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HomeMy WebLinkAboutNCG030513_MONITORING INFO_20181204STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. N C� Q 3 0,S) 3 DOC TYPE ❑HISTORICAL FILE MONITORING REPORTS DOC DATE ❑ YYYYMMDD Semi-annual Stormwater Discharge Monitoring Report 'for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 11/Z6/2018 CERTIFICATE OF COVERAGE NO. NCG030513 SAMPLE COLLECTION YEAR 2018 FACILITY NAME The Goodyear Tire & Rubber Company SAMPLE PERIOD ❑ Jan -June ® July -Dec COUNTY Iredell RECEIVEn- or ❑ Monthly) month PERSON COLLECTING SAMPLES Nicholas Fugitt DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY Pace Analytical Lab Cert. #t 40 DEC 0 4 2018 ❑Zero -flow ❑Water Supply ESA Comments on sample collection or analysis: CE=NTRAi_ FILES ❑Other DWR SECT101+1 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 Part A: Stormwater Benchmarks and Monitoring Results ❑ No discharge this period?' Outfall No. Date Sample Collected) (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ===> - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 (Pond) 10/11/2018 2.24 6.1 6.48 .0059 <0.005 mg/L .0268 <4.8 mg/L NA Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe We miller Name (Print name) Manufacturing Director Title (Print title) Jc,t OoAn" I ( �� zo15 (Signature) ( Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period ?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> - - 15 mg/L 100 mg/L or 5o mg/L* 6.0 — 9.0 SU Not Applicable Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION S. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 0 aceAnalytrcal www.pamlahsmm November 01, 2018 Nicholas Fugitt Goodyear 108 Business Park Drive Statesville, NC 28677 RE: Project: Stormwater 10/11 Pace Project No.: 92403225 Dear Nicholas Fugitt: Pace Ana"cal Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on October 12, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 m aceAnalytical www.paaef ftcom Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersviNe, NC 28078 (704)875-9092 CERTIFICATIONS Project: Stormwater 10111 Pace Project No.: 92403225 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VrginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 (�55'neAnalyficaf' www.pacdabxc= SAMPLE ANALYTE COUNT Project: Stormwater 10111 Pace Project No.: 92403225 Pate Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92403225001 HCV HC21 N11 U1 EPA 1664B JMS 1 PASI-C EPA 1664B JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 2540D-2011 f CRV 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 Pace Analytical Services, LLC aceAnalytrca! • 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 wwwpacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Stormwater 10111 Pace Project No.: 92403225 Sample: HC11 HC21 N11 U1 Lab ID: 92403225001 Collected: 10/11/18 16:00 Received: 10/12118 10:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mglL 4.8 1 10/26/18 04:28 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 4.8 1 10/26/18 04:28 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 5.9 uglL 5.0 1 10/13/18 13:45 10/15/18 03:56 7440-50-8 Lead ND uglL 5.0 1 10/13/18 13:45 10/15/18 03:56 7439-92-1 Zinc 26.8 ug1L 10.0 1 10/13/18 13:45 10/15/18 03:56 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 254OD-2041 Total Suspended Solids 6.1 mglL 2.5 1 10/15/16 19:41 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 13 aceAnalytical www.parrfabs.corn Project: Stormwater 10111 Pace Project No.: 92403225 QC Batch: 438519 QC Batch Method: EPA 1664B Associated Lab Samples: 92403225001 METHOD BLANK: 2410940 Associated Lab Samples: 92403225001 Parameter Units Oil and Grease mg1L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporting Result Limit Anaiyzed Qualifiers ND 4.8 10/26/18 04:27 Pace Anatytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 {704)875-9092 LABORATORY CONTROL SAMPLE: 2410941 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 38.5 36.8 96 78-114 MATRIX SPIKE SAMPLE: 2410942 92403461001 Spike MS MS % Rec Parameter Units Result Cont. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 38.5 36.1 93 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the resutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 aceAnaocal. www.pawkbacorn Project: Stormwater 10111 Pace Project No.: 92403225 QC Batch: 438520 OC Batch Method: EPA 1664E Associated Lab Samples: 92403225001 METHOD BLANK: 2410943 Associated Lab Samples: 924032250G1 Parameter Units Total Petroleum Hydrocarbons mg1L LABORATORY CONTROL SAMPLE: 2410944 Parameter Units Total Petroleum Hydrocarbons mglL MATRIX SPIKE SAMPLE: 2410945 Parameter Units Total Petroleum Hydrocarbons mg1L QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 4.8 10/26/18 04:27 Spike LCS Cone. Result 19.2 20.3 92403461001 Spike Result Cone. ND 19.2 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28o78 (704)875-9092 LCS % Rec % Rec Limits Qualifiers 105 64-132 MS MS % Rec Result % Rec Limits Qualifiers 18.6 95 64-132 Results presented on this page are In the units indicated by the "Unks" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 aceAnalytica!® nww.pacalabs.com QUALITY CONTROL DATA Project: Stormwater 10111 Pace Project No.: 92403225 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 436116 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92403225001 METHOD BLANK: 2399821 Matrix: Water Associated Lab Samples: 92403225001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug1L ND 5.0 10/15/18 03:22 Lead uglL ND 5.0 10/15/18 03:22 Zinc uglL ND 10.0 10/15/18 03:22 LABORATORY CONTROL SAMPLE: 2399822 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug1L 500 509 102 85-115 Lead ug1L 500 486 97 85-115 Zinc ug1L 500 492 98 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399823 2399824 MS MSD 92403307001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper uglL 87.9 500 500 605 605 103 103 70-130 0 Lead uglL 41.8 500 500 528 535 97 99 70-130 1 Zinc ug1L 172 500 500 669 676 99 101 70-130 1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 11101 /2018 10717 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAnalyticaI www.pacelahs.mm QUALITY CONTROL DATA Project: Stormwater 10111 Pace Project No.: 92403225 QC Batch: 436322 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis description: 2540D Total Suspended Solids Associated Lab Samples: 92403225001 METHOD BLANK: 2400698 Matrix: Water Associated Lab Samples: 92403225001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 10/15/18 19:39 LABORAUORY CONTROL SAMPLE: 2400699 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 2400700 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 2400701 Parameter Units Total Suspended Solids mglL Pace Analytical Services, LLC 9800 Kincey Ave. Suite too Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 251 244 97 90-110 92403218004 Dup Result Result 52.8 55.0 92403281002 Dup Result Result 29.0 33.0 RPD Qualifiers 4 RPD Qualifiers 1306 Results presented an this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in futi, Date: 11/01/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 e aceAnalytical wwwpacewft =n QUALIFIERS Project: Stormwater 10/11 Pace Project No.: 92403225 DEFINITIONS ❑F - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MD -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyi ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenyiamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 aceAnalytical WWWpao.4abs.cam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Stormwater 10/11 92403225 Analytical Lab lD Sample ID QC Batch Method QC Batch Analytical Method Batch 92403225001 HC11 HC2 1 N11 U1 EPA 1664B 438519 92403225001 HC11 HC21 N11 U1 EPA 1664E 438520 92403225001 HC11 HC21 N11 U1 EPA 200.7 Rev 4.4 1994 436116 EPA 200.7 Rev 4.4 1994 436140 92403225001 HC11 HC2l N11 U1 SM 2540D-2011 436322 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/01/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised: February 7, 2018 a%eAftalytical 17+ Sample Condition U on Receipt(SCUR) Page 2 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev,06 Pace Carolinas Quality Office Laboratory receiving sa pies: Asheville Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville[] SampleClient Name: WO# : 92403225 • • r_ Project #: � tI111Jill Courier. MFed E. 111 ❑ Commercial ❑Pace ❑Other: 92403225 Custody Seal Present? ❑Yes o Seals Intact? Yes [:]No pate/InitlakPerson Examining Contents: 2 f4 /0/p Packing Material: ffBubble Wrap f ubble Bags []None ❑ Other Thermometer: ❑IR Gun ID: Type of ite: ❑ ffWet Blue Fy� [ Cooler Temp (•C): 5.2 Correction Factor: Add/Subtract (•C) Q Cooler Temp Corrected ("C): 5 . Z! USDA Regulated Soil ([3 N/A, water sample) Did samples originate rn a quarantine zone within the United States: CA, NY, or 5C (check maps)? 11Yes r1No Biological Tissue Frozen? []None❑Yes ❑No EN/A Temp should be above freezing to 6'C []Samples out of temp Criteria. Samples an ice, cooling process has begun Did samples originate from a foreign source [internationally, inrh,Ainv Hawaii anri PuPrm RimI7 FIYet FIN. Comments/Discrepancy: Chain of Custody Present? Wes QNo ❑N/A 1. Samples Arrived within Hold Time?des No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? ❑Yes Na N/A 3. Rush Turn Around Time Requested? []Yes No ❑N/A 4. Sufficient Volume? Q"Yes No ❑N/A S. Correct Containers Used? -Pace Containers Used? ,L�JY s [:IN. ❑N/A ❑No (]N/A 6. Containers Intact? �ys li/es ©No ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes ❑No ETNIA S. Sample Labels Match CCIC? -Includes Date/Time/ID/Analysis Matrix: E3fes w f ❑No ❑N/A 9. Headspace in VOA Vials (>5-6mm)? QYes ❑No N/A 10. Trip Blank present? Trip Blank Custody Seals Present? []Yes Yes ❑No El No N/A N/A 11, COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Dateffime: Field Data Required? 0Yes ❑No Project Manager SCURF Review: Date: r G 2 � Project Manager SRF Review: Date: ! r Page 11 of 13 ,V ZeAnaiyfical- WWW.pectimbi.com CHAIN -OF -CUSTODY ! Analytical Request Document The Chain -or -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. o r Section A Section B Section C m Page. of tl Required Mont Information: Required Project Information: Invoice Information: / m To: Attention: Company: Ropo 1252 'LAA190 `JV14.A 1 Address: Copy To: Company Namo: REGULATORY AGENCY c-ve. Address: CA F- NPDES r GROUND WATER f" DRINKING WATER UST (" RCRA I OTHER Email Order No.: Papa Qin uo Rotmursa: o: 6 Fax: Project Name:l- r"' Paca Projur% Site Location um 14:�tr MonaOar, STATE: Raquostad Due DalarTAT: Project Number: Papa Pmfee 0: Requested Analysis Filtered (YIN) Section D Matrix Codes a y x gaquiradCllom mlermalk0n 11nIRIx.I_000E a COLLECTED Presarvafives Drhrkinn wnmr Dw o Water wT VVrWo Water wW COMPo3ITE Cf]IIPO U _ Product P S—r [NP I Ea x 5oillSolid 5L U O N y SAMPLE ID wilpa w a w F . (A-Z.0.91.-) Air AR w a z H Sample IOs MUST BE UNIQUE Tissue TS O w 0- t�v ka- Z U Other OT U F- 2 G N '2— 2 r2 rC u. 4"' O d 115�fn L L C N f y DATE TIME DATETIME N # = _ z O a Pace Project NOJ Lab I.D. 1 w . c> x 3 + + r 4 5 6 7 S g to 11 12 ADDITIONAL COMMENTS RELINQUISHED BY AFFILIATION DATE TIME ACCEPTED BY! AFFILIATION DATE TIME SAMPLE CONDITIONS 10M118 luau 5 •I- ORIGINAL SAMPLER NAME AND SIGNATURE o ^ `i l PRINT Noma of SAMPLER: a F 1, z o} a Z y 5-1SIGNATURE u ir V U V of SAMPLER: 11 t (MM ODlY Y)d L 1Fr to Imponnnl NUra. by sitlaugl 11119 term ynu aronr=pane Pace's NET 30 nay payment lorms and ++aruu+n0 10 lata charges of 1.5%. pre munm for nn en rcos -1 oid(enjrin 3a days. I I F-ALL-0-020rev.07. 15-May-2007 m CD m N O w m CoLA v m o ' 1 m v 2 G s a n � D CL y N A a rt N 3 m '+ O c O -N C ro CL � LA tD M 3 m M CL � v CL W rt a� Cu N N a ItemN BP4U-125 mL Plastic Unpreserved (N/A) (CI-) 9P3U-250 mL Plastic Unpreserved (N/A) BPZU-500 mL Plastic Unpreserved (N/A) BPIU-1 liter Plastic Unpreserved (N/A) BP4S-125 mL Plastic H2SO4 (PH < 21 (Cl-) ~ BP31N-250 mL plastic HNO3 (pH < 2) BP4Z-125 mL Plastic ZN Acetate & NaOH (>9) BP4C-125 mL Plastic NaOH (PH > 12) (Cl-) WGFU-Wlde•mouthedGlass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (Cl-) AGIH-1 liter Amber HCI (pH < 2) AG3U-250 mL Amber Unpreserved (N/A) (CI-) AG1S-1 liter Amber H2SO4 (pH < 2) AG35-250 mL Amber H2504 (PH < 2) A63A(DG3A)-250 mL Amber NH4C1 (N/A)(CI-) DG91-1-40 mL VOA HCl (N/A) VG9T-40 mL VOA Na2S203 {N/A) VGOU-40 mL Von Unp 1N/Aj DG9P-40 mL VOA H3PO4 (N/A) VOAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SP5T-125 ml.Sterile Plastic (N/A —lab) SPZT-250 mLSterile Plastic (N/A —lab) BP3A-250 mL Plastic (NH2)2SO4 (9.3-9.7) AGOU-100 mL Amber Unpreserved vials (N/A) VSGU-20 m L Scintillation vials (N/A) UG9U-40 mL Amber Unpreserved vials (N/A) r, 3 m z n 7711 0 0 1J N O) November 19, 2018 scra MIL Metal Buyers and Recyclers 4017 �aaG�'�a v CERTIFIED MAIL RETURN RECEIPT REQUESTED 7018 0680 0002 2920 0838 Mr. lames Moore NCDEQ-Regional Office Engineer NC Dept. of Energy, Minerals and Land Resources Mooresville Regional Office 610 East Center Avenue, Suite 301 Mooresville, NC 28115 RE: General Stormwater Permit Sampling Event #8 (July 2018 -- December 2018) And Best Management Practice (BMP) Activity Update Certificate of Coverage No. NCG200513 Dear Mr. Moore: With this submittal, the United Scrap Metal --- Charlotte Facility is providing the latest semi-annual sampling results, which include monthly monitoring for copper and zinc, and an update on BMP activities. For the October 2018 sampling event, copper and zinc concentrations in samples from Outfalls 001 and 002 were below benchmark concentrations while concentrations in the sample from Outfall 003 exceeded benchmark concentrations for those same parameters. In an effort to reduce copper and zinc concentrations in stormwater discharged from the United Scrap Metal (USM) property, the following investigative activities and BMP have been completed or are underway: 1. Sampling and analysis (copper and zinc) of contributory stormwater runoff to each outfall. Attached are results from sampling of stormwater runoff from 1) "Penske": stormwater run-on from the upgradient truck rental operation which contributes to Outfall 003; 2) "Non -Contact": rainfall collected in a clean lab container prior to contact with the any surface; 3) "Gutter": stormwater runoff discharged from the building gutter system; 4) "3A and 313": stormwater runoff from scrap metal collection areas that contribute to Outfall 003. Note: 1) The "Non Contact" sample copper concentration is slightly above the benchmark concentration; 2) The "Gutter" sample zinc concentration is significantly above the benchmark concentration however; the Outfall 001 sample was below the benchmark concentration. 2. Due to similarities between results obtained from the September 17, 2018 investigative sampling event, stormwater samples collected on October 11, 2018 were "split" and sent to two laboratories. Results are attached and concentrations were similar with the exception of COD, which, although elevated for one laboratory, were all below the benchmark concentration. 3. Clean out depressions in drop inlets meant for sediment collection. Once completed, monitor during routine inspections as outlined in the Storrnwater Pollution Prevention Plan (SW 3) and remove collected sediment once full (zinc and copper BMP). Mr. James Moore NC Dept. ofEnergy, Minerals and Land Resources November 19, 2018 Page 2 4. Increase frequency of sweeping paved surfaces to remove potential sources such as loose welding wire and rod scraps (zinc and copper BMP), deposits from tire wear (zinc BMP), dust from brake pads (copper BMP) and hardened residues from raw material containers (zinc BMP). 5. Install catch basin (drop inlet) insert filters with internal high flow bypass in areas with significant industrial activities exposed to stormwater (zinc and copper BMP). 6. Inspect all drainage areas for treated wood that has started to deteriorate. If any is found, review replacement with composite materials or wood known to be treated with a chemical other than CCA (copper BMP). 7. Survey all forklifts and material handling equipment for motor oil and hydraulic fluid leaks. Repair leaks and periodically review motor and hydraulic oil purchases for increasing trends (zinc BMP). 8. Develop and implement an end of day housekeeping program to reduce exposures to rainfall and metal particles that may be carried away by stormwater runoff (copper and zinc BMP). 9. Review lawn care contracts or procedures to determine if there is a potential for application of herbicides and pesticides that contain zinc and/or copper and take precautionary measures to ensure applications, if necessary, are kept to a minimum (zinc and copper BMP). 10. Review all trash dumpster and compactor installations to determine if refuse is exposed to stormwater. Stormwater penetrating open top dumpsters and deposit bins for hydraulic rams will often leak from the containers. Determine means to eliminate exposure of refuse to stormwater (zinc and copper BMP). 11. MetaI recycling roll -off bins and metal cuttings collection bins are often exposed to stormwater. Due to frequent use of the bins, covering with a tarp may not be a workable option. These areas should be inspected for housekeeping and contents (ex. housings that contain fluids) on a weekly basis. Protection from rainfall should be budgeted as business conditions allow. These recycling collection areas often generate heavy powered industrial vehicle traffic; make inspections for hydraulic fluid leaks a priority (zinc and copper BMP). 12. Ensure that outfalls are periodically inspected for sediment deposits. Corroded and failed drain pipes, catch basin, culverts, etc. may be allowing excessive sediment to wash to the outfall. Sediment has the potential to add metal concentrations to stormwater runoff. Rip -rap that is full of sediment should be excavated, sediments removed and disposed, and rip -rap replaced. This is especially true for rip -rap installed upgradient of the outfall. Excessive sediment that continues to deposit in the system may dictate inspection of drainage pipe(s) for failures and identify those in need of repair (zinc and copper BMP). USM will sample stormwater discharges for copper and zinc during the months of November and December while continuing BMP efforts to reduce concentrations of those parameters in stormwater discharges from the property. Should you have any questions or comments, please do not hesitate to contact me at 804-621-7000 or mobile phone 815-693-5052. Sincerely, UNITED SCRAP METAL, INC. John Dergo General Manager Enclosures cc: Adam Wilk— USM National Compliance Manager Tim Monroe —Leaf Environmental & Engineering P.C. Semi-annual Stormwater Discharge Monitoring Report DMR for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted //- Zf- 18 CERTIFICATE OF COVERAGE NO. NCG200513 _ FACILITY NAME United Scrap Metal Inc. COUNTY Mecklenburg PERSON COLLECTING SAMPLES John Dereo, LABORATORY Pace Analytical Services, Inc. Lab Cert. #37706 #377ez Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION Y rARR18 =SAMPLE PERIOD Jan -June X July -Dec or ❑ Monthly' month JSCHARGING TO CLASS ❑ORW ❑HCIW []Trout ❑PNA C, ❑Zero -flow ❑Water Supply ❑SA © [:]Saltwater ®Other C co M 0 PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (5GT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks - - 100 mg/L or 5o mg/0 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L' •0.07S mg/L or 0.210 mg/L5 0.126 mg/L or 0.090 mg/L' Outfall 1 10/11/18 2.46 5.0 mg/L <25 mg/L <5 mg/L 0.0079 mg/L <0.005 mg/L 0.103 mg/L outfall 2 10/11/18 2.46 3.3 mg/L <25 mg/L <5 mg/L 0.0071 mg/L <0.005 mg/L 0.116 mg/L Outfall 3 10/11/18 2.46 9.5 mg/L 35.9 mg/L <5 mg/L 0.0343 mg/L <0.019 mg/L 0.466 vn&IL 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, cluantitation limit, etc. in mg/L. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Note: !f you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or -Tier 3 responses. See General Permit. Part 13: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No dischorge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or_Ver 3 responses. See General Permit. FOR PART AAND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: James Moore Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharae" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are sig iicant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm Permit Date:02/02/2015-12/31/2019 /�_ Z v —118 (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 2ce A rkdy fiCalWWWpamwamm i September 25, 2018 Adam Wilk United Scrap Metal 1545 S. Cicero Avenue Cicero, IL 60804 RE: Project: Cu and Zn Sampling 9117 Pace Project No.: 92400203 Dear Adam Wilk: Pace AnalyUoal Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Enclosed are the analytical results for sample(s) received by the laboratory on September 20, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, CWOL, " I btu Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager 1=ndosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 Gutter Sample Non -Contact Ranin Sample Outfall3A Outfall 3B Penske Sample Sampling Date 9/17/2018 9/17/2018 9/17/2018 9/17/2018 9/17/2018 Copper img/11 Zing (Mg/1) 0.037 0.168 0.0377 0.188 0.0406 0.19 0.0382 0.182 0.0389 0.185 0.010 0.126 1�20AWkai* www:p.com t` Project: Cu and Zn Sampling 9117 Pace Project No.: 92400203 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Fiorida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 vrginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 26078 (704)8759092 This report shall not be reproduced, except in full, without the written consent of Paoe Analytical Services, LLC. Page 2 of 13 aceAnaVica!' i SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kinney Ave. Suite 100 Huntersville, NC 28078 (704)87 59092 Project: Pace Projed No.: Cu and Zn Sampling 9117 92400203 Anatytes Lab ID Sample ID Method Analysts Reported Laboratory 92400203001 Gutter Sample EPA 200.7 Rev 4.4 1994 DS 2 PASI-A 92400203002 Non -Contact Rain Sample EPA 200.7 Rev 4.4 1994 DS 2 PASI-A 92400203003 Outtall 3A EPA 200.7 Rev 4.41994 DS 2 PASI-A 92400203004 Outfall 313 EPA 200.7 Rev 4.4 1994 DS 2 PASI-A 92400203005 Penske Sample (ofisite) EPA 200.7 Rev 4.4 1994 DS 2 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 Of 13 s aceArWyiica! www.a cam i i ANALYTICAL RESULTS Project: Cu and Zn Sampling 9/17 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Pace Project No.: 92400203 Sample: Gutter Sample Lab ID: 92400203001 Collected: 09117118 05:02 Received: 09/20/18 11:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 200.7 MET ICP Copper Zinc Analytical Method: EPA 200.7 Rev 4A 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 37.0 ug/L 5.0 1 09/23/18 23:45 0912411817:08 7440-50-8 168 ug/L 10.0 1 09/23/18 23:45 09/24/18 17:08 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/25/2018 05:26 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 13 ceArkdy i al r1 rewrrpeckb&=n 1 ANALYTICAL RESULTS Project: Cu and Zn Sampling 9117 Pace Project No.: 92400203 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Non -Contact Rain Sample Lab ID: 92400203002 Collected: 09/17118 05:15 Received: 09/20/18 11:55 Matrix: Water Parameters Resutts Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 37.7 ug/L 5.0 1 09/23/18 23:45 09/24/18 17:11 7440-50-8 Zinc 188 ug1L 10.0 1 09/23/18 23:45 09/24/18 17:11 7440-66-6 Date: 09/25/2018 05:26 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 13 Pace Analytical Services, LLC CEAnril li l0 9800 Kincey Ave. Suite 100 kuntersville, NC 28078 www. com t704j875-9092 ANALYTICAL RESULTS Project: Cu and Zn Sampling 91V Pace Project No.: 92400203 Sample: Outfall 3A Lab ID: 92400203003 Collected: 09/17/18 05:35 Received: 09120118 11755 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff 200.7 MET ICP Copper Zinc Analytical Method: EPA 200.7 Rev 4A 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 40.6 ug/L 5.0 1 09/23/18 23:45 09/24/18 17:14 7440-50-8 190 uglL 10.0 1 09/23/18 23:45 09/24/18 17:14 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 09/25/2018 05:26 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13 lrG 111WIl,+a 1 wwwpwekb&catn ANALYTICAL RESULTS Pate Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Project: Cu and Zn Sampling 9117 Pace Project No.: 92400203 Sample: Outfatl 38 Lab ID: 92400203004 Collected: 09/17/18 05:38 Received: 09/20/18 11:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Anatytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 38.2 uglL 5.0 1 09/23/18 23:45 09/24/18 17:17 7440-50-8 Zinc 132 ug/L 10.0 1 09/23/18 23:45 09/24/18 17:17 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, Date: 09/25/2018 05:26 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 Pace Analtrtical Services, LLG G^ /�,��� 1! !e 9800 Kincey Ave. Suite 100 i±+M lJ1/'!I r Huntersville, NC 28078 ' w w" com (704)875-9082 f ANALYTICAL RESULTS Project: Cu and Zn Sampling 9117 Pace Project No.: 92400203 Sample: Penske Sampie (offsite) Lab ID: 9240020300E Collected: 09/17/18 05:10 Received: 09/20/18 11:55 Matrix: Water Parameters 200.7 MET ICP Copper Zinc Date: 09/25/2018 05:26 AM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 38.9 ug1L 5.0 1 09/23/18 23A5 09/24118 17:20 7440-50-8 185 ug/t_ 10.0 1 09/23/18 23:45 09/24/18 17:20 7440-13" REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 13 aceAWrcal' 1 enrm onews.cam I QUALITY CONTROL DATA Project: Cu and Zn Sampling 9117 Pace Project No.: 92400203 QC Batch: 432192 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92400203001, 92400203002, 92400203003, 92400203004. 