WQ0013116_Residual Annual Report 2014_20150220

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Town Of Waynesville WWTP
2014
Annual Biosolid Report
Town Of Waynesville WWTP
566 Walnut Trail
Waynesville NC 28785
828-452-4685
RVIE VEDIDENRI M

Annual Sludge Report
2003
Brief process description
Period of January 12014 to December 312014
The Town Of Waynesville Wastewater Treatment Plant has produced approximately 878.27 metric tons of Class A
l Biosolid Product that is given away for land application. Anaerobic digested sludge is dewatered then blended with
Quick Lime and Agricultural Lime. This mixture is then passed through a pasteurization vessel at a tempterature of 158
degrees farenheit or greater for 30 minutes. Labratory results demonstrate that this product exceeds requirements set
( forth by 40 CFR 503.32 alternative 5 for pathogen reduction and 40 CFR 503.33 option 6 for Vector Attraction
Reduction. Equipment manufactuer for this process was RDP Technologies Inc.
Certification Statement
"I certify under penalty of law that the Class A pathogen requirements in 503.32 (a)
and the vector attraction reduction requirement in 503.33 (b) (6) have been met.
This determination has been made under my direction and supervision in accordance
with the system designed to ensure that qualified personnel. properly gather and evaluate
the information used to determine that the pathogen requirements and vector attraction
reduction requirements have been met. I am aware that there are significant penatlies
for false certification including the possibility of fine and imprisonment.
x Marcy Onieal
Print name
x
Signature
Town Manager
Title
r
Page 1

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this "form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0013116 Laboratory: 1) Environmental Testing Solutions
Facility Name: Town Of Waynesville WWTP 2) Prism Labs.
NPDES # or NCO025321
WQ#:
WWTP Name: Town Of Waynesville WWTP
3) Test America
4) Rogers & Callcott
5)
Limits Limits
Sample or
Composite Date
1/8/14
3/4/14
5/6/14
7/9/14
9/10/14
1115114
Low Quality
Linritmg/kg
xignquatity
Limitmgfkg
MIN
MAX.
AVG.
Percent Solids
53
52
54
47
56
60
47
60
53.6667
Arsenic
6.42
7.23
7.81
5.25
5.32
5.12
75
41
5.12
7.81
6.19167
Cadmium
< 2.05
< 1.93 j<
2.54.
< 2.08
1.88
< 1.89
85
39
< 1.88
2.54
2.06167
Chromium
20.6
20.4
22.6
20.3
18.9
19.5
22.6
,b
Copper
156
119
138
152
135
131
4300
1500
119
156
138.5
Lead
17.8
16.1
17.8
17.4
14.4
15.9
840
300
14.4
17.8
16.5667
Mercury
0.65
0.74
0.57
0.35
0.39
0.54
57
17
0.35
0.74
0.54
Molybdenum
s 5.14
< 4.83
< 6.34
< 5.2
< 4.7
< 4.72
75
18
4.7
< 6.34
5.155
Nickel
11.6
13.5
12.4
11.1
10.6
11.9
420
420
10.6
13.5
11.85
Selenium
< 5.14
< 4.83
< 6.34
< 5.2
< 4.7
< 4.72
100
36
4.7
< 6.34-
5.155
Zinc
315
310
331
320
309
302
7500
2800
302
331
314.5
TKN
12,100
9,060
9,520
10,800
13,000
9,610
9060
13000
10681.7
Ammonia -Nitrogen
380
360
150
430
140
330
140
430
298.333
Nitrate and Nitrite
13.69
25.66
43.7
14.96
16.88
63.3
13.69
63.3
29.6983
TotalPhosphorus
6,350
5,590
5,490
6,650
6,570
6,170
5490
6650
6136.67
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I. am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.'
10,
Signature of Preparer Date /' a¢ " 1,5
Signature Of Permitee -"`;�- �� Date ► 1
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report

Please note that your permit may contain additional parameters to be analyzed than those required to be
summarized on this form.
Permit Number:
WQ0013116
Laboratory: 1)
Environmental Testing Solutions
Facility Name:
Town Of Waynesville WWTP
2)
Prism Labs.
NPDES # or
NCO025321
3)
Test America
WQ#:
4)
Rogers & Callcott
WWTP Name:
Town Of Waynesville WWTP
5)
17......1....1 A ....1.... "-*-
Sample or
Composite Date
1/8/14
3/4/14
5/6/14
7/9/14
9/10/14
11/5/14
MIN.
MAX.
AVG.
Aluminum
15,700
15,400
13,800
21,000
18,700
18,000
13,800
21,000
17,100
Magnesium
6,810
4,700
4,870
4,590
4,280
4,640
4,280
6,810
4,982
PAN
234,600
174,201
187,519
207,630
257,287
288,528
Sodium
500
450
465
425
3,556
435
425
3,556
972
P
Calcium
277,000
285,000
282,000
245,000
237,000
274,000
237,000
285,000
266,667
Potassium
2,320
2,110
2,180
2,250
1,740
2,010
1,740
2,320
2,102
CD
ua
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for mittvatx,
alse information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer Gam- Date -I
Signature of Permitee o Date q
ANNUAL RESIDUAL SAMPLING SUMMARY FORM

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: Town Of Waynesville WWTP Permit Number: WQ0013116
WWTP Name: Town Of Waynesville WWTP NPDES Number: NCO025321
Monitoring Period: From 1/1/2014 To 12/31/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1
Alternative 2
Alternative 3............
Alternative 4
Alternative 5 1 X
Alternative 6
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying
Heat Treatment
Thermophilic
. . . . . . . . . . .
Beta Ray
Gamma Ray
Pasteurization LXJ
Class B:
Alternative 1
Alternative 2
Alternative 3
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Air Drying
Composting
Aerobic Digestion
An erobic Di estion
a g 0
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable
Level in Sludge
Pathogen Density
Number of
Excellences
Frequency
of Analysis
Sample
'Type
Analytical
Technique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2x10tothe 6th
power MPN per
gram of total
solids or 2 x 10 to
the 6th power
CFU per gram of
total solids
1000 mpn per
Earn of total solid
<85
<108
MPN/g
0
Bimonthly
grab
sin 9221-e
Salmonella
bacteria in lieu of
3 MPN per 4
ams total solid
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 Option 2 Option 3 Option 4 Option 5
Option 6 ® Option ? Option 8 Option 9 Option 10
No vector attraction reduction options were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
❑"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
Flattraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Ronnie Norris Chief Operator
Prepr Name and 4T*le (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer Date Signature of Land Applier (if applicable) Date
Permitee Name and Title (type or print) Marcy Onieal Town Manager
Signature Of Permitee C Date 1 Z9 OS -
C
Waynesville WWTP PVRF /2003

ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
PERMIT W00013116 FACILITY NAME: Town Of Waynesville WWTP
PHONE: [phone] COUNTY: Haywood OPERATOR: David Smith
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A, B, and C)
was the facility in oneration during the nast calendar vear? M Yes ❑ko No If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES #
if applicable)
Volume (dry tons)
Recipient Information
Admendment/
Bulking Agent In
Residual In
Product Out
Name(s)
Volume
(dry tons)
Intended use(s)
January
18.32
20.93
39.26
Liming Agent / Hay & Silage Fields
Februa
Waynesville WWTP
Anaerobic Digested Sludge
NC 0025321
16.74
19.12
35.85
See additional Biosolid User Page
Liming Agent / Hay & Silage Fields
March
13.98
15.97
29.96
1
Liming Agent / Hay & Silage Fields
April
20.63
23.56
44.18
Liming Agent / Hay & Silage Fields
May
35.01
39.98
74.99
Liming Agent / Hay & Silage Fields
June
40.45
46.20
86.66
Liming ent/Hay &Silage Fields
g Agent
July
54.62
62.39
117.00
Liming Agent / Hay & Silage Fields
August
44.03
50.29
94.31
Liming Agent / Hay & Silage Fields
Septemb
53.58
61.20
114.77
Liming Agent / Hay & Silage Fields
October
50.11
57.23
107.34
Liming Agent / Hay & Silage Fields
Novembe
33.48
3 8.24
71.72
Liming Agent / Hay & Silage Fields
Decembei
29.04
33.17
62.22
Liming Agent / Hay & Silage Fields
Totals:
Annual (dry tons)
409.99
468.28
878.27
0
Admendment(s) used: Lime Kiln Dust
pulking Agent(s) used: Agricultrial-Lime
* If more space than given is required, please attach additional information sheet(s). Check box if additional sheet(s) are attached
Part C:
Facility was compliant during calendar year 2014 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality. Yes ETI No ❑ If No, please provide a written description why the facility was not compliant.
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water
, Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware
that there are significant penalties for submitting false informaiton, including a possibility o mes and imprisonment for knowing violations."
� is
Signature of Permittee Date Signature of Preparer** Date
(if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r)

Biosolid Recipient's 2012
Wet Tons
WITZIM
-------------
-------------
-------------
-------------
-------------
I V LCl l I J I v
Wet Tons
Average % dry solids 0.54 814.4
Dry Tons

wet weight lbs.
% dry
dry weight lbs.
dry weight tons
dry metric
' Date
per 1.0 ft/3
solids
per 1.0 ft/3
per dump truck - 270 ft/3
tons per load
8-Jan-14
40
0.63
21.2
2.86
2.91
4-Mar-14
42
0.52
21.84
2.95
3.00
6-May-14
45
0.54
24.3
3.28
3.33
19-Jul-14
44
0.47
20.68
2.79
2.84
10-Sep-14
43
0.56
24.08
3.25
3.30
5-Nov-14
42
0.6
25.2
3.40
3.46
0.54
Dry Metric
Dry Metric tons
Metric Tons
Metric Tons
Metric Tons
Month
Loads / Month
Tons / Month
Sludge
Ag. Lime
LKD
Ag. Lime & LKD
Jan.
13.5
39.26
20.93
0.00
18.32
18.32
Feb.
12.33
35.85
19.12
0.00
16.74
16.74
March
10
29.96
15.97
0.00
13.98
13.98
April
14.75
44.18
23.56
0.00
20.63
20.63
May
22.5
74.99
39.98
0.00
35.01
35.01
June
26
86.66
46.20
0.00
40.45
40.45
July
41.25
117.00
62.39
0.00
54.62
54.62
Aug.
33.25
94.31
50.29
0.00
44.03
44.03
Sept.
34.75
114.77
61.20
0.00
53.58
53.58
Oct.
32.5
107.34
57.23
0.00
50.11
50.11
Nov.
20.75
71.72
38.24
0.00
33.48
33.48
Dec.
18
62.22
33.17
0.00
29.04
29.04
279.58
878.27
468.28
0.00
409.99
409.99
Sludge metric tons
468.28
53.32%
Ag. Lime metric tons
0.00
0.00%
LKD metric tons
409.99
46.68%
LKD Cost $16,912
AG. Lime Cost $0
r
r'-

Laboratory
Data

r -"
Project name:
Collection date:
Date received:
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Certificate of Analysis
Town of Waynesville WWTP Project number:
8-Jan-14
8-Jan-14
Sample identification: 503 Lime Sludge - Composite Sample number:
140108.504
112663
Parameter
Method
Result
RL
Units
Date
Analyzed
Analyst
Footnotes
Arsenic
6010 C
6.42
5.14
mg/kg
14-Jan-14
MER
I
Cadmium
6010 C
<2.05
2.05
mg/kg
14-Jan-14
MER
1
Copper
6010 C
156
2.05
mg/kg
14-Jan-14
MER
1
Chromium
6010 C
20.6
5.14
mg/kg
14-Jan-14
MER
I
Lead
6010 C
17.8
2.14
mg/kg
14-Jan-14
MER
1
Molybdenum
6010 C
<5.14
5.14
mg/kg
14-Jan-14
MER
I
Nickel
6010 C
11.6
2.05
mg/kg
14Jan-14
MER
1
Selenium
6010 C
<5.14
5.14
mg/kg
14-Jan-14
MER
1
Zinc
6010 C
315
5.14
mg/kg
14-Jan-14
MER
1
Aluminium
6010 C
15700
257
mg/kg
14-Jan-14
MER
1
Calcium
6010 C
277000
5140
mg/kg
14-Jan-14
MER
I
Magnesium
6010 C
6810
257
mg/kg
14-Jan-14
MER
I
Potassium
6010 C
2320
10.3
mg/kg
14-Jan-14
MER
1
Sodium
6010 C
500
51.4
mg/kg
17-Jan-14
MER
1
Mercury
7471 B
0.65
0.20
mg/kg
10-Jan-14
MER
I
Total Kjeldahl Nitrogen
351.2
12100
168
mg/kg
13-Jan-14
LDP
1
Nitrate + Nitrate
13.69
10.20
mg/kg
14-Jan-14
1, 2
Total Nitrogen
Calculation
12100
168
mg/kg
14-Jan-14
REH
I
Total Phosphorus
200.7
6350
205
mg/kg
14-Jan-14
MER
1
Total Solids
SM2540 G
47.0
0.10
%
10-Jan-14
ASB
I
pH in Soil
SW 846 9045D
12.2
S.U.
8-Jan-14
KEK
% Total Solid
SM 2540 G
53
%
8-Jan-14
KEK
Ammonia Nitrogen
EPA 350.3
380
7.6
mg/kg
10-Jan-14.
KEK
Plant Avaliable Nitrogen
CALC
234600
21-Jan-14
KEK
Multiple Tube Fermentation
SM 9221-E
<95
95
MPN/g
8-Jan-14
KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Methods EPA 9210A and SM 4500NO2 B by LDP and REG.
r~
Date reviewed: �� • Z�'� NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
! NC Drinking Water Certification Number: 37786
Signature: 1011-
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

Project name:
Collection date:
Date received:
Certificate of Analysis
Town of Waynesville WWTP
4-Mar-14
4-Mar-14
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 140304.522
Sample identification: 503 Lime Sludge - Composite Sample number: 113987
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
Arsenic
6010 C
7.23
4.83
mg/kg
1I-Mar-14
MEC
1
Cadmium
6010 C
<1.93
1.93
mg/kg
11-Mar-14
MEC
I
Copper
6010 C
119
1.93
mg/kg
11-Mar-14
MEC
1
Chromium
6010 C
20.4
4.83
mg/kg
I I-Mar-14
MEC
I
Lead
6010 C
16.1
4.83
mg/kg
I1-Mar-14
MEC
I
Molybdenum
6010 C
<4.83
4.83
mg/kg
I I-Mar-14
MEC
I
Nickel
6010 C
13.5
1.93
mg/kg
I I-Mar-14
MEC
I
Selenium
6010 C
<4.83
4.83
mg/kg
I I-Mar-14
MEC
I
Zinc
6010 C
310
4.83
mg/kg
11-Mar-14
MEC
1
Aluminium
6010 C
15400
242
mg/kg
I I-Mar-14
MEC
1
Calcium
6010 C
285000
4830
mg/kg
I I-Mar-14
MEC
I
Magnesium
6010 C
4700
242
mg/kg
l l-Mar-14
MEC
I
Potassium
6010 C
2110
9.67
mg/kg
11-Mar-14
MEC
I
Sodium
6010 C
450
9.67
mg/kg
I1-Mar-14
MEC
1
Mercury
7471B
0.74
0.19
mg/kg
12-Mar-14
MEC
1
Total Kjeldahl Nitrogen
351.2
9060
118
mg/kg
13-Mar-14 .
LDP
I
Nitrate + Nitrate
25.66
9.59
mg/kg
12-Mar-14
1, 2
Total Nitrogen
Calculation
9090
118
mg/kg
13-Mar-14
LDP
1
Total Phosphorus
200.7
5590
193
mg/kg
11-Mar-14
MEC
1
Total Solids
SM2540 G
50.0
0.10
%
5-Mar-14
ASB
1
pH in Soil
SW 846 9045D
12.0
S.U.
5-Mar-14
KEK
% Total Solid
SM 2540 G
52
%
5-Mar-14
KEK
Ammonia Nitrogen
EPA 350.3
360
7.7
mg/kg
7-Mar-14
KEK
Plant Avaliable Nitrogen
CALC
174201
19-Mar-14
KEK
Multiple Tube Fermentation
SM 9221-E
<94
94
MPN/g
5-Mar-14
KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental. .
2. Methods EPA 9210A and SM 450ONO2 B by LDP and REH.
Date reviewed: 03 • I9-H NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
Signature: P' NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc
The results in this report relate only to the samples submitted for analysis.

PO Box 7565
Asheville, NC 28802
ET
Phone:
[phone]
Fax:
[phone]
r'" Environmental Testing Solutions, Inc.
Certificate of Analysis
Project name: Town of Waynesville WWTP
Project number:
140506.535
Collection date: 6-May-14
Date received: 6-May-14
Sample identification: 503 Lime Sludge - Composite
Sample number:
115733
Parameter
Method
Result
RL
Units
Date
Analyzed
Analyst
Footnotes
Arsenic
6010 C
7.81
6.34
mg/kg
13-May-14
MEC
1
Cadmium
6010 C
<2.54
2.54
mg/kg
13-May-14
MEC
1
Copper
6010 C
138
2.54
mg/kg
13-May-14
MEC
1
Chromium
6010 C
22.6
6.34
mg/kg
13-May-14
MEC
1
Lead
6010 C
17.8
6.34
mg/kg
13-May-14
MEC
1
Molybdenum
6010 C
<6.34
6.34
mg/kg
13-May-14
MEC
1
Nickel
6010 C
12.4
2.54
mg/kg
13-May-14
MEC
1
Selenium
6010 C
<6.34
6.34
mg/kg
13-May-14
MEC
I
Zinc
6010 C
331-
6.34
mg/kg
13-May-14
MEC
1
Aluminium
6010 C
13800
317
mg/kg
13-May-14
MEC
1
Calcium
6010 C
282000
6340
mg/kg
13-May-14
MEC
1
Magnesium
6010 C
4870
317
mg/kg
13-May-14
MEC
1
Potassium
6010 C
2180
12.7
mg/kg
13-May-14
MEC
I
w Sodium
6010 C
465
12.7
mg/kg
13-May-14
MEC
1
Mercury
7471B
0.57
0.26
mg/kg
16-May-14
DER
1
Total Kjeldahl Nitrogen
351.2
9520
558
mg/kg
16-May-14
LDP
1
Nitrate + Nitrate as N
-
43.7
26.24
mg/kg
1,2
Total Nitrogen
Calculation
9560
558
mg/kg
16-May-14
LDP
1
Total Phosphorus
200.7
5490
254
mg/kg
16-May-14
MEC
1
Total Solids
SM2540 G
38.0
0.10
%
7-May-14
ASB
1
pH in Soil
SW 846 9045D
12.2
S.U.
6-May-14
KW
% Total Solid
SM 2540 G
54
%
6-May-14
KW
Ammonia Nitrogen
EPA 350.3
150
3.7
mg/kg
11-Maya4
KEK
Plant Avaliable Nitrogen
CALC
187519
30-May-14
KEK
Multiple Tube Fermentation
SM 9221-E
<97
97
MPTUg
7-May-14
KEK
�t
u�
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

