NCG030087_MONITORING INFO_20170623

STORMWATER DIVISION CODING SHEET
NCG PERMITS
PERMIT NO.
� C� Q 3 � � (�7
DOC TYPE
❑HISTORICAL FILE
UCMONITORING REPORTS
DOC DATE
❑ ��OI % OIO a'3
YYYYMMDD

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 6-23-17
CERTIFICATE OF COVERAGE NO. NC-M0087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY Iredell
PERSON COLLECTING SAMPLES _Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC4440 Comments on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2017
SAMPLE PERIOD ® Jan -June ❑ July -Dec
or ❑ Monthly'
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
�� Other C'
JUN 27 -2017
CENTRAL FILESPLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
DWR SECTION
❑ No discharge this period:'
outfall No.
Date Sample
Collected' '
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics-'
Benchmarks =__>
-
-
200 mg/L or 50 mg/L° .
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
SDO 2
5-1-17
.7
6.7
NA
<.05
.0027
.06
<5.92
NA
SDO 3
5-1-17
.7
<4.2
NA
<.05
.0026
.077
<6.85
NA
' Monthly samDline (instead of semi-annual) must
begin with the second consecutive benchmark exceedance for the same Darameter
at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Nate: If you report -a' sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3'responses. See General Permit text.
w
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART iI SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3:,' HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES NO ❑�
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑
REGIONAL OFFICE CONTACT NAME: Mooresville
Mail an on final and one copy of this DMR including all "No Dischar e" re ports,within 30 days o recei t a the lab results or at end o monitoringeriod
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, uhder'penaltyof law, that this document and all attachments were prepared.under my direction or supervision'in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
6/23/2017
(Date)
Permit Date:`11/1/2012�10/31/2017
SWU-2451,1ast revised 10/25/2012
Page 3of3

6-23-17
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
® o
KEWAUNEE
Scientific
Corporation
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Semi -Annual Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
On May V, I took samples from outfalls 2 and 3. 1 was unable to access outfall 1 during the event. As
you will see, there are no results for pH. This was due to miscommunication at the laboratory. I have
attempted to take additional samples but lightning, rain starting during off hours and insufficient time
between rain events have prevented this from happening.
Please let me know if you have any questions or need anything else.
Sincerely,
Scott M. Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
[e-mail]
P.O. BOX IB42, ST,\TI'S\'ILLE, NORTH UROLINA 286H7-1842 • 2700 WEST FRONT STREET, STAMNILLE, NORTH C\ROI.IN/\ ?N677-2927
HiONL 704-873-7202 • FAX [phone]

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 2-2-17
CERTIFICATE Of: COVERAGE No. NCG030087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY tredell
PERSON COLLECTING SAMPLES _Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2016
SAMPLE PERIOD ❑ Jan -June 0 July -Dec
or ❑ Monthly'
DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
RECEIVED ®Other C
FEO 0 9 2017 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
CENTRAL FILES
DWR SECTION � No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics'
Benchmarks ==_>
_
-
100 mg/L or 50 mg/O
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/201,7 SWU-245, last revised 10/25/2012
Page 1 of 3

Note: 1 rt a sample value in excess o/ the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®NO ❑
REGIONAL OFFICE CONTACT NAME: Mooresville
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharae" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties Ar submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of
Permit Date: 11/1/2012-10/31/2017
2/2/2017
(Date)
SW,U-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
6 .3 a C> 51
CERTIFICATE OF COVERAGE NO. NCG03 0 0 0 0 SAMPLE COLLECTION YEAR 2016
FACILITY NAME Galvan Industries, Inc. SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
COUNTY Cabarrus n or X❑ Monthly' December (manth)
PERSON COLLECTING SAMPLES Ian Holdeman
LABORATORY Pace analytical Services
Inc. Lab Cert. # 5342
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
MM..- M l V DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
Q r ❑Zero -flow X❑Water Supply ❑SA
FEB ❑Other
CENTRAL FILES
'DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
X❑ No discharge this period?2
Outfail No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organicss
Benchmarks =__>
-
-
100 mg/L or 50 mg/L°
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or
Stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
�afs�ic�d Londti e
Name (Print name)
PlQ.74- 1,?0nQ4e,-
Title (Pr- t title
2-12Z7.
(signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
FOR PART AAND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR includingall "No Discharge"" reports, within 30 days a receipt of the lab results or at end of monitoring eriod
in the case of "No Discharge"reports] to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. i
am aware tha�X% a�a siggXc�penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2 Z /.
(Signirallfure of Permittee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 3-21-16
CERTIFICATE OF COVERAGE NO. NCG030087
C`PyMPLE COLLECTION YEAR 2016
FACILITY NAME Kewaunee Scientific Corporation SAMPLE PERIOD ® Jan -June ❑ July -Dec
COUNTY Iredell ❑ ❑ [—]Trout or ❑ Monthly'
.?J�&'
PERSON COLLECTING SAMPLES _Scott Hager RECE AGING TO CLASS ORW HQW Trout PNA
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on yj}p ❑Zero -flow ❑Water Supply ❑SA
�
sample collection or analysis:
JUL 2 U 2gother C
CENTRAL FILES /�
DWR SECTION PLEASEMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
Part A: Stormwater Benchmarks and Monitoring Results
No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
`Inches
Total Suspended Solids
pH'
Standard units
Taw
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
I
Total Toxic
Organics
Benchmarks =__>
_
-
100 mg/L or 50 mg/O
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies,
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012
Page 1 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR Plt'(tT A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART li SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ®ENO ❑
REGIONAL OFFICE CONTACT NAME: Mooresville
Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case o "No Dischar e" re orts to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Per
Permit Date:11/1/2012-10/31/2017
7-15/2016
(Date)
SWU-245, last revised 10/2S/2012
Page 3 of 3

KEWAUNEE
Scientific
Corporation
7-15-16
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
RECEIVED
JUL 2 0 201,6
CENTRAL Fli_ES
DWR SECTION
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section is checked for March through June. Due to rain starting on
off hours/weekends and most rain accompanied with lightning we were unable to complete a sampling.
Please let me know if you have any questions or need anything else.
Sincerely,
Sc M. Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
scotthap,[e-mail]
N.O. BON 1842, STAIF.S%'ILLE, NOR IH CAROLINA M687-184' • _1700\VF_ I FRONT STREET, STATESVILLE, NORTH C>ROLINA 2R677-2927
NIR)NE 714-S73-72)If2 • FAX [phone]

Semi-annual Stormwater. Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000.
Date submitted 3-21-16
CERTIFICATE OF COVERAGE N0.,NC-G'030087
FACILITY NAME Kewaunee. Scientific Corporation
COUNTY Iredell
PERSON COLLECTING SAMPLES _Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments.on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2016
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or, ® Monthlyl January/February
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply [:]SA
Other G
REGE tRLDSE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
MAR 2 9 2016
CENTRAL FILES ® No discharge this period:
Outfall No.
bate,Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
i'Total Suspended Solids,
pH,
; Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
i
Hydrocarbons
Total Toxic
s
Organics
Benchmarks =_=>
-
100 rng/L or`50 mg/O
6.0 — 9.0
O.fl07. mg/L
0.03 mg/L
0.067 mg/L `
15 mg/L
1mg/L
1 Monthly sampling (instead of semi-annual) must
begin with the second consecutive benchmark exceedance for the same parameter
at the same outfall.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where.the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition,of Total Toxic Organics is that definition.contained in,the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3 AA

Notellf you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART li SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES M NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑
REGIONAL OFFICE CONTACT NAME: Mooresville
Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case o "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision -in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Krmittee)
Permit Date:11/1/2012-10/31/2017
3/21/2016
(Date)
SWU-245, last revised 10/25/2012
Page 3of3

IN 0
KEWAUNEE
Scientific
Corporation
3-21-16
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern.
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section is checked for both January and February. Due to rain
starting on off hours/weekends and activity restrictions due to surgery we were unable to perform the
monitoring.
Please let me know if you have any questions or need anything else.
Sincerely,
SO t M. Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
[e-mail]
r
PA). BOX I H42, S'IAI FSVII.LF., NORTH CARO LINA 2BW87-1842 • 2700 WES'I' FRONT SIRFET, STATESVI LLF, NORTH CAR( _)I.INA
PHONE 7o-I-873-7-102 • FAX 71W-87i1-7 rih5

Semi-annual Stormwater Discharge Monitoring RegortPR
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 2-17-16
i.
CERTIFICATE OF COVERAGE NO. NCG030087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY Iredell
PERSON COLLECTING SAMPLES Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2015 Or
SAMPLE PERIOD ❑ Jan -June my -De
or ® Monthly'_ December (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
[]zero -flow ❑Water Supply ❑SA
RECEIVED ®Other c
FEB .2 2 2016 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -�
CENTRAL FILES
DWR SECTION
❑ No discharge this period?'
Outfall No.
Date Sample
:
Collected'
(mo/dd
24-hour rainfall
amount,
tnches3
Total Suspended Solids
pH,
Standard units ..
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organicss
Benchmarks
C 5)-
100 mg/L or 50 mg/L4
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
SD01
12-14-
.10
15.33
7.96
.0252
.0025
.31
7.8
NA
SDO 2
12-14- 6
.10
6.67
7.09
.015
.0025
.116
15.7
NA
SDO 3
12-14 16
.10
24.17
6.91
.0884
.0025
.293
10.2
NA
1 Monthly samDline (instead of semi-annuall must
beEin with the second consecutive benchmark exceedance for the same Darameter
at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites maybe eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier Z or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A.BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES X NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑
REGIONAL OFFICE CONTACT NAME: Mooresville
Mail an original and one copy of this DMR including all "Na Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period
in the case o "No Discharae" reports}_to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature oWrmittee)
2/17/2016
(Date)
Permit Date:11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3of3

2-17-16
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
I b4h, 0
KEWAUNEE
Scientific
Corporation
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677,
On December 141h, 2015, l took storm water samples from outfalls 1,2 and 3.
Please let me know if you have any questions or need anything else.
Sincerely,
i
Scott M. Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-971-3238
scotthap,er@_kewaunee.com
P.O. 11OX 1842, SI'AIESVII.LE, N(')R1I1 CAROLINA 28687-1842 • 27oo w[V ST I'RONI STRIIET, SIATI'MIU,I:, NORTH CAR ()I-INA 28677-3727
III V ),NF 704-87:1-7202 • FAX [phone]

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 12-15-15
CERTIFICATE OF COVERAGE NO. NCG030087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY Iredell
PERSON COLLECTING SAMPLES Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2015
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or X Monthly'_ November (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply []SA'"'"
®Other C
r �
3
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
® No discharge this period: C .
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
topper
Lead
Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organicss
Benchmarks
100 mg/L or So mg/L4
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
DEC
L FIL
S
' Monthly samnlinE (instead of semi-annual) must
beein with the second consecutive benchmark exceedance for the same narameter
at the same BYJRall.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012
Page 1 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART -A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES Z NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES EK NO ❑
REGIONAL OFFICE CONTACT NAME: Mooresville
Moil an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant perjalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of
12/15/2015
(Date)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3of3

12-15-15
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section was checked. Due to rain starting on off hours/weekends
and not enough time between rain events we were unable to perform the monitoring. We were able to
perform monitoring in the December 2015 time period and will send results when they arrive.
Please let me know if you have any questions or need anything else.
Sincerely,
Scott M. Hager, CSP GtV G�
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
scotthager([e-mail]
ftc'e f-
DEC I �! ,©
2015
WR SEA ���ES
�r�oN

Semi-annual Stormwater Discharge Monitoring Report
_ for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 10-23-15
CERTIFICATE OF COVERAGE NO. NCG030087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY Iredell �d VED
PERSON COLLECTING SAMPLES _Scott Hager OCT 2 6 2015
LABORATORY Statesville Analytical Lab Cert. NC-#440 Confng9ts-on
sample collection or analysis: ©Wig rI LFi, ,
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2015
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or Monthly' September (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
[]Zero -flow ❑Water Supply ❑SA
®Other C
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
D< No discharge this period?'
Outfall No.
Date Sample
Collected)
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Capper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organicss
Benchmarks ===>
_
-
100 mg/L or 50 mg/L°
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
' Monthly samDline (instead of semi-annual) must
beein with the second consecutive benchmark exceedance for the same oarameter
at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier I, Tier 2, or Tier 3 responses. See General Permit text
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES DK NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES 9 NO ❑
REGIONAL OFFICE CONTACT DAME: Mooresville
Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
10/23/2015
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3of3

nCG-o 36ogl
f
10-23-15
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section was checked. Due to rain starting on off hours/weekends we
were unable to perform the monitoring. We will perform monitoring at the next available date/time in
the October 2015 time period.
Please let me know if you have any questions or need anything else.
Sincerely,
Scott . Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
[e-mail]

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 9-25-15
CERTIFICATE OF COVERAGE NO. N00030087
FACILITY NAME Kewaunee Scientifsc Corporation
COUNTY Iredell
PERSON COLLECTING SAMPLES Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
l
S�ATM LE COLLECTION YEAR 2015
E- 1\1 �LE PERIOD ❑ Jan -June ❑ July -Dec �
y [} or El monthly' August _ (month)
OCT QISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA "M
CENTRAL FILES ❑Zero -flow ❑Water Supply ❑SA=z�g
pWR SECTION NOther C
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 --),
No discharge this period:'
Outfall No.
Date Sample
P
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
Standard units
and
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total nicss
Organics
Benchmarks ===>
_
-
100 mg/L or 50 mg/L4
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1 Monthly sampling (instead of semi-annual) must
begin with the second consecutive benchmark exceedance for the same parameter
at the same outfall.
'For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Note: !f you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS: r
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES jK21 NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES N NO ❑
REGIONAL OFFICE CONTACT NAME: Mooresville
Mail an oriainal and one cony of this DMR. including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitories period
in the case of "No Discharge" reports] to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant pengltjes for submitting false information, including the possibility of fines and imprisonment for knowing violations."
- _1-11,61 9/25/2015
(Signature of rmittee) (Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

is 0
KEWAUNEE
Scientific
Corporation
9-25-15
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section was checked. Due to rain starting on off hours/weekends
and several days away from the facility we were unable to perform the monitoring. We will perform
monitoring at the next available date/time in the September 2015 time period.
Please let me know if you have any questions or need anything else.
Sincerely,
Scott M. Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
scotthaeer(@kewaunee.com
FO BOX 1842, STATESVILLE, NORTH (ARO LIN'A 28687-1842 • 2700 VVF,SF FRONT S'TREI:T, STAIBVILLF, NORTH (AROLINA 28677-2927
PHONE [phone]W • FAX I04-878-75o5

r
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 8-14-15
CERTIFICATE OF COVERAGE NO. NCG030087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY Iredell
PERSON COLLECTING SAMPLES _Scott Hager
LABORATORY Statesville Analytical Lab Cert.
sample collection or analysis:
NC-#440 Comments on
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2015
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or Monthly' July (month] C"7)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
RECEIVED ❑Zero -flow ❑Water Supply ❑SA`0
AUG 19 2015 Other C
CENTRAL FiLffASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
DWR SECTION
❑ No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organicss
Benchmarks
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
SDO1
7-17-15
.2
<3.205
7.86
<.05
.0178
.5415
<5.4
NA
SDO 2
7-17-15
.2
<4.762
5.69
<.05
.0100
.1059
<7.6
NA
SDO 3
7-17-15
.2
<9.5
5.30
<.05
.0025
.194
<6.9
NA
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
-'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433,11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012
Page 1 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART Il SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ® NO ❑
REGIONAL OFFICE CONTACT NAME: Mooresville
Mail an original and one cove of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case o "No Discharge" reports)to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
[Signature of Pe
8/13/2015
(Date)
�` Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3
"

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 7-13-15
CERTIFICATE OF COVERAGE NO. NCG030087'
FACILITY NAME Kewaunee Scientific Corporation
COUNTY Iredell
PERSON COLLECTING SAMPLES _Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440
sample collection or analysis:
Commentsi�co\]SD
O
Part A. Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2015
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ® Monthly' June (month) '
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply ❑SA
Other C
GEN���C� ON
b\N
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -i
® No discharge this period:'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organicss
Benchmarks =__>
_
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
NA
NA
NA
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES []NON
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Perm
7/13/2015
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, fast revised 10/25/2012
Page 3 of 3

T t `
743-15
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
164,
6)
KEWAUNEF
Scientific
Corporation
RE: Storm Water Discharge Monitoring Report
7o Whom It May Concern:
�CC N ED
R �.o�5
SUS 2 n
CEN � �"S1CN
DW
�cc1r'I\1S0
1� tj
CENTPV`"
'WR SEC
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section was checked. Due to rain starting on off hours/weekends
and lightning we were unable to perform the monitoring. We will perform monitoring at the next
available date/time in the July 2015 time period.
Please let me know if you have any questions or need anything else.
Sincerely,
Scott M. Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
scotthaeer(cD kewaunee.com
I'.0 8QX 18.121, SI'AIESVILLF, NOR III (-AR(LINA'!8687-1842 • 2700 WLSF FROM STRI.I:T, tiTATFSVII,I,L, NOR III CAROL INA 28677-21�27
11 -1( )N1: 7 [61-87,1-72172 • FAX 7 ❑4417A-751-

