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NCG030663_MONITORING INFO_20171031
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. NCGD3 0 (/JI,3 �e u DOC TYPE ❑ STORICAL FILE MONITORING REPORTS DOC DATE ❑ Ro I � /0-9/- YYYYMMDD Compliance Inspection Repo Permit: NCG030663 Effective: 08/05/15 Expiration: 10/31/17 Owner: Select Stainless Products LLC 5OC. Effective: Expiration: Facility: Select Stainless Products, LLC County: Mecklenburg 11145 Monroe Rd Region. Mooresville Matthews NC 28105 Contact Person: George Thrower Tile: Phone: 704-841-1090Ext.141 Directions to Facility: Take Route 51 (Matthews Township Parkway) turn north on Charles Street, follow to SSP facility. System Classifications: Primary ORC: Certification: Phone: Secondary ORC(s): On-Ske Repnesentathre(s): Related Permits: Inspection Data: 05/12/2017 Entry Time: 09:OOAM Exit Time: 10:55AM Primary Inspector: Water Quality Program Meckenburg County Phone: 704-336-5449 Secondary Inspectorls): Zahid S khan Phone : Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Metal Fabrication Stormwater Discharge COC Facility Status: Compliant ❑ Not Compliant Question Areas: 0 Storm Water (See attachment summary) Page: 1 ,* pemdt NGG030663 Owner - Fatuity: Select Stainless Products LLC Inspection Daft: 05112/2017 Inspection Type. Compliance Evaluation Reason for Visit Routine Inspection Summary: Select Stainless Products, LLC is located at 11145 Monroe road in Matthews on approximately 8.3 acres. The facility fabricates custom stainless steel and wood products, primarily for use in the food service industry. Charlotte -Mecklenburg Storm Water Services (CMSWS) has not previously inspected this facility. At the time of inspection, Select Stainless Products, LLC was observed to be in compliance with the Mecklenburg County Surface Water Pollution Control Ordinance. The facility has exceeded the permit benchmark for Zinc at Outfall SW-2 during three consecutive semi-annual monitoring events and should proceed with Tiered response actions, per permit requirements. Since facility personnel suspect the adjacent business is the source of stormwater contamination, CMSWS recommends the facility consider conducting additional analytical monitoring to compare pollutant concentrations in runoff discharged onto the Select Stainless property from the adjacent business to flow from the outfall that includes stormwater generated both on -site and off -site. Page: 2 t pew NCG030663 owner - Facility: Select Stainless Products LLC Inspection Date: 05112I2017 InspwWn Type. Compliance Evaluation Reason for VisIL• Routine 5tornrwater Pollution Prevention Plan Yes No NA NE Does the site have a Stommater Pollution Prevention Plan? 0 ❑ ❑ ❑ # Does the Plan include a General Location (USGS) map? N ❑ ❑ ❑ # Does the Plan include a "Narrative Description of Practices"? 0 ❑ ❑ ❑ # Does the Plan include a detailed site map including outfall locations and drainage areas? N ❑ ❑ ❑ # Does the Plan irrdude a list of significant spills occurring during the past 3 years? E ❑ ❑ ❑ # Has the facility evaluated feasible a@ematives to current practices? E ❑ ❑ ❑ # Does the facility provide all necessary secondary containment? ❑ ❑ 0 ❑ # Does the Plan include a BMP summary? 0 ❑ ❑ ❑ # Does the Plan indude a Spilt Prevention and Response Plan (SPRP)? N ❑ ❑ ❑ # Does the Plan include a Preventative Maintenance and Good Housekeeping Plan? ❑ ❑ ❑ # Does the facility provide and document Employee Training? ❑ ❑ ❑ # Does the Plan include a list of Responsible Party(s)? N ❑ ❑ ❑ # Is the Plan reviewed and updated annually? ❑ ■ ❑ ❑ # Does the Plan include a Stormwater Facility Inspection Program? ■ ❑ ❑ ❑ Has the Stomrwater Pollution Prevention Plan been implemented? 0 ❑ ❑ ❑ Comment: Per the facility manager, no significant spills have occurred within the previous three vears. The facility should make an annual "notation of no spills", as per Part II, Section A, 8(a) of the permit. A non-stormwater discharge evaluation was documented during a facility inspection on 5/26/16. CMSWS recommends documenting this evaluation on a separate sheet as oart of the annual upstate or including evaluation criteria on the site insDection document to ensure this evaluation occurs during ambient conditions. CMSWS recommends updating the spill prevention and response plan to include the facifitYs new maintenance su ervisor. Em to ee training was conducted and documented on several dates in January 2017. The last documented stormwater Dollution prevention plan reviewluodate was conducted on 6/8/2015._ The facility should conduct and document an annual review/update of the stormwater pollution prevention plan. Facility inspections were conducted on 12/1/2016'and 5/25/16_ Qualitative Monitoring Yes No NA NE Has the facility conducted its Qualitative Monitoring semi-annually? 0 ❑ ❑ ❑ Page- 3 Pemwt NCG030663 owner - Faculty: Select Stainless Products LLC inspection Data; 05112/2017 Inspection Type: compliance Evaluation Reason for VIM Routine Comment: Qualitative monitoring was conducted on 12/5/16 and 5/17/16. AnahMcal Monitoring Has the facility conducted its Analytical monitoring? # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? Comment: Analvtical monitoring was conducted on 1215116, 12/1116, 5/17/16, and 10127/15. The facili Yes No NA NE ■❑❑❑ ❑ ❑ N ❑ exceeded the benchmark for zinc at both outfalls on the 10/27/15 event, at outfall #002 during the 1215116 and 5/17/16 events. Per chain of custody documentation H analysis is conducted at an offsite laboratory outside of the hold time specified in 40 CFR Part 136; PH analysis should occur within 15 minutes of sample collection. Permit and Outfalls Yes No NA HE # Is a copy of the Permit and the Certificate of Coverage available at the site? 0 ❑ ❑ ❑ # Were all outfalls observed during the inspection? M ❑ 110 # If the facility has representative outfall status, is it property documented by the Division? ❑ ❑ M ❑ # Has the facility evaluated all illicit (non stormwater) discharges? ❑ ❑ M ❑ Comment: The facility has certificate of coverage NCG030663. No stormwater pollution issues were observed at the outfalls. Page: 4 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted February 5, 2018 CERTIFICATE OF COVERAGE NO. NCG03 0 6 6 3 FACILITY NAME elect Stainless Products LLC COUNTY Mecklenburg PERSON COLLECTING SAMPLES Michael Smith LABORATORY: Prism Laboratories Lab Cert. # 402 Comments on sample collection or analysis: Suspect Field pH Meter Malfunction Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ❑ Monthly' January (month) RECEIt�ffGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply []SA FEB 0 8 2018 ❑Other: Class C Secondary Recreation CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 � OWR SECTION No discharge this period?' Outfall No: Date Sample 1 Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard.units Copper 'Lead Zinc . Non -Polar O&G/ Total Petroleum+ Hydrocarbons Total Toxic 15 Organics., Benchmarks ===> _ - 100 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SW-1 2/21/2018 0.05 130 mg/L 5.52 (Field) 0.025 mg/L 0.0051 mg/L 0.21 mg/L 6.6 mg/L <1 mg/L 6.6 HT (Lab) SW-2 1/11/2019 0.05 72 mg/L 4.06 (Field) 0.016 mg/L 0.0079 mg/L 2.0 mg/L <5.0 mg/L <1 mg/L 6.2 HT (Lab) 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." Adam Calton Name (Print name) Maintenance Manaeer Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value In excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfali No. Date Sample f Collected (mo/dd/ r) 2a-hour rainfall amount, Inches; Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L" 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B ' See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 -Wate: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See Genera! Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Khan zahid Mail an orl Ina! and one My 91 this DMR including all "No Discharge" reports within 30 da s o recei t o the lab results or at end o monitorin eriod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted January 18, 2018 CERTIFICATE OF COVERAGE NO. NCG03 0 6 6 3 FACILITY NAME Select Stainless Products LLC COUNTY Mecklenburg PERSON COLLECTING SAMPLES Michael Smith LABORATORY: Prism Laboratories Lab Cert. # 402 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec REC�LPL.EN&S or ❑ Monthly) December (month) ARGiNG TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA JAN 25 Zola . [_]zero -flow ❑Water Supply ❑SA [—]Other: Class C Secondary Recreation DwR SECTION PLEASE PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -) No discharge this period?z Outfall No. Date Sample Collected) (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids pH, Standard units - Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks 100 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SWA 12/20/2017 1.01 140 mg/L 6.82 (Field) 0.016 mg/L <0.005 mg/L 0.25 mg/L 8.3 mg/L <1 mg/L SW-2 22/20/2017 1.01 49 mg/L 6.16 (Field) 0.0087 J mg/L <0.005 mg/L 1.4 mg/L <5.0 mg/L <1 mg/L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. i For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. Thy solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For (hose facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (T70), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." George Thrower III _ Name (Print name) I 0-NS (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX ms where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Khan Zahid Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reportsj. to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those personsgdirectl's�iiefor gatherin the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete a e thaalties for s mitting false information, including the possibility of fines and imprisonment for knowing violations." (Si ature o ) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi- nnual StorMwplpr Dischar a Monitoring Report for North Carolina Division of Water Quality General Permit No. NCGO30000 Date submitted December 4 2017 CERTIFICATE OF COVERAGE No. NCG03 0 6 6.1 FACILITY NAME I §glggProducts C COUNTY Mecklenburg PERSON COLLECTING SAMPLES LABORATORY: Lab Cart. 9 _ Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 20i7 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ❑ REO&%yeM November^ Imonth) �DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA JAN 2 5 2018 zero -flow ❑Water supply [:]SA QrAITRAL FILES Other: Class 1-Secondary Recreation DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ® No discharge this period ?2 OutfalfNo. Date Sam le p Collected i (ma/dd/yr 24-hour rainfall _ amount, ' Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ r _Total Petroleum Hydrocarbons Total Tgxle - s Organics .• Benchmarks ===> 100 mg/L 6.0=9.0 0.007 mg/L 0.03'mg/L .• �i0.067 mg/L 15 mg/L a SW-1 sw-z Monthly sampling ('instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same Darameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found In 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities Oat incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may he waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my Inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility Is Implementing the all the provisions of the solvent management plan Included in the Stormwater Pollution Prevention Plan." r e Thj9&gr III Name (Print name) l-z s-1-7 (Date) Note: Results must be reported In numerical format. fi}a not rerrort Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported In the format. "<XX ms/L". where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must Implement Tier 1, Tler Z or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge Is period?z Out#all No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, a Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended 5ollds - OH. . Beachmarks ===> _ 15 mg/L 100 mg/L or,SO mg/L• 6.0 — 9.0 SU. Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If, you report a sample value In excess of the benchmark, you must Implement Tier 1, Tler 2, or Tier 3 responses. See General Permit text FOR PART A_AND PART R MONITOING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. 4 TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Khan Z.abld ' Mall an orlainal and one cony. of this DMR Includlna all "No Discharge -resorts, within 30 days of receipt of the lab resylts tor at end of monitoring nerlad In the case of "No Dlscharne" reportsl to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPpii<TFD, "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person or persons who manage the system, or those ersons directly r ns for gathering the information, the information submitted Is, to the best of my knowledge and belief, true, accurate, and complete. I yr re that the i r submitting false Information, including the possibility of fines and Imprisonment for knowing violations." (Si atu e o erm tee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted November 28 2017 CERTIFICATE OF COVERAGE NO. NCG03 0 6 6 3 FACILITY NAME Select Stainless Products LLC COUNTY Mecklenburg PERSON COLLECTING SAMPLES Michael O. Smith LABORATORY: Prism Laboratories Lab Cert. # 402 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ❑ Monthly[ October [month) R"VeU CLASS ❑ORW ❑HQW ❑Trout^ ❑PNA ❑Zero -flow ❑Water Supply ❑SA JAN 25 2018 ❑Other: Class C Secondary Recreation CENTRAL F'I DWR SECT i1SE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 ❑ No discharge this period ?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks - - 160 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067. mg/L 15 mg/L 1 mg/L SW-1 10/23/2017 1.09 210 7.9(Field) 0.020 0.0085 0.42 30 e2 SW-2 10/23/2017 1.09 33 7.7 (Field) 0.0043 J <0.005 1.2 <5 <1 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities iMt incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." George Thrower III _ Name (Print name) S afety Manager/Talent Ac uisition & Recruitment Specialist itle Print title) ?6 `nature)� (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PqL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Ej No discharge this period?' Outfall Na. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: ifyft report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? - YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Khan Zahid Mail an origlnal and one copy of this DMR, including_ all "No Discharge" reports, within 30 days of receipt of the lob results for at end of monitorina period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. re that the s' penaltie for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Sig6ature of Per tteej (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Monthly Stormwater Dischar a Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted October 6, 2017 CERTIFICATE OF COVERAGE NO. NCG030663 FACILITY NAME Select Stainiess Prgdugls LL COUNTY Mecklenbure PERSON COLLECTING SAMPLES David Mazorra LABORATORY Lab Cert. # Comments on sample collection or analysis: No Flow SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' seotember (month) I GING TO CLASS ❑ORW ❑HQW []Trout❑PNA RECEIVE ®Zero -flow ❑water5upply [—]SA OCT I X 2017 [—]Other CENTRAL, FILLS PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 3 DWa SECTION 2 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. s The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found In 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring maybe waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is Implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." David R. Mazorra, PE Name (Print name) Senior En i eer Title (Print tie) 10/6/17 _ (5ignatur (Date) Note: Results must be reported In numerical format. Do nolreport Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported In the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must Implement Tler 1, Tier 1, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ® No discharge this f 15ate:Sample .:,:.>;:24-hour: ra all.: ;::.....:....:.l#ected.;:: ;;::,:.amount,::.::::r:. Nan-palar-O&G/.TPH:b Y :::Total Sus ended Solids '::.:: `;.: 3 p........ pH ............:....:• :::.........:....:.......: mo dd : r :::.:.Inches•:::•::::::.. •:.FPA:'.1664. SGT HEM ::; :.............................. i . l.. /y.1. l 1 ::.:...:..... . SW-1 SW-2 Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2of3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text. FOR PART AAND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an orJ final and one capy of this DMIi including all "No Discharge" reports, within 30 days of recel t of the lab results for at end of monitoring eriod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1G17 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person or persons who manage the system, or those persons dir ctly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that t#re are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date: 11/1/2012-10/31/2017 10/6/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 Monthly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE No. NCG030663 FACILITY NAME Select Stainless Products I.I.C. COUNTY Mecklenburg PERSON COLLECTING SAMPLES David Mazorra LABORATORY Prism Laboratories, Inc. Lab Cert. # 402 Comments on sample collection or analysis: An offsite sample was collected in an effort to identify the presence of an offsite source of Zinc. This offsite sample drained into SW-2. Part A: Stormwater Benchmarks and Monitoring Results 017 SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' August (month) DISCHARGING TO CLASS ❑ORW ❑HQW [:]Trout❑PNA RECEIVED ❑Zero -flow ❑Water Supply []SA OCT 11 2017 ®Other Class C CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTION ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids mg/L pH, Standard units Copper mg/L Lead mg/L Zinc mg/L Non -Polar O&G/ Total Petroleum Hydrocarbons mg/L Total Toxic Organics ' mg/! Benchmarks =__> - - 100 6.0 — 9.0 0.007 0.030 0.067 15 1 SW-1 08/31/17 1.25 60 6.5 <0.0010 <0.0010 0.12 <1.1 <1 SW-2 08/31/17 1.25 <2.6 4.3 <0.0010 <0.0010 0.44 <1.1 <1 Offsite-2 08/31/17 1.25 140 6.3 0.011 0.0051 0.088 <1.1 <1 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." David R. Mazorra, PE Name (Print name) Senior Environmental Engineer Title ( nt title) (Signature) (Da 'e) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. (Vote. if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU SW-1 SW-2 Footnotes from Part A also apply to this Part 8 * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2D12 Page 2 of 3 Note. if you` report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART it SECTION B. • TIER 3; HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Khan Zahid Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to. Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there VE alties for submitting false information, including the possibility fines nd imprisonment for knowing violations." a Z� (Signature of Permittee) (Da e) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Case Narrative PIDDGSM -VItABORATORIES. ING Full -Service Analytical & Environmental Solutions GTA (Geo-Tech. Assoc. Inc.) Charlotte Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Monthly SW Lab Submittal Date: 09/01/2017 Prism Work Order: 7090021 09/19/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Data Qualifiers Key Reference: Reviewed By Cara C. Rusmisell Project Manager CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. HT Sample received and analyzed outside of the hold time. OG HEM O&G is less than the reporting limit, therefore TPH (SGT-HEM) is less than the reporting limit. Sample not extracted for TPH (SGT-HEM). BRL Below Reporting Limit MDL Method Detection Limit R_PD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the wntten consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240W - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Tall Free Number: 1-8001529-6364 - Fax: 70415254409 Page 1 of 24 Lih Full-Service Analytical Environmental Solutions �Ll�.aeF�TOXIES ING Sample Receipt Summary 09/19/2017 Prism Work Order: 7090021 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received SW-1 7090021-01 Water 08/31/17 09/01/17 SW-2 7090021-02 Water 08/31/17 09/01/17 Samples were received in good condition at 4.7 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism laboratories, Inc. 449 5pringbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704I52"409 Page 2 of 24 Full -Service Analytical & Laboratory Report j p® � �. ®P } I M Environmental Solutions 0911912017 u�eoN.Ton�s me GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-1 Attn: Dave Mazorra Prism Sample ID: 7090021-01 710 Peninsula Lane, #B Prism Work Order: 7090021 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 08/31/17 15:00 Time Submitted: 09/01/17 11:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DaterTime ID General Chemistry Parameters Oil & Grease (SGT-HEM) BRLOG mg1L 5.0 1.1 1 *166413 9114/17 12:40 SLS P710212 pH 6.5 HT pH Units 1 *SM4500-H B 911117 11:53 BMS P710010 Total Suspended Solids 60 mg1L 8.3 0.40 1 *SM2540 D 917117 12:56 SLS P710094 Organochlorine Pesticides by GCIECD alpha-BHC BRL ug/L 0,051 0.010 1 *608 9114117 17:26 JMC P710086 beta-BHC BRL ug11- 0.051 0.016 1 *608 9/14/17 17:26 JMC P710086 gamma-BHC BRL uglL 0.051 0.013 1 '608 9114/17 17:26 JMC P710086 delta-BHC BRL ug/L 0.051 0.014 1 '608 9114/17 17:26 JMC P710086 Heptachlor BRL ug1L 0.051 0.017 1 '608 9114/17 17:26 JMC P710086 Aldrin BRL ug/L 0.051 0.015 1 *608 9114117 17:26 JMC P710086 Heptachlor Epoxide BRL ug/L 0.051 0,013 1 '608 9114117 17:26 JMC P710086 trans -Chlordane BRL ug/L 0.051 0.027 1 '608 9114117 17:26 JMC P710086 Gs -Chlordane BRL ug/L 0.051 0.042 1 '608 9114117 17:26 JMC P710086 Dieldrin BRL ug/L 0.051 0.014 1 *608 9114117 17:26 JMC P710086 4,4'-DDE BRL ug1L 0.051 0.011 1 '608 9/14/17 17:26 JMC P710086 Endrin BRL ug1L 0.051 0.015 1 *606 9/14117 17:26 JMC P710086 Endosulfan II BRL ug/L 0.051 0.016 1 '608 9/14/17 17:26 JMC P710086 4,4'-DDD BRL ug/L 0.051 0.020 1 *608 9/14/17 17:26 JMC P710086 Endrin Aldehyde BRL ug/L 0,051 0.030 1 1608 9114117 17:26 JMC P710086 Endosulfan Sulfate BRL ug/L D.051 0.016 1 *608 9114117 17:26 JMC P710086 4,4'-DDT BRL ug/L 0.051 0,024 1 '608 9114117 17:26 JMC P710086 Endrin Ketone BRL ug/L 0.051 0.032 1 *608 9114117 17:26 JMC P710086 Methoxychlor BRL ug1L 0.051 0.040 1 *608 9114117 17:26 JMC P710086 Chlordane BRL ug/L 0.51 0.096 1 *608 918117 20:27 JMC P710086 Toxaphene BRL ug1L 0.51 0.076 1 '608 918117 20:27 JMC P710086 Aroclor 1016 BRL ug/L 0.51 0.25 1 '608 918117 20:27 JMC P710086 Aroclor 1221 BRL ug/L 1.0 0.11 1 *608 918117 20:27 JMC P710086 Aroclor 1232 BRL ug/L 0.51 0.16 1 'fi08 918117 2017 JMC P710086 Aroclor 1242 BRL ug1L 0.51 0.14 1 *608 918117 20.27 JMC P710086 Aroclor 1248 BRL ug/L 0.51 0.14 1 'fi08 918117 20:27 JMC P710086 Aroclor 1254 BRL ugll. 0.51 0.16 1 *608 918117 20:27 JMC P710086 Aroclor 1260 BRL ug1L 0.51 0.30 1 '608 918117 20:27 JMC P710086 Surrogate Recovery Control Limits Tetrachloro-m-xylene 81 % 40-134 Decachlorobiphenyt 79 % 13-186 Semivolatile Organic Compounds by GCIMS 1,2,4-Trichlorobenzene BRL ug/L 10 1.5 1 '625 916117 19:34 JMV P7t0065 1 Z-Dichlorobenzene BRL ug/L 10 1.5 1 '625 916117 19:34 JMV P710065 1,2-Diphenylhydrazine (as Azobenzene) BRL ug/L 10 3.0 1 *625 9/6117 19:34 JMV P710065 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 3 of 24 Laboratory Report IS n n( Eun-Service al Solutio 8QkR,^J , V' Environmental Solutions 0911912017 �V I../1BONATOfitE$ ING GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-1 Attn: Dave Mazorra Prism Sample ID: 7090021-01 710 Peninsula Lane, #B Prism Work Order: 7090021 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 08/31/17 15:00 Time Submitted: 09/01/17 11:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis DatelTime Analyst Batch ID 1,3-Dichlorobenzene BRL uglL 10 1.4 1 *625 916117 19:34 JMV P710065 1,4-Dichlorobenzene BRL ug1L 10 1.4 1 'fi25 916117 19:34 JMV P710065 2,4,6-Trichlorophenol BRL ug1L 10 1.9 1 '625 9/6117 19:34 JMV P710065 2,4-Dichlorophenol BRL ug1L 10 1.6 1 *625 916117 19:34 JMV P710065 2,4-Dimethylphenof BRL ug1L 10 2.2 1 '625 916/17 19:34 JMV P710065 2,4-Dinitrophenol BRL ug1L 10 1.3 1 *625 916117 19:34 JMV P710065 2,4-Dinitrotoluene BRL uglL 10 3.1 1 '625 916117 19:34 JMV P710065 2,6-Dinitrotoluene BRL ug1L 10 3.1 1 '625 9/6117 19:34 JMV P710065 2-Chloronaphihalene BRL uglL 10 2.4 1 '625 916117 19:34 JMV P710065 2-Chlorophenol BRL ug1L 10 1.2 1 *625 916117 19:34 JMV P710065 2-Nitrophenof BRL ug1L 10 1.4 1 *625 916117 19:34 JMV P710065 3.3'-Dichlorobenzidine BRL ug1L 10 2.9 1 '625 916117 19:34 JMV P710065 4,6-Dinitro-2-methylphenol BRL • ug1L 10 2.0 1 '625 916117 19:34 JMV P710065 4-Bromophenyl phenyl ether BRL ug1L 10 3.3 1 *625 916117 19:34 JMV P710065 4-Chloro-3-methylphenol BRL uglL 10 2.4 1 *625 916117 19.34 JMV P710065 4-Chlorophenyl phenyl ether BRL ug1L 10 2.3 1 '625 916117 19:34 JMV P710065 4-Nitrophenol BRL ug1L 52 1.7 1 '625 916117 19:34 JMV P710065 Acenaphthene BRL ug1L 10 2A 1 *625 916117 19:34 JMV P710065 Acenaphthylene BRL uglL 10 2A 1 '625 916117 19:34 JMV P710065 Anthracene BRL uglL 10 3.3 1 *625 916117 19:34 JMV P710065 Benzidine BRL ug1L 100 14 1 `625 916117 19:34 JMV P710065 Benzo(a)anthracene BRL ug1L 10 3.2 1 *625 916117 19:34 JMV P710065 Benzo(a)pyrene BRL ug1L 10 3,8 1 *625 916117 19:34 JMV P710065 Benzo(b)fluoranthene BRL uglL 10 3.7 1 *625 916117 19,34 JMV P710065 Benzo(g,hJ)perylene BRL ug1L 10 3.6 1 625 916117 19:34 JMV P710065 Benzo(k)fluoranthene BRL ug1L 10 4.0 1 '625 916117 19:34 JMV P710065 bis(2-Chloroethoxy)methane BRL ug1L 10 1.9 1 *625 916117 19 34 JMV P710065 Bis(2-Chloroethyl)ether BRL uglL 10 1.7 1 `625 916117 19:34 JMV P710065 B'is(2-chloroisopropyl)ether BRLCCv ug/L 10 1.8 1 *625 9/6117 19:34 JMV P710065 Bis(2-Ethylhexyl)phthalate BRL ug1L 10 3.3 1 '625 916117 19:34 JMV P710065 Butyl benzyl phthalate BRL uglL 10 2.7 1 *625 916117 19:34 JMV P710065 Chrysene BRL uglL 10 3.5 1 `625 916117 19:34 JMV P710065 Dibenzo(a,h)anthracene BRL ug1L 10 3.5 1 *625 916117 19:34 JMV P710065 Diethyl phthalate BRL ug1L 10 2A 1 *625 916117 19:34 JMV P710065 Dimethyl phthalate BRL ug1L 10 1.6 1 *625 916117 19:34 JMV P710065 Di-n-butyl phthalate BRL ug/L 10 3.5 1 '625 916117 19:34 JMV P710065 Di-n-octyl phthalate BRL ug1L 10 3.8 1 *625 9/6117 19:34 JMV P710065 Fluoranihene BRL ug1L 10 3.6 1 '625 916117 19:34 JMV P710065 Fluorene BRL uglL 10 2.9 1 *625 9/6117 19:34 JMV P710065 Hexachlorobenzene BRL uglL 10 2.6 1 'S25 916117 19:34 JMV P710065 Hexachlorobutadiene BRL ug1L 10 2.1 1 '625 916117 19:34 JMV P710065 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529.6354 -Toll Fre Page 4 of 24 e Number. 1�001529-6364 -Fax: 7041525-0409 v, ®�I J I S n n Full-Seice Analytical & ' V' EnvironmenSaE Solutions �LABOMTdilE3 LNG Laboratory Report 09/1912017 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Sample Matrix: Water Client Sample ID: SW-1 Prism Sample ID: 7090021-01 Prism Work Order: 7090021 Time Collected: 08/31/17 15:00 Time Submitted: 09/01/17 11:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Hexachlorocyclopentadiene BRL ug/L 10 1.7 1 '625 916117 19:34 JMV P710065 Hexachtoroethane BRL ug/L 10 1.6 1 *625 916117 19:34 JMV P710065 Indeno(1,2,3-cd)pyrene BRL ug1L 10 3.2 1 *625 916117 19:34 JMV P710065 Isophorone BRL ug1L 10 2.2 1 '625 916117 19:34 JMV P710065 Naphthalene BRL ug/L 10 2.2 1 '625 916117 19:34 JMV P710065 Nitrobenzene BRL ug/L 10 1.4 1 '625 916117 19:34 JMV P710065 N-Nitrosodimethylamine BRL ug/L 10 0.86 1 '625 916117 19:34 JMV P710065 N-Nitroso-di-n-propylamine BRL ug/L 10 2.1 1 `625 916117 19:34 JMV P710065 N-Nitrosodiphenylamine BRL ug/L 10 3.0 1 *625 916117 19:34 JMV P710065 Pentachlorophenol BRL ug/L 10 2.2 1 '625 916117 19:34 JMV P710065 Phenanthrene BRL ug/L 10 3.3 1 '625 916117 19:34 JMV P710065 Phenol BRL ug/L 10 0.50 1 '625 916117 19:34 JMV P710065 Pyrene BRL ug/L 10 3.6 1 '625 916117 19:34 JMV P710065 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 74 % 31-144 2-Fluorobiphenyl 68 % 49-118 2-Fluorophenol 47 % 22-84 Nitrobenzene-d5 71 % 43-123 Phenol-05 32 % 10-63 Terphenyl-d14 75 % 49-151 Total Metals Copper BRL mg1L 0,010 0.0010 1 *200.7 9111/17 19:01 JAB P710071 Lead BRL mg[L 0.0050 0.0010 1 *200.7 9111/17 19:01 JAB P710071 Zinc 0.12 mg1L 0.030 0.0013 1 *200.7 9111117 19:01 JAB P710071 Volatile Organic Compounds by GC1M5 1,1,1-Trichloroethane BRL ug/L 5.0 0.061 1 '624 912117 0:04 KDM P710031 1,1,2,2-Tetrachloroethane BRL ug/L 5.0 0,036 1 '624 912117 0:04 KDM P710031 1,1,2-Tdchloroethane BRL ug/L 5.0 0.066 1 '624 912117 0:04 KDM P710031 1,1-Dichloroethane BRL ug/L 5.0 0.083 1 *624 912117 0:04 KDM P710031 1, 1 -Dichloroethylene BRL ug/L 5.0 0,083 1 '624 912117 0:04 KDM P710031 1,2-Dichlorobenzene BRL ug/L 5.0 0.076 1 '624 912117 0:04 KDM P710031 1,2-Dichloroethane BRL ug1L 5.0 0.066 t `624 912117 0:04 KDM P710031 1,2-Dichloropropane BRL ug/L 5.0 0.11 t '624 912117 0:04 KDM P710031 1,3-Dichlorobenzene BRL ug/L 5.0 0.054 1 '624 912117 0:04 KDM P710031 1,4-Dichlorobenzene BRL ug/L 5.0 0.050 1 '624 912117 0:04 KDM P710031 2-Chloroethyl Vinyl Ether BRL ug1L 10 0.37 1 '624 912117 0:04 KDM P710031 Acrolein BRL ug/L 100 0.20 1 *624 912117 0:04 KDM P710031 Acrylonitrile BRL ug/L 100 0.20 1 *624 912117 0:04 KDM P710031 Benzene BRL ug/L 5.0 0.048 1 '624 912117 0:04 KDM P710031 Bromodichloromethane BRL ug1L 5.0 0.062 1 '624 912117 0:04 KDM P710031 Bromoforrn BRL ug/L 5.0 0.040 1 '624 912117 0:04 KDM P710031 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529.6364 • Toll Free Number: 1-800152M364- Fax: 70415254409 Page 5 of 24 Laboratory Report Lot, Full-Servico Analytical & Environmental Solutions 09/19/2017 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-1 Attn: Dave Mazorra Prism Sample 1D: 7090021-01 710 Peninsula Lane, #B Prism Work Order: 7090021 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 08/31/17 15:00 Time Submitted: 09/01/17 11:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime ID Bromomethane BRL ug1L 10 0.18 1 '624 912117 0:04 KDM P710031 Carbon Tetrachloride BRL ug/L 5.0 0.11 1 `624 9017 0:04 KDM P710031 Chlorobenzene BRL ug1L 5.0 0.062 1 "624 912/17 0:04 KDM P710031 Chloroethane BRL ug1L 10 0.22 1 'fi24 912117 0-04 KDM P710031 Chloroform BRL ug/L 5.0 0.076 1 '624 912/17 0:04 KDM P710031 Chloromethane BRL uglL 10 0.079 1 '624 9/2117 0:04 KDM P710031 cis-1,3-Dichloropropylene BRL ug1L 5.0 0.079 1 '624 912117 0:04 KDM P710031 Dibromochloromethane BRL ug/L 5.0 0.081 1 624 912117 0:04 KDM P710031 Ethylbenzene BRL ug1L 5.0 0.061 1 '624 9/2117 0:04 KDM P710031 Methylene Chloride BRL ug1L 5.0 0.083 1 '624 912/17 0:04 KDM P710031 Tetrachloroethylene BRL ug1L 5,0 0098 1 '624 912117 0:04 KDM P710031 Toluene BRL ug1L 5.0 0.044 1 `624 912/17 0:04 KDM P710031 trans-1,2-Dichloroethylene BRL ug/L 5.0 0.094 1 '624 912117 0:04 KDM P710031 trans-1,3-Dichloropropylene BRL ug1L 5.0 0.070 1 '624 9/2117 0:04 KDM P710031 Trichloroethylene BRL uglL 5.0 0.078 1 '624 9/2117 0.04 KDM P710031 Tnchlorofluoromethane BRL uglL 10 0.062 1 '624 9/2/17 0:04 KDM P710031 Vinyl chloride BRL ug1L 10 0.097 1 '624 912/17 0:04 KDM P710031 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 74-126 Dibromofluoromethane 101 % 75-127 Toluene-d8 101 % 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - fax: 704152"409 Page f of 24 .`z Laboratory Report .> Full -Service Analytical & J Environmental Solutions 09119/2017 -®ueonn yes ir+c GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-2 Attn: Dave Mazorra Prism Sample ID: 7090021-02 710 Peninsula Lane, #B Prism Work Order: 7090021 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 08/31/17 15:30 Time Submitted: 09/01/1711:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime ID General Chemistry Parameters Oil & Grease (SGT-HEM) BRLOG mg/L 5.0 1.1 1 '1664B 9/14/17 12:40 SLS P710212 pH 4.3 HT pH Units 1 'SM4500-H B 911117 11:53 SMS P710010 Total Suspended Solids BRL mg1L 2.6 0.40 1 'SM2540 D 917117 12:56 SLS P710094 Organochlorine Pesticides by GCIECD alpha-BHC BRL ug1L 0.054 0.011 1 '608 9/14/17 17:38 JMC P710086 beta-BHC BRL ug1L 0,054 0.017 1 '608 9114117 17:38 JMC P710086 gamma-BHC BRL ug1L 0.054 0.014 1 '608 9114/17 17:38 JMC P710086 delta-BHC BRL uglL 0.054 0.015 1 '608 9/14117 17:38 JMC P710086 Heptachlor BRL ug1L 0.054 0.018 1 '608 9114117 17:38 JMC P710086 Aldnn BRL ug1L 0.054 0.016 1 *608 9114/17 17:38 JMC P710086 Heptachlor Epoxide BRL ug1L 0,054 0,014 1 'fi08 9114117 17:38 JMC P710086 trans -Chlordane BRL uglL 0.054 0.028 1 '608 9114/17 17:38 JMC P710086 Endosulfan I BRL ug1L 0.054 0.021 1 '608 9114117 17:38 JMC P710086 cis -Chlordane BRL ug1L 0.054 0.045 1 *608 9114117 17:38 JMC P710086 Dieldrin BRL ug1L 0.054 0.015 1 1608 9/14117 17:38 JMC P710086 4,4'-DDE BRL ug1L 0.054 0.012 1 '608 9/14/17 17:38 JMC P710086 Endnn BRL uglL 0.054 0.016 1 '608 9114117 17:38 JMC P710086 Endosulfan II BRL ug1L 0.054 0.017 1 608 9/14/17 17:38 JMC P710086 4,4'-DDD BRL ug1L 0.054 0.022 1 608 9/14/17 17:38 JMC P710086 Fndnn Aldehyde BRL uglL 0.054 0.032 1 '608r 9114117 17:38 JMC P710086 Endosulfan Sulfate BRL uglL 0.054 0.017 1 '608 9/14/17 17:38 JMC P710086 4,4'-DDT BRL ug1L 0.054 0.026 1 608 9114117 17:38 JMC P710086 Endnn Ketone BRL ug1L 0.054 0,034 1 '608 9114117 17:38 JMC P710086 Methoxychlor BRL ug1L 0,054 0.042 1 *608 9114117 17:38 JMC P7t0086 Chlordane BRL ug1L 0.54 0.10 1 1608 918117 20:38 JMC P710086 Toxaphene BRL ug1L 0.54 0.080 1 608 918117 20:38 JMC P710086 Aroclor 1016 BRL ug1L 0.54 0,27 1 608 918117 20:38 JMC P710086 Aroclor 1221 BRL ug1L 1.1 0.12 1 '608 918117 20:38 JMC P710086 Aroclor 1232 BRL uglL 0.54 0.17 1 '608 918117 20:38 JMC P710086 Aroclor 1242 BRL uglL 0.54 0.15 1 608 918117 20:38 JMC P710086 Aroclor 1248 BRL ug1L 0.54 0.15 1 '608 918117 20:38 JMC P710086 Arodor 1254 BRL tag1L 0.54 0.17 1 '608 9/8117 20:38 JMC P710086 Aroclor 1260 BRL ug1L 0.54 0.32 1 '608 918117 20:38 JMC P710086 Surrogate Recovery Control Limits Tetrachloro-m-xylene 76 % 40-134 Decachlorobiphenyl 100 % 13-186 Semivolatile Organic Compounds by GUMS 1,2,4-Trichlorobenzene BRL ug1L 11 1.6 1 '625 916117 19:57 JMV P710065 1,2-Dichlorobenzene BRL ug1L 11 1.6 1 '625 916117 19:57 JMV P710065 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, fnc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529.6364 - Fax: 7041525-0409 Page 7 of 24 Full -Service Analytical 8 Laboratory Report ®PRISM Environmental Solutions 09119/2017 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-2 Attn: Dave Mazorra Prism Sample ID: 7090021-02 710 Peninsula Lane, #B Prism Work Order: 7090021 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 08/31/17 15:30 Time Submitted: 09/01/17 11:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis DatelTime Analyst Batch ID 1,2-Diphenylhydrazine (as Azobenzene) BRL ug1L 11 3.2 1 '625 9/6117 19:57 JMV P710065 1,3-Dichlorobenzene BRL ug1L 11 1.5 1 '625 916117 19;57 JMV P710065 1,4-Dichlorobenzene BRL ug1L 11 1.5 1 "625 916117 19:57 JMV P710065 2,4,6-Trichlorophenol BRL ug1L 11 2.1 1 'fi25 916117 19:57 JMV P710065 2,4-Dichlorophenol BRL ug1L 11 1.8 1 '625 916117 19:57 JMV P710065 2,4-Dimethylphenol BRL ug1L 11 2.3 1 '625 9/6117 19:57 JMV P710065 2,4-Dinitrophenol BRL ug1L 11 1.4 1 '625 916117 19:57 JMV P710065 2,4-Dinitrotoluene BRL uglL 11 3.3 1 "625 916117 19:57 JMV P710065 2,6-Dinitrotoluene BRL ug/L 11 3.3 1 '625 916117 19:57 JMV P710065 2-Chloronaphthalene BRL uglL 11 2.6 1 '625 916117 19:57 JMV P710065 2-Chlorophenol BRL ug1L 11 1.3 1 '625 916117 19:57 JMV P710065 2-Nitrophenol BRL ug1L 11 1.6 1 `625 916117 19:57 JMV P710065 3,3'-Dichlorobenzidine BRL ug1L 11 3.1 1 "625 916117 19:57 JMV P710065 4,6-Dinitro-2-methylphenol BRL ug1L 11 2.1 1 `625 916117 19:57 JMV P710065 4-Bromophenyl phenyl ether BRL ug1L 11 3.6 1 '625 916117 19:57 JMV P710065 4-Chloro-3-methylphenol BRL ug1L 11 2.5 1 '625 916117 19:57 JMV P710065 4-Chlorophenyl phenyl ether BRL uglL 11 2.5 1 '625 916117 19:57 JMV P710065 4-Nitrophenol BRL ug1L 56 1.9 1 '625 916117 19:57 JMV P710065 Acenaphthene BRL ug1L 11 2.6 1 'fi25 916117 19:57 JMV P710065 Acenaphthylene BRL ug1L 11 2.6 1 '625 916117 19:57 JMV P710065 Anthracene BRL ug1L 11 3.6 1 `625 916117 19:57 JMV P710065 Benzidine BRL ug1L 110 16 1 `625 916117 19:57 JMV P710065 Benzo(a)anthracene BRL ug1L 11 3.5 1 `625 916117 19:57 JMV P710065 Benzo(a)pyrerte BRL uglL 11 4.1 1 '625 916117 19:57 JMV P710065 Benzo(b)fluoranthene BRL ug1L 11 4.0 1 '625 916/17 19:57 JMV P710065 Benzo(g,hJ)perylene BRL ug1L 11 3.9 1 "625 916117 19:57 JMV P710065 Benzo(k)fluoranthene BRL uglL 11 4.3 1 '625 916117 19:57 JMV P710065 bis(2-Chloroethoxy)methane BRL ug1L 11 2.0 1 '625 916117 19:57 JMV P710065 Bis(2-Chloroethyl)e1her BRL ug1L 11 1.8 1 '625 916117 19:57 JMV P710065 Bis(2-chloroisopropyl)ether BRLCCv uglL 11 1.9 1 "625 916117 19:57 JMV P710065 Bis(2-Ethylhexyl)phthalate BRL ug1L 11 3.5 1 '625 916117 19:57 JMV P710065 Butyl benzyl phthalate BRL ug1L 11 2.9 1 '625 916117 19:57 JMV P710065 Chrysene BRL ugR. 11 3.8 1 `625 916117 19757 JMV P710065 Dibenzo(a,h)anthracene BRL ug/L 11 3.8 1 "625 916117 19:57 JMV P710065 Diethyl phthalate BRL ug1L 11 2.6 1 `625 916117 19:57 JMV P710065 Dimethyl phthalate BRL ug1L 11 1.7 1 `625 916117 19:57 JMV P710065 Di-n-butyl phthalate BRL ug11- 11 3.8 1 '625 916117 19:57 JMV P710065 Di-n-oclyl phthalate BRL uglL 11 4.0 f "625 916117 19:57 JMV P710065 Fluoranthene BRL ug1L 11 3.9 1 '625 916117 19:57 JMV P710065 Fluorene BRL ug1L 11 3.1 1 '625 916117 19:57 JMV P710065 Hexachlorobenzene BRL uglL 11 2.8 1 '625 916117 19:57 JMV P710065 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 8 of 24 Pf Full -Service Anal"cal & Laboratory Report bg I I Environmental Solutions 09/19/2017 -�eonaronies iHc GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-2 Attn: Dave Mazorra Prism Sample ID: 7090021-02 710 Peninsula Lane, #B Prism Work Order: 7090021 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 08/31/17 15:30 Time Submitted: 09/01/17 11:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date> ime ID Hexachlorobutadiene BRL ug/L 11 2.3 1 *625 916/17 19757 JMV P710065 Hexachlorocyclopentadiene BRL ug/L 11 1,8 1 *625 916117 19:57 JMV P710065 Hexachloroethane BRL ug/L 11 1.7 1 '625 9/6117 19:57 JMV P710065 lndeno(1,2,3-cd)pyrene BRL ug/L 11 3.4 1 *625 9/6117 19:57 JMV P710065 Isophorone BRL uglL 11 2.4 1 '625 916117 19:57 JMV P710065 Naphthalene BRL uglL 11 2.3 1 *625 9/6117 19:57 JMV P710065 Nitrobenzene BRL ug/L 11 1.6 1 '625 916117 19:57 JMV P710065 N-Nitrosodimethylamine BRL ug1L 11 0,93 1 *625 916117 19:57 JMV P710065 N-Nitroso-di-n-propylamine BRL ug/L 11 2.3 1 '625 916117 19:57 JMV P710065 N-Nitrosodiphenylamine BRL ug/L 11 3.3 1 '625 9/6117 19:57 JMV P710065 Pentachlorophenol BRL ug/L 11 2.4 1 '625 9/6117 19:57 JMV P710065 Phenanthrene BRL ug/L 11 3.6 1 '625 916117 19:57 JMV P710065 Phenol BRL ug1L 11 0.54 1 '625 916/17 19:57 JMV P710065 Pyrene BRL ug/L 11 3.9 1 *625 916117 19:57 JMV P710065 Surrogate Recovery Control Limits 2,4,6-Tdbromophenol 73 % 31-144 2-Fluorobiphenyl 66 % 49-118 2-Fluorophenol 49 % 22-84 Nitrobenzene-05 72 % 43-123 Phenol-d5 35 % 10-63 Terphenyl-d14 74 % 49-151 Total Metals Copper BRL mg/L 0.010 0.0010 1 *200.7 9/11117 19:08 JAB P710071 Lead BRL mg/L 0.0050 0.0010 1 *200.7 9/11117 19:08 JAB P710071 Zinc 0.44 mg/L 0,030 0.0013 1 '200.7 9111117 19:08 JAB P710071 Volatile Organic Compounds by GUMS 1, 1. 