NCG030625_COMPLETE FILE - HISTORICAL_20171103

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
DOC TYPE
O HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ � � � I
YYYYMMDD

Division of Energy, Mineral, and Land Resources
Land Quality Section / Stormwater Program
w National Pollutant Discharge Elimination System (NPDES)
Energy, Mineral & PERMIT OWNER AFFILIATION DESIGNATION FORM
Land Resources
EWWONMENTAL QUALM (Individual Legally Responsible for Permit)
FOR AGENCY USE ohLY
Date Received
Year
Month Da
Use this form if there has been:
'NO CHANGE in facility ownership or facility name, but the individual
who is legally responsible for the permit has changed.
If the name of the facility has changed, or if the ownership of the facility has changed,
do NOT use this form. Instead, you must fill out a Name -Ownership Change Form
and submit the completed form with all required documentation.
What does "legally responsible individual" mean? RECEIVE®
The person is either:
• the responsible corporate officer (for a corporation); NOV — 3 2017
• the principle executive officer or ranking elected official (for a municipalityle federal or other public
'� R LAND QUALITYagency); STQRMVVATER PERMITTING
• the general partner or proprietor (for a partnership or sole proprietorship);
• or, the duly authorized representative of one of the above.
1) Enter the permit number for which this change in Legally Responsible Individual ("Owner Affiliation")
applies:
Individual Permit (or) Certificate of Coverage
N I C I S I I I I I N. I C I G Q 3 10,(0.Q 151
2) Facility Information:
Facility name:
Company/Owner Organization
Facility address:
A-4 Ids Cooco Ngr0n Amorican Scruiu Cep• eY
1 I i -b 5+ee 1 r G k RJ
Address
OnCwY 1 O+IL N C Z gZ-7 '-
City State Zip
To find the current legally responsible person associated with your permit, go to this website:
http_//deq. ne. gov/about/divisions/energy-mineral-land-resources/energy-mineral-land-permits/stormwater pro uam
and run the Permit Contact Summary Report.
3) OLD OWNER AFFILIATION that should be removed:
Previous legally responsible individual: Aa a k a'tn 9.15Sa n i
First MI Last
4) NEW OWNER AFFILIATION (legally responsible for the permit):
Person legally responsible for this permit:
Cher I I- &rre-
First MI Last
Page 1 of 2
¢.W.t I-o W NFRAF FIL-? 3 N4arch20 l 7

NPDES Stormwater Permit OWNER AFFILATION DESIGNATION Form
(if no Facility Name/Ownership Change)
RIN
Title
11313 Glee-1 Cre k k1
Mailin Arrddress
JV�C_ ZgZ �3
City State Zip
(70q) 50 4 — �o 9 Co ,3 Chi, l . a a r j1e k EO to S. 4414S
Telephone E-mail Ad&6 aGOPCD .0
(IN SaQ -
Fax Number
5) Reason for this change:
Employee or management change
A result of: ❑ Inappropriate or incorrect designation before
❑ Other
If other please explain:
The certification below must be completed and signed by the permit holder.
PERMITTEE CERTIFICATION:
1, (' t? c�j Garrc., — Qri , attest that this application for this change in Owner Affiliation
(person legaley responsible for the permit) has been reviewed and is accurate and complete to the best of my
knowledge. I understand that if all required parts of this form are not completed, this change may not be
processed.
L-7 7)
Signature Date
PLEASE SEND THE COMPLETED FORM TO:
Division of Energy, Mineral, and Land Resources
Stormwater Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
For more information or staff contacts, please call [phone] or visit the website at:
htt p://dgg .nc.go v/about/divisions/energy-mineral-land-resources/stormwater
Page 2 of 2
S WU-OWNERAFFiL-23Mar2017

n
*ESC ANALYTICAL REPORT mVESC
_ .4.9 S.C—E-N.G.F-s May 17, 2016
CITGO-Charlotte, NC
Sample Delivery Group: L833855
Samples Received: 05/06/2016
Project Number: SEMIANN
Description:
Report To: Mr. Jim Utke
7600 Mount Holly Road
Charlotte, NC 28214
( 1: �a5
Entire Report Reviewed By:
Linda Cashman
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC Is
performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
zit T•
may

TABLE OF CONTENTS ONE IAR NA 10.NWIDE.
cpp ccv� Page
'Tc: Table of Contents
3Ss: Sample Summary
4Cn: Case Narrative
'Sr: Sample Results
GI TFALL 031 1-833855-01
60c: Quality Control Summary
Semi Vvla?ile Organic Compounds r—PVSj by Method 525
7GI: Glossary of Terms
°AI: Aecreditations & Locations
'Sc: Chain of Custody
2
3
4 3Ss
5 FCn]
5
El
ACCOUNT:
CITGO-Charlotte, NC
PROJECT: 5DG:
SEMIANN L833855
DATEMN E: PAGE:
OSA7116 46:55 2 of 13

` SAMPLE SUMMARY Qf�`L.nE3_P4T'ivd',rv,
Collected by Colieopo dateltime Received dateAlrne
OUTFALL 001 L833855-01 W W Pob Durham o5laFns ot1 GO oblfD6116 09 00
Method Batch Dilution Preparation Analysis Analyst
_ date/time datehime
Semi Volatile Organic Compounds (GC1MS) by Method 625 WG971573 � 1 05A011611:26 05113A6 01:20 CMJ
ACCOUNT: PROJECT: SDG: DATEITME; PAGE:
CITGO-Charlotte. NC SEMIANN L833855 05I171161&55 3 of 13