Semi-annual Stormwater Discharge Monitorinjq Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 5-29-15 [Q1�
CERTIFICATE OF COVERAGE NO. NCG030087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY . Iredell
PERSON COLLECTING SAMPLES _Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2015
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or Monthly' April (month) s`-
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNAj
❑Zero -flow ❑Water Supply ❑SA
RFr,Fl!/EEI (Other C l�
J U N 01 2015 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
DWR SECTION
INFORMATION PROCESSING UNIT
No discharge this period?Z
Outfall No.
©ate Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organicss
Benchmarks =__>
_
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
NA
NA
NA
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
S Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469,12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
. , .
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR including all "No Discharge"' reports._ within 30 days of receipts the lab results tar at end of monitorina period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
5/29/2015
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
DatiJ1qd 4-2A-1 5 L `
CERTIFICATE OF COVERAGE NO`NCG030087 11 vt SAMPLE COLLECTION YEAR 2015
FACILITY NAME Kewaunee Scientific Corporation
APR 2 9 1025 SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
COUNTY Iredell CENTRAL FILES or ®Monthly'_ March (month)
PERSON COLLECTING SAMPLES _Scott Hager DWR SECTION DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on ❑Zero -flow ❑Water Supply [:]SA .
sample collection or analysis: ®Other C
Part A: Stormwater Benchmarks and Monitoring Results
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
® No discharge this period?Z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
OrganicsS
Benchmarks =__>
-
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
i mg/L
NA
NA
NA
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Note. if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART li SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy Qf this DMR including all "No Dischor e" re orts within 30 days of receipt of the lab results or at end of monitoring eriod
in the case of "No Discharge" reports) o:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Perm
4/24/2015
(Date)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 3

ti
4-24-15
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
11
KEWAUNEE
Scientific
Corporation
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section was checked. Due to rain starting on off hours/weekends we
were unable to perform the monitoring. We will perform monitoring at the next available date/time in
the April 2015 time period.
Please let me know if you have any questions or need anything else.
Sincerely,
�e /--'
Scott . Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
scotthap,[e-mail]
P.(). IV A 1842. STA'I FSVII.I.Ii, NOR'I'I I CAROI.INA-W,87-1843 • 270{1 WFS'IFRONT STR17EI', S' IAUSVIUF, NOR FI CAROI-INA 2%77-2927
IIIIONf. 704-87:1-T-)0"! • FAX 704-87S-7565

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 3-6-15
CERTIFICATE OF COVERAGE NO. NCG030087 SAMPLE COLLECTION YEAR 2015
FACILITY NAME Kewaunee Scientific Corporation SAMPLE PERIOD ❑ Jan -June ❑ July-Dec1
COUNTY Iredell or Monthly' February (month)
PERSON COLLECTING SAMPLES _Scott Hager DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA7J
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on ®Zero -flow ❑ ter Supply ❑S
RECEI` ED
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
Other
MAR 1 () 2015
CENTRAL FILES
DWR SECTION
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
X No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics$
Benchmarks =__>
_
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
NA
NA
NA
1 Monthly samoline (instead of semi-annual) must
beein with the second consecutive benchmark exceedance for the same parameter
at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For"those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Ba$ed upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Scott Hager
Name (Print name)
Safety and Environmental Manager
Title (Print title)
3-6-1S
(Sig f fature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX mdl.", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?2
Outfall Na.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks ===>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 4.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Notec If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO 13
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an on inal and one copy of this DMR including all "No Discharge"' reports, within 30 days o recei t o the lab results or at end o monitoring
eriad
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are signi%ant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of
Permit Date: 11/1/2012-10/31/2017
3/6/2015
(Date)
SWU-245, last revised 10/2S/2012
Page 3 of 3

3-6-15
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
I a
KEWAUNEE
Scientific
Corporation
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section was checked. Due to an extremely cold month and rain
starting on off hours/weekends we were unable to perform the monitoring. We will perform
monitoring at the next available date/time in the March 2015 time period.
Please let me know if you have any questions or need anything else.
Sincerely,
J
Scott . Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
[e-mail]
P.O. E3ON T842, STAIESVILLF, NORTH CAROIINA28687-1N4' • 2700�VFS'I FRONI'STRFFI' STATFSVILLF, NORIII (-AkC)I_I.NNA?8(,77-29r!7
VHONF 704-873-7202 • FAX [phone]

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 2-11-15 • ---TOW
CERTIFICATE OF COVERAGE NO. NCG030087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY Iredell
PERSON COLLECTING SAMPLES _Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
==%V°
SAMPLE COLLECTION YEAR 2015
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ® Monthly' January _ (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNCP
RECEIVED Zero-flowWater Supply
❑
ROther
f=3 19 2015
Q: NTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
":tIVR SECTION
X No discharge this period?z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organics5
Benchmarks =__>
_
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
NA
NA
NA
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-24S, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement forTTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Scott Hager
Name (Print name)
Safety and Environmental Manager
Title (Print title)
2-11-15
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Senchmurks ===>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table S, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an ordinal and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of lab results for of end of monitoring period
in the case o "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of
2/11/2015
(Date)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 3

2-11-15
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
IN 0
KEWAU NEE
Scientific
Corporation
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section was checked. Due to a relatively dry month we were unable
to perform the monitoring. We will perform monitoring at the next available date/time in the February
2015 time period.
Please let me know if you have any questions or need anything else.
Sincerely,
Scott . Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
[e-mail]
V.O. HOX 1842, STMFSVII.EE, NOR IIi CAROI.INA 28087-184' • 27001WESI FRONT STREET, STATESVII.LE, NORTH CARD INA 2W,77-2027
PI IONS 704-87'5-7202 • FAX [phone]

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 1-7-15
CERTIFICATE OF COVERAGE NO. NCG030087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY Iredell
PERSON COLLECTING SAMPLES _Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2014
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ❑ Monthly' December (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
❑Zero -flow ❑Water Supply []SA
RECEIVED ®Other C
JAN 13 2015 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
CENTRAL FILES
DV/R SECTION
No discharge this period:2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organics'
Benchmarks =__>
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
NA
NA
NA
1 Monthly sampling (instead of semi-annual) must
begin with the second consecutive benchmark exceedance for the same parameter
at the same outfall.
z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
`Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Scott Hager
Name (Print name)
Safety and Environmental Manager
Title (Print title)
1-7-15
(Sign e} (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 1, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?z
Outfali Na.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
IncheS
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks
15 mg/L
100 mg/L or 50 mg/L*
6.0 -- 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Per�ttee)
Permit Date: 11/1/2012-10/31/2017
1/7/2015
(Date)
SWU-245, last revised 10/25/2012
Page 3 of 3

1-7-15
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
I 4o (�
KEWAUNEE
Scientific
Corporation
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section was checked. Due to rain starting on off hours and
weekends we were unable to perform the monitoring. We will perform monitoring at the next available
date/time in the January 2015 time period.
Pleaselet me know if you have any questions or need anything else.
Sincerely,
Scott M. Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
[e-mail]
P.H. BOX 1842, SWESVILLE, NORTH CAkOLLVA 28G8i-1842 • '17001VLSI fkON''i', IkEE1; S'IXESVILLF, NORM G1kOl. NA 2R677-2927
PHONE: [phone] • FAX [phone]

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 12-30-14
CERTIFICATE OF COVERAGE NO. NCG030087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY Iredell
PERSON COLLECTING SAMPLES _Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2014
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or ❑ Monthly'_ November _ (mom}�
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PW2
� �� / �1 ❑Zero -flow ❑Water supply 15SD
RE V D ®Other C
JFtN `4 Zli 1i
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OI
DWR SFCTION i
❑ No discharge this period?Z
Outfall No.
Date Sample
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
5
Organics
Benchmarks =_=>
-
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
11-6-14
.4
46
6.66
<.005
.0026
.24
<7.8
NA
2
11-6-14
.4
16
5.93
<.005
.0026
.10
<5.7
NA
3
11-6-14
.4
44
5.89
<.005
.0064
.12
<5.7
NA
1 Monthly sampling (instead of semi-annual) must
begin with the second consecutive benchmark exceedance for the same parameter
at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
0
• Page 1 of 3 0

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Petmit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Scott Hager__
Name (Print name)
Safety and Environmental Manager
Title (Print title)
12-30-14
(Signature) (Date)
Note: Results must be reported in numerical format. Do not reportBelow Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format "<XX m L" where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier I, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 4.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
0
0
Page 2 of 3 .

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME DUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge".reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
{Signature of
12/30/2014
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/2S/2012
0
• Page 3 of 3 0

12-30-14
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
KEWAUNEE
Scientific
Corporation
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
On November 6t4, 2014, 1 took storm water samples from outfalls 1, 2 and 3. Rainfall was intermittent
with heavier rain 15 minutes before.
Please let me know if you have any questions or need anything else.
Sincerely,
Scott M. Hager, CSP
Safety and Environmental Manager
} Kewaunee Scientific Corporation
704-871-3238
5cotthager@kewaunee._com
•
CORPORATE: OFFICLS • I'. O. BOX 1842, SIA11:SVILLE, NORTH CAROLINA 28687-1842 • 2700 WE T FRONT SI'RELI', SIATLSVILIE NORTH C.AkOLINA 28677-2927
PHONE [phone] • FAX [phone]

AP
Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 10-17-14
CERTIFICATE OF COVERAGE NO. NCG030087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY I redell
PERSON COLLECTING SAMPLES _Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2014
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
or CKMonthly; September _ (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
RECEIVED ❑Zero -flow [:]WaterSupply ❑SA
OCT 2 f 2014 ❑Other
CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
DWR SECTION
N No discharge this period ?2
Outfall No.
Date Sample
Collected)
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics5
Benchmarks -__>
_
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z for sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

,r
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Scott Hager
Name (Print name)
Safety and Environmental Manager
Title (Print title)
10-17-14
(Sign re) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L". where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?Z
Outfal{ No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inche53
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
-
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMIi including all "No Discharge" reports, within 30 da s of receipt of the lab results or at end of monitorin-q period
in the case of "No Discharae" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
[Signature of
Permit Date:11/1/2012-10/31/2017
10/17/2014
(Date)
SWU-245, last revised 10/25/2012
Page 3of3

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 9-11-14
CERTIFICATE OF COVERAGE NO. NCG030087 SAMPLE COLLECTION YEAR 2014
FACILITY NAME Kewaunee Scientific Corporation SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
COUNTY Iredell �r C or ❑ Monthly' (month
PERSON COLLECTING SAMPLES _Scott Hager C C � V G[bi$CHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA
LABORATORY Statesville Analytical Lab Cert. NC4440 Comments in G ❑Zero -flow ❑Water Supply ❑SA
�014
sample collection or analysis: Sip 1 ❑Other
LENTP,AL FILES
pWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
Part A: Stormwater Benchmarks and Monitoring Results
No discharge this period?Z
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
lnches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
Organics
Benchmarks =__>
_
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
O
1 Monthiv samoline (instead of semi-annuall must
begin with the second consecutive benchmark exceedance for the same parameter
at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/l/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), 1 certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the Stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Scott Hager
Name (Print name)
Safety and Environmental Manager
Title (Print title)
e_
9-11-14
(Sign re) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX me/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period:
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART Ii SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO '
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR includina all "No Discharge" reports, within 30 days of recelat of he lab results (or at end of monitoring period
in the case o "No Discharge" Worts) to:
Division of water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Perm
9/11/2014
(Date)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 3

9-11-14
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section was checked. Due to rain starting on off hours/weekends
and some lightning we were unable to perform the monitoring. We will perform monitoring at the next
available date/time in the September 2014 time period.
Please let me know if you have any questions or need anything else.
Sincerely, /
G
t M. Hager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
[e-mail]

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Qualit General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03 D OCR Y 7
FACILITY NAME 1�-G w ii u.n ee 7 c i
COUNTY f/
PERSON COLLECTING SAMPLES
LABORATORYLab Cert. # N
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2—
SAMPLE PERIOD ❑ Jan -June ❑ July -Dec
=r1'" or [j] Monthlyl )4, l month
��RGING TO CLASS ❑ORW HQW [—]Trout❑PNA
REC ❑Zero -flow []Water Supply []SA
AUG 14 Z014 2(fther_f /.ass C
CENTRAL PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
�c discharge this period?'
Outfall No.
Date Sample
f
Collected
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total Toxic
s
Organics
Benchmarks =__>
_
-
100 mg/L or 50 mg/L
6.0 — 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
/ v
d
I
1 Monthly samoline [instead of semi-annual] must
beein with the second consecutive benchmark exceedance for the same parameter
at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
SG o p
Name (Print name) I
SLj {G dvi �/7 V/l a Y) liJGl� f4, 1
Title (Print title)
(Signs e) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
!Vote: If you report a sample value In excess of the benchmark, you most implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
D No discharge this period??
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks
15 mg/L
100 mg/L or 50 mg/L'
6.0 — 9.0 SU
,f
Footnotes from Part A also apply to this Part B
" See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier T, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
+ TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR including all "No Discharae" reports, within 30 days of receipt of the lob results for at end of monitoring period
in the case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED;
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
{Signature of Pe
(Date)
Permit Date: 11/1/2012-10/31/2017
SWU-245, last revised 10/25/2012
Page 3 of 3

8-11-14
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the Monthly Stormwater Discharge Monitoring Report for Kewaunee Scientific
Corporation, 2700 West Front Street, Statesville, NC 28677.
As you will see, the "No Discharge" section was checked. Due to rain starting on off hours/weekends
and some lightning we were unable to perform the monitoring. We will perform monitoring at the next
available date/time in the August 2014 time period.
Please let me know if you have any questions or need anything else.
Sincerely,
Scott M. ager, CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
[e-mail]

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted 8-11-14
CERTIFICATE OF COVERAGE NO. NCG030087
FACILITY NAME Kewaunee Scientific Corporation
COUNTY Iredell
PERSON COLLECTING SAMPLES Scott Hager
LABORATORY Statesville Analytical Lab Cert. NC-#440 Comments on
sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
SAMPLE COLLECTION YEAR 2014
SAMPLE PERIOD ® Jan -June ❑ July -Dec
or ❑ Monthly' (month)
DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA
Zero -flow ❑�ater5upply ❑SA
RECEIVED ROther
AUG 15 2014 PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
CENTRAL FILES
DWO/BOG
❑ No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Copper
Lead
Zinc
Non -Polar O&G/Total
Total Petroleum
Hydrocarbons
Toxic
Organics5
Benchmarks =__>
-
-
100 mg/L or 50 mg/L
6.0 -- 9.0
0.007 mg/L
0.03 mg/L
0.067 mg/L
15 mg/L
1 mg/L
1
6-5-14
.5
9.0
5.7
.015
.014
.25
5.8
NA
2
6-5-14
.5
30.7
5.74
.05
.0054
.14
6.2
NA
3
6-5-14
.5
57
5.37
.066
.007
.27
6.3
NA
' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012
Page 1of3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the stormwater Pollution Prevention Plan."
Scott Hager
Name (Print name)
Safety and Environmental Manager
Title (Print title)
8-11-14
(Signatu (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: if you report a sample value In excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
❑ No discharge this period?2
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Non -polar O&G/TPH by
EPA 1664 (SGT-HEM)
Total Suspended Solids
pH
Benchmarks =__>
_
-
15 mg/L
100 mg/L or 50 mg/L*
6.0 — 9.0 SU
Footnotes from Part A also apply to this Part B
* See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
FOR PART AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑
REGIONAL OFFICE CONTACT NAME:
Mall an original and one copy of this DMR Including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period
in the case of "No Discharge" reports) o:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
°I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
(Signature of Per
8/11/2014
(Date)
Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012
Page 3 of 3

8-11-14
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
yam
KEWAUNEE
Scientific
Corporation
RE: Storm Water Discharge Monitoring Report
To Whom It May Concern:
Please see attached the storm water sampling results for Kewaunee Scientific Corporation, 2700 West
Front Street, Statesville, NC 28677.
On June 5th, 2014, 1 took storm water samples from outfall numbers 001, 002 and 003. Rainfall was
intermittent with heavy rain approximately 30 minutes before.
Please let me know if you have any questions or need anything else.
Sincerely,
Scott M. eer, �CSP
Safety and Environmental Manager
Kewaunee Scientific Corporation
704-871-3238
[e-mail]
C(.)k110kAl li OFFICES • 1'. O. BOX 1842, STATESVILLE, NORI'4I CAROL 28687-1842 • 2700 WEST FRONT S'I'HITI', S'I'AI E.SVILLF:, NOR W CAROLINA 28677-2927
P1IONL 704-873-720Z • FAX [phone]

VJ A T���G
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Permit No.: NIC16161.,31610 or Certificate of Coverage No.: NICIGI J/,Y/ eJl01-Y171
Facility Name:.,��rL�.un �_ �`� a.�v_;.,� -� Inc„� g/�•_
County.Phone No. 7 2- 3 £7
Inspector:—lr,�..s.�r•L l . r., s t�a`e
Date of Inspection:
By this signature, I cep that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee. or Designee)
1. OutfaIl Description
OutfalI No: ac'�O Structure (pipe, ditch, etc.) jv- Tip-( 'Pam.
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:104"D //Ve_ —f . -uL)
2. Color.
Describe the color of the discharge using Basic colors (red, brown, blue, etc.) and tint (light, medium,
dark) as descriptors: "LIe? q k
3. Odor
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor,
etc.)
4. Clarity
Choose the number which best describes the clarity of the discharge where I is clear and 10 is very
cloudy:
110. 2 3 4 5 6 7 8 9 10
Page 1
SWU-242-020705

5. Floating Solids
Choose the number which best describes the amount of floating solids in the stormwater discharge where
1 is, no solids and 10 is the surface covered with floating solids:
J 2 3 4 5 6 7 8 9 10
6. Suspended Solids
Choose the number which best describes the amount of suspended solids in the stormwater discharge
where 1�is:
�no solids and 10 is extremely muddy
� 1 J 2 3 4 5 6 7 8 9 10
7. Foam
Is there any foam in the stormwatcr discharge? Yes CNo)
8. Oil Sheen
Is there an oil sheen in the stormwater discharge? Yes No
9. Deposition at Outfall
Is there deposition of material (sediment, etc.) at or immediately below the outfall?
10. Erosion at Outfall
Is there erosion at or immediately below the outfall? Yes oNo
11. Other Obvious Indicators of Stormwater Pollution
List and describe _L `af! ! pf ram-- n fflq, .OLO L127p
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, deposition or erosion may be
indicative of conditions that warrant further investigation and corrective action.
Page 2
S WU-242-020705

