NCG030283_COMPLETE FILE - HISTORICAL_20100208

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
/v
DOC7YPE
HISTORICAL FILE
❑ MONITORING REPORTS
DOC DATE
❑ a?ZII 0 t%al%f
YYYYMMDD

Allocco, Marcia
From:
Allocco, Marcia
Sent:
Monday, February 08, 2010 3:39 PM
To:
'Terry Carter'
Cc:
'Eubanks, Ron'
Subject:
Additional Sampling
Terry,
just wanted to document my site visit last Thursday (2/4/10) and the additional sampling that I requested as
part of your Tier Il response under NCG030283. I wanted to thank you for your assistance during the visit and
for your actions to date to reduce the lead concentrations in the stormwater released from the Dixon Quick
Coupling site.
After reviewing your site it was agreed by all parties present that the following locations would be sampled for
lead in an attempt to determine the source of the elevated lead in the stormwater on site.
• Catch basin behind the warehouse (2 samples) — this catch basin appears to be at the head of the
drainage line that runs through "brass alley". There were two pipes that discharge to this catch basin.
One appears to be a roof drain line and the other pipe's source was not evident and could be adding
stormwater flow from off -site. Both pipes should be sampled. Sampling of this catch basin would give
a "background" concentration for lead before entering "brass alley".
• Discharge pipe at the end of "brass alley" (1 sample) — this sample should show how much lead is
added to stormwater from the brass stored in this area
• Brass storage (1 sample) -- this sample is to be of water poured over the brass rods stored in brass
alley" to ascertain how much lead might be shed from -the storage of this material outside and exposed
to stormwater.
• Current outfall (2 samples) — it was noted during the inspection that there are two pipes that contribute
stormwater to the current "outfall" that is being sampled on site. One pipe comes from the parking lot
and "brass alley" and the other collects stormwater from the drainage line that runs through the main
Dixon manufacturing area. This sample should identify if one of these areas is contributing more lead
than the other to stormwater discharges from the site
During the site visit the compliance status of Atlantic Scrap and Processing facility on Atando Avenue (across
the street) was raised. After some research it was determined that this facility is currently covered under
Certificate of Coverage NCG200351, Wholesale Trade of Metal Waste and Scrap stormwater discharges.
Our database indicates that the facility was inspected for compliance with their NPDES permit in early 2008 by
Ms. Heather Sorensen and Ms. Erin Hall of the Charlotte -Mecklenburg Stormwater Services Group (Mr. Ron
Eubanks's co-workers) and Atlantic Scrap and Processing was found to be compliant with this general permit
at the time of the inspection.
Please forward the stormwater samples results when you get them so we can discuss and determine any
additional sampling/measurements at Dixon Quick Coupling.
Regards,
Marcia
Marcia Allocco, MS - Environmental Chemist
NC Dept. of Env. & Natural Resources (NCDENR)
Division of Water Quality - Surface Water Protection Group
610 East Center Ave., Suite 301, Mooresville, NC 28115
Ph: [phone] Fax. [phone]

Please note: my e-mail address has changed to marcia.allocco(bncdenr.aov
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be
disclosed to third parties.

Allocco, Marcia
From: Eubanks, Ron [[e-mail])
Sent: Thursday, February 04, 2010 4:20 PM
To: Terry Carter
Cc: [e-mail]; [e-mail]; Allocco, Marcia
Subject: Dixon Quick Coupling - Tier Two Monitoring
Terry,
After our meeting earlier today, Marcia and I inspected the adjacent property. From the inspection, we did not identify
any storm drain inlets other than the one large catch basin adjacent to the fence that is covered with vegetation and
underbrush. There was an uncovered scrap metal dumpster on the property, but it was empty. There were no other
obvious indicators of lead contamination observed on the property. As we discussed during the meeting, please plan to
collect storm water samples for lead from the five (5) locations identified during the inspection meeting.. Please send
me an e-mail or contact me at [phone], if you have any questions or need additional information regarding this
matter. Thanks again to you, Crystal, and Scott for your help with the Tier Two storm water monitoring inspection.
Have a good evening.
Ron Eubanks
Environmental Specialist
Mecklenburg County Water Quality Program
700 North Tryon Street
Charlotte, North Carolina 28202
Phone: [phone]
Fax: [phone]
E-mail: Perry. Eubanks(cDMecklenburgCountyNC.gov

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Allocco, Marcia
From: Eubanks, Ron [[e-mail]]
Sent: Monday, December 07, 2009 5:16 PM
To: Pickle, Ken
Cc: Georgoulias, Bethany; Bennett, Bradley; Allocco, Marcia
Subject: RE: Dixon Quick Coupling - NCG030306
Ken,
I apologize for the confusion. There was a concrete storm sewer pipe that drained storm water runoff from the scrap
metal dumpster area at the site. The paved areas around the dumpsters were cleaned and a structural canopy was
installed over the scrap metal dumpsters. To verify if the control measures were successful, clean water was discharged
into the storm sewer at the site from a water truck to simulate a storm event. The sample collected from the water
truck was non -detect for lead; however, the samples collected from the outfall were above the benchmark. In other
words, clean water discharged into the storm sewer at the site was still above the benchmark for lead at the outfall. To
address the possibility of residual lead contamination in the storm sewer at the site, the concrete pipe was replaced with
HDPE pipe. Please send me an e-mail or contact me at [phone], if you have any additional questions or concerns
regarding this matter.
Thank you,
Ron Eubanks
Environmental Specialist
Mecklenburg County Water Quality Program
700 North Tryon Street
Charlotte, North Carolina 28202
Phone: [phone]
Fax: [phone]
E-mail: Perry. Eubanks(&MecklenbumCountyNC.gov
From: Pickle, Ken ( mailto: ken. [e-mail]]
Sent: Monday, December 07, 2009 4:32 PM To: Eubanks, Ron
Cc: Georgoulias, Bethany; Bennett, Bradley; Allocco, Marcia
Subject: RE: Dixon Quick Coupling - NCG030306
Ron,
Just curious really. What am I missing here? A concrete pipe was a potential source for lead contamination? What don't
I understand about these circumstances?
Ken
From: Eubanks, Ron [mailto: Perry. [e-mail]]
Sent: Monday, December 07, 2009 3:46 PM
To: Pickle, Ken
Cc: Georgoulias, Bethany; Bennett, Bradley-, Allocco, Marcia
Subject: RE: Dixon Quick Coupling - NCG030306

Ken,
Thank you for the information. I will discuss your comments with Mr. Terry Carter (Dixon Quick Coupling), who is
currently preparing the Tier 2 response. Dixon Quick Coupling has not installed any structural BMPs to treat lead in the
storm water runoff, but they have installed a structural canopy over the scrap metal dumpsters and they have replaced
a section of the storm water concrete pipe near the outfall that was a possible source of the lead contamination. As I
indicated in the earlier e-mail, Dixon Quick Coupling is also investigating possible off -site sources of lead. Thanks again
for your help. Please send me an e-mail or contact me at [phone], if you have any questions or need additional
information regarding this matter.
Have a good evening.
Ron Eubanks
Environmental Specialist
Mecklenburg County Water duality Program
700 North Tryon Street
Charlotte, North Carolina 28202
Phone: [phone]
Fax: [phone]
E-mail: Pens.Eubanks(&Mecklenbu[gCountyNC.(I
From: Pickle, Ken [mailto:[e-mail]]
Sent: Monday, December 07, 2009 9:17 AM
To: Eubanks, Ron
Cc: Georgoulias, Bethany; Bennett, Bradley; Allocco, Marcia
Subject: RE: Dixon Quick Coupling - NCG030306
Hi Ron, nice to hear from you again. Thanks for your help with Wallace Farm in 2008. I've inserted comments in your
note. unfortunately, we don't have a substantial data base on Tier 2 responses, yet. We do have some few facilities
that have notified us of a Tier 2 status, and I think one or two facilities that have accumulated the four exceedences that
would trigger a DWQ/Meck site visit and determination of feasible responses. But we don't have anything approaching
a 'database', or even an expectation of proper responses, yet.
See my further comments below.
Bethany, any additional help for Ron and Marcia?
Ken
From: Bennett, Bradley
Sent: Wednesday, December 02, 2009 4:13 PM
To: Georgoulias, Bethany; Pickle, Ken
Subject: FW: Dixon Quick Coupling - NCG030306
Hey Guys
I think you can help provide some feedback to Ron on these issues.

Thanks
BB
Bradley Bennett
Stormwater Permitting unit
NC Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Phone: [phone]
Fax: [phone]
Email: [e-mail] (New Email Address)
Web: http://h2o.enr.state.nc.us/su/index.htm
Email correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties.
From: Eubanks, Ron [mailto: Perry. [e-mail]]
Sent: Wednesday, December 02, 2009 3:54 PM
To: Bradley Bennett
Cc: Allocco, Marcia; [e-mail]
Subject: Dixon Quick Coupling - NCG030306
Hey Bradley,
I conducted a Storm Water Compliance Evaluation Inspection at Dixon Quick Coupling (332 Atando Avenue, Charlotte)
on March 27, 2009. Since the inspection, I have been working with Mr. Terry Carter (Dixon Quick Coupling) to address
storm water concerns at the site. As you may be aware, Dixon Quick Coupling has exceeded their benchmark
monitoring requirement for lead and they are currently preparing a Tier Two Response. From inspections at the site and
meetings with Mr. Terry Carter, Dixon Quick Coupling has implemented both structural and nonstructural storm water
control measures to address the elevated concentrations of lead in the storm water runoff from the site.
So, presumably the source of the lead is not a mystery, right? Dixon knows that lead is on their site because it's in their
manufacturing process somewhere, right? And presumably the control measures are primarily avoiding exposure,
rather than treatment?
From a recent storm water monitoring event, samples were collected at multiple locations on the property. There is
some sheet flow from the adjacent property that drains onto the Dixon Quick Coupling property.
Is there some suspicion that lead is coming onto the Dixon site from another source? If so, our general approach would
be that Dixon is responsible for pollutants generated by them, or their predecessors, on their site: but they're not
responsible for pollutants generated by other folks.
The Mecklenburg County Water Quality Program will continue to work with NCDENR-Mooresville Regional Office to
identify potential sources of lead at the Dixon Quick Coupling site and other properties in the surrounding watershed_ In
the meantime, I would like to get some information from you or your staff on how similar facilities have addressed
exceedences of their benchmark monitoring requirements.
For Ter Two, facilities are required to shift into monthly sampling, and attempt again to evaluate the feasibility of some
control response. We have limited data to date. None on lead, as far as I know (This Tiered approach is so new that we
generally pay attention when someone actually installs a control measure in response to the analytical results, and I'm
not aware of any on lead, yet.) But, again, it's usually cheaper for the permittee to control exposure, rather than install
BMPs.

In general folks prefer limiting exposure to finding the site space to accommodate a new structural BMP —generally it's
cheaper, and it doesn't require taking up part of the available space on site.
As long as the permittee is in Tier One, or Tier Two, the initiative is on them to do what they can to meet the
benchmarks. When they hit four exceedences for one parameter at one outfall, their obligation is to contact
DWQ/Meck and we will help them decide what makes sense as far as getting the pollutant discharge under control, if
feasible. It sounds like they have shortcut that process a little bit, and have got you involved early. That's fine, of
course. —
Are there many facilities covered under General Permit No. NCGO30000 that have exceeded the benchmark value for
lead.
I don't have time this week or next to research this for us. My time is spoken for over that period. I'll be glad to help
after Christmas.
If a facility is not able to meet the analytical monitoring requirements of the General Permit, should they apply for an
Individual Permit?
Maybe, but not necessarily. Let's attempt the Tier One response, and the Tier Two response, and see what success they
have. If they continue on and accumulate four exceedences, then an individual permit is an option, but in the
circumstances as I understand them at Dixon, what benefit would that be? They'd still have a lead benchmark that they
can't meet. 5o, while I can imagine circumstances at Dixon that would lead us to require an individual permit, we'd first
rather play out the procedure, go through the steps, and see what progress we can make with them still under the
General Permit. Because:
The new NCG03 General Permit allows DWQ the freedom to direct control measures: previously we more or less
implemented our program by only requiring BMPs within the framework of an Individual Permit. But now, with the
new template for General Permits, we can accomplish that within the General Permit.
Please send me an e-mail or contact me at [phone] to discuss at your convenience. Thank you.
Have a good evening.
Ron Eubanks
Environmental Specialist
Mecklenburg County Water Quality Program
700 North Tryon Street
Charlotte, North Carolina 28202
Phone: [phone]
Fax: [phone]
E-mail: Perry. [e-mail]

Allocco, Marcia
From: Eubanks, Ron [[e-mail]]
Sent: Monday, December 07, 2009 3:59 PM
To: Allocco, Marcia
Cc: Pickle, Ken; Georgoulias, Bethany; Bennett, Bradley
Subject: RE: Dixon Quick Coupling - NCG030306
Hey Marcia,
In addition to some structural controls, Dixon Quick Coupling has also implemented some housekeeping measures such
as routine parking lot sweeping at the site. Please let me know if you want to schedule a follow-up site inspection at
Dixon Quick Coupling, after the Tier 2 response is completed. Please send me an e-mail or contact me at (704) 336-
5446, if you have any questions or need additional information regarding this matter. Thank you.
Have a great week!
Ron Eubanks
Environmental Specialist
Mecklenburg County Water Quality Program
700 North Tryon Street
Charlotte, North Carolina 28202
Phone: [phone]
Fax: [phone]
E-mail: Pent'.Eubanks(c)Mecklenbu[gCountyNC.yov
From: Allocco, Marcia fmailto:[e-mail]]
Sent: Monday, December 07, 2009 9:46 AM
To: Pickle, Ken; Eubanks, Ron
Cc: Georgoulias, Bethany; Bennett, Bradley
Subject: RE: Dixon Quick Coupling - NCG030306
Galvan in Cabarrus County had exceeded the lead numbers for NCG030000 and they had much lower and
compliant numbers after some "housekeeping"
Marcia
From: Pickle, Ken
Sent: Monday, December 07, 2009 9:17 AM
To: [e-mail]
Cc: Georgoulias, Bethany; Bennett, Bradley; Allocco, Marcia
Subject: RE: Dixon Quick Coupling - NCG030306
Hi Ron, nice to hear from you again. Thanks for your help with Wallace Farm in 2008. I've inserted comments in your
note. Unfortunately, we don't have a substantial data base on Tier 2 responses, yet. we do have some few facilities
that have notified us of a Tier 2 status, and I think one or two facilities that have accumulated the four exceedences that
would trigger a DWQ/Meck site visit and determination of feasible responses. But we don't have anything approaching
a `database', or even an expectation of proper responses, yet.
See my further comments below.

Bethany, any additional help for Ron and Marcia?
Ken
From: Bennett, Bradley
Sent: Wednesday, December 02, 2009 4:13 PM
To: Georgoulias, Bethany; Pickle, Ken
Subject: FW: Dixon Quick Coupling - NCG030306
Hey Guys
I think you can help provide some feedback to Ron on these issues.
Thanks
BB
Bradley Bennett
Stormwater Permitting Unit
NC Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Phone: [phone]
Fax.[phone]
Email: [e-mail] (New Email Address)
Web: http://h2o.enr.state.nc.us/su/index,htm
Email correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties.
From: Eubanks, Ron [mailto:[e-mail]]
Sent: Wednesday, December 02, 2009 3:54 PM
To: Bradley Bennett
Cc: Allocco, Marcia; [e-mail]
Subject: Dixon Quick Coupling - NCG030306
Hey Bradley,
conducted a Storm Water Compliance Evaluation Inspection at Dixon Quick Coupling (332 Atando Avenue, Charlotte)
on March 27, 2009. Since the inspection, I have been working with Mr. Terry Carter (Dixon Quick Coupling) to address
storm water concerns at the site. As you may be aware, Dixon Quick Coupling has exceeded their benchmark
monitoring requirement for lead and they are currently preparing a Tier Two Response. From inspections at the site and
meetings with Mr. Terry Carter, Dixon Quick Coupling has implemented both structural and nonstructural storm water
control measures to address the elevated concentrations of lead in the storm water runoff from the site.
So, presumably the source of the lead is not a mystery, right? Dixon knows that lead is on their site because it's in their
manufacturing process somewhere, right? And presumably the control measures are primarily avoiding exposure,
rather than treatment?
From a recent storm water monitoring event, samples were collected at multiple locations on the property. There is
some sheet flow from the adjacent property that drains onto the Dixon Quick Coupling property.

