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NCG030293_MONITORING INFO_20190204
STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. Iv C,,& 2 q,3 DOC TYPE ❑ ,H15TORICAL FILE MONITORING REPORTS DOC DATE o a6 Q a?-d � YYYYMMDD Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 11/27/18_ CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME CIRCOR (Colfax/IMO Industries, Inc.) PERSON COLLECTING SAMPLES Brandon Huggins, Shield Engineering LABORATORY: _Pace Analytical Services, Inc. Lab Cert. # 12 Comments on sample collection or analysis: Benchmark exceedances for copper and zinc at Outfall 004 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly) November (month) DISCHARGING TO CLASS ❑ORW . ❑HQW []Trout ❑PNA RECEIVED ❑Zero -flow ❑Watersupply ❑SA ®Other: Class C -- Dry Fork Creek FEB 0 4 2019 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL. FILES DWR SECTION No discharge this period Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, tnches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organlc55 Benchmarks ===> _ - 100 mg/L or S0 mg/L 6.0 — 9.0 0.01 mg/L 0.07S mg/L 0.126 mg/L 1S mg/L 1 mg/L SDO 004 11/12/18 1.69 35.3 7.3 0.0248 <0.005 0.133 0.8 <0.4687 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit, Table.3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing.to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, SDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX_mg/L where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?2 Outfall No. Date Sample Coflected (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part S See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 I Note:. If you report a sample value In excess of the benchmark, you must Implement Tier 1, Trer 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTIONS. r TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copy of this DMR Includina all "No Discharge" Marts, within 30 days of receipt of the lab results tar at end of monitoring period In the case of "No Discharge" reports] to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION' FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my Inquiry of the person or persons whd manage the system, or those persons directly responsible forgathering the information, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) Permit Date: 11/1/2012-10/31/2017 . (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 EnvLmninental ollolit y Stormwater Discharge Outfall [SDO] Qualitative Monitoring Report Forguidance on filling out this form, please visit hUps:lldeg.nc.gov/about/divisions/.energy-mineral-land- resources/energy-mineral-land-permits/stormwater-permitsfnndes-industrial-sw#ltab-4 Permit.No.: �C/�—/ 3 / fl /��/�..or Certificate of Coverage No.:. .......... .. Facility Name: Circor Pumps North America, LLC. County: Union Phone No. Inspector: ✓'a flit ' Date of Inspection: IIA Z// Time of Inspection: 1 z : -3O Total Event Precipitation (inches): All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, -I certify that this ryport is accurate and complete to the best of my knowledge: of Permittee or Pagel o f 2 SWU-242, Last modified 07/28/2017 M 1 1. Outfali Description: Outfall No. 004 Structure (pipe, ditch, etc.): Concrete Pipe Receiving Stream: DEy F rk C eek Describe the industrial activities that occur within the outfall drainage area: manufacturing pum,Rs/humping eQuil2ment and specialty fluid handling equipment 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: T h _ 1'—A"L� h �' `+n f 3: , - - Odor: Describe any distinct odors that the discharge may have (Le, smells strongly of oil, .............. weak chlorine odor, etc.): Ale, ln'q- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 � 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended l solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: ' 1 � 3 4 5 7. is there any foam in the stormwater discharge? o Yes ENo S. is there an oil sheen in the stormwater diseharge? o Yes oNo 9. Is there evidence of erosion or deposition at the outfall? o Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SM-242, last modified 07/28/2017 ' Pace Analytical Services, LLC ALrUAe� gf �sg J 9800 Kincey Ave. Suite 100 nalAcal Huntersville, NC 28078 *+TM' C+ (704)8759092 November 26, 2018 Jonathan Hunter . .. ..... .. . ....... ...... . ...... . Colfax Fluid Handling 1710 Airport Road Monroe, NC 28110 RE: Project: Stormwater Pace Project No.: 92407047 Dear Jonathan Hunter: Enclosed are the analytical results for sample(s) received by the laboratory on November 13, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Sarah Graham for Angela Baloni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures .. cc: Melinda Greene, Shield'Engineering .. .... ... . . ..... .. . .... . ...... ... . ..... .. . .... ... REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 27 ace Analocale nrpacebbs.com CERTIFICATIONS Project: Stormwater Pace Project No.: 92407047 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 LouisianalNELAP Certification # LA170028 Florida/NELAP Certification # E87627 _North Carolina Drinking Water Certification #: 37706 . _ Kentucky_ UST. Certification #:_84. North Carolina Field Services Certification #: 5342 VrginiaNELAP Certification#: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certfication #: 40 South Carolina Certification #: 99030001 UrginiaNELAP Certification # 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 27 w�rw.paadahs.can SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kinoey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project. Stormwater Pace Project No.: 92407047 Anatytes Lab ID Sample ID Method Analysts Reported Laboratory 92407047001 SDO04 EPA 1664B JMS 1 PASI-C EPA 608.3 ...... SEM . 29 PASI-C EPA 200.7 Rev 4.4 1994 DS 3 PASI-A EPA625.1 BPJ 58 PAS[-C EPA624.1 SAS 34 PASI-C SM 254OD-2011 MJP 1 PASI-A EPA 9040C SMK 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 27 Pace Analytical Services, LLC CARr3ijlCcica?� • 9800 Kincey Ave. Suite 100 B �i Huntersville, NC 28078 -P+ — (704)875-9092 ANALYTICAL RESULTS Project: Stormwater Pace Project No.: 92407047 Sample: SDO04 Lab ID: 92407047001 Collected: 11/13/18 12:30 Received: 11/13/18 12:55 Matrix: Water Parameters 1664 SGT-H.EM, TPH Total Petroleum Hydrocarbons 608 PCB Pest RVE Aldrin alpha-BHC beta-BHC delta-BHC gamma-BHC (Lindane) Chlordane (Technical) alpha -Chlordane gamma -Chlordane 4,4'-DDD 4,4'-DDE 4.4'-DDT Dieldrin Endosulfan I Endosulfan It Endosulfan sulfate Endrin Endrin aldehyde Heptachlor Heptachlor epoxide PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Toxaphene Surrogates Tetrachloro-m-xylene (S) Decachlombiphenyl (S) 200.7 MET ICP Copper Lead Zinc 625 MSSV Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Date: 11/26/2018 11:44 AM Results Units Report Limit OF Prepared Analyzed CAS No. Qua[ Analytical. Method: EPA 1664B ND mg1L 4.8 1 11/2011804:27 Analytical Method: EPA 608.3 Preparation Method: EPA 608.3 NO uglL 0.050 1 11/14/18 14:37 11/16/18 20:55 309-00-2 ND ug/L 0.050 1 11/14/18 14:37 11/16/18 20:55 319-84-6 NO ug/L 0.050 1 11/14/18 14:37 i l /16118 20:55 319-85-7 NO ug/L 0.050 1 11/14/18 14:37 11/16/18 20:55 319-86-8 NO ug/L 0.050 1 11/1411814:37 1111611820:55 58-89-9 NO uglL 0.50 1 11/14/18 14:37 11/16/18 20:55 57-74-9 NO ug/L 0,050 1 11/14/18 14:37 11/16/18 20:55 5103-74-9 NO ug/L 0.050 1 11/14/18 14:37 11/16118 20:55 5103-74-2 NO ug/L 0.050 1 11/14118 14:37 11/16/18 20:55 72-54-8 NO ug/L 0,050 1 11/14/18 14:37 11/16/18 20:55 72-55-9 NO ug/L 0.050 1 11/14/18 14:37 11/16/18 20:55 50-29-3 ND ug/L 0.050 1 11/14/18 14:37 11/16/18 20:55 6057-1 NO ug]L 0.050 1 11/14/18 14:37 11/16/18 20:55 959-98-8 NO ug/L 0.050 1 11/14/18 14:37 11/16/18 20:55 33213-65-9 NO ug/L 0.050 1 11/1411814:37 11/1611820:55 1031-07-8 NO ug/L 0.050 1 11/14/18 14:37 11/16/18 20:55 72-20-8 NO ug/L 0.050 1 11/14/18 14:37 11/16/18 20:55 7421-93-4 ND ug/L 0.050 1 11/14/18 14:37 11/16/18 20:55 76- 4-8 ND ug/L 0.050 1 11/14/18 14:37 11/16/18 20:55 1024-57-3 NO ug1L 0.50 1 11/14/18 14:37 1111611820:55 12674-11-2 NO ug/L 0.50 1 1111411814:37 11/16/18 20:55 11104-28-2 NO uglL 0.50 1 1111411814:37 11/16/18 20:55 11141-16-5 NO uglL 0.50 1 11/14/18 14:37 11/16/18 20:55 53469-21-9 ND ug/L 0.50 1 11/14/18 14:37 11/16/18 20:55 12672-29-6 ND ug/L 0.50 1 11/14/18 14:37 11/16/18 20:55 11097-69-1 NO ug/L 0.50 1 11/1411814:37 1111611820:55 11096-82-5 NO ug1L 0.50 1 11/1411814:37 11/1611820:55 8001-35-2 79 % 60-140 1 11/14/18 14:37 11/16/18 20:55 877-09-8 63 % 60-140 1 1111411814:37 11/1611820:55 2051-24-3 Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 24.8 ugR 5.0 1 11/14/18 07:03 11/18/18 13:23 7440-50-8 ND ug/L 5.0 1 11/14/18 07:03 11/18/18 13:23 7439-92-1 133 691L 10.0 '1 ' 11/14/18 07:03 11/48/18 13:23 7440-66-6 Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 NO ug/L 4.8 1 11/14/1815:20 1111611819:55 83-32-9 NO ug/L 4.8 1 1111411815:20 11116/1819:55 208-96-8 NO ug/L 4.8 1 1111411815:20 1111611819,55 120-12-7 ND ug/L 4.8 1 11114/1815:20 1111611819:55 56-55-3 ND uglL 4.8 1 11114/1815-20 1111611819:55 50-32-0 ND ug/L 4.8 1 1111411815:20 11/16/1819:55 205-99-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 27 1�qneft4dcal* wwtpaoefeh�mm Project: Stormwater Pace Project No.: 92407047 Sample: SDO04 Pace Analytical Services, LLC 9800 Vincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Lab lb: 92407047001 Collected: 11/13/18 12:30 Received: 11/13/18 12:55 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 625 MSSV .. ......... . . Analytical Method: EPA 625.1 Preparation Method:_ EPA.625.1 .. _ _ Benzo(g,h,i)perylene NO ug/L 4.8 1 1111411815:20 1111611819:55 191-24-2 Benzo(k)fluoranthene ND ug/L 4.8 1 1111411815:20 1111511819:55 207-08-9 4-Bromophenylphenyl ether NO ug/L 4.8 1 11/14/18 15:20 11116M8 19:55 101-55-3 Butylbenzylphthalate NO ug/L 4.8 1 11/1411815:20 11/1611819:55 85-68-7 4-Chloro-3-methylphenol NO ug/L 4.8 1 11/1411815:20 11/16/1819:55 59-50-7 bis(2-Chloroethoxy)methane ND ug/L 9.5 1 11/1411815:20 11116/1819:55 111-91-1 bis(2-Chloroethyl)ether NO ug/L 4.8 1 11/1411815:20 11/16/18 19:55 1i1 A�4 to 2-Chloronaphthalene NO ug/L 4.8 1 11/1411815:20 11116/1819:55 91-58-7 2-Chlorophenol NO ug/L 4.8 1 1111411815,20 1111611819:55 95-57-8 4-Chtorophenylphenyl ether ND ug/L 4.8 1 11/14/18 15:20 11/16/18 19:55 7005-72-3 Chrysene ND ug/L 4.8 1 11/14118 15:20 11/16/18 19:55 211 -01-9 Dibenz(a,h)anthracene ND ug/L 4.8 1 11/1411815:20 11/1611819:55 53-70-3 3,3'-Dichlorobenzidine ND ug/L 23.8 1 11/1411815:20 11116/1819:55 91-94-1 2,4-Dichiorophenol ND ugJL 4.8 1 11/14/1815:20 1i11611819:55 120-83-2 Diethyiphthalate NO ug/L. 4.8 1 11114/1815:20 11116/1819:55 84-66-2 2,4-Dimethytphenol ND ug/L 9.5 1 11114/1815:20 11/1611819:55 105-67-9 Dimethylphthalate NO ug/L 4.8 1 11/14/1815:20 11/1611819:55 131-11-3 DFn-butylphthalate NO ug/L 4.8 1 1111411815:20 11116/1819:55 84-74-2 4,6-Din&-o-2-methytphenol NO ug/L 19.0 1 11/1411815:20 1111611819:55 534-52-1 2,4-Dinilrophenol ND ug/L 47.6 1 11/1411615:20 1111611819:55 51-28-5 2,4-Dinitrotoluene NO uglL 4.8 1 11/14/1815:20 1111611819:55 121-14-2 2,6-Dinitrotoluene ND ug/L 4.8 1 11/14/1815:20 11A611819:55 606-20-2 Di-n-octylphthalate N❑ ug/L 4.8 1 11/14/1815:20 11/16/1819:55 117-84-0 bis(2-Ethylhexyi)phthalate NO ug/L 4.8 1 1111411815:20 11116/1819:55 117-81-7 Fluoranthene ND uglL 4.8 1 11/14/1815:20 11116/1819:55 206-44-0 Fluorene NO ug/L 4.8 1 1111411E 15:20 11/16/18 19:55 86-73-7 Hexachloro-1,3-butadiene ND ug/L 4.8 1 11/1411815:20 11/1611819:55 87-68-3 Hexachlorobenzene ND ug/L 4.8 1 1111411815:20 1111611819:55 118-74-1 Hexachlorocydopentadiene NO ug/L 9.5 1 1111411815:20 1111611819:55 77-47-4 Hexachloroethane NO ug1L 4.8 1 11114/1815:20 11/1611819:55 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 4.8 1 1111411815:20 11/16/1819:55 193-39-5 Isophorone ND ug/L 9.5 1 11/14/1815:20 11/1611819:55 78-59-1 Naphthalene NO uglL 4.8 1 11/14/1815:20 1111611819:55 91-20-3 Nitrobenzene NO ug/L 4.8 1 11/14/1815.20 11/16/1819.55 98-95-3 2-Nitrophenol NO ug/L 4.8 1 1111411815:20 11/1611819:55 88-75-5 4-Nitrophenol NO ug1L 47.6 1 11/1411815:20 11/16/1819:55 100-02-7 N-NitrosodimetWamine NO ug/L 4.8 1 1111411E 15:20 11/16/18 19:55 62-75-9 ... N-Nitroso-di-n-propylamine .... ... NO - - - - ug/L. 4:8 1 ...11114/18 15:20 •11/16/18 19:55 621-64-7 N-Nitrosodiphenylamine ND ug/L 9.5 1 11114/1815:20 11/1611819:55 86-1" 2,2'-Oxybis(1-chlaropropane) NO ug/L 4.8 1 11114/1815:20 11116/1819:55 108-60A Pentachlorophenol ND ug/L 9.5 1 1111411815:20 11/1611819:55 87-86-5 Phenanthrene NO ugA- 4.8 1 1111411815:20 11116/1819:55 85-01-8 Phenol ND uglL 4.8 1 1111411815.20 11/16/1819.55 108-95-2 Pyrene NO ug/L 4.8 1 11/14/1815:20 11116/1819.55 129-00-0 1,2,4-Trichlorobenzene ND uglt 4.8 1 1111411815:20 11/1611819:55 120-82-1 2,4,6-Trichlorophenol ND ug1L 9.5 1 11/1411815:20 1111611819:55 88-06-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 27 Pace Analytical Services, LLC acemalylical • 9800 Kiney Ave. Suite 100 Hunserstille, NC 28078 eww-P com (704)875-9092 ANALYTICAL. RESULTS Project: Stormwater Pace Project No.: 92407047 Sample: SDO04 Lab ID: 92407047001 Collected: 11/13/18 12:30 Received: 11/13/18 12:55 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 625 MS5V Analytical Method: EPA 625.1 Preparation Method: EPA 625 . Surrogates Nitrobenzene-d5 (S) 46 % 10-120 1 11/14/18 15:20 11/16/18 19:55 4165-60-0 2-Fluarobiphenyl (S) 44 % 15-120 1 11/14/18 15:20 11/16/18 19:55 321-60-8 Terphenyf-d14 (S) 48 % 11-131 1 11/14/18 15:20 11/16/18 19:55 1718-51-0 Phenol-d6 (S) 17 % 10-120 1 11/14/18 15:20 11/16/18 19:55 13127-88-3 2-Fluorophenol (S) 22 % 10-120 1 11/14118 1520 11/16/18 19:55 367-12-4 2,4,6-Tribmmophenal (S) 64 % 10-137 1 11/14/18 15:20 11/16/18 19:55 118-79-0 624 Volatile Organics Analytical Method: EPA 624.1 Benzene ND ug/L 2.0 1 11/14/18 04:37 71-43-2 Bromodichloromethane NO ug/L 2.0 1 11/14/18 04:37 75-27-4 Bromoform ND ug/L 2.0 1 11/14/18 04:37 75-25-2 Bromomethane NO ug/L 2.0 1 11/14/18 04:37 74-83-9 Carbon tetrachloride ND ug/L 2.0 1 11/14/18 04:37 56-23-5 Chlorobenzene ND ug/L 2.0 1 11/14/18 04:37 108-90-7 Chloroethane ND ug/L 2.0 1 11/14/18 04:37 75-W3 Chloroform ND ug/L 2.0 1 11/14/18 04:37 67-66-3 Chloromethane ND ug/L 2.0 1 11/14/18 04:37 74-87-3 Dibromochloromethane NO ug/L 2.0 1 11/14/18 04:37 124-48-1 1,2-Dirhlorobenzene ND ug/L 2.0 1 11/14/18 04:37 95-50-1 1,3-Dichlorobenzene NO ug/L 2.0 1 11/14/18 04:37 541-73-1 1,4-Dichlorobenzene ND ug/L 2.0 1 11/14/18 04:37 106-4&7 1,1-Dichioroethane ND ug/L 2.0 1 11/14/18 04:37 75-34,3 1,2-Dichloroethane ND ug1L 2.0 1 11/1411804:37 107-06-2 1,1-Dichloroethene NO ug/L 2.0 1 11/1411804:37 75-35-4 cis-1,2-Dichloroethene ND ug/L 2.0 1 11/14/18 04:37 156-59-2 trans-1,2-Dichlaroethene ND ug/L 2.0 1 11/14/18 04:37 156-60-5 1,2-Dichloropropane ND ugR 2.0 1 11/14/18 04:37 78-87-5 cis-1,3-Dichloropropene ND ug/L 2.0 1 11/14/18 04:37 10061-01-5 trans-1,3-❑ichloropropene ND ug/L 2.0 1 11/14/18 04:37 10061-02-6 Ethylbenzene ND ug1L 2.0 1 11/14/18 04:37 100-41-4 Methylene Chloride NO ug/L 2.0 1 11/14/18 04:37 75-09-2 1,1,2,2-Tetrachloroethane NO ug/L 2.0 1 11/14/18 04:37 79-34-5 Tetrachloroethene ND ug/L 2.0 1 11/14/18 04:37 127-18-4 Toluene NO ug/L 2.0 1 11/14/18 04:37 10"8-3 1,1,1-Trichloroethane N❑ ug/L 2.0 1 11/14/18 04:37 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 1 11/14/18 04:37 79-00-5 Trichloroethene ' ND ug/L 2.0 1, 11/14/18 04:37 ' 79-01=6 Trichlorofluoromethane N❑ ug/L 2.0 1 11/14/18 04:37 75-69-4 Vinyl chloride ND ug/L 2.0 1 11/14/18 04:37 75-01-4 Surrogates 4-Bromofluorobenzene (S) 103 % 70-130 1 11/14/18 04:37 460-00-4 Toluene-d8 (S) 106 % 70-130 1 11/14/18 04:37 2037-26-5 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 11/14/18 04:37 17060-07-0 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 35.3 mg/L 8.3 1 11/16/18 10:47 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 27 cAeAn lyfica Mnv.saam ANALYTICAL RESULTS Pace Analytical Services, I_t.0 98001GnceyAve. Suite 100 Huntersville, NC 28078 (704)876-9092 Project: Stormwater Pace Project No.: 92407047 Sample: S0004 Lab ID: 92407047001 Copected: 11/13/18 12:30 Received: 11/13/18 12:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual ...... 9040 phi ............ ...... Analytical Method: EPA 9040C. _ . , ... .... pH at 25 Degrees C 7.2 Std. Units 0.10 1 11/14/18 16:54 H3 Dale: 11/26/2018 11:44 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 27 (�55'cieAnalj&cale twwPice mcom Project: Stormwater Pace Project No_: 92407047 QC Batch: 443323 QC Batch Method: EPA 1664B Associated Lab Samples: 92407047001 METHOD BLANK: 2432563 Associated Lab Samples: 92407047001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE: 2432564 Parameter Units Total Petroleum Hydrocarbons mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 4.8 11/2011804:18 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 19.2 20.3 105 64-132 MATRIX SPIKE SAMPLE: 2432565 35430948001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 4.8U 19.2 21.8 104 64-132 Results presented on this page are in the units Indicated by the'Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Servioes, LLC. Page 8 of 27 p aceftlylica! rvrpacebbs-mm _(� QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 {704)875r9092 Project: Stormwater Pace Project No.: 92407047 QC Batch: 442146 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples_ 92407047001 METHOD BLANK: 2427252 Matrix: Water Associated Lab Samples: 92407047001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 11118/1812:15 Lead ug/L ND 5.0 1111811812:15 Zinc ug1L ND 10.0 11119/1816:37 LABORATORY CONTROL SAMPLE: 2427253 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper ug1L 500 541 108 85-115 Lead ug1L 500 478 96 85-115 Zinc uglL 500 460 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2427254 2427255 MS MSD 92406661001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Quai Copper ug/L 16.6 500 500 547 552 106 107 70-130 1 Lead ug/L ND 500 500 470 472 94 94 70-130 1 Zinc ug/L 31.2 500 500 486 486 91 91 70-130 0 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2427256 2427257 MS MSD 92407021001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Quai Copper ug/L 76.4 500 500 601 603 105 105 70-130 0 Lead ug/L ND 500 500 470 464 94 93 70-130 1 Zinc ug/L 36.0 500 500 491 486 91 90 70-130 1 Results presented on this page are In the units Indicated by the -UnW column except where an alternate unit is presented to the right of the result `. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 27 tww.pa�tpm QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92407047 QC Batch: 442069 Analysis Method: EPA 624.1 QC Batch Method: EPA 624.1 Analysis Description: 624 MSV Associated Lab Samples: 92407047001 METHOD BLANK: 2426941 Associated Lab Samples: 92407047001 Parameter Units Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers 1, 1. 1 -Trichloroethane ug/L NO 2.0 11114/1802:08 1,1,2,2-Tetrachloroethane uglL NO 2.0 1111411802:08 1,1,2-Trichloroethane ug/L NO 2.0 11/14/18 02:08 1,1-Dichloroethane uglL NO 2.0 11/14/18 02:08 1,1-Dichloroethene ug/L NO 2.0 11/14/18 02:08 1,2-Dichlorobenzene ug/L NO 2.0 11/14/18 02:08 1,2-Dichloroethane ug1L NO 2.0 11/14/18 02:08 1,2-Dichloropropane ug/L NO 2.0 11/14/18 02:08 1,3-Dichlorobenzene uglL NO 2.0 1111411802:08 1,4-Dichlorobenzene ug/L ND 2.0 11/14/18 02:08 Benzene uglL NO 2.0 11/14/18 02:08 Bromodichloromethane uglL NO 2.0 11/14/18 02:08 Bromoform ug/L NO 2.0 11/14/18 02:08 Bromomethane ug1L NO 2.0 11/14/18 02:08 Carbon tetrachloride ug/L NO 2.0 11114/18 02:08 Chlorobenzene ug/L NO 2.0 11/14/18 02:08 Chloroethane ug/L NO 2.0 11/14/18 02:08 Chloroform ug1L NO 2.0 11114/18 02:08 Chloromethane ug/L NO 2.0 11/1411802:08 cis-1,2-Dichloroethene ug/L NO 2.0 11/1411802:08 cis-1,3-Dichloropropene uglL NO 2.0 11/14/1802:08 Dibromochloromethane ug/L Nf) 2.0 11/14/18 02:08 Ethylbenzene uglL NO 2.0 11/14/18 02:08 Methylene Chloride ug/L NO 2.0 11/14/18 02:08 Tetrachloroethene ug/L NO 2.0 11/14/18 02:08 Toluene ug/L ND 2.0 11/14/18 02:08 trans-1,2-Dichloroethene ug/L NO 2.0 11114/1802:08 trans-1,3-Dichioropropene uglL NO 2.0 11/14/18 02:08 Trichloroethene uglL NO 2.0 1 ill 4/18 02:08 Trichlorofluoromethane ugfL NO 2.0 11/14/18 02:08 Vinyl chloride ug/L ND 2.0 11/14/18 02:08 1,2-Dichloroethane-d4(S) % 90 70-130 11/14/18 02:08 4-Brornofluorobertzene (S) % 101 70-130 11/14/18 02:08 Tolue6e-d8 (S) % 107 70-130 11/14/18 02:08. LABORATORY CONTROL SAMPLE: 2426942 Pace Analytical Services, LLG 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 Q04)87&9092 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers 1,1,1-Trichloroethane ug/L 20 18.2 91 70-130 1.1,2,2-Tetrachloroethane ug/L 20 18.2 91 60-140 Results presented on this page are in the units indlcawd by the -UnEta' column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 27 0 Project: Stormwater Pace Project No.: 92407047 LABORATORY CONTROL SAMPLE: 2426942 Parameter Units 1,1,2-Trichloroethane ....... ug/L 1,1-Dichloroethane ug/L 1,1-Dichloroethene ug/L 1,2-Dichlorobenzene ug/L 1,2-Dichloroethane ug/L 1,2-Dichloropropane uglL 1,3-Dichloroberizene ug/L 1,4-❑ihlorobenzene ug/L Benzene ug/L Bromodichloromethane ug/L Bromoform ug/L Bromomethane ug/L Carbon tetrachloride uglL Chlorobenzene ug1L Chloroethane ug/L Chloroform ug/L Chloromethane ug/L cis-1,2-Dichloroethene ug/L cis-1,3-Dichlornpropene ug/L Dibromochloromethane ug/L " Ethylbenzene ug/L Methylene Chloride ug/L Tetrachloroethene ug/L Toluene ug/L trans-1,2-Dirhioroethene ug/L trans-1,3-Dichloropropene ug/L Trichloroethene ug/L Trichlorofluoromethane ug/L Vinyl chloride ug/L 1,2-Dichloraethane-d4 (S) % 4-Bromofluorobenzene (S) % Taluene-d8 (S) % Pace Analytical Services, LLC 9800 Kiincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers .20- ...... 19.7..... 98 70-130...... - .. . .......... 20 19.2 96 70-130 20 18.8 94 50-150 20 18.0 90 65-135 20 18.7 94 49-155 20 19.9 100 35-165 20 17.4 87 70-130 20 17.5 87 65-135 20 19.9 100 65-135 20 17.3 87 65-135 20 14.4 72 70-130 20 11.8 59 15-185 20 18.0 90 70-130 20 18.8 94 65-135 20 17.4 87 40-160 20 16.9 84 70-135 20 13.1 66 1-205 20 19.4 97 68-146 20 19.5 98 25-175 20 17.3 86 70-135 20 18.2 91 60-140 20 18.6 93 60-140 20 18.1 90 70-130 20 18.6 93 70-130 20 19.8 99 70-130 20 19.2 96 50-150 20 20.2 101 65-135 20 18.5 93 50-150 20 18.0 90 5-195 97 70-130 104 70-130 99 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE. 2427400 MS MSD 92406069001 Spike Spike Parameter Units Result Cone. Cone. 1,1;1=Trichloroethane .. . ug/L . ND - - 20 ... 20 1,1,2,2-Tetrachloroethane ug/L ND 20 20 1,1,2-Trichloroethane ug/L ND 20 20 1,1-Dichloroethane ug/L ND 20 20 1,1-Dichloroethene ug/L ND 20 20 1,2-Dichlorobenzene ug/L ND 20 20 1,2-Dichloroethane ug/L ND 20 20 1,2-Dichloropropane uglL ND 20 20 2427401 MS MSD MS MSD % Rec Result Result % Rec % Rec Limits RPD Qual 21.6 - 21.3 .. 108 107 ' 52=162 .. 1 ... .. ..... . 18.8 18.0 94 90 46-157 4 21.7 20.7 108 103 52A 50 5 22.0 21.5 110 108 59-155 2 22.1 21.4 ill 107 1-234 3 19.7 19.0 98 95 18-190 4 20.4 19.8 102 99 49-155 3 21.6 21.0 108 105 1-210 3 Results presented on this page are In the units Indicated by the "Units" column except where an atternate unit is presented to the rigid of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 27 aceAnalytical Wrw.paralabs.com Project: Stormwater Pace Project No.: 92407047 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: Parameter 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Ethylbenzene Methylene Chloride Tetrachloroethene Toluene trans-1 ,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S Toluene-d8 (S) QUALITY CONTROL DATA 2427400 2427401 MS MSD 92406069001 Spike Spike Units Result Conc. Conc. ug/L NO 20 20 ug/L ND 20 20 ug/L ND 20 20 ug/L ND 20 20 ug/L NO 20 20 ug/L NO 20 20 ug/L ND 20 20 uglL ND 20 20 ug/L NO 20 20 ug/L ND 20 20 ug/L NO 20 20 ug/L ND 20 20 ug/L ND 20 20 ug/L NO 20 20 ug/L NO 20 20 uglL NO 20 20 ug/L ND 20 20 ug/L ND 20 20 ug/L NO 20 20 ug/L NO 20 20 ug/L NO 20 20 ug/L ND 20 20 ug/L ND 20 20 ) % Pace Analytical services, LLC 9800 Kincey Ave. Suite 100 , Huntersville, NC 28078 (704)875-9092 MS MSD MS MSD % Rec Result Result % Rec % Rec Limits RPD 19.5 18.4 97 92 59-156 6 19.7 18.5 99 92 18A90 6 23.1 22.3 115 111 37-151 3 19.4 18.6 97 93 35-155 5 15.1 14.3 75 71 45-169 5 10.7 11.1 53 56 1-242 4 21.2 19.9 106 100 70-140 6 21.0 20.0 105 100 37-160 5 20.1 19.4 101 97 14-230 4 18.3 17.9 92 90 51-138 2 14.1 13.7 70 68 1-273 3 22.2 21.4 111 107 45-174 4 21.5 21.3 108 107 1-227 1 18.7 17.6 94 88 53-149 6 20.7 19.7 104 98 37-162 5 20.1 19.7 101 98 1-221 2 20.7 20.2 103 101 64-148 3 21.4 20.8 107 104 47-150 3 22.5 21.4 113 107' 54-156 5 21.0 20.5 105 103 17-183 2 23.5 22.4 117 112 70-157 5 21.6 20.9 108 104 17-181 3 20.3 19.6 102 98 1-251 4 92 88 70-130 100 100 70-130 99 99 70-130 Results presented on this page are in the units indicated by the "Units" catumn except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Qual Page 12 of 27 aceAiWca e w�rrpe�6s.mn Project: Stormwater Pace Project No.: 92407047 QC Batch: 442322 QC Batch Method: EPA 608.3 Associated Lab Samples: 92407047001 METHOD BLANK: 2427962 Associated Lab Samples: 92407047001 QUALITY CONTROL DATA Analysis Method: EPA608.3 Analysis Description: 608 PCB Pest Red Vol Matrix: Water Parameter Units Blank Result Reporting Limit Analyzed 4,4'--DDD ug/L N❑ 0.050 11115/1816-34 4,4'-DDE ug/L ND 0.050 1111511816:34 4,4'-DDT uglL ND 0.050 11115/1816:34 Aldrin ug/L ND 0.050 11/15/18 16:34 alpha-BHC ug/L ND 0.050 11115/1816:34 alpha -Chlordane ug/L ND 0.050 11/1511816:34 beta-BHC ug/L ND 0.050 11/1511816:34 Chlordane (Technical) ug/L ND 0.50 11/15/18 16:34 delta-BHC uglL ND 0.050 11/15/18 16:34 Dieldrin ug/L ND 0.050 1111511816:34 Endosulfan I ug/L ND 0.050 11/15/18 16:34 Endosulfan II ug/L ND 0.050 11/15118 16:34 Endosulfan sulfate ug1L NO 0.050 11/15/18 16:34 4 Endrin ug/L ND 0,050 1111511816:34 1 Endrin aldehyde ug/L ND 0.050 11/15/18 16:34 gamma-BHC (Lindane) ug/L ND 0.050 11/15/18 16:34 gamma -Chlordane ug/L ND 0.050 11/1511816:34 Heptachlor ug/L ND 0.050 11/15/18 16:34 Heptachlor epoxide ug/L ND 0.050 11/15/18 16:34 PCB-1016 (Aroclor 1016) ug1L ND 0.50 11/15/18 16:34 PCB-1221 (Arodor 1221) ug/L ND 0.50 11/15/18 16:34 PCB-1232 (Aroclor 1232) ug/L ND 0.50 11/15118 16:34 PCB-1242 (Aroclor 1242) uglL ND 0.50 11/15/18 16:34 PCB-1248 (Aroclor 1248) ug/L ND 0.50 11/15/18 16:34 PCB-1254 (Arodor 1254) ug/L ND 0.50 11/15/18 16:34 PCB-1260 (Arodor 1260) ug/L ND 0.50 11/15/18 16:34 Taxaphene uglL ND 0.50 11115/1816:34 Decachlorobiphenyi (S) % 108 60-140 11/15/18 16:34 Tetrachloro-nrxylene (S) % 105 60-140 11/15/18 16:34 Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2427963 Spike LCS LCS % Rec Pai rrieler Units � - ...Cone. ...Result "k Rec ... Limits Qualifiers .. ............. . 