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
GENERAL PERMIT NO. NCG030000 _ SAMPLES COLLECTED DURING CALENDAR YEAR:
CERTIFICATE OF COVERAGE NO. NCG03 0 0 `[� t (This monitoring report is due at the Division no later than 30 days from
T ? jr;the date the facility receives the sampling results from the laboratory.)
FACILITY NAME /�r-Zi4J/I c r' l; � a n QA) COUNTY
_ •� rgD G�
PERSON COLLECTING SAMPLES PHONE NO.
CERTIFIED LABORATORY 5'i� MI;Ar. !� h; aL, Lab #•'4 '7551,*Ye:
Age—,g Aya'[�ct2 Lab # -14';371/ - PLEASE SIGN ON THE REVERSE 3
Part A: Specific Monitoring Requirements
0utfall
= Date rr
aF 00530
00400"
E181`4I: l�-'
No
.L
Sample;Collected;?
Total Sus eridedlSoLds , °
P
H'
P t
r ,.Lead mfL �'
g
'=0il'ariii'Grease �'
'
TotalToaxc',Or anxcs,
mold'
«, ,
, , ,.1:+:
•
A! .
F r
-
r .F:
m
, ;Standard:.uinitsr_,<
'°Benchmark-
cf
i'
I.Wttlin4 b Nti
G 0 - 9 0
033 t
,; � ':k�
,W' 9_'q1`_
,;tkwi'`100
.. .0 p:•
r _ -30...n,��
I -
'7
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? yes _no`
(if yes, complete Part B} . . I
Part B: Vehicle Maintenance Activity onitoring Requirements
Outfall
No,
a Date archs '�
Sam le Collected;}"
ai -ij
ma(dd/ r;,.;! ,'
,�'ti T y 00556, ,!,
' O�l'attd Grease,'e ;
-''TM;-!-'r4
,;r ,r�.,::;.',,rie /I
;6400530 ' r' °¢ „
.Toftal Suspended Solids;
.'Ik5 4 - 7n� "ikf Fd v'.._
L.. :-s..m /Li k ,•,'`
00400s
k Y pH, ,y
{l ul.1�4
r.:,.r:Sta'n'dard.unrts ,.-
'New` Motor Oil.Usage, .
. �Aii'nual;avera ge al/mo
L , ..
Benchmark
ri?a
i.' �' �.f4 T. y - A �4Sj
1 ti I
:. 00 : '� ,,60
� � S ,i Y i 'r." t R'
. 30 dltr
}i 5✓ H.;_ i 1 '�'
-
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
STORM EVENT CHARACTERISTICS:
Date C s1�`I (first event sampled)
Total Event Precipitation (inches): E t
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches): _ lam_
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
S VVU-245-102107
Page I of 2

Analytical Results
Kewaunee Scientific Corp. For Storm Water
PO Box 1842
Statesville NC 28687
Entered 6/5/2009
Reported: 7/15/2009
Sample Remark
Sample ID
Parameter
Cust ID
Result
Units
Method
Date Analyzed
Analyst
09065-7.1
Lead-Fur/liquid
outfalll
<0.0025
mg/L
SM3113B
6/10/09
MD
09065-7.1
Oil & Grease
outfall 1
5.2
mg/L
EPA 1664
6/10/09
MD
09065-7.1
pH
outfall 1
6.65
STD units
SM4500HB
615109
MD
09065-7.1
TSS
outfalll
11.2
mglL
SM2540D
619109
MD
09065-7.1
TTO
outfall I
See Attached
as noted
6119/09
PACE
09065-7.2
Lead-Fur/liquid
outfall2
<0.0025
mg/L
SM3113B
6/10/09
MD
09065-7.2
oil & Grease
outfall 2
<5.1
mglL
EPA 1664
6/10/09
MD
09065-7.2
pH
outfall 2
6.35
STD units
SM4500HB
615109
MD
09065-7.2
TSS
outfall2
<4
mg/L
SM2540D
619109
MD
09065-7.2
TTO
outfall 2
See Attached
as noted
6/19109
PACE
09065-7.3
Lead-Fur/liquid
outfall3
0.0027
mg/L
SM3113B
6/10109
MD
09065-7.3
Oil & Grease
outfall 3
<5.4
mg/L
EPA 1664
6/10/09
MD
09065-7.3
pH
outfall 3
6.37
STD units
SM4500HB
615109
MD
09065-7.3
TSS
outfall3
<4 -
mglL
SM2540D
6/9/09
MD
09065-7.3
TTO
outfall 3
See Attached
as noted
6119/09
PACE
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NCO0909
P.O. Box 228 • StatesN411e, North Carolina 28687 • 704/872/4697

Condition of Receipt
Sample ID 09065-7.1 Client Kewaunee Scientific Cor
Temp on Arrival 4
pH upon Arrival �2
pH upon Arrival <
pH upon Arrival
pH upon Arrival
pH upon Arrival
Parameter Scheduled Lead-Fur/liquid
W
HNO3
❑
HCl
❑
NaOH
❑
H2SO4
❑
Na2S20
❑
Dechlorinated
Parameter Scheduled Oil & Grease
❑
HNO3
EV
HCI
❑
NaOH
❑
H2SO4
❑
Na2S20
[�
Dechlorinated
Parameter Scheduled pH
❑
HNO3
❑
HCl
NaOH
❑
H2SO4
❑
Na2S20
Dechlorinated
Parameter Scheduled TSS
❑
HNO3
❑
"Cl
❑
NaOH
❑
H2SO4
❑
Na2S20
71
Dechlorinated
Parameter Scheduled TTa
❑
HNO3
❑
Ha
❑
NaOH
❑
H2SO4
❑
Na2S20
❑ Dechlorinated
❑ Chemicals in containers, client
❑ Chemicals upon receipt
0 Received on Ice
❑ Samples chilled upon receipt
6 Chemicals in containers, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
❑r/ Received on Ice
❑ Samples chilled upon receipt
[V Chemicals in containers, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
0 Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
❑ Chemicals in containers, client
❑ Chemicals upon receipt
W Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
Page 1 of l

Analytical
WWW'psookftow
r
June 30, 2009
Ms. Tracy Moore
Statesville Analytical
122 Court Street
Statesville, NC 28677
RE: Project: 09065-7
Pace Project No.: 9245998
Dear Ms. Moore:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on June 08, 2009. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie McKee
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not W reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 1 of 34

ceAnalytical
waw. peceabscom
Project: 09065-7
Pace Project No.: 9245998
Pace Analytical Services, Inc.
2226 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDS
West Virginia Certification #: 357
North Carolina Field Services Certification #: 5342
Virginia Certification #: 00213
North Carolina Drinking Water Certification #: 37706
Tennessee Certification #: 04010
New Jersey Certification #: NCO12
South Carolina Drinking Water Cerl. #: 990060003
Louisiana[LELAP Certification #: 04034
South Carolina Certification #: 990060001
Kentucky UST Certification #: 84
Pennsylvania Certification #: 68-00784
Florida/NELAP Certification #: E87627
Connecticut Certification #: PH-0104
North Carolina Wastewater Certification M 12
Asheville Certification IDS
West Virginia Certification #: 356
Pennsylvania Certification #: 68-03578
Virginia Certification #: 00072
North Carolina Wastewater Certification #: 40
Connecticut Certification #: PH-0106
North Carolina Drinking Water Certification #: 37712
Florida/NELAP Certification #: E87648
North Carolina Bioassay Certification #: 9
Tennessee Certification #: 2980
New Jersey Certification #: NCO11
South Carolina Certification #: 99030001
Massachusetts Certification M M-NC030
South Carolina Bioassay Certification #: 99030002
Louisiana/LELAP Certification #: 03095
Eden Certification IDs
North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738
Virginia Drinking Water Certification #: 00424
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,.
Page 2 of 34

I
Anaijftal
WAW..Pacwlbic+om
f
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 09065-7
Pace Project No.: 9245998
Sample: 09065-7.1 Lab ID: 9245998001 Collected: 06/05/09 06:30 Received: 06/08/09 15:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed
608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3535
CAS No. . Quat
Aldrin
N❑ ug/L
0,050
1
06/11/09 09:00
06123/0913:54
309-00.2
alpha-BHC
NO ug/L
0.050
1
06/11/09 09:00
05/23/09 13:54
319-84-6
beta-BHC
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 13:54
319-85-7
delta-BHC
ND ug/L
0.050
1
06/11/09 09:00
06/23/09 13:54
319-W8
gamma-BHC (Lindane)
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 13:54
58-89-9
Chlordane (Technical)
NO ug/L
0.50
1
06/11/09 09:00
06/23/09 13:54
57-74-9
4,4'-DDD
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 13:54
72-54-8
4,4'-DDE
NO ug1L
0.050
1
06/11/09 09:00
06123/09 13:54
72-55-9
4,4'-DDT
ND ug1L
0.050
1
06/11/09 09:00
06/23/09 1154
50-29-3
Dieldrin
ND ug/L
0r050
1
06/11/09 09:00
061231091154
60-57-1
Endosulfan I
ND ug/L
0.050
1
06111/0909:00
0612310913:54
959-98-6
Endosulfan 11
NO ug/L
0.050
1
06/11/09 09:00
0612310913:54
33213-65-9
Endosutfan sulfate
NO ug/L
0.050
1
06/11/09 09:00
05/23/09 13:54
1031-07-8
Endrin
ND ug/L
0.050
1
06/11/09 09:00
06/23/09 13:54
72-20-8
Endrin aldehyde
ND ug/L
0,050
1
06/11/09 09:00
06/23109 13:54
7421-93-4
Heptachlor
ND ug/L
0.050
1
06/11/09 09:00
06/23/09 13:54
76-44-8
Heptachlor epoxide
NO ug/L
0.050
1
06111/09 09:00
06/23109 13:54
1024-57-3
PCB-1016 (Aroclor 1016)
NO ug/L
0.50
1
06/11/09 09:00
06/23/09 13:54
12674-11-2
PCB-1221 (Aroclor 1221)
NO ug/L
0.50
1
06/11/09 09:00
06/23/09 13:54
111D4-28-2
PC8-1232 (Aroclor 1232)
ND ug/L
0.50
1
06/11/09 09:00
06/23109 13:54
11141-16-5
PC8-1242 (Aroclor 1242)
ND ug/L
0-50
1
06/11/09 09:00
06/23/09 13:54
53469-21-9
PCB-1248 (Arodor 1248)
ND ug/L
0.50
1
06/11/09 09:00
06/23/09 13:54
12672-29-6
PCB-1254 (Aroclor 1264)
NO ug/L
0.50
1
06/11/09 09:00
06123109 1154
11097-69-1
PCB-1260 (Aroclor 1260)
ND ug/L
0.50
1
06/11/09 09:00
06/23/09 13:54
11096-82-5
Toxaphene
NO ug1L
0.50
1
06/11/09 09:00
06/23/09 13:54
8001-35-2
Tetrachloro-m-xylene (S)
59 %
20-110
1
06/11/09 09:00
06/23/09 13:54
877-09-8
Decachlorobiphenyl (S)
65 %
20-138
1
06/11/09 09:00
06/23/09 13:54
2051-24-3
200.7 MET ICP
Analytical Method: EPA200.7
Preparation Method: EPA200-7
Antimony
6.2 ug/L
5.0
1
061111091518
06113109 1140
7440-36-0
Arsenic
ND ug/L
5.0
1
06/11/09 15:18
06/13/09 13:40
7440-38-2
Beryllium
NO ug/L
1.0
1
06/11/09 15:18
06113109 13:40
7440-41-7
Cadmium
NO ug1L
1.0
1
06/11/09 15:18
06/13/09 13:40
7440-43-9
Chromium
ND ug/L
5.0
1
06/1110915:18
06/13/09 13:40
7440-47-3
Copper
5.4 ug/L
5.0
1
06111/0915:18
06/13/09 13:40
7440-50-8
Lead
NO ug/L
5.0
1
06/11/09 15:18
06/13/09 1140
7439-92-1
Nickel
ND ug/L
5.0
1
06111/0915:18
06/13/09 1140
7440-02-0
Selenium
NO ug/L
10.0
1
0611110915:18
06/13/09 13:40
7782-49-2
Silver
ND ug/L
5.0
1
06111109 15: 18
06/1310913:40
7440-224
Thallium
ND ug/L
10.0
1
05/1110915:18
06/1310913:40
7440-28-0
Zinc
131 ug1L
10.0
1
06111/0915:18
06113/0913:40
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1
Preparation Method: EPA 245A
Mercury
NO ug/L
0.20
1
06111/0917:05
06112/0911:27
7439-97-6
Date: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS Page 3 of 34
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

�Jce Analytical
xww.pacebbs.com
i
I
Project: 09065-7
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
ANALYTICAL RESULTS
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Pace Project No.: 9245998
Sample: 09065-7.1 Lab ID: 9245998001 Collected: 06/05/09 06:30 Received: 06/08/09 15:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthylene
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
Anthracene
NO ug/L
7.1
1
06/1210909:00 061191091T58
Benzidine
ND .ug/L
71.4
1
06/12/09 09:00 06/19/09 17:58
Benzo(a)anthracene
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
Benzo(a)pyrene
NO ug/L
7,1
1
06/12109 09:00 06/19/09 17:58
Benzo(b)fluoranthene
ND ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
Benzo(g,h,i)perylene
NO ug/L
7.1
1
06/12/09 09:00 0611910917:58
Benzo(k)fluoranthene
ND ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
4-Bromophenylphenyl ether
ND ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
Butylbenzylphthalate
ND ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
4-Chloro-3-methylphenol
ND ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
bis(2-Chloroethoxy)methane
NO ug/L
14.3
1
06/12/09 09:00 06/19/09 17:58
bis(2-Chloroethyl) ether
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
bis(2-Chloroisopropyl) ether
ND ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
2-Chloronaphthalene
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
2-Chlorophenol
NO ug1L
7.1
1
06/12/09 09:00 06/19/09 17:58
4-Chlorophenylphenyl ether
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
Chrysene
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
Dibenz(a,h)anthracene
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
3,3'-DiChlorobenzidine
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
2,4-Dichlorophenol
ND ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
Diethylphthalate
ND ug/L
7A
1
06/12/09 09:00 06/19/09 17:58
2,4-Dimethylphenol
ND ug/L
14,3
1
06/12/09 09:00 06/19/09 17:58
Dimethylphihalate
ND ug)L
71
1
W12109 09:00 06/19/09 17:58
Di-n-butylphthalate
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
4,6-Dinitro-2-methylphenol
ND ug/L
28.6
1
06/12/09 09:00 06/19/09 17:58
2,4-Dinitrophenol
NO ug/L
71.4
1
06/12/09 09:00 06/19/09 17:58
2,4-Dinitrotoluene
ND ug/L
7.1
1
05112/0909:00 06119/091T58
2,6-Dinitrotoluene
ND ug1L
7.1
1
06/12/09 09:00 06/19109 17:58
Di-n-octylphthalate
NO ug/L
Ti
1
06/12/09 09:00 06/19/09 17:58
1,2-Diphenylhydrazine
NO ug/L
7.1
1
06/1210909:00 06/1910917:58
bis(2-Ethylhexyl)phthalate
NO ug/L
7.1
1
06/12/09 09:00 05/19/09 17:58
Fluoranihene
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
Fluorene
ND ug/L
7A
1
06/12/09 09:00 06/19/09 17:58
Hexachloro-1,3-butadiene
ND ug/L
71
1
06/12/09 09:00 06/19/09 17:58
Hexachlorobenzene
NO ug1L
71
1
06/12/09 09:00 06/19/09 17:58
Hexachlorocyclopentadiene
NO ug/L
14.3
1
06/12/09 09:00 06/19/09 17:58
Hexachloroethane
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17;58
Indeno(1,2,3-cd)pyrene
NO ug/L
7.1
1
06/1210909:00 06119/0917:58
Isophorone
NO ug/L
14.3
1
06/12/09 09:00 06/19/09 17:58
Naphthalene
ND ug1L
7.1
1
06/12/09 09:00 06/19/09 17:58
Nitrobenzene
ND ug/L
7.1
1
06/12/09 09:00 06119/09 17:58
2-Nitrophenol
NO ug/L
7.1
1
06112109 09:00 06/19/09 17:58
4-NitrophenDI
NO ug/L
71 A
1
06/12/09 09:00 06119f09 17:58
N-Nitrosodimethyla mine
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
N-Nitroso-di-n-propylamine
NO ug/L
7.1
1
06/12/09 09:00 06/19/09 17:58
N-Nitrosodiphenylamine
ND ug/L
14.3
1
06/12/09 09:00 06/19109 17:58
Date: 06/30/2009 10:32 AM
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
without the written consent of Pace Analytical
Services. Inc..
CAS No,
208-96-8
120-12-7
92-87-5
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
101-55-3
85-68-7
59-50-7
111-91-1
111-44.4
108-60-1
91-58-7
95-57-8
7005-72.3
218-01-9
53-70-3
91-94-1
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-94-0
122-66-7
117-81-7
206-4-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-20-3
98-95-3
88-75-5
100-02-7
62-75-9
621-64-7
86.30-6
[phone]
Qual
Page 4 of 34

