit of Sellers and
Buyer and their respective successors and permitted assigns.
8. This Bill of Sale may be executed in separate counterparts, each such counterpart
being deemed to be an original instrument, and all such counterparts will together constitute the
same instrument.
[Signature page follows]
-2-

IN WITNESS WHEREOF, the parties hereto have caused this Bill of Sale to be executed
by their respective duly authorized officers as of the date first above written.
MERITOR HEAVY VEHICLE SYSTEMS,
LLC
By: P
Name: Rpd S
Title:
SYPRIS SOLUTIONS, INC.
By:_
Name:
Title:
SYPRIS TECHNOLOGIES, INC.
By:_
Name:
Title:
SYPRIS TECHNOLOGIES KENTON, INC.
BY:.._.
Name:
Title:
[Signature Page to Bill of Sale and Assignment and Assumption Agreement]

IN WITNESS WHEREOF, the parties hereto have caused this Bill of Sale to be executed
by their respective duly authorized officers as of the date first above written.
MERITOR HEAVY VEHICLE SYSTEMS,
LLC
By:_
Naive:
Title:
SYPRIS SOLUTIONS, INC.
By:
Name:
Title:
SYPRIS TECHNOLOGIES, INC.
By:
Name:
Title:
SYPRIS TECHNOLOGIES KENTON, INC.
By:
Name:
Title:
[Signature Page to Bill of Sale and Assignment and Assumption Agreement]

CONFIDENTIAL
ASSET PURCHASE AGREEMENT
by and between
EXECUTION COPY
MERITOR HEAVY VEHICLE SYSTEMS, LLC
and
SYPRIS SOLUTIONS, INC.
Dated as of July 9, 2015
CPAM: 7853833.14

TABLE OF CONTENTS
Page
ARTICLE 1 DEFINITIONS.........................................................................................I
ARTICLE II SALE AND PURCHASE OF ASSETS..................................................I
Section 2.1. Sale and Purchase of Assets ............................ .............I
Section 2.2. Non-Assignabie Contracts and Permits........................................3
ARTICLE III ASSUMPTION OF LIABILITIES..........................................................4
Section 3.1. Assumed Liabilities......................................................................4
Section 3.2. Retained Liabilities......................................................................5
ARTICLE IV PURCHASE PRICE ..................
Section 4.1. Purchase Price ................
5
5
ARTICLEV CLOSING................................................................................................9
Section5.1. Closing ..................................................... .............9
Section 5.2. Closing Deliveries of Seller.........................................................9
Section 5.3. Closing Deliveries of Buyer ............................................
Section 5.4. Transfer Taxes............................................................................10
ARTICLE VI REPRESENTATIONS AND WARRANTIES OF SELLER................10
Section 6.1.
Organization...............................................................................10
Section6.2.
Authority...............................................•----............
Section6.3.
No Breach...................................................................................I 1
Section6.4.
Taxes..........................................................................................
i l
Section 6.5.
Proprietary Rights......................................................................12
Section 6.6.
Assets and Properties.................................................................13
Section6.7.
Litigation....................................................................................16
Section 6.8.
Environmental Matters...............................................................16
Section 6.9.
Governmental Approvals...........................................................17
Section 6.10.
Compliance With Applicable Law.............................................17
Section 6.11.
Employees Matters.....................................................................18
Section 6.12.
Sufficiency of Assets..................................................................20
Section 6.13.
Absence of Material Adverse Effect and Certain Changes or
Events.........................................................................................20
Section6.14.
Contracts.....................................................................................20
Section 6.15.
Financial Information.................................................................21
Section6.16.
No Brokers.................................................................................22
ARTICLE VII REPRESENTATIONS AND WARRANTIES OF BUYER.................22
Section7.1. Organization.............................................................•.................22
Section7.2. Authority......................................................................... ..22
CPAM: 7953833.14

(f) the purchase orders with USM set forth on Schedule 2.1(f) (the "USM
Purchase Orders");
(g) all assignable (after both parties have complied with their obligations
under Section 2.2 to facilitate such assignment) rights under licenses or other agreements
that are necessary for the continued operation of the Business (excluding only those
software licenses listed in item lb of Schedule A to the Transition Agreement (other than
the software licenses listed in item 15 of Schedule A to the Transition Agreement which
are contemplated to be transferred to Buyer)), including those referenced in Section
2.1(c) and those set forth on Schedule 2.1(g) (the "Business Contracts"); provided,
however, that the parties acknowledge such rights shall not be deemed "necessary" to the
extent that practical alternative sources of supply are reasonably available on a timely
basis under the circumstances (it being understood that nothing herein will limit Buyer's
rights under the Transition Agreement);
(h) all rights under Permits (to the extent transferable) that relate to the
Business, including those set forth in Schedule 2.1(h);
(i) except to the extent based upon, arising out of, relating to or caused by
any Excluded Asset or Excluded Liability (or otherwise subject to indemnification by
Seller or Seller Subsidiaries or their Affiliates) and then solely to the extent that Seller is
not fulfilling any of its indemnification obligations with respect thereto, those causes of
action, claims, rights under express or implied warranties, guarantees, indemnities and
similar rights in favor of Seller and/or any Seller Subsidiary, rights of recovery, rights of
set-off, rights of subrogation and all other rights and demands of any nature available to
Seller and/or any Seller Subsidiary to the extent related to the Assets or the Business;
0) the benefits of coverage provided by insurance policies of Seller and
the Seller Subsidiaries (with respect to the Business or the Assets) in respect of matters
occurring on or prior to the Closing Date to the extent set forth in Section 8.7; and
(k) all books and records that are reasonably required to operate the
Business and other books and records as may be mutually agreed by the parties acting
reasonably and in good faith.
The assets, properties and rights of Seller and the Seller Subsidiaries to be
sold, assigned, conveyed, transferred and delivered to Buyer pursuant to this Agreement
are herein collectively referred to as the "Assets".
Section 2.2. Non -Assignable Contracts and Permits. Anything contained
herein to the contrary notwithstanding, this Agreement will not constitute an assignment,
an attempted assignment or an agreement to assign any Contract (or rights thereunder) or
3
CPAM: 7853833.14

Permit (or rights thereunder) if an assignment or attempted assignment of the same
without the Consent of any other party or parties thereto would constitute a breach
thereof or in any way impair the rights of Seller, any Seller Subsidiary or Buyer
thereunder. If any such Consent is not obtained or if an attempted assignment would be
ineffective or would impair Seller's, any Seller Subsidiary's or Buyer's rights under any
such Contract or Permit so that Buyer would not receive all such rights, then Seller will,
and will cause each Seller Subsidiary to, and Buyer will use its commercially reasonable
efforts to cause the full benefits of any such Contract (or rights thereunder) or Permit (or
rights thereunder) to be provided to Buyer in the most cost-effective and practical manner
available under the circumstances. In addition, Seller will, and will cause each Seller
Subsidiary to, take such other actions (at Seller's reasonable expense) as may reasonably
be requested by Buyer in order to place Buyer, insofar as reasonably possible, in the same
position as if such Contract (or rights thereunder) or Permit (or rights thereunder) had
been transferred as contemplated hereby and so that all the benefits relating thereto shall
inure to Buyer. Notwithstanding the foregoing, if any such Consent is not obtained prior
to the Closing, Seller will continue to use and will cause each Seller Subsidiary to
continue to use, and Buyer will use, its commercially reasonable efforts (at Seller's
reasonable expense) to obtain all such Consents (and, if and when such Consents are
obtained, the transfer of the applicable Contract (or rights thereunder) or Permit (or rights
thereunder) will be effected in accordance with the terms of this Agreement). The parties
agree that if such Consents relate to Contracts that are necessary for the continued
operation of the machinery and equipment at the Morganton Facility or Permits that are
necessary for the continued operation of the plant, machinery and equipment at the
Morganton Facility, Seller shall be responsible for all expenses incurred in obtaining'such
Consent pursuant to this Section 2.2. The parties further agree that if such Consents
relate to other Contracts or Permits not covered by the immediately preceding sentence,
Seller will be responsible for all expenses incurred in obtaining such Consents pursuant
to this Section 2.2 up to an aggregate amount of $20,000 and, if Buyer determines to
incur such expenses, Seller and Buyer will share equally such expenses in excess of
$20,000.
ARTICLE III
ASSUMPTION OF LIABILITIES
Section 3.1. Assumed Liabilities. Subject to the terms and conditions set
forth herein, and in reliance upon the representations and warranties contained herein, at
the Closing, in consideration for the sale, assignment, conveyance, transfer and delivery
of the Assets to Buyer, Buyer will assume and undertake to pay, perform and discharge,
in accordance with the terms thereof, only the following Liabilities of Seller and the
Seller Subsidiaries (the "Assumed Liabilities")-
4
CPAM: 7853833.14

Central Files: APS _ SWP _
7/31/2015
Permit Number NCG030664 V Permit Tracking Slip
Program Category Status Project Type'
NPDES SW Active New Project
Permit Type Version Permit Classification
Metal Fabrication Stormwater Discharge COC 1.00 COC
Primary Reviewer RECEIVED
Permit Contact Affiliation
bradley.bennett AUGCoastal SWRule U0 3 2M
Permitted Flow CENTRAL FILESDWR SECTION
Facility
Facility Name
Major/Minor Region
ABB US High Voltage Cable
Minor Mooresville
Location Address
County
12331 Commerce Station Dr
Mecklenburg
Facility Contact Affiliation
Huntersville NC 28078 John Moore
12331 Commerce Station Dr
Owner Huntersville NC 28078
Owner Name Owner Type
Abb Inc Non -Government
Owner Affiliation
John Moore
12331 Commerce Station Dr
Dates/Events Huntersville NC 28078
Scheduled
Orig Issue App Received Draft Initiated Issuance Public Notice issue Effective Expiration
7/31/2015 7/20/2015 7/30/2015 7/31/2015 7/31/2015 40/311 r 9
Regulated Activities Requested /Received Events
Rolling, drawing, and extruding of nonfe RO staff report received 7/22115
RO staff report requested 7/20115
Outfall 001
Waterbody Name Streamindex Number Current Class Subbasin
Cane Creek 13-17-4-2-1 C 03-07-11

A�
..-..rA
CCDF R
North Carolina Department of Environment and Natural Resources
Pat McCrory
Governor
John Moore
ABB Inc. - US High Voltage Cable
12331 Commerce Station Drive
Huntersville, NC 28078
Dear Mr. Moore:
Donald R. van der Vaart
Secretary
July 31, 2015
Subject: General Permit No. NCG030000
ABB US High Voltage Cable
COC NCG030664
Mecklenburg County
In accordance with your application for a discharge permit received on July 20, 2015,
we are forwarding herewith the subject certificate of coverage to discharge under the subject
state NPDES general permit. This permit is issued pursuant to the requirements of North
Carolina General Statute 143-215.1 and the Memorandum of Agreement between North.
Carolina and the US Environmental Protection Agency dated October 15, 2007 (or as
subsequently amended).
Please take notice that this certificate of coverage is not transferable except after notice
to the Division of Energy, Mineral and Land Resources. The Division may require
modification or revocation and reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may
be required by the Division of Energy, Mineral and Land Resources or permits required by
the Division of Water Resources, Coastal Area Management Act or any other federal or local
governmental permit that may be required.
Division of Energy, Mineral, and Land Resources
Energy Section • Geological Survey Section • Land Quality Section
1612 Mail Service Center, Raleigh, North Carolina 27699-1612.919-707-92001 FAX [phone]
512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: http://Portal.ncdenr.oLqLwebArl
An Equal Opportunity 1 Affirmative Action Employer — 50% Recycled 110% Post Consumer Paper

Mr. John Moore
July 31, 2015
Page 2 of 2
If you.have any questions concerning this permit, please contact Bradley Bennett at
telephone number [phone]
Sincere] ,
4d
for Tracy E. Davis, P.E., CPM
cc: Mooresville Regional Office, Zahid Khan
Central Files
Stormwater Permitting Unit Files
Mecklenburg County DEP, Water Quality, 700 N. Tryon Street, Charlotte, NC 28202

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
GENEBAL PERMIT NO, NCG030000
CERTIFICATE OF COy RAE No.NCGO 0664
STORMWATER DISCHARGES
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
ABB, Inc.
is hereby authorized to discharge stormwater from a facility located at
ABB US High Voltage Cable
12331 Commerce Station Drive
Huntersville
Mecklenburg County
to receiving waters designated as Cane Creek, a class C water in the Yadkin Pee -Dee River
Basin, in accordance with the effluent limitations, monitoring requirements, and other
conditions set forth in Parts 1, II, I1I and IV of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective July 31, 2015.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day July 31, 2015.
for Tracy E. Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission

LOCATION MAP:
USGS Maps: Comellus
Latitude: 350 23' 35.51" N NCG030664 Facili
Longitude: 80' 50' 01.91" W ty
ABB Inc. —US High Voltage Location
County: Mecklenburg Cable
Stream .Class: C
Receiving Stream: Cane Creek
Sub -basin: 03-07-11 (Yadkin Pee -Dee River Basin) oYottA Not to Scale

Semi-annual Stormwater DischaEge Monitoring -Re ort
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted d
CERTIFICATE OF COVERAGE NO. NCG03P_ J ,Q 96 (la 4
FACILITY NAME -�4B& s�C„
COUNTY
PERSON COLLECTING SAMPLES
LABORATORY c Lab Cert. ii ,2-
Comments on sample collection or analysis: C(J— [ (pa�
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR KOIJ
SAMPLE PERIOD ❑ Jan -June July -Dec
or ❑ Monthly' month
DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA
❑Zero -flow ❑Wat r Supply []SA[Other u ,
ra"', e,L,x gI,f5, n)
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
No discharge this period?2
Outfall No.
Date Sample
i
Colle
24hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks ==_>
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
,to3
.O
—
r10,06
5'r
S
3
zfli 5-r
�.
7,
5�
oos'v
o. af7
5,c�'�
—
1 Monthly sa pling (instead semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling riods wit o discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipita n must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found In 40 CFR 469.31). .
�w ,ze fov r 4-rmi i
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

i. 0
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO moni oring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
Title (Pri t title) V 6
D 70(b
(S' ature) (D te)
Note: Results must be reported in numerical format. 0 not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?z
Outfall No.
pate Sample
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks ===>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 —9.0 SU
I
If
Footnotes from Part A also apply to this Part 8
* See General Permit text, Table S, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/112012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

0 0
q,
Note: if you report a sample value In excess of the benchmark, you must implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text.
FOR PART AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 5ECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
IWO an original and one copy of this DMR. Includina all "No Discharae" reports, within 30 dovs of receipt of the lab results (or at end of monkgrina period
hLthe cased"No Mcharr{ "r�eaarU) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR 8W NFORMATM-DEPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are s,*nificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
of Permiittee)
*W2. c /
Date
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

aceAnalytical
wWwpaoeleba.cnm
Pace Analytical Services, Inc.
205 East Meadow (toad - Suite A
Eden, NC 27288
[phone]
January 29, 2015
John Moore
ABB, Inc.
12331 Commerce Station
Huntersville, NC 28078
RE: Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Dear John Moore:
Enclosed are the analytical results for sample(s) received by the laboratory on January 13, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Laura J Cooper
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc..
Page f of 40

Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
aceM' alytical Eden, NC 27288
wwwpacewmcom (336)62M921
r
CERTIFICATIONS
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12 VirginialVELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginialVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 40

aceAnalyfical
www.paceia LwM
i
Pace Ana"cal Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE SUMMARY
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Lab ID Sample IC Matrix Date Collected Date Received
92233032001
G-1
Water
01/13/15 09:00
01/13/15 11:30
92233032002
G-2
Water
01/13/15 09:30
01/13/15 11:30
92233032003
G-3
Water
01/13/1510:00
01/1311511:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 40

1��alce Analytical
MWw.pacelaba.ow
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Analytes
Lab ID Sample [D Method Anatysts Reported Laboratory
92233032001 G-1
92233032002 G-2
a
32233032003 G-3
EPA 1664B
CLW
1
PASI-C
EPA 608
RES
27
PASI-C
EPA 200.7
JMW
7
PASI-A
EPA 625
BPJ
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
TEP
1
PASI-A
EPA 9040
MAB
1
PASI-A
EPA 1664B
CLW
1
PASI-C
EPA 608
RES
27
PASI-C
EPA 200.7
JMW
7
PASI-A
EPA 625
BPJ
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
TEP
1
PASI-A
EPA 9040
MAB
1
PASI-A
EPA 1664E
CLW
1
PASI-C
EPA 608
RES
27
PASI-C
EPA 200.7
JMW
7
PASI-A
EPA 625
RES
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
TEP
1
PASI-A
EPA 9040
MAB
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc- Page 4 of 40

aceAnalytical s
WWW'pacelabs.cam
a ,
ANALYTICAL RESULTS
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: G-1
Parameters
La6ID: 92233032001
Results Units
Collected:
Report
Limit
01/13/16 09:00
MDL DF
Received: 01/13/15 11:30 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mglL
5.0
1.1
1
01/15115 08:24
608 GCS Pesticides and PCBs
Analytical Method: EPA 608
Preparation
Method: EPA 3510
Aldrin
ND uglL
0.050
0.050
1
01/15/15 18:15
0112011523:44
309-00-2
alpha-BHC
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/20/15 23:44
319-84-6
beta-13HC
ND ug1L
0.050
0,050
1
01/15/15 18:15
01/20/15 23:44
319-85-7
delta-BHC
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/20/15 23:44
319-86-8
gamma-BHC(Lindane)
ND ug/L
0.050
0,050
1
01/15/15 18:15
01/2011523:44
58-89-9
Chlordane (Technical)
ND ug/L
0,50
0,50
1
01/15/15 18:15
01/20/15 23:44
57-74-9
4,4'-DDD
ND ug/L
0.050
0.050
1
01/15/15 18:15
01120/15 23:44
72-54-8
4,4'-DDE
ND ug/L
0.050
0.050
1
01115/15 18:15
01/20/15 23:44
72-55-9
4,4'-DDT
ND ug1L
0.050
0.050
1
01/15/15 18:15
01/20/15 23:44
50-29-3
Dieldrin
ND ug1L
0.050
0.050
1
01/15/15 18:15
01/20/15 23:44
60-57-1
Endosulfan I
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/20/15 23:44
959-98-8
Endosulfan II
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/20/15 23:44
33213-65-9
Endosulfan sulfate
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/20/15 23:44
1031-07-8
Endrin
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/20/15 23:44
72-20-8
Endrin aldehyde
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/20/15 23:44
7421-93-4
Heptachlor
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/20/15 23:44
76-44-8
Heptachlor epoxide
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/2011523:44
1024-57-3
PCB-1016 (Aroclor 1016)
ND uglL
0.50
0.50
1
01/15/15 18:15
01/20/15 23:44
12674-11-2
PCB-1221 (Aroclor 1221)
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/20/15 23:44
11104-26-2
PCB-1232 (Aroclor 1232)
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/20/15 23:44
11141-16-5
PCB-1242 (Aroclor 1242)
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/20/15 23:44
53469-21-9
PCB-1248 (Aroclor 1248)
ND ug/L
0.50
0.50
1
01/15115 18:15
01/20/15 23.44
12672-29-6
PCB-1254 (Aroclor 1254)
ND ug/L
0.50
0.50
1
01/15/15 18*15
01/20/15 23:44
11097-Wl
PCB-1260 (Aroclor 1260)
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/20/15 23:44
11096-82-5
Toxaphene
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/20/15 23:44
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
54 %
26-110
1
01/15/15 18:15
01/20/15 23:44
877-09-8
DecachlorobiphenylIS)
55 %
20-138
1
01/15/15 18:15
0112011523:44
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method:
EPA 200.7
Cadmium
ND mg/L
0.0010
0.00050
1
01114/151510
01/1411523:11
7440-43-9
Chromium
ND mg/L
0.0050
0.0025
1
01/14/15 15:10
01/14/15 23:11
7440-47-3
Copper
0.0053 mg/L
0.0050
0.0025
1
01/1411515:10
01114/1523:11
7440-50-8
Lead
ND mg/L
0.0050
0.0025
1
01/1411515:10
01115/1518:10
7439-92-1
Nickel
ND mg/L
0.0050
0.0025
1
01/14/15 15:10
01/14/15 23:11
7440-02-0
bilver
ND mg/L
0.0050
0.0025
1
01/1411515:10
01114/1523:11
7440-22-4
Zinc
0.014 mg/L
0.010
0.0025
1
01/14/15 15:10
01/1411523:11
7440-66-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene
ND uglL
5.0
0.25
1
01/15/15 09:30
01/16/1503:15
83-32-9
Acenaphthylene
ND ug1L
5.0
0.21
1
01/15/15 09:30
01/16/15 03:15
208-9"
Anthracene
ND ug/L
5.0
0.14
1
01/15/15 09:30
01/1611503:15
120-12-7
Benzo(a)anthracene
ND ug/L
5.0
0.33
1
01/15/15 09:30
01/16/15 03:15
56-55-3
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except in
full,
Date: 01/29/2015 05:12 PM
without the written consent of Pace Analytical Services,
Inc..
Page 5 of 40