CASE NARRATIVE cY ac.r.aTl :wl.;F.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the c
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the rss]
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
El
H
El
Linda Cashman
technical Servrce Representative 'I
$r
ACCOUNT: PROJECT: SSG: DATEIrIME: PAGE:
CITGO-Charlotte, NC sEMIANN L833855 05tl7/1616:55 4 of 13

OUTFAIL 001 SAMPLE RESULTS - 01 ONE LAB. NAT1 °NWIDE. 4W
Cbtlected dateltime: 05105116 00:00 L833955
Semi Volatile Organic Compourilds (GC/MS) by Method 625
Result Oualifier
MDL
RDL
Dilution
Analysis
Batch
Analyte
mgA
mg/l
mgA
date 1 time
Acenaphihene
U
0.00031b
0.00100
1
05113/201601:20
WG871573
Acenaphthylene
U
0-ON309
0,00100
1
05113r201601:20
VIG87IS72
Anthracene
U
0.000291
0,00100
1
05/1312016 01-20
WG871573
Benzidine
U
0.00432
0,0100
1
05/131201601:20
VJG871573
Ben7o(a(anthracene
U
0.0000975
0.00100
1
05/13/2016 01:20
WG871573
Benzo(b}fluwanthene
U
0.0000896
0.00100
1
05/1312016 01-20
WG871573
Benzo(k)ftuoranthene
U
0.000355
000100
1
05/1312016 01:20
WG871573
8enzo(g,h,i)perylene
U
0000161
0,00100
1
05/1312016 01:20
WG871573
Benzo(alpyrene
U
0.000340
0,00100
1
05/1300160120
WG871573
Bis(2-chlorethoxy)methane
U
0.000329
0.0100
1
05A312016 0120
WG871573
81s(2-chforcethyllether
U
0.00162
0.0100
1
05A 2016 0120
WG871573
Bis(2-chl3rniscpropyl)ether
U
0.000445
0.0100
1
05/13/2016 01-20
WG871573
4-Bromophenyl-phenylethei
U
0-000335
0.0100
1
05/13/2016 01:20
WG871573
2-Chloronaphthalene
U
0.000330
0.00100
1
05A3f201b 01:20
WG871573
4-Chlorophenyt-phenyiether
U
0.000303
HIM
1
05AN2016 01-20
WG871573
Cbrysene
U
0,000332
0.00100
1
05/i3/2016 01-20
WG871573
Diben7(a.h)anthracene
U
0.000279
0.00100
1
OSl13/2016 01:20
WG871573
3,3-Dichlorobenzidine
U
0.00202
0.0100
1
0511312016 0120
WG871573
2,4-DiniV0t0luene
U
0.00165
0.0100
1
05/1312016 0120
WG871573
2,6-Dinitrotoluene
U
0.000279
0.0100
1
05/1312016 01:20
WG87IS73
1,2-0iohenylhydr8zine
U
0.000318
0.0100
1
05/13/2016 01:20
WG871573
Fluoranthene
U
0.000310
0.00100
1
OSA312016 01:20
WG871573
Fluorene
U
0.000323
0.00100
1
05A312016 01:20
WG871573
Hexachlorobenzene
U
0.000341
0,00100
1
05/13/2016 01:20
WG871573
Hexachloro-13-butadiene
U
0.000329
0,0100
1
05/13/2016 01:20
WG871573
Hexachlorocyclopentadiene
U
0.00233
0.0100
1
05/13/2(116 01:20
WG871573
Hexachloroethane
U
0.000365
0,0100
1
05113/2016 01:20
WG871573
lndenc;1,2,3-cd)pyrene
U
0.000279
0.00100
1
05/131201601:20
WG871573
Isaohorone
U
0-000272
0.0100
1
05P312016 0120
WG871573
Naphthalene
U
0.000372
0.00100
1
05/13/2016 01:20
WG871573
Nitrobenzene
U
0.000367
0,0100
1
05/13/2016 01:20
WG871S73
n-Nitrosodimethylamine
U
0.00126
0.0100
1
05/13/2016 01:20
WG871573
n-NiUosodiphenylamine
tJ
0.000304
0.0100
1
05/1312016 01-20
WG871573
n-Nitrosodi-n-propylamine
U
0-000403
0.0100
1
05113/2016 01-20
WG871573
Phenanthrene
U
0.000366
0.00100
1
05/13/2016 01:20
WG871573
Benzylbuty4 phthalate
U
0.000275
0.00300
1
05113/2016 01:20
WG871573
Bis42-ethylhenlIphthalate
0.000979 B. 1
0.000709
0.00300
1
05113/2016 01-20
WG871573
Di-n-butyl phthalate
U
0.000266
0.00300
1
05113/2016.01:20
WG871573
Diethyl phthalate
U
0.000282
0.00300
1
0511312016 01:20
VJG871573
Dimethyl phthalate
U
0.000283
0.00300
1
05/13/2016 0120
WG871573
Di-n-oclyl phthalate
U
0.000278
0.00300
1
05/13/2016 01720
WG871573
Pysene
U
O-OW330
0.00100
1
05/13/2016 01:20
WG871573
1,24-Tnchlorobepzene
U
0.000355
0.0100
1
05/13/2016 01:20
WG871573
4-Chloro-3-methylphenol
u
0000263
0.0100
1
05113/2016 01:20
WG871573
2-Chlorophenol
U
0.000283
0.0100
1
0511312016 01-20
WG871513
2,4-Dichlorophenol
U
0000294
0.0100
1
05113/2016 01:20
WG871573
2,4-Dimethylphenol
U
0,000624
0.0100
1
05113/2016 01:20
WG871573
4,6-Dinitfo-2-methytphenol
U
0.00262
0.0100
1
05AY3 016 01:20
WG871573
2,4-Dinitraphenol
U
0-00325
0.0100
1
05/1312016 01:20
WG871573
2-Nitrophenol
U
O-OW320
0.0100
1
051131201601:20
WG871573
4-Nitrophenol
U
000201
0,0100
1
0511312016 01-20
VIG871573
Pentachlarophenol
U
0-000313
0.0100
1
05tl312016 01:20
WG871573
Phenol
U
0.000334
0.0100
1
05113/2016 01:20
WG871573
2,4,6-Trichlorophenol
U
0,000297
0.0100
1
05A312016 01:20
WG871573
(5%Nitrcbenzene-d5
61.0
21.8-123
0517WO1601:20
VVG871573
(S)2-Fluorabiphenyl
77.5
29-5-131
09131201601:20
WG871573
ACCOUNT:
PROJECT:
56G:
DATFJTIM F"
CITGO-Charlotte. NC
SEMIANN
L833855
05117A616.55
PAGE:
5of13