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
C2AIJa1yt�Cd' ! 2225 Riverside DL 9800 Kincey Ave. Suite 100
�, � Asheville, NC 28804 Huntersville, NC 28078
f [phone] [phone]
ANALYTICAL RESULTS
Project: 09065-7
Pace Project No.: 9245998
Sample: 09065-7.1
Parameters
Lab ID: 9245998001
Results Units
Collected: 06/05/09 06:30
Report Limit OF
Received: 06/08/09 15:00 Matrix: Water
Prepared Analyzed CAS No. Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Pentachlorophenol
NO ug1L
35.7
1
06112/09 09:00
06/19/09 17:58
87-86-5
Phenanthrene
NO uglL
7.1
1
06/12109 09:00
06/19/09 17:58
85-01-8
Phenol
NO ug1L
7.1
1
06112J09 09:00
06/19/09 17:58
108-95-2
Pyrene
NO ug1L
7.1
1
06/12109 09:00
06/19/09 iT58
129-00-0
1,2,4-Trichiorobenzene
ND uglL
7.1
1
06112/0909:00
0611910917:58
120-82-1
2,4,6-Trichlorophenol
ND ug1L
14.3
1
06/12/09 09:00
06/19/09 17:58
88-06-2
NitrobenzeneA5 (S)
60 %
1D-120
1
D6112109 09:00
06/19/09 17:58
4165-60-0
2-Fluorobiphenyl (S)
75 %
15-120
1
06/12/09 09:00
06119/D9 17:58
321-60.8
Terphenyl-d14(S)
60 %
11-131
1
06/12/09 09:00
0611910917:58
1718-51-0
Phenol-d6 (S)
27 %
10-120
1
06/12/09 09:00
06/19/09 17:58
13127-88-3
2-F'luorophenol (S)
28 %
10-120
1
06/12/09 09:00
06/19/09 17:58
367-12-4
2,4,6-Tribromophenol (S)
26 %
10-137
1
06112/09 09:00
06/19/09 17:58
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Acrolein
NO uglL
100
1
06/14/09 20:10
107-02-8
Acrylonitrile
NO uglL
100
1
06/14/09 20:10
107-13-1
Benzene
NO ug1L
5.0
1
06/14/09 20:10
71-43-2
Bromodichloromethane
NO ug1L
5.0
1
06/14/09 20:10
75-274
Bromoform
NO ug1L
5.0
1
06/14/09 20:10
75-25-2
Bromomethane
NO ug1L
10.0
1
06/14/09 20:10
74-83-9
Carbon tetrachloride
NO ug1L
5.0
1
06/14/09 20:10
56-23-5
Chlorobenzene
NO ug1L
5.0
1
06/14/09 20:10
108-90-7
Chloroethane
ND ug1L
10.0
1
06/14/09 20:10
75-00-3
2-Chloroethylvinyl ether
ND ug1L
10.0
1
06/14/09 20:10
110-75-8
Chloroform
ND uglL
5.0
1
06/14/09 20:10
67-66-3
Chloromethane
NO uglL
5.0
1
06/14109 20:10
74-87-3
Dibromochloromethane
NO ug1L
&0
1
06/14109 20:10
124-48-1
12-Dichlorobenzene
NO ug1L
5.0
1
06/14/09 20:10
95-50-1
1,3-Dichlorobenzene
NO ug1L
5.0
1
06/1410920:10
541-73-1
1,4-Dichlorobenzene
NO ug1L
5.0
1
06/14/09 20:10
10646-7
1,1-Dichloroethane
NO uglL
5.0
1
0611410920:10
75-34-3
1,2-1)ichloroethane
NO ug1L
5.0
1
06/14/09 20:10
107-06-2
1,1-Dichloroethene
ND uglL
5.0
1
06/1410920:10
75-35-4
trans-1,2-Dichloroethene
ND ug1L
5.0
1
06/14/09 20:10
156-60-5
1,2-Dichloropropane
N❑ ug/L
5.0
1
06/1410920:10
78-87-5
cis-1,3-Dichloropropene
ND ug1L
5.0
1
06/1410920:10
10061-01-5
trans-1,3-Dichloropropene
NO ug1L
5.0
1
0611410920:10
10061-02-6
Ethylbenzene
NO ug1L
5.0
1
06/14/09 20:10
100-41-4
Nexachloro-1,3-butadiene
NO ug1L
5.0
1
06/14/09 20:10
87-68-3
Methylene Chloride
NO uglL
5.0
1
06/14/09 20:10
75-09-2
Naphthalene
ND ug11-
5.0
1
06/14/09 20:10
91-20-3
1,1,2,2-Tetrachloroethane
ND ug1L
5.0
1
06114/0920:10
79-34.5
Tetrachloroethene
ND ug1L
5.0
1
06/14/09 20:10
127-184
Toluene
ND uglL
5.0
1
06/14/09 20:10
108-88-3
1,1,1-Trichloroethane
NO ug1L
5.0
1
0611410920:10
71-55-6
1,1,2-Trichloroethane
ND ug1L
5.0
1
06/1410920:10
79-00-5
Trichloroethene
NO u911-
5.0
1
06114/0920:10
79-01-6
Date: 06/30/2009 10:32 AM
REPORT OF
LABORATORY ANALYSIS
Page 5 of 34
This report shall not be reproduced, except in
full,
without the written consent of Pace Analytical
Services,
Inc..

ceAnalytrcal
www.paoeleDaoam
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 28804
ANALYTICAL RESULTS
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 09065-7
Pace Project No.: 9245998
Sample: 09065-7.1 Lab ID: 9245998001 Collected: 06105/09 06:30 Received: 06/08/09 15:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua!
624 Volatile Organics Analytical Method: EPA 624
Vinyl chloride
ND ug/L
5.0 1
06/14/09 20:10 75-014
Dibf0M0flt30r0methane (S)
107 %
88-113 1
06/14/09 20:10 1868-53-7
4-Bromofluorobenzene (S)
99 %
86-111 1
06114/09 20:10 460-00-4
Toluene-d8 (S)
97 %
92-105 1
06/14/09 20:10 2037-26-5
1,2-Dichloroethane-d4(S)
97 %
70-130 1
06/14/0920:10 17060-07-0
420.4 Phenolics, Total Analytical Method: EPA 420A
Phenol NO mg/L 0.010 1 06/17/09 15:37 108-95-2 MO
450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg1L 0,0050 1 06/16/09 1 BA0 57-12-5
Sample: 09066-7.2 Lab ID: 9245998002 Collected: 06/05/09 06:30 Received: 06/08/09 15:00 Matrix: Water
Parameters Results Units Report Limrt OF Prepared Analyzed
608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3535
CAS No. Qual
Aldrin
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 14:09 309-00-2
alpha-BHC
NO ug/L
0,050
1
06/11/09 09:00
06/23/09 14:09
319-84-6
beta-BHC
NO ug/L
0.050
1
06/11/09 09:00
06/2310914:09
319-85-7
delta-BHC
ND ug/L
0,050
1
06/11/09 09:00
-06123109 14:09
319-86-8
gamma-BHC(Lindane)
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 14:09
58-89-9
Chlordane (Technical)
NO ug/L
0.50
1
06/11/09 09:00
06/23/09 14:09
57-74-9
4,4'-DDD
NO ug/L
0.050
1
06/11/09 09:00
G6123109 14:09
72-54-8
4,4'-ODE
NO ug/L
0.050
1
06/11/09 09:00
06/23109 14:09
72-55-9
4,4'-DDT
NO ug/L
0.050
1
0611110909:00
0612310914:09
50-29-3
Dieldrin
NO ug/L
0,050
1
06/11/09 09:00
06/23/09 14:09
60-57-1
Endosutfan I
ND ug/L
0.050
1
06/11/09 09:00
06/23/09 14:09
959-98-8
Endosulfan II
ND ug1L
0.050
1
06/11/09 09:00
06/23/09 14:09
33213-65-9
Endosulfan sulfate
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 14:09
1031-07-8
Endrin
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 14:09
72-20-8
Endrin aldehyde
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 14:09
7421-93-4
Heptachlor
ND ug/L
0.050
1
06/11/09 09:00
06/2310914:09
76-44-8
Heptachlor epoxide
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 14:09
1024-57-3
PCB-1016 (Aroclor 1016)
NO ug1L
0.50
1
06/11/09 09:00
06/23/09 14:09
12674-11-2
PCB-1221 (Aroclor 1221)
NO ug1L
0.50
1
06111/0909:00
06/23/09 14:09
11104-28-2
PCB-1232 (Aroclor 1232)
ND ug1L
0.50
1
06/11109 09:00
06/23/09 14:09
11141-16-5
PCB-1242 (Aroclor 1242)
NO ug/L
0.50
1
06111/0909:00
06/23/09 14709
53469-21-9
PCB-1248 (Aroclor 1248)
NO ug/L
0.50
1
06/11/09 09:00
06/23/09 14:09
12672-29-6
PCB-1254 (Aroclor 1254)
NO ug/L
0.50
1
06/11/09 09:00
06/23/09 14:09
11097-69-1
PCB-1260 (Aroclor 1260)
NO ug/L
0.50
1
06/11/09 09:00
06/23/09 14.09
11096-82-5
Toxaphene
NO ug/L
0.50
1
06/11/09 09:00
06/23/09 14:09
8001-35-2
Tetrachloro-m-xylene (S)
46 %
20-110
1
06111/09 09:00
06/23/09 14:09
877-09-8
Decachlorobiphenyl (S)
36 %
20-138
1
06/11/09 09:00
06/23/09 14:09
2051-24-3
Date: 06/30/2009 10:32 AM
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in lull,
without the written consent of Pace Analytical Services, Inc..
. •4cav
Page 6 of 34

aceAnalwical
www.pa0elsba. 0 n
I
Pace Analytical Services, Inc.
2225 Riverside Dr.
Ashevilie, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Project: 09065-7
Pace Project No.: 9245998
Sample: 09066-7.2 Lab ID: 9245998002 Collected: 06/05/09 06:30 Received: 06/08/09 15:00 Matrix: Water
[phone]
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Antimony
NO uglL
5.0
1
06111/09 15:18 06/13/0913:44
7440-36-0
Arsenic
NO ug/L
5.0
1
06111109 15:18 06/13/09 13:44
7440-38-2
Beryllium
ND ug/L
1.0
1
06/111091518 06/1310913:44
7440-41-7
Cadmium
NO ug/L
1.0
1
06/11/09 15:18 06/13/0913:44
7440-43-9
Chromium
NO uglL
5.0
1
06/11/09 15:18 0611310913:44
744047-3
Copper
ND ug/L
5.0
1
06/11/09 15:18 0611310913:44
7440-50.8
Lead
ND ug/L
5.0
1
06/11/09 15:18 06113/0913:44
7439-92-1
Nickel
NO ug1L
5.0
1
06111/091518 05/131091344
7440-02-0
Selenium
NO ug/L
10.0
1
06/11/09 15:18 0611310913:44
7782-49-2
Silver
ND ug/L
5.0
1
06/11/09 15:18 0611310913:44
7440-22-4
Thallium
NO ug/L
10.0
1
06/1110915:18 06/13/09 13:44
7440-28-0
Zinc
ND ug/L
10.0
1
06111/0915:18 06/13/091144
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1 Preparation Method: EPA
245.1
Mercury
NO ug/L
0.20
1
06118/09 09:45 06/18/09 13:19
7439-97-6
625 MSSV
Analytical Method: EPA 625
Preparation Method: EPA 625
Acenaphlhylene
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
208-96.8
Anthracene
ND ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
120-12-7
Benzidine
ND ug/L
66.7
1
06/12/09 09:00 06/24/09 22:40
92-87-5
Benzo(a)anthracene
ND ug/L
6.7
1
06/12/09 09:00 06/24/09 22A0
56-55-3
Benzo(a)pyrene
NO ug/L
6.7
1
05/12/09 09:00 06/24/09 22:40
50-32-8
Benzo(b)fluoranthene
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22A0
205-99-2
Benzo(g,h,i)perylene
ND ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
191-24-2
Benzo(k)fluoranthene
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22A0
207-08-9
4-Bromophenylphenyl ether
NO ug1L
6.7
1
06/12109 09:00 06/24/09 22:40
101-55-3
Butylbenzylphthalate
ND uglL
6.7
1
06/12/09 09:00 06/24/09 22:40
85-68-7
4-Chloro-3-methyiphenol
NO ug1L
6.7
1
06/12/09 09:00 06/24/09 22:40
59-50-7
bis(2-Chloroethoxy)methane
NO ug/L
13.3
1
06/12/09 09:00 06/24/09 22:40
111-91-1
bis(2-Chloroethyl) ether
NO ug/L
6,7
1
06/12/09 09:00 06/24/09 22:40
111-444
bis(2-Chloroisopropyl) ether
NO ug/L
6.7
1
06/12/09 09:00 06/24109 22A0
108-60-1
2-Chloronaphthalene
NO ug1L
6.7
1
06/12/09 09:00 06/24/09 22:40
91-58-7
2-Chlorophenol
ND ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
95-57-8
4-Chlorophenylphenyl ether
NO ug/L
6.7
1
05/12/09 09:00 06/24/09 22:40
7005-72-3
Chrysene
ND ug/L
6.7
1
06/12/09 09-00 06/24109 22:40
218-01-9
Dibenz(a,h)anthracene
ND ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
53-70-3
3,3'-Dichlorobenzidine
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
91-94-1
2,4-Dichlorophenol
NO uglL
6.7
1
06/12/09 09:00 06124109 22:40
120-83-2
Diethylphtha late
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
84-66-2
2,4-Dimethylphenot
NO ug/L
13.3
1
06/12/09 09:00 06/24/09 22:40
105-07-9
Dimethylphthalate
ND ug/L
6.7
1
06/12/09 09:00 06/24/09 22A0
131.11-3
Di-n-butylphthalate
NO ug1L
6.7
1
06112/09 09:00 06/24/09 22:40
64-74-2
4,6-Dinitro-2-methylphenol
NO ug/L
26.7
1
06/12/09 09:00 06/24/09 22A0
534-52-1
2,4-0initrophenol
NO ug/L
66.7
1
06/12109 09:00 06/24/09 22:40
51.28-5
2,4-Dinitrotoluene
NO ug/L
6.7
1
06M2109 09:00 06/24/09 22:40
121-14-2
2,6-Dinilrotoluene
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22A0
606-20-2
Dale: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS Page 7 of 34
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAl IXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
ww pocekftcom Asheville, NC 28804 Huntersville, NC 28078
(VIP )'CA -7175 [phone]
i
ANALYTICAL RESULTS
Project: 09065-7
Pace Project No.: 9245998
Sample: 09065-7.2
Parameters
Lab ID: 9245998002 Collected: 06/05/0906:30
Results Units Report Limit OF
Received: 0610810915:00 Matrix: Water
Prepared Analyzed CAS No. Qual
625 MSSV
Analytical Method: EPA625
Preparation Method: EPA625
Di-n-octylphthalate
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
117-84-0
1,2-Diphenylhydrazine
ND ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
122.66-7
bis(2-Ethylhexyl)phthalate
ND ug/L
6.7
1
06/12/09 09:00 06/24/09 22A0
117-81-7
Fluoranthene
NO ug/L
6.7
1
06/12/09 09:00 06124/09 22:40
206-44-0
Fluorene
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
86-73-7
Hexachloro-1.3-butadiene
NO ug/L
6.7
1
06112/09 09:00 06/24/09 22:40
87-68-3
Hexachlorobenzene
NO uglL
6.7
1
06112/09 09:00 06/24/09 22A0
118-74-1
Hexachlorocyclopentadiene
NO ug/L
13.3
1
06/12/09 09:00 06/24/09 22A0
77-474
Hexachloroethane
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22A0
67-72-1
Indeno(1,2,3-cd)pyrene
NO ug/L
6.7
1
06112109 09:00 06/24109 22740
193-39-5
Isophorone
NO ug/L
13.3
1
06/12/09 09700 06/24/09 22:40
78.59-1
Naphthalene
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
91-20-3
Nitrobenzene
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
98-95-3
2-Nitrophenol
NO ug/L
6.7
1
W12109 09:00 06/24/09 22:40
88.75-5
4-Nitrophenol
NO ug/L
66.7
1
06/12/09 09:00 06/24/09 22:40
100-02-7
N-Nitrosodimethylamine
NO ug/L
6.7
1
06/12/09 09'.00 06/24/09 22:40
62-75-9
N-Nitroso-di-n-propylamine
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
621-64-7
N-Nitrosodiphenylamine
NO uglL
13.3
1
06/12/09 09:00 06/24/09 22:40
86-30-6
Pentachlorophenol
NO ug/L
33.3
1
06/12/09 09:00 06/24/09 22:40
87-86-5
Phenanthrene
ND ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
8501-8
Phenol .
NO ug/L
6.7
1
06/12/09 09:00 D6124/09 22:40
108-95-2
Pyrene
NO ug/L
6.7
1
06/12/09 09:00 06/24/09 22A0
129-00-0
1,2.4-Trichlorobenzene
ND ug/L
6.7
1
06/12/09 09:00 06/24/09 22:40
120-82-1
2,4,6-Trichlorophenol
NO ug/L
13.3
1
06/12/09 09:00 06/24/09 22:40
88-06-2
Nitrobenzene-d5 (S)
42 %
10-120
1
06112/09 09:00 06/24/09 22:40
4165-60-0
2-Fluorobiphenyl (S)
46 %
15-120
1
D6/12109 09:00 06/24/09 22'A0
321-60-8
Terphenyl-d14 (S)
47 %
11-131
1
06/12/09 09:00 06/24/09 22:40
1718-51-0
Phenol-d6 (S)
20 %
10-120
1
06/12/09 09:00 06124109 22:40
13127-88-3
2-Fluorophenol (S)
28 %
10-120
1
06/12/09 09:00 06/24/09 22:40
367-124
2,4,6-Tfibromophenol (S)
55 %
10-137
1
06/12J09 09:00 06/24/09 22:40
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Acrolein
NO ug/L
100
1
06/14/09 20:57
107-02-8
Acrylonitrile
ND ug/L
100
1
06/14/09 20:57
107-13-1
Benzene
NO ug/L
5.0
1
06/14/09 20:57
71-43-2
Bromodichloromethane
ND ug/L
5.0
1
06/14/09 20:57
75-27-4
Bromotorm
ND ug/L
5.0
1
06/14/09 20:57
75-25-2
Bromomethane
NO ug/L
10.0
1
05/14/09 20:57
74-83-9
Carbon tetrachloride
NO ug/L
5.0
1
06/14/09 20:57
56-23-5
Chlorobenzene
NO ug/L
5.0
1
06/14/09 20:57
108-90-7
Chloroethane
NO ug/L
10.0
1
06/14/09 20:57
75-00-3
2-Chloroethylvinyl ether
ND ug/L
10.0
1
06114/09 20:57
110-75-8
Chloroform
ND ug/L
5.0
1
06/14/09 20:57
67-66-3
Chloromethane
NO ug/L
5.0
1
06114/09 20:57
74-87-3
Dibromochloromethane
NO ug/L
5.0
1
06/14/09 20:57
124-48-1
1,2-Dichlorobenzene
ND ug/L
5.0
1
06/14/09 20:57
95-50-1
1,3-Dichlorobenzene
ND ug/L
5.0
1
0611410920:57
541-73-1
Date: 06/3012009 10:32 AM
REPORT OF LABORATORY ANALYSIS
Page 8 of 34
This report shall not be reproduced, except in
full,
without the written consent of Pace Analytical
Services.
Inc..

