HomeMy WebLinkAboutNCG030310_MONITORING INFO_20171127STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
N CC'� D 3
DOC TYPE.
❑ HJ�TORICAL FILE
14�10NITORING REPORTS
DOC DATE
❑ 96) i ll c� I
YYYYMMDD
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Q alit General Permit N6. NCG030000
Date submitted /i 1a1 1-1
OF COVERAGE NO. NCG03 0 3 . / Q SAMPLE COLLECTION YEAR ;�017
VIE oa 51 s4A ly\c. S,' ,e SAMPLE PERIOD ❑ 1an-June EpTuly-Dec
or ❑ Monthly' (month)
LECTI G SAMPLES Doi,, RiRCJ=,J\/F_;E,CSCHARGIN.G TO CLASS DOW E1HQW oTrout
LaabCert.# 497 ❑Zero -flow [:]Watersupply
n sample collection or analysis: N'OV 2 7 2u17 2rOther
C-E6�1�i �EiL FILES
C 'v1 RAL-SECTION E PLEASE REMEMBER TO SIGN ON PAGES 2 AND/I
rmwater Benchmarks and Monitoring Results
No discharge this period?Z
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
-
1.00 mg/L or 50 mg/L4
6.0 — 9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 mg/L
1
1.57
3 `l,S
6.7
N0
N 0
b,005y
RD
C7o.tx�
5
N
FGD
-P
npling (instead of semi-annual) must begin with the second consecutive. benchmark exceedance for the same parameter at the same ou
periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
�cipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge reqL
Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
)rganics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufa(
,stals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained it
elines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semicon
use the definition as found in 40 CFR 4.69.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for ca-
:ture use the definition found in 40 CFf r 469.31).
1/1/2012-10/31/2017 SWU-245, last revised 1(
Page 1 of 3
report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
JD PART B MONITORING RESULTS:
ICHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
EEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS., SEE PERMIT PART II SECTION B.
I: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
;,HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
ICE CONTACT NAME:
x
nal and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitorin
F "No Discharge" reports) to:
ter Quality
-itral Files
rice Center
Carolina 27699-1617
3N THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
!r penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
alified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
there are sig ificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
? mittee) (Dale)
.1/1/2012-10/31/2017
SWU-245, last revised
Page 3 of 3
acmnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: 1
Pace Project No.: 92362698
Sample: 1 Lab ID: 92362698001 Collected: 11/09/17 10:20 Received: 11/09/17 12:05 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
28.1 mg/L
3.4
1
11/10/17 12:35
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L
5.0
1
11/21/17 04:57
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
5.0 ug/L
5.0
1 11/14/17 04:30
11/18/17 04:32 7440-50-8
Lead
ND ug/L
5.0
1 11/14/17 04:30
11/18/17 04:32 7439-92-1
Zinc
53.6 ug/L
10.0
1 11/14/17 04:30
11/18/17 04:32 7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21 /2017 05:55 PM without the written consent of Pace Analytical Services, LLC.
Page 4 of 13
aceAnalytical
www.pacelabs.com
i
ANALYTICAL RESULTS
Project: 1
Pace Project No.: 92362698
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Sample: 1
Lab ID: 92362698002 Collected: 11/09/17 10:30
Received: 11/09/17 12:05 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
34.5 mg/L
4.2
1
11/10/17 12:35
HEM, Oil and Grease
Analyticaf Method: EPA 1664E
Oil and Grease
ND mg/L
5.0
1
11/21/17 04:57
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
ND ug/L
5.0
1
11/14/17 04:30
11/18/17 04:35
7440-50-8
Lead
ND ug/L
5.0
1
11/14/17 04:30
11/18/17 04:35
7439-92-1
Zinc
ND ug/L
10.0
1
11/14/17 04:30
11/18/17 04:35
7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21/2017 05:55 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 13
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Qua ity G neral Permit No. NCG030000
Date submitted 1-7
OF COVERAGE NO. N0003 0 3 _1 Q
VI E N oT 1 S'} zn (- N e4,Au r\, G,o,,- S, �e
S
LECTI G SAMPLES DoiAj, w� vy1tJ�
1( P4c` Ay\c,jvVi�,�l Lab Cert. # 47
n sample collection or analysis:
rmwater Benchmarks and Monitoring Results
SAMPLE COLLECTION EAR d,01
SAMPLE PERIOD Jan -June ❑ July -Dec
or ❑ monthly'_ (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout [
❑Zero -flow ❑Water Supply
[✓Other C- S w
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/i
No discharge this period?'