OUTFAIL 001
SAMPLE RESULTS - 01
O^= LAB. NATIONWIDE �
CbIlecied dateltime: 05105/16 00:00
L833855
SerO Volatile Organic Compounds
(CC;"€ S) 5y Method 61S
r
Result
Qualifier MDL RDL Dilution
Analysis
Batch
Analyte mgA
mgA mgA
date [time
/5) p-TefphenyGdl4 88.7
29.3-137
051732016 0120
WG871573
(S) Phenol-d5 24.4
5, 00-70.1
05n312016 01.-20
WG971573
(5)2-Fluaraphenol 315
10.0-77.9
05/13201601,20
WG871573
(5)2,4,6 hibromophenol 77.5
11.2-130
0"3/20160120
WG871573
F
Fln
r
QG
45c
ACCOUNT: PROJECT: SDG: DATFJTIME: PAGE:
CITGO-Charlatte, NC SEMIANN L833855 05MA616:55 6 of 13

WG871573 QUALITY CONTROL SUMMARY ONE La..& NA710NLVID ,
Semi Volatlle Organic Cam Pounds (GCIMS) by Method 625 L833855-oi
rvlfitlzod Blank 6ARI
(MB) R3136457-3 135112/16 1121
ME Result
ME Ouatdier }AB IADL
ME RDL
Analyte
mg!!
mgll
mgA
A:enuphlrane
L
5.G00316
0.00100
Aceraphthylene
u
0.000309
0.00100
Arvhjacere
u
0.U0791
000100
9e::zidne
u
0 M432
0.0100
Benz-;a)dnthmcene
a
00000975
0.00100
ucnzo;b)tluoranlhepe
a
0.0000896
0.00100
Benzolk;Itiomnlhene
u
O.G00355
O.G0100
9e 1n[g..h,i3perylene
u
0.00M51
0.00100
Benza(elpyrene
u
0.000340
0_G01o0
BEr,2-6brelhorylmelhane
u
0.000329
0.0100
BfsrLdilproeihyllether
u
000162
0.0100
3isf2-chl0wi5ppropyll�?her
u
0A00445
0.0100
e-Br�:ncpher.lip!'.eTAciher
u
0.000335
00100
2-�hkxanaph•� abnP
u
9.000330
0.00100
n-�h�rwhrrry4-phe.^.yFeLher
u
0.090303
0.01o0
Chrysenr.
u
0-000332
0.00100
T.I6enz,a,hlarahr acen�
u
0000279
0.00100
3.3-D:chlvrobenz;oine
a
0.00202
0.0100
2.4-Dlniuvtoluere
a
0.09165
0.0100
2.r,D.,uululuene
0
O.C.N279
O.Glo0
Flr:a:an;here
0
0.000310
0.00100
Fluorene
u
C.CG0373
0.00100
Heruchlorobenzeae
u
O.000341
0.00100
Hevachlor o-1,3�gaoiene
a
0.000329
0.0100
Hesachl=cyclopertad�
V
0.00233
0,0100
Hewhbroethane
u
0.000365
0.0100
lndenu1L2,3-cd;uytene
u
0.000279
0,00100
Isophorone
!1
0.000277
O.OIco
Vzphcialerte
0
0.000372
000100
,Vinobenzene
41
0.000357
0.0100
r-1 rvyztlir:+rthylamire
u
0_00126
O.0100
r-Nivvso0rphenyiamix
0
C C00304
00100
n-'�rtrasatlrrrp:vpylarrine
u
0.009403
0.0100
Phenarthiene
u
0.000366
0.00100
Ernzylbutyl phthalate
u
0.000275
0.00303
Bis,2- Jiy@ieMy4phthaiate
0.000740
0.000709
0.00300
ACCOUNT: PRWECT: SDG- DATErME: PAGE:
CITGO-C1+arbt=e. NC SEMt4NN L833865 DWA61655 7 of 13