9aceAnalyfical
www.pecarr
1
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunter5ville, NC 28078
[phone]
Project: 09065-7
Pace Project No.: 9245998
Sample: 09065.7.2 Lab ID: 9245998002 Collected: 06/05/09 06:30 Received: 06/08/09 15:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed GAS No, Qual
624 Volatile Organics Analytical Method: EPA 624
1,4-Dichlorobenzene
ND ug/L
5.0
1
06/14/09 20:57
106-46.7
1,1-Dichloroethane
NO ug/L
5.0
1
06/14/09 20:57
75-34-3
1,2-Dichloroethane
NO ug/L
5.0
1
06/14/09 20:57
107-06-2
1,1-Dichloroethene
NO ug/L
5.0
1
06/14109 20:57
75-35-4
trans- l,2-Dichloroethene
ND ug/L
5.0
1
06/14/09 20:57
156-60-5
1,2-Dichloropropane
NO ug1L
5.0
1
06/14/09 20:57
78-87-5
cis-1,3-Dichloropropene
NO ug/L
5.0
1
06/1410920:57
10061-01-5
trans- 1, 3-Dichloropropene
ND ug/L
5.0
1
06/14/09 20:57
10061-02-6
Ethylbenzene
ND ug/L
5.0
1
06/14/09 20:57
100-41-4
Hexachloro-1,3-butadiene
NO ug/L
5.0
1
06/14/09 20:57
87-68-3
Methylene Chloride
NO ug/L
5.0
1
06/14/09 20:57
75-09-2
Naphthalene
ND ug1L
5.0
1
06/14/09 20:57
91-20-3
1,1,2,2-Tetrachloroethane
ND uglL
5.0
1
06/14/09 20:57
79-34-5
Tetrachloroethene
ND ug/L
5.0
1
06/14/09 20:57
127-18-4
Toluene
NO ug/L
5.0
1
06/14/09 20:57
108-88-3
1, 1, 1 -Trichloroethane
NO ug/L
5.0
1
06/1410920:57
71.55-6
11,2-Trichloroethane
NO ug/L
5.0
1
06/14/09 20:57
79-00-5
Thchloroethene
NO ug/L
50
1
06/14/09 20:57
79-01-6
Vinyl chloride
NO ug/L
5.0
1
06/14/09 20:57
75-01-4
Dibromofluoromethane(S)
109 %
88-113
1
06/14/09 20:57
1M-53-7
4-Bromofluorobenzene (S)
100 %
86-111
1
06/14/09 20:57
460-00-4
Toluene-d8 (S)
98 %
92-105
1
06/14/09 20:57
2037-26-5
1,2-Dichloroethane-d4(S)
98 %
70-130
1
06/14/09 20:57
17060-07-0
420.4 Phenolics, Total Analytical Method: EPA 420A
Phenol 0.021 mg1L 0.010 1 06/17/0915:37 108-95-2 MO
450OCN£ Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide NO mg/L 0.0050 1 06/16/0918:41 57-12-5
Sample: 09065-7.3 Lab ID: 9245998003 Collected: 06/05/09 06:30 Received: 06/08/09 15:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3535
Alddn
NO ug/L
0.050
1
46111/09 09:00
06/23/09 14:24
309-00-2
alpha-BHC
NO ug/L
0.050
1
06/11/0909:00
06/23/0914:24
319-84-6
beta-BHC
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 14:24
319-85-7
delta-BHC
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 14:24
319-86-8
gamma-SHC(Lindane)
NO ug/L
0.050
1
06111/0909:00
06123/0914:24
58-89-9
Chlordane (Technical)
NO ugll-
0.50
1
06/11109 09:00
06/23/09 14:24
57-74-9
4,4`-DDD
NO ug/L
0.050
1
06/11/0909:00
0612310914:24
72-54-8
4,4'-DDE
NO ug/L
0.050
1
06111/09 09:00
06/23/09 14:24
72-55-9
4,4'-DDT
NO ug/L
0.050
1
06/11/09 09:00
06123/09 14:24
50-29-3
Dieldrin
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 14:24
60-57-1
Date: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS Page 9 of 34
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
N'.' "-u \s
yL !;

ceAnalytical
xnvxr.pacehibsmm
Project: 09065-7
Pace Project No.: 9245998
Sample: 09065-7.3
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 9245998003 Collected: 06/05/09 06:30 Received: 06/08/09 15:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
608 GCS Pesticides and PCSs Analytical Method: EPA608 Preparation Method: EPA 3535
Endosulfan I
NO ug/L
0.050
1
06111/0909:00
06123/0914:24
959-98-8
Endosulfan 11
NO ug/L
0.050
1
W11/09 09:00
06/23109 14;24
33213-65-9
Endosulfan sulfate
ND ug/L
0.050
1
06/11/09 09:00
06/23/09 14:24
1031-07-8
Endrin
NO ug/L
0.050
1
06111/0909:00
06123/0914:24
72-20-8
Endrin aldehyde
NO ug/L
0.050
1
06/11/09 09:00
06123/0914:24
7421.93-4
Heptachlor
NO ug1L
0.050
1
06111/0909:00
06/23/0914;24
76-44-8
Heptachlor epoxide
NO ug/L
0.050
1
06/11/09 09:00
06/23/09 14:24
1024-57-3
PCB-1016 (Aroclor 1016)
NO ug1L
0.5D
1
06111/09 09:00
06123/09 14:24
12674-11-2
PCB-1221 (Aroclor1221)
NO ug/L
0.50
1
06/11/09 09:00
06123/0914:24
11104-28-2
PCB-1232 (Aroclor 1232)
ND ug/L
0,50
1
06/11/09 09700
06/23/09 14:24
11141-16-5
PCB-1242 (Aroclor 1242)
NO ug/L
0.50
1
06/11/09 09:00
06/23/09 14:24
53469-21-9
PCB-1248 (Aroclor 1248)
NO ug/L
0.50
1
06/11/09 09:00
06/23109 14:24
12672-2M
PCB-1254 (Aroclor 1254)
NO ug/L
0,50
1
06/11/09 09:00
06/23/09 14:24
11097-69-1
PCB-1260 (Aroclor 1260)
NO ug/L
0.50
1
06/11/09 09:00
06/23/09 14:24
11096-82-5
Toxaphene
ND ug/L
0.50
1
06/11/09 09:00
06/23109 1424
8001-35-2
Tetrachloro-m-xylene (S)
52 %
20-110
1
06/11/09 09:00
06/23/09 14:24
877-09-8
Decachlorobiphenyl(8)
51 %
20-138
1
06/11/09 09:00
06/2310914:24
2051-24-3
200.7 MET ICP
Analytical Method: EPA 200.7
Preparation Method. EPA
200.7
Antimony
NO ug/L
5.0
1
06/1110915:18
0611310913:58
7440-36-0
Arsenic
NO ug/L
5.0
1
06/11/09 15:18
0611310913:58
7440-38-2
Beryllium
ND ug/L
1.0
1
06/11/09 15:18
06/13/09 13:58
7440-41-7
Cadmium
ND ug/L
1.0
1
06/11/09 15:18
06/13/09 13:58
7440-43-9
Chromium
NO ug/L
5.0
1
06111/09 15:18
06/13/09 13:58
7440-47-3
Copper
NO ug/L
5.0
1
06/11/09 15:18
06/1310913:58
7440-50-8
Lead
NO ug/L
5.0
1
06/11/09 15:18
06/13/09 13:58
7439-92-1
Nickel
NO ug/L
5.0
1
06/11/09 15:18
06/13/09 13:58
7440-02-0
Selenium
NO ug/L
10.0
1
06111/0915:18
06113/0913:58
7782-49-2
Silver
ND ug/L
5.0
1
06/11/09 15:18
06/13/09 13:58
7440-22-4
Thallium
NO ug/L
10A
1
06/11/09 15:18
06/13/09 13:58
7440-28-0
Zinc
22.2 ug/L
10.0
1
06/11109 15:18
06/13/09 13:58
7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1
Preparation Method: EPA
245.1
Mercury
ND uglL
0.20
1
06118/09 09:45
06/18/09 1128
7439-97.6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Aoenaphthylene
NO ug/L
6.0
1
06/12/09 09:00
06/24/09 23:05
208-96-B
Anthracene
NO ug/L
6.0
1
06/12/09 09:00
06/24/09 2105
120-12.7
Benzidine
NO ug1L
59.5
1
06/12/09 09:00
06/24/09 23:05
92-87-5
Benzo(a)anthracene
ND ug/L
6.0
1
06/12/09 09:00
06/24/09 23:05
56-55-3
Benzo(a)pyrene
NO ug/L
6.0
1
06/12/09 09:00
06/24/09 23705
50-32-8
13enzo(b)fluoranthene
ND ug/L
6.0
1
06112109 09:00
06/24/09 23:05
205-99.2
Benzo(g,hJ)perylene
NO ug/L
6.0
1
06/12/09 09:00
06/24/09 23:05
191-24-2
Benzo(k)fluoranthene
NO ug/L
&0
1
06/12/09 09:00
06/24/09 23:05
207-08-9
4-Bromophenylphenyl ether
ND ug1L
6.0
1
06/12/09 09:00
06124/09 23,05
101-55-3
Butylbenzylphthalate
NO ug1L
6.0
1
06/12/09 09:00
06/24/09 23:05
85-68-7
Date: 06/3012009 10'.32 AM REPORT OF LABORATORY ANALYSIS Page 10 of 34
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caAnalytical
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2225 Riverside Dr.
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ANALYTICAL RESULTS
[phone]
Pace Analytical Services, Inc.
9800 Kinr-ey Ave. Suite 100
Huntersvitle, NC 28078
[phone]
Project: 09065-7
Pace Project No.: 9245998
Sample: 09065.7.3 Lab lD: 9245998003 Collected: 06/05/09 06:30 Received: 06/08109 15:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
4-Chloro-3-methylphenol
ND ug1L
6.0
1
06/12/09 09:00 06124109 23:05
59-50-7
bis(2-Chloroethoxy)methane
ND ug1L
11.9
1
06/12/09 09:00 06/24/09 23:05
111-91-1
bis(2-Chloroethyt) ether
NO ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
10"0-1
2-Chloronaphthalene
NO ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
91-58-7
2-Chlorophenol
ND ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
95-57-8
4-Chiorophenylphenyl ether
NO ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
7005-72-3
Chrysene
NO ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
218-01-9
Dibenz(a.h)anthracene
ND ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
53-70-3
3,3'-Dichlorobenzidine
ND ug/L
5.0
1
06/12/09 09:00 06/24/09 23:05
91-94-1
2,4-Dichlorophenol
NO ug1L
6.0
1
06/12/09 09:00 06/24/09 23:05
120.83-2
Diethylphthalate
NO ug/L
6.0
1
061/2/09 09:00 06/24/09 23:05
84-66-2
2,4-Dimethylphenol
ND ug/L
11.9
1
06112109 09:00 06/24/09 23:05
105-67-9
Dimethylphthalate
ND ug1L
6.0
1
06/12/09 09:00 06/24/09 23:05
131-11-3
Di-n-butylphthalate
NO ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
64-74-2
4,6-Dinitro-2- methyl phenol
ND ug/L
23.8
1
06/12/09 09:00 06/24/09 23:05
534-52-1
2,4-Dinitrophenol
ND uglL
59.5
1
06/12/09 09:00 06/24/09 23:05
51-28-5
2,4-Dinitrotoluene
NO ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
121-14-2
2,6-Dinitrotoluene
ND ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
606-20-2
Di-n-octylphthalate
ND ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
117-84-0
1,2-Diphenylhydrazine
ND ug/L
6.0
1
0611210909:00 06124/0923:05
122-66-7
bis(2-Ethylhexyl)phthaiate
NO ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
117-81-7
Fiuoranthene
NO ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
206-44.0
Fluorene
NO ug/L
6.0
1
06/12109 09:00 06/24/09 23:05
W73-7
Hexachloro-1,3-butadiene
NO ug/L
6.0
1
06/1210909:00 06/2410923:05
87-68-3
Hexachlorobenzene
ND ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
118-74-1
Hexachlorocyclopentadiene
NO ug/L
11.9
1
06112J09 09:00 06/24/09 23:05
7747A
Hexachloroethane
ND ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
67-72-1
Indeno(1,2,3-cd)pyrene
NO ug/L
6.0
1
06/12/09 09M 06/24/09 23:05
193-39-5
Isophorone
NO ug/L
11.9
1
06/12/09 09:00 06/24/09 23:05
78-59-1
Naphthalene
ND ug/L
6.0
1
06/12109 09:00 06/24/09 23:05
91-20-3
Nitrobenzene
ND ug/L
6.0
1
06/12/09 D9:00 06/24109 23:05
98-95-3
2-Nitrophenol
ND uglL
6.0
1
06/12/09 09:00 06/24/09 23:05
88-75-5
4-Nitrophenol
ND ug)L
59.5
1
06/12/09 09:00 06/24/09 23:05
100-02-7
N-Nitrosodimethylamine
NO ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
62-75-9
N-Nitroso-di-n-propylamine
ND ug1L
6.0
1
06/12/09 09:00 06/24/09 2105
621-64-7
N-Nitrosodiphenylamine
NO ug/L
11.9
1
06/12/09 09:00 06/24/09 23:05
86-30-6
Pentachlorophenol
ND ug/L
29.8
1
06/12/09 09:00 06/24/09 23:05
87-86-5
Phenanthrene
ND ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
85-01-8
Phenol
ND ug/L
6.0
1
06/12/09 09:00 06/24/09 23:05
108-95-2
Pyrene
ND ug/L
6.0
1
06/12/09 09:00 06124109 23:05
129-00-0
12,4-Trichlorobenzene
ND ug/L
6.0
1
06/12109 09:00 06124/09 23:05
120-82-1
2,4,6-Trichlorophenol
ND ug/L
11.9
1
06/12/09 09:00 06/24/09 23:05
88-06-2
Nitrobenzene-d5 (S)
24 %
10-120
1
06/12/09 09:00 06/24/09 23:05
4165-60-0
2-Fluorobiphenyl(S)
29 %
15-120
1
06/12t0909:00 06/2410923:05
321-60-8
Terphenyl-014 (S)
30 %
11-131
1
06/12/09 09:00 06/24/09 23:05
1718-51-0
Phenol-d6 (S)
11 %
10-120
1
06112109 09:00 06/24/09 23:05
13127-88-3
Date: 06130/2009 10:32 AM REPORT OF LABORATORY ANALYSIS Page 11 of 34
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without the written consent of Pace Analytical Services, Inc-

Iekwlyfical
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Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28076
[phone]
Project. 09065-7
Pace Project No.: 9245998
Sample: 09065-7.3 Lab ID: 9245998003 Collected: 06/05/09 06:30 Received: 06/08/09 15:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual
625 MSSV Analytical Method: EPA625 Preparation Method: EPA625
2-Fluorophenol (S)
16 %
10-120
1
06/12/09 09:00 06124/09 23:05
367-12-4
2,4,6-Tribromophenol (S)
33 %
10-137
1
06/12/09 09:00 06/24/09 23:05
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Acrolein
NO ug/L
100
1
06/14/09 2111
107-02-a
Acrylonitrile
NO ug/L
100
1
06/14/09 21:21
107.13-1
Benzene
NO ug1L
5.0
1
06/14/09 21:21
7143-2
Bromodichloromethane
ND ug/L
5.0
1
06/14/09 21:21
75-274
BrOMDform
ND ug/L
5.0
1
06/14/09 21:21
75-25-2
Bromomethane
ND ug/L
10.0
1
06/14/09 21:21
74-83-9
Carbon tetrachloride
NO ug1L
5.0
1
06/14/09 21:21
56-23-5
Chlorobenzene
NO ug/L
5.0
1
06/14/09 21:21
108-90-7
Chloroethane
ND ug/L
10.0
1
06114/09 21:21
75-00-3
2-Chloroethylvinyl ether
NO ug1L
10.0
1
06Y14/09 21:21
110-75-8
Chloroform
ND uglL
5.0
1
06/14/09 21:21
67-66-3
Chloromethane
NO uglL
5.0
1
06/14/09 21:21
74-87-3
Dibromochloromethane
NO ug/L
5.0
1
06/14/09 21:21
12448-1
1,2-Dichiorobenzene
NO ug/L
5.0
1
06/14/09 21:21
95-50-1
1,3-Dichlorobenzene
NO ug/L
5.0
1
06/1410921:21
541-73-1
1,4-Dichlorobenzene
NO uglL
5.0
1
06/14/09 21:21
106-46-7
1, 1 -Dichloroethane
NO ug/L
5.0
1
06/14/09 21:21
75-34-3
1,2-Dichloroethane
ND ug/L
5.0
1
06/14/09 21:21
107-06-2
1,1-Oichloroethene
NO ug1L
5.0
1
06114/09 21 i21
75-35-4
trans-1,2-DicNoroethene
NO ug/L
5.0
1
06/1410921:21
156-60-5
1,2-Dichloropropane
NO u911-
5.0
1
06/1410921:21
78-87.5
cis-1,3-Dichloropropene
ND ug/L
5.0
1
0611410921:21
10061-01-5
trans-1,3-Dichloropropene
NO ug/L
5.0
1
06/14/09 21:21
10061-02-6
Ethylbenzene
NO ug/L
5.0
1
06114/09 2121
10041-4
Hexachloro-1,3-butadiene
NO ug/L
5.0
1
06/1410921:21
87-68-3
Methylene Chloride
ND ug/L
5.0
1
0611410921:21
75-09-2
Naphthalene
NO ug/L
5.0
1
06/14/09 21:21
91-20-3
1,1,2,2-Tetrachloroethane
NO ug/L
5.0
1
0611410921:21
79-34-5
Tetrachloroethene
ND ug/L
5.0
1
06/14/09 21:21
127-18-4
Toluene
NO ug/L
5.0
1
06/14/09 21:21
108-88-3
1, 1, 1 -Trichloroethane
NO ug/L
5.0
1
06/14/09 21:21
71-55-6
1 ,1 ,2-Trichloroethane
ND ug/L
5.0
1
06114/09 21:21
79-00-5
Trichloroethene
ND ug/L
5.0
1
06/14/09 21:21
79-01-6
Vinyl chloride
ND ug/L
5.0
1
06/14/09 21:21
75-01-4
Dibromofluoromethane (S)
107 %
88-113
1
06114/09'21:21
1868-53-7
4-Bromofluorobenzene (S)
99 %
86-111
1
06/14/09 21:21
460-004
Toluene-d8 (S)
98 %
92-105
1
06/14109 21:21
2037-26-5
1,2-Dichioroethane-d4 (S)
97 %
70-130
1
06/14/09 21:21
17060-07-0
420.4 Phenolics, Total
Analytical Method: EPA 420.4
Phenol
ND mg/L
0.010
1
06/17/09 16:27
108-95-2
Date: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS Page 12 of 34
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Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersviile, NC 28078
Pace Project No.: 9245998
Sample: 09065-7.3 Lab ID: 9245998003 Collected: 06/05/09 06:30 Received. 06/08/09 15:00 Matrix: Water
[phone]
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 0.0050 1
Date: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS
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06116/0918A2 57-12-5
Page 13 of 34