.
Date Sample
1
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH�
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
100 mg/L or 50 mg/L4
6.0 — 9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 mg/L
s
I_
1.8
ND
ND
a . 02S
MMLIN
vt
D
Q.ozs
npling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the ,same ou
periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmar.k here..:
2cipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge regL
Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. ,
Drganics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufai
,stals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained it
elines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semicon
use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for ca
-ture use the definition found in 40 CFR 469.31).
1/1/2012-10/31/2017 SWU-245, last revised 1(
Page 1 of 3
report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
qD PART B MONITORING RESULTS:
ICHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
EEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO Og--"
i, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
:ICE CONTACT NAME:
hal and one copy of this DMR, including all "No Discharge"reports, within 30 days of receipt of t'he lab results (or at end of monitorin
f "No Discharge" reports) to:
ter Quality
ntral Files
/ice Center
Carolina 27699-1617
'aN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
�r penalty of law, that this document and;all attachments were prepared under my direction or supervision in accordance with a system designed to
alified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
t there'are'sig'nificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
P ittee) (Date)
.1/1/2012-10/31/2017 SWU-245, last revised D
Page 3 of 3
aceAnalytical
www.pacelabs.com
i
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: 20226
Pace Project No.: 92338136
Sample: 1
Lab ID: 92338136001 Collected: 04/24/17 11:40
Received: 04/24/17 12:53 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
17.1 mg/L
3.1
1
04/25/17 15:24
HEM, Off and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L
5.0
1
05/02/17 07:23
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
ND ug/L
5.0
1
04/26/1710:25
04/27/1716:58
7440-50-8
Lead
ND ug/L
5.0
1
04/26/1710:25
04/27/1716:58
7439-92-1
Zinc
24.6 ug/L
10.0
1
04/26/1710:25
04/27/1716:58
7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/04/2017 03:19 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 15
aceAnalytical
www.pacelab&com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: 20226
Pace Project No.: 92338136
Sample: 2 Lab ID: 92338136002 Collected: 04/24/17 11:55 Received: 04/24/17 12:53 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
21.9 mg/L
3.7
1
04/26/17 09:20
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L
5.0
1
05/02/17 07:24
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA 200.7
Copper
ND ug/L
5.0
1 04/26/17 10:25
05/02/17 21:30 7440-50-8
Lead
ND ug/L
5.0
1 04/26/17 10:25
05/02/17 21:30 7439-92-1
Zinc
24.6 ug/L
10.0
1 04/26/17 10:25
05/02/17 21:30 7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/04/2017 03:19 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 15
L
aceAnalytical
www pacelabsxom
Project: 1 & 2
Pace Project No.: 92324822
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
�f C G-- o f (919)834-4984
ANALYTICAL RESULTS
Sample: 1
Lab ID: 92324822001 Collected: 12/29/16 09:30
Received: 12/29/16 11:06 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
28.6 mg/L
2.9
1
01/04/17 09:44
HEM, Oil and Grease
Analytical Method: EPA 16646
Oil and Grease
ND mg/L
5.0
1
01/03/17 06:30
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
ND ug/L
5.0
1
01/04/1719:30
01/05/1719:26
7440-50-8
Lead
ND ug/L
5.0
1
01/04/1719:30
01/05/1719:26
7439-92-1
Zinc
45.2 ug/L
10.0
1
01/04/1719:30
01/05/1719:26
7440-66-6
9040 pH
Analytical Method: EPA 9040
pH
5.3 Sid. Units
0.10
1
01/04/17 10:40
H6
Date: 01/06/2017 04:16 PM
RECEIVE®
JAN 23'2017
CENTRAL FILES
DwR SECTION
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 14
aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: 1 & 2
Pace Project No.: 92324822
Sample: 2 Lab ID: 92324822002 Collected: 12/29/16 09:45 Received: 12/29/16 11:06 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
11.7 mg/L
2.5
1
01/04/17 09:44
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L
5.0
1
01/03/17 06:30
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA 200.7
Copper
ND ug/L
5.0
1 01/04/1719:30
01105/1719:29 7440-50-8
Lead
ND ug/L
5.0
1 01/04/1719:30
01/05/1719:29 7439-92-1
Zinc
48.0 ug/L
10.0
1 01/04/1719:30
01105/1719:29 7440-66-6
9040 pH
Analytical Method: EPA 9040
pH
5.3 Std. Units
0.10
1
01/04/17 10:40 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
)F COVERAGE NO. NCG03 O 3 I 0
IE Hoc, 61 4� TnL Nf�a,, Gsvve. S,�e
� j�vN p
ECTIMG SAMPLES Dov_,
_ Pr-f- Av\r,INV,«,l Lab Cert. # (9 i
sample collection or analysis:
mwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 0, Q ,t r�',
SAMPLE PERIOD ❑ Jan -June Mmy-Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout
❑Zero -flow [:]Watersupply
[]Other C. S k,
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/C
[] No discharge this period?'