PO Box 7565
Asheville, NC 28802
T S-
Phone:
[phone]
Fax:
[phone]
SE
34 Environmental Testing Solutions, Inc.
_.
Certificate of Analysis
Project name: Town of Waynesville WWTP
Project number:
140709.506
Collection date: 9-Jul-14
Date received: 9-Jul-14
Sample identification: 503 Lime Sludge - Composite
Sample number:
117876
Parameter
Method
Result
RL
Units
Date
Analyzed
Analyst
Footnotes
Arsenic
6010 C
5.25
5.20
mg/kg
15-Jul-14
MEC
1
Cadmium
6010 C
<2.08
2.08
mg/kg
15-Jul-14
MEC
1
Copper
6010 C
152
2.08
mg/kg
15-Jul-14
NEC
1
Chromium
6010 C
20.3
5.20
mg/kg
15-Jul-14
MEC
1
Lead
6010 C
17.4
5.20
mg/kg
15-Jul-14
MEC
I
Molybdenum
6010 C
<5.20
5.20
mg/kg
15-Jul-14
MEC
I
Nickel
6010 C
11.1
2.08
mg/kg
15-Jul-14
MEC
1
Selenium
'6010 C
<5.20
5.20
mg/kg
15-Jul-14
MEC
1
Zinc
6010 C
320
5.20
mg/kg
15-Jul-14
MEC
1
Aluminium
6010 C
21000
260
mg/kg
15-Jul-14
MEC
I
Calcium
6010 C
245000
5200
mg/kg
15-Jul-14
MEC
I
Magnesium
6010 C
4590
260
mg/kg
15-Jul-14
MEC
1
Potassium
6010 C
2250
10.4
mg/kg
15-Jul-14
MEC
1
Sodium
6010 C
425
10:4
mg/kg
15-Jul-14
MEC
I
Mercury
7471B
0.35
0.21
mg/kg
17-Jul-14
DER
1
Total Kjeldahl Nitrogen
351.2
10800
376
mg/kg
17-Jul-14
LDP
I
Nitrate + Nitrate
14.96
9.46
mg/kg
15-Jul-14
1, 2
Total Nitrogen
Calculation
10800
376
mg/kg
17-Jul-14
LDP
1
Total'Phosphorus
200.7
6650
208
mg/kg
15-Jul-14
MEC
I
Total Solids
SM2540 G
46.0
0.10
%
15-Jul-14
MLR
1
pH in Soil
SW 846 9045D
12.1
S.U.
9-Jul-14
KW
3
% Total Solid
SM 2540 G
47
%
9-Jul-14
KEK
Ammonia Nitrogen
EPA 350.3
430
8.5
mg/kg
11-Jul-14
KEK
Plant Avaliable Nitrogen
CALC
207630
22-Jul-14
KEK
Multiple Tube Fermentation
SM 9221-E
<85
85
MPN/g
9-Jul-14
KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Methods EPA 9210A and SM 4500NO2 B by LDP and REH.
3. Sample analyzed outside holding time.
Date reviewed: dqq•12�lq NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
Signature: NC Drinking Water Certification Number: 37786
' This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Certificate of Analysis
Project name: Town of Waynesville WWTP Project number:
Collection date: 10-Sep-14
Date received: 10-Sep-14
Sample identification: 503 Lime Sludge - Composite Sample number:
140910.511
120048
Parameter
Method
Result
RL
Units
Date
Analyzed
Analyst
Footnotes
Arsenic
6010 C
5.32
4.70
mg/kg
18-Sep-14
MEC
I
Cadmium
6010 C
<1.88
1.88
mg/kg
18-Sep-14
MEC
1
Copper
6010 C
135
1.88
mg/kg
18-Sep-14
MEC
1
Chromium
6010 C
18.9
4.70
mg/kg
18-Sep-14
MEC
I
Lead
6010 C
14.4
4.70
mg/kg
18-Sep-14
MEC
I
Molybdenum
6010 C
<4.70
430
mg/kg
18-Sep-14
MEC
I
Nickel
6010 C
10.6
1.88
mg/kg
18-Sep-14
MEC
1
Selenium
6010 C
<4.70
4.70
mg/kg
18-Sep-14
MEC
I
Zinc
6010 C
309
4.00
mg/kg
18-Sep-14
MEC
I
Aluminium
6010 C
18700
235
mg/kg
18-Sep-14
MEC
I
Calcium
6010 C
237000
4700
mg/kg
18-Sep-14
MEC
I
Magnesium
6010 C
4280
235
mg/kg
18-Sep-14
MEC
1
Potassium
6010 C
1740
9.39
mg/kg
18-Sep-14
MEC
I
Sodium
6010 C
3556
9.39
mg/kg
18-Sep-14
MEC
1,
Mercury
7471B
0.39
0.19
mg/kg
16-Sep-14
DER
I
Total Kjeldahl Nitrogen
351.2
13000
393
mg/kg
17-Sep-14
LDP
I
Nitrate + Nitrate
16.88
9.24
mg/kg
17-Sep-14
1,2
Total Nitrogen
Calculation
13000
393
mg/kg
17-Sep-14
LDP
I
Total Phosphorus
200.7
6570
188
mg/kg
18-Sep-14
MEC
1
Total Solids
SM2540 G
52.0
0.10
%
12-Sep-14
LCB
1
pH in Soil
SW 846 9045D
11.9
S.U.
10-Sep-14
KEK
3
%Total Solid
SM 2540 G
56
%
10-Sep-14
KEK
Ammonia Nitrogen
EPA 350.3
140
7.1
mg/kg
11-Sep-14
KEK
Plant Avaliable Nitrogen
CALC
257287
7-Oct-14
KEK
Multiple Tube Fermentation
SM 9221-E
<101
101
MPN/g
10-Sep-14
KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Methods EPA 9210A and SM 4500NO2 B by LDP and REH.
3. Sample analyzed outside holding time.
Date reviewed:
Data reviewed by:
Signature:
Kelley E. Keenan
0-
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project name: Town of Waynesville WWTP
Project number:
141105.513
Collection date: 5-Nov-14
Date received: 5-Nov-14
Sample identification: 503 Lime Sludge - Composite
Sample number:
121659
•
Parameter
Method
Result
RL
Units
Date
Analyzed
Analyst
Footnotes
Arsenic
6010 C
5.12
4.72
mg/kg
11-Nov-14
MEC
1
Cadmium
6010 C
<1.89
1.89
mg/kg
11-Nov-14
MEC
1
Copper
6010 C
131
1.89
mg/kg
11-Nov-14
MEC
1
Chromium
6010 C
19.5
4.72
mg/kg
11-Nov-14
MEC
1
' Lead
6010 C
15.9
4.72
mg/kg
11-Nov-14
MEC
I
Molybdenum
6010 C
<4.72
4.72
mg/kg
11-Nov-14
MEC
1
Nickel
6010 C
11.9
1.89
mg/kg
11-Nov-14
MEC
1
Selenium
6010 C
<4.72
4.72
mg/kg
11-Nov-14
MEC
1
Zinc -
6010 C
302
4.00
mg/kg
11-Nov-14
MEC
I
Aluminium
6010 C
18000
472
mg/kg
11-Nov-14
MEC
I
Calcium
6010 C
274000
9430
mg/kg
I1-Nov-14
MEC
1
Magnesium
6010 C
4640
472
mg/kg
II-Nov-14
MEC
1
Potassium
6010 C
2010
9.43
mg/kg
11-Nov-14
MEC
1
Sodium
6010 C
435
9.43
mg/kg
11-Nov-14
MEC
1
Mercury
7471B
0.54
0.18
mg/kg
7-Nov-14
DER
1
Total Kjeldahl Nitrogen
351.2
9610
311
mg/kg
13-Nov-14
LDP
1
Nitrate + Nitrate
63.3
11.54
mg/kg
1,2
- Total Nitrogen
Calculation
9670
311
mg/kg
13-Nov-14
LDP
1
Total Phosphorus
200.7
6170
189
mg/kg
11-Nov-14
MEC
1
Total Solids
SM2540 G
52.0
0.10
%
6-Nov-14
LCB
1
pH in Soil
SW 846 9045D
11.8
S.U.
5-Nov-14
KW
3
% Total Solid
SM 2540 G
60
%
5-Nov-14
KW
Ammonia Nitrogen
EPA 350.3
330
6.7
mg/kg
6-Nov-14
KEK
Plant Avaliable Nitrogen
CALC
288528
14-Nov-14
KEK
Multiple Tube Fermentation
SM 9221-E
<108
108
MPN/g
5-Nov-14
KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
i 2. Methods EPA 9210A and SM 4500NO2 B by LDP on 11-11-14 and REH on -11-12-14.
3. Sample analyzed outside holding time.
r'
Date reviewed: NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
' Signature:
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

Load & Temper-a,turq

LOAD TEMPERATURE LOG
YEAR e�
MONTH J(;J�;�i,�
PASTEURIZATION PASTEURIZATION OPERATOR
nATF= A I (IAnC IAI TFIIAP °F CAI IT TFMP OF INITIAI:'
'EPERATED FROM
ISTRIBUTION PILE ANY
THAT DO NOT REACH
AINTAIN 158 OF.
revised: 2/7-25/05

ILI ""K
L.-Sullf
-1 Y
7--
.4
AE
zt
6TJ

LOAD TEMPERATURE LOG
YEAR
MONTH - � L
PASTEURIZATION PASTEURIZATION OPERATOR
DATE # LOADS IN TFIVIP OF ni IT TRMP OF INITIAl
2-41
All J- 6
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KEEP SEPERATED FROM
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LOADS THAT DO NOT REACH
AND MAINTAIN 158 OF.
Fe,ly 1
cr
revised: 2/7-25/05

LOAD TEMPERATURE LOG
YEAR'" Lj
^MONTH
PASTEURIZATION PASTEURIZATION OPERATOR
nATF 41 nAns IN TFMP OF OUT TEMP. OF INITIAL
1A4+t
;cw
,r v
:EEP SEPERATED FROM
LAIN DISTRIBUTION PILE ANY
OADS THAT DO NOT REACH
AND MAINTAIN 158 OF.
revised: 2/7-25/05

y-
f,.
LOAD TEMPERATURE LOG
YEAR
MONTH
PASTEURIZATION PASTEURIZATION OPERATOR
DATE # LOADS IN TEMP. OF OUT TEMP. OF INITIAL
1 c�
74
KEEP SEPERATED FROM
MAIN DISTRIBUTION.PILE ANY
_GADS THAT DO NOT REACH
4ND MAINTAIN 158 OF.
revised: 2/7-25/05

LOAD TEMPERATURE LOG
YEAR Of ff
MONTH (�
PASTEURIZATION PASTEURIZATION OPERATOR
DATE #LOADS IN TEMP. °F OUT TEMP. OF INITIAL
_1 KEEI
MAID
LOAI
AND
r
SEPERATED FROM
I DISTRIBUTION PILE ANY
)S THAT 00 NOT REACH
MAINTAIN 158 OF.
L-
revised: 2/7-25/05

LOAD TEMPERATURE LOG
YEAR
MONTH S rVc
PASTEURIZATION PASTEURIZATION OPERATOR
DATF # I C)An.c; IN TFMP OF OUT Tr=mp. OF INITIAL
IT9
(71
41-r z
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MAIN DISTRIBUTION.PILE ANY
LOADS THAT DO NOT REACH .
4ND MAINTAIN 158 OF.
t/fqY
revised: 2/7-25/05

I
LOAD TEMPERATURE LOG
YEAR
MONTH
PASTEURIZATION PASTEURIZATION OPERATOR
nATF= :a I nAn.q IN TPIAP- OF OUT TEMP. OF INITIAL
ov, cl�,Ql
ci,3
cec C-N
L-1 2 TS
ok A
cr, c
013
(EEP SEPERATED FROM '
RAIN DISTRIBUTION PILE ANY
.OA . DS . THAT DO NOT REACH
kND MAINTAIN 158 OF.
AO
revised: 2/7-25/05

LOAD TEMPERATURE LOG
YEAR 0
MONTH A" 36ts'k-
PASTEURIZATION PASTEURIZATION OPERATOR
DATE # LOADS IN TEMP. OF OUT TEMP. OF INITIAL'
C�
r'
r�
1
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A
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A14
4
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MAIN. DISTRIBUTION PILE ANY
LOADS THAT DO NOT REACH
AND MAINTAIN 158 °F.
revised: 2/7-25/05

LOAD TEMPERATURE LOG..
YEAR 2-a f
MONTH
PASTEURIZATION PASTEURIZATION OPERATOR
M ATE: .9 1 n A r) Q Im tr-hfip Op MIT TEMP_ OF INITIAL
L
t�i -.5
fi`7
141-41
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EEP SEPERATED FROM
IAIN DISTRIBUTION PILE ANY
OADS THAT DO NOT REACH,
,ND MAINTAIN 158 OF.
revised: 217-25/05

LOAD TEMPERATURE LOG
YEAR
MONTH
PASTEURIZATION PASTEURIZATION OPERATOR
DATE #LOADS IN TEMP. OF OUT TEMP. OF INITIAL
it) lit
0
A 4
W7
I I I
') ffe
196
10 2'3
IT -.
113
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fa- 'ice
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9 -14
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-4 If 11%,
KEEP SEPERATED FROM
MAIN DISTRIBUTION PILE ANY
LOADS THAT DO NOT REACH
AND MAINTAIN 158 OF.
revised: 2/7-25/05
0

LOAD TEMPERATURE LOG
YEAR 2�
MONTH 6e01V-e- cl-
PASTEURIZATION PASTEURIZATION OPERATOR
DATE # LOADS IN TEMP. OF OUT TEMP. OF INITIAL.,
�
1
(
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11 13-Jy
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KEEP SEPERATED FROM
MAIN DISTRIBUTION PILE ANY
LOADS THAT DO NOT REACH
AND MAINTAIN 158 OF.
revised: 2M25f05

, LUAU TEMPERATURE LOG .
YEAR 20
MONTH . '
'
PASTEURIZAJIONPASTEUR|ZATk]N OPERATOR
DATE #LOADS IN TEMP. OF . OUT TEMP. OF INITIAL
JZ
jjq
All
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KEEP SBPERAJEOFROM
�MAIN D|STR|8UT|OW' '|LE ANY
'
LOADS THAT DONOT- REACH
AND MAINTAIN 158OF.
revised: 2/7-25/05

PH METER CALIBRATION FOR 503 LIMEI5L00U1--
SM 4500-H+B-2000(Aqueous)
'own of Waynesville WWTP
-66 Walnut Trail
.Vaynesville, NC 28785
N ID: NC01119
Certification #: 194
' instrument ID: VWR Symphony SB70P
- /N: 003367
i Lab
equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot*
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:122703591 Cal Due Date:1213/13
'
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
I
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
.
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
;ORRECTED pH: A ct
2HR
pH
2HR
TEMP. °C
&O- RRECTED pH: f v • :� / = l i . y
24 HR
pH
24 HR
TEMP. oC
fa. � 0
3 - "
DORRECTED pH: 1
0—+ ('nlihrn+inn \/crifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
'- Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
( ale pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIMEISLUDGE
SM 4500-H+B-2000 (Aqueous)
Fown of Waynesville WWTP
i66 Walnut Trail
; Vaynesville, NC 28785
1 ID: NC01119
Certification #: 194
instrument ID: VWR Symphony SB70P
i/N: 003367
n Lab
equipment Maintenance:
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017.
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
'
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
r: ORRECTED pH: P.J. • � ) - C.• ;xq `J) !�
2 HR
PH
2 HR
TEMP. oC
i ;�.6:-7
) � .-L
CORRECTED pH: 0
24 HR
PH
24 HR
TEMP. °C
5"3
r T
-ORRECTED pH: � � - � -C' -,� I = f) ..1 l
Dnct rniihratinn Varifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
'o
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
;Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
--rie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME15LUDGt
SM 4500-H+6-2000 (Aqueous)
'own of Waynesville WWTP
` 166 Walnut Trail
IVayhesville, NC 28785
N ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
/N:003367
i Lab
Cquipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot*
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial *122703591 Cal Due Date:1213/13
'
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
PH 10.;J0
BUFFER
PH 13.0
BUFFER
INITIAL
[BUFFER
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
� BU 14
J . 6
T. ,5 �9
R Ct
i
'ORRECTED pH: (? = ! - : 7
2 HR
2 HR
pH
TEMP-. oC
:;ORRECTED pH: / X -;0 -C, 0 ' / •' `�
24 HR
24 HR
pH
TEMP.°C
CORRECTED pH: cF c / 3
Pncf rnlihratinn Varifiratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
`�
.�
`� •1
i 7-7
-)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
,orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
'-,Actual pH = Measured pH +/- the correction Factor.
\ Fhe initial pH reading is taken after the lime is mixed with the 503 sludge.
fhe pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
�,e pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13
t

PH METER CALIBRATION FUK 5U3 LIMt/SLUlJUt
SM 4500-H+B-2000 (Aqueous)
own of Waynesville WWTP
766 Walnut Trail
,,Vaynesville, NC 28785
'^AID: NC01119
Certification #: 194
instrument ID: VWR Symphony SB70P
/N: 003367
i Lab
equipment Maintenance:
pH 4.01 Lot *A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:122703591 Cal Due Date:12/3/13
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 4.0
TEMP. °C.
OF PH 4.0
BUFFER
CAL.
BUFFER
PH 10.0
TEMP. °C
OF PH 10.0
BUFFER
QC
BUFFER
PH 13.0
TEMP. °C
OF PH 13.0
BUFFER
INITIAL
DATE
t
l` q
?, �.:
-
��c .O`
C1 G
1�
��
I
T 1
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
1/I
"5'60
1 ")-%�;'
i �• 6,2
12 _2 ..
- ORRECTED pH
2 HR
2 HR
pH
TEMP.°C
! .2. I `3
I ;j.,
'- '%-URRECTED pH: ! q - c . �21 -` 1d2: L(a
24 HR
pH
24 HR
TEMP.°C
; ORRECTED pH: 0 .-; A U -AIL-- Lt
0—f r`nlihrn+inn Vcrificatinn
Ph
Temp.
TIME
INITIAL
13.0
°C
10�05
)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other. than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading_ .
_ e pH of this second reading has to be above a pH of 12.
r The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

NH Mt I tK GALIBKA I IUN 1-UK 5U3 LIMt/SLUlJUh
SM 4500-H+B-2000 (Aqueous)
Fown of Waynesville WWTP
-i66 Walnut Trail
_Naynesville, NC 28785
ID: NC01119
ti Certification #: 194
nstrument ID: VWR Symphony SB70P
i/N: 003367
'n Lab
;equipment Maintenance:
PH 4.01 Lot#:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot*
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot*
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
#:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH:
2 HR
PH
2 HR
TEMP. °C
CORRECTED pH: ? • ! j" v ! • l�
24 HR
PH
24 HR
TEMP. °C
,ORRECTED pH: 1..), 7 `r k �Z j = ! =]
Pnst Calihration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
nH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
\ctual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
—e pH of this second reading has to be above a pH of 12.
!'he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised: 9/9/13
C

PH Mt 1 LK UALIUKA I IUN I -UK 5U3 LIMt/511-UUIUL
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
-"566 Walnut Trail
- Waynesville, NC 28785
EPA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
it-31/i -
� ; _
�: ,
q.aoo
I S1 Y oc.
lQ; �a
/ ��. (,`c'.
i3, a
�S- Y `-c
/°6
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
(DATE
CORRECTED pH: l1 -a =� = !��• i %
2 HR
2 HR
pH
TEMP. oC
t.�RRECTED pH: J.2z.Sq •- ja- 3
24HR
pH
24HR
TEMP.°C
CORRECTED pH: 1 -c:- IS = /sN 1
PnGt Calihrntinn Verifiratinn
TIME
INITIAL
Ph
13.0
Temp.
°C
,.--,pH readings must be taken at.25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
.The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
The second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
the pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
.Waynesville, NC 28785
" ID: NC01119
. Certification #: 194
Instrument ID: VWR Symphony SB70P
5/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot*
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial *122703591 Cal Due Date:12/3/13
`
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
�'i i
? tcj
�C''-i
`4 t
�(0
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: / V . 6 _).: I �_ , y--
2HR
pH
2HR
TEMP. °C
CORRECTED pH:
24 H R
24 H R
pH
TEMP.°C
CORRECTED pH: ( • 'c / . 5" ;�
Pnct ralihrntinn VPriflration
Ph
Temp.
TIME
INITIAL
13.0
°C
I �t �• `��
J ,F'
� � i IIY
T� '
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
to pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
'Document changes in lot Vs.
revised: 9/9/13

j .
FM ML I LK GALIBKA I IUN I -UK 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
-)Waynesville, NC 28785
ID: NC01119
..Certification #: 194
.,Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
(._'Equipment Maintenance:
I
pH 4.01 Lot #:A3241 Exp. Date:AUG. 2017
pH 4.01 Lot #: Exp. Date:
pH 10:01 Lot #:A3266 Exp. Date:SEPT. 2014
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4309C86 Exp. Date:SEPT. 2014
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
D}AjT'Ed
TIME
E\FF./
4.0
BUFFER
PH 10.0
BUFFER
PH
BUFFER
INITIAL
//
(' KPH
)913�5.0
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
r
'CORRECTED pH:
2 HR
2 HR
pH
TEMP. °C
,(4_0
ig,i°c.
'+CORRECTED pH: Q, 0yl, i ;5= 0, q
24 H R
pH
24 H R
TEMP. °C
j)
F
CORRECTED pH: 1 �-1;, l _b , Ili -f ).. 4 f
Pnst Calihratinn Verification
Ph
Temp.
TIME
I INITIAL
13.0
°C
j,i
�, .f t
f 3, iC3
I 4
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
' The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
,Document changes in lot #'s.
revised: 9/9/13
C_

rrl IVIC 1 CK kPALIUKA 1 IUN rUK OW LIIYIC/JLUUIjC
SM 4500-H+B-2000 (Aqueous)
r
Town of Waynesville WWTP
566 Walnut Trail
;Waynesville, NC 28785
`A ID: NC01119
Certification #: 194
_jnstrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
'. DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
-TEMP. °C
'30RRECTED pH: (1,
2HR
pH
2HR
TEMP. °C
'
;CORRECTED pH:
24 HR
pH
24 HR
TEMP.°C
CORRECTED pH: l _ t - t' < :- It /) . `y
Pnct Calihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
'Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
rThe initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
-..a pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