Pace Anatytical Services, Inc.
ZoeAnalytical 2D5 East Meadow Road - Suite A
Eden, NC 27288
WWW.PatVla A=n [phone]
ANALYTICAL RESULTS
Project: 2014 SEMI-ANNUAL_
Pace Project No.: 92233032
Sample: G-1 Lab ID: 92233032001 Collected: 01/13/15 09:00 Received: 01/13/15 11:30 Matrix: Water
Report
Parameters
Results
Units Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
625 MSSV
Analytical Method:
EPA 625 Preparation Method: EPA
625
Benzo(a)pyrene
ND ug/L
5.0
0.30
1
01/15/15 09:30
01116/15 03:15
50-32-8
Benzo(b)fluoranthene
ND uglL
5.0
0.28
1
01/15/15 09:30
01/16/15 03:15
205-99-2
Benzo(g,h,i)perylene
ND ug/L
5.0
0.38
1
01/15/15 09:30
01/16/15 03:15
191-24-2
Benzo(k)fluoranthene
ND ug/L
5.0
0.43
1
01/15/15 09:30
01/16/15 03:15
207-08-9
4-13romophenylphenyl ether
ND ug/L
5.0
0.82
1
01/15/15 09:30
01/16/15 03:15
101-55-3
Butylbenzylphthalate
ND uglL
5.0
0.79
1
01/15/15 09:30
01/16/15 03:15
85-68-7
4-Chloro-3-methylphenol
ND ug/L
5.0
3.7
1
01/15/15 09:30
01/16/15 03:15
59-50-7
bis(2-Chloroethoxy)methane
ND ug/L
10.0
0.92
1
01/15/15 09:30
01/16/15 03:15
111-91-1
bis(2-Chloroethyl) ether
ND ug/L
5.0
1.0
1
01/15/15 09:30
01/16/15 03:15
Ill 44 4
bis(2-Chloroisopropyl) ether
ND ug/L
5.0
0.95
1
01/15/15 09:30
01/16/15 03:15
108-60-1
2-Chloronaphthalene
ND ug/L
5.0
0.98
1
01/15/15 09:30
01/16/15 03:15
91-58-7
2-Chlorophenol
ND ug/L
5.0
1.3
1
01/15/15 09:30
01/16/15 03:15
95-57-8
4-Chlorophenylphenyl ether
ND ug/L
5.0
0.87
1
01/15/15 09:30
01/16/15 03:15
7005-72-3
Chrysene
ND ug/L
5.0
0.21
1
01/15/15 09:30
01/16/15 03:15
218-01-9
Dibenz(a,h)anthracene
ND ug/L
5.0
0.55
1
01/15/15 09:30
01/16/15 03:15
53-7D-3
3,3'-Dichlorobenzidine
ND ug/L
25.0
2.1
1
01/15/15 09:30
01/16/15 03:15
91-94-1
2,4-Dichlorophenol
ND ug/L
5.0
1.7
1
01/15/15 09:30
01/16/15 03:15
120-83-2
Diethylphtha late
ND ug/L
5.0
0.58
1
01/15/15 09:30
01/16/15 03:15
84-66-2
2,4-Dimethylphenol
ND ug/L
10.0
1.2
1
01/15/15 09:30
01/16/15 03:15
105-67-9
Dimethylphthalate
ND ug/L
5.0
0.76
1
01/15/15 09:30
01/16/15 03:15
131-11-3
Di-n-butylphthalate
ND ug/L
5.0
0.75
1
01/15/15 09:30
01/16/15 03:15
84-74-2
�,6-Dinitro-2-methylphenol
ND ug/L
20.0
2.6
1
01/15/15 09.30
01/16/15 03:15
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
9.0
1
01/15/15 09:30
01/16/15 03:15
51-28-5
2,4-Dinitrotoluene
ND ug/L
5.0
0.90
1
01/15/15 09:30
01/16/15 03:15
121-14-2
2,6-Dinitrotoluene
ND ug/L
5.0
0.98
1
01/15/15 09:30
01/16/15 03:15
606-20-2
bi-n-octylphthalate
ND ug/L
5.0
0.66
1
01/15/15 09:30
01/16/15 03:15
117-84-0
bis(2-Ethylhexyl)phthalate
ND ug/L
5.0
0.79
1
01/15/15 09:30
01/16/15 03:15
117-81-7
Fiuoranthene
ND ug/L
5.0
0.21
1
01/15115 09:30
01/16/15 03:15
206-44-0
Fluorene
ND ug/L
5.0
0.21
1
01/15115 09:30
01/16/15 03:15
86-73-7
Hexachioro-1,3-butadiene
ND ug/L
5.0
0.94
1
01/15/15 09:30
01/16/15 03:15
87-68-3
Hexachlorobenzene
ND ug/L
5.0
0.72
1
01/15/15 09:30
01/16/15 03:15
11&74-1
Hexachiorocyclopentadiene
ND ug/L
10.0
0.88
1
01/15/15 09:30
01/16115 03:15
77-47-4
Hexachloroethane
ND ug/L
5.0
1.1
1
01/15/15 09:30
01/16/15 03:15
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
5.0
0.29
1
01/15/15 09:30
01/16/15 03:15
193-39-5
isophorone
ND ug/L
10.0
0.89
1
01/15/15 09:30
01/16/15 03:15
78-59-1
Naphthalene
ND ug/L
5.0
0.34
1
01/15/15 09:30
01/16/15 03:15
91-20-3
Nitrobenzene
ND ug/L
5.0
1.1
1
01/15/15 09:30
01/16/15 03:15
98-95-3
2-Nitrophenol
ND ug/L
5.0
0.91
1
01/15/15 09:30
01/16/15 03:15
88-75-5
4-Nitrophenol
ND ug/L
50.0
4.1
1
01/15/15 09:30
01/16/15 03:15
100-02-7
N-Nitrosodimethylamine
ND ug/L
5.0
0.91
1
01/15/15 09:30
01/16/15 03:15
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
5.0
0.99
1
01/15/15 09:30
01/16/15 03:15
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1.0
1
01/15/15 09:30
01/16/15 03:15
86-30-6
Pentachlorophenol
ND ug/L
10.0
4.6
1
01115M5 09:30
01/16/15 03:15
87-86-5
Phenanthrene
ND ug/L
5.0
0.22
1
01/15/15 09:30
01/16/15 03:15
85-01-8
Phenol
ND ug/L
5.0
1.9
1
01/15/15 09:30
01116/15 03:15
108-95-2
Pyrene
ND ug/L
5.0
0.19
1
01/15/15 09:30
01/16/15 03:15
129-00-0
r.
r.
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /29/2015 05:12 PM
without the written consent of
Pace Analytical Services, Inc..
Page 6 of 40

aceAnalylical
WWW..pecefab&=rt
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Sample: G-1 LabID: 92233032001 Collected: 01/13/15 09:00 Received: 01/13/15 11:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyi (S)
TerphenyW14(S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
624 Volatile Organics
Benzene
Bromod ich loromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
C hioroform
Chloromethane
13ibromoch loromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
,1,2-Dichloropropane
c4s-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1-Trick loroethane
1,1,2-Trick loroethane
Trich to roethe ne
Trichlorofluoromethane
Vinyl chloride
Surrogates
4 13romofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichloroethane-d4 (S)
ND ug/L
5.0
0.98 1
01/15M5 09:30
01/16/15 03:15
120-82-1
ND ug/L
%0
1.3 1
01/15115 09:30
01116/15 03:15
88-06-2
42 %
10-120
1
01/15/15 09:30
01/16/15 03:15
4165-60-0
44 %
15-120
1
01/15115 09:30
01/16/15 03:15
321-60-8
74 %
11-131
1
01/16/15 09:30
01/16/15 03.15
1718-51-0
16 %
10-120
1
01/15/15 09:30
01/16/15 03:15
13127-88-3
24 %
10-120
1
01/15/15 09:30
01/16/15 03:15
367-12-4
63 %
10-137
1
01/15/15 09:30
01/16/15 03:15
118-79-6
Analytical Method: EPA 624
ND ug/L
2.0
1.7
1
01/17/15 07:08
71-43-2
ND ug/L
2.0
1.7
1
01/17/15 07:08
75-27-4
ND ug/L
2.0
1.5
1
01/17/15 07:08
75-25-2
ND ug1L
2A
1.0
1
01/17/15 07:08
74-83-9
ND ug/L
2.0
1.9
1
01/1711507:08
56-23-5
ND ug/L
2.0
1.7
1
01/17/15 07:08
108-90-7
ND ug/L
2.0
1.6
1
01/17A5 07:08
75-0D-3
ND ug/L
2.0
1.9
1
01/17/15 07:08
57-66-3
ND ug/L
2.0
1.5
1
01/17/15 07:08
74-87-3
ND ug/L
2.0
1.8
1
01117/15 07:08
124-48-1
ND ug/L
2.0
1.5
1
01/17/15 07:08
95-50-1
ND ug/L
2.0
1.5
1
01/17/15 07:08
541-73-1
ND ug/L
2.0
1.5
1
01/17/15 07:08
106-46-7
ND ug/L
2.0
1.8
1
01/17/15 07:08
75-34-3
ND ug/L
2.0
1.8
1
01/17115 07:08
107-06-2
ND ug/L
2.0
1.9
1
01/17/15 07:08
75-35-4
ND ug/L
2.0
1.8
1
01/17115 07:08
156-59-2
ND ug/L
2.0
1.8
1
01/17/15 07:08
156-60-5
ND ug/L
2.0
1.7
1
01/17/15 07:08
78-87-5
ND ug/L
2.0
1.6
1
01/17/15 07:08
10061-01-5
ND ug/L
2.0
1.6
1
01/17/15 07:08
10061-02-6
ND ug/L
2.0
1.6
1
01117/15 07:08
100-41.4
ND ug/L
2.0
1.9
1
01/17/15 07:08
75-09-2
ND ug/L
2.0
1.5
1
01/17/15 07:08
79-34-5
ND ug/L
2.0
1.8
1
01/17/15 07:08
127-18-4
ND ug/L
2.0
1.6
1
01/17/15 07:08
108-88-3
ND ug/L
2.0
1.9
1
01/17/15 07:08
71-55-6
ND ug/L
2.0
1.7
1
01/17/15 07:08
79-00-5
ND ug/L
2.0
1.8
1
01/1711507:08
79-01-6
ND ug/L
2.0
1.7
1
01/17/15 07:08
75-69-4
ND ug/L
2.0
1.5
1
01/17/15 07:08
75-01-4
95 %
70-130
1
01/17/15 07:08
460-00-4
94 %
70-130
1
01/17/15 07:08
2037-26-5
99 %
70-130
1
01/17/15 07:08
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 40

lacm-nalyficale
W*w.Aecelabacom
i
ANALYTICAL RESULTS
)?roject: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 2728E
[phone]
Sample: G-1 Lab ID: 92233032001 Collected: 01/13115 09:00 Received: 01/13/15 11:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 8.8 mg/L 2.5 2.5 1 01/15/15 04:48
9040 pH
pH
Analytical Method: EPA 9040
7.2 Sid. Units 0.10
0.10
1
01/14/15 12:16
H6
Sample: G-2
Lab ID: 92233032002
Collected:
01/13/15
09:30
Received: 01/13/15
11:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Qil and Grease
ND mg/L
5.0
1.1
1
01/15/15 08:24
608 GCS Pesticides and PCBs
Analytical Method: EPA 608 Preparation
Method: EPA 3510
Aldrin
ND ug/L
0,050
0.050
1
01/15/15 18:15
01/21/15 00:02
309-00-2
alpha-BHC
ND ug1L
0,050
0.050
1
01/15/15 18:15
01/21/15 00:02
319-84-6
beta-BHC
ND ug/L
0.050
0.050
1
01/15/15 18:15
01I21/15 00:02
319-85-7
delta-BHC
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:02
319-86-8
gamma-BHC (Lindane)
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:02
58-89-9
Chlordane (Technical)
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00:02
57-74-9
4,4'-DDD
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:02
72-54-8
4,4'-DDE
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:02
72-55-9
4,4'-DDT
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:02
50-29-3
Dieldrin
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:02
60-57-1
Endosulfan I
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:02
959-98-8
Endosulfanll
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:02
33213-65-9
Endosulfan sulfate
ND ug/L
0.050
0,050
1
01/15/15 18:15
01/21/15 00:02
1031=07-8
Endrin
ND ug/L
0.050
0,050
1
01/15/15 18:15
01/21/15 00:02
72-20-8
Endrin aldehyde
ND ug/L
0.050
0,050
1
01/15/15 18:15
01/21/15 00:02
7421-93-4
Heptachlor
ND ug/L
0.050
0,050
1
01/15/15 18:15
01/21/15 00:02
764"
Heptachlor epoxide
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:02
1024-57-3
PCB-1016 (Aroclor 1016)
ND ug/L
0.50
0.50
1
01/15/15 1815
01/21/15 00:02
12674-11-2
PCB-1221 (Aroclor 1221)
ND ug/L
0.50
0.50
1
01/1511518:15
01/21/15 00:02
11104-28-2
PCB-1232 (AroCIOr 1232)
ND uglL
0.50
0.50
1
01/15/15 18:15
01/21/15 00:02
11141-16-5
PCB-1242 (Aroclor 1242)
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00:02
53469-21-9
PCB-1248 (Aroclor 1248)
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00:02
12672-2M
PCB-1254 (Aroclor 1254)
ND ug/L
0.50
0.50
1
01115/1518:16
01/21/15 00:02
11097-69-1
PCB-1260 (Aroclor 1260)
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00:02
11096-82-5
Toxaphene
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00:02
8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
55 %
20-110
1
01/15/15 18:15
01/21115 00:02
877-09-8
Decachlorobiphenyl (S)
51 %
20-138
1
01/15/15 18:15
01/21/15 00:02
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND mg/L
0.0010
0.00050
1
01/14/15 15:10
01/14/15 2315
7440-43-9
REPORT OF
LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
*Date: 01 /29/2015 05:12 PM
without the written consent of Pace Analytical Services, Inc..
Page 8 of 40

Pace Analytical Services, Inc.
e w Road - Suite A
205 Fast Meadow Eden, NC 27288
! wwwpao wm
[phone]
f
ANALYTICAL RESULTS
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Sample: G-2 Lab ID: 92233032002 Collected: 01/13/15 09:30 Received: 01/13/15 11:30 Matrix: Water
Parameters
200.7 MET ICP
Chromium
Copper
Lead
Nickel
Silver
Zinc
625 MSSV
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Senzo(k)fluoranlhene
4-Bromophenylphenyl ether
Butylbenzyiphtha late
4-C hloro-3-methylphenol
bis(2-Ch to roethoxy)methane
�is(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h )anth racene
3, 3'-DicNorobenzidine
2,4-Dichlorophenol
I7iethylphthalate
2,4-Dimethylphenol
bimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
46-Dinitrotoluene
bi-n-octylphthalate
bis(2-Ethy1hexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1 ,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentad iene
'Hexachloroethane
Indeno(1,2,3-cd)pyrene
Report
Results Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
Analytical Method: EPA 200.7 Preparation
Method:
EPA 200.7
ND mg/L
0.0050
0.0025
1
01/14/15 15:10
01/14/15 23:15
7440-47-3
ND mg/L
0.0050
0.0025
1
01/14/15 15:10
01/14/15 23:15
7440-50-8
ND mg/L
0.0050
0.0025
1
01/14/15 15:10
01/15/15 18:13
7439-92-1
ND mg/L
0,0050
0.0025
1
01/14/15 15:10
01/14/15 23:15
7440-02-0
ND mg/L
0,0050
0.0025
1
01114/15 15:10
01/14/15 23:15
7440-22-4
ND mg/L
0.010
0.0025
1
01/14/15 15:10
01/14/15 23:15
7440-66-6
Analytical Method: EPA 625 Preparation Method EPA 625
ND ug/L
5.0
0.25
1
01/15/15 09,30
01116/15 04:45
83-32-9
ND ug/L
5.0
0.21
1
01/15/15 09:30
01/16/15 04:45
208-96-8
ND ug/L
5.0
0.14
1
01/15/15 09:30
01/16/15 04:45
120-12-7
ND ug/L
5.0
0.33
1
01/15/15 09:30
01/16/15 04:45
56-55-3
ND ug/L
5.0
0.30
1
01/15/15 09:30
01/16/15 04:45
50-32-8
ND ug/L
5.0
0.28
1
01/15/15 09:30
01/16/15 04:45
205-99-2
ND uglL
5.0
0.38
1
01/15/15 09:30
01/16/15 04:45
191-24-2
ND ug/L
5.0
0.43
1
01 /15/15 09:30
01/16/15 04:45
207-08-9
ND ug/L
5.0
0.82
1
01/15/15 09:30
01/16/15 04:45
101-55-3
ND uglL
5.0
0.79
1
01/15/15 09:30
01/16/15 04:45
85-68-7
ND ug/L
5.0
3.7
1
01/15/15 09:30
01/16/15 04:45
59-50-7
ND uglL
10.0
0.92
1
01/15/15 09:30
01/16/15 04:45
111-91-1
ND ug/L
5.0
1.0
1
01/15/15 09:30
01/16/15 04:45
111-44-4
ND ug/L
5.0
0.95
1
01/15/15 09:30
01/16/15 04:45
108-60-1
ND ug/L
5.0
0.98
1
01/15/15 09:30
01/16/15 04:45
91-58-7
ND ug/L
5.0
1.3
1
01/15/15 09:30
01/16/15 04:45
95-57-8
ND ug/L
5.0
0.87
1
01/15/15 09:30
01/16/15 04:45
7005-72-3
ND ug/L
5.0
0.21
1
01/15/15 09:30
01/16/15 04:45
218-01-9
ND ug/L
5.0
0.55
1
01115/15W30
01M6/1504:45
53-70-3
ND ug/L
25.0
2.1
1
01/15/15 09:30
01/16/15 04:45
91-94-1
ND ug/L
5.0
1.7
1
01/15/15 09:30
01/16/15 04:45
120-83-2
ND ug/L
5.0
0.58
1
01/15/15 09:30
01/16/15 04:45
84-66-2
ND ug/L
10.0
1.2
1
01/15/15 09:30
01/16/15 04:45
105-67-9
ND ug/L
5.0
0,76
1
01/15/15 09:30
01/1611504:45
131-11-3
ND ug/L
5.0
0.75
1
01/15/15 09:30
01/16/15 04:45
84-74-2
ND ug/L
20.0
2.6
1
01/15/15 09:30
01/16/15 04A5
534-52-1
ND ug/L
50.0
9.0
1
01/15/15 09:30
01/16/15 04:45
51-28-5
ND ug/L
5.0
0.90
1
01/15/15 09:30
01/16/15 04:45
121-14-2
ND ug/L
5.0
0.98
1
01/15/15 09:30
01/16115 04:45
606-20-2
ND ug/L
5.0
0.66
1
01/15/15 09:30
01/16/15 04:45
117-84-0
ND ug/L
5.0
0.79
1
01/15/15 09:30
01/16/15 04:45
117-81-7
ND ug/L
5.0
0.21
1
01/15/15 09:30
01/16/15 04:45
206-44-0
ND ug/L
5.0
0.21
1
01/15/15 09:30
01/16/15 04:45
86-73-7
ND ug/L
5.0
0.94
1
01/15/15 09:30
01/16/15 04:45
87-68-3
ND u9/L
5.0
0.72
1
01/1511509:30
01/16/15 04:45
118-74-1
ND ug/L
10.0
0.88
1
01/15/15 09:30
01/1611504:45
77-47-4
ND ug/L
5.0
1.1
1
01/15/15 09:30
01/16/15 04:45
67-72-1
ND ug/L
5.0
0.29
1
01/15/15 09:30
01/16/15 04:45
193-39-5
REPORT OF LABORATORY ANALYSIS
Date: 01/29/2015 05:12 PM
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 40

�aceA'na1j6ca1*
»ww.patelafte=
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Sample: G-2
Lab ID: 92233032002
Collected:
01/13115 09:30
Received: 01/13/15 11:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
lsaphorone
ND ug/L
10.0
0.89
1
01/15/15 09:30
01/16/15 04:45
78-59-1
Naphthalene
ND ug1L
5.0
0.34
1
01115/15 09:30
01/16/15 04:45
91-20-3
Nitrobenzene
ND uglL
5.0
1.1
1
01/15/15 09:30
01/16/15 04:45
98-95-3
2-Nitrophenol
ND uglL
5.0
0.91
1
01/15/15 09:30
01/16/15 04:45
88-75-5
4-Nitrophenol
ND ug/L
50.0
4.1
1
01/15/15 09:30
01/16/15 04:45
100-02-7
N-Nitrosodimethylamine
ND uglL
5.0
0.91
1
01/15/15 09:30
01/16/15 04:45
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
5.0
0.99
1
01/15/15 09:30
01/16/15 04:45
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1.0
1
01/15/15 09:30
01/16/15 04:45
86-30-6
Pentachlorophenol
ND ug/L
10.0
4.6
1
01/15/15 09:30
01/16/15 04:45
87-86-5
Phenanthrene
ND ug/L
5.0
0.22
1
01/15/15 09:30
01/16/15 04:45
85-01-8
Phenol
ND ug/L
5.0
1.9
1
01/15/15 09:30
01/16/15 04:45
108-95-2
Pyrene
ND ug./L
5.0
0.19
1
01/15/15 09:30
01/16/15 04:45
129-00-0
T ,2,4-Trichlorobenzene
ND ug/L
5.0
0.98
1
01/15/15 09:30
01/16/15 04:45
120-82-1
2,4,6-Trichlorophenol
ND ug1L
10.0
1.3
1
01/15/15 09:30
01/16/15 04:45
88-06-2
Surrogates
Nitrobenzene-d5 (S)
44 %
1 D-120
1
01/15/15 09:30
01/16/15 04:45
4165-60-0
2-Fluorobiphenyl(S)
46 %
15-120
1
01/15/15 09:30
01/16/15 04:45
321-60-8
Terphenyl-d 14 (S)
70 %
11-131
1
01/1511509:30
01/1611504:45
1718-51-0
Phenol-d6(S)
17 %
10-120
1
01/15/15 09:30
01/1611504:45
13127-88-3
2-Fluorophenol(S)
24 %
10-120
1
01/1511509:30
01/1611504:45
367-12-4
2,4,6-Tribromophenol (S)
57 %
10-137
1
01/15/15 09:30
01/16/15 04:45
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND ug/L
2.0
1.7
1
01/17/15 07:24
71-43-2
Bromodichloromethane
ND ug/L
2.0
1.7
1
01117/15 07:24
75-27-4
Bromofonn
ND ug/L
2.0
1.5
1
01/17/15 07:24
75-25-2
Bromomethane
ND ug/L
2.0
1.0
1
01WA5 07:24
74-83-9
Carbon tetrachloride
ND ug/L
2.0
1.9
1
01/17/15 07:24
56-23-5
Chlorobenzene
ND ug/L
2.0
1.7
1
01/17/15 07:24
108-90-7
Chloroethane
ND uglL
2.0
1.6
1
01/17/15 07:24
75-00-3
Chloroform
ND ug1L
2.0
1.9
1
01/17/15 07:24
67-66-3
Chloromethane
ND ug/L
2.0
1.5
1
01/17/15 07:24
74-87-3
Dibromochloromethane
ND ug/L
2.0
1.8
1
01/17/15 07.24
124-48-1
1,2-Dichlorobenzene
ND ug/L
2.0
1.5
1
01/17/15 07:24
95-50-1
1,3-Dichlorobenzene
ND ug/L
2.0
1.5
1
01/17/15 07:24
541-73-1
1A-Dichlorobenzene
ND ug/L
2.0
1.5
1
01/17/1507:24
106-46-7
1,1-Dichloroethane
ND ug/L
2.0
1.8
1
01/17/15 07:24
75-34-3
1.2-Dichloroethane
ND ug/L
2.0
1.8
1
01/17/15 07:24
107-06-2
I,1-Dichloroethene
ND ug/L
2.0
1.9
1
01/17/15 07:24
75-35-4
cis-1,2-Dichloroethene
ND ug/L
2.0
1.8
1
01/17/15 07:24
156-59-2
trans-1,2-Dichloroethene
ND ug/L
2.0
1.8
1
01117/1507:24
156-60-5
1,2-Dichloropropane
ND ug/L
2.0
1.7
1
01/17/15 07:24
78-87-5
cis-1,3-Dichloropropene
ND ug/L
2.0
1.6
1
01/17/15 07:24
10061-01-5
trans-1,3-Dichloropropene
ND ug/L
2.0
1.6
1
01/17/15 07:24
10061-02-6
Ethylbenzene
ND ug/L
2.0
1.6
1
01/17/15 07:24
100-41-4
Methylene Chloride
ND ug/L
2.0
1.9
1
01/17/15 07:24
75-09-2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced,
except in
full.
Date: 01 /29/2015 05:12 PM
without the written consent of Pace Analytical Services, Inc..
Page 10 of 40