4,4'-DDD ug1L .25 0.21 85 31-141 4,4'-DDE ug/L .25 0.20 80 30-145 4,4'-DDT ug/L .25 0.21 86 25-160 Alddn ug/L .25 0.21 85 42-140 alpha-BHC ug/L .25 0.22 86 37-140 alpha -Chlordane ug/L .25 0.25 100 45-140 beta-BHC ug/L .25 OA8 72 17-147 Results presented on this page are in the units indicated by the 'Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 27 aceAnalytical' wtrwpaaallabacom Project Stormwater Pace Project No.: 92407047 LABORATORY CONTROL SAMPLE: 2427963 Parameter Units delta-BHC ug/L Dieldrin ug/L Endosulfan I ug/L Endosulfan Il ug1L Endosulfan sulfate ug/L Endrin ug/L Endrin aldehyde ug/L gamma-BHC (Lindane) ug/L gamma -Chlordane ug/L Heptachlor ug/L Heptachlor epoxide ug/L Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % QUALITY CONTROL DATA Spike Conc. LCS Result LCS % Rec % Rec Limits . 25 0,21 82 19-140 .25 0.21 84 36-146 .25 0.23 92 45-153 .25 0.22 87 1-202 25 0.23 91 26-144 .25 0.21 86 30-147 .25 0.24 94 50-150 .25 0.22 88 32-140 .25 0.23 92 45-140 .25 0.23 90 34-140 _25 0.21 86 37-142 108 60-140 103 60-140 Pace Analytical Services, LLC 9800 Kircey Ave. Suite 100 Huntersvdle, NC 28078 (704)875-9092 Qualifiers Results presented an this page are in the units indicated by the "Units" Column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 27 CEAnalAcal. wwwP=bb&c= QUALITY CONTROL DATA Project Stormwater Pace Project No.: 92407047 QC Batch: 442357 Analysis Method: EPA625.1 QC Batch Method: EPA 625A Analysis Description: 625 MSS Associated Lab Samples: 92407047001 METHOD BLANK: 2428134 Matrix: Water Associated Lab Samples: 92407047001 Parameter Units Blank Result Reporting Limit Analyzed Qualifiers 1,2,4-Trichlorobenzene uglL ND 5.0 1111611822:44 2,2'-0xybis(1-chloropropane) uglL NO 5.0 11116/1822:44 2,4,6-Trichlorophenol ug/L ND 10.0 11/16118 22:44 2,4-Dichlorophenol ug/L ND 5.0 i1116118 22:44 2,4-Dimethylphenol ug/L NO 10.0 11/16/18 22:44 2,4-Dinitrophenol ug/L ND 50.0 11/16/18 22:44 2,4-Dinitrotoluene ug1L ND 5.0 11/16/18 22:44 2,6-Dinitrotoluene ug/L NO 5.0 11/161i822:44 2-Chioronaphthalene ug/L NO 5.0 11/16/18 22:44 2-Chlorophenol uglL ND 5.0 1 ill 6118 22:44 2-Nitrophenol uglL ND 5.0 11/16/18 22:44 3,3'-Dichlorobenzidine ug/L NO 25.0 11/16/18 22:44 4,6-Dinitro-2-methylphenol ug/L ND 20.0 11/16/18 22:44 l 4-Bromophenylphenyl ether ug/L ND 5.0 11/16/18 22:44 J 4-Chloro-3-methylphenal ug/L NO 5.0 11/16/18 22:44 4-Chlorophenyiphenyl ether ug/L NO 5.0 11/16/18 22:44 4-Nitrophenof ug1L NO 50.0 11/16/18 22:44 Acenaphthene uglL ND 5.0 11116118 22:44 Acenaphthylene ug/L ND 5.0 11/16/18 22:44 AnthraGene ug/L NO 5.0 11/16/18 22:44 Benzo(a)anthracene ug/L NO 5.0 11/16/18 22:44 Benzo(a)pyrene ug/L ND 5.0 11/16/18 22:44 Benzo(b)fluoranthene ug1L NO 5.0 11/16118 22:44 Senzo(g,h,i)perylene ug1L ND 5.0 11/16/18 22:44 Benzo(k)fluoranthene ug/L NO 5.0 11/16/18 22:44 bis(2-Chloroethoxy)methane ug/L NO 10.0 11/16/18 22:44 bis(2-Chloroethyl) ether ug/L NO 5.0 11/16/18 22:44 bis(2-Ethyfhexyl)phthalate ug/L NO 5.0 1111611822:44 Butylbenzylphthalate ug/L ND 5.0 11/16/18 22:44 Ghrysene ug/L ND 5.0 11/16/18 22:44 Di-n-butylphthalate uglL ND 5.0 11/16/18 22:44 Di-n-octylphthalate uglL ND 5.0 11/16/18 22:44 Dibenz(a,h)anthracene ug/L NO 5.0 11/16/18 22:44 Diethylphthalate ......... ...... . ug/L .. . - - - - - NO - - - - - - - 5.0' 11/16/18 22:44 ..... .. Dimethylphthalate ug/L ND 5.0 11/16/18 22:44 Fluoranthene ug/L ND 5.0 11/16/18 22:44 Fluorene ug/L NO 5.0 11/16/18 22:44 Hexachloro-1,3-butadiene ug/L NO 5.0 11/16/18 22:44 Hexachlorobenzene ug/L NO 5.0 11/16/18 22:44 Hexachlorocyclopentadiene ug/L NO 10.0 1lli6118 22:44 Hexachloroethane ug/L ND 5.0 11/16/18 22:44 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntesriille, NG 28078 (704)875-9092 Results presented on this page are in the units indicated by the -Units" column except where an alternate unit is presented to the right of the resulL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/26/2018 11:44 AM without the written consent of Pare Analytical Services, LLC. Page 15 of 27 Analytical 1e19, l wsrw.pecrlaba.aom QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92407047 METHOD BLANK: 2428134 Associated Lab Samples: 92407047001 Parameter Units Matrix: Water Blank Reporting Result Limit Analyzed ... Qualifiers Indeno(1,2,3-cd)pyrene ug/L ND 5.0 11/16/18 22:44 Isophorone ug/L ND 10.0 11/16/18 22:44 N-Nitroso-di-n-propyiamine ug/L ND 5.0 11/16/18 22:44 N-NiLosodimethylamine ug/L ND 5.0 11/16/18 22:44 N-Nitrosodiphenylamine uglL ND 10.0 11/16/18 22:44 Naphthalene ug/L ND 5.0 11/16/18 22:44 Nitrobenzene ug/L ND 5.0 11/16/18 22:44 Pentachlorophenol ug/L ND 10.0 11/16/18 22:44 Phenanthrene ug/L ND 5.0 11/16/18 22:44 Phenol ug/L ND 5.0 11/16/18 22:44 Pyrene ug/L ND 5.0 11/16/18 22:44 2,4,6-Tribromophenol (S) % 40 10-137 11/16/18 22:44 2-Fluorobiphenyl (S) % 68 15-120 11116/18 22:44 2-Fluorophenol (S) % 30 10-120 11116/18 22:44 Nitrobenzene-d5 (S) % 91 10-120 11/16/18 22:44 Phenol-d6 (S) % 19 10-120 11/16/18 22:44 Terphenyl-d14 (S) % 59 11-131 11/16/18 22:44 LABORATORY CONTROL SAMPLE: Parameter 2428135 Units Spike Conc. LCS Result LCS % Rec % Rec. Limits 1,2,4-Trichlorobenzene ug/L 50 32.2 64 44-142 2,2'-Oxybis(1-chloropropane) ug/L 50 37.9 76 36-166 2,4,6-Trichlorophenol uWL 50 37.0 74 37-144 2,4-Dichlorophenol ug/L 50 35.7 71 39-135 2,4-Dimethylphenol uglL 50 35.7 71 32-120 2,4-Dinitrophenoi ug/L 250 135 54 1-191 2,4-Dinitrotoluene ug/L 50 42.7 85 39-139 2,6-Dinitrotoluene ug/L 50 44.7 89 50-158 2-Chloronaphthalene ug/L 50 36.2 72 60-120 2-Chlorophenol uglL 50 31.1 62 23-134 2-Nitrophenol uglL 50 35.4 71 29-181 3,T-Dichlorobenzidine ug/L 100 72.6 73 1-262 4,6-Dinitro-2-methylphenol ug/L 100 77.3 77 1-181 4-Bromophenylphenyl ether ug1L 50 44.2 88 53-127 4-Chloro-3-methylphenol. uglL 100 64.7 65. 22-147. 4-Chlorophenylphenyl ether uglL 50 39.9 80 25-158 4-Nitrophenol ug/L 250 56.6 23 1-132 Acenaphthene ug/L 50 39.5 79 47-145 Acenaphthylene ug/L 50 39.3 79 33-145 Anthracene ug/L 50 45.8 92 27-133 Benzo(a)anthracene ug/L 50 41.9 84 33-143 Benzo(a)pyrene ug/L 50 43.8 88 17-163 Benzo(b)fluoranthene ug/L 50 46.0 92 24-159 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Qual'Ifiers Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 27 GoAnalocal. wrr+vprsoom QUALITY CONTROL DATA Pate Analytical Services, LLC 9800 Kincey Ave. Suite100 Huntersville, NC 28(178 (704)875-9092 Project: Starmwater Pace Project No.: 92407047 LABORATORY CONTROL SAMPLE: 2428135 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers ... Benzo(g.h.l)perylene..... ... ug/L ....... 50 ...... - 38.5 ...... 77 _ .... 1-219 ..... . . .......... . Benzo(k)fluoranthene ug1L 50 40.8 82 11-162 bis(2-Chloroethoxy)methane ug/L 50 38.0 76 33-184 bis(2-Chloroethyl) ether ug/L 50 35.9 72 12-158 bis(2-Ethyihexyl)phthalate ug/L 50 41.6 83 8-158 Butylbenzylphthaiate ug1L 50 41.2 82 1-152 Chrysene ug/L 50 42.8 86 17-168 Di-n-butylphthalate ugtL 50 39.3 79 1-120 Di-n-octylphthalate ug/L 50 48.4 97 4-146 Dibenz(a,h)anthracene ug/L 50 39.6 79 1-227 Diethylphthalate ugfL 50 36.9 74 1-120 Dimethylphthalate ug/L 50 37.4 75 1-120 Fluoranthene ug/L 50 43.2 86 26-137 Fluorene ug/L 50 41.2 82 59-121 Hexachloro-1,3-butadiene ug1L 50 26.0 52 24-120 Hexachlorobenzene ug/L 50 39.7 79 1-152 Hexachlorocydopentadiene ug/L 50 27.2 54 25-150 Hexachloroethane ugIL 50 26.6 53 40-120 Indeno(1,2,3-cd)pyrene uglL 50 44.5 89 1-171 Isophorone ug/L 50 34.8 70 21-196 N-Nitroso-di-n-propylamine ug/L 50 37.1 74 1-230 N-Nitrosodimethylamine u9A- 50 26.7 53 25-150 N-Nitmsodiphenylamine ug/L 50 43.9 88 25-150 Naphthatene ug]L 50 36.4 73 21-133 Nitrobenzene ug/L 50 37.5 75 35-180 Pentachlorophenol ugfL 100 59.4 59 14-176 Phenanthrene ug/L 50 43.5 87 54-120 Phenol ug/L 50 13.9 28 5-120 Pyrene ug/L 50 43.6 87 52-120 2,4,6-Tribromophenol (S) % 77 10-137 2-Fluorobiphenyl (S) % 72 15-120 2-Fluorophenol(S) % 33 10-120 Nitrobenzene-d5 (S) % 72 10-120 Phenot-d6 (S) % 24 10-120 Terphenyt-d14 (S) % 58 11-131 MATRIX SPIKE SAMPLE: 2428136 _ .......... .. . ........... . ... .92407200601 ... Spike MS ..... MS % Rec... ........ . . .. Parameter Units Result Cone. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/L ND 49 16.9 34 44A42 M1 2,T-Oxybis(I-chloropropane) ug[L ND 49 17.4 35 36-166 M1 2,4,6-Trichlorophenol ugfL ND 49 15.9 33 37-144 M1 2,4-Dichlorophenol ug/L ND 49 16.2 33 39-135 M1 2,4-Dimethylphenol ug/L ND 49 10.9 22 32-120 M1 2,4-Dinitrophenol ug/L ND 245 52.9 22 1-191 Results presented on this page are in the units Indicated by the -Unus- column except where an altemate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS TWs report shall not be reproduced, except in fulf, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC, Page 17 of 27 aceAnalytical wrrw.pscale6stx+m QUALITY CONTROL DATA Project: Stormwater Pace Project No_: 92407047 MATRIX SPIKE SAMPLE: 2428136 Pace Analytical Services, LLC 9800 Wincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 92407200001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2,4-Dinitrotoluene uglL ND 49 21.5 44 39-139 2,6-Dinitrotoiuene ug/L ND 49 20.8 42 50-158 M1 2-Chloronaphthalene ug/L ND 49 15.7 32 60-120 M1 2-Chlorophenol ug/L ND 49 45.6 32 23-134 2-Nitrophenol ug/L ND 49 19.1 39 29-182 3,3'-Dichlorobenzidine ug/L ND 98 ND 1 1-262 4,6-Dinetro-2-methytphenol ug/L ND 98 42.9 44 1-181 4-Bromophenylphenyl ether uglL ND 49 21.4 44 53-127 M1 4-Chloro-3-methyiphenol ug[L ND 98 33.4 34 22-147 4-Chlorophenylphenyl ether ug/L ND 49 18.1 37 25-158 4-Nitrophenol ug/L ND 245 30.8J 13 1-132 Acenaphthene ug/L ND 49 17.1 35 47-145 M1 Acenaphthylene ug/L NO 49 16.5 34 33-145 Anthracene ug/L ND 49 24.4 50 27-133 Benzo(a)anthracene ug/L ND 49 24.1 49 33-143 Benzo(a)pyrene ug/L ND 49 23.4 48 17-163 Benzo(b)tluoranthene ug/L ND 49 27.0 55 24-159 Benzo(g,h,i)perylene ug/L ND 49 24A 50 1-219 Senzo(k)fluoranthene ug/L ND 49 23.6 48 11-162 bis(2-Chloroethoxy)methane ug1L ND 49 17.0 35 33-184 bis(2-Chloroethyl) ether ug/L ND 49 15.9 32 12-158 bis(2-Ethylhexyl)phthalate ug/L ND 49 23.7 48 8-158 Butylbenzylphthalate ug/L ND 49 23.1 47 1-152 Chrysene ug/L ND 49 25.7 52 17-168 Di-n-butylphthalate ug/L ND 49 21.4 44 1-120 Di-n-octylphthalate ug/L ND 49 27.2 56 4-146 Dibenz(a,h)anthracene ug1L ND 49 21.6 44 1-227 Diethylphthalate ug/L ND 49 20.8 42 1-120 Dimethylphthalate ug1L N❑ 49 18.6 38 1-120 Fluoranthene ug/L ND 49 23.0 47 26-137 Fluorene ug/L ND 49 19.0 39 59-121 M1 hlexachloro-1,3-butadiene ug/L ND 49 14.9 30 24-120 Hexachlorobenzene ug/L ND 49 20.7 42 1-152 Hexachlorocyclopentadiene ug/L ND 49 11.3 23 25-150 M1 Hexachloroethane ug/L ND 49 13.8 28 40-120 M1 Indeno(1,2,3-cd)pyrene ug1L ND 49 25.1 51 1-171 Isophorone uglL ND 49 15.2 31 21-196 N-Nitroso-di-n-propylarnine ug/L ND 49 15A 31 1-230 N-Nitrosodimethylamine . ug/L . ND... 49 15.0 31 25.150. N-Nhrosodiphenylamine ug/L ND 49 23.8 49 25150 Naphthalene ug/L ND 49 18.1 37 21-133 Nitrobenzene ug/L ND 49 22.8 47 35-180 Pentachlorophenol ug/L ND 98 33.6 34 14-176 Phenanthrene ug/L ND 49 24.5 50 54-120 M1 Phenol ug/L ND 49 7.2 15 5-120 Pyrene ug/L ND 49 26.1 53 52-120 2,4,6-Tribromophenol (S) % 40 10-137 Results presented on this page are in the units Indicated by the -Units- column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 27 4GI'7llRlf�Vul a tt+r WPWslabsmn QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92407047 MATRIX SPIKE SAMPLE: 2428136 9240720000 Parameter Units Result 2-Fiuorobiphenyl (S)............ %. . .... 2-Fluorophenol (S) %Nitrobenzene-d5 (S) %Phenol-d6 (S) %Terpheny1�14 (S) % Pace Analytical Services, LLC MOKincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 1 Spike MS MS % Rec Conc. Result % Rec Limits Qualifiers 31 15-120.................. 17 10-120 34 10-120 12 10-120 28 11-131 SAMPLE DUPLICATE: 2428137 2611497001 Dup Parameter Units Result Result RPD Qualifiers 1,2,4-Trichlorobenzene ug/L ND ND 2,T-0xybis(i-chloropropane) ug/L ND ND 2,4,6-Trichlorophenol ug/L ND ND 2,4-Dichlorophenol ug/L ND ND 2,4-Dimethylphenal ug/L NO ND 2,4-Dinitrophenol ug/L ND ND 2,4-Dinitrotoluene ug/L ND NO 2,6-Dinitrotoiuene ug/L NO ND 2-Chloronaphthalene ug/L ND NO 2-Chlorophenol ug/L ND ND 2-Nitmphenol ug/L NO NO 3,37-Dichlorobenzidine ug/L ND NO 4,6-Dinitro-2-methylphenol ug/L ND NO 4-Bromophenylphenyl ether ug/L ND NO 4-Chloro-3-methylphenol ug/L ND NO 4-Chlorophenylphenyl ether ug/L ND ND 4-Nitrophenol ug/L NO NO Acenaphthene ug/L ND ND Acenaphthylene ug/L ND ND Anthracene ug/L NO ND Benzo(a)anthracene ug/L ND ND Benzo(a)pyrene ug/L ND ND Benzo(b)tluoranthene ug/L ND NO Benzo(g,h,i)perylene ug/L ND NO Benzo(k)tiuoranthene ug/L ND ND bis(2-Chloroethoxy)methane ug/L ND ND bis(2-Chloroethyl) ether ug/L NO NO bis(2-Ethy1hexyl)phthalate ug/L ND ND Butylbenzylphthalate. UA ND. NO Chrysene ug/L NO NO Di-n-butylphthalate ug/L NO NO Di-n-octylphthalate ug/L NO ND Dibenz(a,h)anthracene ug/L ND ND Diethylphthalate ug/L ND ND Dimethylphthalate ug/L ND ND Fluoranthene ug/L NO ND Results presented on this page are in the units Indicated by the 'Units- column except whom an alternate unit ie presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in hull, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 27 aceAnaOcal o w+wpaceiabsmm QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92407047 SAMPLE DUPLICATE: 2428137 Parameter Units 2611497001 Result ❑up Result RPD Qualifiers Fluorene uglL NO NO Hexachloro-1,3-butadiene ug/L NO NO Hexachlorobenzene uglL ND ND Hexachlorocyclopentadiene ug/L NO NO Hexachloroethane uglL NO NO Indeno(1,2,3-cd)pyrene ug1L NO NO Isophorone ug/L NO NO N-Nitroso-di-n-propylamine ug/L NO NO N-Nitrosodimethylamine uglL NO NO N-Nitrosodiphenylamine uglL NO NO Naphthalene ug/L NO ND Nitrobenzene ug/L NO NO Pentachlorophenol ug/L NO NO Phenanthrene ug/L ND NO Phenol ug/L ND NO Pyrene uglL NO NO 2,4,6-Tribromophenol (S) % 36 26 35 2-Fluorobiphenyi (S) % 39 37 6 2-Fluorophenol (S) % 16 15 12 Nitrobenzene-d5 (S) % 50 44 14 Phenol-d6 (S) % 12 11 8 Terphenyi-d14 (S) % 40 26 41 Pace Analytical Services, LLC 9800KinceyAve. Suite100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units Indicated by the 'Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 27 lacieAnalytical' tnew.pawlebsooro QUALITY CONTROL DATA Project: Stormwater Pace Project No.: 92407047 QC Batch: 442811 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92407047001 METHOD BLANK: 2430286 Matrix: Water Associated Lab Samples: 92407047001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 11/16/18 10:42 LABORATORY CONTROL SAMPLE: 2430287 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2430288 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE 2430289 Parameter Units Total Suspended Solids mgA- Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 250 236 94 90-110 92407011001 Dup Result Result RPD Qualifiers ND ND 92407221001 Dup Result Result RPD Qualifiers 31.2 1 30.4 3 ! Resuhs presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the resutL l REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 27 ceAnalidical www.pecffk&L m Project: Stonnwater Pace Project No_: 92407047 QC Batch: 442194 QC Batch Method: EPA 9040C Associated Lab Samples: 92407047001 SAMPLE DUPLICATE. 2427423 Parameter pH at 25 Degrees C SAMPLE DUPLICATE: 2427424 Parameter pH at 25 Degrees C QUALITY CONTROL DATA Analysis Method: EPA 9040C Analysis Description: 9040 pH 92406982001 Dup Units Result Result Std. Units 7.5 7.6 92407140004 Dup Units Result Result Std. Units 6.4 6.4 RPD Qualifiers 0 H3 RPO Qualifiers 0 H3 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 U(14)8759092 Reaults presented an this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the penult. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 27 Pace Analytical Services, LLC Wr.,eArWbaf� 9800 Kincey Ave_ Suite 100 Huntersville. NC 28078 WWWpacewmMm (704)875-9092 QUALIFIERS Project: Stormwater Pace Project No.: 92407047 DEFINITIONS DF - Dilution Factor, i€ reported, represents the factor applied to the reported data due to dilution of the sample aliquot. . ....... N❑ - Not Detected at or above adjusted reporting limit. ..... .......... .. ... . . . . . ............ ..... . TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quentitation Limit. RL - Reporting Limit- The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method B270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matra Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up ` U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyi ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acryionitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte I s ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS \ This report Shall not be reproduced, except in full, Dale: 11/26/2018 11:44 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 27 Pace Analytical Services, LLC C9800 Kincey Ave. Suite 100 B l �caf Huntersville, NC 28078 — (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater Pace Project No.: 92407047 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92407047001 SDO04 EPA1664B 443323 ........... .. .. 92407047001 SDO04 EPA 608.3 .. ... 442322 EPA 608.3 442498 92407047001 SDO04 EPA 200.7 Rev 4.4 1994 442146 EPA 200.7 Rev 4.4 1994 442225 92407047001 SDO04 EPA 625.1 442357 EPA 625.1 442849 92407047001 S0004 EPA624.1 442069 92407047001 SDO04 SM 2540Q-2011 442811 92407047001 SDO04 EPA 9040C 442194 Date: 1112612018 11:44 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 24 of 27 Document Name: Document Revised: February 7, 2018 Sam le Candltion an Rec t(SCEIR) P 1 of 2 Document No.: issuing Authority: (Ana�ytrea!" F-CAR- S-flJ3Rev.06 Pate Carolinas Quality Office Laboratory receivirtg samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville 07 Raleigh[] alent Name: � (�v 9 Project ,4WD' Camier: []Fed Ex UPS ❑LISPS ❑Commercial ,mace []Other 92407047� �� CustadySeat Present?--.. []Yes— -,No- Sealslntact? DYes . .3145...... ' Rate/Initlals Person Emminin= Con Packing Material: []Bubble Wrap �ubble Bags []None :❑ Other BiologicalTissiue Frozen? Thermometer: 92TO45 TwN of ice: �et QBiire ❑N= Dyes oft QN/A EyrR-Gun ID: Cooler Temp ('C): '? _5 Correction Factor Add/Subtract ('Q A i-� Temp should 6e above freezing to fi'[ Cooler Temp Corrected ('C): 3' t []Samples out of temp criteria. Samples an ke, cooling process ' hashegun USDA Regrdated Soll (1j"N/A, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign scorer (Internationally, (`lYes nito iecludhrs Hawaii and Puerto Rico)? ❑Yes ❑No Comments/Disc Chain of Custody Present? Yes No-OWA 1, Samples Arrlmd within hold Time? es ka N/A 2. Sheri Hold Time (<72 hr. 7 Yes E2Nb ❑N/A 3. Rush Turn Around Time Requested? a 090 OWA 4. sufficient Volume? Yes JJNo ❑N/A S. Correct Containers Used? -Pace Comainers Used? gy. of. ONO []NO ❑N/A ❑N/A 6. Cbr%tainersbitact? Na N/A 7. Dissolved inaksb, Samples Field filtered? QVes QNa N/A IL Sample Labels Match_ CQC? , . J -includes Date�menD/Analysis . Matrix: ' V " Yes ONo © QN/A 9. Heads ace in VOA Vials (a5.6mm)7 ©Yea No N/A 20. Trip Blank Present? Trip Blank Custody Seas Present? ❑Yes ❑Yes 26D []N/A /A 12. COMMbi"/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOWICATION/RESOLUnCIN Person contacted: [ ! Project Munger SCURF Review: ` µ f Project Manager SUE Review: Date/Time: Field DateRequired7 []Yes ©No pate: Date: ' t4 _j g Page 25 of 27 o A D -0 w m rn 0 rQ 4 i 3 L, n O i 9, e x e 7 _CL N M M �a S 5 ro � l0 13. � g � N 6 1 R � n C6 f C k l 5 i I l i O � �+ w f+ " I+ ¢ is 07 V 01 V• A W N 1-+ Hamill BP4U•12S mL Plastic Unpreserved (N/A) (Cl-) BP3U-250 r%L Plastic Unpreservmd IN/A) IMU-500 mL Plastic Unpreserved (NIA) BP1U•2 liter Plastic UnRreterved (N/A) I '—" BP4S•125 mL Plastic H2SO4IpH a 2) (Cl-) 8PM-250 mL plastic HNO3 (PH c 2) BP4Z-125 mL PlasticZN Acetate & NaOH (a9) BP4C-1Z5 mL Plastic NBQH IpH > 12) (M) WGFU-Wide-mouthed Glass jar Unpreservods AG1U-11lter Amber Unpreserved (N/A) (CI-) zzzzzz AG1H-1 Cher Amber HCl (pH c 21 AG3U-ZSO mL Amber Unpreserved IN/A) (Cl-) AG15-1 liter Amber HZ504 (pH t 21 AGNS-7SO mL Amber HI504 (pH a 2) AGUIDGMI-250 mL Amber NH4G (N/A)(Cl-) 0G9H40 mL VOA HO (N/A) VG9T-40 mL VOA Na2S203 (N/A) VG9U-40 mL VOA Unp IN/A) D59P•40 mL VOA H3PO4 (N/A) VOAK 16 vials per kit)•5035 kit (NIA) WGK (3 vieh Per k*VPH/Gas kit IN/A) s SPST-125 mL Sterile Plastic (N/A —lab) SPIT-250 ml. Sterile Plastic (N/A —lab) z MA-250 ml Plastic (NHZ)ZSO4 (9.3-9,7) j i AGOU-100 mLAmber Unpresenred vials IN VSGU-20 ml. Scintillation vials IN/A) WSU•40 rnL Amber Unpreserved vials (N/A)f r 3 Mr n O Z. CL 9 07 o ' d x �. SC Co S_ c c d 3 W .8 Cr �a 3 o M Cr Q rL � � n ro Z n� 9 T In m A m R CHAIN -OF -CUSTODY I Analytical Request. Document The Chain -of Custody Is a LEGAL DOCUMENT. All relevant fields must be completed, accurately. Section A Section a section C Required Client Information: Required Project Ifflomilation. Invoice Ikormallon: page: j Of Company. Shield ♦ n Inasr E !Gpw To: Darin t Hafnw Attertiam Addtsts: 4301 IMad-Creels Road Copy To: Company Name; Charlotte, NC 28208 Addrear. I Email: Purchase Order*. Pam Quote: Phone: Fwr. Project Nam: Colfax Fluid HardSIOMV21or Para Project ManaGer anpla.b&Wlabawm �Stzta I Lqm Requested Due Date: I P-!Plw 0: IPWS P[Ofllft 0: 8479.2 NC Raglum"tedd sRI radiffffil.", 4" MAUK COOK ay COLLECTED I Preservatives 1 lkimkkVW&Mr DW W410 I wr walow1j" ww ple"i P SAMPLE ID SWUN.11d OL 00 OL one Character per bcuL WP AR START END hDAM (A.Z 0.9 1 .) Semple Ids cmW I be unique aim, OT 0 IM— - Ts OE TIME DATE TIME 61 1); 3. I 10 .12 r Li I I Ai 6A PRINT Wame of SAMPLER: SIGNATURE at SAMPLER: DATE Signed: OUTUT I?LD ENGINEERING, INC., Noverber 27, 2018 Rich Wallace, Senior Manager, EH&S CIRCOR Pumps North Americd LLC 1710 Airport Road Monroe, North Carolina 28110 Subject: Monthly .Stormwater Sampling .— November 2018 _ ... _ ...... . Certificate of Coverage No. NCGO30293 CIRCOR Pumping Technologies — Monroe, NC Shield Project No. 1150109-02 Dear Mr. Wallace: Shield Engineering, Inc. (Shield) successfully collected a monthly stormwater sample for Stormwater Discharge Outfall (SDO) 9004 at the CIRCOR Pumps North America LLC — Monroe facility for the month of November 2018. The rainfall pH was measured at 73. Total event precipitation was 1.69 inches. In addition to collection of samples, Shield performed Qualitative Monitoring at SDO #004 (attached). Shield has prepared the Stormwater Discharge Monitoring Report (DMR) using the results of analyses from the commercial laboratory that the CIRCOR facility has contracted with and the field values indicated above. The attached DMR should be signed by CIRCOR's authorized representative and then two signed copies of the DMR form should be mailed to the regulatory agency's Central Files. During the November 12, 2018 sampling event, the laboratory measurements of Total Recoverable Copper and Total Recoverable Zinc exceeded the benchmarks with values of 0.0248 mg/L and 0.133 mg/L respectively. Approximately 87% of samples analyzed for Copper since February 2016 have shown benchmark exceedances. However, the percent exceedance for Copper began a downward trend in April of 2017 though spiked in February of 2018. March of 2018 showed a decreased concentration of Copper closer to the benchmark value, but Copper concentration has been on an upward trend to present day. Zinc concentrations have exceeded the benchmark approximately 47% since February 2016. In February 2017 the Zinc benchmark was exceeded with a concentration of 0.0863 mg/L and bordered above and below the benchmark until February of 2018 with an exceeding concentration of 0.198 mg/L. March and April of 2018 showed decreasing concentrations with a slight upwards spike in November 2018. It is important to note that there were no qualifying events from the months of May through October of 2018 and samples could not be collected. Also, effective November 1, 2018, the benchmarks for copper and zinc increased to 0.01 mg/L and 0.126 mg/L respectively. The attached compliance tracking spreadsheet summarizes the analytical results. Please note that Shield began stormwater sampling at the facility in February 2016. Once the facility experiences a rain event that allows Shield to conduct Tier 3 sampling beginning early in the day, Shield will have additional data to evaluate and make recommendations for improvements.in reaching and maintaining benchmark values. Good housekeeping should continue to be routinely emphasized in addition to any further recommendations that Shield will be making following the Tier 3 evaluation. 4301 Taggart Greek Road Telephone 704.394.6913 Charlotte, NC 2820$ www.shieldengineering.cam Fax 704.394.6968 40) CIRCOR remains in Tier Three for Copper and Zinc and remains Tier One for pH. CIRCOR has dropped from Tier Two to Tier One for Total Suspended Solids. Shield will continue to perform monthly sampling per Tier Two requirements until instructed to halt by CIRCOR. Shield greatly appreciates the opportunity to provide environmental services to the CIRCOR. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at (704) 394-6913. Respectfully, SHIELD ENGINEERING, INC. Meli M. Greene Senior Engineer ATTACHMENTS obert L. Griffin, 4PE President/CEO S MELD . /001 CIRCOR v October 5, 2018 Division of Water Quality ATTN: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 CERTIFIED MAIL Subject: August 2018 Stormwater Discharge Monitoring Report (DMR) To Whom It May Concern: Enclosed is the subject DMR for the CIRCOR facility in Monroe, NC. We were unable to collect a monthly sample for Stormwater Discharge Outfall #004 for the month of August. The particulars associated with rainfall events are included in the attached letter dated 9/18/18 from Shield Engineering, Inc. If you have any questions or need additional information, please contact me any time at 704-289-6511, ext. 102620 or by email at rich.wallace@circor.com. Sincerely, �I-1, c_er- Rich Wallace EH&S Manager Industrial 1710 Airport Road I PO Sox 5020 1 Monroe, NC 28110 USA I Tel: +1 704.289.6511 www,eireorpt.com Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 9/18/18 CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME _CIRCOR_(formerly Colf IMO Industries Inc. PERSON COLLECTING SAMPLES NA LABORATORY: NA Lab Cert. # NA Comments on sample collection or analysis: Flo qualifying storm event this month and/or rain events beginning after normal business hours. Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Ian -June ❑ July -Dec or Z Monthly" August, DISCHARGING TO CLASS ❑ORW ❑H.QW []Trout ❑PNA R4,a 11 VV [,.J' I [,.J ❑Zero -flow [—]Water Supply ❑SA 11 ®Other Class C - Dne Fork Greek OCT 2 2 2018 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CEN TRv,L FILES 0:4rR SECTlpiy dNo discharge this period? Outfall No. Date Sample; Collected" (mo/dd/yr) 24•haur rainfall amount, 3 Inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics s Benchmarks ===> _ 100 mg/L or SO mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 1S mg/L 1 mg/L $DO 004 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal Finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed In the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the 5tormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mgjL', where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must Implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Eq No discharge this period? Outfall No. Date Sample Collected' (mo/dd/yr) Z4-hour rainfalt amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L" 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B « See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value In excess of the benchmark, you must Implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FQR PART A AND PART B_MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. a TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL7 YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Me11 an aHain aI and gag-opy—al this DMR i cludin all "No Dischar e" re rts within 30 doXs a receipto the lab results or at end a monitoringeriod . In the case of "No Dlscharae'reports) to: Division of water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS.CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my Inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibillty of fines and imprisonment for knowing violations." (Signature G.J t .. �JQxAv, lytoA t T N Jx-- I Ws//$ (Date) Permit Date: 11/1/2012-10/3V2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Ir *$I—GINEERING, INC. September 18, 2018 Rich Wallace, Senior Manager, EH&S CIRCOR Pumps North America LLC 1710 Airport Road Monroe, North Carolina 28110 Subject: Monthly Stormwater Sampling — August 2018 Certificate of Coverage No. NCG030293 CIRCOR Pumping Technologies — Monroe, NC Shield Project No. 1150109-02 Dear Mr. Wallace: Shield Engineering, Inc. (Shield) was unable to collect a monthly stormwater sample for Stormwater Discharge Outfall (SDO) #004 at the CIRCOR Pumps North America LLC — Monroe facility for the month of August 2018. Measurable rainfall events during the month of August 2018 began on August 1 ", August 18`h, and August 27'h, measuring 0.96 inches, 0.81 inches, and 0.06 inches, respectively. An additional 0.79 inches, 0.29 inches, 0.1.1 inches, 0.22 inches,. 0.20 inches,. 0.16;inches,.0.01 inches, 0.01 inches, 0.46 inches, 0.49-inches, and 1.16 inches. of rainfall weremeasured on August 2"d, August 3d, August 6d', August 7', August 8"', August 10', August T Ph, August.21 ", August 28d', August 3Od% August 31 ".respectively. Each of these events took place on the weekend, after normal business hours, within 72 hours of the last qualifying storm event, or did not produce enough rainfall for discharge. As the seasonal type of storm event is now a high intensity, short duration event, usually commencing in late afternoon through early evening with little to no notice for preparation, Shield will continue to monitor daily weather conditions and attempt to continue coordination of appropriate staff and resources to facilitate adequate sample collection. Per Section 2, Part IV of General Permit No. NCG030000 Shield will attempt to collect a substitute sample and perform a visual assessment during the next qualifying storm event. CIRCOR — Monroe facility should complete all relevant sections on the Stormwater Discharge Monitoring Report (DMR)_ The completed DMR form should then be mailed to the regulatory agency's Central Files. Shield will continue to attempt to perform monthly sampling per Tier Two requirements until instructed to halt by CIRCOR. Shield greatly appreciates the opportunity to provide environmental services to the CIRCOR Pumps North America LLC. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at (704) 394-6913. Respectfully, SHIELD ENGINEERING, INC Melinla-�N� Greene Senior Engineer ATTACHMENT Thomas W. Witncr, PG Principal 4301 Taggart Creek Road Telephone 704.394,6913 Charlotte, NC 2e205 www.shieldengineering.com Fax 704.394.648e - _ Semi-annual Stormwater Discharge Monitoring Report , for North Carolina Division of Water Quality General Permit No. NCGO30000 Date submitted 8/24117 CERTIFICATE OF COVERAGE No. NCG030293 FACILITY NAME Colfax IMO IntlNgries, Inc, PERSON COLLECTING SAMPLES L LABORATORY: N/A Lab Cert. # Comments on sample collection or analysis: No sample collected due to rain events o1jJ114e of.business hours.. on weekends., or within 72 hoursof the last rain event. Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' _July DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []zero -flaw []WaterSupply ❑SA RECEIVED ®Other —Class C — Dry Fork Creek AUG 3 1 2017 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL ll C-,s DWIR SECTION No discharge this eriod ?� Outfall No. Date Sample Collected` (mo/dd/ r) 24-hour rainfall amount, Inches; Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ , Total Petroleum Hydrocarbons Total Toxic Organlcs5 Benchmarks ===> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. a For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. -'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1of3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (70), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<_XX mg/V where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, tier 2, or Tier 3 responses. See General Permit text Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, 3 Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =_-> _ - 15 mg/L 100 mg/L or 50 mg/L• 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B ' See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of ttie benchmark, you must Implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR ART A AND PART B MONITORINGRESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: r M411 an orlainal and one copy of this Dw includina all "No Discharae"reports, within 30 days of receipt of the lob results for at end of monitoring priod in the case of "No Dlscharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mall Service Center Raleigh, North Carolina 27699-1617 YOU MUST -SIGN THIS CERTIFICATION FOR ANY INFORMATION -REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons dir ponsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. } AG re that ere are jignificant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3of3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 8/9/18 CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME CIRCOR (formerly Colfax IMO Industries Inc. PERSON COLLECTING SAMPLES NA LABORATORY: NA Lab Cert. # NA Comments on sample collection or analysis: No qualifying storm event this month and/or rain events beginning -after normal business hours. Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR Zola SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' July RCCEil pFSi��4RGINGTOCLASS ❑ORW ❑HQW []Trout❑PNA G ! 1/ jj ❑Zero -flow [:]watersupply ❑SA SEP 0 7 2018 ®Other. Class C- Dry Fork Creek CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTION gNo discharge this period Outfall No. Date Sample Collected' (mp/dd/yr) 24rainfall amount, Inches3. Total Suspended Solids pH, Standard units Copper Lead Zinc Non-Polar O&G/hour Total Petroleum Hydrocarbons Total Toxic organics' Benchmarks =-> _ 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTOmonitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my Inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they Must be reported in the format.'<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note. if you report a sample value in excess of the benchmark, you must implement Tier 1, Tler 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil er month. FNo discharge this period ?z Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks > _ - 15 mg/L 100 mg/L or 50 mg/L" 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION a. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART tl SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail anoriginal and one cv v this O lndudfn all "N Discha e'° re arts, within 30 days a recef t of the lab results for at end a monitoring dod,. In the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the Information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are fignificant penalties for submitting false information, including the possibility of fines and Imprisonment for knowing violations." of Permittee) Permit Date: 11/1/2012-10/31/2017 9 1,V/ { 8 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 7/6/18 CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME CIRCOR (formerly Colfax/IMO Industries, Inc.1 PERSON COLLECTING SAMPLES NA LABORATORY: NA Lab Cert. # NA Comments on sample collection or analysis: No %2 m��r L t this month and/or rain events beeinnine after n r Ifl s ho AUG 0 7 2018 CENTRAL FILES Part A: Stormwater Benchmarks and MonitorWRes3f Wl0N SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' June DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑zero -flow ❑Water Supply [:]SA ®Other_Class C -- D!y Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 [ZNo discharge this period Outfal! No. Date Sample Collected` (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar 0&G/ tote! Petroleum Hydrocarbons Total Toxic Organicss Benchmarks ==_> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31), Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil p r month. [1I No discharge this period?z Outfall Nv, Date Sample collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 -- 9.0 SU Footnotes frvm Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmork, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCE5 FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on final and one copy of this -MR, Including oil "No Discharge" reports; within 30 days of recel t of the lab results or at -end of monitorin eriod in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signatur o Permittee) Permit Date: 11/1/2012-10/31/2017 8 I eti8 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 _N Semi-annual Stormwater Dischamye Monitorine Reoort for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted _.. U3118._ CERTIFICATE OF COVERAGE NO. NCG030293 SAMPLE COLLECTION YEAR _2018 FACILITY NAME _CIRCOR { olfa LIMO Indust l,es, Iitc.] SAMPLE PERIOD ❑ Jan -June ❑ July -Dec PERSON COLLECTING SAMPLES Bra ndon! Huggins, 5hleld-Enaineering or Z ManthlyL_ April (month). LABORATORY: _Pace Analytical Services, Inc. Lab Cert. # 12 DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA Comments on sampie collection or analysis: Rainw to read at 9.0• R EEC' - V E ❑zerp-flow ❑Water Supply [_]SA benchmark exceedances for nH: canner and zlneat outfall ona CROther Class C — Dry Fork Creek MAY 2 4 2018 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL FILES Part A: Stormwater Benchmarks and Monitoring Results GWR SECTION No discharge this period?' Outfail No. Date Sample pl Collected (mo/dd/ r) . 24-hour rainfall amount, Inches; Total Suspended Solids PH, Standard units ; Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ---> - 100 mg/L or 50 mg/L 6.0 -- 9.0 0.007 mg/L 0.03 mg/L' 0.067 mg/L 15 mg/L 1 mg/L SDO 004 4/23/18 1.13 48.4 i 9.3 0.0195 0.0057 0.104 <5.0 <0.4254 I f Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same 0utfall. 2. For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operatia'ns, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found In 40 CFR 469.12; for electronic crystal manufacture use the definition as found In 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Hate: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 r Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement, "Based upon my Inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certlfy that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included In the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note. Results must be reported 1n numerical format. Do -not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results Are below the applicable limits, they must be:repportedIn—the format. "<XX'Mjj/L1 where XX is the numerical value of the detection limit, reporting limit, etc. In mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text. Part B* Vehicle Maintenance Area Monitoring Results. only for facilities averaging > 55 gal of new oil per month. ... _ O No discharge this:perlod?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar O&G/TPH by EPA .1664 (SGT-HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L' 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B ' See General Permit text, Table S, Identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 9z Nate: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text FOR P,8RTA AND. FART D MONITORING, RESULTS;. A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4'013 MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES gNO ❑ IF YES, HAVE YOU CONTACTED THE'DWQ REGIONALOFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: M it or al and:ane copy of this . includin ,all -" o Dfschar e" re arts within D days o race! the.' ab results tor of end manit dan erl .in_the ras Q "—_o_'Dlscharge"�rie'portsl_to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUSTSIGN_THI—CERTIFICATIONFOR ANY INFDRMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false Information, including the possibility of fines and Imprisonment for knowing violations." of Permitteej y �S (Date) Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 *ENGINEERING, INC. April 16, 2018 John Nixon, Plant Manager CIRCOR Pumps North America LLC 1710 Airport Road Monroe, North Carolina 28110 Subject: Monthly Storrwater Sampling -- March 2018 Certificate of Coverage No. NCG030293 CIRCOR — Monroe, NC Shield Project No. 1150109-02 Dear Mr. Nixon: REC1!: APR 3 p 2018 CEN7-itf.L Ft: D4��R "1 CT/ON Shield Engineering, Inc. (Shield) successfully collected a monthly stormwater sample for Stormwater Discharge Outfall (SDO) #004 at the CIRCOR — Monroe facility for the month of March 2018. During the March 6, 2018 sampling event, Shield's field measurement of pH was 7.9 at SDO #004. Total event precipitation was 0.63 inches. In addition to collection of samples, Shield performed Qualitative Monitoring at SDO 4004 (attached). Shield has prepared the Stormwater Discharge Monitoring Report (DMR) using the results of analyses from the commercial laboratory that the CIRCOR facility has contracted with and the field values indicated above. The attached DMR should be signed by CIRCOR's authorized representative and then two signed copies of the DMR form should be mailed to the regulatory agency's Central Files. The sampling results from the March 6th event show that CIRCOR has exceeded benchmark concentrations for Total Recoverable Copper and Total Recoverable Zinc. CIRCOR remains in Tier Three for Copper and Zinc and remains in Tier Two for Total Suspended Solids. Shield will continue to perform monthly sampling per Tier Two requirements until instructed to halt by CIRCOR. Shield greatly appreciates the opportunity to provide environmental services to the CIRCOR. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at (704) 394-6913. Respectfully, SHIELD ENGINEERIIVG, INC. Melinda . Greene Senior Engineer ATTACHMENTS Thomas W. Witner, PG Principal 4301 Taggart Creek Road Telephone 704,394.6913 Chadot[e, NC 78206 www.shieldenginearing.com Fax 704.394,6968 Semi-annual Stormwater Discharge Monitorine Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted , 4/16/18 CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME CIRCOR [formerly. Colfax IMO'Industries; Inc.) PERSON COLLECTING SAMPLES Brandon Huggigsi Shield Engineering LABORATORY: _Pace Analytical Lab Cert. p 12 Comments on sample collection or analysis:Benchmark exceedances for Copper and, Zinc at Outfail 004. Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' March DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow []water Supply []SA ®Other Class C — Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -) No discharge this period?? Outfail No. Date Sample Collected) (mo/dd/yr) 24-hour rainfall amount, Inches3.. Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic organics" Benchmarks 100 mg/L or 50 mg/L 6.0 -- 9.0 0.007 mg/1 0.03 mg/L 0.067 mg/L is mg/L 1 mg/L SDO 004 3/6/18 0.63 14.8 7.9 0.0158 0.0054 0.119 5.3 <0.4706 F Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall, z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found In 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit pate: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, th�Lmust b _ e reported in the format, "<XX rrsB[L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value In excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month, 0. No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/ r) 24-hour rainfall amount, Inche53 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part 9 * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 -.1 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS;' • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALLTRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SE ION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES VrNO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on inaCand one COPY o this DMR Ind all Discharge" rarts IwiRhin 3I1 days a recei t of the lab'resuits Lor at end of monitoringer in the rase of "No Discftme" reporitsJ Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOV MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I' am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature,4f Permittee) y le/I i; ( Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 ENGINEERING, INC. March 20, 2018 Rebecca Israel Environmental, Health, and Safety Lead CIRCOR Pumps North America LLC 1710 Airport Road Monroe, North Carolina 28110 R& CiEFIV Subject: Monthly Stormwater Sampling — February 201$ ED Certificate of Coverage No. NCGO30293 A4AR p+ % 2018 CIRCOR — Monroe, NC ry7 j � F Shield Project No. 1150109-02 U WR S�CTI�ES Dear Ms. Israel: Shield Engineering, Inc. (Shield) successfully collected a monthly stormwater sample for Stormwater Discharge Outfall (SDO) #004 at the CIRCOR -- Monroe facility for the month of February 2018. During the February 7, 2018 sampling event, Shield's field measurement of pH was 8.9 at SDO 4004. Total event precipitation was 0.56 inches. In addition to collection of samples, Shield performed Qualitative Monitoring at SDO #004 (attached). Shield has prepared the Stormwater Discharge Monitoring Report (DMR) using the results of analyses from the commercial laboratory that the CIRCOR facility has contracted with and the field values indicated above. The attached DMR should be signed by CIRCOR's authorized representative and then two signed copies of the DMR form should be mailed to the regulatory agency's Central Files, Please note that the analysis for Total Toxic Organics (625 MSSV) was extracted out of holding time. This was due to the lab diluting the original sample to a point that caused a non -detect result to be over the benchmark due to the increased reporting limit. The lab re -analyzed the sample at Shield's request and extracted and reported at a dilution factor which allowed the non -detect results to meet a reporting limit that was within the benchmark value. The sampling results from the February 70' event show that CIRCOR has exceeded benchmark concentrations for Total Recoverable Copper, Total Suspended Solids and Total Recoverable Zinc. CIRCOR remains in Tier Three for Copper and has re-entered Tier Three for Zinc and remains in Tier Two for Total Suspended Solids. Shield will continue to perform monthly sampling per Tier Two requirements until instructed to halt by CIRCOR. Shield greatly appreciates the opportunity to provide environmental services to the CIRCOR. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at (704) 394-6913. Respectfully, SHIELD ENGINEERING, EVG L' Melindaneene Senior Engineer ATTACHMENTS o ellenz,.PE Engineering Design Services Department Manager 4301 Taggart Creek Road Telephone 704.394, 6913 Charlotte, NC 20208 www.shieldengineering.com Fax 704.394,6968 Semi-annual Stormwatelr Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted „312O IS CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME CI_RCOR (faMeriy ColfaxJIMO Industries: Inc.) PERSON COLLECTING SAMPLES Brandon Hug ,lns, Shield Enginee[i LABORATORY: Pace Analylfcal Lab Cert. # 12 Comments on sample collection or analysis:Benchmark exceedances for TSS, Cop>oer4nd Zinc at Outfall 004: MSSV fi25 was extracted out of holding time but remained a non -detect. Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' February DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water supply []SA ®Other_Class C — Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this perlod?2 Outfall No. bate Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks =__> - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/l SDO 004 2/7/18 0.56 121 8.9 0.0493 0.0261 0.198 <5.0 <0.4789 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall, 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. `See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring i may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan Included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported In the.farmat. "<)Q(me/L". where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value In excess of the benchmark, you must Implement Tler 1, Tier Z or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period?2 Outfall Na. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks = => - 15 mg/L 100 mg/L or 50 mg/L' 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B " See General Permit text, Table 5, identifying the especially sensitive receiving water classlflcations where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must Implement Tier 1, Tier 2, or Tier 3 responses. See General Permit team. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION a. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONALOFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mall.an orWhal arid one cogy a his DMR includin all "Na Discharge" re orts within 0 do s o recel o he ati results or o manitorin er ad in the case of "No Discharae" reoartsl to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YO U MUST SIGN THIS CERTIFICATION F R ANY INFOR ATI R P RTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." L A/:� (Signature 9ftermittee) Permit Date: 11/1/2012-10/31/2017 t 18�&, (Date) SWU-245, last revised 10/25/2012 x" Page 3 of 3 ROY COOPER Governor MICHAEL S. REGAN &ra wry WILLIAM E. TOBY VINSON, ]R Direclor Energy, Mineral and Land Resources ENVIRONMENTAL QUALITY March 12, 2018 Berry F Major IMO Industries Inc. — IMO Pump Post Office Box 5020 Monroe, North Carolina 28111 Subject: Compliance Evaluation Inspection IMO Industries Inc - IMO Pump NPDES Stormwater Permit NCG030293 Monroe, North Carolina Dear Mr. Major: Enclosed please find a copy of the Compliance Evaluation Inspection Report for the inspection we -conducted at the subject facility on March 1, 2018. The report should be self-explanatory; however, should you have any questions concerning this report, please do not hesitate to contact me at (704) 663-1699 or by email to lynne.hays@ncdenr.gov. Sincerely, Zahid S. Khan, CPM, CPESC, CPSWQ Regional Engineer Land Quality Section _ LH/cys Enclosure c: Stormwater Permitting Branch Statc of North Carolina I Environmental Quality I Encrgy, Mineral and Land Rrsourccs Mooresville Rcgional Oiiicc 1610 fast Ccntm Avcauc I Mooresvillc. NC 29115 704-663-1699 Compliance Inspection Report Permit: NCG030293 Effective: 11l16117 Expiration: 10/31/18 Owner: Circor Pumps North America LLC SOC: Effective: Expiration: Facility: CIRCOR Pumps North America. LLC County: Union 1710 Airport Rd Region: Mooresville Monroe NC 28111 Contact Person: Rebecca Israel Title: Phone: 704-289-8511 Directions to Facility: System Classifications: Primary ORC: Secondary ORC(s): On -Site Representative(s): Related Permits: Inspection Date: 03/01/2018 Primary Inspector: Mary L Hays Secondary Inspector(s): Certification: Phone: Entry Time: 10100AM Exit Time: 10:30AM Phone: 704-235-2146 Reason for Inspection: Routine Inspection Type: Compliance Evaluation Permit Inspection Type: Metai Fabrication Stomrwater Discharge COC Facility Status: ❑ Compliant ❑ Not Compliant Question Areas: 0 Storm Water __ (See -attachment summary.) Page: 1 Permit NCGO30293 Owner- Facility: Circor Pumps North America LLC Inspection Date: 0310112018 Inspection Type : Compliance Evaluation Reason for Visit Routine Inspection Summary: On March 1, 2018, a routine inspection was attempted at the IMO Industries. The facility is currently occupied by CIRCO" Please note this permit is not transferable to any person without prior written notice to and approval from the Director. The permittee is required to notify the Division in writing in the event the permitted facility is sold or closed. Page: 2 Ina ec ronData 3 I- ;Inspecvonjyge_Cgrt Cervalua6on R asoAicyYrs -:p-D lo.-i`- S orniwa#e� Poll�rtic�rt Prevenfiori Paaq Ye$ -M i� aE • Doesif a sitr: have a 5to nwater Pollution Preventim Alan? ❑ ❑ ❑ # Does the Plan include a General Location (EJSCS) map?. 4' ❑ # D6s-die Plan indude a `Nan-AwDescrlptlan of Prackoe '? ❑ ❑ # Floes the Ptah Include a detailed site map including ouifall locadons and drainage areas? ❑ ❑ ❑ # Does the Plan include.a list of significant spills occurring during the past 3 years? ❑ ❑ n # Has the faculty evaluated feasible alternatives to currant pracdces? ❑ ❑ ❑ # Does the facirrty provlde all necessary'secondary containment? Q n ❑- # Does the Plan include a BMP,summary7 ❑ n ❑ # Goes the Flan include a Spill Prevention' and Response Plan (SPRF)? n ❑ . ❑ #'Does the Plan include a Preveritatiae'Marntenance and Good Housekeeping Plait? Q 0 .. ❑ # Does the facility provide: and-dwument.Frrrployee'fraihhg?. ❑ Q Li # f roes #lte Plan -utclude'alistof Responsible Partjt(s)? - - 6ired. and j6. ated annua �j #Roes the Plan include a'Stnirnwater FacrTrtp Vopedion Prdgram? ❑. _ L Has -the Stormwater, Pollution Prevention Plan Been hMiernented? 0 L R —77 Comment _ t dWiitattiye Man9toring Yes No . Ne 'Has the faa'iity conducted b Quar#UyeMonitoring semi-annualij - :❑ ❑ UO -Anal t�ical Monitor}ng: �':Na: He Has die facky conductedb Armlytical mgriiforing.. _ .❑. ❑. # Has ttte facility conduct Bd it Analytical monitoring f#am Viihiele Maintsoance areas? Jj. ❑ n Ca:.eM r _- Yes No ICE. Pei "all Ouifa[ls S. # is a copy .af the hermit and the Gerffeata of CaVefag'availalle at #ye siEe?.: F] '[] ; : # Wei —all au ells obsdmd.during ihe'his�l« tune: .- '-- :�# !f thef�a'i'�has.reQresen�ative trii�ailstatr�is �ptope?tir:cioattn�ntafH?l+D�t�� '_. ' �'n � . _ .�; _ � •-- _ . ... - _ _.y- ..