FM Mt I tK UALUSKA I IUN t-UK OU3 LINIt/,LUlJUt
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
'566 Walnut Trail
,Waynesville, NC 28785
`q ID: NC01119
. Certification #: 194
*Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot* -
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C -
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
'. DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: i ), �-) t` •) (- d ) - is (
2 HR
PH
2 HR
TEMP.oC
-ORRECTED pH:
1;� 4 !r. *) ID. , k i .. o. 4
24 H R
PH
24 H R
TEMP. °C
CORRECTED pH: (),- ) � 0 21 - f l . 11
Pnct r'nlihrntinn \/arifirntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
-) . _ ..
--
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
.3alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
-Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
r- ..4e pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

' 1 11 1�1{-1L.1\ Vf1V1Y1 v\IIVI■ 1 VI\ VVV �II�I�IVrVV V1..
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
_66 Walnut Trail
daynesville, NC 28785
ID: NCO1119
.;ertification #: 194
istrument ID: VWR Symphony SB70P
/N:003367
In Lab
_quipment Maintenance:
r" `l
PH 4.01 Lot *A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot*
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
DATE
TIME
SLOPE
EFF.
BUFFER
PH 4.0
OF PH 4.0
BUFFER'
BUFFER
PH 10.0
OF PH 10.0
BUFFER
BUFFER
PH 13.0
OF PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. oC
:ORRECTED pH: 1.. -2. 3 - 0.1(4 = 11, ict
2 HR
2 HR
PH
TEMP. °C
,:ORRECTED pH:
24 HR
24 HR
PH
TEMP. °C
,ORRECTED pH: �I �� �: - I � • y
Onct ('zAhrntinn Verifiratinn
Ph
Temp.
TIME
INITIAL
13.0
j
\°C
nH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
kctual pH = Measured pH +/- the correction Factor.
r , he initial pH reading is taken after the lime is mixed with the 503 sludge.
he pH of this initial reading has to be above a pH of 12.
r • second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
`fhe pH of the final reading (24 hours latter) has to be above a pH of 11.5.
-)ocument changes in lot Vs.
revised: 9/9/13

rn 1YIL 1 GI\ VML10nA I IV1V 1 VI\ JVJ L.1 n1 VIVL-V VV�
SM 4500-H+B-2000 (Aqueous)
--)wn of Waynesville WWTP
-j6 Walnut Trail
'aynesville, NC 28785
ID: NC01119
v .;ertification #: 194
strument ID: VWR Symphony SB70P
(-�^ Lab03367
-quipment Maintenance:
pH 4.01 Lot *A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer serial #:122703591 Cal Due Date:12/3/13
DATE
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 4.0
TEMP. °C
OF PH 4.0
BUFFER
CAL.
BUFFER
PH 10.0
TEMP. °C
OF PH 10.0
BUFFER
QC
BUFFER
PH 13.0
TEMP. °C
OF PH 13.0
BUFFER
INITIAL
\
COLLECT
ANALYSIS
INITIAL
INITIAL
`DATE
TIME
TIME
PH
TEMP. °C
Cl ''aqs
r `]
=ORRECTED pH: f ',�. (e•l - 0,(oa..=
2 HR
2 HR
pH
TFEMP.oC
{S
i r_1 � 1. `ram-�
i
i�V'%+• l-1
ORRECTED pH: ; i A
24 H R
24 H R
pH
TEMP. °C
ORRECTED pH: d ti �( .w c .+ E ;� .N,
0+ r, lihr-n+inn Vcrificatinn
Ph
Temp.
TIME
INITIAL
13.0
°C
^H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
_alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
r;orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
�- she initial pH reading is taken after the lime is mixed with the 503 sludge.
�.he pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
l ie pH of this second reading has to be above a pH of 12.
the pH of the final reading (24 hours latter) has to be above a pH of 1.1.5.
Jocument changes in lot Vs.
revised: 9/9/13

6
SM 4500-H+B-2000 (Aqueous)
own of Waynesville WWTP
36 Walnut Trail
/aynesville, NC 28785
ID: NC01119
;ertification #: 194
,Istrument ID: VWR Symphony SB70P
/N:003367
„i Lab
quipment Maintenance:
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. oC
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
' DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
i,c(
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
°C
t
i �.
M C7 .� �.i
}TEMP.
\ CA. Ci
,,ORRECTED pH: I )c �� e � �, = /, •r
2HR
PH
2HR
TEMP.°C
ORRECTED pH: Y:. cT I `r,,., i D.-•3l.r
24 H R
PH
24 H R
TEMP.°C
''ORRECTED pH: ,T-7 - G ,tS I I.- `t -�''
D—+ ('�Iihrnfinn Varifinnfinn
Ph
Temp.
TIME
INITIAL
13.0
°C
�H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
:orrection factor (CF) = 0.03 pH units'* (Temp. Measured - 25 Centigrade).
,ctual pH = Measured pH +/- the correction Factor.
-Yhe initial pH reading is taken after the lime is mixed with the 503 sludge.
he pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
r , Id pH of this second reading has to be above a pH of 12.
he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
locument changes in lot;Ws.
revised: 9/9113

r I I I9ILI L_1% Vf1LI YIVII IVI\ I VI\ VVV LIItI V/VLVVVL
SM 4500-H+B-2000 (Aqueous)
-own of Waynesville WWTP
.,66 Walnut Trail
Jaynesville, NC 28785
-DA ID: NC01119
certification #: 194
..istrument ID: VWR Symphony SB70P
/N: 003367
'-i Lab
-quipment Maintenance:
pH 4.01 Lot *A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
,DATE
TIME
EFFrr.//
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13..0
INITIAL
' � �/%
•" ;%
S `-d"
�'� is'L •
i 0 • i ro
Q
r✓
I' "`, C
dBUFFER
F ,� j'
S
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
-ORRECTED pH: i J . 7
2HR
pH
2HR
TEMP. °C
ORRECTED pH: I) - `)C 0. I`T' Ll. -i"
24 HR
pH
24 HR
TEMP.°C
ORRECTED pH: ,) • (,,.. __ C.. ), 4 -1 0,_ 9 . ,
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
^H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
-alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
"orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
-he initial pH reading is taken after the lime is mixed with the 503 sludge.
-'he pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
the pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

rn IVIG 1 Gr% VP%L.J9711A1 IVI\ I WAX JVJ LIItI V/V{-V✓V�
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
„36 Walnut Trail
iaynesville, NC 28785
`7 y ID: NCO1119
certification #: 194
-,strument ID: VWR Symphony SB70P
!N: 003367
1^ Lab
_quipment Maintenance:
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
,-
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
.DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
1-ORRECTED pH: 1 i : io c - - I � - (2-4- '-f
2 HR
2 HR
TEMP. °C
PH
,1{ K
ORRECTED pH: ? =J t•� ; t� - f-ti
24 HR
PH
24 HR
TEMP. °C
rORRECTED pH: i (44 L' +r fit- 2 2
Pnc+ (:alihra+inn Varifirntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
�C'.
^H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
-alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
^orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
,actual pH = Measured pH +/- the correction Factor.
-he initial pH reading is taken after the lime is mixed with the 503 sludge.
,'he pH of this initial reading has to be above a pH of 12-
second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
,Document changes in lot #'s.
revised: 9/9/13

rri Mt I rK UALII:51KA I IUN 1-UK 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
,Jllaynesville, NC 28785
ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
3/N: 003367
in Lab
quipment Maintenance:
PH 4.01 Lot *A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
' DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: 3'
2HR
2HR
PH
TEMP. °C
i t,,
-ORRECTED pH: 1, z .; _`y C-. i
24 HR
24 HR
PH
TEMP. °C
CORRECTED PH
Pnct C ;;Iihration Verification
Ph.
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
j The pH of this initial reading has to be above a pH of 12.
� i second pH reading is taken 2 hours after the initial reading.
...a pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5,
Document changes in lot;Ws.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
j66 Walnut Trail
.'Naynesville, NC 28785
" --"�A1D: NC01119
` Certification #: 194
__nstrument ID: VWR Symphony SB70P
3/N: 003367
'n Lab
quipment Maintenance:
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial *122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH '10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
}�Ir�i 4�-
F� ay i.?
�. V' �
y� 1
il\t S V•_
\�1.�5 y
�\ ��...
���
t�� �
� ��
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PHy
INITIAL
EMP.°C
TEMP. OC
�'ORRECTED pH:,,t t«.�
2 HR
PH
2 HR
TEMP. °C
'ORRECTED pH:
24 H R
PH
24 H R
TEMP.°C
t CORRECTED pH: f t7 €' • J. (- i .
r.
t
Pnct rplihrntinn VPrifiration
Ph
Temp.
TIME
INITIAL
13.0
°C
i;.�,
nH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
the pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
...-a pH of this second reading has to be above a pH of 12.
the pH of the final reading (24 hours latter) has to be above a pH of 11.5.
,Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H'B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
rWaynesville, NC 28785
`'AID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
' DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0.
BUFFER
PH 13.0
BUFFER
INITIAL
liter`
2
1 5
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
._
7
99
CORRECTED pH: i ;?..i I i = kk, �
2 HR
2 HR
PH
TEMP. °C
' 4-
CORRECTED pH: r _�), 7 6-> —0 • I ( d,,., > :j
24 H R
PH
24 H R
TEMP.°C
CORRECTED pH:
Pnst Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
'Actual pH = Measured pH +/- the correction Factor.
'The initial pH reading is taken after the lime is mixed with the 503 sludge.
- The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13
i

rn IVIC I r-m WALIMMA I JUN I -UK OW LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
--'.PA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
.CAL.
TEMP. oC
CAL.
TEMP. °C
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
D/ATBBEj
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
L
rINITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. oC
',if i ' l ci
J"
CORRECTED pH: ;1 • .l - f d .
2 HR
2 HR
pH
TEMP.°C
�). ) t
q,
uORRECTED pH: 1-� _ i t - t -i
24 HR
24 HR
pH
TEMP.°C
'CORRECTED pH: q s ,y,: , ', , ; > .. i , � `l
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
f0..p{rM1�-
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
4ctual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
the pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
,e pH of this second reading has to be above a pH of 12.
the pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9113

rn ina 1 SIC VHLIaI[A 1 1UN rL)K OU3 LIML/SLUIJUE
SM 4500-Hi'B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
__EPA ID: NC01119
Certification #: 194
j instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
N
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
oG''
>
O
i
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. oC
- ' CORRECTED pH:
2 HR
PH
2 HR
TEMP. °C
, _JRRECTED pH:
24 HR
PH
24 HR
TEMP. °C
t a
CORRECTED pH: t �I ^ 6,19 = ?r „7,
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
- The pH of this initial reading has to be above a pH of 12.
----second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
� revised: 9/9/13

rn Mt i tK (:AUi3KATI0N FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
' 566 Walnut Trail
Waynesville, NC 28785
-,SPA ID: NC01119
Certification #: 194
instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
PH 13.00 Lot'#:
Exp. Date:
Checked with Traceable Thermometer Serial *122703591 Cal Due Date:12/3/13
CAL.
TEMP. oC
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
p
} -
q
` -7
CORRECTED pH: .�) , 7 ` • 1 i - f ,ice;.
2 HR
2 HR
PH
TEMP.°C
_JRRECTED pH:
24 H R
24 H R
PH
TEMP.°C
CORRECTED pH: C-
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
PH readings must be taken -at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
- Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
Tie second pH reading is taken 2 hours after the initial reading.
- pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be.above a pH of 11.5.
-Document changes in lot #'s.
revised: 9/9113

PH mt 6 tK GALIBRA rION FOR 503 LIME/SLUDGE
SM 4500-H+13-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
Certification #: 194
instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
K3 ID
CORRECTED pH: ( ,, . i r " 0 _ = V ,3), . C: '-2,
2 HR 2 HR
PH TEMP. °C
_jRRECTED pH: (A. 4- -c�' (�
24 HR 24 HR
H TEMP. °C
p
'CORRECTED pH: I L i
i Post Calibration Verification
i
.I
_jRRECTED pH: (A. 4- -c�' (�
24 HR 24 HR
H TEMP. °C
p
'CORRECTED pH: I L i
i Post Calibration Verification
i
.I
'CORRECTED pH: I L i
i Post Calibration Verification
i
.I
Ph
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
o second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
r The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

rri Wit I tK UALItSKA I ION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
Certification #: 194
instrument ID: VWR Symphony SB70P
S/N: 003367
-In Lab - -
Equipment Maintenance:
PH 4.01 Lot *A3241 Exp. Date:AUG. 2017
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A3266 Exp. Date:SEPT. 2014
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:4309C86 Exp. Date:SEPT. 2014
PH 13.00 Lot #: Exp. Date:
-Checked-with Traceable Thermometer.Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
9Iiii
y
pp
1
F "; .�.
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: it .,?
2 HR
PH
2 HR
TEMP. °C
_jRRECTED pH: i ? ` ; z
24 H R
24 H R
PH
TEMP.°C
CORRECTED pH: ? . irt. <; -•". > r,, =J
c
Post Calibration Verification
r
Ph
Temp.
TIME
INITIAL
13.0
°C
('
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a -conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T-6e second pH reading is taken 2 hours after the initial reading.
r s pH of this second reading has to be above a pH of 12.
r The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
r - Document changes in lot #'s.
revised: 9/9/13

rn IVIc 1 crC %r/1LIDmm 1 IVIV rum 3U3 LIIVIC/JLUI Ut
SM 4500-H-'B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
SPA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:122703591 Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. 0C
`
•y
_
�jy
CORRECTED pH: i ;. ;f c :. > t A - � :=
2HR
pH
2HR
TEMP. °C
�,JRRECTED pH:
24 H R
24 H R
pH
TEMP. °C
CORRECTED pH:
Pncf ('alihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25.centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
a pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

rn [VIM 1 MM I,ALIOKH I IUN t-UK 9U3 LIMt15LUU6E
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
" - 566 Walnut Trail
Waynesville, NC 28785
'AID: NC01119
t ; Certification #: 194
,Instrument ID: VWR Symphony SB70P
S/N:003367
'=-In Lab- - -
Equipment Maintenance:
r'
pH 4.01 Lot#:A3241 Exp. Date:AUG. 2017
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A3266 Exp. Date:SEPT. 2014
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4309C86 Exp. Date:SEPT. 2014
pH 13.00 Lot #: Exp. Date:
- - - Checked with Traceable Thermometer Serial-#:122703591 _-Cal- Due- Date: 12/3/13-
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BLUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
^
CORRECTEDp Fi:
2HR
2HR
pH
TEMP.°C
'CORRECTED pH: '
24 H R
24 H R
pH
TEMP.°C
CORRECTED pH:
Pnct (;;Iihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
r
-The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
`I rie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H-B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
�i Waynesville, NC 28785
( --'A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony S670P
S/N:003367
-in-Lab - - - -
Equipment Maintenance:
r
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot#:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot*
Exp. Date:
-Checked-with Traceable Thermometer Serial #:122703591- Cal Due Date:12/3/13
CAL.
TEMP. °C
CAL.
TEMP. oC
. QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
`t/r `r!`3'
'( tl �M
Li �f'-�
i lfl 1
��.i •�i3- -
I'(�1 b)fs;
r�.�i ,'�; .:,
� � � �!
�1•�!- �-�
� 4:
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH:=�-
2 HR
pH
2 HR
TEMP.°C.
'CORRECTED pH: t' ;�;' f c; _ I ;
24 H R
24 H R
pH
TEMP. °C
iJ"
j_G
CORRECTED pH:
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
- The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
r 'i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
'Document changes in lot #'s.
� revised: 9/9/13

PH Mt I tR CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
"Waynesville, NC 28785
SPA ID: NC01119
Certification * 194
instrument ID: VWR Symphony SB70P
S/N: 003367
" In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot#:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
PH4.0
BUFFER
PH110.0
BUFFER
PH 13.0
BUFFER
INITIAL
-EFF.
C.
,t/
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. oC
CORRECTED pH: i ) - -) : L:' . Vx- f . ,
2 HR
2 HR
pH
TEMP.oC
.,jRRECTED pH:
24 H R
24 H R
pH
TEMP. oC
4
CORRECTED pH: (,)L- � (( --L r ( -)-- G ), M
Pnet r'alihrntinn \/arificatinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
;— 'Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
( pH of this second reading has to be above a pH of 12.
i The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
t revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-SPA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp_ Date:
pH 13.00 Lot #:4309C86
Exp. Date:SEPT. 2014
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:122703591 Cal Due Date:12/3/13
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
ile i`
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. oC
CORRECTED pH:
2 HR
2 HR
pH
TEMP. °C
,,JRRECTED pH: i 'X - r:., C- _ f ),, `s `)
24 HR
pH
24 HR
TEMP. °C
� ORRECTED pH: t/ : ` > r'.1 u ti .)
Pn-,t (alihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
7H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
correction factor (CF) = 0.03 pH units '` (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
fhe initial pH reading is taken after the lime is mixed with the 503 sludge.
fhe pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

-t1 rrl IYIC 1 CIS %_KLIGISp►I IVIY rVR JVJ LIIYI G/a7L✓✓VL
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
'A ID: NC01119
Certification #: 194
,Instrument ID: VWR Symphony SB70P
- S/N: 003367
~1In Lab
Equipment Maintenance:
pH 4.01 Lot *A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot*
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal.Due Date:10/2/15
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 4.0
TEMP. oC
OF PH 4.0
BUFFER
CAL.
BUFFER
PH 10.0
TEMP. oC
OF PH 10.0
BUFFER
QC
BUFFER
PH 13.0
TEMP. oC
OF PH 13.0
BUFFER
INITIAL
DATE
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. oC
13
13
d
CORRECTED pH: la,
2 HR
pH
2 HR
TEMP.°C
CORRECTED pH:
24 H R
24 H R
pH
TEMP.°C
CORRECTED pH:
n..,.a l�..M., +;r \/crifir-nfinn
- -
Ph
Temp.
TIME
INITIAL
13.0
°C
91
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
' The initial pH reading is taken after the lime is mixed with the 503 sludge.
ate pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s. revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000(Aqueous)
Town of Waynesville WWTP
.66 Walnut Trail
Naynesville, NC 28785
"—A ID: NC01119
, Certification #: 194
nstrument ID: VWR Symphony SB70P
3/N: 003367
'n Lab
Cquipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot*
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
•DATE
TIME
SLOPE
EFF.
BUFFER
PH 4.0
OF PH 4.0
BUFFER
BUFFER
PH 10.0
OF PH 10.0
BUFFER
BUFFER
PH 13.0
OF PH 13.0
BUFFER
INITIAL
Ct
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
hI
CORRECTED pH: C" 0, J LC
2HR
pH
2HR
TEMP.°C
�,ORRECTED pH: �..r:....? I \ j � i ` -1 .
r`
24 HR
24 HR
pH`
TEMP. °C
(
3
i
CORRECTED pH: 6 7 ._ 13 —rt
r-j-+ Vcrifiratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
,--,.The pH of this initial reading has to be above a pH of 12.
`_- a second pH reading is taken 2 hours after the initial reading.
't i he pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

r
t-rl IVIC I CM I+HLIOMM I nim rVR DUO L11VIC/0LU1J%ZC
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
"- 566 Walnut Trail
-Waynesville, NC 28785
~A ID: NC01119
Certification #: 194
nstrument ID: VWR Symphony SB70P
r J,S/N:003367
In Lab
C-quipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot *4404169
Exp. Date:MAR. 2015
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 4.0
TEMP. °C
OF PH 4.0
BUFFER
CAL.
BUFFER
PH 10.0
TEMP. oC
OF PH 10.0
BUFFER
QC
BUFFER
PH 13.0
TEMP. oC
OF PH 13.0
BUFFER
INITIAL
. DATE
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: 1 D. k(' S, S X �
2 HR
pH
2 HR
TEMP. °C
1r
_CORRECTED pH: 9 � �; / `c;T G
24 H R
pH
24 H R
TEMP. °C
Q. I
( k.\,3
CORRECTED pH: i t ,+" r 5- -- r A C�
- -
Ph
Temp.
TIME
INITIAL
13.0
oC
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
t" -'-The initial pH reading is taken after the lime is mixed with the 503 sludge.
--, The pH of this initial reading has to be above a pH of 12.
a second pH reading is taken 2 hours after the initial reading.
I he pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
r Document changes in lot #IS. revised: 9/9/13
t

r 11 IYIL 1 LI\ %0r%L1LJ1\f1I IVIY I VI\ JVJ LIIYIIL11.7L.L0LJ\71L
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
'566 Walnut Trail
Naynesville, NC 28785
•.�A ID: NC01119
I Certification* 194
_Instrument ID: VWR Symphony SB70P
S/N: 003367
l'n Lab
quipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
' DATE
TIME
SLOPE
EFF.
BUFFER
PH 4.0
OF PH 4.0
BUFFER
BUFFER
PH 10.0
OF PH 10.0
BUFFER
BUFFER
PH 13.0
OF PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: -A. -
2 HR
pH
2 HR
TEMP. °C
t ) L-'Q(
-. C "-I
,CORRECTED pH: ()�,`V4 _y ,1,-'0„27'
24HR
pH
24HR
TEMP.°C
CORRECTED pH: / . a. , '(' _ !`5 1
�_'
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
'calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
r Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
-- 3 second pH reading is taken 2 hours after the initial reading.
( i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs. revised: 9/9/13

r'rl IVIC 1 E:M UALIGISH 1 IVIV rVR .7VJ LIINI G/JLIJ LlV IL
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
'566 Walnut Trail
Waynesville, NC 28785
4ID: NC01119
,YL; Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot#:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
Z�/ fy
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH'
INITIAL
TEMP.0C
CORRECTED pH: 01,
2 HR
pH
2 HR
TEMP.°C
�_. �_ 2
�
CORRECTED pH:
r,
24 H R
PH
24 H R
TEMP. °C
_��
6 1,
CORRECTED pH: fa-_26 - 0,
Ph
Temp.
TIME
INITIAL
13.0
°C
lL i5
r-15.
i3 :�)-3
k� F, ­
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade. .
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
-The pH of this initial reading has to be above a pH of 12.
�e second pH reading is taken 2 hours after the initial reading.
The pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