1 -Trichloroethane BRL ug/L 5.0 0.061 1 *624 912117 0:30 KDM P710031 1,1,2,2-Tetrachloroethane BRL ug/L 5.0 0.036 1 '624 912/17 0:30 KOM P710031 1.1,2-Trichloroethane BRL ug/L 5.0 0.066 1 '624 912/17 0:30 KDM P710031 1,1-Dichloroethane BRL ug1L 5.0 0.083 1 '624 912117 0:30 KDM P710031 1,1-Dichloroethylene BRL ug/L 5.0 0.083 1 '624 912117 a30 KDM P710031 1,2-Dichlorobenzene BRL ug1L 5.0 0.076 1 '624 912117 0:30 KDM P710031 1,2-Dichloroethane BRL ug/L 5.0 0.066 1 '624 912/17 0:30 KDM P710031 1,2-Dichloropropane BRL ug/L 5.0 0,11 1 '624 912/17 0:30 KDM P710031 1,3-Dichlorobenzene BRL uglL 5.0 0.054 1 *624 912117 0:30 KDM P710031 1,4-Dichlorobenzene BRL uglL 5.0 0.050 1 '624 912117 0:30 KDM P710031 2-Chloroethyl Vinyl Ether BRL uglL 10 0.37 1 '624 912117 0:30 KDM P710031 Acrolein BRL uglL 100 0.20 1 '624 912/17 0:30 KDM P710031 Acrylonitrile BRL ug/L 100 0.20 1 '624 912117 0:30 KDM P710031 Benzene BRL ug/L 5.0 0.048 1 '624 9/2117 0:30 KOM P710031 Bromodichloromethane BRL ug/L 5.0 0,062 1 *624 9/2117 0:30 KDM P710031 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 24050 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 9 of 24 . Laboratory Report ��P❑ �> �R I S M � ll-Service Analytical 8 Environmental Solutions 09/19/2017 iI LABOR�idilES IHG. GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-2 Attn: Dave Mazorra Prism Sample ID: 7090021-02 710 Peninsula Lane, #B Prism Work Order: 7090021 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 08/31/17 15:30 Time Submitted: 09101117 11:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Bromoform BRL ug1L 5.0 0.040 1 '624 912117 0:30 KDM P710031 Bromomethane BRL uglL 10 0.18 1 '624 912117 0:30 KDM P710031 Carbon Tetrachloride BRL uglL 5.0 0.11 1 '624 912117 0:30 KDM P710031 Chlorobenzene BRL ug1L 5.0 0.062 1 '624 912117 0:30 KDM P710031 Chloroethane BRL ug1L 10 0.22 1 '624 912117 0:30 KDM P710031 Chloroform BRL ug1L 5.0 0.076 1 "624 912I17 0:30 KDM P710031 Chloromethane BRL uglL 10 0.079 1 "624 912117 0:30 KDM P710031 cis-1,3-Dichloropro pylene BRL ug1L 5.0 0.079 1 '524 912117 0:30 KDM P710031 Dibromochloromethane BRL ug1L 5.0 0.081 1 '624 912117 0:30 KDM P710031 Ethy[benzene BRL uglL 5.0 0.061 1 `624 912117 0:30 KDM P710031 Methylene Chloride BRL ug1L 5.0 0.083 1 '624 912117 0:30 KDM P710031 Tetrachloroethylene BRL uglL 5.0 0.098 1 '624 912117 0:30 KDM P710031 Toluene BRL ug1L 5.0 0.044 1 '624 912117 0:30 KDM P710031 trans- 1,2-Dichloroethylene BRL uglL 5,0 0.094 1 `624 912117 0:30 KDM P710031 trans- 1,3-Dichloropropylene BRL ug1L 5.0 0.070 1 '624 912117 0:30 KDM P710031 Trichloroethylone BRL ug1L 5.0 0.078 1 `624 912117 0:30 KDM P710031 Trichlorofluoromethane BRL ug1L 10 0.062 1 "624 912117 0:30 KDM P710031 Vinyl chloride BRL ug1L 10 0.097 1 '524 912117 0:30 KDM P710031 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 74-126 Dibromofluorometharie 99 % 75 127 Toluene-d8 101 % 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/629-6364 - Toll Free Number: 1-8001529-9364 - Fax: 7041525-0409 Page 10 of 24 ��I -� /. Fun -Service al Solutions 8 ' V Environmental Solutions e-�sOnaTon��S iwc Level II QC Report 9119117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 volatile Organic Compounds by GC1MS - Quality Control Prism Work Order: 7090021 Time Submitted: 9/1/2017 11.00:00AM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710031 - 624 Blank (P710031-BLK1 ) Prepared & Analyzed: 09/01/17 1, 1, 1 -Trichloroethane BRL 5.0 ug/L 1,1,2,2-Tetrachloroethane BRL 5.0 ug/L 1,1,2-Trichloroethane BRL 5.0 ug1L 1,1-Dichloroethane BRL 5.0 uglL 1,1-Dichloroethylene BRL 5.0 ug/L 1,2-Dichlorobenzene BRL 5.0 ug/L 1,2-Dichioroethane BRL 5.0 ug1L 1,2-Dichioropropane BRL 5.0 ug/L 1,3-Dichiorobenzene BRL 5.0 ug/L 1,4-Dichlorobenzene BRL 5.0 ug/L 2-Chloroethyt Vinyl Ether BRL 10 ug/L Acrolein BRL 100 uglL Acrylonitrile BRL 100 ug/L Benzene BRL 5.0 ug/L Bromodichloromethane BRL 5.0 ug/L Bromoform BRL 5.0 ug/L Bromomethane BRL 10 ug/L Carbon Tetrachloride BRL 5.0 ug/L Chlorobenzene BRL 5.0 ug/L Chloroethane BRL 10 ug/L Chloroform BRL 5.0 ug/L Chloromethane BRL 10 ug/L cis-1,3-Dichloropropylene BRL 5.0 ug/L Dibromochloromethane BRL 5.0 ug/L Ethylbenzene BRL 5.0 ug/L Methylene Chloride BRL 5.0 ug/L Tetrachloroethylene BRL 5.0 ug/L Toluene BRL 5.0 ug/L trans-1,2-Dichloroethylene BRL 5.0 ug/L trans-1,3-❑ichloropropylene BRL 5.0 ug/L Trichloroethylene BRL &0 ug/L Trichlorofluoromethane BRL 10 ug/L Vinyl chloride BRL 10 ug/L TIC'Heptane 0.00 ug/L Surrogate.4-Sromofluorobenzene 50.8 ug/L 50.00 102 74-126 Surrogate: DibromoRuoromethane 50.1 ug/L 50.00 100 75-127 Surrogate. Toluene-l8 49.2 ug/L 50,00 98 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 11 of 24 n, ®P IR I S M Full -Service Analytical & , Environmental Solutions -�Z�7FASORIES ING Level II QC Report 9119117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Prism Work Order: 7090021 Attn: Dave Mazorra Time Submitted: 9/1/2017 11:00:OOAM 710 Peninsula Lane, #B Charlotte, NC 28273 Volatile Organic Compounds by GCIMS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710031 - 624 LCS (P710031-BSI) Prepared & Analyzed: 09/01/17 1,1,1-Trichioroethane 21.3 5.0 uglL 20.00 106 52-162 1,1,2,2-Tetrachloroethane 22.3 5.0 ugIL 20.00 112 46-157 1,1,2-Trichloroethane 21.8 5.0 ug/L 20.00 109 52-150 1,1-Dichloroethane 21.8 5.0 ug/L 20.00 109 59-155 1,1-Dichloroethylene 23.0 5.0 ug[L 20.00 115 10-234 1,2-Dichlorobenzene 22.2 5.0 ug/L 20.00 111 18-190 1.2-Dichloroethane 21.3 5.0 ug/L 20.00 107 49-155 1,2-Dichloropropane 21.9 5.0 ug/L 20.00 110 10-210 1,3-Dichlombenzene 22.4 5.0 ug1L 20.00 112 59-156 1,4-Dichlorobenzene 22.0 5.0 ug/L 20.00 110 18-190 2-Chloroethyl Vinyl Ether 19.5 10 ug/L 20.00 97 10-305 Acrolein 42.8 100 ug/L 40.00 107 10-196 Acryloniirile 43.0 100 ug[L 40.00 108 60-134 Benzene 22.5 5.0 ug/L 20.00 112 37-151 Bromodichloromethane 22.4 5.0 ug/L 20.00 112 35-155 Bromoform 20.3 5.0 ug/L 20.00 102 45-169 Bromomethane 23.5 10 ug/L 20.00 117 10-242 Carbon Tetrachloride 20.7 5.0 ug/L 20.00 103 70-140 Chlorobenzene 21.8 5.0 ug/L 20.00 109 37-160 Chloroethane 22.3 10 ug/L 20.00 112 14-230 Chloroform 21.8 5.0 ug/L 20.00 109 51-138 Chloromethane 20.3 10 ug/L 20.00 101 10-273 cis-1,3-Dichloropropylene 22.6 5.0 ug/L 20.00 114 10-227 Dibromochloromethane 20.7 5.0 ug/L 20.00 103 53-149 Ethylbenzene 22.9 5.0 ug/L 20.00 115 37-162 Methylene Chloride 20.0 5.0 ug/L 20.00 100 10-221 Tetrachloroethylene 22.9 5.0 ugtL 20.00 114 64-148 Toluene 22.5 5.0 ug/L 20.00 113 47-150 trans-1,2-Dichloroethylene 22.4 5.0 ug/L 20.00 112 54-156 trans-1,3-Dichloropropylene 23,1 5.0 ug[L 20.00 116 17-183 Trichloroethylene 22.9 5.0 ug/L 20.00 114 71-157 Trichlorofluoromethane 22.0 10 ug/L 20,00 110 17-181 Vinyl chloride 21.9 10 ug/L 20.00 110 10-251 Surrogate:4-Bromofluoroberizene 48.8 ug/L 50.00 98 74-126 Surrogate: Dibromofluoromethane 49.1 uyk 50.00 98 75-127 Surrogate: Toluene d8 49.6 uglL 50.00 99 74-122 This report should not be reproduced, except in its entirety, urithoul the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 12 of 24 AIMR I n n EnviFull-ronmental al Solution s ' V' Environmental Solutions LAHaiWTDAIES 1 G Level II QC Report 9119117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Volatile Organic Compounds by GClMS - Quality Control Analyze Batch P710031 - 624 Reporting Result Limit Units Prism Work Order: 7090021 Time Submitted: 9/1/2017 11:0O:OOAM Spike Source Level Result %REC %REC RPD Limits RPD Limit Notes LCS Dup IP710031-BSD1) Prepared & Analyzed: 09/01/17 1, 1. 1 -Trichloroethane 21.4 5.0 ug/L 20.00 107 52-162 0A 20 1,1,2,2-Tetrachloroethane 21A 5.0 ug/L 20.00 107 46-157 4 20 1,1,2-Trichloroethane 21.5 5.0 ug/L 20.00 107 52-150 2 20 1,1-Dichloroethane 22.2 5.0 ugfL 20.00 ill 59-155 2 20 1,1-Dichloroethylene 23.0 5.0 ugfL 20.00 115 10-234 0.2 20 1,2-Dichlorobenzene 21.5 5,0 ug/L 20,00 107 18-190 3 20 1,2-Dichloroethane 21.3 5.0 ug/L 20.00 107 49-155 0.05 20 1,2-Dichloropropane 21.1 5.0 ugfL 20.00 109 10-240 1 20 1,3-Dichlorobenzene 21.6 5.0 ug/L 20.00 108 59-156 4 20 1,4-Dichlorobenzene 21.4 5.0 ug/L 20.00 107 18-190 3 20 2-Chloroethyl Vinyl Ether 20.4 10 ug/L 20.00 102 10-305 5 20 Acrolein 41.3 100 uglL 40.00 103 10-196 4 20 Acrylonitrile 40.9 100 ug/L 40.00 102 60-134 5 20 Benzene 22.5 5.0 uglL 20.00 112 37-151 0.04 20 Bromodichloromethane 22.2 5.0 uWL 20.00 111 35-155 0.8 20 Bromoform 19.2 5.15 ug1L 20.00 96 45-169 6 20 Bromomethane 24.8 10 ug1L 20.00 124 10-242 6 20 Carbon Tetrachloride 20.7 5.0 ug/L 20.00 104 70-140 0.2 20 Chlorobenzene 21.7 5.0 ug/L 20.00 109 37-160 0.6 20 Chloroethane 22.6 10 ug/L 20.00 113 14-230 1 20 Chloroform 22.2 5.0 ug/L 20.00 ill 51-138 2 20 Chloromethane 22.1 10 ugfL 20.00 110 10-273 8 20 cis-1,3-Dichloropropylene 22.7 5.0 ugfL 20.00 114 10-227 0.2 20 Dibromochloromethane 20.0 5.0 ug/L 20.00 100 53-149 3 20 Ethylbenzene 22.7 5.0 ug/L 20.00 113 37-162 1 20 Methylene Chloride 20.1 5.0 uglL 20.00 100 10-221 0.2 20 Tetrachloroethylene 22.4 5.0 ug/L 20.00 112 64-148 2 20 Toluene 22.6 5.0 ug/L 20.00 113 47-150 0.3 20 trans-1,2-Dichloroethylene 22.4 5.0 ug/L 20.00 112 54-156 0.04 20 trans-1,3-Dichloropropylene 22.8 5.0 uglL 20.00 114 17-163 1 20 Trichloroethylene 23.2 5.0 ug/L 20.00 116 71-157 1 20 Trichlorofluoromethane 22.2 10 ugfL 20.00 ill 17-181 0,9 20 Vinyl chloride 22.0 10 ug/L 20.00 110 10-251 0.4 20 Surrogate:4-Bromofluombenzene 49.7 ug/L 50.00 99 74-126 Surrogate: Dibromofluoromethene 50.8 ug/L 50.00 102 75-127 Surrogate: Toluene -dB 50.1 ug/L 50.00 100 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364- Toll Free Number: 1-800/629-6364 - Fax: 7041525-0409 Page 13 of 24 , Full-S® �0 n n Environmental Analytical s ' V' En viranmenfaf Solutions ,�iJ1BO11LmaE& Level II QC Report 9/19/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GCIMS - Quality Control Analyte Batch P710065 - 625 Reporting Result Limit Units Prism Work Order: 7090021 Time Submitted: 9/1/2017 11:00:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P710065-BLKt) Prepared & Analyzed: 09/06/17 1,2,4-Tdchlorobenzene BRL 10 uglL 1,2-Dichlorobenzene BRL 10 ug1L 1,2-Diphenylhydrazine (as Azobenzene) BRL 10 ug1L 1,3-D'ichlorobenzene BRL 10 uglL 1,4-Dichlorobenzene BRL 10 ug1L 2,4,6-Trichlorophenol BRL 10 uglL 2,4-Dichlorophencl BRL 10 ug1L 2,4-Dimethylphenol BRL 10 ug1L 2,4-Dinitrophenol BRL 10 ug1L 2,4-Dinitrotoluene BRL 10 ug1L 2,6-Dinitrotoluene BRL 10 uglL 2-Chloronaphthalene BRL 10 uglL 2-Chlorophenol BRL 10 ug1L 2-Nitrophenol BRL 10 ug1L 3,3'-DichlorobenzAine BRL 10 ug1L 4,6-Dinit n-2-methylphenol BRL 10 ug1L 4-Bromophenyl phenyl ether BRL 10 uglL 4-Chloro-3-methylphenol BRL 10 ug1L 4-Chlorophenyl phenyl ether BRL 10 uglL 4-Nitrophenol BRL 50 ug1L Acenaphthene BRL 10 ug1L Acenaphthylene BRL 10 uglL Anthracene BRL 10 uglL Benzidine BRL 100 ug1L Benzo(a)anthracene BRL 10 uglL Benzo(a)pyrene BRL 10 ug1L Benzo(b)fluoranthene BRL 10 ug/L Benzo(g,h,i)perytene BRL 10 ug1L Benzo(k)fluoranthene BRL 10 ug1L bis(2-Chloroethoxy)methane BRL 10 ug1L Bis(2-Chloroethyl)ether BRL 10 uglL Bis(2--hloroisopropyl)ether BRL 10 ug1L Bis(2-Ethylhexyl)phthalate BRL 10 ug1L Butyl benzyi phthalate BRL 10 ug1L Chrysene BRL 10 ug1L Dibenzo(a,h)anthracene BRL 10 ug1L D'ieihyl phthalate BRL 10 ug1L Dimethyl phthalate BRL t0 ug1L Di-n-butyl phthalate BRL 10 uglL Di-n-octyl phthalate BRL 10 uglL Fluoranthene BRL 10 ug1L Fluorene BRL 10 ug1L Hexachlorobenzene BRL 10 ug1L Hexachlorobutadiene BRL 10 ug1L Hexachlorocyclopentadiene BRL 10 uglL Hexachloroethane BRL 10 uglL This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Tolf Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 14 & 24 WMADI A n Fun -Service Analytical I`\Y/' Environmental SolutionsonsneannnxnsS we Level II QC Report 9119/17 GTA (Geo-Tech. Assoc. inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GC1MS - Quality Control Prism Work Order: 7090021 Time Submitted: 9/1/2017 11:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result % REC Limits RPD Limit Notes Batch P710065 - 625 Blank (P710065-81-KI) Prepared & Analyzed: 09/06/17 Indeno(1,2,3-cd)pyrene BRL 10 ug1L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug1L Nitrobenzene BRL 10 ug/L N-Nitrosodimethylamine BRL 10 ug1L N-Nitroso-di-n-propylamine BRL 10 uglL N-Nitrosodiphenylamine BRL 10 ug1L Pentachlorophenol BRL 10 ug1L Phenanthrene BRL 10 uglL Phenol BRL 10 ug/L Pyrene BRL 10 ug1L Surrogate:2,4,6-Tribromophenal 67.4 ug/L 100.0 67 31-144 Surrogate:2-Ftuorobiphenyl 34.2 ug/L 50.00 68 49-118 Surrogate:2-Fluorophenol 59.8 ug/L 100.0 60 22-84 Surrogate: Nitrobenzene-d5 37.3 ug/L 50.00 75 43-123 Surrogate: Phenot-d5 40.0 ug/L 100.0 40 10-63 Surrogate: Tetphenyl-d 14 41.0 u91L 50.00 82 49-151 LCS (P710065-BSI) Prepared & Analyzed: 09/06/17 1,2,4-Tiichlorobenzene 54.4 10 ug1L 100.0 54 44-142 1,2-Dichlorobenzene 64.9 10 ug1L 100.0 65 32-129 1,2-Diphenylhydrazine (as Azobenzene) 79.8 10 ug/L 100.0 80 40-135 1,3-Dichlorobenzene 64.4 10 ug/L 100.0 64 20-124 1,4-Dichlorobenzene 63.8 10 ug/L 100.0 64 20-124 2,4,6-Trichlorophenol 80.0 10 ug/L 100.0 80 37-144 2,4-Dichlorophenol 60.5 10 ug1L 100,0 60 39-135 2,4-Dimethylphenol 68.7 10 ug1L 100.0 69 32-119 2,4-Dinitrophenol 62.4 10 ug1L 100.0 62 10-191 2,4-Dinitrotoluene 74.4 10 ug1L 100.0 74 39-139 2,6-Dinitrotoluene 76.0 10 ug1L 100.0 76 50-158 2-Chloronaphthalene 71.2 10 ug/L 100.0 71 60-116 2-Chlorophenol 75.6 10 ug1L 100.0 76 23-134 2-Nitrophenol 61.2 10 ug/L 100.0 61 29-182 3,T-Dichlorobenzidine 71.0 10 ug/L 100.0 71 10-262 4,6-Dinitro-2-methylphenol 79.9 10 ug1L 100.0 80 10-181 4-Bromophenyl phenyl ether 70A 10 ug1L 100.0 70 53-127 4-Chloro-3-methylphenol 66.1 10 ug/L 100.0 66 22-147 4-Chlorophenyl phenyl ether 70.4 10 ug/L 100.0 70 25-158 4-Nitrophenol 47.6 50 ug/L 100.0 48 10-132 Acenaphthene 72.4 10 ugiL 100.0 72 47-145 Acenaphthylene 72.2 10 ug/L 100.0 72 33-145 Anthracene 76.8 10 ug1L 100.0 77 27-133 Benzidine 63.1 100 ug/L 100.0 63 15-150 Benzo(a)anthracene 65.0 10 ug1L 100.0 65 33-143 Benzo(a)pyrene 70.6 10 ug1L 100.0 71 17-163 Benzo(b)1luoranthene 67.5 10 ug1L 100.0 68 24-159 Senzo(g,h,i)perylene 72.6 10 ug1L 100.0 73 10-219 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 15 of 24 � w I�r I S „ %� Full -Service Analytical r� ' V' Environmental Solutions �'ttaonwrauEs naC Level II QC Report 9119117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NIC 28273 Semivolatile Organic Compounds by GCIMS - Quality Control Analyte Batch P710065 - 625 Reporting Result Limit Units Prism Work Order: 7090021 Time Submitted: 9/1/2017 11:00:00AM Spike Source Level Result %REC %REC RPD Limits RPD Limit Notes LCS (P710065-BSI) Prepared & Analyzed: 09/06/17 Benzo(k)fluoranthene 70.8 10 ug1L 100.0 71 11-162 bis(2-Chloroethoxy)methane 57.9 10 ug1L 100.0 58 33-184 Bis(2-Chloroethyl)ether 52.6 10 ug1L 100.0 53 12-158 Bis(2-chloroisopropyl)ether 79.3 10 ug1L 100.0 79 36-166 Bis(2-Ethylhexyl)phthalate 69,1 10 ug1L 100.0 69 10-158 Butyl benzyl phthalate 59.8 10 uglL 100.0 60 10-152 Chrysene 61.8 10 ug1L 100.0 62 17-168 Dibenzo(a,h)anthracene 38.9 10 ug1L 100.0 39 10-227 Diethyl phthalate 59.2 10 ug1L 100.0 59 10-114 Dimethyl phthalate 32.8 10 ug1L 100.0 33 10-112 Di-n-butyl phthalate 69.6 10 ug1L 100.0 70 10-118 Di-n-octyl phthalate 72.6 10 ug1L 100.0 73 10-146 Fluoranthene 72.5 10 uglL 100.0 72 26-137 Fluorene 72.3 10 ugfL 100.0 72 59-121 Hexachlorobenzene 75.1 10 uglL 100.0 75 10-152 Hexachlorobutadiene 56.0 10 ug/L 100.0 56 24-116 Hexachlorocyclopentadiene 74,9 10 ug1L 100.0 75 32-117 Hexachloroethane 64.8 10 ug1L 100.0 65 40-113 Indeno(1,2,3-cd)pyrene 77.6 10 ug1L 100.0 78 10-171 Isophorone 65.7 10 ug/L 100.0 66 21-196 Naphthalene 55.2 10 uglL 100.0 55 21-133 Nitrobenzene 54.2 10 ug1L 100.0 54 35-180 N-Nitrosodimethylamine 40.6 10 uglL 100.0 41 10-119 N-Nitroso-di-n-propylamine 73.6 10 ug1L 100.0 74 10-230 N-Nitrosodiphenylamine 92.9 10 uglL 100.0 93 69-152 Pentachlorophenol 86.4 10 ug1L 100.0 86 14-176 Phenanthrene 74.5 10 uglL 100.0 74 54-120 Phenol 42.3 10 uglL 100.0 42 10-112 Pyrene 61.6 10 ug1L 100.0 62 52-115 Surrogate: 2,4,6-Tribromophenol 82.5 ug/L 100.0 83 31-144 Surrogate:2-Fluorobiphenyl 35.9 ug/L 50.00 72 49-118 Surrogate:2-Fluorophenol 55.3 ug/L 100.0 55 22-84 Surrogate: Nitrobenzene-d5 29.9 ug/L 50.00 60 43-123 Surrogate: Phenol-d5 37.4 ug/L 100.0 37 10-63 Surrogate: Terphenyl-414 37.0 ug2 50.00 74 49-151 This report should not be reproduced, except in its entirety, without the wntten consent of Prism Laboratories, Inc. 449 Sptingbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 70415254409 Page 16 of 24 4 AiuI S n %� Full -Service Analyticak & � 'v' Environmental Soiutlons 7iwaonnranes irec Level II QC Report 9/19117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 7090021 Time Submitted: 9/1/2017 11:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710065 - 625 LCS Dup (P710065-BSD1) Prepared & Analyzed: 09/06/17 1,2,4-Tdchlorobenzene 55.9 10 uglL 100.0 56 44-142 3 20 1,2-Dichlorobenzene 67.0 10 uglL 100.0 67 32-129 3 20 1,2-Diphenylhydrazine (as Azobenzene) 82.1 10 uglL 100,0 82 40-135 3 20 1,3-Dichlorobenzene 67.1 10 uglL 100.0 67 20-124 4 20 1,4-Dichlorobenzene 65.7 10 uglL 100.0 66 20-124 3 20 2,4,6-Tdchiorophenol 76.3 10 uglL 100.0 76 37-144 5 20 2,4-Dichlorophenol 56.6 10 ug/L 100.0 57 39-135 7 20 2,4-Dimethylphenol 63.4 10 uglL 100.0 63 32-119 8 20 2,4-Dinitrophenol 62.9 10 ug/L 100.0 63 10-191 0.8 20 2,4-Dinitrotoluene 76.7 10 ug/L 100.0 77 39-139 3 20 2,6-Dinitrotoluene 80,0 10 ug/L 100.0 80 50-158 5 20 2-Chloronaphthalene 72.3 10 ug/L 100.0 72 60-118 2 20 2-Chlorophenol 69.2 10 ug/L 100.0 69 23-134 9 20 2-Nitrophenol 57.6 10 uglL 100,0 58 29-182 6 20 3,3'-Dichlorobenzidine 72.6 10 uglL 100.0 73 10-262 2 20 4,6-Dinitro-2-methylphenol 75.6 10 uglL 100.0 76 10-181 6 20 4-Bromophenyt phenyl ether 72,4 10 uglL 100.0 72 53-127 3 20 4-Chlonr3-methytphenol 60.8 10 ug/L 100.0 61 22-147 8 20 4-Chlorophenyl phenyl ether 73.5 10 ug/L 100.0 73 25-158 4 20 4-Nitrophenol 44.8 5o UA 100.0 45 10-132 6 20 Acenaphthene 75.1 10 ug/L 100.0 75 47-145 4 20 Acenaphthylene 74.5 10 uglL 100.0 74 33-145 3 20 Anthracene 78.2 10 uglL 100.0 78 27-133 2 20 Benzidine 63.2 100 ug/L 100.0 63 15-150 0.1 20 Benzo(a)anthracene 66.2 10 ug1L 100.0 66 33-143 2 20 Benzo(a)pyrene 71.0 10 ug1L 100.0 71 17-163 0.5 20 Benzo(b)fluoranthene 67.5 10 uglL 100.0 67 24-159 0.1 20 Benzo(g,h,i)perylene 74.1 10 uglL 100.0 74 10-219 2 20 Benzo(k)tluoranthene 70.8 10 uglL 100.0 71 11-162 0.1 20 bis(2-Chloroethoxy)methane 59.8 10 uglL 100.0 60 33-184 3 20 Bis(2-Chloroethyl)ether 55.5 10 ug& 100.0 55 12-158 5 20 Bis(2-chloroisopropyl)ether 79.0 10 uglL 100.0 79 36-166 0.3 20 Bis(2-Ethylhexyl)phthalate 69.8 10 ug1L 100.0 70 10-156 1 20 Butyl benzyl phthalate 55.8 10 uglL 100.0 56 10-152 7 20 Chrysene 62.8 10 uglL 100.0 63 17-168 2 20 Dibenzo(a,h)anthracene 40.6 10 ug1L 100.0 41 10-227 4 20 Diethyl phthalate 57.8 10 ug1L 100.0 58 10-114 2 20 Dimethyl phthalate 31.3 10 ug/L 100,0 31 10-112 5 20 Di-n-butyl phthalate 68.8 10 ug/L 100.0 69 10-118 1 20 Di-n-oetyl phthalate 72.6 10 ug/L 100.0 73 10-146 0.04 20 Fluoranthene 74.1 10 ug1L 100.0 74 26-137 2 20 Fluorene 74.6 10 ug1L 100.0 75 59-121 3 20 Hexachlorobenzene 77.1 10 UA 100.0 77 10-152 3 20 Hexachlorobutadiene 57.9 10 ug/L 100.0 58 24-116 3 20 Hexachlorocyclopentadiene 77.1 10 uglL 100.0 77 32-117 3 20 Hexachloroethane 66.1 10 ug/L 100.0 66 40-113 2 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-0364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 17 of 24 ;e � �� - I n n Full -Service Analytical & ' V' Environmental Solutions �L�9q+I1TOfl1ES ING Level li QC Report 9119/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GC1MS - Quality Control Prism Work Order: 7090021 Time Submitted: 9/1/2017 11:00:00AM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710065 - 625 LCS Dup {P710065-BSD1} Prepared & Analyzed: 09/06/17 Indeno(1,2,3-cd)pyrene 80.1 10 ug1L 100.0 80 10-171 3 20 Isophorone 67.2 10 ug1L 100.0 67 21-196 2 20 Naphthalene 56.7 10 ug1L 100.0 57 21-133 3 20 Ndrobenzene 56.6 10 ug1L 100.0 57 35-180 4 20 N-Nitrosodimethylamine 40.8 10 ug/L 100.0 41 10-419 0.5 20 N-Nitroso-di-n-propylamine 73.7 10 ug1L 100.0 74 10-230 0.05 20 N-Nitrosodiphenylamine 95.6 10 ug/L 100.0 96 69-152 3 20 Pentachlorophenol 80.7 10 ugtL 100.0 81 14-176 7 20 Phenanthrene 76.2 10 uglL 100.0 76 54-120 2 20 Phenol 41.4 10 ug1L 100.0 41 10-112 2 20 Pyrene 63.5 10 ug1L 100.0 63 52-115 3 20 Surrogate- 2,4,6-Tnbromophenot 76.9 ug/L 100.0 77 31-144 Surrogate:2-Fluorobiphenyl 37.8 ug/L 50.00 76 49-118 Surrogate:2-Fluorophenol 50.8 ug/L 100.0 51 22-84 Surrogate: Nitrobenzene-d5 31,6 ug/L 50.00 63 43-123 Surrogate: Phenol-d5 33.9 u91L 100.0 34 10-63 Surrogate: Terphenyl-d14 38.3 ug/L 50.00 77 49-151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Tolt Free Number: 1-800/529-6364 - Fax: 704/625-0409 Page 18 of 24 v. Level II QC Report ®�d1.11< n /� Full -Service Analytical 8 9119117 r�1_ � V' Environmental Solutions ��ueaenTonres iwc GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Prism Work Order: 7090021 Attn: Dave Mazorra Time Submitted: 9/1/2017 11:00:OOAM 710 Peninsula Lane, #B Charlotte, NC 28273 Organochlorine Pesticides by GCIECD - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710086 - 608 Blank (P710086-BLK7) Prepared: 09/07/17 Analyzed: 09/08/17 alpha-BHC BRL 0.050 ug1L beta-BHC BRL 0.050 ug1L gamma-BHC BRL 0.050 ug1L delta-BHC BRL 0.050 ug1L Heptachior BRL 0.050 u91L Alddn BRL 0.050 ug1L Heptachlor Epoxide BRL 0.050 ug1L trans -Chlordane BRL 0,050 uglL Endosulfan I BRL 0.050 uglL cis -Chlordane BRL 0.050 ug1L Dieldrin BRL 0.050 uglL 4.4'-ODE BRL 0.050 uglL Endrin BRL 0.050 ug1L Endosulfan 11 BRL 0.050 uglL 4,4'-DDD BRL 0.050 UA Endrin Aldehyde BRL 0.050 uglL Endosultan Sulfate BRL 0.050 ug1L 4,4'-DDT BRL 0.050 uglL Endrin Ketone BRL 0.050 ug1L Methoxychlor BRL 0.050 ug1L Chlordane BRL 0.50 ug1L Toxaphene BRL 0.50 ug1L Aroclor 1016 BRL 0.50 ug1L Arocior 1221 BRL 1.0 ug1L Aroclor 1232 BRL 0.50 ug1L Arodor 1242 BRL 0.50 uglL Arodor 1248 BRL 0.50 uglL Aroclor 1254 BRL 0.50 uglL Arodor 1260 BRL 0.50 uglL Surrogate: Tetrachloro-m-xylene 0.686 uglL 1.000 69 40-134 Surrogate: Decachloroblphenyl 1,01 uglL 1.000 101 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - To[] Free Number: 1-8001529-6364 - Fax. 70415254409 Page 19 of 24 All; Full-Service Analytical & tR I S M Enviranmental Solutions Level II QC Report 9/19117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Organochlorine Pesticides by GCIECD - Quality Control Analyte Batch P710086 - 608 Reporting Result Limit Units Prism Work Order: 7090021 Time Submitted: 9/1/2017 11:00:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P710086-BSI) Prepared: 09/07/17 Analyzed: 09/08/17 alpha-BHC 0.812 0.050 ug/L 1.000 81 37-134 beta-BHC 0.809 0.050 ug1L 1.000 81 17-147 gamma-BHC 0.816 0.050 ug/L 1.000 82 32-127 delta-8HC 0.702 0.050 ug1L 1.000 70 19-140 Heptachlor 0.749 0.050 ug1L 1.000 75 34-111 Alden 0.715 0.050 ug/L 1.000 72 42-122 Heptachlor Epoxide 0,821 0.050 ug1L 1.000 82 37-142 trans -Chlordane 0.803 0.050 ug1L 1.000 80 45-119 Endosulfan 1 0.837 0.050 ug1L 1.000 84 45-153 cis -Chlordane 0.815 0.050 ugiL 1.000 82 45-119 Dieldrin 0.836 0.050 ug1L 1.000 84 36-146 4,4'-DDE 0.793 0.050 ug1L 1.000 79 30-145 Endrin 0.817 0.050 UA 1.000 82 30-147 Endosulfan II 0.870 0,050 uglL 1.000 87 10-202 4,4'-D❑D 0.831 0.050 ug1L 1.000 83 31-141 Lndrin Aldehyde 0.842 0.050 ug1L 1,000 84 51-132 Endosulfan Sulfate 0.830 0.050 ug/L 1.000 83 26-144 4,4'-DDT 0.835 0.050 ug/L 1.000 84 25-160 Endrin Ketone 0:911 0.050 ug1L 1.000 91 58-134 Methoxychlor 0.861 0.050 ug/L 1.000 86 54-145 Surrogate: Tetrachloro-m-xylene 0.568 ug/L 1.000 57 40-134 Surrogate: Decachiorobiphenyl 0.677 ug/L 1.000 68 13-186 LCS (P710086-BS2) Prepared: 09/07/17 Analyzed: 09/08/17 Chlordane 8.62 0.50 ug/L 10.00 86 50-150 Surrogate: Tetrachloro-m-xylene 0.563 ug/L 1.000 56 40-134 Surrogate: Decachlorobiphenyl 1.18 ug/L 1.000 118 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7DV529-6364 - To0 Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 20 of 24 4 IPk R ISM LABOeATfI�ES u1c, Fall -Service Analytical & Environmental Solutions Level II QC Report 9119/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Organochlorine Pesticides by GCIECD - Quality Control Prism Work Order: 7090021 Time Submitted: 9/1/2017 11:00:00AM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710086 - 608 LCS (P710086-BS3) Prepared: 09/07/17 Analyzed: 09/08/17 Toxaphene 9.09 0.50 ug/L 10.00 91 41-126 Surrogate: Tetrachloro-m-xylene 0.588 ug/L 1.000 59 40-134 Surrogate: Decachlorobiphenyl 0,954 ug/L 1.000 95 13-186 LCS (P710086-43S4) Prepared: 09/07/17 Analyzed: 09/08/17 Chlordane BRL 0.50 uglL 50-150 Toxaphene BRL 0.50 ug1L 41-126 Aroclor 1016 7.95 0.50 ug/L 10.00 80 50-114 Aroclor 1260 9.80 0.50 ug/L 10.00 98 10-127 Surrogate: Tetrachloro-m-xylene 0.813 ug/L 1.000 81 40-134 Surrogate: Decachlorobiphenyl 0.907 ug/L 1.000 91 13-186 LCS Dup (P710086-BSD1) Prepared: 09/07/17 Analyzed: 09/08/17 alpha-BHC 0.798 0.050 ug1L 1.000 80 37-134 2 20 beta-BHC 0.791 0.050 ug/L 1.000 79 17-147 2 20 gamma-BHC 0,804 0.050 uglL 1.000 80 32-127 1 20 delta-BHC 0.687 0.050 ug/L 1.000 69 19-140 2 20 Heptachlor 0.756 0,050 ugtL 1.000 76 34-111 0.9 20 Aldrin 0.713 0.050 uglL 1.000 71 42-122 0.3 20 Heptachlor Epoxide 0.808 0.050 uglL 1.000 81 37-142 2 20 trans -Chlordane 0.811 0.050 ug/L 1.000 81 45-119 1 20 Endosulfan 1 0.822 0A50 uglL 1.000 82 45-153 2 20 cis -Chlordane 0.807 0.050 ug/L 1.000 81 45-119 1 20 Dieldrin 0.833 0,050 uglL 1.000 83 36-146 0.4 20 4,4'-DDE 0.834 0.050 ug/L 1.000 83 30-145 5 20 Endrin 0.846 0,050 ug/L 1.000 85 30-147 4 20 Endosulfan II 0.861 0.050 ug/L 1.000 86 10-202 1 20 4,4'-DDD 0.842 0.050 ug/L 1.000 84 31-141 1 20 Endrin Aldehyde 0.789 0.050 ug/L 1.000 79 51-132 7 20 Endosulfan Sulfate 0.838 0,050 ug/L 1.000 84 26-144 1 20 4,4'-DDT 0.883 0.050 ug/L 1.000 88 25-160 6 20 Endrin Ketone 0.930 0.050 ug1L 1.000 93 58-134 2 20 Methoxychlor 0.904 0.050 uglL 1A00 90 54-145 5 20 Surrogate: Tetrachloro-m-xylene 0.589 ug/L 1.000 59 40-134 Surrogate: Decachlorobiphenyl 0.497 ug/L 1,000 50 13-188 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 21 0f 27471 0��'R I S M Environmental Full-ServiceeAnalytical s Environmental Solutions -©weow�n s1i Level II QC Report 9119/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Total Metals - Quality Control Prism Work Order: 7090021 Time Submitted: 9/1/2017 11:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710071 - 200.7 Blank (P710071-BLK1) Prepared: 09/07/17 Analyzed: 09/11/17 Copper BRL 0.010 mg1L Lead BRL 0.0050 mg1L Zinc BRL 0.030 mglL LCS (P710071-BS1) Prepared: 09/07/17 Analyzed: 09/11/17 Copper 0.244 mglL 0.2500 97 65-115 Lead 0.252 mg1L 0.2500 101 85-115 Zinc 0.263 mg/L 0.2500 105 85-115 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240W - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 22 of 24 :�.1 ®P' RISM L4eaRFTORIE& IM Fult-Service Analytical & Environmental Solutions Level II QC Report 9119/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 General Chemistry Parameters - Quality Control Analyte Project: Monthly SW Reporting Result Limit Units Prism Work Order: 7090021 Time Submitted: 9/1/2017 11:00:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P710010 - NO PREP LCS (P710010-BSI) Prepared & Analyzed: 09/01/17 pH 6.88 pH Units 6.880 100 98.5-101.5 Batch P710094 - NO PREP Blank (P710094-131-1(1) Prepared & Analyzed: 09/07/17 Total Suspended Solids BRL 5.0 mglL LCS (P710094-BSI) Prepared & Analyzed: 09/07/17 Total Suspended Solids 480 5.0 mglL 477.0 101 90-110 Batch P710212 - NO PREP Blank (P710212-BLKI) Prepared & Analyzed: 09/14117 Oil & Grease (SGT-HEM) BRL 5.0 mg1L OG Prep Method: 608 Lab Number Batch Initial Sample Extraction Data Final Datefrime 7090021-01 P710086 980 mL 10 mL 09/07/17 9:15 7090021-01 P710086 980 mL 10 mL 09/07/17 9A5 7090021-02 P710086 920 mL 10 mL 09/07/17 9:15 7090021-02 P710086 920 mL 10 mL 09/07/17 9-15 Prep Method: 625 Lab Number Batch Initial Final Datefrime 7090021-01 P710065 960 mL 1 mL 09/06/17 13:16 7090021-02 P710065 890 mL 1 mL 09/06/17 13:16 Prep Method: 200.7 Lab Number Batch Initlal Final DatelTime 7090021-01 P710071 50 mL 50 mL 09/07/17 8:05 7090021-02 P710071 50 mL 50 mL 09/07/17 8:05 Prep Method: 624 Lab Number Batch Initial Final Datefrime 7090021-01 P710031 10 mL 10 mL 09/01117 9:22 7090021-02 P710031 10 mL 10 mL 09/01/17 9:22 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543 Phone_ 70WS29-6364 -Toll Free Number: 1-800f529-6364 - Fax: 704/525-0404 Page 23 of 24 F,—,, ����fFull-Service Analytical & Environmental Solutions �.S' IAVORAWRIES INC 4149 5pringbrook Road • O'Imrlotte, NC 28217 Phone 7041529-6364 Fax: 7041525-0409 Client Company Name: Report To/Contact Name: r7ulr.(� _ Reporting Address: t W- -- CHAIN OF CUSTODY RECORD PAGE LQF�— QUOTE # TO ENSURE PROPER BILLING: . , Project Name: 14yi USTEN/ V 10 PX� � \-I 5 J Short Hold Analysis: Yes)(:!1W UST Pr ct: (Yes) - "Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) provisions !or QC rRequirements Invoice To: 57 s Qh An r Q r a_._ 4,c ogn- Address: Phone: Fax (Yes) (No): Purchase Order No.lBiNing Reference 3-�d 7 � 1 Email Address: Jojaz&rm corARequested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days Q 4 Days ❑ 5 Days EDD Type: PDF ExC I he "Working Days" ❑ 6-9 Days tandard 10 days 0 RushMust Be Pre-Approved WorkkSC Site Location Name. 4) CZ;F1 S Samples received after 14:00 will be processed next business day. Site Location Physical Address:. Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TO BE FILLED IN B CIE TISAMPLING PERSONNEL Certification: NELAC DOD FL NC OTHER N/A Water Chlorinated. YES— NO -A am y)on Collection: YESA NO CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER PRESERVA• TIVES� O �e REQUESTED A-vpw f ip REMARKS �0 PRISM LAB ID NO. 'TYPE SEE BELOW NO. SIZE ` W " 1 i } 1s-00 x �j X kr K X-X- x v, _ f✓L C Sampler's Signature Sampled By (Print Name) i Affiliation ,.WN FIRMLY - 3 .. IES Upon relinquishing, this Chain of Custod a your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted In writing to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized. T5M.,-USE ONLY Relinquish y(Signature) ecervad By: ( gnatura ate i ilaryours Additional Comments: Site Arrivat:Tirne; Relinquished By: (Signature) Received By: (Sig ture) Date Site DepartUta Time: Relinquish By: (Signature) Received or Pri m La . ratades By: to . Field Tech'Fee: v ..Mileage: Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTJVDY SEALS FOR TRAVSPORTATfOU TO THE LABORATORY. 