- - 11�'j3ie faalevafuate'e�alE�ii�` i�b� �� as by ati< Go rtient = = - ' oReport eport Semi-annualStormwater Discharge Monitrin for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 2/7/18 CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME CIRCOR (formerly Colfax/1MO,industrles, Inc.) RCL11777 !1 I=U PERSON COLLECTING SAMPLES NA MAR 0 8 2018 LABORATORY: NA Lab Cert. # NA Comments on sample collection or analysis:No samples due to notEcN1-R/-\L FILE-,$ enough flow,andlor rainfall events after normalbusinesshours MR SECTION Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2016 SAMPLE PERIOD ❑ Jan -June [] July -Dec or ® Monthlyl,_ January DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ®Other Class C — Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?Z Outfall No. Date Sam le p Collected" (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids p H, Standard units Copper Lead Zinc Non -Polar O&GJ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks => _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. sThe total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found In 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permlt Date: 11/1/2012-10/31/2017 Swu-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported In the format, "<XX me/0 where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, rer 2, or Tier 3 responses. See General Permit text. Part 8: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?z Outfall No. Date Sample Collected" (mo/dd/yr) 24-hour rainfall amount, Inches a Non -polar O&G/TPH by EPA 1664 (SGT HEM) Total Suspended Solids pH Benchmarks 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 Su Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier z, or Tier responses. See General Permit text. R PARTA AND PART B MONORINg RgqLTS; • A BENCHMARK EXCEEDANCE TRIGGERS TIER 2 REQUIREMENTS. SEE PERMIT PART li SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. s TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO El REGIONAL OFFICE CONTACT NAME: a �� a�r�Inuf ondQne coptr of this DMR lnclu lirrrt all "Wry. Dlsr haraeu_ ��rts,_ i i ln:3(1 �a�+s_+a1 roc t of the"hi b resents_ for art �ndf of monitorlaa aerfad in the case of "No Discharme" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN IMIJ C991FICATION FOR ANY A 10 O D•: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the Information, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." [Signatur6f #ermittee) 2 Z, zis [Date] Permit Date: 11J1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 W. E. W ENGINEERING, INC. January 9, 2018 Rebecca Israel Environmental, Health, and Safety Lead CIRCOR Pumps North America LLC 1710 Airport Road Monroe, North Carolina 28110 Subject: Monthly Stormwater Sampling — December 2017 Certificate of Coverage No. NCGO30293 CIRCOR — Monroe, NC Shield project No. 1150109-02 Dear Ms. Israel:: RECEIVED JAN 2 9 2018 CENTRAL FILES DWR SECTION Shield Engineering, Inc. (Shield) successfully collected a monthly sormwater sample for Stormwater Discharge Outfall (SDO) #004 at the CIRCOR — Monroe facility for the month of December 2017. During the December 20, 2017 sampling event, Shield's field measurement of pH was 8.3 at SDO #004. Total event precipitation was 1.27 inches. In addition to collection of samples, Shield performed Qualitative Monitoring at SDO 4004 (attached). Shield has prepared the Stormwater Discharge Monitoring Report (DMR) using the results of analyses from the commercial laboratory that the CIRCOR facility has contracted with and the field values indicated above. The attached DMR should be signed by CIRCOR's authorized representative and then two signed copies of the DMR form should be mailed to the regulatory agency's Central Files. The sampling results from the December 20'h event show that CIRCOR has exceeded benchmark concentrations for Total Recoverable Copper. CIRCOR remains in Tier Three for Copper and Tier Two for Total Suspended Solids; however, since the last three consecutive samples for Zinc have been above the benchmarks, CIRCOR is no longer in Tier Two for Zinc. Shield will continue to perform monthly sampling per Tier Two requirements until instructed to halt by CIRCOR. Shield greatly appreciates the opportunity to provide environmental services to the CIRCOR. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at (704) 394-6913. Respectfully, SHIELD ENGINEERING, INC Melinda - reene Senior Engineer ATTACHMENTS C. Boland, PE pal Engineer 4301 Taggart Creek Road Charlotte, NC 28208 www.shieldengineering.com Telephone 704:394.6913 Fax 704.394.6968 1� I Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 1 8 18 CERTIFICATE OF COVERAGE NO. NCG030293 SAMPLE COLLECTION YEAR 2017 FACILITY NAME CIRCOR (formerly Colfax IMO Industries Inc SAMPLE PERIOD ❑ Jan -June ❑ July -Dec PERSON COLLECTING SAMPLES Irandon Hu ins Shield Engineerin or ® Monthly' December LABORATORY: Pace Analytical Lab Cert. # 12 DISCHARGING TO CLASS ❑ORW ❑HQW []Trout QPNA Comments on sample collection or anatysis:eenchmark exceedance for [,Zero -flow ❑Water Supply ❑SA Capper at SDO 004 .®.Other Class C—'Dry Fork Creek Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks 100 mg/L or So mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 12/20/17 1.27 28.4 8.3 0.0095 <0.005 0.0587 <5.0 <0.4873 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling Is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). t Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 , Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total taxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan Included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, the must be ortd in the format "<XX mg/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part g: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period,72 Outfall No. Date Sample 1 Collected (mo/dd/ r) 24-hour rainfall amount, Inches; Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks mg/L 100 mg/L or S0 mg/L' 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B • See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: li/i/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mallon original and one copy of this DMR clod all "Na Discharge &orkS within 30 d4 n receJ t o ihe�lab results or at en o onitorin erio In the case. o "No Discha e" regqrts Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am awa p_that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." r �� l►A°�nw t �« k k / r q I of Perrro ee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 lug. Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out thisform, please visit e: ova u dLymiii iin -l`a d- resources%,enema l-land7permitjlstormwater-p,�1nndes-industi°ial svyr b-A' Permit No L/V-. A-121-!�1 or Certificate of Coverage: No:: Facility Name: - C I KC ©_k. PLAmA95- -A4n/-fi%t. /' w-ert c As. L L C County:, .. +rl 1-b Yk _ _ -- Phone No. Inspector. _ i `) Date of Inspection: 2- f Time of Inspection:. 3 0 Total Event Precipitation (inches): I-R Z -2 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: e (Signature of Permittee or Designee) I. Outfall Description: Outfall No. �� Structure (pipe, ditch, etc.): A6�le r%,'-/, Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Pagel of 2 SWU-242, fast modified 07/28/2017 2. Color: Describe the color of the discharge usi _g basic colors {red, brown, blue, etc.} and tint (light, medium, dark) as descriptors: n 3. Odor: Describe any distinct odor that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): �} k 2 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: L/ 2 3 4 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where `1 its no solids and 5 is extremely muddy: 1(� J 3 4 5 7. Is there any foam in the stormwater dischargO Yes No: ✓e�y s ,g � t 8. Is there an oil sheen in the stormwater discharp? Ye No. 9. Is there evidence of erosion.or deposition at the outfaV o Yes oNo- 10. Other obvious Indicators of 5tormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 �JceAtWcal eww.padaGs.aom December 29, 2017 Rebecca Israel Colfax Fluid Handling 1710 Airport Road Monroe, NC 28110 RE: Project: Colfax Stormwater Pace Project No.: 92367956 Dear Rebecca Israel: Pace Analytical Services, LLC WN leincey Ave. Suits 1Do Huntarsville, NC ZSo7a (704)8759092 Enclosed are the analytical results for sample(s) received by the laboratory on December 21, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions conceming this report, please feel free to contact me. Sincerely, ZI Sarah Graham for Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enaosures cc: Melinda Greene, Shield Engineering REPORT OF LABORATORY ANALYSIS This report shaft not be reproduced. w=pt in hrtl, without the written consent or Pace Analytical Ser ems, LLC. Page 1 of 31 Pace Armlytieal Sarvisas, LLC m +a1!2ocal 9800 Kirtcey Ave. Suite ]00 Hijnteraville. NC 28078 ' WWW4eceWmmm (704)075-9092 E CERTIFICATIONS Project Colfax SkWrnwater Pace Project No,: 92367956 Charlotte Certification IDs 9800 KnceyAve, Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #. 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville CoM icatlon 1Ds 2225 Riverside Drive, Asheville, NC 28804 Flodda/NELAP Certification#: E87848 . Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 South Carolina Certification # 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 vrginiaNELAP Certification #. 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification # 99030001 VrginlalVEtAP Certification 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, without the written oorisent of Pace Analytical Servim. LLC. Page 2 0f 31 lice Arwcal' wrrpecs�.sam+ i SAMPLE ANALYTE COUNT Project: Colfax Ston7hvater Pace Project No.: 92367M Pus Analyti 41 Swvl es. LLC 98M Kinney Ave, Suite 100 Hunters ile, NC 2a078 (704)875-9092 Lab ID Sample ID Method Anatysts Reported Laboratory 92367956001 SOO-04 EPA 16648 JMS 1 PASI-C EPA W8 PKS 27 PASI-C EPA 200.7 SER 3 PASI-A EPA625 RES 58 PASI-C EPA624 GAYV 34 PASI-C SM 25400 SLS 1 PASI-A EPA9040 ECH 1 PASI-A REPORT OF LABORATORY ANALYSIS This report snap not be reproduced, exc w in ru0, without the wrrtlen cooscra of Pecs Analytical Services, LLC. Page 3 of 31 • eeAnraly>fical �rww.pacrlsbssnm PROJECT NARRATIVE Project: Colfax Stormwater Pace Project No.: 92367956 Method: EPA 1664E Description: 1664 SGT-HEM, TPH client: Colfax Fluid Handling Date: December 29, 2017 Pace Ana"cal Sorvk s LLC 9800 Kkicey Ave, Suite 100 Hunteraville, NC 28078 (704)87Fr9092 General Information: 1 sample was analyzed for EPA 166413. AD samples were received In acceptable condition with arty exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCl1R) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (Including M5 Tune as applicable): All criteria were within method requirements with any exceptions noted below.. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below, Method Blank: All anatytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report snail riot be reproduced, except in full, without the written consent of Pace Analytical Servian, LLC. Page 4 of 31 PwaAnaiytlrai Semites, LLC 98001GnrEyAve. Suite 100 LeiI"Ufo lKr+ Hun ermine, NC 2907E ~f rwscMacai *WM (704)975-9092 PROJECT NARRATIVE Project: Cotfax Stormwater Pace Project No.: 92367956 Method: EPA ti,o8 Description: 608 GCS Pesticides and PCBs Client: Colfax Fluid Handling Date: December 29, 2017 General In1b... w ion- 1 sample was analyzed for EPA 608. Ail samples were received in acceptable condition with any exceptions noted below or on the chain -of custody andlor the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the mettrod required hold times wish any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 3510 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with arry exceptions noted below: Surrogates: All surrogates were within QC limits with arty exceptions noted below. Method Blank: AD anatytes were below the report limit in the method blank, where applicable, with arty exceptions noted below. Laboratory Control Spike: Ail laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This repot strait not be mp Vdurtd, except in full, without the writlan Consent of Pace AnaiyUcW Sorv;des, LLC, Page 5 of 31 Pace Analytical Swvlcm. LLC a 9800IGr=yAve. Suite 100 , Huntersville, NC 2e070 °°a'p 1Oom (7041076-4092 1 PROJECT NARRATIVE Project: Colfax Stormwater Pace Project No.: 92367956 Method: EPA 200.7 Description: 200.7 MET ICP Client: Colfax Fluid Handling Date: December 29, 2017 General information: 1 sample was analyzed for EPA 200.7. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody andfor the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required told times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 200.7 with any exceptions noted below. Initial Calibrations (Including MS Time as applicable): An criteria were within method requirements with any exceptons noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Method Blank: AD analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, erupt in full. without the written consent of Pace AnaNrkei Services, LLC. Page 6 of 31 Pace AnatydcW Services, LLC a4I/`1I� l� • 980o Kncey Ave. Suit 100 4 r1J/`TIl Huntffrsvilte. NC 28078 wwat:earn (704)9759092 t PROJECT NARRATIVE Project: Colfax Stormwater Pace Project No. 92367956 Method: EPA 625 Description: 625 MSSV Client: Colfax Fluid Handling Date: December 29, 2017 General Intonation: f sample was analyzed for EPA 625_ Al samples were received in acceptable condition with any exceptions noted below or on the chain -of custody andfor the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with arty exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 625 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable). - Ail criteria were within method requirements with any exceptions noted below. Continuing Caliilwation: All criteria were withn method requirements with any exceptions noted below. Internal Standards: All internal standards were within QC limb with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC Emits with any exceptions noted below. QC Batch: 392115 131: RPD value was outside control limits. - LCSD (Lab ID: 2175542) • 2,4,6-Trichlorophenol • 2,4-Dinitrophenol • 4,6-Dinitro-2-rnetlWhenol • 4-Nitrophenoi • Pentachlorophenol Matrix Spines: All percer t recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report stroll rot be reproduced. except in full, without the written consent of Pane Analytical Se. vsQa, LLC. Page 7 of 31 www.paafebacam PROJECT NARRATIVE Project: Colfax Stormwater Pace Project No.: 92367956 Method: EPA 624 Description: 624 Volatile Organics Client: Colfax Fluid Handling Date: December 29, 2617 Pace Anatydcsi Services, LLC 9900 Kjr=y Ave. Suite 100 Hurbersville, NC 26078 (704)875-9092 General Information: 1 sample was analyzed for EPA 624. All samples were received in acceptable condition with any exceptions noted below or an the chain -of custody andtor the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: Ail criteria were within method requirements with any exceptions noted below. Internal Standards: An internal standards were within QC limits with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report fimit in the method blank, where applicable, with any exceptions noted below Laboratory Control Spike: AN laboratory control spike compounds were within QC fimits wrth any exceptions noted below. Matrix Spikes: Ail percent recoveries and relative percent differences (RPOs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, exrapt in full, without the written consent of PawAnatyticel Services, I.I.C. Page 8 of 31 1�-20eAnapcalo t www.paaalah=n s PROJECT NARRATIVE Project: Colfax Starmwater Pace Project No.: 92367956 Method: SM 2WD Description: 2540D Total Suspended Solids Client Colfax Fluid Handling Date: December 29, 2017 Pace Analytical Services, LLC 9900 Kncey Ave, Suite 100 Hurstersvlle, NC 20079 (704)875-9092 General Information: 1 sample was analyzed for SM 2WD.: All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody an ifor the sample condition upon receipt form (SCUR) attached at the end of this report, Hold Time: Tile samples were analyzed within the method required hold times with any exceptions rented below, Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. QC Batch: 392427 D6: The precision between the sample and sample duplicate exceeded laboratory control limits. • DUP (Lab ID: 2176883) • Total Suspended Solids Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in U, without the written consent or Pace Analytical Services, LLC. Page 9 of 31 AnaVicalo WWW paceletrsm n F i PROJECT NARRATIVE Project: Colfax Stormwater Pace Project No.: 92367956 Method: EPA SW Description: 9040 pH Client: Colfax Fluid Handling Date: December 29, 2017 Pats Anatytical Servicas, LLC 980C lCincey Ave. Suite 100 - HuntersviAe, NC 25078 (704)875-9092 General Information: 1 sample was analyzed for EPA 9040. All samples were received in acceptable condition with any exceptions noted below or an the chain -of custody andlor the sample condition upon receipt form (SOUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below, H6: Analysis initiated outside of the 15 minute EPA required holding time. • SDO-04 (Lab ID: 92367956001) Method Hlank Al anaiytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: Al laboratory Control spike compounds were within OC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: Al duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Anaiybral Services, LLC. Page 10 of 31 Pace Analy "l Serwkes, LLC n d�� l�+� a 9800 Kincey Ave. Suite 100 lytical Hurrtersvft, NC 26078 �f ceAnawww4-vw.i.com (704)875-9092 ANALYTICAL RESULTS P-*Ct Colfax Stornwater Pare Pr*c1 No,: 92367956 Sample: SDO-04 Lab ID: 92367956001 Collected: 1220/17 09:30 Received: 1212111712:55 Matrbc: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua] 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg/L 5,0 1 12128/17 05:16 608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510 Aldrin NO ug/L 0.050 1 12/22/17 07:44 1222117 20:26 309-00-2 alpha-BHC NO ug/L U50 1 12/22/17 07:44 1222/17 20:26 319-84-6 beta-BHC NO ug/L 0,050 1 12/22/17 07:44 1222117 20:26 319-85-7 detta-BHC NO ug/L (I.050 1 1222117 07A4 12/Z2117 2026 319.86-8 gamma-BHC (Lindane) NO uglL 0.050 1 12/22/17 07:44 1222117 20:26 58-89-9 Chbordane (Technical) NO ug/L 0.50 1 1222117 07:44 1222/17 20:26 57-74-9 4,4'-ODD NO ug/L 0.050 1 1222/17 (17:44 i2/22117 20:26 72-5" 4,4'-DDE NO ug/L 0.050 1 1222117 07:44 1222/17 20:26 72-55-9 4,4'-DDT NO ug/L 0.450 1 1222/17 0744 1222/i7 20:26 50-29-3 Dieldrin NO ug/L 0.050 1 12=17 07:44 1=17 2026 60-57-1 Endosdfan I NO uglL 0.050 1 12122/17 07:40 12rM17 20:26 959-98-8 Endosuifan 11 NO uglL 0A50 1 1222117 07:44 1222J17 20:26 33213-65-9 Endosulfan suffate NO uglL 0.050 1 1 =1 7 07:44 12=17 20:26 1031-07-8 Endrin NO ugR 0,050 1 1222/17 07:44 1=17 20:26 72-20-8 Endrin aldehyde NO uglL 0.050 1 1 =1 7 07:44 1222/17 20:26 7421-93-4 Heptachlor NO ug1L 0.050 1 12/22/17 07:44 1222/17 20:26 76-44-8 Heptachlor epoxide NO ug1L 0.050 1 12/22/17 07:44 1222117 20:26 1024-57-3 PCB-1016 (Arador 1016) NO u9/L 0,50 1 1222/17 07:44 12=17 20:26 12674-11-2 PCB-1221 (Arocior 1221) NO u9/L 0.50 1 1222117 07:44 12/22/17 20:26 11104-28-2 PCB-1232 (Arodor 1232) NO ug/L 0,50 1 1222117 07:44 1222/17 20:26 11141-16-5 PCB-1242 (Arodor 1242) ND ug/L 0,50 1 12/22/17 07:44 1222/17 20:26 53469-21-9 PCB-1248 (Amcor 1248) ND u9n- 0.50 1 12 W17 07:44 1222/17 20:26 12672-29-6 PCB-1254 (Arodor 1254) ND ug/L 0.50 1 12122/17 07:44 1222/17 20:26 11097-69-1 PCB-1260 (Arodor 1260) ND ug/L 0.50 1 1222/17 07:44 1222117 2026 11096-82-5 Toxaphene NO ug/L 0.50 1 12=17 07:44 1222117 20:26 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 60 % 20-110 1 1222117 07:44 12QV17 20:26 877-09-8 Decachlorobiphenyl (S) 36 % 20-138 1 1222117 07:44 1222117 20:26 2051-24-3 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 9-5 u9/1- SA 1 12/27/17 20:11 12/29/17 07:10 7440-50-8 Lead ND ug1L 5.0 1 1227117 20:11 1229117 07:10 7439-92-1 Zinc 58.7 u9/1. 10.0 1 1227/17 20:11 12/29117 07:10 7440-66-6 625 MSSV Analytical Method: EPA625 Preparation Method: EPA625 Aaenaphthene NO ug/L 5.0 1 12122J17 09:53 1227117 05:17 83-32-9 Acenaphb*ene NO ug/L 5.0 1 12r22/17 09:53 1227/17 05:17 208-96-8 Anthracene NO ug/L 5.0 1 1=17 09:53 1227117 05;17 120-12-7 Benzo(a)anthraoene NO ug/L 5.0 1 12rM17 09:53 1227A7 05:17 56-55-3 Benzo(a)pyrene ND ugh. 5.0 1 12/22/17 09:53 1227117 05:17 50-32-8 Benzo(b)8uoranthene ND ug1L 5.o 1 12rml7 09:53 12/27117 05:17 205-99-2 Benzo(g,h,i)perylene NO ug/L 5.0 1 1222117 09:53 1227117 05:17 191-24-2 Benzo(k)ftuoranthene NO u911- 5.0 1 1222/17 09:53 1227/17 05:17 207-08-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fill, Dale: 12292017 04:47 PM without the written consent of Pace Analytical Servkma, LLC. Page 11 of 31 Pace Analytical Services, LLC 9800KinceyAve. Suite100 yQcar0 I�Wce Fiuntersville, NC 2BU76 = (7041875-9092 I ANALYTICAL RESULTS Project: Colfax Stormwater Pace Project No.: 92367956 Sample: SDO-04 1.a610: 9236795=1 Collected: 12/20/17 09:30 Received'. 1221117 12:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 4-Bromophenylphenyl ether ND ug/L 5.0 1 1222/17 09:53 1227/17 D5:17 101-55-3 Butylbenzylphthalate ND ug/L 5.0 1 12/22/17 09:53 12/27/17 05:17 85.68-7 4-Chioro-3-methylphenol ND ug1L 5.0 1 12122/17 09:53 12/27117 05:17 59-50-7 bis(2-Chloroethoxy)mett►ane ND ug/L 10.0 1 12122/17 09:53 1227/17 05.17 111-91-1 bis(2-Chloroethyl) ether ND u911- 5.0 1 12/22/17 09:53 1227117 05:17 111 44 4 2-Chloronaphthalene ND ug/L 5.0 1 12122I17 09:53 1227117 05:17 91-58-7 2-Chlorophenoi ND ug1L 5.0 1 12/22/17 09:53 1227/17 05:17 95-57-8 4-Chlorophenyip"l ether ND ug/L 5.0 1 12/22/17 09:53 1227/17 05:17 7005-72-3 Chrysene ND u91L 5.0 1 12=17 09:53 1227117 0517 218-01-9 Dibenz(a,h)anthracene ND ug/L 5.0 1 1222117 09:53 12127/17 05:17 53-70-3 3,T-Dchlorobenzidine ND ug1L 25.0 1 12122/17 09:53 12/27/17 05:17 91-94-1 2,4-Dichlorophenoi ND ug/L 5.0 1 1 ZQV17 09:53 1227117 05:17 120-83-2 Diethylphthalate ND ug/L 5.0 1 1222117 09:53 12/27/17 05:17 84-66-2 2,4-Dimetttylphenol ND ug/L 10.0 1 1222/17 09:53 12/27/17 05:17 105-67-9 Dimethylphthalate ND ug1L 5.0 1 1222/17 D9:53 1227117 05A7 131-11-3 Di-n-butylphthalate ND uglL 5.0 1 1222/17 09:53 1227117 05:17 84-74-2 4,6-Dinitro-2-methylphenoi ND uglL 20.0 1 1222117 09:53 1227/17 05:17 534-52-1 2,4-Dinitropheriol ND ug/L 50.0 1 1222117 09:53 1227117 05:17 51-28-5 2,4-Dinitrotoluene ND ug/L 5.0 1 1222/17 09:53 12127/17 05:17 121-14-2 2,6-Dinitrotoluene ND ug/L 5.0 1 1222117 09:53 1227117 05:17 606-20-2 Di-n-octylphthalate ND ug/L 5.0 1 1222/17 09:53 12/27/17 05:17 117-84-0 bis(2-Ethylhexyl)phthatate ND ugA- 5.0 1 1222117 09:53 1227117 05:17 117-81-7 Ftuoranthene ND ug/L 5.0 1 12/22117 09:53 1227117 05:17 206-44-0 Fluorene ND ug/L 5.0 `1 1222117 09:53 1227117 05:17 W73-7 Hexachloro-1,3-butadiene ND ug/L 5.0 1 1222117 D9:53 1227117 05:17 87-68-3 Hexachlorobenzene ND ug/L 5.0 1 1222117 09:53 1227117 05:17 118-74-1 HexacHorocycfopentadiene ND ug1L 10.0 1 1222117 09:53 12f27117 05:17 77-47-4 Hexachioroetharie ND ug/L 5.0 1 1222117 D9:53 12/27/17 05:17 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 5.0 1 1222M709:53 122711705:17 193-39-5 Isophorone ND ug/L 10.0 1 1222/17 09:53 1227117 05:17 78-59-1 Naphthalene ND ug1L 5.0 1 12122117 09:53 1227117 05:17 91-20-3 Nitrobenzene ND ug/L 5.0 1 12/Ml7 09:53 1227117 05:17 98-95-3 2-Nitrophenol NO ug/L 5.0 1 12/22►17 09:53 1227117 05:17 W75-5 4-Nitrophenol NO uglL 50.0 1 12/Ml7 09:53 1227117 05:17 100.02-7 N-Nitrosodimethylarnine ND u91L 510 1 1222/17 09:53 1227117 05:17 62-75-9 N-NiVnso-di-n-propylamine ND ug/L 5.0 1 12/22/17 09:53 1227117 05:17 621-64-7 N-Nitmaodiphenylamine ND ug/L 10.0 1 12122/17 09.--53 12/27/17 05:17 86-30-6 2,Z-Oxybis(1-chloropropane) ND ug/L 5.0 1 1222J17 09:53 1227117 05:17 108.60-1 Perltac hlorophenoi ND ug1L 10.0 1 12/22/17 09:53 1227/17 05:17 87-86-5 Phenanthrene ND ug1L 5.0 1 12122J17 09:53 1227/17 05:17 85-01-8 Phenol ND ug/L 5.0 1 12122/17 09:53 1227117 05:17 108-95-2 Pyrene ND ug/L 5.0 1 12/22/17 09:53 12127/17 05:17 129-00-0 1,24-Trichlorobenzene ND ug/L 5.0 1 1222117 09:53 1227/17 05:17 120-82-1 2,4,6-Trichlomphenal ND ug/L 10.0 1 12122/17 09:53 1227117 05:17 W06-2 surrogates Nitrobenzene-d5 (S) 35 % 10-120 1 12i22J17 09:53 1227/17 05:17 4165-60-0 2-Fluorobiphenyl (S) 31 % 15-120 1 12122/17 09:53 1227/17 05:17 321.60-8 REPORT OF LABORATORY ANALYSIS Thin report shall not be reproduced, except in Full, Date: 12292017 04:47 PM without the wridan consent of Pace Anaiytic al SerAces, LLC, Page 12 of 31 �eAnalyhcal . www.pecdabarm+ F ANALYTICAL RESULTS Pace Analytical Samicas, LLC 98001GncayAve. Suite 100 Huntersvflle, NC 28070 f704)875-9092 Protect: Colfax Stormwater Pace Project No.. 92367956 - Sample: SOO-04 lab ID: 92367956001 Collected: 1220/17 09:30 Received: 12MM7 12:55 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA625 Preparation Method: EPA625 Surrogates Terpherlyl-d14 (S) 72 % 11-131 1 12/22/17 09:53 11212711170517 1718-51-0 Phenol d6 (S) 10 % 10-120 1 12122/17 09:53 12/27/17 05:17 13127-88-3 2-Ftuorophenol (S) 16 % 10-120 1. 1222/17 09:53 12F27117 05:17 367-12-4 2,4,6-Tribromophenol (S) 57 % 10-137 1 12171/17 09:53 12/27/17 05:17 118-79-6 624 Volatile Organics Analytical Method: EPA 624 Benzene NO ug1L 2.0 1 1228/1713:14 7143-2 Bromodichloromethane NO ug/L 2.0 1: 12121311713:14 75-274 Bromoform NO ug/L 2.0 1 1212811713:14 75-25-2 Bromometharte NO ug/L 2A 11 12128/1713:14 74-83-9 Carbon tetrachloride NO ug/L 2-0 1; 12128/1713:14 56-23-5 Chlorobenzene NO ug/L 2.0 '1 12128/1713:14 108-90-7 Chloroethane NO ug/L 2.0 1 12/28117 13:14 75-00-3 Chloroform NO ug1L 2.0 1 1212611713:14 67-M3 Chloromethane ND ug/L 2.0 1 1212811713:14 74-87-3 Dibromochloromethane NO u91L 2.0 1 1212811713:14 124-48-1 1,2-Dichlorobenzene ND ugA- 2.0 1 12128117 13:14 95-50-1 1,3-Dichlorobenzene NO ug/L 2.0 1 12/28/1713:14 541-73-1 1.4-Dichlorobertzene NO ug/L 2,0 1 12)2811713:14 106-46-7 1,1-Dichloroethane ND ug/L 2.0 1 12128/1713:14 75-34-3 1,2-Dichloroethane ND ug/L 2.0 A 12/28/17 13:14 107-06-2 1,1-Dichloroethene ND ug/L 2.0 1 1228/1713-14 75-35-4 ds-1,2-DicNoroethene NO ug1L 2.0 1 12/2811713:14 156-59-2 trans-1,2-DichlorDethene NO ug/L 2.0 1 1212811713:14 156-60-5 1,2-Dichioropropane NO ug/L 2.0 1 12/2811713:14 78-87-5 cis-1,3-Dichloropropene NO ug1L 2.0 1 1212811713:14 10061-01-5 trans-1,3-Dichloropropene NO ug/L 2.0 1 12/28/17 13:14 10061-02-6 Ethylbenzene ND ug/L 2.0 1 122811713:14 100-414 Methylene Chloride ND ugh- 2.0 1 1212611713:14 75409-2 1,1,2,2-Tetrachloroethane ND ug/L 2.0 :1. 