YH Mt 1 tK UAL11i1KA11UN 1-UK OW LIMt/SLULJUh
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Naynesville, NC 28785
=4A ID: NC01119
Certification #: 194
.nstrument ID: VWR Symphony SB70P
3/N: 003367
'n Lab
equipment Maintenance:
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
. CAL.
TEMP. oC
QC
TEMP. °C
%
TIME
SLOPE
EFF.
BUFFER
PH 4.0
OF PH 4.0
BUFFER
BUFFER
PH 10.0
OF PH 10.0
BUFFER
BUFFER
PH 13.0
OF PH 13.0
BUFFER
INITIAL
+DATE
'A-0
VA \hc
ff
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
r-_C
�ORRECTED pH
,
2 HR
PH
2 HR
TEMP.°C
CORRECTED pH: ) Z U " 0,12 ` 1,:1: 01
24 H R
24 H R
pH
TEMP.°C
.CORRECTED pH: / �. 2`t - �� l h = (� . L,�'r
N
0—+ (`nlihrntinn Vmrifirratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
10
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
,The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
.1
revised: 9/9/13

_ rl'7 IYIC 1 GR IiHLIGICN I IVIV 1'VI[ .7VJ LIIYIC/.7 LUIJ �7C
SM 4500-H-'B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
�A ID: NC01119
? Certification #: 194
,Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015 _
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
' DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
EA
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP.0C
r�1
'C.) Z)
j
I Iw
CORRECTED pH:
L )
2 HR
I
2 HR
pH
TEMP. °C
'CORRECTED pH: (y, — 0, 12 ' ( )-4-'
24 H R
24 H R
pH
TEMP. °C
ill L, —1
—0�1-(-
CORRECTED pH: t x
n . + t- el;hro+inn \/ariflnatinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
r The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
- - 3 second pH reading is taken 2 hours after the initial reading.
( ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of.11.5.
Document changes in lot #'S.
revised: 9/9/13

PH Mt 1 tK UALIMKA I IUN rUK OU3 LIIVIC/,LUUIaC
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
�-4k ID: NCO1119
Certification #: 194
Instrument ID: VWR Symphony SB70P
(-"'S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot*
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
ulo
CORRECTED pH: ( 7 - C" ! `, PL,
2HR
pH
2 H R�
TEMP.°C
'CORRECTED pH:
A 1 7I -- V
24 H R
24 H R
pl-{
TEMP. °C
( ',CORRECTED pH: ; n.•'t ?,
0—+ rnlihrn+inn \/crifirntinn
a:_ 7
Ph
Temp.
TIME
INITIAL
13.0
oc
1 0:'..L::
T_`�
( � ) i
'XU - i
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
t
The initial pH reading is taken after the lime is mixed with the 503 sludge.
-� The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
l ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'S.
revised: 9/9/13
r�

PH METER CALIBRATION FOR 503 LIME/SLUDGE
.qnn a.1;nn-H+B-2000 (Aaueous)
Town of Waynesville WWTP
566 Walnut Trail
`Waynesville, NC 28785
'AID: NC01119
..0 Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
DATE
i
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #: .
Exp. Date:
pH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
4 ,
CORRECTED pH:
2 HR
pH
2 HR
TEMP.°C
r,
'CORRECTEDpH: %' "�' �, /'"�
24 H R
pH
24 H R
TEMP.°C
CORRECTED pH: i <)" L " 1!;1- {1 1/
r.,Uk —+iron Vnrifir-n inn
Ph
Temp.
TIME
INITIAL
13.0
oC
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured- 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
."The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
" i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s. revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
'Waynesville, NC 28785
ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
PH 13.0
BUFFER
INITIAL
BUFFER
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
DATE
CORRECTED pH:
2 HR
PH
2 HR
TEMP.°C
1,2:7q
V2o;t, f
CORRECTED pH: 17 y �` • i _ l 2 �-
24 H R
PH
24 H R
TEMP.°C
, CORRECTED pH: (n17" r L ✓
j
0—f r`nlihrn+inn \/=rifirrafinn
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade: At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to'the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
,_. Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
` second pH reading is taken 2 hours after the initial reading.
ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
�)A ID: NCO1119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
•c 4
G>! /ti i V-
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH:
7
2 HR
pH
2 HR
TEMP. °C
CORRECTED pH: ! -�—' -) -
24 HR
pH
24 HR
TEMP. °C
"
, iv , .
CORRECTED pH: If - > -3
Pnat r'alihration VAfIfiC9tion
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH Mt I.tK GALMSKATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
;,Waynesville, NC 28785
"} "'A ID: NC01119
. ,C Certification #: 194
'Instrument ID: VWR Symphony SB70P
r ` S/N: 003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH:
13. -3 et -- 6. c �-r = 1.3: 3-3
l ?
t-'
2 HR
2 HR
PH
TEMP.°C
CORRECTED pH: • .j - `' • '2
-
24 HR 24 HR
pH TEMP. °C
t 3 LQ 8 !S` 0
,CORRECTED pH: / i`; - n.€'s ' ! ,' . - .
Dnc+ r nlihrn+inn Varifiratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
r
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
l ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-14+13-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
(. Waynesville, NC 28785
-EPA ID: NCO1119
Certification #: 194
` Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
PH 4.01 Lot #:
Exp. Date:
PH 10.01.Lot#:A3266
Exp. Date:SEPT. 2014
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
'
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
(Cf�
•.�
�9.42
.c'I
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: (? Y5 - 0, CV
2HR
2HR
PH
TEMP. °C
„JRRECTED pH:
24 HR
PH
24 HR
TEMP.°C
_., CORRECTED pH: 1A.-
Pnct r'.alihratinn VPrifir_atinn
Ph
Temp.
TIME
INITIAL
13.0
°C
I
@.
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
( The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
a pH of this second reading has to be above a pH of 12.
r The pH of the final reading (24 hours latter) has to be above a pH of 11.5,
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
,Town of Waynesville WWTP
566 Walnut Trail
- Waynesville, NC 28785
` —1A ID: NCO1119
Certification #: 194
Instrument ID: VWR Symphony SB70P
' SIN: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A3241
Exp. Date:AUG. 2017
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A3266
Exp. Date:SEPT. 2014
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
*130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: G- 4
2HR
2HR
pH
TEMP. °C
P�,�, ;?.
k ` t Vz
CORRECTED pH:
24 HR
pH
24 HR
TEMP.°C
j
4 � `�—ti�d
l L•�
CORRECTED pH:
Dr,c+ ('nlihra+inn Varifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
f5
t'-
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
T� Actual pH =Measured pH +/- the correction Factor.
! The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
a second pH reading is taken 2 hours after the initial reading.
r l ne pH of this second reading has to be above a pH of 12.
- The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
666 Walnut Trail
` Vaynesville, NC 28785
ID: NC01119
Certification #: 194
- .nstrument ID: VWR Symphony SB70P
i/N: 003367
n Lab
equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH.4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
,DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
Lj
i� � ,
qL
I
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
o.,�fti
CORRECTED pH: I r 'A i3L
f ,
t ,
2 HR
PH
2 HR
TEMP.°C
'CORRECTED pH:
24 H R
PH
24 H R
TEMP. °C
d�.q
.0_`t.,
' r
,CORRECTED pH: (, q I -�..a !
Pnet (nlihratinn Varifirntion
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
'calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
-Actual pH = Measured pH +/- the correction Factor.
IThe initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
i second pH reading is taken 2 hours after the initial reading.
a a pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
' SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
,566 Walnut Trail
Waynesville, NC 28785
--PAID: NCO1119
Certification #: 194
Instrument ID: VWR Symphony SB70P
_.SIN:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: - Exp. Date:
pH 10.01 Lot.*A4102 Exp. Date:APR. 2015
pH 10.01 Lot* Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
DATE
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 4.0
TEMP. °C
OF PH 4.0
BUFFER
CAL.
BUFFER
PH 10.0
TEMP. °C
OF PH 10.0
QC
BUFFER
PH 13.0
TEMP. °C
OF PH 13.0
BUFFER
INITIAL
^BUFFER
I
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH:
2 HR
pH
2 HR
TEMP. °C
CORRECTED pH: d
24 HR
24'HR
pH
TEMP. °C
CORRECTED pH: I J- 1-t cl - V . L' I )' 1-7-
n ..+ t- ,Nk—+'— Xlcrifir nfinn
Ph
Temp.
TIME
INITIAL
13.0
°C
i4l; `o
;"V,)
i, t
,pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
\ Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
e second pH reading is taken 2 hours after the initial reading.
.,e pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs. revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
SPA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0.
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
.tea°
.4-I
I 10
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP.0C
p
CORRECTED pH:
2 HR
pH
2 HR
TEMP. °C
' -;ORRECTED pH:
24HR
pH
24HR
TEMP.°C
CORRECTED pH: � i.. [A c t } P L
0--+ r`nHhro+inn Varifir-ntinn
Ph
Temp.
7TIME
INITIAL
13.0
°C
h, '. r c
I —A —ILL—
i :3 ; o t'
- i'l "I (.1
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
t Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
—tie second pH reading is taken 2 hours after the initial reading.
ie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

' ~1
PH METER CALIBRATION FOR 503 LIMEISLUDGE
SM 4500-H+B-2000 (Aqueous)
i" 'Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-�q ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
;'Equipment Maintenance:
PH
4.01 Lot #:A4105
Exp. Date:APR. 2018
PH
4.01 Lot #:
Exp. Date:
PH
10.01 Lot #:A4102
Exp. Date:APR. 2015
PH
10.01 Lot #:
Exp. Date:
PH
13.00 Lot #:4404169
Exp. Date:MAR. 2015
PH
13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
4.0
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
6 lei 1-
4 �-0�
��t.� ���
y ttPH
d.� �F )
iBUFFER
rh�`�y
iC",,)
n. �i
i � •'(� N^
!/� 3 r�
�T
I C�
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. oC
kV
CORRECTED pH:
2HR
PH
_2HR
TEMP. °C
CORRECTED pH:
24 H R
PH
24 H R
TEMP.°C
CORRECTED pH: i .� . ( ` ("t
r:)n-f r'-lihrn+inn Varifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
)PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
-. Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
Jhe pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 919/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
own of Waynesville WWTP
66 Walnut Trail
daynesville, NC 28785
'AID: NC01119
�,; Certification #: 194
u,nstrument ID: VWR Symphony SB70P
>/N: 003367
n Lab
equipment Maintenance:
DATE
cldcl !`f
PH 4.01 Lot #:A4105
Exp. Date:APR. 2018
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
TIME
SLOPE
EFF.
CAL.
BUFFER
PH 4.0
TEMP. °C
OF PH 4.0
BUFFER
CAL.
BUFFER
PH 10.0
TEMP. °C
OF PH 10.0
BUFFER
QC
BUFFER
PH 13.0
TEMP. °C
OF PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
14
CORRECTED pH: i . (, `i ' e Y. P-2 '5L6
2 HR
PH
2 HR
TEMP.°C
ICORRECTED pH:
24 H R
PH
24 H R
TEMP.°C
:CORRECTED pH: -CT`i- C%I
r�-._a l+..I:M...Fir.n \/crifir�4inn
-
- - -
Ph
Temp.
TIME
INITIAL
13.0
°C
j
�. l�
i '� i-� l��
� ''•fit^; y
-'
='pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
-� Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
)-.Tbe pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
- I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs. revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
( A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2115
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
�4'
�j �N
���. c�
� ? "
13
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: k I-)'-,- C., kX = (�-..L1
2 HR
pH
2 HR
TEMP. °C
(1� •6I
V. '-
CORRECTED pH: ( h
24 H R
pH
24 H R
TEMP. °C
CORRECTED pH:
Pnct (:;Iihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
1be pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I he pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
k ID: NC01119
Ivc; Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date: -
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:4404169 Exp. Date: MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: (�. �3� 0, Sl- i �:
2 HR
2 HR
PH
TEMP. °C
CORRECTED pH:
24 H R
24 H R
pH
TEMP. °C
CORRECTED pH: i _). - 4 c _. 0,1 � - CI-1 c7,
D^o+ ('nlihra+inn Varifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
r
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
e second pH reading is taken 2 hours after the initial reading.
The pH of this second reading has to be above a pH of 12.
y The pH of the final reading (24 hours latter) has -to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
1 SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-_"AID: NC01119
Certification #: 194
I Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
( i
PH 4.01 Lot #:A4105
Exp. Date:APR. 2018
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date: MAR. 2015
PH 13.00 Lot #:.
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
TIME
EFF.
PH 4.0
FFER
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
-^DATE
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
p
CORRECTED pH: QQ - - '-f -apt ' F. k a4-`a-
2 HR
PH
2 HR
TEMP.°C
{ k .l7 '1
.# i`i -`•i.
CORRECTED pH: � •{>_ "k ` `'' • t `? .. l;- P-, "y
24 HR
PH
24 HR
TEM.P. °C
CORRECTED pH:. - L
Dnc+ C'-mlihm+inn Varifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
r , Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
ne pH of this second reading has to be above a pH of 12.
" The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIMEISLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
�'A ID: NC01119
-,G Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH
4.01 Lot #:A4105
Exp. Date:APR. 2018
pH
4.01 Lot #:
Exp. Date:
pH
10.01 Lot #:A4102
Exp. Date:APR. 2015
pH
10.01 Lot #:
Exp. Date:
pH
13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH
13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
'
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: r 9 , 4 �
2HR
2HR
pH
TEMP.°C
CORRECTED pH: :�.• <p' f- r { `i
24 H R
pH
24 H R
TEMP.oC
CORRECTED pH: ;1 L i. `a t -�-.
Duet (`nlihrntinn VPrifinntion
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
` Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
,- Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I he pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

.PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
\'QA ID: NC01119
,rC Certification #: 194
' 'Instrument ID: VWR Symphony SB70P
I. . S/N: 003367
In Lab
Equipment Maintenance:
c�
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date.10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
Ift
LA
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. oC
CORRECTED pH: !
2 HR
pH
2 HR
TEMP.°C
p \ tt c€
7
CORRECTED pH:�
24 H R
24 H R
pH
TEMP.°C
CORRECTED pH: 3 t
o + r`nGhr-m+inn Varifirratinn
_ - -
-_--
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
i The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I he pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
= Waynesville, NC 28785
-�—pA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH.4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL.
j
-, d
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. 0C
CORRECTED pH:
2HR
2HR
pH
TEMP.°C
LORRECTED pH: 0 ,t,- 6 "" V ; i --) ~: } '-A' , 416
24 H R
24 H R
pH
TEMP. °C
CORRECTED pH: 1 . .6 C' ,,32 ' (.�--
Dnc+ r'olihra+inn Varifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
r..
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
` The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
Cr. , ie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000(Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
SPA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
SIN:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. 0C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
'
•.-�'�`
y$ ,,ma�-yy
Y i..' < <`. G,
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
,� ' f l i FS_t.
�� �, (... 4`
t';9 . i 'y
y
S� • t''C' .Y'
i �•y`
CORRECTED pH:
2HR
2HR
pH
TEMP. °C
1' . I, n
L,JRRECTED pH: i --7 . dw.: ' t <'i ,- /A - r_j
24 HR
24'HR
pH
TEMP. °C
CORRECTED pH: ( �;. —° . . / (�Lt
Pnct (:alihratinn VPrifirntion
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
t
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
e second pH reading is taken 2 hours after the initial reading.
!. .,e pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in. lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
,Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
---'A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot#:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date: 10/2/15
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH{;13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP°C
Q
.
CORRECTED pH: I A- ) - F,, = f ?, • 3 ?
2 HR
pH
2 HR
TEMP. °C
II."),�
, ,,�,i
CORRECTED pH: l )1k . �� - .. (V- C ' - 4 ), . }_- v
24 H R
pH
24 H R
TEMP. °C
CORRECTED pH:!
a
Pnct (-Plihratinn VPrificatinn
Ph
Temp.
TIME
INITIAL
13.0
°C
,pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
•Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
x
The initial pH reading is taken after the lime is mixed with the 503 sludge.
-- The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I. i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
' Waynesville, NC 28785
-`'A ID,: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
_ S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4106 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date: .
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
�N,r
+^✓
1
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. oC
fl./
CORRECTED pH: i ,) . (2 "i
2HR
pH
2HR
TEMP.°C
CORRECTED pH: a V0 `0 " " ( -A- 14'C'
24 HR
24 HR
pH
TEMP.°C
0
CORRECTED pH: /-`r -� • / ` 'fir
Pnct ralihrntinn Vpnfiratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
e second pH reading is taken 2 hours after the initial reading.
i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
iA ID: NC01119
Certification #: 194
j Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
t - i 1. t- s,;,-: i � .i'✓:'
PH 4.01 Lot #:A4105
Exp. Date:APR. 2018
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL. '
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
10.0
BUFFER
PH 13.0
BUFFER
INITIAL
gPH
1
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. oC
CORRECTED pH
.2 HR
PH
2 HR
TEMP. °C
CORRECTED pH: 1 x. r1 ,, ?-;-
24HR
PH
24HR
TEMP. °C
CORRECTED pH:
PnGt Calihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units " (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above.a pH of 11.5.
Document changes in lot #'s.
revised: 919/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
. ''A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. oC
CAL.
TEMP. °C
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE .
COLLECT
TIME
ANALYSIS
INITIAL
PH
INITIAL
TEMP. °C
\TIME
CORRECTED pH: ; , . ) ,y ` C, 1 0 = LL �; >
2 HR
PH
2 HR
TEMP.°C
3 � !': r'
�
CORRECTED pH:
24HR
24HR'
PH
TEMP. °C
CORRECTED pH: I ), -,_,? — C, -r 2: , t
Pnct ralihrntinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
_The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
oe pH of this second reading has to be above a pH of 12.
' The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
( F--'A ID: NCO1119
_, Certification #: 194
' Instrument ID: VWR Symphony SB70P
,S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot *A4105
Exp. Date:APR. 2018
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot #-.
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
ail
CORRECTED pH: it ) . (:4 - rs_ I J- � /A,f
2HR
pH
2HR
TEMP. °C
({{
CORRECTED PH:
Y
24 H R
PH
24 H R
TEMP. °C
CORRECTED pH: � -
Pnst Calihration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
i�
The initial pH reading is taken after the lime is mixed with the 503 sludge.
-,The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
(1 ie pH of this second reading has to be above a pH of 12.
-The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
i Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
1 —`'A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105
Exp. Date:APR. 2018
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot*
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
f
-\ 'ri:
P�'- _ :
�4 •i.>F'
�'y - t?`—
' e� �
! 1A` l
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
•� F L'
q
i _Z
i f
CORRECTED pH: - C- t -3-44U
2HR
2HR
PH
TEMP. °C
CORRECTED pH:
24 HR
PH
24 HR
TEMP. °C
CORRECTED pH: / , 4 `j - f I`s f A
Pnct (-alihrntinn Varifirratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
- -The pH of this initial reading has to be above a pH of 12.
le second pH reading is taken 2 hours after the initial reading.
I he pH of this second reading has to be above a pH of 12.
'Y The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
C, -IA ID: NC01119
'iC Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL -
°C
6 �•1 it 1 ��
'� �,
�'. �..:
�'*, • f �-'
^^yTEMP.
Alt-' . ��-
-, CORRECTED pH: i �l- • iJ . r' S
2HR
pH
2HR
TEMP.°C
'..~' CORRECTED pH: G
24 HR
pH
24 HR
TEMP. °C
CORRECTED pH:.'���
Pnct (;alihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
Ct
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
• The initial pH reading is taken after the lime is mixed with the 503 sludge.
,,.T-he pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
+. I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