5XAnalytical
` www.pe[adabs.oam
r
f
FA11TIA&11DfAq:1*1111111K
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Sample: G-2
Lab ID: 92233032002
Collected:
01/13115 09:30
Received:
01/13/15 11:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624
1,1,2,2-Tetrachloroethane
ND ug/L
2.0
1.5
1
01/17/15 07:24
79-34-5
Tetrachloroethene
NO ug/L
2.0
1.8
1
01/17/15 07:24
127-18-4
Toluene
NO ug1L
2.0
1.6
1
01/17/15 07:24
108-88-3
1,1,1-Trichloroethane
ND ug/L
2.0
1.9
1
01/17/15 07:24
71-55-6
1,1,2-Trichloroethane
ND uglL
2.0
1.7
1
01/17/15 07:24
79-00-5
Trichloroethene
ND uglL
2.0
1.8
1
01/17/15 07:24
79-01-6
Trichlorofluoromethane
ND ug/L
2.0
1.7
1
01/17/15 07:24
75-69-4
Vnyl chloride
ND ug/L
2.0
1.5
1
0111711507:24
75-014
Surrogates
4-Bromofluorobenzene (S)
97 %
70-130
1
01/17/15 07:24
460-00-4
Toluene-d8 (S)
95 %
70-130
1
01/17/15 07:24
2037-26-5
1,2-Dichloroethane-d4 (S)
96 %
70-130
1
01/17/15 07:24
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
4.2 mg/L
2.5
2.5
1
01M5115 04:48
9040 pH
Analytical Method: EPA 9040
pH
6.9 Std. Units
0.10
0.10
1
01/14/15 12:28
H6
Sample: G-3
Lab ID: 92233032003
Collected:
01/13/15 10:00
Received:
01/13/15 i1:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
HEM, Oil and Grease
Oil and Grease
608 GCS Pesticides and PCBs
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
.Endosulfan I
Endosulfan 11
Endosulfan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
Analytical Method: EPA 1664E
ND mg1L 5.0 1.1 1 01/15/15 0825
Analytical Method: EPA 608 Preparation Method: EPA 3510
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:19
309-00-2
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:19
319-84-6
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/1500.19
319-85-7
ND uglL
0.050
0.050
1
01/15/15 18:15
01/21/15 00:19
319-86-8
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21115 00:19
58-89-9
ND uglL
0.50
0.50
1
01/15/15 18:15
01/21/15 00:19
57-74-9
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:19
72-54-8
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:19
72-55-9
ND ug1L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:19
50-29-3
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:19
60-57-1
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:19
959-98-8
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:19
33213-65-9
ND ug/L
0.050
0.050
1
01/15/15 18:15
01 /21115 00:19
1031-07-8
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:19
72-20-8
ND ug/L
0.050
0.050
1
01/15/15 18:15
01/21/15 00:19
7421-93-4
ND ug/L
0.050
0.050
1
01/15/15 18:15
01121/15 00:19
76-44-8
ND uglL
0.050
0.050
1
01/15/15 1815
01/21/15 00:1.9
1024-57-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
hate: 01/29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 40

aceAnalytical
r www.pacebbs.cw
Pace Anatytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Sample: G-3 Lab ID: 92233032003 Collected: 01/13115 10:00 Received: 01/13/15 11:30 Matrix: Water
Parameters
608 GCS Pesticides and PCBs
PCB-1016 (Arodor 1016)
PCB-1221 (Arodor 1221)
PCB-1232 (Arodor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Arodor 1248)
PCB-1254 (Arodor 1254)
PCB-1260 (Arodor 1260)
Toxaphene
Surrogates
tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
200.7 MET ICP
Cadmium
Chromium
Copper
Lead
Nickel
gilver
Zinc
625 MSSV
1-
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
4-Bromophenylphenyl ether
Butylbenzylphthatate
4-Chloro-3-methylphenol
bis(2-Ch loroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
3, 3'-D i ch t o ro b e n t id i ne
2,4-Dichlorophenol
Diethylphlhalate
2,4-1)imethylphenol
Dimethylphthalate
c
Report
Results Units Limit MDL DF Prepared Analyzed CAS No, Qual
Analytical Method: EPA 608 Preparation Method: EPA 3510
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00:19
12674-11-2
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00:19
11104-28-2
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00:19
11141-16-5
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00:19
53469-21-9
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00.19
12672-29-6
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00:19
11097-69-1
ND ug/L
0.50
0,50
1
01/15/15 18:15
01/21/15 00:19
11096-82-5
ND ug/L
0.50
0.50
1
01/15/15 18:15
01/21/15 00:19
8001-35-2
58 %
20-110
1
01/15/15 18:15
01/21/15 00:19
877-09-8
65 %
20-138
1
01/15/15 18:15
01/21/15 00:19
2051-24-3
Analytical Method: EPA
200.7 Preparation Method: EPA 200.7
ND mg/L
0.0010
0.00050
1
01/14/15 15:10
01/14/15 23:21
7440-43-9
ND mg/L
0.0050
0,0025
1
01/14/15 15:10
01/14/15 2121
7440-47-3
ND mg/L
0.0050
0.0025
1
01/14/15 15:10
01/14/15 2321
7440-50-8
ND mg1L
0.0050
0.0025
1
01/14/15 15:10
01/1511518:20
7439-92-1
ND mg/L
0.0050
0.0025
1
01/14/15 15:10
01/14/15 23:21
7440-02-0
ND mg/L
0.0050
0.0025
1
01/14/15 15:10
01/14/15 23:21
7440-22A
0.017 mg/L
0.010
0.0025
1
01/14/15 15:10
01/14/15 23:21
744D-6"
Analytical Method: EPA625
Preparation Method: EPA625
ND ug/L
5.0
0.25
1
01/15/16 09:30
01/22/15 02:58
83-32-9
ND ug/L
5.0
0.21
1
01/15/15 09:30
01/22/15 02:58
208-96-8
ND ug/L
5.0
0.14
1
01/15/15 09:30
01122 I5 02:58
120-12-7
ND ug/L
5.0
0.33
1
01/15/15 09:30
01/22/15 02:58
56-55-3
ND ug/L
&0
0.30
1
01/15/15 09:30
01/22/15 02:58
50-32-8
ND ug/L
5.0
0.28
1
01/15/15 09:30
01/22/15 02:58
205-99-2
ND ug/L
5.0
0.38
1
01/15/15 09:30
01/22/15 02:58
191-24.2
ND ug/L
5.0
0.43
1
01115/15 09:30
01/22/15 02:58
207-08-9
ND ug/L
5.0
0.82
1
01/15/15 09:30
01/22/15 02:58
101-55-3
ND ug/L
5.0
0.79
1
01/15/15 09:30
01/22/15 02:58
85-68-7
ND ug/L
5.0
3.7
1
01/15/15 09.30
01/22/15 02:58
59-50-7
ND uglL
10.0
0.92
1
01/15/15 09:30
01/22/15 02:58
111-91.1
ND ug/L
5.0
1.0
1
01/15/15 09:30
01/22/15 02:58
111-44-4
ND ug/L
5.0
0.95
1
01/15/15 09:30
01/22/15 02:58
108-60-1
ND uglL
5.0
0.98
1
01/15/15 09:30
01/22/15 02:58
91-58-7
ND uglL
5.0
1.3
1
01/15115 09.30
01/22/15 02:58
W57-8
ND ug/L
5.0
0.87
1
01/15/15 09:30
01/22/15 02:58
7005-72-3
ND ug/L
5.0
0.21
1
01115/15 09:30
01/22/15 02:58
218-01-9
ND ug/L
5.0
0.55
1
01/15/15 09:30
01/22/15 02:58
53-70-3
ND ug/L
25.0
2.1
1
01/15/15 09:30
01/22/15 02:58
91-94-1
ND ug/L
5.0
1.7
1
01/15/15 09:30
01/22/15 02:58
120-83-2
ND ug/L
5.0
0.58
1
01/15/15 09:30
01/22/15 02:58
84-66-2
ND ug/L
10.0
1.2
1
01115/15 09:30
01/22/15 02:58
105-67-9
ND ug/L
5.0
0.76
1
01/15/15 09:30
01/22/15 02:58
131-11.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 01/29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 40

aceAnalytical*
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ANALYTICAL RESULTS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Sample: G-3
Lab ID: 92233032003
Collected:
01/13/15 10:00
Received: 01/13/15 11:30 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Oual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-butylphthalate
ND ug1L
5.0
0.75
1
01/15/15 09:30
01/22/15 02:58
84-74-2
4,6-Dinitro-2-methylphenol
ND uglL
20.0
2.6
1
01/15/15 09:30
01/22/15 02:58
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
9.0
1
01/15/15 09:30
01/22/15 02:58
51-28-5
2,4-Dinitrotoluene
ND ug/L
5.0
0.90
1
01/15/15 09:30
01/22/15 02:58
121-14-2
2,6-Dinitrotoluene
ND ug/L
5.0
0.98
1
01/15/15 09:30
01/22/15 02:58
606-20-2
Di-n-octylphthalate
ND ug/L
5.0
0.66
1
01 /15/15 09:30
01/22/15 02:58
117-84-0
bis(2-Ethylhexyl)phthalate
ND ug/L
5.0
0.79
1
01/15/15 09:30
01/22/15 02:58
117-81-7
Fluoranthene
ND ug/L
5.0
0.21
1
01/15/15 09:30
01/22/15 02:58
206-44-0
Fluorene
ND ug1L
5.0
0.21
1
01/15/15 09:30
01/22/15 02:58
86-73-7
Hexachloro-1,3-butadiene
ND uglL
5.0
0.94
1
01/15/15 09:30
01/22/15 02:58
87-68-3
Hexachlorobenzene
ND ug/L
5.0
0.72
1
01/15/15 09:30
01/22/15 02:58
118-74-1
Hexachlorocyclopentadiene
ND ug/L
10.0
0.88
1
01/15/15 09:30
01/22/15 02:58
77-47-4
Hexachloroethane
ND ug/L
5.0
1.1
1
01/15/15 09:30
01/22/15 02:58
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug/L
5.0
0.29
1
01/15/15 09:30
01/22/15 02:58
193-39-5
Isophorone
ND ug/L
10.0
0.89
1
01/15/15 09:30
01/22/15 02:58
78-59-1
Naphthalene
ND ug/L
5.0
0.34
1
01/15/15 09:30
01/22/15 02:58
91-20-3
Nitrobenzene
ND ug/L
5.0
1.1
1
01/15/15 09:30
01/22/15 02:58
98-95-3
.2-Nitrophenol
ND ug/L
5.0
0.91
1
01/15/15 09:30
01/22/15 02:58
88-75-5
4-Nitrophenol
ND ug/L
50.0
4.1
1
01/15/15 09:30
01/22/15 02:58
100-02-7
N-Nitrosodimethylamine
ND ug/L
5.0
0.91
1
01/15/15 09:30
01/22/15 02:58
62-75-9
N-Nitroso-di-n-propylamine
ND ug/L
5.0
0.99
1
01115/15 09:30
01/22/15 02:58
621-64-7
N-Nitrosodiphenylamine
ND ug/L
10.0
1.0
1
01/15/15 09:30
01/22/15 02:58
86-30-6
Pentachlorophenol
ND ug/L
10.0
4.6
1
01/15/15 09:30
01/22/15 02:58
87-86-5
Phenanthrene
ND ug/L
5.0
0.22
1
01/15/15 09:30
01/22/15 02:58
85-01-8
Phenol
ND ug/L
5.0
1.9
1
01/15/15 09:30
01/22/15 02:58
108-95-2
Pyrene
ND ug/L
5.0
0.19
1
01/15/15 09:30
01/22/15 02:58
129-00-0
1,2,4-Trichlorobenzene
ND ug/L
5.0
0.98
1
01/15/15 09:30
01/22/15 02:58
120-82-1
2,4,6-Trichlorophenol
ND ug/L
10.0
1.3
1
01/15/15 09:30
01/22/15 02:58
88-06-2
Surrogates
Nitrobenzene-d5 (S)
39 %
10-120
1
01/15115 09:30
01/22/15 02:58
4165-60-0
2-Fluorobiphenyl (S)
39 %
15-120
1
01/15115 09:30
01/22/15 02:58
321-60-8
Terphenyl-d14 (S)
66 %
11-131
1
01/15/15 09:30
01/22/15 02:58
1718-51-0
Phenol-d6 (S)
18 %
10-120
1
01/15/15 09:30
01/22/15 02:58
13127-68-3
2-Fluorophenol (S)
23 %
10-120
1
01/15/15 09:30
01/22/15 02:58
367-12-4
2,4,6-Tribromophenol (S)
58 %
10-137
1
01/15/15 09:30
01/22/15 02:58
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
ND ug/L
2.0
1.7
1
01/14/1519:54
71A3-2
Bromodichloromethane
ND uglL
2.0
1.7
1
01/1411519:54
75-27-4
Bromoform
ND ug/L
2.0
1.5
1
01/14/1519:54
75-25-2
Bromomethane
ND ug/L
2.0
1.0
1
01/1411519:54
74-83-9
Carbon tetrachloride
ND ug/L
2.0
1.9
1
01/14/15 19:54
56-23-5
Chtorobenzene
ND uglL
2.0
1.7
1
01114/15 19:54
108-90-7
Chloroethane
ND ug/L
2.0
1.6
1
01114/1519:54
75-00-3
Chloroform
ND ug/L
2.0
1.9
1
01114/1519:54
67-66-3
Chloromethane
r;
ND ug1L
2.0
1.5
1
01/14/1519:54
74-87-3
REPORT OF LABORATORY
ANALYSIS
This report
shall not be reproduced, except in full,
Date: 01 /29/2015 05:12 PM
without the written
consent of Pace Analytical Services, Inc..
Page 13 of 40

aceAnalytical
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ANALYTICAL RESULTS
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(335)62M921
Sample: G-3
Lab ID: 92233032003
Collected:
01/13/15 10:00
Received: 01/13/15 11:30 Matrix: Water
Report
s Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624
Dibromochloromethane
NO ug/L
2.0
1.8
1
01/14/15 19:54
124-48-1
i,2-Dichlorobenzene
ND ug/L
2.0
1.5
1
0111411519:54
95-50-1
1,3-Dichlorobenzene
ND ug/L
2.0
1.5
1
01/1411519:54
541-73-1
1,4-Dichlorobenzene
ND uglL
2.0
1.5
1
01/14/15 19:54
106-46-7
1, 1 -Dichloroethane
ND ug/L
2.0
1.8
1
01114/1519:54
75-34-3
i,2-Dichloroethane
ND ug/L
2.0
1.8
1
01114/1519:54
107-06-2
1. 1 -Dichloroethene
ND ug/L
2.0
1.9
1
01114/1519:54
75-35-4
cis-1,2-Dichloroethene
ND ug/L
2.0
1.8
1
01/14/15 19:54
156-59-2
trans-1,2-Dichloroethene
ND ug1L
2.0
1.8
1
01/14/1519i54
156-60-5
1,2-Dichloropropane
ND ug/L
2.0
1.7
1
01/14/15 19:54
78-87-5
cis- 1,3-Dichloropropene
ND uglL
2.0
1.6
1
01114/1519:54
10061-01-5
'trans- 1, 3-Dichlorop ropene
ND ug/L
2.0
1.6
1
01114/1519:54
10061-02-6
Ethylbenzene
ND ug/L
2.0
1.6
1
01/14/15 19:54
100-41-4
Methylene Chloride
ND ug/L
2.0
1.9
1
01/14/15 19:54
75-09-2
-1 1,2,2-Tetrachloroethane
ND ug/L
2.0
1.5
1
01/1411519:54
79-34-5
Tetrachloroethene
ND ug/L
2.0
1.8
1
01/14/15 19:54
127-18-4
Toluene
ND uglL
2.0
1.6
1
01/1411519:54
108-88-3
1,1,1-Trichloroethane
ND ug/L
2.0
1.9
1
0111411519:54
71-55-6
;1,1,2-Trichloroethane
ND ug/L
2.0
1.7
1
01/1411519:54
79-00-5
Trichloroethene
ND ug/L
2.0
1.8
1
01/1411519:54
79-01-6
Trichlorofluoromethane
ND ug/L
2.0
1.7
1
01/14/15 19:54
75-69-4
Vinyl chloride
ND ug/L
2.0
1.5
1
01/14/15 19:54
75-01-4
Surrogates
4Bromo@uorobenzene (S)
94 %
70-130
1
01/14/15 19:54
46G-00-4
lroluene-dB (S)
94 %
70-130
1
01/14/15 19:54
2037-26-5
I,2-Dichloroethane-d4 (S)
102 %
70-130
1
01/14115 19:54
17060-07-0
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 20.7 mg1L 2.8 2.8 1 01/15/15 04:49
9040 pH Analytical Method: EPA 9040
PH 7.6 Std, Units 0.10 0,10 1 01/14/15 12:48 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Elate: 01 /29/2015 05:12 PM without the written consent of Pace Analytical Services. Inc.. Page 14 of 40

Pace Analytical Services, Inc.
aceMalytica!
205 East Meadow Road - Suite A
Eden, NC 27288
wwwpeceiaba.cant
f
[phone]
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
QC Batch: GCSV/20072
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664B
Analysis Description:
1664 HEM, Oil and Grease
Associated Lab Samples: 92233032001, 92233032002, 92233032003
METHOD BLANK: 1370632
Matrix: Water
Associated Lab Samples: 92233032001, 92233032002, 92233032003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Oil and Grease mg/L
ND 5.0 01/15/15 08:19
LABORATORY CONTROL SAMPLE: 1370633
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Oil and Grease mg/L
40 37A
94 76-114
MATRIX SPIKE SAMPLE: 1370634
92233081002 Spike
MS MS
% Rec
Parameter Units
Result Conc.
Result % Rec
Limits Qualifiers
Oil and Grease mg/L
32.1 40
66.7 86
78-114
Results presented on this page am in the units indicated by the "Units' cotumn except whore an alternate unit is presented to the right of the rewit.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 40

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QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
'Pace Project No.: 92233032
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QC Batch: MPRP/17719
Analysis Method: EPA200.7
QC Batch Method: EPA200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92233032001, 92233032002, 92233032003
METHOD BLANK: 1370022
Matrix: Water
Associated Lab Samples: 92233032001, 92233032002, 92233032003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Cadmium
mg/L
ND
0.0010
01/14/15 22:31
Chromium
mg/L
ND
0.0050
01/14/15 22:31
Copper
mg/L
ND
0.0050
01/14/15 22:31
Lead
mg/L
ND
0.0050
01/14/15 22:31
Nickel
mg/L
ND
0.0050
01/14/15 22:31
Silver
mg/L
ND
0.0050
01114M 5 22:31
Zinc
mg/L
ND
0.010
01/14/15 22:31
'LABORATORY CONTROL SAMPLE:
1370023
Spike
LCS
LCS %
Rec
Parameter
Units
Cone.
Result
% Rec Limits Qualifiers
Cadmium
mg/L
.5
0,49
97
85-115
Chromium
mg/L
.5
0,48
96
85-115
Copper
mg/L
.5
0.50
99
85-115
Lead
mg/L.
.5
0A7
95
85-115
Nickel
mg/L
.5
0.48
96
W115
Silver
mg/L
.25
0.24
97
85-115
Zinc
mg/L
.5
0.46
93
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1370024
1370025
MS
MSD
92232810001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Cadmium
mg/L
ND
.5
.5 0.49
0.49
97
98
70-130
1
20
Chromium
mg/L
ND
.5
.5 0.48
0.48
96
96
70-130
0
20
Copper
mg/L
21.7 ug1L
.5
.5 0.52
0.52
100
100
70-130
0
20
'Lead
mg/L
ND
.5
.5 0.48
0.48
96
96
70-130
1
20
Nickel
mg/L
ND
.5
.5 0.48
0.49
96
97
70-130
1
20
Silver
mg/L
ND
.25
.25
0.24
0.24
97
97
70-130
0
20
Zinc
mg/L
289 ug/L
.5
.5 0.75
0.76
93
94
70-130
1
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1370026
1370027
MS
MSD
92233037001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Cadmium
mg/L
ND
.5
.5 0.48
0.49
97
98
70-130
2
20
Chromium
mgfL
ND
.5
.5 0.48
0.48
95
96
70-130
1
20
Results presented on this page ere in the units Indicated by the 'Units' column except when an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 40
iy
1

lceAn'alytical'
www.Pacem&com
I ,
E
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1370026
1370027
MS
MSD
92233037001 Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Copper
mg/L
14.8 ug/L
.5 .5
0.51
0.52
99
100
70-130
1
20
Lead
mg/L
ND
.5 .5
0.49
0.49
97
97
70-130
1
20
Nickel
mg/L
ND
.5 .5
0.48
0.49
96
97
70-130
2
20
Silver
mg/L
ND .25
.25
0.24
0.24
97
98
70-130
1
20
Zinc
mg/L
27.1 ug/L
.5 .5
0.49
0.50
92
94
70-130
2
20
Results presented on this page are in the units indicated by the'UnIW column except where an attomate unit Is presented to the right of the result -
REPORT OF LABORATORY ANALYSIS
'this report shall not be reproduced, except in full,
Date: 01/29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc..
Page 17 of 40

aceAnalytical
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QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
QC Batch: MSV/29994 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92233032003
METHOD BLANK: 1370212
Associated Lab Samples: 92233032003
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
2.0
01/14/15 14:53
1,1,2,2-Tetrachloroethane
ug/L
ND
2.0
01114/1514:53
1,1,2-Trichloroethane
ug/L
ND
2.0
01/14/15 14:53
1,1-Dichloroethane
ug1L
ND
2.0
01/1411514:53
1,1-Dichloroethene
ug/L
ND
2.0
01/14/15 14:53
1,2-Dichlorobenzene
ug/L
ND
2.0
01/14/15 14:53
1,2-Dichloroethane
ug1L
ND
2.0
01/14/15 14:53
1,2-Dichloropropane
ug/L
ND
2.0
01/14/15 14:53
1,3-Dichlorobenzene
ug/L
ND
2.0
01/1411514:53
1,4-Dichlorobenzene
ug/L
ND
2.0
01/14/15 14:53
Benzene
ug/L
ND
2.0
01/1411514:53
Bromodichloromethane
ug/L
ND
2.0
01/1411514:53
Bromoform
ug/L
ND
2.0
01114/1514:53
Bromomethane
ug/L
ND
2.0
01114/1514:53
Carbon tetrachloride
ug/L
ND
2.0
01/14/15 14:53
Chlorobenzene
ug/L
ND
2.0
01/14/15 14:53
Qhloroethane
ug/L
ND
2.0
01/14/15 14:53
Chloroform
ug/L
ND
2.0
01/14/15 14:53
Chloromethane
ug/L
ND
2.0
01/14/15 14:53
cis-1,2-Dichloroethene
ug/L
ND
2.0
01/1411514:53
cis- 1,3-Dichloropropene
ug1L
ND
2.0
0111411514:53
Dibromochloromethane
ug/L
ND
2.0
01/14/15 14:53
Ethylbenzene
ug/L
ND
2.0
01/1411514:53
Methylene Chloride
ug/L
ND
2.0
01/14/15 14:53
Tetrachloroethene
ug/L
ND
2.0
01/14/15 14:53
Toluene
ug/L
ND
2.0
01/14/1514*53
trans-1,2-Dichloroethene
ug/L
ND
2.0
01/14/15 14:53
trans- 1, 3-Dichloropropene
ug/L
ND
2.0
01/14/15 14:53
Trichloroethene
ug/L
ND
2.0
01/14/15 14:53
Trichlorofluoromelhane
ug/L
ND
2.0
01/14/15 14:53
-Vnyl chloride
ug/L
ND
2.0
01/14/15 14:53
1,2-Dichloroethane-d4 (S)
%
101
70-130
01/14/15 14:53
4-Bromofluorobenzene (S)
%
104
70-130
01/14/15 14:53
toluene-d8 (S)
%
95
70-130
01/14/15 14:53
LABORATORY CONTROL SAMPLE: 1370213
Spike LCS
Parameter Units Conc. Result
1,1,1-Trichloroethane ug/L 20 19.1
•1,1,2,2-Tetrachloroethane ug/L 20 20.7
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NO 27288
[phone]
Qualifiers
LCS % Rec
% Rec Limits Qualifiers
96 52-162
103 46-157
Results presented on this page are In the units Indicated by the'Untts' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 40

aceAnalytical`
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Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
LABORATORY CONTROL SAMPLE:
1370213
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
1,1,2-Trichloroethane
ug/L
20
20.8
104
52-150
1,1-Dichloroethane
ug/L
20
19.5
97
59-155
1,1-Dichloroethene
ug/L
20
18.8
94
1-234
9,2-Dichlorobenzene
ug/L
20
21.8
109
18-190
1,2-Dichloroethane
ug/L
20
17.5
87
49-155
1,2-Dichloropropane
ug/L
20
19.6
98
1-210
1,3-Dichlorobenzene
ug/L
20
21.6
108
59-156
1,4-Dichlorobenzene
ug/L
20
21.7
109
18-190
Benzene
ug/L
20
21.3
106
37-151
Bromodichloromethane
ug/L
20
17.5
88
35-155
Bromoform
ug[L
20
19.6
98
45-169
Bromomethane
ug/L
20
18.5
93
1-242
Carbon tetrachloride
ug/L
20
20.3
101
70-140
Chlorobenzene
ug/L
20
21.1
106
37-160
Chloroelhane
ug/L
20
17.5
87
14-230
Chloroform
ug/L
20
17.7
89
51-138
Chloromethane
ug/L
20
18.3
92
1-273
cis-1,2-Dichloroethene
ug/L
20
19.5
98
68-146
cis-1,3-Dichloropropene
ug/L
20
19.7
99
1-227
Dibromochloromethane
ug/L
20
19.3
96
53-149
Ethylbenzene
ug/L
20
20.9
104
37-162
Methylene Chloride
ug/L
20
17.6
88
1-221
Tetrachloroethene
ug/L
20
21.3
107
64-148
Toluene
ug/L
20
20.0
100
47-150
tran5-1,2-Dichloroethene
ug/L
20
20.3
101
54-156
trans-1,3-Dichloropropene
ug/L
20
20.1
101
17-183
Trichloroethene
ug/L
20
21.1
105
71-157
Trichlorofluoromethane
ug/L
20
20.2
101
17-181
Vinyl chloride
ug/L
20
18.9
95
1-251
1,2-Dichloroethane-d4 (S)
%
97
70-130
4-Bromofluorobenzene (S)
%
104
70-130
Toluene-d8 (S)
%
96
70-130
MATRIX SPIKE SAMPLE: 1370215
Parameter
1,1,1-Trichloroethane
ug/L
1,1,2,2-Tetrachloroethane
ug/L
1,1,2-Trichloroethane
ug/L
Al. 1-Dichloroethane
ug/L
1, 1 -Dichloroethene
ug/L
1,2-Dichlorobenzene
ug/L
1,2-Dichloroethane
ug/L
1,2-Dichloropropane
ug/L
1,3-Dichlorobenzene
ug/L
92232098001
Units Result
Spike
Cone.
MS MS
Result % Rec
ND
ND
ND
ND
ND
ND
ND
ND
ND
% Rec
Limits Qualifiers
20
21.3
106
46-171
20
20.3
102
73-159
20
21.4
107
64-152
20
21.2
106
43-172
20
21.3
106
48-189
20
21.8
109
54-154
20
19.0
95
42-171
20
20.6
103
55-157
20
21.7
108
57-148
Results presented on this page are in the units Indicated by the'UnIW column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Date: 01/29/2015 05:12 PM
s
II
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 40