Is there some suspicion that lead is coming onto the Dixon site from another source? If so, our general approach would
be that Dixon is responsible for pollutants generated by them, or their predecessors, on their site: but they're not
responsible for pollutants generated by other folks.
The Mecklenburg County Water Quality Program will continue to work with NCDENR-Mooresville Regional Office to
identify potential sources of lead at the Dixon Quick Coupling site and other properties in the surrounding watershed. In
the meantime, I would like to get some information from you or your staff on how similar facilities have addressed
exceedences of their benchmark monitoring requirements.
For Tier Two, facilities are required to shift into monthly sampling, and attempt again to evaluate the feasibility of some
control response. We have limited data to date. None on lead, as far as I know (This Tiered approach is so new that we
generally pay attention when someone actually installs a control measure in response to the analytical results, and I'm
not aware of any on lead, yet.) But, again, it's usually cheaper for the permittee to control exposure, rather than install
13MPs.
In general folks prefer limiting exposure to finding the site space to accommodate a new structural BMP— generally it's
cheaper, and it doesn't require taking up part of the available space on site.
As long as the permittee is in Tier One, or Tier Two, the initiative is on them to do what they can to meet the
benchmarks. When they hit four exceedences for one parameter at one outfall, their obligation is to contact
DWQ/Meck and we will help them decide what makes sense as far as getting the pollutant discharge under control, if
feasible. it sounds like they have shortcut that process a little bit, and have got you involved early. That's fine, of
course.
Are there many facilities covered under General Permit No. NCG030000 that have exceeded the benchmark value for
lead.
don't have time this week or next to research this for us. My time is spoken for over that period. I'll be glad to help
after Christmas.
If a facility is not able to meet the analytical monitoring requirements of the General Permit, should they apply for an
Individual Permit?
Maybe, but not necessarily. Let's attempt the Tier One response, and the Tier Two response, and see what success they
have. If they continue on and accumulate four exceedences, then an individual permit is an option, but in the
circumstances as I understand them,at Dixon, what benefit would that be? They'd still have a lead benchmark that they
can't meet. 5o, while I can imagine circumstances at Dixon that would lead us to require an individual permit, we'd first
rather play out the procedure, go through the steps, and see what progress we can make with them still under the
General Permit. Because:
The new NCG03 General Permit allows DWQ the freedom to direct control measures: previously we more or less
implemented our program by only requiring BMPs within the framework of an Individual Permit_ But now, with the
new template for General Permits, we can accomplish that within the General Permit.
Please send me an e-mail or contact me at [phone] to discuss at your convenience. Thank you.
Have a good evening.
Ron Eubanks

Environmental Specialist
Mecklenburg County Water Quality Program
700 North Tryon Street
Charlotte, North Carolina 28202
Phone: [phone]
Fax: [phone]
E-mail: Perry. Eubanks �MecklenbumCuntyNC.gov

Tier One and Tier Two Response
Permit NCG030000
The Right ConnectionTM
Dixon Quick Coupling
A Member of the Dixon Group
DEC 19 2009
December 14, 2009
Terry Carter Facilities Engineer

1.0 Introduction
Dixon Quick Coupling is a manufacturer of Quick Disconnect Couplings_ These
couplings are made from a variety of materials including brass, steel and stainless steel.
Dixon Quick Coupling is located at 332 Atando Avenue Charlotte North Carolina on
approximately 4.2 Acres_ Dixon Quick Coupling's facility has approximately 77,835
square feet under roof.
Beginning in February 2009, Dixon Quick Coupling began its storm water
management practices depicted in General Permit NCG03000. It became apparent that we
are exceeding our benchmark goal in total lead. Working together with Aware
Environmental, located in Charlotte, we immediately began taking measures to correct this
issue.
Ron Eubanks with the Mecklenburg County Storm Water Quality Program came to
our facility to conduct a storm water compliance evaluation. Dixon Quick Coupling passed
this inspection knowing that we were expected to work towards meeting our total lead
permit threshold. We worked closely with Ron, and at times ran split storm water samples
that were tested by the City of Charlotte, producing results at or near the result levels
analyzed by Pace Analytical. Pace Analytical is a local laboratory located in Huntersville,
NC used by Dixon Quick Coupling in the testing of storm water.
The following pages are details of measures taken to reduce total lead.
2.0 Testing and Control Measures
• February 27, 2009
Ist qualifying storm event
Samples were taken by Dixon Quick Coupling and tested by Pace Analytical for Ph,
Total Lead, Total Suspended Solids, Oil and Grease
• March 06, 2009
Received test results listed below for the storm event dated February 27, 2009
Table 1
Outfall
Date
Total Suspended
Lead,
Oil and
No.
Collected
Solids
pH Total
Grease
No. 2
1 Feb 27, 2009
108 m
7.9 .314 m /L 1
16.7 m /L
Dixon Quick Coupling knowing that we were above our benchmarks on total lead
took the following steps to correct the issue:

March 16, 2009
• Dixon Quick Coupling excavated the area adjacent to the storm drain and added
rock around the perimeter of the shipping area to alleviate the soil erosion in those
areas. Bales of wheat straw were added to the entrance of the storm drain to catch
any foreign debris before entering the storm drain.
• March 21, 2009
Dixon Quick Coupling had the entire shipping area pressure washed, having all
residue properly removed from the premises.
• April 30, 2009
Dixon Quick Coupling purchased a building to cover and contain the scrap chip
dumpsters stored in the shipping area.
• July 28, 2009
1st qualifying storm event after improvement activities were complete.
Samples were taken by Dixon Quick Coupling and tested by Pace Analytical for Ph,
Total Lead, Total Suspended Solids, Oil and Grease
• August 5, 2009
Received test results listed below for the storm event dated July 28, 2009
Table 2
Outfall Date Total Suspended Lead, Oil and
No. Collected Solids pH Total Grease
No.2 July 8, 2009 4.2 mg/L 6.0 .101 mg/L I None detected
Dixon Quick Coupling knowing that we remained above our benchmarks on total
lead took the following steps to correct the issue.
• August 24 2009
Dixon Quick Coupling performed a mock storm event.
A water truck was hired to bring water to our facility to aid in determining the
source of the lead causing us to exceed our total lead benchmark.
The process for the aforementioned is as follows:
l . The water truck would park within 20 feet from the entrance of the storm drain.
2. The driver of the water truck would start the water draining from his truck.
3 _ A sample was taken directly from the truck.
4. The water from the truck was allowed to follow the path of a normal rain event
and another sample was taken from outfall No.2.
5. The sample taken directly from the truck as well as the sample taken from
outfall No.2 was tested for total lead by Pace Analytical.

Ron Eubanks with the Mecklenburg Division of Water Quality was present for
this test and ran split samples that were tested by the City of Charlotte. These test
results are listed along with samples tested by Pace Analytical.
• August 29, 2009
Received test results listed below for the Mock Storm Event dated August 29, 2009.
Table 3 DQC Sampling
Outfall No. Date Collected Total Suspended Solids pH Lead, Total Oil and Grease
Water Truck
August 29, 2009
1
1 None Detected
No.2
August 29, 2009
.041 m
Table 3 DWQ Sampling
Outfall No. Date Collected Total Suspended Solids pH Lead, Total Oil and Grease
Water Truck
August 29, 2009
None Detected
No.2
August 29, 2009
.180 m
• September 9, 2009
Dixon Quick Coupling replaced the storm drain from the entrance to the junction
box where storm water samples are taken_ The floor was also re -poured to help in
the reduction of lead in the drain.
• September 23, 2009
Dixon Quick Coupling performed another mock storm event. Samples were taken
and tested for Total Lead by Pace Analytical.
Ron Eubanks with the Mecklenburg Division of Water Quality was present for this
test and ran split samples that were tested by the City of Charlotte. These test results
are listed along with samples tested by Pace Analytical.
• September 25, 2009
Received test results listed below for the Mock Storm. Event dated September 23,
2009,
Table 4 DQC Sam lin
Outtall No. Date Collected Total Suspended Solids pH Lead, Total Oil and Grease
Water Truck
September 23, 2009
None Detected
No.2
September 23, 201
.145
Table 4 DWQ SampUmg
Outfall No. Date Collected Total Suspended Solids pH Lead, Total Oil and Grease
Water Truck
I September 23, 2009
1
1
1 None Detected
No.2
J_September23,200,9
I
1
1 .210 MqAt

September 28, 2009
Dixon Quick Coupling moved the brass turnings trailer under the new building to
help prevent rain from being filtered through the brass turnings. The shipping area
is now being swept twice weekly and any turnings or other particulate found in the
shipping area is removed.
• October 17, 2009
Dixon Quick Coupling had the entire slipping area pressure washed having all
residue properly removed from the premises.
• October 22, 2009
Dixon Quick Coupling performed another mock storm event. Samples were
taken and tested for total lead by Pace Analytical.
• October 26, 2009
Received test results listed below for the Mock Storm Event dated October 22, 2009
Table 5
Outfall No. Date Collected Total Suspended Solids pH Lead, Total Oil and Grease
Water Truck
October a 2009
None Detected
No. 2
October 22, 2009
.056 m
• November 10, 2009
1:4 qualifying storm event after further improvements were made.
• November 13, 2009
Received test results listed below for the storm event dated November 13, 2009.
Table 6
Outfall No. Date Collected Total Suspended Solids pH Lead, Total Oil and Grease
No.2
November 10, 2009
102 m
7.5
.314
1 None Detected
• As a part of the November 13, 2009 testing, we also sampled storm water coming
onto our property from an adjacent property as well as other areas on our property
depicted below. These samples were tested for total lead only.
Table 7
Outfall No. Date Collected Total Suspended Solids pH Lead, Total Oil and Grease
Behind Warehouse
November 10, 2009
.0393 mg/L
Loading Dock
November 10, 2009
.194 m /L
Roof at Shipping
November 10, 2009
.026 mWL
• December 8, 2009
Dixon Quick Coupling performed Tier 11 Stormwater sampling.

• Received test results listed below for the Storm Event dated December 8,
2009.
Table S
Outfall No. Date Collected Total Suspended Solids pH Lead, Total Oil and Grease
No.2
December 8, 2009
24.5 mg/L
7.5
.103 mg1L
8.4 mg/L
3.0 Conclusion
Dixon Quick Coupling will continue to monitor and to the best of our ability determine the
source of lead on the property. General housekeeping along with other potential structural
BMP's are being researched.
One concern, as referenced in Table 7, refers to a total lead concentration of .0393mg/L
which was taken from behind our warehouse of storm water coming from an adjacent
property_ This sample also exceeds the current threshold prior to entering the Dixon Quick
Coupling property. It appears that the failure to meet the total lead threshold could be
complicated by the run off from adjacent properties.
Please find enclosed all test reports, as well as before and after pictures of measures taken
to become compliant in total lead.
Any assistance your office can give in this matter will be greatly appreciated.

February 2009 Before Improvements to Shipping Area

May 2009 After Improvements to Shipping Area

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aceAnalyfical-
warai.1sciolallaxam
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody 13 a LEGAL DOCUMENT. All relevant fields must be Completed accurately.
Section A Section 8Section C
Pop: Of
Required Client Information; Required Pm)M Information: hyalce Informatlow
Report To: Attention;
ComT,
1178905
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K �q,,JQ,,r,5 Ca,ot kick" br edge-
AddlU
Copy To:
cam Name
KL
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"042
0%Q
Address:
F NPDEs r GROUND WATER r— DRINKING WATER
r— LIST r— RCRA OTHER
Email To:
Purchase Order Na.:
Pace Quote
Phone:
"ad Name:
Q.JICK co,"Ril-11
Pam Project
Manager.
t,
Requested Due DstwJTAT-
1proled Number.
acl b
Pam Prom
N.
Section 0 Matrix Codes
COLLECTED
"UftdCU@ni Infomw*n MURIX I CODE
1
Preservatives
DrinklingWater DW
8
water WT
Waste Water Ww
COMPOSITE
START
COMPOSITE
ENDIGf"
Product P
Soll/Solld SL
SAMPLE ID Oil of.
ps WP
(A-Z. 0-9 1,.) Air AR
Sample lDs MUST BE UNIQUE Tlasue TS
UJI
IM
a4w
w
Other OT
8
Ilk
rN
0
2
DATE
TIME
I DATE
TIME
I
A
x
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Pace Project NOJ Lab I.D.
'A
lienDly.
10.0,4
Al
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III
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SAMPLE CONDITIONS
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ORIGINAL
.M
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PRINT Name of SAMPLER.
V
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DATE Stoned
SIGNATURE of SAMPLER:
-1, X-1
(MM/Dorm: 0
I CA
19
'Important Note: By signing this form you are noDeptino Pace's NET 30 day payment term and monasino to late rharoes of 1.6% oar month for any involle not onto WOW 30 daysNI-1— F-ALL-U-wurevw. i9-may-zuu7

11!; eAnalytical'
I
i
Client u ' 01
-
Courier: ❑ Fed Ex ❑ UPS ❑ USPSP Client ❑ Commercial ❑ Pace Other
Custody Seal on Cooler/Box Present: ❑ yes Wno Seals intact: ❑ yes Ono
Packing Material: ❑ Bubble Wrap j"ubble Bags ❑ None ❑Other
Thermometer Used T060 Type of Ice: (-Vi)t Blue None --- -famples on ice, cooling process has begun
Cooler Temperature U , 'i
Temp should be above freezing to 6'C
Biological Tissue is Frozen: Yes No NIA Date and itiats of pers examining
conten
Comments:
Chain of Custody Present:
At iYes
❑No
❑NIA
i.
Chain of Custody Filled Out:
Byes
❑No
ONIA
2.
Chain of Custody Relinquished:
BTes
❑No
❑NIA
3_
Sampler Name & Signature on COC:
s
❑No
❑NIA
4.
Samples Arrived within Hold Time:
tJres
❑No
❑NIA
5.
Short Hold Time Analysis (<72hr):
❑Yes .Ono
❑NIA
6.
Rush Turn Around Time Requested:
❑Yes
Brio
❑NIA
7.
Sufficient Volume:
fes
❑No
❑NIA
8.
Correct Containers Used:
-Pace Containers Used:
$ices
Byes
❑No
❑No
❑NIA
❑NIA
g.
Containers Intact:
.21 s
❑No
❑NIA
10. .
Filtered volume received for Dissolved tests
❑Yes
❑No -ESNIA
11.
Sample Labels match CDC:
-Includes date/time/ID/Analysis Matrix:
OY-es— ❑No
LA)-7
❑NIA
12.
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation.
exceptions: VOA, coliform. TOC, obG, 1MI-DRO (water) _
U*e5
Yes
❑Yes
❑No
❑No
❑No
❑NIA
❑N1A
13.
Initial when completed
Samples checked for dechlo6nation:,
❑Yes
[:)No — taNM
14.
Headspace in VOA Vials (>6mm):
❑Yes
❑No
L3W
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (if purchased): NIA
❑Yes
❑Yes
❑No
❑No
.CLwK
910A'
16.
Client Notification/ Resolution: Field Data Required? Y I N I NIA
Person Contacted: Date rime:
Comments/ Resolution:
Project Manager Review:
Date:262 (d
Note-. Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( Le out of hold, incorrect preservative, out of temp, incorrect containers)

Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
March 06, 2009
Ms. Carol Hambridge
Aware Environmental
PO Box 2669
Matthews, NC 28106
RE: Project: Dixon Quick Coupling
Pace Project No.: 9238936
Dear Ms. Hambridge:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 27, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie McKee
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
l'
Page 1 of 9

n�, Pace Analytical Services, Inc. Pace Analytical Services, Inc.
�
alA 2225 Riverside Dr, 9800 ICnoeyAve. Suite 100
wwwpaJ " om Asheville, NC 28804 Huntersville, NC 28076
[phone] [phone]
CERTIFICATIONS
Project: Dixon Quids Coupling
Pace Project No.: 9238936
Charlotte Certification IDs
West Virginia Certification M 357
North Carolina Field Services Certification M 5342
Virginia Certification M 00213
North Carolina Drinking Water Certification M 37706
Tennessee Certification M 04010
New Jersey Certification M NC012
South Carolina Drinking Water Cert M 990060003
Louisiana/LELAP Certification M 04034
South Carolina Certification M 9900600D1
Kentucky UST Certification M 84
Pennsylvania Certification #: 68-00784
FloridaMELAP Certification M E87627
Connecticut Certification #: PH-0104
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
West Virginia Certification #: 356
Pennsylvania Certification #: 68-03578
Virginia Certification #: 00072
North Carolina Wastewater Certification M 40
Connecticut Certification M PH-0106
North Carolina Drinking Water Certification M 37712
Florida/NELAP Certification M E87648
North Carolina Bioassay Certification #: 9
Tennessee Certification #: 2980
New Jersey Certification M NC011
South Carolina Certification M 99030001
Massachusetts Certification #: M-NC030
South Carolina Bioassay Certification #: 99030002
LouisianalLELAP Certification #: 03095
Eden Certification IDs
North Carolina Wastewater Certification M 633
North Carolina Drinking Water Certification M 37738
Virginia Drinking Water Certification M 00424
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 9
•ccc

ceAnaly�i{cal
a�ww.Amaedaha.o4m
Project: Dixon Quids Coupling
Pace Project No.. 9238936
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
woo Kncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
9238936001 Sample Location #2 EPA 1664A
DNP
1
PASI-C
EPA200.7
SHB
1
PASI-A
EPA 9040
TEE
1
PASI-A
SM 2540D
SAJ
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc..
4q �M CCp�O.
o
Page 3of9

a
Pace Analytical Services, Inc.
AWcal
2225 Riverside Dr.
WWW. cem
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Dixon Quick Coupling
Pace Project No.: 9238936
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 +
[phone]
Sample: Sample Location #2
Parameters
Lab ID: 9238936001 Collected: 02/27/09 13:10 Received:
Results Units Report Limit DF Prepared
02/27/09 14:40 Matrix: Water
Analyzed CAS No. Quaff
HEM, Oil and Grease
Analytical Method: EPA 1664A
Oil and Grease
16.7 mg/L
5.0 1
03/05/09 11:11
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead
314 ug/L
5.0 1 03/03/09 10:15 03/03/09 21:24 7439-92-1
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
108 mg/L
20.0 1
03/04/09 13:11
9040 pH
Analytical Method: EPA 9040
pH
7.9 Std. Units
0.10 1
03/03/09 16:30 H6
Date: 03/06/2009 02:26 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
\4
Page 4 of 9

ceftVical
Project: Dbcon Quick Coupling
Pace Project No.: 9238936
QC Batch: WE T 7430
QC Batch Method: EPA 9040
Associated Lab Samptes: 9238936001
SAMPLE DUPLICATE: 244602
Parameter Units
pH Std. Units
Date: 03l0612009 02:26 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description: 9040 pH
9238856001 Dup
Result Result RPD Qualifiers
9.0 9.0 0 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 9

wwwwolmlarm
Project: Dixon Quick Coupling
Pace Project No.: 9238936
QC Batch: WET17435
QC Batch Method: SM 2540D
Associated Lab Samples: 9238936001
METHOD BLANK: 244608
Associated Lab Samples: 9238936001
Parameter Units
Total Suspended Solids mg/L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 1.0 03/04/0913:11
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 ■
[phone]
LABORATORY CONTROL SAMPLE: 244609
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mglL 250 224 90 BD-120
SAMPLE DUPLICATE: 244610
Parameter
Total Suspended Solids
Date: 03/06/2009 02:26 PM
9238936001
Units Result
mglL 108
Dup
Result
104
RPD Qualifiers
4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 9

eArWbal
WWWPgaele &WM
Project: Dixon Quick Coupling
Pace Project No.: 9238936
QC Batch: GCSV/4885
QC Batch Method: EPA 1664A
Associated Lab Samples: 9238936001
METHOD BLANK 245321
Associated Lab Samples: 9238936001
Parameter Units
Oil and Grease mg1L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 1664A
Analysis Description: 1664 HEM, Oil and Grease
Matrix. Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 03/05/0910:51
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078 •
[phone]
LABORATORY CONTROL SAMPLE.
245322
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 36.4
91
78-114
MATRIX SPIKE SAMPLE:
245323
9238494001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits
Oil and Grease
mg/L
ND 40
31.2
78
78-114
Date: 03106/2009 02:26 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
��r1•
Qualifiers
Page 7 of 9

ceAnalytical
www,paeela8scorrt.
Project: Dixon Quick Coupling
Pace Project No.: 9238936
QC Batch: MPRP/3911
QC Batch Method: EPA 200.7
Associated Lab Samples: 9238936001
METHOD BLANK: 244011
Associated Lab Samples: 9238936001
Parameter Units
ug/L
Lead
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 200.7
Analysis Description: 200.7 MET
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 5.0 03/03/09 20:24
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 •
[phone]
LABORATORY CONTROL SAMPLE: 244012
Spike LCS LCS % Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Lead ug/L 500 459 92 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 244013
244014
MS
MSD
9238743001
Spike
Spike
MS MSD MS MSD % Rec
Parameter Units Result
Conc.
Conc.
Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND
500
500
444 432 89 86 70-130 3
SAMPLE DUPLICATE: 244015
Parameter
Lead
Date: 03/06/2009 02:26 PM
9238743002 Dup
Units Result Result RPD Qualifiers
ug1L ND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 9

IrAeAnalytcal
WWW..Aaaelab&C=
QUALIFIERS
Project: Dixon Quick Coupling
Pace Project No.: 9238936
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Knoey Ave. Suite 100
Huntersviile, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis initiated more than 15 minutes after sample collection.
[phone]
Date: 03/06/2009 02:26 PM REPORT OF LABORATORY ANALYSIS Page 9 of 9
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
is

t -♦
. aceAnalyticala
arrwssdlaas.tam
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Pago: of
Required Client information: Required Project Information: Involes Information:
Compan Report To: �+ Attention:
O 619
i , '_ f
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Address:
Copy Ta: ,
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Company Name:
W „ eV C
....� ... _ ... .... _ .. _ .. -
REGiUIiATQRY;AfiENCY" •`
Address:
F NPDES r GROUNDWATER I- DRINKING WATER
r UST i— RCRA (" OTHER
Email To:
Purchase Order No.:
Paw Quote
Rehrenw:
G: Fax:
Project Name
Pa°° Praia
'81tR LOCatlpn
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Requeabd Due DatwrTAT:
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Requested
Alialysis'Filtered.(YlNJ'
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Section D Matrix Codes
z'
R"WredClient Information M&Mxl 1 CODE
COLLECTED
Pteseri/ (ws
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Water water ow
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Water wr
Waste Water ww
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C BI��09rTE
cotr�osl�tE
Soillsolid SL
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SAMPLE ID Wipe �
<
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(AM 0.TBE Air AR
Sample IDs MUST 13E UNIQUE Tissue TS
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BATE
TIME
DATE
TIME
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RELINQUISNFDBYlAFFILIATION
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TIME
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DATE
TIME'
SAMPLQCONbRIONB
Pi Va►7.�i Y ysOn Qr.a..,.
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SAMPLER NAME AND SIGNATURE 0.Zew
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PRINT Name of SAMPLER.
ORIGINAL
8
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SIGNATURE of SAMPLER: n BATE Signed
l-� (MMIWD
'Important Note: By signing this form you are accapdng Pace's NET 30 day payment terms and egrgsing to into charges of 1.5% per month (or any Invol not geld within 30 days. IF F-ALL-Q-020rov.07, 15-May-2007

w_ _ r triple nditipi U oiiAdmp {
FaceAnalytical Client Nam 1 Dyum [�'y C&,dnq, Project #_
if
❑ ❑ UPS ❑ USPS Client ❑ Courier: Fed Ex mmercial El Pace Cithar
CustodySeal on Cooler/Box Present: Prot Di]e':Qate;rNlA T
❑ yes no Seals intact: � yes ❑ no r:
I?rgtTlame^ /A,
Packing Material: ❑ Bumble Wrap Bubble Bags ❑ None ❑Other
Thermometer used T060 Type of lce�o Blue None Samples on ice. cooling process has begun
TemperatureQ
Biological Tissue is Frozen: Yes No NIA
9
Initials f er n examCooler
=Ie'and
ts:
Temp should be above freezing to 6'C
Comments:
Chain of Custody Present:
Yes
ONO
❑NIA
1.
Chain of Custody Filled Out:
Ye
ONO
❑N/A
2.
Chain of Custody Relinquished:
Ye
ONO
❑NIA'
3.
Sampler Name & Signature on COC:
Ye
ONO
(]NIA
4.
Samples Arrived within Hold Time:
Yes
ONO
❑NIA
5.
Short Hold Time Analysis (<72hr):
❑Ye
No
❑NIA
6.
Rush Turn Around Time Requested:
Yes
ONO
❑NIA
7.
Sufficient Volume:
a
ONO
❑NIA
8.
Correct Containers Used:
Yes�es
ONO
❑NIA
g.
-Pace Containers Used:
Idly;
❑No-
❑NIA
Containers Intact:
Yes
ONO
❑wA
10. .
Filtered volume received for Dissolved tests
❑Ye
ONO
NIA
11.
Sample Labels match CDC:
WrYes
ONO
❑NIA
12.
-includes date/time/ID/Analysis Matrix:
W r4
All containers needing preservation have been checked. .
es ❑No
©NIA
13.
All containers needing preservation are found to be in
Yes
❑No
❑NlA
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-ORO (water)
❑Yes
❑No
Initial when completed
Samples checked for dechlorination:
❑Yes
ONO
Nl
14,
Headspace in VOA Vials ( >6mm):
Dyes
ONO
vlw
15.
Trip Blank Present:
❑Yes.
❑No-,
NIA
. 6.
Trip Blank Custody Seals Present
EIYes'ONO
IA
Pace Trip Blank Lot #f (if purchased): NIA
Client Notification! Resolution: Field Data Required? Y / N I NIA
Person Contacted: DatelTime-
Commentsl Resolution:
Project Manager Review: Z A,1 }-F . _ . Date: _Q 2 — 21
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office (i.e out of hold, incorrect preservative, out of temp, incorrect containers)

• Pace Analytical Services, Inc. Pace Analytical Services, Inc.
IrAeAnaocN 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
[phone] (704)B75-9092
August 05, 2009
Ms. Carol Hambridge
Aware Environmental
PO Box 2669
Matthews, NC 28106
RE: Project: DIXION QUICK COUPLING N290-10
Pace Project No.: 9249616
Dear Ms. Hambridge:
Enclosed are the analytical results for sample(s) received by the laboratory on July 29, 2009. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions conceming this report, please feel free to contact me.
Sincerely,
Kevin Herring for
Bonnie McKee
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�f`�1a
Page 1 of 9

e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 IGncey Ave. Suite 100
wwiicpea�tabsoam
Asheville, NC 28804 Huntersville, NC 2807E
[phone] [phone]
Project: DIXION QUICK COUPLING N2W10
Pace Project No.: 9249616
Charlotte Certification IDs
Connecticut Certification #: PH-0104
Flodda/NELAP Certification #: E87627
West Virginia Certification #: 357
Virginia Certification #: 00213
Tennessee Certification #: 04010
South Carolina Drinking Water Cert. #. 990060003
South Carolina Certification M. 990060001
Asheville Certification lDs
Connecticut Certification #: PH-0106
Virginia Certification #: 00072
Tennessee Certification #: 2980
South Carolina Certification #: 99030001
South Carolina Bioassay Certification M 99030002
Pennsylvania Certification #: 68-03578
West Virginia Certification #: 356
CERTIFICATIONS
Pennsylvania Certification #: 68-00764
North Carolina Wastewater Certification #: 12
North Carolina Field Services Certification #: 5342
North Carolina Drinking Water Certification #: 37706
.New Jersey Certification #: NC012
Louisiana/LELAP Certification #: 04034
Kentucky UST Certification #: 84
North Carolina Drinking Water Certification * 37712
North Carolina Bioassay Certification M 9
New Jersey Certification #: NC011
Massachusetts Certification #: M-NC030
Louisiana/LELAP Certification #: 03095
Florida/NELAP Certification #: E67648
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services; Inc..
Page 2 of 9

0
ww�paoe(atiscam
Project: DIXION QUICK COUPLING 14290-10
Pace Project No.: 9249616
Lab ID Sample ID
9249616001 SAMPLE LOCATION NO.2
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
(B28)254-7176
SAMPLE ANALYTE COUNT
Method Analysts
EPA 1664A
EAJ
EPA 200.7
SHB
EPA 9040
DMN
SM 2540D
TEE
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, _
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Reported Laboratory
1
PASI-C
1
PASI-A
1
PASI-A
1
PASI-A
Page 3 of 9

ace AnaVical `
wwwP aelab&oam
Project: DIXION QUICK COUPLING N290-10
Pace Project No.: 9249615
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 26804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SAMPLE LOCATION NO.2
Parameters
Laic ID: 9249616001 Collected: 07/28/09 16:45 Received:
Results Units Report Limit DF Prepared
07/29/09 09:20 Matrix: Water
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664A
Oil and Grease
ND mg/L
5.0
1
08/04/09 12:30
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead
101 ug/L
5.0
1 07/31/0913:20 08/0110914:44 7439-92-1
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
4.2 mg l-
4.2
1
07/31/09 14:48
9040 pH
Analytical Method: EPA 9040
pH
6.0 Std. Units
0.10
1
07/31/09 17:40 H6
Date: 08/05/2009 01:30 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 9

Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: DIXION QUICK COUPLING N290-10
Pace Project No.: 9249616
QC Batch: GCSV/5942 Analysis Method: EPA 1664A
QC Batch Method: EPA 1664A Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 9249616001
METHOD BLANK: 317468 Matrix: Water
Associated Lab Samples: 9249616001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 0810410912:22
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
317469
Spike LCS
LCS
% Rec
Parameter
Units
Cone. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 38.6
96
78-114
MATRIX SPIKE SAMPLE:
317470
9249137005 Spike
MS
MS
% Rec
Parameter
Units
Result Cone.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
38.5
93
78-114
Date: 08/05/2009 01:30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Ana"cal Services, Inc..
Page 5 of 9

aceArlalyfical
wowpacalaba car+
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(828)2547176
QUALITY CONTROL DATA
Project: DIXION QUICK COUPLING N290-10
Pace Project No.: 9249616
QC Batch: MPRP/4844 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9249616001
METHOD BLANK: 316214
Associated Lab Samples: 9249616001
Parameter Units
Lead ug/L
LABORATORY CONTROL SAMPLE. 316215
Parameter Units
Lead ug/L
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 08/01/0914:07
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
500 521 104 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 316216
316217
MS
MSD
9249713001
Spike
Spike
MS MSD MS MSD % Rec
Parameter Units Result
Cone.
Cone.
Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND
500
500
494 497 99 99 70-130 .6
SAMPLE DUPLICATE: 316218
Parameter
Lead
Date: OS/05/2009 01:30 PM
9249713002 Dup
Units Result Resuft RPD Qualifiers
ug1L ND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ina.
5`q y ♦CCO Of
�n
Page 6 of 9