122811713:14 79-34-5 Tetrachloroethene ND ug1L 2.0 1 1212811713:14 127-18-4 Toluene ND ug/L 2.0 1 1212811713:14 108-88-3 1,1,1-Trirhloroethane ND ug1L 2.0 1 1212811713:14 71-55-6 1,1,2-Trichlornethane ND ug1L 2.0 -1' 1228/1713:14 79-00-5 Trichloroethene ND ug/L 2.0 1 121281171114 79-01-6 Trichloral9uoromethane NO ug1L 2.0 1 1228/171314 75-69-4 Vlnyl chloride NO ug/L 2.0 1' 1228117 13:14 75-01-4 Surrogates 4-Bromofluambenzene (S) 96 % 70-130 1 1228117 13:14 480-004 Toluene-d8 (S) 129 % 70-130 1 12121Y17 13:14 2037-26-5 1,2-Dichloroethane-64 (S) 92 % 70-130 1 12/28/1713:14 17060-07-0 25400 Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids 28.4 mg/L 5.0 1 1227117 08:51 Date: 122MO17 04:47 PM REPORT OF LABORATORY ANALYSIS This report she➢ not be reproduced, e)=pt in full, without the written consent cf Pace Analytical Services, LLC, Page 13 of 31 1!2ceAnaoicale < www4wcvlmb&cau i I ANALYTICAL RESULTS Paco Analytical Services, LLC 9800 KkceyAve. Sutts too HuntemOille, NC 2B079 (704)975-9092 Project: Colfax Stommater Pace Project No.: 92367956 Sample: SDO-04 Lab iD: 92357956001 Collected: 1200117 09:30 Received: 1Z?1117 12:55 Matmt: Water Parameters Resu is Units Report Limit DF Prepared Analyzed CAS No. Qua] SO40 pH Analytical Method: EPA 9040 pH 6.6 Std. [Units 0.10 1 12122/17 15:00 H6 Date: 1212912017 04:47 PM REPORT OF LABORATORY ANALYSIS This report shah riot be reproduced, except in fun, without the written consent of Pace Analytical Services, L.I.C. Page 14 of 31 • I Afk3J� icai v wwW4icewbLcum r QUALITY CONTROL DATA Project: Colfax Stormwater Pace Project No.: 92367956 QC Batch: 392579 Analysis Method: EPA 1664E QC Bat& Method: EPA 1664E Analysis Description: 1654 SGT-HEM, TPH Associated Lab Samples: 92367956MI METHOD BLANK: 2177552 Matrix: Water Associated Lab Samples: 92367956001 Blank Reporting Parameter Units Result Limit AnaWed Qualifiers Total Petroleum Hydrocarbons mg1L NO 5.0 12/28/17 05:02 Pace Analytical Services, LLC 9800 Kincey Ave., Suits 100 Huntenn'lle. NC 26078 (704)e75-0092 LABORATORY CONTROL SAMPLE: 2177553 Spike LCS LCS % Rec Parameter Units Cono, Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mglL 20 19.9 100 64-132 MATRIX SPIKE SAMPLE: 2177554 92367810001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L ND 1 20 16.9 94 64-132 Room presented on aft page are in the unit ire a -ed try the 1wi a' c*k=m acrpr +nee a al6ertr anit Is press t to ttur dot of the r M REPORT OF LABORATORY ANALYSIS This report shag not be reproduced, except in full, Dale: 1212912017 04:47 PM wdhout the written consent of Pace AnatAcat Services, LLC. Page 15 of 31 U[i l` nalj&al e i ww#ascmL+tacan i Project: Colfax Storr inter Pace Project Na_: 92367956 OC Batch: 392W QC Batch Method: EPA 200.7 Associated Lab Samples: 92367956001 METHOD BLANK: 2177472 Associated Lacy Samples: 92367956001 Parameter Copper Lead zinc QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Wafer Blank Reporting Units Result Limit Analyzed Qualifiers ug/L ... ND 5.6 12/291i705:48 u9/L ND 5.0 1229/17 05:48 ug/L ND 10.0 1229117 05:48 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntereville, NC 20078 (704)8759091 LABORATORY CONTROL SAMPLE: 2177473 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 488 96 85-115 Lead ug/L 500 451 90 85-115 Zinc ug/L 500 430 86 M115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2177474 2177475 MS MSD 92367811001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper 1.19/1- 18.2 1000 1000 1110 1110 109 109 70-130 0 Lead ug/L ND 1000 1000 747 746 74 74 7D-130 0 Zinc ug/L 12.8 1000 1000 854 846 84 83 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2177476 2177477 MS MSD 92367800004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Capper ug/L ND 1000 1000 971 960 97 96 70-130 1 Lead ug/L ND 1000 1000 896 892 89 89 70-130 0 Zinc u9/L 10.0 1000 1000 891 887 88 88 70-130 0 Resuas praapr. en thla page ue In do units InmcaUd by the -Un[W ralucin except where an alto. to unl lz prasentad tD the rVd arthe rewAL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12292017 04:47 PM without the written consent of Pace Anaiytirnl Services, LLC. Page 16 of 31 ceAnalylbcal www4wwffW:Ssrnrn t QUALITY CONTROL DATA Project Colfax Stormwater Pace Project No.: 92367956 QC Batch: 392648 OC Batch Method: EPA624 Associated Lab Samples: 92367956001 Analysis Method: EPA 624 Analysis Descriptlorr- 624 MSV METHOD BLANK 2177866 Matrix: Water Associated Lab Samples: 92367956001 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1-Trichloroethane Lig/L NO 2.0 t22811708A3 1,1,2,2-Tetrachloroethane ug/L NO 2.0 1212811708:43 1,1,2-Trichloroethane ug/L NO 2.0 1201117 08 A3 1,1-Dichloroethane ug/L NO 2.0 122811708:43 1,1-Dichloroethene ug/L NO 2.0 122811708:43 1,2-Dichlombenzene ug/L NO 2.0 12128117 08:43 1,2-Dichiaroethane ug/L NO 2.0. 1228117 08:43 1,2-Dichloropropane ug/L NO 2-0 1228117 08:43 1,3-Dichiarobenzene ug/L NO 2.0 1212811708:43 1,4-Dichlorobenzene ug/L NO 2.0 1228117 08:43 Benzene u911- NO 2.0 1228/17 08:43 Bromodichioremethane ug/L NO 2.0 1228117 08:43 Bromoform u911- NO 2.0 1228117 08:43 Bromometi ane ug/L NO 2.0 12/28/17 08:43 Carbon tetrachloride ug/L NO 2.0 1228117 08:43 Chloroberuene ug/L NO 2.0 1228/17 08:43 Chloroetharle ug/L NO 2.0 12128/17 08:43 Chloroform u911L NO 2.0 1228/17 08:43 Chloromethane uglL ND 2.0 1228117 08:43 cis-1,2-Dichloroethene ug/L NO 2.0 1228117 08:43 ds-1,3-Dichloropropene ug1L ND 2.0 1228117 08:43 Dibromochforomethane ug/L ND 2.0 1228117 08:43 Ethylbenzene ug►L ND 2.0 1228/17 08:43 Methylene Chloride ug1L NO 2.0 1228/17 08:43 Tetrachloroethene ug/L ND 2.0 1228117 08:43 Toluene ug/L- NO 2.0 12/28/17 08:43 trans-1,2-DicNaroethene ug/L NO 2-0 12/28/17 08:43 trans-1,3-Dichioropropene ug1L ND 2.0 12/28/17 08:43 Trichioroethene ug1L NO 2.0 1228117 08:43 Trichlorotluorornethane ug/L ND 2.0 12128/17 08:43 Vinyl chloride ug/L ND 2.0 1228117 08A3 1,2-Dichioroethane-d4 (S) % 92 70-130 1212R117 08:43 4-Bromailuorohenzene (S) % 95 70-130 1228/17 08:43 Toluene-d8 (S) % 102 70-130 1228/17 08A3 LABORATORY CONTROL SAMPLE 2177867 Qualifiers Pace Ana"cal Services, LLC 9800 Kincey Ave- Suite 100 Hurhtersville, NC 28070 (704)87"092 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers 1.1,1-Trichioroethane uglL 20 .. ,..-_.. 18.0--.....-...._._._......go ............... 52-162 1,1,2,2-Tetrachloroethane u91L 20 192 96 46-157 Bosuns prase .. an this pope are In the unto Indicated by the "Un W column mc" wthare an alte unit Is praaerAed to the right or the mault REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, axwpl m W. Date: 1229/2017 04A7 PM without Ithe written consent of Pace Analytical Services, LLC. Page 17 of 31 ceAnalytical warstpaw�ibecwn i QUALITY CONTROL DATA Project: Colfax Stormwater Pace Project No.: 92367956 LABORATORY CONTROL SAMPLE: Parameter 21T7867 Units Spike Coric. LCS Result LCS % Rec % Rec Limits 1,1,2-Trichloroethane ug/L 20 17.1 86 52-150 1,1-Dichloroethane ug/L 20 15.7 79 59-155 1,1-Dichloroethene ug/L 20 17.7 86 1-234 1,2-Dichloroberizene ug/L 20 20.5 103 18-190 1,2-Dichloroethane ug/L 20 17.9 90 49-155 1,2-Dichloropropane ug/L 20 17.6 88 1-210 1,3-Dichlorobenzene ug/L 20 20.6 103 59-156 1,4-Dichlorobenzene ug/L 20 20.2 101 18-190 Benzene ug/L 20 17.1 85 37-151 Bromodichloromethane ug/L 20 17.1 86 35-165 Bromoform ug/L 20 20.7 104 45-169 Bromomethane ug/L 20 19.2 96 1-242 Carbon tetrachloride ug/L 20 16.7 84 70-140 Chloroberizene ug/L 20 19.6 98 37-160 Chtoroethane ug1L 20 19.4 97 14-230 Chloroform ug/L 20 16.2 81 51-138 Chloromethane ug/L 20 15.7 79 1-273 cis-1,2-0iehloroethene U91L 20 15.9 79 68-146 cis-1,3-Dichloropropene ug/L 20 18.1 91 1-227 Dibromochloromethane ug/L 20 19A 97 53-149 Ethylbenzene ug/L 20 192 96 37-162 Methylene Chloride ug/L 20 14,9 75 1-221 Tetrachloroethene ug/L 20 19,7 99 64-148 Toluene ug/L 20 16.7 83 47-150 trans-11,2-Dichloroethene ug/L 20 16.8 84 54-156 trans-1,3-DicNoropropene ug/L 20 16.9 84 17-183 Trichloroethene ug/L 20 17.7 89 71-157 Trichlorefluoremethane ug/L 20 17A 87 17-181 Vinyl chloride ug/L 20 16.7 84 1-251 1,2-Diehloroethane-d4 (S) % 92 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8 (S) % 85 70-130 Pace Analytical Services, LLC 9800 Kncey Ave Suite 100 Hurtersv0c, NC 28078 (704)875-9092 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2178156 2170157 MS MSD 92367867001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone Conc. Result Result % Rec % Rec Limits RPD Qual 1,1,1-Trichloroethane ug/L NO 20 20 18.9 21.0 94 105 46-171 11 1,1,2,2-Tetrachloroethane uglL NO 20 20 17.4 18.8 87 94 73-159 8 1,1,2-Trichloroethane ug/L NO 20 20 23.6 19,3 118 97 64-152 20 1,1-Dichloroethane ug/L ND 20 20 16.3 18.8 82 94 43-172 14 1,1-Dichloreethene ug/L NO 20 20 21.3 23.4 106 117 48-189 9 1,2-Dichlorobenzene ug/L ND 20 20 20.0 19.7 100 98 54-154 2 1,2-Dichlorcethane ugh.. ND 20 20 17.6 20.3 88 101 42-171 14 1,2-Dichiampropene ugfL NO 20 20 20,6 23.2 103 116 55-157 12 RfaWts presented on this page are In Me units InWcated by the "Units" eolurrm Kept vgwm an aeanmte unit is prswW to the right of tha result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full. Date: 12129/2017 04:47 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 31 Z,42,CeAnaocale wrrpsc�wm x DUALITY CONTROL DATA Project: Colfax Stomiwater Pace Project No.: 92367956 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2178156 Parameter 92367867001 Units Result MS Spike Conc. 1,3-Dichlorobenzene ug/L NO 20 1,4-Dichlorohenzene ug/L NO 20 Benzene ug/L NO 20 Bromodichloromethane ug/L NO 20 Bromoform ug/L NO 20 Bromomethane ug/L NO 20 Carbon tetrachloride ugiL NO 20 Chlorobenzene ug/L ND 20 Chloroethane ug/L NO 20 Chloroform ug/L ND 20 Chloromethane ug/L NO 20 cis-1,2-Dichloroethene ug/L NO 20 cis-1.3-Dichloropropene ug/L NO 20 Dlbromochloromethane ugA- ND 20 Ethylbenzene ug/L ND 20 Methylene Chloride ug/L NO 20 Tetrachlorcethene ug/L ND 20 Toluene ugti NO 20 trans-1.2-Dichloroettme ug/L NO 20 trans-1,3-Dichlompropene ug/L NO 20 Trichloroethene ug/L ND 20 Trichlorofluoromethane ug/L NO 20 Vinyl chloride ug/L ND 20 1,2-Dichloroethane-d4(S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % Pace Analytical Services, LLC 9800 KlnceyAve. Suite 100 Hunter Ae, NC 2so7B (704)875-9092 MSD Spike Conc. 2178157 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD 20 20,7 21.0 104 105 57-148 1 20 20.7 20.3 103 101 58-149 2 20 19.0 20.4 95 102 54-163 7 20 20.0 21.8 100 109 56-152 8 20 19.1 20.2 95 101 53-151 6 20 17A 20.2 87 101 10-200 15 20 20.4 21.6 102 108 41-175 6 20 21.7 21.4 109 107 67-152 2 20 24A 26.8 122 134 23-200 9 20 17.2 19.5 86 98 51-166 13 20 16.8 19.9 84 100 40-175 17 20 17.1 19.3 85 97 45-174 12 20 22.5 19.8 112 99 38-146 13 20 19.9 20.8 100 104 65-144 4 20 21.5 21A 108 107 57-152 1 20 14.9 16.6 74 83 40-167 11 20 22.2 22.8 111 114 59-155 3 20 22.9 192 115 95 47-162 18 20 16.7 19.0 84 95 47-178 13 20 22.1 19.5 110 97 39-148 13 20 23.0 22.0 115 110 60-153 4 20 21.0 22.7 105 113 42-199 6 20 20.4 23.0 102 115 46-176 12 86 100 70-130 93 99 70-130 107 89 70-130 Aesulte prastnhd an thbr page ■rs In the units Indiested by 9w -Unit' column ex upt Ware an dhmate unit Is prmlhd to the HGM of "Is weal!. REPORT OF LABORATORY ANALYSIS This report shag not he reproduced, except in full. Date: 12/29=17 04:47 PM wid=A the wrftn consent of Pace Ana"cai Services, LLC. Qual Page 19 of 31 2ce Analytical" teurpaC@4b&ccra I QUALITY CONTROL DATA Project: Colfax Stormwater Pace Project No.. 92367956 QC Batch: 392085 QC Batch Method: EPA 3510 Associated Lab Samples: 92367956001 Analysis Method: EPA 608 Analysis Description: 608 GCS Pest PCB METHOD BLANK 2175428 Matrix: Water Associated Lab Samples: 92367956001 Blank Reporting Parameter Units Result Limit Analyzed 4,4'-DDD ug/L NO 0.050 12122/17 21:21 4,4'-DDE ug/L NO 0.050 12122/17 21:21 4,4'-DDT ug& ND D.050 12122/17 21:21 AJdnn ug/L NO 0.050 12122/17 21:21 alpha-BHC ug/L NO 0.050 12122/17 21:21 beta-BHC ug/L ND 0.050 12/22/17 21:21 Chlordane (Technical) ug/L NO 0,50 12=17 21:21 delta-BHC ugfL ND 0,050 1=1721:21 Dieldrin ug/L NO 0.050 12/22/17 21:21 Endosulfan I ug/L NO 0,050 12/22/17 21:21 Endosulfan 11 ug/L ND 0.050 12/22/17 21:21 Endosulfan sulfate uglL NO 0.050 12/22/17 21:21 Endrin ug/L NO 0,050 12/22/1721:21 Endrin aldehyde ug/L NO 0,050 12/22/17 21:21 gamma-BHC (Undane) ug/L NO 0,050 12/22/17 21:21 Heptachlor ug/L NO 0.050 12/22/17 21:21 Heptachlor epoxide ug/L NO 0.050 12r22/17 21:21 PCB-1016 (Arodor 1016) ug/L NO 0.50 12/22/17 21:21 PCB-1221 (Arodor 1221) ug/L NO 0.50 12/22/17 21:21 PCB-1232 (Aroclor 1232) ug/L NO 0.50 12/22/17 21:21 PCB-1242 (Arodor 1242) ug/L NO 0.50 12122/17 21:21 PCB-1248 (Aroclor 1248) ug/L NO 0.50 12/22/17 21:21 PCB-1254 (Arodor 1254) ug/L NO 0.50 12122/17 21:21 PCB-1260 (Arodor 1260) ug/L NO 0-50 1222/17 21:21 Toxaphene ug/L NO 0-50 12Y22117 21:21 Decachlorobiphenyl (S) % 99 20-138 1222/17 21:21 Tetrachloro-m-xytene (S) % 81 20-110 12f22117 21:21 Qualifiers Pace Analytical Swvic es, LLC 9900 Kincey Ave. Suite 100 Huntemville. NC 28070 (704)8759092 LABORATORY CONTROL SAMPLE & LCSD: 2175429 2175430 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 4,4'-DDD ug/L .25 0.22 0.22 87 87 31-141 0 30 4,4'-DOE ug/L .25 0.21 0.20 84 80 30-145 4 30 4,4'-DDT ug/L .25 0.22 0.22 89 89 25-160 0 30 Aldrin ug/L .25 0.19 0.17 76 68 42-122 12 30 atpha-BHC ug/L .25 0-18 0.16 72 63 37-134 13 30 beta-BHC u91L .25 0.16 0.15 66 60 17-147 10 30 delta-BHC ug/L .25 0.21 0.19 86 78 19-140 10 30 Dieldrin ug/L .25 0.20 0.19 81 77 36-146 5 30 Endosulfan I ug/L 25 0,21 0.19 83 78 4&153 6 30 Rasutts presented on ifs page ■re In the units Inereated by thew+eta• column except wlwrr an mamma Lmlt Is pnmen d to the fight of the reWt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1 Z29/2017 04:47 PM withctd the written ranarnt of Pace Analytical Servk=. LLC, Page 20 of 31 nalyfical �sG wvwcpepeimba.wm i 1 Project: Colfax Stomn+vater Pace Project No.: 92367956 LABORATORY CONTROL SAMPLE & LCSD: 2175429 Parameter Endosulfan II Endosuifan sulfate Endrin Endrin aldehyde gamma-BHC (Lindane) Heptachlor Heptachlor epoxide DecacHarobiphertyl (S) Tetrachloro-nt-xylene (S) Units ug/L ug1L ug/L uglL ug/L ug/L ug/L. % % QUALITY CONTROL DATA Spike Cane 2175430 LCS LCSD Result Result LCS LCSD % Rec % Rec. % Rae Limits 25 0.21 0,21 85 86 1-202 .25 0.23 0.23 91 92 26-144 .25 0.22 0.20 87 82 30-147 :25 0,19 0.18 78 74 50-150 .25 0.19 0.17 76 67 32-127 ,25 0,19 0.16 78 67 34-111 :25 0.20 0:19 82 75 41-126 94 97 20-138 89 76 20-110 Pace Analytical Services, LLC 9800 1Gncey Ave. Suite 100 Hunterswlle, NC 28073 (7a4)875-9092 Max RPD RPD Quafifiers 1 30 1 30 6 30 5 30 12 30 16 30 10 30 rtaudb pnseshd on Oft papa are to thw untls Irmucalai M the -Units" column except wdmn on ■nem.ta unit laprementadto the rWH after rogat. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 12R9/2017 04.47 PM without the written consent of Paco Anayticiiil Services, LLC. Page 21 of 31 Ana"cal e t QUALITY CONTROL DATA Project: Colfax Stormwater Pace Project No.: 92367956 QC Batch_ 392115 QC Batch Method: EPA 625 Associated Lab Samples: 92367956001 Analysis Method: Analysis Description EPA 625 625 MSS METHOD BLANK: 2175540 Matrix: Water Associated Lab Samples: 92367956001 Blank Reporting Parameter Units Result Limit Analyzed 1,2,4-Trichlorobenzene U91L ND 5.0 12/26117 22:00 2,2'-Oxybis(i-chloropropane) u91L ND 5.0 12/26117 22:00 2,4,6-Trichlorophenol ug/L NO 10.0 12126/17 22:00 2,4-Dichlorophenol ug1L NO 5.0 12/26/17 22:00 2,4-Dimethylphenol ug/L NO 10.0 12/26/17 22:00 2,4-Dinitrophenol ug1L ND 50-0 12/26/17 22:00 2,4-Dinitrotoluene ug1L ND 5-0 12/26/17 22:00 2,6-Dinitrotoluene ug1L ND 5.0 12/26/17 22:00 2-Chloronaphthalene ug/L ND 5.0 12/26/17 22:00 2-Chlorophenol ug/L ND 5.0 12126/17 22:00 2-Nitrophenoi ug/L ND 5.0 12r26117 22:00 3,3'-Dichlorobenzidine ug/L ND 25.0 1212EV17 22:00 4,6-Dinitro-2-methylphenol ug/L ND 20.0 12126/17 22:00 4-Bromophenylphenyl ether U91L NO 5.0 12/26117 22:00 4-Chloro-3-methylphenoi ug/L ND 5.0 12f26117 22:00 4-Chlorophenylphenyl ether 4L ND 5.0 12/26/17 22:00 4-Nitrophenol ug/L ND 50.0 12/26117 22:00 Acenaphthene ug/L NO 5.0 12/26117 22:00 Acenaphthylene ug/L ND 5.0 12126117 22:00 Anthracene ug1L NO 5.0 12126/17 22:00 Benzo(a)anthracene ug/L NO 5.0 12/26/17 22:00 Benzo(a)pyrene ug1L ND 5.0 12/26/17 22:00 Benzo(b)fluoranthene u91L NO 5.0 12126/17 22:00 Benzo(g,h,e)perylene ug/L ND 5.0 12/26H7 22:00 Benzo(k)fluoranthene ug/L ND 5A 12/26/17 22:00 bis(2-Chlaroethoxy)methane ug/L ND 10.0 12/26/17 22:00 bis(2-Chloroethyl) ether LKA ND 5.0 12/26117 22:00 bis(2-Ethylhexyl)phthalate ug/L ND 5.0 12/26/17 22:00 Butylbenzylphthalate ug/L ND 5.0 12/26/17 22:00 Chrysene ug/L ND 5.0 12/25117 22:00 Din-butylphthalate u91L ND 5.0 12/26/17 22:00 DH-n-octylphthalate ug1L ND 5.0 12/2&17 22:00 Diberiz(a,h)anthracene ug1L ND 5.0 1212&1722:00 Diethytphthalate ug/L ND 5.0 12/26/17 22:00 Dimethylphthatate ugA- ND 5.0 12/26/17 22:00 Fluoranthene ug1L ND 5.0 12/26/17 22:00 Fluorene ug/L ND 5.0 12/26/17 22:00 Hexachloro-1,3-butadiene ug/L ND 5.0 12126/17 22:00 Hexachlorobenzene ug/L ND 5.0 12/25117 22:00 Hexarhicrocyclopentadiene ug/L ND 10-0 12/2&17 22:00 Hexachloroethane ug1L NO 5.0 12126117 22:00 Qualifiers Pace Analy4al Services, LLC 9800 KinceyAve. Suite 100 Huniereville, NC 28078 (704)875-9092 Resrtts prnerded co (Wa page an In the units IndlcatM by the "Units' column except whore an ahemab unit to presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shag not be reproduced, toctept in full, Date: 12/2912017 04:47 PM without the written consent or Pace Analytical Services, LLC. Page 22 of 31 W eAnalytical' sn►ttcpecbffaf>¢tam t QUALITY CONTROL DATA Project: Colfax Stormwater Pace Project No.: 92367956 Pace Anal So. vitee, L LC 9600 KlnoeyAve, Suibe 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK 2175540 Matrix: Water Associated Lab Samples: 92367956001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Indeno(1,2,3-cd)pyrene ug/L NO 5.0 1226/17 22:00 Isophorone ug/L NO 10.0 1226117 22:00 N-Nitroso-di-n-propylamine uglL NO 5.0 12126117 22:00 N-Nitrosodimethylamine uglL NO 5.0 1226/17 22:00 N-Nitresodiphertylamine ug/L ND 10.0 12/26/17 22:00 Naphthalene ug/L ND 5.0 1226117 22:00 Nitrobenzene ug4- ND 5.0 1226117 22:00 Pentachlorophenol ug/L ND 10.0 12/26/17 22:00 Phenanthrene ug/L NO 5.0 1226117 22:00 Phenol u911- NO 5.0 1226,r17 22:00 Pyrene ug/L NO 5.0 12126/17 22:00 2,4,6-Tdbromophenol (S) % 91 10-137 12126117 22:00 2-Fluorobiphenyl (S) % 76 15-120 1226117 22:00 2-Fluorophenol (S) % 42 10-120 12/26/17 22:00 NitrobenzeneA5 (S) % 82 10-120 12/26/17 22:00 Phenol-d6 (S) % 27 10-120 1226117 22:00 Terphenyt-d14 (S) % 73 11-131 12/26/17 22:00 LABORATORY CONTROL SAMPLE & LCSD: 2175541 2175542 Spice LCS LCSD LCS LCSD % Rec Max Parameter Units Conc, Result Result % Rec % Rec Limits RPD RPD Qualifiers 1,2,4-Tdchlorober¢ene ug/L 50 37.3 35.2 75 70 44-142 6 30 2,7-Oxybis(1-chloropropane) u91L 50 33.7 32.4 67 65 36-166 4 30 2,4,6-Trichlorophenol ugfL 50 43A 30.1 86 60 37-144 35 30 R1 2,4-Dichlorophenol u91L 50 42.2 36.7 84 73 1-191 14 30 2,4-Dimethylphenol ug/L 50 38.6 38A 77 76 32-119 1 30 2,4-Dinitrophenol ug/L 250 156 97A 63 39 1-181 47 30 R1 24-Dinitrotoluene ug/L 50 53A 43.7 107 87 39-139 20 30 2,6-Dinitrotoiuene LKA 50 48.3 45.4 97 91 50-158 6 30 2-Chiaronaphthalene ug/L 50 38.8 38.5 78 77 60-118 1 30 2-Chlorophenol ug/L 50 37.2 33.8 74 68 23-134 10 30 2-Nitrophenol ug/L 50 43.8 34.9 68 70 29-182 22 30 3J-Dichlorobenzidine ug/L 100 96.5 90.4 96 90 1-262 7 30 4,6-Diroo-2-methylphenol ug/L 100 75.8 53;9 76 54 1-181 34 30 R1 4-Bromophanylpher yl ether ug1L 50 39.3 41.6 79 83 53-127 6 30 4-Ctdoro-3-methylphenot ug/L 100 91.1 87.6 91 88 22-147 4 30 4-Chioraphenrlphenyl ether ug1L 50 45.3 41.5 91 83 25-158 9 30 4-Nitrophenol ug/L 250 97.5 53.9 39 22 1-132 58 30 R1 Acenaphthene ug/L 50 43.3 40.3 , 87 81 47-145 7 30 Acenaphtr&ne ug/L 50 43.7 41.8 87 84 33-145 4 30 Anthracene ug/L 50 45.1 43.2 90 86 1-166 4 30 13enzo(a)anthracene ug/L 50 44.1 42.6 88 85 33-143 4 30 Benzo(a)pyrene ug/L 50 46.7 45.8 93 92 17-163 2 30 Bertzo(b)fluorardhene ug1L 50 45.9 44.2 92 88 24-159 4 30 Rmulta presentad on this page am In the urdts Indlcaeed by tha -Units" wlrmm except when an saemate unR is presented to the rlght of the resutt. REPORT OF LABORATORY ANALYSIS This report ahetl not be reproduced, except in full, Date: 12/2912017 04:47 PM without tt,e written consent of Paw A"Vfti=W Services, LLC, Page 23 of 31 eeAnalytical' wevepacefadsCom QUALITY CONTROL DATA Project_ Colfax Storrrwvater Pace Project No.: 92367956 Pate Analyticai Services, LLC 9800 Kincey Ave, Suite 100 Hunicrsville, NC 28078 (704)8759092 LABORATORY CONTROL SAMPLE & LCSD: 2175541 Parameter Units Spike Cone 2175542 LCS LCSD Result Resutt LCS LCSD % Rec % Rec % Rec Limits RPD Max RPD Qualifiers Benzo(g,h,i)perylene Ug/L 50 44.3 42.8 89 86 1-219 3 30 Senzn(k)fluoranthene ugll- 50 44.9 45A 90 91 11-162 1 30 bis(2-Chloroethoxy)methane ug/L 50 42.7 40.1 85 80 33-184 6 30 bis(2-Chlaroethyl) ether ug/L 50 40.7 40.6 81 81 12-158 0 30 bis(2-Ethylhexyl)phthalate U911- 50 46.1 47.1 92 94 8-158 2 30 Butylbenzylphthalate ug/L 50 47.3 49.1 95 98 1-152 4 30 Chrysene UgIL 50 44.4 42.7 89 85 17-168 4 30 Dkrl-butylphthalate Ug/L 50 46.9 44.8 94 90 1-118 5 30 Di-n-octylphthalate ugli- 50 57.6 54.7 115 109 4-146 5 30 Dibenz(a,h)ardhracene ug/L 50 46.7 45.9 93 92 1-227 2 30 Diethytphthalate uglL 50 47.5 43.8 95 88 1-114 8 30 Dimethylphthatate ugJL 50 44.8 41.4 90 83 1-112 8 30 Fluoranthene LOL 50 47.0 42.2 94 84 26-137 11 30 Fluorene Ug/L 50 50.8 43.9 102 88 59-121 14 30 Hexacttloro-1,3-butadiene ug1L 50 36.1 33.2 72 66 24-116 8 30 Hexachlorobenzene Ug/L 50 41.5 42.1 83 84 1-152 1 30 Hexac hlorocyclopentadiene Ug/L 50 20.5 21.5 41 43 25-150 5 30 Hexachloroethane ug/L 50 31.2 30.4 62 61 40-113 3 30 Indeno(1,2,3-cd)pyrene ug1L 50 43.6 42.0 87 84 1-171 4 30 Isophorone ug/L 50 42.2 39.8 84 80 21-196 6 30 N-Nitroso-di-n-propylamine Ug/L 50 39.3 38.3 79 77 1-230 3 30 N-Nitrosodimelhytamine. Ug/L 50 26.5 26.3 53 53 25-150 1 30 N-Nttrosodiphenylamine ug/L 50 39.7 40.8 79 82 25-150 3 30 Naphthalene ug/L 50 39.2 37.0 78 74 21-133 6 30 Nitrobenzene 1-191L 50 43.9 39.7 88 79 35-180 10 30 Pentachlorophenol UVL 100 83.1 56.6 83 57 14-1T6 38 30 R1 Phenanthrene Ug/L 50 43.5 42.0 87 84 54-120 4 30 Phenol Ug1L 50 17.4 17.1 35 34 5-112 1 30 Pyrene ug/L 50 41.3 43.1 83 86 52-115 4 30 2,4,6-Tribromophenol (S) % 92 69 10-137 2-Fluorobiphenyl(S) % 76 74 15-120 2-Fluorophenol (S) % 45 38 10-120 Nitrobenzene-d5 (S) % 88 82 10-120 Phenol-d6 (S) % 29 28 10-120 Terphenyi-d14 (S) % 75 85 11-131 Rmdto presentsd on M papa an In the units IndbesW by Me -Urdts^ column except w1m an aRarnsh unit Is presented to the right or the reeutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in toil, Dale: 12129MI7 04:47 PM without the written consent at Pace Analytical' Services, LLC, Page 24 of 31 N c.eAnayical wnrcaoelaba.tam Project: Cotfax Stormwater Pace Project No.: 92397956 QC Batch: 392427 QC Batch Me6lod: SM 2540D Associated Lab Samples: 92367956001 METHOD BLANK: 2176880 Associated Lab Samples: 923679WO01 Parameter Total Suspended Solids QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 25400 Total Suspended Solids Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers mglL ND 2.5 12/27/17 08:50 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28079 (704)875-9092 LABORATORY CONTROL SAMPLE: 2176881 Spike LCS LCS % Rec Parameter Units Conc, Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 250 100 90-110 SAMPLE DUPLICATE: 2176a82 92367956001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 28.4 29.0 2 SAMPLE DUPLICATE: 2176883 92367981005 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 16A 17.5 7 D6 Result prven7rtl en this page am In Cn utdts indicaW e7 the'LNts" cWu m excw teams m attemats untt is praenoa to tM dpht or the Rauh REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, c=pt in fill, Dale: 12/29/2017 04:47 PM without the wnwn eeavent of Pam Atmlytical Services, LLC.: Page 25 of 31 Pass Analytical Serviras, LLC ( � Wcal a 9900 Kinsey Ave. Suite 100 � �1J/`�'11K1 Hunieraville, NC 28078 (704)875-9092 f 3 QUALITY CONTROL DATA Project: Coifmr Stomwwater Pace Project No.: 92367956 l QC Batch: 392108 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lai, Samples. 92367956001 SAMPLE DUPLICATE: 2175511 92367960001 Dup Parameter Units Result Result RPO Qualifiers pH Std. Units 7.0 7.0 1 H6 SAMPLE DUPLICATE: 2175612 92367997004 Dup Parameter Units Result Result RPD Qualifiers pH Std. Units 6.9 6.9 0 H6 Reauth presented an" page are In the unita tntlkatad by ON -Unitr wlumn aanpt When an aaamate unit is Pnaanead to me right artt» resutL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, exoept in W, Date: 12 /2017 04:47 PM without the written consent of Pace Ana"cai Services. LLC. Page 26 of 31 Pace Analytical Semiaes, LLC ��r�t� 00 N ��cal 9800 Ki nt ey Ave. Suite 100 VG Hunberavitle, NC 28078 y e b� mm (704)975-W92 1 s QUALIFIERS Project Colfax Stomrwater Pace Project No.: 92367956 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit POL- Practical Quantitation Limit. RL - Reporting LimiL S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration.. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrtle by EPA Method 8260. N-Ni rosodiphenylamine decomposes and cannot be separated from DipherTylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical Is TNI accredited. Contact your Pace PM for the current fist of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA requtred holding lime. R1 RPD value was outside control Writs - REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, enept in full, Date: 12/29/2017 04:47 PM without the written consent of Pace Analytical Services, LLC, Page 27 of 31 �A aocal* W WWPe®Ivb& WM F QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Anslytieal Servieea, LLC 9800 Kincey Ave, Suite 100 Hurdersas, NC 25078 (7D4)875-9092 Project: Colfax StonTmater Pace Pr*ct No.: 92367956 Analytical Lab ID Sample ID QC Batch Method QC Hatch Analytical Method Batch 923679S6001 SDO-04 EPA 1664E 392579 92367956001 SOO-04 EPA 3510 392085 EPA 608 92367956001 SOO-04 EPA2001 392548 EPA200.7 92367966001 SDO-04 EPA 625 392115 EPA 625 92367956001 SDO-04 EPA 624 392648 92367956001 SDO-04 SM 2540D 392427 92367956001 SOO-04 EPA 9040 392108 Date: 12f1912017 04:47 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pau Analytical Services, LLC. 392129 392596 392339 Page 28 of 31 Document Name: Document Revised: August 4, 2017 Sample Condition Upon Recel t(SCURi Pa e 1 of 2 jARci�fCBr Document No.: ! Issuing Authority: r F-0AR-CS-033-Rev.04 ( Pace Quality office Laboratory receiving samples: Asheville Q Edeno Greenwood Huntefsville?�' Raleigh❑ Mechannii[sviilen . Client Name: 11 WO# , 9i 236.. 5Q Project te; _ I Courier: ❑fe Ex J ❑UP5 ❑i15P5 ❑Client III 11111111111111111ommercial ace ❑Other: Zr custody Seal Present? ❑yes [INC'" Seals intact? ❑Yes EfN'o �!f 1 `Date/Inlilals Person Examining Contents:`'+ Packing Material: []Bubble Wrap ❑ bble Bags ❑None ❑ Other Blatagical Tissue Frozen? Thermometer; ❑yes ❑No [�JA ❑ IR Gun ID: l t.tJ._. Type of tee_ Wet ©81ue ❑None Correction Factor: Cooler Temp Corrected ('Cj: c . , Temp should be above freezing to 6'C - []Samples out of temp criterta.5amples an ice, cooling process has begun USDA Regulated Soil ( Q N/A, water samplel Did samples ororsAte In a quarantine zone within the United 5tates: CA, NY, or SC (check mapsi? Did samples originate from a foreign source (in; natty, f-7v� . r -Tm mrtnEin� rtawaii an 1 Vnertn RIra17 t—lybS He Commenu/Disve anev: Chain of Custody Present? fTfts No N/A 1. Samples Arrived within Hold 'f1me7 ON. N A 2. Short Hold Time Analysis 0Z hr.)? OYeJ No ❑NIA 3. Rush Tom Around Times Requested? O�/va% Na IA- 4. Sufficient Volume? pKrz ❑No ❑N(A S" Correct Containers Used? -Pace Containers Used? Yes es ON. ONo QN/A N A 6. Containerslntact? 