WG871573 QUALITY CONTROL SUMMARY
Semf Volatile Organlc Compounds 1GC/M51 by Method 625 te33855-07
IM0143136457-3 05,124611,21
MB P-d?
MB Oualrher M2 MOIL
MR RDL
Analyte
ntgA
mgA
mgA
via -butyl phthotaie
a
0-000266
0.0030J
Dii.hyl phthalate
11
0.000282
0.0020)
D"crrthyl p^.thaldtt
u
O.G00293
O.G0301
Dmn rir phthalate
u
O.ON273
0.00300
Syr-ne
u
O.G00330
0,00100
1,24.1r 1&blohenzene
u
13 GOD355
0-0100
l.3-Dipne.^ydrazine
u
0000318
0.0100
4-Chloro-3-meai*hend
u
0-000263
0.0300
2-Chkrvplrecol
0
0-000253
0.0100
2-N1!mphen0l
U
0-000320
0.0100
4-Naruahenol
u
0-06201
0.0100
p-,!achbroohenol
u
0-000313
0.0100
- nen�l
u
0-000334
O.Oy00
24,F,i rth36roph-A
u
0-000297
0.0TO
24-Drd:brop^e.�f
it
0.000284
0.0100
2.4-D mrt?gtphen�l
tl
0.000624
0.0100
4 CL[,nitro-2.methyiphennl
0
0.G0262
0.0100
2A-0.n.'ropheaol
u
0.00325
0.0100
rSJ7Ja:ahenzerse-d5
813
275423
i.512-FArprobO,h i 7
94.5
29.5731
(S)p-feraherojM
103
29.3.137
is)Pheno+-d5
31..0
5.00-70.1
1ST 217rro+aoAencl
49.7
10.0 "..4
15)2.4,6-Mb,omopheno1
AM
172-C30
Laboratory r,ml of Sample iLCS) • Laborator_: Control Sample DupL-ate ;LCSD
{LCS) R3136457-1 OSA2A6 la34 - {LC5DI R3136457-2 O5A2Ab 10:57
Spike Amo,.t
Lf-S Result
LCSD Resuh
Lt5 Rec.
LCSD Rec.
Rec. Limas
Analyze
mQ4
mgA
m9n
%
%
16
A_r phltwe
0.0500
0.0461
0.0436
92,2
97.2
38.7-109
Atenaplditylene
0.0500
0.0495
e.G516
990
103
36.4106
AnrnraCene
00500
00492
O.C503
985
101
43&113
9envd�ce
00500
0,0290
0.0269
57.9
57.7
100-165
9enn;alaailuacene
00500
0.0479
U1482
95-R
95.3
512-112
9enr"JI'Lo:anLhme
00500
00487
0.0495
97,5
99.0
47-6-111
ACCOUNT: PROIECF:
C11GG- hedcim. N. - SEMIANN
ONE Ei!$. NATlorvviDE.
LCS Ounlifier LCSD 0uelifw RPD
RPD Lvnfts
%
s6
--------- - ---._..__._ 5.28�^ ---
71.5
4.27
21
2.05
18.8
0.390
40
0.570
20
1-55
20
DATErrrME: PAGE:
L833855
05n7r151eSS B of 13