rn IVIC I CK UALUSKA I IUN I-UIt 503 LIME/SLUDGE
i SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
.AID: NC01119
ivC Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
-� Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot* Exp. Date:
PH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
PH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. oC
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH:
2HR
PH
2HR
TEMP.°C
i .7If
,)0.0`c
CORRECTED pH:
24 H R
PH
24 H R
TEMP.°C
31
L
CORRECTED pH: 1 �1, �� .. e . I
Pnct Calihratinn Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
(--'The initial pH reading is taken after the lime is mixed with the 503 sludge.
-,,-The pH of this initial reading has to be above a pH of 12.
a second pH reading is taken 2 hours after the initial reading.
I'he pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIMEISLUDGE
SM 4500-H+B-2000 (Aqueous)
TIME
INITIAL
Ph
13.0
Temp.
°C
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-`10A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 00.3367
In Lab
-' Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
E+.,FF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
INITIAL
SBUFFER
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
6;y
z
CORRECTED pH:
2 HR
pH
2 HR
TEMP. °C
CORRECTED pH: i '-01-.
24 HR
pH
24 HR
TEMP.°C
CORRECTED pH: k :?
Post Calibration Verification
{
. pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade. -
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
'The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
to pH of this second reading has to be above a pH of 12.
-,The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
( Town of Waynesville WWTP
566 Walnut Trail
' - Waynesville, NC 28785
c ``-EPA ID: NC01119
Certification #: 194
v Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance: -
PH 4.01 Lot #:A4105
Exp. Date:APR. 2018
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
13.0
BUFFER
INITIAL
gDATE
gPH
r
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME_
TIME
PH
TEMP. °C
vt
CORRECTED pH: �. -A i - c i �k - 1-55
2 HR 2 HR
PH TEMP.°C
�-,JRRECTED pH
ti
24 H R
24 H R
pH TEMP.°C
f CORRECTED pH: 1
PnSt Calihrntinn Verification
TIME
�-,JRRECTED pH
ti
24 H R
24 H R
pH TEMP.°C
f CORRECTED pH: 1
PnSt Calihrntinn Verification
TIME
f CORRECTED pH: 1
PnSt Calihrntinn Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
-Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
- The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
-The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
� revised:9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
'Waynesville, NC 28785
NCO1119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
. INITIAL
DATE
TIME
TIME
PH
TEMP. °C
r ; CORRECTED pH: i' - _..t . 6 I - l
2 HR
2 HR
pH
TEMP.°C
CORRECTED pH: (r... o,;, - �• , i '� ; t, ``�
24 H R
24 H R
pH
TEMP.°C
,CORRECTED pH: I "_ ;.>, c, � a. f Via. `>_ a
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
Iu�
t'.' V
1°i1
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:,alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
= Actual pH = Measured pH +/- the correction Factor.
'The initial pH reading is taken after the lime is mixed with the 503 sludge.
the pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
' revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
^-)A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony S670P
1
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105
Exp. Date:APR. 2018
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot #:
Exp. Date. -
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
-
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER .
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
7)A -ice
CORRECTED pH:
i?
0
2 HR
PH
2 HR
TEMP.°C
1 ,2: 3i
le" .; C,
CORRECTED pH: I.. 3
24 HR
24 HR
PH
TEMP.°C
CORRECTED pH: !
Pnct C .glihratinn Verification
Ph
Temp.
TIME
I INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
a second pH reading is taken 2 hours after the initial reading.
I he pH of this second reading has to, be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a -pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
.� SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
"'A ID: NC01119
.� Certification #: 194
Instrument ID: VWR Symphony SB70P
'S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot*
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
IC(,ct
i3.,c)
6`'C
COLLECT
ANALYSIS
INITIAL
INITIAL
TIME
TIME
PH
TiE�MP.'C
}DATE
CORRECTED pH: i>1: z�!o - C- i 6 _. 1,?..,0F
2 HR
pH
2 HR
TEMP.°C
CORRECTED pH
n
24 H R
pH
24 H R
TEMP.oC
,CORRECTED pH
Pnct C Plihrntinn Varificatinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours [after) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

rn ivii= i cry L mi-iDmm i iury rum ous L11v1c1aLUUt-7t
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
r--°A ID: NC01119
. Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
Exp. Date:APR. 2018
Exp. Date:
Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot*4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
pH 4.01 Lot #:A4105
pH 4.01 Lot #:
pH 10.01 Lot #:A4102
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
ef
C°'
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: ;, ". -�. ,� . i ,,; ;', *
2 HR
2 HR
pH
TEMP. °C
I�,uRRECTED pH: i7cn: (--L - 0 15 = 0- 1
24 FIR
pH
24 HR
TEMP. °C
CORRECTED pH: (:I '� I .. '--1A -•3 6
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
R,,
L l t./
,i ,
:: 0 x
� .
mot, - _ '�
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
-alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
'�'-o second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Naynesville, NC 28785
` A ID: NC01119
Certification #: 194
,Jnstrument ID: VWR Symphony SB70P
5/N: 003367
1n Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot* Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot* Exp. Date:
PH 13.00 Lot*4404169 Exp. Date:MAR. 2015
PH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:1012/15
CAL.
TEMP. °C
`CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10-.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
�Ei3
0
0,
q«�'"1
�?%.tl`'�
i0,rlr
61, eF'
13;oei
11 7
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
-7 7'
'3'C
19,0
CORRECTED pH: 1
2 HR
PH
2 HR
TEMP. °C
-ORRECTED pH: >: S-yi _. 6; V F -= 1—�z I i
24 H R
PH
24 H R
TEMP. °C
Y
CORRECTED pH: �'� �° / = ,3
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
1,
g.7.`+�n'`j
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
' a pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
"A ID: NC01119
Certification #: 194
` Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date. -
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
*130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
lJ lry
7. 50
j D. s,v
0.&1
IT(I—C
i�£;fj4
�C'; l ^d.
� �: c? 8
�Lj •t?fc"..
�i Y.
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
i
_3
CORRECTED pH: :. S _ T a;2 ; y�5
2 HR
2 HR
pH
TEMP. °C
z..
CORRECTED pH: 12.q :3 - 0, - 1-?: ? 6
24 H R
pH
24 H R
TEMP.°C
'- CORRECTED pH
Pnst Calihration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
r,
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
'Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
'-'Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I he pH of this second reading has to be above a pH of 12.
' The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
^"'A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
qh
L'
50 ?
LI �
7
I9<
3, Cj
.
i� e' "e,q/1
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. oC
CORRECTED pH:
2 HR
pH
2 HR
TEMP.°C
CORRECTED pH: l 0: 1 r1 - ) -Q , ..3 S­
24 H R
pH
24 H R
TEMP. °C
". i
AC `'
CORRECTED pH: a. 3'
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units " (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
A ID: NC01119
,.0 Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot *A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: (, -?-% ,0 •(')- (I,, C `�
2 HR
2 HR
pH
TEMP.°C
CORRECTED pH: d) — ) -- 0- 11� -- +� � `� ' -
24 HR
24 HR
pH
TEMP.°C
i �, '5 t
i- 8- )
CORRECTED pH:�
Pnst Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
'The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
3 second pH reading is taken 2 hours after the initial reading.
I he pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s..
revised: 9/9/13
r

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
_EPA ID: NC01119
'C Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
91)
Cl- -
—0
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH:
2 HR
2 HR
pH
TEMP. °C
I A
,,JRRECTED pH: t "-); i - o-i = 471 _5T 3
24 HR
pH
24 HR
TEMP. °C
q J
d _-1 T
CORRECTED pH: 0 - i - , t 7 13
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
;actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
the pH of this initial reading has to be above a pH of 12.
t"e second pH reading is taken 2 hours after the initial reading.
✓ a pH of this second reading has to be above a pH of 12.
-- The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
"Document changes in lot #'s.
C
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
,Town of Waynesville WWTP
566 Walnut Trail
'Waynesville, NC 28785
'A ID: NC01119-
:4C Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
` ,
�y''`j .14
9 - d;,%
(
1 t J . G
l t °i
1
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH:
2HR
pH
2HR
TEMP.°C
CORRECTED pH:
24 H R
24 H R
pH
TEMP.°C
\ 'CORRECTED pH: (, "i 6A. -3 r1
Dnct ( nlihratinn Varifirntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
3 second pH reading is taken 2 hours after the initial reading.
The pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 919/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
"'A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot *A4105 Exp. Date:APR. 2018
pH 4.01 Lot* Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 201.5
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
+ `
• C k
\ . io "
f 4;` .' i
c�.1� ' "< '
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: ii. 14 - C,
2HR
2HR
pH
TEMP. °C
CORRECTED pH: (1.•`ic— C1,I-5 ; (}• I)-"
24 HR
pH
24 HR
TEMP. °C
CORRECTED pH: + (� • `� I C , A ( t1 ),
Pnct r.nIihratinn Varifirntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot 9s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIMEISLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
'---'A ID: NC011,19
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105
Exp. Date:APR. 2018
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date: MAR. 2015
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
*130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BU�3FFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
z�/17"/r-r
`1v
���j.
L 0
(mil-�
(�i
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: f A. (, ( --0,C r f A , ," �)--
2HR
PH
2HR
TEMP. °C
)0
i 7 , i-,
CORRECTED pH: Oa->L -e<07;
24 HR
24 HR
PH
TEMP. °C
CORRECTED pH: ► �� . c_" - �' `i
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
r ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
~°A ID: NC01119
F .. Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot* Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date: MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
QC-:". l
(0
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
°C
i�4 -
4
p 4�
,TEMP.
CORRECTED pH: CA,
2 HR
pH
2 HR
TEMP. °C
-� c' 7 e,
CORRECTED pH: 1• : qd -&: I- = ld:.3,2
24 H R
pH.
24 H R
TEMP.°C
�
t
CORRECTED pH:
Pnct rniffirntinn VPrifir ntinn
TIME
INITIAL
Ph
13.0
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
- Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
( `The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH 'of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours [after) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9113

i
PH METER CALIBRATION FOR 503 LIMEISLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
�"A ID: NC01119
,C Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
co
CORRECTED pH:
2 HR
PH
2 HR
TEMP. °C
CORRECTED pH:
24 HR
PH
24 HR
TEMP. °C
CORRECTED pH:
Pnst CAihr2tion Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
_actual pH = Measured pH +/- the correction Factor.
%'The initial pH reading is taken after the lime is mixed with the 503 sludge.
,_ `T:he pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
`Document changes in lot Vs.
' revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
;`"--PA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105
Exp. Date:APR. 2018
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. oC
CORRECTED pH: i • `s) - K_,_ t _ �� - .�s
2 HR
ppgH
2 HR
TEMP. °C
`\
C
r•� ' 4'
CORRECTED pH: i,
24HR
24HR
PH
TEMP. °C
CORRECTED pH: -'• ; i '
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
pie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

rn IVIC 1 CM 1rHLI0r%A I IVN rVK OW LIIYIt/JLUUht
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
- "A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
i S/N:003367
In Lab
- Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #-A4102 Exp. Date:APR. 2015
PH 10.01 Lot* Exp. Date:
PH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15'
CAL.
TEMP. oC
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
�t
t
�.
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: fc = )4. Q, 64
2 HR
PH
2 HR
TEMP. °C
,CORRECTED pH: L: zi
24 HR
PH
24 HR
TEMP.°C
.
.El -
CORRECTED pH: IA, (t � • t / � +�
Pnst f niffirntinn Verificatinn
TIME
INITIAL
Ph
13.0
Temp.
°C
-pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor,
r- ,The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
' , second pH reading is taken 2 hours after the initial reading.
ne pH of this second reading has to be above a pH of 12.
,-The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

J
' 1
PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
FI 566 Walnut Trail
Waynesville, NC 28785
-'A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot *4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
�
a
/
CORRECTED pH: �.�'� �'• '(a..c
2HR
pH
2HR
TEMP.°C
'CORRECTED pH: (r,. J _. e--, t < _ 11- 6, t
24HR
pH
24HR
TEMP. °C
`.CORRECTED pH: Q- =2q -0 "/Y-
Pnct C:glihratinn Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
}
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
� ,Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
%The initial pH reading is taken after the lime is mixed with the 503 sludge.
,The pH of this initial reading has to be above a pH of 12-
? second pH reading is taken 2 hours after the initial reading.
f ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

rri Mr- 1 CK UALIMMA I IVry rum OU3 LIIVICIOLUUIoC
~ SM 4500-H+B-2000 (Aqueous)
- Town of Waynesville WWTP .
l 566 Walnut Trail
Waynesville, NC 28785
SPA ID: NC01119
r ; Certification #: 194
Instrument ID: VWR Symphony SB70P
! S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot *A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
<:
Ct
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: )N -C , `r
2 HR
pH
2 HR
TEMP. °C
`%,JRRECTED pH: `A • (.r. �:,- r r.;` ... ; .. S
24 HR
pH
24 HR
TEMP.°C
CORRECTED pH: I „.. `I a": t ; /k ..�
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
f '.0.3
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
^`e second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13
T�

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
'A ID: NC01119
.0 Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
` "oo
I\its
b l •Q (.i
'6 _?. t iF
27 7
i
COLLECT
ANALYSIS
INITIAL
INITIAL
TIME
TIME
PH
TEMPT. °C
rDATE
_. CORRECTED pH: ',
r '
1
r-
2 HR
pH
2 HR
TEMP. oC
f
CORRECTED pH:
24 HR
pH
24 HR
TEMP. °C
CORRECTED pH: I. �. - `y " �- , ! - B a - 3 i.,
Pnct r..alihrntinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
` Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
T e pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

NH Mt 1 tK GALItiKA I IUN I -UK 5US LIMt/SLUUUh
SM 4500-H+B-2000 (Aqueous)
,1 Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-;�PA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot *A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp.. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. oC
CORRECTED pH: i 5
2 HR
pH
2 HR
TEMP.°C
(a, 3q
( 0,
_ uORRECTED pH:
24 HR
24 HR
pH
TEMP. °C
CORRECTED pH: i A_ )-9� -c' - P � 1,� (c, Z)
Pnct ('nIffiratinn Varificatlnn
Ph
Temp.
TIME
INITIAL
13.0
°C
,pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
--,Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
rThe initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
ie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours [after) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUU(at
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
--_ r Waynesville, NC 28785
"``711A ID: NC01119
Certification #: 194
. Instrument ID: VWR Symphony SB70P
SIN: 003367
In Lab
'Equipment Maintenance:
PH 4.01 Lot *A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot *A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot *4404169 Exp. Date:MAR. 2015
PH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:1012/15
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
L .�;
1,t-
ts' -�,
r.�;
COLLECT
ANALYSIS,
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. oC
CORRECTED pH: i '=; i -
2HR
PH
2HR
TEMP. °C
CORRECTED pH: ~'s " 7 z I
24 H R
PH
24 H R
TEMP. °C
CORRECTED pH:
Pnct (alihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
— Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
'Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
< _ The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i fie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
{. Waynesville, NC 28785
,"---'A ID: NCO1119
Certification #: 194
Instrument ID: VWR Symphony SB70P
' S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot* Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date: -
pH 13.00 Lot#:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
_
CAL.
TEMP. °C .
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
d;
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
96
1 CORRECTED pH:r.>•
2 HR
pH
2 HR
TEMP.oC
�tt.•�r:
CORRECTED pH: 1 �. -�, �' ► `� f-��
24 H R
pH
24 HR
TEMP.°C
,CORRECTED pH:
( Post Calibration Verification
�J
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
— Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
,The initial pH reading is taken after the lime is mixed with the 503 sludge.
_-, The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
_ Document changes in lot #'s.
revised: 9/9/13

PH Mt I tK UALItfKA 1 IUN I -UK OW LIMtJILUUCat
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
)Waynesville, NC 28785
'A ID: NC01119
,C Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot *A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH4.0
BUFFER
PH 10.01
BUFFER
13.0
BUFFER
INITIAL
L4 itr
dPH
1
.
1
CORRECTED pH
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
!
i �i i %��
J' C t
�'-""3 �?
� ` i` �
{
�j rT ` l:"l
\ r
OL tom' •��
2 HR
2 HR
TEMP.J.00
jpH
CORRECTED pH: I, 5 5 �` l - '
i
24 HR
pH
24 HR
TEMP.°C
.CORRECTED pH: ;',.�. ; - �- - ! 3.4 ?-
ra
Pnct (nlihratinn Varifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
4
� ' o
tv, i -J.
V3. 05
L1 p
I - o i!
S
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
— Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
J Actual pH = Measured pH +/- the correction Factor.
' s
,The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
1 he pH of this second reading has to be above a pH of 12.
-----,The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/5L000t
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
)Waynesville, NC 28785
41D: NC01119
Certification #: 194
- Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
l Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot* Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2115
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER-
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. oC
CORRECTED pH: i `« •y G
2HR
2HR
pH
TEMP. °C
I" -t
:ko , y`
CORRECTED pH: i. ��4 •mot-U
24 HR
24 HR
pH
TEMP. °C
f q 3
) CORRECTED pH: t 1 C , / - ' Q,'4 .
D-c+ ('nlihrn+inn Varifiratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
f
Y
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
-The pH of this initial reading has to be above a pH of 12.,
e second pH reading is taken 2 hours after the initial reading.
fhe pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
`k ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
1n Lab
Equipment Maintenance:
pH 4.01 Lot *A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot* Exp. Date:
pH 13.00 Lot *4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
10.0
BUFFER
PH 13.0
BUFFER
INITIAL
rf °�fC-��f�+l
•? 3 i'
��" S �
`"l ` }.� lrJ���
• � �
yPH
i �� ` � �Y
��t . �
� � . U�'Y'
� .C, 4 �
--�-. <..'
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
i
CORRECTED pH: i i<
2 HR
2 HR
pH
TEMP. °C
CORRECTEDpH:
24 HR
pH
24 HR
TEMP. °C
IA<,rQ:>
CORRECTED pH:
Dnct r`nlihrntinn Varifiratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
- pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion .
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
'The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I he pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13
0

PH MEl tK GALIUKA I IUN f UK Sus LIMt/JLUIJUM
t SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
.566 Walnut Trail
.,Waynesville, NC 28785
,EPA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367 -
`y In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH:
2HR
2HR
PH
TEMP. °C
JRRECTED pH:
24 HR
PH
24 HR
TEMP.°C
-6--3
M.1
CORRECTED pH:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard'temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 1.2.
1" a second pH reading is taken 2 hours after the initial reading.
a pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
_'Document changes in lot Vs.
revised: 919/13