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
=>
_
100 m"�g/LL or 50 mJg/L4
6.0(- 9.0
0.007 mg/L
0.033 mg/L
mg/L
1�5fmg/L
7 p
y-
6/ 3, 10 Y✓,.C_l
LJ;
1���
d \
y0.067
0 , 0 �'p.� tKc [
1 �1 lD
^ 1
rp
•
'
pling (instead of semi-annual) must be with the second consecutive benchmark exceedance for the same parameter at the same out
periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
:ipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requi
'ermit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
rganics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufac-
tals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in
lines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semicond
se the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for catl
ure use the definition found in 40 CFR 469.31).
11/2012-10/31/2017 SWU-245, last revised 10i
Page 1 of 3
?port a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
PART B MONITORING RESULTS:
:HMARK E_XCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
-DANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B
HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE'OUTFALL? YES ❑ NO l/
HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ -
=E CONTACT NAME:
al and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring
"No Discharge" reports) to:
�r Quality
:ral Files
:e Center
.arolina 27699-1617
V THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
lified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
irectly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
:here are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
�mittee) (Dade)
./1/2012-10/31/2017 SWU-245, last revised 10,
Page 3 of 3
i � o
1--, ',-lGaceAnalytical
www.pacelabs.coni
i
----
6701 Conference Drive
Raleigh, NC 27607
(919)634-4984
ANALYTICAL RESULTS
Project: 1 & 2
Pace Project No.: 92324822
Sample: 1 Lab ID: 92324822001 Collected: 12/29/16 09:30 Received: 12/29/16 11:06 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Total Suspended Solids
HEM, Oil and Grease
Oil and Grease
200.7 MET ICP
Copper
Lead
Zinc
9040 pH
pH
Analytical Method: SM 2540D
28.6 mg/L
2.9
1
01/04/17 09:44
Analytical Method: EPA 1664E
ND mg/L
5.0
1
01/03/17 06:30
Analytical Method: EPA 200.7 Preparation
Method: EPA 200.7
ND ug/L
5.0
1 01/04/1719:30
01/05/1719:26 7440-50-8
ND uy/L
'3.0
1 01/04/1719:30
01/05/1719:26 7439-92-1
45.2 ug/L
10.0
1 01/04/1719:30
01105/1719:26 7440-66-6
Analytical Method: EPA 9040
5.3 Std. Units
0.10
1
01/04/17 10:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /06/2017 04:16 PM without the written consent of Pace Analytical Services, LLC.
H6
Page 4 of 14
• Pace Analytical Services, LLC
�aceAnalytical 6701 ConferenceDrive7
Raleigh, NC 276760
wvm.pacelabs.com
(919)834-4984
ANALYTICAL RESULTS
Project: 1 & 2
Pace Project No.: 92324822
Sample: 2 Lab ID: 92324822002 Collected: 12/29/16 09:45 Received: 12/29/16 11:06 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
11.7 mg/L
2.5
1
01/04/17 09:44
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L
5.0
1
01/03/17 06:30
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method:
EPA 200.7
Copper
ND ug/L
5.0
1 01104/1719:30
01/05/1719:29 7440-50-8
Lead
ND ug/L
5.0
1 01/04/1719:30
01/05/1719:29 7439-92-1
Zinc
48.0 ug/L
10.0
1 01/04/1719:30
01/05/1719:29 7440-66-6
9040 pH
Analytical Method: EPA 9040
pH
5.3 Std. Units
0.10
1
01/04/17 10:40 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/06/2017 04:16 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14
Semi-annual Stormwater Discharge Monitoring Report
_w - for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted / 1,q //7
OF COVERAGE NO. NCG03 O 3 1 C7
VIE _ Hoc, S hA T-r\(- G.o„e. &, e
S
LECTI G SAMPLES Doy!, Nit oJ
Y Rp{
ice- Ayni@L 4LL t Lab Cert. # V7
n sample collection or analysis:
rmwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 20 I (D
SAMPLE PERIOD ❑ J6n-June my - Dec
or ❑ Monthly' (month)
D RGING TO CLASS ❑ORW ❑HQW ❑Trout
JAN 2 3 2017 ❑Zero -flow [:]Watersupply
[✓'Other C S k.