I"A
oAtWcal
*wwPMXbb&0=
Project: DIXION QUICK COUPLING N29D-10
Pace Project No.: 9249616
QC Batch: WET/9224
QC Batch Method: SM 2540D
Associated Lab Samples: 9249616001
METHOD BLANK: 316320
Associated Lab Samples: 9249616001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE:
316321-
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 316322
Parameter
Units
Total Suspended Solids
mg/L
Date: 08/05/2009 01:30 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Pace Analytical Services, Inc.
9800 IGncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrb(: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 07/31/0914:46
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 270 108 80-120
9249858001 Dup
Resuft Result
ND ND
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 9

1ace/iqa1 s
W&WFaGWabtaont
Project: DIXION QUICK COUPLING N290-10
Pace Project No.: 9249616
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETl9228 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 9249616001
SAMPLE DUPLICATE: 316327
9249500001 Dup
Parameter Units Result Result RPD Qualifiers
pH Std. Units 7.1 7.1 0 H6
Date: 08/05/2009 01.30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
y [COy
�r s
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078 ,
[phone]
Page 8 of 9

wr'wAeoefaLsoan
QUALIFIERS
Project: DIXION QUICK COUPLING N290-10
Pace Project No_: 9249516
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 KnceyAve. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable_
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
HS Analysis initiated more than 15 minutes after sample collection.
Date. 08/05/2009 01:30 PM REPORT OF LABORATORY ANALYSIS Page 9 of 9
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

:f ,DaceArralyi a is 1'
wws.aacatsha.esm
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C Page. of
Required Client Information: Required Project Informatlon: Invoice Informatfon: ^ ^ ^
Campan Rew" Tw - Attention: b L b
, eR is r
Address; Q Copy To: Compan me:
REGULATORY.AGENCY
y v.Ile
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Address.
r- NODES 1' GROUND WATER r DRINKING WATER
F^ UST j'" RCRA (' OTHER
Email To:
Purchase Order No.:
Pace quote
RNennce:
P ne:
fax:
Project N
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Ped Pro.Igo
anagr:
Site Location
STATE: _yG
Regwatsd ue AT:
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,Ty.Req��ttited
Atieljfsls
Filleted
(YM}
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Section D Matrix Codes
RequlmdClientlnfamatlon pE
$
COLLECTED
Preservatives
'st
Drinking water DW
o
Water wT
Waste Water WW
r5
CotrrosTE
COMPOenE
END00M
_
Product P
aTAAT
Soil/Sodd SL
oilOL
L
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SAMPLE ID wP
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Semple IDs MUST BE UNIQUE Tissue TS
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X
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DATE
TIME
DATE
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Pace Project No,J Lab I.D.
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ADDITIONAL COMMENTS
RELINQUISHED BY 1 AFFILIATION
•' DATE
ME' +
w ACCEPTEp
SY! AFf141AT1ON
DATE
TIME
SAMPLE CONDITIONS
Tarr
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Cove usr�
ORIGINAL
SAMPLER NAME AND SIGNATURE
PRINT Name of SAMPLER: Q to +. rfCr
E
+
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SIGNATURE of SAMPLER: DATE Signed
(MM/Do
y
9mporlant Note: 6y slgninp this form you are accepting PwA's NET 30 day payment terms and awaeinq to late Chases nr 1.5-6 ee th tnr env lnvnira not neln wnhin M7 rave F-ALL-0-020rev.07. f 5-May-2007

IN ill M,
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• aceAralytical
Client Name• an Project # 1 5(!0$
Courier: ❑ Fed Ex ❑ UPS ❑ USPS Client eno
mmerciat ❑ Pace Other
CustodySeal an Cooler/Box Present: es Seats intact: Pro 4Q►te3Date 1`skff[�❑ Y❑ Yes �o =� 4-
Packing Material: ❑ Bubble Wrap ❑Bubble Sags None 00ther
Thermometer Used T060 Type of Ice:A07),
et Blue None Samples on ice. caofrnR process has begun
Cooler Temperature ,
Temp should be above freezing to 6'C
V
Biological -Tissue is Frozen: Yes No NIA
Comments -
Date and initia o erso i ing
contents:
Chain of Custody Present:
dy7
❑No
❑NIA
11.
Chain- of Custody Filled Out:
dyv
❑No
❑NIA
2.
Chain'of Custody Relinquished:
As,
0No
©NIA
3,
Sampler Name & Signature on COC:
Ye
❑No
❑NIA
4.
Samples Arrived within Hold Time:
Yes
ONO
❑NIA
5.
Short Hold Time Analysis (<72hr):
OYej,
No
❑NIA
$,
Rush Turn Around Time Requested:
Yes
❑No
❑NIA
7_
Sufficient Volume:
zlyoe
ONO
❑NIA
8.
Correct Containers used:-.
-Pace Containers Used:
Ye
IQye
❑No
❑No.
❑NIA
❑NIA
g•
Containers Intact:
0111
ZYes
❑No
❑NIA
10, .
Filtered volume received for Dissolved tests
❑Yes
ON.
NIA
11,
Sample Labels match COC:
-Includes date/timeAD/Analysis Matrix:
❑Yes
No
❑NIA
12_ �pfeit/e 0. /�wrr� S rA 8� S
All containers needing preservation have been checked..
All containers needing preservation are found to be in
compliance with EPA recommeridation.
exceptions: VOA, coliform, TOC, O&G, VA-DRO (water)
Yes
/Ye.
Oyes.
❑No
❑No
ONO
❑NIA
❑NIA
13. � Des �
Initial when completed
W L'., `, wan n`tGc
iJ`*`� (� `fi'
CcAfin Q
Samples checked for dechlorination:
Oyes
ONO
NIA
14.
Headspace in VOA Vials ( >6mm):
❑Yes
ONO
Owl
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (it purchased): NIA
❑Yes
❑Yes
❑No •
ONO
dN
NIA
16.
Client Notification/ Resolution: Field Data Required? Y / N / NIA
Person Contacted. Date/Time:
Comments/ Resolution:
Project Manager Review: &Y • , Date: GY (P Q
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office (i.e out of hold, incorrect preservative, out of ternp, incorrect containers)

#8572: Metals
Page 1 of 2
BEST
PRACTICAL TM
X Results
e Ticket 8572 created in queue 'Rush Requests'
X Ticket metadata
X The Basics
Id: 8572
Status: new
Left: 0 min
Priority: 99/99
Queue, Rush Requests
X Custom Fields
Tests:
a
Lead
Number of Samples:
a
1
Sample Matrix:
a
Water
Client:
a
Dixon Quick
Coupling
Project Name/Reference:
'
Dixon Quick
Coupling
Rush Surcharge Multiplier:
o
(no value)
Requested TAT:
a
2 day
Date Required By:
o
09/26/09
Total Revenue of Rush
'
(no value)
Project:
Expected Date of Arrival:
a
09/24/09
Comments:
a
(no value)
SVOA Approval:
a
(no value)
SVOA Rejection Reason:
a
(no value)
SVOA Renegotiated TAT:
a
(no value)
VOA Approval:
a
(no value)
VOA Rejection Reason:
a
(no value)
VOA Renegotiated TAT:
a
(no value)
Metals Approval:
.
(no value)
Metals Rejection Reason:
a
(no value)
Metals Renegotiated TAT:
a
(no value)
Wet Chem Approval:
o
(no value)
Wet Chem Rejection
o
(no value)
Reason:
Wet Chem Renegotiated
o
(no value)
TAT:
Final Outcome:
a
(no value)
Lost Reason:
a
(no value)
Proj #:
a
(no value)
Did Lab meet agreed TAT?:
o
(no value)
Comments for missed TAT
o
(no value)
date:
X People
Owner: bhelton
<[e-mail]>
Preferences I L.ogout
Logged in as bheiton
X Dates
Created: Mon Aug 24 13:47:34 2009
Starts: Not set
Started: Not set
Con ct Not set
Due: Tue Aug 2S 17:45:58 2009
Closed: Not set
Updated: Mon Aug 24 13:47:36 2009 by
bheiton
X Links
Depends on:
Depended on by:
Parents:
Children:
Refers to:
Referred to by:
http://92]abtrack/7icket/Create.html
8/24/2009

ImARalyieaf
WWWWcel ftmn
August 31, 2009
Terry Carter
Dixon Quick Coupling
332 Atando Ave
Charlotte, NC 28206
RE: Project: DIXON QUICK COUPLING
Pace Project No.: 9251568
Dear Terry Carter.
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PaceAna"cal Services, Inc.
9800 IGncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on August 24, 2009. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brandon Helton
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Lp�Q
Page 1 of 8

IeAnalyfjcal a
�r+r:pa6e(aGsoom.
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviiie, NC 28078
Project: DIXON QUICK COUPLING
Pace Project No.: 9251568
Asheville Certification iDs
Connecticut Certification #: PH-0106
Florida/NELAP Certification #: E87648
Louisiana/LELAP Certification #: 03095
Massachusetts Certification #•. M-NC030
New Jersey Certification #: NC011
North Carolina Bioassay Certification #: 9
West Virginia Certification #: 356
[phone]
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
Pennsylvania Certification #: 68-03578
South Carolina Bioassay Certification #: 99030002
South Carolina Certification M. 99030001
Tennessee Certification #: 2980
Virginia Certification #: 00072
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
!L a
[phone]
Page 2 of 8

ceAnaly ical e
ww*paeef min
Project: DIXON QUICK COUPLING
Pace Project No.: 9251568
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
9251568001 TRUCK SAMPLE EPA 200.7 SHB 1 PASI-A
9261568002 OUTFALL EPA 200.7 SHB 1 PASI A
REPORT OF LABORATORY ANALYSES
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 8

�Ice
Analyiical
W*W.Pac@absxaxen
Project: DIXON QUICK COUPLING
Pace Project No.: 9251568
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Anatytical Services, Inc.
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Sample. TRUCK SAMPLE Lab ID: 9251568001 Coffected: 08/24/09 10:30 Received: 08/24/09 11:35 Matra: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead ND ug1L 5.0 1 08/25/09 11:50 08/26/09 00:23 7439-92-1
Sample: OUTFALL Lab ID: 9261668002 Collected: 08/24/09 10:30 Received: 08/24/09 11:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 2007
Lead 41.0 ug/L 5.0 1 08/28/09 10:50 08/29/09 06:24 7439-92-1
Date: 08/31/2009 05:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 8

IeAnalytical�
pae &Ws.c=
Project: DIXON QUICK COUPLING
Pace Project No.: 9251568
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MPRP/4982 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description. 200.7 MET
Associated Lab Samples: 9251568002
METHOD BLANK 328856 Matrix: Water
Associated Lab Samples: 9251568002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Lead ug/L ND 5.0 08/29/09 06:06
LABORATORY CONTROL SAMPLE: 328857
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Lead ug/L 500 467 93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 328858 328859
MS MSD
9251568002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua]
Lead ug/L 41.0 500 500 479 480 88 88 70-130 0
SAMPLE DUPLICATE: 328860
Parameter
Lead
Date: 08/31/2009 05:17 PM
9251860001 Dup
Units Result Result
ug/L ND ND
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 8

f�ce,4nalytical.
Project: DIXON QUICK COUPLING
Pace Project No.: 9251568
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 28804
[phone]
QUALITY CONTROL DATA
f
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MPRP/4960 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9251568001
METHOD BLANK 326710 Matrix: Water
Associated Lab Samples: 9251568001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Lead ug/L ND 5.0 08/26/09 00:14
LABORATORY CONTROL SAMPLE: 326711
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Lead ug/L 500 487 97 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 326712 326713
MS MSD
9251568001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 500 476 468 95 94 70-130 2
SAMPLE DUPLICATE: 326714
Parameter
Lead
Date: 08/31/2009 05:17 PM
9251574001 Dup
Units Result Result
ug/L 145 141
RPD Qualifiers
3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytcai Services, Inc..
o ,
Page 6 of 8

aceAnaVieal.
rrWPVc0bDxcorrl
QUALIFIERS
Project: DIXON QUICK COUPLING
Pace Project No.: 9251558
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
980D KinceyAve. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed anatyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited anatytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
[phone]
Date: 08/31/2009 05:17 PM REPORT OF LABORATORY ANALYSIS Page 7 of 8
This report shall not be reproduced, except in hull,
without the written consent of Pace Analytical Services, Inc..

/�k'WkWcal*
f wwrcpecerabs.00nr
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DIXON QUICK COUPLING
Pace Project No.: 9251568
Pace Analytical Services, Inc.
98001GnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
9251568001 TRUCK SAMPLE EPA 200.7 MPRP/4960 EPA 200.7 ICP/4604
9251568002 OUTFALL EPA 2001 MPRP/4982 EPA 200.7 ICP/4620
Date: 08/31/2009 05.17 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 8

,)!;'
e.l.he enee
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain-O-Custody is a LEGA- L DOCUMENT. Ail relevant fields must be completed accurately.
Section A Section 8 Section C
Page: of
Required Client Information: Required Project Information: Involte Information:
Comw u C . Report To: err ! f Attention:
Vresji
1326908
Add
ii � � Au
Copy To:
Campany Name:,
R6l31JIATORY. AGENCY
1041 s I. -AG $ l0
Address:
r NPDES r GROUNDWATER r DRINKING WATER
j UST r RCRA r OTHER
it To:
Purchase Order No.:
Pans Quote
P na: fax:
O
Project e:
1 bV% 091r,ic Cb u ' fn
Pete "ad
Ma-
8RD Location
; SrATE.
RequestedProJadNumber:
PaeProfile#:
Requested
Analysls
Flltered
(Y/N)
Section D Matrix Codes
o'
z;
Requ1ndClfenelnfarma8on �JATnuc r CODE:
COLLECTED
Preservatives
P;
Drinking Water DW
Water WT
zi
0
Waste Water WW
Product P
COMPOSITE
START
COMPOSITE
ENMRAD
Soil/Solid SL.
Oilwipe
iiiW333
SAMPLE ID WP
SA Z, 0 9! r) Air AR
a
y
a
2�3��'�
Sample IDs MUST BE UNIQUE Tissue TS
O
a
Other OT10
Q
8
r1
0C
9
O
O
p�
�
x
Z1
DATE
TIME
DATE
TIME
1 1
1
1
Paco Project NoJ Las I.D.
1
1&xmo Ia. I
too. as
<g„
i
2
is ;k,
Q
V,as
9
5'<
�F,
rid
7
.1 {
9
yc
10A
11
F
12
ADDITIONAL COMMENTS
REUNOUISMEDSYIAFFILIATION'
DATE
TIME -
ACCE ll!YIAFMLIATION•
DATE
TIME
SAMPLE CONDITIONS
5
is,
ORIGINAL
SAMPLER NAME AND SIGNATURE
a
E
�I
PRINT Name of SAMPLER: *-,-r ( r
SIGNATURE of SAMPLER:
DATE Signed
IT
`—
MWDD :
'ImWnani Note: By signina this form you am aeeeoiina Pace's NET 30 day oavmant efara end arv-nine In WA rmnn— nt I FY — —th ft..nv Inv rw —W -thin Ym n.— F_Ai 14n-n7nnmv 07 T R-Mav-9nn7