PH METER CALIBRATION FOR 5133 LIMt/SLUU(it
J, SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
4 ID: NC01119
Certification #: 194
'Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015.
pH 13.00 Lot* Exp. Date:
Checked with•Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
'((a/'f
2, l 5
nEFF.
��
.t9
� .��`
(� , �?
�Lt,��o
� c
i c�.
5-
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: f
2 HR
pH
2 HR
TEMP.°C
0,17 0
��` ,
_CORRECTED pH: i l l
24HR
pH
24HR
TEMP. 0C
J
' fi
p
CORRECTED H: I ),. C� `r 0 r `"' -
D„c+ (`nlihra+inn Varifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
L'•
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
J`The initial pH reading is -taken after the lime is mixed with the 503 sludge.
:Cie pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I ne pH of this second reading has to be above a pH of 12.
.The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H-'B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
kaynesville, NC 28785
\ ID: NC01119
yt; Certification #: 194
instrument ID: VWR Symphony SB70P
3/N: 003367
n Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot* Exp. Date:
PH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
c.0 5'' 3
�- - t�' d
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE,
TIME
TIME
PH
TEMP. °C
Ck
CORRECTED pH: -1 / L -7
2HR
PH
2HR
TEMP.°C
:,ORRECTED pH: 91 ) t /tea '=
24 H R
pH
24 H R
TEMP.°C
' f
--ORRECTED pH:
0 + ('n1ihrn+inn Varifinnfinn
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
I" " Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
- Actual pH = Measured pH +/- the correction Factor.
( The initial pH reading is taken after the lime is mixed with the 503 sludge.
=he pH of this initial reading has to be above a pH of 12.
e second pH reading is taken 2 hours after the initial reading.
The pH of this second reading has to be above a pH of 12.
r The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH Mt I t_K UALIUKAI IVM ruK Sus LIIVIC/JLuuvC
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
W,-iynesville, NC 28785
k ID: NC01119
NC Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105
Exp. Date:APR. 2018
PH 4.01 Lot*
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
a! tfi / l
` 1 �U
/-E�.F�•F.
` J
j
1� h/
'�`C'
, ls'
ri"'y
P -r
t
) p f
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: k.
2HR
PH
2HR
TEMP.°C
t i
:-Z, �
CORRECTED pH: 0., 7"-.c,--1 ... 0- 5 `2
24 H R'
24 H R
PH
TEMP. °C
CORRECTED pH: ' "-'� l try 4 ~' . L1 L�
Dnc+ ('olihratinn Varifinn inn
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
she pH of this initial reading has to be above a pH of 12.
,-le second pH reading is taken 2 hours after the initial reading.
The pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9113

PH METER CALIBKA I IUN 1-UK 5U"S LIMt15LU1JUt
SM 4500-H+B-2000 (Aqueous)
,Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
^�, ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
SIN: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot#:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
'BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
Chi. 4>�°
��i•
�: 4zt
CORRECTED pH:
2HR
2HR
pH
TEMP.°C
CORRECTED pH:
24 H R
pH
24 H R
TEMP.°C
S
3s%
-CORRECTED pH: ( o l = Jti • 3
Dnc+ ('olihmfinn Vorifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
:The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I he pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

1JN Mt I tK UALMSKA 1 iuN rum Ou3. LIIVIC1QLUUl7C
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
�"� ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
SIN: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot#:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
DATE
TIME
SLOPE
EFF.
BUFFER
PH 4.0
OF PH 4.0
BUFFER
BUFFER
PH 10.0
OF PH 10.0
BUFFER
BUFFER
PH 13.0
OF PH 13.0
BUFFER
INITIAL
,
,
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH:
2 HR
pH
2 HR
TEMP. °C
CORRECTED pH: 1',), d;e5 - L',0 1. 3
24 H R
pH
24 H R
TEMP. °C
li C)a?/
—:�LG,,f
CORRECTED pH: /
0—+ !'`nlihrn+inn Varifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
Tie pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
( I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

VH Mt 1 tK UALIUKA I IVIV rum OU3 LIIVIC/JLUL)"r-
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
'41D: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
pH 4.01 Lot #:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2018
Exp. Date:
Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date -.MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
TIME
EFF.
PH 4.0
BUFFER
Pi H 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PHA
INITIAL
TEMP. °C
CORRECTED pH: t a .? � `c=, t-:�- 7 !} L -�
2 HR
2 HR
pH
TEMP. °C
CORRECTED pH: 7--t C, - if* = 12. 5 1
24 H R
pH
24 H R
TEMP. °C
r, i. ":"
(`i r�"
CORRECTED pH: ( ) t `5 r `} /' - `i L
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
C,
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I he pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH Mt tK t;ALIbKAI IUN r•VK Sus LIMt/'LLIUUt
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
.-'::PA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot *4404169 Exp. Date:MAR. 2015
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. 0C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
rill jJ/ t _
jam t'Y)
� 1 `)
1
CORRECTED pH: ( ) -5;kR 0, (`�
2 HR
PH
2 HR
TEMP.°C
wRRECTED pH: 1-,) ) d: --Q, K �I
24 H R
PH
24 H R
TEMP.°C
CORRECTED pH: ( 0. - t%
Pnct ('alihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
`e second pH reading is taken 2 hours after the initial reading.
ie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH Mt I tK UALIUKA I IUN I -UK bU3 LIMt/5LU1JUt
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
``4 ID: NC01119
.. Certification #: 194
Instrument ID: VWR Symphony SB70P
'S/N:003367
In Lab
'Equipment Maintenance:
pH 4.01 Lot *A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial 4:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
Ci-
o
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP.0C
CORRECTED pH: I' —)-'S ? - --. 15 J I u13-
2HR
pH
2HR
TEMP. °C
tr
CORRECTED pH: c ` ! `� d3 C:, 5-
24 H R
24 H R
pH
TEMP.°C
CORRECTED pH: - .t ?- = 11- f; Lt
Pnct r'.alihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
- -Itie pH of this initial reading has to be above a pH of 12.
' : second pH reading is taken 2 hours after the initial reading.
I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous) -
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
—`'A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot ##:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
TIME
EFFp.
PH 4.0
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
a1DATE
\BUFFER
%
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
420
1:ct...
IV,I
CORRECTED pH: ,),•7011 -0
2 HR
PH
2 HR
TEMP.°C
CORRECTED pH:
24 HR
PH
24 HR
TEMP. OC
7 � i � �
� � : tJ •K.
CORRECTED pH: i 3
Pnct (' lihrntinn Varifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION .FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
% ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF..
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
s
�INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. oC
CORRECTED pH: 1 H = `i - c� . r S` 1 q . q q
2 HR
pH
2 HR
TEMP. °C
—i
CORRECTED pH: 1r..'� ZI o.-S= /-2_ ?'`t
24 HR
pH
24 HR
TEMP.0C
CORRECTED pH: tA.-C,.lS, = /A-. 3
Post Calibration Verification
Ph
.Temp.
TIME
INITIAL
13.0
°C
C-
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
Tize pH of this initial reading has to be above a pH of 12,
second pH reading is taken 2 hours after the initial reading.
The pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUD(3t
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
`"A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab -
Equipment Maintenance: .
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot* Exp. Date:
pH 13.00 Lot#:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP.•°C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: I 1 ac31A 5,
2 HR
2 HR
pH
TEMP.oC
CORRECTED pH: { .0 f- e i - IL 2 (e-
24 H R
24 H R
TEMP.oC
ppH
X6
CORRECTED pH: ta.• > +' -I:1. �_f�...
Dnc+ ('niihmfinn Varifinntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
iG, c,,-.
T 7
I I . ;z� o
I )(3-I
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
le pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot;Ws.
revised: 9/9/13

F'H IVIL I CK I:ALItSKA 1 IUN 1-UK OU3 LIMt/5L000t:
SM 4500=H+13-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
—''A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
Ufa,?f 1 `t
;:)-c'
0
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. oC
-Rf5
CORRECTED pH:
2 HR
pH
2 HR
TEMP.°C
CORRECTED pH: 1 3,- b'q .-C k
24 H R
24 H R
pH
TEMP.//°C
CORRECTED pH:
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
- Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

NH Mt 1 tK GALMSKA 1 IUN I UK 5U3 LIMt/JLUUVt
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail pH 4.01 Lot *A4105 Exp. Date:APR. 2018
Waynesville, NC 28785 pH 4.01 Lot #: Exp. Date:
---`'A ID: NCO1119 pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
Certification #: 194 pH 10.01 Lot #: Exp. Date:
Instrument ID: VWR Symphony SB70P pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
S/N: 003367 pH 13.00 Lot #: Exp. Date:
In Lab
- Equipment Maintenance:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
'�'It��
i.'�t
`�-�
•cam{
Tf�,�
G 4
? iL
��.�t
,�
; >
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH:
2 HR
2 HR
PH
TEMP. °C
CORRECTED pH:
24 H R
PH
24 H R
TEMP. °C
CORRECTED pH: I A `'e I 0 , / :) 7 '?,
Post Calibration Verification
INITIAL
Ph
13.0
Temp.
°C
yppTIME
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
e second pH reading is taken 2 hours after the initial reading.
oe pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

NH ME 1 ER CALIBRATION FOR 593 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
a Waynesville, NC 28785
—OA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot*
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. OC
CAL.
TEMP. OC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
��ii713�I
! , j�
�A�"3-
aje
la
ctx
�1�,.it'
���;�
Ii +�.
.*
r •�
j
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. OC
1'c cl
CORRECTED pH:
2HR
pH
2HR
TEMP. OC
CORRECTED pH: 12 ,`15?
24 HR
24 HR
pH
TEMP. OC
n
CORRECTED pH:
Po-,t (alihration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
,pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units'` (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i pie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH Mt 1 tK UALItiKA I IUN t-UK 5U3 LIM11=/5LUIJUE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
Certification #: 194
_.- instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:4404169 Exp. Date: MAR. 2015
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal. Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
4.0
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
ak
yyP��H
1BUFFER
C:' l
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
(Cl
CORRECTED pH: ( 1, 5 1 � _ (a.. (,7
2 HR
PH
2 HR
TEMP. °C
@
—jRRECTED pH: � `�. ?� C• ae:.i '. �,?.G 7
24 H R
PH
24 H R
TEMP. °C
CORRECTED pH: U.. E ' -e• 1 .2 i',A- c '?
Pnct C'alihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading. is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
T19 second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

1'19 IVIC 1 CK WALIOMA I IUN rUK OU3 LIIVIC/JLUWUM
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
i °AID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003387
In Lab,
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot#:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: (: , `t 9- - v' • 14 --
2 HR
pH
2 HR
TEMP.°C
z LL'
CORRECTED pH:
24 HR
24 HR
pH
TEMP. °C
•� t
U
CORRECTED pH: i ' - 1-' % t A"• 7 -7
Pnst Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
H
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
— Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH Mt 1 tK GALItiKA I IUN FUK 5U3 LIMt/SLU1JUt
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
—"A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date: .
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. 0C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
,
CORRECTED pH:-j_�%•_
2 HR
2 HR
pH
TEMP. °C
i;z-6v-
fq•`_)
CORRECTED pH:
24 H R
pH
24 H R
TEMP.°C
CORRECTED pH: G- r?
Dne+ ('nlihmfinn \/arifiratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
- pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
I
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
--"A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
1 .- .7`�
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: �, `� «= P "--70
2 HR
pH
2 HR
TEMP. °C
F
rc' - 's
CORRECTED pH: i c)• `? G •i = (, /n
24 H R
pH
24 H R
TEMP. °C
y
CORRECTED pH: f - � 4 - c •t -? i 1 ('
Pnct C alihratinn VPrificatinn
Ph
Temp.
TIME
INITIAL
13.0
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
- correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
iie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

1'H Mt I tK I:ALItSKA I IUN 1-UK 5Ud LIIVIt/SLU1JUt
SM 4500-H+B-2000 (Aqueous)
l
T
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
--'AID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
r
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2115
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
c�.
(I\•c Q
m
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
a
CORRECTED pH: Q. 44
2 HR
pH
2 HR
TEMP.°C
CORRECTED pH: J2;1v i '- 0� j,) - 12: 5 7
24 HR
pH
24 HR
TEMP. °C
/, '.1 - Q-
A I.1 ---V
CORRECTED pH:
Pnet (nlihrntinn Varifiratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

VH Mr-1 CK UALI[SKA1IVIV t"UK OU.f LIIVI1=/5LUUUt
r SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
`FDA ID: NC01119 -
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
EFF.
PH 4.0
BUFFER
PH 10.0
PH 13.0
BUFFER
INITIAL
J'r4Ai�6`�
rTIME
f C.3�'
E��j.�
` �' �1
,��t �.
ice' Q�
rBUFFER
J 1�
i
�t S 4
�`-
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
Vr.aVI'i
��
. _ 6� "
i � v
-�' .-1 Y
CORRECTED pH:
2HR
pH
2HR
TEMP.. °C
`CORRECTED pH: t �. "X, 'C; C,'; - 0"1 1
24 H R
pH
24 H R
TEMP.°C
CORRECTED pH: 6 £ -'.,t
IPnct (-. lihrntinn \/arifiratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
- Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

- PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-__"'�'A ID: NCO 1119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: P -7't tom°. f 2�
2 HR
2 HR
pH
TEMP.oC
I`
CORRECTED pH: f . ` _G 15 r.�, IS
24 HR
pH
24 HR
TEMP.°C
CORRECTED pH: . � . 2? -C G
Pnct C niihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
Q. X 7
I `'-,
Y?- v�.
(q, L
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
_,alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
;'- The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
I ne pH of this second reading has to be above a pH of 12.
r ` The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

I'M Mt I tK UAL11i11A I IUN 1-UK 5U3 LIMt/5LUU(at
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
{ 566 Walnut Trail
Waynesville, NC 28785
-1--PA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
li
PH 4.01 Lot #:A4105
Exp. Date:APR. 2018
PH 4.01 Lot*:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
/
.•- cad �,,�
P1
r �i�
(Qi
>
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
���/��
�;.••�a
".�• /fig
.z
��•7
CORRECTED pH:
2HR
PH
2HR
TEMP. °C
CORRECTED pH: 0_ 2-i -gj -; -
24 H R
PH
24 H R
TEMP.°C
;)
` . �
CORRECTED pH:
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
-alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
r The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
, ,e pH of this second reading has to be above a pH of 12.
.The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

VN IVIt I tK UALIIJKA I IUN I -UK 5U;5 LIML15LUDUE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
EPA ID: NC01119
Certification #: 194
instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
_ Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot#:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. oC
/ /
CORRECTED pH: a
2HR
pH
2HR
TEMP. oC
-jRRECTED pH:
24 H R
pH
24 H R
TEMP.'C
CORRECTED pH: /2, -Cl 'r. ."`/' I )-, �?' 3
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
`-
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
— Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
=he second pH reading is taken 2 hours after the initial reading.
e pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
l Document changes in lot #'s.
revised: 9/9/13

PH Mt I tK GALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-1-PA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: • Exp. Date: -
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot#:4404169 Exp. Date:MAR. 2015
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:1012/15
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
10.0
BUFFER
PH 13.0
BUFFER
INITIAL
dd
pPH
9 o-
rlA, C, —
i • i
i ` y �
c%
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: i
2 HR
2 HR
PH
TEMP.oC
t.,ORRECTED pH:
24 H R
24 H R
PH
TEMP.°C
CORRECTED pH:
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
nH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
-Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
the pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
PH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours [after) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

rrn Mr- I trc UALMSKA I IUN FUK 5U3 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-SPA ID: NC01119
C Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot#:4404169 Exp. Date:MAR. 2015
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
i I-?,
iifi.5/Eif'
_{.
-C .
i 7_.
f
1 `''
i
1,C-
t i
2
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
'CORRECTED pH:;7-
2 HR
PH
2 HR
TEMP. °C
,( A.�,5
t `t - -,)-
.;ORRECTED pH: i•• ' `; `<r .. t I' G
24 H R
24 H R
PH
TEMP.°C
CORRECTED pH:
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
L)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
.alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
r�
,Correction factor (CF) = 0.03 pH units'` (Temp. Measured - 25 Centigrade).
actual pH = Measured pH +/- the correction Factor.
—he initial pH reading is taken after the lime is mixed with the 503 sludge.
-he pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
..e pH of this second reading has to be above a pH of 12.
-he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Jocument changes in lot #'s.
revised: 9/9/13
�-t

IJH Mt I tK GALIIJKA I ION FOR 503 LIME/SLUDGE
SM 4500-H+13-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
'r"A ID: NCO1119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
pH 4.01 Lot #:
pH 10.01 Lot #:A4102
pH 10.01 Lot #:
pH 13.00 Lot #:4404169
Exp. Date:APR. 2018
Exp. Date:
Exp. Date:APR. 2015
Exp. Date:
Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
L
CORRECTED pH: 1' . 71 -r = 6 C' /
2 HR
pH
2 HR
TEMP.°C
CORRECTED pH: i ; i{ - c; G" /A.C, ?
24 HR
24 HR
pH
TEMP. °C
CORRECTED pH: LA q'4 L-17=12 r,,`7
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
;alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
fhe pH of this initial reading has to be above a pH of 12.
_ second pH reading is taken 2 hours after the initial reading.
i , ,e pH of this second reading has to be above a pH of 12.
fhe pH of the final reading (24 hours latter) has to be above a pH of 11.5.
.Document changes in lot #'s.
revised: 9/9/13

PH Mt I tK GALII3KA HUN FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
t -QA ID: NC01119
Certification #: 194
t Instrument ID: VWR Symphony SB70P
S/N: 003367
' In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot*
Exp: Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. oC
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
' DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
tfq,q
Ll,t o
1. f°f
!�, in
l�:. �l °C
6 7�+
} j, �
/"Z; J.
.
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: i t> %'a ' e`". 2Li - 1�2;
2HR
2HR
pH
TEMP.°C
CORRECTED pH: 1" , 4 l •- i - i�2.Ilif
24 H R
pH
24 H R
TEMP.°C
11:?�;
i('�.(r,
CORRECTED pH: i -_ •A i - 1).4q
Pnct (alihratinn Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
,
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
-alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
- Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
' I Ile pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #Is.
revised: 9/9/13

Prl Mr- 1 CM UTAL16KA I IVIV rUK OUS LIIVIC/5LVUC7t
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
- 566 Walnut Trail
Waynesville, NC 28785
----'A ID: NCO 1119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot*:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. oC
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
F.
E04
PH 4.0
BUFFER
PH) 1y0.0
BUFFER
PH 13.0
BUFFER
INITIAL
/DATE
1(/F�
4/%
y/(TIME
•( dam'
l/
1
'! \. /t✓ `ry
�I- \
.`!
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: d a .� I -c • 5 =,.
2 HR
pH
2 HR
TEMP. oC
CORRECTED pH: t"? 3.4 -c- , \ (k,z-I' 4
24 HR
pH
24 HR
TEMP.oC
)-
( i .(.
;ORRECTED pH: - X V r
Post Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
IL)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
-r;orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
I :actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
fie pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
""I ne pH of this second reading has to be above a pH of 12.
- The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
-Document changes in lot #'s.
revised: 9/9/13

FN iwta tK UALIt3KAI IUN FUR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
- —DA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot#:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
a
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: 13 -01 0 . t f - (I _ Q i
2 HR
pH
2 HR
TEMP. °C
a
_
CORRECTED pH: t ), - 0 c-P _
24 H R
pH
24 H R
TEMP. °C
CORRECTED pH: 40 � J4 = 4). 7'i"
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
c� s v.
I
(3 1
4 �, -?-
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
-Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
kctual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
he pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
` ie pH of this second reading has to be above a pH of 12.
.,'he pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Jocument changes in lot #'s.*
revised: 9/9/13

rN Mr- I r-K I,ALRSKA i 1UN I -UK OU3 LIMt/JLUIJUI=
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
=-OA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
SIN: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
f Y! •�.�f ♦` ! 4 f�
( - L: �
�a i .�
y ' �} \
l—c'i�.� i
� � . �! �,
/3� �t . f `..
�e.l i �
�� s
DATE
COLLECT
TIME
ANALYSIS,
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: ( k"!�??. - • t i / 3
2 HR
pH
2 HR
TEMP. °C
CORRECTED pH:
24HR
24HR
pH
TEMP.°C
s
2,
CORRECTED pH:
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
YY i G
T5
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the .pH reading to the standard temperattite of 25 centigrade.
- Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
the pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i ,,e pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
' revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
A ID: NC01119
r,d✓ Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot*: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
'tl�<�f{�.�
J'_c"i`�
�'t� 1
�-•J Is%`Li
{BUFFER
\����J.
� J,lti �
��� � v
��- ��
t�_�..7
� 7
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: d . 'c 3
2HR
pH
2HR
TEMP. °C
CORRECTED pH
24 H R
pH
24 H R
TEMP. °C
CORRECTED pH:
Pnct r'alihratinn VPrifirntinn
Ph
Temp.
TIME
INITIAL
13.0
°C
I CIS �.
off readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
zhe pH of this initial reading has to be above a pH of 12.
e second pH reading is taken 2 hours after the initial reading.
The pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