DVVR CLES
TION PLEASE REMEMBER TO SIGN ON PAGES 2 AND i
CN l
❑ No discharge this period?Z
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Total Suspended Solids
pH,
Standard units
Copper
Lend
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
100 mg/L or 50 mg/L4
6.0 — 9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 mg/L
aC, 14-
o.7
04 . L
S�3
N n
NO
n . O ys I
No
o. -7
1.
npling (instead of semi-annual) must begin with the second consecutive benchmark CeY�ce forthe same parameter at the same ou
periods with no discharge at any single outfall, you must still submit this discharge on re ort with a checkmark here.
ecipitation must be recorded using data from an on -site rain gauge. Unattended sites maibI r aewaiver of the rain gauge reqL
Permit, Table 3 identifying the especially sensitive receiving water classifications where the more' rot��cri e enchmark applies.
Organics sampling is applicable only for those facilities which perform metal finishing operations, manOOff ae :F conductors, manufai
�stals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is th, ktdefinition contained it
elines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 406CFR 433.11; for semicon
use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for ca-
-ture use the definition found in 40 CFR 469.31).
1/1/2012-10/31/2017 SWU-245, last revised 1(
Page 1 of 3
report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
JD PART B MONITORING RESULTS:
ICHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
EEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
4: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO [(/�
HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
:ICE CONTACT NAME:
nal and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitorin
F "No Discharge" reports) to:
ter Quality
-itral Files
rice Center
Carolina 27699-1617
3N THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
�r penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
alified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complet,
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
rmittee)
.1/1/2012-10/31/2017
SWU-245, last revised 1i
Page 3 of 3
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Qu4lity General Permit No. NCG030000��
Date submitted /2
AU _ 9 2n
OF COVERAGE NO. NCG03 -
AE �o� 141 tr C_ NUA01\ G10ve. S-�,e
LECTI G SAMPLES our,, N1eVV\,0VJ
Y Pc.,e- Lab Cert. # i
n sample collection or analysis:
rmwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR AOI � Q�JVr,
SAMPLE PERIOD [t;rJan-June. ❑ July-"Dec?Fltgrj� ri3 elS
or El monthly'
(month)
DISCHARGING TO CLASS ❑ORW . ❑HQW [—]Trout
❑Zero -flow ❑Water Supply
[✓Other
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/t
❑ No discharge this period?2
'
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
==>
_
-
100 mg/L or 50 mg/L4
6.0 — 9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 mg/L
`f /� ►4
.a
33.7
G, S?
NO
NO
O.oA3
ND
iz i4
_
1.z
Ttb
ND
ND
0.oa3
npling (instead of semi-annual) must begin with the second consecutive benchmark exceedanc:e for the same parameter at the same ou
g periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
ecipitation must be recorded using data from an en -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge reqL
I Permit, Table 3 identifying the especially sensitive receiving water classifications where the m,,,re protective benchmark applies.
Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufac
�stals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained it
elines for the facility subject to the requirement to sample (for metal finishing use the definition as foupnd�`n 40 CFR 433.11; for semicon
use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition assJound in 40 CFR 469.22; and for cal
-ture use the definition found in 40 CFR 469.31).
jet
1/1/2012-10/31/2017
SWU-245, last revised 1(
Page 1 of 3
report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
JD PART B MONITORING RESULTS:
ICHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
EEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
4: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ['
HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
ICE CONTACT NAME: "
nal and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt!'of the lab results (or at end of monitorin,
F "No Discharge" reports) to:
r
ter Quality
itral Files
rice Center
Carolina 27699-1617
3N THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
�r penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
alified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
there are significant pens 'es for submitting false information, including the possibility of fines and imprisonment for knowing violations."
�
3ermittee) (Date)
'l/2012-10/31/2017 SWU-245, last revised 11
Page 3 of 3
Results
Attal rcaloz
Home
(formation
293433 Client Project:Sampling 04/12
Pace Project Nbr:92293433
Z293433002 Sample:2
Lab Id:92293433002
Welcome, Doug Niemond.