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Project. 09065-7
Pace Project No.: 9245998
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
OC Batch: MSVf7326 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 9245998002, 9246998003
METHOD BLANK: 294488
Associated Lab Samples:
Parameter
9245998002. 9245998003
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1,1-Trichloroethane
uglL
ND
5.0
06114/0911:50
1,1,2,2-Tetrachloroethane
ug1L
NO
5.0
06/14/09 11 : 50
1,1,2-Trichloroethane
ug1L
NO
5.0
06/14/0911-50
1,1-Dichloroethane
ug1L
NO
5.0
0611410911:50
1,1-Dichloroethene
ug1L
ND
5.0
0611410911:50
1,2-Dichlorobenzene
ug1L
ND
5.0
0611410911:50
12-Dichloroethane
ug1L
ND
5.0
06/14/09 11:50
1,2-Dichloropropane
ug1L
ND
5.0
06/1410911:50
1,3-Dichtorobenzene
uglL
NO
5.0
06/1410911:50
1,4-Dichlorobenzene
ug1L
ND
5.0
06114/0911:50
2-Chloroethylvinyl ether
ug1L
ND
10.0
06/14/09 11:50
Acrolein
ug1L
NO
100
0611410911:50
Acryionhrile
uglL
NO
100
06114/0911:50
Benzene
ug1L
ND
5.0
06114/09 11 :50
Bromodichloromethane
ug1L
NO
5.0
• 06/1410911:50
Bromoform
ug1L
NO
5.0
06/1410911:50
9romomethane
ug1L
NO
10.0
06/14/0911:50
Carbon tetrachloride
ug1L
NO
5.0
06/14/09 11:50
Chlofobenzene
ug1L
NO
5.0
06/14109 11 :50
Chloroethane
ug1L
ND
10.0
06/14/09 11:50
Chloroform
uglL
NO
5.0
06/1410911:50
Chloromethane
ugrL
NO
5.0
06/14/09 11:50
cis-1,3-Dichloropropene
ug1L
NO
5.0
06/14/09 11:50
Dibromochloromethane
ug1L
ND
5.0
06/14/09 11:50
Ethylbenzene
uglL
NO
5.0
06114/0911:50
Hexachloro-1,3-butadiene
ug1L
ND
5.0
06/14/09 11:50
Methylene Chloride
ug1L
7.2
5.0
06/14/09 11:50
Naphthalene
ug1L
NO
5.0
06/14/09 11:50
Tetrachloroethene
uglL
ND
5.0
0611410911:50
Toluene
ug1L
NO
5.0
06/14/09 11:50
trans-1,2-Dichloroethene
ug/L
NO
5.0
06/1410911:50
trans- l.3-Dichloropropene
ug/L
NO
5.0
0611410911:50
Trichlorcethene
uglL
NO
5.0
0611410911:50
Vinyl chloride
ug1L
ND
5.0
06/14/09 11:50
1,2-Dichloroethane-d4 (S)
%
92
70-130
05/14/09 11:50
4-Bromottuorobenzene (S)
%
106
86.111
06/14/09 11:50
Dibromofluoromethane (S)
%
98
88-113
06/14/09 11:50
Toluene-d8 (S)
%
98
92-105
06/14/09 11:50
Qualifiers
C9
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Date: 06/30/2009 1a32 AM REPORT OF LABORATORY ANALYSIS . Page 14 of 34
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w ti

,y • Pace Analytical Services, Inc.
Ice 2225 Riverside Dr.
MOcare Asheville, NC 28804
r [phone]
i
QUALITY CONTROL DATA
Project: 09065-7
Pace Project No.� 9245998
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 294489
Spike
Parameter Units Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1, 1, 1 -Trichloroethane
ug/L
20
24.6
123
52-162
1,1,2,2-Tetrachloroethane
uglL
20
23.5
118
46-157
11,2-Trichloroethane
ug/L
20
24A
122
52-150
1,1-Dichloroethane
ug/L
20
25.9
129
59-155
1,1-Dichloroethene
uglL
20
25.6
128
1-234
1,2-Dichlorobenzene
ug/L
20
23.9
119
18-190
1,2-Dichloroethane
ugJL
20
23.3
116
49-155
1,2-Dichloropropane
ug/L
20
25.6
128
1-210
1,3-Dichlorobenxene
ug/L
20
23.4
117
59-156
1,4-Dichlorobenzene
ug/L
20
25.6
128
18-190
2-Chloroethylvinyl ether
ug/L
40
45.2
113
1-305
Acrolein
uglt-
100
120
120
15-152
Acrylonitrile
ug/L
100
232
232
75-132 L3
Benzene
ug/L
20
25.0
125
37-151
Bromodichloromethane
ug/L
20
24.3
122
35-155
Bromoform
ug/L
20
24.9
125
45.169
Bromomethane
ug/L
20
30.3
152
1-242
Carbon tetrachloride
ug/L
20
25.5
127
70-140
Chlorobenzene
ug/L
20
23.4
117
37-160
Chloroethane
ug/L
20
25.2
126
14-230
Chloroform
ug/L
20
23.8
119
51-138
Chloromethane
ug/L
20
24.3
122
1-273
cis-1,3-Dichloropropene
ug/L
20
25.2
126
1-227
Dibromochloromethane
ug/L
20
23.4
117
53-149
Ethylbenzene
ug/L
20
24.7
123
37-162
Hexachloro-1,3-butadiene
ug/L
20
28A
140
70-130 L3
Methylene Chloride
ug/L
20
29.6
148
1-221
Naphthalene
uglL
20
26.4
132
70-130 SO
Tetrachloroethene
ug/L
20
27.7
138
64-148
Toluene
ug/L
20
24.3
122
47-150
trans-1,2-Dichloroethene
ug/L
20
24.2
121
54-156
trans-1,3-Dichioropropene
ug/L
20
25.2
126
17-183
Trichloroethene
ug/L
20
25.3
127
71-157
Vinyl chloride
ug/L
20
24.8
124
1-251
1,2-Dichloroethene-d4 (S)
%
91
70-130
4-BromoAuorobenzene (S)
%
108
86-111
Dibromofluaromethane (S)
%
96
88-113
Toluene-d8 (S)
%
99
92-105
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
294512
294513
MS
MSD
9245902001 Spike
Spike MS
MSD
MS MSD
% Rec
Parameter
Units
Result Cone.
Cone. Result
Result
% Rec % Rec
Limits RPD
1,1,1-Thchloroethane
ug/L
NO 20
20 24.5
22.9
123 114
46-171 7
1,1,2,2-Tetrachloroethane
ug/L
NO 20
20 22.6
22.1
113 111
73-159 2
1,1,2-Trichloroethane
ug/L
ND 20
20 23.5
22.3
118 112
64-152 5
1. 1 -Dichloroethane
ug/L
NO 20
20 26.1
24.8
131 124
43-172 5
Date: 06/30/2009 10:32 AM
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in full,
without the written consent
of Pace Analytical Services, Inc..
,. .ccova
Qua!
Page 15 of 34

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalyfical 2225 Riverside Dr. 9800 KlnceyAve. Suite 100
w,WWcom Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project. 09065-7
Pace Project No.: 9245998
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
294512
294513
MS
MSD
9245902001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,1-Dichloroethene
ug/L
ND
20
20
26.0
24.7
130
123
48-189
5
1,2-Dichlorobenzene
ug/L
ND
20
20
23.2
22.4
116
112
54-154
3
1,2-Dichloroethane
ug/L
NO
20
20
23.3
21.6
117
108
42-171
8
1,2-Dichloropropane
ug/L
NO
20
20
25.4
24.1
127
121
55-157
5
1,3-Dichlorobenzene
ug/L
NO
20
20
23.2
22.4
116
112
57-148
4
1,4-Dichlorobenzene
ug/L
ND
20
20
25.4
24.0
127
120
58-149
5
2-Chloroethylvinyl ether
ug/L
NO
40
40
ND
NO
0
0
70.130
P5
Acrolein
ug/L
ND
100
100
116
108
116
108
70-130
7
Acrylonitrile
ug/L
NO
100
100
225
216
225
216
70-130
4 MO
Benzene
u911-
ND
20
20
24.5
23.1
123
116
54-163
6
Bromodichloromethane
ug/L
NO
20
20
23.9
22.9
119
114
56-152
4
Bromoform
uglL
ND
20
20
24.5
23.3
122
117
53-151
5
Bromomethane
ug/L
ND
20
20
33.0
30.4
165
152
10-200
8
Carbon tetrachloride
ug/L
NO
20
20
25.8
24.6
129
123
41-175
5
Chlorobenzene
ug/L
NO
20
20
22.7
21.7
114
108
67.152
5
Chloroethane
ug/L
NO
20
20
25.2
23.7
126
119
23-200
6
Chloroform
ug/t
ND
20
20
23.6
22.2
118
111
51-166
6
Chloromethane
ug1L
NO
20
20
22.8
21.7
114
109
40-175
5
cis- 1,3-Dichloropropene
ug/L
NO
20
20
24.4
23.3
122
116
38-146
5
Dibromochloromethane
ug/L
NO
20
20
22.6
21.9
113
110
65-144
3
Ethylbenzene
ug/L
ND
20
20
24.2
23.2
121
116
57-152
4
Hexachloro-1,3-butadiene
ug/L
ND
20
20
29.7
27.6
149
138
70-130
8 MD
Methyiene Chloride
ug/L
ND
20
20
24,6
23.8
118
114
40-167
3
Naphthalene
ug/L
ND
20
20
24.8
24.9
124
124
70-130
.3
Tetrachloroethene
ug/L
ND
20
20
27.3
26.3
137
132
59-155
4
Toluene
ug/L
NO
20
20
24.1
22.8
120
114
47-162
6
trans- 1,2-Dichloroethene
ug/L
ND
20
20
23.9
22.6
120
113
47.178
6
trans-1,3-Dichloropropene
uglL
NO
20
20
24.2
23.3
121
117
39-148
4
Trichloroethene
ug/L
NO
20
20
25.0
23.9
125
119
60-153
5
Vinyl chloride
u91L
NO
20
20
25.6
23.9
128
119
46-176
7
1,2-Dichloroethane-d4 (S)
%
93
94
70-130
4-Bromofluorobenzene (S)
%
106
108
86-111
Dibromofluoromethane (S)
%
96
96
88-113
Toluene-d8 (S)
%
100
100
92-105
Date: 06/30/2009 10:32 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fu!J.
without the written consent of Pace Analytical Services, Inc..
Page 16 of 34

10Analytical
www.Awwabs com
i
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
09065-7
Pace Project No.:
9245998
QC Batch.
WETA15288 Analysis Method: EPA 420.4
QC Batch Method:
EPA 420.4 Analysis Description: 420.4 Phenolics
Associated Lab Samples: 9245998001, 9245998002, 9245998003
METHOD BLANK: 295598 Matfix: Water
Associated Lab Samples: 9245998001, 9245998002. 9245998003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenol mg1L ND 0.010 0611710915:37
LABORATORY CONTROL SAMPLE: 295599
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phenol mg1L .25 0.26 102 90-110
MATRIX SPIKE SAMPLE:
295607
9245998001
Spike
MS
MS
°Ao Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Phenol
mg1L
ND
.25
0.21
83
90-110 MO
MATRIX SPIKE SAMPLE:
295608
9245998002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Phenol
mg1L
0.021
.25
0.23
83
90-110 MO
SAMPLE DUPLICATE: 295609
9245998003 Dup
Parameter Units Result Result RPD Qualifiers
Phenol mg1L ND ND
SAMPLE DUPLICATE. 295610
9246108001 Dup
Parameter Units Result Result RPD Qualifiers
Phenol mg1L ND ND
Date: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS
ThiS report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 17 of 34

ace Analyfical
www.Pa>xktabsmm
Project: 09065-7
Pace Project No.: 9245998
Pace Analytical Services, Inc.
2225 Riverside Or,
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: OEXTf7072 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 9245998001, 9245998002, 9245998003
METHOD BLANK: 293288 Matrix: Water
Associated Lab Samples: 9245998001, 9245998002, 9245998003
Blank Reporting
Parameter Units Result Limit
12,4-Trichlorobenzene
uglL
NO
1,2-Diphenylhydrazine
ug/L
NO
2,4.6-Thchlorophenol
uglL
NO
2,4-Dichlorophenol
u91L
ND
2,4-Dimethylphenol
uglL
NO
2,4-Dinitrophenol
uglL
ND
2,4-Dinitrototuene
uglL
ND
2,6-Dinitrotoluene
ug)L
ND
2-Chloronaphthalene
ug)L
ND
2-Chlorophenol
ug1L
NO
2-Nitrophenol
uglL
NO
3,3'-Dichlorobenzidine
ug/L
ND
4,6-Dinitro-2-methytphenol
ug/L
NO
4-Bromophenylphenyl ether
ug1L
NO
4-Chloro-3-methylphenol
ug/L
NO
4-Chlorophenylpheny) ether
ug/L
ND
4-Nitrophenol
ug1L
NO
Acenaphthylene
ug/L
NO
Anthracene
ug/L
NO
Benzidine
ug/L
NO
Benzo(a)anthracene
ug/L
NO
Benzo(a)pyrene
ug/L
NO
Benzo(b)fluoranthene
ug1L
NO
Benzo(g,h,i)perylene
ug/L
NO
Benzo(k)ftuoranthene
ug/L
NO
bis(2-Chloroethoxy)methane
ug/L
NO
bis(2-Chloroethyl) ether
ug1L
NO
bis(2-Chloroisopropyl) ether
ug/L
NO
bis(2-Ethylhexyl)phthalate
ug/L
NO
Butylbenzylphihalate
ug/L
ND
Chrysene
ug/L
NO
Di-n-butylphthalate
ug/L
NO
Di-n-octylphthalate
ug/L
NO
Dibenz(a,h)anthracene
ug/L
NO
Diethylphtha late
ug/L
NO
Dimethylphthalate
ug/L
NO
Fluoranthene
ug/L
NO
Fluorene
ug/L
NO
Hexachloro-1,3-btitadiene
ug/L
ND
Hexachlorobenzene
ug/L
ND
Hexachlorocyclopentadiene
ug/L
NO
Hexachloroethane
ug1L
NO
Indeno(1,2,3-ed)pyrene
ug/L
NO
Analyzed
5.0
06/1410912:49
5.0
06114/0912:49
10.0
0611410912749
5.0
06/14/09 12:49
10.0
06/14/0912:49
50.0
06/1410912:49
5.0
06/14/0912:49
5.0
06/14/09 12:49
5.0
06114/0912:49
5.0
06/14109 12:49
5.0
06/1410912:49
5.0
06/1410912A9
20.0
06/1410912:49
5.0
06/1410912:49
5.0
06/1410912:49
5.0
06114/0912:49
50.0
06/1410912:49
5.0
06114/0912:49
5.0
06/14/09 12:49
50.0
06/1410912:49
5.0
06114/0912:49
5.0
06114/0912:49
5.0
06114/09 12:49
5.0
06/1410912:49
5.0
06/1410912:49
10.0
06/14/0912:49
5.0
06/14/0912:49
5.0
06/14/0912:49
5.0
06/14109 12:49
5.0
06/14/0912:49
5.0
06114/0912:49
5.0
06/14/0912A9
5.0
06/1410912:49
5.0
06/14/0912:49
5.0
06/14/0912:49
5.0
06/14/0912:49
5.0
06/14/0912:49
5.0
06114/0912:49
5-0
06/14/0912:49
5.0
D6114109 12:49
10.0
06/14/0912:49
5.0
06/14109 12:49
5.0
06/14/0912:49
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Date: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS Page 18 of 34
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..