IF'M Mt I tK (;ALIIJKA I ION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
11
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
—'`'A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot #: Exp. Date:
pH 13.00 Lot#:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL:
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
6` G'�
1 r `
1 JQ
o'
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH:I-
2 HR
pH
2 HR
TEMP. °C
Q,. 2
AC,�-i
CORRECTED pH: C-A
24 HR
pH
24 HR
TEMP. °C
i <-',;
C? .7
CORRECTED pH: 1,�- ,_ V � 12 j `l -7
PnSt Calihratinn Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
- Correction factor (CF) 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
ie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
`-'QA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date -APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH.4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
Fl��/!4
`�'.�.,�
1. io
43 j.lC=
f i •.�-�
CORRECTED pH: I.la;
2 HR
pH
2 HR
TEMP.°C
-
� � `� t
I0',-?
i
CORRECTED pH: 7 c^. ( S L?-
24HR
pH .
24HR
TEMP.°C
CORRECTED pH: i A- �2 Q - U 0) "1 r •. f " I.
Pnct (-:Rlihratinn Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
�- Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
Th__e pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i oe pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
..---°A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot#:4404169 Exp. Date:MAR. 2015
PH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. oC
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER'
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: $ ') , ek ck - t
2HR
PH
2HR
TEMP. °C
q 93
(C:z 6
CORRECTED pH: ( • `� = iv7?
24 HR
PH
24 HR
TEMP.°C
id, Si
(q-+
CORRECTED pH: (A. P ,1- C A Gq'
Pnst Calihrntion Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
, ie pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
-qPA ID: NC01119
C Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
PH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial #:130580240. Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. °C
CORRECTED pH: ( .. 5z
2 HR
PH
.2 HR
TEMP.°C
LORRECTED pH:
24 HR
PH
24 HR
TEMP. °C
CORRECTED pH:
Pnct (-:;Iihratinn Verifirntinn
TIME
INITIAL
Ph
13.0
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
r Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
- second pH reading is taken 2 hours after the initial reading.
, , ,e pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot;Ts.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
I
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
RPA ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot*
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot #:
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
0t ((/14-
L'C;N
'). I c,
(�.
o y.n
CORRECTED pH: (, ..; -,,..
2 HR
2 HR
pH
TEMP. °C
,,iRRECTED pH: / i• ),,C1 40, A ( _-( 10
24 H R
24 H R
pH
TEMP. oC
5
CORRECTED pH: # A, I",� ..� . 19�.0 c
Pnct ralihrntinn Varifiratinn
Ph
Temp.
TIME
INITIAL
13.0
°C
C? `, ` 7
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 1.2.
L`e second pH reading is taken 2 hours after the initial reading.
pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours [after) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
— IA ID: NC01119
, Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
PH 4.01 Lot #:A4105 Exp. Date:APR. 2018
PH 4.01 Lot #: Exp. Date:
PH 10.01 Lot #:A4102 Exp. Date:APR. 2015
PH 10.01 Lot #: Exp. Date:
PH 13.00 Lot#:4404169 Exp. Date:MAR. 2015
PH 13.00 Lot* Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
COLLECT
ANALYSIS
INITIAL
INITIAL
DATE
TIME
TIME
PH
TEMP. oC
CORRECTED pH:
2HR
2HR
PH
TEMP.°C
CORRECTED pH: (-A , '%R -t_ , A'A ` P • 7 L(
24HR
24HR
PH
TEMP.°C
CORRECTED pH: ( "� `'-n1 -o d I -( a --)4f
Pnct (Plihrntinn Varifinatinn
TIME
INITIAL
Ph
13.0
Temp.
°C
PH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
�, second pH reading is taken 2 hours after the initial reading.
, ,e pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
,- Document changes in lot #'s.-
revised: 9/9/13

- PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
_Waynesville, NC 28785
�'A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N: 003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
to 0S,
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
?'i�
i eftf r�-
S�c;c�
CORRECTED pH:
2 HR
PH
2 HR
TEMP. °C
q�$
'CORRECTED pH: 0, l;-z = �� �►
24 HR
PH
24 HR
TEMP. °C
,A.? S
( ky
:,ORRECTED pH:
Pnct (ali6rntion Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
-)H readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
- .orrection factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
-T.he pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
i ne pH of this second reading has to be above a pH of 12.
-The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
'Document changes in lot Vs.
revised: 919/13

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
�A ID: NCO1119
Certification #: 194
Instrument ID: VWR Symphony SB70P
SIN: 003367
In Lab
Equipment Maintenance:
PH 4.01 Lot *A4105
Exp. Date:APR. 2018
PH 4.01 Lot #:
Exp. Date:
PH 10.01 Lot #:A4102
Exp. Date:APR. 2015
PH 10.01 Lot #:
Exp. Date:
PH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
PH 13.00 Lot*
Exp. Date:
Checked with Traceable Thermometer Serial #:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
EFF(.
PH14.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
J jDATE
\TIME
`
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH:
2HR
PH
2HR
TEMP.°C
� R I �- -7
1 12� • '-I—
CORRECTED pH: Ii "C= -,�, i = 1 �• b ,)-
24 H R
PH
24 H R
TEMP. °C
- CORRECTED pH: -? ` o- ( - i` 11"4>
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
rr".. t 0
"T-5
13..E
.3 -
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
_ Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading,
ne pH of this second reading has to be above a pH of 12.
The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot #'s.
revised: 9/9113

PH METER CALIBRATION FOR 503 LIME/SLUDGE
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105
Exp. Date:APR. 2018
pH 4.01 Lot #:
Exp. Date:
pH 10.01 Lot #:A4102
Exp. Date:APR. 2015
pH 10.01 Lot*
Exp. Date:
pH 13.00 Lot #:4404169
Exp. Date:MAR. 2015
pH 13.00 Lot #:
Exp. Date:
Checked with Traceable Thermometer Serial
#:130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. oC
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
DATE
TIME
EFF.
PH 4.0
BUFFER
PH 10.0
BUFFER
PH 13.0
BUFFER
INITIAL
eta-3� (q
�� "
4 ..
1 cx, '
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP. °C
CORRECTED pH: 1 -i^j-?
2 HR
pH
2 HR
TEMP.°C
CORRECTED pH: k)" � � - C-
24 H R
24 H R
pH
TEMP. QC
t-: 4
( . -,I
CORRECTED pH:
Pnst Calibration Verification
Ph
Temp.
TIME
INITIAL
13.0
°C
�"
pH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
calculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
Actual pH = Measured pH +/- the correction Factor.
The initial pH reading is taken after the lime is mixed with the 503 sludge.
--,The pH of this initial reading has to be above a pH of 12.
second pH reading is taken 2 hours after the initial reading.
r I ne pH of this second reading has to be above a pH of 12.
-The pH of the final reading (24 hours latter) has to be above a pH of 11.5.
Document changes in lot Vs.
revised: 9/9/13

PH Mt I tK (:ALIIJKA 1 IUN f UK 3U:S LIMt/5LU1JUt
SM 4500-H+B-2000 (Aqueous)
Town of Waynesville WWTP
566 Walnut Trail
Waynesville, NC 28785
'A ID: NC01119
Certification #: 194
Instrument ID: VWR Symphony SB70P
,S/N:003367
In Lab
Equipment Maintenance:
pH 4.01 Lot #:A4105 Exp. Date:APR. 2018
pH 4.01 Lot #: Exp. Date:
pH 10.01 Lot #:A4102 Exp. Date:APR. 2015
pH 10.01 Lot* Exp. Date:
pH 13.00 Lot #:4404169 Exp. Date:MAR. 2015
pH 13.00 Lot #: Exp. Date:
Checked with Traceable Thermometer Serial *130580240 Cal Due Date:10/2/15
CAL.
TEMP. °C
CAL.
TEMP. °C
QC
TEMP. °C
SLOPE
BUFFER
OF PH 4.0
BUFFER
OF PH 10.0
BUFFER
OF PH 13.0
' DATE
TIME
EFF.
PH 4.0
BLUFFER
10.0
BUFFER
PH
BUFFER
INITIAL
6ii LUl!
6e l
"t �. (i"
l '
i CJ
(PH
Y .%
♦ 6 ,
[113.0
I'
� l
DATE
COLLECT
TIME
ANALYSIS
TIME
INITIAL
PH
INITIAL
TEMP-.` °C
4
5 ', 4 e:
CORRECTED pH:
f 5 'J^Z, 15
r`
2 HR
pH
2 HR
TEMP. °C
1•3.1a
19,10
24 HR
pH
24 HR
TEMP. °C
CORRECTED pH: -20 - 01 • I _ / �Ca
Post Calibration Verification
TIME
INITIAL
Ph
13.0
Temp.
°C
Ib%to
25
1 1 145
1 1qt 3cc-
aH readings must be taken at 25 centigrade, or corrected to 25 centigrade. At other than 25 centigrade, a conversion
:alculation may be used to correct the pH reading to the standard temperature of 25 centigrade.
_ Correction factor (CF) = 0.03 pH units * (Temp. Measured - 25 Centigrade).
\ctual pH = Measured pH +/- the correction Factor.
•f he initial pH reading is taken after the lime is mixed with the 503 sludge.
Fhe pH of this initial reading has to be above a pH of 12.
second pH reading -is taken 2 hours after the initial reading.
r lie pH of this second reading has to be above a pH of 12.
the pH of the final reading (24 hours latter) has to be above a pH of 11.5.
)ocument changes in lot #'s.
revised: 9/9/13

TCLP

PO Box 7565
Asheville, NC 28802
ETS.
Phone:
[phone]
Fax:
[phone]
I Environmental Testing Solutions, Inc.
Certificate Of Analysis
Project name: Town of Waynesville WWTP
Project number:
140506.534
Collection date: 6-May-14
Date received: 6-May-14
Sample identification: 503 Lime Sludge - Composite
Sample number:
115732
ti
Parameter
Method
Result
RL
Units
Deed
Analyst
Footnotes
A
Reactive Cyanide
335.4
<0.132
0.132
mg/kg
20-May-14
ECHEM
3
-' Reactive Sulfide
SM 4500 S D
<0.264
0.264
mg/kg
20-May-14
ECHEM
3
• + Ignitability
SW 846 1030
<0.8
0.8
mm/sec
16-May-14
ECHEM
3
% Total Solid
SM 2540 B
45.4
%
7-May-14
ECHEM
3
pH in Soil
9045 C
12.2
S.U.
6-May-14
KW
Arsenic - TCLP
6010 C
<0.25
0.25
mg/L
19-May-14
MEC
1
Barium - TCLP
6010 C
<2.5
2.5
mg/L
19-May-14
MEC
1
Cadmium -TCLP
6010 C
<0.05
0.05
mg/L
19-May-14
MEC
1
• Chromium - TCLP
6010 C
<0.10
0.10
mg/L
19-May-14
MEC
1
Lead - TCLP
6010 C
<0.25
0.25
mg/L
19-May-14
MEC
1
Selenium - TCLP
6010 C
<0.25
0.25
mg/L
19-May-14
MEC
1
Silver - TCLP
6010 C
<0.10
0.10
mg/L
19-May-14
MEC
1
Mercury - TCLP
7470A
<0.0020
0.0020
mg/L
16-May-14
DER
1
Full Scan TCLP Organics
See attached sheets
1,3
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Methods EPA 9210A and SM 450ONO2 B by LDP and REH on 05-13-14 and 05-14-14.
3. Sample analzyed by Envio Chemists, Inc.
Date reviewed: NC Certification Number: 600
Data reviewed by: Kelley E. Keenan SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
Signature:
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

Dear Client: .
Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of
custody for samples that were received on May 07, 2014. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses
performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval
for each test method unless otherwise qualified. Estimated uncertainty is available upon request.
Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or
the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by
mistake, please notify Rogers and Callcott immediately.
We strive to provide excellent service to our clients. Please contact Amy Ashley, your Project Manager, at [e-mail] or
(864)-335-4962 if you have any questions about this report.
Amy Ashley
Project Manager
This report'm no! he re reduced, exae tin 71, without written permission rom Ro rs &iCdllcott, Inc. cY P P f P f 8e -
" _
PO Box:5655 .1 :GreemAlle; SC 2960671 426-Fairforest Way-1 :Greenvilie, SC 29607. 1:main; 864.232A% 1 fax'864.232.-6140 -rogersandcallcottx6m
an employee owned company

Roers.altc�tt
`, ENVI:RONMENTAL
Certificate of Analysis
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St.
Asheville, NC 28801-4310
Sample Number Sample Description
4050230-01 Waynesville WWTP 503 Lime Sludge -Comp
4050230-02 Waynesville WWTP 503 Lime Sludge -Comp
South Carolina Greenville Laboratory Identification 23105
South Carolina Columbia Laboratory Identification 40572
North Carolina Laboratory Certification Number 27
North Carolina Drinking Water Lab Number 45710
NEUP Laboratory Identification E87822
Project: Waynesville WWTP
Work Order: 4050230
Received: 05/07/2014 10:20
Matrix Sampled Type
Sludge 05/06/14 09:15 Composite
Sludge 05/06/14 09:15 Composite
PO Box 5655 1 Greenville, SC.29606 1 426 fairforest Way 1 Greenville, SC 29607 I main 864.232,1556 1 fax 864.232,6140 roprsandcallcott.com
an employee -owned company.
0512912014 11:52 This report may not be reproduced, except in full, without written pennission from Rogers & Callcon, Ina ire L

m v -
a s i' ;■
M
.nnnnnnnn
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
Sample Data
Sample Number 4050230-01
Sample Description Waynesville WWTP 503 Lime Sludge -Comp collected on 05/06/14 09:15
Reporting
Parameter
Result
Limit
Units
DF
Analyzed
Method
Flag Analyst
Batch
General Chemistry Parameters
Nitrate as N, extractable
32.9
21.0
mg/kg dry
2.00
05/13/14 15:45
EPA 9210A
LDP
B4E0428
Nitrite as N, extractable
10.8
5.24
mg/kg dry
50.0
05/14/14 13:45
SM4500NO2B-2011
REH
134E0500
Total Kjeldahl Nitrogen
9520
558
mg/kg dry
10.0
05/16/14 14:24
EPA 351.2
LDP
134E0076
Total Nitrogen (TKN+Nitrate+Nitrite)
9560
558
mg/kg dry
10.0
05/16/14 14:24
-
LDP
B4E0493
Total Solids
38.0
0.10
%
1.00
05/07/14 14:09
SM 2540G
ASB
B4E0247
Total Metals
Mercury
0.57
0.26
-g/kg dry
5.00
05/16/14 14:11
EPA 7471B
DER
B4E0494
Aluminum
13800.
317
-g/kg dry
50.0
05/13/14 12:15
EPA 6010C
MEC
B4E0350
Arsenic
7.81
6.34
mg/kg dry
1.00
05/13/14 12:18
EPA 6010C
MEC
134E0350
Cadmium
ND
2.54
mg/kg dry
1.00
05/13/14 12:18
EPA 6010C
NEC
134E0350
Calcium
282000
6340
mg/kg dry
1,000
05/13/14 12:12
EPA 6010C
MEC
134E0350
Chromium
22.6
6.34
mg/kg dry
1.00
05/13/14 12:18
EPA 6010C
MEC
134E0350
Copper
138
2.54
mg/kg dry
1.00
05/13/14 12:18
EPA 6010C
MEC
B4E0350
Lead
17.8
6.34
mg/kg dry
1.00
05/13/14 12:18
EPA 6010C
MEC
B4E0350
Magnesium
4870
317
mg/kg dry
50.0
05/13/14 12:15 _
EPA 6010C
MEC
B4E0350
Molybdenum
ND
6.34
mg/kg dry
1.00
05/13/14 12:18
EPA 6010C
MEC
B4E0350
Nickel
12.4
2.54
mg/kg dry
1.00 •
05/13/14 12:18
EPA 6010C
MEC
B4E0350
Potassium
2180
12.7
mg/kgdry
1.00
05/13/14 12:18
EPA6010C
MEC
B4E0350
Selenium
ND
6.34
mg/kg dry
1.00
05/13/14 12:18
EPA 6010C
MEC
134E0350
Sodium
465
12.7
mg/kg dry
1.00
05/13/14 12:18
EPA 6010C
MEC
134E0350
Total Phosphorus as P
5490
254
mg/kg dry
50.0
05/13/14 12:15
EPA 6010C
MEC
134E0350
Zinc
331
6.34
mg/kg dry
1.00
05/13/14 12:18
EPA 6010C
MEC
134E0350
PO Box,5655 I Greenville, SC 29606 1 426 Fai,rorest Why. 1 Greenville, SC 29607 1 main 864.112.1556 16 864.232.6140 romrsd1 dgaIICOtt.G0171 , _
an employee -owned company .
0512912014 11:52 This report may not be reproducer, except in full, without written permission from Rogers & Callcott, Inc.

Environmental Testing Solutions Project:. Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
Sample Number 4050230-02
Sample Description Waynesville WWTP 503 Lime Sludge -Comp collected on 05/06/14
09:15
Reporting
Parameter
Result
Limit
Units
DF
Analyzed
Method
Flag Analyst
Batch
TCLP Metals
Mercury-
ND
0,0020
mg/L
10.0
05/16/14 11:39
EPA 7470A
DER
B4E0534
Arsenic
ND
0.25
mg/L
5.00
05/14/14 13:51
EPA 6010C
MEC
B4E0543
Barium
ND
2.50
mg/L
5.00
05/19/14 13:51
EPA 6010C
MEC
B4E0543
Cadmium
ND
0.05
mg/L
5.00
05/19/14 13:51
EPA 6010C
MEC
B4E0543
Chromium
ND
0.10
mg/L
5.00
05/19/14 13:51
EPA 601OC
MEC
B4E0543
Lead
ND
0.25
mg/L
5.00
05/19/14 13:51
EPA 6010C
MEC
B4E0543
Selenium
ND
0.25
mg/L
5.00
05/19/14 13:51
EPA 6010C
MEC
B4E0543
Silver
ND
0.10
mg/L
5.00
05/19/14 13:51
EPA 6010C
MEC
B4E0543
TCLP Volatile Organics
Benzene
ND
0.100
mg/L
50.0
05/21/14 17:50
EPA 8260B
ARM
B4E0933
t
'
2-Butanone (MEK)
ND
0.200
mg/L
50.0
05/21/14 17:50
EPA 8260B
ARM
B4E0933
Carbon tetrachloride
ND
0.100
mg/L
50.0
05/21/14 17:50
EPA 8260B
ARM
B4E0933
Chlorobenzene
ND
0.100
mg/L
50.0
05/21/14 17:50
EPA 8260B
ARM
B4E0933
Chloroform
ND
0.100
mg/L
50.0
05/21/14 17:50
EPA 8260B
ARM
B4E0933
1,2-Dichloroethane
ND
0.100
mg/L
50.0
05/21/14 17:50
EPA 8260B
ARM
B4E0933
1,4-Dichlorobenzene
ND
0.100
mg/L
50.0
05/21/14 17:50
EPA 8260E
ARM
B4E0933
1,1-Dichloroethene
ND
0.100
mg/L
50.0
05/21/14 17:50
EPA 8260B
ARM
B4E0933
Tetrachloroethene
ND
0.100
mg/L
50.0
05/21/14 17:50
EPA 8260B
ARM
B4E0933
Trichloroethene
ND
0.100
mg/L
50.0
05/21/14 17:50
EPA 8260B
ARM
B4E0933
Vinyl chloride
ND
0.100
mg/L
50.0
05/21/14 17:50
EPA 8260B
ARM
B4E0933
Surrogates
% REC
%REC Limits
Flag
1,2-Dichloroerhane-D4
83
70-130
Toluene-D8
92
70-130
4-BromoJluoroben-,ene
114
70-130
TCLP Semi -Volatile Organics
2-Methylphenol (o-Cresol)
ND
0.100
mg/L
10.0
05/21/14 18:47
EPA 8270D
RIM
B4EO741
3/4-Methylphenol(m,p-Cresol)
ND
0.100
mg/L
10.0
05/21/14 18:47
EPA 8270D
RIM
B4E0741
total Cresol
ND
0.200
mg/L
10.0
05/21/14 18:47
EPA 8270D
RIM
B4E0741
2,4-Dinitrotoluene
ND
0.100
mg/L
10.0
05/21/14 18:47
EPA 9270D
RIM
B4EO741
Hexachlorobenzene
ND
0.100
mg/L
10.0
05/21/14 18:47
EPA 8270D
RJM
B4E0741
Hexachlorobutadiene
ND
0.100
mg/L
10.0
05/21/14 18:47
EPA 8270D
RJM
B4E0741
Hexachloroethane
ND
0.100
mg/L
10.0
05/21/14 18:47
EPA 8270D
RJM
B4E0741
Nitrobenzene
ND
0.100
mg/L
10.0
05/21/14 18:47
EPA 8270D
RJM
B4E0741
Pentachlorophenol
ND
0.100
mg/L
10.0
05/21/14 18:47
EPA 8270D
RJM
B4E0741
PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864,232,1556 I fax [phone] rogersandcallcott.Com
an employee -owned company
0512912014 11:52 This report may not be reproducer, except in full, without written permission from Rogers 8 C'allcon, Inc. a >x .