Give us your feedback here
Change Password Lo4our
Container Orders Results EDDs Data Notifications Resources Help
Project Status:Complete
Matrix:Water
Collected Date:04/12/2016
Received Date:04/12/2016
' MET ICP EPA 200.7 Complete
Oil and Grease EPA 1664B Complete
9t EPA 9040 Complete
D Total Suspended Solids SM 2540D Complete
✓ Method
its Only
)rt Limit, MDL=Method Detection Limit, DF=Dilution Factor, Bas=Basis, Qual=Qualifiers
esc
rs
Total Suspended
48.0
mg/L
4.5
4.5
1
04/14/2016 11:18
NA
Solids
B
Oil and Grease
ND
mg/L
5.0
1.1
1
04/26/2016 08:03
NA
7
Zinc
23.3
ug/L
10.0
2.5
1
04/20/2016 21:55
NA
7
Lead
ND
ug/L
5.0
2.5
1
04/20/2016 21:55
NA
7
Copper
ND
ug/L
5.0
2.5
1
04/20/2016 21:55
NA
pH
7.0
Std. Units
0.10
0.10
1
04/14/2016 13:55
NA
Date
M
: List
c Fnunri
Nabs.conVClientPortal/mrc/sarrpleDetails/modelAndVieud. projectlD=92293433&cl ientPrciect=Sampling %2004/12&projectStatus=Complete&systemlD=lims92&hsn=1707930¤
Results
Analytical
Home
formation
293433 Client Project:Sampling 04/12
Pace Project Nbr:92293433
?293433001 Sample:1
Lab Id:92293433001
Give us your feedback here
Welcome, Doug Niemond. Chance Password Lo out
Container Orders Results EDDs Data Notifications Resources Help
Project Status:Complete
Matrix:Water
Collected Date:04/12/2016
Received Date:04/12/2016
MET ICP EPA 200.7 Complete
Oil and Grease EPA 1664E Complete
fit EPA 9040 Complete
Total Suspended Solids SM 2540D Complete
w
r Method
its Only
in Limit, MDL=Method Detection Limit, DF=Dilution Factor, Bas=Basis, Qual=Qualifiers
esc
Total Suspended
33.7
mg/L
4.2
4.2
1
04/14/2016 11:15
NA
Solids
Oil and Grease
ND
mg/L
5.0
1.1
1
04/26/2016 08:03
NA
Lead
ND
ug/L
5.0
2.5
1
04/20/2016 21:52
NA
Copper
ND
ug/L
5.0
2.5
1
04/20/2016 21:52
NA
Zinc
22.6
ug/L
10.0
2.5
1
04/20/2016 21:52
NA
pH
6.8
Std. Units
0.10
0.10
1
04/14/2016 13:55
NA
Date
List
� Fr,iinrl
Nabs.conYClientPorta/n-wJsampleDetails/modelAndView?projectlD=92293433&clientProject=Sarr#ing%2004/12&projectStatus=Corr>plete&systemlD=lims92&hsrr=1707925¤
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 7 31 1 44
OF COVERAGE NO. NCG03 O 3 1 0
Ll
VIE rlP_ 51 c�� lhNf4,iw. Grove. S-' e
n
LECTI G SAMPLES Dour.,
Y Pam« Ancj:4V 1 Lab Cert. # 67
n sample collection or analysis:
rmwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR _ a (' I L
SAMPLE PERIOD ❑ Jan -June FWJt ly-Dec
or ❑ Monthly" (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout [
❑Zero -flow ❑Water Supply
RECEIVED ED ['Other c. Sit,*
JAN O 2406 REMEMBER TO SIGN ON PAGES 2 AND/
CENTRAL FILES
DWR SECTION
No discharge this period?Z
'
Date Sample
Collected"
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
==>
-
-
100 mg/L or 50 mg/L4
6.0 — 9.0
0.007 mg/L
0.033 mg/L
0.067 mg/L
15 mg/L
l
a I
41, 4
7.7
0.00i
ND
v.o 7
ND
O,4
ti
od
ND
O. oal-
NO
-npling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same oL
g periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
ecipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge regi
I Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufa
fstals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained ii
elines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semicon
use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for ca
-ture use the definition found in 40 CFR 469.31).