92400203005 METHOD BLANK: 2382496 Matrix: Water Associated Lab Samples: 92400203001, 92400203002, 92400203003, 92400203004, 92400203005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L NO 5.0 OW411815:47 Zinc ug/L NO 10.0 0912411815:47 Pace Analytical Services, LLC 9800 Kiocey Ave. Suite 100 Huntersville, NC 2B078 (704)8759092 LABORATORY CONTROL SAMPLE: 2382497 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 492 98 85-115 Zinc ug/L 500 476 95 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2382498 2382499 MS MSD 92400335001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 502 505 99 100 70-130 1 Zinc ug/L 47.6 500 500 529 540 96 98 70.130 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2382500 2382501 MS MSD 92400216001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Copper ug(L NO 500 500 502 320 100 64 70-130 44 M1,R1 Zinc ug1L 44.7 500 500 537 355 98 62 70-130 41 M1,R1 Results presented on this page are in the unit indlcated by the "Unks- coiumn except whom an alternate unit is presented to the right of the msutt, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 09/25/2018 05:26 AM without the written consent of Pace Analytical Services, LLC- Page 9 of 13 1!zAtWXical� i E QUALIFIERS Project: Cu and Zn Sampling 9117 Pace Project No.: 92400203 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 PQL - Practical Quantifation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyle in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nilrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pare Analytical is TN accredited. Contact your Pace PM for the current list of accredited anaiytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/25/2018 0&26 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 /IceArdytical* wrw.pacelaba.mm f f QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Cu and Zn Sampling 9/17 Pace Project No.: 92400203 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875r9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92400203001 Gutter Sample EPA 200.7 Rev 4.4 1994 432192 EPA 200.7 Rev 4.4 1994 432216 92400203002 Non -Contact Rain Sample EPA 200.7 Rev 4.4 1994 432192 EPA 200.7 Rev 4.4 1994 432216 92400203003 Outfail 3A EPA 200.7 Rev 4.4 1994 432192 EPA 200.7 Rev 4.4 1994 432216 92400203004 Outfall 3B EPA 200.7 Rev 4.4 1994 432192 EPA 200.7 Rev 4.4 1994 432216 92400203005 Penske Sample (offsite) EPA 2007 Rev 4.4 1994 432192 EPA 200.7 Rev 4A 1994 432216 Date: 09/25/2018 05:26 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 13 Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville D— Raleigh❑ Mechanicsville[] Client Name: -1 ?tLyd • Gt�Od � (01 - Project : Courier; ❑F d Ex UPS ❑USPS Client [ommerpal ace Other: Custody Seal Present? []Yes []0—o Seats InUct? []Yes . hla patelinmals Paton Examint" Packing Material-. ❑Bubble wrap ❑Hubble Bags tease ❑ Other OHlologkcal�Frouea7 Thermometer: Yes ft N A ��Gun ID: 92TO45 Type of Ica: et .❑Blue []None Cooler Temp l'[j: I ? Carrecftn Factor: Add/Subtract J*Q -O- i �^ Temp should be above freezing to 6*C Cooler Temp Corrected l'tj: ©samples out of temp criteria. samples an ice, cooling process has begun USDA Regulated Sol) j.Q-N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did sarnpies originate horn a foreign source (internationally, nYes MNo indudimHawaii and Puerto RimPrIYes 11No Comments/Dlscnepan"; Chain of Custody Present? EJ"s ELM N/A I. Samples Arrived within Hold Time? es ONG N/A 2. Short Hold Time knalysb 1<72 hr.17 a IV. ONIA 3. Rush Tum Around TimeRequested? Yes r No []N/A 4. Sufficient Vatume? GM ON* []N/A S. Correct Containers Used? -Pace Containers Used? ❑9es Dyes []No ❑No OHM ❑ A 6. Containers Intact? firve, No N/A 7. Dissolved analysis-. Samples Field Filtered? ❑Yes Oft 15MA S. Sample Labeh Match CDC? -Includes Dateffi ne/]D/Ana sis Matrix: Ej►m VVT ❑No []N/A 9. beads ace in VOA Vials (>5-6rnml? ❑YrA 13M, OWA 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes (390 Wo ❑N/A N/A 11, COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLIMON Field Data Required? []Yes []NO Person contacted: DateMme: Project Manager SCURF Review: { _ Date: "1 Project Manager SRF Review: Date: C� Ci Page 12 of 13 CHAIN -OF -CUSTODY 1 Analytical Request Document PaceNarlylicat �' �.. . The Chain -of -Custody is a LEGAL DOCUMENT. All relevant Gelds must be completed accir13teEy. i rn Section A Section S Section C 0 Required Client Information: Required Project Information; Invoice Infarmation: Pau : 1 Of t COmpany: Uniled Scrap Molal Report To: John De!go/Ashley Hamillon Atientl-I Address: 9925 Breoklord Street Copy To Company Namo: Charlotte, NC 28273 Address: 111r, I I litagulawwZgenvy Emasl: Purchase Order e_ Pace Quota. I Phone; Fa>I Project Nome Cu and Zn sam Ire Pace Project MonW. an la.heioni calab$ corn •: -i ` : State I Location Requested Due Dale, Proleq N: Pero Profile #; 8513-1 E NC ' R uested An is Filtered Y7N - a � Z MATWA coot 3 4°, COLLECTED Presefvatives } uM01-9 w. a Dw le 0 . . W w..o-wn.. vw Plft Rse xd P i 3 0 N _ el.a SL SAMPLE ID tF."TSTAFITT END w F a m au One Character par hex. wow vra AR . u, C, r~ m u � ,4 0 U 2GY IAZ, 0•9I..1 Ad `� g , m � Sample ids must he unique Tn,�. .�+, u�i Fj a G m a y Cz) D t a n mME DATE TIME .r S 2 = Z 7ci i' • 6 %I- ,2 s` , LA awv *La 7 �B I I ;9 12' 'ADD{TIONAL COMMENTS - RELINCthSHEt) IAFFILIA DATE TIME ACCEPTED BYr AFFILIATION •• DATE c T1M :: �•'' SAMPLE COHDiT10N9 . lsr ., r� I r SAMPLER NAME: AND SIGNATURE . PRINT Name of SAMPLER: E m M IL SIGNATURE of SAIApLER: DATE SirJncd; " m i= m I.;of >. to U r (A� aceAnalyflcal wwwpaaakftcom October 29, 2018 Adam Wilk United Scrap Metal 1545 S. Cicero Avenue Cicero, IL 60804 RE: Project: Stormwater Pace Project No.: 92403446 Dear Adam Wilk: Pace Analytical services, LLc 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 RECEIVED DEC 6 2013 DEW-DEMLR Land Quality Section A"oresville Regiornal ice Enclosed are the analytical results for sample(s) received by the laboratory on October 15, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, kept in full, . without the written consent of pace Analytical Services, LLC. Page 1 of 20 aceAnalytical www'P8cobfto n Project: Stormwater Pace Project No.: 92403446 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 900 Huntersville, NC 28078 (704)87E-9092 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification t 5342 North Carolina Wastewater Certification #: 12 CERTIFICATIONS South Carolina Certification #: 99006001 Florida[NELAP Certification #: E87627 Kentucky UST Certification #: 84 MrginiaNELAP Certification #: 460221 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NEIAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VrginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 20 aceAnalsrtical o Wnv.Pecateesmm Project: Stormwater Pare Project No.: 92403446 Lab iD Sample ID 92403446001 Penske 92403446002 Non Contact 92403446003 Gutter 92403446004 3A 92403446005 3B 92403446006 OutfallI 92403446007 Outfall2 92403446008 Outfall3 F Pace Analytical Services, LLC 980D Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A EPA 200.7 Rev 4.41994 SH1 3 PASI-A EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A EPA 1664B JMS 1 PASI-C EPA 2007 Rev 4.4 1994 SH1 3 PASI-A SM 2540D-2011 CRV 1 PASI--A SM 5220D-2011 GC 1 PASI-A EPA 1664E JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 254OD-2011 CRV 1 PASI-A SM 5220D-2011 GC 1 PASI-A EPA 1664E JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 SHi 3 PASI-A SM 2WD-2011 CRV 1 PASI-A SM 5220D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 20 aceAnalyfical www.pacefabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 Project: Stormwater Pace Project No.: 92403446 Sample: Penske La61D: 92403446001 Collected: 1011111811:05 Received: 10/15/18 10:15 MaWx: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Capper 5.8 ug/L 5.0 1 10/16/18 01:17 10/17/18 02:55 7440-50-8 Lead ND ug[L 5.0 1 11011611180117 10/17/18 02:55 7439-92-1 Zinc 14.7 ug/L 10.0 1 10/16/18 01:17 10/17/18 02:55 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/29/2018 03A6 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 20 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 L amaly ml Huntersville, NC 28078 mrw.PMbbsmm (704)875-9092 ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92403446 Sample: Non Contact Lab ID: 92403446002 Collected: 10/11/18 11:09 Received: 10/15/18 10:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 10.6 ug/L 5.0 1 10/16/18 01:17 10/17/18 03:14 7440-50-8 Lead ND ug/L 5.0 1 10/16/18 01:17 10/17/18 03:14 7439-92-1 Zinc 20.4 ug/L 10.0 1 10/16/18 01:17 10/17/18 03:14 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 03:46 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 20 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 10U lkceMalXimls Huntersville, NC 28078 WWW.paceh?°SC n (704)875-9092 ANALYTICAL RESULTS Project: Storrnwater Pace Project No.: 92403446 Sample: Gutter Lab lD: 92403446003 Collected: 10/11/18 11:00 Received: 10/15/18 10:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qua] 200.7 MET [CP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4A 1994 Copper ND uglL 5.0 1 10/16/18 01:17 10/17/18 03:17 7440-50-8 Lead ND ug/L 5.0 1 10116/18 01:17 10/17/18 03:17 7439-92-1 Zinc 364 uglL 10-0 1 10/16/18 01:17 10/17/18 03:17 7440-66-6 REPORT OF LABORATORY ANALYSIS This reportshail not be reproduced, except in full, Date: 10/29/2018 03:46 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 20 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 aceARalyt�cal Huntersville, NC 28078 wwwcom (704)875-9092 ANALYTICAL. RESULTS Project: Stormwater Pace Project No.: 92403446 Sample: 3A Lab ID: 92403446004 Collected: 10/11/18 10:45 Received: 101151181015 Matrix: Water Parameters Results Units Report Limit DE Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 33.9 ug1L 5.0 1 10/16/18 01:17 10/17/18 03:20 7440-50-8 Lead 14.3 ugll- 5.0 1 10/16/18 01:17 10/17/18 03:20 7439-92-1 Zinc 468 uglL 10.0 1 10/16/18 01:17 10/17/18 03:20 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be repmduced, except in full. Dale: 10/29/2018 03:46 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 20 Pace Analytical Services, LLC 9800 Kincey Ave. Suite too aceMalytical HuntersWle, NC 28078 > (7o4)875-9o82 ANALYTICAL RESULTS Project: Slormwater Pace Project No.: 92403446 Sample: 3B LabID: 92403446005 Collected: 10/11/18 11:01 Received: 10/15/18 10:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA200.7 Rev4.4 1994 Preparation Method: EPA200.7 Rev 4.4 1994 Copper 69.0 ug1L 5.0 1 10/16/18 01:17 10/17/18 03:23 7440-50-8 Lead 14.7 ug/L 5.0 1 10116/18 01:17 10/17/18 03:23 7439-92-1 Zinc 225 ug1L 10.0 1 10/16/18 01:17 10/17/18 03:23 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 03:46 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 20 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville, NC 28078 www.paceiabs.com (704)875-9092 ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92403446 Sample: Ouffall 1 Lad lD: 92403446006 Collected: 10/11/18 09:54 Received: 10/15/18 10:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND ' mg/L 5.0 1 10/29118 03:42 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4A 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 7.9 ug1L 5.0 1 10/16/18 01 A 7 10/17/18 03:26 7440-50-8 Lead ND ug/L 5.0 1 10/16/18 01:17 10/17/18 03:26 7439-92-1 Zinc 103 ug/L 10.0 1 10/16/18 01:17 10/17/18 03:26 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 5.0 mg/L 2.8 1 10/16/18 15:57 5220D COD Analytical Method: SM 5220D-20il Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg1L 25.0 1 10/17/18 16:30 10/17/18 21:48 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 03:46 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 20 aceAnal,A a @ www.pacalabs.wm ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 92403446 Sample: Ouffall 2 Lab ID: 92403446007 Collected: 10/11/18 10:30 Received: 10115118 10:15 Matrix: Water Parameters Results Units Report Limit DE Prepared Analyzed CAS No. Qua[ HEM, Oil and Grease Oil and Grease 200.7 MET ICP Capper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids 5220D COD Chemical Oxygen Demand Date: 10/2912018 03:46 PM Analytical Method: EPA 1664B ND mgfL 5.0 1 10/29/18 03A2 Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 7.1 ug1L 5.0 1 10116/18 01:17 10/17/18 03:29 7440-50-8 ND ug1L 5.0 1 10/16/18 01:17 10/17/18 03:29 7439-92-1 116 ug1L 10.0 1 10116/18 01:17 10/17/18 03:29 744D-66-6 Analytical Method: SM 254OD-2011 3.3 mgJL 2.5 1 1011611815:58 Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 ND mg1L 25.0 1 10/1711816:30 1011711821A9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 20 aceAnalytical www.pacahbs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Pace Project No.: 92403446 Sample: Outfall 3 Lab lD: 92403446008 Collected: 10/11/18 10:48 Received: 10/15/18 10:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] HEM, Oil and Grease Oil and Grease 200.7 MET ICP Copper Lead Zinc 2540D Total Suspended Solids Total Suspended Solids 5220D COD Chemical Oxygen Demand Date: 10/29/2018 03:46 PM Analytical Method: EPA 1664B ND mg/L 5.0 1 10/29/18 03:43 Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 34.3 ug/L 5.0 1 10/16/18 01:17 10/17/18 03:32 7440-50-8 18.8 ug/L 5.0 1 10/16/18 01:17 10/17/18 03:32 7439-92-1 466 ug/L 10.0 1 10/16/18 01:17 10/17/18 03:32 7440-66-6 Analytical Method: SM 254OD-2011 9.5 mg/L 2.6 1 10/1611815:59 Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 35.9 mg/L 25.0 1 10/17/18 16:30 10/17/18 21:50 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 20 acemalAcal wxwpaeelabseom QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92403446 QC Batch: 438868 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92403446006, 92403446007, 92403446008 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 2412354 Matrix: Water Associated Lab Samples: 92403446006, 92403446007, 92403446008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mglL ND 4.8 10/29/18 03:41 LABORATORY CONTROL SAMPLE: 2412355 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg1L 38.5 36.9 96 78-114 MATRIX SPIKE SAMPLE: 2412356 92403952001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 38.5 380 99 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 03:46 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 20 aceAnaly�ica! wwwpacela6amm QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92403446 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 436340 Analysis Method: EPA 2003 Rev 4.4 1994 QC Batch Method: EPA200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92403446001, 92403446002, 92403446003, 92403446004, 92403446005, 92403446006, 92403446007, 92403446008 METHOD BLANK: 2400748 Matrix: Water Associated Lab Samples: 92403446001, 92403446002, 92403446003, 92403446004, 92403446005, 92403446006, 92403446007, 92403446008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper uglL ND 5.0 10/17/18 02:49 Lead - ug1L ND 5.0 10/17/18 02:49 Zinc uglL ND 10.0 10/17/18 02:49 LABORATORY CONTROL SAMPLE: 2400749 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper ug1L 500 500 100 85-115 Lead ug/L 500 465 93 85-115 Zinc uglL 500 466 93 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400750 2400751 MS MSD 92403446001 Spike Spike MS Parameter Units Result Cone. Cone. Result Copper ug1L 5.8 500 500 521 Lead uglL ND 500 500 485 Zinc ug1L 14.7 500 500 509 MSD MS MSD % Rec Result % Rec % Rec Limits RPD Qual 524 103 104 70-130 0 490 97 98 70-130 1 512 99 100 70-130 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/29/2018 03:46 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 20 aceAnaocal' wwwpacafebamm QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92403446 Pace Analytical Services, LLC 9800 Kincey Ave. Suite Soo Huntersvii1e, NC 28078 (704)875-9092 QC Batch: 436470 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92403446006, 92403446007, 92403446008 METHOD BLANK: 2401568 Matrix: Water Associated Lab Samples: 92403446006, 92403446007, 92403446008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 10/16/18 15:53 LABORATORY CONTROL SAMPLE: 2401569 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mg[L 251 250 100 90-110 SAMPLE DUPLICATE: 2401570 92403503001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 95.0 88.3 7 D6 SAMPLE DUPLICATE: 2401571 92403504003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL ND ND Results presented on this page are in the units indicated by the-Unlis" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Cull. Date: 1012912018 03:46 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 20 aceAnalytical www.panetaescam QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92403446 QC Batch: 436753 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92403445006, 92403446007, 92403446008 METHOD BLANK: 2402786 Matrix: Water Associated Lab Samples: 92403446006, 92403446007, 92403446008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg1L ND 25.0 10/17/18 21:46 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)B75-9092 LABORATORY CONTROL SAMPLE: 2402787 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 763 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2402788 2402789 MS MSD 92403444001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Chemical Oxygen Demand mg/L 31.0 100 100 139 139 108 108 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2402790 2402791 MS MSD 92403534001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua] Chemical Oxygen Demand mg1L T7.7 100 100 183 145 106 69 90-110 22 M1,R1 Results presented on this page are In the units Indicated by the "!]nits" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 10/29/2018 03:46 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 20 aceftlytical e WW Wpiacelebs cam QUALIFIERS Project: Stormwater Pace Project No.: 92403446 DEFINITIONS DF - Dilution Factor, it reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. Pace Analytical Services, LLC 9BOD Kincey Ave. Suite 100 Huntersville, NC 2807E (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Dipheny[hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyses. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/29/2018 03:46 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 20 aceAnalytical e www.patetaba.=n QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No-: Stormwater 92403446 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92403446006 Outfall 1 EPA 1664E 438868 92403446007 Outfall 2 EPA 1664B 438868 92403446008 Outfall 3 EPA 1664B 438868 92403446001 Penske EPA 200.7 Rev 4.4 1994 436340 EPA 200.7 Rev 4.4 1994 436354 92403446002 Non Contact EPA 200.7 Rev 4.4 1994 436340 EPA 2007 Rev 4.4 1994 436354 92403446003 Gutter EPA 200.7 Rev 4A 1994 436340 EPA 200.7 Rev 4.4 1994 436354 92403446004 3A EPA 200.7 Rev 4.4 1994 435340 EPA 200.7 Rev 4.4 1994 436354 92403446005 3B EPA 200.7 Rev 4.4 1994 436340 EPA 200.7 Rev 4.4 1994 436354 92403446006 Outfall 1 EPA 200.7 Rev 4.4 1994 436340 EPA 200.7 Rev 4.4 1994 436354 92403446007 Outfall 2 EPA 200.7 Rev 4.4 1994 436340 EPA 2007 Rev 4.4 1994 435354 92403446008 Outfall 3 EPA 200.7 Rev 4.4 1994 436340 EPA 200.7 Rev 4.4 1994 436354 92403446006 Outfall 1 SM 25401)-2011 436470 92403446007 Outfall 2 SM 254OD-2011 436470 92403446008 Outfall 3 SM 254OD-2011 435470 92403446006 Outfall 1 SM 5220D-2011 436753 SM 5220D-2011 436823 92403446007 Outfall 2 SM 5220D-2011 436753 SM 5220D-2011 436823 92403446008 Outfall 3 SM 522OD-2011 436753 SM 5220D-2011 436823 Date: 10/29/2018 03:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 20 rx" "AWL— !2 _ 1� ` Document Name: Sample Condition Upon Recel t(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Downtent No-_—___� F-CAR-CS-U33-Rev.06 Issuing Authority: Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville a"- Raleigh[] Mechanicsville❑ SampleCondition Clienttllame: Wp# : 92403446 Upon Rett-ipt. ProJecttf:UNU Courier: []Fed Ex ❑UPS ❑ SPS ❑[Cent l I� I� �� �� ❑ Commercial 41race ]]Other: / 92403446 Custody SealPresent7 ❑Yes ,3No Seats Intact? Dyes p14o L 11�1���� Date/hritlaV Person Examining Contents: (J Packing Material: ,QBubble Wrap (i]Suhble sags ❑None ❑ Other Biological Tissue Frozen? Thermometer: Oyes ❑No,.❑N/A ❑ IR Gun I D: 92T045 Type of ice: (31Net []Blue []Nona Cooler Temp ('C): iJ' G Correction Factor: Add/Subtract (T) _� ) Temp should be above freezing to 6'C Cooler Temp Corrected {. C):' m out of tam csiteria.5am Samples on Ice, cooling ❑Sa pies p p 6 Process hasbegun USDA Regulated Sall (0 ilk water sample) Did samples originate in a quarantine Zone within the United States. CA, NY, or SC (Check maps)? Did samples originate from a foreign source {Internationally, I71vac naln inrk,Atna Ha,caa and Dcxmtn Mr.17 r1Vot CINn Commimts/Discrepancr. Chain of Custody Present? 1214. LIN. NIA 1. Samples Afrived within Hold Time? Yes ON. N/A 2. Short Hold Time Ana h (<72 hr.)? Yes WK. ❑NIA 3. Rush Turn Around Time Re uested7 OY. No ❑N/A 4. Sufficient Volume? es J2NO ❑N/A 5. Correct Containers Used? -Pace Containers Used? Wes Ures ONO Quo ❑N/A ❑N A 6. Containers totact? pYes Ono ❑NIA 7. Dissolved analysis: Samples Field Filtered? JOYes No NIA B. Sample Labels Match COC? -Includes Datel7imeAD/Anal is . Matrix: PYes ONO ©N/A 9. Heads ace in VOA Vials (>5-6mm)? Yes No /A 10• Trip Blank Present? Trip Blank Custody Seats Present? ❑Yes ❑Yes ONO No /]N/A �N/A 11. COMMENTS/SAMPLE DISCREPANCY I Field Data Required? ❑Yes ONO (urn p u S (unI-CtI C`,I Li�`u I (11 U0�- tg_r'u' itys- Nub] Ci jf-ria kuI 5CU-1 tc, - ki -rr_-1 ?CO 110q a kLwr- CLIENT NoiiFirATION/RESOLUTION Person contacted: Datefrime: Project Manager SCURF Review: n Date: Project Manager SRFReview: IDate: Page 18 of 20 w m 0 N 0 L 3 v G T w a n a: b a CL C rn 3 a 9 �s 6 N B) �Iya� q CL Cu tt .� rC rn a n qu A N W MO m -4 O1 trl L W N 1-` Harrill zzz—zzzzzz zz BP41111-125 ml Plastic Unpreserved (N/A) (CI-) BP3U-250 ml. Plastic Unpreserved IN/Al 8P2U-500 mL Plastic Unpreserved IN/A) BP1U-1 liter Plastic Unpreserved (N/A) r BP45 12S mL PlastlC HZSO4 )pH <Zl (CI-) BP3N-250 mL plastic HNO3 (pH a 2) BP4Z-125 mL Plastic ZN Acetate & NaOH (>9i zzzBP4C-125 mL Plastic NaOM (pH > 12) (CI-) WGFU-Wide-mouthedGiassjar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (Cl-) A61H-1 liter Amber HCI (pH a 2) AG3U-250 mL Amber Unpreserved IN/A) (CI-) AGlii liter Amber H2SO4 (pti a 2) AG34-250 mL Amber H2504 (pH < 2) iz A63A(DGBA)-250 mL Amber NH4CI (N/A)(CI-) DG9HAO mL VOA HCI (N/A) VG9T4D mL VOA Na25203 (N/A) V09Ua40 mL VOA Unp IN/A) DG9P-4D mL VOA H3PO4 (N/A) VOAK (6 viah per k)t)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit IN/A) SPST-125 mL Sterile Plastic (N/A— lab) SP2T-250 mL Sterile Plastic IN/A — lab) BP3A-250 rat. Plastic INH2)25D4 (9.3-9.7) AGOU-1D0 mLAmber Unpreserved vials IN/A) VSGU-20 mL Scintillation vials (NIA) DG9U-40 mL Amber Unpreserved vials IN/A) -o 3 1� t7 C ro v !v eF ro t9 N (D r+ tea.. A K i CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed acc urately. Section A Section a Section C Required Client nfomyatlon: Required Project Information: invoice information: Page ; i Of 1 Company: U 'led Scra Metal Report To: John Derflo/Alihley Hamilton Attention q Address: 9425 Drooklord Street Copy To; Company Nara: Chartede. NC 2073 Address: ReflulataryAgancy Email: A1A A, Q!74t Purchase Order p: Paco Quote: Phone; IFax Project Name: Slomrwwor Para Project Manager, gMelaAmlonl0pacalabs.com, u _ State'l Location •x Requested Due ate: Project IF: Pace Profila #: 6513-1 NC - tedAnat a Filtered a � uATam CODE 9 COLLECTED Preservatives •r ' QW*" W" VN wea wr H V V walow" V%w f• M C` 4 SAMPLE ID a ad a $ START END y �jn„ �� One character per box µ Alt w n l V On.. OT aIftMul.d I8ampla Ida must be unique Taw. To a t° ��y 7C m w OgOgg s Z z � a 0 DATE TIME DATE T[ME x T 0 J°•w /oww 1I- 2 W o- ptafm w-1 'i 4; G ar't r 40MI la-Ih Iq- Q fl"4 AnomoNALcoMMtorls I unlaulsHEDerIAFrTLIATtoN DATe itlAt .' z•: yam_ . ACCEPIEDBYIAFFlUATION �. Ddita i' +m TMt sAn+PLt coNomoNs �► l� S� Z 4 3 b,L SAMPLER NANI!; AND stGNATutiE._ .. �nk PRINT Name of SAMPLER:^ �¢f o � m � 9 � m •G SIGNATURE of SAMPLER: DATE Signed: � a�9 0 u) 0 N 0 0 N e) m al a conmtest° nwlLrnt'Ju. L"ow+rom 39 Spruce Street' East Longmeadow, MA 01028 ' FAX 413/525-6405 ` TEL. 413/525-2332 October 29, 2018 John Dergo Single Projects 2018 9925 Brookford St. Charlotte, NC 28273 Project Location: United Scrap Metal Client Job Number: Project Number: [none] Laboratory Work Order Number: 18J0883 Enclosed are results of analyses for samples received by the laboratory on October 17, 2018. 1f you have any questions concerning this report, please feel free to contact me. Sincerely, V&1 4vn%J.