05, ON. N/A 7. Dissolved ana "s: Samples Field Filtered? Oyes o N/A 9. Sample Labels Match CDC? -Includes Date/Time/ID/Analysis Matriw: q3lt^ j es ' v ONO ❑N/A 9. Readipce In VOA VI915 (-15-6mm ? ❑Yes (:)NIA 10. Trip Blank Present? Trip Blank Custody Seals Present? []Yes OYes Q40 Olio ❑N/A ❑N/A 11. CLIENT NOTIFICATION/RESOLUTION Field Data Required? LiYes, LINO Person Contacted. Date/Time: Comments/Sample Discrepancy: tot ID of split containers Project Manager SCURF Review: Date: _ I'Z 11111 Project Manager SRF Review: �FDate: Note: Whenever there is a discrepancy affecting Nanh Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e, Out of hold, incorrect preservative, out of temp, incorrect containers) Page 29 of 311 N CJ 1 3 D Q 1 n a 9 n n 2 n 'x c 0 a A n Q � N o t. A v R 3 � '7 n w Y Q � a. s a O M a to N tP 3 'ro, a q Q- b fi A ;y a 6' a F� M D 3 c a n � n o n � M K n r a' Hem9 zzzzzzzzzzzz OP41.1-125 mL Plastic Unpreserved (N/A) (Ct-) BP3U-25O mL Plastic Unpreserved IN/A) $132U-500 mL Plastic Unpreserved IN/A) OPIU-1 liter Plastic Unpreserved (N/A) BP45-125 mL Plastic 1-12504 tpH c 21 (CI-) t SPIN-250 mL plastic HN01 (pH 4 2) VzBP42-125 mL Plastic TN Acetate & NaOH 1�9) zzzzzzzBP4C-125 mt Plastic NaOH IpH > 12) (Cl.) WGFU• W ide-mouthed Glass jar U n p reserved AGIU-1 liter Amber Unpreserved (N/A) (CI-) AGIH-1 liver Amber HCI (pH - 21 AMU-250mi. Amber Unpreserved (N/Al tCt-) AGIS-1 liter Amber H2504 (pH c 2) AMS-750 mL Amber H2504 tPH c 2) A631A(DGIA(-2S0 mL Amber NMCl IN/A)(CI-) OGSH-40 mL VOA HC1 (N/A) VG9T-40 mL VOA Na2S203 {NIA) VG9U-40 mL VOA Unp (N/Al 0091340 mL VOA 143PO4 (N/A) VOAK (6 vials per kit)-5035 kit tN/A) V/GK 13 vials per klt)-VPH/Gas kit (N/A) SPST-125 mL Sterile Plastic (N/A —lab) SP2T-250 MIL Sterile Plastic (NIA — lab) 0P3A-250 mL Plastic (NH2)2SD4 (93.9.7) Cubitainer VSGU-20 mL Scintillation vlais (N/A) GN w Ul Cn CHAIN -OF -CUSTODY I Analytical Request Document Fr' 1 he Chm1n-cl-Cus?cdy is e 1 FCAL UOCU EN1. AN lelemit fields must be complrlr_d accutately. Suction A Section R Section G R1rquked C14-nI hllormm ICn: Required Prgjvet IntmrnallOd: !Huck- Ini—jr— Pano°• 1 (W Cnm{•r.nY 51: c'❑ Ftcleur, l u U:n-HLlnl kt:• rG.en - - .... . Arrlcr: C; Tsnnu•1 Creak Rego ., ._ .. CODY to ., company Name CIm,lsmm NC ,bjCe Ru II Agem EmcIP uhitncrp: _:,�r c,nraodi-nnu edm - - ........ .. Nackiple owr r •I;jbC* Pare Ouotc pncnr, ,; Oc1�L--'A-1:i Fa■ —4111 Prcj^L. Now'c, .wryiW, :rn •la•'! PmiOO N ... „ _.. PIK,) Prejecl Muriagart nimle di.fr0rcwsw: cr'wlnlls ecm, _. ... 5lare r Location Rc:.rayt,: a D— Oc:c ...., .... 1`101110 C 7S 11I NC '---Re uested Anil siF Filirrrd (YIN) ti:r1R:r CnnE I 9; .. COLLEc1t:U. - 'Z .Preservatives } - 0'—v ow ' 4 W'- �I m 1 V NwI 'd rr W. I e • q Lo Lo s b R �r x..�n al SAMPLE ID� ,' o START END w t- One Cherecler per bo=. >'N•r• wo :w n u� a w c (A-Z. 0.9! -1 AIR dr. of Semple Ids must be unique T11ATLTI111DAME t' O Y nl V OR' - i M TIME u'� • rSl S 2; Z I H r QI w rc pia K �✓• 5 C C wT 4 1 L. 3 X X % X X X X c c3 A WT 1 % % X X 7 6 7 E 9 ,6 T1 ,z ADOMMALCOMMENTS AEUNCtUIS11E0 aY 1 A"ILrATIDN DATE TIME ACCEPTrDmYrA"1u AT10N DATE TIME SAMPLE LONDIrlONS ref A I , . m SAMPLER NAME AND "NATURE W V F 0 �; PRINT laamri gt!A►'RL£R: cc p wI „ 0 o 5 i w SIGNATURE of $AMPL.ERI J,,•' -DATIL Signed:. A, Z ! .� Er 8 t] -r. Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 12 13 17 CERTIFICATE OF COVERAGE No.'N00030293 Rt��,jC SAMPLE COLLECTION YEAR 2017 FACILITY NAME Colfax IMO Industries Inc. 1�i E PERIOD ❑ Jan -June ❑ July -Dec PERSON COLLECTING SAMPLES NLA JAN p z�r or ® Monthly' November LABORATORY: N/A Lab Cert. # WACHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA Comments on sample collection or analysis: No sample collected duet r pRMgT10NPROPROCESSING trNi DWR,3ECT/ON ❑Zero -flow ❑Water Supply []SA�`� rain events outside of business hours, on weekends, or within 72 hours of ®Other_Class C — Dry Fork Creek the last rain event. PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 Part A: Stormwater Benchmarks and Monitoring Results ❑ No discharge this period? Outfall No. Date Sample p Collected' (mo/dd/yr) 24-hour rainfall amount, inches3 Total Suspended Solids p H, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks ===> - - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L i mg/L SDO 004 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 t Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." C O 1C Name (Print name) Title {Pri t ti I z( /..z // 7 LA0) -7 Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L" 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text. FOR PART A AND PARTS MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME; „ Mail an original and one copy ,., _ of this D MR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Dischame" reports). to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 11 16 17 CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME Colfax/IMO Industries, Inc. PERSON COLLECTING SAMPLES Brandon Huggins/Shield Engineering LABORATORY: Pace Analytical Lab Cert. # 12 Comments on sample collection or analysis:Benchmark exceedances for TSS_and _Cooper at SDO#004 Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' October RE �; IVECffypRGING TO CLASS ❑ORW ❑HQW [:]Trout []PNA ��--ii vv..11 []Zero -flow ❑Water Supply ❑SA NUN 27 Z017 ®Other_Class C— Dry Fork Creek CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTION 'No discharge this period?' Outfall No. Date Sample p Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids p H, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks 100 mg/L or SO mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L i mg/L SDO 004 10/16/17 0.24 5.6 7.4 0.0101 <0.005 0.0791 <5.0 <0.4873 '"Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the 5tormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, then must „ be „ „ reported in the format, "<XX mtt/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?Z Outfall No. Date Sample Collected mo/dd/ r) 24-hour rainfall amount, Inche53 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =--> - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 2 of 3 4� dF Note: If you report a sample value In excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. OR PART A AND PART g MONITORINC3-RESULTS:. • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an orlainal and one .coov of this MR. includina all wNo.Dfscharae"-reoorts, within 30 dovs of recefat:of the lab results for at end of Monitorina berlod In_the _caseot,"No Dfschame" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIF19ATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons dir t nsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I arry�+ �e that thff are sigiNficant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." / LIF-Ilk \� -) P, 117 re of Perm - (Date) Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 MCDENR Stormwater Discharge Out€all (SDO) Qualitative Monitoring Report Forguidance on filling out thisform, please visit: httorllgo�tal.nrdenr.org/we�wq6v /sulni2 Os v#t b-4 Permit No.: �/ r�/ �f r �v j or Certificate of Coverage No.: h[/f;/WQ/�/ Facility Name: cie Eck County: - t(4 i D r) Inspector: J pu rim& !i-ia {_6 rSo n _5z& Date of Inspection: 1 9- 0 Time of Inspection: `f 6 Total Event Precipitation (inches): O ie No. .. v\ Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) [J Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. I certify thattghis report is accurate and complete to the best of my knowledge: (SignaturepfFlermittee or Designee) Page 1 of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. S 0 L - 00 9 Structure (pipe, ditch, etc.) Receiving Stream: Describe the industrial activities that occur within the outfall drainage area:-M ail u-14tc !Lt -01 2. Color: Describe the color of the dilc.harge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: _ G 3. Odor: Describe any distinct odors that the weak chlorine odor, etc.): __ S}"i _�� o!f _ o cha a may have (i.e., smells strongly of oil, 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 0 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: Q 2 3 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes (Ng/ a. Is there an oil sheen in the stormwater discharge? Ye No 9. Is there evidence of erosion or deposition at the outfall? Yes N 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, last modified 10/25/2012 CHAIWOF4USTODY I Analytical Request Document The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately. r. WIT ,ws w Wm I wr SAMPLE ID R�Mliw M Ons Character per box, W.P. WP ternple Ids must be'LI'lique TUN" To r t • �„®®®®�®�,®� ICI•' h!a '��_f'hnr p'. r r m : yt ■�®�il�itf®�i����il ��®It����®®�■ k ■ ■nso®ls®®o.■ 100 0 001 monsommons mo,:m■unn11on i® :�� ■ommmmo®moso.mon ■10001®■®s®n ON ■���f�®���®����®0 ■1®111010 101 -t R ,om®.®®,sommo.s, ®0.1■®1®0.®0 MISSION go mom.-®®®®.,.,,.m 11.1.®11®0., 01110001 4`a hf}�'y^'1 ; YI.n ' •.1� ` 1 $" i. 1� I , u. '"1�p oifi ,; "'r 001 ` S- yS��-. 7 �Nf7(T�I 1 � '� {� � �. iS! �:{�f; � y �•���.......+ {wwr ceAnaVical• i J """'.pecafe6icorn October 26, 2017 Rebecca Israel Colfax Fluid Handling 1710 Airport Road Monroe, NC 28110 RE: Project: Colfax Fluid Handling Stormwat Pace Project No.: 92359523 Dear Rebecca Israel: Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersvin , NC 2807t9 {704)a7&9092 Enclosed are the analytical results for sample(s) received by the laboratory on October 17, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs_com (704)875-9092 Project Manager Endosures REPORT OF LABORATORY ANALYSIS This report shad not he reproduced, except in fug, without the written consent of PaceAnelytiral Services, LLC. Pagel of 29 Pace Analy and Services, LLC 8800 Kineey Ave. Suite 100 1!20kWcal's Huntersvilk , NC 23078 www4acewsoom (704)8759092 CERTIFICATIONS Project: GaHax Fluid Handling Stormwat Pace Project No.: 92359523 Charlotte Certification Mis 98DO i incey Ave. Ste 100, Hunlersville, NC 28078 Louisiana/NELAP Certification # 1A170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Gertificatlon #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87548 Massachusetts Certification #: M-NC030 North Carorrna Drinking Water Certification #: 37712 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirgirualVELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification # 99030001 Virginla/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report short not be reproduced, except in full, without the written consent of Pace Anaiyt=l Services, LLC. Page 2 of 29 Pace Analytical Services, LLC 'Mal"Cale a 9800 Kinsey Ave. Suite 100 Huntersviile, NC 28079 s'WW' C= (704)875-9C92 SAMPLE ANALYTE COUNT Project: Colfax Fluid Handling Stprmwat Pace Project No.: 92359523 Analytts Lab ID Sample ID Method Analysts Reported Laboratory 92359523001 SOO-004 EPA 16648 JMS I PASI-C EPA 606 PKS 27 PASI-C EPA 200.7 CDF 3 PASI-A EPA 625 RES 58 PASI-C EPA 624 GAW 34 PASI-C SM 2540D SLB t PASI-A EPA 9040 ECN 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent cf Pace Analytical Services, LLC. Page 3 of 29 Pace Aezlytiral Servfcss, LLC s 600 neyAve. Suite 100 ceMa cal Huntersville, NC 28D78 r+rW.pa�tracan (7W )B7S9092 ANALYTICAL RESULTS Project: Colfax Fluid Handling Storrnwat Pace Project No.- 92359523 Sample: S004)04 Lab ID: 92359523001 Collected: 11011161170946 Received: 1011711712:54 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1864 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons NO mg/L 5.0 1 10119/17 05:33 608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510 Atdrin ND ug/L 0.050 1 10/20/17 12:37 10/25/17 03A8 309-00-2 alpha-BHC NO ug/L 0.050 1 10/20/17 12:37 10125/17 03:48 319-84-6 beta-BHC NO u91L 0.050 1 10/20/17 12:37 1025117 03748 319-85-7 delta-BHC NO ug/L 0.050 1 10/2011712:37 1012511703:48 319-86-8 gamma-BHC (Lindane) NO ug/L 0.050 1 1020/17 12:37 10/25/17 03:48 58-89-9 Chlordane (Technical) ND ug(L 0.50 1 1020117 12:37 1025117 03:48 57-74-9 4,4'-DDD NO ug/L 0.050 -1 10120(17 12:37 10/25117 03:48 72-54-8 4,*-DDE ND ug/L 0.050 1 10120(17 12:37 10/25/17 03:48 72-55-9 M1 4,4'-DDT NO ug/L 0;050 1 1020117 12:37 1025117 03:48 50-29-3 Dieldrin NO ug(L 0.050 1. 10IM17 12:37 1 OQ5117 03:48 60-57-1 Endosulfan I NO ug/L 0.050 1 1020/17 12:37 1025117 03:48 959-98-8 Endosulfan II ND ug/L 0.050 .1 1020/17 12:37 1025117 03:48 33213-65 9 Endosulfan subte NO ug1L 0.050 1, 1020/17 12:37 1025117 WAS 1031-07-8 Endrin ND u91L 0.050 1 10/20/17 12:37 1025117 03:48 72-20-8 Endrin aldehyde NO ug(L 0.050 1 1020117 12:37 1025117 03:48 7421-93-4 Heptachlor ND ug(L 0.050 1, 1020/1712:37 1025/1703:48 76-44-8 Heptachlor epoxide NO ug1L 0,050 i 10120117 12:37 1025117 03:48 1024-57-3 PCB-1016 (Arodor 1016) ND U911L 0.50 1 1020117 12:37 1025/17 03:48 12674-11-2 PCB-1221 (Arodor 1221) NO u91L 0.50 1 1020117 12:37 10/25117 03:48 11104-28-2 PCB-1232 (Arodor 1232) ND LKA 0.50 1 1020117 12:37 1025/17 03:48 11141-16-5 PC13-1242 (Arodor 1242) NO ug/L 0,50 1 1020/17 12:37 1025117 03:48 53469-21-9 PCB-1246 (Arodor 1248) ND ug1L 0.50 1 1020117 12:37 101251V 03:48 12672-29-b PCB-1254 (Arodor 1254) NO ug/L 0.50 1 10/20/17 12:37 10/25/17 03:48 11097-69-1 PCB-1260 (Arodor 1260) NO ug/L 0.50 1 10/20/17 12:37 1025117 0148 11096-82-5 Toxaphene ND ug/L 0.50 1 1020/17 12:37 1025117 0148 8001-35-2 Surrogates Tetrachloro.m-xylene (S) 59 % 20-110 1 10/20/17 12:37 1025117 03:48 877-09-8 Decachlorobiphertyl (S) 23 % 20-138 1 1020/17 12:37 1025/17 03:48 2051-24-3 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 10.1 ug(L 5.0 1 10/18/17 20:15 10/19/17 19:17 7440-50-8 Lead ND ug/L 5.0 1 10/18/17 20:15 10/19/17 19:17 7439-92-1 Zinc 79.1 ug(L 10.0 1 10/1all 7 20:15 10/19/17 19:17 7440-6" 625 MSSV Analytical Method: EPA625 Preparation Method: EPA625 Acenaphthene ND u911- 5.0 1 10119/17 15:30 1022/17 06:41 83-32-9 Acenaphthylene ND ug1L 5,0 1 10119/17 15:30 1022117 06:41 208-96-8 Anthraoene NO ug/L 5,0 1 10/19/17 15:30 10/W17 06A1 120-12-7 Benzo(a)anthracene ND ug/L 5.0 1 10119/17 15:30 1022117116:41 W55-3 Bertzo(a)pyrene ND ug/L 5.0 1 10119/17 15:30 1022117 06:41 50-32-8 Benzo(k)fluoranMene ND ug/L 5.0 1 1WI911715:30 1022/1706:41 205-99-2 Benzo(g,hj1perylene NO ug/L 5.0 1 1011911715:30 1012211706:41 191-24-2 Benzo(k)fluorartthene NO u91 5.0 1 10/19/17 15:30 1022117 06:41 207-08-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in NO, Date: 10/26/2017 04:57 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 29 Pace Analytical Services, LLC a100 cmnaVical' 9800Hun� v e, CPqncey Ave, ut 078 """4uKAbbs-cDm (764)875-9092 ANALYTICAL RESULTS Project: Colfax Fluid Handling Stormwat Pace Project No.: 92359523 Sample_ SDO-004 tab ID: 92359523001 Collected: 10/16/17 09:46 Received: 10/17117 42:54 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 625 MSSV Analytical Method: EPA625 Preparation Method: EPA625 4-Bromophenylphenyl ether NO ug/L 5.0 1 10119/17 15:30 10122/17 06:41 101-55-3 Butylbenzylphthalate NO ug/L 5.0 1. 10119/1715:30 10/22/17 06:41 85-68-7 4-Chlom-3-methylphenoi NO ug/L 5.0 1 10119117 15,30 10/22/17 06:41 59-50-7 bis(2-Chloroethoxy)methane NO ug/L 10.0 1 10119117 15:30 1012211706:41 111-91-1 bis(2-Chtaroethyo ether NO ugA- 5.0 1 10/19/17 15:30 10/22117 0&41 111 444 2-Chloronaphthatene NO uglL 5.0 1 10/19/17 15:30 10122/17 06:41 91-58-7 L2 2-Chlorophenol NO ugJL 5.0 1 10/19/17 15:30 10/22/17 06:41 95-57-8 4-Chlorophenylpt"l ether NO ug/L 5.0 1 10/19/17 15:30 10122/17 06:41 7005-72-3 Chrysene ND ug/L 5.0 1 10/19/17 15:30 10)22/17 06:41 218-01-9 Dibenz(a,h)anthracene NO ug/L 5.0 1 10/19/17 15:30 10/22/17 06:41 53-70-3 3,3'-Dichlorobenzidine NO ug1L 25,0 1 10/19/17 15:30 10122/17 06:41 91-94-1 2,4-Dichlorophenol NO ug/L 5.0 1 10/19/17 15:30 10/22/17 06:41 12G42-2 Diethylphthalate NO ug/L 5.0 1 10/19/17 15:30 10/22J17 06:41 84-66-2 2,4-Dimethylphenol NO ug/L 1010 1 10119117 15:30 10/22/17 06:41 105-67-9 Dimethylphthalate NO ugJL 5.0 1 10119/17 15:30 10/22/17 06:41 131-11-3 Di-n-butytphthalate NO ug/L 5.0 1 1D119117 15:30 10/22/17 06:41 84-74-2 4,6-Dinitro-2-methylphenol ND ug/L 20.0 1 10/19/17 15:30 10122/17 06:41 534-52-1 2,4-Dinitraphenol ND ug/L 50.0 1 10119117 15:30 10/2211706:41 51-28-5 2,4-DinRrotoluene ND ug1L 5.0 1 10/19/17 15:30 10122J17 06:41 121-14-2 2,6-Dinitratoluene ND ug/L 5.0 1 10/19/17 15:30 10/22/17 06:41 606-20-2 Di-n-oetylphthalate ND ug/L 5.0 1 10/19/17 15:30 10/22/17 06:41 117-84-0 bis(2-Ethy1hexyl)phthalate NO ug1L 5.0 1 10/19/17 15:30 10/2211706:41 117-81-7 Fluoran then NO ug/L 5.0 1 10/19/17 15:30 10122/17 06:41 206-44-0 Fluorene NO ug/L 5.0 1 10/19/17 15:30 10122/17 06:41 86-73-7 Hexachloro-1,3-butadiene ND ug/L 5.0 1 10/19/17 15:30 10/22/17 06:41 87-68-3 Hexachlorobenzene NO ug1L 5.0 1 10/19/17 15:30 10/P2/17 06:41 118-74-1 Hexachlorocyclopentadiene ND ug/L 10.0 1 10119/17 15:30 10/22117 06:41 77-47-4 Hexachloroethane ND ug1L 5,0 1 10119/17 15:30 10/22J17 06:41 67-72-1 L2 lndeno(1,2,3-cd)pyrene ND ug/L 5.0 1 1011911715:30 10/22/17 06:41 193-39-5 Isophorone ND ugA- 10.0 1 10/19/17 15:30 10/22/17 06:41 78-59-1 Naphthalene NO ug/L 5.0 1 10119/17 15:30 10/22/17 06:41 91-20-3 Nitrobenzene NO ug/L 5.0 1 10119/17 15:30 10/22/17 06:41 98-95-3 2-Nitrophenol NO ug/L 5.0 1 10/19117 15:30 10/22/17 06:41 88-75-5 4-Nitrophenol NO ug/L 50.0 1 10/19/17 15:30 10/22/17 06:41 100-02-7 N-Nitrasodimethylamine NO ug1L 5.0 1 10/19/17 15:30 10/22/17 06:41 62-75-9 N-Nitroso-ditrpropylamine NO ug1L 5,0 41 10119/17 15:30 10/22/17 06:41 621-64-7 N-Nitrosodiphenytamine NO ug/L 10.0 1 10/19/17 15:30 10/22/17 06:41 86-30-6 2,2'-Oxybis(1-chloropropane) NO ug/L 5.0 1 10/19/17 15:30 10/22/17 06:41 108-60-1 Pentachlorophenol NO ug/L 10.0 1 10/19/17 15:30 10/22/17 06:41 87-86-5 Phenanthrene NO uglL 5.0 1 10119/17 15:30 10/22/17 06:41 85-01-8 Phenol ND ug1L 5.0 1 10/19/17 15:30 10/22/17 06:41 108-95-2 Pyrene NO ug1L 5.0 1 10/19/1715:30 10122/17 06:41 129-00-0 1,2,4-Trichlorobenzene NO ug/L 5.0 1 10/1911715:30 10/2211706Al 120-82-1 2,4,6-Trichtorophenol NO ug/L 10.0 1 10/19/17 15:30 10122J17 06:41 88-06-2 su►rogates Nitrobenzene-d5 (S) 62 % 10-120 1 10119/17 15:30 10r12117 06:41 4165-60-0 2-Fluorobiphenyl (S) 60 % 15-120 1 10/19/17 15:30 10/22/17 06:41 321-60-8 REPORT OP LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10126J2017 04:57 PM without the written consent of Pace Analytical Services, L.L.C. Page 5 of 29 Pace Analytical Services, LLG r i eAnao ar 9800 KirKR� AveNC 28078 S 28 Huniersviae, 078 _- w4rWPff0 Wbsmm (704)8759092 i i i ANALYTICAL RESULTS Project: Colfax Fluid Handling Stomwrat Pace Project No.: 92359523 Sample: SDO-004 tab ID: 92359623001 Collected: 10116/17 09:46 Received: 10/17117 12:54 Matrix: water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA625 Preparation Method: EPA625 Surrogates Terphenyl-d14 (S) 67 % 11-131 1 10/19117 15:30 10/22/17 06.41 1718-51-0 Phenol-d6 (5) 23 % 10-120 1 10/19/17 15:30 10/22117 06:41 13127-88-3 2-Fluorophenol (S) 31 % 10-120 1 10/19/17 15:30 10122/17 06:41 357-12.4 2,4,6-Tribromophenol (S) 90 % 10-137 1 10/19/17 15:30 1022/17 06:41 118-79-6 624 Volatile Organics Analytical Method: EPA 624 Benzene ND ug/L 2,0 1 1026117 09:54 71-43-2 Bromodichloromethane NO ug1L 2.0 1 1=611709:54 75-27-4 Bromofonn NO ug1L 2.0 1 10/26/17 09:54 75-25-2 Bromomethane NO ug1L 2,0 1 1MU17 D9:54 7442-9 Carbon tetrachloride NO uglL 2.0 1 10/26/17 D9:54 56-23-5 Chlorcbenzene NO ug/L 2.0 1 10126/17 09:54 108-90-7 Chlorcethane NO u911. 2.0 1 10/26117 09:54 75-00-3 Chloroform NO ug1L 2.0 1 1012&17 09:54 67-66-3 Chloromethane NO ug1L 2.0 1 10/26/17 09:54 74-87-3 Dibromochiommethane ND ug1L 2.0 1 10/26117 09:54 124-48-1 1,2-Dichiorobenzene NO ug1L 2.0 1 1026117 09!54 95-50-1 1,3-Dichlorobenzene NO ug/L 2.0 1 10/26/17 09:54 541-73-1 1,4-Dichlorobenzene NO ugfL 2.0 1 10/26/17 09:54 106-46-7 1,1-Dichloroethane NO ug1L 2.0 1 1026117 09:54 75-34-3 1,2-Dichloroelhane ND ug1L 2.0 1 10/26/17 09:54 107.06-2 1,1-0ichloroethene NO ug/L 2.0 1 10/26117 09:54 75-35-4 cis-1,2-Dichloroethene NO ug1L 2.0 1 1026117 D9:54 156-59-2 trans-11,2-Dirhloroethene NO ug1L 2.0 1 10/26/17 09:54 156-60-5 1,2-Dichiaropropane NO ug1L 2.0 1 1026117 09:54 78-87-5 as-1,3-Dichloropropene NO ug1L 2,0 1 10/2611709.54 10061-01-5 trans-1,3-Dictiloropropene NO ugA- 2.0 1 1026/1709:54 10061-02-6 Ethyibenzene ND uglL 2,0 1 10/26/17 09:54 100-41-4 Methylene Chloride NO ug/L 2.0 1 1026117 09:54 75-09-2 1,1,2.2-Tetrachloroethane NO ug1L 2.0 1 10/2611709:54 79-34-5 Tetrachloroethene NO ug1L 2.0 1 10/26/17 09:54 127-184 Toluene ND ug1L 2.0 1 10/26/17 09:54 108-88-3 1,1,1-Trichloroethane NO Ug/L 2,0 1 10/26117 09:54 71-55-6 1,1,2-Trichloroethane NO uglL 2.0 1 1026/1709:54 79-00-5 Trichioroethene NO ug/L 2.0 1 1026/17 09:54 79-01-0 Trichiorofluoromethane NO ug1L 2.0 1 10/26117 09:54 75-69-4 Vinyl chloride NO ug1L 2.0 1 10126/17 09:54 75-01-4 Surrogates 4-Brornofluorobenzer►e (S) 101 % 70-130 1 10126/17 09:54 46D-00-4 Toluene-d8 (S) 103 % 70-130 1 10/26/17 09:54 2037-26-5 1,2-Dichloroethane-04(S) 97 % 70-130 1 102611709:54 17060-07-0 25400 Total Suspended Solids Anaytical Method: SM 2540D Total Suspended Solids 5.6 mg/L 5-0 1 10/19117 08:30 Date: 1026/2017 04:57 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 6 of 29 PacoAnatyticai Services, LLC e CEA�SI.IGal 98001unceyAve, Suite toe UG fUit Hurgersville, NC 28078 I wMPacetabswrrs (704)875-9092 i i ANALYTICAL RESULTS Project: Colfax Fluid Handling Stormont I Pace Project No:: 92359523 Sample: SDO-004 Lab lD: 92359523001 Collected: 10/16/17 09:46 Received: 10/17117 12:54 Mabix. Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4040 pH Analytical Method: EPAg040 PH 6.8 Std. Units 0.10 1 10118/17 00:00 H6 Date: 10126/2017 04:57 PM REPORT OF LABORATORY ANALYSIS This report shell not be reprodumd, e=ept in full, without the written cansent of Pace Analytical Services, LLC, Page 7 of 29 L'eAllaij/ tale wwntpanlahs.wm Project: Colfax Fluid Handling Stnnfmat Pace Project No., 92359523 QC Bath: 383031 QC Batch Method: EPA 1654B Associated lab Samples: 92359523001 METHOD BLANK 2122861 Associated Lab Samples: 92359523001 Parameter Units Total Petroleum Hydrocarbons mg1L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 10119/17 05:20 Pace Ana"cal Serviem, LLC 98M Ka=y Ave. Suite 100 Huntersvilo, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2122862 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons nxA 20 19.1 96 64-132 MATRIX SPIKE SAMPLE: 2122863 92358374001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec unfits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 18.7 94 64-132 Roults preswrted on this pap are In the units intlfsated by the "Units' column except wtwe an alternate unit Is presented to the nptd of the rewrt REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10r2612017 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 29 Y ;aceAnalyfjcale wmepecawacom QUALITY CONTROL DATA Project: Colfax Fluid Handling Stormwat Pace Project No.: 92359523 QC Batch: 382919 Analysis Method: EPA 200.7 QC Batch Method: EPA200.7 Analysis Description: 200:7 MET Associated Lab Samples: 92359523001 METHOD BLANK: 2122101 Matrix: Water Associated Lab Samples: 923599523001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 1011911717:41 Lead ug/L N❑ 5.0 1011911717:41 Zinc ug/L ND 10.0 10/19/1717:41 Pace Analytical services, LLC 9800 Kincey Ave, Suite 100 Hu,ft vil , NC 2tt079 (704)875-9092 LABORATORY CONTROL SAMPLE_ 2122102 Spike LCS LCS % Rec Parameter units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 51B 104 85-115 Lead ug/L 500 492 98 85-115 Zinc ug/L 500 491 98 85-115 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2122103 2122104 MS MSD 92358797001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result %Rec %Rec Limits RPD Qua! Copper ug/L 12.9 500 500 533 536 104 105 70-130 i Lead ug/L ND 500 500 464 469 93 94 70-130 1 Zinc ug/L 37.1 500 500 511 518 95 96 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2122105 2122106 MS MSD 92359320001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 3.0J 500 500 527 527 105 105 70-130 0 Lead ug1L ND 500 500 489 480 98 96 70-130 2 Zinc ug1L ND 500 500 494 480 98 96 70-130 3 Results presented on this page are In the units Indicated by the "units" column except whet• an alternate unit Is presented to the right of the reeatL REPORT OF LABORATORY ANALYSIS This report shall not be repraduced, e=pt in full, Date: 10/2612017 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 29 ArWcal /�Z -pa-w om 1 QUALITY CONTROL DATA Project: Colfax Fluid Handling Stomtwat Pace Project No.: 92359523 QC Batch: 384041 QC Batch Method: EPA 624 Associated Lab Samples: 92359523001 Analysis Method: EPA 624 Analysis Description: 624 MSV METHOD BLANK: 2128427 Matrix: Water Associated Lab Samples: 92359523001 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1-Trichloroethane ugA- NO 2.0 10/26/1709:02 1,1,2,2-Tetrachlaroethane ug/L NO 2.0 10/26117.09:02 1,1,2-Trichloroethane ug/L NO 2.0 1026/1709:02 1,1-Didioroethane ug/L ND 2.0 1012611709:02 1,1-Dichloroethene ug/L ND 2.0 10/26117 09:02 1,2-Dichlorabenzene ug/L NO 2.0 10/25/17 09:02 1,2-Dichlaroethane ug/L NO 2.0 10/26/17 09:02 1,2-Dichloropropane ug/L ND 2.0 10/2611709:02 1,3-Dichlorobenzene ug/L ND 2.0 10/2611709:02 1,4-Dichlorobenzene ug/L NO 2.0 10/2611709:02 Benzene ug/L NO 2.0 10/26/17 09:02 Bromodichloromethane ug/L ND 2.0 10/26/17 09:02 Bromoform ug/L ND 2.0 1026117 09:02 Bromomelhane ug1L NO 2.0 10126/17 09:02 Carbon tetrachloride ug/L ND 2.0 10126/17 09:02 Chlorobenzene ug/L NO 2.0 10/26/17 09:02 Chloroethane ug1L ND 2.0 10/26/17 09:02 Chloroform ug/L ND 2.0 1026117 09:02 Chloromethane ug/L ND 2.0 10/26/17 09:02 cis-1,2-Dichloroethene ug/L NO 2.0 1026/1709:02 c4s-1,3-Dichloropropene ug/L NO 2.0 1026/1709:02 Dibromoctdorometharte ug/L NO 2.0 10/26/17 09:02 Ethylbenzene ug/L NO 2.0 1026/1709:02 Methylene Chloride ug1L NO 2.0 1026/17 09:02 Tetrachloroethene uglL ND 2.0 10/26/17 09:02 Toluene uglL ND 2.0 10/26/17 09:02 trams-1,2-Dichlaroethene ug/L ND 2.0 10/26/17 09:02 trans-1,3-Dichloropropene ug/L NO 2.0 10126/17 09:02 Trichloroethene ug/L NO 2.0 10/26/17 09:02 Trichtorofluoromethane ug/L • ND 2.0 10/26/17 09:02 Vinyl chloride ug/L ND 2.0 10126/17 09:02 1,2-01cWroethane-d4 (S) % 94 70-130 10/2611709:02 4-Bromafluorobenzene (S) % 101 70-130 10/26/17 09:02 Toluene-d8 (S) % 103 70-130 1026117 09:02 LABORATORY CONTROL SAMPLE: 2128428 Qualifiers Pace Analytical Services, LLC 9800 Kncey Ave. Suite r 00 Huntersvtile, NC 28078 (704)875-9092 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1-Trichloroethane ug/L 20 20.1 101 52-162 1,1,2,2-Tetrachloroethane ug/L 20 17.4 87 46-157 Reauas presented on aft pme Are In bw uNb indicated by ON -UFOW cotrman except wbve an alt nuft unit Ls presented to the TIVM or the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 102612017 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 29 Pace Analytical Services, LLC e 9800 Kincey Ave. Suite 100 ceAnalybcal Huntersv7le, NC 28078 aww.p (704)875-9092 E QUALITY CONTROL DATA i Project: Colfax Fluid Handling Stone at Pace Project No.: 92359523 , LABORATORY CONTROL SAMPLE: 2128428 Spike LCS LCS % Rec j Parameter Units Cone. Result % Rec Limits Qualifiers 1,12-Trichloroethane ugR 20 19.0 95 52-150 1,1-Dichloroethane ug/L 20 19.6 98 59-155 11-Dichloroethene uglL 20 21-9 110 1-234 1,2-Dichloroberizene ug/L 20 19.6 98 18-190 1,2-Dichloroethane u91L 20 19.2 96 49-155 1,2-Dichloropropane ugR 20 19Z 98 1-210 1,3-Dichlorobenzene ug/L 20 19.7 98 59-156 1,4-Dichlorobenzene uglL 20 19,5 98 18-190 Benzene ug/L 20 19.2 96 37-151 Bromedichloromethane ug/L 20 19,3 96 35-155 Bromoform ug/L 20 20.3 101 45-169 Bromomethane ugR 20 27.6 138 1-242 Carbon tetrachloride ugR 20 20.6 103 70-140 Chlorobenzene ug/L 20 19.0 95 37-160 Chloruethane ug/L 20 19.6 98 14-230 Chloroform uglL 20 18.1 90 51-138 Chloromethane ugR 20 212 106 1-273 as-1,2-Dichloroethene ug/L 20 20.3 102 68-146 cis-1,3-Dichlorapropene