1/1/2012-10/31/2017 SWU-245, last revised
Page 1 of 3
report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
JD PART B MONITORING RESULTS:
ICHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
EEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
t: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑
HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
:ICE CONTACT NAME:
nal and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitorin
F "No Discharge" reports) to:
ter Quality
ntral Files
rice Center
Carolina 27699-1617
.iN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
�r penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
alified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complet,
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
ermittee) (Date)
.1/1/2012-10/31/2017 SWU-245, last revised 11
Page 3 of 3
aceAnalytical
www.pacelabs.corn
December 03, 2014
Mr. Doug Niemond
Hog Slat, Inc.
400 Clinton Street
Newton Grove, NC 28366
RE: Project: Stormwater Nov 2014
Pace Project No.: 92227189
Dear Mr. Niemond:
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Enclosed are the analytical results for sample(s) received by the laboratory on November 25, 2014.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Liamm Carrubba
liamm.carrubba@pacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 1 of 13
aceAnalytical
www.pacelabs.com
Project: Stormwater Nov 2014
Pace Project No.: 92227189
Raleigh Certification IDs
6701 Conference Drive, Raleigh, NC 27607
North Carolina Wastewater Certification M 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification M 357
MrginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification M 356
VrginiaNELAP Certification M 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Page 2 of 13
aceMalXiol
www.pacelabs.com
Project: Stormwater Nov 2014
Pace Project No.: 92227189
Lab ID Sample ID
92227189001 1
92227189002 2
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
SAMPLE ANALYTE COUNT
Method
Analysts
Analyses
Reported
Laboratory
EPA 1664E
CLW
1
PASI-C
EPA 200.7
JMW
3
PASI-A
SM 2540D
RC
1
PASI-R
SM 4500-H+B
LJl
1
PASI-R
EPA 1664E
CLW
1
PASI-C
EPA200.7
JMW
3
PASI-A
SM 2540D
RC
1
PASI-R
SM 4500-H+B
LJI
1
PASI-R
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 13
aceAnalytical
www.pacelabs.cw
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Project: Stormwater Nov 2014
Pace Project No.: 92227189
Sample: 1 Lab ID: 92227189001 Collected: 11/25/14 11:20 Received: 11/25/14 12:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT HEM, TPH
Analytical Method: EPA 1664E
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
12/03/14 08:54
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 2001
Copper
14.5 ug/L
5.0
1 12/01/14 15:15
12/01/14 23:53 7440-50-8
Lead
ND ug/L
5.0
1 12/01/14 15:15
12/01/14 23:53 7439-92-1
Zinc
70.2 ug/L
10.0
1 12/01/14 15:15
12/01/14 23:53 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
42.4 mg/L
10.0
1
11129/14 12:02
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
7.7 Std. Units
1.0
1
12/01/14 15:10 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2014 05:32 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 13
Pace Analytical Services, Inc.
aceAnalytical ® 6701 Conference Drive
Raleigh, NC 27607
www.pacelabs.com
. (919)834-4984
i
ANALYTICAL RESULTS
Project: Stormwater Nov 2014
Pace Project No.: 92227189
Sample: 2 Lab ID: 92227189002 Collected: 11/25/14 11:10 Received: 11/25/14 12:15 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Total Petroleum Hydrocarbons
ND mg/L
5.0
1
12/03/14 08:55
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Copper
18.0 ug/L
5.0
1
12/01/14 15:15
12/01/14 23:56
7440-50-8
Lead
ND ug/L
5.0
1
12/01/14 15:15
12/01/14 23:56
7439-92-1
Zinc
217 ug/L
10.0
1
12/01/14 15:15
12/01/14 23:56
7440-66-6
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
90.4 mg/L
20.0
1
11129/14 12:03
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
7.4 Std. Units
1.0
1
12/01/14 15:10
H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2014 05:32 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 13
aceAnalytical
WWW.paCBi3b5.COR1
Project: Stomtwater Nov 2014
Pace Project No.: 92227189
QC Batch: GCSV/19661
QC Batch Method: EPA 1664E
Associated Lab Samples: 92227189001, 92227189002
METHOD BLANK: 1341673
Associated Lab Samples: 92227189001, 92227189002
Parameter Units
Total Petroleum Hydrocarbons mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 1664E
Analysis Description: 1664 SGT-HEM, TPH
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 12/03/14 08:42
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)634-4984
LABORATORY CONTROL SAMPLE:
1341674
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Total Petroleum Hydrocarbons
mg/L
20 17.5
87
64-132
MATRIX SPIKE SAMPLE:
1341675
35165582001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
I <5.0 20
16.6
81
64-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2014 05:32 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 13
aceAnalytical
www.pacelabscom
i
QUALITY CONTROL DATA
Project: Stormwater Nov 2014
Pace Project No.: 92227189
QC Batch: MPRP/17440 Analysis Method: EPA200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92227189001, 92227189002
METHOD BLANK: 1340459
Associated Lab Samples: 92227189001, 92227189002
Parameter Units
Copper
Lead
Zinc
ug/L
ug/L
ug/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 5.0 12/01/14 22:26
ND 5.0 12/01/14 22:26
ND 10.0 12/01/14 22:26
LABORATORY CONTROL SAMPLE:
1340460
Spike LCS LCS
% Rec
Parameter
Units
Cone. Result % Rec
Limits
Copper
ug/L
500 496 99
85-115
Lead
ug/L
500 486 97
85-115
Zinc
ug/L
500 478 96
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1340461
MS
92227411008 Spike
Parameter Units Result Cone.