` Kerry K_ McGee Project Manager Table of Contents Page 1 of 26 Table of Contents Table of Contents Sample Summary Case Narrative Sample Results 18JO883-01 18JO883-02 18J0893-03 18J0883-04 18JO883-05 18J0883-06 18J0883-07 18JO883-08 Sample Preparation Information QC Data Metals Analyses (Total) B215499 Conventional Chemistry Parameters by EPAIAPHAISW-846 Methods (Total) B214991 B215092 B215403 Flag/Qualifier Summary Certifications Chain of Custody/Sample Receipt 3 4 5 5 6 7 8 9 10 12 14 16 17 17 17 18 18 18 18 19 20 21 Page 2 of 26 Table of Contents comtesto ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 ' TEL. 413I525-2332 Single Projacts_2018 9925 Brookfard St. REPORT DATE; 10/29/2018 Charlotte, NC 28273 PURCHASE ORDER NUMBER: ATTN: John Dergo PROJECT NUMBER: [none] ANALYTICAL SUMMARY WORK ORDER NUMBER 1810883 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this reppatt. PROJECT LOCATION: United Scrap Metal FIELD SAMPLE 4 LAB ID: MATRIX SAMPLE DESCRIPTION • TEST SUB LAB 3A ISJOB83-01 Waste Water EPA 200.7 3B I8JOB83-02 Waste Water EPA 200.7 Penske IBJ0883-03 Waste Water EPA200.7 Gutter Sample 1930883-04 waste Water EPA 200.7 Nan Contact Rain ISJ0883-05 Waste Water EPA200,7 Outfall 1 19J0883-06 Waste Water EPA 1664E EPA 200.7 EPA 410.4 SM21-22 2540D Outfall 2 1810883-07 Waste Water EPA 1664B EPA 200.7 EPA 410A SM21-22 2540D Outfall 3 1810993-08 Waste Water EPA 1664E EPA 200.7 EPA 410.4 SM21-22 2540D Page 3 of 26 Table of Contents conwtx-st° MIALYMAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 ' FAX 4131525-6405 - TEL, 413I525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved mcdrodologies listed in this document, and that based upon my inquiry of those individuals inmtediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington praject Manager Page 4 of 26 Table of Contents conTtest" ANALrnGALLABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 ' TEL. 413I525-2332 Project Location: United Scrap Metal Samplc Description: Work Order: IBJ0883 Date Received: 10/17/2018 Field Sample #: 3A Sampled: 10/11/2018 10:45 Samnle ID: 18J0883-01 Samnlc Matrix: Waste Water Metals Analyses (Total) Date DatefTime Analyte Results RL Units Dilution Flag/Qua[ Method Prepared Analyzed Analyst Copper 0.031 0.0050 mglL l EPA 200.7 10/23/18 10/24118 13:13 QNW Zinc 0.49 0.010 mg/L I EPA 200.7 10/23/18 W24118 13:13 QNW Page 5 of 26 Table of Contents con4tc-st° 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 4131525-6405 `TEL. 4131525-2332 Pmject Location: United Scrap Metal Sample Description: Work Order: 1830883 Date Received: 10/17/2018 Field Sample N: 3B Sampled: 10/11/2018 11:00 Samnle ID: ISJOS83-02 SamD]e Matrix: Waste Water Metals Analyses (Total) Analyte Results RL Units Dilution. Copper 0.068 0.0050 mg/L I Zinc 0.24 0.010 mglL l Date Date Time Method Prepared Analyzed Analyst EPA 200.7 10/23/18 10/24/18 13:19 QNW EPA200.7 10/23/18 102411813:19 QNW Page 6 of 26 Table of Contents ticonmltfsd`� ANALWWAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 " FAX 4131525-6405 ' TEL 413/525-2332 Project Location: Unitcd Scrap Metal Sample Description: Work order: 1810883 Date Received: 1011720 i 8 Field Sample#: Penske Sampled: 1011WO18 11:05 Sample ID: ISJ0883-03 Sample Matrix: Waste Water Metals Analyses (Total) Date DatrJTime Analyte Results RL Units Dilution FlaglQual Method Prepared Analyzed Analyst Copper 0.0057 0.0050 mg/L l EPA 200.7 10/23/18 10/24/18 13:24 QNW Zinc 0.018 0.010 0191L 1 EPA 200.7 1 U 3118 10/24/18 13:24 QN W Page 7 of 26 Table of Contents conmtesl'O nwnl_rn IAL UMORATORV 39 Spruce Street' East Longmeadow, MA 01028 ' FAX 413/525-6405 ' TEL. 4131525-2332 Project Location: United Scrap Metal Semple Description: Work Order: 18JO883 Dace Received: 10117l2018 Field Sample 4. Gutter Sample Sampled: ]0111l2018 11:06 Samnle ID: 18J0883-04 Sample Matrix: Waste Water Metals Analyses (Total) Date DatelTime Analyte Results RL Units Dilution FIaglQual Method Prepared Analyzed Analyst Copper ND 0.0050 mg/L 1 EPA200.7 10/23/18 10/24/1813:30 QNW Zinc 0.23 0.010 mg/L 1 EPA 200.7 10/23/18 1024/18 13:30 QNW Page 8 of 26 Table of Contents Con test® AAIALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 ' FAX 4131525-6405 ' TEL. 413/525-2332 Project Location: United Scrap Metal Sample Description: Work Order: 1810883 Date Received: 10/17/2019 Fidd Sample @: Non Contact Rain Sampled: 10/11/2018 11:08 Sample ID: I8J0S93-05 Sam41e Matrix: Waste Wafer Metals Analyses (Total) Date DatetTime Aualyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Copper 0.0084 0.0050 mg/L 1 EPA 2003 10/23/18 10/24/18 13:07 QNW Zinc 0,016 0.010 mgll. 1 EPA200.7 10/23/19 10/2411813:07 QNW Page 9 of 26 ton -test° ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 ' FAX 4131525-6405 ' TEL, 4131525-2332 Project Location: United Scrap Metal Sample Description: Work Order: 1810a83 Date Received: 10/17/2013 Field Sample N: Outfatt 1 Sample ID: ISS0883-06 StartDatefrime: 101112018 10:00:00AM Sample Matrix: Waste Water Stan Datell'trne: 10/11/2018 10:08;00AM Metals Analyses (Total) Date DatelCime Analyte Results RL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst Copper 0.012 0.0050 mglL 1 EPA200.7 10/23/18 10/24/1813:36 QNW Lead ND 0.0050 m81L 1 EPA200.7 1023/19 10241181136 QNW Zinc 0.11 0.010 mg/L I EPA 200.7 1023/18 1024/18 13:36 QNW Page 'E4 of 26 co n M te s-- to IT ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 ' FAX 413/525-6405 ' TEL. 4131525-2332 Project Location: United Scrap Metal Sample Description: Work Order: I8i0883 Date Received: 10117/2018 Field Sample k: Outfall 1 Sample ID: IS.i0883-06 StartDatelrime: 10/11/2018 I0:00:OOAM Sample Matrix: Waste Water Stoo Date/rime: 10/11/2018 10:08:00.AM Conventional Cbemistry Parameters by EPAIAP"SW-846 Methods (Total) Date Date/Time Analyte iiesults RL Units Dilution FtaglQual Method Prepared Analyzed Analyst Chemical Oxygen Demand 23 15 mg/L 1 EPA 410.4 10123/18 - 10/23/18 10:15 MMH Total Suspended Solids 3.0 1.0 mg/L I SM21-22 2540D 10117/18 10/17/18 14:00 LL Oil & Grease (HEM) ND 1.4 mglL I EPA 1664B 10118/18 10/18/18 12:45 LL Page 11 of 26 .1 cornmtesd ' AHACjT1 l LABORATORY Table of Contents 39 Spruce Street' East Longmeadow. MA 01028 ' FAX 413/525-6405 ` TEL. 413/525-2332 Project Location: United Scrap Metal Sample Description: Wart; Order: ISJO883 Date Received: IOAV2018 Field Sample #: Outfall 2 Sample ID: ISJ0S047 Start DateTime: 10/11/2018 10:30:OOAM SamDle Matrix: Waste Water Stop Date/1"ime: 10/11/2018 10:34:00AM Metals Analyses (Total) Date Date/Time Analyte Results RL Units Dilution FluglQual Method Prepared Analyzed Analyst Copper 0.0681 0.0050 mg/L I EPA200.7 10123118 10n411813:42 QNW Lead ND 0.0050 mg/L 1 EPA200.7 10/23118 10/24/1813:42 QNW Zinc 0.12 0.010 mg/L I EPA200.7 10123/18 10/2411813:42 QNW 7-1 Page 12 of 26 Table of Contents .. ,WconTtescr AL,R1t:NL ulsowlro�r 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 ` TEL. 4131525-2332 Project Location: united Scrap Metal Sample Description: Work Order: ISJO883 Daze Reeoived: 10/17/2018 Field Sampled: Oatfall2 Sample III: 18d0SM-07 Start Datefl`tme: 10111MIS 10:30:OOAM Sample Matrix: Waste Water Stoo Datefrime: 10/11/2018 10:34:OOAM Conventional Chemistry Parameters by EPAIAPHAISW446 Methods (Total) Date Date/Time Analyte Results RL Units Dilution FlaglQnal Method Prepared Analyzed Analyst Chemical Oxygen Demand 26 15 mgAL 1 EPA410.4 10/23/18 10123/1810:15 MMH Total Suspended Solids ND 1.0 mg/L 1 SM21-22 2540D 10/17/18 10117/18 14:00 LL Oil & Grease (HEM) NO 1.4 mg1L 1 EPA 1664B ]0118l18 10/18/18 12:45 LL Page 13 of 26 Table of Contents joh 0nftet. "vv-Y CAL EABOMM" 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 ' TEL. 413/525-2332 Project Location: United Scrap Metal Sample Description: Work Order: 18JO883 Date Received: E011712018 Field Sample N: Outfall3 Sample 1D: ISdOS83-08 Stan Date/Time: 10/11/2018 10:42:OOAM Samole Matrix: Waste Water Stan Date/Time: 10/11/2018 10:46:00AM Metals Analyses (Total) Date Datetrime Analyte Results T RL Umits Dilution FlaglQual Method Prepared Analyzed Analyst Copper 0.033 0.0050 -91L 1 EPA 200.7 10/23/19 1024118 13:47 QNW Lead ND 0.0050 mg/L l EPA200.7 10/23/19 10/24/181147 QNW Zinc 0.50 0.010 ma& I EPA 200.7 10/23/18 1024/18 13:47 QNW Page 14 of 26 44 - - a4es "� ANALYTWAL LABORATORY Table of Contents 38 Spruce Street' East Longmeadow, MA 01028 . FAX 4131525-6405 ' TEL. 41315252332 Project Location: United Scrap Metal Sample Description: Work Order: 1810883 Date Received: 1011712019 Field Sample N: Outfall 3 Sample ID: ISS0883-08 StartDateliune: 10/11/2018 1042:00AM Sample Matrix: Waste Water Stoo DatetTime: 10/11/2018 10:46:00AM C00ven601221 Chemistry Parameters by EPA/APHAISW-946 Methods (Total) Date Date)Time Analyte Results RL Units Dilution FIRVQual Method Prepared Analyzed Analyst Chemical Oxygen Demand 53 15 mg1L 1 EPA410.4 101231I8 102311810A5 MMH Total Suspended Solids ND 2.0 mplL I SM21-22 2540D 10/17/18 10/17/18 14:00 LI, Oil & Grease (HEM) ND 1.4 mglL 1 EPA 166413 10118/18 10/18/18 12:45 LL Page 1 5 of 26 cao n"t x-s- n> LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 4131525-6405 ' TEL. 4131525-2332 Sample Extraction Data EPA 16648 Lab Number [Field ID] Batch Initial [mL] Date 18JO883-06 [Outfall 11 B215092 1000 10/18/18 18J0883-07 [Outfa112] B215092 980 1o118118 18J0883-08 [Outfall 31 B215092 1000 10/18118 Prep Method: EPA 200.7-EPA 200.7 Lab Number [Field ID] Batch Initial ]mL] Final [mL] Date Table of Contents 1830993-0113A] B215499 50.0 50.0 10/23/18 1830983-02 [3B] B215499 50.0 50.0 10/23/18 1830993-03 [Penske] B215499 50.0 50.0 1023118 18J0883-04 [Gutter Sample] B215499 50.0 50.0 1023/19 18JO883-05 [Non Contact Rain] 8215499 30.0 50.0 10/23/18 18J0883-G6 [Outfall 1] B215499 50.0 50.0 1023118 18J0883-07 [Outfall 2] B215499 50.0 50.0 10/23/18 18J0883-08 [Outfall 3] B215499 50.0 50.0 1023/18 EPA 410.4 Lab Number [Field 1131 Batch Initial [mL] F-mal [mL] Date 18J0883-06 [Outfall 1] 13215403 2.00 2.00 1023/18 1810883-07 LOutfall 21 B215403 2.00 2.00 1023118 18J0883-08 LOutfal€ 31 B215403 2.00 2.00 1023118 SM21-22 2540D Lab Number [Field ID] Batch Initial [mL] Date ISJO883-06 [Outfall 1] 13214991 500 10/17/18 19JO883-07 [Outfall 21 13214991 500 10/17/18 1830983-08 [Outfall 3] 13214991 255 10/17/18 Page 16 of 26 0 COnmtEstg 39 Spruce Street ` East Longmeadaw, MA 01028 ' FAX 413/525-6405 ` TEL. 413/525-2332 Q IIALITX CONTROL Metals Analyses (Total) - Quality Control Table of Contents Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch 13215499 - EPA 200.7 Blank(B215499-BLK1) Prepared: 10/23/18 Analyzed: 10/24/18 Copper ND 0.0050 mg/L Lead NOD 0.0050 mg/L Zinc ND 0,010 mg/L LCS (B215499-BSI) Prepared: 10/23118 Analyzed: 10/24/18 Copper 0.910 0.0050 mg/L 1,00 91.0 85-115 Lead 0.493 0.0050 mg/L - 0.500 98.5 85-115 Zinc 0.976 0.010 mg/L 1.00 97.6 85-115 LCS Dup (B215499-BSDI) Prepared: 10/23/18 Analyzed: f0/24118 Copper 0.933 0.0050 mg/L. 1.00 93.3 85-115 2.42 20 ' Lead 0.506 0.0050 mg/L 0.50D 101 85-115 2.75 20 Zinc 0.994 0.010 mg/L 1.00 99.4 85-115 1.83 20 Duplicate (B215499-DUPI) Source: 18I0883-05 Prepared: 10/23/18 Analyzed: 1D/24/18 Copper 0.00833 0.0050 mg/L 0.00842 1.14 20 Lead ND 0.0054 mg/L ND NC 20 Zinc 0.0166 0.010 mg/L 0.0161 2.93 20 Matrix Spike (B215499-MSi) Source•. 1SJ0883-05 Prepared: 10/23/18 Analyzed: 10/24/18 Copper 0.949 0.0050 mg1L. 1.00 0.00942 94.0 70-130 Lead 0.506 0.0050 mg/L 0.500 ND 101 70-130 Zinc 1.01 0.010 mg/L I.00 0.0161 99.7 70-130 Page 17 of 26 Table of Contents T 39 Spruce Street' East Longmeadow, MA 01028 ' FAX 413/525-6405 ' TEL. 4131525-2332 QUALITY CONTROL Conventional Chemistry Parameters by EPMAPHA/SW-846 Methods (Total) - Quality Contort Reporting Spike Source %aREC RPD Analyte Result Limit Units level Result %RFC Limits RPD Limit Notes Batch B214991 - SM21-22 2540D Blank (B214991-BLKI) Prepared & Analyzed: 10/17/18 Total Suspended Solids ND - 2.5 mg/L. LCS (B21499I-BSI) Prepared & Analyzed: 10/17/10 Total Suspended Solids 155 5.0 mg1l. 200 77.5 64.3-117 Batch 111215092 - EPA 1664B Blank (B215092-BLK1) Prepared & Analyzed: 10/18118 Oil & Grease (HEM) ND 1.4 mg/L LCS (B215092-BSI) Prepared & Analyzed: 10/18/18 Oil & Grease (HEM) 22 mg/L 20.0 110 78-114 Duplicate (B215092-1)UPI) Source: 1Sd0883-08 Prepared & Analyzed10/18/18 Oil & Grease (HEM) ND 1.4 mg/L ND NC 18 Batch B215403 - EPA 410.4 Blank (B215403-BLKI) Prepared &Analyzed: 10123/18 Chemical Oxygen Demand ND 15 mg/L LCS (B2] 5403-BS 1) Prepared & Analyzed: 10/23118 Chemical Oxygen Demand 190 15 m91L 200 95.8 90-110 LCS Dup (B2I S403-BSDI) Prepared & Analyzed: 10/23/18 Chemical Oxygen Demand 190 15 mg/L 200 95.9 90-110 0.00 7.06 Page 18 of 26 tic-On-RUS-V - ANALYFiCAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028' FAX 413/525-6405 'TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY • QC result is outside ofestahlished limits. t Wide recovery limits established for difficult compound. i Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level ND Not Detected RL Reporting Limit is at the level of quantitation (LDQ) DL Detection Limit is the lower limit of detection determined by the MDL study MCL Maximum Contaminant Level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted urdem specified in the ease narrative section. Table of Contents Page 19 of 26 Table of Contents an±ksr ANALYTICAL LAHORAToRY 39 Sprure Street' East Longmeadow, MA 01028 *FAX 413/525-6405 ' TEL 4131525-2332 CERTIFICATIONS Certified Analyses included in this Report Anslyte Certifications EPA 16648 in Water Oil & Grease (HEM) CTMA,NH,NYRl,NC,ME,VA EPA 100.71n Water Copper CT,MA,NH,NY,RI,NC,ME VA Lead CT,MA,NH,NY,RI,NC,ME VA Zinc CT,MA,NH,NY,RI,NC,ME VA EPA 410.4 in Water Chemical Oxygen Demand CTMA,NH,NY RI,NC,ME,VA SM21-221S40D in Water Total Suspended Solids CT MA NH,NY,RJ,NC,ME VA The CON -TEST Environmental Laboratory operates under the fallowing certifications and acereditatioas: Code Description Number Expires ATHA AIHA-LAP, LLC - ISO17025:2005 100033 03/1/2020 MA Massachusetts DEP M-MAI00 06130/2019 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/l/2019 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2019 RI Rhode Island Department of Health LAOOOI12 12130/2018 NC North Carolina Div, of Water Quality 652 12131/2018 NJ New Jersey DEP MA007 NELAP 06/302019 FL Florida Department of Health E871027 NELAP 06/30/2019 VT Vermont Department of Health Lead Laboratory LL015036 07/302019 ME State of Maine 2011028 06/92019 VA Commonwealth of Virginia 460217 12/142018 NH-P New Hampshire Environmental Lab 2557 NELAP 09/62019 VT-DW VumontDeparuntntofHealth Drinking Water VT-255716 06/122019 NC-DW North Carolina Department of Health 25703 07/312019 Page 20 of 26 co Address: 999.v - P Project location: Prajett Number: RaImmarmpr.�7ils r Con -Test QPM NamefNutnber: krvoice Reopten: fo Ka ovg-� ht;Q: (/vemv.eontestlabs_cam Doc N 379 Rev 1-03242017 Phom 413.5232332 CHAIN OF L MODY RECORD (morth Caroffrm) 39 Spruce Street Pete — d r� Pmc d13-+32y4ROS East Langmeadaw, MA M028 [mall: IMl1�t�t1l�ltlabf.l:olrl -Day 10" N of Ca"Wriers tore) te/1Ynte: .� a. .72. c 9: p3 Recelv+ed by: (signature) ED RelangWdaed try: (Swiaturei an co N Received by: (SISmatiue) a N Cn Due Date: Ptesmadorr Cade tR Container Code i iiay t] 3-Day 0 YSl REQUIEM 2•Day •day O ! Field FRtwM 0 Lob to Filter Foen»tt: F7OCdC C lO other: 4V N %' 33T0 me Data » Rewinid; � Reid Filtered ... Emu To: wrAKQ W.t d eM Leh M Fitter %To#: GW Q GRwndNht�r 'th W-t Ows<k►alar to kiraglMner ro-It-a tta-Ir.� A e Air w1� L S ■ SoR ; Ao off • A�-fr-1b SSOL � d . Ni �i A -/fro �o-+r.�r � � o ■ atfier tie ... ooNr': ro-►fdR G /O -ft •1 � !p Nr-re Wild r v �f H • HCL Iffrav Alm.. M - Methanal _rr-ray t ■ -tt M - Nkrtt Add i S - Sutferiie Acid a - Sodium Bisulfato X a 5odfum Hydroxide T - Sodium ihiasulfate 0.Other (please Dtaase use the fotlarang mdes to indicate posstble sample cgncentr #m definc'I within the Cast: Code column above: H - Mjh; M - Madum; L - Low; C - Cleary, U - Unknown = A Program 1 orma on c - Ctm . 2L USCA Q USrfTtutt Fund P - plastic sl-- Sterne GYrPC SWS Landfill 0 REC V -Vial MI. IH55 0"ned Landfill S - Summa Cantder IH9b State Lead T-Tedlar Bag IJ MSCC Other: O . Other (plem define) Project Entity Other r t ❑ liwmmreat ❑ hlun%*alfty ❑ ChtomatoRram ❑ Soxhtot C7 Federal ❑ bmwnfi■ad ❑ AHM-LAP,LLC E) Non Smrhiet ❑ City ❑ SMaol Cr rn 0 n O CD a E N Table of Contents I Have Not Confirmed Sample Container Numbers With Lab Staff Before Relinquishing Over Samples te S � AlVAL.YTIGAIr LABORATORY .. c hit ......................... ............................ -........... Login Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False Statement will be brought to the attention of the Client - State True or False Client (/hi tf $Cra P Received By so Date Time How were the samples In Cooler �T^ No Cooler On Ice 7- No Ice received? Direct from Sampling Ambient Melted Ice Were sam lac wifhin By Gun # Actual Temp - y. & 2_ G p Temperature? 2-6°C '- By Blank # Actual Temp - Was Custody Seal Intact? �4 _ Were Samples Tampered with? r✓/� Was COC Relinquished ? Does Chain Agree With Samples? 7' T Are there brokenfleaking/loose caps on any samples? I: Is COG in ink/ Legible? t- Were samples received wilhin holding time? e_ Did COC include all ien1 # Analysis _ T Sampler Name pertinent Information? Project .r ID's Collection Dates/Times. _ -- Are Sample labels filled out and legible? i Are there Lab to Filters? F Who was notified? Are there Rushes? F Who was notified? Are there Short Holds? Who was noted? is there enough Volume? Is there Headspace where applicable? , MS/MSD? F Proper Media/Containers Used? -_ Is splitting samples required? Were trip blanks received? F On COG? r Do all samples have the proper pH? T-� Acid P 4c?=_ Base 1771 1 Liter Amb. s; 1 Liter Plastic Unp- 16 oz Amb. HCL- 500 mL Amb. 500 mL Plastic 8oz Amb/Clear Meoh- 250 mL Amb, 250 mL Plastic 'I 4oz Amb/Clear Bisulfate- Col./Bacteria Flashpoint 2oz Amb/Clear DI- Other Plastic Other Glass Enure Thiosultate- SOC Kit Plastic Bag Frozen: Sulfuric- Perchlorate Ziplock Un 1 Liter Amb. 1 Liter Plastic 16 oz Amb. HCL- 500 mL Amb. 500 mL Plastic 8oz Amb/Clear Meoh- 250 mL Amb. 250 mL Plastic 4oz Amb/Clear Bisulfate- Col.lBacteria Flashpoint 2oz Amb/Clear DI- Other Plastic Other Glass Encore Thiosulfate-1 I SOC Kit I Plastic Bag Frozen: Sulfuric- Perchlorate Ziplock Comments: Table of Contents 10/16/2018 Track your package or shipment with FedEx Tracking ex-t` TRACK ANOTHER SHIPMENT 773477662078'� Delivered Tuesday 10/16/2018 at 8-45 am DELIVERED Signed for by: B.BECCA GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM Charlajle, NC US TO EAST LONGMEA00"', MA US Travel History Multiple -piece Shipment 1Oil 6/2018 - Tuesday 10,15/201 B - Monday 8:45 am Expand History 1:14 pin OUR COMPANY MORE FROM FEDEX Shipment Facts Ata:t; PdEx rf-deR Ekx3 ftdE%: CongAtil;k 0o Porikhr Cc"j;0jjjc Ifr ;' 1c1IkIA) DeMo1wr lk-,(A]rce CPl w in•rrstcr ReLl.*r-s New":rAyn FedEx Ctms Bordtt "Mc s ContScl Us FOLLOW FEDEx Delivered FAST LONGMEADOW. MA 9. 7 Lj Shipment information sent to FedEX - U) .rn LANGUAGE � M I � i ChangR (:(xmN)' i Y English httpslAvww.farlex.com/appOedextrack/?aclian-track&trackingnumber-773477662078&cntrypode=us&ocate=en_US Page 23 of 26 10I17/2018 Track your package or shipment with FedEx Tracking Table of Contents Est TRACK ANOTHER SHIPMENT 773477662284 Delivered Wednesday 10/17/2018 at 9:03 am DELIVERED Signed for by: B,BECCA GET STATUS UPDATES 013TAIN PROOF OF DELIVERY FROM Charlotte, NC US TO EAST LONGMEADOW, MA US 10117/2018 - Wednesday 9:03 am Delivered EAST LONGMEADOW, MA Expand History \/ 10/15/2018 - Monday 1:14 pm Shipment information sent to FedEx OUR COMPANY About FedEx Our Portfolio Investor Relations Careers FedEx Blog 1� O U) 7z, -1 0 tL M X httpsJlwww.fedex.comlappslfedextrackRaction=track&tracknumbers773477662284&tocafe=en US&cntry_code=us Page 24 of 26 contest" Phone:413-525-2332 ^U AVMµ uoaR.rowr Fax: 413^525•G445 Email: infooicontestlabs.com Address: Phone: 70 Project Location:r Project Number: Project Manager: Con -Test quote Name/Number; Invoice Recipient: C*. Sampled By: . i„ )" • http://www.contestlabs.com Doc m 379 Rev 1_03242017 CHAIN of CUSTODY RECORD (North Carolina) 39 spruce street East Longmeadow, MA 01028 7-Day ❑ 10-Day [] Due Date: f� -MIS „, P +7 1-Day [] 3-Day ❑ ANALYSIS REOUIENTED 2-Day ❑ 4-Day ❑ 111NMR1,11111121, Format: PDF EXCEL F;" Other: CLP Like Data Pkg Required: Li Fax To 1: ro ir-r8 10-0 r (v. ,QA !a: (A.) fig Page _ of IF of Containers Preservation Code Container Code ::s �. Comments; Please usea the following codes to indicate possible sample concentration c^� wlthln the Conc Code column above: H - High; M - Medium; L - Low: C - Clean: U - Unknown Relinquished nattrr Date/Time:; I,�: e� + 4 $ CJI�F111r1 Inunnatimli r 2L DSCA ❑ UST/Trust Fund SWS Landfill ❑ REG Rc .ived : { ' Ili it.ure) Date/Time: GWPC 114SB Orphaned Landfill State Lead '..si,Sumfri SWSL Re i qul d b : (signature) I Date/Time: 1HSB t.rV#1,rJg, Other; MSCC ;' ;;r;• Ri 'p Id by: (signature) t Date/Time: L�l 1 ° ti ro ,:: C) fished by: (signature) Date/Time: Rr N Project Entity Other PC8 ONLY n p❑ Government ❑ MuniClpality ❑ Chromatogram ❑ Soxhlet ❑ Federal ❑ Brownfield ❑ A1HA-LAP,LLC ❑ Non Soxhlet C_ .d by: (signature) Date/Time: n Citv n School w Table of Contents I Have Not: Confirmed Sample Container Numbers With Lab Staff Before Relinquishing sar�s+�rncAt �aB�r�a�a��r Over Samples lay.............................................................. ................... Login Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False Statement will be brought to the attention of the Client - State True or False Client --un Received By Date Time How were the samples In Cooler No Cooler On Ice T No Ice received? Direct from Sampling Ambient Melted Ice B G A lT Were samples within y un # ctua emp Temperature? 2-6'C By Blank # Actual Temp - _E Was Custody Seal Intact? �I� _ Were Samples Tampered with? Was COC Relinquished ? T Does Chain Agree With Samples? 7 Are there broken/leaking/loose caps on any samples? F Is COC in ink/ Legible? - Were samples received within holding time? Did COC include all Client Analysis^ Sampler Name "r pertinent Information? Project r ID's t Collection Dates/Times Are Sample labels filled out and legible? Are there Lab to Filters? Who was noted? Are there Rushes? — Who was notified? Are there Short Holds? _ Who was noted? Is there enough Volume? Is there Headspace where applicable? MSIMSD?��� r_ Proper Media/Containers Used? -1— Is splitting samples required? r� Were trip blanks received? On COC? Do all samples have the proper pH? Acid /- L Base Unp- 1 Liter Amb. 1 Liter Plastic 16 oz Amb. HCL- 500 mL Amb. 500 mL Plastic Boz Amb/Clear Meoh- 250 mL Amb. 250 mL Plastic 4oz Amb/Clear Bisulfate- CoIJBacteria Flash pint 2oz Amb/Clear Dl- Other Plastic Other Glass Encore Thiosulfate- SOC Kit Plastic Baa Frozen: Un - 1 Liter Amb. 1 Liter Plastic 16 oz Amb. HCL- 500 mL Amb. 500 mL Plastic Boz Amb/Clear Meoh- 250 mL Amb. 250 mL Plastic 4oz Amb/Clear Bisulfate- Col.Bacterla Flash pint 2oz Amb/Clear DI- Other Plastic Other Glass Encore Thiosulfate4 SOC Kit Plastic Baa Frozen: 6.1.e„k U(\S Qr")A, led �`�S4,n� Ginac r,s 26 of 26 ff rD-- - 4"'0 i "1 I Qi The Goodyear Tire & Rubber Company — Statesville Mold Plant 108 Business Park Drive Statesville, NC 28677 January 18, 2018 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Storm Water DMR, General Permit NCG030000, COG NCG030513 Dear Mr. or Ms., The Goodyear Tire & Rubber Company — Statesville Mold Plant is covered under North Carolina General Storm Water Permit NCG030000. The permit requires submission of a discharge monitoring report within 30-days of receiving analytical results. No events occurred during the months of July through December, so no sample was collected from outfall #1. If further information is required please do not hesitate to contact me at 704-928-4508. Sincerely, Carlton Williams, L.J Regional Environmental Manager JAN2 2018 The Goodyear Tire & Rubber Company .,_,vTRk 1 WR SECToNS Certified Mail No. 7014 2120 0000 7370 5795 Return Receipt Requested Attachment cc: file Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted Januarx 18, 2018 CERTIFICATE OF COVERAGE No. NCG030513 FACILITY NAME The Goodvear Tire & Rubber Comoan COUNTY Iredell PERSON COLLECTING SAMPLES Emily Roy LABORATORY Pace Analytical Lab Cert. # 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW 7-Trout ❑PNA ❑Zero -flaw [:]watersupply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR-3 4 ® No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics' Benchmarks ===> - - 100 mg/L or 50 mg/L" 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 No discharge ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor :manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe We2milier Name (Print name) Manufacturing Director �Titl (Print ntit) �. (Signature) ( Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX m L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier .1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period? Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART li SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an on final and one copy of this DMR including all "No Discharge"' reports, within 30 days of receipt of the lab results or at end of monitoring eriod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) L , ZG a; (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 The Goodyear Tire & Rubber Company — Statesville Mold Plant 108 Business Park Drive Statesville, NC 28677 July 26, 2017 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Storm Water DMR, General Permit NCG030000, COG NCG030513 Dear Mr. or Ms., REC-Iva) AUG 08 2017 CENTRAL FILES D1NR SECTION The Goodyear Tire & Rubber Company — Statesville Mold Plant is covered under North Carolina General Stonn Water Permit NCG030000. The permit requires submission of a discharge monitoring report within 30-days of receiving analytical results. No events occurred during the months of January through June, so no sample was collected from outfall 41. If further information is required please do not hesitate to contact me at 704-928-4508. Sincerely, Em�-Q� e-�C-'-- Emily.Roy, Safety, Training and Environmental Manager The Goodyear Tire & Rubber Company Certified Mail No. 7014 2120 0000 7370 5788 Return Receipt Requested Attachment cc. file Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted July 26, 2017 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Company COUNTY Iredell PERSON COLLECTING SAMPLES Emily Roy LABORATORY Pace Analytical_ Lab Cert. t# 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthly'_ (month) DISCHARGING TO CLASS ❑ORW ❑HQW�❑Trout ❑PNA ❑Zero -flow [:]Watersupply [:]SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ® No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ===> - - 100 mg/L or 50 mg/O 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 No discharge 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ' See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring Tay be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General hrmit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." ,foe Weemiller Name (Print name) _Manufacturing Director Title (Print title) Joe, W -I I'L-1 � 0 (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me1L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 2 of 3 - Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. 4 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B, • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an on final and one copy of this DMR including all "No Discharge" reports within 30 days of receipt of the lab results or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: 1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." J6110- GJecl (Signature of 1 n (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted January 24, 2017 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Comoan COUNTY Iredell PERSON COLLECTING SAMPLES Emily Roy LABORATORY_ Pace Analytical Lab Cert. #i 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' (month) DARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA �yGC�� ❑Zero -flow ❑Water Supply []SA 3AN 21 �D17 ❑other CD�� CT ON PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ® No discharge this period?' Outfali No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ===> - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L O.QfW V,67 mg/L 15 mg/L 1 mg/L 001 No discharge 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. ' For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe Weamiiler Name (Print name) Manufacturing Director Title (Print title) JQJA4�� (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. (Vote: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period ?2 Outf all No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. + TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all Discharge" reports, within 30 days o receipt of the lab results !or at end of monitoring period in the case of "No Discharge" reports to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date:11/1/2012-10/31/2017 I A4 12or7 (date) SWU-245, last revised 10/25/2012 Page 3 of 3 vo(z) D"qq r'affc�gM The Goodyear Tire & Rubber Company — Statesville Mold Plant 108 Business Park Drive Statesville, NC 28677 July 26, 2016 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE6 lVED AUG 02 2016 CENTRAL FILES ©V�1R SECTION RE: Storm Water DMR, General Permit NCG030000, COG NCG030513 To whom it may concern: The Goodyear Tire & Rubber Company — Statesville Mold Plant is covered under North Carolina General Storm Water Permit NCG030000. The permit requires submission of a discharge monitoring report within 30-days of receiving analytical results. No events occurred during the months of January through June, so no sample was collected from outfall 41. If further information is required please do not hesitate to contact me at 704-928-4508. Sincerely, &j--) ?I Emily Roy Safety, Training & Environmental Manager The Goodyear Tire & Rubber Company Certified Mail No. 7014 2120 0000 7370 5764 Return Receipt Requested Attachment cc: file Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted July 26, 2016 CERTIFICATE OF COVERAGE No. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Comoan COUNTY Iredell PERSON COLLECTING SAMPLES Emily Roy LABORATORY Pace Analytical Lab Cert. # 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ❑ Monthly' (month) REC �, 9�S�ARGING TO CLASS ❑ORW ❑HQW [—]Trout❑PNA j/ ❑Zero -flow ❑Water Supply ❑SA AUG 02 2016 ❑other CENTRAL FILETS PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 � DWR SECTION ® No discharge this period?2 Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids P , H Standard units Copper Lead Zinc Non-Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics-' Benchmarks ===> _ - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L i mg/L 001 No discharge 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), i certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Jae Wepmiller Name (Print name) Manufacturing Director Title (Print ti e) _j �7 Z� zo E, (Signature) (Da e) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/2S/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results !or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Joe,VV�.Ct/V�vl •� (Signature of Permitte Permit Date: 11/1/2012-10/31/2017 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report r / for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted _January 21, 2016 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodvear Tire & Rubber Comoan COUNTY Iredell PERSON COLLECTING SAMPLES Emily Roy LABORATORY Pace Analytical Lab Cert. # 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ® July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ® No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead - Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organicss Benchmarks==> - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001 No discharge 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Storm water Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." .toe Weemiller Name (Print name) Manufacturing Director Title (Print title) .Jae. (� c z-7 AZO r� (Signature) (Da(e) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, the)tmust be reported in the format, "<XX mg L where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar 0&G/TPH by EPA 1664 (5GT-HEM) Total suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11j1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 .0 Note: if y'ru report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one cogy of this DMR including all "'No Discharge"' reports, within 30 days of receipt of the lab results or at end of monitoring eriod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." {Signature of perm lz-7100t so (Kate) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual St_ormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted January 21, 2016 CERTIFICATE OF COVERAGE No. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Compan COUNTY Iredell PERSON COLLECTING SAMPLES Emily Roy LABORATORY Pace Analytical Lab Cert. # 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' December_ _ (month] DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other RECEIVED FEB 01 2016 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL FILES DWR SECTION ® No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids , P H Standard units Copper Lead Zinc Non-Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 002 No discharge 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. for those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe WeQmiller _ Name (Print name) Manufacturing Director Title (Print title) Jam. �j I c z, zo/6 (Signature) (Dat ) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format,_"<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier I, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. pate Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit bate: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. .-I, FOR PART'A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an orialnol and one copy of this DMR, including all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitorina Period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Jam. (Signature of l A(Q ! ( ate) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted Aril 9 2015 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Company COUNTY Iredell PERSON COLLECTING SAMPLES Kristin Flora LABORATORY_ Pace Analytical Lab Cert. # _40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results r : SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' March month DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks ==_> - - 100 mg/L or 50 mg/O 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 002 03/27/2015 0.20 0.0059 mg/I 0.0201 mg/I ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for 70 monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General' Permit. For those facilities electing to employ the 70 monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe We miller Name (Print name) Manufacturing_Director Title (Print title) j� aa��, I 4 R za15 (Signature) ( ate) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, theymust be reported in the format "<XX m L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =_-> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copes of this DMlt including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to. Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Q Za /5 (Date Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 c�oor�,rr�gc� The Goodyear Tire & Rubber Company — Statesville Mold Plant 108 Business Park Drive Statesville, NC 28677 April 9, 2015 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Storm Water DMR, General Permit NCG030000, COG NCG030513 Dear Mr. or Ms, •TFcie/ APR I 2015 DW F��ES C77KN The Goodyear Tire & Rubber Company — Statesville Plant (Goodyear) is covered under North Carolina General Storm Water Permit NCG030000. The permit requires submission of a discharge monitoring report 30-days of receiving analytical results. Please find enclosed a DMR for a sample collected on March 27, 2015. A sample was collected from outfall #2. If further information is required please do not hesitate to contact me at 704-928-4504. Sincerely, Kristin Flora Manager, Human Resources The Goodyear Tire & Rubber Company Certified Mail No. 7012 3050 0001 8620 6937 Return Receipt Requested Attachment cc: file aceARalytical w+wrpaeeFascsom f d - March 31, 2015 Mr. Scott Stevens Goodyear 108 Business Park Drive Statesville, NC 28677 RE: Project: Outfail Pace Project No.: 92243116 Dear Mr. Stevens: Pace Analytical Services, Inc. 98DO KinceyArne. Suite 1Do HuntersviUe, Nc 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on March 27, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen chdstophenderouen@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 9 e ace 14nali cal i Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project Outtall Pace Project No.: 92243116 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 FioridalNELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 Vrginia(VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 9 Pace Analytical Services, Inc. acM alytifcal 9800 Kincey Ave. Suite 100 Huntersville, NC 2B078 www-p�oam I (704)87"092 SAMPLE ANALYTE COUNT Project Outfall Pace Project No_: 92243116 Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92243116001 OUTFALL #2 EPA 200.7 JMW 2 PASI-A 92243116002 RAINWATER EPA200.7 JMW 2 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 9 Pace Analytical Services, Inc. �j1/++�gj��gj /+� l 9800 Kinsey Ave. Suite 100 LiVI+/V (C[l��c Huntersville, NC 28078 r wwwp com I (704)875-9092 ANALYTICAL RESULTS Project Outfall Pace Project No.: 92243116 Sample: OUTFALL #2 Lab ID: 92243116001 Collected: 03/27/15 09:50 Received: 03/27/15 16:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 5.9 ug1L 5.0 1 03/30/15 12:40 03/31/15 00:44 7440-50-8 Zinc 20.1 ug1L 10.0 1 03/30/15 12:40 03/31/15 00:44 744M" Sample: RAINWATER Lab ID: 92243116002 Collected: 03/27/15 09:50 Received: 03/27/15 16:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND ug1L 5.0 1 03/30/15 12:40 03/31/15 00:47 7440-50-8 Zinc 10.3 ug/L 10.0 1 03/30/15 12:40 03/31/15 00:47 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 03/31/2015 04:54 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 9 ;5ceAnalyfical" W&W4*Cekb&cQm Project: Outfall Pace Project No.: 92243116 QC Batch: MPRP/18170 QC Batch Method: EPA 200.7 Associated Lab Samples: 92243116001, 92243116002 METHOD BLANK: 1422322 Associated Lab Samples: 92243116001, 92243116002 Parameter Units Copper ug/L Zinc ug/L QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5A 03/30/15 23:29 ND 10.0 03/30/15 23:29 Pate Analytical Services, Inc. 9B00 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1422323 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper ug/L 500 481 96 85-115 Zinc ug/L 500 468 94 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1422324 1422325 MS MSD 92243074002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 9.2 500 500 486 491 95 96 70-130 1 Zinc ug(L 41.0 500 500 492 492 90 90 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1422326 1422327 MS MSD 92242915001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 0.028 500 500 529 540 100 102 71-130 2 mg1L Zinc ug/L 0.10 500 500 569 579 94 96 70-130 2 mg/L Results presented on this page are in the units Indicated by tile 'Units' column exceptwhere an altemate unit Is presented to the right of the resutt. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 03/31/2015 04:54 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 _ aceAnaly6cal w+vxcpace�hs.cnm 1 - t QUALIFIERS Project: . outfall Pace Project No.: 92243116 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quandtation Limit RL - Reporting Limit. Pace Analytical Services, Inc. 98M Kincey Ave. Suite 100 Huntesville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/31/2015 04:54 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 9 9 aceAnalytkal wirw4XWeiabs.ra0rrr f, t QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Outfall Pace Project No.: 92243116 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite100 Huntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical !Method Batch 92243116001 OUTFALL #2 EPA 200.7 MPRP/18170 EPA 200.7 ICP/16325 92243116002 RAINWATER EPA 200.7 MPRP/18170 EPA 200.7 ICP/16325 Date: 03/31/2015 04:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 9 •�P�ceAnalytical' CHAIN -OF -CUSTODY / Analytical Request Document The Chaln-of•Custady is a LEGAL DOCUMENT. Al relevant fields must be completed accurately. Pape: of rn d Section A Section B Section C 4 8 Required Client Information: Required "act information; Invoice Infonnatlon: Company: Report To: Attention: Address: s5 n j` f,inpAddress: r. Copy To: Company REGULATORY AGENCY T" NPDES r GROUNDWATER i LIST— RCRA r DRINKING WATER (— OTHER I T y Purchase Order No.: Pan �� Pate rXVI Z 2 Pho e, ProjNama: Paco Project Site Lowtion r >Ltect anaaer. STATE. NC.J Requested Due DetofTAT: Project Number. Paee Pronle M: /� V Requested Analysis Filtered [YM) Section D Matrix Cottas r Z Required Cltont Information !x.ccssg s COLLECTED Preservatives > Ir Drinking Water DIN U Water Waste Water WT WW 3 rj m START ENMRA6 w Z Product P 4 • q0. �• SoiVSolid SL 0 0 InN SAMPLE ID Oil �? e w m c {A-Z, 0-81 r) pa Air YOL AR w0 w 0. Z Sample 10s MUST BE UNIQUE Tissue TS O Z Otherci Orr x w w 0 c �+ LU LL 0 z OATS TIME t1ATG TIME # z O „ay Pace Project No.! Lab I.D. 1 �2 7t 2 2 (Cb 2 N L 3 a 5 8 7 S 4 1 t) 11 12 ADOTTIONALCOMMENTS RELINQUISHED BYIAFRUATION DATE TIME ACCEPTED BYlAFFILIATION DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE ORIGINAL & c PRINT Nome of SAMPLER: SIGNATURE of SAMPL 3 2 ~ rr n m {MM1DDg1YY)tl / •Importam Note: By dgmhg this iorm you are accepting Pace's NET 30 Cay payment tens and agreeing to late charges 01.5% Per month ter arty Wjoices not paid vrilhin 30 days. l � F-ALL-0-020rev.07, 15-May-2007 i ' _ CBft1J8%IfG�I� Document Name: I Document Revised: September 1.L. ZU14 iditinn i.innn Rar_aint fS[_I IRi Paae 1 of 2 1 Pace office Client Name; (,.,6Rd Y-m r Courier: ❑ Fed lac ❑ UPS❑ LISPS❑ Cuent❑ CommerclaE❑ Pa Other Custody Seal on Cooler/Box Present: ❑ yes V no Seals Intact: ❑ yes no Packing Material: ❑ Bubble 1l[)p ❑ Bubble Bags ❑ None Other Thermometer Used: IR Guts T14 Type of ice: t Blue None (Samples on Ice, cooling process has begun Temn Correction Factor T1401 No Correction Corrected Cooler Temp.:-C Biological Tissue Is Frozen: Yes No irA� Dace and f s o ing contents Temp should be above freezing to 6'G Comments: � Chain of Custody Present Yes ONO ❑WA 1. Chain of Custody Filled Out: Yes ONO ❑N/A 2. Chain of Custody Relin uished: W-a [IN, ❑NIA 3. Sampler Name & S' nature on COC: OfYes ❑No ❑WA 4. Samples Arrived within Hold Time: i$(Yes [IV, ❑NIA 5. Short Hold Time Analysis <72hr : Oyes do. ❑tuA B. Rush Turn Around Time Requested: ❑Yes @6 ❑NIA 7. Sufficient Volume: DYes dKI ❑NIA 8. € !�I ell Correct Containers Used: llllYes ON, ❑NIA 9. gym -Pace Containers Used: ONO ❑NIA Containers Intact: Yes ONO DIVA 10. Filtered volume received for Dissolved tests ❑Yes ❑No 1A 11. Sample Labels match COC: Dreg ONO ❑NIA 12. -Includes dateliimelll /Ana! sis Matrix: All containers needing preservation have been checked. VYes ONO ❑NIA 13. All containers needing preservation are found to be in des ONO ❑NIA compliance with EPA recommendation. exceptrorm VOA, coIIrorm, TOC, O&G, W!-DRO &atao �( Dyes ;[1No Samples checked for dechlorination: ❑Yes ONO 14. Heads ace in VOA Vials >6mm : Dyes ONO 016 15. Trip Blank Present: Dyes ONO ?VA 16. Trip Blank Custody Seals Present ❑Yes ONO d/WA ,Pace Trip Blank Lot # i€purchased) Client Notification/ Resolution: Field Data Required? Y / N Person Contacted: DateMme: Comments/ Resolution: SCURF Review: Date: `3rZ �� W0# . 92Z43116 SRF Review: Date: Dote: Whenever there is a discrepancy affeding North Caroina compliance I I samples, a copy of this form YAP be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, Incorrect preservative, out of temp, 92243116 Incorrect containers) I Page 9 of 9 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted: 03/03/2015 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Company_ COUNTY Iredell PERSON COLLECTING SAMPLES N/A LABORATORY N/A Lab Cert. # _N/A Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results w SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' February lmt,4TI DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA =.. ❑Zero -flow ❑Water Supply ❑SA V' []Other v9pv PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -9 ® No discharge this period?' + Outfail No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total. Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks ===> _ - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0,03 mg/L 0.067 mg/L 15 mg/L i mg/L 01 No Flow 02 No Flow 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfali. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General.. Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons'directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe Weemiller Name (Print name) Manufacturing Director Title (Print title) 3 3 2oLS (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/IL", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ==_> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Not Applicable Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: If you report a sample value in excess of the benchmark, you must Implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PARTS MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO If YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copv of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (SignatureLbf Permittee) Permit Date: 11/1/2012-10/31/2017 3 3 !o .� (Date] SWU-245, last revised 10/25/2012 Page 3 of 3 ( rBa, 7a 2A L- -Ip2 99) Dflq The Goodyear Tire & Rubber Company — Statesville Mold Plant 108 Business Park Drive R EC E i E D Statesville, NC 28677 I MAR 0 5 2015 March 03, 2015 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 CENTRAL FILES DWR SECTION RE: Storm Water DMR, General Permit NCG030000, COG NCG030513 Dear Sir or Ms. The Goodyear Tire & Rubber Co. — Statesville Plant (Goodyear) is covered under North Carolina General Storm Water Permit NCG030000. The permit requires submission of a discharge monitoring report within 30 days of receiving analytical results. Please find enclosed a DMR for a monthly sample from February 2015. No samples were collected due to no qualifying rain events during the month and it was too slippery to get a sample during the snow/ice showers. If further information is required please do not hesitate to contact us. Sincerely, S-U4 s4uq� - Scott Stevens EHS Manager The Goodyear Tire & Rubber Co. Certified Mail No. 7011 1570 0003 5901 9056 Return Receipt Requested Attachment cc: file Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted: 02/09/15 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Company COUNTY Iredell PERSON COLLECTING SAMPLES Kristin Flora LABORATORY Pace Analytical Lab Cert. # 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE: PERIOD ® Jan -June ❑ July -Dec or ® Monthly' May month DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA []Zero -flow ❑Water Supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics' Benchmarks =__> _ - 100 mg/L or 50 mg/L" 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 01 No Flow 02 05/29/15 0.25 ND 7.4 0.011 mg/L ND 0.024 mg/L ND NA ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. ' Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe We miller Name (Print name) Manufacturing Director Title (Print title) 7 7 Lo/� (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX ma/IL", where XX is the numerical value of the detection limit, reporting limit, etc. In mg/L. Note: If you report a sample value In excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-245, fast revised 10/25/2012 Page 2 of 3 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. pate Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches' Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Not Applicable Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note, if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mall an orialnal and one coon of this DMR, includina all "No Discharge" reoorts. within 30 days of recelat of the lab results for at end of monitorina period in the case of "No Discharge" reports] to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ,21e_ (Signature of Permit Date: 11/1/2012-10/31/2017 7 z zv fs ( Date ) SWU-245, last revised 10/25/2012 Page 3 of 3 Z000gzU cL) The Goodyear Tire & Rubber Company — Statesville Mold Plant 108 Business Park Drive Statesville, NC 28677 July 7, 2015 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Storm Water DMR, General Permit NCG030000, COG NCG030513 Dear Sir or Ms. RleCiEl VED JUL 13 2015 CENTRAL F►L DWR SECTION The Goodyear Tire & Rubber Co. — Statesville Plant (Goodyear) is covered under North Carolina General Storm Water Permit NCG030000 Please find enclosed a DMR for a monthly sample from May 2015. If further information is required please do not hesitate to contact us. Sinc rely, Kristin Flora Manager, Human Resources The Goodyear Tire & Rubber Co. Certified Mail No. 7011 1570 0003 5901 9087 Return Receipt Requested Attachment cc: file CeAnaIXical' M9vrp9P�iLam June 16, 2015 Mrs. Kristin Flora Goodyear 108 Business Park Drive Statesville, NC 28677 RE: Project: THE GOODYEAR PROJECT SAMPLING Pace Project No.: 92252113 Dear Mrs. Flora: Pace Analytical Services, Inc. 98W IGnoey Ave. Suite 100 Hunters Ue, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on May 29, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the mitten conserd of Pace Analytical Services, Inc.. Page 1 of 11 aceAnalytical o www.paoeiabs.00m f CERTIFICATIONS Project: THE GOODYEAR PROJECT SAMPLING Pace Project No.: 92252113 Pace Analyttcal Services, hrc. 9a00 iGnosy Ave. Suite t t10 Huntersvilie, NC 2807a (704)975-9092 Charlotte Certification We 9800 Kincey Ave_ Ste 100, Huntersvitle, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VrginialVELAP Certification #: 460221 South Carolina Certification #: 99006W1 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 FloridafNELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NCO30 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginialVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fun, without the wftm consent of Pace Analytical Services, Ina. Page 2 of 11 (�Ik'ceAfflljdicale wwwpacehftcom SAMPLE ANALYTE COUNT Project THE GOODYEAR PROJECT SAMPLING Pace Project No_: 92252113 Pace Analytical Services, Inc_ 9800 Kincey Aye. Suite 1oo Huntersville, NC 28078 (704)876-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92252113001 OUTFALL 02 05-29-2015 PH 7.4 EPA 1664E CLW 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuo, wfthoul the written consent of Pace Analytical Services, Inc., Page 3 of 11 C1l'i8/'1(&lI�1C�l s www.pacekb&wM ANALYTICAL RESULTS Project: THE GOODYEAR PROJECT SAMPLING Pace Project No.: 92252113 Pace Analytical Services, Inc. 9800 ruro ey Ave. Suite 100 Huntafsville, NC 28078 (704)875-9092 Sample: OUTFALL #2 05-29-2015 Lab ID: 92262113001 Collected: 05/29/15 10:45 Received: 05129115 16:00 Matrix: Water PH 7.4 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 06/05/15 09:27 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 0.011 mg/L 0,0050 1 06102J1517:30 0610311516:40 7440-50-8 Lead ND mg/L 0.0050 1 06M2/1517:30 D6/03/1516:40 7439-92-1 Zinc 0.024 mg/L 0.010 1 06MV1517:30 06/03/1516:40 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids ND mg/L 11.4 1 06/05/15 19:29 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in W, Date: 06/16/2015 05:11 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 Pace Analyrical Services, Inc. ® 9800 Kncey Ave. Suite 100 aceMalXical Huntmville, NC 28078 w w"' •cam (704)875-9092 QUALITY CONTROL DATA Projed: THE GOODYEAR PROJECT SAMPLING Pace Project No.: 92252113 QC Batch: GCSV/21557 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92252113001 METHOD BLANK: 1476492 Matrix: Water Associated Lab Samples: 92252113001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 06/05J15 09:20 LABORATORY CONTROL SAMPLE: 1476493 Spike LCS LCS % Rec Parameter Units Conn Result % Rec Limits Qualifiers Oil and Grease mg/L 40 38.5 96 78-114 MATRIX SPIKE SAMPLE: 1476494 35190941002 Spike MS MS % Rec Parameter Units Result Conc_ Result % Rec Limits Qualifiers Oil and Grease mg/L 4AJ 40 42A 95 78-114 ResuRs presented on this page are in the unft Indkated by the'UnW column except Where an attemate unit It presetrted to the ripM of the msutL REPORT OF LABORATORY ANALYSIS This repot shall not be reproduced, except in full. Date: 06/16/2015 05:11 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 aceAnalytical. www.pacelebs.cnm QUALITY CONTROL DATA Project: THE GOODYEAR PROJECT SAMPLING Pace Project No.: 92252113 QC Batch: MPRP/18589 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92252113001 METHOD BLANK: 1473002 Matibc Water Associated Lab Samples: 92252113001 Blank Reporting Parameter Units Result Limit Analyzed Copper mg/L ND 0.0050 06103/1515:51 Lead mgfL ND 0.0050 06103/1515:51 Zinc mg1L ND 0.010 0610311515:51 Qualifiers Pace Analytical Services, Inc. 98M Korey Ave. Suite 100 Hurtler>ville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1473003 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L .5 0.47 94 85-115 Lead mg1L _5 0.47 93 85-115 Zinc mg/L .5 0.47 94 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1473004 1473005 MS MSD 92252168001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 784 _5 .5 1.3 1.3 96 100 70-130 2 Lead m91L ND .5 .5 0.46 0.48 92 96 70-130 4 Zinc mg/L 60.6 .5 .5 0.53 0.55 94 97 70-130 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1473006 1473007 MS MSD 92252136001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cane. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L ND .5 .5 0.50 0.47 100 94 70-130 7 Lead mg/L ND _5 .5 0.49 0.46 98 92 70-130 6 Zinc m91L ND _5 .5 0.49 0.47 97 92 70-130 5 Results preserved on this page are In the units Indicated by the'UnitV column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in ful, Date: 06/16/2015 05:11 PM wittwut the written conserrt of Pace Analytical Services, Inc.. Page 6 of 11 e acmnalytical www.pacelabscom QUALITY CONTROL DATA Project: THE GOODYEAR PROJECT SAMPLING Pace Project No.: 92252113 QC Batch: WET/37927 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92252113001 METHOD BLANK: 1477475 Associated Lab Samples: 92252113001 Parameter Units Total Suspended Solids m9fL LABORATORY CONTROL SAMPLE: 1477476 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1477477 Parameter Total Suspended Solids SAMPLE DUPLICATE: 1477478 Parameter Total Suspended Solids Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huribmsville, NC 28078 (704)8759092 Matrix: Water Blank Reporting ResuS limit Analyzed Qualifiers ND 2.5 0610511519:21 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 250 252 101 90-110 92252715001 Dup Units Result Result RPD Qualifiers mg/L 308 306 1 92252078003 Dup Units Result Result RPD Qualifiers mg/L ND ND Results presented on this page are in the units Indicated by the "Unas' cow= a:cape Where an aten ate unit is presented to the right of the insult REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/16/2015 05:11 PM without the written consent of Pace Analytical Services, Inc.. page 7 of 11 acmnaVical WW..parebtL$LCom QUALIFIERS Project: THE GOODYtAR PROJECT SAMPLING Pace Project No.: 92252113 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot_ ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. POL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical services, inc. 98M IGnoeyAve. Suite too Huntersvine, NC 28078 (704)875.9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anatyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodipherrylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each anatyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shad not be reproduced, except in fun, Date: 06/162015 05:11 PM wMW the wntWn consent of Pace Anahtical Services, Inc . Page 8 of 11 r7C8AT1alyfiC,al w w.P8C si3b&C0M QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: THE GOODYEAR PROJECT SAMPLING Pace Project No.: 92252113 Pace Anatyfical SemIces, htc. 9800 Kinney Ave. Suite.100 Huntersvilfe, NC 28078 (704)8759092 Analytical Lab 1D Sample ID QC Batch Method QC Batch Analytical Method Batch 92252113001 OUTFALL #2 05-29-2015 PH 7.4 EPA 1664E GCSV/21557 92252113001 OUTFALL #2 05-29-2015 PH 7.4 EPA 200.7 MPRPl18589 EPA 200.7 ICP/16677 92252113001 OUTFALL #2 05-29-2015 PH 7.4 SM 2540D WET/37927 Date: 06/1612015 05:11 PM REPORT OF LABORATORY ANALYSIS This report shaft not be reproduced, except in full, without the w n ten consent of Pace Analytical Services, Inc.. Page 9 of 11 aceAnalj cal " www,pacwahs.com Section A Required Client Information: CHAIN -OF -CUSTODY ! Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section B Section C Required Proiect Information: Invni— Infonnation- 0 Q e- Paga: of m Company.t I —r e Rap1o� To: _p .� Attention, 181 r 8 U J Y r;: iG1 i I ►'J r: t t. i^ i ddross �/l Copy To: Company Name: REGULATORY AGENCY i V 1, K; 9- Tl bf f Address: `- NPD£S F- GROUNDWATER 1 - DRINKING WATER r UST RCRA OTHER E A,To: „ i 1 \r! Iri.— • C� rv-� !: i ✓. Purchase Order No.: Z Paw Quota Rofaronw: ane: Fax 1 J r ' 5 _ "r � fLFJ''/ i� r Project Name: Qars arojoct Managdr. Site Location STATE;` Requested Duo DateffAT: Project Number: Pace Profile p: 1 (1TV, ` RdP sted Analysis Filtered (YfN) Section D Matrix Codes Required Client information MATRIX f Ct]OE s' 3 's COLLECTED Preservatives '> Drinking Water DW 0U $ - Water Nrf Waste Water ww Product P $ U upCOMPOSITE START coswPosmTe EN01GRAe o soll/sotld SL �� y SAMPLE ID oil OL w m r (A-Z, 0-9 f:} Air AR Sample IDs MUST BE UNIQUE Tissue TS w 6 d ¢ z Z m t o V i 7k Qatar aT X W .r w O UU. a) v o N a a R + V m � z w 4 c�z M C n �� 1= DATE TIME HATE TIME N = 3 z Z O a a) a Pace Project No./ Lab I.D. I 2 r7,44 r 3 4 5 6 7 a 9 10 11 12 gT11E ADDITIONAL COMMFNTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY f AFFILIATION DATE SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE ORIGINAL m m ! PRINT Name of SAMPLER; .r' J.�; �'n Jam( ,� � .a �2 L) ti SIGNATURE of SAMPLE=11�'� f " ''..� ^ DATE Signed / _ �� a m Y U m E (MMIDD/YY): �' �Il,� N to riw� "— "r -w—w — —rw — —piing racas Ive i w aay paymom term$ IN agreeing to late charges of 1.5"% par month for any invoices not paid Minn 30 days. ` F-ALL-0-020rev.07, 15-May-2007 sample Condition Upon Receipt (SCUR Page 1 of 2` (/ Document Number: Issuing Authority: F-CHR-CS-003-rev.16 Pace Huntersville Quali Office Client name._ IJUG_fl yt?u l S 41i�A It 5o i �p • Page 2 of 2 is for Internal Use Only Courier. ❑ Fed Ex ❑ UPS❑ USPE❑ Client[] mercial❑ ace here Custody Seal on Cooierll3ox Present: El yes no Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble VDp ❑ Bubble Bags ❑ None ❑ Other thermometer Used: IR Gun 4 type of lce: Wet Blue None Samples on ice, cooling process has begun remp Correction Factor T1 01 No Correction 9 Date and Initials offpe on Intng : orrected Cooler Terrip.: of - •C Biological Tissue Is Frozen: Yes No QUA contents: l� � remp should be above freezing to VC Comments: ,hWn'of'Custod Present:" es gAKElNIA 1. ;hain of Custody Filled Out: ❑ es o ❑NIA 2. 'hain of Custody Relinquished: Yes PLO-11-0 WA 3. Sampler Name & Signature on COC: es DIVA 4. Samples Arrived within Hold Time: es - ON, A 5. ihort Hold Time Analysis (<72hr): OYes - o A 6. lush Turn Around Time Requested: ❑Yes o IA 7. Sufficient Volume: ❑Yes ❑NIA 8. p3 H ,orrect Containers Used: -Pace Containers Used: Na Yes No ❑NrA ❑NIA g, .ontainers Intact: es ❑No ❑WA =iltered volume received for Dissolved tests Dyes o A r. Sample Labels match COG: -Includes date/time/ID/Analysis Matrix: es ❑No ❑NIA 12, UI containers needing preservation have been checked. MI containers needing preservation are found to be In xmVIlance with EPA recommendation. wceprmns: VOA, coliform, TOC, O&G, Wl-DRO (water) ONO ❑NIA Z ❑No A Illy, o 13. Samples checked for dechlorination: ❑Yes ❑No DWA 44, jeads ace in VOA Vials >6mm : ❑Yes 20No NIA rrip Blank Present: rrip Blank Custody Seals Present ❑Yes ON, ❑Yes ❑No rA ❑ A . 'ace Tri -Blank-Lot #Jif urchased :--- '.11ent Notification/ Resolution: Field Data Required? Y I N Person Contacted: Date/Time: Comments/ Resolution: SCURF Review.1 MNY IlDate: SRF Review: Bate: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e out of hold, incorrect preservative, out of temp, Incorrect containers) 140g:92252113 uimiHp�i�anm Page 11 of 11 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted: 02/09/15 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Company COUNTY Iredell PERSON COLLECTING SAMPLES Scott Stevens LABORATORY Pace Analytical Lab Cert. # 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ® Jan -June ❑ July -Dec or ® Monthly' January lmonthl DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA, []Zero -flow ❑Water supply ❑SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 ❑ No discharge this period?' Outfali No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks ===> - - 100 mg/L or 50 mg/L" 6.0 — 9.0 0.007 mg/L 0.'03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 01 No Flow 02 01/23/15 0.25 24 mg/L 7.01 0.0114 mg/L ND 0.0976 mg/L ND NA ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Storm water Pollution Prevention Plan may so certify, and the requirement for TTO monitoring. may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), i certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe Wegmiller Name (Print name) Manufacturing Director Title (Print title) JOB- W Z/Q/Z0 !S (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported, in the format, "<XX mp,/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfali No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Not Applicable Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or 'Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART Il SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mall an origlnal and one copy of this DMR, including all "No Discharge" repor7swhhin 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of ?,6/00/5- (datef Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 IceAnalytical W&VpWd8bscnm January 29, 2015 Mr. Scott Stevens Goodyear 108 Business Park Drive Statesville, NC 28677 RE: Project: Stormwater 1123 Pace Project No.: 92234800 Dear Mr. Stevens: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on January 23, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of i 1 aceAnalytical' rMw.ps0e0tDacam CERTIFICATIONS Project: Stormwater 1123 Pace Project No.: 92234800 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: EB7627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 Pace Analytical Services, Inc. ra�- 1 9800 Kincey Ave. Suite 100 G�i<i 1V`I`l Huntersville, NC 28078 �rpbsmm (704)875-9092 SAMPLE ANALYTE COUNT Project: Stormwaler 1l23 Pace Project No.: 92234800 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92234800001 2015-01 EPA 1664E CLW 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2540D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 Pace Analytical Services, Inc. aceMalyfia• 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 www.peodebawm (704)875-9092 ANALYTICAL RESULTS Project: Stormwater 1123 Pace Project No.: 92234800 Sample: 2015-01 Parameters Lab ID: 92234800001 Collected: 01/23/15 10:15 Results Units Report Limit DF Received: 01/23/15 15:15 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg]L 5.0 1 01/26/15 16:23 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 11.4 ug/L 5.0 1 01/26/15 15:20 01/27/15 06:03 7440-50-8 Lead ND ug/L 5.0 1 01/26/15 15:20 01/27/15 06:03 7439-92-1 Zinc 97.6 uglL 10.0 1 01/26/15 15:20 01/27/15 06:03 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 24.0 mg1L 6.2 1 01/28/15 17:50 D6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/29/2015 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 ceAnalytical • r'r'r'.p�bscvnt QUALITY CONTROL DATA Project: Stormwater 1123 Pace Project No.: 92234800 QC Batch: GCSV120181 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92234800001 METHOD BLANK: 1377773 Associated Lab Samples: 92234800001 Parameter Units Oil and Grease mg1L LABORATORY CONTROL SAMPLE: 1377774 Parameter Units Oil and Grease mg1L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 01/26/15 16:09 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 40 36.2 90 78-114 MATRIX SPIKE SAMPLE: 1377775 92234802001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 25.3 40.8 62.2 90 78-114 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit IS presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/29/2015 02:46 PM without the written consent of Pace Analytical Services, Inc,. Page 5 of 11 ceAnalytical0 ntrw.paoeleb&svrrt Project: Stormwater 1123 Pace Project No.: 92234800 QC Batch: MPRP117774 QC Batch Method: EPA200.7 Associated Lab Samples: 92234800001 METHOD BLANK: 1377709 Associated Lab Samples: 92234800001 Parameter Units ug1L ug1L ug1L Copper Lead Zinc QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed NO 5.0 01/27/15 0418 ND 5.0 01/27/15 04:18 NO 10.0 01127YI5 04:18 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1377710 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper uglL 500 482 96 85-115 Lead uglL 500 473 95 85-115 Zinc uglL 500 460 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1377711 1377712 > MS MSD 92234840004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper ug1L 23.6 500 500 514 523 98 100 70-130 2 Lead ug1L 15.3 500 500 451 459 87 89 70-130 2 Zinc ug1L 59.5 500 500 502 518 813 92 70-130 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1377713 1377714 MS MSD 92234546001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug1L 268 500 500 737 749 94 96 70-130 2 Lead ug1L 5.4 500 500 465 463 92 92 70-130 0 Zinc uglL 587 500 500 1020 1040 87 91 70-130 2 Results presented on this page ara in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/29/2015 02:46 PM without the written consent of Pace Analytical Services, Inc,. Page 6 of 11 Pace Analytical Services, Inc. /+n ��e� �.�J• L�eil:tlII�L�Lif 9800 Kincey Ave. Suite 10o Huntersville, NC 28078 • (704)875-9092 QUALITY CONTROL DATA Project: Stormwater 1123 Pace Project No.: 92234800 QC Batch: WET135454 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 922348001)01 METHOD BLANK: 1379915 Matrix: Water Associated Lab Samples: 92234800001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 01/28/15 17:47 LABORATORY CONTROL SAMPLE: 1379916 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 242 97 90-110 SAMPLE DUPLICATE: 1379917 92234800001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 24.0 30.5 24 D6 SAMPLE DUPLICATE: 1379918 92234932001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL ND N❑ . Results presented on this page are In the units indicated by the "units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/29/2015 02:46 PM without the written consent of Pare Analytical Services, Inc.. Page 7 of 11 'CeAna4ftafe rnrpacebb&com QUALIFIERS Project: Stormwater 1/23 Pace Project No.: 92234800 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PAS[-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/29/2015 02:46 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 • aceA�ralytical . trrlrpO�D?.R7gt QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater 1123 Pace Project No.: 92234800 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704)B75-9092 Lab Id Sample ID QC Batch Method QC Batch Analytical Method 92234800001 2015-01 EPA 1664B GCSVI20181 92234800001 2015-01 EPA200.7 MPRPI17774 EPA200.7 92234800001 2016-01 SM 2540D WET135454 Date: 01/29/2015 02:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch ICP116002 Page 9 of 11 CHAIN -OF -CUSTODY 1 Analytical Request Document o PaceAnalytical • The Chair of tody isa LEGAL da must DOCUMENT. AP relevant Aelt be cornpWW aeetrraleiy. ....y�rtJab,.eea m a Section A Section B Socdon C Required Ctieml Information: Requlrod Pn*= Wo manes: invoke trdarrnaeon; .�t �. I;epartTo �s ent,en: Page: of 158565 0 r X/ Imo— Copy To. CompzV Name: REGULATORY AGENCY Cr ftJ� 1 .Z 7 Address: _ NPDES GRouND WATER " DRINIONG WATER UST RCRA OTHER EmalTo: 1 Pu �0 we&darNO.: Pow tt.remncQ +7�Fatr. Project Nano: Mara ar: SEte Lxetinn STATE: _LA1L►(; Rogwstod Due DwarrAT: Project Nran7er: PWfte. 'Requested Ana"IS Filtered (YIN) Sectlon D Matrix Codas R.gat dCtfw 1,w ma MAswl[ 1 [bn. Drfnidrg Water DW Water WT Wasu Water WW Ptoauu P wrsofid SL SAMPLE 1D oax )L WT- 0-9 r ; 1 Air AR Barn7eIDS MUST BEUKIQUE Tissue TS Othu OT = U.2pp O U COLLECTED q w Q PresorvaIrms = Y CAuaoat7tAn srT OLr;e [NPCMO �� = x ° z i O F- N a� .,a tr 12 Z3-tffoo Paco Protect Nod Lab I.D. DATE TIME DATA TIME 2 ' 7 4 5 a 9 10 11 11 ADDITIONAL COMMENTS RELINQUISNEOaWAFFWATION DATE TIME ACCEPTED RV f AFFILIATtON DATA TIME SAMPLE CONDITIONS i�31 2:2 c• r•��• is r ^;i:(�6'\;•�.� SAMPLER NAME AND SIGNATURE y } .. E E, PRINT Name of SAMPLER: SIGNATURE of SAMPLER: DATE Signed MNVDDrM: -+1irrqq . Pace's NET >D Eay payreant terms and aveeatq to We dorges of 1.b% w rrtenih top dq InYprpey not paid *me 30 SC m F-ALL-W2Urev.97. S 5-May-ZW 'Lm.v r ,l Nab. By+%aroma Iris form roe W.&4s;r+y /, IJ00Analytiay" i Document Number: F-CHR-CS-003-rev.15 1 of 2 Pace Huntersville Quality Office Client Name: � Courier: ❑ Fed Ex ❑ und LISPS❑ Client❑ Commercial rPace ther + ` I Custody Seat on Cooler/Box Present: ❑ yes n Seals intact: ❑ yes ❑ no p ad: Packing Material: ❑ Bubble VDp EjQubble Bags None ❑ Other Thermometer Used: IR Gun T1411 Type of Ice: We Blue None [3,�amples on ice, cooling process has begun Temo Correction Factor T1401 -No Correction Corrected Cooler Temp.: 'C Biological Tissue Is Frozen: Yea No rA g Date and Initials of person xaIning fs contents: Temp should be above freezing to 6'C Comments: Chain of Custody Present: es ONO ❑MA 1. Chain of Custody Filled Out: ONO ❑WA 2. Chain of Custodytin Reutshed: ',Wea C.3Yes ON, ❑wA 3. Sampler Name & Signature on COC: ❑Yes &(No ❑WA 4. Samples Arrived within Hold Time: VK,, [IN. ❑wA 5. Short Hold Time Analysis A2h : ❑Yes Mo ❑N!A 6. Rush Turn Around Time Requested; Oyes MNo ❑wA 7, Sufficient Volume: Yes ©Na ❑wA 8. Correct Contalners Used: Vea ❑No OwA 9. -Pace Containers Used: .tires ONO ❑wA Containers Intact: 1'Jrres ONO ❑wA 10. Filtered volume received for Dissolved tests ❑Yes ONO L (rA 11. Sample Labels match COC: es ❑No ❑wA 12. -Includes date/tfineAD/Ana sis Matrix: All cmtalners needing preservatton have been chocked. Yes ONO ❑wA 13. All containers needtng preservation are found to be In es ONO ❑wA compliance with EPA recommendation. exceptlons: VOA, eo!lform, TOC, OaG, VA-DR0 ter) CQYea ONO Samples checked for dechlorination: ❑Yea ONO N!A 14, Heads ace in VOA Vials >Bmm): ❑Yes ONO 061A 15, Trip Blank Present: ❑Yoe ONO MA 16. Trip Blank Custody Seals Present ❑Yes ONO V/WA Pace Trip Blank Lot # Qfpurchased): Client Notification/ Resolution: Field Data Required? Y / N Person Contacted: Dateff ime: Comments/ Resolution: SCURF Review: 1 4 1 Date: I r xt , s SRF Review; Date: �c i3 Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, incorrect preservative, out of temp. Incorrect containers) 1o�#9zz3�41$0:0= - f. A: Page 11 of 11 The Goodyear Tire & Rubber Company — Statesville Mold Plant 108 Business Park Drive Statesville, NC 28677 February 09, 2015 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Storm Water DMR, General Permit NCG030000, COG NCG030513 Dear Sir or Ms., RECEIVE® FEB 12 2015 CENTRAL FILES &M SECTION The Goodyear Tire & Rubber Co. — Statesville Plant (Goodyear) is covered under North Carolina General Storm Water Permit NCG030000. The permit requires submission of a discharge monitoring report within 30 days of receiving analytical results. Please find enclosed a DMA for a sample collected on January 23, 2014. A sample was collected from outfall #2. If further information is required please do not hesitate to contact us. Sincerely, Sc,--,* girt� Scott Stevens ERS Manager The Goodyear Tire & Rubber Co. Certified Mail No. 7011 1570 0003 5901 9018 Return Receipt Requested Attachment cc. file Semi-annual Stormwater Discharge -Monitoring Re ort for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted September 16, 2015 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Comoan COUNTY Iredell PERSON COLLECTING SAMPLES Kristin Flora LABORATORY Pace Analytical_ Lab Cert. # 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' August (month] DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA RECEIV i ED ❑Zero -flow ❑Water Supply ESA RC ❑Other M-J SEP 24 2015 Mmom CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTION ® No discharge this period ?z Outfall No. Date Sample l Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended solids P H, Standard units Copper Lead Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons - Total nics Organics Benchmarks ===> _ - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 002 No discharge 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived, The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last'discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe We miller Name (Print name) Manufacturing Director Title (Print title) J� (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical the format. When results are below the applicable limits, y must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses, See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. n No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an orlainal._and one copy.of_this. DMR,_includina_.all "No Discharae".reports, within 30 days of receipt of the lab results (or at end of monitorina period in the case of "No Discharge" reports) to: Division of Water Quality . Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." JOB (Signature of Pe Cjr (, 1,701S (Date Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 V_ Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted October 29, 2015 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Comoan COUNTY Iredell PERSON COLLECTING SAMPLES Kristin Flora LABORATORY Pace Analytical Lab Cert. # 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 MbPERIOD ❑ Jan -June ❑ July -Dec Rc� or ® Monthly' September (month) NOV 0 4132 TARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA CENTRAL FILES ❑Other DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -) ® No discharge this period?' Outfall No. Date Sample Collected l (mo/dd/yr) 2a-hour rainfall amount, Inches Total Suspended Solids P H, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics' Benchmarks ===> _ - 100 mg/L or 50 mg/L4 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 002 No discharge 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Storm water Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may heyaived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report, I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe Wegmiller Name (Print name) Manufacturing Director Title (Print title) r (Signature) (Da() Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, the must be reported in the format "<XX m L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 -- 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 FS .{ Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART it SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one coov of this DMIt including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitorina oeriod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." jol, r (Signature of Permittee) fa , ,F zais (Date SWU-245, last revised 10/25/2012 Page 3 of 3 Permit Date:11/1/2012-10/31/2017 r' Semi-annual Stormw er Discharge_ . _ at Monitoring Report I for North Carolina Division of Water Quality General Permit No. NCG03000 Date submitted November 24, 2015 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Company COUNTY Iredell PERSON COLLECTING SAMPLES Kristin Flora LABORATORY_ Pace Analytical Lab Cert. h _40 Comments on sample collection or analysis: No sample collected — No Discharge during the month Part A: Stormwater Benchmarks and Monitoring Results co)))e SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly'_ April (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA RECEIVED ❑Other DEC 14 2015 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL FILES DWR SECTION ® No discharge this period?' Outfall No. Date Sample 1 Collected (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics' Benchmarks ===> - - 100 mg/L or 50 mg/L" 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 002 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. A See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/2-5/2012 Page 1 of 3 .d% Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may bd waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe Wegmiller Name (Print name) Manufacturing Director Title (Print title) Joler w t Y7-L1/Ig5_ (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement 'tier I, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you,report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitorina oeriod in the case a "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: ".1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Jae- /zc� �al� (Signature of Permitte (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 ?r Semi-annual Stormwater_D_is_cha_rge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG03000 . Date submitted November 24, 2015 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Company COUNTY Iredell PERSON COLLECTING SAMPLES Kristin Flora LABORATORY_ Pace Analytical Lab Cert. # _40 Comments on sample collection or analysis: No sample collected - No Discharge during the month Part A: Stormwater Benchmarks and Monitoring Results copy SAMPLE COLLECTION YEAR 201S SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' June (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA RECEIVED ❑Zero -flow ❑Water Supply ❑SA [—]Other OEC 14 2015 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL FILES DWR SECTION ® No discharge this period?' Outfall No. Date Sample Collected) (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics' Benchmarks ===> - - 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0,067 mg/L 15 mg/L 1 mg/L 002 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe Weemiller Name (Print name) Manufacturing Director Title(Printtitle) `..JO-t._ Ll�1 (Signature) ( ate) Note. Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. r 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "'No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of i�S (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report ` for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted November 13, 2015 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodvear Tire & Rubber Comnan COUNTY Iredell PERSON COLLECTING SAMPLES Kristin Flora LABORATORY Pace Analytical Lab Cert. h 40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec •� or ® Monthly' October (month} DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA 1 I []Other � RECEIVED Q PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 NOV 2 3 2915 _04 CENTRAL FILES ® No discharge this period?' n,R.- Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units ION Copper Lead Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics' Benchmarks 100 mg/L or 50 mg/L" 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 002 No discharge 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 r Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be wai;red. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." Joe We2miller Name (Print name) Manufacturing, Director Title ryry(Print title)] ✓a2, W i � � �o !.5 (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART lI SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of -receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permit Date:ll/1/2012-10/31/2017 )' 16 A7 ( ate) SWU-245, last revised 10/25/2012 Page 3 of 3 ram_ ..... rg- �a .. f .r J, f K The Goodyear Tire & Rubber Company — Statesville Mold Plant 108 Business Park Drive Statesville, NC 28677 November 13, 2015 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Storm Water DMR, General Permit NCG030000, COG NCG030513 Dear Mr. or Ms, The Goodyear Tire & Rubber Company — Statesville Plant (Goodyear) is covered under North Carolina General Storm Water Permit NCG030000. The permit requires submission of a discharge monitoring report 30-days of receiving analytical results. No events occurred during the month of October, so no sample was collected from outfall #2. If further information is required please do not hesitate to contact me at 704-928-4508. Sincerely, Emily Roy Safety, Training and Environmental Manager The Goodyear Tire & Rubber Company Certified Mail No. 7011 1570 0003 5901 9124 Return Receipt Requested Attachment cc: file Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG0300 Date submitted November 13, 2015 _ CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Company COUNTY Iredell T PERSON COLLECTING SAMPLES Emily Roy LABORATORY Pace Analvtical Lab Cert. # 40 Comments on sample collection or analysis: RECEIVED DEC 14 2015 Part A: Stormwater Benchmarks and Monitoring Results CENTRAL. FILES DWR SECTION SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑July -Dec or ® Monthly'November lMon 1 DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero -flow ❑Water Supply [_]SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ® No discharge this period?' Outfall No. Date Sample Collected i (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pr d Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ===> - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 002 No discharge ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring ma,,, -be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe Weemiller Name (Print name) Manufacturing Director Title (Print title) (Signature) (Date} Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfali No. Hate Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L" 6.0 — 4.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier I, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER ATANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." J (Signature of l Z Zozr (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 crj-ooDi�acz The Goodyear Tire & Rubber Company — Statesville Mold Plant 108 Business Park Drive Statesville, NC 28677 November 24, 2015 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Storm Water DMRs, General Permit NCG030000, COG NCG030513 Dear Mr. or Ms, The Goodyear Tire & Rubber Company — Statesville Plant (Goodyear) is covered under North Carolina General Storm Water Permit NCG030000. The permit requires submission of a discharge monitoring report 30-days of receiving analytical results. During a recent review of our records we were unable to locate file copies of the No Discharge DMRs for the months of April, .tune and July. Please find enclosed a DMR for each of these months. If further information is required please do not hesitate to contact me at 704-928-4508. Sincerely, Emily Roy EHS Manager The Goodyear Tire & Rubber Company Certified Mail No. 7011 1570 0003 5901 9131 0 Return Receipt Requested z CD Attachments rn D cc: file -4 -n Z cz� G; M Ce) Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted November 24, 2015 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Company. COUNTY Iredell PERSON COLLECTING SAMPLES Kristin Flora LABORATORY_ Pace Analytical Lab Cert. # _40 Comments on sample collection or analysis: No sample collected — No Discharge during the month Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' July month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA RECEIVED []Zero -flow ❑water Supply []SA DEC 14 2015 []Other CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTION N No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks ===> - - 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 002 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ' See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe We miller Name (Print name) Manufacturing Director Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period ?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 r' y Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES 1N A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME-. Mail an on final and one copy of this DMA including all "No Discharge" reports, within 30 daysof receip I o the lab results or at end of monitoring eriod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." L/t/YVI� '� I - ( Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 F Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted: 01/45/15 CERTIFICATE OF COVERAGE NO. NCG030513 FACILITY NAME The Goodyear Tire & Rubber Company COUNTY Iredell PERSON COLLECTING SAMPLES Scott Stevens LABORATORY Pace Analytical Lab Cert. # _40 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2014 :11110- SAMPLE PERIOD ❑ Jan -June ® July -Dec 0. or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA 5..2 ❑Zero -flow [:]WaterSupply ❑SAS, ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 „ ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Nan -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics' Benchmarks ===> - - 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 01 No Flow 02 12/05/14 0.01 9.9 mg/L 7.20 0.0099 mg/L ND 0.0693 mg/L ND NA 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. ' Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469,22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring ' may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Joe Weemiller Name (Print name) Manufacturing Director Title(Printtitle) LJL== (Signature) ate) Note: Results must be reported in numerical format. Do not report Below Detection limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintanznce Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Outfali No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches a Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Not Applicable Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. + TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I -^- ..am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ,�e_' (Signature of Atee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 (�Iaceklalytical e Wrwyacabbswin December 12, 2014 Mr. Scott Stevens Goodyear 108 Business Park Drive Statesville, NC 28677 RE: Project: Stormwater 12/5/14 Pace Project No.: 92228417 Dear Mr. Stevens: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on December 05, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample anaiyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Endosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 aceAnalyticat Nw 4mmiaba.cnm Project: Stormwater 12/5114 Pace Project No.: 92228417 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersvil le, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certificatlon #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Florida/NEtAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 aceAnalytical W*WP&8A1b&=n SAMPLE ANALYTE COUNT Project: Stormwater 1215114 Pace Project No.: 92228417 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.r9092 Anafytes Lab ID Sample ID Method Analysts Reported Laboratory 92228417001 2014-02 EPA 1664B CLW 1 PASI-C EPA 200.7 JMW 3 PASI-A SM 2640D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 aceAnalytical WWW4WMbb& arrr ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilre, NC 28078 (704)8759092 Project: Stormwater 1215114 Pace Project No.: 92228417 Sample: 2014-02 Lab ID: 92228417001 Collected: 12/05/14 10:15 Received: 12/05/14 13:18 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 12/09/14 09:12 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 9.9 ug1L 5.0 1 12/08/14 15:25 12/10/14 20:25 7440-50-8 Lead ND ug1L 5.0 1 12108/14 15:25 12/10/14 20:25 7439-92-1 Zinc 69.3 ug1L 10.0 1 12108/14 15:25 12/10/14 20:25 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 9.9 mg1L 3.7 1 12/10/14 14:55 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12112/2014 11:59 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 IaceAnaocal* (�mrw.pae�bawm QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater 1215114 Pace Project No.: 92228417 QC Batch: GCSVI19728 Analysis Method: EPA 1664B QC Hatch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92228417001 METHOD BLANK: 1346505 Matrix: Water Associated Lab Samples: 92228417001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 12/09/14 09:04 LABORATORY CONTROL SAMPLE: 1346506 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 34.3 86 78-114 MATRIX SPIKE SAMPLE: 1346507 92228229001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 35.6 92 78-114 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12112/2014 11:59 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 ;5ceAn'a"cals worw.paoetahs tam Project: Stormwater 1215114 Pace Project No.: 92228417 QC Batch: MPRP117496 QC Batch Method: EPA200.7 Associated Lab Samples: 92228417001 METHOD BLANK: 1346119 Associated Lab Samples: 92228417001 Parameter Units ug1L uglL uglL Copper Lead Zinc QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed ND 5.0 12/1011418:45 ND 5.0 12/10/1418:45 ND 10.0 12/10/1418:45 Qualifiers Pace Anatytica I Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 LABORATORY CONTROL SAMPLE: 1346120 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper uglL 500 528 106 85-115 Lead uglL 500 503 101 85-115 Zinc ug1L 500 477 95 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1346121 1346122 MS MSD 92228444002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Copper uglL 58.8 500 500 594 589 107 106 70-130 1 Lead uglL ND 500 500 502 494 100 99 70-130 2 Zinc ug1L 390 500 500 • 860 861 94 94 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1346123 1346124 MS MSD 92228390001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 5.0 500 500 527 518 104 103 70-130 2 Lead ug/L ND 500 500 502 496 100 99 70-130 1 Zinc uglL 187 500 500 654 647 93 92 70-130 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12112/2014 11:59 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 11 (�15'neMapml@ www.pacem&corn QUALITY CONTROL DATA Project: Stormwater 1215114 Pace Project No.: 92228417 QC Batch: WET134696 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92228417001 METHOD BLANK_ 1348071 Associated Lab Samples: 92228417001 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: 1348072 Parameter Units Total Suspended Solids mglL SAMPLE DUPLICATE: 1348073 Parameter Total Suspended Solids Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 1o0 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 12/10/14 14:48 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 238 95 90-110 92228289001 Dup Units Result Result mglL 1770 1950 SAMPLE DUPLICATE: 1348074 92228647002 Dup Parameter Units Result Result Total Suspended Solids mg1L 30.0 25.0 RPD Qualifiers 10 RPD Qualifiers 18 D6 Results presented on this page are in the units Indicated by the -Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 12/12/2014 11:69 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aceAnalytica!° nrlY.pacews Gore QUALIFIERS Project: Stormwater 12/5114 Pace Project No.: 92228417 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvitle, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNi - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2014 11:59 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 "Cl wMrpacadabs.mm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Storrnwater 1215/14 Pace Project No.: 92228417 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875,W92 Analytical Lab I❑ Sample ID QC Batch Method QC Batch Analytical Method Batch 92228417001 2014-02 EPA 1664B GCSV119728 92228417001 2014-02 EPA 200.7 MPRP117496 EPA 200.7 ICP115763 92228417001 2014-02 SM 2540D WET134696 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/12/2014 11:59 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 11 CHAIN -OF -CUSTODY /Analytical Request Pocument 'nw Ch2w&oWLstody b a LEGAL DOCUMENT.AU rdwrzt fields avast be cxr~ 8C==IY- f�3 J 5.1.0 21- 16 ro ftz�lelfj MA ]Eel .4'gr-1 NPDES r- GROUND WATER. r- DRINJUNG WATER UST RCRA 7 OTHER I. 1�n W_5159WE�- WIMIM Mmmm� M-MME M. MMMWIPIWM� • T�vul{ M= vy 59wv = TOM YCU we Hb730CwpSYrmwftm mid ago, iq bwmmww$CfI4%porwambrm7h not V* "LOW 70 dayL FALL-Q-02QfISv.VT, 1.&MV1QoU Document Name: I Document Revised: September;a. M14 f Acf�Alfnlyfrctrr' RlumDer: 003=rewl6 Cllen# Name: Huntersvine Courier: ❑ Fed Ex ❑ UPS[] USPS[] Client[] Commercial❑•0ce Other Custody Seat on Cooler/Box Present: ❑ yea Vo Seals intact: ❑. 'yes ❑ no Elm Packing Material: ❑ Bubble VE)p ❑ Bub �e ads ❑ None ❑ Other' Thermometer Used: IR Gun �� Type of lce � Blue Nbne.Sampfas on Ice, tooting process'hae begun Temp Correction Factor _ T1 1 No Correction Corrected Cooler Temp.:y �C Biological Tlasus Is Frozen: yes No. WAA Temp should be above freezing to 6*0 Comments: Date and In tl= s f person examining contents: 11- t Chain of Custody Present: Yes- ONO ❑NIA 1. Chain of Custody Filled Out: Yes ON* ❑NIA 2. Chain of Custody Relinquished: OYea ❑No ❑NIA 3. Sampler Name & Si nature on COC: ❑Yax E1ff,'ONIA 4. Samples Arrived within Hold Time: -es OHO ❑NIA 5. Short Hold Tlme Analysis <72hr : ❑Ye ❑ffo- dNIA 0. Rush Tura Around Time Requested: OYes ot+i�❑NrA 7. Sufficient Volume: ©Yt NIA 8. Correct Containers Used: 1---DYas ONO ❑NIA -Pace Containers Used: M Vre-3 ❑No OWA 9. Containers Intact: DYea ❑No ❑wA 1o. Filtered volume received for Dissolved tests ❑ices )No lEfWA 11. Sample Labels match COC: ` Yea ©M�❑NIA -Indudes dateAlme/ID/Anal sls Matrix: 12. Ali conlalners needing preservation have been checked. ,PY6-ONo ❑NIA All containars needing preservation are found to be In r t�/.'❑No ❑WA compliance with EPA recommendation. j•" w exceptions: VOA, collromL TOG, OSO,1M-ORO t2too ,-ay—*,- ❑ No 13. Samples checked for dechlodnatlon: ❑Yes ON VA 14. Heads ace In VOA Vlals >6mm : OYes ONO JDWK 16. Trip Blank Present: Oyes ONO ❑Nrl1 Trip Blank Custody Seals Present OYes ONO ONIA Paoe Trip Blank Lot # Of purchased): Ia. Client Notification/ Resolution: Field Data Required? Y i N Person Contacted: Date/Time: Comments/ Resolution: SCURF Revlew: A" Date: I SRF Review. G- Date: / Note: • Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (I.e out of hold. Incorrect preservative, out of (emp, Al Incorrect contalners) l �" .WOE •..j92228�4r1.7�f . - - 92220417 f Page 11 of 11 The Goodyear Tire & Rubber Company — Statesville Mold Plant 108 Business Park Drive Statesville, NC 28677 January 05, 2015 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Storm Water DMR, General Permit NCG030000, COG NCG030513 Dear Sir or Ms., REFCEIVED JAN 0 7.2015 CENrR,gL RLES DWR SECTION The Goodyear Tire & Rubber Co. — Statesville Plant (Goodyear) is covered under North Carolina General Storm Water Permit NCG030000. The permit requires submission of a discharge monitoring report 30-days of receiving analytical results. Please find enclosed a DMR for a sample collected on December 05, 2014. A sample was collected from outfall ##2. If further information is required please do not hesitate to contact us. Sincerely, S S Scott Stevens EHS Manager The Goodyear Tire & Rubber Co. Certified Mail No. 7011 1570 0003 5901 9001 Return Receipt Requested Attachment cc: file Semi-annual Stormwater Discharge MonitoringReport for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted: 07/09/14 CERTIFICATE OF COVERAGE NO. NCG030513 SAMPLE COLLECTION YEAR 2014 FACILITY NAME The Goodyear Tire & Rubber Company SAMPLE PERIOD ® Jan -June ❑ July -Dec COUNTY Iredell or ❑ Monthly' (month) PERSON COLLECTING SAMPLES Scott Stevens "�DISCHARGING TO CLASS ❑ORW ❑HQW [:]Trout ❑PNA LABORATORY _Pace Analytical Lab Cert. # 40 RECEIVED ❑Zero -flow ❑Water Suppiy ❑SA Comments on sample collection or analysis: JUL 14 2014 [_]Other CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWQ/BOG Part A: Stormwater Benchmarks and Monitoring Results ❑ No discharge this period ?2 Outfall No. Date Sample Collected) (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ===> _ - 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 01 No Flow 02 06/16/14 0.01 156 7.27 0.0182 0.0052 0.111 5.7 NA 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is.that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469,12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (70),1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." Joe We9miller_ Name (Print name) Manufacturing Director Title (Print title) 7 a (Signature) (D te) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?1 Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 2664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Not Applicable 1 7- Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Note: !f you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one coov of this DMR, including all "No Discharae" reports. within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permit Date: 11/1/2012-10/31/2017 7 a ( at ) SWU-245, last revised 10/25/2012 Page 3 of 3 ceAnalytical WMID rolahs-oom July 07, 2014 Mr. Scott Stevens Goodyear 108 Business Park Drive Statesville, NC 28677 RE: Project: STORMWATER Pace Project No.: 92205574 Dear Mr. Stevens: Pate Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huniersville, NC 28078 (704)87 r9092 Enclosed are the analytical results for sample(s) received by the laboratory on June 17, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen for Tabitha M Dacal tabitha.dacal@pacelabs.com Project Manager Enclosures, cc: Mr. Claude Wagner, Goodyear REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 11 Pace Analytical Services, Mt. 7ceM*ical ® 9800 Kincey Ave. Suite 100 �;aHuntersville, NC 28078 www.p&cmo&bs.com (704)875-9092 CERTIFICATIONS Project: STORMWATER Pace Project No.: 92205574 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 26078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginiafVELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDS 2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Flodda/NELAP Certification # E87W South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 11 Icul eAnalytical www.paWabs-mm SAMPLE ANALYTE COUNT Project: STORMWATER Pace Project No.: 92205574 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92205574001 2014-01 EPA 1664E CI-W 1 PAS!-C EPA 200.7 JMW 3 PASI-A SM 2540D WRC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 11 Pace Analytical Services, Inc. e 9800 Kincey Ave. Suite 100 Y aceAnalytrcal Huntersville, NC 28078 rnrrrpacala6s.corrr (704)875-9092 I ANALYTICAL RESULTS Project: STORMWATER Pace Project No.: 92205574 Sample: 2014-01 Lab ID: 92205574001 Collected: 06/16/14 15:15 Received: 06/17114 10:56 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease 5.7 mg1L 5.0 1 06/18/14 12:48 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Lead 5.2 ug/L 5.0 1 06/18/14 15:30 06/19/14 18:50 7439-92-1 250D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 156 mg1L 16.7 1 06/18/14 16:41 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, Date: 06/2412014 05:47 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 11 aceAnalytrcals wwwPecalabs.wm Project: STORMWATER Pace Project No.: 92205574 QC Batch: GCSV117952 QC Batch Method: EPA 1664E Associated Lab Samples: 92205574001 METHOD BLANK: 1223498 Associated Lab Samples: 92205574001 Parameter Units Oil and Grease mg1L LABORATORY CONTROL SAMPLE: 1223499 Parameter Units Oil and Grease mg7L Pace Analytical Services, Inc_ 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 06118/1412:43 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 40 38.5 96 78-114 MATRIX SPIKE SAMPLE: 1223500 92205690001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 38.4 91 78-114 Results presented on this page are In the units indicated by the -units' column except where an alternate snit Is presented to the rtgm of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/07/2014 04:53 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 a oAnalyticale www.Pws b3'ovm Project: STORMWATER Pace Project No.: 92205574 QC Batch: MPRP116248 QC Batch Method: EPA 200.7 Associated Lab Samples: 92205574001 METHOD BLANK: 1224002 Associated Lab Samples: 92205574001 Parameter Units ug1L ug1L ug1L Copper Lead Zinc QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed ND 5.0 06/19/1417:47 ND 5.0 06/19/1417:47 ND 10.0 06/1911417:47 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 2807a (704)875-9092 LABORATORY CONTROL SAMPLE: 1224003 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug1L 500 492 98 85-115 Lead ug/L 500 481 96 85-115 Zinc uglL 500 466 93 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1224004 1224005 MS MSD 92205120001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Copper ug1L ND 500 500 476 495 95 98 70-130 4 Lead ug1L ND 500 S00 439 456 88 91 70-130 4 Zinc ug/L 22.3 500 500 478 496 91 95 70-130 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1224006 1224007 MS MSD 92205120002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Copper uglL ND 500 500 517 520 103 104 70-130 V Lead uglL ND 500 500 492 497 98 99 70-130 1 Zinc uglL 22.6 500 500 572 580 110 111 70-130 1 Results presented on this page are in the units indicated by the -units" column except Where an attemate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, Date: 07/07/2014 04:53 PM without the written consent of Pace Analytical Services, Inc.. Qual Qual Page 6 of 11 aceAnalytr"cal e www.pacslaDs.txxn QUALITY CONTROL DATA Project: STORMWATER Pace Project No.