10C Group No. y_ SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTI RECEIVED AT THE LAhORATORY. Q Fed Ex ❑ UPS ❑ Hand -delivered O Prism Field Service ❑ Othe, 1 [ VCR NPDES: I UST GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: je NC O 5CI O❑ NC ❑ SC NC © SC d NC r- SC ❑❑ NC U SC J NC O SC o NC C] 5C O NC ❑ SC L3 NC ❑ SC ' ❑❑ 171 01—f;n. TI = Tnflnn-I inert r-an VISA = Vnlatilp Orrugnlr:. Analvsls (Zero Head SDBCei f)t=ttC;lhl b d y` f IPRISM -®U46 ORATOR JES INC. Full -Service Analytical & Environmental Solutions GTA (Geo-Tech. Assoc. Inc.) Charlotte Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Offsite - Monthly SW Lab Submittal Date: 09/01 /2017 Prism Work Order: 7090022 Case Narrative 09/19/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Data Qualifiers Key Reference: Reviewed By Cara C. Rusmisell Project Manager CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. HT Sample received and analyzed outside of the hold time. OG HEM O&G is less than the reporting limit, therefore TPH (SGT-HEM) is less than the reporting limit. Sample not extracted for TPH (SGT-HEM). BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit- All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc, 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 70V525-UG9 Page 1 of 20 Fufl-Service Analytical & 126"R I S r v, � Environmental Solutions �'umn„�s iHc Sample Receipt Summary 09/19/2017 Prism Work Order: 7090022 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received Offsite-2 7090022-01 Water 08/31/17 09/01/17 Samples were received in good condition at 4.7 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 2 of 20 ®P1 �' S n n I Full -Service mi So do s V r Envfronmentel Solutions LA&OPPiOAES i1aG Laboratory Report 0911 9/2017 GTA (Geo-Tech. Assoc. Inc.) Charlotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Offsite - Monthly SW Sample Matrix: Water Client Sample ID: Offsite-2 Prism Sample ID: 7090022-01 Prism Work Order: 7090022 Time Collected: 08/31/17 15:15 Time Submitted: 09/01/17 11:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date(Tme ID General Chemistry Parameters Oil & Grease (SGT-HEM) BRLOG mg/L 5.0 1.1 1 '1664B 9114/17 13:30 SLS P710212 pH 6.3 HT pH Units 1 'SM4500-I.1 B 911117 11:53 BMS P710010 Total Suspended Solids 140 mg1L 17 0.40 1 'SM2540 D 917117 13:34 SLS P710094 Organochlorine Pesticides by GCIECD alpha-BHC BRL ug1L 0,052 0.010 1 '608 9/14/17 17'.50 JMC P710086 beta-BHC BRL ug/L 0.052 0.016 1 *608 9114117 17:50 JMC P710086 gamma-BHC BRL ug/L 0.052 0.013 1 `608 9114117 17:50 JMC P710086 delta-BHC BRL uglL 0.052 0.014 1 '608 9114117 17:50 JMC P710086 Heptachlor BRL ug/L 0,052 0.018 1 '608 9114117 17:50 JMC P710086 Aidhn BRL ug/L 0.052 0.015 1 '608 9114/17 17:50 JMC P710086 Heptachlor Epoxide BRL ug/L 0.052 0,013 1 '608 9/14/17 17:50 JMC P710086 trans -Chlordane BRL ug/L 0.052 0.027 1 '608 9/14117 17:50 JMC P710086 Endosulfan 1 0.20 ug/L 0.052 0.020 1 '608 9114117 17:50 JMC P710086 cis -Chlordane BRL ug/L 0.052 0.042 1 '606 9114117 17:50 JMC P710086 Dieldrin BRL ug/L 0.052 0.014 1 '608 9114117 17:50 JMC P710086 4,4'-DDE BRL ug1L 0.052 0.011 1 *608 9114117 17:50 JMC P710086 Endrin BRL uglL 0.052 0.015 1 '608 9114117 17:50 JMC P710086 Endosulfan II BRL ug1L 0.052 0.016 1 '608 9114117 17:50 JMC P710086 4 4'-DDD BRL ug1L 0.052 0.021 t *608 9/14117 17:50 JMC P710086 Endrin Aldehyde BRL ug1L 0.052 0.030 1 '608 9/14/17 17:50 JMC P710086 Endosulfan Sulfate BRL ug/L 0.052 0,016 1 1608 9114117 17:50 JMC P710086 4,4'-DDT BRL ug/L 0.052 0.025 1 '6q$ 9114/17 17:50 JMC P710086 Endrin Ketone BRL ug/L 0,052 0.032 -;> 1 *608 9114117 17:50 JMC P710086 Methoxychlor BRL ug/L 0.052 0,040 1 *608 9114/17 17:50 JMC P710086 Chlordane BRL ug/L 0.52 0.097 1 •608 918117 20:50 JMC P710086 Toxaphene BRL ug/L 0,52 0.076 1 `608 918117 20:50 JMC P710086 Aroclor 1016 BRL ug/L 0.52,i 0.25 1 `608 918117 20:50 JMG P710086 Arodor 1221 BRL ug/L 1.0 0.11 1 *608 918117 20:50 JMC P710086 Aroclor 1232 BRL ug/L 0.52 0,16 1 '608 918117 20:50 JMC P710086 Aroclor 1242 BRL ug/L 0.52 0.14 1 `608 918117 20:50 JMC P710086 Aroclor 1248 BRL ug/L 0.52 0.14 1 `608 918117 20:50 JMC 1`7100$6 Arodor 1254 BRL ug/L 0.52 0.16 1 '608 918117 20:50 JMC P710086 Aroclor 1260 BRL ug/L 0,52 0.31 1 '608 918117 20:50 JMC P710086 Surrogate Recovery Control Limits Tetrachloro-m-xylene 74 % 40-134 Decachlorobiphenyl 76 % 13-186 Semivolatile Organic Compounds by GClMS 12,4-Trichlorobenzene BRL ug/L i0 1.5 1 '625 916117 20:20 JMV P710065 1,2-Dichlorobenzene BRL ug/L 10 1.5 1 '625 916117 20:20 JMV P710065 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 70416294364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 3 of 20 Laboratory Report Full -Service Analytical & Environmental Solutions 09M 9/2♦71 7 T twaotaTOR1E5y irw GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Offsite - Monthly SW Client Sample ID: Offsite-2 Attn: Dave Mazorra Prism Sample ID: 7090022-01 710 Peninsula Lane, #B Prism Work Order: 7090022 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 08/31/17 15:15 Time Submitted: 09/01117 11:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,2-Diphenylhydrazine (as Azobenzene) BRL ug1L 10 3.0 1 '625 916117 20:20 JMV P710065 1,3-Dichlorobenzene BRL ug1L 10 1.4 1 '625 916117 20:20 JMV P710065 1,4-Dichlorobenzene BRL ug1L 10 1 A 1 '625 916117 20:20 JMV P710065 2,4,6-Trichlarophenoi BRL ug1L 10 1.9 1 '625 916117 20:20 JMV P710065 2,4-Dichlorophenol BRL uglL 10 1.6 1 1625 916/17 20:20 JMV P710065 2,4-Dimethylphenol BRL uglL 10 2.2 1 '625 916117 20:20 JMV P710065 2,4-Dinitrophenol BRL uglL 10 1.3 1 "625 916117 20:20 JMV P710065 2,4-Dinitrotoluene BRL uglL 10 3.1 1 'S25 916117 20:20 JMV P710065 2,6-Dinitrotoluene BRL uglL 10 3.1 1 '62S 916117 20:20 JMV P710065 2-Chloronaphthalene BRL ug/L 10 2.4 1 '625 916117 20:20 JMV P710065 2-Chlorophenol BRL ug1L 10 1.2 1 '625 916117 20:20 JMV P710065 2-Nitrophenol BRL ug1L 10 1.4 1 `625 916117 20:20 JMV P710065 3,3'-Dichlorobenzidine BRL ug1L 10 2.9 1 `625 916117 20:20 JMV P710065 4,6-Dinitro-2-methylphenol BRL uglL 10 2.0 1 '625 916117 20:20 JMV P710065 4-Bromophenyl phenyl ether BRL uglL 10 3.3 1 '625 916117 20:20 JMV P710065 4-Chloro-3-methylphenol BRL uglL 10 2.4 1 `625 916117 20:20 JMV P710065 4-Chlorophenyl phenyl ether BRL ug1L 10 2.3 1 '625 916117 20:20 JMV P710065 4-Nitrophenof BRL ug1L 52 1.7 1 `625 916117 20720 JMV P710065 Acenaphthene BRL ug1L 10 2.4 1 '625 916117 20720 JMV P710065 Acenaphthylene BRL ug1L 10 2.4 1 "625 916117 20:20 JMV P710065 Anthracene BRL uglL 10 3.3 1 '625 916117 20:20 JMV P710065 Benzidine BRL uglL 100 14 1 `625 916117 20:20 JMV P710065 Benzo(a)anthracene BRL uglL 10 3.2 1 '625 916117 20-20 JMV 13710065 Benzo(a)pyrene BRL ug1L 10 3.8 1 "625 916117 20:20 JMV P710065 Benzo(b)ffuoranthene BRL ugll- 10 3.7 1 '625 916117 20:20 JMV P710065 Benzo(g,hJ)perylene BRL ug1L 10 3.6 1 '625 916117 20:20 JMV P710065 Benzo(k)tiuotanthene BRL ug1L 10 4.0 1 '625 916117 20:20 JMV P710065 bis(2-Chloroetho)cy)methane BRL ug/L 10 1.9 1 '625 916117 20:20 JMV P710065 Bis(2-Chloroethyl)ether BRL ug/L 10 1.7 1 '625 916117 20:20 JMV P710065 Bis(2-chloroisopropyl)ether BRLCCV ug/L 10 1.8 1 '625 916117 20:20 JMV P710065 Bis(2-Eihylhexyl)phthalate BRL ug1L 10 3.3 1 `625 916117 20:20 JMV P710065 Butyl benzyl phthalate BRL uglL 10 2.7 1 '625 916117 20:20 JMV P710065 Chrysene BRL uglL 10 3.5 1 '625 916117 20:20 JMV P710065 Dibenzo(a,h)anthracene BRL ug1L 10 3.5 1 '625 916117 20:20 JMV P710065 Diethyl phthalate BRL ug1L 10 2.4 1 `625 916117 20:20 JMV P710065 Dimethyl phthalate BRL uglL 10 1.6 1 `625 916117 20:20 JMV P710065 Di-n-butyl phthalate BRL uglL 10 3.5 1 "625 916117 20:20 JMV P710065 Di-n-Wyl phthalate BRL ug1L 10 3.8 1 '625 916117 20:20 JMV P710065 Fluoranthene BRL uglL 10 3.6 1 '625 916117 20:20 JMV P710065 Fluorene BRL uglL 10 2.9 1 '625 916117 20:20 JMV P710065 - Hexachlorobenzene BRL ug1L 10 2.6 1 "625 916117 20:20 JMV P710065 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800IS29-6364 - Fax: 70416254409 Page 4 of 20 Lu'ajb Laboratory Report Full -Service Anal ical& Environmental Sotions 09/19/2017 LS-M GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Offsite - Monthly SW Client Sample ID: Otfsite-2 Attn: Dave Mazorra Prism Sample ID: 7090022-01 710 Peninsula Lane, #B Prism Work Order: 7090022 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 08/31/17 15:15 Time Submitted: 09101 /17 11:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis DatelTime Analyst Batch ID Hexachlorobutadiene BRL uglL 10 2.1 1 '625 916117 20:20 JMV P710065 Hexachlorocyclopentadiene BRL ug1L 10 1.7 1 '625 916117 20:20 JMV P710065 Hexachloroethane BRL ug1L 10 1.6 1 '625 916117 20:20 JMV P710065 Indeno(1,2,3-cd)pyrene BRL ug/L 10 3.2 1 '625 916117 20:20 JMV P710065 Isophorone BRL ug1L 10 2.2 1 '625 916117 20:20 JMV P710065 Naphthalene BRL ug1L 10 2.2 1 '625 916117 20:20 JMV P710065 Nitrobenzene BRL ug1L 10 1.4 1 '625 916117 20:20 JMV P710065 N-Nitrosodimethylamine BRL ug1L 10 0.86 1 '625 916117 20:20 JMV P710065 N-Nitroso-di-n-propylamine BRL ug1L 10 2A 1 '625 916117 20:20 JMV P710065 N-Nitrosodiphenyiarnine BRL ug1L 10 3.0 1 '625 916117 20:20 JMV P710065 Pentachlarophenol BRL uglL 10 2.2 1 '625 916117 20:20 JMV P710065 Phenanthrene BRL ug1L 10 3.3 1 '625 916117 20:20 JMV P710065 Phenol BRL ug1L 10 0.50 1 '625 916117 20:20 JMV P710065 Pyrene BRL UA 10 3.6 1 '625 916117 20:20 JMV P710065 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 71 % 31-144 2-Fluorobiphenyl 63 % 49-118 2-Fluorophenol 46 % 22-84 Nitrobenzene-d5 69 % 43-123 Phenol-d5 34 % 10-63 Terphenyl-d14 72 % 49-151 Total Metals Copper 0.011 mg1L 0.010 0.0010 1 '200.7 9111117 19:14 JAB P710071 Lead 0.0051 fnglL 0.0050 0.0010 1 '200.7 9111117 19:14 JAB P710071 Zinc 0.088 mg1L 0.030 0.0013 1 1200.7 9111117 19:14 JAB P710071 Volatile Organic Compounds by GC/MS 1, 1, 1 -Trichloroethane BRL ug1L 5.0 0.061 1 '624 912117 0:56 KDM P710031 1,1,2,2-Tetrachloroethane BRL ug/L 5.0 0,036 1 '624 912117 0:56 KDM P710031 1,1,2-Trichloroethane BRL ug1L 5.0 0.066 1 '624 9017 0:56 KDM P710031 1,1-Dichicroethane BRL ug1L 5.0 0.083 1 '624 912117 0:56 KDM P710031 1,1-❑ichloroethylene BRL ug1L 5.0 0.083 1 '624 912117 0:56 KDM P710031 1,2-Dichlorobenzene BRL uglL 5.0 0,076 1 '624 912117 0:56 KDM P710031 1,2-Dichloroethane BRL ug1L 5.0 0.066 1 '624 912117 0:56 KDM P710031 1,2-Dichloropropane BRL ug1L 5.0 0.11 1 '624 912117 0:56 KDM P710031 1,3-Dichlorobenzene BRL ug1L 5.0 0.054 1 '624 912117 0:56 KDM P710031 1,4-Dichicrobenzene BRL ug]L 5.0 0.050 1 '624 912117 0:56 KDM P710031 2-Chloroethyl Vinyl Ether BRL uglL 10 0.37 1 '624 912117 0:56 KDM PA0031 Acrolein BRL ug[L 100 0.20 1 '624 912117 0:56 KDM P710031 Acrylonitrile BRL ug1L 100 0.20 1 'fi24 912117 0:56 KDM P710031 Benzene BRL uglL 5.0 0.048 1 '624 912117 0:56 KDM P710031 Bromodichloromethane BRL uglL 5.0 0.062 1 '624 912117 0:56 KDM P710031 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Sox 240543 - Charlotte, NC 28224.OW Phone: 7041529-0364 - Toll Free Number: 1-8001529-6364 - Fax: 7041526-0409 Page 5 of 20 0 I 1, Full -Service Analytical r`• ' V' Environmental Solutions .Jr L;01Uigert$ wG Laboratory Report 09/ 1912017 GTA (Geo-Tech. Assoc. Inc.) Charlotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Offsite - Monthly SW Sample Matrix: Water Client Sample ID: Offsite-2 Prism Sample ID: 7090022-01 Prism Work Order: 7090022 Time Collected: 08/31/17 15:15 Time Submitted: 09/01/17 11:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DateTrime ID Bromoform BRL ug/L Bromomethane BRL ug/L Carbon Tetrachloride BRL ug1L Chlorobenzene BRL ug/L Chloroethane BRL ug/L Chloroform BRL ug/L Chloromethane BRL ug/L cis-1,3-Dichloropropylene BRL ug1L Dibromochiaromethane BRL ug1L Ethylbenzene BRL ug/L Methylene Chloride BRL ug1L Tetrachloroethylene BRL ug1L Toluene BRL ug1L trans- 1,2-Dichloroethylene BRL ug/L trans-1, 3-Dichloropropylene BRL ug/L Trichloroethylene BRL ug/L Trichlorofluoromethane BRL ug/L Vinyl chloride BRL ug/L 5.0 0.040 1 '624 912117 0:56 KDM P710031 10 0.18 1 '624 912117 0:56 KDM P710031 5.0 0.11 1 '624 912117 0:56 KDM P710031 5,0 0.062 1 '624 9/2/17 0:56 KDM P710031 10 0.22 1 '624 912/17 0:56 KDM P710031 5.0 0.076 1 "624 9/2117 0:56 KDM P710031 10 0.079 1 '624 912117 0:56 KDM P710031 5.0 0.079 1 '624 912117 0:56 KDM P710031 5.0 0.081 1 "624 9/2117 0:56 KDM P710031 5.0 0.061 1 `624 9/2117 0:56 KDM P710031 5.0 0.083 1 '624 9/2/17 0:56 KDM P710031 5.0 0.098 1 `624 9/2/17 0:56 KDM P710031 5.0 0.044 1 '624 912117 0:56 KDM P710031 5.0 0.094 1 '624 912/17 0:56 KDM P710031 5.0 0.070 1 "624 9/2117 0.56 KDM P710031 5.0 0.078 1 `624 9/2117 0:56 KDM P710031 10 0,062 1 '624 9/2/17 0:56 KDM P710031 10 0.097 1 '624 912/17 0:56 KDM P710031 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 74-126 Dibromofluoromethane 100 % 75-127 Toluene-d8 100 % 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 6 Of 20 y. i Fu11-Service analytical & Environmental Solutions LA6eR�NME% 1l Level II QC Report 9119/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Offsite - Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Volatile Organic Compounds by GClMS - Quality Control Prism Work Order: 7090022 Time Submitted: 9/1 /2017 11:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710031 - 624 Blank (Py10031-BLK1) _ Prepared & Analyzed: 09/0Ill 7 1, 1, 1 -Trichloroethane BRL 5.0 ug/L 1,1,2,2-Tetrachloroethane BRL 5.0 ug1L 1,1,2-Trichloroethane BRL 5.0 ug/L 1,1-Dichloroethane BRL 5.0 ug1L 1,1-Dichloroethylene BRL 5.0 uglL 1,2-Dichlorobenzene BRL 5.0 ug1L 1,2-Dichloroethane BRL 5.0 ug/L 12-Dichloropropane BRL 5.0 ug/L 1,3-Dichiorobenzene BRL 5.0 ug1L 1,4-Dichlorobenzene BRL 5.0 ugtL 2-Chloroethyl Vinyl Ether BRL 10 ug1L Acrolein BRL 100 ug1L Acrylonitrile BRL 100 ug1L Benzene BRL 5.0 ug1L Bromodichloromethane BRL 5.0 ug1L Bromoform BRL 5.0 ug1L Bromomethane BRL 10 ug1L Carbon Tetrachloride BRL 5.0 uglL Chlorobenzene BRL 5.0 ug1L Chloroethane BRL 10 ug/L Chloroform BRL 5.0 ug1L Chloromethane BRL 10 ug/L cis-1,3-Dichlaropropylene BRL 5.0 uglL Dibromochloromethane BRL 5.0 ug1L Ethylbenzene BRL 5.0 ug1L Methylene Chloride BRL 5.0 ug1L Tetrachloroethylene BRL 5.0 ug1L Toluene BRL 5.0 ug1L trans-1,2-Dichloroethylene BRL 5.o ug1L trans-1,3-Dichloropropylene BRL 5.0 ug/L Trichloroethylene BRL 5.0 ug/L Trichlorofluoromethane BRL 10 ug1L Vinyl chloride BRL 10 uglL TIC:Heptane 0.00 ug/L Surrogate:4-8rornofluorobenzene 50.8 ug/L 50.00 102 74-126 Surrogate: Dibromofluoromethane 50.1 ug/L 50,00 100 75-127 Surrogate: Toluene -dB 49.2 ug/L 50.00 98 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543 Phone: 7041529-0364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 7 of 20 /Ma nibw LS M Full -Service Analytical & r�Environmental Solutions Level II QC Report 9119117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Offsite - Monthly SW Volatile Organic Compounds by GCIMS - Quality Control Prism Work Order. 7090022 Time Submitted: 9/1/2017 11:00:OOAM Reporting Spike Source %REC RPD Analyse Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710031 - 624 LCS (P710031-BSI) Prepared & Analyzed: 09/01/17 1. 1. 1 -Trichloroethane 21.3 5.0 ug1L 20.00 106 52-162 1,1,2,2-Tetrachloroethane 22.3 5.0 ug1L 20.00 112 46-157 1,1,2-Trichlonoethane 21.8 5.0 ug1L 20.00 109 52-150 1,1-Dichlomethane 21.8 5,0 uglL 20.00 109 59-155 1,1-Dichloroethylene 23.0 5.0 uglL 20.00 115 10-234 1,2-Dichlorobenzene 22.2 5.0 uglL 20.00 ill 18-190 1,2-Dichloroethane 21.3 5.0 uglL 20.00 107 49-155 1,2-Dichloropropane 21.9 5.0 uglL 20,00 110 10-210 1,3-Dichlorobenzene 22.4 5.0 ug1L 20.00 112 59-156 1,4-Dichlorobenzene 22.0 5,0 ug1L 20.00 110 18-190 2-Chloroethyl Vinyl Ether 19.5 10 uglL 20.00 97 10-305 Acrolein 42.8 100 ug1L 40.00 107 10-196 Acrylonitrile 43.0 100 ug1L 40.00 108 60-134 Benzene 22.5 5.0 ug1L 20.00 112 37-151 Bromodichloromethane 22A 5.0 uglL 20.00 112 35-155 Bromoform 20.3 5.0 uglL 20.00 102 45-169 Bromomethane 23.5 10 ug1L 20.00 117 10-242 Carbon Tetrachloride 20.7 5.0 ug1L 20.00 103 70-140 Chlorobenzene 21.8 5.0 ug1L 20.00 109 37-160 Chloroethane 22.3 10 uglL 20.00 112 14-230 Chloroform 21.8 5.0 uglL 20.00 109 51-138 Chloromethane 20.3 10 ug1L 20.00 101 10-273 cis- 1,3-Dichloropropylene 22.8 5.0 IrglL 20.00 114 10-227 Dibromochloromethane 20.7 5.0 uglL 20.00 103 53-149 Ethylbenzene 22.9 5.0 uglL 20.00 115 37-162 Methylene Chloride 20.0 5.0 uglL 20.00 100 10-221 Tetrachloroethylene 22.9 5.0 ug1L 20.00 114 64-148 Toluene 22.5 5.0 uglL 20.00 113 47-150 trans-1,2-Dichloroethylene 22.4 5.0 uglL 20,00 112 54-156 trans-1,3-Dichloropropylene 23.1 5.0 uglL 20.00 116 17-183 Trichloroethytene 22.9 5.0 uglL 20.00 114 71-157 Tdchlorofluoromethane 22.0 10 uglL 20.00 110 17-181 Vinyl chloride 21.9 10 uglL 20.00 110 10-251 Sunogate:4-Bromotluorobenzene 48,8 uglL 50.00 96 74-126 Surrogate: Dibromofluoromethane 49.1 uglL 50.00 98 75-127 Surrogate: Toluene-d8 49.6 uglL 50.00 99 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704152"409 Page 8 of 20 d Apma 1 1 Level II QC Report aFull-Service Analytical& I mi Environmental Solutions 9119I17 t/1gORATORIE$ IRG GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Offsite - Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Volatile Organic Compounds by GCIMS - Quality Control Analyte Batch P710031 - 624 Reporting Result Limit Units Prism Work Order: 7090022 Time Submitted: 9/1/2017 11:00:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P710031-BSD1) Prepared & Analyzed: 09/01/17 1.1,1-Trichloroethane 21.4 5.0 ug1L 20.00 107 52-162 0A 20 1,1,2,2-Tetrachloroethane 21.4 5.0 uglL 20.00 107 46-157 4 20 1, 1,2-Trich loroethane 21.5 5.0 ug/L 20.00 107 52-150 2 20 1,1-Dichloroethane 22.2 5.0 ug1L 20.00 111 59-155 2 20 1,1-Dichloroethylene 23.0 5.0 ug1L 20.00 115 10-234 0.2 20 1,2-Dichlorobenzene 21.5 5.0 ug/L 20.00 107 18-190 3 20 1,2-Dichtoroethane 21.3 5.0 ug1L 20.00 107 49-155 0.05 20 1,2-Dichloropropane 21.7 5.0 ugtL 20.00 109 10-210 1 20 1,3-Dichlorobenzene 21.6 5.0 ug/L 20.00 108 59-156 4 20 1,4-Dichlorobenzene 21.4 5.0 ug1L 20.00 107 18-190 3 20 2-Chloroethyl Vinyl Ether 20.4 10 ug1L 20,00 102 10-305 5 20 Acrolein 41.3 100 ug1L 40.00 103 10-196 4 20 Acrylonitrile 40.9 100 ug1L 40,00 102 60-134 5 20 Benzene 22.5 5.0 UA 20.00 112 37-151 0.04 20 Bromodichloromethane 22.2 5.0 ug/L 20.00 111 35-155 0.8 20 Bromoform 19.2 5.0 ug/L 20.00 96 45-169 6 20 Bromomethane 24.8 10 ug1L 20.00 124 10-242 6 20 Carbon Tetrachloride 20.7 5.0 ug1L 20.00 104 70-140 0.2 20 Chlorobenzene 21.7 5.0 ug/L 20.00 109 37-160 0.6 20 Chloroethane 22.6 10 ug1L 20.00 113 14-230 1 20 Chloroform 22.2 5.0 uglL 20,00 ill 51-138 2 20 Chloromethane 22.1 10 ug1L 20.00 110 10-273 8 20 cis-1,3-Dichloropropylene 22.7 5.0 ug/L 20.00 114 10-227 0.2 20 Dibromochloromethane 20.0 5.0 ug1L 20,00 100 53-149 3 20 Ethylbenzene 22.7 5.0 ug1L 20.00 113 37-162 1 20 Methyiene Chloride 20.1 5.0 ug1L 20,00 100 10-221 0.2 20 Tetrachloroethylene 22.4 5.0 ug1L 20.00 112 64-148 2 20 Toluene 22.6 5.0 ug1L 20.00 113 47-150 0.3 20 trans- 1, 2-Dichloroethylene 22A 5.0 ug1L 20.00 112 54-156 0.04 20 trans- 1, 3-Dichloropropylene 22.8 5.0 ug1L 20.00 114 17-183 1 20 Trichloroethylene 23.2 5.0 ug1L 20.00 116 71-157 1 20 Trichlorofluoromethane 22.2 10 ug1L 20.00 ill 17-161 0.9 20 Vinyl chloride 22.0 10 ug/L 20.00 110 10-251 0.4 20 Surrogate:4-Bromofluorobenzene 49.7 ug/L 50.00 99 74-126 Surrogate: Dibromotluoromethane 50.8 ug/L 50.00 102 75427 Surrogate: Toluene-l8 50.1 ug/L 50.00 100 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 9 of 20 P' R I S M Full -Service Analytical i Envimnm8nta3 Solutions �Duea�asoinea irrc Level II QC Report 9/19117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Offsite - Monthly SW Prism Work Order: 7090022 Attn: Dave Mazorra Time Submitted: 9/1/2017 11:00:OOAM 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source °/REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710065 - 625 Blank (P710065-BLK7) Prepared & Analyzed: 09/06/17 1,2,4-Trichlorobenzene BRL 10 ug/L 1,2-Dichlorobenzene BRL 10 ug/L 1,2-Diphenylhydrazine (as Azobenzene) BRL 10 ug/L 1,3-Dichlorobenzene BRL 10 ug/L 1,4-Dichlorobenzene BRL 10 ug/L 2,4,6-Trichlorophenol BRL 10 ug/L 2,4-Dichlorophenol BRL 10 ug/L 2,4-Dimethylphenol BRL 10 ug1L 2,4-Dinitrophenol BRL 10 ug1L 2,4-Dinitrotoluene BRL 10 ug/L 2,6-Dinitrotoluene BRL 10 ug/L 2-Chloronaphthalene BRL 10 ug/L 2-Chlorophenol BRL 10 ug/L 2-Nitrophenol BRL 10 ug1L 3,T-Dichlorobenzidine BRL 10 ug/L 4,6-Dinitro-2-methylphenol BRL 10 ug/L 4-Bromophenyl phenyl ether BRL 10 ug/L 4-Chloro-3-methylphenol BRL 10 ug/L 4-Chlorophenyl phenyl ether BRL 10 ug/L 4-Nitrophenol BRL 50 ug1L Acenaphthene BRL 10 uglL Acenaphthylene BRL 10 ug/L Anthracene BRL 10 ug/L Benzidine BRL 100 ug/L Benzo(a)anthracene BRL 10 ug/L Benzo(a)pyrene BRL 10 ug/L Benzo(b)fluoranihene BRL 10 ug/L Benzo(g,h,i)perylene BRL 10 ug/L Benzo(k)fluoranthene BRL 10 ug1L bis(2 Chloroethoxy)methane BRL 10 ug/L Bis(2-Chlomethyl)ether BRL 10 ug/L Bis(2-chloroisopropyl)ether BRL 10 ug/L Bis(2-Ethylhexyl)phthalate BRL 10 ug/L Butyl benzyl phthalate BRL 10 uglL Chrysene BRL 10 ug/L Dibenzo(a,h)anthracene BRL 10 ug/L Diethyl phthalate BRL 10 ug1L Dimethyl phthalate BRL 10 ug/L Di-n-butyl phthalate BRL 10 ug/L Di-n-octyl phthalate BRL 10 ug/L Fiuoranthene BRL 10 ug/L Fluorene BRL 10 ug/L Hexachlorobenzene BRL 10 ug/L Hexachlorobutadiene BRL 10 ug/L Hexachlorocyclopentadiene BRL 10 ug/L Hexachloroelhane BRL 10 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 10 of 20 APIQ I n A 1 Full -Service Analytical iul ' V t Environmental SoEutions ��iweonaronies uic Level II QC Report 9119/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Offsite - Monthly SW Semivolatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 7090022 Time Submitted: 9/1/2017 11:00:OOAM Reporting Spike Source %REC RPO Analyle Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710065 - 625 Blank (P710065-BLK1) Prepared & Analyzed: 09/06/17 Indeno(1,2,3-cd)pyrene BRL 10 ug1L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug1L Nitrobenzene BRL 10 ug1L N-Nitrosadimethylamine BRL 10 ug1L N-Nitroso-di-n-propylamine BRL 10 ug/L N-Nitrosodiphenylamine BRL 10 ug/L Pentachlorophenol BRL 10 ugrL Phenanthrene 8RL 10 ug1L Phenol BRL 10 ug1L Pyrene BRL 10 ug/L Surrogate: 2,4,6-Tribromophenol 67.4 ug/L 100.0 67 31-144 Surnagate:2-Fluorobiphenyl 34.2 u91L 50.00 68 49-118 Surrogate:2-Fluorophenol 59.8 u91L 100.0 60 22-84 Surrogate: Nitrobenzene-d5 37.3 ug/L 50.00 75 43-123 Surrogate: Phenol-d5 40.0 ug/L 100.0 40 10-63 Surrogate: Terphenyl-04 41.0 ug/L 50.00 82 49-151 LCS (P710065-BS1) Prepared & Analyzed: 09/06/17 1,2,4-Trichlorobenzene 54.4 10 ug1L 100.0 54 44-142 1,2-Dichlorobenzene 64.9 10 ug1L 100.0 65 32-129 1,2-Diphenyihydrazine (as Azobenzene) 79.8 10 ug1L 100.0 80 40-135 1,3-Dichlorobenzene 64.4 10 ug/L 100.0 64 20-124 1,4-Dichlorobenzene 63.8 10 ug1L 100.0 64 20-124 2,4,6-Tdchlorophenol 80.0 10 ug1L 100.0 80 37-144 2,4-Dichlorophenol 60.5 10 ug1L 100.0 60 39-135 2,4-Dimethylphenol 68.7 10 uA 100.0 69 32-119 2,4-Dinitrophenol 62A 10 ug/L 100.0 62 10-191 2,4-Dinitrotoluene 74.4 10 ug1L 100.0 74 39-139 2,6-Dinitrotoluene 76.0 10 ug1L 100.0 76 50-158 2-Chloronaphthalene 71.2 10 ug1L 100.0 71 60-118 2-Chlorophenol 75.6 10 ug/L 100.0 76 23-134 2-Nitrophenol 61.2 10 ug1L 100.0 61 29-182 3,3'-Dichlorobenzidine 71.0 10 ug1L 100.0 71 10-262 4,6-Dinitro-2-methylphenol 79.9 10 uglL 100.0 80 10-181 4-8romophenyl phenyl ether 70.1 10 uglL 100.0 70 53-127 4-Chloro-3-methylphenol 66.1 10 ug1L 100.0 66 22-147 4-Chlorophenyt phenyl ether 70.4 10 ug1L 100.0 70 25-158 4-Nitrophenol 47.6 50 ug1L 100.0 48 10-132 Acenaphthene 72.4 10 ug1L 100.0 72 47-145 Acenaphthylene 72.2 10 ug/L 100,0 72 33-145 Anthracene 76.8 10 ug/L 100.0 77 27-133 Benzidine 63.1 100 ug1L 100.0 63 15-150 Benzo(a)anthracene 65.0 10 uglL 100.0 65 33-143 Benzo(a)pyrene 70.6 10 ug1L 100.0 71 17-163 Banzo(b)fluoranthene 67.5 10 ug1L 100.0 68 24-159 Benze(g,h,i)perylene 72.6 10 ug1L 100.0 73 10-219 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 29224-0543 Phone: 7e41529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 L Page 11 of 20 ®� }R I S M Full -Service Analytical 8 �_ Environmental Solutions ,O c' ownrauEs we Level II QC Report 9/19117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Offsite - Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GCIMS - Quality Control Analyte Batch P710065 - 625 Reporting Result Limit Units Prism Work Order: 7090022 Time Submitted: 9/1/2017 11:00:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P710065-BS1) Prepared & Analyzed: 09/06/17 Benzo(k)fluoranthene 70.8 10 uglL 100.0 71 11-162 bis(2-Chloroethoxy)methane 57.9 10 ug1L 100.0 58 33-184 Bis(2-Chloroethyl)ether 52.6 10 uglL 100.0 53 12-158 Bis(2-chloroisopropyl)ether 79.3 10 uglL 100.0 79 36-166 Bis(2-Ethylhexyl)phthalate 69.1 10 uglL 100.0 69 10-158 Butyl benzyl phthalate 59.8 10 uglL 100.0 60 10-152 Chrysene 61.8 10 ug1L 100.0 62 17-168 Dibenzo(a,h)anthracene 38.9 10 ug1L 100.0 39 10-227 Diethyl phthalate 59.2 10 ug1L 100.0 59 10-114 Dimethyl phthalate 32.8 10 uglL 100.0 33 10-112 Di-n-butyl phthalate 69.6 10 uglL 100.0 70 10-118 Di-n-octyl phthalate 72.6 10 uglL 100.0 73 10-146 Fluoranthene 72.5 10 ug1L 100.0 72 26-137 Fluorene 72.3 10 ug1L 1 MID 72 59-121 Hexachlorobenzene 75.1 10 ug1L 100.0 75 10-152 Hexachlorobutadiene 56.0 10 uglL 100.0 56 24-116 Hexachlorocyclopentadiene 74.9 10 uglL 100.0 75 32-117 Hexachloroethane 64.8 10 uglL 100.0 65 40-113 lndeno(1,2,3-cd)pyrene 77.6 10 uglL 100.0 78 10-171 Isophorone 65.7 10 ug1L 100.0 66 21-196 Naphthalene 55.2 10 ugtL 100.0 55 21-133 Nilrobenzene 54.2 10 uglL 100.0 54 35-180 N-Nitrasodimethylamine 40.6 10 uglL 100.0 41 10-119 N-Nitroso-di-n-propylamine 73.6 10 uglL 100.0 74 10-230 N-Nitrosodiphenylamine 92.9 10 uglL 100.0 93 69-152 Pentachlorophenol 86.4 10 uglL 100.0 86 14-176 Phenanthrene 74.5 10 uglL 100.0 74 54-120 Phenol 42.3 10 uglL 100.0 42 10-112 Pyrene 61.6 10 uglL 100.0 62 52-115 Surrogate. 2,4,6-Tribronlophenol 82.6 ug/L 100.0 83 31-144 Surrogate:2-Fluorobiphenyl 35.9 ug/L 50.00 72 49-118 Surrogate:2-Fluorophenol 55.3 uglL 100.0 55 22-84 Surrogate: Nitrobenzene-d5 29.9 ug/L 50.00 60 43-123 Surrogate.- Phenol-d5 37.4 uglL 100.0 37 10-63 Surrogate: Terphenyl-d14 37.0 uglL 50.00 74 49-151 This report should not be reproduced, except in its entirety, without the written consent of Pnsm Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041525-0409 Page 12 of 2� A bii Full-Service Analytical & I M Environmental Solutions L�ad1A1O NEa 1e Level II QC Report 9/19/17 GTA (Geo-Tech. Assoc. inc.) Charlotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Offsite - Monthly SW Semivolatile Organic Compounds by GCIMS - Quality Control Analyte Batch P710065 - 625 Prism Work Order: 7090022 Time Submitted: 9/1/2017 11:00:00AM Reporting Spike Source %REC RP❑ Result Limit Units Level Result %REG Limits RPD Limit Notes LCS Dup (1271006_5-BSD1) _ - Prepared & Analyzed: 09/06/17 1,2,4-Trichlorobenzene 55.9 10 ug/L 100.0 56 44-142 3 20 1,2-Dichlombenzene 67.0 10 ug1L 100.0 67 32-129 3 20 1,2-Diphenyihydrazine (as Azabenzene) 82.1 10 ug/L 100.0 82 40-135 3 20 1,3-Dichlorobenzene 67.1 10 ug/L 100.0 67 20-124 4 20 1,4-Dichlorobenzene 65.7 10 ug/L 100.0 66 20-124 3 20 2,4,6-Trichlorophenel 76.3 10 ug/L 100.0 76 37-144 5 20 2,4-Dichlorophenol 56.6 10 ug/L 100.0 57 39-135 7 20 2,4-Dimethylphenol 63.4 10 ug/L 100.0 63 32-119 8 20 2,4-Dinitrophenol 62.9 10 ug/L 100.0 63 10-191 0.8 20 2,4-Dinitrotoluene 76.7 10 ug1L 100.0 77 39-139 3 20 2,6-Dinitrotoluene 80.0 10 ug1L 100.0 80 50-158 5 20 2-Chlomnaphthalene 72.3 10 ug1L 100.0 72 60-118 2 20 2-Chlomphenol 69.2 10 ug/L 100.0 69 23-134 9 20 2-Nitrophenol 57.6 10 ug1L 100.0 58 29-182 6 20 3,3'-Dichlorobenzidine 72.6 10 ug/L 100.0 73 10-262 2 20 4,6-Dinitro-2-methylphenol 75.6 10 ug/L 100.0 76 10-181 6 20 4-Bromophenyl phenyl ether 72.4 10 ug/L 100.0 72 53-127 3 20 4-Chloro-3-methylphenol 60.8 10 ug/L 100.0 61 22-147 8 20 4-Chlorophenyl phenyl ether 73.5 10 uglL 100.0 73 25-158 4 20 4-Nitrophenol 44.8 50 ug/L 100.0 45 10-132 6 20 Acenaphthene 75.1 10 ug/L 100.0 75 47-145 4 20 Acenaphthylene 74.5 10 ug/L 100.0 74 33-145 3 20 Anthracene 78.2 10 ug1L 100.0 78 27-133 2 20 Benzidine 63.2 100 ug1L 100.0 63 15-150 0.1 20 Benzo(a)anthracene 66.2 10 ug1L 100.0 66 33-143 2 20 Benzo(a)pyrene 71.0 10 ug1L 100.0 71 17-163 0.5 20 Benzo(b)fluoranthene 67.5 10 ug/L 100.0 67 24-159 0.1 20 Benzo(g,h,i)perylene 74.1 10 ug1L 100.0 74 10-219 2 20 Benzo(k)fluoranthene 70.8 10 ug/L 100.0 71 11-162 0.1 20 bis(2-Chloroethoxy)methane 59.8 10 ug/L 100.0 60 33-184 3 20 Bis(2-Chloroethyl)ether 55.5 10 uglL 100.0 55 12-158 5 20 Bis(2-chlomisopropyl)ether 79.0 10 ug/L 100.0 79 36-166 0.3 20 Bis(2-Ethylhexyl)phthalate 69.8 10 ug/L 100.0 70 10-158 1 20 Butyl benzyl phthalate 55.8 10 ugfL 100.0 56 10-152 7 20 Chrysene 62.8 10 ug/L 100.0 63 17-168 2 20 Dibenzo(a,h)anthracene 40.6 10 ug/L 100.0 41 10-227 4 20 Diethyl phthalate 57.8 10 ua 100.0 58 10-114 2 20 Dimethyl phthalate 31.3 10 ug1L 100.0 31 10-112 5 20 Di-n-butyl phthalate 68.8 10 ug1L 100.0 69 10-118 1 20 Di-n-octyl phthalate 72.6 10 ug/L 100.0 73 10-146 0.04 20 Fluoranthene 74.1 10 ug1L 100.0 74 26-137 2 20 Fluorene 74.6 10 ug1L 100.0 75 59-121 3 20 Hexachlorobenzene 77.1 10 uglL 100.0 77 10-152 3 20 Hexachlorobutadiene 57.9 10 ug/L 100.0 58 24-116 3 20 Hexachlorocyclopentadiene 77.1 10 ug[L 100.0 77 32-117 3 20 Hexachloroethane 66.1 10 ug/L 100.0 66 40-113 2 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 70415254409 Page 13 of 20 AiiLi■ f S M � Full -Service Analytical & Environmental Solutions �OLAadIntOXiE; lNC Level II QC Report 9/19/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: OfFsite - Monthly SW Attn: pave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GCIMS - Quality Control Reporting Analyte Result Limit Units Prism Work Order: 7090022 Time Submitted: 9/1/2017 11:00:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P710065 - 625 LCS Dup (P710065-BSD1) Prepared & Analyzed: 09/06/17 Indeno(1,2,3-cd)pyrene 80.1 10 ugIL 100.0 80 10-171 3 20 Isophorone 67.2 10 ug1L 100.0 67 21-196 2 20 Naphthalene 56.7 10 ug1L 100.0 57 21-133 3 20 Nitrobenzene 5&.6 10 ugtL 100.0 57 35-180 4 20 N-Nitrosodimethylamine 40.8 10 ug1L 100.0 41 10-119 0.5 20 N-Nitroso-di-n-propylamine 73.7 10 uglL 100,0 74 10-230 0.05 20 N-Nitrosodiphenylamine 95.6 10 uglL 100.0 96 69-152 3 20 Pentachlorophenol 80.7 10 ug1L 100.0 81 14-176 7 20 Phenanthrene 76.2 10 uglL 100.0 76 54-120 2 20 Phenol 41.4 10 uglL 100.0 41 10-112 2 20 Pyrene 63.5 10 ug1L 100.0 63 52-115 3 20 Surrogate: 2,4,6 Tribromophenol 76.9 u91L 100.0 77 31-144 Surrogate:2-Fluorobiphenyl 37.8 U91L 50.00 76 49-118 Surrogate:2-Fluorophenol 50.8 ug7L 100.0 51 22-64 Surrogate: Nitrobenzene-d5 31,6 ug/L 50.00 63 43-123 Surrogate: Phenol-d5 33.9 ug/L 100.0 34 10-63 Surrogate: TerphenyW14 38.3 uglL 50.00 77 49-151 This report should not be reproduced, except in its entirety, without the wntten consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-0364 - Toll Free Number: 1-800/529-6364 - Fax: 70415264409 Page 14 of 20 0.1 R ISM Rig uTowes, INC Full -Service Analylical & Environmental Solutions Level II QC Report 9119/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: OfFsite - Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #13 Charlotte, NC 28273 Organochlorine Pesticides by GCIECD - Quality Control Prism Work Order: 7090022 Time Submitted: 9/1/2017 11:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710086 - 608 Blank (P710086-BLK1) Prepared: 09/07/17 Analyzed: 09/08/17 alpha-BHC BRL 0.050 ug/L beta-BHC BRL 0.050 ug/L gamma-BHC BRL 0.050 ug/L delta-BHC BRL 0.050 uglL Heptachlor BRL 0.050 ug/L Akirin BRL 0.050 ug1L Heptachlor Epoxide BRL 0.050 ug1L trans -Chlordane BRL 0.050 ug/L Endosulfan I BRL 0.050 ug1L cis -Chlordane BRL 0.050 ug1L Dieldrin BRL 0.050 ug/L 4,4'-DDE BRL 0.050 ug/L Endnn BRL 0.050 ug/L Endosulfan II BRL 0.050 ug/L 4,4'-DDD BRL 0.050 ug/L Endrin Aldehyde BRL 0.050 uglL Endosulfan Sulfate BRL 0.050 ug/L 4,4'-DDT BRL 0.050 ug1L Endrin Ketone BRL 0.050 ug/L Methoxychlor BRL 0.050 ug/L Chlordane BRL 0.50 ug1L Toxaphene BRL 0.50 ug/L Aroclor 1016 BRL 0.50 ug/L Aroclor 1221 BRL 1.0 ug/L Aroclor 1232 BRL 0.50 ug/L Aroclor 1242 BRL 0.50 ug/L Aroclor 1248 BRL 0,50 ug/L Aroclor 1254 BRL 0.50 UM Aroclor 1260 BRL 0.50 ug/L Surrogate: Tetrachloro-m-xylene 0.686 ug/L 1.000 69 40-134 Surrogate: Decachlorobiphenyl 1.01 ug/L 1.000 101 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7044529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 L Page 15 of 20 M I Full-Sevice Analytical & /m6fibASGEnvironmental Solutions Level 11 QC Report 9119l17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Offsite - Monthly SW Attm Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Organochlorine Pesticides by GC/ECD -Quality Control Prism Work Order: 7090022 Time Submitted: 9/1/2017 11:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710086 - 608 LCS (P710086-BSI) Prepared: 09/07/17 Analyzed: 09/08/17 alpha-BHC 0.812 0.050 ug1L 1.000 81 37-134 beta-BHC 0.809 0.050 uglL 1.000 81 17-147 gamma-BHC 0.816 0.050 uglL 1.000 82 32-127 delta-BHC 0.702 0.050 ug1L 1.000 70 19-140 Heptachlor 0.749 0.050 ug1L 1.000 75 34-111 Aldrin 0.715 0.050 ug1L 1.000 72 42-122 Heptachlor Epoxide 0.821 0.050 ug1L 1.000 82 37-142 trans -Chlordane 0.803 0.050 ug1L 1.000 80 45-119 Endosulfan 1 0.837 0A50 uglL 1.000 84 45-153 cis -Chlordane 0.815 0.050 ug1L 1.000 82 45-119 Dieldrin 0.836 0.050 ug1L 1,000 84 36-146 4,4'-DDE 0.793 0.050 ug1L 1.000 79 30-145 Endrin 0.817 0.050 ug1L 1.000 82 30-147 Endosulfan II 0.870 0.050 ug1L 1.000 87 10-202 4,4'-DDD 0.831 0.050 ug1L 1.000 83 31-141 Endrin Aldehyde 0,842 0.050 ug1L 1.00o 84 51-132 Endosulfan Sulfate 0.830 0.050 ug1L 1.000 83 26-144 4,4'-DDT 0.835 0.050 ug1L 1.000 84 25-160 Endrin Ketone 0.911 0.050 uglL 1.000 91 58-134 Methoxychlor 0.861 0.050 ug1L 1.000 86 54-145 Surrogate. Tetrachtoro-m-xylene 0.568 uglL 1.000 57 40-134 Surrogate: Decachlorobiphenyl 0.677 ug/L 1.000 68 13-186 LCS (P710086-BS2) Prepared: 09/07/17 Analyzed: 09/08/17 Chlordane 8,62 0.50 ug1L 10.00 86 50-150 Surrogate: Tetrachloro-m-xylene 0,563 ug/L 1.000 56 40-134 Surrogate: Decachlorobiphenyl 1.18 ug/L 1.000 118 13-166 This report should not be reproduced, except in its enlirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704t529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 16 of 20 Pf � 2 ISM Full -Service Analytical & Environmental Solutions �L�90MTOf IlEs lx Level 11 QC Report 9119/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: OfFsite - Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Organochlorine Pesticides by GCIECD - Quality Control Prism Work Order 7090022 Time Submitted: 9/1/2017 11:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710086 - 608 LCS (P710086-BS3) Prepared: 09/07/17 Analyzed: 09/08/17 Toxaphene 9.09 0.50 ug1L 10.00 91 41-126 Surrogate: Tetrachloro-m-xylene 0.588 u91L 1.000 59 40-134 Surrogate: Decachlorabiphenyl 0.954 ug/L 1.000 95 13-186 LCS (P710086-BS4) Prepared: 09/07/17 Analyzed: 09/08/17 Chlordane BRL 0,50 ug1L 50-150 Toxaphene BRL 0.50 ug1L 41-126 Aroclor 1016 7.95 0.50 ug1L 10.00 80 50-114 Aroclor 1260 9.80 0.50 ug1L 10,00 98 10-127 Surrogate: Tetrachloro-m-xylene 0.813 ug/L 1.000 81 40-134 Surrogate: Decachlorobiphenyl 0.907 u91L 1.000 91 13-186 LCS Dup (P710086-BSD1) Prepared: 09/07/17 Analyzed: 09/08/17 alpha-BHC 0.798 0.050 ug1L 1.000 80 37-134 2 20 beta-BHC 0.791 0.050 ug1L 1.000 79 17-147 2 20 gamma-BHC 0.804 0.050 ug/L 1.000 80 32-127 1 20 delta-BHC 0.687 0.050 ug1L 1.000 69 19-140 2 20 Heptachlor 0.756 0,050 uglL 1,000 76 34-111 0.9 20 Aldrin 0.713 0.050 ug1L 1.000 71 42-122 0.3 20 Heptachlor Epoxide 0.808 0.050 ug/L 1.000 81 37-142 2 20 trans -Chlordane 0.811 0.050 ug1L 1.000 81 45-119 1 20 Endosulfan 1 0.822 0.050 uglL 1.000 82 45-153 2 20 cis -Chlordane 0.807 0.050 ug/L 1.000 81 45-119 1 20 Dieldrin 0.833 0.050 ug/L 1.000 83 36-146 0.4 20 4,4'-DDE 0.834 0.050 ug/L 1MID 83 30-145 5 20 Endrin 0.846 0.050 ug/L 1.000 85 30-147 4 20 Endosulfan II 0.661 0.050 ug1L 1.000 86 10-202 1 20 4,4'-DDD 0.842 0.050 ug/L 1.000 84 31-141 1 20 Endrin Aldehyde 0.789 0.050 ug/L 1.000 79 51-132 7 20 Endosulfan Sulfate 0.838 0.050 ug/L 1.000 84 26-144 1 20 4,4'-DDT 0.883 0.050 uglL 1.000 88 25-160 6 20 Endrin Ketone 0.930 0,050 ug1L 1.000 93 58-134 2 20 Methoxychbr 0.904 0.050 ug/L 1.000 90 54-145 5 20 Surrogate: Tetrachloro-m xylene 0.589 ug/L 1.000 59 40-134 Surrogate: Decachlarobiphenyl 0.497 ug/L 1.000 50 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 17 of 20 I S ,l " I i.Full-Service Analytical ' V' EnvOnmen[el Solutions Level II QC Report 9119117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Offsite - Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Total Metals - Quality Control Prism Work Order: 7090022 Time Submitted: 9/1/2017 11:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P710071 - 200.7 Blank (P710071-BLK1) Prepared: 09/07/17 Analyzed: 09/11/17 Copper BRL 0.010 mglL Lead BRL 0.0050 mglL Zinc BRL 0.030 mglL LC5 (P710071-BS1) Prepared: 09/07/17 Analyzed: 09/11/17 Copper 0.244 mglL 0.2500 97 85-115 Lead 0.252 mg1L 0.2500 101 $5-115 Zinc 0.263 mglL 0.2500 105 85-115 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 2405Q - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: 1-8001529-6364 - Fax: 70W52"409 Page 18 of 20 a EService Analytical ' V' Environmental Solutions ���neoa�ron�Ea uec Level H QC Report 9/19/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 General Chemistry Parameters -Quality Control Analyte Batch P710010 - NO PREP Project: OfFsite - Monthly SW Prism Work Order: 7090022 Time Submitted: 9/1/2017 11:00:00AM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS (P71001043S1) Prepared & Analyzed: 09/01/17 pH 6.88 pH Units 6.880 100 98.5-101.5 Duplicate (P710010-DUP2) Source: 7090022-01 Prepared & Analyzed: 09/01/17 pH 6.35 pH Units 6.26 1 10 Batch P710094 - NO PREP Blank (P710094-BLKI) Prepared & Analyzed: 09/07/17 Total Suspended Solids BRL 5.0 mg/L LCS (P710094-BSI) Prepared &_Analyzed: 09/07/17 Total Suspended Solids 480 5.0 mg/L 477.0 101 90-110 Batch P710212 - NO PREP Blank (P710212-BLK1) Prepared & Analyzed: 09/14/17 Oil & Grease (SGT-HEM) BRL 5.0 mglL OG Sample Extraction Data Prep Method:608 Lab Number Batch Initial Final DateMme 7090022-01 P710086 970 mL 10 mL 09/07/17 9:15 7090022-01 P710086 970 mL 10 mL 09/07/17 915 Prep Method: 625 Lab Number Batch Initial Final Datemme 7090022-a1 P710065 960 mL 1 mL 09/06/17 13-16 Prep Method: 200.7 Lab Number Batch Initial Final Date[Time 7090022-01 P710071 50 mL 50 mL 09/07/17 8:05 Prep Method: 624 Lab Number Batch Initial Final DatefTime 7090022-01 P710031 10 mL 10 mL 09/01/17 9:22 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 141001529-6364 - Fax: 7041525-0409 Page 19 of 2fl 1 .I a■ :I S M � Fullironmenrvicp Analytical $. Environmental Solutions AUCHAMFUrtz! INC 449 Springbrook Road • Charlotte, NC 28217 Phone 704J529-6364 • F'ax;7041525-0409 Client Company Name: ,//AA Report To/Contact Name: Ax ro-A-- Reporting'Address:-7fo &dl.