Copper ug/L 49.6 500
Lead ug/L 7.2 500
Zinc ug/L 54.1 500
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1340463
MS
92227014001 Spike
Parameter Units Result Cone.
Copper ug/L ND 500
Lead ug/L ND 500
Zinc ug/L 0.065 500
mg/L
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Qualifiers
1340462
MSD
Spike
MS
MSD
MS
MSD
% Rec
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
500
560
560
102
102
70-130
0
500
480
479
94
94
70-130
0
500
522
521
94
93
70-130
0
1340464
MSD
Spike
MS
MSD
MS
MSD
% Rec
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
500
506
512
101
102
70-130
1
500
494
498
99
99
70-130
1
500
549
555
97
98
70-130
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2014 05:32 PM without the written consent of Pace Analytical Services, Inc..
Qua[
Qual
Page 7 of 13
1�;aneAnalyfical
www.pacelabscom
QUALITY CONTROL DATA
Project: Stormwater Nov 2014
Pace Project No.: 92227189
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
QC Batch: RWET/7619
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92227189001, 92227189002
METHOD BLANK: 1340035
Matrix: Water
Associated Lab Samples: 92227189001, 92227189002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids mg/L
ND 2.5 1129/14 11:56
LABORATORY CONTROL SAMPLE: 1340036
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids mg/L
250 210
84 90-110 LO
SAMPLE DUPLICATE: 1340037
92226863001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 6630 6170 7
SAMPLE DUPLICATE: 1340047
92226864001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 104 112 8
Results presented on this page are In the units indicated by the "Units" column except where an attemate unit is presented to the rig" of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2014 05:32 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 13
aceAnalytical
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QUALITY CONTROL DATA
Project: Stormwater Nov 2014
Pace Project No.: 92227189
QC Batch: RWET/7626 Analysis Method: SM 4500-H+B
QC Batch Method: SM 4500-H+B Analysis Description: 4500H+B pH Raleigh
Associated Lab Samples: 92227189001, 92227189002
SAMPLE DUPLICATE: 1340389
92226480001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 8.3 8.3 0 H6
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2014 05:32 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 13
aceAnalytical
w ww.pacelabscom
QUALIFIERS
Project: Stormwater Nov 2014
Pace Project No.: 92227189
DEFINITIONS
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-R Pace Analytical Services - Raleigh
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2014 05:32 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13
ceAnalytical
—pacWa6sc=
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Stormwater Nov 2014
Pace Project No.: 92227189
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)834-4984
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92227189001
1
EPA 1664B
GCSV/19661
92227189002
2
EPA 1664B
GCSV/19661
92227189001
1
EPA 200.7
MPRP/17440 EPA 200.7
92227189002
2
EPA 200.7
MPRP/17440 EPA 200.7
92227189001
1
SM 2540D
RWET/7619
92227189002
2
SM 2540D
RWETf7619
92227189001
1
SM 4500-H+B
RWETf7626
92227189002
2
SM 4500-H+B
RWET11626
Date: 12/03/2014 05:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICP/15718
ICP/15718
Page 11 of 13
Document Name: Sample Condition Upon
Document Revisod: April 04, 2013
,'•:.-PaceArlalytical'
Receipt SCUR
Pa e 1 of 2
Document No.:
Issuing Authorities:
��-a•+c<+MDa aDn+
'
F- L-CS-O 1-r v.02
Pace Asheville Quak Office
Client Name:110%5I UT
Where Received: Huntersyille [] Ashevill` Eden Ralei h
Courier (Circle): - Fed Ex UPS, USPS 4C50�9n Commercial Paco Other
Custody Seal on CooledlBox Present: C]yes no Seals Intact: Oyes ❑ no
Packing Material: 0 Bubble Wrap Bubble Bags None Other
Circle Thermometer Used; IR Gun : 22065387 of Ice: We Blue None [J Samples on foe, cooling process has begun
IR Oun eac 1220853T)1
Temp Correction Factor: Add S tract ► t.A C Data and Initials of p�ereon examining
Corrected Cooler Temp.: t . C 8iologlcal Tlsswe Is Frozen: Yes No tJ1A checo to / es a n�
TemD should be above rreaAr to B°C Gnmmanta*
Chain of Ctistody Present
es ONO
ON/A
1.