WG871573
QUALITY CONTROL SUMMARY
O e LAB. NAT$ONWIDP.
Sem1 Volatile 09-ic
Compounds
1GCIM51 6y Method 625
-t833855-01
-
Leb�r'aiPl' :_o^irpl
;gem0r
(L:.":1) • L37Cr21?cty Tpni€o1
S%lrtp
{: DLIpIiUlY�
:;LCS-C'j
"
ILCS� R3136457-1 05712116 1034 • [LCSD) P3136457-2 05112l1610:57
€
Spl;e Amount LCS Resup
TCSD Result
LCS Rec.
LCSO Rec.
R- timtts LCS Oualrf a LCSD Oualrher
RFD
RPD Laaes
Araly!e
mgA
mgA
.'nga
%
x
6
9"- *'kft01an1te ,
00500
0.0478
0.C484
95.6
96,8
49.4-114
Q7
20
6mz=19h.]peryiene
0.0500
0.0564
00565
03
113
45.2417
D.110
20
8-n!ejpyrene
0.0500
0.0900
0.04913
953
99.5
45.6-10E
0140
20
Bisl7{hlCrethoxyprrethane
0.0500
6.0419
0,0438
83.7
87.7
37.2-111
4.61
24.1
_
B6s7-uhhtrpethynethe,
GA500
0.036E
OAM5
73.6
77.1
22,Fr108
4.66
77.9
CTl
Bis!7-ch10r0isopmpyljeiher
0.0500
0.0428
0.0439
85.5
87.9
329-100
2.72
25.1
4-81pwcpheny phenyleLher
G0500
0.0533
00546
107
109
407-116
2.16
71
St
2-Chlorpnsphthalene
0.0500
0.0451
OA477
90.1
95.5
33.E-105
579
23
4-[idurcphenyl-phenyleC+er
0.0500
0.0479
0.0509
95.7
102
39.0-113
5.08
20.9
Chrysene
0.0590
0.0494
00504
9B.7
101
54.6-120
2.07
20
D.benz(a,hlan!h: Scene
0.0500
0.0554
0.0556
ill
ill
42.8-115
0.350
20
3.3-pichloro6enzldine
0.0500
0.0657
O.C564
131
133
27.2-142
1.07
22.3
' CI
74.;3'gd+plClc?ae
0.0500
0.0517
00524
103
105
31.2-105
1.47
22
7.5-0�arctolue^e
0.0500
0,0495
0.0513
;9.9
103
30-6-106
In
23.1
'r!_b:anih^=e
0.0500
0A579
09524
704
IQS
45.9-115
0.940
201
Fkf�rs^.e
0.0500
0.0460
OXA79
91.9
95.9
41.0-112
4.21
20.2
h:--3rh101Ob`r ZSne
0.0500
0.0544
0.0565
109
114
38.5-M
434
20.1
Hwacnloro-1,3.butdd•ene
0.0500
0.0440
0,0458
87.3
91.6
16.1-104
41L
31-2
Hecachlomrydopeotadiene
0.0500
0.0401
MW
80.1
892
10.G121
137
27.9
H,dchloioelhane
0.0500
0.0361
0.0376
72.3
75.2
15.5-99.8
390
30.7
Inderafl,2.3-cdjpyrene
0.0500
0.0561
0,0556
112
ill
45.0-116
3.970
20
1sw"C'une
00500
O.Wo
0.0442
941
98.3
35.4-112
4.90
21.5
Naph:i+glen=
00500
0.0402
0 C-427
80.3
854
32,2-101
613
23.8
Nr11cbe^.zene
0(1500
0.0393
0-0419
787
83.9
31.4-106
647
25.7
mNlmsod:me:hylamine
O.C500
00152
0-6%2
30.4
32.6
to.",)1
6.54
37.5
n-NiI,Dsoclvhe-ylamire
0.0500
0.0491
0.0496
38.1
992
44.4-113
1.09
20
r1-N'liusac!4 -p,"amhe
U100
0.0425
0.0425
55.1
85.0
33.2-105
L05D0
23.7
Phenar,Opene
C.0500
0.0482
0.0473
46.4
95.9
46.4-113
0510
20
Benzyaburyi phthalate
C.0500
0.0481
0.0491
96.1
98.1
31.8-123
2.05
20,7
9-Q-e0yherphihalate
0.0500
0.0491
0.0478
36.2
95.5
36.9-134
0310
23.6
E�nbvlyl phthalate
0.0600
0.0492
0.0511
38.3
102
41.B-120
3.9E
20.2
NeTHA phthalate
0.0500
0.0496
0.0512
99.3
102
36.5-129
3.06
20
0imelhyl phthalate
00500
0.0498
00516
39.7
103
35.3-129
343
70.8
0i+rodyl phthalate
0.0500
00482
0.0455
964
97.1
39.7-112 _
0,670
211
Py: ene
0Lr5D0
0-0493
0.0500
985
100
46.3-117
1.51
70
1,2,4-lrichlotohwrzerw_
06500
0.0403
0.0425
806
651
223-951
5-36
27.5
ACCoONT: PROJECT: SDG: DATCa*AE PAGE
C7T000- anode. NC SEMIANN LB33865 05AMS 1655 9nt13

WG871573 QUALITY CONTROL SUMMARY
Sark Volatile Organic Compounds IGCIM51 by Method 62S L833855-01
Laboratory Control SalrplF (LC3) • Laborator! Control Sample DupEicaV(LCSDj
fWAF LAB. NA?IGNWID=.
(LCS] R3136457-1 05112116
10 34 • RCSD]
f13136457-2
05712l75 10.57
:.c
Spice Amount
LC5 Res At
LCSD Resell
LC5 Am
tCSD Rec.
Rec. Lards LC5 Oualdiet LCSD Owl6m
RPD
RPD Lends
;-; ----�
muVyte
rngd
mgR
mgA
a
•c
-5
'6
%
_ `
1.2-Diphenylhytlra2me
0.0500
0.0432
0-0440
55.5
88.1
37.6-11
1.87
21.1
4-Moro-}- eZh"enol
0.0500
0.0453
0.0457
90.7
91.3
35.7-100
G.730
22.9
�
2-C'Namphew1
0.0500
00379
0.0383
75,B
765
26.2-91.5
0990
26.5
7 GDichlcmr�, rcI
0.0500
0 C461
0.0477
37.2
95.3
21.4-103
231
249
_
i S-Di:na;hylphznpl
0.0500
0,0419
0-C-474
B3.8
84,7
IL9107
1.13
25.7
Cfl
4.6,1=o-2-.rohytphenol
0.0500
0,0455
0.0471
91.0
943
184.148
349
24-4
2.rDmVom" of
0.0500
00270
0.0293
539
58.5
24,2-128
8.23
70.5
`
2 YNophenol
0.0500
0.0437
O.G459
87,4
91.9
25.9-106
499
26.9
axSuophewl
0.0500
0,0179
0.023
35.9
35.5
10.0-52.7
1.90
40
Peaac.^.toroperenA
0.0500
0-0437
O.C453
874
905
10.9-97,4
3.46
35.1
o�enoi
0.0500
0-0169
0.0191
3-17
36.1
10.0.57.9
6.79
35
2.4r,TrirMorophend
00500
0.04%
0.0499
99.1
99.8
29.8-107
0.730
24.1
G3
fS)NT.'06 , tre-d5
307
818
2f8-723
iSJ27hmrrbpheryt
98.2
96.6
29.5IN
fS]f.7erpherry4-d74
709
108
293-137
f5/ °hewo d5
32.1
33.7
5.00.70. f
'---�
isj2F"F Mewl
536
51.4
f0.077.9
^�L
75124.6-7nbrnmcphen434
175
7P1
77.2-130
ACCOUNT: PROJECT: SDG: DATEMMF4 PAGE:
DTGO-Chv0otte. NC SEMVW N L833855 05A711616 55 10 0713