- 92205574 QC Batch: WET/31646 Analysis Method: SM 2540D QC Batch Method: Sint 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92205574001 METHOD BLANK: 1224146 Associated Lab Samples: 92205574001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 1224147 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1224148 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1224149 Parameter Units Total Suspended Solids mg/L Pace Analytical services, Inc. 9800 Kincey Ave. Surie 100 Huntersville, NC 2BO78 (704)8759092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 06/18/14 16:33 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 268 107 80-120 92205691001 Dup Result Result RPD Qualifiers 238 235 1 92205424003 pup Result Result RPD Qualifiers 12.7 41.2 106 D6 Results presented on this page are in the units indicated by the 'Units' column except where an alternate unit is presented to the fight of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/07/2014 04:53 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11 aceAnallytical e ! www.p wm I QUALIFIERS Project: STORMWATER Pace Project No.: 92205574 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 23078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Di phenylhydrazine (8270listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Arad preservation may not be appropriate for 2-Chloroethylvinyi ether, Styrene, and Vinyl chloride. LOD - Limit of Detection. LOQ - Limit of Quantitation. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 07/07/2014 04:53 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 11 1cleAaWical mvw:paWAbs.oam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER Pace Project No.: 92205574 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92205574001 2014-01 EPA 1664B GCSV117952 92205574001 2014-01 EPA 200.7 MPRP116248 EPA 200.7 ICP114684 92205574001 2014-01 SM 25401) WET131646 Date: 07/07/2014 04:53 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Tull, without the written consent of Pace Analytical Services, Inc.. Page 9 of 11 I "LAIM111=IIt I4d111C, vu4.w ut.,u wv✓+.u• , �+•+- -•- �AwWca!• Sam le Condition Upon Receipt (SCUR) Page 1 of 2 Document Number: Issuing Authority: F-CHR-CS-003-rev.14 Pace Huntersville Qualit y Office Client Name: .} Courier:,t/Fe1 Ex1n UPS❑ USPSE] Client❑ Commerciald Pace Other Q Dq Custody Seal on Cooler/Box Present: ❑ yes I )' Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble Wrap Wubbl gs ❑ None ❑ OtherThermometer Used: IR Gun T7162 Type of ice: Wet Blue None Samples on ice, cooling process has begun Tems) Correction Factor T1102: No Correction T1301: No Correction Corrected Cooler Temp.: <<LI •C Temp should be above freezing to 6°C Biological Tissue is Frozen: Yes No N/A Comments: Date and Initial of person examining contents' OjJ (O�ti11`a Chain of Custody Present: Yes ❑No ❑NIA 1. Chain of Custody Filled Out: Yes ❑No ❑NIA 2. Chain of Custody Relinquished: Yes ❑No ❑NIA 3. Sampler Name & Signature on COC: Yes ❑No ❑NIA 4. Samples Arrived within Hold Time: Yes ❑No ❑NIA 5. Short Hold Time Analysis <72hr : ❑Yes 6N. ❑NIA 6. Rush Turn Around Time Requested: ❑Yea ANo 11wA 7. Sufficient Volume: Sifes ❑No ❑NIA 8. Correct Containers Used, -Pace Containers Used: Yes ❑No jYes ❑No ❑wA ❑NrA 9. Containers Intact: j3Yes ❑No ❑NIA 10. Filtered volume received for Dissolved tests ❑Yes ❑Na d NIA 11, Sample Labels match COC: -Includes dateltimellD/Anal sis Matrix: es ❑No ❑NIA 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, collform, TOC, O&G, VWDRO (water) Yes ❑No dyes ❑No Yes ❑Na ❑NIA ❑N1A 13. Samples checked for dechlorination: ❑Yes ❑No NIA 14. Headspace in VOA Vials ( 7Bmm): I]Yes ❑No NIA 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): Dyes ONO ❑Yes ❑No A tA 16. Client Notification! Resolution: Field Data Required? Y / N Person Contacted: DatelTime: Comments/ Resolution: SCURF Review: y10 date: SRF Review: Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) Place label here coo#:92205574 ���1flfl�Ill �Nll l'I 92205574 Page 10 of 11 i • aceAnal4ical' CHAIN -OF -CUSTODY 1 Analytical Request Document o The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. www.pacalses, com Page: of Section A Section S Section C Required Client Information. Required Project Informatian: invoice Irdormation: Company: ,r. L r Report To: C -yam Attention: JE r r R xt7 it 1799747 f0 �. Add ross'. p �' ^_. Fite F 4I Ccpy To: Cun,pany Name: REGULATORY AGENCY S+R .i1) • "C Z ,7 7 Address: ( NPDES I GROUND WATER bRINKING WATER f* UST ("RCRA F OTHER Ema'.I To, J � ur a hasp Order No . Paco uorn O $tO���C1�� S �[' •� anrerenre: Pho e. Farr ^�D PrName: pace P,gea Site Location 7�'-g'73 6 7 luprader: STATE: 1 iIVC Requested Due Datel7AT: Project Numhe,, Pace Pm' -le or: !\ r lJ Requested Analysis Filtered (YIN) Section D Mari: COtlQb ~ Z Rqu�m6cront mlmmetw, MATRIX I GODF° COLLECTED Preservatives `s Drinking Water DW O Z O Water WIT Waste W6lef WW �+ F U m COM-OSITE STMT I: umPOSITE t-utiw59 L) Z MIXfuCt P Soil'Sohd 51. p y. SAMPLE ID °i1 ri'rpe WP (A-Z. 0-91 ,-) Ar AR Q w a Uj Z H p ° Sample Me MUST BE UNIQUE Tissue TS C,her OT O a 751 t!r V j � X a. u -45 F o WJ=�0t �,517 C F Q ¢ mMOaN14 rn DATE TIME DATE T1ME rn _ _ = Z Z Z. O y X Pace Project Nod Lob I.D. Zola-o �c Is:rS i 1 n K 2 9 4 5 6 7 8 9 ,0 H Tt ADDITIONAL COMMENTS RELINQUISHED BY ! AFFILIATION DATE TIME ACCEPTED BY) AFFILIATION DATE TIME SAMPLE CONDITIONS t ORIGINAL SAMPLER NAME AND SIGNATURE v o PRINT Name of SAMPLER: t'UY n S °1 ? `�' Z r w >` h ° �� .' E SIGNATURE vt SAMPLER: DATE Signed / (MMl0D1YY): -nnl.IlPn'. Note, by srnmha Iros Inrm y9u me accrntlmg r"'n� �� a NET 3p caypt,yrnent terms .rn.r;tqr—oj(j to tat= cnrrges of 5%per month'nr anv rnvotc- -trn pat]—!h., 3o dnya F-ALL-0-070rev.C7, 1 �)-Mny�2007 0 co ) 9 9 * V/ ZZ-Aj L 0DrD The Goodyear Tire & Rubber Company — Statesville Mold Plant 108 Business Park Drive Statesville, NC 28677 July 9, 2014 Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: Storm Water DMR, General Permit NCG030000, COG NCG030513 Dear Sir or Ms., The Goodyear Tire & Rubber Co. — Statesville Plant (Goodyear) is covered under North Carolina General Storm Water Permit NCG030000. The permit requires submission of a discharge monitoring report 30-days of receiving analytical results. Please find enclosed a DMR for a sample collected on June 16, 2014. A sample was collected from outfall #2. If further information is required please do not hesitate to contact us. Sincerely, 5,# Sk,,.c,,.o Scott Stevens EHS Manager The Goodyear Tire & Rubber Co. Certified Mail No. 7011 1570 0003 5901 8974 Return Receipt Requested Attachment cc: file Semi-annual Stormwater Discharge Monitoring Report (DMR) for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted 9-19 —t CERTIFICATE OF COVERAGE NO. NCG200513 FACILITY NAME United Scrap Metal Inc. COUNTY Mecklenburg PERSON COLLECTING SAMPLES John Dergo LABORATORY Pace Analytical Services, Inc. Lab Cert. Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 /� � SAMPLE PERIOD / or X Monthly' September, 2018 (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA J ❑Zero -flow [:]Watersupply [:]SA ❑Saltwater ®Other C Q PLEASE REMEMBER TO SIGN ON THE REVERSE 4 No discharge this period: Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks ==> - - 100 mg/L or 50 mg/O 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/LS 0.075 mg/L or 0.210 mg/L5 0.126 mg/L or 0.090 mg/LS Outfall 1 09/17/18 3.95 0.174 mg/L Outfall 2 09/17/18 3.95 0.04 mg/L 0.0176 mg/L 0.197 mg/L Outfall 3 09/17/18 3.95 0.04 mg/L 0.0132 mg/L 0.172 mg/L " Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfail. Z For sampling periods with no discharge at any single outfail, you must still submit'this discharge monitoring report with a checkmark here. 3The-total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. k See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. s Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they, must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Outfall No, Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =_=> _ - 15 mg/L 100 mg/L or 50 mg/0 Footnotes from Part A also apply to this Part B ❑ No discharge this period o r 1 � rn Sao fD 7- 9 ao z q o'cnx w n r- M M i M Note: If ou report a sample value in excess of the benchmark ou must implement Tier 1 Tier 2 or Tier 3 res onses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES® NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: lames Moore Mail an original and one coov of this DMR, including all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharae" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Date) Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 2of2 Permit: NGG200513 SOC: County: Mecklenburg Region: Mooresville Contact Person: John Dergo Compliance Inspection Resort Effective: 09/24/15 Expiration: 12l31119 Owner: United Scrap Metal Inc Effective: Expiration: Facility: United Scrap Metal, Inc, 9925 Brookford St Title: Charlotte NC 28273 Phone: 815-693-5052 Directions to Facility: I-77 South Exit 1A to Westinghouse Blvd, tum right onto Westinghouse Blvd, drive 1 mile then tum left onto Brookford Street, System Classifications: Primary ORC: Certification: Phone: Secondary ORC(s): On -Site Representative(s): Related Permits: Inspection Date: 08/22/2018 Entry Time: 02:30PM Exit Time: 04:00PM Primary Inspector: James D Moore Phone: Secondary Inspector(s)- Lily C Kay Reason for Inspection: Routine Inspection Type: Technical Assistance Permit Inspection Type: Wholesale Trade of Metal Waste and Scrap Stomtwater Discharge COC Facility Status: Compliant Not Compliant Question Areas: 0 Storm Water (See attachment summary) Page: 1 Permit: NCG200513 Owner - Facility: United Scrap Metal Inc Inspection Date: 08a212018 Inspection Type: Technical Assistance Reason for Visit: Routine Anahrtical Monitoring Has the facility conducted its Analytical monitoring? # Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas? Comment: Analvtical results indicate have exceeded benchmark values for conger and zinc. A "Tiered" Yes No NA WE ❑ ❑ ❑ ❑❑■❑ investigative report by Leaf Environmental was reviewed during the inspection. Additional investigative sampling was recommended during the inspection. 1) gutter sample. 2) non contact rainfall sample. 3) outtall 3 inside the fence and 4) Penske offsite impact sample. Pettnit and Qutfall Yes No NA WE # Is a copy of the Permit and the Certificate of Coverage available at the site? M ❑ ❑ ❑ # Were all outfalls observed during the inspection? ❑ ❑ ❑ # If the facility has representative outfall status, is it properly documented by the Division? 110 ❑ # Has the facility evaluated all illicit (non stormwater) discharges? M ❑ ❑ ❑ Comment: All outfalls were observed , based on future test results, the facility may be a candidate for representative outfall status. Page: 3 permit: NCG200513 owner - Facility: United Scrap Metal Inc Inspection Date: 0812212018 Inspection Type. Technical Assistance Reason for Visit: Routine Inspection Summary: Please email the test results for the recommended investigative sampling when you receive. Thank you for your Tier III Notification. Please call to discuss next steps after the sampling data is submitted. James Moore 704.235.2138. Page: 2 Stormwater "Tiered" Investigative Actions & Site Specific Best Mann ement Practices Stormwater General Permit Certificate of Coverage NCG200513 United Scrap Metal — Charlotte Facility 9925 Brookford Street Charlotte, NC 28273 The United Scrap Metal (USM) — Charlotte facility is currently required to sample stormwater discharges from all outfalls monthly for both copper (Cu) and zinc (Zn). The USM — Charlotte facility discharges stormwater runoff under permit NCG200513, which was issued initially on September 24, 2015 and prior to commencing operations. Review of analytical results thus far (see attached table) indicates the following with respect to Cu and Zn concentrations in stormwater runoff: • Zinc concentrations have not increased substantially since the initial sampling event; • Copper concentrations are on the rise. USM requested both third -party review of site operations and NCDEMLR assistance in an effort to meet stormwater permit benchmarks. On August 2, 2018, Tina Monroe, P.E., of Leaf Environmental & Engineering, P.C., toured the USM — Charlotte facility to assist with a strategy to reduce Cu and Zn concentrations in stormwater (SW) discharges from the site. During the tour of the site, no significant soil erosion or sediment deposits were observed at Outfall 003 or the location where flow from combined Outfalls 001 and 002 discharge into the receiving stream. This document has been completed to highlight recommendations for both additional data gathering activities and some initial Best Management Practices (BMP) designed to assist USM with their compliance efforts as detailed below. Based on future monitoring results, additional investigative activities and/or BMPs may be necessary. Data Gathering: 1. Obtain a sample of rainfall in a clean container, transfer to a laboratory supplied container and submit by chain -of -custody (COC) protocol for total copper and zinc analysis by EPA Method 200.7. Also, obtain the pH of the rainwater sample immediately upon collection and record. 2. Sample stormwater "run-on" that comingles with stormwater runoff from the site prior to discharging from Outfall 003. Off site and up gradient industrial activities includes a truck rental business (see Photographic Log), which provides the potential for tire and brake pad dust that contain up to 1 % zinc and 4% copper respectively. Two such sampling locations are the catch basin and grass lined Swale shown in the attached Photographic Log. Obtain the samples in a laboratory supplied container and submit by COC protocol for total copper and zinc analysis by EPA Method 200.7. 3. Sample two contributing drain pipes that discharge stormwater from the site to Outfall 003 and submit by chain -of -custody (COC) protocol for total copper and zinc analysis by EPA Method 200.7. Both locations are shown in the attached Photographic Log. 4. Review recent records to determine any new raw material customers and/or scrap metals that have the potential to increase exposures to copper or copper containing materials (note the recent increase in stormwater runoff copper concentrations). Initial BMPs• The below BMPs are recommended after the August 2, 2018 facility review and are intended to provide simple, site specific means to control copper and zinc concentrations in stormwater runoff without significant, new capital expenditure. The general BMP list previously submitted to USM should be periodically reviewed prior to facility inspections (ex. galvanized duct work exposed to stormwater that is beginning to show signs of corrosion). 1. Tire dust has the potential to contain up to 1 % zinc and brake pads may contain greater than 4% copper. Sweeping paved surfaces where powered industrial vehicles (PN) and delivery vehicles operated should be a routine activity and include disposal of dust removed, rather than just sweeping to the side of the road. 2. Periodically inspect raw material piles for pressure treated wood. Many of the new chemicals used still contain copper. Also, periodically inspect galvanized duct, fencing, etc. for corrosion and apply zinc —free coating as needed (zinc BMT). Emphasize preventive maintenance of hydraulic systems on PIVs. Hydraulic fluids may contain up to 50 ppm copper_ This includes not only quick repairs, but wiping off residuals from equipment surfaces and storing of the rags in sealed containers. 4. Periodically inspect high traffic areas for motor oil leaks. Motor oils may contain significant concentrations of both copper and zinc (>200 ppm). Consider pressure washing areas with motor oil deposits and capturing the runoff for disposal as a non -hazardous waste. 5. Keep the fuel transfer area clean (see Photographic Log). Even ultra low diesel fuel may contain up to 3 ppm (3600 ppb) copper and zinc. 5. Develop and implement an end of day housekeeping program to reduce exposures to rainfall . metal particles that may be carried away by stormwater. runoff (copper and zinc BAfP). 7. It was noted during the review that a future project may entail excavation to provide more staging area for scrap deliveries. Future grading activities should include a review for the potential to provide 1) increase "sheet" type stormwater runoff and 2) addition of a long and level vegetative strip down gradient of industrial activities, which is constructed with top soil containing peat, compost or optimally, a biochar product generated from sludge (copper and zinc BMP). $. The outside cutting area generates metal particulate available to be carried away by stormwater runoff. Consideration should be given to conducting cutting operations under a metal shelter (roof only) and thus protected from rainfall. Stormwater "run-on," should be diverted around the cutting operation and housekeeping conducted daily (copper and zinc BMP). 9. Drop inlets observed on site were provided with inserts designed to capture particulate. Inserts should be inspected regularly and changed out on a regular basis. During "change out", ensure that any depressed section in the catch basin is free of sediment accumulations (copper and zinc BMP). (Note that the pH of rairrwater has the potential to be less than 6.0, thus even a solid exposed to stormwater runoff in the storm drainage system for an extended period of time may leach metals.) 10. Metal recycling roll -off bins and metal cuttings collection bins are exposed to stormwater. Due to frequent use of the bins, covering with a tarp may not be a workable option, although covering at the end of each wok day should be considered. These bins and surrounding areas should be inspected for housekeeping and contents (ex. housings that contain fluids) on a daily basis. Protection from rainfall should be budgeted as business conditions allow. These recycling collection areas often generate heavy powered industrial vehicle traffic; make inspections for hydraulic fluid and oil leaks a priority (zinc and copper BMP). Stormwater Quantitative Monitoring - Analytical Results (NPDES General Permit COC NCG200513) United Scrap Metal, Inc. 9925 Bmokford Street, Charlotte, NC 28273 Permit Total Chemical Event Sampling Suspended Oxygen Oil & Number Date Solids Demand Grease Copper Lead Zinc (mv) Ong") (mg11) (m911) (m911) (m911) 3 6/15/2016 < 6.2 36.0 56 c0,0131, < 0.0050 Q360 4 11/292016 < 2.5 < 25.0 < 5.0 < 0.0050 < 0.0050 <0.01 5 4/2412017 6.6 < 25.0 < 5.0 0.0098 < 0.0050 0.122 6 12/6/2017 4.6 < 25.0 < 5.0 0.0093 < 0.0050 OA4 Outfall 001 7 6112/2018 20.3 < 25.0 < 5.0 0,0319 < 0.0050 0W7 3 8 7I1612418 �-58.9 10 3 6/15/2016 < 3.2 < 25.0 < 5.3 0.0120 < 0.0050 0:760 4 i112912016 < 2.5 < 25.0 < 5.0 < 0.005 < 0.0050 <0.Oi 5 4/24/2017 ' 6.8 < 25.0 < 5.0 0.010 < 0.0050 0 l 30 6 i 2/612017 5.0 < 25.0 < 5.0 0.0116 < 0.0050 0,510 Outfall 002 7 6/12/2018 11.5 < 25.0 < 5.0 &03 7 < 0,0050 1 8 7/1612018 - 0.0176 ^ 9 10 11 3 6/15/2016 < 2.6 < 25.0 < 5.3 0.0113 < 0.0050 0.708 4 11129/2016 < 2.5 < 25A < 5.0 < 0.005 < 0.0050 <0.01 5 4124/2017 4.2 < 25.0 < 5.0 0.0 i 4 < 0.0050 0.128 6 12/612017 5.3 < 25.0 < 5.0 0.0124 < 0.0050 0:543 Outfail 003 7 61121201E 3B.0 < 25.0 < 5.0 r < 0.0050 . a 711&2018 #11 ,, 0,0132 9 10 11 Benchmark 100 120 15 0.010 0.075 0,126 K.xxx Red text indicates benchmark exceedance triggering "Tier I" requirements. x.X ck; Red text and yellow shading indicates two consecutive benchmark exceedances triggering "Tier H" requirements. +. Red shading indicates four or more benchmark exceedances triggering "Tier III" requirements, which includes NCDEMLR notification. ` try A 46. LLI rye Ln lf s ; N. 4? IV LJ z •` T aM J T� .�& � 4 rye ♦ a aT �' - �i ?��L � �` � 1 _ Y Project No.: 239016 1 USMISPPP w "'ram Sample stormwater• from • c • swale forObtain sample prior to site point source SW • - PHOTOGRAPHICfBrookford Street United Scrap Metal Charlotte, W, � "I- A, 0 1 IS LLI EJ th INS— c?� - LD UJ 5. Clean up residual deposits on equipment and on the ground In fuel transfer areas. Project No.: 239016 T Drawn BY: •f • -f p Y ' ■ j. _�r6. Rental truck business east and up gradient from USM- Tire dust may contain up to 1% Zn. PHOTOGRAPHIC f United Scrap Metal iChadotte, Stormwater "Tiered" Investigative Actions & Site Specific Best Management Practices Stormwater General Permit Certificate of Coverage NCG200513 United Scrap Metal — Charlotte Facility 9925 Brookford Street Charlotte, NC 28273 The United Scrap Metal (USM) — Charlotte facility is currently required to sample stormwater discharges from all outfalls monthly for both copper (Cu) and zinc (Zn). The USM — Charlotte facility discharges stormwater runoff under permit NCG200513, which was issued initially on September 24, 2015 and prior to commencing operations. Review of analytical results thus far (see attached table) indicates the following with respect to Cu and Zn concentrations in stormwater runoff: Zinc concentrations have not increased substantially since the initial sampling event; Copper concentrations are on the rise. USM requested both third party review of site operations and NCDEMLR assistance in an effort to meet stormwater permit benchmarks. On August 2, 2018, Tim Monroe, P.E., of Leaf Environmental & Engineering, P.C., toured the USM — CharIotte facility to assist with a strategy to reduce Cu and Zn concentrations in stormwater (SW) discharges from the site. During the tour of the site, no significant soil erosion or sediment deposits were observed at Outfall 003 or the location where flow from combined Outfalls 001 and 002 discharge into the receiving stream. This document has been completed to highlight'`ieconmendations for both additional data gathering activities and some initial Best Management Practices (BMP) designed to assist USM with their compliance efforts as detailed below. Based on future monitoring results, additional investigative activities and/or BMPs may be necessary. Data Gathering: 1. Obtain a sample of rainfall in a clean container, transfer to a laboratory supplied container and submit by chain -of -custody (COC) protocol for total copper and zinc analysis by EPA Method 200.7. Also, obtain the pH of the rainwater sample immediately upon collection and record. Sample stormwater "run-on" that comingles with stormwater runoff from the site prior to discharging from Outfall 003. Off site and up gradient industrial activities includes a truck rental business (see Photographic Log), which provides the potential for tire and brake pad dust that contain up to 1 % zinc and 4% copper respectively. Two such sampling locations are the catch basin and grass lined swale shown in the attached Photographic Log. Obtain the samples in a laboratory supplied container and submit by COC protocol for total copper and zinc analysis by EPA Method 200.7. 8. The outside cutting area generates metal particulate available to be carried away by stormwater runoff. Consideration should be given to conducting cutting operations under a metal shelter (roof only) and thus protected from rainfall. Stormwater "run-on" should be diverted around the cutting operation and housekeeping conducted daily (copper and zinc BMP). 9. Drop inlets observed on site were provided with inserts designed to capture particulate. Inserts should be inspected regularly and changed out on a regular basis. During "change out", ensure that any depressed section in the catch basin is free of sediment accumulations (copper and zinc BAP). (Note that the pH of rainwater has the potential to be less than 6.0, thus even a solid exposed to stormwater runoff in the storm drainage system for an extended period of time may leach metals.) 10. Metal recycling roll -off bins and metal cuttings collection bins are exposed to stormwater. Due to frequent use of the bins, covering with a tarp may not be a workable option, although covering at the end of each wok day should be considered. These bins and surrounding areas should be inspected for housekeeping and contents (ex. housings that contain fluids) on a daily basis. Protection from rainfall should be budgeted as business conditions allow. These recycling collection areas often generate heavy powered industrial vehicle traffic; make inspections for hydraulic fluid and oil leaks a priority (zinc and copper BMP). 5tormwater Quantitative Monitoring - Analytical Results (NPDES General Permit COG NCG200513) United Scrap Metal, Inc. 9925 Brookford Street, Charlotte, NC 28273 Permit Total Chemical Event Sampling Suspended Oxygen Oil & Number Date Solids Demand Grease Copper Lead Zinc (mg/1) (mg/1) (mgll) (frig/I) (mg/1) (Mg/1) 3 6/15/2016 < 6.2 36.0 66 0.0131 < 0.0050 0.880 4 11/29/2016 < 2.5 < 25.0 < 5.0 < 0,0050 < 0.0050 <0.01 5 4/24/2017 6.6 < 25.0 < 5.0 0.0098 < 0.0050 0.122 6 12/6/2017 4.8 < 25.0 < 5.0 0.0093 < 0.0050 0,485 Outfall 001 7 6/12/2018 20.3 < 25.0 < 5.0 0.0319 < 0.0050 0,739 8 7/16/2018 0.581 10 11 3 6/16/2016 < 3.2 < 25.0 < 5.3 0.0120 < 0.0050 0.760 4 11/2912016 < 2.5 < 25.0 < 5.0 < 0.065 < 0.0050 <O.d1 5 4/24/2017 6.8 < 25.0 < 5.0 0.010 < 0.0050 0.130 6 12/6/2017 5.0 < 25.0 < 5.0 0.0116 < 0.0050 0 510 Outfall 002 7 6/12/2018 11.5 < 25.0 < 5.0 0.0327 < 0.0050 8 7/16/2018 0.0176 9 10 11 3 6115/2016 < 2.6 < 25.0 < 5.3 0,0113 < 0.0050 0.708 4 11129/2016 < 2.5 < 25.0 < 5.0 < 0.005 < 0.0050 <0.01 5 4/24/2017 4.2 < 25.0 < 5.0 0.014 < 0.0050 0.128 6 12/6/2017 5.3 < 25.0 < 5.0 0,0124 < 0.0050 0.543 Outfall 003 7 6/12/2018 38.0 < 25.0 < 5.0 1 < 0.6060 8 7/16/2018 d. 0.0132 9 10 11 Benchmark 100 120 15 0.010 0.075 0.126 x.xxx Red text indicates benchmark exceedance triggering 'Tier l" requirements. k.Xxx Red text and yellow shading indicates two consecutive benchmark exceedances triggering "Tier il" requirements. 'a ": Red shading Indicates four or more benchmark exceedances to enn 'Tier III" !.., 9 99 9 ' requirements, which includes NCDEMLR notification. up t�me.