Chain of Custody Filled Out
es ONO
❑WA
2.
Chain of Custody Relinquished:
yos ONo
❑NIA
3.
.Sampler Name & St nature on COC:
Yes ONO
❑NIA
4.
Sam les Arrived within Hold Time:
Yee Elmo
OWA
5.
Short Hold Time Anal is' <72hr :
OYes ONO
ONIA
6.
Rush. Turn Around Time Re uested:
Oyes FIN.
t7WA
7.
Sufficient Volume:
es ONO
ONIA
8.
Correct Containers Used:
-Pace Containers Used:
YfY. ONO
4Y. ON.
ONIA
ONiA
9.
Containers Intact:
es ONo
❑WA
10.
Filtered volume.received for Dissolved tests
Oyes ONo
XJNIA
11.
Sample Labels match COO:
-includes date/tlme/ID/Analysis Matri:p
Y, Q►ao
DWA
12.
A8 containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation.
exceptions: VOA, ooCrorm, Toc. ow. wwrto ter)
Yes ONo
OR*
Yes ONO
13111A
OWA
13.
Samples checked for dechlorinatton:
Yes ONO
OWA
-14.
Heads ace In VOA Vials >6mm :
'Dyes ONo
ONIA
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # if urchased):
❑Yea ONO
Ores ONO
NIA
WA
16.
Client Notification! Resolution: Field Data Required? Y / N
Person Contacted: DatefTlme:
Comments/ Resolution:
Note: Whenever there Is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification -Office i I-o out of hold, incorrect preservative, out of temp, 92227189 .
incorrect containers)
Page 12 of 13
aceAnalyilcal "
www-pacelabs.com
6701 Conference Drive, Raleigh, NC 27607
ph: (919) 834-4984, fax: (919) BM-6497
NCVirW Cert U, NCDW Cert#37731
Chain of Custody W.O.# LIM
Report Results To: ^�►
Company: ! i0 S�4� J.tn<.,
Address:.
t3OX 3oti n' c
k V t,,.Av � GI'Ove— N C as-344
Attn:.��►Y1 @�ny0hJ
Phone: 910 - SW-6/37
Fax: �I10 — ,57519 -- 1 fif-
Sampled by (signature):
Bill To: <
`•'k = Project Reference:
• .:Number:
Purchase Order
UR'6andard Report Delivery
■ Rush Report Delivery
"Rush lxoleds are subled to prior eppmwil by
the LiticKetory
Requested Due Date:
i 'J1i0. ,f.., b`�". +•` Tdirt �a-s.11"�y Ft�st T p'�>1 V-.t. �f> >a a r.y `. 3: p> -- W : 3 Y .i 'v Er..;, ;r
a {vy}, +r '.f ,��s�S 3 �1t x� ,f^ ;r f,'` �! � t fit. ti. vac �f i L1
�rv' FSi. "��.fl r�19! i';1 F� e"lY �J v� s•,. tJ wry, #';i^' 5'� rr:�rS t }} �' �4 r
.t� ft }..e �j ,,. t 6� s tea
-Ir tl .'. P.t�f ~� � ...F.?..wee `+..:....1_.� ,! �Rr,4.: l.t.,, .L � ;�! �'` t>'
_ §: t s..: .h N fY,. a� t .:
tTi: e -
L
�f 1•�i
`�iti JI
■��■ t3 W
�vrha;W
Relinquished nature)
Received by n
)N
Date
414Relln
Time
fished by (signature)
Received by (slpature)
Time
Relinquished by (signature)
Received by (signature)
Date
Time
Receipt conditions (LOnly)
❑ 4t2"C ❑ Temp:` °C
Res. Chlorine:
O Absent ❑ Present O nta
Add preseru <2?
Oyes ONO O rda
Base preserv. >12?
❑ Yes ❑ No ❑ rda
2-
Page 13 of 13