% aceAr�alytica!- n
Client Name: y--- Project # ` :;� 6 �LP(P
Courier: ❑ fled Ex ❑ UPS ❑ USPS jent ❑ Commercial ❑ Pace Other OptionI==3A
CustodySeal on Cooler/Box Present: es no Seals intact: Prof Dte Dafe NIA `-
❑Y ❑yes
Prod Nart7e _ Ntf
.._ ,f�_
Packing Material: ❑ Bubble Wrap []Bubble Bags �e ❑Other
Thermometer Used T060 Type of lce: et _)�lue None Samples on ice, cooling process has begun
Cooler Temperature.
Temp should be above freezing to 6'C
#-�'
Biological E Is Frozen: Yes No NIA
Comments:
gate and ]nit is of person examining
contents: �s
Chain of Custody Present:
--f1Yes
ONo
❑NIA
1.
12.
Chain of Custody Filled Out:
_,L;i'res
ONo
❑NIA
Chain of Custody Relinquished:
es
ONO
❑NIA
3.
Sampler Name & Signature on COC:
J.93res
ONO
❑NIA
4.
Samples Arrived within Hold Time:
ONo
❑NIA
5.
Short Hold Time Analysis (<72hr):
❑Yes PW'
ONIA
6.
Rush Turn Around Time Requested:
s
ONo
❑NIA
7.
Sufficient Volume:
es
ONO
❑NIA
$.
Correct Containers Used:
-Pace Containers Used:
s
es
ONO
ONo.
❑NIA
❑NIA
9.
Containers Intact:
_
ONO
❑NIA
10. .
Filtered volume received for Dissolved tests
❑Yes
ONO.
11.
Sample Labels matchCOC:
-Includes date/time/ID/Analysis Matrix:
Oyes P<_❑NIA
12. ,� ( a(}s, . r�' T��1^S�rNr,cc
a kw.
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with ERA recommersdation.
exceptions: VOA, mlitorm, TOC, O&G. VA-DRO (water)
,,QY-es
❑Yes
ONO
ONO
ONO
❑NIA
❑NIA
13.
Initial when.completed
Samples checked for dechlorination:,
❑Yes
ONO
14.
Headspace in VOA Vials (>6mm):
❑Yes
ONO �A
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (if purchased): NIA
❑Yes
❑Yes
❑No -tfN/A
ONO
A
16.
Client Notification/ Resolution: Field Data Required? Y I N J NIA
Person Contacted: Datefrime:
Comments/ Resolution:
Project Manager Review: C(�(,t� Date: 2 (�
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office (i.e out of hold, incorrect preservative, out of temp, incorrect containers)

ceAnalytical'
r wwvpacefabxcam.
1
September 25, 2009
Terry Carter
Dixon Quick Coupling
332 Atando Ave
Charlotte, NC 28206
RE: Project: DIXON QUICK COUPLING 9/23
Pace Project No.: 9253667
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 ICincey Ave. Suite 100
Huntersville. NC 28078
Dear Terry Carter:
Enclosed are the analytical results for sample(s) received by the laboratory on September 23, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brandon Helton
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the mitten consent of Pace Analytical Services, Inc..
goo
`i'.'_
[phone]
Page 9 of 7

V[iI'7!!R�%Ql
wwwpeoefafraoom
Project_ DIXON QUICK COUPLING 9/23
Pace Project No.: 9253667
Asheville Certification IDs
West Virginia Certification #: 356
Virginia Certification*: 00072
Tennessee Certification #: 2980
South Carolina Certification * 99030001
South Carolina Bioassay Certification #: 99030002
Pennsylvania Certification #: 68-03578
Connecticut Certification #: PH-0106
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
North Carolina Drinking Water Certification #: 37712
North Carolina Bioassay Certification #: 9
New .Jersey Certification #: NC011
Massachusetts Certification M. M-NC030
Louisiana/LELAP Certification #: 03095
Florida/NELAP Certification #: E87648
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall nol be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
w
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 7

��aceAna'
Project: DIXON QUICK COUPLING 9/23
Pace Project No.: 9253667
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
I
Pace Analytical Services, Inc.
9800 Kinoey Ave. Suite 100
Hurrtersville, NC 28078 ,
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
9253667001 SAMPLE 1 WATER TRUCK EPA 200.7 SHB 1 PASI-A
9253667002 SAMPLE 2 LOCATION #2 EPA200.7 SHB 1 PASI A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
V4 •`�.,�1i
Page 3 of 7

1J
S
"OeAnalyfical*
www.p�apei�h�aoar
Project: DIXON QUICK COUPLING 9/23
Pace Project No.: 9253667
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
98001C1nceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SAMPLE 1 WATER TRUCK Lab ID: 9253667001 Collected: 09/23/09 10:35 Received: 09/23/09 11:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead ND ug/L 5.0 1 09/24/09 12,00 09/24/09 20:49 7439-92-1
Sample: SAMPLE 2 LOCATION #2 Lab ID: 9253667002 Collected: 09/23/09 10:35 Received: 09/23/09 11:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead 145 ug/L 5.0 1 09/24/09 12:00 09/24/09 21:02 7439-92-1
Date: 09/25/2009 04:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
O « tp n
a
�\-J z
Page 4 of 7

1���IceAnaVicale
J tiw wPscat"conl
Project: DIXON QUICK COUPLING 9/23
Pace Project No.: 9253667
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/5114 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9253667001, 9253667002
METHOD BLANK: 340854 Matra: Water
Associated Lab Samples: 9253667001, 9253667002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Lead ug/L ND 5.0 09/24/09 20:31
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 340855
Spike
LCS
LCS
% Rec
Parameter Units
Cone.
Result
% Rec
Limits Qualifiers
Lead ug/L
500
504
101
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 340856
340857
MS
MSD
9253667001
Spike
Spike MS
MSD
MS MSD % Rec
Parameter Units Result
Conc.
Conc. Result
Result
% Rec % Rec Limits RPD Qual
Lead ug/L ND
500
500 469
475
94 95 70-130 '1
SAMPLE DUPLICATE: 340858
Parameter
Lead
Date: 09/25/2009 04:05 PM
Units
ug/L
9253667002 Dup
Result Result
145 144
RPD Qualifiers
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
0 Cps
Page 5 of 7

,�Ir,l W*WPaCebb&=n
QUALIFIERS
Project: DVON QUICK COUPLING 9/23
Pace Project No.: 9253667
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviffe, NC 28D78 •
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot; or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrac Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
Date: 09/25R0D9 04:05 PM REPORT OF LABORATORY ANALYSIS Page 6 of 7
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
«o.

Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 288D4
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DIXON QUICK COUPLING 9123
Pace Project No.: 9253667
PaceAna"cal Services, Inc.
98DO Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
9253667001 SAMPLE 1 WATER TRUCK EPA 200.7 MPRP/5114 EPA 200.7 ICP14746
9253667002 SAMPLE 2 LOCATION #2 EPA 200.7 MPRP/5114 EPA 200.7 ICP14746
Date: 09/25/2009 04:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.reo at`
Page 7 of 7

. aceAnal1�ical'
y`
..w. n■eN■h. rtnm
CHAIN -OF -CUSTODY I Analytical Request Document
The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B section C
Page: of
Required Client Information: Required Project Information, Invoice Informatlon:
Compare RapoA To: Attention:
^ ^ ^ O
s b y
/� _
{
t< t Lam+ C
Address 3
Copy To:
Company Name:
REGULATOR_ Y AGENCY
bra'
r NPDSS r GROUND WATER r- DRINKING WATER
r UST j— RCRA r OTHER
Email T
Purchase Cyder No.:
Para Quote
eI
Reference:
Phone:
Felt: •[CIS►
Project Nam t
11t I
Pace Pmjeq
Slte Location
.-3 4 •
tC3�1 a+ C as I n
Manager. .
ct
Roque
Project Number.
Pen Profile M:
stelfA :
54
STATE:
;.•.,..
Regilested:AnalysisFiltared
{YINj
Ssetion D Matrix Codes
FM
RequlradCgent lalormation MATRIX r CODE
e
COLLECTED
Preservatives
S~'t
Ddrlklydg Water DW
water wT
u
O
Q
r dte water yyvlf
Product
c010111 E
srAar
co mpoallE
fNOVCtRMB
SollfSold SL
►
SAMPLE ID OL
c7
Wipe
(A-Z, 0-9I ,-) Air AR
Semple ID; MUST BE UNIQUE Tissue TS
U
uJ
a
Other O7
2
d
S
'
DATE
TIME
DATE
TIME
u
O
Pace Project No./ Lab I.D.
1
r
frF-,
2
f
of A1�1
3
5.
4
!S
:sr
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12
ADDITIONAL COMMENTS
RELINCUISHEb BY I AFFILIATION
DATE ';
TIME
ACCEPTED BY.I' AFFILIATION'
DATE
TIME
SAMPLE CONDITIONS
to l a%
IS!
P't
UN
r
Pt�
SAMPLERNAMEAND SIGNATURE
ORIGINAL
PRINT Name of SAMPLER: it r C.9%tiee
a
X
DATE Signed
SIGNATURE of SAMPLER:
m
F,
U
- MM1DD q
*Important Nate: By signing this dam you am aaoepwq Pace's NET 30 day payment terns and agreeing to late charges of 1.5% per month danv impLas real raid wAhln an n.-

AM_ And_iPQM. -eceip
-FaceAnalyfica!'
Client Name: _ t �L�- _ Project # 92 55 Sr7
Courier: ❑ Fed Ex ❑ UPS ❑ USP , Client ❑ Commercial
Custody Seal on Cooler/Box Present: ❑ yes no Seat;
Packing Material: ❑ Bubble Wrap []Bubble Bags None
Thermometer Used T060 iCrtYV1�� �,X4pe of lce:(l
I_7 Pace Other Q.Otidiiap% w
Pro Due Date N/Ar
intact: yes �o-r
rr� a[ile�/e3"s
❑
❑Othef
� �_:.
Blue n Samples on ice, cooling process has begun
Biological 1—
Cooler Temperature �" 4 i g-cat Tissue is Frozen: Yes No NIA
Temp should be above freezing to 61C Comments:
Date and lnit- f of persgrs exami
contents:
Chain of Custody Present:
s
ONO
❑NIA
1.
Chain of Custody Filled Out:
oYrs
❑No
❑NIA
2•
Chain of Custody Relinquished:
Yes
❑-No
❑NIA
3.
Sampler Name & Signature on COC:
es
ONO
❑NIA
4.
Samples Arrived within Hold Time:
es
❑flo
❑NIA
5.
Short Hold Time Analysis (<72hr):
Dyes i7o
❑NIA
6•
Rush Turn Around Time Requested:
es
❑tJo :ONIA
7_
Sufficient Volume:
Yes
Oft
❑NIA
8.
Correct -Containers Used:
-Pace Containers Used:
Yes
es
❑lira
❑N.-
ON/A
❑NfA
9. -
Containers Intact:
es
ONO
'❑NIA
10. .
Filtered volume received for Dissolved tests
❑Yes
ONO
11.
Sample Labels match COC:
-includes date/lime/ID/Analysis Matrix:
Dyes o __[]N/A
12, .�� S S � rJ S�mnk
r� 1_ C�.t �° I t� L1 95 7
All containers needing preservation have been checked.
All containers needing preservation are found to be in
with EPA recommendation.
exceptions: VOA, coGrorm. TOC. O&G. WI-DRO (water)
es ❑No
es No
Dyes ONO
't 1� 1N1A
❑N1A
�'"' Z 1 J t 1[ O
13y.- L ya {. _ S I r C'r/?-
�u 1�-�-.�}[ 1 t>O�compliance
111^
Initial when comp* h� YJ� ; I L r n , 1A
i
Samples checked for dechlorination.-
❑Yes
ONO
NIA
14.
Headspace in VOA Vials (>6mm):
❑Yes
ONO
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (if purchased): NIA
Dyes
❑Yes
ONO .
ONO
��A
t�N/A
IA
16.
Client Notification/ Resolution: Field Data Required? Y / N / N/A
Person Contacted:
Comments/ Resolution:
Date/Time:
Project Manager Review:. Date: /d ­2Z —Q
15
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers)

N
ceAnaVical
WWW48iale MWM
October 26, 2009
Mr. Terry Carter
Dixon Quick Coupling
332 Atando Ave
Charlotte, NC 28206
RE: Project: Dixon Quick Coupling 10/22
Pace Project No.: 9255879
Dear Mr. Carter:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 22, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brandon Helton
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This reporl shall not be reproduced, except in hip,
without the written consent of Pace Analytical Services, Inc..
p �� ♦GCp�\y
�n
Page 1 of 7

aceAnalyticai"
WWWPW&Wm0om
Project: Dixon Quick Coupling 10122
Pace Project No.: 9255879
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Asheville Certification Ids
West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712
Virginia Certification M 00072
North Carolina Bioassay Certification M 9
Tennessee Certification #: 2980
New Jersey Certification #: NC011
South Carolina Certification * 99030001
Massachusetts Certification #. M-NCO30
South Carolina Bioassay Certification M 99030002
Louisiana/LEIAP Certification #: 03095
Pennsylvania Certification #: 68-03578
Florida/NELAP Certification #: E87648
Connecticut Certification #: PH-0106
North Carolina Wastewater Certification M 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Tull,
without the written consent of Pace Analytical Services, Inc..
. ,'.♦.C. n
yo.
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 7

IeAnalyticaf
ww*tpatl0ab&0=
Project: Dixon Quick Coupling 10122
Pace Project No.: 9255879
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 ICincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
9255879001 SAMPLE 1 WATER TRUCK EPA 200.7 JMW 1 PAS! A
9255879002 SAMPLE 2 LOCATION 2 EPA200.7 JMW 1 PASIA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, exoept in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 7

eAtWcaI
wwrcpaoawmew
Project: Dixon Quids Coupling 10/22
Pace Project No.: 9255879
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 1 OD
Huntersville, NC 28078
[phone]
Sample: SAMPLE 1 WATER TRUCK Lab ID: 92SN79001 Collected: 10/22/09 14.35 Received: 10/22/09 15:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 NET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead ND ug/i_ 5.0 1 10/23/09 14:50 10/26/09 14:25 7439-92-1
Sample: SAMPLE 2 LOCATION 2 Lab ID: 9256879002 Collected: 10/22/09 14:30 Received: 1012210915:24 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead 56.1 ug1L 5.0 1 10/2310914:50 10126/0914:29 7439-92-1
Date: 10/26/2009 03:33 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
LM •CCp�
Page 4 of 7

IcleAnalydcal
W&Wpaml0moem
Project: Dixon Quick Coupling 10/22
Pace Project No-: 9255879
QC Batch: MPRP/5262
QC Batch Method: EPA 200.7
Associated Lab Samples: 9255879001, 9255879002
METHOD BLANK: 355394
Associated Lab Samples: 9255879001, 9255879002
Parameter Units
Lead ug/L
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 200.7
Analysis Description: 200.7 MET
Matrix: Water
Blank Reporting
Result Limit Analyzed
ND 5.0 10126/0913:47
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 355395
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Lead ug/L 500 498 100 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 355396 355397
MS MSD
9255481012 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc- Conc. Result Result % Rec % Rec Limits RPD Qual
Lead ug/L ND 500 506 487 493 97 98 70-130 1
SAMPLE DUPLICATE: 355398
Parameter
Lead
Date: 10/26/2009 03:33 PM
9255481013 Dup
Units Result Result
ug/L ND ND
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 7