/�IaceA-nalyficale
! aWW.peoefahscaa
i
i
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
MATRIX SPIKE SAMPLE:
1370215
92232098001
Spike
MS
MS
% Rec
Parameter
Units Result
Conc.
Result
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
ND
20
21.3
106
58-149
Benzene
ug/L
ND
20
22A
112
54-163
Bromodichloromethane
ug/L
ND
20
19.2
96
56-152
Bromoform
ug/L
ND
20
20.3
102
53-151
Bromomethane
ug/L
ND
20
16.8
84
10-200
Carbon tetrachloride
ug/L
ND
20
23.4
117
41-175
Chlorobenzene
ug/L
ND
20
22.1
110
67-152
Chloroethane
ug/L
ND
20
19.0
95
23-200
Chloroform
ug/L
ND
20
18.6
93
51-166
Chloromethane
ug/L
ND
20
17.3
87
40-175
cis-1,2-Dichloroethene
ug/L
ND
20
21.3
107
45-174
cis-1,3-Dichloropropene
ug/L
ND
20
17.5
87
38-146
Dibromochloromethane
ug/L
ND
20
20.5
102
65-144
Ethyibenzene
ug/L
ND
20
22.3
112
57-152
Methylene Chloride
ug/L
ND
20
19.2
93
40-167
Tetrachloroethene
ug/L
ND
20
22.5
112
59-155
Toluene
ug/L
ND
20
21.7
109
47-162
trans-1,2-Dichbroethene
ug/L
ND
20
21.6
108
47-178
trans-1,3-Dichloropropene
ug/L
ND
20
18.5
93
39-148
Trichloroethene
ug/L
ND
20
23.2
116
60-153
Trichlorofluoromethane
ug/L
ND
20
23.6
118
42-199
Vinyl chloride
ug/L
ND
20
20.0
100
46-176
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene -dB (S)
%
95
70-130
SAMPLE DUPLICATE: 1370214
92232810002
Dup
Max
Parameter
Units Result
Result
RPD
RPD
Qualifiers
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
.1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
'1,3-Dichlorobenzene
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
1.7J
30
Benzene
ug/L
ND
ND
30
Bromodichloromethane
ug/L
2.4
2.6
5
30
Bromoform
ug/L
ND
ND
30
Bromomethane
ug/L
ND
ND
30
Carbon tetrachloride
ug/L
ND
ND
30
Chlorobenzene
ug/L
ND
ND
30
Results presented on this page are In the units indicated by the "Units" column except when: an altemate unit Is
presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 01/29/2015 05:12 PM
without the written consent of Pace Analytical Services, Inc..
Page 20 of 40

aceAna/j &ca /
1! www.paDebbs.com
i
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
SAMPLE DUPLICATE: 1370214
Parameter
knits
92232810002
Result
Dup
Result
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
12.5
12.5
Chloromethane
ugtL
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ugfL
ND
ND
Dibromochloromethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans-1,3-Dichloropropene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
97
99
4-Bromofluorobenzene (S)
%
96
93
Toluene -dB (S)
%
94
95
RPD
0
1
4
1
Max
RPD
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the 'Units" column except where an alternate unit Is presented to the right of the result.
Date: 01/29/2015 05:12 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 21 of 40

5 aceAnalytical e
i
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
.QC Batch: MSV/30026 Analysis Method: EPAfi24
QC Batch Method: EPAfi24 Analysis Description: 624 MSV
Associated Lab Samples: 92233032001, 92233032002
METHOD BLANK: 1372627
Associated Lab Samples: 92233032001, 92233032002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
2.0
01/16/15 23:18
1,1,2,2-Tetrachloroethane
ug/L
ND
2.0
01/16/15 23:18
1,1,2-Trichloroethane
ug/L
ND
2.0
01/16/15 23:18
1,1-Dichloroethane
ug/L
ND
2.0
01/16/15 23:18
1,1-Dichloroethene
ug/L
ND
2.0
0111611523:18
1,2-Dichlorobenzene
uglL
ND
2.0
01/1611523:18
1,2-Dichloroethane
uglL
ND
2.0
01/1611523:18
1,2-Dichloropropane
ug/L
ND
2.0
01/16/15 23:18
1,3-Dichlorobenzene
ug/L
ND
2.0
01/16/15 23:18
1,4-Dichlorobenzene
ug/L
ND
2.0
01/16/15 23:18
Benzene
ug/L
ND
2.0
01/16/15 23:18
Bromodichloromethane
ug/L
ND
2.0
01/16/15 23:18
Bromoform
uglL
ND
2.0
01/16/15 23:18
Bromomethane
ug/L
ND
2.0
01/16/15 23:18
.Carbon tetrachloride
ug/L
ND
2.0
01/16/15 23:18
Chlorobenzene
ug/L
ND
2A
01/16/15 23:18
Chloroethane
ug/L
ND
2.0
01/16/15 23:18
Chloroform
ug/L
ND
2.0
01/16/15 23:18
Chloromethane
ug/L
ND
2.0
01/16/15 23:18
cis-1,2-Dichloroethene
uglL
ND
2.0
01/16/15 23:18
cis- 1, 3-Dichloropropene
ug/L
ND
2.0
01/16/15 23:18
Dibromochloromethane
ug/L
ND
2.0
01/16/15 23:18
Ethylbenzene
ug/L
ND
2.0
01/16/15 23:18
Methylene Chloride
ug/L
ND
2.0
01/16/15 23:18
Tetrachloroethene
ug/L
ND
2.0
01/16/15 23:18
Toluene
ug/L
ND
2.0
01/16/15 23:18
trans-1,2-Dichloroethene
ug/L
ND
2.0
01/1611523:18
trans-1,3-Dichloropropene
ug/L
ND
2.0
0111611523:18
Trichloroethene
ug/L
ND
2.0
01/16/15 23:18
Trichlorofluoromethane
ug/L
ND
2.0
01/16/15 23:18
Vnyl chloride
uglL
ND
2.0
01/16/15 23:18
1,2-Dichloroelhane-d4(S)
%
93
70-130
01/1611523:18
4-Bromofluorobenzene (S)
%
106
70-130
01/16/15 23:18
Toluene-d8 (S)
%
93
70-130
01/16/15 23:18
LABORATORY CONTROL_ SAMPLE: 1372628
Parameter
Units
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)523-892 t
Qualifiers
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
'i,1,1-Trichloroethane ug/L 20 18.7 94 52-162
1,1,2,2-Tetrachloroethane ug/L 20 19.2 96 46-157
Results presented on this page are in the units Indicated by the "Units" column eseept where an aliemata unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull,
Date: 01 /29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 40

CeAnalytical.
` Wompacelabxcam
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
"Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
LABORATORY CONTROL SAMPLE: 1372628
Parameter
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
i ,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
'Chiorobenzene
Chloroethane
Chloroform
Chloromethane
Cis-1,2-Dichloroethene
cis-1, 3-Dichloropropene
Dibromochloromethene
Ethylbenzene
Methylene Chloride
Tetrachloroethene
Toluene
trans-i,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trich lorofluoromethane
Vinyl chloride
1,2-Dichloroethene-d4 (S)
4-Bromofiuorobenzene (S)
Toluene -dB (S)
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug1L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
o�
o�
o�
QUALITY CONTROL DATA
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
20
20.0
100
52-150
20
18.5
92
59-155
20
17.5
88
1-234
20
20.6
103
18-190
20
17.5
87
49-155
20
19.2
96
1-210
20
20.3
101
59-156
20
20.2
101
18-190
20
20.1
100
37-151
20
17.4
87
35-155
20
18.6
93
45-169
20
11.9
59
1-242
20
19.6
98
70-140
20
19.9
100
37-160
20
14.2
71
14-230
20
17.3
86
51-138
20
13.8
69
1-273
20
19.3
97
68-146
20
18.8
94
1-227
20
18.6
93
53-149
20
19.6
98
37A 62
20
18.2
91
1-221
20
19.7
99
64-148
20
19.5
98
47-150
20
19.7
99
54-156
20
19.4
97
17-183
20
20.2
101
71-157
20
18.5
93
17-181
20
15.5
77
1-251
99
70-130
103
70-130
97
70-130
Qualifiers
MATRIX SPIKE SAMPLE_
1372633
92232777002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
NO
20
19.6
98
46-171
1,1,2,2-Tetrachloroethane
ug/L
ND
20
18.3
92
73-159
1,1,2-Trichloroethane
ug/L
ND
20
20.2
101
64-152
,1,1-Dichloroethene
ug/L
ND
20
19.7
99
43-172
1,1-Dichloroethene
ug/L
ND
20
19.3
97
48-189
1,2-Dichlorobenzene
ug/L
ND
20
16.0
80
54-154
1,2-Dichloroethane
ug/L
ND
20
17.0
85
42-171
1,2-Dichloropropane
ug/L
ND
20
20.0
100
55-157
1,3-Dichlorobenzene
ug/L
NO
20
15.9
79
57-148
Results presented on this page ere In the units Indicated by the "Units" column except where an alternate unit is presented to the right ai the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 40

aceAnalyflcal.
www.paaelabsmm
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
MATRIX SPIKE SAMPLE: 1372633
Parameter
1,4-Dichlorobenzene
Benzene
Bromod ichloromethane
Bromoform
8romomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethene
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Ethylbenzene
Methylene Chloride
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans- 1,3-Dichloropropene
Trichloroethene
Trich lorofluoromethane
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-t8 (S)
a
SAMPLE DUPLICATE: 1372632
Parameter
1,1,1-Trich loroethane
.1,1, 2,2-Tetrachlo roethane
1,1,2-Trcchloroethane
1,1-Dichloroethane
-1,1-Dichloroethene
'1, 2-Dichlorobenzene
;1,2-Dichloroethane
,1, 2-Dichloropropane
.1, 3-Dick lorobenzene
-1,4-Dichlorobenzene
Benzene
Bromodichloromethane
Bromoform
8romomethane
Carbon tetrachloride
Chlorobenzene
QUALITY CONTROL DATA
Units
92232777002
Result
Spike
Cone.
MS
Result
ug[L
NO
20
16.2
ug1L,
NO
20
22.2
ug/L
NO
20
18.7
ug/L
NO
20
19A
ug/L
NO
20
7.9
ug/L
NO
20
20.4
ug/L
NO
20
19.4
ug/L
NO
20
19.0
ug1L
24.2
20
38.5
ug/L
NO
20
13.9
ug/L
NO
20
19.8
ug/L
ND
20
18.6
uglL
ND
20
19.3
ug/L
NO
20
17.7
ug/L
NO
20
16.3
ug/L
NO
20
18.5
ug/L
NO
20
21.3
ug/L
NO
20
19.8
ug/L
NO
20
18.7
ug/L
NO
20
22.3
ug/L
NO
20
20.9
ug/L
NO
20
18.5
MS
% Rec
% Rec
Limits
81 58-149
11'1 54-163
93 56-152
97 53-151
39 10-200
102 41-175
97 67-152
95 23-200
71 51-166
70 40-175
99 45-174
93 38-146
96 65-144
88 57-152
78 40-167
93 59-155
101 47-162
99 47-178
93 39-148
112 60-153
105 42-199
92 46A 76
88 70-130
95 70-130
95 70-130
92232710001
Dup
Max
Units
Result
Result RPD
RPD Qualifiers
ug/L
NO
NO
30
ug1L
NO
NO
30
ug/L
NO
NO
30
ug1L
NO
NO
30
u911-
NO
NO
30
ug/L
NO
NO
30
ug/L
NO
NO
30
ug/L
NO
NO
30
ug/L
NO
NO
30
ug/L
NO
NO
30
ug/L
NO
ND
30
ug/L
NO
NO
30
ug/L
NO
NO
30
ug/L
NO
NO
30
ug/L
NO
NO
30
ug/L
NO
NO
30
Results presented on this page are In the units Indicated by the "Unite column except where an altemabe unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc..
Qualifiers
Page 24 of 40

Analytical'
www.PaMkb&o=
1
QUALITY CONTROL
DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
SAMPLE DUPLICATE: 1372632
_
92232710001
Dup
Parameter
Units
Result
Result
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
6.2
6.2
Chloromethane
ug/L
ND
ND
cis- 1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ugfL
ND
ND
Dibromochloromethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans-1,3-Dichloropropene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
99
97
4-Bromofluorobenzene (S)
%
96
96
Toluene-d8 (S)
%
94
94
RPD
0
2
1
0
Max
RPD
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Pace Ana"cal services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Qualifiers
Results presented on this papa are in the units Indicated by the "Units" coturtm except where an alternate unit is presented to the right of the result
a REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
v
Date: 01/29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc..
Page 25 of 40

ceAna1j&a1 *
www.pecelabs.can
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
QC Batch: OEXT/32333 Analysis Method: EPA 608
QC Batch Method: EPA 3510 Analysis Description: 608 GCS Pest PCB
Associated Lab Samples: 92233032001, 92233032002, 92233032003
METHOD BLANK: 1371575
Associated Lab Samples:
Parameter
4,4'-DDD
4,4'-DDE
4,4'-DDT
Aldrin
alpha-BHC
beta-BHC
Chlordane (Technical)
delta-BHC
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Toxaphene
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
Matrix: Water
92233032001,92233032002,92233032003
Blank
Units Result
Reporting
Limit Analyzed Qualifiers
ug/L
NO
0.050
01/20/1519:56
ug/L
NO
0.050
01120/1519:56
uglL
NO
0.050
01/20/1519:56
ug/L
NO
0.050
0112011519:56
ug/L
NO
0,050
0112011519:56
uglL
NO
0,050
01/20/1519:56
ug/L
NO
0.50
01120/1519:56
ug/L
NO
0.050
01/2011519:56
ug/L
NO
0.050
01/20/1519:56
ug/L
NO
0.050
01/2011519:56
ug/L
NO
0.050
01/2011519:56
ug/L
NO
0.050
01/2011519:56
ug/L
ND
0.050
01/20/1519:56
ug/L
NO
0.050
01/20/1519:56
ug l-
NO
0.050
01/20/15 19:56
ug/L
NO
0.050
01/20/1519:56
ug/L
NO
0.050
01/20/1519:56
uglL
NO
0.50
01/20/1519:56
ug/L
NO
0.50
01120/1519:56
ug/L
NO
0.50
01120/1519:56
uglL
NO
0.50
01120/1519:56
ug/L
NO
0.50
01120/1519:56
uglL
NO
0.50
01/2011519:56
ug/L
NO
0.50
01120/1519:56
ug/L
NO
0.50
01/20/1519:56
%
76
20-138
01/2011519:56
%
82
20-110
01 /20/15 19:56
LABORATORY CONTROL SAMPLE: 1371576
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
4,4'-DDD
uglL
.25
0.22
89
31-141
4,4'-DDE
ug/L
.25
0.21
85
30-145
4,4'-DDT
ug/L
.25
0.21
85
25-160
Aldrin
ug/L
.25
0.18
72
42-122
alpha-BHC
ug/L
.25
0.24
98
37-134
beta-BHC
ug/L
.25
0.26
104
17-147
delta-BHC
ug/L
.25
0,26
103
19-140
Dieldrin
uglL
.25
0.22
90
36-146
Endosulfan I
ug/L
.25
0.23
93
45-153
Results presented on this page are in the units Indicated by the "units" cotumn except where an alternate unit is presented to the right of the result
i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 26 of 40

Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
aceAnalytical ` Eden, NC 27268
1
"WW'0' =n [phone]
QUALITY CONTROL DATA
Project. 2014 SEMI-ANNUAL
.Pace Project No.: 92233032
LABORATORY CONTROL SAMPLE:
Parameter
1371576
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Qualifiers
Endosulfan 11
ug/L
.25
0.24
96
1-202
Endosulfan sulfate
ug/L
.25
0.23
94
26-144
Endrin
ug/L
.25
0.23
92
30-147
Endrin aldehyde
ug/L
25
0.19
76
50-150
gamma-BHC (Lindane)
ug/L
.25
0.24
98
32-127
Heptachlor
ug/L
.25
0.18
73
34-111
Heptachlor epoxide
ugfL
.25
0,22
90
41-126
Decachlorobiphenyl (S)
%
86
20-138
Tetrachloro-m-xylene (S)
°%
96
20-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1371577
1371578
MS
MSD
92233037001
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
e% Rec e% Rec
Limits
RPD
RPD Qual
4,4'-DDD
ug1L
ND
.5
.5
0.41
0.41
84
82
31-141
2
30
4,4'-DDE
ug/L
ND
.5
.5
0.38
0.39
77
78
30-145
1
30
4,4'-DDT
ug/L
ND
.5
.5
0.36
0.39
73
79
25-160
8
30
Aldrin
ug/L
ND
.5
.5
0.39
0.40
78
81
42-122
4
30
alpha-BHC
ug/L
ND
.5
.5
0,42
0.40
84
81
37-134
4
30
beta-BHC
ug/L
ND
.5
.5
0.55
0.54
110
109
17-147
2
30
delta-BHC
ug/L
ND
.5
.5
0.47
0.45
94
90
19-140
5
30
Dieldrin
ug/L
ND
.5
.5
0.39
0.40
80
80
36-146
0
30
Endosulfan I
ug/L
ND
.5
.5
0.42
0.42
85
84
45-153
1
30
Endosulfan II
ug/L
ND
.5
.5
0.41
0.40
83
81
1-202
3
30
Endosulfan sulfate
ug/L
ND
.5
.5
0.43
0.41
87
83
26-144
4
30
Endrin
ug/L
ND
.5
.5
0.44
0,44
89
89
30-147
0
30
Endrin aldehyde
ug/L
ND
.5
.5
0.34
0.35
69
71
50-150
3
30
gamma-BHC (Lindane)
ug/L
ND
.5
.5
0.41
0.41
84
82
32-127
2
30
Heptachlor
ug/L
ND
.5
.5
0.38
0.39
77
80
34-111
3
30
Heptachlor epoxide
ug/L
ND
.5
.5
0.39
0.38
79
78
41-126
2
30
Decachlorobiphenyl (S)
°%
58
28
20-138
Tetrachloro-m-xylene (S)
%
84
84
20-110
Results presented on this page are in the units Indicated by the -Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /29/2016 05:12 PM without the written consent of Pace Analytical Services, Inc- Page 27 of 40

/�WceAn'afyficaf'
M7YW.p80elai7A00nT
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
QC Batch: OEXT/32298 Analysis Method: EPA625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92233032001, 92233032002, 92233032003
METHOD BLANK: 1370688 Matrix: Water
Associated Lab Samples: 92233032001, 92233032002, 92233032003
Blank Reporting
Parameter Units Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
01/15/15 23:12
2.4,6-Trichlorophenol
ug/L
ND
10.0
01/15/15 23:12
2,4-Dichlorophenol
ug/L
ND
5.0
01/15/15 23:12
2,4-Dimethylphenol
ug/L
ND
10.0
01/15/15 23:12
2,4-Dinitrophenol
ug/L
ND
50.0
01/15/15 23:12
2,4-Dinitrotoluene
ug/L
ND
5.0
01/15/15 23:12
2,6-Dinitrotoluene
ug/L
ND
5.0
01/15/15 23:12
2-Chloronaphthalene
ug/L
ND
5.0
01/15/15 23:12
2-Chlorophenol
ug/L
ND
5.0
01/15/15 23:12
2-Nitrophenol
ug/L
ND
5.0
01/15/15 23:12
3,3'-Dichlorobenzidine
ug/L
ND
25.0
01/15/15 23:12
4,6- Din itro-2-methylphenol
ug/L
ND
20.0
01/15115 23:12
4-Bromophenylphenyl ether
ug/L
ND
5.0
01/15115 23:12
4-Chloro-3-methylphenol
ug/L
ND
5.0
01/15/15 23:12
4-Chlorophenylphenyl ether
ug/L
ND
5.0
01/15/15 23:12
4-Nitrophenol
ug/L
ND
50.0
01/15/15 23:12
Acenaphthene
ug/L
ND
5.0
01115/15 23.12
Acenaphthylene
ug/L
ND
5.0
01/15/15 23:12
Anthracene
ug/L
ND
5.0
01/15/15 23:12
Benzo(a)anthracene
ug/L
ND
5.0
01/15/15 23:12
Benzo(a)pyrene
ug/L
ND
5.0
01/15/15 23:12
Benzo(b)fluoranthene
ug/L
ND
5.0
01/15/15 23:12
Benzo(g,h,i)peryiene
ug/L
ND
5.0
01/15/15 23:12
Benzo(k)fluoranthene
ug/L
ND
5.0
01/15/15 23:12
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
01/15/15 23:12
bis(2-Chloroethyl) ether
ug/L
ND
5.0
01/15/15 23:12
bis(2-Chloroisopropyl) ether
ug/L
ND
5.0
01/15/15 23:12
6is(2-Ethyihexyl)phthalate
ug/L
ND
5.0
01/15/15 23:12
Butylbenzylphthalate
ug/L
ND
5.0
01/15/15 23:12
Chrysene
ug/L
ND
5.0
01/1511523:12
Di-n-butylphthalate
ug/L
ND
5.0
01/1511523:12
Di-n-octylphthalate
ug/L
ND
5.0
01/15/15 23:12
Dibenz(a,h)anthracene
ug/L
ND.
5.0
01/1511523:12
Diethylphthalate
ug/L
ND
5.0
01/1511523:12
Dimethylphthalate
ug/L
ND
5.0
01/1511523:12
Fluoranthene
ug/L
ND
5.0
01/1511523:12
Fluorene
ug/L
ND
5.0
01/15/15 23:12
Hexachloro-1,3-butadiene
ug/L
ND
5.0
01/1511523A2
Hexachiorobenzene
ug/L
ND
5.0
01/15/15 23:12
I- lexachlorocyclopentadiene
uglL
ND
10.0
01/15/1523A2
Hexachloroethane
uglL
ND
5.0
01/15/15 23:12
Qualifiers
Results presented on this page ere In the units Indicated by the "Units" column except where an aitemate unit Is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 28 of 40