7c,
®
Pace Analytical Services, Inc.
' y
"10 '�' !
2225 Riverside Dr.
WWW'Pqc0AAbk&ooM
Asheville, NC 28804
1
[phone]
QUALITY CONTROL DATA
Project: 09065-7
Pace Project No.: 9245998
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 104
Huntersville, NC 28078
METHOD BLANK: 293288
Matrix:
Water
Associated Lab Samples:
9245998001, 9245998002, 9245998003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Isophorone
ug/L
ND
10.0
0611410912:49
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
06114/0912:49
N-Nitrosodlmethylamine
ug/L
NO
5.0
0611410912:49
N-Nitrosodiphenylamine
ug/L
NO
10.0
06114/0912:49
Naphthalene
ug/L
NO
5.0
06/1410912:49
Nitrobenzene
ug/L
NO
5.0
06/1410912:49
Pentachlorophenol
ug/L
NO
25.0
06/14/0912.49
Phenanthrene
ug1L
NO
5.0
06/14/0912:49
Phenol
ug/L
NO
5.0
06/14/0912A9
Pyrene
ug1L
NO
5.0
06/14/0912:49
2,4,6-Tdbromophenol (S)
%
88
10-137
06114/09 12:49
2-Fluorobiphenyl (S)
%
58
15-120
06/14/09 12:49
2-Fluorophenol (S)
%
85
10-120
06/14/09 12:49
Nitrobenzene-d5 (S)
%
50
10-120
06/14/09 12:49
Phenol-d6 (S)
%
86
10-120
06/14/09 12:49
Terphenyl-04 (S)
%
83
11-131
06/14/09 12A9
LABORATORY CONTROL SAMPLE: 293289
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
Rec Limits
Qualifiers
1,2,4-Trichlorobenzene
ug1L
50
29.5
59
44-142
1,2-Diphenylhydrazine
uglL
50
20.4
41
25-150
2,4,6-Trichlorophenol
uglL
50
26.1
52
37-144
2,4-Dichlorophenol
ug1L
50
35.9
72
1-191
2,4-Dimethylphenol
ug1L
50
28.8
58
32-119
2,4-Dlnitrophenol
ug1L
50
47.11
94
1-181
2,4-Dinitrotoluene
ug)L
50
33.0
fib
39-139
2,6-Dinitrotoluene
uglL
50
40.0
80
50.158
2-Chloronaphihalene
ug1L
50
31.0
62
60-118
2-Chiorophenol
ug/L
50
41.6
83
23-134
2-Nitrophenol
ug/L
50
33.6
67
29-182
3,3'-Dichiorobenzidine
ug/L
50
49.3
99
1.262
4,6-Dinitro-2-methylphenol
ug/L
50
30.2
60
1-181
4-9romophenylphenyl ether
ug/L
50
39.9
80
53-127
4-Chi oro-3-methylphenol
ug/L
50
33.7
67
22-147
4-Chiorophenylphenyl ether
ug/L
50
25.8
52
25-158
4-Nitrophenol
ug1L
50
31.73
63
1-132
Acenaphthy)ene
ug/L
50
42.8
86
33-145
Anthracene
ug/L
50
35.1
70
1-166
Benzidine
ug]L
50
ND
94
25-150
Benzo(a)anthracene
ug/L
50
42.0
84
33-143
Benzo(a)pyrene
ug/L
50
35.5
71
17-163
Senzo(b)fluoranthene
ug1L
50
30.7
61
24-159
Benzo(g,h,i)perylene
ug/L
50
55.6
111
1-219
Benzo(k)fluoranthene
ug1L
50
29.6
59
11-162
Date: 06/30/2009 10:32 AM
REPORT OF LABORATORY ANALYSIS
This report Shall
not
he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,.
[phone]
Page 19 of 34

IeAnalytical
s+h+'.Awdiib&ccm
Project: 09065-7
Pace Project No.: 9245998
LABORATORY CONTROL SAMPLE: 293289
Parameter
bis(2-Chloroelhoxy)methene
ug/L
bis(2-Chloroethyl) ether
ug/L
bis(2-Chloroisopropyl) ether
ug/L
bis(2-Ethylhexyl)phthalate
ug/L
Butylbertzylphthalate
ug/L
Chrysene
ug/L
Di-n-butylphthalate
ug1L
Di-n-octylphthalate
ug1L
Dibenz(a,h)anthracene
ug/L
Diethylphthalate
ug/L
Dimethylphthalate
ug/L
Ftuoranthene
ug/L
Fluorene
ug/L
Hexachloro-1,3-butadiene
ug/L
Hexachlorobenzene
ug/L
Hexachiorocyciopentadiene
ug/L
Hexachloroethane
ug/L
Indeno(1,2,3-cd)py(ene
ug1L
Isophorone
ug/L
N-Nitroso-di-n-propylamine
ug/L
N-Nitrosodimethylamine
ug/L
N-Nitrosodiphenylamine
ug/L
Naphthalene
ug/L
Nitrobenzene
ug/L
Pentachlorophenol
ug/L
Phenanthrene
ug/L
Phenol
ug/L
Pyrene
ug/L
2,4,6-Tribromophenol (S)
°%
2-Fluorobiphenyl (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike
Units Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
50
27.8
56
33-184
50
43.1
86
12-158
50
32.5
65
36-166
50
30.4
61
8-158
50
32.5
65
1-152
50
29.6
59
17-168
50
24.9
50
1-118
50
22.6
45
4-146
50
55.5
111
1-227
50
32.3
65
1-114
50
6.7
13
1-112
50
31.3
63
26-137
50
39.2
78
59-121
50
29.3
59
24-116
50
45.3
91
1-152
50
36.5
73
25-150
50
31.4
63
40-113
50
50.0
100
1-171
50
23.3
47
21-196
50
35.5
71
1-230
50
39.4
79
25-150
50
37,6
75
25-150
50
25.7
51
21-133
50
23.0
46
35-180
50
47.0
94
14-176
50
35.1
70
54-120
50
31.0
62
5-112
50
45.2
90
52-115
104
10-137
56
15-120
84
10-120
48
10.120
85
10-120
80
11.131
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 293290
293291
MS
MSD
9245958002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
°% Rec
% Rec
Limits
RPD Qua]
12,4-Trichlorobenzene
ug/L
ND
111
111
53.1
72.8
48
65
44-142
31 R1
1,2-Diphenythydrazine
ug/L
ND
111
111
40.2
49.4
36
44
25-150
21
2,4,6-Trichlorophenol
uglL
ND
111
Ill
45.0
57.5
41
52
37-144
24
2,4-Dichlorophenol
ug1L
ND
111
111
89.4
48.5
80
44
1-191
59 R1
2,4-Dimethylphenol
ug/L
ND
111
111
64.2
44.8
58
40
32.119
36 R1
2,4-Dinitrophenol
ug/L
ND
111
111
ND
26J
17
23
1-181
2,4-Dinitrotoluene
ug/L
ND
11t
111
115
55.4
104
50
39-139
70 RI
2,6-Dinitrotoluene
ug/L
ND
111
111
73.9
91.7
66
82
50-158
21
Date: 06/30/2009 10:32 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in toll,
without the written consent of Pace Analytical Services, Inc..
Page 20 of 34

e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
1ceAnal*al 2225 Riverside (7r. 9800 Kincey Ave, Suite 100
W,w, Asheville, NC 28804 Huntersville, NC 28078
1 [phone] [phone]
QUALITY CONTROL DATA
Project: 09065-7
Pace Project No.: 9245998
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 293290
9245958002
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
293291
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
2-Chloronaphthalene
ug1L
NO
111
ill
97.6
82.3
88
74
60-118
17
2-Chlorophenol
ug1L
NO
ill
ill
51.3
55.7
46
50
23-134
8
2-Nitrophenol
ug1L
NO
ill
ill
55.9
62.8
50
57
29-182
12
3,3'-Dichlorobenzidine
ug/L
NO
111
ill
40.0
59.3
36
53
1.262
39 R1
4,6-Dinitro-2-methylphenol
ug/L
NO
ill
111
31.4J
37.7J
28
34
1-181
4-Bromophenylphenyl ether
ug/L
NO
111
ill
70.2
84.5
63
76
53-127
18
4-Chloro-3-methylphenol
ug/L
NO
ill
ill
40.4
51.0
36
46
22-147
23
4-Chlorophenylphenyl ether
ug/L
NO
ill
117
50.5
64.5
46
58
25-158
24
4-Nitrophenol
ug/L
NO
ill
ill
58.4.1
73.9J
53
66
1-132
Acenaphthylene
u91L
ND
ill
ill
45.8
55.9
41
50
33-145
20
Anthracene
ug/L
ND
ill
ill
45.7
57.1
41
51
1-166
22
Benzidine
ug/L
NO
ill
111
NO
ND
69
76
25-150
Benzo(a)anthracene
uglL
NO
ill
ill
42.0
53.3
38
48
33-143
24
Benzo(a)pyrene
ug/L
ND
111
ill
41,5
54.8
37
49
17-163
28
Benzo(b)fluoranthene
ug/L
ND
ill
111
36.3
48.1
33
43
24-159
28
Benzo(g,h,i)perylene
ug/L
NO
111
ill
40.3
49.0
36
44
1.219
20
Senzo(k)fluoranthene
ug1L
ND
ill
ill
37,1
49.1
33
44
11-162
28
bis(2-Chloroethoxy)methane
ug1L
NO
ill
ill
64.5
49.4
58
44
33-184
27
bis(2-Chloroethyl)ether
ug/L
NO
111
ill
55.4
67,0
50
60
12-158
19
bis(2-Chloroisopropyl) ether
ug1L
NO
ill
ill
50A
55.3
45
50
36-166
9
bis(2-Ethylhexyl)phthalate
ug/L
NO
ill
111
40.1
51.8
36
47
8-158
25
Butylbenzylphthalate
ug/L
NO
ill
ill
38.7
49.8
35
45
1-152
25
Chrysene
ug1L
ND
ill
111
42.0
53.5
38
48
17-168
24
Di-n-butylphthalale
ug1L
NO
ill
ill
40.3
51.0
36
46
1-118
23
Di-n-octylphthalate
ug/L
ND
ill
ill
37.9
48.4
34
44
4-146
24
Dibenz(a,h)anthracene
ug/L
ND
ill
111
39.5
49.0
36
44
1-227
21
Diethylphthalate
ug1L
NO
ill
ill
39.8
51.6
36
46
1-114
26
Dimethylphthalate
uglL
ND
ill
ill
41.5
52.7
37
47
1-112
24
Fluoranthene
ug/L
NO
ill
ill
45.6
57.6
41
52
26-137
23
Fluorene.
ug1L
ND
ill
ill
59.8
58.7
54
53
59-121
2 MO
Hexachtoro-1,3-butadiene
ug/L
ND
ill
ill
49.3
49.6
44
45
24-116
.6
Hexachlorobenzene
ug/L
NO
111
ill
44.9
57.2
40
51
1-152
24
Hexachlorocyclopentadiene
ug/L
NO
ill
ill
542
33.5
49
30
25-150
47 R1
Hexachloroethane
ug/L
ND
ill
ill
47.2
47.7
43
43
40-113
.9
Indeno(1,2,3-cd)pyrene
ug/L
NO
ill
ill
77.2
49.7
fig
45
1-171
43 R1
Isophorone
ug1L
ND
ill
11i
61.7
48.9
56
44
21-196
23
N-Nitroso-di-n-propylamine
ug/L
ND
ill
111
59.7
68.3
54
61
1-230
13
N-Nitrosodimethylamine
ug/L
ND
ill
ill
48.0
56.1
43
51
25-150
16
N-Nitrosodiphenylamine
ug/L
ND
111
ill
46.1
58.0
41
52
25-150
23
Naphthalene
ug1L
NO
ill
111
53.2
46.4
48
42
21-133
14
Nitrobenzene
ug1L
NO
111
ill
55.0
62.0
49
56
35-180
12
Pentachlorophenol
ug/L
ND
ill
ill
371
47.4J
33
43
14-176
Phenanlhrene
ug1L
NO
ill
ill
97.7
116
88
105
54-120
17
Phenol
ug/L
NO
ill
ill
50.7
49.7
46
45
5-112
2
Pyrene
ug1L
NO
ill
ill
114
124
102
112
52.115
9
2,4,6-Tribromophenol (S)
%
33
51
10-137
2-Fluorobiphenyl (S)
%
54
62
15-120
Date: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS Page 21 of 34
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
:r ;�

ceAnalytical
www.pec�s.mm
r
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 09065-7
Pace Project No.: 9245998
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 293290
293291
MS
MSD
9245958002 Spike
Spike MS MSD MS
MSD
% Rec
Parameter
Units Result Conc,
Conc, Result Result % Rec
% Rec
Limits RPD Qual
2-Fluorophenol (S)
%
23
25
10-120
Nitrobenzene-d5 (S)
%
54
79
10-120
Phenol-d6 (S)
%
25
31
10-120
Terphenyl-d14 (S)
W
48
45
11-131
Date: 06/30/2009 10:32 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, inc..
Page 22 of 34

® Pace Analytical Services, Inc.
`emal cal 2225 Riverside Dr.
www. CVk MM Asheville, NC 26804
[phone]
I
QUALITY CONTROL DATA
Project: 09065-7
Pace Project No.: 9245998
QC Batch: WETA15286 Analysis Method: SM 4500-CN-E
QC Batch Method: SM 4500-CN-E Analysis Description: 4500CNE Cyanide, Total
Associated Lab Samples: 9245998001, 9245998002, 9245998003
METHOD BLANK: 295419 Matrix: Water
Associated Lab Samples: 9245998001, 9245998002, 9245998003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide mg1L NO 0.0050 06/1610918:30
LABORATORY CONTROL SAMPLE: 295420
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Cyanide
mg/L
.1 0A1
107
M120
MATRIX SPIKE SAMPLE:
295421
9245890013 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Cyanide
mg/L
_ NO
1 0.098
96
75-125
SAMPLE DUPLICATE: 295422
9246491001 pup
Parameter
Units
Result Result
RPO
Qualifiers
Cyanide
mg1L
ND
ND
Date: 06/30/2009 10:32 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 23 of 34

Pace Services, Inc. PaceAnafytical Services, Inc.
1eAmOcal® 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www � Asheville, NC 28804 Huntersville, NC 28078
i [phone] [phone]
QUALITY CONTROL DATA
Project: 09065-7
Pace Project No.: 9245998
QC Batch: MPRP14552 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9245998001, 9245998002. 9245998003
METHOD BLANK: 292811 Matrix: Water
Associated Lab Samples: 9245998001. 9245998002, 9245998003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony ug/L NO 5.0 0611310912:19
Arsenic ug/L ND 5.0 06/13/0912:19
Beryllium uglL NO 1.0 06113/0912:19
Cadmium ug/L ND 1.0 06/1310912:19
Chromium ug/L ND 5.0 0611310912:19
Copper ug/L NO 5.0 06/1310912:19
Lead ug/L ND 5.0 0611310912:19
Nickel ug/L ND 5.0 06/1310912719
Selenium uglL NO 10.0 06/1310912:19
Silver ug/L NO 5.0 06/13/0912:19
Thallium ug/L ND 10.0 06/13/0912:19
Zinc ug/L NO 10.0 06/1310912:19
LABORATORY CONTROL SAMPLE: 292812
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Antimony ug/L 500 497 99 85-115
Arsenic ug/L 500 491 98 85-115
Beryllium ug/L 500 490 98 85-115
Cadmium ugIL 500 483 97 85-115
Chromium ug/L 500 489 98 85-115
Copper ug/L 500 485 97 85-115
Lead uglL 500 485 97 85-115
Nickel ug/L 500 488 98 85-115
Selenium ug/L 500 468 98 85-115
Silver ug/L 250 246 98 85-115
Thallium ug/L 500 464 93 85-115
Zinc uglL 500 49D 98 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 292813 _ 292814
MS MSD
9245561054 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone, Result Result % Rec % Rec Limits RPD Qua]
Antimony ug/L NO 500 500 497 468 99 94 70-130 6
Arsenic ug/L ND 500 500 490 465 98 93 70.130 5
Beryllium uglL NO 500 500 490 463 98 93 70-130 6
Cadmium ug/L ND 500 500 479 452 96 90 70-130 6
Chromium ug/L ND 500 500 493 466 98 93 70-130 6
Copper ug/L 6.6 500 500 525 495 104 98 70-130 6
Lead ug11- ND 500 500 482 456 96 91 70-130 6
Date: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS Page 24 of 34
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
. «o,o

•
Pace Analytical Services, Inc.
kwoal
2225 Riverside Dr.
WWW'PaceAftoom
Asheville, NC 28804
i
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 09065-7
Pace Project No.: 9245998
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
292813
292814
MS
MSD
9245561054
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nickel
ug/L
NO
500
500
497
468
99
93
70-130
6
Selenium
ug/L
NO.
500
500
487
463
97
92
70-130
5
Silver
ug/L
ND
250
250
251
239
100
95
70-130
5
Thallium
ug/L
NO
500
500
463
444
92
89
70-130
4
Zinc
ug/L
14.1
500
500
5"
489
106
95
70-130
11
SAMPLE DUPLICATE: 292815
9245935001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Antimony
ug/L
NO
ND
Arsenic
ug/L
ND
ND
Beryllium
ug/L
ND
ND
Cadmium
ug/L
ND
ND
Chromium
ug/L
54.7
55.2
.9
Copper
ug/L
15.9
15.8
.6
Lead
ug/L
ND
ND
Nickel
ug/L
ND
2.5J
Selenium
ug/L
ND
NO
Silver
ug/L
ND
86.1
Thallium
ug/L
NO
NO
Zinc
ug/L
13.6
60.1
126 R1
Date: 06/30/2009 10:32 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Without the Written consent of Pace Analytical Services, Inc..
Page 25 of 34

• Pace Analytical Services, Inc.
1ceAwlyfical 2225 Riverside Dr.
�wpecekelmmnr Asheville, NC 28804
f [phone]
QUALITY CONTROL DATA
Project: 09065-7
Pace Project No.: 9245998
QC Batch: MSV17324
Analysis Method:
EPA 624
QC Batch Method: EPA 624,
Analysis Description:
624 MSV
Associated Lab Samples: 9245998001
METHOD BLANK: 294484
Matrix: Water
Associated Lab Samples: 9245998001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
1,1,1-Tdchloroethane
ug1L
NO
5.0
06/1410912:14
1,1,2,2-Tetrachloroethane
uglL
ND
5.0
06/14/09 12:14
1,1,2-Trichloroethane
ug/L
NO
5.0
06114/0912:14
1,1-Dichloroethane
ug)L
NO
5.0
06/14/09 12:14
1,1-Dichloroethene
ug/L
NO
5.0
06/14/09 12:14
1,2-Dichlorobenzene
ug/L
NO
5.0
0604109 12:14
12-Dichloroethane
ug/L
NO
5.0
06/1410912:14
1,2-Dichloropropane
ug1L
NO
5.0
06/1410912:14
1,3-Dichlorobenzene
ug/L
NO
5.0
06/14/09 12:14
1,4-Dichlorobenzene
ug/L
NO
5.0
06/14/09 12:14
2-Chloroethylvinyl ether
ug/L
NO
10.0
06/14/09 12:14
Acrolein
ug/L
NO
100
06114/0912:14
Acrylonitrile
ug/L
NO
100
06/14/09 12:14
Benzene
ug/L
NO
5.0
06114/0912:14
Bromodichloromethane
ug/L
NO
5.0
0611410912:14
Bromoform
ug/L
NO
5.0
06/1410912:14
Bromomethane
ug/L
NO
10.0
06114/0912:14
Carbon tetrachloride
ug/L
NO
5 0
06/14/09 12:14
Chlorobenzene
ug/L
NO
5.0
06/14/0912:14
Chloroethane
ug/L
NO
10.0
06/1410912:14
Chloroform
ug/L
NO
5.0
06/14/0912A4
Chloromethane
ug/L
NO
5.0
06/14/09 12:14
cis-1,3-Dichloropropene
ug/L
NO
5.0
D611 4/09 12:14
Dibromochloromethane
ug/L
NO
5.0
06/1410912A4
Ethylbenzene
ug/L
NO
5.0
06/14/09 12:14
Hexachloro-1,3-butadiene
ug/L
NO
5.0
06/14/0912:14
Methylene Chloride
ug/L
7.3
5.0
06/14/09 12:14 C9
Naphthalene
ug1L
NO
5.0
06/14/0912:14
Tetrachloroethene
ug/L
NO
5.0
06l14/0912:14
Toluene
ug/L
NO
5.0
0611410912:14
trans-1,2-Dichloroethene
ug/L
NO
5.0
06114/0912:14
trans- 1,3-Dichloropropene,
ug/L
NO
5.0
06114/0912:14
Trichloroethene
ug/L
NO
5.0
06114/0912:14
Vinyl chloride
ug/L
NO
5.0
06/14109 12:14
1,2-Dichloroethane-d4 (S)
%
94
70-130
06/14/09 12:14
4-Bromofluorobenzene (8)
%
106
86-111
06/14/09 12:14
Dibromofluoromethane (S)
%
99
88-113
06/14/09 12:14
Toluene-d8 (S)
%
97
92-105
06/14/09 12:14
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Date: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS Page 26 of 34
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