ug/L 20 19.6 98 1-227 Dibromochloromethane ugR 20 19.4 97 53-149 Ethylbenzene ug/L 20 18.8 94 37-162 Methylene Chloride ugR 20 18.8 94 1-221 Tetrachloroethene ug/L 20 20.7 104 64-148 Toluene uglL 20 18.9 95 47-150 trans-1,2-Dichloroethene ugR 20 19.9 99 54-156 trans-1,3-Dichloropropene ug/L 20 19A 97 17-183 Trichioroethene ug/L 20 20.7 103 71-157 Trichiorofluoromethane ug/L 20 20-7 104 17-181 Vinyl Chloride ugR 20 21.8 109 1-251 1,2-Dichloroethane-d4 (S) % 102 70-130 4-Bromofluorobenzene (S) % 95 70-130 Toluene-d8 (S) % 96 70-130 MATRIX SPIKE SAMPLE: 212WO 92360161004 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1-Trichloroethane ugR NO 20 22.0 110 46-171 1,1,2,2-Tetrachloroethane ug/L NO 20 23.3 116 73-159 1,12-Trichloroethane ugR ND 20 24.0 120 64-152 1,1-Dichloroethane ug/L NO 20 22.6 113 43-172 1,1-Dichloroethene ug/L NO 20 23.1 115 48-189 1,2-Dichlorobenzene uglL NO 20 23.1 116 54-154 1,2-Dichloroethane ug/L NO 20 23.4 117 42-171 1,2-Dichloropropane ug/L NO 20 24.5 123 55-157 1,3-Dichlorobenzene ugR NO 20 22.8 114 57-148 Results peesented m this page are In the units indksted by Ow "Unite' column except where an alternateunit is presented loom right of the result REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, enept In full, Date: 1012612017 04:57 PM without the written consent of Pace Analyti'call Services, LLC. Page 11 of 29 Pace Analytical services, LLC + 9800I(inceyAve. Suite100 p 7ZAna"Cal Huntereville, NC 28078 e wewpece/a M=P l704)e75-9092 QUALITY CONTROL DATA Project: Colfax Fluid Handling Stomtwat Pace Project No.: 92359523 MATRIX SPIKE SAMPLE: Parameter 2128430 Units 92360161004 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,4-1)ichlombenzene Lot ND 20 22.7 114 58-149 Benzene ug/L ND 20 232 116 54-163 Bromodichioromethane u91L NO 20 23.0 115 56-152 Bromoform ug/L ND 20 22.0 110 53-151 Bromomethane ug/L NO 20 15.6 73 10-200 Carbon tetracMoride ug/L NO 20 21.9 109 41-175 Chlorobenzene ug/L ND 20 23.8 119 67-152 Chloroethane ug/L ND 20 21A 107 23-200 Chloroform ug/L NO 20 21.3 107 51-166 Chloromethane u91L ND 20 222 102 40-175 cis-1,2-Dichloroethene ug/L ND 20 23.6 118 45-174 cis-1.3-Dichloropropene ug/L NO 20 24.2 121 38-146 Dibromochloromethane ug/L NO 20 22.3 111 65-144 Ethylbenzene u91L NO 20 22.4 112 57-152 Methylene Chloride ug/L NO 20 21.0 105 40-167 Tetrachloroethene ug/L NO 20 24.5 122 59-156 Toluene ug/L NO 20 23A 117 47-562 trans-1,2-Dichloroethene ug/L NO 20 23.6 118 47-178 trans-i,3-Dichloropropene ttg1L NO 20 23.1 116 39-148 Trichlomethene ug/L ND 20 24.0 120 60-153 Trichloro8uoromethane U91L ND 20 23.3 116 42-199 Vinyl chloride U91L NO 20 24.1 120 46-176 1,2-Dichloroethane-d4(S) % 95 70-130 4-Bromofluorobenzene (S) % 97 70-130 Toluene-dS (S) % 96 70-130 SAMPLE DUPLICATE: 2128429 Parameter Units 92350161003 Result Dup Result RPD Qualifiers 1,1,1-Trichioroethane tt9/L ND` ND 1,1,2,2-TetracNoroethane U91L NO NO 1,1,2-Trichloroettwne ug/L NO NO 1,1-Dichloroethane ug/L ND NO 1,1-Dichloroethene ug/L ND NO 1,2-Dictitorobenzene uglL ND ND 1,2-Dichionaethane ug/L NO ND 1,2-Dichloropropane uglL NO ND 1,3-Dichlorobenzene ug/L ND NO 1,4-Dichlorobenzene ug/L ND ND Benzene ug/L ND ND Bromodichloromethane ug1L NO ND Bromoform ug/L NO NO Bromomethane ug/L ND ND Carbon tetrachloride ug/L NO ND Chlorobenzene ug/L ND ND Rsadts d on this pays ■re in the units Indreatad by the "limb" aNuns7 s:cept VAM an aRerrta. unit is preaerdad to the rWd of the rerun. REPORT Of LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/26/20i7 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 29 ceAnalytrcar' _4 tewapacslahmm i i QUALITY CONTROL DATA Project: Colfax Fluid Handling Stormwat Pace Project No., 92359523 SAMPLE DUPLICATE: 2128429 E 92360161003 Dup i Parameter Units Result Result Chloroethane ug/L NO ND Chloroform ug/L ND ND Chloromethane ug/L ND N❑ cis-1,2-Dichloroethene ug/L ND ND f cis-1,3-Dichloropropene ug/L ND ND Dituomochloromethane ug/L ND ND Ethylbenzene ug/L ND ND Methylene Chloride ug/L ND ND fff E Tetrachloroethene ug/L ND ND Toluene ug/L ND ND (f ( trans-1,2-Dichloroethene ug/L ND ND trans-1.3-Dichiampropene uglL ND ND 1€ Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND [ Vinyl chloride ug1L ND ND 1,2-aichloroethane-d4 (S) % 98 97 4-Bromofluoroberizerte (S) % 101 101 Toluene-d8 (S) % 103 103 RPD Qualifiers 2 0 1 Pace Analytical Servicas, LLC 9000 KinceyAve.. Suite 100 HurttersNHe. NC 28078 (7D4)375.9%2 Rasults presmtad on tole papa ire In the units Indicated by the'UMW column except weber, an eRernate tall Is presented to the right of the remit REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in hull, Date: 10/2W017 04:57 PM without the written consent oh Pace Analytical Services, LLC. Page 13 of 29 www.pyRlaBacom QUALITY CONTROL DATA Project: Colfax Fluid Handling Stormwrat Pace Project No.: 92359523 QC Batch: 383313 QC Batch Method: EPA 3510 Associated Lab Samples: 92359523001 Analysis Method: Analysis Description: EPA608 608 GCS Pest PCB METHOD BLANK: 2124584 Matrix: Water Associated Lab Samples: 92359523001 Blank Reporting Parameter Units Result Limit Analyzed 4,4'-DDD ug/L ND 0,050 1025/17 04:25 4,4'-DDE uglL ND 0.050 10125/17 04:25 4,4'-DDT ug/L NO 0.050 10125/17 04:25 Aldrin ug/L NO 0.050 10/25/17 04:25 alpha-BHC ug/L ND 0.050 10/25/17 04:25 beta-BHC ug/L ND 0,050 1012511704:25 Chlordane (Technical) ug1L ND 0.50 1025/17 04:25 delta-BHC ug/L NO 0.050 10/25117 04:25 Dieldrin ug/L NO 0.050 10/25/17 04:25 Endosultan 1 ug/L NO 0.050 1025117 04:25 Endosulfan II ug/L ND 0.050 i025117 04:25 Endosutfan sulfate ug/L NO 0.050 1025117 04:25 Endrin ug/L NO 0,050 1025117 04:25 Endrin aldetryde uglL ND 0,050 1025117 04:25 gamma-BHC (Lindane) ug/L ND 0.050 1025117 04:25 Heptachlor ug/L ND 0,050 1025117 04:25 Heptachlor epoxide ug1L NO 0.050 1025117 04:25 PCB-1016 (Aroctor 1015) ug/L NO 0.50 1025/17 04:25 PCB-1221 (Arodor 1221) ug/L NO 0.50 1025/1704:25 PCB-1232 (Arodor 1232) ug/L NO 0.50 1025/17 04:25 PCB-1242 (Arodor 1242) ug/L NO 0.50 1025117 04:25 PC13-1248 (Aroclor 1248) ug/L ND 0.50 1025117 04:25 PCB-1254 (Arodor 1254) ug/L NO 0.50 1025/17 04:25 PCB-1260 (Amdor 1260) ug/L ND 0.50 10/25/17 04:25 Toxaphene ugA- NO 0.50 1025/17 04:25 Decachlorobiphenyl (S) % 58 20-138 1025/17 04:25 Tetrachloro4n-xytene (S) % 78 20-110 1025117 04:25 Qualifiers Pace Artalyticat services. LLC Saco IGnceyAve, Suite io0 HunterwAle. NC 28078 (704)9759092 LABORATORY CONTROL SAMPLE: Parameter 2124585 Units Spike Conc. LCS Result LCS % Rec % Rec limits Qualifiers 4,4'-DDD ug/L .25 0.23 92 31-141 4,4'-D❑E ug1L .25 0.20 82 30-145 4,4'-DDT ugtL :25 0.22 91 25-160 Aldrin ug/L 25 0.17 69 42-122 alpha-BHC ug/L .25 0.19 75 37-134 beta-BHC ug1L .25 0.17 69 17-147 delta-BHC uglL .25 0.21 87 19-140 Dieidrin ug1L .25 0.21 83 35-146 Endosulfan I ug/L .25 0.21 84 45-153 PAmAts presented on this pays are In the unite andacsted by Me'ehrats' ootumn except where an a3t nuft unit lapraaanted to the rV%t orthe rezWt, REPORT OF LABORATORY ANALYSIS 'this report shall not be reproduced, except in full. Date: 10262017 04:57 PM without the written consent of Pace Analytical Services, LLC,. Page 14 of 29 2eAnaVical' Pace Analytical Services, LLG 9800 KlnceyAve, Suite 100 Huntersville, NC 28078 WWWPaskbscom (704)876-e0e2 i s QUALITY CONTROL DATA Project: Colfax Fluid Handling Stormwat Pace Project No.: 92359523 LABORATORY CONTROL SAMPLE: 2124585 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Endosulfan II ug/L .25 0,22 91 1-202 Endosulfan sulfate ug/L .25 0:24 96 26-144 Endrin ttg/L .25 0.22 88 30-147 Endrin aldehyde ug/L .25 0.19 79 50-150 gamrna-BHC (Undane) ug/L .25 0.19 77 32-127 Heptachlor ug/L 25 0.17 70 34-111 Heptachlor epoxide ug/L .25 0.21 83 41-126 Decachlorobiphenyl (S) % 80 20-138 Tetrachloro-rn-xylene (S) % 77 20-110 MATRIX SPIKE SAMPLE: 2124586 92359523001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 4,4'-DDD 1-19/1- NO 25 0,22 90 31-141 4,4'-DDE ug/L NO .25 12.9 5190 30-145 M1 4,4'-DDT ug/L NO .25 0,21 86 25-160 j Aldrin ug/L NO .25 0.18 71 42-122 alpha-BHC ug/L NO .25 0.19 78 37-134 beta-BHC ug/L ND .25 0.16 66 17-147 delta-BHC ug/L NO .25 0.26 105 19-140 Dieldrin ug/L ND .25 0.29 118 36-146 Endosulfan I ugA- NO .25 0.20 83 45-153 Endosulfan 11 ug/L NO .25 0.23 92 1-202 Endosulfan sulfate ugA- NO .25 0.21 83 26-144 Endrin ug/L NO 25 0.20 82 30-147 Endrin aldehyde ug/L NO .25 0.15 61 50-150 gamma-BHC (Lindane) ug1L NO .25 0,17 71 32-127 Heptachlor ugtL NO .25 0.21 83 34-111 Heptachlor epoxide ug/L NO .25 0A9 77 41-126 DecachlorabipherrylIS) % 29 20-138 Tetrachloro-m-xylene (S) % 65 20-110 SAMPLE OUPLICATE: 2124587 92359547001 Dup Parameter Units Result Result RPD Qualifiers 4,4'-DOD ug/L NO NO 4,4'-DDE ug/L ND NO 4,4'-DDT ugh NO NO Aldrin ugfL ND NO alpha-BHC ug/L NO NO beta-BHC ugh. ND ND Chlordane (Technical) u911- NO ND delta-BHC ug[L ND ND Dieldrin ug/L NO ND Results pie,. , on this page an in the units indkated by the ^urefs- coturrm except where an aaam■ts unit h pru at ed to the right of the result REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, Date: 10/ 612017 04:57 PM without the written consent of Pace Analytical Services, LLC _ Page 15 of 29 ceAnalyfcLil e wlwparataGxeaa s QUALITY CONTROL DATA Project: Colfax Fluid Handling Stommat Pace Project No.: 92359523 SAMPLE DUPLICATE: 2124587 Parameter Units 92359547D01 Result Dup Result RPD Endosulfan I ug/L ND ND Endosulfan II ug/L ND ND Endosulfan sulfate ug/L NO ND Endrin ug/L NO ND Endrin aldehyde ug/L ND ND gamma-BHC (Undane) ug/L ND ND Heptachlor u91L NO ND Heptachlor epoxide ug/L ND ND PCB-1016 (Arocior 1016) ug/L ND ND PCB-1221 (Arodor 1221) ug/L ND ND PCB-1232 (Arodor 1232) ug/L NO ND PCB-1242 (Arodor 1242) ug/L ND ND PCB-1248 (Arodor 1248) ug/L ND ND PCB-1254 (Arodor 1254) ug/L ND ND PCB-1260 (Arodor 1260) u91L ND ND Toxaphene ug/L ND ND Qualifiers Pace Arm"cal Services, LLC 98DO Kncey Ave. Suite 100 HuntersvdEe, NC 28078 (7D4)875-9092 Rewra presented on this page air in the units Indicated by the'UnW column except whirr An imamate unR is presorted W the right of the rwA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Suit. Date. 10/26/2017 04:57 PM without the wntten consent of Pate Analytical Services, LLC. Page 16 of 29 ceAna,�rtical` � W wavcpacetabscom QUALITY CONTROL DATA Project: Colfax Fluid Handling Stormmrat Pace Project No.: 92359523 QC Batch: 383124 Analysis Method: EPA625 QC Batch Method: EPA625 Analysis Description: 625 MSS Associated Lab Samples: 92359523001 METHOD BLANK: 2123336 Associated Lab Samples: 92359523001 Parameter Units Matrix: Water Blank Reporting Result Limit Analyzed 1,24-Trichlorobenzene ug/L NO 5.0 1021/17 21:50 2.2'-Oxybis(1-chloropropane) ug/L ND 5.0 1021117 21:50 2,4,6-Trichlorophenol ug/L ND 10.0 10121/17 21:50 2,4-Dichlorophenol uglt ND 5.0 10/21/17 21:50 2,4-Dimethylphenol ug/L NO 10.0 10/21/17 21:50 2,4-Dinitrophenol ug1L NO 50.0 1021117 21:50 24-Dlnitrotoluene ug/L NO 5.0 1021117 21:50 2,6-Dinitrotoluene ug/L NO 5.0 10/21/17 21:50 2-Chloronaphthalerte ug/L NO 5.0 1021117 21:50 2-Chlorophenol ug/L NO 5.0 1021/17 21:50 2-Nitrophenol ug/L NO 5.0 1021/17 21:50 33-Dichlorobenzidine ugfL NO 25.0 1021/17 21:50 4,6-Dinitro-2-medWiphenol ug/L NO 20.0 1021/17 21:50 4-Bromophenylpherryl ether ug/L NO . 5:0 10/21/17 21:50 4-Chloro-3-methylphenol ug/L NO 5.0 1021117 21:50 4-Chiorophenylphenyl ether uglL ND 5.0 1021/IT 21:50 4-Nitrophenol ug/L NO 50.0 10/21/17 21:50 Acenaphthene ug1L NO 5.0 10/21/17 21:50 Acenaphthyiene ug/L NO 5.0 1021I17 21:50 Anthracene ug/L NO 5.0 10121/17 21:50 Benzo(a)anthracene ug/L NO 5.0 1021/17 21:50 Benzo(a)pyrene ug/L NO 5.0 10/21/17 21:50 Benzo(b)fluoranthene uglL NO 5.0 10/21/17 21:50 Benzo(g,h,i)perylene ug1L NO 5.0 10/21/17 21:50 Benzo(k)fluoranthene ugfL NO 5.0 10/21/17 21;50 bis(2-Chloroethoxy)methane ug1L NO 10.0 10/21/17 21:50 bis(2-r-hloroethyi) ether ugfL NO 5.0 1021/17 21:50 bis(2-Ethylhexy1)phtha1ate u91L NO 5.0 10/21/17 21:50 Butylbenzylphthalate u911- NO 5.0 1021117 21:50 Chrysene uglL NO 5.0 1021117 21:50 Di-n-butylphthalate uglL NO 5.0 10/21117 21:50 Di-n-octyiphthalate ug1L NO 5.0 1021117 21:50 Diberiz(a,h)anthracene ug1L NO 5.0 1021/1721;50 Diethylphthalate uglL NO 5.0 1=111721:50 Dimethylphthalate ug/L NO 5.0 1021/17 21:50 Fluoranthene ugfL NO 5.0 10121/17 21:50 Fluorene ug/L NO 5.0 1021/17 21:50 Hexachloro-1,3-butadiene 1.1911- NO 5.0 10/21/17 21:50 Hexachlorobenzene ug/L NO 5.0 1WI/17 21:50 Hexachlorocyclopentadiene ug/L NO 10.0 1021/17 21:50 Hexachloroethane ug/L NO 5.0 10/21/17 21:50 Qualifiers Pace Ana"cal Services, LLC 9800 Kincey Ave, Suite 100 Hunterwiile, NC 29078 (7o4)875-9092 Results preseniad on Mta papa are In the units IrWicated by the "Urdta" coiunm except where an alternate unit In presented to the rtynt or Me resWL REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, exmpt in lull, Date: i 0/262017 04:57 PM without the written coment of Pace Analytical Services, LLC. Page 17 of 29 eAnaor-al www.Pacerab3.C= QUALITY CONTROL DATA Project: Colfax Fluid Handling Stormwat Pace Project No.: 92359523 METHOD BLANK: 2123336 Associated Lab Samples: 92359523001 Parameter Units Matrix: Water Blank Reporting Result Limit Analyzed Indeno(1,2,3-cd)pyrene ug/L ND 5.0 10121/17 21:50 Isophorone ug/L NO 10.0 10/21117 21:50 N-Nltroso-di-n-propylamine ug/L NO 5.0 1ORl/1721:50 N-Nitrosodimethytamine uglL NO 5.0 10/21/17 21:50 N-Nitrosodiphenylamine uglL NO 10.0 10/21/17 21:50 Naphthalene uglL NO 5.0 10f21/17 21:50 Nitrobenzene ug/L NO 5.0 1021117 21:50 Pentachiorophenal u91L NO 10.0 10/21/17 21:50 Phenanthrene ug/L NO 5.0 UY21117 21:50 Phenol ug1L NO 5.0 1021117 21:50 Pyrene ug/L NO 5.0 1021117 21:50 2A.6-Tribromophenol (S) % 72 10-137 1021117 21:50 2-Ftuorobiphertyl (S) % 32 15-120 1021/17 21:50 2-Fluorophenol (S) % 16 10-120 1021117 21:50 Nitrobenzene-d5 (5) % 34 10-120 1021117 21:50 Phenol-d6 (S) % 12 ID-120 1021117 21:50 Terphenyt-d14 (S) % 73 11-131 1021117 21:50 LABORATORY CONTROL SAMPLE: Parameter 2123337 Units Spike Conc. LC5 LCS Result % Rec 1,2,4-Trichlorobenzene ug/L 50 21.9 2,2'-Oxybis(1-chl0roprop0ne) ug/L 50 24.0 2,4,6-Trichlorophenot ug/L 50 32.0 2,4-Dichlorophenol ugR 50 28.2 2,4-Dimethyiphenol ug/L 50 34.5 2,4-Dtnitrophenol uglL 250 237 2,4-Dinitrotoluene u911- 50 45.4 2,6-Dinitrotoiuene ug/L 50 41.7 2-Chloronaphthalene ug/L 50 28.7 2-Chlorophenol ug/L 50 25.2 2-Nitrophenol ug/L 50 28.3 3,3'-Dichlorobenzidine ugh- 100 89.1 4,6-Dinitro-2-methylphenol ug/L 100 103 4-Bromophenylpherly1 ether u91L 50 37.4 4-Chloro-3-methylphenol ug/L 100 65.1 4-Chlorophenytphenyl ether ug/L 50 32.9 4-Nitrophenol ug/L 250 94.9 Acenaphtherle ug/L 50 31.8 Acenaphthyiene uglL 5o 32.0 Anthracene ug/L 50 44.9 Benzo(a)anthracene ug/L 50 47,5 Benzo(a)pyrene ug/L 50 47.0 Benzo(b)fluorardhene ug/L 50 45.3 Pace Anarytlical Servkae, LLC 9800 I(incey Ave„ Suits 100 Huntersvdle. NC 28078 (704)8759092 Qualifiers % Rec Limits Qualifiers 44 44142 48 36-166 64 37-144 56 1-191 59 32-119 95 1-181 91 39-139 83 50-158 57 60-118 L2 50 23-134 57 29-182 89 1-262 103 1-181 75 53-127 65 22-147 56 25-158 38 1-132 64 47-145 64 33-145 90 1-166 95 33-143 94 17-163 91 24-159 Resuft presented on Mb page are in the unite Indicated by the 'Units' ealurnn a Dept whir* en alternate unit le prdreMea to the dgM of Me result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/26/2017 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 29 G8A1 goical ® wwiermc�abticatt i QUALITY CONTROL DATA Project: Colfax Fluid Handling Stormwat Pace Project No_, 92359523 LABORATORY CONTROL SAMPLE: 2123337 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntemvifte, NC 20078 (704)875-9092 Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Benzo(g,h,i)peryfene ug/L 50 45.5 91 1-219 Benzo(k)Suaranthene ug/L 50 47.1 94 11-162 bis(2-Chloroethoxy)methane ug& 50 30.9 62 33-184 bis(2-Chloroethyl) ether ug/L 50 28.5 57 12-158 bis(2-Ethylhexyl)phthalate ug/L 50 45.9 92 8-158 Butylbenzylphthalate ug1L 50 45.9 92 1-152 Chrysene ugA- 50 48.3 97 17-168 Di-n-butylphthalate ug/L 50 47.5 95 1-118 Di-n-octylphthalate ug1L 50 43.5 87 4-146 Dibenz(a,h)anthracene ug/L 50 46.6 93 1-227 Diethylphthalate ug1L 50 42.9 8fi 1-114 Dimethylphthalate vglL 50 40.1 80 1-112 Fluoranthene ug/L 50 49.7 99 26-137 Fluorene ug/L 50 37.0 74 59-121 Hexachloro-1,3-butadiene ug/L 50 18.1 36 24-116 Hexachlorobenzene ug/L 50 40.6 81 1-152 Hexachlarocyclopentadiene ug/L 50 23.8 48 25-150 Hexachloroethane 11911- 50 10.3 37 40-113 L2 Indeno(1,2,3-cd)pyrene ug/L 50 4619 94 1-171 lsophorone u9/L 50 31.9 64 21-196 N-Nitreso-di-n-propylamine u9/1- 50 30.8 62 1-230 N-Nitrosodimethylamine ug/L 50 16.9 34 25-150 N-Nitrosodiphenylamine ug/L 50 39.7 79 25-150 Naphthalene ug/L 50 25.2 50 21-133 Nitrobenzene ug/L 50 29A 59 35-180 Pentachlorophenol ug/L 100 92A 92 14-176 Phenanthrene ug/L 50 44.3 89 54-120 Phenol ug/L 50 11.8 24 5-112 Pyrene ug/L 50 49.2 98 52-115 44,6-Tribromopher of (S) % 87 10-137 2-Fluorobiphenyl (S) % 57 15-120 2-Fluorophenol (S) % 30 10-120 Nitrobenzene-cl5 (S) % 56 10-120 Phenol-d6 (S) % 21 10-120 Terphenyi-d14 (S) % 85 11-131 MATRIX SPIKE SAMPLE: 2123338 35340529002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/L 0-98U 50 11.1 22 44-142 M1 2,2'-Oxybis(1-chloropropane) ug/L 0-95U 50 8.9 18 36-166 M1 2,4,6 Trichlorophenol ug/L 1.3U 50 24.4 49 37-144 2,4-Dichiarophencl ug/L 1.7U 50 15.8 32 1-191 2,4-Dimethylphenol ug/L 1.2U 50 17.8 36 32-119 2,4-❑inilrophenol tig/L 9.OU 250 176 71 1-181 Results presented an this page are In the units Indicated by Me "Units" column except when an sttamate unit to presented to the right or the msalt. REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full. Date: i 0l26/2017 04:57 PM without the written consent d Pace Analytical Services, LLC. Page 19 of 29 ceAnalytr'cal e wwtvpacarabsaom i QUALITY CONTROL DATA Project: Colfax Fluid Handling Storrrmat Pace Project No.: 92359523 Pace Analytical Services, LLC 9800 Kutcey Ave. Suits 100 Huntersviile, NC 20078 (704)875-9092 MATRIX SPIKE SAMPLE: Parameter 2123338 Units 35340529002 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 2,4-Dintirotoluene ug/L 0.90U 50 40.3 81 39-139 2,6-Dinitrotohuene ug/L 0.98U 50 31.4 63 50-158 2-Chloronaphthalene ug/L 0.981.1 50 14.9 30 60-118 M0 2-Chlorophenoi ug/L 1-3U 50 11.5 23 23-134 2-Ndrophenol u91L 0.91U 50 12.9 26 29-182 M1 3,3'-DichtorobenAdine ug/L 2.1U 100 79.3 79 1-262 4,6-Dinitro-2-methylphenot ug/L 2.6U 100 94.8 95 1-181 4-Bromopherrylphenyt ether ug/L 0.82U 50 30.9 fit 53-127 4-Chloro-3-methytphenot ug/L 3.7U 100 572 57 22-147 4-Chlorophenylphenyl ether ug/L 0.87U 50 22.1 44 25-158 4-14itrophenol ug/L 4.1U 250 79.2 32 1-132 Acenaphthene ug/L 0.25U 50 18.0 36 47-145 MI Acenaphthylene ug/L 0,21U 50 18.2 36 33-145 Anthracene u9/L 0.14U 50 41.5 83 1-166 Benzo(a)anthracene ug/L 0.33U 50 45.1 90 33-143 Benzo(a)pyrene ug/L 1.11.1 50 43.9 86 17-163 Benzo(b)8uoranthene ug/L 0,28U 50 42.7 85 24-159 Benzo(g,h,i)perylene ug/L 2.6J 50 43.3 82 1-219 Benzo(k)fluorardhene ug/L 0.43U 50 43.8 88 11-162 bis(2-Chtoroethoxy)methane ug/L 0.92U 50 13.6 27 33-184 M1 b1s(2-Chloroethyi) ether ug/L 1.OU 50 12.7 25 12-158 bis(2-Ethythexy0phlhalate ug/L 0.79U 50 444 90 8-158 Butylbenzylphthalate ug/L 0.79U 50 45.8 92 1-152 Chrysene ug/L 0.21U so 46A 93 17-168 Di-n-butylphthalate ug/L 0.75U 50 45A 91 1.118 Dit-, c phthalate ug/L 0.66U 50 41.7 83 4-146 Dibenz(a,h)anthracene ug1L 2AJ 50 43.0 81 1-227 Dtelhylphthalate ug1L 0.58U 50 36,2 72 1-114 Dimethytphthalate uglL 0.76U 50 292 58 1-112 Fluoranthene ug/L 0.21U 50 46.9 94 26-137 Fluorene ug/L 0.21U 50 25.9 52 59-121 M1 Hexachloro-1,3-butadiene ug/L 0.94U 50 9.6 19 24-116 M1 Hexachlorobenzene ug1L 0.72U 50 34.7 69 1-152 Hexachlorocyclopentadiene ug/L 0.88U 50 10.2 20 25-150 M1 Hexachloroethane ug/L 1.1U 50 9,5 19 40-113 MO indeno(1,2.3-cd)pyrene ug/L 2.7J 50 44.4 83 1-171 Isophorone ug/L 0.69U 50 14.2 28 21-196 N-Nitroso-di-n-propylamine ug/L 0-99U 50 13.4 27 1-230 N-Nitrosodime"lamine ug/L 0.91U 50 7.9 16 25-150 M1 N-Nitrosodipheriylamine ug/L 1.0U 50 36.6 73 25-150 Naphthalene ug/L 0.34U 50 13.0 26 21-133 Nitrobenzene ug/L 1.1U 50 15.1 30 35-180 M1 Pentachlompherrol ug/L 4.6U 100 84.8 85 14.176 Phenanthrene u9/L 0.22U 50 40.7 81 54120 Phenol u9/L 1.9U 50 5.1 10 5-112 Pyrene ug/L 0.19U 50 49.0 98 52-115 2,4,6-Tribromophenol (S) % 83 10-137 Results presented on this page are in the unita Indicated by the "units- column exc"A %tm an alternate UM to presented to the d9ht of the resulL REPORT OF LABORATORY ANALYSIS This report shag not be reproduced, except in full, Date: 10/26/2017 04:57 PM without the written consent or Pace Analytical Services, LLC. Page 20 of 29 ceAnalj cal' r w wpacedabsmm QUALITY CONTROL DATA Project- Colfax Fluid Handling Stormwat Pace Project No-: 92359523 MATRIX SPIKE SAMPLE: 2123338 35340529002 Spike MS Parameter Units Result Cone. Result Pace Analytical Services, LLC 9800 Kincey Ave. suite 100 Huntersrrille, NC 28078 (7N)W"092 MS % Rec % Rec Limits Qualifiers 2-Ftuorobiphenyl (S) % 28 15-120 2-Fluorophenol (S) % 13 10-120 Nitrobenzene-d5(S) % 27 10-120 Phenol-d6 (S) % 9 10-120 SO Terphenyt-d14 (S) % 74 11-131 SAMPLE DUPLICATE: 2123339 Parameter Units 35340529004 Result Dup Result RFD Qualifiers 1,2,4-Tdchlarobenzene ug/L 0.98U NO 2,2'-0xybis(1-chloropropane) ug/L O,95U ND 2,4,6-Trichlorophenol ug/L 1.3U N❑ 2,4-Dichlorophenol ug/L 1.7U N❑ 2,4-Dimethylphenal ug/L 1.21.1 ND 2,4-Dinitrophenol ug/L 9.OU NO 2,4-Dinitrotoluene ug/L 0,90U ND 2,6-Dinitrotoluerie ug/L 0.98U ND 2-Chloronaphthatene ug/L 0.98U ND 2-Chlorophenol ug/L 1.3U ND 2-Nitropheno4 ug/L 0.91 U NO 3,3'-Dichlorobenzidine ug/L 2A U NO 4.6-Dinitro-2-methylphenol ug/L 2.6U NO 4-Brornophenytphenyl ether ug/L 0.82U NO 4-Chloro-3-methylphenel ug/L 3.7U ND 4-Chlorophenytphenyl ether ug/L 0.87U ND 4-Nitrophenol ug/L 4AU ND Acenaphthene ug/L 0.25U ND Acenaphthylene ug/L 0.21 U NO Anthracene ug/L 0,14U ND Senzo(a)anthracene ug/L 0.33U ND Benzo(a)pyrene ug/L O.30U ND Benzo(b)fluoranthene ug/L 0.28U NO Benzo(g,h,t)perytene ug/L 2.OJ 1.51 Berizo(k)fluoranthene u91L 0.43U NO bis(2-Chloroethoxy)methane ug/L 0.92U ND bis(2-Chloroethyl) ether ug/L 1.OU ND bis(2-Ethylhexyl)phthalate ug/L 0.79U ND Butyibenzylphthaiate ug/L 0.79U NO Chrysene ugA- 0.21U NO Di-n-butylphthalate ug/L 0.75U NO Di-n-octylphthalate ug1L 0,661.1 NO Dibertz(a, h)anthracene ug1L 1.61 1.3J Diethylphthalate UA O.58U NO Dimethylphthalate WIL 0.76U ND Fluoranthene ug/L 0.21U ND Results presented on We page an in the unite Indicated by me'UrW column except when an aMmsts unl le presented to the rigid sr the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1012612017 04:57 PM without tiro written consent of Pace Analytical Services, LLC, Page 21 of 29 IAnalytical WWW..paceiab&WM t QUALITY CONTROL DATA Proud: Colfax Fluid Handling Stonnurat Pace Project No.! 92359523 SAMPLE DUPLICATE: 2123339 Parameter Ur11ts 35340529004 Result Dup Result Fluorene� ug/L 0.21 U ND Hexachloro-1,3-butadiene ug/L 0.94U NO Hexachlorobenzene Ug/L 0.72U NO Hexachlorocyclopentadiene ug/L 0.88U ND Hexachloroethane u911- 1JU ND lndeno(1.2,3-cd)pyrene ug/L 2.0.1 1AJ Isophorone ug/L 0.89U NO N-Nitroso-di-nrpropylamine ug/L 0.991J NO N-NitrosodlmeWamine ug/L 0.91U NO N-Nitrosodiphenylamine ug/L 1.0U ND Naphthalene ug/L 0.34U NO Nitrobenzene ug/L 1.1U NO Pentachloraphenol ug/L 4.6U NO Phenanttmene u9/L 0.22U ND Phenol ug/L 1.9U NO Pyrene u91L 0.19U NO 2,4,6-Tribromophenel (S) % 63 83 2-Fluorobiphenyl (S) % 34 33 2-Fluorophenot (S) % 18 17 Nitrobenzene-d5 (S) % 38 34 Phenol -de (S) % 11 11 Terphenyl-d14 (S) % 75 55 RPD Qualifiers 26 3 7 13 2 30 Pace Analytical Services, LLC 9ti00 Kneey Ave, Suite 10o Huntersviile, NC 28078 (714)8759092 Results presented on this pipe are In the urM Intllcatsd try the "Unft column except when sn tlteruute uuth Is presented to the riptd of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, Date: 10PZ6l2017 04:57 PM without the written consent of Paw Analytical Services, LLC. Page 22 of 29 ceAnalytical. S www.pacalals X= i ' QUALITY CONTROL DATA Project: Colfax Fluid Handling Stormwal Pace Project No.: 92359523 QC Batch: 383044 Analysis Method: SM 25QD QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92359523001 Pup Analytical Services, LLC 9800 Mnceyave, Suita 100 Huntersville, NC 2007E (704)B75-9092 METHOD BLANK: 2122886 Matrix: Water Associated Lab Samples: 92359523001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 10/19/17 08:27 LABORATORY CONTROL SAMFLE: 2122887 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids m91L 250 240 96 90-110 SAMPLE DUPLICATE: 2122888 92359687001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 167 154 806 SAMPLE DUPLICATE: 2122889 92359523001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 5.6 5.6 0 Remits presented an this pope are in the units indicated by the "Units" column except where an alternate unit is presented to On right of lire result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 1 D12612017 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 29 _ aceAnalytical e wrw.paceiabsoan Project: Colfax Fluid Handling Stormwat Pace Project No.: 92359523 QC Batch: 382906 QC Batch Method: EPA 9040 Associated Lab Samples: 92359523001 SAMPLE DUPLICATE: 2121888 Parameter Units PH Sid. Units QUALITY CONTROL DATA Analysis Method: EPA 9040 Analysis Description_ 9040 PH 92369432001 Dup Result Result RPD Qualifiers 2.6 2.5 3 H5 Pace Analytical Servh=. LLC 9800 Kirim Ave, Suite S ao Huntefsville, NC 29079 (704)875-9092 Rtsuae presented on this page are In She unus Indlcatad by #w "Unite' caleme axcept where an aeemate unit Is pnasnted to en 11CM of the MWIL REPORT OF LABORATORY ANALYSIS This repart shah not be reproduced, except in full, Date: i0l2612017 0057 PM without the written misent of Pea Anaiywni Servms, LLC: Page 24 of 29 Pace Analytical Services, LLC er�� s 100 acGAiwlydical 9e0q ante Ave. S 26078 Huntersvilk, NC 28g78 www mm (704)675-9092 QUALIFIERS Project: Calfax Fluid Handling Stormwat Pace Project No.: 92359523 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit- S - Surrogate 1,2-Dipheny1hydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidefines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SWW Chapter 4 for the analysis of Ac rolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenyiamine decomposes and cannot be separated from Diphenytamine using Method 8270, The result reported for each analyze is a combined concentration_ Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyze in associated samples may be biased low. Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. So Surrogate recovery outside laboratory control limits, REPORT OF LABORATORY ANALYSIS This report shad not be reproduced, except in full. Dale: 10/26/2017 04:57 PM without the written consent d Pace Analytical Services, L-C. Page 25 of 29 i 1 ' ., eeAnalytical riwcparafabacWrr i i QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Colfax Fluid Handling Stommmt Pace Project No.: 92359523 Pace Anahytical SerAcea, LLC saw K K"Am Suite IGO Huntersvdia, NC 28078 (7D4)87"D92 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92369623001 SDO-004 EPA 1664E 383031 92359523001 SDO-004 EPA 3510 383313 EPA 608 3B3549 92359523001 SOO-004 EPA 200.7 382919 EPA 200.7 3B3127 92359523001 SDO-004 EPA 625 383124 EPA 625 383447 923595730D1 SDO-004 EPA 624 384041 92359523001 SDO-004 SIN 2540D 383044 92359523001 SD0-004 EPA9040 382906 Date: i 0/26J2017 04:57 PM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the wfit w consent of Pam Analy&W Services, LLC,. Page 26 of 29 Document Name: Document Revised: August 4, 2017 Sample Condition Upon Recei t(SCUR) Page 1 of 1 Document No.: I Issuing Authority: -.r c EAWh;c7!