` GLOSSARY OF TERMS ON' FLA8,NA 1 1N-WI
Abbreviations and Definitions
SDG
Sample Delivery Group.
MDL
Method Detection Limit.
RDL
Reported Detection Limit.
ND.0
Not detected at the Reporting Limit (or MDL where applicable).
RPD
Relative Percent Difference.
(dry)
Results are reported based on the dry weight of the sample. [this will only be present on a dry
report basis for sails].
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD)
from a quality control sample. The Original Sample may not be included within the reported SDG.
(S)
Surrogate (Surrogate Standard) - Analyzes added to every blank, sample, Laboratory Control
Sample/Duplicate and Matrix SpikelDuplicate: used to evaluate analytical efficiency by measuring
recovery. Surrogates are not expected to be detected in all environmental media.
Rec.
Recovery.
SQL
Sample Detection Limit.
MQL
Method Ouantitation Limit.
Unadj. MQL
Unadjusted Method Ouantitation Limit,
Qualifier Description
B The same analyze is found in the associated blank.
J The identification of the analyze is acceptable: the reported value is an estimate.
ACCOUNT: PROJECT: SDG: DATEITIME:
CITGO-Charlotte, NC SLMIANN LM3855 050/1616:55
PAGE:
11 of 13

'
ACCREDITATIONS & LOCATIONS
C}t,,_LAB. NA-f•'_.:',iWIrc:
�
ESC Lac Sciences is
the only eevlronmental IaborateTy sc: edliedfcemfied:o sup3c t
yow work nationmde ; o- one locatio.. O-e phone call, one point of contact, are laboratory. No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capabiI4 horn our single location laboratory is comparable to the coBeCrve totals of the
f
-etwork lahoramnes n o,r industry. The mist signifirant henelil to our 'uneloratinn'
design is the design of cur tahnralory ca-pus, Tne model Is rD-ducive
to accsfera-eo prodwaVity,
decreasing turn -around time. and preventing cross contamination, thus protecting sample integrity. Our focus an premium quality and prompt service allows us to he YOUR LAB OF CHOICE.
Not all certificatlons hetd by the laboratory are applicable to the results reported in the
attached report.
r
Alabama
_ 40660
Nevada
TN-03-2002-34
s
Alaska
U5T-080
New Hampshire
2975
SS
Arizona
AZ0612
New Jersey—NELAP
TNO02
Arkansas
88-0469
New Mexico
TN00003
01157CA
New York
11742
RnCalifornia
Colorado
TN00003
North Carolina
Env375
Conneticut
PH-0197
North Carolina
DW21704
Florida
E87487
North Carolina =
41
Georgia
NELAP
North Dakota
A-140
rQC
Georgia
923
Ohio-VAP
CL0069
Idaho
TNO0003
Oklahoma
9915
Indians
200008
Oregon
TN200002
�G�
Indiana
C-TN-01
Pennsylvania
979
66-02979
Iowa
364
Rhode Island
221
Kansas
E-10277
South Carolina
84004
Kentucky'
90010
South Dakota
n!a
IN
Kentucky'
16
Tennessee'"
2006
Louisiana
A130792
Texas
T 104704245-07-TX
c
Maine
TN0002
Texas s
LAS0152
SC
Maryland
324
Utah
6157585858
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
109
Minnesota
047-999-395
Washington
C1915
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093991E
Montana
CERT0086
Wyoming
A2LA
Nebraska
NE-05-15-05
E i irC. Pa!ty
& F Cjerai Accreditaticifi5
QLA - ISO 17025 1461.01 AIHA 100789
A2LA - 150 17025' 1461.02 DOD 1461,01
Canada 1461.01 USDA 5-67674
EPA-Crypto TN00003
' Drinking Water ' Underground Storage Tanks ' Aquatic Toxicrry ` ChemicalfMicrohiologtcal ' Mold "+Accreditation not applicable
(cur
ESC Lab Sciences has sixty -tour client support censers that provide s=-mole plckuo arid!=r :he delivery of sampling supplies. if y� - would like assistance from one of or support offices, UsasP
contact our -n a ecc. ESC Lab Sceences performs all testing at our central laboratory.
rnT
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• �rev f•
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r_ r.-
ACCOUNT:
CITGO-Charlotte, NC
PROJECT:
SEMIANN
SOG: DATFJTIME: PAGE:
L933855 05117R61655 12 of 13