�aveAnWical"
WWWP803WM ow
QUALIFIERS
Project: Damn Quids Coupling 10r22
Pace Project No.: 9255879
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
[phone]
Date: 10/26r2009 03:33 PM REPORT OF LABORATORY ANALYSIS Page 6 of 7
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

s
Pace Analytical Services, Inc.
n
r nayi
2225 Riverside Dr.
,m' om1
Asheville, NC 28804
f
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Dixon Quick Coupling 10/22
Pace Project No.: 9255879
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
9255879001 SAMPLE 1 WATER TRUCK EPA 200.7 MPRPI5262 EPA 200.7 ICP14883
9255879002 SAMPLE 2 LOCATION 2 EPA 200.7 MPRPI5262 EPA 200.7 ICP/4883
Date: 10/26/2009 03:33 PM .
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.moo
CLI
Page 7 of 7

' PaceAnall��+}ical e
m.wn-IeE�.eem
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Choin-0f-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A . Section 8 Section C
Pape: of
Required Client Information: Required Project Information: Invoice Informatlorr.
Compan • RaW To: Attention:
1358595
d
Address;Copy
To:
Company Name
REf3ULATORYACiENCY
re
Address:
F— NPDES r GROUNDWATER r DRINKING WATER
r UST ( RCRA r OTHER
Email T
purchase Order No.:
Pace Quote
Reference:
R
Phone; uw.
"ad Nam '
Pea pmea
Site Location
`
-.RC aJ I
Manager.
SYA TE:
Requested Due T:
ProJad Number.
Psu Promo e: C! 3 '
19equeatea
ane.jysis
Fatered
(YIN)
Section D Matrix Codes
.�
2 '
Required ClientInformaaon L
8
COLLECTED
Preservatives
:;:.t
Dnnklna Water DW
Water WT
Waste Water WW
Product P
V
COMPOGITR
START
COMPpaITa
ENDKaaaS
SoillSolid SL
SAMPLE ID DII OL
WF
0-9
_
W
x
(A-Z. Aires R
Sample IDS MUST BE UNIQUE Tissue TS
p
w
IL
1 ttt...JJJIII
Other OTg
U
pp
+
FF
Q
dz,
U
m�
'W
TIME
=
D=LK
Q
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av�1
N`--
Pace Pro d.
DATE
TIME
DATE
es[►:
4
act
m ,-, a
dr
&
Ie
r
2.
3
4.
p
i
8
T
ie,•
9
10
12
ADDITIONAL COMMENTS
RELINOUIBHEDBYIAFFILIATION
DATE,
TIM4
ACCEPTEDBYIAFFILIATION'.
DATE'
TIME
SAMPLE CONDITIONS
e« try
c
�•
?"�''
,.-�
Cis upL
SAMPLER NAME AND SIGNATURE
ORIGINAL
PRINT Name of SAMPLER: fir„CL
2
S
SIGNATURE of SAMATE S
P DMMMDlpned
m
y
'Important Note: By e4nlnq this form you we eccapfin Paws NET 30 day eavmenr rwrmn AM w r—im m rw. rn.m....r � S� -... ........__ __..._'Important_ - _. - _.. .... -- .

-ndifioi:�1l�A R� 1e 0ipf
2Vace&alytical-
Client Name?- _ �-fl - _ _ Project # 4�q 5 V30
Courier: ❑Fed Ex ❑UPS ❑ USPS Client El Commercial ❑ Pace Other :O #iof-'�'.. = y`'``
I� 4� � w — _
Custody Seal on Cooler/Box Present: ❑ yes no Seals intact: ❑ yes noroJ Q DatellA'
1701sNme .vF rlfA
Packing Material: ❑ Bubble Wrap _,ell5ubble Bags ❑ None ❑Other
Thermometer Used T060 / Type of Ic We Blue None IlKsamnles on ice, coolinq process has begun
Cooler Temperature
Ile-
Biological is Frozen: Yes No NIA
Date and rtials of person examining
A
conten t
Tarnp should be above freezing to 6"C
Comments:
Chain of Custody Present:
es
ONo
❑NIA
1.
Chair] of Custody Filled Out:
Yes
❑No
IINIA
I
Chain of Custody RBfinquished:
es
ONo
ONIA
3,
Sampler Name & Signature on COC:
Yes
ONo
❑NIA
4.
Samples Arrived within Hold Time:
Yes
ONo
ONIA
5.
Short Hold Time Analysis (<72hr):
OYes0ITo—
❑NIA
6.
Rush Turn Around Time Requested:
Iff Yes
ONo
❑NIA
7.
Sufficient Volume: -
eADryes
ONO
ON/A
8.
Correct Containers lased:
2Tes
ONo
0:VA
9.
-Pace Containers Used:
Yes
ONo
❑NIA
Containers Intact:
Yes
ONo
OWA
10. .
Filtered volume received for Dissolved tests
OYes
ONo
641A
11. 9
& f A3-12ft .
Sample Labels match COC:
OYes f No
El N/A
12.
-Includes date/time/ID/Analysis Matrix:
Ail containers needing preservation have been checked.
s
ONo
ON1A
13,
All containers needing preservation are found to be in
es
ONo
❑NIA
compliance with EPA recommendation.
exceptions: VOA, coliforni, TOC, 0&G, V111-ORO (water)
Oyes
ONo
Initial when completed
Samples checked for de chlorination:
OYes
ONo NIA
14_
Headspace in VOA Vials ( >6mm):
OYes
ONo
RCA
15.
Trip Blank Present:
Oyes
ONo .
�!A
16.
Trip Blank Custody Seals Present
OYes
ONo
A
Pace Trip Blank Lot # (if purchased)! NIA
Client Notification/ Resolution: Field Data Required? Y I N I NIA
Person Contacted: Date/Time:
Comments/ Resolution:
Project Manager Review: N[E{ _ Date: / ^/D - 00
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office (i.e out of hold, incorrect preservative, out of temp, incorrect containers)

ceAnalA(,(i! r
( . WW&Pab3hb&MM
November 12, 2009
Mr. Tent' Carter
Dixon Quick Coupling
332 Atando Ave
Charlotte, NC 28206
RE: Project: DIXON QUICK COUPLING
Pace Project No.: 9257130
Dear Mr. Carter:
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
[phone]
Pace Anaytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on November 10, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brandon Helton
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical: Services, Inc..
[phone]
Page 1 of 10

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
CeArW " 2225 Riverside Dr. 9800 KEnceyAve. Suite 100
Wimpamliftcom Asheville. NC 28804 Huntersv ilie, NC 28078
[phone] [phone]
CERTIFICATIONS
Project: DIXON QUICK COUPLING
Pace Project No.: 9257130
Charlotte Certification IDS
West Virginia Certification M 357
North Carolinabrinking Water Certification #: 37706
Virginia Certification M 00213
North Carolina Field Services Certification #: 5342
Connecticut Certification #: PH-0104
North Carolina Wastewater Certification M 12
Florida/NELAP Certification #: E87627
Pennsylvania Certification M. 68-00784
Kentucky UST Certification #: 84
South Carolina Certification #: 990060001
Louisiana/LELAP Certification M 04034
South Carolina Drinking Water Cart. #: 990060003
New Jersey Certification #: NCO12
Tennessee Certification #: 04010
Asheville Certification IDS
West Virginia Certification #: 356
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
Pennsylvania Certification #: 68-03578
Louisiana/LELAP Certification #: 03095
South Carolina Bioassay Certification #: 99030002
Massachusetts Certification M M-NCO30
South Carolina Certification #: 99030001
New Jersey Certification #: NC011
Tennessee Certification #: 2980
North Carolina Bioassay Certification #: 9
Virginia Certification #: 00072
Connecticut Certification M PH-0106
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 10
cca�
w r
�'�z

/��Ce W*W'0W8AftCoM
Project: DIXON QUICK COUPLING
Pace Project No.: 9257130
Lacs ID Sample ID
9257130001 SAMPLE LOCATION 2
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
EPA1664A
EPA 200.7
EPA 9D40
SM 2540D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analysts
CLW
JMW
DMN
DMN
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Reported Laboratory
1 PASI-C
1 PASI-A
1 PASI-A
1 PASI-A
Page 3 of 10

a
Cel4lla%/fIC81
trwr�paceJa6soam
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: DIXON QUICK COUPLING
Pace Project No.: 9257130
Sample: SAMPLE LOCATION 2 Lab ID: 9267130001 Collected: 11/10/09 11:45 Received: 11/10/09 13:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664A
Oil and Grease
ND mg/L
5.0 1
11/11/09 08:52
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead
314 ug/L
5.0 1 11/1110913:20
1111110917:26 7439-92-1
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
102 mg/L
8.3 1
11/11/09 20.45
9040 pH
Analytical Method: EPA 9040
pH
7.5 Std. knits
0.10 1
11/11/09 18:35
Date: 11/122009 02:51 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
t
W
H6
Page 4 of 10

,�aceAfflocal`
wwwpxaft&wm
Project: DIXON QUICK COUPLING
Pace Project No.: 9257130
QC Batch: WET110446
QC Batch Method: EPA 9040
Associated Lab Samples: 9257130001
SAMPLE DUPLICATE: 365174
Pa rameter Units
pH
Date: 11/12/2009 02:51 PM
Std. Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NO 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description: 9040 pH
9257130001 Dup
Result Result RPD Qualifiers
7.5 7.5 0 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Anatytical Services, Inc.
9800 KinceyAve, Suite 100
Huntersville, NO 28078
[phone]
Page 5 of 10

yAW.Pacefebao=
Project: DIXON QUICK COUPLING
Pace Project No.: 9257130
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/5368 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9257130001
METHOD BLANK: 364655
Associated Lab Samples: 9257130001
Matra: Water
Blank Reporting
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units
Result
Limit
Analyzed Qualifiers
Lead ug/L
ND
5.0
11/1110916:50
LABORATORY CONTROL SAMPLE: 364656
Spike
LIDS
LCS % Rec
Parameter Units
Cone.
Result
% Rec Limits Qualifiers
Lead ug/L
500
523
105 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 364657
364658
MS
MSD
9257127001
Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result
Cone.
Cone,
Result
Result % Rec % Rec Limits RPD Qual
Lead ug/L 194
500
500
648
651 91 91 70-130 0
SAMPLE DUPLICATE: 364659
Parameter
Lead
Date: 11/12200902:51 PM
9257127002 Dup
Units Result Result
ug/L 39.3 38.2
RPD Qualifiers
3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
•9 ,N ACCOAO
Page 6 of 10

Project: DIXON QUICK COUPLING
Pace Project No.: 9257130
QC Batch: GCSV/6665
QC Batch Method: EPA 1664A
Associated Lab Samples: 9257130001
METHOD BLANK: 364674
Associated Lab Samples: 9257130001
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL SAMPLE: 364675
Parameter Units
Oil and Grease mg/L
MATRIX SPIKE SAMPLE: 364676
Parameter Units
Oil and Grease mg/L
Date: 11/12/2009 02:51 PM
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 1664A
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 11/11/0908:51
Spike LCS LCS
Cone. Result °% Rec
40 36.7 92
9257130001 Spike MS
Result Conc. Result
ND 48.8 43.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9B00 10nceyAve. Suite 100
Huntersville, NC 2BO78
[phone]
°% Rec
Limits Qualifiers
78-114
MS °% Rec
°% Rec Limits Qualifiers
83 78-114
Page 7 of 10

I"A l al lcQ!
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Project: DIXON QUICK COUPLING
Pace Project No.: 9257130
QC Batch: WET/10448
QC Batch Method: SM 2540D
Associated Lab Samples: 9257130001
METHOD BLANK: 365279
Associated Lab Samples: 9257130001
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE: 365280
Parameter Units
Total Suspended Solids mg/L
SAMPLE DUPLICATE: 365281
Parameter
Total Suspended Solids
Date: 11/12/2009 02:51 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 11/11/0920:45
Spike LCS
Conc. Result
250 260
9257130001 Dup
Units Result Result
mg/L 102 108
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
. [phone]
LCS % Rec
% Rec Limits Qualifiers
104 80-120
RPD Qualifiers
6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 10

'rAeAnWid�
QUALIFIERS
Project: DVON QUICK COUPLING
Pace Project No.: 9257130
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 `
(704)875-9D92
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrb( Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis initiated more than 15 minutes after sample collection.
Date: 1111W009 02:51 PM REPORT OF LABORATORY ANALYSIS Page 9 of 10
This report shall not be reproduced, except in full,
without the written consent of Pace Anayticai Services, Inc..
,y CCO�
4LE S� 1
Y

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E
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DIXON QUICK COUPLING
Pace Project No.: 9257130
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078 i
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
9257130001
SAMPLE LOCATION 2
EPA200.7
MPRP15368 EPA200.7 ICP/4979
9257130001
SAMPLE LOCATION 2
EPA 1664A
GCSV16665
9257130001
SAMPLE LOCATION 2
EPA 9040
WEi-110446
9257130001
SAMPLE LOCATION 2
SM 2540D
WETl113448
Date: 11/12/2009 02:51 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the mitten consent of Pace Analytical Services, Inc..
Page 10 of 10

�PaceAnal ical'
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section 6 Section C
Page: o!
Required Client Information: Required Project Information: Invoice Information:
t �} �'} p q ']
Go any: Report To: err Attontlon•
a QP
1 3 3 4 1 J
133413
XO e{ f e r r _C
Address:
Copy To:
Company Name:
REGULATORY AGENCY
i. •,
Crha_lot t
Address:
r NPDES i— GROUND WATER [" DRINKING WATER
r UST 1— RCRA r OTHER
E it To:
Purchase Order No.:
Pau Ouate
K T; n Qv t C+ +ty
Reference:
Phone:
Fax. /
Project Name:
QJ i
Pace Pm lei
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IS or, Locatlon
3 S
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Manager: , e-
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Requested Due DstslrAT:
Aspkp
Project Number.
Peas Profile s, ! '
ReOested
Analysis
Filtered
(YIN)
Section D Matrix Codes
a
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Requlred0lontlnformsiYw MATRIx !CODE
8
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COLLECTED
Preservatives
s.
Drinking Water DW
0
b
Water WT
WatBf
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COMPOSITE
START
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ENG1GRAn
W
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Product
SoIVSoGd SL
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SAMPLE 1D Oil
wP
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Wipe
(A.Z. 0-9 1; ? Air AR
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Sample IDS MUST BE UNtOUE Tissue TS
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DATE
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pace Pro ect No./ Lab I.D.
la
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3
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8
7
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11
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ADDITIONAL COMMENTS
RELINQUISHED BY t AFFILIATION
DATE
TIME
ACCEPTED BY! AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
C P r w-r JXOh 44c
��
SS
Z
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ORIGINAL
SAMPLER NAME AND SIGNATURE
U
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PRINT Name of SAMPLER:
m
F11:MM1DDlYY
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SIGNATURE of SAMPLE
DATE Signed
:
'Important Nate; By sVrdng Wo farm you are accepting Pace's NET 30 day payment terms and agreeing to Into charges of 1.5% oar mnath fnr .nv Ynvnlr...va —Id A.Wvn a�•—