µ � �t'.ti f`y*' •` . '!1 ./� �! � •C� � ��"S'int � �I _ `'{{ I�• �•�,� �'�=�~mot 1 j Ltl •l••�•j!s • �� -�=� 1 1 itil' h�� i 1993r zIrl t Z : 9-1U P.4 It W U Z z wz - w 5wz ZEqIf d w fl 5. Clean up residual deposits on equipment and on the ground in fuel transfer areas. Project No.: 239016 Date: Auq, 2018 Drawn By: " SRG �,; Approved By: File: - E t } USM/SPPP Page: 3 of 3 Notes: t 6. Rental truck business east and up gradient from USM. Tire dust may contain up to 1 % Zn. PHOTOGRAPHIC LOG 9925 Brookford Street United Scrap Metal Charlotte, NC 28273 3. Sample two contributing drain pipes that discharge stormwater from the site to Outfall 003 and submit by chain -of -custody (COC) protocol for total copper and zinc analysis by EPA Method 200.7. Both locations are shown in the attached Photographic Log. 4. Review recent records to determine any new raw material customers and/or scrap metals that have the potential to increase exposures to copper or copper containing materials (note the recent increase in stormwater runoff copper concentrations). Initial BMPs: The below BMPs are recommended after the August 2, 2018 facility review and are intended to provide simple, site specific means to control copper and zinc concentrations in stormwater runoff without significant, new capital expenditure. The general BMP list previously submitted to USM should be periodically reviewed prior to facility inspections (ex. galvanized duct work exposed to stormwater that is beginning to show signs of corrosion). Tire dust has the potential to contain up to 1 % zinc and brake pads may contain greater than 4% copper_ Sweeping paved surfaces where powered industrial vehicles (PIV) and delivery vehicles operated should be a routine activity and include disposal of dust removed, rather thanjust sweeping to the side of the road. 2. Periodically inspect raw material piles for pressure treated wood. Many of the new chemicals used still contain copper. Also, periodically inspect galvanized duct, fencing, etc. for corrosion and apply zinc —free coating as needed (zinc BMP). 3. Emphasize preventive maintenance of hydraulic systems on PIVs. Hydraulic fluids may contain up to 50 ppm copper. This includes not only quick repairs, but wiping off residuals from equipment surfaces and storing of the rags in sealed containers. 4. Periodically inspect high traffic areas for motor oil leaks. Motor oils may contain significant concentrations of both copper and zinc (>200 ppm). Consider pressure washing areas with motor oil deposits and capturing the runoff for disposal as a non -hazardous waste. 5. Keep the fuel transfer area clean (see Photographic Log). Even ultra low diesel fuel may contain up to 3 ppm (3000 ppb) copper and zinc. 6. Develop and implement an end of day housekeeping program to reduce exposures to rainfall metal particles that may be carried away by stormwater runoff (copper and zinc BMP). 7. It was noted during the review that a future project may entail excavation to provide more staging area for scrap deliveries. Future grading activities should include a review for the potential to provide 1) increase "sheet" type stormwater runoff and 2) addition of a long and level vegetative strip down gradient of industrial activities, which is constructed with top soil containing peat, compost or optimally, a biochar product generated from sludge (copper and zinc BMP). January 16, 2019 scra Mik Metal Buyers and Recyclers Mr. James Moore NCDEQ-Regional Office Engineer NC Dept. of Energy, Minerals and Land Resources Mooresville Regional Office 610 East Center Avenue, Suite 301 CERTIFIED MAIL RETURN RECEIPT REQUESTED 7018 0680 0002 2920 0869 -A kl—A Mooresville, NC 28115 o r y .C. RE: General Stormwater Permit Monthly Sampling Event (December 2018)�Q�ti Certificate of Coverage No. NCG200513 9 °y?��r� o Ln 9 `9 Dear Mr. Moore: all- 0- ce With this submittal, the United Scrap Metal — Charlotte Facility is providing the latest nnthly sampling results. Monthly monitoring is currently required for copper and zinc. For the December 2018 sampling event, copper and zinc concentrations in samples from Outfalls 001 and 002 and the zinc concentration in the sample from Outfall 003 were below benchmark concentrations, while the copper concentrations in the sample from Outfall 003 slightly exceeded the benchmark concentration. USM will sample stormwater discharges for copper and zinc during the month of January 2019 from Outfall 003, while continuing BMP efforts to reduce concentrations of those parameters in stormwater discharges from the property. Outfalls 001 & 002 have had three consecutive results below benchmark concentrations for copper and zinc therefore; semi-annual monitoring will resume for those parameters at those two outfalls. Should you have any questions or comments, please do not hesitate to contact me at 804-621-7000 or mobile phone 815-693-5052. Sincerely, UNITED SCRAP METAL, INC. John Dergo General Manager Enclosures cc: - Adam Wilk - USM National Compliance Manager Tim Monroe — Leaf Environmental & Engineering, P.C. Semi-annual Stormwater Discharge Monitoring Report (DMR] for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted CERTIFICATE OF COVERAGE NO. NCG200513 FACILITY NAME United Scrap Metal, Inc. COUNTY Mecklenburg a PERSON COLLECTING SAMPLES John Dergo o. v LABORATORY Pace Analytical Services Inc. Lab Cert. #40 #3771 . -2 z Comments on sample collection or analysis: b o cn 3 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 AMPLE PERIOD or X Monthly' December, 2018 (month) MDISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA z J ❑Zero -flow [—]Watersupply [:]SA G- M ❑Saltwater ®Other C ri N w M PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids Chemical Oxygen Demand Non -polar all & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks ==> - - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L' 0.075 mg/L or 0.210 mg/O 0.126 mg/L or 0.090 mg/L5 Outfall 1 12/14/18 1.22 0.0087 mg/L <0.005 mg/L 0.0889 mg/L Outfall 2 12/14/18 1.22 0.0070 mg/L <0.005 mg/L 0.0928 mg/L outfalf 3 12/14/18 1.22 0.0160 mg/L 0.0055 mg/L 0.0836 mg/L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfalf, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective T55 benchmark applies. s Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If ou report a sample value in excess of the benchmarkyou must implement Tier 1 Tier 2 or Tler 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inchee Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks ===> _ - 15 mg/L 100 mg/L or 50 mg/O Footnotes from Part A also apply to this Part B Note: !f you report a sample value in excess of the benchmark you must impIement Tier 1 Tier 2 or Tier 3 Ms oases. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: James Moore Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results Lr at end of monitoring period in the case of "No Discharge" reports] to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penplties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Perm Permit Date:02/02/2015-12/31/2019 (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 Stormwater Quantitative Monitoring - Analytical Results (NPDES General Permit COC NCG200513) United Scrap Metal, Inc. 9925 Brookford Street, Charlotte, NC 28273 Permit Event Number Sampling Date Total Suspended Solids Chemical Oxygen Demand Oil & Grease Copper Lead Zinc m9 mg mg m9 mg mg 3 6/15/2016 < 6.2 36.0 66 0.0131 < 0.0050 0.880 4 11/29/2016 < 2.5 < 25.0 < 5.6 < 0.0050 < 0.0050 <0.01 5 4/24/2017 6.6 < 25.0 < 5.0 0.0098 < 0.0050 0.122 6 12/6/2017 4.8 < 25.0 < 5.0 0.0093 < 0.0050 0.485 Outfall 001 7 6/12/2018 20.3 < 25.0 < 5.0 0.0319 < 0.0050 0.739 8 7/16/2018 ND 0,581 0.0079 < 0 -- 0.1 03 9 9/17/2018 10 10/11/2018 5.0 ND 11 11/24/2018 0.0071 < 0.0050 0.076 12 12/14/2018 0.0087 <0.0050 0.0889 3 6/15/2016 < 3.2 < 25.0 < 5.3 0.0120 < 0.0050 0.760 4 11/29/2016 < 2.5 < 25.0 < 5.0 < 0.005 < 0.0050 <0.01 5 4/24/2017 6.8 < 25.0 < 5.0 0.010 < 0.0050 0.130 6 12/6/2017 5.0 < 25.0 < 5.0 0.0116 < 0.0050 0.510 Outtall 002 7 6/12/2018 11.5 < 25.0 < 5.0 0.0327 < 0.0050 0 8 7/16/2018 Tu t 0.0176 t 9 9/17/2018 1., s • 10 1 10/11/2018 3.3 ND ND 0.0071 < 0.0050 0.116 11 11/24/2018 0,0053 < 0.0050 0.0482 12 1 12/14/2018 0.0070 <0.0050 0.0928 3 6/15/2016 < 2.6 < 25.0 < 5.3 0.0113 < 0.0050 0.708 4 11 /29/2016 < 2.5 < 25.0 < 5.0 < 0.005 < 0.0050 <0.01 5 4/24/2017 4.2 < 25.0 < 5.0 0.014 < 0.0050 0.128 6 12/6/2017 5.3 < 25.0 < 5.0 0.0124 < 0.0050 0.543 Dutfall003 7 6/12/2018 38.0 < 25.0 < 5.0 ; , ! < 0.0050 1 8 7/16/2018 �; . 11Ia 0.0132 u 0.019 9 q 0 ,. 9 10 9/17/2018 10/11/2018 9.5 35.9 ND 11 11/24/2018 0.0065 e • 0.0055 0.0833 0.0836 12 12/14/2018 Benchmark 1 100 ( 120 15 1 0.010 0.075 1 0.126 x.xxx Red text indicates benchmark exceedance triggering "Tier I" requirements. x.xxx Red text and yellow shading indicates two consecutive benchmark exceedances triggering "Tier II" requirements. Z1�9Red shading indicates four or more benchmark exceedances triggering "Tier Ili" requirements, which includes NCDEMLR notification. lw- Wk screp Metal Buyers and Recyclers February 15, 2019p ,F-P jai �00 CERTIFIED MAIL RETURN RECEIPT REQUESTED `O 7018 0680 0002 2920 2672 Mr. James Moore NCDEQ - Regional Office Engineer NC Dept. of Energy, Minerals and Land Resources Mooresville Regional Office 610 East Center Avenue, Suite 301 Mooresville, NC 28115 RE: General Stormwater Permit Monthly Sampling Event (January 2019) Certificate of Coverage No. NCG200513 Dear Mr. Moore: With this submittal, the United Scrap Metal — Charlotte Facility is providing the latest monthly sampling results. Monthly monitoring is currently required for copper and zinc. For the January 2019 sampling event, analytical results for copper and zinc at Outfall 002 and zinc at Outfall 001 were above benchmark concentrations, which will trigger implementation of Tier I activities for those parameters. Copper concentrations in the sample taken from Outfall 003 were again, slightly above benchmark values and, therefore, monthly monitoring must continue for that parameter. At a minimum, USM will sample stormwater discharges for copper at Outfall 003 during the month of February 2019, while continuing BMP efforts to reduce concentrations of copper and zinc from all outfalls and implement Tier 1 activities for copper and zinc in Drainage Area 2 (Outfall 002) and zinc in Drainage Area l (Outfall 001). Should you have any questions or comments, please do not hesitate to contact me at 804-621-7000 or mobile phone 815-693-5052. Sincerely, UNITED SCRAP METAL, INC. John Dergo General Manager Enclosures CC: Adam Wilk — U.SM National Compliance Manager Tim Monroe — Leaf Environmental & Engineering, P.C. Semi-annual Stormwater Discharge Monitoring Report DMR for North Carolina DFMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted ,2 -/9-19 CERTIFICATE OF COVERAGE No. NCG200513 FACILITY NAME United Scran Metal. Inc. COUNTY Mecklenburg o PERSON COLLECTING SAMPLES John Dergo LABORATORY Pace Analytical Services, Inc. Lab Cert. #40 1 #30 11 a -, Comments on sample collection or analysis:CD m ' b tv O � b n Part A: Stormwater Benchmarks and Monitoring Resti is SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD or X Monthly' January, 2019 (month) +� DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA []Zero -flow ❑Water Supply [:]SA I ❑Saltwater ®Other C PLEASE REMEMBER TO SIGN ON THE REVERSE 4 v ❑ No discharge this period?Z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks =_> _ - 100 mg/L or 50 mg/L4 120 mg/L 15 mg/L 0.010 mg/L or. 0.005 mg/L' 0.075 mg/L or 0.210 mg/L5 0.126 mg/L or 0.090 mg/L' Outfall 1 1/24/19 1.23 0.0061 mg/L <0.0050 mg/L 0.457 mg/L Outfall 2 1/24/19 1.23 0.0130 mg/L <0.0050 mg/L 0.493 mg/L Outfall 3 1/24/19 1.23 0.0136 mg/L <0.0050 mg/L 0.0434 mg/L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they must be reported in the format "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: l you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?Z Outfall Na. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> _ - 15 mg/L 100 mg/L or SO mg/L Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark you must implement Tier 1 Tier 2 or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES® NO ❑ 1F YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: lames Moore Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results tor at end of monitoring period in the case o "No Discharge"' reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permit Date:02/02/2015-12/31/2019 a-,.119-iY (Date) SWU-256, last revised 1/28/2015 Page 2 of 2 wRECEI scra A_V D Metal Buyers and Recyclers �R r 81p19 March 11, 2019 a�NR illp �asd Qua i S �R or v111e Repl, on CERTIFIED MAIL cQ RETURN RECEIPT REQUESTED 7017 0530 0000 4137 0501 Mr. James Moore NCDEQ-Regional Office Engineer NC Dept. of Energy, Minerals and Land Resources Mooresville Regional Office 610 East Center Avenue, Suite 301 Mooresville, NC 28115 RE: General Stormwater Permit Monthly Sampling Event (February 2019) Certificate of Coverage No. NCG200513 Dear Mr. Moore: With this submittal, the United Scrap Metal — Charlotte Facility (USM) is providing the latest monthly sampling results. Monthly monitoring is currently required for copper from Outfall 003. For the February 2019 sampling event, analytical results for copper at Outfall 003 were slightly above benchmark concentrations and have potentially plateaued. At a minimum, USM will sample Outfall 003 for copper during the month of March 2019 along with continuing BMP efforts to reduce concentrations of copper in runoff from Drainage Area 3. Should you have any questions or comments, please do not hesitate to contact me at 804-621- 7000 or mobile phone 815-693-5052. Sincerely, UNITED SCRAP METAL, INC. John Dergo General Manager Enclosures CC_ Adam Wilk-- USMNational Compliance Manager Tim Monroe — Leaf Environmental c& Engineering, P. C. Semi-annual Stormwater Discharge Monitoring Report (DMRJ for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted CERTIFICATE OF COVERAGE NO. NCG200513 FACILITY NAME United Scrap Metal, Inc. COUNTY Mecklenburg PERSON COLLECTING SAMPLES John Derso LABORATORY Pace Analytical Services, Inc. Lab Cert. #40/ #37712 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD or X Monthly" February, 2019 (month] DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero -flow []WaterSupply ❑SA ❑Saltwater ®Other C PLEASE REMEMBER TO SIGN ON THE REVERSE 4 ❑ No discharge this period?z Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, lnches3 Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (SGT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks =_> _ - 100 mg/L or s0 mg/0 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/12 0.075 mg/L or 0.210 mg/LS 0.126 mg/L or 0.090 mg/L5 Outfall1 NA Outfa1[ 2 NA Outfall 3 2/19/19 0.10 0.0133 mg/1 0.0082 mg/L 0.0700 mg/L "Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the sarn ftrameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with V cdegmark here 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a��'II E'9_ th rain e requirement. Qk 4 See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protet t�� S b !hmapplies. s Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. 4u zo o Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL1Aa-detecfi-,44D, her similar non - numerical format. When results are below the applicable limits, they must be reported in the format, "<XX m,g/L", where XX is the n ical value of the detection limit, reporting limit, quantitation limit, etc. in mg/L. Note: If ou report a sample value in excess of the benchmark you must implement Tier 1 Tier 2 or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period: Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, IncheS3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/0 Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark �you _mug implement Tier 1,Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: ^3 • A SfNGI_E BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCE5 IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFACE TRIGGER TIER 2 REQUIREMENTS. .' u � ZU • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO;�' IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ® NO ❑ �4 REGIONAL OFFICE CONTACT NAME: James Moore `� � ca Mail an oriainal and one cony of this DMR, includina all "No Discharae" reports. within 30 days of receipt of the lab results (or at end of monitoring period in the case o "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: I certify, under penalty of taw, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. L am aware that these are signifj;pnt penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 3 f a. -('9 (Date) Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 2 of 2 Stormwater Quantitative Monitoring - Analytical (NPDES General Permit COC NCG200513) United Scrap Metal, Inc. 9925 Brookford Street, Charlotte, NC 28273 Res uls�D MAR 18 2019 Permit Sample Event Number or Monthly Sampling Event (MSE) Sampling Date Total Suspended Solids Chemical Oxygen Demand 11 Oil & Grease L ?yj00 Copper �i;•�;(; 3''d Q, af1i' .3s t'S.fi,E�3; Lean ilal �,r Zinc (Mg/1) (mg/1) (mg/1) (mg/1) (mg/1) (mg/1) 3 6/15/2016 < 6.2 36.0 66 0.0131 < 0.0050 0.880 4 11/29/2016 < 2.5 < 25.0 < 5.0 < 0.0050 < 0.0050 <0.01 5 4/24/2017 6.6 < 25.0 < 5.0 0.0098 < 0.0050 0.122 6 12/6/2017 4.8 < 25.0 < 5.0 0.0093 < 0.0050 0.485 7 6/12/2018 20.3 < 25.0 < 5.0 0.0319 < 0.0050 0.739 MSE 7/16/2018 0.581 1 : " ;. Outfall001 MSE 911712018 8 10/11/2018 5.0 ND ND 0.0079 < 0.0050 0.103 MSE 11/24/2018 0.0071 < 0.0050 ..076 MSE 12/14/2018 0.0087 <0.0050 0.0889 MSE 1/24/2019 0.0061 <0.0050 0.457 3 6/15/2016 < 3.2 < 25.0 < 5.3 0.0120 < 0.0050 0,760 4 11 /29/2016 < 2.5 < 25.0 < 5.0 < 0.005 < 0.0050 <0.01 5 4/24/2017 6.8 < 25.0 < 5.0 0.010 < 0.0050 0.130 6 12/6/2017 5.0 < 25.0 < 5.0 0.0116 < 0.0050 0.510 7 6/12/2018 11.5 < 25.0 < 5.0 0.0327 < 0.0050 e MSE 7/16/2018 0.0176 a ,v Outfall 002 MSE 9/17/2018 21.0 . • a'. , 8 10/11/2018 3.3 ND ND 0.0071 < 0.0050 0.116 MSE 11/24/2018 0.0053 < 0.0050 0,0482 MSE 12/14/2018 0.0070 <0.0050 0.0928 MSE 1/24/2019 0.0130 <0.0050 0.493 3 6/15/2016 < 2.6 < 25.0 < 5.3 0.0113 < 0.0050 0.708 4 11/29/2016 < 2.5 < 25.0 < 5.0 < 0.005 < 0.0050 <0.01 5 4/24/2017 4.2 < 25.0 < 5.0 0.014 < 0.0050 0.128 6 12/6/2017 5.3 < 25.0 < 5.0 0.0124 < 0.0050 0.543 7 6/12/2018 38.0 < 25.0 < 5.0 a 1 < 0.0050 MSE 7/16/2018 0.0132 1 Outfall 003 MSE 9/17/2018 8 10/11/2018 9.5 1 35.9 ND 0.019 a • .. MSE 11/24/2018 1 0.0065 0.D833 MSE 12/14/2018 0.0055 0.0636 MSE 1/24/2019 i <0.0050 0.0434 MSE 211912019 t 0.0082 0.0700 Benchmark 100 120 j 15 0.010 0.075 0.126 x.)= x.)= fir_^ MSE = Monthly Sampling Event Red text indicates benchmark exceedance triggering "Tier I" requirements. Red text and yellow shading indicates two consecutive benchmark exceedances triggering "Tier II" requirements. Red shading indicates four or more benchmark exceedances triggering Tier III" requirements, which includes NCDEMLR notification. December 14, 2018 w 4Mik scra Metal Buyers and Recyciers CERTIFIED MAIL RETURN RECEIPT REQUESTED 7018 0680 0002 2919 4519 Mr. James Moore NCDEQ-Regional Office Engineer NC Dept. of Energy, Minerals and Land Resources Mooresville Regional Office 610 East Center Avenue; Suite 301 Mooresville, NC 28115 RE: General Stormwater Permit Monthly Sampling Event (November 2018). Certificate of Coverage No. NCG200513 Dear Mr. Moore: o 70 0 CD A rn � Zr C r. to 0 co With this submittal, the United Scrap Metal -- Charlotte Facility is providing the latest monthly sampling results. Monthly monitoring is currently required for copper and zinc. For the November 2018 sampling event, copper and zinc concentrations in samples from Outfalls 001 and 002 and the zinc concentration in the sample from Outfall 003 were below benchmark concentrations, while the copper concentrations in the sample from Outfall 003 exceeded the benchmark concentration. USM will sample stormwater discharges for copper and zinc during the month of December while continuing BMP efforts to reduce concentrations of those parameters in stormwater discharges from the property. Should you have any questions or comments, please do not hesitate to contact me at 804-621- 7000 or mobile phone 815-693-5052. Sincerely, UNITED SCRAP METAL, INC. John Dergo General Manager Enclosures cc_ Adam Wilk-- USM National Compliance Manager Tim Monroe — Leaf Environmental & Engineering, P. C. Stormwater Quantitative Monitoring - Analytical Results (NPDES General Permit COC NCG200513) United Scrap Metal, Inc. 9925 Brookford Street, Charlotte, NC 28273 Permit Event Number Sampling Date Total Suspended Solids Chemical Oxygen Demand Oil & Grease Copper Lead Zinc mg) (mg (mg/) (mg mg (mg 3 6/15/2016 < 6.2 36.0 66 0.0131 < 0.0050 E 0.880 4 11 /29/2016 < 2.5 < 25.0 < 5.0 < 0.0050 < 0.0050 <0.01 5 4/24/2017 6.6 < 25.0 < 5.0 0.0098 < 0.0050 0.122 6 12/6/2017 4.8 < 25.0 < 5.0 0.0093 < 0.0050 0.485 Outfall 001 7 6/12/2018 20.3 < 25.0 < 5.0 0.0319 < 0.0050 0.739 8 7/16/2018 0.581 9 9/17/2018 10 10/11/20181 5.0 ND ND 0.0079 < 0,0050 0.103 11 11/24/2018 0.0071 < 0.0050 0.076 12 3 t 6/1512016 < 3.2 25.0 < 5.3 0.0120 < 0.0050 0.760 4 11/29/2016 < 2.5 < 25.0 < 5.0 < 0.005 < 0.0050 <0.01 5 4/24/2017 6.8 < 25.0 < 5.0 0.010 < 0,0050 0.130 6 12/6/2017 5.D < 25.0 < 5.0 0.0116 < 0.0050 0.510 Outfall 002 7 6/12/2018 11.5 < 25.0 < 5.0 0.0327 < 0.005D 8 7/16/2018 - i (v10 .,•r+ �r � ; 0 �� �' o.:, � 0.0176 i,. . ,. �y�al • iry N1J�l�:j/(,r.F , 9 9/17/2018 10 10/11/2018 3.3 ND ND 0.0071 < 0.0050 0.116 11 11/24/2018 0.0053 < 0.0050 0.0482 12 1 1 i 3 6/15/2016 < 2.6 < 25.0 < 5.3 0.0113 < 0.0050 1 0.708 4 11/29/2016 < 2.5 < 25.0 < 5.0 < 0.005 < 0.0050 <0.01 5 4/24/2017 4.2 < 25.0 < 5.0 0.014 < 0.0050 0.128 6 12/6/2017 5.3 < 25.0 < 5.0 0.0124 < 0.0050 0.543 Outfall D03 7 6/12/201 B 38.0 < 25.0 < 5.D ;,(0aJ 3 ?#9 �' a ; i;',��' i;'; i 3P.V;`' ,.` < 0,0050 +�Y 8 7/16/2018 9 10 9/17/2018 10/ 11 /2018 9.5 35.9 N D 0.019 11 11 /24/2018 0.0065 0.0833 12 Benchmark 1 100 120 15 0.010 0.075 1 O.i26 Xxxx Red text indicates benchmark exceedance triggering "Tier I" requirements. Xxxx Red text and yellow shading indicates two consecutive benchmark exceedances triggering "Tier II" requirements. }?_,j;d;, Red shading indicates four or more benchmark exceedances triggering "Tier III" requirements, which includes NCDEMLR notification. Semi-annual Stormwater Discharge_ Monitoring Report (DMRI for North Carolina DEMLR General Permit No. NCG200000 — Scrap Metal Recycling Date submitted (.2 ~ / `(- lf? CERTIFICATE OF COVERAGE No. NCG200513 FACILITY NAME United Scrap Metal, Inc. COUNTY Mecklenburg PERSON COLLECTING SAMPLES Ashley Hamilton � an LABORATORY Pace Analytical Services, Inc. Lab Cert. #40 / #37712 10 Z Comments on sample collection or analysis: b Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 AMPLE PERIOD or X Monthly' November, 2018 (month) c� MISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA �} ❑Zero -flow ❑Water Supply ❑SA r� �. ❑Saltwater ®Other C c.Q 1 PLEASE REMEMBER TO SIGN ON THE REVERSE °° a ❑ No discharge this period:' Outfall Na. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids Chemical Oxygen Demand Non -polar oil & grease EPA Method 1664 (5GT-HEM) Copper, Total Lead, Total Zinc, Total Benchmarks =_> - - 100 mg/L or 50 mg/O 120 mg/L 15 mg/L 0.010 mg/L or 0.005 mg/L5 0.075 mg/L or 0.210 mg/LS 0.126 mg/L or 0.090 mg/LS Outfall 1 11/24/18 0.63 0,0071 mg/L <0.005 mg/L 0.0760 mg/L Outfalf 2 11/24/18 0.63 0.0053 mg/L <0.005 mg/L 0.0482 mg/L Outfall 3 11/24/18 0.63 0.0215 mg/L 0.0065 mg/L 0.0833 mg/L 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit text, Table 3 or Table 4, identifying protected receiving water classifications where the more protective TSS benchmark applies. 5 Stormwater discharges into receiving waters classified as saltwater are subject to the second listed benchmark. Note: Results must be reported in numerical format. For example, do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non - numerical format. When results are below the applicable limits, they_must be reported in the format, "<XX mg/L", where XX is the numerical value ofthe detection limit, reporting limit, quantitation limit, etc. in mg/L. Nate: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2� or Tier 3 responses. See General Permit. Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2013 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, lncheS3 Non -polar O&G by EPA 1664 (SGT-HEM) Total Suspended Solids Benchmarks 15 mg/L 100 mg/L or 50 mg/L Footnotes from Part A also apply to this Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit. FOR PART A AND PART B MONITORING RESULTS: • A SINGLE BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. + TIER 3: HAS YOUR FACILiTY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES® NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE AS REQUIRED BY THE PERMIT? YES ® NO ❑ REGIONAL OFFICE CONTACT NAME: James Moore Mail an original and one coov of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitorina Period in the case o "No Discharge" reports) to: Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27G99-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are ignificant enalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." %a -/- ,c4 [Signature of Per(ittee) ls;p� (Date) Permit Date: 02/02/2015-12/31/2019 SWU-256, last revised 1/28/2015 Page 2of2