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7fWA
NCDENR
North Carolina Department of Environment and Natural Resources
Beverly Eaves Perdue
Governor
Division of Water Quality
Charles Wakild, P. E.
Director
September 14, 2012
Mr. David S. Chrismer
c/o Atlas Copco Compressors, LLC.
1800 Overview Drive
Rock Hill, South Carolina 29730
D1vI = OF Lj),,1LJ RE3 UHSeeFreeman
L OBAL I-fy SLCi10 Secretary
e-►T-" - .. �: :
DEC I - Z013
Subject: General Permit No. NG030000
Atlas Copco Compressors, LLC.
COC No. NCGO30625
Mecklenburg County NC
Dear Mr. Chrismer:
In accordance with your application for a stormwater discharge permit received on June 22, 2012,
we are forwarding herewith the subject certificate of coverage (COC) to discharge under the subject state
NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General
Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the US
Environmental Protection Agency dated October 15, 2007 (or as subsequently amended).
If any parts, measurement frequencies, or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the
Division of Water Quality. The Division of Water Quality may require modification or revocation and
reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain
other permits which may be required by the Division of Water Quality or permits required by the Division
of Land Resources, Coastal Area Management Act or any other federal or local governmental permit that
may be required.
Please note that the attached permit expires on October 31, 2012. Your COC will be
automatically renewed to cover the full 5 year term of the soon to be reissued permit. In the interim you
must abide by the terms of the expiring permit. You can review the proposed general permit changes
once they are posted at: http://portal.ncdenr.org/web/wq/ws/su/current-notices
If you have any questions concerning this permit, please contact Bill Diuguid, Staff Planner,
Stormwater Permitting, at telephone number [phone].
Sincerely,
opjGINAL SIGNED
PICKLE
B1
for Charles Wakild, P.E.
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Raleigh, North Carolina 27604
Phone: [phone] FAX: [phone] Customer Service: 1-877-623-6748
Internet: yvww.ncwaterquafitV.o
None
rthCarolina
Naturally
An Equal Opportunity 1 Affirmative Action Employer

COC No. PJCG030625
Mr. David S. Chrismer
Atlas Copco Compressors, LLC.
September 14, 2012
cc: Mooresville Regional Office
Central Files
Stormwater Permitting Unit Files
Attachments
Page 2 of 2

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030625
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
Atlas Copeo Compressors, LLC
is hereby authorized to discharge stormwater from a facility located at
Atlas Copco Compressors, LLC
11313 Steele Creek Road
Charlotte
Mecklenburg County
to receiving waters designated as Steele Creek, a Class C water body, Catawba River Basin; in accordance with the
effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, II, 111, IV, V and VI of
General Permit No. NCG030000, as attached.
This Certificate of Coverage shall become effective September 14, 2012.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day September 14, 2012.
Charles Wakild, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

IM
r `Ar _
i"3 �,c� Licc'�`'Ca_'���i3C'!c_�i`l`'~` v ';:}•. .�. _• _ f f _ .

� FN t
NCDENR
North Carolina Department of Environment and Natural Resources
Beverly Eaves Perdue
Governor
Division of Water Quality
Charles Wakild, R E.
Director
September 14, 2012
Mr. David S. Chrismer
c/o Atlas Copco Compressors, LLC,
1800 Overview Drive
Rock Hill, South Carolina 29730
Subject: General Permit No. NG030000
Atlas Copco Compressors, LLC.
COC No. NCG030625
Mecklenburg County NC
Dee Freeman
Secretary
Dear Mr. Chrismer.
In accordance with your application for a stormwater discharge permit received on June 22, 2012,
we are forwarding herewith the subject certificate of coverage (COC) to discharge under the subject state
NPDES general permit. This permit is issued pursuant to the requirements of North Carolina General
Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the US
Environmental Protection Agency dated October 15, 2007 (or as subsequently amended).
If any parts, measurement frequencies, or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual"permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the
Division of Water Quality. The Division of Water Quality may require modification or revocation and
reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain
other permits which may be required by the Division of Water Quality or permits required by the Division
of Land Resources, Coastal Area Management Act or any other federal or local governmental permit that
may be required.
Please note that the attached permit expires on October 31, 2012. Your COC will be
automatically renewed to cover the full 5 year term of the soon to be reissued permit. In the interim you
must abide by the terms of the expiring permit. You can review the proposed general permit changes
once they are posted at: http://portal.ncdenr.org/web/wq/ws/su/current-notices
If you have any questions concerning this permit, please contact Bill Diuguid, Staff Planner,
Stormwater Permitting, at telephone number [phone].
Sincerely,
ORIGINAL SIGNED B)
KEN PICKLE
for Charles Wakild, P.E.
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Ralegh, North Carolina 27604
Phone: [phone] FAX: [phone] Customer Service: 1-877-623-6748
Internet: www.ncwaterguality.org
NonrthCarohna
Nataally
An Equal Opportunity L affirmative Action Employer

COC No. NCG030625
Mr. David S. Chrismer
Atlas Copco Compressors, LLC.
September 14, 2012
cc: Mooresville Regional Office
Central Files
Stormwater Permitting Unit Files
Attachments
Page 2 of 2

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030625
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
Atlas Copco Compressors, LLC
is hereby authorized to discharge stormwater from a facility located at
Atlas Copco Compressors, LLC
11313 Steele Creek Road
Charlotte
Mecklenburg County
to receiving waters designated as Steele Creek, a Class C water body, Catawba River Basin; in accordance with the
effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, 11, III, IV, V and VI of
General Permit No. NCG030000, as attached.
This Certificate of Coverage shall become effective September 14, 2012.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day September 14, 2012,
Charles Wakild, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