%t CHAIN of CUSTODY DECOR® PAGE OF —L QUOTE N TO ENSURE PROPER BILLING: [t l •J i/t/ Project Dame: `t ' �� 'e .S` �!y Short Hold Analysis: (Yes) Q& Project: (Yes) "Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV) provisions aallor QC Requirements Invoice To ra e bfv) Address: Phone: _Fax (Yes) (No : Purchase Order No./Billing Reference 3J�1 77 IZ Email Address: gtfV 2n /',ra1t_ • C10 Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days O 5 Days TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Certification: NELAC DoD FL NC_U_ EDD Type: PDF Excel-25,Qther "Working Days" ❑ 6-9 Days OL45tandard 10 days I] Push Work Must Be ed Site Location Name: S Samples received after 14:00 will be processed next business day. Site Location Physical Address: Turnaround time Is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) SC OTHER NIA Water Chlorinated: YES_ NOX Sample Iced Upon Collec ' n: YES NO_ CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER PRESERVA- TIVES ANALYSIS REQUESTED [� REMARKS ® / �O PRISM LAB ID NO. "TYPE SEE BELOW NO. SIZE I �� t. .. sampler's Signature Sampled By (Print Name) ') Illation Upon relinquishing, this Chain of Custody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted In writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. Relinquished y: Signature Receive y: (Signature) ate MlliliarylHours Additional Comments: Site Arrival Time: Relinquished By: (Signature) Received By: (SI ture) Date .ilte Dapaaure Time: Relinquished By: (Signature) Receiv or P sm La alorle By: r Date Field Tech Fee: y 2 � � .. � , � • r Mileage. Method o Shipment: NO : ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH C TODY SEALS FOR SPOR ATION TO THE LABORATORY. GOC Group No. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC rlL RECEIVED AT THE SORATORY. , Q Fed F-x ❑ UPS ❑ Hand -delivered 0 Prism Field Service ❑ Other CLA I UST. GROUNDWATER: DRINKING WATER: SOLIDWASTE: RSCIRC LANDFILL IRDES NC Q SCC] NC Q ❑NC ❑ S❑ NC ❑ S❑ NC ❑ SC CIAkNC 0 SC ❑ NC ❑ SC ❑ NCEl SC ❑ NC ] C I n n ] ❑ *ftr1NTAINFR TYPF C17nF8: A = Amhar C = Clear G= Glass P = Plastic: TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) noff Ih I A Monthly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No, NCG030000 Date submitted August 18, 2017 CERTIFICATE OF COVERAGE NO. NCG030663 FACILITY NAME Select Stainless Products LLC COUNTY Mecklenburg PERSON COLLECTING SAMPLES David Mazorra LABORATORY Prism Laboratories, Inc. Lab Cert. # 402 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' July (month) RECEIVLDDHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA AUG 28 2W ®Other Class C CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTION ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids mg/L pH, Standard units Copper mg/L Lead mg/L Zinc mg/L Non -Polar O&G/ Total Petroleum Hydrocarbons mg/L Total Toxic s Organics mg/L Benchmarks =_=> - - 100 6.0 — 9.0 0.007 0.030 0.067 is 1 5W-1 07/28/17 0.46 90 6.2 0.015 <0.0009 0.24 <1.1 <1 SW-2 07/28/17 0.46 9.8 5.4 <0.0004 <0.0009 1.7 <1.1 <1 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 7 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." David R. Mazorra PE Name (Print name) Senior Environmental Engineer _ Title Pri t ti 11 U (Signature) (Da ) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period:2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU SW-1 SW-2 Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail. an original and one copy of this DMR,including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" regorts) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware t t there a nificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature rmittee) (Dat Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 PsiR1SM �lABORATORIE$!MG Full -Service Analytical & Environmental Solutions NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Case Narrative 08/14/2017 GTA (Geo-Tech. Assoc. Inc.) Charlotte Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Monthly SW Lab Submittal Date: 07/31/2017 Prism Work Order, 7070509 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. 6. *'W"� Cara C. Rusmisell Project Manager Data Qualifiers Key Reference: G e� Reviewed By Cara C. Rusmisell Project Manager HT Sample received and analyzed outside of the hold time. OG HEM O&G is less than the reporting limit, therefore TPH (SGT-HEM) is less than the reporting limit. Sample not extracted for TPH (SGT-HEM). BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1800/62"364 - Fax: 704/526.0409 Page i of 44 - Full -Service Analytical d ism i Environmental Solutions J..1W. 08/14/2017 Prism Work Order: 7070509 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received SW-1 7070509-01 Water 07/28/17 07/31/17 SW-2 7070509-02 Water 07/28/17 07/31/17 Samples were received in good condition at 3.6 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 5pringbroolc Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 2 of 24 S2 R ISM Environmental an Solutions Laboratory Report Environmental Solutions 0611412017 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-1 Attn: Dave Mazorra Prism Sample ID: 7070509-01 710 Peninsula Lane, #B Prism Work Order: 7070509 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 07/28/17 17:15 Time Submitted: 07/31/17 12A5 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Dateri-ime ID General Chemistry Parameters Oil & Grease (SGT-HEM) BRLOG mg1L 5.0 1.1 1 '1664B 818117 12:30 SLS P7HO154 pH 6.2 HT pH Units 1 "SNI45D" B 7131117 13:21 SLS P7430485 Total Suspended Solids 90 mg1L 12 0.40 1 'SM2S40 D 814117 10:13 SLS P7HO104 Organochlorine Pesticides by GCIECD alpha-BHC BRL ug1L 0.051 0.010 1 '608 818117 18:18 JMC P7H0031 beta-BHC BRL uglL 0.051 0.016 1 `608 818117 18:18 JMC P7H0031 gamma-BHC BRL uglL 0.051 0.013 1 '608 818117 18:18 JMC P7H0031 delta-BHC BRL ug1L 0.051 0.014 1 `fi08 818117 18:18 JMC P7H0031 Heptachlor BRL ug1L 0.051 0.017 1 '608 818117 18:18 JMC P7H0031 Aldrin BRL ug1L 0.051 0.015 1 1608 818117 18:18 JMC P7H0031 Heptachlor Epoxide BRL ug1L 0.051 0.013 1 *608 818117 18:18 JMC P7H0031 trans -Chlordane BRL ug/L 0.051 0.027 1 '608 818117 18:18 JMC P7H0031 Endosulfan I BRL ug1L 0.051 0.019 1 `608 818117 18:18 JMC P7H0031 cis -Chlordane BRL ug1L 0,051 0.042 1 '608 818117 18:18 JMC P7H0031 Dieldrin BRL uglL 0.051 0.014 1 '608 818117 18:18 JMC P7H0031 4,4'-DDE BRL ug1L 0.051 0,011 1 'fi08 818117 18:18 JMC P7H0031 Endrin BRL ug1L 0.051 0.015 1 '608 818117 18:18 JMC P7110031 Endosulfan II BRL ug1L 0,051 0.016 1 '608 818117 18:18 JMC P7H0031 4,4'-DDD BRL ug1L 0.051 0.020 1 *608 818117 18:18 JMC P7H0031 Endrin Aldehyde BRL ug1L 0.051 0,030 1 '6D8 818117 18:18 JMC P7H0031 Endosulfan Sulfate BRL uglL 0.051 0,016 1 '608 818117 18:18 JMC P7H0031 4,4'-DDT BRL ug1L 0.051 0.024 1 `608 818117 18:18 JMC P7H0031 Endrin Ketone BRL uglL 0.051 0,032 1 '608 518117 18:18 JMC P7H0031 Methoxychlor BRL ug1L 0.051 0.040 1 '608 818117 16:1$ JMC P7H0031 Chlordane BRL ug1L 0.51 0.096 1 '608 818117 18:18 JMC P7H0031 Toxaphene BRL ug1L 0.51 0.076 1 '608 818117 18:18 JMC P7H0031 Arodor 1016 BRL ug1L 0.51 0.25 1 `608 818117 18:18 JMC P7H0031 Arodor 1221 BRL ug1L 1.0 0.11 1 '608 818117 18:18 JMC P7H0031 Aroclor 1232 BRL ug1L 0.51 0.16 1 '608 818117 18:18 JMC P7110031 Aroclor 1242 BRL ug1L 0.51 0.14 1 `6O8 818117 18:18 JMC P7H0031 Arodor 1248 BRL ug1L 0.51 0.14 1 `608 818117 1&18 JMC P7H0031 Arodor 1254 BRL ug1L 0.51 0,16 1 '608 818117 18:18 JMC P7110031 Arodor 1260 BRL uglL 0.51 0.30 1 `608 818117 18:18 JMC P7110031 Surrogate Recovery Control Limits Tetrachloro-m-xylene 53 % 40-134 Derachlorobiphenyl 47 % 13-186 Semivolatile Organic Compounds by GUMS 1,2,4-Trichlorobenzene BRL ug1L 10 1.5 1 '625 $11117 20:30 JMV P7H0007 1,2-Dichlorobenzene BRL ug/L 10 1.5 1 '625 811117 20:30 JMV 137H0007 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/629-6364 . Fax: 704/526-W9 Page 3 of 24 L&�NSFull -Service Analytical & M Environmental Solutions a:anr� we Laboratory Report 08/14/2017 GTA (Geo-Tech. Assoc. Inc.) Chadotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Monthly SW Sample Matrix: Water Client Sample ID: SW-1 Prism Sample ID: 7070509-01 Prism Work Order: 7070509 Time Collected: 07/28/17 17:15 Time Submitted: 07/31/17 12:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime ID 1,2-Diphenylhydrazine (as Azobenzene) BRL ug1L 10 3.0 1 '625 811117 20:30 JMV P7H0007 1,3-D'ichlorobenzene BRL ug1L 10 1A 1 '625 811117 20:30 JMV P71-10007 1,4-Dichtorobenzene BR{_ uglL 10 1.4 1 "625 811117 20:30 JMV P7H0007 2,4,6-Tdchlorophenol BRL uglL 10 1.9 1 '625 811117 20:30 JMV P71HI0007 2,4-Dichlorophenol BRL ug1L 10 1.6 1 '625 $11117 20:30 JMV 1371-10007 2,4-Dimethylphenol BRL uglL 10 2.2 1 '625 811117 20:30 JMV P7H0007 2,4-Dinitrophenol BRL ug1L 10 1.3 1 "625 811117 20M JMV P7H0007 2,4-Dinitrotoluene BRL ug/L 10 3.1 1 '625 811117 20:30 JMV P7H0007 2,6-Dinitrotoluene BRL ug1L 10 3.1 1 '625 811117 20:30 JMV P7H0o07 2-Chloronaphthalene BRL uglL 10 2.4 1 '625 811117 20:30 JMV P7H0007 2-Chlorophenol BRL ug1L 10 1.2 1 "625 811117 20:30 JMV P7H0007 2-Nitrophenol BRL ug1L 10 1.4 1 '625 811117 20:30 JMV P7H0007 3,3'-Dichlorobenzidine BRL ug1L 10 2.9 1 '625 811117 20:30 JMV P7H0007 4,6-Dinitro-2-methylphenol BRL ug1L 10 2.0 1 "625 811117 20:30 JMV P7H0007 4-Bromophenyl phenyl ether BRL ug1L 10 3.3 1 '625 811117 20:30 JMV P7H0007 4-Chloro-3-methylphenol BRL uglL 10 2.4 1 '625 811117 20:30 JMV P71-10007 4-Chlorophenyl phenyl ether BRL ug1L 10 2.3 1 '625 811117 20:30 JMV P71-10007 4-Nitrophenol BRL ug1L 52 1.7 1 "625 811117 20:30 JMV P7H0007 Acenaphthene BRL uglL 10 2.4 1 '625 811117 20:30 JMV P7H0007 Acenaphthylene BRL uglL 10 2.4 1 '625 811117 20:30 JMV P7H0007 Anthracene BRL ug1L 10 3.3 1 "625 811117 20:30 JMV P7H0007 Benzidine BRL uglL 100 14 1 "625 811117 20:30 JMV P71-10007 Benzo(a)anthracene BRL ug1L 10 3.2 1 '625 811117 20:30 JMV P7H0007 Benzo(a)pyrene BRL ug1L 10 3.8 1 '625 811117 20:30 JMV P7H0007 Benzo(b)fluoranthene BRL ug1L 10 3.7 1 '625 811117 20:30 JMV P7H0007 Benzo(g,h,i)perylene BRL ug1L 10 3,6 1 `625 811117 20:30 JMV P7H0007 Benzo(k)fluoranthene BRL ug1L 10 4.0 1 '625 811117 20:30 JMV P7H0007 bis(2-Chloroethoxy)methane BRL ug1L 10 1.9 1 '625 811117 20:30 JMV P71-10007 Bis(2-Chloraethyl)ether BRL ug1L 10 1.7 1 '625 811117 20:30 JMV P7H0007 Bis(2-chloroisopropyl)ether BRL uglL 10 1.8 1 '625 811117 20:30 JMV P7H0007 Bis(2-Ethylhexyl)phthalate BRL ug1L 10 3.3 1 '625 811117 20M JMV P7H0007 Butyl benzyl phthalate BRL ug1L 10 2.7 1 '625 811117 20:30 JMV P71-10007 Chrysene BRL ug1L 10 3.5 1 'fi25 811117 20:30 JMV P7H0007 Dibenzo(a,h)anthracene BRL u9lL 10 3.5 1 '625 811117 20:30 JMV P71-10007 Diethyl phthalate BRL ug1L 10 2A 1 '625 811117 20:30 JMV P71-10007 Dimethyl phthalate BRL uglL 10 1.6 1 "625 811117 20:30 JMV P7H0007 Di-n-butyl phthalate BRL ug1L 10 3.5 1 '625 811117 20:30 JMV P7H0007 Di-n-octyl phthalate BRL ug1L 10 3.8 1 625 811117 20:30 JMV P7H0007 Fluoranthene BRL ug1L 10 3.6 1 `625 811117 20:30 JMV P7H0007 Fiuorene BRL ug1L 10 2.9 1 '625 811117 20:30 JMV P7H0007 Hexachlorobenzene BRL uglL 10 2.6 1 '625 811117 20:30 JMV P7H0007 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 70415294364 - Toll Free Number: 1-8001629-6364 • Fax: 704/526-0409 Page 4 of 24 Laboratory Report Q21 I n n I Fullron ten Analytical 8 r� 1 V � Environmental Solutl0na Q$f1412017 iweartw�an�tt we GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-1 Attn: Dave Mazorra Prism Sample ID: 7070509-01 710 Peninsula Lane, #B Prism Work Order: 7070509 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 07/28/17 17:15 Time Submitted: 07/31/17 12:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Hexachlorobutadiene BRL ug1L Hexachlorocyclopentadiene BRL ug(L Hexachloroethane BRL uglL Indeno(1,2,3-td)pyrene BRL ug1L Isophorone BRL uglL Naphthalene BRL ug1L Nitrobenzene BRL ug1L N-Nitrosodimethylamine BRL uglL N-Nitroso-di-n-propylamine BRL ug1L N-Nitrosodiphenylamine BRL ug1L Pentachloraphenol BRL ug& Phenanthrene BRL ug1L Phenol BRL ug1L Pyrene BRL ug1L Total Metals 10 2.1 1 `625 811117 20:30 JMV P7H0007 10 1.7 1 `625 811117 20:30 JMV P7H0007 10 1.6 1 "625 811117 20:30 JMV P71-10007 10 3.2 1 *625 811117 20:30 JMV P71-10007 10 2.2 1 *625 811117 20:30 JMV P71-10007 10 2.2 1 `625 811117 20:30 JMV P71-10007 10 1.4 1 '625 811117 20:30 JMV P7H0007 10 0.86 1 `625 811117 20:30 JMV P7H0007 10 2.1 1 '625 811117 20:30 JMV P7H0007 10 3.0 1 `625 811117 20:30 JMV P7H0007 10 Z2 1 `625 811117 20:30 JMV P7H0007 10 3.3 1 *625 811117 20-30 JMV P7H0007 10 0,50 1 *625 811117 20:30 JMV P71-10007 10 3.6 1 '625 811117 20:30 JMV P71-10007 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 56 % 31-144 2-Fluorobiphenyl 56 % 49-118 2-Fluorophenol 37 % 22-84 Nitrobenzene-d5 47 % 43-123 Phenol-d5 27 % 10-63 Terphenyl-d14 68 % 49-151 Copper 0.015 mg1L 0.010 0.00040 1 •200.7 817/17 15:27 JAB P7H0091 Lead BRL mg1L 0.0050 0,00090 1 *200.7 817117 15:27 JAB P7HOO91 Zinc 0.24 mglL 0.030 0.010 1 *200.7 8r7117 15:27 JAB P7H0091 Volatile Organic Compounds by GUMS 1,1,1-Trichloroethane BRL ug1L 5.0 0.061 1 *624 812117 18:45 KDM P7HOO66 1,1,2,2-Tetrachloroethane BRL uglL 5.0 0.036 1 *624 812117 18:45 KDM P7HOO66 1. 1, 2-Trichloroethane BRL ug1L 5.0 0.066 1 '624 812117 18:45 KDM P7HOO66 1,1-Dichloroethane BRL ug1L 5.0 0,083 1 *624 812117 18:45 KDM P7140066 1,1-Dichlomethylerne BRL ug/L 5.0 0.083 1 *624 812117 18:45 KDM P7HOO66 1,2-Dichlorobenzene BRL ug1L 5.0 0.076 1 *624 812117 18A5 KDM P7HOO66 1,2-Dichloroethane BRL ug1L 5.0 0.066 1 *624 812117 18:45 KDM P7HOO66 1,2-Dichloropropane BRL ug1L 5.0 0,11 1 *624 812117 18:45 KDM P7HOO66 1,3-Dichtombenzene BRL ug1L 5.0 0.054 1 'fi24 812J17 18:45 KDM P7HOO66 1,4-Dichlombenzene BRL ug1L 5.0 0.050 1 *524 $12117 18:45 KDM P7HOO66 2-Chloroethyl Vinyl Ether BRL ug1L 10 0.37 1 *624 812117 18:45 KDM P7HOO66 Acrolein BRL uglL 100 0.20 1 *624 8017 18:45 KDM P7HOO66 Acrylonitrile BRL uglL 100 0.20 1 *624 812117 18:45 KDM P7H0066 Benzene BRL uglL 5.0 0.04$ 1 `fi24 812117 18:45 KDM P71-10066 Bromodichloromethane BRL ug1L 5.0 0.062 1 `624 812117 18:45 KDM P71-10066 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 5pringbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-M9 Page 5 of 24 LJOP-R I S M I Fun -Service Analytical & Environmental solutlons %Ama Tomam 1 w Laboratory Report 08/14/2017 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-1 Attn: Dave Mazorra Prism Sample ID: 7070509-01 710 Peninsula Lane, #B Prism Work Order: 7070509 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 07/28/17 17:15 Time Submitted: 07/31/17 12:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime ID Bromotorm BRL ug1L 5.0 0.040 1 '624 812117 18:45 KDM P7H0066 Bromomethane BRL ug1L 10 0.18 1 '624 812J17 18:45 KDM P71-10056 Carbon Tetrachloride BRL uglL 5.0 0.11 1 '624 812117 18:45 KDM P7H0066 Chlorobenzene BRL uglL 5.0 0.062 1 '624 812117 18:45 KDM P7110066 Chloroethane BRL ug1L 10 0.22 1 •624 812117 18:45 KDM P7H0066 Chloroform BRL ug1L 5.0 0.076 1 '624 812117 18:45 KDM 1371-110066 Chloromethane BRL uglL 10 0.079 1 '624 812117 18:45 KDM P7H0066 cis-1,3-Dichloropropylene BRL uglL 5.0 0.079 1 `624 812117 18:45 KDM P7H0066 Dibromofluaromethane BRL uglL 5.0 0.081 1 '624 812117 18A5 KDM P7140066 Ethylbenzene BRL ug1L 5.0 0.061 1 '624 812117 18:45 KDM P7H0066 Methylene Chloride BRL uglL 5.0 0.083 1 "624 812117 18:45 KDM P7110066 Tetrachloroethylene BRL ug1L 5.0 0.098 1 '624 812117 18:45 KDM P7H0066 Toluene BRL ug1L 5.0 0.044 1 `624 812117 18:45 KDM P7H0066 trans-1,2-Dichloroethyfene BRL ug1L 5.0 0.094 1 `624 812117 18:45 KDM P7110066 trans-1,3-Dichloropropylene BRL ug1L 5.0 0.070 1 '624 812117 16A5 KDM P71-10066 Trichloroethylene BRL ug1L 5.0 0.078 1 '624 812117 18:45 KDM P71HI0066 Trichlorofluoromethane BRL ug1L 10 0.062 1 `624 612117 18:45 KDM P7H0066 Vinyl chloride BRL ug1L 10 0.097 1 '624 812117 18:45 KDM P71110066 Surrogate Recovery Control Limits 4-Bromofluorobenzene 106 % 74-126 Dibromofluoromethane 95 % 75-121 Toluene-0 100 % 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 6 of 24 Laboratory Report 2. Lw..LS /� I Fult-Service AnalytiG91 8 08/14/2017 / Environmental Solutlonc Ne GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-2 Attn. Dave Mazorra Prism Sample ID: 7070509-02 710 Peninsula Lane, #B Prism Work Order: 7070509 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 07/28/17 17:30 Time Submitted: 07/31/17 12:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters Oil & Grease (SGT-HEM) BRLOG mg/L 5.0 1.1 1 '1664B 818/17 13:30 SLS P71-10154 pH 5A HT pH Units 1 *SM4500-H B 7131/17 13:17 SLS P7G0485 Total Suspended Solids 9.8 mg1L 2.7 0.40 1 *SM2540 D 814117 10:13 SLS P7H0104 Organochlorine Pesticides by GC/ECD alpha-BHC BRL ug/L 0.055 0.011 1 `608 8/8/17 18:30 JMC P7H0031 beta-BHC BRL ug/L 0.055 0.018 1 *608 818117 18:30 JMC P7H0031 gamma-BHC BRL ug/L 0.055 0.014 1 '608 818117 18:30 JMC P7H0031 delta-BHC BRL ug/L 0.055 0.015 1 *608 818117 18:30 JMC PIH0031 Heptachlor BRL ug1L 0.055 0.019 1 1608 818117 18:30 JMC P7H0D31 Aldrin BRL ug/L 0.055 0.016 1 *608 8/8117 18:30 JMC P7H0031 Hoptachlor Epoxide BRL uglL 0.055 0.014 1 *608 8/8117 18:30 JMC P7HOD31 trans -Chlordane BRL ug/L 0.055 0.029 1 '608 6/8117 18:30 JMC P7H0031 Endosulfan I BRL ug/L 0.055 0.021 1 *608 818117 18:30 JMC P7H0031 cis -Chlordane BRL ug/L 0.055 0.045 1 *608 818117 18:30 JMC P7H0031 Dieldrin BRL ug/L 0.055 0.015 1 '608 818/17 18:30 JMC P7H0031 4,4'-DDE BRL ug1L 0.055 0.012 1 '6D8 818/17 18:30 JMC P71-10031 Endrin BRL ug/L 0.055 0.016 1 *608 818117 18:30 JMC P7H0031 Endosulfan 11 BRL ug/L 0.055 0.018 1 *608 818117 18:30 JMC P7Hoo31 4,4'-DDD BRL ug/L 0.055 0.022 1 '608 $18117 18:30 JMC P71-10031 Endrin Aldehyde BRL ug1L 0.055 0.032 1 *608 8/8117 18:30 JMC P7H0031 Endosulfan Sulfate BRL ug/L 0.055 0.018 1 *608 818/17 18:30 JMC P7HDD31 4,4'-DDT BRL ug1L 0,055 0.026 1 '608 8/8111 18:30 JMC P7H0031 Endrin Ketone BRL ug1L 0,055 0.034 1 *608 818117 18:30 JMC P7H0031 Methoxychlor BRL ug/L 0.055 0.043 1 *608 818117 18:30 JMC P7H0031 Chlordane BRL ug/L 0.55 0.10 1 *608 818117 18:30 JMC P7H0031 Toxaphene BRL ug/L 0.55 0.081 1 'fi08 818/17 18:30 JMC P7H0031 Arodor 1016 BRL ug/L D.55 0.27 1 '608 818117 18:30 JMC P7H0031 Arodor 1221 BRL uglL 1.1 0.12 1 *608 8/8117 18:30 JMC P7H0031 Aroclor 1232 BRL ug/L 0.55 0.18 1 *608 818117 18:30 JMC P7H0031 Arodor 1242 BRL ug/L 0.55 0.15 1 *608 818117 18:30 JMC P7H0031 Aroclor 1248 BRL uglL 0.55 0.15 1 *608 B/8/17 18:30 JMC P7H0031 Arodor 1254 BRL ug/L 0.55 0.18 1 *608 818117 1830 JMC P7H0031 Aroclor 1260 BRL ug1L 0,55 0.33 1 *608 818117 18:30 JMC P7H0031 Surrogate Recovery Control Limits Tetrachloro-m-xylene 63 % 40-134 Decachlorobiphenyl 36 % 13-186 Semivolatile Organic Compounds by GUMS 1,2,4-Trichlorobenzene BRL ug1L 11 1.5 1 '625 811117 20:52 JMV P7HD007 1,2-Dichlorobenzene BRL ug/L 11 1.5 1 '625 811117 20:52 JMV P7H0007 This report should not be reproduced, except in its entirety, without the written consent of Prism laboratories, Inc. 449 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 7 of 24 ' (FuniService al Soj ical S Environmental SolWiong Oi§ V GTA (Geo-Tech. Assoc. Inc.) Charlotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Monthly SW Sample Matrix: Water Laboratory Report 08/14/2017 Client Sample ID: SW-2 Prism Sample ID: 7070509-02 Prism Work Order: 7070509 Time Collected: 07/28/17 17:30 Time Submitted: 07/31/17 12:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,2-Diphenylhydrazine (as Azobenzene) BRL ug1L 11 3.0 1 '625 $11117 20:52 JMV P7110007 1,3-Dichlorobenzene BRL ug1L 11 1.4 1 '625 811117 20:52 JMV P7H0007 1,4-Dichlorobenzene BRL ug[L 11 1.4 1 '625 811117 20:52 JMV P7H0007 2,4,6-Trichlorophenol BRL ug1L 11 1.9 1 '625 811117 20:52 JMV P7H0007 2,4-Dichlorophenol BRL ug1L 11 1.7 1 "625 811117 20:52 JMV P7110007 2,4-Dimethylphenol BRL ug1L 11 2.2 1 '625 811117 20.52 JMV P7H0007 2,4-Dinitrophenol BRL ug/L 11 1.3 1 '625 811117 20:52 JMV P7H0007 2,4-Dinitrotoluene BRL ug1L 11 3.1 1 `625 811117 20:52 JMV P7110007 2,6-Dinitrotoluene BRL ug1L 11 3.1 1 '625 811117 20:52 JMV P7H0007 2-Chloronaphthalene BRL ug1L 11 2.5 1 '625 811117 20:52 JMV P7H0007 2-Chlorophenol BRL ug1L 11 1.2 1 'fi25 811117 20:52 JMV P7H0007 2-Nitrophenol BRL ug/L 11 1.5 1 '625 811117 20:52 JMV P7H0007 3,3'-Dichlorobenzidine BRL ug/L 11 2.9 1 'fi25 811117 20:52 JMV P7140007 4,6-Dinitro-2-methylphenol BRL ug1L 11 2.0 1 '625 811117 20:52 JMV P7H0007 4-Bromophenyl phenyl ether BRL ug1L 11 3.3 1 '625 811117 20:52 JMV P7H0007 4-Chloro-3-methylphenol BRL uglL 11 2.4 1 '625 811117 20:52 JMV P7H0007 4-Chlorophenyl phenyl ether BRL ug/L 11 2.3 1 '625 811117 20:52 JMV P7H0007 4-Nitrophenol BRL ug1L 53 1.8 1 'fi25 811117 20:52 JMV P7H0007 Acenaphthene BRL ug1L 11 2.4 1 '625 811117 20:52 JMV P7H0007 Acenaphthylene BRL ug/L 11 2A 1 `625 811117 20:52 JMV P7H0007 Anthracene BRL ug1L 11 3.3 1 '625 811117 20:52 JMV P71110007 Benzidine BRL ug1L 110 15 1 'fi25 811117 20:52 JMV P7H0007 Benzo(a)anthracene BRL ug1L 11 3.3 1 '625 811117 20:52 JMV P7H0007 Benzo(a)pyrene BRL ug[L 11 3.8 1 "625 811117 20:52 JMV P7H0007 Benzo(b)fluoranthene BRL ug1L 11 3.7 1 'fi25 811117 20:52 JMV P71-10007 Benzo(g,hJ)perylene BRL ug1L 11 3.7 1 'fi25 811117 20:52 JMV P7H0007 Benzo(k)fluoranthene BRL ug1L 11 4.0 1 '625 811117 20:52 JMV P7110007 bis(2-Chloroethoxy)methane BRL ug1L 11 1.9 1 '625 811117 20:52 JMV P7110007 Bis(2-ChloroethyDether BRL ug(L 11 1.7 1 `625 8/1117 20:52 JMV P7H0007 Bis(2-r-hloroisopropyl)ether BRL ug1L 11 1.8 1 '625 811117 20:52 JMV P7110007 Bis(2-Ethylhexyl)phthalate BRL ug1L 11 3.3 1 `625 811117 20:52 JMV P7110007 Butyl benzyl phthalate BRL ug1L 11 2.7 1 '625 811117 20:52 JMV P7110007 Chrysene BRL ug1L 11 3.6 1 '625 811117 20:52 JMV P71-10007 Dibenzo(a,h)anthracene BRL ug1L 11 3,6 1 "625 811117 20:52 JMV P7110007 Diethyl phthalate BRL ug1L 11 2.4 1 'fi25 811117 20:52 JMV P7110007 Dimethyi phthalate BRL ug1L 11 1.6 1 '625 811117 20:52 JMV P71-10007 Di-n-butyl phthalate BRL ug1L 11 Is 1 '625 811117 20:52 JMV P7110007 Di-n-octyl phthalate BRL ug1L 11 3.8 1 '625 811117 20:52 JMV P7H0007 Fluoranthene BRL ug1L 11 3.7 1 '625 811117 20:52 JMV P7H0007 Fluorene BRL ug/L 11 2.9 1 '625 811117 20:52 JMV P7H0007 Hexachlorobenzene BRL ug1L 11 2.6 1 'fi25 811117 20:52 JMV P7140007 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 8 of 24 \ Full -Service Analytical & Laboratory Report >�P�� I i�r L Environmental Solutions 08/14I2017 ��aaawLM GTA (Geo-Tech. Assoc. Inc.) Charlotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Monthly SW Client Sample ID: SW-2 Prism Sample ID: 7070509-02 Prism Work Order: 7070509 Sample Matrix: Water Time Collected: 07/28/17 17:30 Time Submitted: 07/31/17 12:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTme ID HexacNorobutadiene BRL ug/L 11 2.1 1 *625 8/1117 20;52 JMV P7H0007 Hexachlorocyclopentadiene BRL ug/L 11 1.7 1 `625 8/1117 20:52 JMV P71-10007 Hexarhioroethane BRL uglL 11 1.6 1 •625 811117 20:52 JMV P71-10007 Indeno(1,2,3-cd)pyrene BRL ug/L 11 3.2 1 '625 811/17 20:52 JMV P71-10007 Isophorone BRL ug/L 11 2.2 1 '625 811117 20:52 JMV P71-10007 Naphthalene BRL uglL 11 2.2 1 '625 811/17 20:52 JMV P7H0007 Nitrobenzene BRL ug/L 11 1.5 1 *625 8/1117 20:52 JMV P71-110007 N-Nitrosodimethylamine BRL ug/L 11 0.87 1 *625 8/1117 20:52 JMV P71-10007 N-Nitroso-di-n-propylamine BRL ug/L 11 2.1 1 *625 811117 20:52 JMV P71-10007 N-Nitrosodiphenylamine BRL ug/L 11 3.1 1 *625 811117 20:52 JMV P7H0007 Pentachlorophenol BRL ug/L 11 2.2 1 '625 811117 20:52 JMV P7140007 Phenanthrene BRL ug/L 11 3.4 1 '625 811/17 20:52 JMV P71-10007 Phenol BRL uglL 11 0.51 1 '625 811/17 20:52 JMV P7H0007 Pyrene BRL uglL 11 3.7 1 '625 811/17 20:52 JMV P71-10007 Surrogate Recovery Control Limits 2,4,6-Tdbromophenol 60 % 31-144 2-Fluorobiphenyl 72 % 49-118 2-Fluorophenol 25 % 22-84 Nitrobenzene-d5 62 % 43-123 Phenol-d5 31 % 10-63 Terphenyl-d14 96 % 49-151 Total Metals Copper BRL mg1L 0.010 0.00040 1 *200.7 817117 15:36 JAB P7H0091 Lead BRL mg1L 0.0050 0.00090 1 '200.7 W117 15:36 JAB P7H0091 Zinc 1.7 mg/L 0.030 0.010 1 *200.7 817117 15:36 JAB P71i0091 Volatile Organic Compounds by GUMS 1,1,1-Trichloroethane BRL ug/L 5.0 0.061 1 '624 812117 19:11 KDM P71-10066 1,1,2,2-Tetrachloroethane BRL ug/L 5.0 0.036 1 '624 812/17 19:11 KDM P71-10066 1,1,2-Trichloroethane BRL ug1L 5.0 0.066 1 '624 812/17 19:11 KDM 1371-10066 1,1-Dichloroethane BRL ug/L 5.0 0.083 1 *624 8/2117 19:11 KDM 1371-10066 1,1-Dichloroethylene BRL ug/L 5.0 0.083 1 *624 8/2117 19:11 KDM 1371-10066 1,2-Dichlorobenzene BRL ug/L 5.0 0.076 1 *624 812117 mil KDM P71-10066 1,2-Dichloroethane BRL ug1L 5.0 0,066 1 '624 8/2117 19:11 KDM P7140066 1,2-Dichloropropane BRL ug1L 5.0 0.11 1 *624 812117 19:11 KDM P71-10066 1,3-Dichlorobenzene BRL uglL 5.0 0.054 1 '624 812117 19:11 KDM P71-10066 1,4-Dichiambenzene BRL ug/L 5.0 0.050 1 '624 812117 19:11 KDM P71-10066 2-Chloroethyl Vinyl Ether BRL ug/L 10 0.37 1 *624 812117 19:11 KDM P71-10066 Acrolein BRL ug1L 100 0.20 1 '624 812/17 19:11 KDM P71-10066 Acrylonitrile BRL ug/L 100 0.20 1 *624 812117 19:11 KDM P7H0066 Benzene BRL ug1L 5.0 0.048 1 `624 812/17 19:11 KDM P71-10066 Bromodichloromethane BRL uglL 5.0 0.062 1 *624 812117 19:11 KDM P71-10066 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-80015294364- Fax: 7041525-0409 Page 9 of 24 Laboratory Report Full -Service Analytical & RISM I Enironmental Solutions �m6 W. 08114/20171AAAA GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Client Sample ID: SW-2 Attn: Dave Mazorra Prism Sample ID: 7070509-02 710 Peninsula Lane, #B Prism Work Order: 7070509 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 07128/17 17:30 Time Submitted: 07/31/17 12:45 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis DateFrime Analyst Batch ID Bromoform BRL ug/L 5.0 0.040 1 `624 812117 19:11 KDM P7H0066 Bromomethane BRL ug/L 10 0.18 1 "624 812117 19:11 KDM P71-10066 Carbon Tetrachloride BRL ug/L 5.0 0.11 1 '624 812117 19:11 KDM P7H0066 Chlorobenzene BRL ug/L 5.0 0.062 1 '624 812117 19:11 KDM P71-10066 Chloroethane BRL ug/L 10 0.22 1 '624 812117 19:11 KDM P7H0066 Chloroform BRL ug/L 5.0 0.076 1 "624 812117 19:11 KDM P7H0066 Chloromethane BRL ug/L 10 0.079 1 `fi24 $12117 19:11 KDM P7H0066 cis- 1, 3-Dichloropropylene BRL ug/L 5.0 0,079 1 '624 812117 19:11 KDM P7H0066 Dibromochloromethane BRL ug/L 5.0 0.081 1 `624 812117 19:11 KDM P7HO066 Ethylbenzene BRL ug/L 5.0 0.061 1 "624 812117 19:11 KDM P7H0o66 Methytene Chloride BRL ug/L 5.0 0.083 1 '624 812117 19:11 KDM P71-I0066 Tetrachloroethylene BRL ug1L 5.0 0.098 1 '624 812/17 19:11 KDM P7H0066 Toluene BRL ug/L 5.0 0.044 1 '624 812117 19:11 KDM P7H0066 trans-1,2-Dichloroethylene BRL ug/L 5.0 0.094 1 '624 812/17 19:11 KDM P7H0066 trans- 1, 3-Dichloropropylene BRL ug/L 5.0 0.070 1 '624 812117 19:11 KDM P7H0066 Trichloroethylene BRL ug1L 5.0 0,078 1 '624 8/2117 19:11 KDM P7HO066 Trichlorofluoromethane BRL ug/L 10 0.062 1 '624 812117 19:11 KDM P71`10066 Vinyl chloride BRL ug/L 10 0.097 1 `624 812/17 19:11 KDM P7H0066 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 74-126 Dibromofluoromethane 102 % 75-127 Toluene-d8 92 % 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 70416254409 Page 10 0f 24 AP n FuAnalytical IS Envimirimental Solutans d'uaow�oa� me Level II QC Report 8/14/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 volatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 7070509 Time Submitted-. 7/31/2017 12:45:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P71-10066 - 624 Blank (P71-10066-BLK1) Prepared & Analyzed: 08/02/17 1,1,1-THchloroethane BRL 5.0 ug/L 1,1,2,2-Tetrachloroethane BRL 5.0 ug/L 1,1,2-Tdchloreethane BRL 5.0 ug/L 1,1-Dichloroethane BRL 5.0 ug1L 1,1-Dichloroethylene BRL 5.0 ug/L 1,2-Dichlorobenzene BRL 5A ug/L 1,2-Dichloroethane BRL 5.0 ug/L 1,2-Dichloropropane BRL 5.0 ug/L 1,3-Dichlorobenzene BRL 5.0 ug/L 1,4-Dichlorobenzene BRL S.D ug/L 2-Chloroethyl Vinyl Ether BRL 10 ug/L Acrolein BRL 1013 ug/L AMIonitrile BRL 100 ug/L Benzene BRL 5.0 ug/L Bromodichloromethane BRL 5.0 ug/L Bromoform BRL 5.0 ug/L Bromomethane BRL 10 ug/L Carbon Tetrachloride BRL 5.0 ugtL Chlorobenzene BRL 5.0 ugtL Chloroethane BRL 10 ug/L Chloroform BRL 5.0 ug/L Chloromethane BRL 10 ug/L cis-1,3-Dichloropropylene BRL 5.0 ug/L Dibromochloromethane BRL 5.0 ug/L Ethylbenzene BRL 5.0 ug/L Methylene Chloride BRL 5.0 ug/L Tetrachloroethylene BRL 5.0 ug1L Toluene BRL 5.0 ug/L trans-1,2-Dichloroethylene BRL 5.0 ug/L trans-1,3-Dichloropropylene BRL 5.0 ug/L Trichloroethylene BRL 5.D ug/L Trichlorofluoromethane BRL 10 ug/L Vinyl chloride BRL 10 ug/L Surrogate:4-Sromofluorobenzene 49.9 ug/L 50.00 100 74-126 Suaogate: Dibromofluoromethene 54.1 ug/L 50.00 108 75-127 Surrogate: Toluene-/8 46.7 ug/L 50.00 93 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529.6364 - Fax: 70M525-0409 Page 11 of 24 ISM Envi LJ� .+I■..� Full -Service Analytical 8 Environmental Solutions --%VBOHIlT ES INC. Level II QC Report 8/14/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #8 Charlotte, NC 28273 Volatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 7070509 Time Submitted: 7/31/2017 12:45:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7HOQ66 - 624 LCS (P71-10066-BS1) Prepared & Analyzed: 08/02/17 1,1,1-Trichloroethane 26.1 5.0 ugR 20.00 131 52-162 1,1,2,2-Tetrachloroethane 16.7 5.0 ug/L 20.00 84 46-157 1,1,2-Trichloroethane 21.7 5.0 ugR 20.00 108 52-150 1,1-Dichloroethane 20.9 5.0 ugtL 20.00 105 59-155 1,1-Dichloroethylene 22.5 5.0 ug/L 20,00 113 10-234 1,2-Dichlorobenzene 19.1 5.0 ug/L 20.00 96 18-190 1,2-Dichloroethane 24.7 5.0 ug/L 20.00 124 49-155 1,2-Dichloropropane 18.8 5.0 ug1L 20.00 94 10-210 1,3-Dichlarobenzene 19.4 5.0 ugR 20.00 97 59-156 1,4-Dichlorobenzene 18.9 5.0 ug/L 20.00 95 18-190 2-Chlomethyl Vinyl Ether 23.2 10 ug/L 20.00 116 10-305 Acrolein 25.5 100 ug/L 40.00 64 10-196 Acrylonitrile 38.3 100 ugR 40.00 96 60-134 Benzene 20.8 5.0 ugR 20.00 104 37-151 Bromodichloromethane 23.5 5.0 ug/L 20.00 118 35-155 Bromoform 21.0 5.0 ug/L 20.00 105 45-169 Bromomethane 14A 10 ug/L 20.00 72 10-242 Carbon Tetrachloride 27.0 5.0 ug/L 20.00 135 70-140 Chlorobenzene 20.7 5.0 ug/L 20.00 103 37-160 Chloroethane 16.4 10 ugR 20.00 62 14-230 Chloroform 23.8 5.0 ug/L 20.00 119 51-138 Chloromethane 13.3 10 ug/L 20.00 66 10-273 cis-1,3-Dichloropropylene 22.2 5.0 ug/L 20.00 ill 10-227 Dibromochloromethane 22.3 5.0 ug/L 20.00 112 53-149 Ethylbenzene 21.2 5.0 ugR 20.00 106 37-162 Methylene Chloride 18.2 5.0 ug1L 20.00 91 10-221 Tetrachloroethylene 21.9 5.0 ug1L 20A0 109 64-148 Toluene 21.3 5.0 ug/L 20.00 106 47-150 trans-1,2-Dichloroethylene 21.7 5.0 ug/L 20.00 108 54-156 trans-1,3-Dichloropropylene 23.3 5.0 ugR 20.00 116 17-183 Trichloroethylene 21.7 5.0 ug/L 20.00 108 71-157 Trichlorofluoromethane 26.1 10 ug/L 20.00 130 17-181 Vinyl chloride 16.6 10 ug/L 20.00 83 10-251 Surrogate:4-Brornoftuorobenzene 48.9 ug/L 50.00 98 74-126 Surrogate: DibromoRuoromethane 54.8 ug/L 50.00 110 75-127 Surrogate: Toluene-d8 47.8 ug/L 50.00 96 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 26224-0543 Phone: 704/529-0364 - Toll Free Number: 1-8001529-0364 - Fax: 7041525-0409 Page 12 of 24 �ISM Oaonwioace, MG. Full -Service Analytical 8 Environmental Solutions Level II QC Report 8114/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Volatile Organic Compounds by GC1MS - Quality Control Anaiyte Batch P71110066 - 624 Reporting Result Limit Units Prism Work Order: 7070509 Time Submitted: 7/31/2017 12:45:0013M Spike Source Level Result %REC %REC RPD Limits RPD Limit Notes LCS Dup {157110066-BSD1) Prepared & Analyzed: 08/02/17 1,1,1-Trichloroethane 25.3 5.0 ug/L 20.00 126 52-162 3 20 1,1,2,2-Tetrachloroethane 17.1 5.0 ug/L 20.00 85 46-157 2 20 1,1,2-Trichloroethane 21.9 5.0 ug/L 20.00 109 52-150 0.8 20 1,1-Dichloroethane 20.8 5.0 ug1L 20.00 104 59-155 0.7 20 1,1-Dichloroethylene 21.6 5.0 ug1L 20.00 108 10-234 5 20 1,2-Dichlorobenzene 19.9 5.0 ug/L 20.00 100 18-190 4 20 1,2-Dichloroethane 24.8 5.0 ug1L 20.00 124 49-155 0.6 20 1,2-Dichloropropane 18.9 5.0 ug/L 20.00 95 10-210 0.6 20 1,3-Dichlorobenzene 19.7 5.0 ug1L 20.00 99 59-156 2 20 1,4-Dichlorobenzene 19.5 5.0 ug/L 20.00 97 18-190 3 20 2-Chloroethyl Vinyl Ether 23.7 10 ug1L 20.00 119 10-305 2 20 Acrolein 25.8 100 ug/L 40.00 65 10-196 1 20 Acryionitrile 37.1 100 ugfL 40.00 93 60-134 3 20 Benzene 19.9 5.0 ug/L 20.00 100 37-151 4 20 Bromodichloromethane 23.1 5.0 ug/L 20.00 116 35-155 2 20 Bromoform 20.6 5.0 ug1L 20.00 103 45-169 2 20 Bromomethane 14.5 10 ug/L 20,00 73 10-242 0,6 20 Carbon Tetrachloride 26.1 5.0 ug/L 20.00 130 70-140 3 20 Chlorobenzene 19.5 5.0 ug/L 20,00 98 37-160 6 20 Chloroethane 15.4 10 ug/L 20.00 77 14-230 7 20 Chloroform 22.0 5.0 ug/L 20.00 110 51-138 8 20 Chloromethane 12.8 10 ug1L 20.00 64 10-273 4 20 cis- 1, 3-Dichloropropylene 21.5 5.0 ug/L 20.00 108 10-227 3 20 Dibromochloromethane 21.9 5.0 ug1L 20.00 109 53-149 2 20 Ethylbenzene 20.6 5.0 ug/L 20.00 103 37-162 3 20 Methylene Chloride 17.9 5.0 ug/L 20.00 89 10-221 2 20 Tetrachloroelhylene 20.7 5.0 ug1L 20.00 103 64-148 6 20 Toluene 20.6 5.0 ug1L 20.00 103 47-150 3 20 trans-1,2-Dichloroethylene 20.6 5.0 Ug1L 20.00 103 54-156 5 20 trans-1,3-Dichloropropylene 22.9 5.0 ug1L 20.00 114 17-183 2 20 Trichloroethylene 21.6 5.0 ug1L 20.00 108 71-157 0.2 20 Trichlorofluoromethane 23.6 10 ug/L 20.00 118 17-181 10 20 Vinyl chloride 16.4 10 ug/L 20.00 82 10-251 0.9 20 Surrogate:4-8romotluorobenzene 51.9 U91L 50.00 104 74-126 Surrogate: Dibromofluoromethane 53.2 U91L 50.00 106 75-127 Surrogate: Toluene-d8 46.9 ug/L 50.00 94 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Chartotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 13 of 24 I S M I Full -Service al solution 8 Environmental solutions taea�iawaa nQ Level II QC Report 8114/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GUMS - Quality Control Analyte Batch P7H0007 - 625 Reporting Result Limit Units Prism Work Order: 7070509 Time Submitted: 7/31/2017 12:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P71-10007-131-Ki) Prepared & Analyzed: 08/01/17 1,2,4-Tdchlorobenzene BRL 10 ug/L 1,2-Dichlorobenzene BRL 10 ug/L 1,2-Dipheny1hydrazine (as Azobenzene) BRL 10 ug/L 1,3-Dichlorobenzene BRL 10 ug/L 1,4-Dichlorobenzene BRL 10 ug/L 2,4,6-Trichlorophenol BRL 10 ug/L 2,4-Dichlorophenol BRL 10 ug/L 2 4-Dimethylphenol BRL 10 ug1L 2,4-Dinitrophenol BRL 10 ug/L 2,4-Dinitrotoluene BRL 10 ug1L 2,6-Dinitrotoluene BRL 10 ug/L 2-Chloronaphthalene BRL 10 ug1L 2-Chlorophenol BRL 10 ug/L 2-Nitrophenol BRL 10 ug/L 3,3'-Dichlorobenzidine BRL 10 ug/L 4,6-Dinitro-2-methylphenol BRL 10 ug/L 4-Bromophenyl phenyl ether BRL 10 ug/L 4-Chloro-3-methylphenol BRL 10 ug/L 4-Chlorophenyl phenyl ether BRL 10 uglL 4-Nitrophenol BRL 50 ug/L Acenaphthene BRL 10 uglL Acenaphthylene BRL 10 ug/L Anthracene BRL 10 ug1L Benzidine BRL 100 ug)L Benzo(a)anthracene BRL 10 ug/L Benzo(a)pyrene BRL 10 ug/L Benzo(b)fluoranthene BRL 10 ug/L Benzo(g,h,i)perylene BRL 10 ug/L Benzo(k)fluoranthene BRL 10 ug/L bis(2-Chloroethoxy)methane BRL 10 ug/L Bis(2-Chloroethyl)ether BRL 10 ug/L Bis(2-chloroisopropyl)ether BRL 10 uglL Bis(2-Ethylhexyl)phthalate BRL 10 ug/L Butyl benzyl phthalate BRL 10 ug/L Chrysene BRL 10 ug/L Dibenzo(a,h)anthracene BRL 10 ug/L Diethyl phthalate BRL 10 ug/L Dimethyl phthalate BRL 10 ug1L Di-n-butyl phthalate BRL 10 ug/L Di-n-octyl phthalate BRL 10 ug/L Fluoranthene BRL 10 uglL Fluorene BRL 10 ug/L Hexachlorobenzene BRL 10 ug/L Hexachlorobutadiene BRL 10 ug1L Hexachlorocyclopentadiene BRL 10 ug1L Hexachloroethene BRL 10 uglL This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-800/529-6364 - Fax: 70415264409 Page 14 of 24 Full -Service Ma! ical 8 M I �` 6U']R Environmental Solutions ��JueauamEs me Level II QC Report 8/14117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GCIMS - Quality Control Analyte Batch P71-10007 - 625 Reporting Result Limit Unks Prism Work Order: 7070509 Time Submitted: 7/31/2017 12:45:0013M Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P7H0007-BLK1) Prepared & Analyzed: 08/01/17 Indeno(1,2,3-cd)pyrene BRL 10 uglL Isophorone BRL 10 ug/L Naphthalene BRL 10 ug/L Nitrobenzene BRL 10 ug1L N-Nitrosodimethylamine BRL 10 ug/L N-Nitroso-di-n-propylamine BRL 10 ug1L N-Nitrosodiphenylamine BRL 10 ug/L Pentachlorophenol BRL 10 ug/L Phenanthrene BRL 10 ug/L Phenot BRL 10 uglL Pyrene BRL 10 ug/L Surrogate:2,4,6-Tribromophenol 74.5 ug/L 100.0 74 31-144 Surrogate:2-Fluorobiphenyl 37.3 ug/L 50.00 75 49-118 Surrogate:2-Fluorophenol 50.9 U91L 100.0 51 22-84 Surrogate: Nitrobenzene-d 35.7 ug/L 50.00 71 43-123 Surrogate: Phenol45 34.4 U91L 100.0 34 10-63 Surrogate: Terphenyl-d 14 46.8 ug/L 50.00 94 49-151 LCS (P71-10007-BS1) Prepared & Analyzed: 08/01/17 1,2,4-Tdchlorobenzene 58.4 10 ug1L 100.0 58 44-142 1,2-Dichlorobenzene 58.0 10 ug1L 100.0 58 32-129 1,2-❑iphenylhydra7ine (as Azobenzene) 78.0 10 ug1L 100.0 78 40-135 1,3-Dichlorobenzene SCIB 10 ug1L 100.0 55 20-124 1,4-Dichlorobenzene 55.3 10 um 100.0 55 20-124 2,4,6-Tdchlorophenol 67.9 10 ug/L 100.0 68 37-144 2,4-Dichlorophenol 67.6 10 uglL 100.0 68 39-135 2,4-Dimethylphenol 95.4 10 ug1L 100.0 95 32-119 2,4-Dinitrophenol 47.6 10 ug/L 100.0 48 10-191 2,4-Dinitrotoluene 76.0 10 ug/L 100.0 76 39-139 2,6-Dinitrotoluene 82.3 10 ug/L 100.0 82 50-158 2-Chloronaphthalene 70.0 10 ug/L 100.0 70 60-118 2-Chlorophenol 71.5 10 ug/L 100.0 72 23-134 2-Nitrophenol 65.6 10 ug/L 100.0 66 29-182 3,T-Dichlorobenzidine 84.6 10 ug/L 100.0 85 10-262 4,6-Dinitro-2-methytphenol 59.5 10 