�WceAn'alyfical*
wwwpacelabs.com
r
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
METHOD BLANK: 1370688
Matrix: Water
Associated Lab Samples: 92233032001, 92233032002, 92233032003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
01/15/15 23:12
Isophorone
ug/L
ND
10.0
01/15/15 23:12
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
01/15/15 23:12
N-Nitrosodimethylamine
ug/L
ND
5.0
01/15/15 23:12
N-Nitrosodiphenylamine
ug/L
ND
10.0
01/15/15 23:12
Naphthalene
ug/L
ND
5.0
01/15/15 23:12
Nitrobenzene
ug/L
ND
5.0
01/15/15 23:12
Pentachlorophenol
ug/L
ND
10.0
01/15/15 23:12
Phenanthrene
ug/L
ND
5.0
01/15/15 23:12
Phenol
ug1L
ND
5.0
01/15/15 23:12
Pyrene
ug/L
ND
5.0
01/15/15 23:12
2,4,6-Tribromophenot (S)
°%
48
10-137
01/15/15 23:12
2-Fluorobiphenyl(S)
°%
45
15-120
01/1511523:12
2-Fluorophenol(S)
e%
24
10-120
01/1511523:12
Nitrobenzene-d5(3)
e%
42
10-120
01/1511523:12
Phenol-d6 (S)
%
16
10-120
01/15/15 23:12
Terphenyl-d14 (S)
e%
76
11-131
01/15/15 23:12
LABORATORY CONTROL SAMPLE:
1370689
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits
Qualifiers
1,2,4-Trichlorobenzene
ug1L
50
24.8
50
44-142
2,4,6-Trichlorophenol
ug1L
50
29.3
59
37-144
2,4-Dichlorophenol
ug/L
50
28.2
56
1-191
2,4-Dimethylphenol
ug/L
50
26.2
52
32-119
2,4-Dinitrophenol
ug/L
250
192
77
1-181
2,4-Dinitrotoluene
ug/L
50
42.9
86
39-139
2,6-Dinitrotoluene
ug1L
50
411
82
50-158
2-Chloronaphthalene
ug/L
50
27.8
56
60-118 L2
2-Chlorophenol
uglL
50
24.5
49
23-134
2-Nitrophenol
ug1L
50
29.2
58
29-182
3,3'-Dichlorobenzidine
ug1L
100
82.4
82
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
86.0
86
1-181
4-Bromophenylphenyl ether
ug/L
50
39.8
80
53-127
4-Chloro-3-methylphenol
uglL
100
58.8
59
22-147
4-Chlorophenylphenyl ether
ug1L
50
36.2
72
25-158
4-Nitrophenol
ug1L
250
81.9
33
1-132
Acenaphthene
ug1L
50
32.6
65
47-145
Acenaphthylene
ug1L
50
32.7
65
33-145
Anlhracene
ug1L
50
43.1
86
1-166
Benzo(a)anthracene
ug1L
50
44.9
90
33-143
Benzo(a)pyrene
ug1L
50
49.1
98
17-163
Benzo(b)fluoranthene
ug/L
50
47.1
94
24-159
Benzo(g,h,i)perylene
ug/L
50
45.1
90
1-219
Results pmsentad on this page are In the units indicated by the'Units' column except where an anemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduoed, except in full,
bate: 01 /29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc..
Page 29 of 40

Pace Analytical Services, Inc.
�laeAirralytrca! 0 205 East Meadow Road - Suite A
Eden, NC 27288
W'e'4moobscom [phone]
i
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
LABORATORY CONTROL SAMPLE: 1370689
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Benzo(k)fluoranthene
ug/L
50
42.4
85
11-162
bis(2-Chloroethoxy)methane
ug/L
50
26.9
54
33-184
bis(2-Chloroethyl) ether
ug/L
50
26.5
53
12-158
6is(2-Chloroisopropyl) ether
ug/L
50
22.0
44
36-166
bis(2-Ethylhexyl)phthalate
ug/L
50
49.3
99
8-158
Butylbenzylphthalate
ug/L
50
49.1
98
1-152
Chrysene
ug/L
50
45.5
91
17-168
Di-n-butylphthalate
ug/L
50
46.7
93
1-118
Di-n-octylphthalate
ug/L
50
59.0
118
4-146
Dibenz(a,h)anthracene
ug/L
50
47.0
94
1-227
Diethylphthalate
uglL
50
43.8
88
1-114
Dimethylphthalate
ug/L
50
40.5
81
1-112
Fluoranthene
ug/L
50
46.5
93
26-137
Fluorene
ug/L
50
38.8
78
59-121
Hexachloro-1,3-butadiene
ug/L
50
24.3
49
24-116
Hexachlorobenzene
ug/L
50
40.6
81
1-152
Hexachlorocyclopentadiene
ug/L
50
24.7
49
25-150
Hexachloroelhane
ug/L
50
21A
42
40-113
lndeno(1,2,3-cd)pyrene
ug/L
50
49.8
100
1-171
lsophorone
ug/L
50
27.4
55
21-196
N-Nitroso-di-n-propylamine
ug/L
50
25.3
51
1-230
N-Nitrosodimethylamine
ug/L
50
16.6
33
25-150
N-Nitrosodiphenylamine
ug/L
50
41.0
82
25-150
Naphthalene
ug/L
50
26.8
54
21-133
Nitrobenzene
ug/L
50
26.5
53
35-180
Pentachlorophenol
ug/L
100
81.1
81
14-176
Phenanthrene
ug/L
50
41.0
82
54-120
Phenol
ug/L
50
11.3
23
5-112
Pyrene
ug/L
50
43.6
87
52-115
2,4,6-Tribromophenol (S)
%
83
10-137
2-Fluorobiphenyl (S)
%
56
15-120
2-Fluorophenol (S)
%
29
10-120
Nitrobenzene-d5 (S)
%
51
10-120
Phenol-d6 (S)
%
20
10-120
Terphenyi-cI14 (S)
%
86
11-131
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
1,2,4-Trichlorobenzene
2,4,6-Trichlorophenol
2,4-Dichlorophenoi
2,4-Dimethylphenol
2,4-Dinitrophenol
1370690
MS
92233032001
Spike
Units
Result
Conc.
ug/L
ND
100
ug/L
ND
100
ug/L
ND
100
ug/L
ND
100
ug/L
ND
500
1370691
MSD
Spike
MS
MSD
MS
MSD
% Rec
Max
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
100
45.3
44.5
45
44
44-142
2
30
100
49.8
50.6
50
51
37-144
2
30
100
48.0
46.1
48
46
1-191
4
30
100
47.2
46.8
47
47
32-119
1
30
500
357
366
71
73
1-181
3
30
Results presented on this page are in the units indicated by the'Units7 column except where an alternate unit is presented to the right of the result
g REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc..
Page 30 of 40

aceAnalytical
www.pacelabs.cam
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1370690
1370691
MS
MSD
92233032001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
2,4-Dinitrotoluene
ug/L
ND
100
100
85.4
86.4
85
86
39-139
1
30
2,6-Dinitrotoluene
ug/L
ND
100
100
77.8
78.7
78
79
50-158
1
30
2-Chloronaphthalene
uglL
ND
100
100
47.0
47.0
47
47
W118
0
30 MO
2-Chlorophenol
ug/L
ND
100
100
43.8
44.4
44
44
23-134
1
30
2-Nitrophenol
ug/L
ND
100
100
49.7
48.0
50
48
29-182
3
30
3,3'-Dichlorobenzidine
ug/L
ND
200
200
159
161
80
80
1-262
1
30
4,6-Dindro-2-methylphenol
ug/L
ND
200
200
165
172
83
86
1-181
4
30
4-Bromophenylphenyl ether
ug/L
ND
100
100
73.5
77.9
73
78
53-127
6
30
4-Chloro-3-methylphenol
ug/L
ND
200
200
112
109
56
55
22-147
3
30
4-Chlorophenylphenyl ether
ug/L
ND
100
100
63.9
66.0
64
66
25-158
3
30
4-Nitrophenol
ug/L
ND
500
500
237
249
47
50
1-132
5
30
Acenaphthene
ug/L
ND
100
100
55.6
55.5
56
56
47-145
0
30
Acenaphthylene
uglL
ND
100
100
56.0
56.0
56
56
33-145
0
30
Anthracene
ug/L
ND
100
100
81.7
84.9
82
85
1-166
4
30
Benzo(a)anthracene
ug/L
ND
100
100
87.2
92.0
87
92
33-143
5
30
Benzo(a)pyrene
ug/L
ND
100
100
91.1
95.0
91
95
17-163
4
30
Benzo(b)fluoranthene
ug/L
ND
100
100
89.8
96.9
90
97
24-159
8
30
Benzo(g,h,i)perylene
uglL
ND
100
100
87.5
87.6
87
88
1-219
0
30
Benzo(k)fluoranthene
ug/L
ND
100
100
81.0
84.2
81
84
11-162
4
30
bis(2-Chloroethoxy)methane
ug/L
ND
100
100
44.4
44.7
44
45
33-184
1
30
6is(2-Chloroelhyl) ether
ug/L
ND
100
100
45.1
45.9
45
46
12-158
2
30
bis(2-Chloroisopropyl) ether
ug/L
ND
100
100
37.2
38.2
37
38
36-166
3
30
bis(2-Ethylhexyl)phthalate
ug/L
ND
100
100
93.4
99.9
93
100
8-158
7
30
Butylbenzylphthalate
ug/L
ND
100
100
94.7
101
95
101
1-152
7
30
Chrysene
ug/L
ND
100
100
87.0
92.4
87
92
17-168
6
30
l3i-n-butylphthalate
ug/L
ND
100
100
89.8
94.8
90
95
1-118
5
30
Di-n-octylphthalate
ug/L
ND
100
100
111
114
111
114
4-146
3
30
Dibenz(a,h)anthracene
ug1L
ND
100
100
93.2
92.6
93
93
1-227
1
30
biethylphthalate
ug/L
ND
100
100
84.6
87.6
85
88
1-114
4
30
Dimethylphthalate
ug1L
ND
100
100
77.1
81.1
77
81
1-112
5
30
Fluoranthene
ug[L
ND
100
100
90.2
93.1
90
93
26-137
3
30
Fluorene
ug1L
ND
100
100
70.1
71.7
70
72
59-121
2
30
Hexachloro-1,3-butadiene
ug/L
ND
100
100
45.1
42.9
45
43
24-116
5
30
Hexachlorobenzene
ug1L
ND
100
100
77.0
79.6
77
80
1-152
3
30
Hexachlorocyclopentadiene
ug/L
ND
100
100
41.1
40.6
41
41
25-150
1
30
fiexachloroethane
ug/L
ND
100
100
39.4
39.9
39
40
40-113
1
30 M1
Indeno(1,2,3-cd)pyrene
ug/L
ND
100
100
95.4
97.6
95
98
1-171
2
30
Isophorone
ug/L
ND
100
100
45.8
46.3
46
46
21-196
1
30
N-Nitroso-di-n-propylamine
ug1L
ND
100
100
43.2
42.0
43
42
1-230
3
30
N-Nitrosodimethylamine
ug/L
ND
100
100
34.9
37.7
35
38
25-150
8
30
N-Nitrosodiphenylamine
ug/L
ND
100
100
76.9
82.2
77
82
25-150
7
30
Naphthalene
ug/L
ND
100
100
47.5
46.8
47
47
21-133
2
30
Nitrobenzene
ug/L
ND
100
100
44.6
45.1
45
45
35-180
1
30
Pentachlorophenol
ug/L
ND
200
200
150
151
75
76
14-176
1
30
Phenanthrene
ug/L
ND
100
100
79.7
82.6
80
83
54-120
4
30
Phenol
ug/L
ND
100
100
27.2
27.7
27
28
5-112
2
30
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 01/29/2015 0512 PM without the written consent of Pace Analytical Services, Inc.. Page 31 of 40

Pace Analytical Services, tnc.
205 East Meadow Road - Suite A
aceMalytical Eden, NC 27288
www•P bs =n [phone]
i
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1370690
1370691
MS
MSD
92233032001 Spike
Spike
MS
MSD MS
MSD
% Rec Max
Parameter Units Resuft Cone.
Cone.
Result
Result % Rec
% Rec
Limits RPD RPD Qual
Pyrene ug1L ND 100
100
84.0
90.6 84
91
52-115 8 30
2,4,6-Tribromophenol(S) %
77
82
10-137
2-Fluorobiphenyl (S) %
46
46
15-120
2-Fluorophenol(S) %
30
32
10-120
Nitrobenzene-d5 (S) %
43
44
10-120
Phenol-d6 (S) %
24
25
10-120
Terphenyl-d14 (S) %
79
86
11-131
Results presented on this page are In the units Indicated by the -UnW colunm except where an alternate unit Is presented to the light of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 32 of 40

aceAnalytical
www.pacefahscanr
r '
3
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
QC Batch: WET135241 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92233032001, 92233032002, 92233032003
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
METHOD BLANK: 1370609
Matrix: Water
Associated Lab Samples: 92233032001, 92233032002, 92233032003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Total Suspended Solids
mg/L
ND
2.5
01/15/15 04:43
LABORATORY CONTROL SAMPLE:
1370610
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250
262
105
90-110
SAMPLE DUPLICATE: 1370611
92233160001
Dup
Max
Parameter
Units
Result
Result
RPD
RPD Qualifiers
Total Suspended Solids
mg/L
28.8
29.6
3 10
SAMPLE DUPLICATE: 1370612
92232952001
Dup
Max
Parameter
Units
Result
Result
RPD
RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
10
Results presented on this page are in the units Indicated by the "Units" caiurm except where an ahemate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc..
Page 33 of 40

aceAnalytical
www.PacelaGxcam
r
i
QUALITY CONTROL DATA
Project: 2014 SEMI-ANNUAL.
Pace Project No.: 92233032
QC Batch: WET/35221 Analysis Method: EPA9040
QC Batch Method: EPA 9040 Analysis Description_ 9040 pH
Associated Lab Samples: 92233032001, 92233032002, 92233032003
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE DUPLICATE: 1369593
92233132001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
pH Std. Units 6.7 6.4 4 9 D6,H6
SAMPLE DUPLICATE: 1369594
Parameter
pH
92233032003 Dup Max
Units Result Result RPD RPD Qualifiers
Std. Units 7.6 7.6 0 9 H6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the "suit
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 34 of 40

Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
acemalytical Eden, NC 27288
Nwwpaowabs•cam [phone]
QUALIFIERS
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
DEFINITIONS
DF - Dilution Factor, 0 reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting IimiL
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
Acid preservation may not be appropriate for 2-Chloroethyhrinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NI`tAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MD Matrix spike recovery andfor matrix spike duplicate recovery was outside laboratory control limits.
M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/29/2015 05:12 PM without the written consent of Pace Analytical Services, Inc.. Page 35 of 40

aceAnalytical
rnvw.pe00ftc=
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: 2014 SEMI-ANNUAL
Pace Project No.: 92233032
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92233032001
G-1
EPA 1664B
GCSVI20072
92233032002
G-2
EPA 1664B
GCSV/20072
92233032003
G-3
EPA 1664B
GCSV/20072
92233032001
G-1
EPA 3510
0EXT/32333
EPA 608
92233032002
G-2
EPA 3510
OEXT/32333
EPA 608
92233032003
G-3
EPA 3510
OEXT/32333
EPA 608
92233032001
G-1
EPA 200.7
MPRP117719
EPA 200.7
92233032002
G-2
EPA 200.7
MPRP117719
EPA 200.7
92233032003
G-3
EPA 200.7
MPRP/17719
EPA 200.7
92233032001
G-1
EPA 625
OEXT/32298
EPA 625
92233032002
G-2
EPA 625
OEXT/32298
EPA 625
92233032003
G-3
EPA 625
OEXT/32298
EPA 625
92233032001
G-1
EPA624
MSV/30026
92233032002
G-2
EPA624
MSV/30026
92233032003
G-3
EPA 624
MSV/29994
92233032001
G-1
SM 2540D
WET/35241
92233032002
G-2
SM 2540D
WET/35241
92233032003
G-3
SM 2540D
WET135241
92233032001
G-1
EPA 9040
WET/35221
92233032002
G-2
EPA 9040
WET135221
92233032003
G-3
EPA 9040
WET/35221
Date: 01/29/2015 05:12 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
GCSV/20120
GCSV/20120
GCSV/20120
ICP/15950
ICP/15950
ICP/15950
MSSV/10198
MSSV110198
MSSVI10198
Page 36 of 40

- ace,41ralytical"
uocumeni rvame:
Condition U on Recei
Document Number:
F-CHR-CS-003-rev.15
UVcurrtUIR MWViSGU. ♦ UPLUJIlual X— -v
Paae 1 of 2
Pace Huntersville Quality Office
Client Name:
Courier: ❑ Fed Ex ❑ UPS❑ LISPS❑ lien h Commercial[] Pace Other p s
Custody Seal on CoolerBox Present: ❑ yes Ifl2no Seats Intact: ❑ yes ❑ no
Packing Material: ❑ Bubble VDp ❑ Bub�ags ❑ None ❑ Other
Thermometer Used: IR Gun T 40 Type of IcOC19Blue None P-6amples on Ice, cooling process has begun
Temp Correction Factor T1401 No Correction
Corrected Cooler Temp., - •C
Biological Tissue Is Frozen: Yes No NIA
Date and Initials of person examining
�
contents:
Temp should be above freezing to 6'C
Comments:
Chain of Custody Present:
- rre`s ❑No
❑NIA
1.
Chain of Custody Filled Out:
QYes ❑No
❑WA
2.
Chain of CustodX Relinquished:
E]Yes []No
❑NIA
3.
Sampler Name & Signature on COC:
❑Yes LINO
❑NIA
4.
Samples Arrived within Hold Time:
❑Yes_j2No ❑MIA
5.
Short Hold Time Analysis c72hr :
❑Yes PN6
❑NIA
6.
Rush Turn Around Time Re uested:
Oyes a•❑NrA
7,
Sufficient Volume:
` Yes ONO
❑NIA
8.
Correct Containers Used:
es�' ❑uo
❑NIA
9.
-Pace Containers Used:
8Ve3 ❑No
❑wA
Containers Intact:
fees []No
❑NIA
10.
Filtered volume received for Dissolved tests
❑Yes ❑Noo
Pkfg
11.
Sample Labels match COC:
❑Yes( No ❑NIA
12rt. (h j
�i� r y/ r • 'a 5 .
-includes date/time11D1Anai sis Matrix:
"I,
Z.
7 ,f{<-ram
Ali containers needing preservation have been checked.
❑Yes []No
❑NIA
13.
W 3
Ail containers needing preservation are found to be in
❑Yes ❑No
❑NIA
compliance with EPA recommendation.
ONo
exoeptlons: VOA, oolirorm,TOC.O&G.W-ORO(water)
6s
Samples checked for dechlodnation:
it es ❑No
DIVA
14.
Headspace in VOA Vials >6mm :
es ONO
❑NIA
15. ^ I.
Trip Blank Present:
❑Yes ❑No
OWIA
18.
Trip Blank Custody Seals Present
❑Yes ONo
E26A
Pace Trip Blank t_ot # if purchased):
','Client Notification/ Resoluti n: f1 �� Field Data Required? Y 1 N
Person Contacted: Iv W(� Datefiime:
- Commentsl-Resolution:: CjC�y1ti-(� -`j „ (� �fi[ ----l�I-� �-3�.[,ti.rl?-0•-4'• �i�� (-a ._ ---
SCURF Review: Date:
SRF Review: Date: { Uo# • 92233032
Note: Whenever there is a discrepancy affecting North Carolina compliance'
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, Incorrect preservative, out of temp, l82233032
Incorrect containers)
Page 37 of 40

PaceAnal1 RI -
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CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. AS relevant Gelds must be completed accurately.
rction A Section B Section C
Page. ' I of . J
puired Client Information: Required Project Infarrrmfion: Invoice Inforrnatlon:
wn Report To: Attention.
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CHAIN -OF -CUSTODY 1 Analytical Request Document
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CHAIN -OF -CUSTODY If Analytical Request Document i p
The Chain -of -Custody is a LEGAL DOCUMENT. Aft relevant fields must be completed axurately.
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action A Section B Section C
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squired Client tnformatbn:. Required Project 1Morrnation: Invoice IMormatlon:
ampan RepertTa: yy
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REGULAT., -- — ENCY•,.
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NPDESGROUND WATER r DRINKING WATER
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FHB 16 2Q15
AMPADWR� CT1ON
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidanceo►rfillingout thisform,please visit. http:fJnortal.ncdenr.org/web/=/ws/sm/npdessw#tab-4
Permit No.: Nj-w22l.
Facility Name:
County:
Inspector: �oN
Date of Inspection:
Time of Inspection:
010AQ/ or Certificate of Coverage No.:
13
Total Event Precipitation (inches): / 0S-
Phone No.
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
&J"Y'es ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event" However,
some permits do not have this requirement Please refer to these definitions, if applicable.
A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee s
obtains approval from the local DWQ Regional Office.
BY this signa, ylre, I cerdfy*at this report is accurate and complete to the best of my knowledge:
of Permittee`or Designee)
Page 1 of 2
SWU-242, fast modified 10/25/2012

a
1. outfall Description:
Outfall No. _ Structure (pipe, ditch, etc.) P. /
Receiving Stream: /71I1l' jefJe DQ�yj
Describe� the industrial activities hat occur within the outfall drainage area:
� a4 i� Lam` 4 ✓t °t I o f �irf S� b f?a�n .
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark] as descriptors: beow l _
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): i?rrn&.
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 3 (tp 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 <0— 5
AM b. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-24Z last modified 10/25/2012

0
r.
1. Outfall Description:
Outfall No. Structure (pipe, di h, etc,) + 010
Receiving Stream: u nar'�'t pej + i� ('�� + we bo-S-A
Describe the industrial activities that occur within the outfa drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:.;Ea&u2ti
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weals chlorine odor, etc.): n ()"Y�
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 3 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 5
5. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 & 5
7. Is there any foam in the stormwater discharge? Yes Mn
8. Is there an oil sheen in the stormwater discharge? YesN
9. Is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious Indicators of Stormwater Pollution:
List and describe y7@1'`� _
9 % Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