! 3ceAnalytical
Client Name: " oJJ ay{ Project # g2-5'�o FS
Courier ❑ Fed Ex ❑ UPS ❑ USPS [� Client ❑ Commercial ❑ Pace Other ;Optlonaf: k'
Custody Seal on Cooler/Box Present. (❑ yes no Seals intact: ❑ yes no pkotF Date�l`J A
R�Q� lvan-te �,�NIE�,
Packing Material: ❑ Bubble Wrap Bubble Bags ❑ Nan ❑other fit,
Thermometer Used T060 Type of Ice- Wet Blue None d� 1 Samples on ice, cooling process has begun
Cooler Temperature
Temp should be above freezing to 6°C
~�
Biological Tissue is Frozen: Yes t r 1Z
Comments:
Date and I i W,,p e so examining
contents. 0
Chain of Custody Present:
Yes
❑No
❑NIA
1.
Chain of Custody Felted Out:
Yes
ONO
❑NIA
2.
Chain of Custody Relinquished:
Yes
❑No
❑NIA
3.
Sampler Name & Signature on COC_
Yes
ONO
❑NIA
4.
Samples Arrived within Hold Time:
Yes
ONO
❑NIA
5.
Short Hold Time Analysis (<72hr):
Dyes
No
❑NIA
6,
Rush Turn Around Time Requested:
Ayes
I e7f OW100
7.
Sufficient Volume: r
Yes
ONO
❑NIA
8.
Correct Containers Used:
-Pace Containers Used:
Yes
VIYeS
LINO
ONO-
0NIA
❑NIA
9.
Containers Intact:
Yes
❑No
❑NIA
10. .
Filtered volume received for Dissolved tests
Dyes
ONO
&NIA
11.
Sample Labels match COC..
-includes date/time/ID/Analysis Matrix:
❑Yes
KNo
❑NIA
12,
All containers needing preservalion have been checked. .
All containers needing pre5.ervation are found to be in
compliance with EPA recommendation.
exceptions: VOA, colirorm. TOc, O&G, WI-DRO (water)
Yes
�l es
/
0Yes
❑No
❑No
❑No
❑NIA
❑NIA
13.
Initial when completed
Samples checked for dechlorination:
❑Yes
❑No
MA
14.
Headspace in VOA Vials ( >6mm):
❑Yes
ONO
NIA
15,
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (i€ purchased): N/A
Dyes
Oyes
❑No .
❑No
�NIA
t�INIA
16.
Client Notification/ Resolution: Field Data Required? Y I N I N/A
Person Contacted:
Comments/ Resolution:
Date/Time:
Project Manager Review; Bm N Date: /Z — r7 D g
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wilt be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers)

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
,�aceAnaVical@ 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwa,pacalab .00m Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
Project: DIXON QUICK COUPLING
Pace Project No.: 9259083
Charlotte Certification IDs
9800 Kinoey Ave. - Ste 100 Huntersville, NC 28078
West Virginia Certification #: 357
Connecticut Certification #: PH-0104
Fiorida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NCO12
North Carolina Drinking Water Certification #: 37706
Asheville Certification IDs
2225 Riverside Dr. Asheville, NC 28804
Connecticut Certification #: PH-0106
Louisiana/LELAP Certification #: 03095
Massachusetts Certification #: M-NC030
New Jersey Certification #: NC01i
North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pennsylvania Certification #: 68-00784
South Carolina Certification #: 990060001
South Carolina Drinking Water Cert. #: 990060003
Tennessee Certification #: 04010
Virginia Certification #: 00213
Pennsylvania Certification #: 68-03578
South Carolina Bioassay Certification #: 99030002
South Carolina Certification #: 99030001
Tennessee Certification #: 2980
Virginia Certification #: 00072
West Virginia Certification #: 356
Florida/NELAP Certification #: E87648
REPORT OF LABORATORY ANALYSIS
This report shall not tre reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.pco a
r
Page 2 of 10

IeAnalytical e
wwwpacehiftcam
Project: DIXON QUICK COUPLING
Pace Project No.: 9259083
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kinoey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
9259083001 SAMPLE LOCATION NO 2 EPA 1664A
CLW
1
PASI-C
EPA2001
JMW
1
PASI-A
SM 2540D
TEE
1
PASI-A
EPA 9040
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
A.
Page 3 of 10

�eMalytical
www.Pacalabsoom
Project: DIXON QUICK COUPLING
Pace Project No.: 9259083
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SAMPLE LOCATION NO 2 Lab ID: 9259083001 Collected: 12/08/09 16:50 Received: 12/09/09 08:55 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No_ Qual
HEM, Oil and Grease
Analytical Method: EPA 1664A
Oil and Grease
8.4 mg1L
5.0
1
12/09/09 14:01
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation
Method: EPA 200.7
Lead
103 ug/L
5.0
1 12/10/09 10:00
12/10/09 13:59 7439-92-1
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
24.5 mg/L
22.7
1
12/10/09 17:02
9040 pH
Analytical Method: EPA 9040
pH
7.2 Std. Units
0.10
1
12/10/09 21:35
Date: 12/11/2009 02:17 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
H6
Page 4 of 10

aceAnalytical
WWW..P8cgk &00M
Project: DIXON QUICK COUPLING
Pace Project No.: 9269083
QC Batch: GCSV/6819
OC Batch Method: EPA 1664A
Associated Lab Samples: 9259083001
METHOD BLANK: 376789
Associated Lab Samples: 9259083001
Parameter
Units
Oil and Grease
mg/L
LABORATORY CONTROL SAMPLE:
376790
Parameter
Units
Oil and Grease
mg/L
MATRIX SPIKE SAMPLE:
376791
Parameter
Units
Oil and Grease
mg1L
Date: 12/11/2009 02:17 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 1664A
Analysis Description: 1664 ITEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 12/09/09 14:01
Spike LCS LCS
Cone. Result % Rec
40 34.8 87
9259106005 Spike MS
Result Cone. Result
ND 40 37.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
78-114
MS % Rec
% Rec Limits Qualifiers
93 78-114
Page 5 of 10

1��alceAnalyfibale
t www.pacelab&OOM
I
Project: DIXON QUICK COUPLING
Pace Project No.: 9259083
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 26804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/5512 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9259083001
METHOD BLANK: 377211 Matrix: Water
Associated Lab Samples: 9259083001
Blank Reporting
Pace Analytical Services, Inc.
9B00 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units
Result
Limit
Analyzed Qualifiers
Lead ug/L
ND
5.0
12/1010913:52
LABORATORY CONTROL SAMPLE: 377212
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
Lead ug/L
500
510
102 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 377213
377214
MS
MSD
9259083001
Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result
Conc.
Conc.
Result
Result % Rec % Rec Limits RPD Qual
Lead ug/L 103
500
500
607
607 101 101 70-130 0
SAMPLE DUPLICATE: 377215
Parameter
Lead
Date: 12/11/2009 02:17 PM
9259116001 Dup
Units Result Result
ug/L ND ND
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
,:
Page 6 of 10

aceftlXical s
wwvpacebb&=n
Project: DIXON QUICK COUPLING
Pace Project No.: 9259083
QC Batch: WET110769
QC Batch Method: SM 2540D
Associated Lab Samples: 9259083001
METHOD BLANK: 377645
Associated Lab Samples: 9259083001
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE: 377646
Parameter Units
Total Suspended Solids mg/L
SAMPLE DUPLICATE: 377647
Parameter
Total Suspended Solids
Date: 12/11/2009 02:17 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28076
(7041875-9092
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 12/10/09 17:01
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 236 94 80-120
9259083001 Dup
Units Result Result RPD Qualifiers
mg/L 24.5 25.5 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 10

C ARaljftal`
r wry PzCek arom
1
Project: DIXON QUICK COUPLING
Pace Project No.: 9259083
QC Batch: VVET110767
QC Batch Method: EPA 9040
Associated Lab Samples: 9259083001
SAMPLE DUPLICATE: 377610
Parameter Units
pH
Date: 12/11 /2009 02:17 PM
Std. Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description: 9040 pH
9258433001 Dup
Result Result RPD Qualifiers
7.4 7.4 0 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
e� -
ii
Pace Analytical Services, Inc.
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 10

1��I=Analyfical*
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t
QUALIFIERS
Project: DIXON QUICK COUPLING
Pace Project No.: 9259083
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
HB Analysis initiated more than 15 minutes after sample collection.
[phone]
Date: 12/11/2009 02:17 PM REPORT OF LABORATORY ANALYSIS Page 9 of 10
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ifieh&

ac6Anayical
xww.pa A%bs.aam
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DIXON QUICK COUPLING
Pace Project No.: 9259083
Pace Analytical Services, Inc. ,
9800 Kincey Ave. Suite 100 ,
Huntersville, NC 28078 •
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
9259083001
SAMPLE LOCATION NO 2
EPA 1664A
GCSVI6819
9259083001
SAMPLE LOCATION NO 2
EPA 200.7
MPRP15512 EPA 200.7
9259083001
SAMPLE LOCATION NO 2
SM 2540D
WETl10769
9259083001
SAMPLE LOCATION NO 2
EPA 9040
WET110767
Date: 12/11/2009 02:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICP/5110
Page 10 of 10

aceAnal ical'
eww eealeh..eem
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C
Page: of
Required Client Information: Required Project Information: Invoice Information:
Company: A Report ToAttention;
1326911
f
Addre
Copy,Tc:
Company Nam
I�
REGULATORY AGENCY
+Q
OV1 J O r
Address:
NPDEs r GROUND WATER F-• DRINKING WATER
r UST r— RCRA r OTHER
E all To: r
Purchase Order NO.:
Pace Quale
A 3i I r►t s
Reference:
Phone; F ><: + ;CA
`rr
jact Name;
Pete Project
Site LOcagon
O QM'
Manager.
5Ti{TE:
R*qursted s a
Project Number.
Pace Pmflle q 3�1 J
�I (
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes
d
z
Required Client Information MATRIx !CODE
9
COLLECTED
Preservatives
.r
Drinking Water DW
z
Water WT
Produ,:tWaste WW
Soillsolid SL
L)
0
COMPOSITE
START
COMPOSITE
END/GRAB
J
SAMPLE ID O1;Aa ,°�,
i3
W
r
c
(A-z, as r; I Air AR
uw
uj
a
r1
Z
bi
J
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Sample IDs MUST BE UNIQUE Tissue TS
O
w
-*
Other OT
U
X
O
�
U
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=
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d
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yy
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DATE
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ADDITIONAL COMMENTS
RELIN4Uk$HED BY AFFILIATION
DATE
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DATE
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SAMPLE CONDITION$
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SAMPLER NAME AND SIGNATURE
ORIGINAL
PRINT Nam* of SAMPLER:
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DATE Signed
SIGNATURE of SAMPL
y03
-V.A! (MMIDDIYY):
'Impartam Note: By signing this farm you are accepting Pece's NET 30 day oeymnnt In"11 end nnr..lna m Ion. 1h.—. m t n.c ^...i 1— t..—1I^.,1'^--'-'.-

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Client Name:-. Project # 17Z5 7TZ'7
Courier: ❑ Fed Ex UPS LISPS Client ❑ ❑ ❑Commercial ❑ Pace Other OptionaC•
Custody Seal on Cooler/Box Present: ❑ yes no Seals intact: ❑ yes no P ;g Dui Datef t to :_
Packing Material: ❑ Bubble Wrap Bubble Bags" o None _We❑Other ��_
Thermometer Used T060 Type of Ice:(;et) I
Blue None /f Samnles on ice coolino process has beaun
Cooler Temperature
mac.. I
BiologicalTissue is Frozen: Yes Na NIA
Date and Initials of person examining
C
contents:
Temp should �e above freezing to 6'C
Comments:
Chain of Custody Present:
Yes
❑No
❑NIA
1,
Chain of Custody Filled Out:
es
QNo
❑NrA
2_
Chain of Custody Relinquished:
Yes
❑No
❑NIA
I
Sampler Name & Signature on COC:
Yes
❑No
❑NIA
4,
Samples Arrived within Hold Time:
❑Yes
❑No
❑N!A
5. A p cyfC. Ic- C E or
Short Hold Time Analysis (<72hr):
❑Yes-,210
❑NIA
6.
Rush Turn Around Time Requested:
e<Ye�s
t]No
❑N/A
7.
Sufficient Volume:
Yes
❑No
❑N/A
8.
Correct -Containers Used:
Yes
❑No
❑N1A
9•
-Pace Containers Used:
Yes
❑Na.
❑N1A
Containers Intact:
,,4�es
❑No
❑N/A
10. .
Filtered volume received for Dissolved tests
❑Yes
❑No
A
11. '
Sample Labels match COC:
&a es
ONo
❑NIA
12.
-includes dateltime/ID/Analysis Matrix:
All containers needing preservation have been checked,
Yes
❑No
❑NIA
13, '
All containers needing preservation are found to be in
❑No
©N1A
compliance with EPA recommendations
exceptions: VOA, coliform, TOC, O&G, WI-DRO(water)
❑Yes
❑No
initial.when completed
Samples checked for dechforination:
❑Yes
❑No
NIA
14.
Headspace in VOA Vials (>6mm):
Dyes
❑No
2rNIA
15.
Trip Blank Present:
Dyes
❑No
A
.
Trip Blank Custody Seals Present
Dyes
❑No
NIA
Pace Trip Blank Lot # (if purchased): NIA
Client Notification/ Resolution: Field Data Required? Y / N / NIA
Person Contacted:
Comments/ Resolufion:
Date/Time:
Project Manager Review: �56,% 1 Date: 11 -1 d • O R
Gl'e'
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers)

aceARayicaf.
wmpsceladaccm
Project: SAMPLING 11/10
Pace Project No.: 9257127
Asheville Certification IDs
West Virginia Certification #: 356
Virginia Certification #: 00072
Tennessee Certification #: 2980
South Carolina Certification #: 99030001
South Carolina Bioassay Certification M 99030002
Pennsylvania Certification #: 6"3578
Connecticut Certification #: PH-0106
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
CERTIFICATIONS
North Carolina Drinking Water Certification #: 37712
North Carolina Bioassay Certification #: 9
New Jersey Certification* NC011
Massachusetts Certification #: M-NCO30
Louisiana/LELAP Certification #: 03095
FloridalNELAP Certification #: E87648
North Carolina Wastewater Certification M 40
REPORT OF LABORATORY ANALYSIS Page 2 of 7
This report shall not be reproduced, except in hull,
without the written consent of Pace Analytical Services, Inc..
�lne`=

f .
aceAnaljftal'
kwxrps.oarr!
Project: SAMPLING 11/10
Pace Project No_: 9257127
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Ana"s
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
9257127001
LOADING DOCK
EPA 200.7
JMW
1
PASI-A
9257127002
BEHIND WAREHOUSE
EPA 200.7
JMW
1
PASI-A
9257127003
ROOF AT SHIPPING
EPA 200.7
JMW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
CCO�
Page 3 of 7

f•
• ® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
�acl
a Q%j',ji1/tlJsall2225 Riverside Dr. 9800 KinceyAve. Suite 100
uwna!lcabbb&camaJr Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
ANALYTICAL RESULTS
Project: SAMPLING 11/10
Pace Project No.: 9257127
Sample: LOADING DOCK
Lab ID: 9257127001
Collected: 11/10/09 00:00
Received: 11/10/09 13:00 Matrix:Water
Parameters
Results Units
Report Limit DF
Prepared
Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead
194 ug/L
5.0 1
11/11/0913:20
11/11/0916:58 7439-92-1
Sample: BEHIND WAREHOUSE
Lab ID: 9257127002
Collected: 11/10/09 00.00
Received: 11/10/09 13:00 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared
Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead
39.3 ug/L
5.0 1
1111110913:20
11/1110917:14 7439-92-1
Sample: ROOF AT SHIPPING
Lab ID: 9257127003
Collected: 11/10/09 00:00
Received: 11/10/09 13:00 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared
Analyzed CAS No, Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Lead
26.0 ug/L
5.0 1
11/1110913:20
1111110917:23 7439-92-1
Date: 11/12/2009 02:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
uiJ_J:
Page 4 of 7

e Pace Analytical Services, Inc. Pace Services, Inc.
�aceAnayicaAnalytical
l 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
xwwpsmwmcnm Asheville, NC 28804 Huntersville, NC 25078
[phone] (704)875r9092
QUALITY CONTROL DATA
Project: SAMPLING 11/10
Pace Project No.: 9257127
QC Batch: MPRP/5368
Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 9257127001, 9257127002, 9257127003
METHOD BLANK: 364655
Matrix: Water
Associated Lab Samples: 9257127001, 9257127002, 9257127003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Lead ug/L
ND 5.0
1111110916:50
LABORATORY CONTROL SAMPLE: 364656
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Lead ug/L
500 523
105 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 364657
364658
MS MSD
9257127001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Lead ug/L 194
500 500 648
651 91 91 70-130 0
SAMPLE DUPLICATE: 364659
9257127002 Dup
Parameter Units
Result Result
RPD Qualifiers
Lead ug/L
39.3 38.2
3
Date: 11/12/2009 02:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in hull,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 7