ug/L 100.0 59 10-181 4-Bromophenyl phenyl ether 71.9 10 ug/L 100.0 72 53-127 4-Chloro-3-methytphenol 76.2 10 ug/L 100.0 76 22-147 4-Chlorophenyl phenyl ether 66.8 10 ug/L 100.0 67 25-158 4-Nitrophenol 35.2 50 ug1L 100.0 35 10-132 Acenaphthene 70.1 10 ug1L 100.0 70 47-145 Acenaphthylene 72.0 10 ug1L 100.0 72 33-145 Anthracene 74.5 10 ug1L 100.0 74 27-133 Benzidine 54.1 100 ug1L 100.0 54 15-150 Benzo(a)anthracene 72.9 10 UgIL 100.0 73 33-143 Benzo(a)pyrene 76.4 10 ug1L 100.0 76 17-163 Benzo(b)fluoranthene 74.6 10 ug/L 100.0 75 24-159 Benzo(g,h,i)perylene 74.5 10 ug/L 100.0 74 10-219 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704152&4409 Page 15 of 24 FunService Analytical & Envisronmental Solutions '7c�eowatowea we Level II QC Report 8114/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P71HI0007 - 625 Reporting Result Limit Units Prism Work Order: 7070509 Time Submitted: 7/31/2017 12:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P71-10007-131SI) Prepared 8 Analyzed: 08/01/17 _ Senzo(k)fluoranthene 70A 10 ug/L 100.0 70 11-162 bis(2-Chloroethoxy)methane 65.6 10 ug1L 100.0 66 33-184 Bis(2-Chloroethyl)ether 50.2 10 ug/L 100.0 50 12-158 Bis(2-chloroisopropyl)ether 60.9 10 ug1L 100.0 61 36-166 Bis(2-Ethylhexyl)phthalate 74.0 10 ug/L 100.0 74 10-158 Butyl benzyi phthalate 55.2 10 ug/L 100.0 55 10-152 Chrysene 73.7 10 ug1L 100.0 74 17-168 Dibenzo(a,h)anthracene 53.7 10 ug/L 100.0 54 10-227 Diethyl phthalate 53.0 10 uglL 100.0 53 10-114 Dimethyl phthalate 24.3 10 ug/L 100.0 24 10-112 Di-n-butyl phthalate 70.4 10 ug1L 100.0 70 10-118 Di-n-octyl phthalate 74.1 10 ug1L 100.0 74 10-146 Fluoranthene 74.7 10 ug/L 100.0 75 26-137 Fluorene 68.6 10 ug/L 100.0 69 59-121 Hexachlorobenzene 78.3 10 ug1L 100.0 78 10-152 Hexachlorobutadiene 55.7 10 ug/L 100.0 56 24-116 Hexachlorocyclopentadiene 61.7 10 ug/L 100.0 62 32-117 Hexachloroethane 51.0 10 ug/L 100.0 51 40-113 Indeno(1,2,3-cd)pyre ne 93.9 10 ug/L 100.0 94 10-171 Isophorone 72.3 10 ug1L 100.0 72 21-196 Naphthalene 63.9 10 ug11- 100.0 64 21-133 Nitrobenzene 62.5 10 ug1L 100.0 63 35-180 N-Nitrosodimethylamine 53.6 10 ug/L 100.0 54 10-119 N-Nitroso-dial-propylamine 71.2 10 ug1L 100.0 71 10-230 N-Nitrosodiphenylamine 92.3 10 ug/L 100.0 92 69-152 Pentachlorophenol 79.7 10 ug1L 100.0 80 14-176 Phenanthrene 74.4 10 ug1L 100.0 74 54-120 Phenol 40.1 10 ug1L 100.0 40 10-112 Pyrene 70.2 10 uglL 100.0 70 52-115 Surrogate: 2,4,6-Tribromophenol 75.4 ug/L 100.0 75 31-144 Surrogate:2-Fluorobrphenyl 37.0 ug/L 50.00 74 49-118 Surrogate:2-Fluorophenol 47.7 uglL 100.0 48 22-84 Surrogate: Ndrubenzene-d5 33.4 uglL 50.00 67 43-123 Surrogate: Phenol-d5 33,1 ug/L 100.0 33 10-63 Surrogate. Terphenyl-d14 46.3 ug/L 50.00 93 49-151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704IS29-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 r Page 16 of 24 � Level II QC Report EIc...." R I S n A ( Full -Service Analytical d 8/14/17 V' Environmental Solutiona ��/i.sna„owes Mc. GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #6 Charlotte, NC 28273 5emivolatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 7070509 Time Submitted: 7/31/2017 12:45:OOPM Reporting Spike Source %nREC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7H0007 - 625 LCS Dup (P71-10007-IRSD1) Prepared 8 Analyzed: 08/01/17 1,24-Trichlombenzene 55.4 10 ug/L 100.0 55 44-142 5 20 1,2-Dichlorobenzene 54.1 10 ug/L 100.0 54 32-129 7 20 1, 2-Diphenylhydrazine (as Azobenzene) 78.7 10 ug/L 100.0 79 40-135 0.9 20 1,3-Dichlorobenzene 51.3 10 ug/L 100.0 51 20-124 6 20 1,4-Dichlorobenzene 52.2 10 ug/L 100.0 52 20-124 6 20 2,4,6-Trichlorophenol 72.0 10 ug1L 100.0 72 37-144 6 20 2,4-Dichlorophenol 67.9 10 ug/L 100.0 68 39-135 0,5 20 2,4-Dimethylphenol 93.5 10 ug/L 100.0 93 32-119 2 20 2,4-Dinitrophenol 43.9 10 ug1L 100.0 44 10-191 a 20 2,4-Dinitrotoluene 77.0 10 ug/L 100.0 77 39-139 1 20 2,6-Dinitrotoluene 84.1 10 ug/L 100.0 84 50-158 2 20 2-Chloronaphthalene 68.9 10 ug/L 100.0 69 60-118 2 20 2-Chloraphenol 70.1 10 ug/L 100.0 70 23-134 2 20 2-Nitrophenol $7.6 10 ug/L 100.0 68 29-182 3 20 3,3'-Dichlorobenzidine 86.0 10 ug/L 100.0 86 10-262 2 20 4,6-Dinitro-2-methylphenol 62.8 10 ug1L 100.0 63 10-181 6 20 4-Bromophenyl phenyl ether 73.2 10 ug/L 100.0 73 53-127 2 20 4-Chloro-3-methylphenol 74.6 10 ug/L 100.0 75 22-147 2 20 4-Chlorophenyl phenyl ether 69.0 10 ug/L 100.0 69 25-158 3 20 4-Nitrophenol 36.7 50 ug/L 100.0 37 10-132 4 20 Acenaphthene 70.2 10 ug/L 10D.0 70 47-145 0.06 20 Acenaphthylene 72.3 10 ug1L 100.0 72 33-145 0.5 20 Anlhracene 76.7 10 uglL 100.0 77 27-133 3 20 Benzidine 53.2 100 uglL 100.0 53 15-150 2 20 Benzo(a)anthracene 73.8 10 ug/L 100.0 74 33-143 1 20 Benzo(a)pyrene 77.0 10 uglL 100.0 77 17-163 0.8 20 Benzo(b)iluoranthene 75.6 10 ug/L 100.0 76 24-159 1 20 Benzo(g,h,i)perylene 74.7 10 ug/L 100.0 75 10-219 0.2 20 Benzo(k)ftuoranthene 71.3 10 ug/L 100.0 71 11-162 1 20 bis(2-Chloroethoxy)methane 65.4 10 ug/L 100.0 65 33-1B4 0.4 20 Bis(2-Chloroethyi)ether 59.0 10 ug/L 100.0 59 12-158 16 20 Bis(2-chloroisopmpyl)ether 57.8 10 ug/L 100.0 58 36-166 5 20 Bis(2-Ethylhexyl)phthala1e 75.4 10 ug/L 100.0 75 10-158 2 20 Butyl benzyl phthalate 58.3 10 ug1L 100.0 58 10-152 6 20 Chrysene 74.4 10 ug/L 100.0 74 17-168 0.9 20 Dibenzo(a,h)anthracene 52.8 10 ug/L 100.0 53 10-227 2 20 Diethyl phthalate 57.3 10 ug1L 100.0 57 10-114 8 20 Dimethyl phthalate 28.2 10 ug/L 100.0 28 10-112 15 20 Di-r butyl phthalate 71.8 10 ug/L 100.0 72 10-118 2 20 ❑i-n-octyl phthalate 74.6 10 ug/L 100.0 75 10-146 0.9 20 Fluoranthene 76.6 10 ug/L 100.0 77 26-137 2 20 Fluorene 69.9 10 ug/L 100.0 70 59-121 2 20 Hexachlorobenzene 78.5 10 ug/L 100.0 79 10-152 0.3 20 Hexachlorobutadiene 51.7 10 ug/L 100.0 52 24-116 7 20 Hexachlorocyclopentadiene 57.8 10 ug/L 100.0 58 32-117 6 20 Hexachloroethane 46.4 10 ug/L 100.0 46 40-113 10 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.D. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-80015294364 - Fax: 7041525.0409 Page 17 of 24 Level II QC Report Full -Service Analytical8/14/17�PRISM I Environmental Solutions ',lueoeur>�a iwc GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Prism Work Order: 7070509 Attn: Dave Mazorra Time Submitted: 7/31/2017 12.45:00PM 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P71I0007 - 625 LCS Dup (P7H0007-BSD1) Prepared &Analyzed: 08/01/17 Indeno(1,2,3-cd)pyrene 93.7 10 ug/L 100.0 94 10-171 0.2 20 Isophorone 72.0 10 ug/L 100.0 72 21-196 0.4 20 Naphthalene 62.1 10 ug/L 100.0 62 21-133 3 20 Nitrobenzene 60.7 10 ug/L 100,0 61 35-180 3 20 N-Nitrosodimethylamine 51.1 10 ug/L 100.0 51 10-119 5 20 N-Nitroso-di-n-propylamine 69.3 10 uglL 100.0 69 10-230 3 20 N-Nitrosodiphenylamine 93.4 10 ug/L 100.0 93 69-152 1 20 Pentachlorophenol 76.8 10 ug/L 100.0 77 14-176 4 20 Phenanthrene 76.3 10 ug/L 100.0 76 54-120 2 20 Phenol 38.6 10 ug/L 100.0 39 10-112 4 20 Pyrene 72.1 10 ug/L 100.0 72 52-115 3 20 Surrogate: 2,4,6-Tribromophenol 80.7 uglL 100.0 81 31-144 Surrogate:2-Fluorobiphenyl 37.0 u9k 50,00 74 49-118 Surrogate:2-Fluorophenol 46.6 ug/L 100.0 47 22-84 Surrogate: Nitrobenzene-d5 32.9 ug/L 50.00 66 43-123 Surrogate: Phenol-15 32.1 uglL 100.0 32 10-63 Surrogate: Terphenyl-&4 46.9 uglL 50.00 94 49-151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 5pringbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 18 of 24 Full- d� I S n /� I Environmental al Solutions 8 ® ' V' Environmental Solutions ��''ueorwon�s Nc GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Organochlorine Pesticides by GClECD - Quality Control Analyte Batch P7H0031 - 608 Reporting Result Limit Units Level It QC Report 8114/17 Prism Work Order: 7070509 Time Submitted: 7/31/2017 12:45.00PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P7H0031-BLK1) Prepared: 08/02/17 Analyzed: 08/08/17 alpha-BHC BRL 0.050 ug1L . beta-BHC BRL 0.050 ug1L gamma-BHC BRL 0.050 ug1L delta-BHC BRL 0.050 ug1L Heptachlor BRL 0.050 ug1L Aldrin BRL 0.050 ug1L Heptachlor Epoxide BRL 0.050 ug1L trans -Chlordane BRL 0,050 ug1L Endosulfan I BRL 0.050 ug1L cis -Chlordane BRL 0,050 uglL Dieldrin BRL 0,050 ug1L 4,4'-DOE BRL 0.050 ug1L Endrin BRL 0.050 ug/L Endosulfan II BRL 0.050 ug1L 4,4'-DDD BRL 0.050 ug1L Endrin Aldehyde BRL 0.050 ug1L Endosulfan Sulfate BRL 0,050 ugiL 4,4'-DDT BRL 0.050 ug1L Endrin Ketone BRL 0,050 ug1L Methoxychlor BRL 0.050 uglL Chlordane BRL 0,50 ug1L Toxaphene BRL 0.50 ug1L Aroclor 1016 BRL 0,50 uglL Aroclor 1221 BRL 1.0 ug1L Aroclor 1232 BRL 0.50 ug1L Aroclor 1242 BRL 0.50 ug1L Aroclor 1248 BRL 0.50 ug1L Aroclor 1254 BRL 0.50 ug1L Aroclor 1260 BRL 0.5o ug1L Surrogate: 7etrachloro-m-xylene 0,568 ug/L 1.000 57 40-134 Surrogate: Decachlorobiphenyl 0.686 ug/L 1.000 69 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 70415294364 - Toll Free Number: 1-80015294364 - Fax: 70415254M9 Page 19 of 24 Level II QC Report AP R�SM Full -Service Anaiylical &8114/17 Environmental Solutions7 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Organochlorine Pesticides by GCIECD - Quality Control Prism Work Order: 7070509 Time Submitted: 7/31/2017 12:45:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7H0031 - 608 LCS (P7H0031-BSI) Prepared: 08/02/17 Analyzed: 08/08/17 alpha-BHC 0.768 0.050 ug/L 1.000 77 37-134 beta-BHC 0.719 0.050 ug/L 1.000 72 17-147 gamma-BHC 0.775 0.050 ug/L 1.000 77 32-127 delta-BHC 0.589 0.050 ug1L 1.000 59 19-140 Heptachlor 0.805 0.050 ug/L 1.000 80 34-111 Aldrin 0.728 0.050 ug/L 1,000 73 42-122 Heptachlor Epoxide 0.778 0.050 ug1L 1.000 78 37-142 trans -Chlordane 0.765 0.050 ug/L 1.000 76 45-119 Endosulfan 1 0.773 0.050 ug/L 1.000 77 45-153 cis -Chlordane 0.750 0.050 ug/L 1.000 75 45-119 Dieldrin 0.768 0.050 uglL 1.000 77 36-146 4.4'-DOE 0.750 0,050 ug/L 1,000 75 30-145 Endrin 0.833 0.050 ug/L 1.000 83 30-147 Endosulfan II 0.754 0.050 ug/L 1.000 75 10-202 4,4'-DDD 0.732 0.050 ug/L 1.000 73 31-141 Endrin Aldehyde 0.720 0.050 ug/L 1.000 72 68-139 Endosulfan Sulfate 0.711 0.050 ug/L 1.000 71 26-144 4,4'-DDT 0,768 0.050 ug1L 1.000 77 25-160 Endrin Ketone 0.724 0.050 ug/L 1.000 72 68-150 Methoxychlor 0.820 0.050 uWL 1.000 82 70-157 Surrogate: Tetrachloro-m-xylene 0.673 ug1L 1.000 67 40-134 Surrogate: Decachlorobiphenyl 0.485 ug/L 1.000 49 13-186 LCS (P7110031-13S2) Prepared: 08/02/17 Analyzed: 08/08/17 Chlordane 6.94 0.50 ug/L 10.00 69 50-150 Surrogate: Tetrachloro-m-xylene Surrogate: Decachlorobiphenyl 0.660 0.474 ug1L 1.000 66 40-134 ug1L 1,000 47 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc, 449 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704t52M364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 20 of 24 � Full -Service Anaiyticel 6 �PIR I ! Y /A1 � i Environmental Solutions `'VL.BCMATMIF& n Level II QC Report 8/14/17 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Organochlorine Pesticides by GCIECD - Quality Control Analyte Batch P71-10031 - 608 Reporting Result Limit Units Prism Work Order: 7070509 Time Submitted: 7/31/2017 12:45:00PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P7H0031-BS3) Prepared: 08/02/17 Analyzed: 08/08/17 Toxaphene 6.61 0.50 ug1L 10.00 66 41-126 Surrogate: Tetrachloro-m-xylene 0.644 ug/L 1.000 64 40-134 Surrogate: Decachlorobiphenyl 0.465 ug/L 1.000 47 13-196 LCS (P7H0031-13S4) Prepared: 08/02/17 Analyzed: 08/08/17 Aroclor 1016 6.11 0.50 ug/L 10.00 61 50-114 Aroclor 1260 5,93 0.50 ug/L 10.00 59 10-127 Surrogate: Tetrachloro-m-xylene 0.553 ug/L 1.000 55 40-134 Surrogate: Decachlorobiphenyl 0.579 ug/L 1.000 58 13-186 LCS Dup (P71H10031-13SD7) Prepared: 08/02/17 Analyzed: 08/08/17 alpha-BHC 0.718 0.050 ug1L 1.000 72 37-134 7 20 beta-BHC 0.690 0.050 ug1L 1.000 69 17-147 4 20 gamma-BHC 0.728 0.050 ug/L 1.000 73 32-127 6 20 delta-BHC 0,569 0.050 ug/L 1.000 57 19-140 4 20 Heptachlor 0.776 0.050 ug/L 1.000 78 34-111 4 20 Aldrin 0.705 0.050 ug/L 1.000 71 42-122 3 20 Heptachlor Epoxide 0.727 0.050 ug1L 1.000 73 37-142 7 20 trans -Chlordane 0.722 0.050 ug/L 1.000 72 45-119 6 20 Endosulfan 1 0.727 0.050 ug1L 1.000 73 45-153 6 20 cis -Chlordane 0.712 0.050 ug/L 1.000 71 45-119 5 20 Dieldrin 0.718 0.050 ug/L 1.000 72 36-146 7 20 4,4'-DDE 0.705 0.050 ug1L 1.000 71 30-145 6 20 Endrin 0.787 0.050 ug1L 1.000 79 30-147 6 20 Endosultan It 0.726 0.050 uglL 1.000 73 10-202 4 20 4,4'-DDD 0.700 0.050 ug/L L000 70 31-141 4 20 Endrin Aldehyde 0.700 0.050 ug1L 1.000 70 68-139 3 20 Endosulfan Sulfate 0.699 0,050 ug1L 1.000 70 26-144 2 20 4,4'-DDT 0.748 0.050 ugJL 1.000 75 25-160 3 20 Endrin Ketone 0.713 0.050 uglL 1.000 71 68-150 1 20 Methoxychlor 0.809 0.050 ug/L 1.000 81 70-157 1 20 Surrogate: Tetrachloro-m-xylene 0,642 ug/L 1.000 64 40-f34 Surrogate: Decachlorobiphenyl 0.627 ug/L f.000 63 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704152"364 - Toll Free Number: 1.8001529-6364 - Fax: 704/525-M9 Page 21 of 24 AhRISM I Fun -Service Analytical 8 Environmental Solutions �'7uuaawiawes, we Level II QC Report 8114117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Total Metals - Quality Control Prism Work Order: 7070569 Time Submitted: 7/31/2017 12:45:OOPM Reporting Spike Source %REC RPD Analyse Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7H0091 - 200.7 Blank (1371-10091-13LKi) Prepared: 08/04/17 Analyzed: 08/07/17 Copper BRL 0.010 mg1L Lead BRL 0.0050 mglL Zinc BRL 0,030 mg/L LCS (P71-10091-13SI) Prepared: 08/04/17 Analyzed: 08/07/17 Copper 0.258 0.010 mg/L 0.2500 103 85-115 Lead 0,262 0.0050 mg/L 0.2500 105 85-115 Zinc 0.266 0.030 mg/L 0.2500 106 85-115 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 22 of 24 PRISM Full -Service cel a Environmental al SaluSclutlpns 5%waaumA FI aw Level II QC Report 8114117 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Monthly SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 General Chemistry parameters - Quality Control Analyte Reporting Result Limit Units Prism Work Order: 7070509 Time Submitted: 7/31/2017 12:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P7G0485 - NO PREP LCS (1P7G0465-BS1) Prepared & Analyzed: 07/31/17 pH 6.89 pH Units 6,880 100 98.5-101.5 HT Batch P71-10104 - NO PREP Blank (P7H0104-8LK1) Prepared & Analyzed: 08/04/17 Total Suspended Solids BRL 5,0 mg/L LCS (P7140104-13S1) Prepared & Analyzed: 08/04/17 Total Suspended Solids 480 5.0 mg/L 477.0 102 90-110 Batch P71-10154 - NO PREP Blank (P7H0154-BLK1) Prepared & Analyzed: 08/08/17 Oil & Grease (SGT-HEM) BRL 5.0 mg/L Sample Extraction Data Prep Method: 608 Lab Number Batch Initial Final DatelTme 7070509-01 P7H0031 980 mL 10 mL 08102/17 8:25 7070509-02 P71-10031 910 mL 10 mL 08/02/17 8:25 Prep Method: 625 Lab Number Batch Initial Final Datemme 7070509-01 P71-10007 960 mL 1 mL 08/01/17 8:40 7070509-02 1371-10007 950 mL 1 mL 08/01/17 8:40 Prep Method: 200.7 Lab Number Batch Initial Final DatelTime 7070509-01 P71-10091 50 mL 50 mL 081o4117 8:10 7070509-02 P71-10091 50 mL 50 mL 08/04/17 8:10 Prep Method: 624 Lab Number Batch Initial Final DatelYme 7070509-01 P71-10066 10 mL 10 mL 08/02117 9:02 7070509-02 P71-10066 10 mL 10 mL 08/02117 9:02 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. "9 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-0364 - Toll Free Number: 1-800152"364 - Fax: 7041525-0409 Page 23 7 24 ff Pull -Service Analytical & Environmental Swufi )n5 i.nWr{.n'rI.xnFrs,;kk:. 449 Springbrook Road • Charlotte, INC 28217 Prone 7041529-6364 Fa 7041525.040 Client Company Name: Report TolContact Name: rnnk- Reporting Address: -71Q 3 -J i,z h 1Z CHAIN OF CUSTODY RECORD PAGE OF -�— QUOTE 0 TO ENSURE PROPER BILLING,. Project Name: RA A � . 5-ki Short Hold Analysis: '(Ye§fCX@W UST Prot: (Yes) "Please ATTACH any project specific reporting (QC LEVEL I II III IV) provisions and/or QC Requirements Invoice To: Address: Phone: D-V a Fax (Yes) (No): Purchase Order No./Billing Reference 12 TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Email Address: �P--4 e-,s �I . C0 wt Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC h Work dust Be EDD Type: PDF Excel�Other "Working Days" l7 6-9 Days ❑ Standard 10 days ❑ Rush re Site Location Name: act- . 7'ALA rS Samples received after 14:00 will be processed next business day. Sc OTHER NIA Site Location Physical Address: lj j`+ `i!VIt,. tee e_J Turnaround time Is based on business days, excluding weekends and holidays. Water Chlorinated: YES NO A tSES REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES_ NO TIME MATRIX SAMPLE CONTAINER ANALYSIS R UEST PRISM CLIENT SAMPLE DESCRIPTION DATE COLLECTED COLLECTED MILITARY (SOIL, WATER OR PRESERVA- TIVES REMARKS � 1 NO 'TYPE HOURS SLUDGE) SEE BELOW NO SIZE S Z � 0; t M40 Sampler's Signature Sampled 8y (Print Name) �' I/pQ1/ Affiliation Upon relingy'shing, this Chain of Custody Is your authorization for Prism proceed with the analyses as requested above. Any changes must be PRISM USE ONLY submitted fi riting to the Prism Project Manager. There will be charges any changes after aDaLyses have been initialized. ellnquis By; sl na a Received y: nature ate ..9 Mary. ours Additional Comments: 51te Arr,4al 71me T 1_,S t Refinquis ed Ig ture) Received By: Slgnatur to - Site pepailure'lime Field Tech Fee Relinquished By: (Signature) Received La prat rfeS�Bv: 4 Date r Irism yCi- 1 l J ' Mileage: Method of Shipment: NOT : ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY S FOR TRANSPORTATION TO THE LABORAT RY. CQC roue O.i.F S PLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY. a ❑ Fed Ex ❑UPS Hand -delivered U Prism FIeld Service U Olher NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RGRA: CERCLA LANDFILL OTHER: FOR TERMS & CONDITIONS ).NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC O SC ❑ NC 0 SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC I ❑ NC ❑ SC n n ❑ ❑ ❑ ❑ ❑ ❑ ...�..�....�., ....-- ----o A - A -. k-- r - r+l— r--- r_l— 0 - IDI—fl- TI n TRflnn-I inarl r:nn %/nA c 1/nlafila nrnaninc Annhi¢Ic 17Rrn HRRrt RnarR1 r Monthly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG030663 FACILITY NAME Select Stainless Products LLC COUNTY Mecklenburg PERSON COLLECTING SAMPLES David Mazorra LABORATORY Lab Cert. # Comments on sample collection or analysis: No Flow Part A: Stormwater Benchmarks and Monitoring Results June 30, 2017 SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly) June (month) DISCHARGJL19TO CLASS ❑ORW ❑HQW []Trout❑PNA RECENE ®Zero -flaw ❑Water Supply ❑SA jUL O i 20V ❑Other CENTRAL FILISE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTION ® No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Nan -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics, Benchmarks =-_> _ - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SW-1 SW-2 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." David R. Mazorra PE Name (Print name) Senior Environmental Engineer Title 30 (Signature) (Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part 0: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ® No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 - 9.0 SU Sw-1 Sw-z Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note; ff you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on final and one copy of this MR, including all "No Discharge" reports, within 30 days of re Iptof the lob results or at endof monitoring eriod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware that there aya significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Z-,Z//Z-- 0 1 (Signature of Pe mittee) (Dat Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 ism pies, INC Full -Service Analytical & Environmental Solutions GTA (Geo-Tech. Assoc. Inc.) Charlotte Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Semi -Annual SW Lab Submittal Date: 12108/2016 Prism Work Order: 6120191 Case Narrative 12/21 /2016 RCJVE) JAN 2 5 2017 CENTRAL Fl oWR SECTION This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. G� Cara C. Rusmisell Project Manager Data Qualifiers Key Reference: Reviewed By Cara C. Rusmisell Project Manager HT Sample received and analyzed outside of the hold time. OG HEM O&G is less than the reporting limit, therefore TPH (SGT-HEM) is less than the reporting limit. Sample not extracted for TPH (SGT-HEM). BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J_ This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704162"409 Page 1 of 20 I h 1 ^"3 Pull -Service Analytical & ZP R ISM I Environmental Solutions Sample Receipt Summary 12/21 /2016 Prism Work Order: 6120191 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received SW-2 6120191-01 Water 12/05/16 12/08/16 Samples were received in good condition at 3.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 L Page 2 of 20 nAP.Ra � Full -Service Analytical & ISM I Environmental Solutions 4� Laboratory Report 12121 /2016 GTA (Geo-Tech. Assoc. Inc.) Charlotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Sample Matrix: Water Client Sample ID: SW-2 Prism Sample ID: 6120191-01 Prism Work Order: 6120191 Time Collected: 12/05/16 12:00 Time Submitted: 12/08/16 16:05 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime ID General Chemistry Parameters Oil & Grease (SGT-HEM) BRLor, mg1L 5.0 1.1 1 '1664B 12121/16 11:10 TJY P61-0356 pH 6.1 HT pH Units 1 'SM4500-H B 1219/16 13:35 EGG PSLO187 Total Suspended Solids 4.4 mg1L 3A 0.80 1 "SM2540 D 12/12116 12.17 SLS P61_0214 Organochlorine Pesticides by GCIECD alpha-BHC BRL ug1L 0.050 0.012 1 '608 12/13/16 14:24 JMC P6L0205 beta-BHC BRL ug1L 0.050 0.019 1 '608 12/13/16 14:24 JMC P61_0205 gamma-BHC BRL ug1L 0.050 0,013 1 '608 12/13/16 14:24 JMC P61_0205 delta-BHC BRL ug1L 0.050 0.017 1 608 12/13/16 14:24 JMC P61-0205 Heptachlor BRL ug1L 0.050 0.015 1 1608 QJ13i16 14:24 JMC P6L0205 Aldan BRL ug1L 0.050 0.015 1 '608 12/13/16 14:24 JMC P61_0205 Heptachlor Epoxide BRL ug1L 0.050 0.018 1 606 12/13/16 14:24 JMC P61_0205 trans -Chlordane BRL ug1L 0.050 0.019 1 '6D8 12/13/16 14:24 JMC P61-0205 Endosulfan I BRL ug1L 0.050 0.019 1 '608 12/13/16 14:24 JMC P61_0205 cis -Chlordane BRL ug1L 0.050 0.018 1 '608 12/13/16 14:24 JMC P61_0205 Dieldrin BRL ug1L 0.050 0.022 1 '608 12/13/16 14:24 JMC P61_0205 4,4'-DDE BRL ug1L 0.050 0.028 1 '6D8 12/13/16 1424 JMC P61_0205 Endrin BRL ug1L 0.050 0.020 1 '608 12/13/16 14:24 JMC P61_0205 Endosulfan II BRL ug1L 0.050 0.025 1 '608 12/13/16 14:24 JMC 1361-0205 4,4'-DDD BRL ug1L 0.050 0.028 1 '608 12/13/16 14:24 JMC P61_0205 Endrin Aldehyde BRL ug1L 0.050 0.027 1 '608 12/13/16 14-24 JMC P61-0205 Endosulfan Sutfate BRL ug1L 0.050 0.027 1 '608 12/13/16 14:24 JMC P61_0205 4,4'-DDT BRL ug1L 0.050 0.027 1 *608 12/13/16 14:24 JMC P61_0205 Endrin Ketone BRL ug1L 0.050 0.028 1 '608 12/13/16 14:24 JMC 1361_0205 Methoxychlor BRL ug1L 0.050 0.033 1 '608 12/13/16 14724 JMC P61-0205 Chlordane BRL ug1L 0.50 0.094 1 '608 12/13/16 14:24 JMC P61-0205 Toxaphene BRL ug1L 0.50 0.32 1 *608 12/13/16 14:24 JMC P61_0205 Arodor 1016 BRL ug1L 0.50 0.24 1 '608 12/13/16 14:24 JMC P6L0205 Arodor 1221 BRL ug1L 1.0 0.11 1 '608 12/13/16 14:24 JMC P6L0205 Arodor 1232 BRL ug1L 0.50 0.16 1 '6Q8 12/13/16 14:24 JMC P6LD205 Arodor 1242 BRL ug1L 0.50 0.14 1 '608 12/13/16 14:24 JMC P6L0205 Arodor 1248 BRL ug1L 0.50 0.14 1 '608 12113/16 14:24 JMC P61_0205 Arodor 1254 BRL ug1L 0.50 0.16 1 '608 12113/16 14:24 JMC P61_0205 Arodor 1260 BRL ug1L 0.50 0.30 1 '608 12113/16 14:24 JMC P61_0205 Surrogate Recovery Control Limits Tetrachloro-m-xylene 76 % 40-134 Decachlorobiphenyl 70 % 13-186 Semivolatile Organic Compounds by GUMS 1,2,4-Trichlorobenzene BRL ug1L 10 1.5 1 '625 12112116 20:28 JMV P61_01198 1,2-Dichlorobenzene BRL ug1L 10 1.4 1 '625 12/12/16 20:28 JMV P61-0198 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 3 of 2O I � Laboratory Report /_11 ��� �Full-Service Ana3yticai 8L.....JR I � �/ Environmental Solutions 12121/2016 '7ueowmw� 1H GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Client Sample ID: SW-2 Attn: Dave Mazorra Prism Sample ID: 6120191-01 710 Peninsula Lane, #B Prism Work Order: 6120191 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 12/05/16 12:00 Time Submitted: 12/08/16 16:05 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,2-Diphenylhydrazine (as Azobenzene) BRL ug/L 10 2.9 1 *625 12/12/16 20:23 JMV P61_0198 1,3-Dichlorobenzene BRL ug1L 10 1.3 1 *625 12/12/16 20:28 JMV P6L0198 1,4-Dichlorobenzene BRL ug1L 10 1.4 1 '625 12/12/16 20:28 JMV P61_0198 2,4,6-Tdchlorophenol BRL ug/L 10 1.8 1 *625 12/12/16 20:28 JMV P61_0198 2,4-Dichicrophenol BRL ug1L 10 1.6 1 '625 12/12/16 20:28 JMV P6L0198 2,4-Dimethylphenol BRL ug/L 10 2.1 1 *625 12/12/16 20:28 JMV P61_0198 2,4-Dinitrophenol BRL ug/L 10 1.2 1 '625 12/12/16 20:28 JMV P61_0198 2,4-Dinitrotoluene BRL ug/L 10 2.9 1 *625 12/12/16 20-28 JMV P61-0198 2,6-Dinitrotoluene BRL ug1L 10 2.9 1 *625 12/12/16 20:28 JMV P61_0198 2-Chloronaphthelene BRL ug1L 10 2.3 1 *625 12/12/16 20:28 JMV P6L0198 2-Chlorophenol BRL ug1L 10 1.1 1 '625 12/12/16 20:28 JMV P6L0198 2-Nitrophenol BRL ug1L 10 1.4 1 *625 12/12/16 20:28 JMV P61_0198 3,3'-Dichlorobenzidine BRL ug1L 10 2.8 1 *625 12/12/16 20:28 JMV P61_0198 4,6-Dinitro-2-methylphenol BRL ug1L 10 1.9 1 '625 12/12/16 20:28 JMV P61_0198 4-Bromophenyl phenyl ether BRL ug1L 10 3.2 1 *625 12/12/16 20:28 JMV P61_0198 4-Chloro-3-methylphenol BRL ug1L 10 2.3 1 *625 12/12/16 20:28 JMV P61_0198 4-Chlorophenyl phenyl ether BRL ug1L 10 2.2 1 *625 12/12/16 20:28 JMV P61_0198 4-Nitrophenol BRL ug1L 50 1.7 1 *625 12/12/16 20:28 JMV P6L0198 Acenaphthene BRL ug/L 10 2.3 1 '625 12/12/16 20:26 JMV P61_0198 Acenaphthylene BRL ug1L 10 2.3 1 *625 12/12/16 20:28 JMV P61-0198 Anthracene BRL ug1L 10 3.2 1 625 12/12/16 20:28 JMV P61-0198 Benzidine BRL ug1L 100 14 1 *625 12/12/16 20:28 JMV P61_0198 Benzo(a)anthracene BRL ug/L 10 3.1 1 '625 12/12/16 20:28 JMV P61_0198 Benzo(a)pyrene BRL ug1L 10 3.6 1 *625 12/12/16 20:28 JMV P61_0198 Benzo(b)fluoranthene BRL ug1L 10 3.5 1 '625 12/12/16 20:28 JMV P61_0198 Benzo(g,hJ)perylene BRL ug/L 10 3,5 1 *625 12/12/16 20:28 JMV PBLO198 Benzo(k)fluoranthene BRL ug/L 10 3.8 1 '625 12/12/16 20:28 JMV P6L0198 bis(2-Chloroethoxy)methane BRL ugIL 10 1.8 1 *625 12/12116 20:28 JMV P61_0198 Bis(2-Chloroethyl)ether BRL ug/L 10 1.6 1 '625 12/12/16 20:28 JMV P61-0198 Bis(2-chloroisopropygether BRL ug1L 10 1.7 1 *625 12/12/16 20:28 JMV P6L0198 Bis(2-Ethylhexyl)phthalate BRL uglL 10 3.1 1 '625 12/12116 20:28 JMV P61_0198 Butyl benzyl phthalate BRL ugJL 10 2.6 1 *625 12/12/16 20:2a JMV P61_01198 Chrysene BRL ug1L 10 3.4 1 *625 12/12/16 20:28 JMV P61_0198 Dibenzo(a,h)anthracene BRL ug/L 10 3.4 1 *625 12/12/16 20:28 JMV 1361-0198 Diethyl phthalate BRL ug/L 10 2.3 1 *625 12112/16 20:28 JMV P61_0198 Dimethyl phthalate BRL ugIL t0 1.5 1 '625 12112/16 20:28 JMV P61-0198 Di-n-butyl phthalate BRL ug/L 10 3A 1 *625 12/12/16 20:28 JMV P60198 Di-n-octyl phthalate BRL ug1L 10 3.6 1 *625 12/12/16 20:28 JMV P61_0198 Fluoranthene BRL ug1L 10 3.5 1 *625 12/12/16 20:28 JMV P61_0198 Fluorene BRL ugIL 10 2.8 1 *625 12J12J16 2U8 JMV P61_0198 Hexachlorobenzene BRL ug/L 10 2.5 1 '625 12/12/16 20:28 JMV P61_0198 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 5pringbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone. 704/529.6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 4 of 20 f�' �Full-Service Analytical 8 Laboratory Report IS M I environmental Solutions 12/21/2016 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Client Sample ID: SW-2 Attn: Dave Mazorra Prism Sample ID: 6120191-01 710 Peninsula Lane, #B Prism Work Order: 6120191 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 12/05/16 12:00 Time Submitted: 12/08/16 16:05 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Hexachlorobutadiene BRL ug1L 10 2.0 1 '625 12/12/16 20:28 JMV P61-0198 Hexachlorocyclopentadiene BRL ug/L 10 1.6 1 *625 12/12/16 20:28 JMV P61-0196 Hexachloroethane BRL ug/L 10 1.5 1 *625 12/12/16 20:28 JMV P61-0198 Indeno(1,2,3-od)pyrene BRL ug/L 10 3.1 1 *625 12/12/16 20:28 JMV P61-0198 Isophorone BRL ug/L 10 2.1 1 *625 12/12/16 2028 JMV P61,0198 Naphthalene BRL ug1L 10 2.1 1 `625 12/12/16 20:28 JMV P6L0198 Nitrobenzene BRL ug1L 10 1.4 1 *625 12/12/16 20:28 JMV P61-0198 N-Nitrosodimethylamine BRL ug1L 10 0.83 1 *625 12/12/16 20:28 JMV P61-0198 N-Nitroso-di-n-propylamine BRL ug1L 10 2.0 1 *625 12/12116 20:28 JMV P61-0198 N-Nitrosodiphenylamine BRL ug/L 10 2.9 1 *625 12/12/16 20:28 JMV P61-0198 Pentachlorophenol BRL ug1L 10 2.1 1 *625 12/12/16 20:28 JMV P61-0198 Phenanthrene BRL ug/L 10 3.2 1 *525 12/12116 20:28 JMV P61-0198 Phenol BRL ug/L 10 0.48 1 *625 12112116 20:28 JMV P61-0198 Pyrene BRL ug/L 10 3.5 1 *625 12/12116 20:28 JMV P61-0198 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 71 % 31-144 2-Fluorobiphenyl 74 % 49-118 2-Fluorophenol 51 % 22-84 Nitrobenzene-d5 72 % 43-123 Phenol-d5 36 % 10-63 Terphenyl-d14 74 % 49-151 Total Metals Copper BRL mg1L 0.010 0.00040 1 *200.7 12/21/16 0:17 bgm P61-0237 Lead BRL mg1L 0.0050 0.00090 1 '200.7 i2121116 0:17 bgm P61-0237 Zinc 0,15 mg1L 0,030 0.010 1 `2DD.7 12121116 0:17 bgm PSLO237 Volatile Organic Compounds by GUMS 1. 1, 1 -Trichloroethane BRL ug/L 5.0 0.061 1 *624 12/14/16 3:34 KDM P61-0234 1. 1, 2,2-Tetrachloroethane BRL UA 5.0 0.036 1 '624 12114/16 3:34 KDM P61-0234 1,1,2-Trichloroethane BRL ug/L 5.0 0.066 1 *624 12/14/16 3:34 KDM P61-0234 1,1-Dichloroethane BRL ug1L 5.0 0.083 1 `624 12/14/16 3:34 KDM P61-0234 1,1-Dichloroethylene BRL ug1L 5.0 0.083 1 *624 1214116 3:34 KDM P61-0234 1,2-Dichlorobenzene BRL ug/L 5.0 0.076 1 `624 12/14/16 3:34 KDM P61-0234 1,2-Dichloroethane BRL ug/L 5.0 0.066 1 `624 12/14/16 3:34 KDM P61-0234 1,2-Dichloropropane BRL ug/L 5.0 0.11 1 `624 12/14/16 3:34 KDM P61-0234 1,3-Dichlorobenzene BRL ug/L 5.0 0.054 1 *624 12/14/16 3:34 KDM P6L0234 1,4-Dichlorobenzene BRL ug/L 5.0 0.050 1 '624 12/14/16 3:34 KDM P6L0234 2-Chloroethyl Vinyl Ether BRL ug/L 10 0.37 1 *624 12/14/16 3:34 KDM P61-0234 Acrolein BRL ug/L 100 0,20 1 '624 12/14/16 3:34 KDM P61-0234 Acrylonitrile BRL ug/L 100 0,20 1 *624 12114/16 3:34 KDM P61-0234 Benzene BRL ug/L 5.0 0.048 1 *624 12114/16 3:34 KDM P61-0234 Bromodichloromethane BRL ug/L 5.0 0.062 1 '624 12/14/16 3:34 KDM P61-0234 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, inc. 449 5pringbrook Road - P.O. Box 2405Q - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704t525-0409 Page 5 of 20 Laboratory Report /LLJ Full-sevice Analytical a ISMI Envlrnantal Sootian�'-y� 12/21/2016 iHc GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Client Sample ID: SW-2 Attn: Dave Mazorra Prism Sample ID: 6120191-01 710 Peninsula Lane, #B Prism Work Order: 6120191 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 12/05/16 12:00 Time Submitted: 12/08/16 16:05 Parameter Result units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime ID Bromoform BRL ug/L 5.0 0.040 1 '624 12/14116 3:34 KDM P61_0234 Bromomethane BRL ug1L 10 0.18 1 *624 12/14/16 3:34 KDM P6L0234 Carbon Tetrachloride BRL ug1L 5.0 0.11 1 '624 12/14/16 3:34 KDM P61_0234 Chlorobenzene BRL ug/L 5.0 0.062 1 '624 12/14/16 3:34 KDM P6L0234 Chloroethane BRL ug/L 10 0.22 1 `624 12/14/16 3:34 KDM P61_0234 Chloroform BRL ug1L 5.0 0.076 1 *624 12/14/16 3:34 KDM P61_0234 Chloromethane BRL ug1L 10 0.079 1 '624 12/14/16 3:34 KDM P61_0234 cis-1,3-Dichloropropylene BRL ug1L 5.0 0,079 1 '624 12/14116 3:34 KDM P6L0234 Dibromochloromethane BRL ug/L 5.0 0.081 1 '624 12/14116 3:34 KDM P6L0234 Ethylbenzene BRL ug1L 5.0 0,061 1 '624 12114/16 3:34 KDM 1`61-0234 Methylene Chloride BRL ug1L 5.0 0.083 1 *624 12/14/16 3:34 KDM P61_0234 Tetrachloroethylene BRL ug1L 5.0 0.098 1 '624 12/14/16 3:34 KDM P61_0234 Toluene BRL ug1L 5.0 0,044 1 '624 12/14/16 3:34 KDM P61_0234 trans- 1,2-Dichloroethylene BRL ug/L 5.0 0.094 1 *624 12/14/16 3:34 KDM P61_0234 trans- 1,3-Dichlorapropylene BRL ug[L 5.0 0.070 1 "624 12/14/16 3:34 KDM P61_0234 TdcNioroethylene BRL ug1L 5.0 0.078 1 'fi24 12/14/16 3:34 KDM P61_0234 Trichlorofluoromethane BRL ug1L 10 0.062 1 '624 12114/16 3-34 KDM P61_0234 Vinyl chloride BRL ug1L 10 0.097 1 '624 12/14/16 3:34 KDM P61_0234 Surrogate Recovery Control Limits 4-Bromofluorobenzene 98 % 74-126 Dibromofluoromethane 107 % 75-127 Toluene-d8 109 % 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 6 of 20 A Full -Service Analytical & P R I M I Environmental Solutions ' �'r7�.aaw�lawea u.e Level II QC Report 12/21/16 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Volatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 6120191 Time Submitted,. 