1. Outfall Description:
Outfall No. Structure (pipe, ditch, etc.)
Receiving Stream: CAA 11
�escribe the industrial activitiesUthat occur within the out ll drainAge area:
i,1 W L r n nk,,r,4 . D P,,, 4 S �u , �. �,Z.�C� ►lo % t,�i / -f,n , 6
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:,
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weals chlorine odor, etc.): ACTT-e_
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 3 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 04 5
Afth 6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 W 5
7. Is there any foam in the stormwater discharge? Yes ] o
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes` &J
10. Other Obvious Indicators of Stormwater Pollution:
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2of2
A)
SWU-24Z, Last modified 10/25/2012

fS� �
Semi-annual Stormwater Discharge Monitoring Report
♦ i for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
�1
CERTIFICATE OF COVERAGE NO. NCG03 0
FACILITY NAME �►uJt 4?2
COUNTY r+ bU4
PERSON COLLECTING SAMPL S 1= . M n'aRE
LABORATORY PQ CCL Lab Cert. # / 2 We+,f&sA wQ s 1
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR .3 — ..;?a 16' C"D
SAMPLE PERIOD ❑i Jan -June ❑ July -Dec
or [] Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HCiW ❑Trout ❑PNA�
❑Zero -flow []Water Supply ❑SA"
[Other Crn 17aM ed -6Ct61 -/-e14y -10
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?'
Outfail No.
Date Sample
Collected i
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Total Suspended Solids
p , H
Standard units
Copper
Lead
Zinc
Non-Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks ===>
-
-
100 mg/L or 50 mg/1.
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
L
0
6. w s-
Q t90 ar
D. of o
5`�-
2
Ir zor5
75
1 ,3 1.►oos
o.DmS
0.A10
—
3
r' 1r za1S
5 u
Z 1,
40.005,
01oos
O, of o
S 1,
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

C
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
. may 99 waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Name (Print name)
olls xanaeate
Title (Print title)
/91g:Zture) ate)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<n me/l". where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period
Qutiall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)Total
Suspended Solids
pH
Benchmarks ==m>
-
-
15 mg/L
100 mg/L or 50 mg/L'
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mall an original and one copy of this DMR, including all "No Discharae" reports, within 30 dayrs of receipt of the lab results tar at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
XgW MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and Imprisonment for knowing violations."
JW, �-, off. g?13
Ignature of Permlttee) ( te)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

s
e�Lti .s 1.� m'
V
September 3, 2015
Central Files
NC DENR
Division of Water Quality
1617 Mail Service CenterQ
Raleigh, NC 27699-1617
� Q �p15
SEP
Certificate of Coverage NGG030664
Southwire
GE R� GT otS
DW
12331 Commerce Station Dr.
Huntersville, NC 28078
Dear Sir/Madam:
Please be in receipt of the Qualitative and Analytical Monitoring Data for this facility. Note that the
company name is now Southwire and not ABB. (Notice of Change of Ownership on file)
This report covers required sampling for Year 3 Sample 5 Period 1.
Thank you,
John E. Moore CSP, CHMM, MBA
Southwire Huntersville OHS Manager
JEM/jm

�ioo
-47,
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out thisform, please visit: http://12ortal.ncdenr.orizlweh/wg/Mismtmpdessw#tab-4
Permit No.: X/L &/ _/ 3/-d ,M or Certificate of Coverage No.: �I/�/�/ 40 0/ /
� Facility Dame: ou-W;w � 4AU nfelew. If it l)c,�r
County: ccti-evi bvQ Phone No. __ 764/ - 379` g600
Inspector: :&pHN l=. aoR-E
Date of Inspection: b' ` // — 7-015
Time of Inspection: 11: 39M
i/
Total Event Precipitation (inches): 1..?5
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
eyes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event"or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event" However,
some permits do not have this requirement Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter E
interval is representative for local storm events during the sampling period, and the permittee i
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
of Permittee or Designee)
SWU-242,Iastmodified 10/25/2012

1. Outfall Description:
qPOutfall No. 2- '.
Receiving Stream: U/? flCII
Describe the industrial activi
(pipe, ditch, etc.)
DRR-?'nz2 �f7'trb�i
occur within the outfall d
/m -71" , 19nl2 Y'i 5 /
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: _ /,Qkern w4oe
3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): dldx�
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 � � 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 fl 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 &7 3 4 5
7. Is there any foam in the stormwater discharge? Yes
S. Is there an oil sheen in the stormwater discharge? Yes =o
9. Is there evidence of erosion or deposition at the outfall? Yeso
10. Other Obvious Indicators of Stormwater Pollution:
list and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
i ✓ctL OtZsiri
- SWU-242, LaA moddled 10/25/2012

1. Outfall Description:
Outfall No.. Structure (pipe,ditch etc.)
Receiving Stream: i.//7 170 -ecr4 nntaiu rW K x, we►et
Describe the industrial activities that occur within the outfall drainage area:
jo_�I?e,c. %fit
2. Color. Describe the color of the discharge using bas}}c colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 116? —
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 g�) 3 4 5
5. floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 C2:2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 t_9- 3 4 5
7. Is there any foam in the stormwater discharge? Yes
S. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes <ND
10. Other Obvious Indicators of Stormwater Pollution:
list and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
k—W) may be indicative of pollutant exposure. These conditions warrant further investigation.
SWU-242, Last modified 10/25/2012

I. Outfall Description: z
Outfall No. 3 Structure (pipe, ditch, etc.) 1
Receiving Stream: an aAma QF PAN n r r %
Describe the industp al activities that occur within the 'outfall
twill lllkteRiaf APrewjriA_ .Q oaxi bin r-er~,t,
area:
4ao.5
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
[light, medium, dark) as descriptors: _ _B00w r.1 _
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): h Qyte-
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3Q 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 ® 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious indicators of Stormwater Pollution:
List and describe _ /I orktc_
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
i? vto- I�Gts, ,•
i
swa-242, Lan modified 10/25/2012

ceAnalytircal
August 20, 2015
John Moore
Southwire
12331 Commerce Station
Huntersville, NC 28078
RE: Project: Semi -Annual August 2015
Pace Project No.: 92263080
Dear John Moore:
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
Enclosed are the analytical results for sample(s) received by the laboratory on August 12, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, Inc..
[phone]
Page 1 of 36

aceArWcal'
www4woeffxmm
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Charlotte Certification Ills
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification lDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VEIAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carotina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VEIAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 36
0
•
•

V Wbal e
we peadabaoam
SAMPLE SUMMARY
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
I3361623-8921
Lab ID
Sample 1D
Matrix
Date Collected
Date Received
92263080001
Sample 1
Water
OB/11/15 17:30
08/12/15 11:30
92263080002
Sample 2
Water
08/11/15 17:30
08/12/15 11:30
92263080003
Sample 3
Water
08/11/15 17:30
08112/15 11.30
r
�J
• REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 36

aceAnalytical'
wmvpsp wm
SAMPLE ANALYTE COUNT
Project: Semi -Annual August 2015
Pace Project No_: 92263080
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analyses
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92263080001
Sample 1
EPA 1664E
JMS
1
PASI-C
EPA 608
SWB
27
PASI-C
EPA 200.7
JDA
7
PAS! -A
EPA 625
Bpi
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
SAM
1
PASI-A
EPA 9040
MLS
1
PASI-A
92263080002
Sample 2
EPA 16648
JMS
1
PASI-C
EPA608
SWB
27
PASI-C
EPA200.7
JDA
7
PASI-A
EPA 625
Bpi
58
PASI-C
EPA 624
GAW
34
PASI-C
SM 2540D
SAM
1
PASI-A
EPA 9040
MLS
1
PASI-A
92263080003
Sample 3
EPA 1664B
JMS
i
PASI-C
EPA 608
SWB
27
PASI-C
EPA200.7
JDA
7
PASI-A
EPA 625
Bpi
58
PASI-C
EPA624
GAW
34
PASI-C
SM 2540D
SAM
1
PAS! -A
EPA 9040
MLS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Anatytical Services, Inc.. Page 4 of 36
E
E

•
ANALYTICAL RESULTS
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Pace Analytical Services, Inc.
2D5 East Meadow Road - Suite A
Eden, NC 27288-
[phone]
Sample: Sample 1 Lab (D: 92263080001 Collected: 08/11/15 17:30 Received: 08/12/15 11:30 Matrix: Water
Report
Parameters Results Units Limit MDL DE Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO
mg1L
5.0
1.1
1
08/18/15 08:30
608 GCS Pesticides and PCBs
Anatocal
Method: EPA 608 Preparation Method: EPA 3510
Aldrin
NO
ugIL
0.050
0.050
1
08/17/15 12:42
08/1911518:48 309400-2
alpha-BHC
NO
ug1L
0.050
0,050
1
08/17/15 12:42
08/19/15 18:48 31944-6
beta-BHC
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/1518:48 319485-7
delta-BHC
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08/1911518:48 319436-6
gamma-BHC (Lindane)
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 18:48 58-09-9
Chlordane (Technical)
NO
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 18:48 57-74-9
4,4'-DDD
NO
ug/L
0.050
0.050
1
08117/15 12:42
0811911518:48 72-54-8
4,4'-DDE
NO
ug[L
0.050
0.050
1
0811711512:42
08119/1518:48 72-55-9
4,4'-DDT
NO
ug/L
0.050
0.050
1
08/1711512:42
08/1911518748 50-29-3
Dieldrin
NO
41-
0.050
0.050
1
08/1711512:42
0811911518:48 60-57-1
Endosulfan I
NO
ug1L
0.050
0.050
1
08/17/15 12:42
08/19/15 18:48 959-98-8
Endosulfan II
NO
ug1L
0.050
0.050
1
08/17/15 12:42
08/19/15 18:48 33213-65-9
Endosulfan sulfate
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 18:48 1031-07-8
Endrin
NO
ug/L
0.050
0.050
1
08117/15 12:42
08/19/15 18:48 72-20-8
Endrin aldehyde
0.054
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 18:48 7421-93-4
Heptachlor
NO
ug/L
0.050
0.050
1
08117/15 12:42
08/1911518:48 76-44-8
Heptachlor epoxide
NO
UA
0.050
0.050
1
OW17115 12:42
08/19/15 18:48 1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 18:48 12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 18:48 11104-28-2
PCB-1232 (Aroclor 1232)
ND
ugfL
0.50
0.50
1
08/17/15 12:42
08/19/15 18:48 11141-16-5
PCB-1242 (Aroclor 1242)
NO
ug1L
0.50
0,50
1
08/17/15 12:42
08/19/15 18:48 53469-21-9
PCB-1248 (Aroclor 1248)
NO
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 18:48 12672-29-6
PCB-1254 (Aroclor 1254)
NO
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 18:48 11097-69-1
PCB-1260 (Aroclor 1260)
NO
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 18:48 11096-82-5
Toxaphene
NO
ug/L
0.50
0.50
1
08/1711512.42
08119/1518:48 8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
38
%
20-110
1
08/17/15 12:42
08/19/15 18:48 877-09-8
Decachlorobiphenyl (S)
45
%
20-138
1
08/17/15 12:42
08/19/15 1&48 2051-24-3
200.7 MET ICP
Anatytiral Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
NO
m91L
0.0010
0.00050
1
08/13/15 16:00
08/18/15 00:46 7440 43-9
Chromium
ND
mg1L
0.0050
0.0025
1
08/13/15 16:00
08/18/15 00:46 7440-47-3
Copper
NO
mgfL.
0.0050
0.0025
1
08/13/15 16:00
08/18/15 00:46 7440-50-8
Lead
NO
mg/L
0.0050
0.0025
1
0811311516:00
08/18/1514:39 7439-92-1
Nickel
ND
mgfL
0.0050
0.0025
1
08/13/15 16:00
08118/15 00:46 7440-02-0
Silver
ND
mg1L
0,0050
0.0025
1
08/13/15 16:00
08/18/15 00:46 7440-22-4
Zinc
ND
mg1L
0.010
0.0025
1
08/13/15 16:00
08/18115 00:46 74404"
625 MSSV
Anaytical Method: EPA625 Preparation Method:
EPA625
Acenaphthene
NO
ug1L
5.0
0.25
1
08/13/15 13:00
08/17/15 23:24 83-32-9
Acenaphthylene
NO
ug/L
5.0
0.21
1
08/13/15 13:00
08/17/15 23:24 208-96-8
Anthracene
ND
ug/L
5.0
0.14
1
08/13/15 13:00
08117/15 23:24 120-12-7
Benzo(a)anthracene
NO
ug/L
5.0
0.33
1
08/13115 13:00
08117/15 23:24 56-55-3
• REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Tull,
Date: 08/20/2015 04:15 PM without tde written consent of Pace Analytical Services, Inc.. Page 5 of 36

aceAnalytical
W*WP ceAftW n
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
•
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Sample: Sample 1
Lab 10: 92263080001
Collected:
08111/15 17:30
Received: 08/12/15 11:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed CAS No. Qual
625 MSSV
Analytical Method: EPA625 Preparation Method: EPA625
Benzo(a)pyrerte
NO
ug/L
5.0
0.30
1
08/13/15 13:00
08/17/15 23:24 50-32-8
Benzo(b)fluoranthene
NO
ug/L
5.0
0.28
1
08/13/15 13:00
08/17/15 23:24 205-99-2
Benzo(g,11.0perylene
NO
ug/L
5.0
0.38
1
08113/1513:00
08/17/15 23:24 191-24-2
Benzo(k)fluoranthene
NO
ug/L
5.0
0.43
1
08/13/15 13:00
08/17/15 23:24 207-08-9
4-Bromophenylphenyl ether
NO
ug/L
5.0
0.82
1
08/13/15 13:00
08/17/15 23:24 101-55-3
Butylbenzylphthalate
NO
ug/L
5.0
0,79
1
08/13/15 13:00
08/17/15 23:24 85-68-7
4-Chloro-3-methylphenol
NO
ug1L
5.0
3.7
1
08/13/15 13:00
08/17/15 23:24 59-50-7
bis(2-Chloroethoxy)methane
NO
uglL
10.0
0.92
1
08/13/15 13:00
08/17/15 23:24 111-91-1
bis(2-Chioroethyl) ether
NO
ug/L
5.0
1.0
1
08/13/15 13:00
08/17/15 23:24 111 44 4
bis(2 -Chi oroisopropyl) ether
NO
ug/L
5.0
0.95
1
08/13/15 13:00
08/17/15 23:24 108-60-1
2-Chloronaphthalene
ND
ug1L
5.0
0.98
1
0811311513:00
08/17/15 23:24 91-58-7
2-Chlorophenol
NO
ug/L
5.0
1.3
1
08113/15 13:00
08/17/15 23:24 95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
0.87
1
08/13/15 13:00
08/17/15 23:24 7005-72-3
Chrysene
NO
ug/L
5.0
0.21
1
08/13/15 13:00
08/17/15 23:24 218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
0.55
1
08/13/15 13:00
08/17/15 23:24 53-70-3
3,3'-Dichiorobenzidine
NO
ug/L
25.0
2.1
1
08/13/15 13:00
08/17/15 23:24 91-94-1
2,4-Dichlorophenol
ND
-A
5.0
1.7
1
08113/15 13:00
08/17/15 23:24 120483-2
Diethytphthalate
ND
ug/L
5.0
0.58
1
08/13/15 13:00
08/17/15 23:24 84-66-2
•
2,4-Dimethylphenol
NO
ug/L
10.0
1.2
1
08/13/15 13:00
08/17/15 23:24 105-67-9
Dimethylphthalate
NO
ug/L
5.0
0.76
1
08/13/15 13:00
08/17/15 23:24 131-11-3
Di-n-butylphthalate
NO
ug/L
5.0
0.75
1
08/13/15 13:00
08/17/15 23:24 84-74-2
4,6-Dinitm-2-methylphenol
NO
ug1L
20.0
2.6
1
08/13/15 13:00
08/17/15 2124 534452-1
2,4-Dinitrophenol
NO
ug/L
50.0
9.0
1
08/13/15 13:00
08/17/15 23:24 51-28-5
2,4-Dinitrotoluene
NO
ug/L
5.0
0.90
1
08/13/15 13:00
08/17/15 23:24 121-14-2
2,6-Dinitrotoiuene
NO
ug1L
5.0
0.98
1
08/13/15 13:00
08/17/15 23:24 606-20-2
Di-n-octylphthalate
NO
uglL
5.0
0.66
1
08/13/15 13:00
08/17/15 23:24 117-84-0
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
0.79
1
08/13/15 13:00
08/17/15 23:24 117-81-7
Fluoranthene
NO
ug/L
5.0
0.21
1
08/13M5 13:00
08/17/15 23:24 206A4-0
Fluorene
NO
ug/L
5.0
0,21
1
08/13/15 13:00
08/17/15 23:24 86-73-7
Hexachlaro-1,3-butadiene
NO
ug/L
5.0
0.94
1
08/13/15 13:00
08/17/15 23:24 87-68-3
Hexachlorobenzene
NO
ug/L
5.0
0.72
1
08/13/15 13:00
08/17/15 23:24 118-74-1
Hexachlorocyclopentadiene
NO
ug/L
10.0
0.88
1
08/13/15 13:00
08/17/15 23:24 77-47-4
Hexachloroethane
NO
ug/L
5.0
1.1
1
08/13/15 13:00
08/17/15 23:24 67-72-1
Indeno(1,2,3-cd)pyrene
NO
ug1L
5.0
0,29
1
08/13/15 13:00
08/17/15 23:24 193-39-5
Isophorone
NO
ug/L
10.0
0.89
1
08/13/15 13:00
08/17/15 23:24 78-59-1
Naphthalene
NO
ug/L
5.0
0.34
1
08/13/15 13:00
08/17/15 23:24 91-20-3
Nitrobenzene
NO
u91L
5.0
1.1
1
08/13/15 13:00
08/17/15 23:24 98-95-3
2-Nitrophenol
ND
ug/L
5.0
0.91
1
08113/15 13:00
08/17/15 23:24 M75-5
4-Nitrophenol
NO
ug/L
50.0
4.1
1
08/13/15 13:00
08/17/15 23:24 100-02-7
N-Nitroso6methylamine
NO
ug/L
5.0
0.91
1
08/13/15 13:00
08/17/15 23:24 62-75-9
N-Nitroso-di-n-propylamine
NO
ug1L
5.0
0.99
1
08/13115 13:00
08/17/15 23:24 621- 4-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1.0
1
08/13/15 13:00
08117/15 23:24 W30-6
Pentachlorophenal
ND
ug/L
10.0
4,6
1
08/13/15 13:00
08/17/15 23:24 87-86-5
Phenanthrene
NO
ug/L
5.0
0,22
1
08/13/15 13:60
0&17115 23:24 85-01-8
Phenol
NO
ug/L
5.0
1.9
1
08/13/15 13:00
08/17/15 23:24 108-95-2
Pyrene
NO
ug1L
5.0
0.19
1
08/13/15 1100
08/17/15 2124 129-00-0
•
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/20/2015 04:15 PM
without the written
consent of Pace Analytical Services, Inc..
Page 6 of 36

Mn►+r.pec�a6:cnrrt
•
ANALYTICAL RESULTS
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Pace Analytical Services, Inc_
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Sample 1 Lab ID: 92263080001 Collected: 08/11/15 17:30 Received: 08/12/15 11:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
625 MSSV
Analytical Method: EPA625 Preparation Method: EPA625
1,2,4-Trichlorobenzene
ND
ug/L
5.0
0.98
1
08/13/15 13:00
08/17/15 23:24 120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1.3
1
08/13/15 13:00
08/17/15 23:24 88-06-2
Surrogates
Nitrobenzene-d5 (S)
52
%
10-120
1
08/13/15 13.00
08/17/15 23:24 4165-60-0
2-Ftuorobiphenyl (S)
54
%
15-120
1
08113/15 13:00
08/17/15 23:24 321-60-8
Terphenyl-04 (S)
82
%
11-131
1
08/13/15 13:00
08/17/15 23:24 1718-51-0
Phenol-06 (S)
18
%
10-120
1
08113115 13:00
08/17/15 23:24 13127-08-3
2-Fluorophenol (S)
29
%
10-120
1
08/13/15 13:00
08/17/15 23:24 367-12-4
2,4,6-Tribromophenol (S)
69
%
10-137
1
08/13/15 13:00
08/17/15 23:24 118.79-6
624 Volatile Organics
Analytical Method: EPA624
Benzene
ND
ug/L
2.0
1.7
1
08/14/15 22:45 7143-2
Bromodichloromethane
ND
ug1L
2.0
1.7
1
08/14/15 22:45 75-274
Bromoform
ND
ug1L
2.0
1.5
1
08/14/15 22:45 75-25-2
Bromomethane
ND
ug/L
2.0
1.0
1
08/14/15 22:45 74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1.9
1
08/14/15 22:45 56-23-5
Chtorobenzene
ND
ug/L
2.0
1.7
1
08/14/15 22:45 108-90-7
Chloroethane
ND
ug/L
2.0
1.6
1
08/14/15 22:45 75-00-3
Chloroform
ND
ug/L
2.0
1.9
1
08/14/15 22:45 67-66-3
Chloromethane
ND
ug1L
2.0
1.5
1
08/14115 22:45 74-87-3
Dibromochloromethane
ND
ug/L
2.0
1.8
1
08/14/15 22:45 124 48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
1.5
1
08/14/15 22:45 95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1.5
1
08/14/15 22:45 541-73-1
1,4-Dichlorobenzene
NO
ug1L
2.0
1.5
1
08/14/15 22:45 106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
1.8
1
08/14/15 22:45 75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
1.8
1
08114/15 22:45 107406-2
1,1-Dichloroethene
NO
ug/L
2.0
1.9
1
08/14/15 22:45 75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
1.8
1
08/14/15 22:45 156-59-2
trans-1,2-Dichlonoethene
ND
ug1L
2.0
1.8
1
08/1411522:45 156-60-5
1,2-Dichloropropane
ND
ugIL
2.0
1.7
1
08/14/15 22:45 78-87-5
cis- 1,3-Dichloropropene
NO
ug1L
2.0
1.6
1
08/14/15 22:45 10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
2.0
1.6
1
08/1411522:45 10061-02-6
Ethylbenzene
ND
ug1L
2.0
1.6
1
08/14/15 22:45 100-414
Methylene Chloride
ND
ug/L
2.0
1.9
1
08/14/15 22:45 75-09-2
1,1,2,2-Tetrachloroethene
ND
uglt-
2.0
1.5
1
08114/15 22:45 79-34-5
Tetrachloroethene
ND
ug/L
2.0
1.8
1
08/14/15 22:45 127-18-4
Toluene
ND
ug/L
2.0
1.6
1
08/14/15 22:45 108-8&3
1,1,1-Trichloroethane
ND
ug1L
2.0
1.9
1
0811411522:45 71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1.7
1
08/14115 22:45 79-00-5
Trichloroethene
NO
ug/L
2.0
1.8
1
08/14/15 22:45 79-01-6
Trichlorofluoromethane
ND
ug/L
2.0
1.7
1
08/14/15 22:45 75-09-4
Vinyl chloride
ND
ug/L
2.0
1.5
1
08/14/15 22:45 75-01-4
Surrogates
4-Bromofluorobenzene (S)
103
%
70-130
1
08/14/15 22:45 460400-4
Toluene -dB (S)
100
%
70-130
1
08/14/15 22:45 2037-26-5
1,2-Dlchloroethane-d4 (S)
107
%
70-130
1
08/14/15 22:45 17060-07-0
C.
Date: 08/20/2015 04:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in tint,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 36

ceAnalytical
wwacparztabsada
ANALYTICAL RESULTS
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Sample 1 Lab ID: 92263080001 Collected: 0&1Ill 5 17:30 Received: 08/12/15 11:30 Matrix: Water
Report
Parameters Results Units limit MDL DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 5.0 5.0 1 08/14/15 13:15
9040 pH Analytical Method: EPA 9040
pH 6.4 Std. Units 0.10 0.10 1 08/13115 12:25 H6
Sample: Sample 2
Lab ID: 92263080002
Coltected:
08/11/15 17:30
Received: 08/12/15 11:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND
m91L
5.0
IA
1
08/18/15 08:31
508 GCS Pesticides and PCBs
Analytical Method: EPA608 Preparation Method: EPA 3510
Aldrin
ND
ug/L
0.050
0.050
1
08/17/15 12:42
OW19/15 02:50 309-M2
alpha-BHC
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19//15 02:50 319-84-6
beta-13HC
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 319-85-7
delta-BHC
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 319-86-8
gamma-BHC (Lindane)
ND
ug1L
0.050
0,050
1
08/17/15 12:42
08/19/15 02:50 58-89-9
Chlordane (Technical)
ND
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 02:50 57-74-9
4,4'-DDD
ND
ug/L
0.050
0,050
1
08/17/15 12:42
08/19/15 02:50 72-54-8
4,4'-DDE
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 72-55-9
4,4'-DDT
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 50-29-3
Dieldrin
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 60-57-1 "
Endosulfan I
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 959-98-8
Endosulfan [l
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 33213-65-9
Endosuffan sulfate
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 1031-07-8
Endrin
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 72-20-8
Endrin aldehyde
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 7421-93-4
Heptachlor
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 76-44-8
Heptachlor epoxide
ND
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 02:50 1024-57-3
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 02:50 12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 02:50 1110428-2
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 02:50 11141-16-5
PCB-1242 (Aroclor.1242)
ND
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 02:50 53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 02:50 12672-29.6
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 02:50 11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug1L
0.50
0.50
1
08/17/15 12:42
08/19/15 02:50 11096-82-5
Taxaphene
ND
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 02:50 8001-35-2
Surrogates
Tetrachlora-m-xylene (S)
84
%
20-110
1
08/17/15 12:42
08/19/15 02:50 877-09-8
Decachlorobiphenyl (S)
50
%
20-138
1
08/17/15 12:42
08/19/15 02:50 2051-24-3
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 2003
Cadmium ND mg/L 0.0010 0.00050 1 08/13/15 16:00 08/18/15 00:55 7440-43-9
Date: 08/20/2015 04:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 36
E
E
0