®
Pace Analytical Services, Inc.
I71 JQf l/}�VR!
2225 Riverside Dr.
WWW JJ''
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project. 09065-7
Pace Project No.: 9245998
LABORATORY CONTROL SAMPLE: 294485
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units Cone.
Result
% Rec
Limits Qualifies
1,1.1-Trichloroethane
ug/L
20
19.6
98
52-162
1,1,2,2-Telrachloroethane
ug/L
20
19.0
95
46-157
1,1,2-Trichioroethane
ug/L
20
19.5
97
52-150
1,1-Dichloroethane
ug1L
20
20.6
103
59-155
1,1-Dichloroethene
ug/L
20
20.5
103
1-234
1,2-Dichlorobenzene
ug/L
20
19.3
96
18-190
12-Dichloroethane
ug/L
20
19.1
95
49-155
1,2-Dichloropropane
ug/L
20
20.6
103
1-210
1,3-Dichlorobenzene
ug/L
20
19.2
96
59-156
1,4-Dichlorobenzene
ug/L
20
20.5
103
18-190
2-Chloroethylvinyl ether
ug/L
40
39.3
98
1-305
Acrolein
ug1L
100
95.6J
96
15-152
Acrylonitrile
ug/L
100
183
183
75-132 LO
Benzene
ug/L
20
19.7
98
37-151
Bromodichloromethane
ug/L
20
18.8
94
35-155
Bromoform
ug/L
20
18.8
94
45-169
Bromomethane
ug/L
20
25.6
126
1-242
Carbon tetrachloride
ug/L
20
19A
97
70-140
Chlorobenzene
ug/L
20
18.7
94
37-160
Chloroethane
ug/L
20
19.8
99
14-230
Chloroform
ug/L
20
19.3
96
51-138
Chloromethane
ug/L
20
21.4
107
1-273
cis-1,3-Dichloropropene
ug/L
20
18.0
90
1.227
Dibromochloromethane
ug/L
20
17.9
89
53-149
Ethylbenzene
ug/L
20
20.0
100
37-162
Hexachloro-1,3-butadiene
ug/L
20
22.2
111
70-130
Methylene Chloride
ug/L
20
20.2
101
1-221
Naphthalene
ug/L
20
20.6
103
70-130
Tetrachloroethene
ug/L
20
22.2
111
64-148
Toluene
ug/L
20
19.6
98
47-150
trans- 1,2-Dichloroethene
ug1L
20
19.2
96
54-156
trans-1,3-Dichloropropene
ug/L
20
18.1
91
17-183
Trichloroethene
ug/L
20
20.2
101
71-157
Vinyl chloride
ug/L
20
20.0
100
1-251
12-Dichloroethane-d4(S)
%
92
70-130
4-Bromofluorobenzene (S)
%
109
86-111
Dibromofluoromethane (S)
%
96
88-113
Toluene-d8 (S)
%
100
92-105
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
294514
294515
MS
MSD
9245998001 Spike
Spike MS
MSD
MS MSD
% Rec
Parameter
Units
Result Cone.
Cone. Result
Result
% Rec % Rec
Limits RPD
1,1,1-Trichloroethane
ug/L
ND 20
20 21A
24.9
107 125
46-171 15
1,1,2,2-Tetrachloroethane
ug/L
NO 20
20 19.2
24.0
96 120
73-159 22
1,1,2-Trichloroethane
ug/L
ND 20
20 19.7
24.6
99 123
64-152 22
1,1-Dichloroethane
ug1L
ND 20
20 22.3
26.5
112 133
43-172 17
Date: 06/30/2009 10:32 AM
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc._
- ii_R�dt�lrr.f
Qual
Page 27 of 34

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
/�ceMalyfical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwwpocolaftcom Asheville, NC 28804 Huntersville, NC 28078
QUALITY CONTROL DATA
Project: 09065-7
Pace Project No.: 9245998
[phone] [phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 294514
9245998001
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
294515
M5
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1. 1 -Dichloroethene
ug/L
ND
20
20
22.3
26.8
112
134
48-189
18
1,2-Dichiorobenzene
ug/L
ND
20
20
18 7
23.1
93
116
54-154
21
1,2-Dichloroethane
ug/L
ND
20
20
19.3
23.7
96
119
42-171
21
1,2-Dichloropropane
ug/L
NO
20
20
21.1
26.1
106
130
55.157
21
1,3-Dichlorobenzene
ug/L
NO
20
20
19.0
23.2
95
116
57-148
20
14-Dichlorobenzene
ug/L
NO
20
20
20.4
25.1
102
125
58-149
21
2-Chloroethylvinyt ether
ug/L
NO
40
40
NO
NO
0
0
70-130
P5
Acrolein
ug/L
NO
100
100
98.7J
121
99
121
70-130
Acrylonitnie
ug/L
NO
100
100
101
121
101
121
70-130
18
Benzene
ug/L
NO
20
20
20.9
25.4
105
127
54-163
19
Bromodichloromethane
ug/L
ND
20
20
20.0
24.4
100
122
56-152
20
Bromoform
ug/L
NO
20
20
20.4
25.8
102
129
53-151
24
Bromomethane
ug/L
ND
20
20
19.8
29.9
99
150
10-200
41 MO
Carbon tetrachloride
ug/L
NO
20
20
22.0
26.2
110
131
41-175
18
Chlorobenzene
ug/L
N❑
20
20
19.8
23.7
99
118
67-152
18
Chloroethane
ug/L
NO
20
20
22.6
26.4
113
132
23-200
15
Chloroform
ug/L
NO
20
20
20.3
25.5
102
128
51-166
23
Chloromethane
ug/L
ND
20
20
21.3
24.3
106
121
40-175
13
cis-1,3-Dichloropropene
ug/L
NO
20
20
19.8
25.2
99
126
38-146
24
Dibromochloromethane
ug]L
NO
20
20
19.5
24.5
98
123
65-144
23
Ethylbenzene
ug/L
NO
20
20
20.5
24.6
102
123
57-152
18
Hexachloro-1,3-butadiene
ug/L
NO
20
20
19.9
25A
100
127
70-130
24
Methylene Chloride
ug/L
NO
20
20
21.9
25.8
109
129
40-167
16
Naphthalene
ug/L
NO
20
20
18.4
25.1
92
125
70-130
31 MO
Tetrachloroethene
ug/L
NO
20
20
24D
28.6.
120
143
59-155
17
Toluene
ug/L
ND
20
20
20.0
24A
100
122
47.162
20
trans- 1, 2-Dichloroethene
ug/L
ND
20
20
21 A
24.9
106
125
47-178
16
trans-1,3-Dichloropropene
ug/L
ND
20
20
20.1
25.4
100
127
39-148
24
Trichloroethene
ug/L
ND
20
20
21.6
25.8
108
129
60-153
18
Vinyl chloride
ug/L
NO
20
20
22.6
26.4
113
132
46-176
15
1,2-Dichloroethane-d4(S)
%
92
90
70-130
4-Bromofluorobenzene (S)
%
108
109
86-111
Dibromofluoromethane (S)
%
98
97
88-113
Toluene-d8 (S)
%
98
98
92-105
Date: 06/3012009 10:32 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, Inc..
Page 28 of 34

ceAnalytical •
www.pacadebs.cam
Project: 09065-7
Pace Project No.: 9245998
QC Batch: MERP12220
QC Batch Method: EPA 245.1
Associated Lab Samples: 9245998002. 9245998003
METHOD BLANK: 295294
Associated Lab Samples: 9245998002, 9245998003
Parameter Units
Mercury ug/L
LABORATORY CONTROL SAMPLE: 295295
Parameter Units
Mercury ug1L
Pace Analytical Services, Inc,
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 245.1
Analysis Description: 245.1 Mercury
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.20 061181091114
Pace Analytical Services, Inc.
9800 Kincey Ave. SuRe 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.5 101 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 295296 295297
MS MSD
9245998002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Mercury ug/L NO 2.5 2.5 2.5 2.5 98 100 70-130 2
SAMPLE DUPLICATE: 295298
9245998003 Dup
Parameter Units Result Result RPD Qualifiers
Mercury ug1L NO ND
Date: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Me -
Page 29 of 34

aceAnalytical
w wwpecolab&0om
j
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 09065-7
Pace Project No.: 9245998
QC Batch: OEXT17051 Analysis Method: EPA608
QC Batch Method: EPA 3535 Analysis Description: 608 GCS Pest PCB
Associated Lab Samples. 9245998001, 9245998002, 9245998003
METHOD BLANK: 292558
Associated Lab Samples:
Parameter
Matrix: Water
9245998001, 9245998002, 9245998003
Blank Reporting
Units Result Limit
Analyzed
4,4'-DDD
4L
ND
0.050
06/23109 05:00
4,4'-DDE
ug/L
ND
0.050
06/23/09 05:00
4,4'-DDT
ug/L
ND
0.050
06/23/09 05:00
Aldrin
ug/L
ND
0.050
06/23/09 05:00
alpha-BHC
ug/L
NO
0.050
06123/09 05:00
beta-BHC
ug/L
ND
0.050
06/23/09 05:00
Chlordane (Technical)
ug/L
NO
0.50
06/23/09 05:00
delta-BHC
ug/L
ND
0.050
06/23/09 05:00
Dieldhn
ug/L
NO
0.050
D6123/09 05:00
Endosulfan I
ug1L
NO
0.050
06/23/09 05:00
Endosulfan It
ug/L
ND
0.050
06/23/09 05:00
Endosulfan sulfate
ug/L
NO
0.050
06/23/09 05:00
Endrin
ug/L
NO
0.050
06/23/09 05:00
Endrin aldehyde
ug/L
ND
0.050
06/23/09 05:00
gamma-BHC (Lindane)
ug/L
ND
0.050
06/23/09 05:00
Heptachlor
ug/L
NO
0.050
06/23/09 05:00
Heptachlor epoxide
ug/L
ND
0.050
06/23/09 05:00
PCB-1016 (Aroclor 1016)
uglL
NO
0,50
06/23/09 05:00
PCB-1221 (Aroclor 1221)
ug/L
ND
0.50
06/23/09 05.00
PCB-1232 (Aroclor 1232)
ug/L
NO
0.50
06/23/09 05:00
PCB-1242 (Aroclor 1242)
ug/L
NO
0.50
06/23/09 05:00
PCB-1248 (Aroclor 1248)
ug/L
NO
0.50
06/23/09 05:00
PCB-1254 (Aroclor 1254)
ug/L
NO
0.50
05/23/09 05:00
PCB-1260 (Arodor 1260)
ug/L
NO
0.50
06/23/09 05:00
Toxaphene
ug/L
NO
0.50
06/23/09 05:00
Decachiorobiphenyl (S)
%
57
20.138
06/23/09 05:00
Tetrachloro-m-xylene (S)
%
43
20-110
06/23/09 05:00
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
292559
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
4,4'-DDD
ug1L
.08
0.068
86
31-141
4,4'-DDE
ug1L
.08
0.056
70
30-145
4,4'-DDT
ug1L
.08
0 052
65
25-160
Atdrin
ug1L
.06
ND
61
42-122
alpha-BHC
ugJL
.08
NO
61
37-134
beta-BHC
uglL
.08
0.070
88
17-147
delta-BHC
uglL
.08
0.064
81
19-140
Dieldrin
uglL
.08
0.063
79
36-146
Endosulfan I
ug)L
08
0.066
82
45-153
Endosulfan 11
ug/L
.08
0.066
82
1-202
Date: 06130/2009 10:32 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analyticai Services, !nc .
51� s
Pate Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NO 28078
[phone]
Qualifiers
Page 30 of 34

Pace Analytical Services, Inc.
Anaiybca
2225 Riverside Dr,
WWW'Paceililftcom
Asheville, NC 28804
+
[phone]
i Q
QUALITY CONTROL DATA
Pate AnalyNtal Services, Inc.
9800 KinceyAve. Suite 100
Huntersvilte. NC 28078
[phone]
Project. 09065-7
Pace Project No.: 9245998
LA90GtATORY CONTROL SAMPLE: 292559
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Endosuffan sulfate
ug/L
.08
0.074
92
26-144
Endrin
ug/L
.08
0.067
84
30-147
Endrin aldehyde
uglL
.08
0.082
103
50-150
gamma-8HC (Lindane)
ug/L
.08
0.056
70
32-127
Heptachlor
ug/L
.08
0,069
86
34-111
Heptachlor epoxide
ug1L
.08
0.066
82
41-126
Decachlorobiphenyl (S)
%
88
20-138
Tetrachloro-m-xylene (S)
%
71
20-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE'.
292560
292561
MS
MSD
9245902001
Spike
Spike MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc-
Conc. Result
Result
°% Rec % Rec
Limits
RPD
4,4'-ODD
ug/L
ND
.17
.17
NO
0.11
53
66
31-141
4,4'-DDE
ug/L
ND
.17
.17
ND
NO
39
49
30-145
4,4'-DDT
ug/L
ND
.17
.17
ND
NO
35
44
25-160
Aldrin
ug/L
ND
.17
.17
ND
NO
51
50
42-122
afpha-SHC
ug/L
ND
.17
.17
NO
ND
52
60
37-134
beta-13HC
ug/L
NO
.17
A7
NO
0.12
57
72
17-147
delta-8HC
ug/L
NO
.17
.17
ND
0.14
59
80
19-140
Dieldrin
uglL
ND
.17
.17
ND
NO
43
56
36-146
Endosulfan I
ug/L
ND
.17
A7
ND
0.11
53
62
45-153
Endosulfan tl
ug/L
NO
A7
.17
NO
NO
47
51
1-202
Endosulfan sulfate
ug/L
ND
17
.17
0.13
0.12
76
69
26.144
10
Endrin
ug/L
NO
.17
.17
0.14
0.18
82
103
30-147
23
Endrin aldehyde
ug/L
NO
.17
.17
0.12
NO
67
60
50-150
gamma-8HC (Lindane)
ug/L
NO
17
.17
ND
NO
44
59
32.127
Heptachlor
ug/L
NO
.17
.17
0.13
0.17
77
101
34-111
26
Heptachlor epoxide
ug/L
NO
.17
.17
ND
0.11
51
61
41-126
Decachlorobiphenyl (S)
%
36
52
20-138
Tetrachloro-m-xylene (S)
%
38
50
20-110
Date: 06/30/2009 10:32 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent
of�Pace
+Analytical Services, Inc..
is
Quaff
Page 31 of 34

•
ceAnalytical
wnwpaaebbs corm
Project: 09065-7
Pace Project No.: 9245998
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP/2204 Analysis Method: EPA 245.1
QC Batch Method: EPA 245.1 Analysis Description: 245.1 Mercury
Associated Lab Samples: 9245998001
METHOD BLANK: 292682
Associated Lab Samples; 9245998001
Parameter Units
Mercury ug/L
LABORATORY CONTROL SAMPLE: 292683
Parameter Units
Mercury ug/L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 0.20 06/12/0910:08
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.7 106 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 292684 292685
MS MSD
9246224001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L 0.76 2.5 2.5 2.6 2.7 76 77 70-130 1
SAMPLE DUPLICATE: 292686
Parameter
Mercury
Date: 06/30/2009 10:32 AM
9246224002 Dup
Units Result Result RPD Qualifiers
ug/L NO ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, ft-
-' eh
Page 32 of 34

1��2ceAnalytical
WWW.PW0&bs.cam
f
QUALIFIERS
Project: 09065-7
Pace Project No.: 9245998
DEFINITIONS
Pace Analytical services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Ditudon Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MID -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
ANALYTE QUALIFIERS
C9 Common Laboratory Contaminant.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
MO Matrix spike recovery was outside laboratory control limits.
P5 The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.
R1 RPD value was outside control limits.
So Surrogate recovery outside laboratory control limits.
Date: 06/30/2009 10:32 AM REPORT OF LABORATORY ANALYSIS Page 33 of 34
This report shall not be reproduced, except in full,
without the written Consent of Pace Analytical Services, Inc..

• Pace Analytical Services, Inc.
��f j/ c l 2225 Riverside Dr.
wyw A�orer Asheville, NC 28804
[phone]
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
09065-7
Pace Project No.:
9245998
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
9245998001
09065-7.1
EPA 3535
OEXT/7051
EPA 608
GCSV/5639
9246998002
09065-7.2
EPA 3535
OEXT17051
EPA 608
GCSV/5639
9245998003
09065-7.3
EPA 3535
OEXT17051
EPA 608
GCSV/5639
9245998001
09065-7.1
EPA 245.1
MERP12204
EPA 245.1
MERC/2199
9245999001
09065-7.1
EPA200.7
MPRP14552
EPA 200.7
ICP14231
9245998002
09065-7.2
EPA 200.7
MPRP14552
EPA 200.7
ICP/4231
9246998003
09066-7.3
EPA 200.7
MPRP/4552
EPA 200.7
ICP14231
9245998001
09065-7.1
EPA625
OEXT17072
EPA 625
MSSV/2806
$245998002
09065-7.2
EPA 625
OEXT17072
EPA 625
MSSV/2806
9245998003
09065-7.3
EPA625
OEXT/7072
EPA625
MSSV/2806
9245998001
09065-7.1
EPA 624
MSV17324
9245998002
09065-7.2
EPA 624
MSV17326
9245998003
09065-7.3
EPA 624
MSV17326
9245998002
09065-7.2
EPA 245.1
MERP/2220
EPA 245.1
MERC/2213
9246998003
09065-7.3
EPA 245.1
MERP/2220
EPA 245.1
MERC12213
9245998001
09065-7.1
SM 4500-CN-E
WETA/5286
9245998002
09065-7.2
SM 4500-CN-E
WETA15286
9245998003
09066-7.3
SM 4500-CN-E
WETA/5286
9245998001
09065-7.1
EPA 420.4
WETA/5288
9245998002
09065-7.2
EPA 420.4
WETA/5288
9246999003
09066-7.3
EPA420.4
WETA/5288
Date: 06/30/2009 10:32 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, inc..
Page 34 of 34