�eAnaoicale
WWWpeceftbimm
QUALIFIERS
Project: SAMPLING 11/10
Pace Project No.: 9257127
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kinney Ave. Suite 100
Huntersville. NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 fisted analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
Date: 11/12/2009 02:51 PM REPORT OF LABORATORY ANALYSIS Page 6 of 7
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

,�aceAnalytical
www.pecelabscom
Project: SAMPLING 11110
Pace Project No.: 9257127
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
Asheville, NC 28804
Huntersville, NC 28078
(B28)254-7176
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
9257127001
LOADING DOCK
EPA 200.7
MPRP/5368
EPA 200.7
ICP/4979
9257127002
BEHIND WAREHOUSE
EPA 200.7
MPRPl5368
EPA 200.7
ICP/4979
9257127003
ROOF AT SHIPPING
EPA 200.7
MPRP/5368
EPA 200.7
ICP/4979
Date: 11/12/200902:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 7

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
,,,, : , .
Gregory J; Thbrpe, Ph.D.
"Acting Director
Division bf Water Quality
December 27, 2001
RANDALL J MULLINS
PERFECTING COUPLING CO
PO BOX 790068
CHARLOTTE, NC 28206
Subject: NPDES Stormwater Permit Renewal
PERFECTING COUPLING CO
COC Number NCG030283
Mecklenburg County
Dear Permittee:
APR T 0 2302
Your facility is currently covered for stormwater discharge under General Permit NCG030000. This permit expires
on August 31, 2002. The Division staff is currently in the process of rewriting this permit and is scheduled to have
the permit reissued by late summer of 2002. Once the permit is reissued, your facility would be eligible for
continued coverage under the reissued permit.
In order to assure your continued coverage under the general permit, you must apply to the Division of Water
Quality (DWQ) for renewal of your permit coverage.. To make this renewal process easier, we are informing you in
advance that your permit will be expiring. Enclosed you will find a General Permit Coverage Renewal
Application Form. The application must be completed and returned by March 4, 2002 in order to assure continued
coverage under the general permit.
Failure to request renewal within this time period may result in a civil assessment of at least $250.00. Larger
penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility
without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and
could result in assessments of civil penalties of up to $10,000 per day.
Please note that recent federal legislation has extended the "no exposure exclusion" to all operators of industrial
facilities in any of the 1 I categories of "storm water discharges associated with industrial activity," (except
construction activities). If you feel your facility can certify a condition of "no exposure", i.e. the facilty industrial
materials and operations are not exposed to stormwater, you can apply for the no exposure exclusion. For additional
information contact the Central Office Stormwater Staff member listed below or check the Stormwater & General
Permits Unit Web Site at http://h2o.enr.state.nc.us/su/stormwater.htmi
If the subject stormwater discharge to waters of the state has been terminated, please complete the enclosed
Rescission Request Form. Mailing instructions are listed on the bottom of the form. You will be notified when the
rescission process has been completed.
If you have any questions regarding the permit renewal procedures please contact Mike Parker of the Mooresville
Regional Office at 704-663-1699 or Bill Mills of the Central Office Stormwater Unit at [phone], ext. 548
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Mooresville Regional Office
T
NCDENR
i i ' iJ
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1-800-623-7748

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
August 23, 2002
MARK N HALL
PERFECTING COUPLING CO
PO BOX 790068
CHARLOTTE, NC 28206
Subject: NPDES Stormwater Permit Renewal
PERFECTING COUPLING CO
COC Number NCG030283
Mecklenburg County
Dear Permittee:
In response to your renewal application for continued coverage under general permit NCG030000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued stormwater general permit. This permit is reissued
pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement
between the state of North Carolina and the U.S. Environmental Protection Agency, dated December 6, 1983.
The following information is included with your permit package:
* A new Certificate of Coverage
* A copy of General Stormwater Permit NCG030000
* A copy of the Analytical Monitoring Form (DMR)
* A copy of a Technical Bulletin for the general permit
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or
decree.
If you have any questions regarding this permit package please contact Bill Mills of the Central Office Stormwater
and General Permits Unit at [phone], ext. 548
cc: Central Files
Stormwater & General Permits Unit Files
Mooresville Regional Office
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
NC DEPT. O
AN0N'A t•-r?AL SCO"URCES
AUG 2 9 2002
'ATA
NCW R
N. C. Division of Waler Quality 1617 Mail Service Center Raleigh, NC 27699-1617 [phone] Customer Service
1- 800-623-7748

I*.
NCDENR
North Carolina Department of Environment and Natural Resources
Beverly Eaves Perdue
Governor
Mr. Scott Clark, General Manager
332 Atando Ave.
Charlotte, NC 28206
Dear Mr. Clark:
Division of Water Quality
Coleen H. Sullins
Director
April 6, 2010
Subject: Stormwater Monitoring Results
Dixon Quick Coupling
332 Atando Ave.
NPDES Stormwater Permit NCG NCG030000
Certificate of Coverage — NCG030283
Mecklenburg County
Dee Freeman
Enclosed are the monitoring results from the samples collected of the discharge from Stormwater Outfall 001 at the
subject facility. The samples analyzed were grab samples collected during the sampling investigation performed on
November 10, 2009, by Andrew Martin of Charlotte -Mecklenburg Storm Water Services_
This sampling investigation was conducted as part of a cooperative working agreement between Mecklenburg
County and the Division of Water Quality. In addition, the inspection was conducted on behalf of the City of
Charlotte in compliance with the City's NPDES Permit, NCS000240, Part II Section H.
The enclosed monitoring results indicate that the stormwater discharged on November 10, 2009, contained an
elevated concentration of lead compared with the benchmark values contained in Stormwater general permit
NCG030000. In addition, elevated concentrations of zinc and copper were also detected as compared with the
Division's benchmarks developed.for individual stormwater permits (copper - 7 µg/L; zinc - 67 µg/L). These values
also exceed the applicable stream standards for toxic substances (copper - 7 µglL; zinc - 50 µg/L). Since the
stormwater sample was not collected in -stream, the stream standards do not apply; however, these standards can
be used to indicate the potential of your runoff to impact the receiving stream.
Please review the requirements of your stormwater permit and take the required stepslactions to reduce the
concentration of lead, copper, and zinc leaving your site. Through the.development and, implementation of
stormwater management programs it is the Division of Water Quality's expectation that stormwater discharges at
industrial sites covered by NPDES stormwater permits do not impact receiving waters.
The enclosed results should be self-explanatory; however should you have any questions concerning the sampling
results or have any questions regarding your permit, please do not hesitate to contact Andrew Martin with CMSWS
or Ms. Marcia Allocco of the Division of Water Quality at [phone].
Sincerely,
for Robert B_ Krebs, Regional Supervisor.
Surface Water Protection Section
Mooresville Regional Office
cc: Water Quality Central Files
Craig Miller, City of Charlotte
Rusty Rozzelle, MCWQP
Mooresville Regional Office
Location: 610 Fast Center Ave., Suite 301 Mooresville, NC 28115
Phone: [phone] Fax: [phone] Customer Service: 1-877-623-6748
Internet http!Yportal.ncdenr.cr;'weblwq
OfiE
NorthCarona
V17t%1r71111

Scott Clark, Dixon Quick Coupling
Stormwater Sampling, Page 2
April 6, 2010
ADDENDUM
The National Pollutant Discharge Elimination System (NPDES) program was established under the federal
Clean Water Act and then delegated to the Division of Water Quality for implementation in North Carolina. The
NPDES permitting program for stormwater discharges was established in 1990. Phase 1 focuses on site and
operations planning to reduce pollutant sources.
Through the NPDES permitting program industrial facilities that fall into one of the subject ten categories are
required to obtain permit coverage under a general permit or an individual permit, depending upon the
facilities SIC code and the industrial activity occurring at the facility. There are currently 19 active general
stormwater permits in North Carolina. One condition that is applicable to both the general permits and
individual stormwater permits is the requirement to develop and implement site -specific comprehensive
Stormwater Pollution Prevention plans (SPPP). These plans are required to include a comprehensive
evaluation of the site and operations to reduce pollutant sources and prevent pollutant discharge.
Copies of the general permits and accompanying documents can be accessed from the following webpage:
http://h2o.enr,state.nc.us/su/Forms_Documents.htm_ Permit text, technical bulletins, discharge monitoring
forms, and a Notice of Intent [which is the application for coverage under a NPDES General Stormwater
Permit] can be found on this website.
The following items are a subset of permit requirements and are listed to assist you and help bring your
attention to certain permitting issues, process and condition requirements of your permit_ Please see the
above mentioned website to obtain a copy of the permit so you may fully comply with all the conditions therein.
Failure to properly comply with conditions of the permit, like those buffeted below, is a violation(s) of
the permit and subject to civil penalty assessment(s) of up to $25,000.00 per day.
• Industrial facilities that fall into one of the subject ten categories are required to obtain permit coverage
under a general NPDES stormwater permit or an individual NPDES stormwater permit
• All persons desiring to have facilities covered by a General Permit must register with the Division of
Water Quality (DWQ) by filing of a Notice of Intent (NOI) and Applicable Fees.
• This Notice of Intent (NOI) must be submitted and a Certificate of Coverage issued prior to any
discharge of stormwater associated with the industrial activity, process wastewater, andlor mine
dewatering.
• Once the Notice of Intent is received, DWQ will review and determine whether a Certificate of Coverage
(COC) may be issued. If this Certificate of Coverage is issued the facility is covered by the General
Permit. That is, the permittee is authorized to discharge stormwater, process wastewater, and/or mine
dewatering pursuant to the type of General Permit until the permit expires or is modified or revoked.
• Any other point -source discharge to surface waters of the state is prohibited unless it is an allowable
non-stormwater discharge or is covered by another permit, authorization, or approval.
• There are currently 19 active general permits. Permit conditions vary accordingly-, however, most of the
permits have the following condition requirements (you must read your entire permit to ensure full
compliance):
o Development and compliance with the Stormwater Pollution Prevention Plan
o Collection, reporting, and recording of Analytical Monitoring
Mooresville Regional Office
Location: 610 East Center Ave., Suite 301 Mooresviile, NC 28115 One t Phone: [phone] Fax: [phone] Customer Service: 1-877-623-6748 NOrthCarofina
Entemet:www.ncwaterquality.org - rn `r�
An Equal Opportunity 1 A`firmative Acton Employer - 30% RecycleVO% Past Consumer paper A�tuL yi`1

Scott Clark, Dixon Quick Coupling
Stormwater Sampling, Page 3
April 6. 2010
o Collection, reporting, and recording of Qualitative Monitoring
o Collection, reporting, and recording of Vehicle Maintenance Monitoring (if applicable)
o Records — Visual monitoring shall be documented and records maintained at the facility along
with the Stormwater Pollution Prevention Plan. Copies of the analytical monitoring results shall
also be maintained on site. The Permittee shall retain records of all monitoring information,
including all calibration and maintenance records and all original strip -chart recordings for
continuous monitoring instrumentation, and copies of all reports required by this general permit
for a period of at least 5 years from the date of the sample measurement, report, or application.
o Expiration — The permittee is not authorized to discharge after the expiration date of the general
permit. In order to receive automatic authorization to discharge beyond the expiration date, the
permittee shall submit forms and fees as are required by the agency authorized to issue permits
no later than 180-days prior to the expiration date. Any permittee that has not requested
renewal at least 180 days prior to expiration, or any permittee that does not have a permit after
the expiration and has not requested renewal at least 180 days prior to expiration, will be
subject to enforcement. Failure to renew your permit is a violation.
o Transfer — The Certificate of Coverage (COC) issued pursuant to this general permit is not
transferable to any person expect after notice to and approval•by the Director. The Director may
require modification or revocation and reissuance of the Certificate of Coverage to change the
name and incorporate such other requirements as may be necessary under the Clean Water
Act. The Permit is NOT transferable.
o Name Change, Closure, or Facility Ownership change — Permittee is required to notify the
Division in writing in the event the permitted facility is sold or closed. The Division of Water
Quality views changes of name or ownership as a modification that requires the Director's
approval and reissuance of the permit. Name and ownership changes require you to complete a
Name/Ownership Change Form from the Division and mail it back to the Division of Water
Quality along with all appropriate information.
o Proper Operation and Maintenance is a requirement of the permit.
Mooresville Regional office
Location: 610 East Center Ave., Suite 301 Mooresville, NC 28115
Phone: [phone] Fax: [phone] Customer Service:1-877-623-6748
Internet www.neNaterquality.org
ne
Noc6dhCarohna
Naturally
An Equal opportunity 1 Affirmative Action Employer - 30% Recycled110% Post Consumer paper

ANALYTICAL RESULTS SHEET
Name of Facility: Dixon Quick Coupling
Grab: ® Composite: ❑
Sample Date(s): November 10, 2009
NPDES Permit No.: NCG030283
Sample Location: Outfall SDO #001
County: Mecklenburg
Temperature
17.04 °C
Fecal coliform (CFU/100 mL)
<100/100 mL
Dissolved Oxygen
9.48 mg/L
E. Coli (MPN1100 mL)
<100/100 mL
Conductivity
41 µS/cm
Enterococcus (MPN/100 mL)
7,2001100 mL
pH
9.04 SU
Ammonia -nitrogen (NH3-N)
0.13 mg1L
Turbidity
7.1 NTU
Total Kjeldahl Nitrogen (TKN)
0.28 mg/L
Biological Oxygen Demand, 5-day
(BODO
5.9 mg/L
Nitrate/Nitrite-nitrogen (NO2 and NO3)
0.32 mg/L
Chemical Oxygen Demand (COD)
49 mg/L
Total Phosphorus (P)
0.069 mg1L
Total Suspended Solids (TSS)
19 mg/L
Chromium (Cr)
6.4 µg/L
Total Sediment Concentration
18 mg/L
Copper (Cu)
170 µg/L
Oil & Grease
<5.0 mg/L
Lead (Pb)
61 µg/L*
Total Toxic Organics (TTO)
"*
Zinc (Zn)
290 µg/L
Denotes an exceedance of the permit benchmark values
"" Did not sample for this parameter

Allocco, Marcia
From: Terry Carter [[e-mail]]
Sent: Sunday, February 28, 2010 12:18 PM
To: Allocco, Marcia; Eubanks, Ron
Cc: Crystal Mccabe; Scott Clark
Good Morning,
The results of Lead Testing previously discussed are listed below.
Sample 1A - 9.9 uglL 1.0099 mglL
Sample iB - 114 ug1L / .114 mglL
Taken from behind the building where the 2 drains meet and drain out the front of the loading dock.
Sample 2 - 50.6 uglL 1 .0506 mglL
Taken from the front of the loading dock.
Sample 3 — 294 uglL 1 .294 mglL
The isolated sample taken from Sample Location 2 where normal storm water samples are gathered.
My plan is to take set of samples from the alley where brass is stored. They are calling for rain on Tuesday. I will send
those results as soon as they are available. In the interim, if you can think of further testing that might help us please do
not hesitate to contact me.
Thank You,
Terry Carter
Dixon Quick Coupling
Ph: 704-405-3523