12/8/2016 4:05:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6LO234 - 624 Blank (P61-0234-131-K1) Prepared & Analyzed: 12/13/16 1,1,1-Trichloroethane BRL 5.0 ug/L 1,1,2,2-Tetrachloroethane BRL 5,0 ug/L 1,1,2-Tdrhioroethane BRL 5.0 ug/L 1,1-Dichloroethane BRL 5.0 ug/L 1,1-Dichloroethylene BRL 5.0 UA 1,2-Dichlorobenzene BRL 5.0 ug1L 1,2-Dichloroethane BRL 5,0 ug/L 1,2-Dichloropropane BRL 5.0 ug/L 1,3-Dichlorobenzene BRL 5.0 ug/L 1,4-Dichlorobenzene BRL 5.0 ugfL 2-Chloroethyl Vinyl Ether BRL 10 ugfL Acrolein BRL 100 ugfL Acrylonitrile BRL 100 ug/L Benzene BRL 5.0 ug/L Bromodichloromethane BRL 5.0 ug/L Bromoform BRL 5.0 ug/L Bromomethane BRL 10 ug/L Carbon Tetrachloride BRL 5.0 ug/L Chlorobenzene BRL 5.0 ug/L Chloroethane BRL 10 uglL Chloroform BRL 5.0 ugIL Chloromethane BRL 10 ug/L cis- 1,3-Dichloropropylene BRL 5.0 ug1L Dibromochloromethane BRL 5.0 uglL Ethylbenzene BRL 5.o uglL Methylene Chloride BRL 5.0 uglL Tetrachlaroethylene BRL 5.0 ug/L Toluene BRL 5.0 uglL trans- 1,2-Dichloroethylene BRL 5.0 ugfL trans- 1,3-Dichloroprapytene BRL 5.0 uglL Trichloroethylene BRL 5.0 uglL Trichlorofluoromethane BRL 10 ug/L Vinyl chloride BRL 10 ugfL Surrogate:4-BmmoRuorobenzene 47.7 ug/L 50.00 95 74-126 Surrogate: Dibromofluoromethane 51.5 ug1L 50.00 103 75-127 Surrogate: Totuene-d8 54.9 ug/L 50.00 110 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364- Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 7 of 20 \ Level II QC Report Full -Service Analytical 8 AM-221 S M Environmental Solutions 12/21/16 �'7ueoswron:es u.c GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P61_0234 - 624 Reporting Result Limit Units Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P6L0234-8S1) Prepared & Analyzed: 12/13/16 1,1,1-Tnchloroethane 19.8 5.0 ugiL 20.00 99 52-162 1,1,2,2-Tetrachloroethane 22.3 5.0 ug1L 20.00 112 46-157 1,1,2-Trichloroethane 19.1 5.0 ug1L 20.00 95 52-150 1,1-Dichloroethane 18.0 5.0 ug1L 20.00 90 59-155 1,1-Dichloroethylene 20.9 5.0 ug1L 20.00 104 10-234 1,2-Dichlorobenzene 22,9 5.0 ugiL 20.00 114 18-190 1,2-Dichloroethane 18.8 5.0 ugiL 20.00 94 49-155 1,2-Dichloropropane 18.6 5.0 ugiL 20.00 93 10-210 1,3-Dichlorobenzene 22.5 5.0 ug1L 20.00 112 59-156 1,4-Dichlorobenzene 22.5 5.0 ug1L 20.00 113 18-190 2-Chloroethyl Vinyl Ether 18.4 10 ug/L 20,00 92 10-305 Acrolein 38.6 100 ug1L 40.00 97 10-196 Acrylonitrile 35.8 100 ug1L 40.00 89 60-134 Benzene 18.8 5.0 ug1L 20.00 94 37-151 Bromodichloromethane 18.2 5.0 ugiL 20.00 91 35-155 Bromoform 21.0 5.0 ug1L 20.00 105 45-169 Bromomethane 19.3 10 ug1L 20.00 96 10-242 Carbon Tetrachloride 22.1 5.0 ugiL 20.00 111 70-140 Chlorobenzene 21.7 5.0 ugiL 20.00 108 37-160 Chloroethane 19.7 10 ug1L 20.00 99 14-230 Chloroform 17.8 5.0 ug1L 20.00 89 51-138 Chloromethane 20.7 10 ugiL 20.00 103 10-273 cis-1,3-Dichloropropylene 18.8 5.0 ugiL 20.00 94 10-227 Dibromochloromethane 21.8 5.0 ugiL 20.00 109 53-149 Ethylbenzene 22.3 5.0 ug1L 20.00 112 37-162 Methylene Chloride 16.8 5.0 ugiL 20.00 84 10-221 Tetrachloroethyiene 23.8 5.0 ug1L 20.00 119 64-148 Toluene 18.9 5.0 ug1L 20.00 95 47-150 trans- 1,2-Dichloroethylene 19.0 5.0 ugiL 20.00 95 54-156 trans-1,3-Dichloropropylene 19.2 5.0 ug1L 20.00 96 17-183 Trichloroethylene 19.7 5.0 ugiL 20.00 98 71-157 Trichlorofluoromethane 27.2 10 ug1L 20.00 136 17-181 Vinyl chloride 21.8 10 ug1L 20.00 109 10-251 Surrogate:4-Bromofluombenzene 47.0 ug1L 50.00 94 74-126 Surrogate: DibromoNuoromethane 50.0 ugiL 50.00 100 75-127 Surrogate: Toluene-d8 55.6 ug1L 50.00 111 74-122 This report should not be reproduced, except in its entirety, without the written consent of Pnsm Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 8 of 20 Full -Service Anahytieal & "P : M I Environmental Solutions Level 11 QC Report 12/21/16 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Volatile Organic Compounds by GC1MS - Quality Control Analyte Batch PGL0234 - 624 Reporting Result Limit Units Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05:OOPM Spike Source %4REC RPD Level Result %REC Limits RPD Limit Noies LCS Dup (P6t-0234-13SD1) Prepared & Analyzed: 12/13/16 1,1,1-Trichloroethane 19A 5.0 ug/L 20.00 95 52-162 4 20 1,1,2,2-Tetrachloroethane 22.5 5.0 ug/L 20.00 112 46-157 0.8 20 1,1,2-Tdchloroethane 18.9 5.0 ug/L 20.00 95 52-150 0.6 20 1,1-Dichloroethane 17,9 5.0 ug/L 20.00 90 59-155 0.6 20 1,1-Dichloroethylene 20.1 5.0 ug/L 20.00 100 10-234 4 20 1,2-Dichlorobenzene 23.0 5.0 ug/L 20.00 115 18-190 0.7 20 1,2-Dichlorocthane 17.8 5.0 ug1L 2000 89 49-155 5 20 1,2-Dichloropropane 18.2 5.0 ug/L 20.00 91 10-210 2 20 1,3-Dichlorobenzene 22.9 5.0 ug/L 20.00 114 59-156 2 20 1,4-Dichlorobenzene 22.6 5.0 ug/L 20.00 113 18-190 0.1 20 2-Chloroethyl Vinyl Ether 16.9 10 ug1L 20.00 84 10-305 8 20 Acrolein 40.9 100 ug1L 40.00 102 10-196 6 20 Acrylonitdle 36.5 100 ug/L 40.00 91 60-134 2 20 Benzene 18.4 5.0 uglL 20.00 92 37-151 3 20 Bromodichloromethene 18.2 5.0 ug/L 20.00 91 35-155 0.2 20 Bromoform 20.5 5.0 ug/L 20.00 102 45-169 3 20 Bromomethane 19.6 10 ug/L 20.00 98 10-242 2 20 Carbon Tetrachloride 21.1 5.0 ug/L 20.00 105 70-140 5 20 Chlorobenzene 21.3 5.0 ug/L 20.00 106 37-160 2 20 Chloroethane 18.6 10 ugtL 20.00 93 14-230 6 20 Chloroform 17.8 5.0 uglL 20.00 89 51-138 0.5 20 Chloromethane 19.7 10 ugtL 20,00 9$ 10-273 5 20 cis- 1,3-Dichloropropylene 18A 5.0 ug1L 20.00 92 10-227 2 20 Dibromochloromethane 21.6 5.0 ug1L 20,00 106 53-149 0.9 20 Ethylbenzene 21.7 5.0 ug1L 20.00 108 37-162 3 20 Methylene Chloride 16.4 5.0 ug1L 20,00 82 10-221 2 20 Tetrachloroethylene 22.9 5.0 uglL 20.00 115 64-148 4 20 Toluene 18.6 5.0 ug1L 20,00 93 47-150 2 20 trans- 1,2-Dichloroethylene 18.6 5.0 ug1L 20.00 93 54-156 2 20 trans- 1,3-Dichloropropylene 19.0 5.0 ug/L 20,00 95 17-183 0.8 20 Trichloroethylene 19.8 5.0 uglL 20.00 99 71-157 0.4 20 Trichloroftuoromethane 26.2 10 ug1L 20.00 131 17-181 4 20 Vinyl chloride 21.4 10 uglL 20.00 107 10-251 2 20 Surrogate:4-Bromofluorobenzene 48.5 ug/L 50.00 97 74-126 Surrogate: Dibromotluoromethane 49.2 ug/L 50.00 98 75-127 Surrogate: Toluene-d8 54.4 ug/L 50.00 109 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 9 of 20 Level 11 QC Repdrt FuD-Service Analytical 8 12/21/16 P R I S M Environmental Solutions GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P61_0198 - 625 Blank (1361-0198-BLK1) 12,4-Trichlorobenzene BRL 10 uglL 12-Dichlorobenzene BRL 10 uglL 1,2-Diphenylhydra7ine (as Azobenzerle) BRL 10 uglL 1,3-Dichlorobenzene BRL 10 ug/L 1,4-Dichlorobenzene BRL 10 uglL 2,4,6-Trichlorophenol BRL 10 ug1L 2,4-Dichlorophenol BRL 10 ug1L 2,4-Dimethylphenol BRL 10 ug1L 2,4-Dinitrophenol BRL 10 uglL 2,4-Dinitrotoluene BRL 10 ug1L 2,6-Dinitrotoluene BRL 10 ug1L 2-Chloronaphthalene BRL 10 ug1L 2-Chlorophenol BRL 10 uglL 2-Nitrophenol BRL 10 ug1L 3,3'-Dichlorobenzidine BRL 10 ug1L 4,6-Dinitro-2-methylphenol BRL 10 uglL 4-Bromophenyi phenyl ether BRL 10 uglL 4-Chloro-3-methylphenol BRL 10 uglL 4-Chlorophenyl phenyl ether BRL 10 ug1L 4-Nitrophenol BRL 50 ug/L Acenaphthene BRL 10 ug1L Acenaphthylene BRL 10 ug1L Anthracene BRL 10 ug1L Senzidine BRL 100 uglL Benzo(a)anthracene BRL 10 uglL Senzo(a)pyrene BRL 10 uglL Benzo(b)fluoranthene BRL 10 uglL Benzo(g,h,i)perylene BRL 10 uglL Benzo(k)fluoranthene BRL 10 uglL bis(2-Chloroethoxy)methane BRL 10 ug1L Bis(2-Chloroethyl)ether BRL 10 uglL Bis(2-chloroisopropyl)ether BRL 10 ug1L Bis(2-Ethylhexyl)phthalate BRL 10 uglL Butyl benzyl phthalate BRL 10 ug1L Chrysene BRL 10 ug1L Dibenzo(a,h)anthracene BRL 10 uglL Diethyl phthalate BRL 10 ug1L Dimethyl phthalate BRL 10 uglL Di-n-butyl phthalate BRL 10 ug1L Di-n-octyl phthalate BRL 10 uglL Ruoranthene BRL 10 ug1L Fluorene BRL 10 ug1L Hexachlorobenzene BRL 10 uglL Hexachlorobutadiene BRL 10 ug1L Hexachlorocyclopentadiene BRL 10 ug1L Hexachloroethane BRL 10 ug/L Prepared & Analyzed: 12/12/16 This report should not be reproduced. except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 117 of 20 N1.1 P R J S M Environmental en en al SOl do s AEnvironmental Solutions ' ��iapuTq�s u� Level II QC Report 12/21/16 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #)3 Charlotte, NC 28273 Semivolatile Organic Compounds by GClMS - Quality Control Analyte Batch P6L0198 - 625 Reporting Result Limit Units Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05MPM Spike Source %REC RPD Level Result '/ REC Limits RPD Limit Notes Blank (P6L0198-BLK1) Prepared & Analyzed: 12/12/16 Indeno(1,2,3-cd)pyrene BRL 10 ug1L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug/L Nitrobenzene BRL 10 ug1L N-Nitrosodimethylamine BRL 10 uglL N-Nitroso-di-n-propylamine BRL 10 ug/L N-Nitrosodiphenylamine BRL 10 ug/L Pentachlorophenol BRL 10 ug/L Phenanthrene BRL 10 ug/L Phenol BRL 10 ug/L Pyrene BRL 10 uglL Surrogate: 2,4,5-Tribromophenol 61.3 u91L 100.0 61 31-144 Surrogate:2-Fluombiphenyl 35.8 ug/L 50.00 72 49-118 Surrogate:2-Fluorophenol 46.2 ug/L 100.0 46 22-84 Surrogate: Nitrobenzene-d5 35.4 ug/L 50.00 71 43-123 Surrogate: Phenol-d5 29-6 u91L 100.0 30 10-63 Surrogate: Terphenyl-d14 32.4 ug/L 50.00 65 49-151 LCS (P6LD198-BS1) Prepared & Analyzed: 12/12/16 1,2,4-Trichlorobenzene 56.6 10 ug/L 100.0 57 44-142 1,2-Dichlorobenzene 65.0 10 ug1L 100.0 65 32-129 1,2-Diphenylhydrazine(as Azobenzene) 84.7 10 ug1L 100.0 85 40-135 1,3-Dichlorobenzene 63.1 10 ug1L 100.0 63 20-124 IA-Dichlorobenzene 63.8 10 ug1L 100A 64 20-124 2,4,6-Trichlorophenol 74.4 10 ug/L 100.0 74 37-144 2,4-Dichlorophenol 59.8 10 ug/L 100.0 60 39-135 2,4-Dimethylphenol 67.9 10 ug/L 100.0 68 32-119 2,4-Dinitrophenol 33.1 10 ug/L 100.0 33 10-191 2,4-Dinitrotoluene 81A 10 uglL 100.0 81 39-139 2,6-Dinitrotoluene 83.0 10 uglL 100.0 63 50-158 2-Chloronaphthalene 85.6 10 ug1L 100.0 86 60-118 2-Chlorophenol 70.9 10 ug/L 100.0 71 23-134 2-Nitrophenol 61.9 10 ug/L 100.0 62 29-182 3,3'-Dichlorobenzidine 84.8 10 ug1L 100.0 85 10-262 4,6-Dinitro-2-methylphenol 65.9 10 ug/L 100.0 66 10-181 4-Bromophenyl phenyl ether 77.9 10 uglL 100.0 78 53-127 4-Chloro-3-methylphenol 63.2 10 ug/L 100.0 63 22-147 4-Chlorophenyl phenyl ether 75.6 10 uglL 100.0 76 25-158 4-Nitrophenol 34.3 50 ug/L 100.0 34 10-132 Acenaphthene 72.9 10 ug/L 100.0 73 47-145 Acenaphthylene 74.6 10 ug1L 100.0 75 33-145 Anthracene 74A 10 ug1L 100.0 74 27-133 Benzidine 23.3 100 ug1L 100.0 23 15-150 Benzo(a)anthracene 77,7 10 ug1L 100.0 78 33-143 Benzo(a)pyrene 82.7 10 ug1L 100.0 83 17-163 Benzo(b)tluoranthene 83.0 10 ug1L 100.0 83 24-159 Benzo(g,h,i)perylene 79.4 10 ug1L 100.0 79 10-219 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page � 1 7 20 A.aM Full-Service Analytical Environmental Solutions rawea 1x Level II QC Report 12/21/16 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #13 Charlotte, NC 28273 Semivolatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6L0198 - 625 LCS (P61-8198-13S1) Prepared & Analyzed; 12/12/16 Benzo(k)Mucranthene 77.9 10 ug/L 100.0 78 11-162 bis(2-Chloroethoxy)methane 61.6 10 uglL 100.0 62 33-184 Bis(2-Chlomethyl)ether 62.8 10 uglL 100.0 63 12-158 Bis(2-chloroisopropyl)ether 72.4 10 ug/L 100.0 72 36-166 Bis(2-Ethylhexyl)phthalate 86.7 10 ug/L 100.0 87 10-158 Butyl benzyl phthalate 87A 10 uglL 100.0 87 10-152 Chrysene 77.5 10 uglL 100.0 78 17-168 Dibenzo(a,h)anthracene 78.0 10 uglL 100.0 78 10-227 Diethyl phthalate 78.0 10 uglL 100.0 78 10-114 Dimethyl phthalate 68.5 10 uglL 100.0 68 10-112 Di-n-butyl phthalate 77.6 10 uglL 100.0 78 10-118 Di-n-octyl phthalate 87.0 10 ug1L 100.0 87 10-146 Fluoranthene 73.8 10 uglL 100.0 74 26-137 Fluorene 74.8 10 uglL 100.0 75 59-121 Hexachlorobenzene 76.0 10 ugfL 100.0 76 10-152 Hexachlorobutadiene 55.6 10 uglL 100.0 56 24-116 Hexachlorocyclopentadiene 58.9 10 uglL 100.0 59 32-117 Hexachloroethane 64.3 10 uglL 100.0 64 40-113 Indeno(1,2,3-cd)pyrene 93.4 10 ug/L 100.0 93 10-171 Isophorone 65.7 10 ugtL 100.0 66 21-196 Naphthalene 56.8 10 uglL 100.0 57 21-133 Nitrobenzene 65.0 10 uglL 100.0 65 35-180 N-Nitrosodimethylamine 51.6 10 uglL 100.0 52 10-119 N-Nitroso-di-n-propylamine 73.7 10 ug1L 100.0 74 10-230 N-Nitrosodiphenylamine 77.8 10 uglL 100.0 78 69-152 Pentachlorophenol 58.4 10 uglL 100.0 58 14-176 Phenanthrene 75.6 10 uglL 100.0 76 54-120 Phenol 34.8 10 uglL 100.0 35 10-112 Pyrene 76A 10 ug1L 100.0 76 52-115 Surrogate:2,4,e-Tribromophenol 75.8 ug/L 100.0 76 31-144 Surrogate:2-Fluorobipherryl 42.0 ug/L 50.00 84 49-118 Surrogate:2-Fluorophenol 53.2 ug7L 100.0 53 22-84 Surrogate: Nitrobenzene-d5 34.6 ug/L 50.00 69 43-123 Surrogate: Phenol-d5 34.8 ug/L 100.0 35 10-63 Surrogate: Terphenyl-d14 38.8 ug/L 50.00 78 49-151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 L Page 12 of 20 � P RFull-Service Analytical B M En.ironmental Solutians -'�ifaanRron�a u+c Level II QC Report 12/21/16 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GCIMS - Quality Control Analyte Batch P61-0198 - 625 Reporting Result Limit Units Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05:0013M Spike Source %REC RP❑ Level Result %REC Limits RPD Limit Notes LCS Dup (P61-0198-8SDI) Prepared 8 Analyzed: 12/12/16 1,2,4-Trichlorobenzene 57.8 10 ug1L 100.0 58 44-142 2 20 1,2-Dichlorobenzene 65.7 10 uglL 100.0 66 32-129 1 20 1,2-Diphenylhydrazine(as Azobonzene) 88.1 10 ug1L 100.0 88 40-135 4 20 1,3-Dichlorobenzene 63.2 10 ug1L 100.0 63 20-124 0.2 20 1,4-1)ichlorobenzene 64.4 10 ug1L 100.0 64 20-124 0.8 20 2,4,6-Trichlorophenol 76.0 10 ug1L 100.0 76 37-144 2 20 2,4-Dichlorophenol 60.0 10 ug1L 100.0 60 39-135 0.3 20 2,4-Dimethylphenol 69.5 10 ug1L 100.0 70 32-119 2 20 2,4-Dinitrophenol 37.4 10 ug1L 100.0 37 10-191 12 20 2,4-Dinitrololuene 84,5 10 ug1L 100.0 84 39-139 4 20 2,6-Dinitrololuene 86.6 10 ug1L 100.0 87 50-158 4 20 2-Chloronaphthalene 88.6 10 uglL 100.0 89 60-118 4 20 2-Chlorophenol 71.0 10 ug1L 100.0 71 23-134 0.07 20 2-Nitrophenol 61A 10 uglL 100.0 61 29-182 0.8 20 3,3'-Dichlorobenzidine 88.4 10 ug1L 100.0 88 10-262 4 20 4,6-Dinitro-2-methyl phenol 63.6 10 ug1L 100.0 64 10-181 4 20 4-Bromophenyl phenyl ether 81.4 10 ug1L 100.0 81 53-127 4 20 4-Chloro-3-methylphenol 64.0 10 uglL 100.0 64 22-147 1 20 4-Chlorophenyl phenyl ether 78.3 10 uglL 100.0 78 25-158 3 20 4-Nitrophenol 34.8 50 uglL 100.0 35 10-132 1 20 Acenaphthene 75.9 10 ug1L 100.0 76 47-145 4 20 Acenaphthylene 77.2 10 uglL 100.0 77 33-145 3 20 Anthracene 77.1 10 ug1L 100.0 77 27-133 4 20 Benzidine 25.0 100 ug1L 100.0 25 15-150 7 20 Benzo(a)anthracene 80.8 10 ug1L 100.0 81 33-143 4 20 Benzo(a)pyrene 86.0 10 ug1L 100.0 86 17-163 4 20 Benzo(b)fluoranthene 86.5 10 ug1L 100.0 86 24-159 4 20 Benzo(g,h,i)perylene 52.7 10 uglL 100.0 83 10-219 4 20 Benzo(k)fluoranthene 81.1 10 ug1L 100.0 81 11-162 4 20 bis(2-Ch loroethoxy) methane 63.4 10 ug1L 100.0 63 33-184 3 20 Bis(2-Chloroethyl)ether 65.4 10 uglL 100.0 65 12-158 4 20 Bis(2-chloroisopropyl)ether 73.6 10 uglL 100.0 74 36-166 2 20 Bis(2-Ethylhexyl)phthalate 89.1 10 uglL 100.0 89 10-158 3 20 Butyl benzyl phthalate 91.1 10 uglL 100.0 91 10-152 4 20 Chrysene 80.8 10 ug1L 100.0 81 17-168 4 20 Dibenzo(a,h)anthracene 81.4 10 ug1L 100.0 81 10-227 4 20 Diethyl phthalate 80.7 10 ug1L 100.0 81 10-114 3 20 Dimethyl phthalate 74.2 10 ug1L 100.0 74 10-112 8 20 Di -;)-butyl phthalate 80.8 10 ug1L 100.0 81 10-118 4 20 Di-n-octyl phthalate 90.6 10 ugfL 100.0 91 10-146 4 20 Fluoranthene 76.6 10 ug1L 100.0 77 26-137 4 20 Fluorene 76.7 10 ug/L 100.0 77 59-121 3 20 Hexachlorobenzene 78.9 10 uglL 100.0 79 10-152 4 20 Hexachlorobutadiene 55.B 10 ug1L 100.0 56 24-116 0.4 20 Hexachlorocyclopentadiene 60.5 10 uglL 100.0 60 32-117 3 20 Hexachloroethane 65.2 10 ug1L 100.0 65 40-113 1 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Phone: 704I529-6364 - Toll Free Box 24OW - Charlotte, NC 28224-0543 Number: 1-8001529-6364 - Fax: 7041525-0409 Page 13 of 2fl �r ;e \ a Fu11-Service Analytical 8 R I S M � Environmental Solutions '71waoWOMCM -ac Level 11 QC Report 12/21/16 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Semivolatile Organic Compounds by GC1MS -Quality Control Analyte Batch P61-0198 - 625 Reporting Result Limit Units Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05:00PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P61-0198-13SD1) Prepared & Analyzed: 12/12/16 Indeno(1,2,3-cd)pyrene 97.9 10 ug/L 100.0 98 10-171 5 20 Isophorone 67.8 10 ug/L 100.0 68 21-196 3 20 Naphthalene 57.8 10 ug/L 100.0 58 21-133 2 20 Nitrobenzene 66.5 10 ug/L 100.0 67 35-180 2 20 N-Nitrosodimethylamine 53.2 10 ug/L 100.0 53 10-119 3 20 N-Nitroso-di-n-propylamine 77.7 10 ug/L 100.0 78 10-230 5 20 N-Nitrosodiphenylamine 81.9 10 ug/L 100.0 82 69-152 5 20 Pentachlorophenol 57.9 10 ug/L 100.0 58 14-176 0.9 20 Phenanthrene 78.6 10 ug/L 100.0 79 54-120 4 20 Phenol 35.2 10 ug/L 100.0 35 10-112 1 20 Pyrene 80.2 10 ug/L 100.0 80 52-115 5 20 Surrogate. 2,4,6-Tribromophenol 73.3 ug/L 100.0 73 31-144 Surrogate:2-Fluoroblphenyl 41.9 ug/L 50.00 84 49-118 Surrogate:2-Fluorophenol 51.1 ug/L 100.0 51 22-84 Surrogate: Nitrobenzene45 33.0 ug/L 50.00 66 43-123 Surrogate: Pheno!-d5 33.6 ug/L ]00.0 34 10-63 Surrogate: Terphenyl-d14 39.2 ugA 50.00 78 49-151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 14 of 20 Full -Service Analytical & j[ M I Environmental Solutions D eaaaawlaa�a Ina Level II QC Report 12/21/16 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Organochlorine Pesticides by GCIECD - Quality Control Analyte Batch P6LO205 - 608 Reporting Result Limit Units Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P61-0205-81-M) Prepared: 12/12/16 Analyzed: 12/13/16 alpha-BHC BRL 0.050 ugR beta-BHC BRL 0.050 ugR gamma-BHC BRL 0.050 ugR delta-BHC BRL 0.050 ugR Heptachlor BRL 0.050 ugR Aldrin BRL 0.050 ugR Heptachlor Epoxide BRL 0.050 ug1L trans -Chlordane BRL 0.050 ugR Endosulfan I BRL 0.050 ugR cis -Chlordane BRL 0.050 ugR Dieldrin BRL 0.050 uglL 4,4'-DDE BRL 0.050 uglL Endrin BRL 0.050 ugR Endosulfan II BRL 0.050 ug1L 4,4'-DDD BRL 0.050 ugR Endrin Aldehyde BRL 0.050 ugR Endosulfan Sulfate BRL 0.050 ug1L 4,4'-DDT BRL 0.050 ugR Endrin Ketone BRL 0.050 ug1L Methoxychlor BRL 0.050 ugR Chlordane BRL 0.50 ugR Toxaphene BRL 0.50 ug1L Aroclor 1016 BRL 0.50 ugR Aroclor 1221 BRL 1.0 ugR Aroclor 1232 BRL 0.50 ug1L Aroclor 1242 BRL 0.50 ugR Arodor 1248 BRL 0.50 ugR Aroclor 1254 BRL 0.50 ugR Aroclor 1260 BRL 0.50 ugR Surrogate: Tetrachloro-m-xylene 0.742 ug/L 1.000 74 40-134 Surrogate: Decachlorobiphenyl 0.844 ug/L 1.000 84 13-166 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 5pringbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800t529-6364 - Fax: 7041525-0409 Page 15 of 20 L1. 1 ! Full -Service Analytical $ =� �R ISM I Environmental Saluteons %T[ S. isc Level II QC Report 12/21 /16 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Organochlorine Pesticides by GCIECD - Quality Control Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05:00PM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P611_0205 - 608 LCS (P6L0205-BSI) Prepared: 12/12/16 Analyzed: 12/13/16 alpha-BHC 0,563 0.050 ug1L 1.000 86 37-134 beta-BHC 0.911 0.050 ug/L 1.000 91 17-147 gamma-BHC 0,897 0.050 ug1L 1.000 90 32-127 delta-BHC 0.908 0.050 ug/L 1.000 91 19-140 Heptachlor 1.00 0.050 ug/L 1.000 100 34-111 Aldrin 0.888 0.050 ug/L 1,000 89 42-122 Heptachlor Epoxide 0.957 0.050 ug/L 1.000 96 37-142 trans -Chlordane 0.949 0.050 ug1L 1.000 95 45-119 Endosulfan 1 0.935 0.050 ugfL 1.000 93 45-153 cis -Chlordane 0.936 0.050 ug1L 1.000 94 45-119 Dieldrin 0.978 0.050 ug[L 1.000 98 36-146 4,4'-DDE 0.999 0.050 ug/L 1.000 100 30-145 Endrin 1.08 0.050 ugfL 1.000 106 30-147 Endosulfan II 1.01 0.050 ug/L 1.000 101 10-202 4 4'-DDD 0.994 0.050 ug1L 1.000 99 31-141 Endrin Aldehyde 1.02 0.050 ugfL 1.000 102 68-139 Endosulfan Sulfate 1.03 0.050 ugfL 1.000 103 26-144 4,4'-DDT 1.08 0.050 ug1L 1.000 108 25-160 Endrin Ketone 1,01 0.050 ug/L 1.000 101 68-150 Methoxychlor 1.15 0.050 ug/L 1.000 115 70-157 Surrogate: Tetrachloro-m-xyfene 0.819 ug/L 1.000 82 40-134 Surrogate: Decachlorobiphenyl 0.851 ug/L 1.000 85 13-186 LCS (P6L0205-BS2) Prepared: 12/12/16 Analyzed: 12/13/16 Chlordane 8.12 0.50 ug/L 10.00 81 50-150 Surrogate: Tetrachloro-m-xyfene 0.745 ug/L 1.000 75 40-134 Surrogate: Decachlorobiphenyl 0,824 ug/L 1.000 82 13-186 This repart should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800152M364 - Fax: 704I525-0409 Page 16 of 20 ®Full -Service Analytical & a .� ISM I Environmental Solutions ~a Level II QC Report 12/21/16 GTA (Geo-Tech. Assoc. Inc.) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, IBC 28273 Organochlorine Pesticides by GCIECD - Quality Control Analyte Batch P61_0205 - 608 Reporting Result Limit Units Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05:04PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (PSL0205-BS3) Prepared: 12/12/16 Analyzed: 12/13/16 Toxaphene 8.97 0.50 ug1L 10.00 90 41-126 Surrogate: Tetrachloro-m-xylene 0.748 ug/L 1.000 75 40-134 Surrogate: Decachlorobiphenyl 0.760 ug/L 1.000 76 13-188 LCS (P6L0205-BS4) Prepared: 12/12/16 Analyzed: 12/13/16 Arodor 1016 11.0 0.50 uglL 10.00 110 50-114 Aroclor 1260 11.2 0.50 ug1L 10.00 112 10-127 Surrogate: Tetrachloro-m-xylene 0.758 ug/L 1.000 77 40-134 Surrogate: Decachlorobiphenyl 0.812 ug/L i.00o 61 13-186 LCS Dup (P6L0205-BSD1) Prepared: 12/12/16 Analyzed: 12/13/16 alpha-BHC 0.876 0.050 ug1L 1.000 88 37-134 2 20 beta-BHC 0.912 0.050 uglL 1.000 91 17-147 0.1 20 gamma-BHC 0.902 0.050 ug1L 1.000 90 32-127 0.5 20 delta-BHC 0.906 0.050 uglL 1.000 91 19-140 0.2 20 Heptachlor 1.01 0.050 ug1L 1.000 101 34-111 0.4 20 Aldrin 0.878 0.050 ug/L 1.000 88 42-122 1 20 Heptachlor Epoxide 0.946 0.050 ug1L 1.000 95 37-142 1 20 trans -Chlordane 0.898 0.050 ug1L 1.000 90 45-119 5 20 Endosulfan 1 0.907 0.050 ug/L 1.000 91 45-153 3 20 cis -Chlordane 0.904 0.050 ug1L 1.000 90 45-119 3 20 Dieldrin 0.961 0.050 ug1L 1.000 96 36-146 2 20 4,4'-DDE 0.984 0.050 uglL 1.000 98 30-145 2 20 Endrin 1.07 0.050 ug1L 1.000 107 30-147 0.3 20 Endosulfan 11 0.996 0.050 uglL 1.000 100 10-202 1 20 4,4'-DDD 0.980 0.050 ug1L 1.000 98 31-141 1 20 Endrin Aldehyde 1.02 0.050 ug1L 1.000 102 68-139 0.2 20 Endosulfan Sulfate 1.02 0.050 ug1L 1.000 102 26-144 0.6 20 4,4'-DDT 1.08 0.050 ug1L 1.000 108 25-160 0 20 Endrin Ketone 1.01 0.050 ug1L 1.000 101 68-150 0.5 20 Methoxychlor 1.14 0.050 ug1L 1.000 114 70-157 0.7 20 Surrogate. Tetrachloro-m-xylene 0.789 ug/L 1.000 79 40-134 Surrogate: Decachlorobiphenyl 0.602 ug/L 1.000 80 13-166 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O- Box 24OS43 - Charlotte, NC 28224-0543 Phone: 704t529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 17 of 20 a. � Full -Service Analytical & F RE!- ISM I Environmental Solutions �7LASOPAMAIE1 1I Level II QC Repoirt 12/21/16 GTA (Geo-Tech. Assoc. Inc-) Charlotte Project: Semi -Annual SW Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Total Metals - Quality Control Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P61_0237 - 200.7 Blank (P61_0237-BLK1) Prepared: 12/14/16 Analyzed: 12/20/16 Copper BRL 0.010 mg1L Lead BRL 0.0050 mg1L Zinc SRL 0.030 mg1L LCS (P61_0237-13SI) Prepared: 12/14/16 Analyzed: 12/20/16 Copper 0.245 0.010 mg1L 0.2500 98 85-115 Lead 0.259 0.0050 mg1L 0.2500 104 85-115 Zinc 0.263 o.030 mglL 0.2500 105 85-115 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 18 of 2O PAN �. QPA a Full -Service Analytical 8 I M Environmental Solutions • �Illlr► � o.5.. Level II QC Report 12/21/16 GTA (Geo-Tech. Assoc. Inc.) Charlotte Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 General Chemistry Parameters - Quality Control Analyte Batch P61_0187 - NO PREP Project: Semi -Annual SW Prism Work Order: 6120191 Time Submitted: 12/8/2016 4:05:00PM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS (P61-0187-13 Prepared & Analyzed: 12/09/16 _ pH 6.80 pH Units 6.880 99 98.5-101.5 Duplicate (PSL0187-DUPi) Source: 6120191-01 Prepared & Analyzed: 12/09/16 pH 6.22 pH Units 6.10 2 10 Batch P61_0214 - NO PREP Blank (P6L0214-BLK1) Prepared & Analyzed: 12/12/16 Total Suspended Solids BRL 5.0 mglL LCS (P6L0214-BS1) Prepared & Analyzed: 12/12/16 Total Suspended Solids 490 5.0 mg1L 477.0 102 9a-110 Batch P61_0356 - NO PREP Blank (P61-0356-BLK7) Prepared & Analyzed: 12/21/16 Oil & Grease (SGT-HEM) BRL 5.0 mg1L OG Sample Extraction Data Prep Method: 608 Lab Number Batch Initial Final Date/Time 6120191-01 P6L0205 1000 mL 10 mL 12/12/16 12:30 Prep Method: 626 Lab Number Batch Initial Final Datelrime 6120191-01 P61_0196 1000 mL 1 mL 12/12/16 9:00 Prep Method: 200.7 Lab Number Batch Initial Final DateMme 6120191-01 P61_0237 50 mL 50 mL 12114/16 7:45 Prep Method: 624 Lab Number Batch Initial Final Date/Time 6120191-01 P6L0234 10 mL 10 mL 12/13/16 12:39 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704l529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704l525-0409 Page 19 of 2O Ism Full -Service Analytical R �•', Environmental Solutions wy I.AaARATOpIE$lNO. 449 Springbrook Road • Charlotte, NC 28217 Phone 7041529.6364 • Fax: 7041525-0409 Client Company Name: 6 S (11r .,- <,a Report To/Contact Name:Reporting Address: Address: -% 10 vteu,l <, L,+ lit. 1...tn Ak V a C— kc, d to -4-k- , N I r CHAIN OF CUSTODY RECOIL® PAGE 1 OF ' QUOTE # TO ENSURE tPROPER BILLING: Project Name: M Y' ` A kAti 1 W _ Short Hold Analysis: (Yes) (6& UST Project: (Yes) ( *Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) provisions and/or QC Requirements Invoice To: Address: `X�. ya,�. —• Phone: `2-]30L) Fax o� Purchase Order No.lBllling Reference Email Address: C +v�X -z-Ct f A, � F?h r dnvl Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days EDD Type: PDF Excel)� Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days U RushrWork Must Be ._ Site Location Name: 'Sc? 1 e.� �C i , t C. S5 j j 1..�_ Samples received after 14:00 will be processed next business day. Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays, (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Certification: NELAC DOD FL NC_ SC OTHER NIA Water Chlorinated: YES NO Sample Iced Upon Collection: YES-L NO CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER PRESERVA-� TIVES ANALYSIS ED REMARKS , ; �� �Oqp \,r1 �� PRISM LAB ID NO. "TYPE SEE BELOW NO SIZE 12. 0 { X,, rn'1 uU��Tt ice` V Sampler's Signature 7 Sampled By (Print Name) j_r1VV— d1y'✓1w Affiliation Upon relinquishing, this Chain of Custody Is your authorization for Prism W proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges f r any changes after analyses have been initialized. dill einquis y: !ff reReceived y: Nnalure {- ateMIlitatylHours Additional Comments: SiteAl•hvall'Ime Refrnquished By: (Si nature) Received By: `Signature Dale C � - 1J✓ Site Departure. me: r Jr Field Tech Fee ! Relinquished By: {Signature} 1� Rape ed For Pri Laboratories By: ��bale * � �, � I r � } °- •° 1I-,e Method of Shipment: NOTE: ALL'SAMPLE COOLERS SHOULD BE TAPED SHUT WITH C ODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No. SAMPLES ARE NOT7CCEPTED AND VERIFIED AGAINST COC IL RECEIVED AT THE LABORATORY. 1 j 0 Fed Ex ❑LIPS Q Hand-deiiv, 9 Pdam Field Service Ll Other G 111,40 (Gh NPDES: UST: GROUNDWAT NC El SCI 6 NER: DRINKING WATER: SOLED WASTE: RCRA: CERCLA LANDFILL OTHER: ' O C ❑ SC � ❑ NC ❑ SC � C1 NC El SIC El NC ❑ SC 0 NC ❑ 5C 0 NC ElSC ❑ NC ❑ SC El NC ❑ SC ❑ Al *rnkrrAlxi'no TvOr7 rAnKc• A = Amhor r. = (Tear R= (yIaS5 P = Plastic: TL = Teflon -Lined Cep VOA = Volatile Organics Analysis (Zero Head Space) .J ism ��lAaORAiDRIES INC. GTA Associates, Inc. Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 NC Certification No, 402 Full -Service Analytical & NC Drinking Water Cert No. 37735 Environmental Solutions SC Certification No. 99012 f Project: Semi -Annual SW Lab Submittal Date: 12/02/2016 Prism Work Order: 6120060 Case Narrative 12/20/2016 RECEIVED JAN 2 5 2017 CENTRAL FILES DWR SECTION This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. G Cara C. Rusmisell Project Manager Data Qualifiers Key Reference: Reviewed By Cara C. Rusmisell Project Manager CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. D RPD value outside of the control limits. HT Sample received and analyzed outside of the hold time. L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken. OG HEM O&G is less than the reporting limit, therefore TPH (SGT-HEM) is less than the reporting limit. Sample not extracted for TPH (SGT-HEM). SE Surrogate recovery outside the QC limits due to emulsion. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7WS29-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 1 of 21 Sample Receipt Summary / .b�n� � Fvll-Service Analytical & ISM Environmental Solutions 12/20/2016 ®;7usan,.�onies Prism Work Order. 6120060 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received SW-1 6120060-01 Water 12/01/16 12/02/16 Samples were received in good condition at 2.2 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-0364 - Toll Free Number: 1-80015294364 - Fax: 7041525-0409 Page 2 of 21 Full -Service Analytical 8 M I Environmental Solutions Laboratory Report 12/20/2016 GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Sample Matrix: Water Client Sample ID: SW-1 Prism Sample ID: 6120060-01 Prism Work Order: 6120060 Time Collected: 12/01/16 12:30 Time Submitted: 12/02/16 10:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datef ime ID General Chemistry Parameters Oil & Grease (SGT-HEM) BRLOG mg/L 5.0 1.1 1 *166413 12/14/16 6:57 TJY 1361-0251 pH 6.4 HT pH Units 1 'SNM00-H 6 1212116 15:43 EGC P61L0075 Total Suspended Solids 7.8 mg1L 3.1 0.80 1 *SM2540 D 12/8116 9:35 SLS P61-0153 Organochlorine Pesticides by GCIECD alpha-BHC BRL ug/L 0.050 0,012 1 *608 12113/16 14:01 JMC P61-0072 beta-BHC 0.15 ug/L 0.050 0.019 1 *608 12113/16 14:01 JMC P61L0072 gamma-BHC $RL ug/L 0.050 0.013 1 *608 12/13/16 14:01 JMC P6L0072 delta-BHC BRL ug11. 0.050 0.017 1 *608 12/13/16 14:01 JMC P6L0072 Heptachlor BRLCCV ug/L 0.050 0.015 1 *608 12/13/16 14;01 JMC P60072 Alden BRL ug/L 0.050 0.015 1 'fi08 12/13/16 14:01 JMC P61-0072 Heptachlor Epoxide BRL ug/L 0.050 0.018 1 *608 12/13/16 14:01 JMC PBL0072 trans -Chlordane BRLCCV ug/L 0.050 0.019 1 *608 12/13/16 14:01 JMC P61-0072 Endosulfan I BRLCCV ug/L 0.050 0.019 1 '608 12/13116 14:01 JMC P6L0D72 cis -Chlordane BRL ug1L 0.050 0.018 1 *608 12/13/16 14:01 JMC P6L0072 Dieidrin BRLCCV ug/L 0,050 0.022 1 *608 12/13/16 14:01 JMC P61-0072 4,4'-DDE BRL ug/L 0.050 0.028 1 'fi08 12/13/16 14:01 JMC P6L0072 Endrin BRLCCV ug/L 0.050 0.020 1 *608 12/13/16 14:01 JMC P61-0072 Endosulfan 11 BRLCCV ug/L 0,050 0.025 1 *608 12/13/16 14:01 JMC P61-0072 4,4'-DDD BRLCCV uglL 0.050 0.028 1 'fi08 12/13/16 14:01 JMC P61-0072 Endrin Aldehyde BRLCCV ug/L 0.050 0.027 1 *608 12/13/16 14:01 JMC P61-0072 Endosulfan Sulfate BRLCCV ug1L 0,050 0.027 1 *608 12113/16 14:01 JMC PGL0072 4,4'-DDT BRLCCV ug/L 0.050 0.027 1 '608 12113/16 14:01 JMC P61-0072 Endrin Ketone BRLCCV ug/L 0.050 0.028 1 *608 12113116 14:01 JMC P61-0072 Melhoxychlor BRLCCV ug/L 0,050 0.033 1 1608 12/13/16 14:01 JMC PGL0072 Chlordane BRLCCV ug1L 0.50 0.094 1 *608 12113116 14:01 JMC P61-0072 Toxaphene BRL ug1L 0.50 0.32 1 '608 12113/16 14:01 JMC P61-0072 Arodor 1016 BRL ug1L 0.50 0.24 1 *608 12/13/16 14:01 JMC P61-0072 Arodor 1221 BRL ug/L 1.0 0.11 1 *608 12/13/16 14701 JMC P60072 Aroclor 1232 BRL ug/L 0.50 0.16 1 *608 12/13/16 14:01 JMC P61-0072 Arodor 1242 BRL ug1L 0.50 0,14 1 *608 12/13/16 14:01 JMC P61-0072 Arodor 1248 BRL ugR 0.50 0.14 1 'fi08 12/13/16 14:01 JMC P61-0072 Arodor 1254 BRL ug/L 0.50 0.16 1 '608 12/13/16 14:01 JMC P61-0072 Arodor 1260 BRL ug1L 0.50 0.30 1 *608 12/13/16 14:01 JMC P61-0072 Surrogate Recovery Control Limits Tetrachloro-m-xylene 70 % 40-134 Decachlorobiphenyl 62 % 13-186 Semivolatile Organic Compounds by GCIMS 1,2,4-Trichlorobenzene BRL ug/L 10 1.5 1 '625 12/8116 17:21 JMV P61-0113 1,2-Dichlorobenzene BRL ug/L 10 1.4 1 'fi25 12/8116 17:21 JMV P61-0113 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - p.o. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-000/529-6364 - Fax: 7041625-0409 Page 3 of 21 .� Laboratory Report P R nFull I I -Service Analytical 8 � �/' Environmental Solutions 12120/2016 �7.wBow.aaw�s n.c. GTA Associates, Inc. Project: Semi -Annual SW Client Sample ID: SW-1 Attn: Dave Mazorra Prism Sample ID: 6120060-01 710 Peninsula Lane, #B Prism Work Order: 6120060 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 12/01/16 12:30 Time Submitted: 12/02/16 10:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst DatelTime Batch ID 1,2-Diphenylhydrazine (as Azobenzene) BRL ug/L 10 2.9 1 '625 12/8116 17:21 JMV P61_0113 1,3-Dichlorobenzene BRL ug1L 10 1.3 1 "625 1218/16 17:21 JMV P61_0113 1,4-Dichlorobenzene BRL ug1L 10 1A 1 '625 1218116 1721 JMV P$L0113 2,4,6-Trichlorophenol BRL ug/L 10 1.8 1 *625 1218116 17:21 JMV 1361-0113 2,4-Dichlorophenol BRL ug/L 10 1.6 1 '625 1218116 17:21 JMV P61_0113 2,4-Dimethylphenol BRL ug/L 10 2.1 1 '625 1218116 17:21 JMV P6L0113 2,4-Dinitrophenol BRL ug/L 10 1.2 1 `625 12/8116 17:21 JMV P61-0113 2,4-Dinitrotoluene BRL ug1L 10 2.9 1 *625 12/8/16 17:21 JMV P6L0113 2,6-Dinitrotoluene BRL ug/L 10 2.9 1 '625 1218116 17:21 JMV P61_0113 2-Chloronaphthalene BRL ug/L 10 2,3 1 '625 1218116 17:21 JMV P61-0113 2-Chloraphenol BRL ug/L 10 1.1 1 '625 1218116 17:21 JMV P61-0113 2-Nitrophenol BRL ug1L 10 1.4 1 '625 12/8116 17:21 JMV P61-0113 3,3'-Dichiorobenzidine BRL ug/L 10 2.8 1 *625 12/8116 17:21 JMV P61-0113 4,6-Dinitro-2-methylphenol BRL ug1L 10 1.9 1 *625 1218116 17:21 JMV P61_0113 4-Bromophenyl phenyl ether BRL ug1L 10 3.2 1 '625 12/8116 17:21 JMV P61-0113 4-Chloro-3-methylphenol BRL ug1L 10 2.3 1 *625 1218116 17:21 JMV 1361-0113 4-Chlorophenyi phenyl ether BRL ug/L 10 2.2 1 '625 12/8116 17:21 JMV P61_0113 4-Nitrophenol BRL ug/L 50 1.7 1 *625 12/8116 17:21 JMV 1361-0113 Acenaphthene BRL ug/L 10 2.3 1 '625 1218116 17:21 JMV P61_0113 Acenaphthylene BRL ug/L 10 2.3 1 *625 1218116 17:21 JMV P6Lo113 Anthracene BRL ug/L 10 3.2 1 *625 12/8116 17:21 JMV P61_0113 Benzidine BRL ug/L too 14 1 *625 12/8116 17.21 JMV P61_0113 Benzo(a)anthracene BRL ug1L 10 3.1 1 `625 1218116 17:21 JMV P61_0113 Benzo(a)pyrene BRL ug/L 10 3.6 1 *625 1218/16 17:21 JMV 1361_0113 Benzo(b)ffuoranthene BRL ug1L 10 3.5 1 *625 1218/16 17:21 JMV P61_0113 Benzo(g,h,i)perylene BRL ug1L 10 3.5 1 *625 12/8116 17:21 JMV P61_0113 Senzo(k)fluoranthene BRL ug/L 10 3.8 1 '625 12/8116 17:21 JMV P61_0113 bis(2-Chloroethoxy)methane BRL ug/L 10 1.8 1 *625 1218116 17:21 JMV 1361-0113 Bis(2-Chloroethyl)ether BRL ug1L 10 1.6 1 '625 1218116 17:21 JMV P61-0113 Bis(2-chloroisopropyl)ether BRL ug1L 10 1.7 1 *625 1218116 17:21 JMV P6L0113 Bis(2-Ethylhexyl)phthalate BRL ug1L 10 3.1 1 '625 12/8116 17:21 JMV P61-0113 Butyl benzyl phthalate BRL ug1L 10 2.6 1 *625 12/8116 17:21 JMV P61_0113 Chrysene BRL ug1L 10 3A 1 '625 1218116 17:21 JMV P6L0113 Dibenzo(a,h)anthracene BRL ug/L 10 3.4 1 *625 12/8116 17:21 JMV P61L0113 Diethyl phthalate BRL ug1L 10 2.3 1 '625 12/8116 17:21 JMV P61-0113 Dimethyl phthalate BRL ug1L 10 1.5 1 '625 1218/16 17:21 JMV P61_0113 Di-n-butyl phthalate BRL ug/L 10 3.4 1 *625 1218116 17:21 JMV 1061-0113 Di-n-octyl phthalate BRL ug/L 10 3.6 1 '625 1218116 17:21 JMV P61_0113 Fluoranthene BRL ug1L 10 3.5 1 '625 1218/16 17:21 JMV P61_0113 Fluorene BRL ug1L 10 2.8 1 '625 1218116 17:21 JMV P61_0113 Hexachlorobenzene BRL ug1L 10 2.5 1 '625 1218116 17:21 JMV P61-0113 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Tolt Free Number: 1.8001529-6364 - Fax. Page 4 of 21 7041525-0409 � a Full -Service Analytical & �P R ISm Environmentar Solutions Laboratory Report 1 2121)12016 GTA Associates, Inc. Project: Semi -Annual SW Client Sample ID: SW-1 Attn: Dave Mazorra Prism Sample ID: 6120060-01 710 Peninsula Lane, #B Prism Work Order: 6120060 Charlotte, NC 28273 Sample Matrix: Water Time Collected: 12101116 12:30 Time Submitted: 12/02/16 10:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Datefrime Analyst Batch ID Hexachlorobutadiene BRL ug1L 10 2.0 1 '625 1218/16 17:21 JMV P6L0113 Hexachlorocyclopentadiene BRL ug1L 10 1.6 1 '625 1218116 17:21 JMV P61_0113 Hexachloroethane BRL ug1L 10 1.5 1 '625 1218116 17:21 JMV P61_0113 Indeno(1,2,3{:d)pyrene BRL ug1L 10 3.1 1 '625 1218116 17:21 JMV P61_0113 Isophorone BRL ug1L 10 2.1 1 '625 1218/16 17:21 JMV P61_0113 Naphthalene BRL ug1L 10 2.1 1 "625 1218/16 17:21 JMV P61_0113 Nitrobenzene BRL uglt. 10 1.4 1 '625 1218/16 17:21 JMV P61_0113 N-Nitrosodimethylamine BRL ug1L 10 0.83 1 '625 1218/16 17:21 JMV P61-0113 N-Nitroso-di-n-propylarnine BRL ug1L 10 2.0 1 '625 1218/16 17:21 JMV PBLO113 N-Nitrosodiphenylamine BRL ug1L 10 2.9 1 '625 1218/16 17:21 JMV P61-0113 Pentachlorophenol BRL ug1L 10 2.1 1 "625 1218116 17:21 JMV P6L0113 Phenanthrene BRL uglL 10 3.2 1 '625 1218116 17:21 JMV P6L0113 Phenol BRL ug1L 10 0.48 1 '625 1218116 17:21 JMV P6L0113 Pyrene BRL uglL 10 3.5 1 '625 1218/16 17:21 JMV P61_0113 Total Metals Copper 0.017 mg1L Lead BRL mg1L Zinc 0.10 mg1L Volatile Organic Compounds by GCIMS Surrogate Recovery Control Limits 2,4,6-Tribromophenol 71 % 31-144 2-Fluorobiphenyl 50 % 49-118 2-Fluorophenol 34 % 22-84 Nitrobenzene-d5 31 % 43-123 SE Phenol-d5 23 % 70-63 Terphenyl-d14 59 % 49-151 0.010 0.00040 1 '200.7 12I6116 20:24 bgm P61_0279 0.0050 0.00090 1 '200.7 12/14/16 21:19 bgm P61_0191 0.030 0.010 1 '200.7 12114116 21:19 bgm P61-0191 1,1,1-Trichloroethane BRL ug1L 5.0 0.061 1 '624 12/14/16 0:10 KDM P61_0234 1,1,2,2-Tetrachloroethane BRL ug1L &0 0.036 1 '624 12/14/16 0:10 KDM P6L0234 1, 1, 2-Trichloroethane BRL ug1L 5.0 0.066 1 '624 12114/16 0:10 KDM P61_0234 1,1-Dichloroethane BRL ug/L 5.0 0.083 1 '624 12/14/16 0:10 KDM P61_0234 1.1-Dichloroethylene BRL uglL 5.0 0.083 1 '624 12/14116 0:10 KDM P61_0234 1,2-Dichlorobenzene BRL ug1L 5.0 0.076 1 '624 12114/16 0:10 KDM P6L0234 1,2-Dichloroethane BRL ug1L 5.0 0.066 1 '624 12/14/16 0:10 KDM P61_0234 1,2-Dichloropropane BRL uglL 5.0 0.11 1 '624 12/14/16 0:10 KDM P61_0234 1,3-Dichlorobenzene BRL uglL 5.0 0.054 1 "624 12114116 0:10 KDM P61_0234 1,4-Dichlorobenzene BRL ug1L 5.0 0.050 1 '624 12/14/16 0:10 KDM P61_0234 2-Chloroethyl Vinyl Ether BRL ug1L 10 0,37 1 '624 12114/16 0:10 KDM P61_0234 Acrolein BRL ug1L 100 0.20 1 '624 12/14116 0:10 KDM P6L0234 Acrylonitrile BRL uglL 100 0.20 1 '624 12114116 0:10 KDM P61-0234 Benzene BRL ug1L 5.0 0.048 1 '624 12/14/16 0:10 KDM P61_0234 Bromodichloromethane BRL ug1L 5.0 0.062 1 '624 12114116 0:10 KDM P61_0234 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 5 of 21 Analytical Laboratory Report $ fik,Full-ServiceISM I Environmental Solutions 12/20/2016 -7 s I� GTA Associates, Inc. Project: Semi -Annual SW Client Sample ID: SW-1 Attn: Dave Mazorra Prism Sample ID: 6120060-01 710 Peninsula Lane, #B Prism Work Order: 6120060 Charlotte, IBC 28273 Sample Matrix: Water Time Collected: 12/01/16 12:30 Time Submitted: 12/02/16 10:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Bromoform BRL ug1L 5.0 0.040 1 *624 12/14/16 0:10 KDM P61_0234 Bromomethane BRL ug1L 10 0.18 1 'fi24 12/14/16 0:10 KDM P61_0234 Carbon Tetrachloride BRL ug1L 5.0 0.11 1 '624 12/14/16 0:10 KDM P61_0234 Chlorobenzene BRL ug1L 5.0 o.062 1 '624 12/14/16 0:10 KDM P61_0234 Chloroethane BRL ug1L 10 0.22 1 "624 12/14/16 0:10 KDM P61_0234 Chloroform BRL uglL 5.0 0.076 1 '624 12/14/16 0:10 KDM P61_0234 Chloromethane BRL ug1L 10 0.079 1 *624 12/14/16 0:10 KDM P61_0234 cis-1,3-Dichloropropylene BRL ug/L 5.0 0.079 1 *624 12/14/16 0:10 KDM P61-0234 Dibromochloromethane BRL ug1L 5,0 0.081 1 *624 12114/16 0:10 KDM P61_0234 Ethylbenzene BRL ug/L 5.0 0,061 1 *624 12/14/16 0:10 KDM P61-0234 Methylene Chloride BRL ug1L 5.0 0.083 1 '624 12114/16 0:10 KDM P61-0234 Tetrachloroethylene BRL ug/L 5.0 0.098 1 *624 12/14/16 0:10 KDM P6L0234 Toluene BRL ug1L 5.0 0,044 1 *624 12/14/16 0:10 KDM PGL0234 trans-1,2-Dichloroethylene BRL ug/L 5.0 0.094 1 *624 12/14/16 0:10 KDM 1361-0234 trans-1,3-Dichloropropylene BRL ug/L 5.0 0.070 1 '624 12/14/16 0:10 KDM P6L0234 Trichloroethylene BRL u911- 5.0 0.078 1 '624 12/14/16 0:10 KDM 1061-0234 Thchlorofluoromethane BRL ug1L 10 0.062 1 '624 12/14/16 0:10 KDM P61_0234 Vinyl chloride BRL uglL 10 o.o97 1 'fi24 12/14/16 0:10 KDM P61-0234 Surrogate Recovery Control Limits 4-Bromofluorobenzene 96 % 74-126 Dibromofluoromethane 105 % 75-127 Toluene-d8 109 % 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-OW 77-7-1 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 6 of 21 �GFIMi mFull-Service Analytical & R I M Environments! Solutions '.'L---oar,.