- � L � � - � t E � ..at - N •1�5
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Diuquid, Bill
From: Parker, Michael
Sent: Thursday, September 13, 2012 7:54 AM
To: Diuguid, Bill
Subject: RE: NCG030625 Atlas Copco Compressors LLC NOI
Feel free to issue this permit.
From: Diuguid, Bill
Sent: Wednesday, September 12, 2012 12:06 PM
To: Parker, Michael
Subject: NCG030625 Atlas Copco Compressors LLC NOI
Michael Parker, Mooresville Regional Office:
Please review the attached NOI application with the objective of responding to me with a recommendation to issue the
permit. I recognize that you may not visit each new permittee during this NOI review, but it affords you the opportunity
to log the permit into your regional database and add the facility to a future monitoring and compliance visit schedule.
Therefore, your recommendation now to issue the permit serves as your acknowledgement that (1) the facility is located
in your region, (2) that there are no current complaints outstanding about the facility that have not been dealt with, and
(3) that the facility may ultimately be inspected by the regional staff. I've also attached a scanned copy of the NOI and a
location map for your review.
COC # Facility 1 Location I City/County
_ __ , _
NCG030625 Atlas Copco Compressors LLC 111313 Steele Creek Road Charlotte/Mecklenburg -
If you need any more info, give me a call. If you could send me a recommendation to issue the permit by 10/12/2012,
I'd appreciate it, so I can issue their COC. I cannot issue the permit until the respective regional office reviews and
comments back to me with a recommendation to issue the permit.
Thanks.
Bill
Bill Diuguid, AICP
Staff Planner, Stormwater Permitting
Wetlands and Stormwater Branch
Division of Water Quality I NCDENR
1617 Mail Service Center (Mail)
512 N. Salisbury St, Raleigh, NC 27604 1 9th Floor (Location & Parcels)
Raleigh North Carolina 27699-1617
Phone: [phone] Fax: [phone]
Website: http://portal.ncdenr.ora/web/wq/wslsu
E-mail correspondence to and from this address maybe subject to the North Carolina Public Records taw and maybe disclosed to third parties.

Jun, 22, 2fl2 11:26AM
�0
RECEIVED BY ASAP
p\, ATLAS COPCO COMPRESSORS LLC MAY 09 2012
1800 Overview Dr, Rock Hill, SC 29730
DISBURSEMENT AUTHORIZATION
THIS FORM TO BE USED FOR ALL PAYMENTS NOT OTHERWISE COVERED BY AN INVOICE
DATE:
AMOUNT REQUESTED T 7
l (9b (90
AMOUNT IN WORDS
PAYABLE TO:
NcC- NAME
a ► I orb STREET: ._
(? i�a►!�rv« C��-ter
CITYISTATE �N _ _ zIR
`(0
puR�
TRAVEL. ADVANCE MILEAGE REIMBURSEMENT
TEMPORARY ----PERMANENT MILES RATE AMOUNT
OTHER
r
=DESCRIaq O t`
e cd
PAYMENT METHOD: Cash D1rbursamentl-IMII$15 �
c
CHECK: °O CASH; m
DATE NEEDED: - RCVD BY:
JUN 2 2 2012
SEND TO: VC% DATED: -
INSTRUCTIONS:
c
1. COMPLETE APPROPRIATE AREAS REQUESTED BY
2. HAVE REQUEST APPROVED BY YOUR APPROVED BY:
RESPONSiBLE MANAGER. inq
3, ATTACH DOCUMENTS AS DEEDED TO SUPPORT REQUEST
4. SUBMIT APPROVED FORM WITH ATTACHMENTS
ACCOUNT DISTRIBUTIOM
ACCOUNT S
ACCOUNT $
CHECK NO. DATED
020001. Rev. 2. il/2011

. ,
:dun. 22. 2012 11:2V'n AMN;,, S B
NCO030000 N.0,1.
Final Checklist
This application will be returned as Incomplete unless all of the following Items have boon Included:
X Check for $100 made payable to NCDE:NR,
x This completed application and all supporting documents.
x A site diagram showing, at a minimum, (existing or proposed),
(a) outline of dralnage areas, (b) stolmwater {management structures, (c) location of stormwater outralls
corresponding to the drainage areas, (d) runoff conveyance features, (a) areas where materials are stored,
(I) Impervious areas, (g) site properly lines.
X Copy of county map or USGS quad sheet with the lacallon of the facility clearly marked on the map.
Mall the entire package to:
Stormwater Permitting Unit
Divlalon of Water Quality
1617 Mall Service Center
Raleigh, North Carolina 27699.1617
The submission of this document does not guarantee coverage under the General permit.
For questions, please contact the DWQ Regional Office for your area.
DWQ Regional Office Comm Information:
Asheville Office ......
[phone]
Fayeltevllle Office ...
[phone]
MoOrpsvllle Office ...
[phone]
Raleigh Office ........
[phone]
Washington Office ...(262)
940-6481
Wilmington Office ...
[phone]
Winston-Salem ... _.,
[phone]
Central Office .........
[phone]
Page 4 of 4
SWU 218-071408 Last i0v1sod VON

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ATLAS COPCO; COMPRESSORS LCC f CHECK DATE yf� ti 5 9 7 4,6 3
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