0"Wlyd!
nww.pec&Uh .mm
ANALYTICAL RESULTS
Project: Semi -Annual August 2015
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
Pace Project No.: 92263080
Sample: Sample 2 Lab ID: 92263080002 Collected: 08/11/15 17:30 Received: 08/12/15 11:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed
[phone]
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 2003
Chromium
NO
mg/L
0.0050
0.0025
1
08113M5 16:00
08/18/15 00:55
7440-47-3
Copper
NO
mg/L
0.0050
0.0025
1
08/13/15 16:00
08/18/15 00:55
7440-50-8
Lead
NO
mg/L
0.0050
0.0025
1
08/1311516:00
08/1811514:48
7439-92-1
Nickel
NO
mg/L
0.0050
0.0025
1
08/13/15 16:00
08118/15 00:55
7440-02-0
Silver
NO
mg/L
0.0050
0.0025
1
08/13/15 16:00
08118/15 00:55
7440-22-4
Zinc
0.010
mg/L
0.010
0.0025
1
08/13/15 16:00
08/18/15 00:55
7440-66-6
625 MSSV
Analytical Method: EPA625 Preparation Method: EPA625
Acenaphthene
ND
ug/L
5.0
0.25
1
08/13/15 13:00
08/17/15 23:52
83-32-9
Acenaphthylene
ND
ug/L
5.0
0.21
1
08/13/15 13:00
08/17/15 23:52
208-%6 8
Anthracene
ND
ug/L
5.0
0.14
1
OW13/15 13:01)
08/17/15 23:52
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
0.33
1
08/13/15 13:00
08/17/15 23:52
56-55-3
Benzo(a)pyrene
ND
ug1L
5.0
0.30
1
08/13/15 13:00
08/17/15 23:52
50-32-8
Benzo(b)fluoranthene
NO
ug/L
5.0
0.28
1
08/13/15 13:00
08/17/15 23:52
205-99-2
Benzo(g,h,i)perytene
ND
ug/L
5.0
0.38
1
08/13/15 13:00
08117/15 23:52
191-24-2
Benzo(k)fluoranthene
NO
ug/L
5.0
0.43
1
08/13/15 13:00
08/17/15 23:52
207-08-9
4-Bromophenylphenyl ether
ND
ug1L
5.0
0.82
1
08/13/15 13:00
08/17/15 23:52
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
0.79
1
08/13/15 13:00
08/17/15 23:52
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
3.7
1
08/13/15 13:00
OW17115 23:52
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
0.92
1
08/13/15 13:00
08/17/15 23:52
111-91-1
bis(2-Chloroethyl) ether
NO
ug/L
5.0
1.0
1
08/13115 13:00
08/17/15 23:52
111-44-4
bis(2-Chloroisopropyl) ether
NO
uglL
5.0
0.95
1
08/13/15 13:00
08/17/15 23:52
108-00-1
2-Chloronsphthalene
NO
ug/L
5.0
0.98
1
08/13/15 13:00
08/17/15 23:52
91-58-7
2-Chlorophenol
NO
ug/L
5.0
1.3
1
08/13/15 13:00
08/17/15 23:52
95-57-8
4-Chlarophenylphenyl ether
NO
ug1L
5.0
0.87
1
08/13/15 13:00
08/17/15 23:52
7005-72-3
Chrysene
NO
ug/L
5.0
0.21
1
08/13/15 13:00
08/17/15 23.52
218-01-9
Dibenz(a,h)anthracene
NO
ug1L
5.0
0.55
1
08/13/15 13:00
08117/15 23:52
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
2.1
1
08/13/15 13:00
Oa117115 23:52
91-94-1
2,4-Dichlorophenol
ND
ug1L
5.0
1.7
1
08/13/15 13:00
08/17/15 23:52
120-83-2
Diethylphthalate
NO
ug/L
5.0
0.58
1
08113/15 13:00
08/17/15 23:52
84-06-2
2,4-Dimethylphenol
NO
ug/L
10.0
1.2
1
08113(15 13:00
08/17/15 23:52
105-67-9
Dimethylphthalate
NO
ug/L
5.0
0.76
1
08/13/15 13:00
08/17/15 23:52
131-11-3
Difi-butylphthaiate
NO
ug/L
5.0
0.75
1
08/13/15 13:00
08/17/15 23:52
84-74-2
4,6-Dinitro-2-methylphenol
NO
uglL
20.0
2.6
1
08/13/15 13:00
08/17/15 23:52
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
9.0
1
08/13/15 13:00
08/11/15 23:52
51-28-5
2,4-Dinitrotoluene
NO
ug1L
5.0
0.90
1
08/13/15 13:00
08/17/15 23:52
121-14-2
2,6-Dinitrotoluene
NO
uglL
5.0
0.98
1
08/13/15 13:00
08/17/15 2152
606-20-2
Di-n-octylphthalate
NO
ug/L
5.0
0.66
1
08/13/15 13:00
08/17/15 23:52
117-84-0
bis(2-Ethy1hexyi)phthalate
NO
ug/L
5.0
0.79
1
08/13/15 13:00
08/17/15 23:52
117-81-7
Fluoranthene
ND
ug/L
5.0
0.21
1
08/13/15 13:00
08/17/15 23:52
206-44-0
Fluorene
NO
ug/L
5.0
0.21
1
08113/15 13:00
08/17/15 23:52
86-73-7
Hexachloro-1,3-butadiene
NO
ug/L
5.0
0.94
1
08/13/15 13:00
08/17/15 23:52
87-68-3
Hexachiorobenzene
NO
ug/L
5.0
0.72
1
08113/15 13:00
08/17/15 23:52
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
0.88
1
08/13/15 13:00
08/17/15 23:52
77-47-4
Hexachioroethane
NO
u91L
5.0
1.1
1
08/13/15 13:00
08/17/15 23:52
67-72-1
Indeno(1,2,3-cd)pyrene
ND
uglL
5.0
0.29
1
08/13/15 13:00
08/17/15 23:52
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull.
Date: 08120QO15 04:15 PM
without the written consent of Pace Analytical Services, Inc..
Page 9 of 36

Pace Analytical Services, Inc.
C�� _ _ � 1��'• 205 East Meadow Road -Suite A
�jl/`� Eden, NC 27286
wwwpewis6s.00m [phone]
W
ANALYTICAL RESULTS
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Sample: Sample 2
Parameters
Lab lD: 92263080002
Results Units
Collected:
Report
Limit
08/11/15 17:30
MDL OF
Received: 08112A5 11:30 Matrix: Water
Prepared Analyzed CAS No. Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Isophorone
NO
ug/L
10.0
0.89
1
08/13/15 13:00
08/17/15 23:52
78-59-1
Naphthalene
NO
ug/L
5.0
0.34
1
08/13/15 13:00
08/17/15 23:52
91-20-3
Nitrobenzene
NO
uglL
5.0
1.1
1
08/13/15 13:00
08/17/15 23:52
98-95-3
2-Nitrophenol
ND
ug/L
5.0
0.91
1
08/13/15 13:00
08/17/15 23:52
88-75-5
4-Nitrophenol
NO
ug/L
50.0
4A
1
08/13/15 13:00
08/17/15 23:52
100-02-7
N-Nitrosodimethyiamine
ND
ug1L
5.0
0.91
1
08113/15 13:00
08/17/15 23:52
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
5.0
0.99
1
08/13/15 13:00
08/17/15 23:52
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1-0
1
08/13/15 13:00
08/17/15 23:52
86-30-6
Pentachlorophenol
NO
ug1L
10.0
4.6
1
08/13/15 13:00
08/17/15 23.52
87-86-5
Phenanthrene
ND
ug/L
5.0
0.22
1
08113/15 13:00
08/17/15 23:52
85-01-8
Phenol
ND
ug/L
5.0
1.9
1
08/13/15 1100
08/17/15 23:52
108-95-2
Pyrene
NO
ug/L
5.0
0.19
1
08113/15 13.00
08/17/15 23:52
129-00-0
1,2,4-Trichlorobenzene
NO
ug1L
5.0
0.98
1
08/1311513:00
08/1711523:52
120-82-1
2,4,6-Trichlorophenol
NO
ug1L
10.0
1.3
1
08/13/15 13:00
08/17/15 23:52
88-06-2
Surrogates
Nitrobenzene-d5 (S)
74
%
10-120
1
08/13/15 13:00
08/17/15 23:52
4165-60-0
2-Fluorobiphenyl (S)
76
%
15-120
1
08/13/15 13:00
08/17/15 23:52
321-60-8
Terphenyi-d14 (S)
83
%
11-131
1
08/13/15 13:00
OS/17/15 23:52
1718-51-0
Phenol-d6 (S)
23
%
10-120
1
08/13/15 13:00
08/17/15 23:52
13127-88-3
2-Fluorophenol (S)
37
%
10-120
1
08/13/15 13:00
08/17/15 23:52
367-12-4
2,4,6-Tribromophenol (S)
78
%
10-137
1
08/13/15 13:00
08/17/15 23:52
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Benzene
NO
ug/L
2.0
1.7
1
08/14/15 23:02
71-43-2
Bromodichloromethane
NO
ug/L
2.0
1.7
1
08/14/15 23:02
75-27-4
Bromoform
ND
41911-
2.0
1.5
1
08114/15 23:02
75-25-2
Bromomethane
NO
ug/L
2.0 ,
1.0
1
08/14/15 23:02
74-83-9
Carbon tetrachloride
NO
ug1L
2.0
1.9
1
0&14/15 23.02
56-23-5
Chlorobenzene
NO
ug/L
2.0
1.7
1
08/14/15 23:02
108-90-7
Chloroethane
NO
ug/L
2.0
1.6
1
08/14/15 23:02
75-00-3
Chloroform
NO
ug1L
2.0
1.9
1
08/14/15 23:02
67-66-3
Chloromethane
NO
ug/L
2.0
1.5
1
08/14/15 23:02
74-87-3
Dibromochloromethane
NO
ug/L
2.0
1.8
1
08/14/15 23:02
124 48 1
1,2-Dichlorobenzene
NO
ug/L
2.0
1.5
1
08/14/15 23:02
95-50-1
1,3-Dichlombenzene
NO
ugA-
2.0
1.5
1
08/14/15 23:02
541-73-1
14-Dichlorobenzene
NO
ug/L
2.0
1.5
1
08/14/15 23:02
106-46-7
1,1-Dichloroethane
NO
ug/L
2.0
1.8
1
08/14/15 23:02
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1.8
1
08/14/15 23:02
107-W2
1,1-Dichlaroethene
NO
ug/L
2.0
1.9
1
08/14/15 23:02
75-35-4
cis-12-Dichloroethene
NO
ug/L
2.0
1.8
1
08/14/15 23:02
156-59-2
trans-1,2-Dichloroethene
NO
ug1L
2.0
1.8
1
08/14/15 23:02
156-60-5
1,2-Dichloropropane
NO
ug1L
2.0
1.7
1
08114/15 23:02
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2-0
1.6
1
08/14/15 23:02
10061-01-5
trans-1,3-Dichlompropene
NO
ug/L
2.0
1.6
1
08/14/15 23:02
10061-02-6
Ethylbenzene
ND
ug/L
2.0
1.6
1
08/14/15 23:02
100-41-4
Methylene Chloride
ND
ug/L
2.0
1.9
1
08/14/15 23:02
75-09-2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in
full,
Date: 08/20/2015 04:15 PM
without the wrtden
consent of Pace Analytical Services, Inc..
Page 10 of 36

ceAr�lytical
rrw:peoetabs.00rn
•
ANALYTICAL RESULTS
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Sample 2 Lab ID: 92263080002 Collected: 08/11/15 17:30 Received: 08/12/15 11:30 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS ND. Qual
624 Volatile Organics Analytical Method: EPA 624
1,1,2,2-Tetrachloroethane
ND
ug1L
2.0
1.5
1
08/14/15 23:02 79-34-5
Tetrachloroethene
ND
ug/L
2.0
1.8
1
08/14/15 23:02 127-18-4
Toluene
NO
ug/L
2.0
1.6
1
08/14/15 23:02 108-88-3
1,1,1-Trichloroethane
NO
ug/L
2.0
1.9
1
08/14/1523:02 71-55-6
1,1,2-Trichloroethane
NO
ug/L
2.0
1.7
1
08/14/15 23:02 79-00-5
Trichloroethene
NO
ug/L
2.0
1.8
1
08/14/15 23:02 79-01-6
Trichlorofluoromethane
NO
ug/L
2.0
1.7
1
08/14/15 23:02 75-69-4
Vinyl chloride
NO
ug/L
2.0
1.5
1
08/14/15 23:02 75-01-4
Surrogates
4-Bromoiiuombenzene (S)
101
%
70-130
1
08/14/15 23:02 460-00-4
Toluene-08 (S)
102
%
70-130
1
08/14/15 23:02 2037-26-5
1,2-Dichloroethane-d4 (S)
107
%
70-130
1
08/14/15 23:02 17060-07-0
2540D Total Suispended Solids Analytical Method: SM 2540D
Total Suspended Solids 11.3 mg1L 2.5 2.5 1 08/14/15 13:15
9040 pH Analytical Method: EPA 9040
. pH 6A Std. Units 0.10 0.10 1 08/13/15 12:25
I:[I
Sample: Sample 3
Lab iD: 92263080003
Collected: 08/11/15 17:30
Received: 08/12/15 11:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical
Method: EPA 1664E
Oil and Grease
NO
mg/L
5.0
1.1
1
08/18/15 08:32
608 GCS Pesticides and PCBs
Analytical
Method: EPA 608 Preparation Method: EPA 3510
Aldrin
NO
ug/L
0.050
0.050
1
08/17115 12:42
08/19/15 03:08 309-00-2
alpha-BHC
NO
ug1L
0.050
0.050
1
08/17/15 12:42
08/19/15 03:08 319-84-6
beta-BHC
NO
ug1L
0.050
0.050
1
08/17/15 12:42
08/19/15 03:08 319-85-7
delta-BHC
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 03:08 319-86-8
gamma-BHC (Lindane)
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 03:08 58-89-9
Chlordane (Technical)
NO
ug/L
0.50
0.50
1
08/17/15 12:42
08/19115 03:08 57-74-9
4,4'-DDD
NO
ug1L
0.050
0.050
1
08/17/15 12:42
08/19/15 03:08 72-54-8
4,4'-DDE
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08119/15 03:08 72-55-9
4,4'-DDT
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 03:08 50-29-3
Dieldrin
NO
ug/L
0.050
0.050
1
08117/15 12.42
08119/15 03:08 60-57-1
Endosulfan I
NO
ug1L
0.050
0.050
1
08/17/15 12:42
08/19/15 03:08 959-98-8
Endosulfan II
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 03:08 33213f5-9
Endosulfan sulfate
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 03:08 1031-07-8
Endrin
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 03:08 72-20-8
Endrin aldehyde
NO
ug1L
0.050
0.050
1
08/17115 12:42
08/19/15 03:08 7421-934
Heptachlor
NO
ug/L
0.050
0.050
1
08/17/15 12:42
08/19/15 03:08 76-44-8
Heptachlor epoxide
NO
ug/L
0,050
0,050
1
08/17/15 12:42
08/19/15 03:08 1024-57-3
• REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/2012015 04:15 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 36

Pace Anatyiacal Services, Inc.
Cn n ,,,, 1:,,,,! 205 East Meadow Road - Suite A
`i/�jkj�1V�( Eden, NC 27288
w*wPm chb.am
[phone]
ANALYTICAL RESULTS
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Sample: Sample 3 Lab ID: 92263080003 Collected. 08/11/15 17:30 Received: 08/12/15 11:30 Matrix: Water
Parameters
Results
Units
Report
Limit
MDL
OF
Prepared
Analyzed CAS No. Qual
608 GCS Pesticides and PCBs
Anaiytical Method: EPA 608 Preparation Method: EPA 3510
PCB-1016 (Aroclor 1016)
NO
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 03:08 12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 03:08 11104-28-2
PCB-1232 (Aroclor 1232)
ND
uglL
0.50
0.50
1
08/17/15 12:42
08/19/15 03:08 11141-16-5
PCB-1242 (Aroclor 1242)
ND
u91L
0.50
0.50
1
08/17/15 12:42
08/19/15 03:08 53469-21-9
PCB-1248 (Aroclor 1248)
NO
ug/L
0.50
0.50
1
08/17/15 12.42
08/19/15 03:08 12672-29.8
PCB-1254 (Aroclor 1254)
NO
ug/L
0.50
0,50
1
08/17/15 12:42
08/19/15 03:08 11097-69-1
PCB-1260 (Aroclor 1260)
NO
ug/L
0.50
0.50
1
08/17/15 12:42
08/19/15 03:08 11096-82-5
Toxaphene
ND
ug1L
0.50
0.50
1
08/17/15 12:42
08/19/15 03:08 8001-35-2
Surrogates
Tetrachloro-m-xylene (S)
49
%
20-110
1
08/17/15 12:42
08/19/15 03:08 877-09-8
Decachlorobiphenyl (S)
51
%
20-138
1
08/17/15 12:42
08/19/15 03:08 2051-243
200.7 MET ICP
Analytical
Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
NO
mg/L
0.0010
0.00050
1
08/13/15 16:00
08/18/15 00:58 7440-43-9
Chromium
NO
mg/L
0.0050
0.0025
1
08/13/15 16:00
08/18/15 00:58 7440-47-3
Copper
NO
mg/L
0.0050
0.0025
1
08/13/15 16:00
08/18/15 00:58 7440-50-8
Lead
ND
mg1L
0.0050
0.0025
1
08113/1516:00
0811811514:51 7439-92-1
Nickel
NO
mg/L
0.0050
0.0025
1
08/13/15 16:00
08/18/15 00.58 7440-02-0
Silver
NO
mg/L
0.0050
0.0025
1
08/13/15 16:00
08/18/15 00:58 7440-22-4
•
Zinc
NO
mg/L
0.010
0,0025
1
08/13/15 16:00
08/18/15 00:58 7440-66-6
625 MSSV
Analytical
Method: EPA 625 Preparation Method: EPA
625
Acenaphthene
NO
ug/L
5.0
0.25
1
08/13/15 13:00
08/18/15 00:19 83-32-9
Acenaphthylene
NO
ug/L
5.0
0.21
1
08/13/15 13:00
08/18/15 00:19 208-96-8
Anthracene
ND
ug/L
5.0
0,14
1
08/13/15 13:00
08/18/15 00.19 120-12-7
Berizo(a)anthracene
NO
ug1L
5.0
0,33
1
08/13/15 13:00
08/18/15 00:19 56-55-3
Benzo(a)pyrene
NO
ug/L
5.0
0.30
1
08/13/15 13:00
08/18/15 00:19 50-32-8
Benzo(b)fluoranlhene
NO
ug/L
5.0
0.28
1
08/13/15 13:00
08/18/15 00:19 205-99-2
Benzo(g,h,i)perylene
NO
ug/L
5.0
0.38
1
08/13/15 13:00
08/18/15 00:19 191-24-2
Senzo(k) luoranthene
NO
ug/L
5.0
0.43
1
08/13/15 13:00
08/18/15 00:19 207-OS-9
4-Bromophenylphenyl ether
NO
ug1L
5.0
0.82
1
08/13/15 13:00
08/18/15 00:19 101-55-3
BuWbenzylphthalate
NO
ug/L
5.0
0.79
1
08/13/15 13:00
08/18/15 00:19 85-68-7
4-Chloro-3-methylphenol
NO
ug/L
5.0
3.7
1
08/13/15 13:00
08/18/15 00:19 59-50-7
bis(2-Chloroethoxy)methane
NO
ug/L
10.0
0.92
1
08/13/15 13:00
08/18/15 00:19 111-91-1
bis(2-Chloroethyi) ether
NO
ug/L
5.0
1.0
1
08/13/15 13:00
08/18115 00:19 111-44-4
bis(2-Chloroisopropyt) ether
NO
ug/L
5.0
0.95
1
08/13/15 13:00
08/18/15 00:19 108-60-1
2-Chloronaphthalene
ND
u911-
5.0
0.98
1
08/13/15 13:00
08/18/15 00:19 91-58-7
2-Chlorophenol
NO
ug1L
5.0
1.3
1
08/13/15 13:00
08/18/15 00:19 95-57-8
4-Chlorophenylphenyl ether
NO
ug1L
5.0
0,87
1
08/13/15 13:00
08/18/15 00:19 7005-72-3
Chrysene
NO
ug/L
5.0
0.21
1
08/13/15 13:00
08/18/15 00:19 218-01-9
Dibenz(a,h)anthracerte
NO
ug/L
5.0
0.55
1
08/13/15 13:00
08/18/15 00:19 53-70-3
3,X-Dichlorobenzidine
NO
ug/L
25.0
2.1
1
08/13/15 13:00
08/18/15 00:19 91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1.7
1
08/13/15 13:00
08/18/15 00:19 120-83-2
Diethylphthalate
NO
uglL
5.0
0,58
1
08/13/15 13:00
08/18/15 00:19 84-66-2
2,4-Dimethylphenol
NO
ug/L
10.0
1.2
1
08/13/15 13:00
08/18/15 00:19 105-67-9
Dimethylphthalate
NO
ug/L
5.0
0.76
1
08/13/15 13:00
08/18/15 00:19 131-11-3
•
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in
full,
Date: 08/20I2015 04:15 PM
without the written consent of
Pace Analytical Services, Inc..
Page 12 of 36