-CL Level 11 QC Report 12/20/16 GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Volatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00:00AM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch MUM - 624 Blank (11361_0234-BLK1 j Prepared & Analyzed: 12/13/16 1,1,1-Trichloroethane BRL 5.0 ug/L 1,1,2,2-Tetrachloroethane BRL 5.0 ug1L 1,1,2-Trcchloroethane BRL 5.0 ug/L 1,1-Dichloroethane BRL 5.0 ug/L 1,1-Dichloroethylene BRL 5.0 ug/L 1,2-Dichlorobenzene BRL 5.0 uglL 1,2-Dichloroethane BRL 5.0 ug1L 1,2-Dichloropropane BRL 5.0 ug/L 1,3-Dichlorobenzene BRL 5.0 ug/L 1,4-Dichlorobenzene BRL 5.0 ug/L 2-Chloroethyl Vinyl Ether BRL 10 uglL Acrolein BRL 100 ug/L Acrylonitrile BRL 100 ug/L Benzene BRL 5.0 ug/L Bromodichloromethane BRL 5.0 ug/L Bromoform BRL 5.0 ug1L Bromomethane BRL 10 ug1L Carbon Tetrachloride BRL 5.0 ug/L Chlorobenzene BRL 5,0 ug1L Chloroethane BRL 10 ug/L Chloroform BRL 5.0 ug/L Chloromethane BRL 10 ug/L cis-1,3-Dichloropropylene BRL 5.0 ug/L Dibromochloromethane BRL 5.0 ug1L Ethylbenzene BRL 5.0 uglL Methylene Chloride BRL 5.0 uglL Tetrachlaroethylene BRL 5.0 ug/L Toluene BRL 5.0 ug1L trans-1,2-Dichloroethylene BRL 5.0 ug1L trans-1,3-Dichloropropylene BRL 5.0 ug1L Trichloroethylene BRL 5.0 ug1L Tdchlorofluoromethane BRL 10 uglL Vinyl chloride BRL 10 ug/L Surrogate:4-Bromofluorobenzene 47.7 ug/L 50,00 95 74-126 Surrogate: DlbromoBuoromethane 51.5 ug/L 50.00 103 75-127 Surrogate: Toluene-d8 54.9 ug/L 50.00 110 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 5pringbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 70W52M364 - Toll Free Number: 1.8001529-6364 - Fax: 704/525-0409 Page 7 of 21 A Levii QC Report Full -Service Analytical & AA P R ISM Environmental Salutians 12/2011 6 Es.1W_ GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Volatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 6120060 Time Submitted! 12/2/2016 10:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6L0234 - 624 LCS (P6L0234-i Prepared & Analyzed: 12/13/16 1, 1, 1 -Trichloroethane 19.8 5.0 uglL 20.00 99 52-162 1,1,2,2-Tetrachloroethane 22.3 5.0 uglL 20.00 112 46-157 1,1,2-Trichloroethane 19.1 5.0 ug1L 20.00 95 52-150 1,1-Dichloroethane 18.0 5.0 ug1L 20.00 90 59-155 1,1-Dichloroethylene 20.9 5.0 ug1L 20.00 104 10-234 1,2-Dichlorobenzene 22.9 5.0 ug1L 20.00 114 18-190 1,2-Dichloroethane 18.8 5.0 ug1L 20.00 94 49-155 1,2-Dichloropropane 18.6 5.0 uglL 20.00 93 10-210 1,3-Dichlorobenzene 22.5 5.0 uglL 20.00 112 59-156 1,4-Dichlorobenzene 22.5 5.0 ug1L 20.00 113 18-190 2-Chloroethyl Vinyl Ether 18.4 10 uglL 20.00 92 10-305 Acrolein 38.6 100 ug1L 40.00 97 10-196 Acrylonitrile 35.8 100 ug1L 40.00 89 60-134 Benzene 18.8 5.0 ug1L 20.00 94 37-151 Bromodichloromethane 18.2 5.0 uglL 20.00 91 35-155 Bromoform 21.0 5.0 uglL 20.00 105 45-169 Bromomethane 19.3 10 uglL 20.00 96 10-242 Carbon Tetrachloride 22.1 5.0 uglL 20.00 ill 70-140 Chlorobenzene 21.7 5.0 uglL 20.00 108 37-160 Chloroethane 19.7 10 ug1L 20.00 99 14-230 Chloroform 47.8 5.0 ug1L 20.00 89 51-138 Chicromethane 20.7 10 uglL 20.00 103 10-273 cis-1,3-Dichloropropylene 18,8 5.0 ug1L 20.00 94 10-227 Dibromochloromethane 21.8 5,0 ug1L 20.00 109 53-149 Ethylbenzene 22.3 5.0 uglL 20.00 112 37-162 Methylene Chloride 16.8 5.0 uglL 20.00 84 10-221 Tetrachloroethylene 23.6 5.0 uglL 20.00 119 64-148 Toluene 18.9 5.0 uglL 20.00 95 47-150 trans-1,2-Dichloroethylene 19.0 5.0 uglL 20.00 95 54-156 trans- 1,3-Dichloropropylene 19.2 5.0 ug/L 20.00 96 17-183 Trichloroethylene 19.7 5.0 uglL 20.00 98 71-157 Trichlorofluoromethane 27.2 10 uglL 20.00 136 17-181 Vinyl chloride 21.8 10 uglL 20.00 109 10-251 Surrogate:4-Bramofluorobenzene 47.0 ug/L 50.00 94 74-126 Surrogate- Dibromofluoromethane 50.0 ug/L 50,00 100 75-127 Surrogate: Toluene-d8 55.6 ug/L 50.00 l i i 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Humber: 1-8001529-6364 - Fax: 704152"409 Page 8 of 21 � Level II QC Report Fun -Service Analytical&kci I VI Environmental Solutions 1212011$�e'7iAeowerorXM con GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Volatile Organic Compounds by GC1MS - Quality Control Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit units Level Result %REC Limits RPD Limit Notes Batch PGL0234 - 624 LCS Dup (P61-0234-13SD9) Prepared & Analyzed: 12/13/16 1,1,1-Tdchloroethane 19.1 5.0 uglL 20.00 95 52-162 4 20 1,1,2,2-Tetrachloroethane 22.5 5.0 uglL 20.00 112 46-157 0.8 20 1, 1, 2-Trichloroethane 18.9 5.0 uglL 20.00 95 52-150 0.6 20 1,1-Dichloroethane 17.9 5.0 uglL 20.00 90 59-155 0.6 20 1,1-Dichloroethylene 20.1 5.0 ug/L 20.00 100 10-234 4 20 1,2-Dichlorobenzene 23.0 5.0 uglL 20,00 115 18-190 0.7 20 1.2-Dichloroethane 17.8 5.0 uglL 20.00 89 49-155 5 20 1,2-Dichloropropane 18.2 5.0 ug1L 20.00 91 10-210 2 20 1,3-Dichlorobenzene 22.9 5.0 ug1L 20.00 114 59-156 2 20 1,4-Dichlorobenzene 22.6 5.0 ug/L 20.00 113 18-190 0.1 20 2-Chloroethyl Vinyl Ether 16.9 10 ug1L 20.00 84 10-305 8 20 Acrolein 40.9 100 ug1L 40.00 102 10-196 6 20 Acrylonitrile 36.5 100 ug1L 40.00 91 60-134 2 20 Benzene 18.4 5.0 ug1L 20.00 92 37-151 3 20 Bromodichloromethane 18.2 5.0 uglL 20.00 91 35-155 0,2 20 Bromoform 20.5 5.0 ug1L 20.00 102 45-169 3 20 Bromomethane 19,6 10 uglL 20.00 98 10-242 2 20 Carbon Tetrachloride 21.1 5.0 uglL 20.00 105 70-140 5 20 Chlorobenzene 21.3 5.0 ug1L 20.00 106 37-160 2 20 Chloroethane 18.6 10 uglL 20.00 93 14-230 6 20 Chloroform 17,8 5.0 uglL 20.00 89 51-136 0.5 20 Chloromethane 19.7 10 uglL 20.00 98 10-273 5 20 cis-1,3-Dichloropropylene 18.4 5.0 uglL 20.00 92 10-227 2 20 Dibromochloromethane 21.6 5.0 uglL 20.00 108 53-149 0.9 20 Ethyibenzene 21.7 5.0 uglL 20.00 108 37-162 3 20 Methylene Chloride 16.4 5.0 uglL 20.00 82 10-221 2 20 Tetrachloroethylene 22.9 5.0 ug1L 20.00 115 64-148 4 20 Toluene 18.6 5.0 uglL 20.00 93 47-150 2 20 trans-1,2-Dichloroethylene 18.6 5.0 ug1L 20.00 93 54-156 2 20 trans- 1,3-Dichloropropylene 19.0 5.0 ug1L 20.00 95 17-183 0.8 20 Trichloroethylene 19.8 5.0 uglL 20.00 99 71-157 0.4 20 Trichlorofluoromethane 26.2 10 ug1L 20.00 131 17-151 4 20 Vinyl chloride 21.4 10 ug/L 20.00 107 10-251 2 20 Surrogate:4-Bromofluorobenzene 48.5 ug/L 50.00 97 74-126 Surrogate: Dibromofluoromethene 4R2 ug/L 50.00 98 75-127 Surrogate:7oluene-d8 54A ug/L 50.00 109 74-122 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 70V526-0409 Page 9 of 21 A-,FI',\R, Level JI QC Report Full -Service Analytical& 12/20/16 S M I Environmental Salutions ��usuucrowes me GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Semivolatile Organic Compounds by GC1MS - Quality Control Analyte Batch P6LO113 - 625 Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (P61-0113-131-Ki) Prepared: 12/07/16 Analyzed: 12/08/16 1,2,4-Trichlorobenzene BRL 10 ug1L 1,2-Dichlorobenzene BRL 10 ug1L 1,2-Diphenylhydrazine (as Azobenzene) BRL 10 ug/L 1,3-Dichlorobenzene BRL 10 ug1L 1,4-Dichlorobenzene BRL 10 ug./L 2,4,6-Trichlorophenol BRL 10 ug/L 2,4-Dichlorophenol BRL 10 ug1L 2,4-Dimethylphenol BRL 10 ug/L 2,4-Dinitrophenol BRL 10 ug1L 2,4-Dinitrotoluene BRL 10 ug/L 2,6-Dinitrotoluene BRL 10 ug/L 2-Chloronaphthalene BRL 10 uglL 2-Chlorophenol BRL 10 ug/L 2-Nitrophenol BRL 10 ug/L 3,3'-Dichlorobenzidine BRL 10 ug1L 4,6-Dinitro-2-methylphenol BRL 10 ug1L 4-Bromophenyl phenyl ether BRL 10 ug]L 4-Chloro-3-methylphenol BRL 10 ug1L 4-Chlorophenyl phenyl ether BRL 10 ug1L 4-Nitrophenol BRL so ug1L Acenaphthene BRL 10 ug1L Acenaphthylene BRL 10 ug1L Anthracene BRL 10 ug1L Benzidine BRL 100 ug1L Benzo(a)anthracene BRL 10 ug1L Benzo(a)pyrene BRL 10 ug1L Benzo(b)fluoranthene BRL 10 ug1L Benzo(g,h,i)perylene BRL 10 ug1L Senzo(k)fluoranthene BRL 10 ug/L bis(2-Chloroethoxy)methane BRL 10 ug1L Bis(2-Chloroethyl)ether BRL 10 ug1L Bis(2-chloroisopmpyl)ether BRL 10 ug/L Sis(2-Ethylhexyl)phtha1ate BRL 10 ug1L Butyl benzyl phthalate BRL 10 ug1L Chrysene BRL 10 ug1L Dibenzo(a,h)anthracene BRL 10 uglL Diethyl phthalate BRL 10 uglL Dimethyl phthalate BRL 10 ug/L Di-n-butyl phthalate BRL 10 ug1L Di-n-octyl phthalate BRL 10 ug1L Fluoranthene BRL 10 ug1L Fluorene BRL 10 ug1L Hexachlorobenzene BRL 10 ug1L Hexachlorobutadiene BRL 10 ug1L Hexachlorocydopentadiene BRL 10 ug1L Hexachloroethane BRL 10 ug1L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/529-0364 - Toll Free Number: 1-8001529-0364 - Fax: 7041525-0409 Page 10 of 21 f Level II QC Report �P R I S M Full-mnmae Analytical Environmental Solutionss 12I20116 ®'VtAM ups oc GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Semivolatile Organic Compounds by GUMS - Quality Control Analyte Batch P6L0113 - 625 Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (PSL0113-BLK1) Prepared: 12/07/16 Analyzed: 12/08/16 Indeno(1,2,3-cd)pyrene BRL 10 ug1L Isophorone BRL 10 ug1L Naphthalene BRL 10 ug1L Nitrobenzene BRL 10 ug1L N-Nitrasodimethylamine BRL 10 ug/L N-Nitroso-di-n-propylamine BRL 10 ug1L N-Nitrosodiphenylamine BRL 10 ug/L Pentachlorophenol BRL 10 ug1L Phenanthrene BRL 10 ug1L Phenol BRL 10 ug1L Pyrene BRL 10 ug1L Surrogate: 2,4,6-Tribromophenol 70.7 u91L 100.0 71 31-144 Surrogate:2-Ftuorobiphenyt 39.9 ug1L 50.00 so 49-118 Surrogate:2-Ftuorophenol 48.0 ug/L 100.0 48 22-84 Surrogate. Nitrobenzene-d5 38.1 ug/L 50.00 76 43-123 Surrogate. Phenol-d5 32.0 ug/L 100.0 32 10-63 Surrogate: Terphenyt-d14 41.0 ug/L 50.00 82 49-151 LCS (P611-8113-BSI) Prepared: 12/07/16 Analyzed: 12/08/16 1,2,4-Trichlorobenzene 52.0 10 ug/L 100.0 52 44-142 1,2-Dichlorobenzene 57.2 10 ug/L 100.0 57 32-129 1,2-Diphenylhydrazine (as Azobenzene) 69.2 10 ug1L 100.0 69 40-135 1,3-Dichlorobenzene 55.9 10 ug/L 100.0 56 20-124 1,4-Dichlorobenzene 56.7 10 ug1L 100.0 57 20-124 2,4,6-Trichlorophenol 56.7 10 ug1L 100.0 57 37-144 2,4-Dichlorophenol 48.0 10 ug1L 100.0 48 39-135 2,4-Dimethylphenol 55,8 10 ug1L 100.0 56 32-119 2,4-Dinitrophenol 30.0 10 ug1L 100.0 30 10-191 2,4-Dinitrotoluene 70.3 10 ug1L 100.0 70 39-139 2,6-Dinitrotoluene 70.8 10 ug1L 100.0 71 50-158 2-Chloronaphthalene 79.9 10 ug1L 100.0 80 60-118 2-Chlorophenol 55.8 10 ug1L 100.0 56 23-134 2-Nitrophenol 48.6 10 ug1L 100.0 49 29-182 3,T-Dichlorobenzidine 74.8 10 ug1L 100.0 75 10-262 4,6-Dinitro-2-methylphenol 52.1 10 ug/L 100.0 52 10-181 4-Bromophenyl phenyl ether 68.0 10 ug/L 100.0 68 53-127 4-Chloro-3-methylphenol 51.4 10 ug1L 100.0 51 22-147 4-Chlorophenyl phenyl ether 67.6 10 ug1L 100.0 68 25-158 4-Nitrophenol 25.7 50 ug1L 100.0 26 10-132 Acenaphthene 63.6 10 ug/L 100.0 64 47-145 Acenaphthylene 60.2 10 ug1L 100.0 60 33-145 Anthracene 61.9 10 ug1L 100.0 fit 27-133 Benzidine BRL 100 ug1L 100.0 15-150 L1 Benzo(a)anthracene 68.8 10 ug/L 100.0 69 33-143 Benzo(a)pyrene 76.0 10 uglL 100.0 76 17-163 Benzo(b)fluaranthene 73.2 10 ug/L 100.0 73 24-159 Benzo(g,hJ)perylene 75.0 10 uglL 100.0 75 10-219 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-0364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 11 of 21 Full -Service Analytical 8 J Environmental Solutions �7�.�eanAmuea �Hc, Level•II QC Report 12/20/16 GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #13 Charlotte, NC 28273 Project: Semi -Annual SW Semivolatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit !Votes Batch P6LO113 - 625 LCS (P6L0113-BS1) Prepared: 12/07/16 Analyzed: 12/08/16 Benzo(k)fluoranthene 74.4 10 ug/L 100.0 74 11-162 bis(2-Chloroethoxy)methane 54.7 10 ug1L 100.0 55 33-184 Bis(2-Chloroethyl)ether 61.2 10 ug1L 100.0 61 12-158 Bis(2-chloroisopropyl)ether 59.5 10 ug/L 100.0 60 36-166 Bis(2-Ethylhexyl)phthalate 73.8 10 ug/L 100.0 74 10-158 Butyl benzyl phthalate 72.2 10 ug1L 100.0 72 10-152 Chrysene 69.6 10 ug1L 100.0 70 17-168 Dibenzo(a,h)anthracene 75.6 10 ug/L 100.0 76 10-227 Diethyl phthalate 64.8 10 ug/L 100.0 65 10-114 Dimethyl phthalate 54.2 10 ug/L 100.0 54 10-112 Di-n-butyl phthalate 62.7 10 ug/L 100.0 63 10-118 Di-n-octyl phthalate 76.6 10 ug1L 100.0 77 10-146 Fluoranthene 60.9 10 ug1L 100.0 61 2e-137 Fluorene 65.4 10 ug1L 100.0 65 59-121 Hexactlorobenzene 67.4 10 ug/L 100,0 67 10-152 Hexachlorobutadiene 50.5 10 ug1L 100.0 50 24-116 Hexachlorocyclopentadiene 66.5 10 ug/L 100.0 67 32-117 Hexachloroethane 56.3 10 ug/L 100.0 56 40-113 Indeno(1,2,3-Gd)pyrene 94.2 10 ug/L 100.0 94 10-171 Isophorone 56.5 10 ug/L 100.0 56 21-196 Naphthalene 48.4 10 ug1L 100.0 48 21-133 Nitrobenzene 57.1 10 ug/L 100.0 57 35-160 N-Nitrosodimethylamine 43.2 10 ug/L 100.0 43 10-119 N-Nitroso-di-n-propylamine 65.0 10 ug1L 100.0 65 10-230 N-Nitrosodiphenylamine 66.9 10 ug/L 100.0 67 69-152 Pentachlorophenol 46.0 10 ug1L 100.0 46 14-176 Phenanthrene 61.8 10 ug/L 100.0 62 54-120 Phenol 26.8 10 ug1L 100,0 27 10-112 Pyrene 61.5 10 uglL 100.0 62 52-115 Surrogate: 2,4,6-Tribromophenol 59.8 uglL 100.0 60 31-144 Surrogate:2-Fluombiphenyl 37.5 uglt_ 50.00 75 49-118 Surrogate:2-Fluorophenol 41.7 ug/L 100.0 42 22-84 Surrogate: Nitrobenzene-d5 30.6 ug/L 50.00 61 43-123 Surrogate: Phenol-d5 28.0 ug/L 100.0 28 10-63 Surrogate: Terphenyl-d14 35.6 ug/L 50.00 71 49-151 L1 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 12 of 21 Full -Service Analytical & rpa DO, ISM Environmental Salutions 'Afilwir �TCWgEaIW- Level II QC Report 12/20/16 GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Semivolatile Organic Compounds by GCIMS - Quality Control Analyte P61-0113 - 625 Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS Pup (P61-0113-BSD1) Prepared: 12/07/16 Analyzed: 12/08/16 1,2,4-Tdchlorobenzene 51.8 10 ug/L 100.0 52 44-142 0.4 20 1,2-Dichlorobenzene 58.3 10 ug/L 100.0 58 32-129 2 20 1, 2-Diphenylhyd razine (as Azobenzene) 76.4 10 ug/L 100.0 76 40-135 10 20 1,3-Dichlorobenzene 57.1 10 ug1L 100.0 57 20-124 2 20 1,4-Dichlorobenzene 57,5 10 ug/L 100.0 57 20-124 1 20 2,4,6-Trichlorophenol 70.1 10 ug/L 100.0 70 37-144 21 20 D 2,4-Dichlorophenol 52.0 t0 ug/L 100.0 52 39-135 8 20 2,4-Dimethylphenol 59.3 10 ug/L 100.0 59 32-119 6 20 2,4-Dinitrophenol 52.3 10 ug/L 100.0 52 10-191 54 20 D 2,4-Dinitrotoluene 80.9 10 ug/L 100.0 81 39-139 14 20 2,6-Dinitrotoluene 81.6 10 ug/L 100.0 82 50-158 14 20 2-Chloronaphthalene 86.1 10 ug/L 100.0 86 60-118 7 20 2-Chlorophenol 58.6 10 ug/L 100.0 59 23-134 5 20 2-Nitrophenol 52.4 10 ug1L 100.0 52 29-182 8 20 3,3'-Dichlorobenzidine 86.3 10 ug1L 100.0 86 10-262 14 20 4,6-Dinitro-2-methylphenol 71.6 10 ug/L 100.0 72 10-181 32 20 D 4-Bromophenyl phenyl ether 77.5 10 ug/L 100.0 78 53-127 13 20 4-Chloro-3-methylphenol 60.5 10 ug/L 100.0 60 22-147 16 20 4-Chlorophenyl phenyl ether 76.3 10 ug/L 100.0 76 25-158 12 20 4-Nitrophenol 35.3 50 ug/L 100.0 35 10-132 31 20 ❑ Acenaphthene 71.9 10 uglL 100.0 72 47-145 12 20 Acenaphthylene 6$,0 10 uglL 100.0 fib 33-145 9 20 Anthracene 68.9 10 uglL 100.0 69 27-133 11 20 Benzidine 14.8 100 ug1L 100.0 15 15-150 12 20 Benzo(a)anthracene 78.4 10 uglL 100.0 78 33-143 13 20 Benzo(a)pyrene $7.7 10 ug1L 100.0 88 17-163 14 20 Benzo(b)fluoranthene 85.2 10 ug[L 100.0 85 24-159 15 20 Benzo(g,h,i)perylene $7.1 10 ug1L 100.0 87 10-219 15 20 Benzo(k)fluoranthene 86.1 10 ug/L 100.0 86 11-162 15 20 bis(2-Chloroethoxy)methane 56.2 10 ug/L 100.0 56 33-184 3 20 Bis(2-Chloroethyl)ether 62.3 10 ug/L 100.0 62 12-158 2 20 Bis(2-�-'hloroisopropyl)ether 60.9 10 ug/L 100.0 61 36-166 2 20 Bis(2-Ethyihexyl)phthalate 83.8 10 ug/L 100.0 a4 10-158 13 20 Butyl benzyl phthalate 82.7 10 ug/L 100.0 83 10-152 13 20 Chrysene 80.1 10 ug/L 100.0 80 17-168 14 20 Dibenzo(a,h)anthracene 87.6 10 ug/L 100.0 88 10-227 15 20 Diethyl phthalate 76.2 10 ug/L 100.0 76 10-114 16 20 Dimethyl phthalate 67.7 10 ugR. 100.0 68 10-112 22 20 D Di-n-butyl phthalate 69.8 10 ug/L 100.0 70 10-118 11 20 Di-n-octyl phthalate 88.6 10 ugR. 100.0 89 10-146 15 20 Fluoranthene 68.1 10 ug1L 100.0 68 26-137 11 20 Fluorene 73.7 10 ug/L 100.0 74 59-121 12 20 Hexachlorobenzene 76.0 10 ug/L 100.0 76 10-152 12 20 Hexachlorobutadiene 50.5 10 uglL 100.0 50 24-116 0.08 20 Hexachlorocyclopentadiene 68.5 10 ug/L 100.0 68 32-117 3 20 Hexachloroethane 56.7 10 uglL 1MID 57 40-113 0.7 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-GS43 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 70415254409 Page 13 of 21 Level II QC Report R Full -Service Analytical & f S M Environmental Solutions 12/20/18 ZO14R �"7ueauiaraes u¢. GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Semivolatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P61-0113 - 626 LCS Dup (P61-0113-BSD1) Prepared: 12/07/16 Analyzed: 12/08/16 Indeno(1,2,3-cd)pyrene 109 10 uglL 100.0 109 10-171 15 20 Isophorone 59.2 10 uglL 100,0 59 21-196 5 20 Naphthalene 49.6 10 ug/t_ 100.0 50 21-133 3 20 Nitrobenzene 57.8 10 uglL 100.0 58 35-180 1 20 N-Nitrosodimethylamine 44.2 10 ug1L 100.0 44 10-119 2 20 N-Nitros"i-n-propylamine 68,2 10 ug1L 100.0 6a 10-230 5 20 N-Nitrosodiphenylamine 75.7 10 uglL 100.0 76 69-152 12 20 Pentachlorophenol 67.1 10 ug1L 100.0 67 14-176 37 20 ❑ Phenanthrene 68.9 10 ug1L 100.0 69 54-120 11 20 Phenol 29.1 10 ugtL 100.0 29 10-112 8 20 Pyrene 70.4 10 ug1L 100.0 70 52-115 14 20 Surrogate. 2,4,6-Tribromophenol 73.7 ug/L 100.0 74 31-144 Surrogate.2-Fluorobiphenyl 36.4 ug/L 60.00 77 49-118 Surrogate: 2-Fluorophenol 42.8 ug/L 100.0 43 2284 Surrogate: Nitrobenzene-d5 29.5 ug/L 50.00 59 43-123 Surrogate: Phenol-l5 28.9 ug/L 100.0 29 10-63 Surrogate: Terohenyl-rli4 39.0 uglL 50.00 78 49-151 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toil Free Number: 1-800/629-6364 - Fax: 7041525-0409 Page 14 of 21 Full -Service Analytical 8 R I M I Environmental Solutions Level II QC Report 12/20/16 GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Organochlorine Pesticides by GCIECD - Quality Control Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch MOM - 608 Blank (P6 0072-BLKi) Prepared: 12/05/16 Analyzed: 12/13/16 alpha-BHC BRL 0.050 ug1L beta-BHC BRL 0.050 ug1L gamma-BHC BRL 0.050 ugtL delta-BHC BRL 0.050 ug/L Heptachlor BRL 0.050 ug1L Aldrin BRL 0.050 ugtL Heptachlor Epoxide BRL 0.050 ug1L trans -Chlordane BRL 0.050 ugtL Endosulfan I BRL 0.050 ug1L cis -Chlordane BRL 0.050 ug/L Dieldrin BRL 0.050 ug/L 4,4'-DDE BRL 0.050 ug/L Endrin BRL 0.050 ug1L Endosulfan II BRL 0.050 ug1L 4,4'-DDD BRL 0.050 ug/L Endrin Aldehyde BRL 0.050 ug/L Endosulfan Sulfate BRL 0.050 ug/L 4,4'-DDT BRL 0.050 ug/L Endrin Ketone BRL 0.050 ug/L Methoxychlor BRL 0.050 ug/L Chlordane BRL 0.50 ug/L Toxaphene BRL 0.50 ug/L Arodor 1016 BRL 0.50 ug/L Arodor 1221 BRL 1.0 ug/L Arodor 1232 BRL 0.50 ug/L Arodor 1242 BRL 0,50 ug1L Arodor 1248 BRL 0.50 ug/L Arodor 1254 BRL 0.50 ug/L Aroclor 1260 BRL 0.50 ug/L Surrogate: Tetrachloro-m-xylene 0.690 dg/L 1.000 69 40-134 Surrogate: Decachlorobiphenyl 0.758 ug/L 1.000 76 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8D0t529-0364 - Fax: 70415254409 Page 15 of 21 jP1©I C n n Full -Service Analytical 8 R J f V' Environmental Solutions .7i..arnlaaes u,c Level al QC Report 12/20/16 GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Organochlorine Pesticides by GCIECD - Quality Control Analyte Batch P61_0072 - 608 Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00:00AM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS (P6L0072-BSI) Prepared: 12/05/16 Analyzed: 12/13/16 alpha-BHC 1.07 0.050 uglL 1.000 107 37-134 beta-BHC 1.12 0.050 uglL 1.000 112 17-147 gamma-BHC 1.10 0,050 ug/L 1.000 110 32-127 delta-BHC 1.03 0.050 ug/L 1.000 103 19-140 Heptachlor 1.18 0.050 ug/L 1.000 118 34-111 Li Aldrin 1.07 0.050 ug/L 1.000 107 42-122 Heptachlor Epoxide 1.16 0.050 uglL 1.000 116 37-142 trans -Chlordane 1.15 0.050 ug/L 1.000 115 45-119 Endosulfan 1 1.14 0.050 ug/L 1.000 114 45-153 cis -Chlordane 1.15 0.050 ug/L 1.000 115 45-119 Dieldrin 1.18 0.050 ug/L 1.000 118 36-146 4,4'-DDE 1.20 0.050 ug/L 1.000 120 30-145 Endrin 1.29 0.050 ug/L 1.000 129 30-147 Endosulfan II 1.21 0.050 ug/L 1.000 121 10-202 4,4'-DDD 1,19 0.050 ugrL 1,000 119 31-141 Endrin Aldehyde 1.18 0.050 ug/L 1.000 118 68-139 Endosulfan Sulfate 1.20 0.050 ug/L 1.000 120 26-144 4,4'-DDT 1.27 0.050 uglL 1.000 127 25-160 Endrin Ketone 1.21 0.050 uglL 1.000 121 68-150 Methoxychlor 1.28 0.050 ug/L 1.000 128 70-157 Surrogate: Tetrachloro-m-xylene 0.782 ug/L 1.000 78 40-134 Surrogate- Decachlorobiphenyl 0.829 ug/L 1.000 83 13-186 LCS (P6L0072-BS2) Prepared: 12/05/16 Analyzed: 12/13/16 Chlordane 8.02 0.50 ug/L 10.00 80 50-150 Surrogate' Tetrachloro-m-xylene 0.715 ug/L 1.000 72 40 134 Surrogate: Decachlorobiphenyl 0.797 ug/L 1.000 80 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 16 of 21 Level II QC Report Pur a Full -Service Analytical 8 12/20/16 R ISM I Environmental Solutions ��i.aeawau�S n�c GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #i3 Charlotte, NC 28273 Project: Semi -Annual SW Organochlorine Pesticides by GC/ECD - Quality Control Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00:00AM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P61_0072 - 608 LCS (P61-0072-13S3) Prepared: 12I05/16 Analyzed: 12/13/16 Toxaphene 9.43 0.50 ug/L 10.00 94 41-126 Surrogate: Tetrachloro-m-xylene 0.770 ug/L 1,000 77 40-134 Sumagate: Decachlorobiphenyt 0.815 ug/L 1.000 81 13-186 LCS (P61-0072-13S4) Prepared: 12/05/16 Analyzed: 12/13/16 Arodor 1016 9.37 0.50 ug/L 10.00 94 50-114 Arodor 1260 9.52 0,50 ug[L MOO 95 10-127 Surrogate: Tetrachloro-m-xylene 0.781 ug/L 1.000 78 40-134 Surrogate: Decachlorobiphenyl 0.835 ug/L 1.000 64 13-186 LCS Dup (P6L0072-13SD1) Prepared: 12/05/16 Analyzed: 12/13/16 alpha-BHC 0.922 0,050 ug1L 1.000 92 37-134 14 20 beta-BHC 0.992 0.050 ug/L 1.000 99 17-147 13 20 gamma-BHC 0.955 0.050 ug/L 1.000 96 32-127 14 20 delta-BHC 0.907 0.050 ug/L 1.000 91 19-140 13 20 Heptachlor 0,978 0.050 ug/L 1.000 98 34-111 18 20 Aldrin 0.875 0.050 ug1L 1,000 88 42-122 20 20 Heptachlor Epoxide 1.01 0.050 ug/L 1.000 101 37-142 13 20 trans -Chlordane 1.00 0.050 uglL 1,000 100 45-119 14 20 Endosulfan 1 0,997 0.050 ug/L 1.000 100 45-153 13 20 cis -Chlordane 1.00 0.050 ug/L 1,000 100 45-119 14 20 Dieldlin 1.02 0.050 ug/L 1.000 102 36-146 14 20 4,4'-DDE 1.04 0.050 uglL 1.000 104 30-145 14 20 Endrin 1.13 0.050 ug1L 1.000 113 30-147 13 20 Endosulfan II 1.07 0.050 ug/L 1.000 107 10-202 13 20 4,4'-DDD 1.04 0.050 ug1L 1.000 104 31-141 13 20 Endrin Aldehyde 1.04 0.050 ug/L 1.000 104 68-139 13 20 Endosulfan Sulfate 1.07 0.050 ug/L 1.000 107 26-144 12 20 4,4'-DDT 1.12 0.050 ug/L 1.000 112 25-160 13 20 Endrin Ketone 1.07 0.050 ug1L 1.000 107 68-150 12 20 Methoxychlor 1.18 0.050 ug1L 1.000 118 70-157 8 20 Surrogate: Tetrachloro-m-xylene 0.622 ug/L 1.000 62 40-134 Surrogate: Decachlorobiphenyl 0.698 ug/L 1.000 70 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 24050 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 17 of 21 Aid A Level 11 QC Report Full -Service Analytical & 12/20/16 R. ISM Environmental Solutions -' iwaoaxmnMa tM GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Project: Semi -Annual SW Organochlorine Pesticides by GCIEC❑ - Quality Control Analyte Batch P61_0072 - 608 Reporting Result Limit Units Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00MAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike (P61-0072-MS1) Source: 6120060-01 Prepared: 12/05/16 Analyzed: 12/13/16 alpha-BHC 1.84 0.10 ug1L 2.000 BRL 92 37-134 beta-BHC 2.09 0.10 ug1L 2.000 0.154 97 17-147 gamma-BHC 1.95 0.10 uglL 2.000 0.0279 96 32-127 delta-BHC 1.87 0.10 ug1L 2.000 0.0494 91 19-140 Heptachlor 2.25 0.10 ug/L 2.000 0.0389 ill 34-111 Alden 1.97 0.10 uglL 2.000 BRL 98 42-122 Heptachlor Epoxide 2.13 0.10 uglL 2.000 BRL 107 37-142 trans -Chlordane 2.06 0.10 ug1L 2.000 BRL 103 45-119 Endosulfan 1 2.04 0.10 ug1L 2.000 BRL 102 45-153 cis -Chlordane 2.10 0.10 ug1L 2.000 BRL 105 45-119 Dieldrin 2.21 0.10 uglL 2.000 BRL 110 36-146 4,4'-DDE 2.24 0.10 uglL 2.000 BRL 112 30-145 Endrin 2.59 0.10 uglL 2.000 BRL 130 30-147 Endosulfan 11 2.31 0.10 ug1L 2.000 BRL 115 10-202 4,4'-DDD 2.26 0,10 ugrL 2.000 BRL 113 31-141 Endrin Aldehyde 2.24 0.10 uglL 2.000 BRL 112 15-165 Endosulfan Sulfate 2.31 0,10 uglL 2,000 BRL 116 26-144 4,4'-DDT 2.43 0.10 uglL 2.000 BRL 122 25-160 Endrin Ketone 2.29 0,10 uglL 2,000 BRL 115 29-172 Methoxychlor 2.58 0.10 ug1L 2.000 BRL 129 34-187 Surrogate: Tetrachloro-m-xylene 1.44 uglL 2.000 72 40-134 Surrogate: Decachloroblphenyl 1.33 uglL 2.000 66 13-186 Matrix Spike ❑up (P6L0072-MS❑1) Source: 6120060-01 Prepared: 12/05/16 Analyzed: 12/13/16 alpha-BHC 1.79 0.10 ug1L 2.000 BRL 89 37-434 3 31 beta-BHC 2.05 0.10 uglL 2.000 0.154 95 17-147 2 29 gamma-BHC 1.90 0,10 uglL 2.000 0.0279 94 32-127 3 32 delta-BHC 1.86 0.10 ug1L 2.000 0.0494 91 19-140 0.7 27 Heptachlor 2.19 0.10 ug1L 2.000 0.0389 108 34-111 3 36 Aldrin 1.93 0.10 ug1L 2.000 BRL 96 42-122 2 35 Heptachlor Epoxide 2.11 0.10 ug1L 2.000 BRL 106 37-142 1 36 trans -Chlordane 2.03 0.10 uglL 2.000 BRL 101 45-119 2 34 Endosulfan I 2.o2 0.10 ug1L 2.000 BRL 101 45-153 0,8 40 Cis -Chlordane 2.08 0.10 uglL 2.000 BRL 104 45-119 0.8 40 Dieldrin 2.19 0,10 ug1L 2.000 BRL 110 36-146 0.6 28 4,4'-DDE 2.22 0.10 uglL 2.000 BRL 111 30-145 0.8 38 Endrin 2.61 0.10 ug1L 2.000 BRL 130 30-147 0.6 27 Endosulfan II 2.32 0.10 ug1L 2.000 BRL 116 10-202 0.6 32 4,4'-DDD 2.27 0.10 uglL 2.000 BRL 114 31-141 0.3 29 Endrin Aldehyde 2.24 0,10 ug1L 2.000 BRL 112 15-165 0.2 33 Endosulfan Sulfate 2.34 0.10 ug1L 2.000 BRL 117 26-144 1 36 4,4'-DDT 2.41 0.10 ug1L 2.000 BRL 121 25-160 0.9 30 Endrin Ketone 2.32 0.10 ug1L 2.000 BRL 116 29-172 1 29 Methoxychlor 2.61 0.10 uglL 2.000 BRL 131 34-187 1 34 Surrogate: Tetrachloro-m-xylene 1.38 uglL 2.000 69 40-134 Surrogate: Decachlorobiphenyl 1.24 ug/L 2.000 62 13-186 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529.6364 - Fax: 7041525-0409 Page 18 of 21 Full -Service Analytical & Ald hid R ISM I Environmental Solutions �'%-ueavvor�a o� Level II QC Report 12/20/16 GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 Total Metals - Quality Control Analyte Project: Semi -Annual SW Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00:00AM Reporting Spike Source %REC RPM Result Limit units Level Result %REC Limits RPM Limit Notes Batch P6L0191 - 200.7 Blank (P6L0191-BLKI) Prepared: 12/12/16 Analyzed: 12/14/16 Lead BRL 0.0050 mglL Zinc BRL 0.030 mglL LCS (P6L0191-BS1) Prepared: 12/12/16 Analyzed: 12114I16 Lead 0.261 0.0050 mglL 0.2500 104 85-115 Zinc 0.270 0.030 mgiL 0.2500 108 85-115 Batch P6L0279 - 200.7 Blank (P61-0279-131_K1) Prepared & Analyzed: IW6116 Copper BRL 0.010 mglL LCS (P6L0279-BSI) Prepared & Analyzed: 12/16/16 Copper 0.260 0.010 mglL 0.2500 104 85-115 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.D. Box 240543 - Charlotte, NC 28224.0643 Phone: 704I52"364 - Toll Free Number: 1-8001529-6364 - Fax: 70415254409 Page 19 of 21 Full -Service Analytical & &:k-_iR ISMEnvironmental Solutions 7 ADORAT ES RIG Level dl QC Report 12/20/16 GTA Associates, Inc. Attn: Dave Mazorra 710 Peninsula Lane, #B Charlotte, NC 28273 General Chemistry Parameters - Quality Control Project: Semi -Annual SW Prism Work Order: 6120060 Time Submitted: 12/2/2016 10:00MAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P6L0075 - NO PREP LCS (P6L0075-BS1) Prepared & Analyzed: 12/02/16 pH 6.65 pH Units 6.880 100 98.5-101.5 Duplicate (P61_0075-DUPI) _ Source: 6120060-01 Prepared & Analyzed: 12/02/16 pH 6.45 pH Units 6.42 0.5 10 Batch PK0153 - NO PREP Blank (P61-0153-131-K1) Prepared & Analyzed: 12/08/16 Total Suspended Solids BRL 5.0 mglL LCS (1561-0153-13SI) Prepared & Analyzed: 12/08/16 Total Suspended Solids 480 5.0 mg1L 477.0 100 90-110 Batch P6L0251 - NO PREP Blank (1261-0251-BI-M) Oil & Grease (SGT-HEM) BRL Prep Method: 608 red & Analyzed: 12/14/16 5.0 mg1L Sample Extraction Data Lab Number Batch Initial Final DatelTime 6120060-01 P61-0072 1000 mL 10 mL 12/05/16 12-50 Prep Method: 625 Lab Number Batch Initial Final DatelTime 6120060-01 P61_0113 1000 mL 1 mL 1ZI07/16 9:10 Prep Method: 200.7 Lab Number Batch initial Final DatelTime 6120060-01 P61_0279 50 mL 50 mL 12/16/16 7:45 6120060-01 P61_0191 50 mL 50 mL 12/12/16 7:40 Prep Method_ 624 Lab Number Batch Initial Final Date/Time 6120060-01 P61-0234 10 mL 10 mL 12/13/16 12:39 OG This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001629-6364 - Fax: 70415254409 Page 20 of 21 S FullService Analytical R Environmental Solutions LARORATORMS, INC. 449 Springbrook Road • Charlotte, NC 28217 Phone 7041529-6364 - Fax: 7041525.0409 Client Company Name: 'I Report To/Contact Name; Reporting Address: ,its s,.-, L-ri �r CiHAM OF CUSTODY RECORD PAOE _� OF J_ QUOTE 9 TO ENSURE PROPER BILLINNO: Project Name:s�rk ,iimkltss, -5cwt,I-r°rmoc`l -tAJ Short Hold Analysis: (Yes) fInQ UST Project: (Yes) (1tO *Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) provisions aagor QC Requirements Invoice To:�" Address: _ Phone: 7c ,iS;''5Z 3sA Fax (Yes) (1616): Purchase Order No./BIIling Reference 3.57e 17 3 f3� Email Address: _ �Is�l Q tl„i' }� �6'LemRequested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ s Days EDD Type: PDF Excel Y Other �"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ RushMust Be re Ap Work Site Location Name: a� ir'9 % ' Samples received after 14:00 will be processed next business day. Site location Physical Address: MIS- 3" I° Turnaround time is based on business days, excluding weekends and holidays. {SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES (SEE �'� RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TO BE FILLED IN BY CLIENTISAMPL.ING PERSONNEL Certification: NELAC DOD FL NC c°�B Scoved OTHER NIA Water Chlorinated: YES, NO - Sample Iced Upon Collection: YES. NO CLIENT DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER O, SLUDGE SAMPLE CONTAINER PRESERVA• TIVES ANALYSIS REQUESTED m �O' ! 0 "Q REMARKS REMARKSSAMPLE �> 3m �q1� ,�I� PRISM !D NO "TYPE SEE BELOW NO. SIZE :- - µ _ Sampler's Signature Sampled By (Print Name) Affiliation Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. et nqu d B Received By: (Signature) ate taryoursAdditional Comments: Relinquished By: (Signature) Reeeivad By: S gnature) Date �.,�6., Relinquished By: Signature Received For,9trsmEabo esge., ale 6L �� i `���r� Method of Shipment: NOTE' ALL AMPLE COOLERS SHOULD BE TAPED SHUT VVITl�t- USTODY SEALS FOR TRANSPORTATION TO HE LAB RATORY. CO Group No. r SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CQ"NTIL RECEIVED AT THE LABORATORY. SlteArrival,Tlme _' - Site Drj1 Tlure Ttme FIe4d Tech L] Fed Ex ❑ UPS O Hand-dellvered ❑ Prism Field Service ❑ Other 47 NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: ' ' QNC❑SC� ANC ❑SC I oNC ❑SC oNC ❑! oNC ❑SC ❑NC❑SC ❑NC ❑5C ❑NC ❑SC ❑NC ❑SC TERMS & , nlairinlbl *rr%hNTAIK1C0 TV0= r%.nnFQ. A = Amhor r = r..IAAr r;= C;lass P = Plastic: TI_ = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted January 17, 2017 CERTIFICATE OF COVERAGE NO. NCG03-0 &_ SAMPLE COLLECTION YEAR 2016 FACILITY NAME Select Stainless Products, LLC SAMPLE PERIOD ❑ Jan -June ® July -Dec Monthly' , (month) COUNTY Mecklenburg_or _ PERSON COLLECTING SAMPLES David Mazorra DISCHARGING TO CLASS ❑0RW ❑HQW ❑Trout ❑PNA LABORATORYErism Laboratories Lab Cert. # 402 RECEIVED ❑Zero -flow ❑Water Supply [:]SA Comments on sample collection or analysis: BAN 2 5 2017 ❑Other Class C - SecondEl[y Recreation CENTRAL FILE' PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 �l Part A: 5tormwater Benchmarks and Monitoring Results DWR SECTION ❑ No dischas period?2 Outfall No. Date Sample Collected' Imo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Polar 0&G/ l To troleum d arbons AW Total Toxic Organics5 Benchmarks =_=> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 5 / 1 mg/L SW-1 12/01/16 0.43 7.8 6.4 0.017 <0.0009 0.10 <5. 0.15 SW-2 12 05 16 < < <5.0 <0.01 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. A See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total .Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." David R. Mazorra Name (Print name) Senior Engineer Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L". where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' N/A Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:41/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 I Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for Tf0 monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit: For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TfO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." David R. Mazorra Name (Print name) Senior Engineer Title kDrint titlK) ) 11 (Signature) (D te) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on final and one copy of this DMR including all "No Dischar e" reports, within 30 days of receipt of the lab results Lor at end of monitoring eriod in the case of "No Discharge" -reports) to. Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are signjficant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permit Date:11/1/2012-10/31/2017 t (? 17 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit. http: jjportal.nc ennorg/webAr/names-stormwaterl Permit No.: N/�_/_/^/`/!/_/_/ or Certificate of Coverage No.; Facility Name: Select Stainless Products, LLC County: Mecklenburg Phone No, 704-841-1090 Inspector: David Mazorra Date of Inspection:-12-1-9njr Time of Inspection: j?•nn pm Total Event Precipitation (inches): 0.43 (24 hr) Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ® Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm even t" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatureAcerti"at this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Pagel of 2 SWU-242, Last modified 7/31/2013 1. Outfall Description: Outfall No. SW-1 Structure (pipe, ditch, etc.) Pipe Receiving Stream: Wet weather ditch, eventually discharges to McAlpine Creek Watershed Describe the industrial activities that occur within the outfall drainage area: Waste 1 scrap storage, loading / unloading of materials, vehicle parking 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Clear 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 10 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: C, 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 01 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes CN_)o 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Slight erosion at pipe outlet, likely caused by forceful flow from the roof, not pollutants. Note. Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 7/31/2013 STORM WATER SITE COMPLIANCE EVALUATION FORM SELECT STAINLESS PRODUCTS, LLC MATTHEWS, NC Date: 12:00 pm 12-5-2016 Inspector: David Mazorra Weather Conditions (indicate any recent precipitation and current conditions, conduct inspection under dry weather conditions): Cloudv. --50 dearees F. 9 hours since last rain event. DIRECTIONS: Check areas below for evidence of pollutants entering storm water system. If the condition of an area is not acceptable, note why and list corrective actions to be taken. Document all follow-up action. Maintain a record of inspections by filing this document in Appendix B of this SWPPP. Activity/Area Condition Comments, Work Required (Good or Not Acceptable) to Correct 1. Loading Bay 1 (LBI) • Signs of Leakage to SDs Good No work required 2. Loading Bay 2 (LB2) • Signs of Leakage to SDs Good No work required 3. Storm Drain I (SDI) • Signs of Pollutants Good No work required 4. Storm Drain 2 (SD2) Signs of Pollutants Good No work required 5. Storm Drain 3 (SD3) • Signs of Pollutants Good No work required 6. Waste Bins and Trash All containers in good shape Compactor no evidence of spillage or • Containment Integrity discharge No work required • Evidence of Spillage • Evidence of Discharge Activity/Area Condition Comments, Work Required (Good or Not Acceptable) to Correct 7. Metal Scrap Storage • Evidence of Discharge No evidence of discharge No work required 8. Wood Scrap Storage • Evidence of Discharge No evidence of discharge No work required 9. Roof Drain Exits • Signs of Pollutants Good, no signs of pollutants No work required 10. Outfall SW1 Minimal water flow is present in • Dry Weather Flow Outfall SW-1. Water is visible in • Condition the wet weather ditch with slow No work required • Color, Sheen, Foam, flow. Water is clear with no Staining, etc. obvious sheen, foam, staining, PIC 11. Outfall SW2 Minimal water flow is present in • Dry Weather Flow Outfall SW2. Water is visible in the • Condition wet weather ditch with slow flow. No work required • Color, Sheen, Foam, Water is clear with no obvious Staining, etc. sheen, foam, staining, etc. Notes: 1. Follow-up inspection required for any conditions found not acceptable. 2. Description of potential pollutants and pollution prevention measures and control in SWPPP to be revised in accordance with inspections. Narrative description of storm water control system, outdoor plant equipment, and systems: The ADCs listed above appear to be in good condition. A neighboring industrial facility, Stronghaven Container Company, located upstream of SSP, is suspected to be a significant source of stormwater pollutants. A cyclone, which is out of service, and miscellaneous piping on the roof of SSP,constructed of galvanized metal, may also contribu to the elevated levels of zinc found in discharge. SSP will await INC DWQ recommendations upon inspection of neighboring facility CERTIFICATION: "I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. I, Signature/Position /J - ,/ Date ANow&A—a NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: httortal.nc enr.or web lr n des-stor-mwater Permit No.: N/C/_/_/_/�/_/_/_/ or Certificate of Coverage No.: Facility Name: Select Stainless Products, LLC County: Mecklenburg Phone No. 704-841-1090 Inspector: David Mazorra Date of Inspection: 12-5-2016 Time of Inspection: 12:00 PM Total Event Precipitation (inches): 0.89 (24 hr) Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) © Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm even t"or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I ctify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Page 1 of 2 SWU-242, Last modified 7/31/2013 1. Outfall Description: Outfall No. SW-2 Structure (pipe, ditch, etc.) Pipe W Receiving Stream: wet weather ditch, eventually discharges to McAlpine Creek Watershed Describe the industrial activities that occur within the outfall drainage area: Minirnal waste 1 scrap storage 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Clear 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): None 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: lO 2 3 4. 