< F-CAR-CS-033-Rev,04 Pace Quality Office Laboratory receiving samples: Asheville ❑ rEdeno Greenwood ❑ Hunterstfille ❑ Ralelgh❑ Mechanicsville[] Client Name: Projectill: WO# : 92359523 tt Courier. Fed E>, ❑UPS QIJSPS ial ue QOther:� ❑ CommercP iertt ��' 1 � ���I I �� 9235 I, - Custody Seal Present? ❑Yes Seals Intact? ❑Yes .E]No Date/initials Person Examining Contents: Packing Material: ❑Bubble Wrap JDBubbie Bags ❑None ❑ Other 8!olagicel Tissue Frozen? Thermometer. f�{ ,- Q'res (_ 1i q ❑N/A iJwet ❑Blue ©None T1 ❑ IR Gun ID: I Typo of Ica: Correction Factor: Cooler Temp Corrected ('CI; 3, Temp should be above freezing to VC _ _ ❑Sampies out a( temp crilerla. Samples an ice, cooling process has begun USDA Regulated SoiIkO N/A, water sample] Did samples originate in a quarantine zone within the United States: CA, Nyr ar SC (check maps)? Vd Iamples originate from a foreign source (internationally, l—lyes ni' lra includirtrHavali and Puerto Rlml? eves M CantmMlS��isV ancyi Chain of Custody Present? Yet lEINo N/A 1. _ Sam IesArrived within Hold Time? r Yes_. CINO N/A Short [told Time Ana is <72 hr.? yet 17Nsi" _ /A 3 Rush Turn Around Time ltunited? Yes too . N/A 4. Sufficient Volume? Ayes ©No ❑N/A S, Correct ContMnerS Used? -Pace Containers Used? -EIYes Ova ❑NO No ❑N/A N/A 6. Containers Intact? es ,9 V4 7. Dissolved ana isist Sam Its Field Filtered? LJVIA 0- Sample Labels Match COC? -tnctudes Date/Time/t0/Analysis Matrix: r©res i ❑Na ❑N/A 9. Head space In VOA Vials 6 >5-mms I I Elves v Lases f � ❑114/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑ves ores 0"a- ❑No ❑N/A ❑f,/A it. CLIENT NOTIFICATION/R ESOLUTIO N Person Contacted: Comments/Sample Discrepancy: Lot 10 of split containers: Date/Time: Field Data Required? Oyes ❑No Project Manager SCURF Review: Date: / VI' — It Project Manager SRF Review: i s_�z lL' _ Date: Noce!: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le. Out of hold, incorrect preservathre,aut of temp, incorrect containers) Page 27 Of 29 m 3 n a R v n n f c o = n n a N w r ^ O a � a M rA ro � 3 a a � R IN D a M N q C p � 6 9 n � n a n 9 sr H N .• `.. � � m v o+ w a N .• - ltemlf $P4U425 mL Plastic Unpreserved IN/A) (Cl-I • MU•250 mL Plastic Unpreserved (N/A) $P2U.SDD mL Plastic Unpreserved (N/A) SP1U-1 liter Plastir. Unpreserved (N/A) BP4S•12S mL PlastkH2SO4 IpH <2) (CI - I BP3N-250 mL plastk: HNO3 IpH < 2) T-Z BP4Z-115 ml Plastic 2N Acetate & NaOH (>9) BP4C-125 mL Plastic NaOH (pH > 221 (CI-1 WGI'U-Wife-mouthed Glass jar Unpreserved AG1U-1 alter Amber Unpreserved (NJAI (CI-) fv AG1H-1 titer Amber HCI IpH < 21 AG3U-250 mt.Amber Unpresemed (N/AI (CI-1 AG1S•1 liter Amber 112504 tpH c 2) AG3S-7.50 mL Amber H2504 IpH < 2) AMAIDGMI.750 mtAmber NH4C1 (N/AJ(CI-) J OG9H-4OmLVOAf1C1 (N/AI ' VG9T-40 mL VOA Na25203 INN VG9U40 mL VOA Unp (N/A) 0G9P.40 mL VOA H3PO4 IN/A) VOAK (6 vials per kitl-SD35 kit (N/AI VJGK (3 vials per kit)-VPH/Gas kit (N/A) SP5T-125 MLSter0a Plastic(N/A -tabl SP2T-250 mL Sterile Plastic (N/A - lab) BP3A-250 ml Plastic (NH212564 (9.3-9.7) Cubrtalnor VSGU-2o mi Scintillation vials MAI GN L O 7 PxCrIrLT7r1r Jf CHAIN -OF -CUSTODY ! Analytical Request Document • The Chain -of -Custody is a LEGAL DOCUMENT, All retevanl fields must be completed accurately. Seclien A Section a Section C . tctuii0el Client ITltormatien: Re wed Pro -CI Inlermalion: Invoice Inlormalion: Pd a 1 t of 1 Co meny.' Shield Emin Repon TO: DennyNetner - Allenhon Address, U01 Ye an Creek Road Copy To - - Company Name CherroVe NC 2820E Address. R ulata A99"clif Email Purchase Order F. paw Ulwle Phone Fee pawl Narw; Cod s Fiyid Handling 8fatmwator Pace Prolad Manager: Sng"IM.bWanippacelabs com State r Locatron Requested Due Dete: Pro"0; Paco PreBle X. : eaiDd. NC Reciinested A Iv0s Fatorod YJN "TRix ccm 9 COLLECTED Preservatives y C pm,mgwmn ew Walxr � iJ � w.�w w.,.,. •� w SAMPLE ID S.-M = ci START ENO H 4 One Character per boa. ti°�M 8a n m u. S 25 59,5 2,3 orV,' oT! u y a Semple Id. muat ba unlgw W f t lL ~ 3 O r�i a V 4 ro 8 6 Q N N n 4 s DATE TrME DATE TIME +� w x x S z = rr,, 5'DC)-��C `� s il'Y. X 3Y y F24 5 i 6 7 8 9 10 11 12 ADDITIONAL coMUEws RELNOUISHro BY r AF19UAnoN I3ATC TIME A 6TrAFCTLJATI0N GATE Time SAMPLE"NUMDNS SAMPLER NAME AND SIGNATURE n s" PRINT Memo or SAMPLER: ri C1 y r Gr g SIGNATURE of SAMPLER: ♦ /r GATE Signed!of • U Semi-annual Stormwater Discharge Monitoring „Report for North Carolina Division of Water Quality General Permlt No. NCG030000 Date submitted 10/9117 CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME Colfax/IMO Industries, Inc, ``1 I r� PERSON COLLECTING SAMPLES Joanna Harbison S ieid En Ineer _, EC E 1 V E Q LABORATORY:._ pace Analytical Lab Cert. # 12 �T 2 0 Z017 Comments on sample collection or analysis:Oenchmark exceedances r TSS and Ccapetat SDO#0114 CENTRAL FILES DWR SECTION Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Morithlyl September DISCHARGING TO CLASS :❑ORW ❑HQW [—]Trout ❑PNA ❑Zero -flow [—]WaterSupply ❑SA ZOther_Class C — Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 El No discharge i`hls period. Outfalt No. Date Sam le p Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids p H, Standard units' Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ===> _ - 100 mg/L or 50 mg/L 6.0 _ 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L SDO 004 9/6/17 0.85 130 6.63 0.0117 0.0052 0.0519 <5.0 <0.4904 ' MontFily sampling (Instead of -annual) must begin with the second cpnsecutive..benchmark exceedance for the same parameter at the soma outfali., 2 For sampling -periods with no discharge-at.any single dutfall, you must.still.'submit this:discharge monitoring report with Weheckmark here. 3The 'total precipitati6h. ust be recorded using:data from anon -site rain gauge; Unattended sites may be�eligible for a waivergf,tlie rain gauge: requirem ent. 4 See General Permit, Table 3 Identifying the esptclally;sehtltive'receiving water classifications where the n6re'proteetive benchmark applies, Total Toxic Organics sampling i§applicable only for:those facilities which perform metal finishing operations; manufacture. semicond,uctors,.manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found In 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the stormwater Pollution Prevention Plan may so certify, and the requirement forTTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported In numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, the4 must be reported In the format, "<XX rnitIV. where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value In excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gat of new oil per month. No discharge this period?Z Outfali No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Ilnches3 Non -polar O&G/TPH by EPA 1664 SGT-HEM) Total Suspended Solids pH Benchmarks ===> _ 15 mg/L 100 mg/L or 50 mg/L" 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must Implement 71er 1, Tier 2, or Tier 3 responses. See General Permit text FOR PART_A AND PART B MONITORING RE5ULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL7 YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an on !no! and one.cap KaftDMR including -off "No f115cha e" reports, within 30 days o race! t of the lab results jor at end of manLtorina gerlod In the case of No Dlschame"_reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS E IFl TION FOR AN N REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responle for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware tljat there are signi cant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ature of Permitteej Permit Date: 11/1/2012-10/31/2017 /dA� l (pate) SWU-245, last revised 10/25/2012 Page 3 of 3 n `yr ENGINEERING, INC_ �'�' N September 18, 2017 Rebecca Israel''' Environmental, Health, and Safety Lead Colfax Fluid Handling 1710 Airport Road Monroe, North Carolina 28110 Subject: Monthly Stormwater Sampling — August 2017 Certificate of Coverage No: NCG030293� Colfax/IMO Industries — Monroe, NC Shield Project No. 1150109-02 Dear Ms. Israel: Shield Engineering, Inc. (Shield) was unable to collect a -monthly stormwater sample for Stormwater Discharge Outfall (SDO) #004 at the Colfax — Monroe facility for the month of August 2017. Shield did mobilize towards the facility and attempt to collect a sample on August 31; however, the rain did not produce a discharge from the facility during business hours. Shield was able to collect a sample for September. The September sampling results and reports will be submitted under separate cover once results are received from the laboratory. Measurable rainfall events during the month of August 2017 began on August 7`h, August 22'd, and August 29h, each measuring 0.68 inches, 0.17 inches, and 0.01 inches, respectively on those days. An additional 0.10 inches, 0.31 inches, 0.95 inches, 0.12 inches, 0.66 inches, 0.12 inches, 0.05 inches, 0.14 inches, 0.15 inches, 0.11 inches, and 1.25 inches of rain were measured on August 8`h, August I Ith, August 120', August 13`h, August 10, August 15`h, August 171h, August 18`h, August 23`d, August 24`h, and August 31", respectively. Each of these events took place on the weekend, after normal business hours, or within 72 hours of the last qualifying storm event. As the seasonal type of storm event is now expected to change to high intensity, short duration events, usually commencing in late afternoon through early evening with little to no notice for preparation, Shield will continue to monitor daily weather conditions and attempt to continue coordination of appropriate staff and resources to facilitate adequate sample collection. Per Section 2, Part IV of General Permit No. NCG030000 Shield will attempt to collect a substitute sample and perform a visual assessment during the next qualifying storm event. Colfax — Monroe facility should complete all relevant sections on the Stormwater Discharge Monitoring Report (DMR). The completed DMR form should then be mailed to the regulatory agency's Central Files. Shield will continue to attempt to perform monthly sampling per Tier Two requirements until instructed to halt by Colfax. Shield greatly appreciates the opportunity to provide environmental services to the Colfax/IMO Industries. If you have any questions in reference to this document or require further information, please feel free to contact either of the undersigned at (704) 394-6913. Respectfully, SHIELD ENGINEERING, INC. QeIin a M. Green Senior Engineer ATTACHMENT C. Boland, PE pal Engineer 4301 Taggart Creek Road Telephow 704.394.013 Charlotte, NC 28208 www.shieldengineering.com Fax 7&4,394.6968 Semi-annual Stormwater Discharge Monitorinjig Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 9/15/17 CERTIFICATE OF COVERAGE NO. NCG030293 FACILITY NAME Colfax/IMO Industries, Inc. PERSON COLLECTING SAMPLES W - LABORATORY: N/A Lab Cert. # NLA Comments on sample collection or analysis: No sample collected due to rain events outside of business hours on weekends or within 72 hours of, the last rain event. Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' August DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ®Other —Class C — Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected' Imo/dd/yr) 24-hour rainfall amount, lnches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks ==W> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L ' 0.067 mg/L 15 mg/L 1 mg/L SDO 004 ---- -- - Monthly sampling sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. The total precipitation must be recorded using data from an on -site rain gauge, Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/l/2D12-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for T70 monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TI'O monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported -in the:format,"<XX Rtl?%l.", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period? Clutfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks = => _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value In excess of the benchmark, you must Implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART li SECTION S. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an orW o) and one copy o this DMR, indudina all -"No Discharge" reports, within 30 dabs of recelat of the lab. results (or arend.of monitoring period In the case of "No Discharge"reports) tn: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "1 certlfy, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified per so roperly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons dire ly r ponsib a for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. ageaVanthat tha e signific4ht penalties for submitting false information, including the possibility of fines and Imprisonment for knowing violations." re Permit Date: 11/1/2012-10/31/2017 7 (Date) SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharee Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 12-1-15 CERTIFICATE OF COVERAGE NO. NCG03 0 2 9 3 FACILITY NAME IMO Pump COUNTY Union PERSON COLLECTING SAMPLES William Iy1er 1 Daniel Cox LABORATORY Pace Analytical tab Cert. # 12 Comments on sample collection or analysis: Now kh-0lenJbht1hTier 3) Failed for Co er'& Zinc Part A: Stormwater Benchmarks and Monitoring Results 00 r SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD 0 Jan -June ❑ July -Dec RECEIVED or Monthly' October fmanrh) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑P Nff DEC 14 ZU1b []Zero -flow ❑Water supply ❑ al CENTRAL FILES ®other Class C - Dry Fork Cre DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -) n No discharge this period? Outfall No. Date Sam le p Collected' (mo/dd/yr) 24hour rainfall amount, 3 Inches Total Suspended Solids p H, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Or ganicss Benchmarks ===> - - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L OF-4 10/27/15 0.15" 3.8 mg/L 6.5 0.008 < 0.005 0.06 11. < 5.0 < 0.002 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 12-1-15 CERTIFICATE OF COVERAGE NO. NCG03 0 2 9 3 FACILITY NAME IMO Pump COUNTY Union PERSON COLLECTING SAMPLES I iam Plyler / Daniel Cox LABORATORY_ Pace_AnalAical Lab Cert. # 12 Comments on sample collection or analysis: Failed for Copper Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD R Jan -June ❑July -Dec or Monthly' September fmonth) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA Zero -flow ❑Water Supply SA Other ClaSS C - Dry For Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 No discharge this period Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicsg Benchmarks ===> _ - 100 mg/L or 50 mg/1. 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L OF-4 09/24/15 0.32" < 5.0 mg/L 6.6 0.0077 < 0.005 0.0657 < 5.0 < 0.002 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 for sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469,12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 9-25-15 CERTIFICATE OF COVERAGE NO. NCG03 0 2 9 3 FACILITY NAME IMO PUMP COUNTY Union PERSON COLLECTING SAMPLES William Plyler / Daniel Cox LABORATORY Pace Analytical Lab Cert. # 12 Comments on sample collection or analysis: Passed: All -Criteria Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or Monthly' month DISCHARGING TO CLASS ❑ORW HQW ❑Trout ❑PNA Zero -flow []WaterSupply ❑❑SA Other Class C - Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 El No discharge this period ?� Outfall No. Date Sam le f Collected (mo/dd/yr) 24-hour rainfall amount. Inches3 Total Suspended Solids pr Standard units d Copper Lead Zinc Non -Polar 08.G/ Total Petroleum Hydrocarbons Total Toxic Organics 5 Benchmarks -=-> - - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L. 1 mg/L OF-4 08/31/15 0.11" 7.2 mg/L 6.6 <0.005 < 0.005 0.0551 < 5.0 0.0012 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 Semi-annual Stormwater Discharize Monitoring Relimirt for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 7-23-15 CERTIFICATE OF COVERAGE NO. NCG03 0 2 9 3 FACILITY NAME IMO Pump COUNTY Union PERSON COLLECTING SAMPLES William Plyler LABORATORY Pace Analytical Lab Cert. # 12 Comments on sample collection or analysis: Failed for Copper and Zinc Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or ® Monthly' Jul month DISCHARGING TO CLASS ❑ORW HQW []Trout [ ]PNA Zero -flow []WaterSupply ❑SA Other Class C - Dry Fork Creek PLEASE REMEMBER TO SIGN ON PAGES Z AND/OR 3 4 No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ==_> - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L OF-4 07/23/15 0.08" 3.4 mg/L 6.4 0.0133 < 0.005 0.148 < 5.0 < .002 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics Is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), l certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Preventio%% Plan. Q/" �aSan Ke,�Ghe r� Name (Print name) Title (Print title) (Sig re) ( ate) Note: Results must be reported In numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must Implement Tier 1, Tier 2, or Tier 3 responses. See General permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. El No discharge this period ?2 Outfall No. Date Sample Collected (mo/dd/yr) 24-hour rainfall amount, Inche2 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =_=> _ 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 f Note: if you report a sample value In excess of the benchmark, you must Implement Tier I, Tier 1, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART it SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: 1 "a 1phcharge" reports. within 30 days of receipt of thg lgk &—sUltj Lor gt cad 0 In the case of "No Dfscharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORT�,D: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware that there are significant pen4ftl for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1Si ure of Permittee} {Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 , Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 1-8-15 CERTIFICATE OF COVERAGE NO. NCG03 0 2 9 3 SAMPLE COLLECTION YEAR 2015 FACILITY NAME IMO Pump �.. SAMPLE PERIOD RJan-June ❑July-Dec COUNTY Union orMonthly' October - (month) PERSON COLLECTING SAMPLES I iam I ler / Daniel Cox DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY_ Pace Analytical Lab Cert. # 12 ❑Zero -flow ❑Water supply []SA Comments on sample collection or analysis: --RECEIVED [Nother Class C - Dry Fork Creek Failed Benchmark for Zinc rjq A 5 2016 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 Part A: Stormwater Benchmarks and Monitoring Results % _N*V AL FILES No discharge this period ?� outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L OF - 4 12/17/15 0.28" < 5.0 mg/L 6.3 0.0064 < 0.005 0.140 < 5.0 < 0.002 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. S Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date:11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my Inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility Is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Preventio7 Plan." Name (Print name) S nr r Title (Print title) (Si ure) (Date) Note: Results must be reported in numerical format. Do not reportBelow Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX ma/L'. where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value In excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See Genera! Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period-? Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks IS mg/L 100 mg/L or So mg/L' 6.0 — 9.0 SU !Footnotes from Part A also apply to this Part B See General Permit text, Table 5, Identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value In excess of the benchmark, you must Implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO IN REGIONAL OFFICE CONTACT NAME: Mail an orlalnal and one copy of this DMR, including all ."No Discharge" reports, within 30 days of receipt of the lab results !or at end of monitoring period In the caste of"No 2lsch-rge"=2rts)-to_: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharee Monitoring -Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 9-25-15 CERTIFICATE OF COVERAGE NO. NCG03 0 2 9 3 FACILITY NAME _ IMO PUMP COUNTY Union PERSON COLLECTING SAMPLES William Plvler / Daniel Cox LABORATORY Pace Analydical Lab Cert. # 12 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results RECEIVED OCT 12 2015 CENTRAL FILES SAMPLE COLLECTION YEAR 2015 DWR SECTIOU.. SAMPLE PERIOD R Jan -June ❑ July -Dec � or Monthlymonth DISCHARGING TO CLASS ❑ORW HQW ❑Trout ❑PNA rn Zero -flow []Watersupply SA Other Class C - Dry ForICCreep PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24haur rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total,Petroleum Hydrocarbons Toxic Organics' Benchmarks - - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L OF-4 08/31/15 0.11" 7.2 mg/L 6.6 <0.005 < 0.005 0.0551 < 5.0 0.0012 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. A See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found In 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported In numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported In the format. "<XX mg/L". where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected (mo/dd/ r) 24-hour rainfall amount, Inches' Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 100 mg/L or 50 mg/L• 6.0 - 9.0 SU Footnotes from Part A also apply to this Part B ' See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Nate: If you report a sample value In excess of the benchmark, you must Implement Tier 1, Tier Z, or Tier 3 responses. See General Permit text. FOR PARTA AND PART B (MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL7 YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mall an oNaiaal gad one copv of this DMR. Including all "No Discharge" reports, within 30 daa 2f receipt of the lab results (or at end of monitoring period In the case gf Nyg J-reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIgNTHIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are sign ifIcaptpena[ties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (signat e o e mittee (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 pate submitted 7-14-15 f CERTIFICATE OF COVERAGE NO. NCG03 0 2 9 3 FACILITY NAME NO Pump COUNTY Union PERSON COLLECTING SAMPLES William Plyier LABORATORY_Pace Analytical Lab Cert. # 12 Comments on sample collection or anal We are implementing Tier 2 Responses Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2015 SAMPLE PERIOD ® Jan -June ❑ July -Dec G` or El 'Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA RECEIVED []Zero -flow []WaterSupply ❑SA JUL Z 9, ?i',15 ®other Class C - Dry Fork Creek CEN j-F<Ali FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 D Vn ❑ No discharge this period Outfall No. Date Sample p Collected' (mo/dd/yr) 24-hour rainfall amount, lnches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks =__> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 06/27/15 0A 9" 7.8 m /L 6.0 0.0086 < 0.005 0.0527 < 5.0 < .002 —OF-4 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/i where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?? Outfall No. Date Sample Collected' '(mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =_=> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 5U i Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 I Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one cony of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case o "No Discharge' re orts 'to: Division of Water Quality Attn: DWQ Central Fifes 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete, am aware thayAhere are signiifigant penalties foy�ubmitting false information, including the possibility of fines and imprisonment for knowing violations." U U (Date) Permit Date: 11/1/2012-10/31/2017 i SWU-245, last revised 10/25/2012 Page 3 of 3 lib Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 7/14114 CERTIFICATE OF COVERAGE NO. NCG03 0 2 9 3 FACILITY NAME IMO Pump COUNTY Union PERSON COLLECTING SAMPLES Daniel Cox LABORATORY Pace Analytical Lab Cert. # 37706 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results RECEIVE . AUG 0 6 2014 CENTRAL P&ES SAMPLE COLLECTION YEAR 2014 DWQ/BOG SAMPLE PERIOD ® Jan -June ❑ July -Dec 0 Monthly' month Rl i D or O CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA AUG 0 ®Other Class C Dry Fork Creek CENTRAL FiLELPLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 OWQ1§OG ❑ No discharge this period?z Outfall No. Date Sample p Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Sus Suspended Solids p H, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks ===> - - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 0174 06/27/14 0.41 1n3 6.3 mg/L 6.3 0.0055 mg/L <0.005 mg/L 0.048 mg/L <0.005 mg/L 0.005 mg/L ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. "See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. , 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/201.7 SWU-245, last revised 10/25/2012 Page 1 of 3 I Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics Into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is Implementing the all the provisions of the solvent management plan Included in the Starmwater Pollution Prevention Plan." Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported In numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX melt". where XX is the numerical value of the detection limit, reporting limit, etc, in mg/L. Note: if you report a sample value In excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. No discharge this period? Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inche2 Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks ===> - - 15 mg/L 100 mg/L or So mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table S, Identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: if you report a sample value In excess of the benchmark, you must implement Tier 1, 77er 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEED ENCES FORTH E SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ No ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copv of th_ is DMR. Including all "No Discharge" resorts, within 30 days of recizlgt of the lakfesults (or at end of monftodna nerlod In the cased "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mall Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons dirertjy reSponsible for r g the /lnfrmation, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that t a _ lgniflq�nt n tl for subing false information, Including the possibility of fines and imprisonment for knowing violations." 7 .2 (Signature of Permittee) (Date Permit Date: 11/1/2012-10/31/2017 SWU-24S, last revised 10/25/2012 Page 3 of 3