i
ANALYTICAL RESULTS
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Pace Analytical Services, Inc_
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Sample 3 Lab ID: 92263080003 Collected: 08/Y1/15 17:30 Received: 08/12/15 11:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No_ Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-butylphthalale
ND
ug/L
5.0
0.75
1
08/13/15 13:00
08/18/15 00:19 84-74-2
4,6-Dinitro-2-methylphenol
ND
ug1L
20.0
2.6
1
08/13/15 13:00
08/18/15 00:19 534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
9.0
1
08/13/15 13:00
08/18/15 00:19 51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
0.90
1
08/13/15 13:00
08/18/15 00:19 121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
0.98
1
08/13/15 13:00
08/18/15 00:19 606-20-2
Di-n-0ctylphthalate
ND
ug1L
5.0
0.66
1
08/13115 13:00
08/18/15 00:19 117-84-0
bis(2-Ethythexyl)phthalate
ND
ug1L
5.0
0.79
1
08/13/15 13:00
08/18/15 00:19 117-81-7
Fluoranthene
ND
ug1L
5.0
0.21
1
08/13115 13*00
08/18/15 00:19 206-44-0
Fluorene
ND
ug/L
5.0
0.21
1
08/13/15 13:00
08/18/15 00:19 86-73-7
Hexachloro-1.3-butadiene
ND
ug/L
5.0
0.94
1
08/13/15 13:00
08/18/15 00:19 87-68-3
Hexachlorobenzene
ND
u911-
5.0
0.72
1
08/13/15 13:00
08/18/15 00:19 118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
0.88
1
08M3115 13:00
08/18/15 00:19 77-47-4
Hexachloroethane
ND
ug1L
5.0
1.1
1
08/13/15 13:00
08/18/15 00:19 57-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
0.29
1
08/1311513:00
08118/1500:19 193-39-5
Isophorone
ND
ug/L
10.0
0.89
1
08/13/15 13:00
08/18/15 00:19 78-59-1
Naphthalene
ND
ug/L
5.0
0.34
1
08/13/15 13:00
08/18/15 00:19 91-20-3
Nitrobenzene
ND
ug/L
5.0
1.1
1
08/13/15 13:00
08/18/15 00:19 98-95-3
ND
ug/L
5.0
0.91
1
08/13/15 13:00
08/18/15 00:19 88-75-5
•2-Nitrophenol
4-Nitrophenoi
ND
ug/L
50.0
4.1
1
08/13/15 13:00
08/1&15 00:19 100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
0.91
1
08/13/15 13:00
08/18/15 00:19 62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
0.99
1
08/13/15 13:00
08/18/15 00:19 621-64-7
N-Nitrosodiphenylartiine
ND
ug/L
10.0
1.0
1
08/13115 13:00
08/18/15 00:19 86-30-6
Pentachlorophenol
ND
ug1L
10.0
4.6
1
08/13/15 13:00
08/18/15 00:19 87-86-5
Phenanthrene
ND
ug/L
5.0
0.22
1
08/13/15 13:00
08/18/15 00:19 85-01-8
Phenol
ND
ug1L
5.0
1.9
1
08/13/15 13:00
08/18/15 00,19 108-95-2
Pyrene
ND
ug1L
5.0
0.19
1
08/13/15 13:00
0&18/15 00:19 129-00-0
12,4-Trichlorot>enzene
ND
ug/L
5.0
0.98
1
08/13/15 13:00
08/18/15 00:19 120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1.3
1
08/13/15 13:00
08/18/15 00:19 88-06-2
Surrogates
Nitrobenzene-d5 (S)
60
%
10-120
1
08/13/15 13:00
08/18/15 00:19 4165-60-0
2-Ftuorobiphenyl (S)
58
%
15-120
1
08/13/15 13:00
08/18/15 00:19 321-60-8
Terphenyl-014 (S)
87
%
11-131
1
08/13/15 13:00
08/18/15 00:19 1718-51-0
Phenol-d6 (S)
17
%
10-120
1
08/13/15 13:00
08/18/15 00:19 13127488-3
2-Fluorophenol (S)
28
%
10-120
1
08/13/15 13:00
08A8/15 00.19 367-12-4
2.4.6-Tribromophenol (S)
71
%
10-137
1
08/13/15 13:00
08/18/15 00:19 118-79-6
624 Volatile Organics
Analytical Method: EPA624
Benzene
ND
ug&
2.0
1.7
1
08114/1523:36 71-43-2
Bromodichloromethane
ND
ug/L
2.0
1.7
1
08/14/15 23:36 75-27-4
Bromoform
ND
ug1L
2.0
1.5
1
08/14/15 23:36 75-25-2
Bromomethane
ND
ug1L
2.0
1.0
1
08/14/15 23:36 74483-9
Carbon tetrachloride
ND
ug/L
2.0
1.9
1
08/14/15 23:36 56-23-5
Chlorobenzene
ND
ug1L
2.0
1.7
1
08/14/15 23:36 108-90-7
Chloroethane
ND
ug1L
2.0
1.6
1
08/14/15 23:36 75-00-3
Chloroform
ND
ug/L
2.0
1.9
1
08/14/15 23:36 67.66-3
Chloromethane
ND
ug/L
2.0
1.5
1
08/14/15 23:36 74-87-3
• REPORT OF LABORATORY ANALYSIS
• This report shall not be reproduced, except in full,
Date: 08120/2015 04:15 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 36

ceArWcal
www.pacdapxcnrrr
ANALYTICAL RESULTS
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Sample 3 Lab ID: 92263080003 Collected: 08/11/15 17:30 Received: 08/12/15 11:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
624 Volatile Organics
Dibromochloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
11-Dichloroethene
cis-1,2-Dichioroethene
trans-1 ,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethytbenzene
Methylene Chloride
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
Vinyl chloride
Surrogates
4-Bromofluorobenzene (S)
Toluene-08 (S)
1,2-Dichloroethane-d4 (S)
25400 Total Suspended Solids
Total Suspended Solids
9040 pH
pH
Date: 08120/2015 04:15 PM
Analytical Method: EPA624
ND
ug1L
2.0
1.8
1
08/14/15 23:36 124 48-1
ND
ug1L
2.0
1.5
1
08/14/15 23:36 95-50-1
ND
ug/L
2.0
1.5
1
08/14/15 23:36 541-73-1
ND
ug/L
2.0
1.5
1
08/14/15 23:36 106-46-7
ND
ug/L
2.0
1.8
1
08/14/15 23:36 75-34-3
ND
ug1L
2.o
1.8
1
08/14/15 23:36 107-06-2
ND
ug/L
2.0
1.9
1
08/14/15 23:36 75-35-4
ND
ug/L
2.0
1.8
1
08/14/15 23:36 156-59-2
ND
ug1L
2.0
1.8
1
08/14/15 23:36 156-60-5
ND
ug/L
2.0
1.7
1
08/14/15 23:36 78-87-5
ND
ug/L
2.0
1.6
1
08/14/15 23:36 10061-01-5
ND
ug/L
2.0
1.6
1
08/14/15 23:36 10061-02-6
ND
ug1L
2.0
1.6
1
08/14/15 23:36 100-41-4
ND
ug/L
2.0
1.9
1
08/14/15 23:36 75-09-2
ND
ug/L
2.0
1.5
1
08/14/15 23:36 79-34-5
ND
ug/L
2.0
1.8
1
08/14115 23:36 127-18-4
ND
ugA-
2.0
1.6
1
08/14/15 23:36 108-88-3
ND
ug/L
2.0
1.9
1
08/14/15 23:36 71-55-6
ND
ug/L
2.0
1.7
1
08/14/15 23:36 79-00-5
ND
ug/L
2.0
1.8
1
08/14/15 23:36 79-01-6
ND
ug/L
2.0
1.7
1
08/14/15 23:36 75-69-4
ND
ug/L
2.0
1.5
1
08/14/15 2136 75-01-4
102
%
70-130
1
08/14/15 23:36 460-00-4
104
%
70-130
1
08/14/15 23:36 2037-26-5
107
%
70-130
1
08/14/15 23:36 17060-07-0
Analytical
Method: SM 2540D
8.2
mg1L
2.5
2.5
1
08/14/1513:16
Analytical
Method: EPA9040
6.7
Std, Units
0.10
0.10
1
08/13/15 12:25 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 36
is
•

ceAnalytical"
wwwPecelabscarn
QUALITY CONTROL DATA
Project: Semi -Annual August 2015
Pace Project No.: M63080
QC Batch: GCSV/22297 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92263080001, 92263080002, 92263080003
METHOD BLANK: 1535727 Matrix: Water
Associated Lab Samples: 92263080001, 92263080002, 92263080003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 08/18/15 08:17
LABORATORY CONTROL SAMPLE: 1535728
Parameter Units
Oil and Grease mg/L
MATRIX SPIKE SAMPLE: 1535729
Parameter Units
. Oil and Grease mg/L
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Spike LOS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 36.0 90 78-114
92262556001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 40 37.7 90 78-114
Results presented on this pope are in the units Wdlcrtod btr ehr 1Wts- column except w1w an aHernam unit Is presented to Ow rtgd of the result
• REPORT OF LABORATORY ANALYSIS
• This report sha11 not be reproduced, except in full,
Date: 0812WO15 04:15 PM without the written consent of Pace Analytical Services, Inc..
Page 15 of 36

ceAfialytical e
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QUALITY CONTROL DATA
ProjecL Semi -Annual August 2015
Pace Project No.: 92263080
QC Batch: MPRP/19247 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92263080001, 92263080002, 92263080003
METHOD BLANK: 1533236 Matrix: Water
Associated Lab Samples: 92263080001, 92263080002, 92263080003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Cadmium
mg/L
ND
0.0010
08/18/15 00:40
Chromium
mg/L
NO
0.0050
08/18/15 00:40
Copper
mg/L
ND
0.0050
08/18/15 00:40
Lead
mg/L
ND
0.0050
08118/1514:33
Nickel
mg/L
ND
0.0050
08/18/15 00:40
Silver
mg/L
ND
0.0050
08/18/15 00:40
Zinc
mg/L
ND
0.010
08/18/15 00:40
LABORATORY CONTROL SAMPLE:
1533237
Parameter
Units
Cadmium
mg/L
Chromium
mg/L
Copper
mg1L
Lead
mg/L
Nickel
mg/L
Silver
mg/L
Zinc
mg/L
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Qualifiers
Spike
LCS
LCS
% Rec
Conc.
Result
% Rec
Limits Qualifiers
.5
0.45
91
85-115
.5
0.45
90
85-115
.5
0.46
91
85-115
.5
0.46
92
85-115
.5
0.45
90
85-115
.25
023
91
85-115
.5
0.45
91
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1533238
1533239
MS
MSD
92263080001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc,
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Cadmium
mg/L
ND
5
.5
0,46
0.53
92
107
70-130
15
20
Chromium
mg/L
ND
.5
.5
0.46
0.53
92
106
70-130
15
20
Copper
mg/L
ND
.5
.5
0.47
0.54
93
108
70-130
15
20
Lead
mg/L
ND
.5
.5
0.47
0,55
93
109
70-130
15
20
Nickel
mglL
ND
.5
.5
0.46
0.53
92
106
70-130
15
20
Silver
mg1L
ND
.25
.25
0.23
0.26
91
106
70-130
15
20
Zinc
mg/L
ND
.5
.5
0.46
0.54
92
106
70-130
14
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1533240
1533241
MS
MSD
92263064001 Spike
Spike MS
MSD MS
MSD % Rec Max
Parameter Units Result Conc.
Conc, Result
Result % Rec
% Rec Limits RPD RPD Qual
Cadmium mg/L ND .5
.5 0.58
0.58 116
116 70-130 1 20
Chromium mg/L 11.1 ug/L .5
.5 0.44
0.44 86
85 70-130 0 20
Results presented on this paW are In the units indicated b7 the
"ll+ W column except where an alternate unit Is preserrte to the rVrt of the reautL
REPORT OF LABORATORY ANALYSIS
This n:pon shall not be reproduced, except in full.
Date: 08/20/2015 0415 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 36
0
0

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ceAnalytical
r+rs'�eoe�e:mm
i
i
QUALITY CONTROL DATA
Project: Semi -Annual August 2015
Pace Project No.: 92263080
Pace Analydcal Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1533240
1533241
MS
MSD
92263064001
Spike
Spike
MS
MSD
MS
MSD
°% Rec
Max
Parameter
Units
Result
Conc.
Cone.
Result
Result
°% Rec
% Rec
Limits
RPD
RPD Qual
Copper
mg/L
5.1 ug1L
.5
.5
0.56
0.56
112
111
70-130
0
20
Lead
mg/L
ND
.5
.5
0.37
0.37
74
74
70-130
1
20
Nickel
mg1L
873 ug/L
.5
.5
1.2
1.2
74
70
70-130
2
20
Silver
mg1L
ND
.25
.25
0.33
0.32
130
129
70-130
1
20
Zinc
mg/L
ND
.5
.5
0.44
0.44
86
86
70-130
0
20
Results presented on this papa am in the emits kxftWed by the "Wars" column except wove an altrernris unit is presented to the FW of the result
REPORT OF LABORATORY ANALYSIS
• This report shall not be reproduced. except in fup,
Date: 08/20/2015 04:15 PM without the written consent of Pace Analytical Services, Inc..
Page 17 of 36

e
CeAnalytical
whw 4%wdatsaom
QUALITY CONTROL DATA
Project: Semi -Annual August 2015
Pace Project No.: 92263080
QC Batch: MSV/33003
Analysis Method: EPA 624
QC Batch Method: EPA624
Analysis Description: 624 MSV
Associated Lab Samples: 92263080001, 92263080002, 92263080003
METHOD BLANK: 1534706
Matrix:
Water
Associated Lab Samples: 92263080001, 92263080002, 92263080003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
NO
2.0
08/1411512:28
1,1,2,2-Tetrachloroethane
ug/L
ND
2.0
08114/1512:28
1,1,2-Trichlaroethane
uglL
NO
2.0
0811411512:28
1,1-Dichloroethane
ug/L
ND
2.4
08/14/1512:28
1,1-Dichloroethene
ug/L
NO
2.0
08/14/1512:28
1,2-Dichlorobenzene
ug/L
NO
2.0
0811411512:28
1,2-Dichloroethane
ugJL
NO
2.0
0811411512:28
1,2-Dichloropropane
ug/L
NO
2.0
08114/1512:28
1,3-Dichlorobenzene
ug1L
NO
2.0
0811411512:28
1,4-Dichlorobenzene
ug/L
NO
2.0
08/1411512:28
Benzene
ug/L
NO
2.0
08/141151218
Bromodichloromethane
ug/L
NO
2.0
08/1411512:28
Bromoform
ug/L
NO
2.0
0811411512:28
Bromomethane
ug/L
NO
2.0
08/14/1512:28
Carbon tetrachloride
ug/L
NO
2.0
08/14/15 12:28
Chlorobenzene
ug/L
NO
2.0
08/1411512:28
Chloroethane
ug/L
NO
2.0
08/1411512:28
Chloroform
ug/L
NO
2.0
0811411512:28
Chloromethane
ug/L
ND
2.0
08114/1512:28
cis-1,2-Dichloroethene
ug/L
NO
2.0
08114/1512:28
cis-1,3-Dichloropropene
ug/L
ND
2.0
0811411512:28
Dibromochloromethane
ug/L
NO
2.0
0811411512:28
Ethylbenzene
ug/L
ND
2.0
0811411512:28
Methylene Chloride
ug/L
NO
2.0
08/14/15 12:28
Tetrachloroethene
ug/L
NO
2.0
08114/1512:28
Toluene
ug/L
NO
2.0
0811411512:28
trans-1,2-Dichloroethene
ug/L
NO
2.0
0811411512:28
trans-1,3-0ichlompropene
ug/L
ND
2.0
0811411512:28
Trichloroethene
ug/L
NO
2.0
08114/1512:28
Trichlorofluoromethane
ug/L
NO
2.0
0811411512:28
Vinyl chloride
ug/L
NO
2.0
08/14/15 12:28
1,2-Dichloroethane-d4 (S)
%
104
70-130
08/14/15 12:28
4-Bromofluorobenzene (S)
%
100
70-130
08/14115 12:28
Toluene-d8 (S)
%
104
70-130
08/14/15 12:28
Qualifiers
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1534707
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec. Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 20.8 104 52-162
1,1,2,2-Tetrachloroethane ug/L 20 18.7 94 46-157
Results presented on this page are In the trots Indicated by the -Units- column except where an aternats unit Is prosented to the r d of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/20/2015 04:15 PM without the written consent of Pace Analytical Services, Inc..
0
:7
•
Page 18 of 36

CeAr�lytiCal
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27268
[phone]
Project: Semi -Annual August 2015
Pace Project No.: 92263080
LABORATORY CONTROL SAMPLE:
1534707
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits
Qualsners
1,1,2-Trichloroethane
ug/L
20
18.5
92
52-150
1,1-Dichloroethane
ug/L
20
20.9
104
59-155
1,1-Dichloroethene
ugfL
20
22.6
113
1-234
12-Dichlorobenzene
ug1L
20
20.3
102
18-190
1,2-Dichloroethane
ug/L
20
18.6
93
49-155
1,2-Dichloropropane
ug1L
20
19.6
98
1-210
1,3-Dichlorobenzene
ug1L
20
20.2
101
59-156
1,4-Dichlorobenzene
ug/L
20
20.0
100
18-190
Benzene
ug1L
20
20.0
100
37-151
Bromodichloromethane
ug/L
20
20.7
104
35-155
Bromoform
ug/L
20
19.9
100
45-169
Bromomethane
ug/L
20
23.3
116
1-242
Carbon tetrachloride
ug/L
20
22.3
111
70-140
Chlorobenzene
ug/L
20
19.5
98
37-160
Chloroethane
ug/L
20
19.7
99
14-230
Chloroform
ug/L
20
20.6
103
51-138
Chloromethane
ug/L
20
20.9
104
1-273
cis-1,2-Dichloroethene
u91L
20
20.7
104
68-146
cis-1,3-Dichloropropene
ug/L
20
20.4
102
1-227
Dibromochloromethane
ug/L
20
20.6
103
53-149
Ethylbenzene
ug/L
20
19.7
99
37-162
Methylene Chloride
ug/L
20
21.8
109
1-221
Tetrachloroethene
ug/L
20
19.1
96
64-148
Toluene
ug/L
20
19.5
98
47-150
trans-12-Dichloroethene
ug/L
20
21.3
106
54-156
trans-1,3-Dichloropropene
ug/L
20
20.5
103
17-183
Trichloroethene
ug/L
20
19.6
98
71-157
Trichlorofluoromethane
ug/L
20
21.9
110
17-181
Vinyl chloride
ug/L
20
20.2
101
1-251
1,2-Dichloroethane-d4(S)
%
103
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
99
70-130
MATRIX SPIKE SAMPLE:
1534709
92263080003
Spike
MS
MS
% Rec
Parameter
Units
Result
Cone.
Result
% Rec
Limits Qualifiers
1, 1, 1 -Trichloroethane
ug1L
ND
20
23.6
118
46-171
1,1,2,2-Tetrachoroethene
ug/L
ND
20
20.6
103
73-159
1,1,2-Trichloroethane
ug/L
ND
20
21.3
107
64-152
1,1-Dichloroethane
ug/L
ND
20
21.7
109
43-172
1,1-Dichloroe#mne
ug/L
ND
20
25.7
128
48-189
1,2-Dichlorobenzene
ug/L
ND
20
20.8
104
54-154
1,2-Dichioroethane
ug1L
ND
20
21.8
108
42-171
1,2-Dichloropropane
ug/L
ND
20
22.3
112
55-157
1,3-Dichlorobenzene
ug/L
ND
20
21.4
107
57-148
Resu is presented an Oft page are in Vo unft 6agcMd try the Zlydta' eahnnn ezoepR where an 910ernata unit is pto pre fWd of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/20/2015 04-15 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 36
r

ceArWcal e
wwwcpeoetaftmm
QUALITY CONTROL DATA
Project: Semi -Annual August 2015
Pace Project No.: 92263080
PaceAnatyttcal Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
MATRIX SPIKE SAMPLE:
Parameter
1534709
Units
92263080003
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
NO
20
20.9
105
58-149
Benzene
ug/L
NO
20
23.2
116
54-163
Bromodichloromethane
ug/L
ND
20
25.0
118
56-152
Bromoform
ug/L
ND
20
21.3
106
53-151
Bromomethane
ug/L
NO
20
20.2
101
10-200
Carbon tetrachloride
ug/L
ND
20
24.4
122
41-175
Chlorobenzene
ug/L
ND
20
20.7
103
67-152
Chloroethane
ug/L
ND
20
24.4
122
23-200
Chloroform
ug/L
ND
20
24.1
117
51-166
Chforomethane
ug/L
ND
20
25.4
127
40-175
cis-1,2-Dichloroethene
ug/L
ND
20
23.8
119
45-174
cis-1,3-Dichloropropene
ug/L
ND
20
20.5
103
38-146
Dibromochlommethane
ug/L
ND
20
23.5
110
65-144
Ethylbenzene
ug/L
NO
20
20.6
103
57-152
Methylene Chloride
ug/L
ND
20
26.0
130
40-167
Tetrachloroethene
ug/L
ND
20
19.6
98
59-155
Toluene
ug/L
ND
20
21.3
106
47-162
trans-1,2-Dichtoroethene
ug/L
ND
20
23.8
119
47-178
trans- 1, 3-Dichloropropene
ug/L
ND
20
21.7
109
39-148
Trichloroethene
ug/L
NO
20
21.6
108
60-153
Trichlorofluoromethane
ug/L
ND
20
26.2
131
42-199
Vrrnyl chloride
ug/L
ND
20
21.7
109
46-176
1,2-Dichloroethane-d!4 (S)
%
106
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
SAMPLE DUPLICATE: 1534708
Parameter
Units
92263080002
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1-Trichloroethane
ug/L
NO
ND
30
1,1,22-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
NO
30
1,1-Dichloroethane
ug1L
ND
NO
30
1,1-Dichloroethene
ug/L
ND
NO
30
1,2-Dihlorobenzene
ug/L
NO
ND
30
1,2-Dichioroethane
ug/L
NO
ND
30
1,2-Dichloropropane
ug/L
NO
ND
30
1,3-Dichlorobenzene
u911-
ND
ND
30
1,4-Dichlorobenzene
ug1L
ND
ND
30
Benzene
ug/L
ND
NO
30
Bromodichloromethane
ug/L
ND
NO
30
Bromoform
ug/L
ND
NO
30
Bromomethane
ug/L
NO
NO
30
Carbon tetrachloride
ug/L
ND
ND
30
Chlorobenzene
ug/L
NA
ND
30
Results pr a ntsd an thla pate am in tiro writs irWlcated by the "Urdta" column excW Mm an alternate unit Is preswftd to the right of the reautL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/20/2015 04:15 PM without the written consent of Pace Analytical Sencces, Inc..
E
lJ
•
Page 20 of 36

CHAIN.OF.CUS# Analytical Request Document 2��J� _ •_
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