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: CD 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Slight erosion at pipe outlet, likely caused by flow / force of discharged water, not pollutants. Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, last modified 7/31/2013 STORM WATER SITE COMPLIANCE EVALUATION FORM SELECT STAINLESS PRODUCTS, LLC MATTHEWS, NC Date: 12:00 pm 12-1-2016 inspector: David Mazorra Weather Conditions (indicate any recent precipitation and current conditions, conduct inspection under dry weather conditions): Clear and sunny, —70 degrees F. 18 hours since last rain event. DIRECTIONS: Check areas below for evidence of pollutants entering storm water system. If the condition of an area is not acceptable, note why and list corrective actions to be taken. Document all follow-up action. Maintain a record of inspections by filing this document in Appendix B of this SWPPP. Activity/Area Condition Comments, Work Required (Good or Not Acceptable) to Correct I. Loading Bay 1 (LB1) • Signs of Leakage to SDs Good No work required 2. Loading Bay 2 (LB2) Signs of Leakage to SDs Good No work required 3. Storm Drain 1(SDi) • Signs of Pollutants Good No work required 4. Storm Drain 2 (SD2) • Signs of Pollutants Good No work required 5. Storm Drain 3 (SD3) • Signs of Pollutants Good No work required 6. Waste Bins and Trash All containers in good shape Compactor no evidence of spillage or • Containment Integrity discharge No work required • Evidence of Spillage • Evidence of Discharge Activity/Area Condition Comments, Work Required (Good or Not Acceptable) to Correct 7. Metal Scrap Storage Evidence of Discharge No evidence of discharge No work required S. Wood Scrap Storage • Evidence of Discharge No evidence of discharge No work required 9. Roof Drain Exits • Signs of Pollutants Good, no signs of pollutants No work required 10. Outfall SW1 Minimal water flow is present in • Dry Weather Flow Outfall SW-1. Water is visible in • Condition the wet weather ditch with slow No work required • Color, Sheen, Foam, flow. Water is clear with no Staining, etc. obvious sheen, foam, staining, 11. Outfall SW2 No water flow is present in Outfall • Dry Weather Flow SW-2. No water is present in the Follow up scheduled for • Condition wet weather ditch due to the large the next rain event. • Color, Sheen, Foam, aggregate base of the railroad Staining, etc. tracks. Notes: 1. Follow-up inspection required for any conditions found not acceptable. 2. Description of potential pollutants and pollution prevention measures and control in SWPPP to be revised in accordance with inspections. Narrative description of storm water control system, outdoor plant equipment, and systems. The AOCs listed above appear to be in good condition. A neighboring industrial facility, Stronghaven Container Company, located upstream of SSP, is suspected to be a significant source of stormwater pollutants. A cyclone, which is out of service, and miscellaneous piping on the roof of SSP,constructed of galvanized metal, may also contribu to the elevated levels of zinc found in discharge. SSP will await NC DWQ recommendations upon inspection of neighboring facility. CERTIFICATION: "I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violatioA. 117 Signature/Position Date Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 6-02-2016 CERTIFICATE OF COVERAGE NO. NCG03Q .fL _L.L FACILITY NAME Select Stainless Products, LLC COUNTY Mecklenburg PERSON COLLECTING SAMPLES Geoffrey Gilbert LABORATORY ESC Lgb Science Lab Cert. # 41 - Charlatte Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results RECE! V et) JUN 0 9 2016 CEN7WF,k Fr SAMPLE COLLECTION YEAR 2016 DWR SECTrpN SAMPLE PERIOD KI;Jan-June ❑ July -Dec or{`Monthly+ _ (month) DiSCHARGING TO CLASS ❑ORW ❑HQW ❑Trout QPNA xvor ❑Zero -flow ❑Water supply ❑5A Ar ❑other reation PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 —) 11 No discharge this period?1 Outfall No. Date Sample p Collected) (mo/dd/ r) 24-hour rainfall amount, Inches Total Suspended Solids p H, Standard units Copper Lead Zinc Hon -Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks =_=> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SW-1 05/17/16 0.55 33.1 6.9 <0.005 <0.005 0.0574 <5.26 <0.01 SW-2 c <0.005 0,1300 < <0.01 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benam I ex `eedad a `f f t "� rameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge meri o eckmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligib a f8r a fiver ofthe rain gauge requirement, " See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 F6cilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my Inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility Is Implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." N/A Name (Print name) Title (Print title) (Signature) (Hate) (Vote: Results must be reported in numerical format. Do not reuart Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non-numerlcal format. When results are below the applicable limits, they must be reported in the format."<XX mg&", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. (Vote: If you report a sample value in excess of the benchmark, you must Implement Ver 1, Tler 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new ail per month. No discharge this period?2 NIA Outfall No. Date Sample Collected' (mo/dd/ r) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (5GT HEM) Total Suspended Solids pH Benchmarks =a=> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 910 SU Footnotes from Part A also apply.to this Part B * See General Permit text, Table 5, Identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value In excess of the benchmark, you must Implement Tier 1, Tler 2, or Tier 3 responses. See Genera! Permit text. FOR PART A AND PART B MO TO INGRESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an arlainal and one cogy of this! d!n o b s resub lor at end at nito in In he cow of No Q&dW=A'=j2iTs) o: Division of Water Quality Attn. DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance with a system designed to ass a tha le rsonnei properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or th a sons irectl sponsible for gat ring the information, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. a a e th t ere r si nifi ant pen Y s for submitting false information, including the possibility of fines and Imprisonment for knowing violations." 6' /lv �Slgnature of Permitteey (Date) Permit Date; 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 4ijol000-SELECT STAINLESS PROOLICTS, LLC December 7, 2015 Division of Water Quality RECEIVED 1617 Mail Service Center DEC 10 Z015 Raleigh, North Carolina 27699-1617 CENTRAL FILES Re: Semi -Annual Stormwater Sampling at Select Stainless Products, LOAZAJI,W) Dear DEQ- Division of Water Quality: Select Stainless Products, LLC (SSP) retained GTA Associates, Inc. (GTA0bencfor -annual stormwater sampling at our Matthews, NC facility. The sampling is requireivision o Water Quality General Permit No. NCG030000. SSP's Certificate of Coverage N63. GTA collected samples at the facility from the two permitted outfalls (SW-hown permit outfalls in attached Site Drainage Map) on October 27, 2015. The results ot (summarized in Table 1) indicate that SW-1 was in exceedance of the DEQfor both copper and zinc, with levels of 0.134 mg/L and 1.38 mg/L respectively. SW-2 was in exceedance of the DEQ benchmark for zinc with a concentration of 8.24 mg/L. Tier 1 tasks, as outlined in NCG03000, were subsequently completed by SSP/GTA. GTA also collected additional stormwater samples on November 18, 2015 in an effort to determine the source of the exceedances. Four (4) samples were collected and analyzed for copper and zinc. The locations of the additional sampling sites (SW-1 through S W4) are displayed in the attached Site Drainage Map, (the labeling of these sampling sites does not correspond with the original permitted SW-1 and SW-2). Sampling point SW-1 was selected because of its location immediately down gradient of SSP's neighboring facility, Stronghaven Containers Company (SCC). Locations SW-2, SW-3, and SW4 were chosen to track the metal concentrations along the southern and eastern sides of the SSP facility. The results of the additional sampling are summarized in Table 2. The stormwater collected from SW-1 (immediately down gradient from SCC) registered the highest concentrations of both copper and zinc, with readings of 0.034 mg/L and 1.13 mglL respectively_ Amer analyzing the sampling results and inspecting the surrounding topography, it is SSP's opinion that the neighboring SCC facility appears to be the primary contributor to the excessive metal concentrations detected in the stormwater runoff. SSP intends to continue in 2016 with its semi-annual stormwater sampling and will advise DEQ of subsequent sampling results. In the interim sho have any quest' dlor comments following review of the attached, please do not hesitate to calIMMUN S- 1 Yh-aLrd J. Murphy Facilities Engineer (302) 653-3000 ext. 3087 11145 Monroe Rd. Matthews NC. 28105 Phone: 888-843-2345 Fax: 704.841.1590 www.selectstainless.com Table 1 Select Stainless Products, LLC Stormwater Benchmarks and Monitoring Results 10-27-2015 GTA # 35151367 Page 1 of 1 Outfall No. Date Sample Collected 1 (mo/dd/yr) 24-hour rainfall amount (inches Total Suspended Solids (mg/L) pH Standard Units Copper mg/L} Lead mg/L Zinc m L) Non -Polar O&G/ Total Petroleum Hydrocarbons mg/L) Total Toxic Organics mg/L Benchmarks => -- -- 100 mg/L 6.0 - 9.0 0.007 0.03 0.067 is 1 SW-1 10/27/2015 0.90 24.9 7.1 0.134 < 0.005 1.38 < 5.0 < 0.01 SW-2 10/27/2015 0.90 5.0 6.3 < 0.005 < 0.005 8.24 < 5.0 < 0.01 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Highlighted values are in exceedance of NC 0EQ benchmarks Table 2 Select Stainless Products, LLC Stormwater Benchmarks and Monitoring Results 11-18-2015 FddjyrjJ 24-hour rainfall Outfall No.amount CopperF inches m /,U ) Wdenchmarg� �DT007� llllllllllllll)0?067� 5w-1 11/18/2015 1.10 O:b34'" - .1.13 SW-2 11/18/2015 1.10 "0A001". "; ` 0.483 SW-3 11/18/2015 1.10 < 0.005 0.423 SW-4 11/18/2015 1.10 0.0072 0.231 HighligF ted values are in exceedance of NC DEQ benchmarks GTA # 35IS1367 Page 1 of 1 c xa +ww rrnw .olw r .a • .1 a* xr vc ora, '.am.. i avw 30"WHa RUID r«,our� .Iw.>r '.ulrlu� wrerlma.n ,`•• •'•�• • ,>._, � 3 [ L`� a �'�1 oil'S17foow MINNA M3139 '7M'S31Yg0iilUAo _ `� ` ' ,I",y, '•'• +,,G L�y9> � � 2" 1 Yg7oN3Vl7MAx5 +V 5 oor M(v )i3 �661 oo[Mnu[ikM VpO r tecu rwwm "rVI 711d011 ""r" +�.a+ -,•, ,,,,n'� u" �� '¢, a =une •srnnnmrxaa me .LYMCO lYIKINNG M1] ffMV 1rJ VILO3o • 1 �,,.y, 1 "„ L c<"pa S� �' r�` '" ti nhi sunaoRsrVZO nv MWnw.nxw hrrwW'm'IL 4r wia'aw�wlYrriusrw Ya.4.rsww"+r�� �/: ea"p",i�.."w'��' P m >W� I _...!� a` •`yn =M�' � ,.•V .rrM + yr..n•�....w„.,:", `"'...a:` OI I gtYYS� • �•l l�w,^«�".p'rr"p�~) r• ,_= :— n n� wr.v °""� I C'M a =t [SL �/�/ • r �� � ,/. P 3 '� � � ;A VI 1 _ i � " ...q 1 •A� i � it 1 ' M" �+n. � N _ Ir tY ➢r Y`V• '.t =gf�•�rl - — \ ` e.rr irZ7: Air+ , tP i, 1 m�eKrr.;rszs . wsr ii'ai cov--Y+Y.e'C:tx »wr n Central Files: APS — SWP. 8/5/2015 r Permit Number NCG030663 Permit Tracking Slip Program Category Status Project Type NPDES SW In review New Project Permit Type Version Permit Ctassification Metal Fabrication Stormwater Discharge COG COC Primary Reviewer bill.diuguid ' Coastal SWRule Permitted Flow Facility AUG 2 6 2915 CENTRAL FILES DWR SECTION Permit Contact Affiliation Facility Name Major/Minor Region Select Stainless Products, LLC Minor Mooresville location Address County i I W Monroe Rd Mecklenburg Matthews NC 28105 Owner Owner Name Select Stainless Products I.I.0 Facility Contact Affiliation George Thrower 11145 Monroe Rd Matthews NC 28105 Owner Type Non-Govemrnent Owner Affiliation Richard Murphy 100 Industrial Blvd Dates/Events Clayton DE 19938 Scheduled Orig Issue App Received Draft Initiated issuance Public Notice Issue Effective Expiration 7i712015 Regulated Activities Metal products manufacture Wfall 1 $/k.-1 i i/.5K%- 1 cl :?1'r -9 Requested /Received Events RO staff report received 7/16/15 y RO staff report requested 7113/15 Waterbody Name Streamindex Number Current Class Subbasin McAlpine Creek (Waverty Lake) 11-137-9 C 034)8-34 2 A i2. ENR North Carolina Department of Environment and Natural Resources Pat McCrory Donald R. van der Vaart Governor Secretary August 5, 2015 Mr. Richard J. Murphy, Facilities Engineer Select Stainless Products LLC P.O.Box 1129 Clayton, Delaware 19938 Subject: General Permit: No. NCG030000 Select Stainless Products LLC COC No. NCG030663 Mecklenburg County Dear Mr. Murphy: In accordance with your application for a discharge permit received on July 7, 2015, we are forwarding herewith the subject certificate of coverage (COC) to discharge under the subject state - NPDES general permit This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection Agency dated October 15, 2007 (or as subsequently amended). If any parts, measurement frequencies, or sampling requirements contained in this permit are unacceptable to you, you have the right to request an individual permit by submitting an individual permit application. Unless such demand is made, this certificate of coverage shall be final and binding. Please take notice that this certificate of coverage is not transferable except after notice to the Division of Energy, Mineral and Land Resources (Division). The Division may require modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal requirements to obtain other permits which may be required by the Division or permits required by the Division of Water Resources, Coastal Area Management Act or any other federal, state or local governmental permit that may be required. If you have any questions concerning this permit, please contact Bill Diuguid, Stormwater Program Planner at telephone number (919) 807-6369. Sincerely, for Tracy E. Davis, P.E., CPM, Director Division of Energy, Mineral and Land Resources cc: Mooresville Regional Office Central Files Stormwater Permitting Unit Files Attachments Division of Energy, Mineral, and Land Resources Energy Secclion - Geological Survey Section • Land Quality Section 1612 Mail Service Center, Raleigh, North Carolina 27699-1612.919-707-9200 / FAX: 919-715-8801 512 North Salisbury Street, Raleigh, North Carolina 27604 - Intemet: hgp:lloortal.ncdenr.org/webl An Equal Opportunity 1 Affirmative Action Employer — 50% Recycled 110% Post Consumer Paper STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF ENERGY, MINERAL AND LAND RESOURCES GENERAL PERMIT NO. NCG030000 CERTIFICATE OF COVERAGE No. NCG030663 STORMWATER DISCHARGES NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Select Stainless Products, LLC is hereby authorized to discharge stormwater from a facility located at Select Stainless Products, LLC 11145 Monroe Road Matthews Mecklenburg County to receiving waters designated as an unnamed tributary to McAlpine Creek, a Class C waterbody to Catawba River Basin; in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, 11, III, IV, V and VI of General Permit No. NCG030000, as attached. This Certificate of Coverage shall become effective August 5, 2015. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day August 5, 2015. 6) 14-�Aj 4ve--� for Tracy E. Davis, P.E., CPM, Director Division of Energy, Mineral and Land Resources By Authority of the Environmental Management Commission Ln 0 to �O O n L m a cn Ln v m C) z m z C m r m m r m r n z o a o z m m = Z O 3 v c m —1 Cn z a r- 0 ^' d go HIS C � (n m 0 G N z 0 CL w 6-i m A. NCDENR �ar Ermummou �fftmm� NOTICE OF INTENT National Pollutant NCG©3000D: Division of Water Quality / Surface Water Protection Section National Pohutant Discharge Elimination System �D U JUL . ° 7 zo r$ f � STORMWATER DISCHARGES fas coverage under General Permit classified as: SIC (Standard Industrial Classification) 335 Railing, Drawing, and Extruding of Nonferrous Metals SIC 3.98 Metal Heat Treating SIC 34 Fabricated Metal Products SIC 35 Industrial and Commercial Machinery SIC 36 Electronic and Other Eiecbrical Equipment SIC 37 Transportation Equipment SIC 38 Measuring, Analyzing, and Controlling Instruments For gu"dons, please c6 ntW the DWQ Regional Of xe for your amaL Sae page 4. (Please print or type) 1) Mailing address of ownerloperator (address to which all permit correspondencewill be mailed): Name SCuccz S'TK { WtAslm f gouA[ -r L I i Mt'7 —.Street Address fQ BC% I Ig City G State ZIP Code Telephone No. 3&�2 &S3 - 3827 Fax: 3 bZ (IrS3 - 2'a-61z 2) Location of facility producing discharge: Facility Name 5g—Ler-T SM IL3LESS ALdhuexc ,r. L-L-C Facility Contact —r"-a0W V4L-- Street Address _ l Wa— 1hQAJAO A1C0. _ -- City ryJA-7Ttt . 'ic State A?e Z1P Cods N'lb_ S' _ County %hLc,Gll�nlRct�G _ -_- Telephone No. _ gH 1-! O ark Iwo Fait gY- 144 ► - t SQ Emall _a..t✓1.,..,� t..p� ,� t�{s�# �S • covet 3) Physical Location infom aWrr Please provide a narrative description of how to gat to the facility (use street distance and direction from a roadway intersection)- TiMGE Aotd _ state road numbers, and is copy of a county map or USGS quad sheet. with the fadiity doey located must be submfded with this app€ w iom) 4) Latitude 3 e 4' 91.3 t Longitude - 100 ti s r 3`i .`) ; (deg, min, sec) Pagel of 4 SWU-21"71405 Last revised 7114M r NCGO30000 N.O.L 5) This NPDES Penult Application applies to which of the following: ❑ New or Proposed Facility Date operation is to begin K Usting 6) Standard Industrial Classification: Provide the 4-digit Standard Industrial Classification Corte (SIC Code) that describes the primary industrial activity at this fadliiy- SIC Code. 3 �i 4 t 7) Provide a brief narrative description of the types of industrial activities and products nulmdac:tumd at thisfacility: crr4uirF UT_ SUzk to-s- S) Discharge points I Receiving waters: s- u116. 03 - 0 - 3'Sf C.L As s G How many discharge points (dies, pikes, channels, eettc.) convey storrnwater from the property? �. What is the name of the'body or bodies of water creels, stream, rimer, lake, etc.) that Me'facl . stormwater discharges end up in? pwA Receiving water clessification: Is this a 303(d) Ilsted stream'. , yES Has a TMDL been approved for this watershed? IffS If the site stwmwatar discharges to a separate storm sewer system, name the operator -of the separate storm sewer system (e.g. City of Raleigh municipal storm sewer). w/f7 9) goes this facility have any other NPDES permits? © Yes if yes, list the permit numbers for all current NPDES permits for this fa c@ty. 10) Does this facility have any Non -Discharge permits (ex: recycle permit)? No 0 Yes If yes, fist the permit numbers far all current Non -Discharge permits for this facility: 11) Does this facility employ any best management practices for starrnwater control? 14 No ❑ Yes (Show any structural BMPs on the site diagram-) If yes, please.iariefly describe: 12) Does tMs facility have a SWnnwater Pollution Prevention Plan? 1Q No ❑ Yes If yes, when was it implemented? 13) Are vehicle maintenance activities occurring at this facility? No ❑ Yes 14) Hazardous Waste: a) Is this facility a Hazardous Waste Treatment, Storage, or disposal Facility? )1 No ❑ Yes Page 2 of 4 S U-21&071408 last revised 7114M " NCG030000 N.Q.I. b) Is this faciliity a Small Quantity Generator (less than 1000 -kg. of hazardous waste generated per month) of hazardous waste? 9 No ❑ Yes C) Is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste generated per month) of hazardous waste? Id No © Yes d) . Is hazardous waste stored in the 100 year flood plain? PINO ❑ Yes if yes, include information to demonstrate protection from flooding. e) If you answered yes to questions b. ore., please provide the following inform *m: Type(s) of waste: How is material stored: Where is material stared: How many disposal shipments per year. Name of transport I disposal vendor Vendor address: 15) Certification: North Carolina General Statute 143-215.BB (i) provides that: Any person wtm toroamlragfy makes any false Aatnent, Win, or eertilk2rlion in any application, mnard, report, plan, or other document filed or required to be maintained under this Art)c le or a ode implementing this Article; or who Vwwtngty makes a false stetsment of a material fact in a rainmaking proceeding or contested case under this Article. or who falsifies, tampers wRh, or kna ngty renders tnaomrate any recording or mondortmtg device or method required to be operated or.maimta{ned under this Artide or rules of the Commission implernenting this Article shall be guilty of a Dass 2 misdemeanorwhich nW inckWe a lure riot to ameed ten thousand dollars ($10,000). I hereby request coverage under the referenced General Permit i understand that coverage under this permit will constitute the permit requirements for the discharges) and is enforceable in the same mariner as an individual permit. I certify that I am familiar with the information contained in this application and that to the best of my knowlexlge and belief such information is true, complete, and accurate. Printed Name of Person Signing: QtCb}Arft_D 3. k u"H `Y This Notice of Intent must be accompanied by a check or money order for $100.00, made payable to: NCDSNR Page 3 of 4 SWU-21 "71403 Lae revised 7114/06 z NCGO30000 N.0.11. Freal Checklist This application will be nftmed as incomplete unless all of the following items have.been Included: � Thisfmr $100 ied application all s''�N�. P:p .zl;t � 4 11 aZ, ! � pp Ming documents. A site diagram showiM, at a minimum, (wdsting or proposed}; (a) outline of drange areas, (b) st rmwater management structures, (c) location of.st irrmwater-outfalls corresponding to the drainage areas..(d) runoff cohveyance,featuires. (a) areas where materials are stared, (f) impendws areas, (g) site property lines- Copy of county map or USGS quad sheet with the location of the facility clearly marked on the map - titian the entire package to: atormwater Permbrig Unit Division of Water Quality 1617 Mail Service Center Raleigh, North Carolir a 27699-1617 Note The subrr&mlo a of this document does not guarantee coverage under the General Permit. For ques#mnsY please contact the DING Regional Office for your area. On Ft"llonal Office Contact Inforrrmation: Asheville Office...._ (828) 2964500 Fayetteville Of ioe .-. (910) 433-3300 Mooresville Office ... (704) 663-7599 Raleigh Office _._..... (919) 791-4200 Washington Office ... (252) 946-Mi Wilmington Office,...(910) 7W7215 Winston-Salem --.... (336) 771-6M Central Office ___......(919) 807-6300 Page 4 of 4 SWU-218-07i4M Last mined 7114MB Semi-annual - r .,, , , � Monitoring Report A, for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG03Q Q Q 3— SAMPLE COLLECTION YEAR 2015 FACILITY NAME Select Stainless Products, LLC SAMPLE PERIOD ❑ Jan -June @ July -Dec COUNTY Mecklenburg or ❑ Monthly' lmonthl PERSON COLLECTING SAMPLES Geoffrey Gilbert DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY Pace Analytical Lab Cert. # 40 - Asheville. #12 Huntersville []Zero -flow ❑Water Supply []SA Comments on sample collection or analysis: ❑Other Qlazus Q - Secmdau Recreation Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids PH, Standard units Copper Lead Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics, Benchmarks - - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SW-1 10/27/15 0.90 24.9 7.1 0.134 <0.005 1.38 <5.0 <0.01 SW-2 10/27/15 ago 6.3 < p < < <0.01 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics Into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." PI C; km r% T. Rk,d J*N Name (Print name) .. N/A Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX ma/L where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note, if you report a sample value In excess of the benchmark, you must Implement Tier 1, Tler 2, or Tler 3 responses. See General Permit text. Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period ?2 N/A putfall No. Date Sample Collected' (mo/dd/ r) 24-hour rainfall amount, Inches3 Non -polar 0&G/TPH by EPA 1664 (SGT-HEM)Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part 8 * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: !f you report a sample value in excess of the benchmark, you must implement Tier 1, rer 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an orlainal and one copv of this DMR, lncludina all "No Discharae" reports, within 30 days_of receipt of the lab results for at end of monitorina Period In the case of "No Discharge"XRprW) Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that ualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or se sons tly re onsibte for gathering the information, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I dam are^t the �i a gnificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permit Date: 11/1/2012-10/31/2017 ( Date) SWU-245, last revised 10/25/2012 Page 3 of 3 Compliance Inspection Report Permit: NCGO30663 Effective: 11/16/17 Expiration: • 10/31/18 Owner. Select Stainless Products LLC SOC: Effective: Expiration: Facility: - Select Stainless Products, LLC County: Mecklenburg 11145 Monroe Rd Region: Mooresville Matthews NC 28105 Contact Person: George Thrower Tittle: Phone: 704-841-1090 Ext.141 Directions to Facility: Take Route 51 (Matthews Township Parkway) turn north on Charles Street, follow to SSP facility_ System Classifications: Primary ORC: Certification: Phone: Secondary ORC(s): On -Site Representatne(s): Related Permits: Inspection Date: 07/25/2018 Entry Time: 12:15PM Exit Time: 12:40PM Primary Inspector: James D Moore Phone: Secondary tnspector(s): Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Metal Fabrication Stomwwater Discharge COC Facility Status: Compliant Not Compliant Question Areas: 0 Storm Water (See attachment summary) Page: 1 permit: NCG030663 Owner - Facility: Select Stainless Products LLC Inspection Data: 07/2512018 Inspection Type: Compliance Evaluation Reason for Visit: Routine Inspection Summary: The facility closed in June and all the contents were auctioned off in early July.l recommend permit rescission at this time. Page: 2 s F ya, t Environmental Quality Division of Energy, Nfineral & Land Resources Land Quality SectiordSturmwater Permitting Program National Pollutant C7i; harge Elimination System RESCISSION REQUEST FORA POR AGENCY USE ONLY Rate Received Year Mwtri tin Please fill out and return this form if you no longer need to maintain your NPDES stormwater permit. ij Enter the permit number to which this request applies: Individual Permit (of) Certificate of Coverage 2) Owner/Facility Information: • Final correspondence will be mailed to the cddreu noted below Owner/Facility Name Select Stainless products, LLC Facility Contact Mr. Richard J. Murphy Street Address 11145 Monroe Rd City Matthews --- State NC ZIP Code 28105 County Mecidenburg E-mail Address rmurt,hy@"legrp•wm Telephone No. 302 632 - 8770 Fax: 302 653 - 2702 3) Reason for rescission request (This is Leaul information. Attach separate sheet if necessary): ❑+ Facility dosed or is closing on 5/25/18 . All industrial activities have ceased such that no discharges of stormwater are contaminated by exposure to industrial activities or materials. Facility sold to on . If the facility will continue operations under the new owner it may be more appropriate to request an ownership change to reissue to permit to the new owner. ❑ Other: 4) Certification: t, as an authorized ntative, hereby request rescission of coverage under the NPDES Stormwater Permit for the subject facility. m farm Wit r wi the Information contained in this request and to the best of my knowledge and belief such inforp ac te. Signature Date a Pichard J. Murphy Facilities Engineer Print or type name of person signing above Title Please return this completed rescission request form to: Revised 20183aniO DEMLR - Storrnwater Program Dept. of Environmental Quality 1612 ,Mail Service Center Raleigh, North Carolina 27699-1612 APlease consider the environment before printing this e-mail. To better serve our clients, Maser Consulting is pleased to announce it has opened an office in Charlotte, NC. in addition, we have established new services that include Unmanned Aerial System (UAS) and Right -of -Way land acquisition. We're proud to be part of such an Award -Winning company! Click herr to share ktihv you think Maser Consulting is one afthe Best! DISCLAIMER This e-mail is confidential. It may also be legally privileged. If you are not the addressee you may not copy, forward, disclose or use any part of this email text or attachments. !f you have received this message in error, please delete it and all copies from your system and notify the sender immediately by return e-mail. Internet communications cannot be guaranteed to be timely, secure, error or virus free. The sender does not accept liability for any errors or omissions. Any drawings, sketches, images, or data are to be understood as copyright protected. V FOR AGE Division of Energy. Mineral & Land Resources pate Received �� Year Norcrh [ia Land Quality Section/Stormwater Permitting Program t ' National Pallutant Discharge Elimination System �Jiviri7runF1? find{ Quality RESCISSION REQUEST FORM f Please fill out and return this form if you no longer need to maintain your NPDES stormwater permit. 1) Enter the permit number to which this request applies: individual Permit (or) Certificate of Coverage N _C s [ 03 0 6 6 3 2) Owner jFacility Information; Final correspondence wltt be marled to the address noted below Owner/Facility Name Select Stainless ProdurLs, LLC Facility Contact Mr. Richard J. Murphy Street Address 11145 Monroe Rd City Matthews State NC ZIP Code 28105 County Mecklenburg E-mail Address rmurphY@eag{egro.cczm Telephone No. 302 632T- 8770 T Fax: 302 653 - 2702 3) Reason for rescission request (This is Muired information. Attach separate sheet if necessary): ❑✓ Facility closed or is closing on 5125118 . All industrial activities have ceased such that no discharges of storrnwater are contaminated by exposure to industrial activities or materials. Facility sold to on . If the facility will continue operations under the new owner it may be more appropriate to request an ownership change to reissue to permit to the new owner. ❑ Other: 4) Certification: I, as an authorized ntative, hereby request rescission of coverage under the NPDES Stormwater Permit for the subject facility. rn farm Xpnydacte. r wl the Information contained in this request and to the best of my knowledge and belief such inforMil Signature pate Ri&.,ard J. Murphy Facilities Engineer Print or type name of person, signing above Title Please return this completed rescission request form to Revised 20183an.30 DEMLR - Stormwater Program Dept. of Environmental Quality 1612 Mail Service Center Raleigh, North Carolina 27699-1612 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted June 27 2018 CERTIFICATE OF COVERAGE No. NCG03 0 6 6 3 FACILITY NAME Select Stainiess Products LLC COUNTY _ Mecklenburg PERSON COLLECTING SAMPLES LABORATORY: Lab Cert. t# Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ❑ Monthly' May (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ®Other:_C_ I_ass.C_Secandary Recreation PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -3 ® No discharge this period Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics' Benchmarks 100 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L IS mg/L 1 mg/L ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found In 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility Is implementing the all the provisions of the solvent management plan included In the Stormwater Pollution Prevention Plan." Richard J ur Name (Print name) Facilities EnRineer int l ] (Signature)IrN{vote) Note: Results must be reported In numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be re ort d In the format "<XX mg/L" where XX is the numerical value of the detection limit, reporting limit, etc, in mg/L. Note. if you report a sample Value In excess of the benchmark, you must Implement Tier 1, Tier 2, or Tler 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new all per month. ❑ No dischorge this period?2 Outfall No. pate Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar OSG/TPH by EPA 1664 (SGT-HEM) Total suspended Solids PH Benchmarks is mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 5U Footnotes from Part A also apply to this Part B " See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies: Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text FOR PART AAND _PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART Ii SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE: CONTACT NAME: Khan Zahld Mg1l an r! final and one co o this DMIt Includin a!1 "No Discha e" revolts, within 30 days of receipjLof the fob results for at end of monitoringerlod In the case.of "No Discha e" re orts to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YQu.mi T SIGN THIS CERTIFICATION FOR. ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualifled personnel properly gather and evaluate the Information submitted. Based on my Inquiry of the person or persons who manage the system, or those p S'tllcly responsible fathering the Information, the information submitted 1S, to the best of my knowledge and belief, true, accurate, and complete. I m ar that thork arq significant alties for submitting false information, Including the possibility of fines and Imprisonment for knowing violations." {Signature of Permit Date: 11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted _ . - June 27,_2018 CERTIFICATE OF COVERAGE NO. NCG03 0 6 6 3 FACILITY NAME Select Stainless Products LLC COUNTY _Mecklenburg PERSON COLLECTING SAMPLES LABORATORY: Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018___--- ,_— SAMPLE PERIOD ❑ Jar' -June ❑ July -Dec or ❑ Monthly' Mpy (manthl DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water supply ❑SA ®Other: Class C Secondary Recreation PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this period ?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&GfTotal Total Petroleum Hydrocarbons Toxic Organics' Benchmarks =__> _ - 100 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L ' Monthly sampling (instead of semi=annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. I For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites maybe eligible for a waiver of the rain gauge requirement. `See General Permit, Table 3 identifying the especially sensltive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring -may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Richard J. Muroby _ Name (Print name) Facilities Enizineer nt I } (Signature) (Bate) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, NO, or other similar non -numerical format. When results are below the applicable limits, they must be reported In the format, "cXX m>lt L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note. If you report a sample value In excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SOT -HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L• 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit hate: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART It SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Khan Zahid Wit ail orlainal and one copy of this DMIt lnrludln a!1 "No Dlscha e" reports within 30 da s o rerei t o the lob results or at end o monitarin eriod Base of. "No Discharge" Meortsi to: in the, Division of Water. Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YQg MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or thos rr1s'dir ly responsible forgathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I m ar tfrat th r ark significant alties for submltting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permit Date:11/1/2012-10/31/2017 0 c� CWIA- (Date) SWU-245, last revised 10/25/2012 Page 3 of 3