din6tJ
S i a.
r is
'%IIIR�RRR�R '
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4650230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
Sample Number 4050230-02
Sample Description Waynesville WWTP 503 Lime Sludge -Comp collected on 05/06/14 09:15
Reporting
Parameter
Result
Limit
Units
DF
Analyzed
Method
Flag Analyst
Batch
i
TCLP Semi -Volatile Organics
Pyridine
ND
0.100
mg/L
10.0
05/21/14 18:47
EPA 8270D
RJM
134E0741
2,4,5-Trichlorophenol
ND
0.100
mg/L
10.0
05/21/14 18:47
EPA 8270D
RJM
134E0741
1 2,4,6-Trichlorophenol
ND
0.100
mg/L
10.0
05/21/14 18:47
EPA 8270D
RJM
134E0741
Surrogates
%REC
%REC Limits
Flag
Nitrobenzene-D5
72
35-114
2-Fluorobiphenyl
79
43-116
2-Fluorophenol
47
21-110
Phenol-D5
31
10-110
2,4,6-Tribromophenal
97
10-123
Terphenyl-DI-I
70
33-141
TCLP Pesticides
Gamma-BHC (Lindane)
ND
0.00050
mg/L
10.0
05/23/14 23:30
EPA 8081B
RKH
B4E0743
Chlordane
ND
0.0050
mg/L
10.0
05/23/14 23:30
EPA 8081B
RKH
134E0743
Endrin
ND
0.00050
mg/L
10.0
05/23/14 23:30
EPA 8081B
RKH
B4E0743
Heptachlor
ND
0.00050
mg/L
10.0
05/23/14 23:30
EPA 8081B
RKH
134E0743
Heptachlor epoxide
ND
0.00050
mg/L
10.0
05/23/14 23:30
EPA 8081B
RKH
B4E0743
Toxaphene
ND
0.0050
mg/L
10.0
05/23/14 23:30
EPA 808113
RKH
B4E0743
Methoxychlor
ND
0.00050
mg/L
10.0
05/23/14 23:30
EPA 8081B
RKH
B4E0743
Surrogates
%REC
%REC Limits
Flag
2,4,5,6-Tetrachloro-m xylene 97 60-130
Decachlorobiphenyl 82 30-150
PO Box 5655 1- Greenville, SC 29606 1 426 Nirkrest Way.( Greenville, SC 29607 1 main 864.2321556 1 fax 864.232,6140 rogersandCa�kOtLCOM
an employee -owned company
0512912014 11:52 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. � s

Environmental Testing Solutions -Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
General Chemistry Parameters
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter . Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0076 - EPA 351.2-TKN
_ Blank;(B4E0076-BLKI)
Total Kjeldahl Nitrogen ND 10.0 mg/kg wet
Duplicate (B4E0076-DUPI) Source: 4050040-01
Total Kjeldahl Nitrogen 44700 1570- mg/kg dry 57200
Matrix Spike (B4E0076-MS1) Source: 4050040-01
Total Kjeldahl Nitrogen 102000 1570 mg/kg dry 47200 57200 95 65-130
Reference (B4E0076-SRMl)
Total Kjeldahl Nitrogen 1230 33.9 mg/kg wet 1160 106 57-143
l
Batch B4E0247 - General Prep - Solids
Duplicate (B4E0247-DUPl) Source: 4050092-01
25 30
Total Solids 1.70 0.10 % 1.70 0 15
Batch B4E0428 - Nitrate Extractable
Blank (B4E0428-BLKI)
Nitrate as N, extractable ND 4.0 mg/kg wet
i
r nO i AcnAgo o01%
Nitrate as N, extractable 38.1 4.0 mg/kg wet 40.0 95 85-115
Duplicate (B4E0428-DUPl) Source: 4050230-01
Nitrate as N, extractable 32.9 21.0 mg/kg dry 32.9 0 30
Matrix Spike (B4E0428-MSl) Source: 4050230-01
Nitrate as N, extractable 130 21.0 mg/kg dry 105 32.9 93 65-130
Batch B4E0500 - Nitrite Extractable
Blank (B4E0500-BLKI)
Nitrite as N, extractable
ND 0.04 mg/kg wet
PO Box 5655 1 Greenville SC 29606 1426 Fairforest Way I Greenville, SC 29607 I main 864.232,1556 1 fax-864.232.6140 - rOgerSalldcalkott.COf1'1.
an employee -owned Company_
0512912014 11:52 This reportmay not be reproduced, except in full, without written permission front Rogers & Callcon, Inc.

6 ge
rs-S�__Catic®tt
ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
General Chemistry Parameters
Quality Control Summary
Reporting Spike Source I %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0500 - Nitrite Extractable
LCS (B4E0500-BS1)'
Nitrite as N, extractable 0.193 0.04 mg/kg wet 0.200 97 85-115
Matrix Spike (B4E0500-MSl) Source: 4050230-01
Nitrite as N, extractable 25.5 5.24 mg/kg dry 15.7 10.8 94 65-130
Matrix Spike DUD (B4E0500-MSDI) Source: 4050230-01
Nitrite as N, extractable 25.7 5.24 mg/kg dry 15.7 10.8 95 65-130 0.7 30
PO Box_ 5655 1 Greenville SC 29606 1 426 Fairforest Way I Greenville, SC 24607 1 main 864.232.1556 1 fax [phone]. rggel"Sa.11dCallCOtt.com.
an employee -owned company
O512912014 11:52 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc.

s"esavc`�� O
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0350 - EPA 3050B
Blank (B4E0350-BLK1)
Aluminum
ND
0.05
mg/kg wet
Arsenic
ND
0.05
mg/kg wet
Cadmium
ND
0.02
mg/kg wet
Calcium
ND
0.05
mg/kg wet
Chromium
ND
0.05
mg/kg wet
Copper
ND
0.02
mg/kg wet
Lead
ND
0.05
mg/kg wet
Magnesium
ND
0.05
mg/kg wet
Molybdenum
ND
0.05
mg/kg wet
Nickel
ND
0.02
mg/kg wet
Potassium
ND
0.10
mg/kg wet
Selenium
ND
0.05
mg/kg wet
Sodium
ND
0.10
mg/kg wet
Total Phosphorus as P
ND
0.04
mg/kg wet
Zinc
ND
0.05
mg/kg wet
Blank (B4E0350-BLK2)
Aluminum
ND
0.05
mg/kg wet
Arsenic
ND
0.05
mg/kg wet
Cadmium
ND
0.02
mg/kg wet
Calcium
ND
0.05
mg/kg wet
Chromium
ND
0.05
mg/kg wet
Copper
ND
0.02
mg/kg wet
Lead
ND
0.05
mg/kg wet
Magnesium
ND
0.05
mg/kg wet
Molybdenum
ND
0.05
mg/kg wet
Nickel
ND
0.02
mg/kg wet
Potassium
ND
0.10
mg/kg wet
Selenium
ND
0.05
mg/kg wet
Sodium
ND
0.10
mg/kg wet
Total Phosphorus as P
ND
0.04
mg/kg wet
Zinc
ND
0.05
mg/kg wet
LCS (B4E0350-BSI)
Aluminum
1.00
0.05
mg/kg wet 1.00 100 80-120
Arsenic
0.99
0.05
mg/kg wet 1.00 99 80-120
PO Box 5655 I Greenville, SC 2460b 1426 Fairiorest Way I Greenville SC 29607 'I main 864.232.1556 I fax 864:232.6140
POgBesan callCOttxom'
an employee -owned .company -
OS/29/20I4 11:52&..
This 'report may not be reproduced, except in full, without written permission front Rogers & Callcot;'Inc.
m

.�
• ! - •LL 6tt.
�a aaaa■ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 288014310 Reported: 05/29/14 11:52
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0350 - EPA 3050B
{
LCS (B4E0350-BSI)
Cadmium
0.99
0.02
mg/kg wet
1.00
99
80-120
"
Calcium
0.98
0.05
mg/kg wet
1.00
98
80-120
Chromium
0.97
0.05
mg/kg wet
1.00
97
80-120
Copper
1.00
0.02
mg/kg wet
1.00
100
80-120
Lead
0.98
0.05
mg/kg wet
1.00
98
80-120
Magnesium
0.98
0.05
mg/kg wet
1.00
98
80-120
Molybdenum
1.00
0.05
mg/kg wet
1.00
100
80-120
!
Nickel
0.99
0.02
mg/kg wet
1.00
99
80-120
Potassium
10.3
0.10
mg/kg wet
10.0
103
80-120
Selenium
0.97
0.05
mg/kg wet
1.00
97
80-120
Sodium
1.00
0.10
mg/kg wet
1.00
100
80-120
Total Phosphorus as P
1.01
0.04
mg/kg wet
1.00
101
80-120
`
Zinc
0.98
0.05
mg/kg wet
1.00
98
80-120
LCS (194E0350-BS2)
'
Aluminum
1.01
0.05
mg/kg wet
1.00
101
80-120
Arsenic
1.02
0.05
mg/kg wet
1.00
102
80-120
Cadmium
1.02
0.02
mg/kg wet
1.00
102
80-120
'
Calcium
1.09
0.05
mg/kg wet
1.00
109
80-120
t
Chromium
1.00
0.05
mg/kg wet
1.00
100
80-120
•
Copper
1.02
0.02
mg/kg wet
1.00
102
80-120
Lead
1.01
0.05
mg/kg wet
1.00
101
80-120
Magnesium
1.01
0.05
mg/kg wet
1.00
101
80-120
Molybdenum
1.05
0.05
mg/kg wet
1.00
105
80-120
Nickel
1.02
0.02
mg/kg wet
1.00
102
80-120
Potassium
10.5
0.10
mg/kg wet
10.0
105
80-120
Selenium
1.02
0.05
mg/kg wet
1.00
102
80-120
Sodium
1.01
0.10
mg/kgwet
1.00
101
80-120
Total Phosphorus as P
1.04
0.04
mg/kg wet
1.00
104
80-120
Zinc
1.00
0.05
mg/kg wet
1.00
100
80-120
Matrix Spike (B4E0350-MSI)
Source: 4050236-01
j
Aluminum
'7470
4.49
mg/kg dry
89.8
4880 NR
75-125
S3
Arsenic
84.3
4.49
mg/kg dry
99.8
ND 91
75-125
Cadmium
80.9
1.80
mg/kg dry
89.8 •
ND 90
75-125
Calcium
7260
4.49
mg/kg dry
89.8
10900 NR
75-125
S3
PO Box 5655 1 Greenville, SC 29606 -1 426 Fairforesc Way
I Greenville, SC 29607
1 main 864.232.1556 I fax [phone]
rogersandcallcott.com
an employee-owned;company ...
0512912014 11:52
This report may not be reproduced, except in,full, without
written permission from'Rogers cC Callcoh, Inc.
w ��

Rogers &-ca, 11cott
ENV"IR,QNMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC . Limits RPD Limit Flags
Batch B4E0350 - EPA 3050B
Matrix Spike (B4E0350-MS1) Source: 4050236-01
Chromium
93.1
Copper
123
Lead
87.2
Magnesium
2960
Molybdenum
81.5
Nickel
84.2
Potassium
1880
Selenium
81.5
Sodium
160
Total Phosphorus as P
939
Zinc
190
Matrix Spike Dup (B4E0350-MSDI)
Source: 4050236-01
Aluminum
6660
Arsenic
84.1
Cadmium
81.5
Calcium
8010
Chromium
94.8
Copper
121
Lead
87.5
Magnesium
3310
- Molybdenum
83.5
Nickel
84.4
Potassium
1930
Selenium
83.7
Sodium
162
Total Phosphorus as P
845
Zinc
342
Post Spike (B4E0350-PS1) "
Source: 4050236-01
Arsenic
87.2
Cadmium
82.6
Chromium
96.4
Copper
119
Lead
89.4
Molybdenum
99.7
4.49
mg/kg dry
89.8
16.5
85
75-125
1.80
mg/kg dry
89.8
37.4
96
75-125
4.49
mg/kg dry
89.8
8.86
87
75-125
4.49
mg/kg dry
89.8
4350
NR
75-125
4.49
mg/kg dry
89.8
ND
89
75-125
1.80
mg/kg dry
89.8
6.35
87
75-125
8.98
mg/kg dry
898
1100
86
75-125
4.49
mg/kg dry
89.8
ND
89
75-125
8.98
mg/kg dry
89.8
78.3
91
75-125
7.18
mg/kg dry
89.8
612
364
75-125
4.49
mg/kg dry
89.8
126
71
75-125
4.45
mg/kg dry
89.0
4880
NR
75-125
12
4.45
mg/kg dry
89.0
ND
92
75-125
0.2
1.78
mg/kg dry
89.0
ND
91
75-125
0.7
4.45
mg/kg dry
99.0
10900
NR
75-125
10
4.45
mg/kg dry
89.0
16.5
88
75-125
2
1.78
mg/kg dry
89.0
37.4
94
75-125
2
4.45
mg/kg dry
89.0
8.86
88
75-125
0.4
4.45
mg/kg dry
89.0
4350
NR
75-125
11
4.45
mg/kg dry
89.0
ND
92
75-125
2
1.78
mg/kg dry
89.0
6.35
88
75-125
0.2
8.90
mg/kg dry
990
1100
93
75-125
3
4.45
mg/kg dry
89.0
ND
92
75-125
3
8.90
mg/kg dry
89.0
78.3
93
75-125
0.7
7.12
mg/kg dry
89.0
612
262
75-125
11
4.45
mg/kg dry
89.0
126
243
75-125
57
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
S3
S1
Pl, Sl
S3
S3
S3
S1
Pl, S1
4.54
mg/kg dry
90.9
ND
93
80-120
1.82
mg/kg dry
90.9
ND
90
80-120
4.54
mg/kg dry
90.9
16.5
88
80-120
1.82
mg/kg dry
90.9
37.4
89
80-120
4.54
mg/kg dry
90.9
8.86
89
80-120
4.54
mg/kg dry
90.9
ND
97
80-120
PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864132.1556 I fax [phone] rogersandcallcolm.com
an employee -owned company
0512912014 11:52 This report may not be reproduced, except in full, without written permission from Rogers d Callcot; Inc.

Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B4E0350 - EPA 3050B
Post Spike (B4E0350-PSI)
Source: 4050236-01
Nickel
86.6
1.82
mg/kg dry
90.9
6.35
88
80-120
Potassium
1850
9.09
mg/kg dry
909
1100
82
80-120
Selenium
86.9
4.54
mg/kg dry
90.9
ND
94
80-120
Sodium
159
9.09
mg/kg dry
90.9
78.3
89
80-120
Zinc
202
4.54
mg/kg dry
90.9
126
84
80-120
Post Spike (B4E0350-PS2)
Source: 4050236-01
Total Phosphorus as P.
768
14.5
mg/kg dry
182
612
86
80-120
Post Spike(B4E0350-PS3)
Source:4050236-01
Aluminum ND 11400 mg/kg dry 4540 4880 96 80-120
Calcium 16200 11400 mg/kg dry 4540 10900 117 80-120
Magnesium ND 11400 mg/kg dry 4540 4350 98 80-120
Reference (B4E0350-SRM1)
Aluminum
8870 -
496
mg/kg wet
13900
64
36-119
Arsenic
92.0
9.93
mg/kg wet
101
91
65-124
Cadmium
175
3.97
mg/kgwet
199
88
68-117
Calcium
9740
496
mg/kg wet
12900
75
64-110
Chromium
146
9.93
mg/kg wet
144
101
79-146
Copper
166
3.97
mg/kg wet
187
89
72-120
_ Lead
122
9.93
mg/kg wet
138
88
68420
Magnesium
2650
496
mg/kg wet
3300
80
57-117
Molybdenum
79.0
9.93
mg/kg wet
85.4
93
60-115
Nickel
76.9
3.97
mg/kg wet
97.9
87
68-121
Potassium
1780
19.9
mg/kg wet
2210
80
57-137
Selenium
106
9.93
mg/kg wet
125
85
59-120
Sodium
163
19.9
mg/kg wet
261
62
21-141
Zinc
154
9.93
mg/kg wet
179
86
64-123
Reference (NE0350-SRM2)
Total Phosphorus as P
395
7.90
mg/kg wet
409
97
43.7-156
PO Box 5655 1 Greenville, 5C 29606 1.426 Fairforest Way I Greenville, 5C 29607 1 main 864.232.1556 1 fax [phone] rQgersandcallcott.con1
an employee -owned company
0512912014 11:52 This report may not be reproducer, except in full, without written permission from Rogers & Callcon, Inc.

R g r t6ft
E'NVIRONMEN -AL
Environmental Testing Solutions Project: - Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
Total Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit' Flags
Batch B4E0494 - EPA 7471B
Blank (B4E0494-BLKI)
Mercury
ND
0.020
mg/kg wet
Blank (B4E0494-BLK2)
Mercury
ND
0.020
mg/kg wet
LCS (B4E0494-BS1)
Mercury
0.47
0.020
mg/kg wet
0.500
94
80-120
LCS (B4E0494-BS2)
Mercury
0.51
0.020
mg/kg wet
0.500
103
80-120
Matrix Spike (B4E0494-MS1)
Source: 4050230-01
Mercury
7.0
0.25
mg/kg dry
6.20 0.57
104
80-120
Matrix Spike Dup (B4E0494-MSDI)
Source: 4050230-01
Mercury
7.0
0.25
mg/kg dry
6.27 0.57
103
80-120 0.6 20
Reference (B4E0494-SRM1)
Mercury
12
0.097
mg/kg wet
10.5
ill
51-149
i
PO Sox 5655 1 Greenville, SC 29606 1 426 FairForest, Way I Greenville, SC 29607 '1 inain 864.232A 556 ("fax [phone]'Og2t"S1t1dc lcOtt.0017i .
an employee -owned company.
05/29/2014 II:52 This report may not be reproduced, except in full, without written permission fmnz Rokers & Callcon, Inc.

LCOU
gerS-
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: * 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit units Level Result % REC Limits RPD Limit Flags
Batch B4E0534 - EPA 7470A
Blank (B4E0534-BLKI)
Mercury
ND
0.0002
mg/L
Blank (B4E0534-BLK2)
Mercury
ND
0.0020
mg/L
Blank (B4E0534-BLK3)
Mercury
ND
0.0020
mg/L
` LCS (B4E0534-BSI)
' Mercury
0.0050
0.0002
mg/L
0.00500
101
85-115
LCS (B4E0534-BS2)
Mercury
0.0526
0.0020
mg/L
0.0500
105
85-115
Matrix Spike (B4E0534-MSl)
Source: 4050181-01
Mercury
0.116
0.0040
mg/L
0.0500
0.0648
103
75-125
Matrix Spike (B4E0534-MS3)
Source: 4050191-01
Mercury
0.0540
0.0020
mg/L
0.0500
ND
108
75-125
Matra Spike (B4E0534-MS4)
Source: 4050230-02
Mercury
0.0541
0.0020
mg/L
0.0500
ND
108
75-125
--—1GIatriz Spike(B4E0534-MSS)----------
ouice: 405 333= —
------------------------
Mercury
0.0531
0.0020
mg/L
0.0500
ND
106
75-125
Matra Spike (B4E0534-MS6)
Source: 4050333-03
Mercury
0.0531
0.0020
mg/L
0.0500
ND
106
75-125
Matra Spike (B4E0534-MS7)
Source: 4050350-01
Mercury
0.0541
0.0020
mg/L
0.0500
ND
108
75-125
Matra Spike (B4E0534-MS8)
Source: 4050419-01
Mercury
0,0537
0.0020
mg/L
0.0500
ND
107
75-125
PO Box 5655 1 Greenville, SC 29606 1 426 Nirforest Way I Greenville,
SC 29607l: main 964.232.1556
1
fax 864.232,6140
rOgers811dcallcOtt.COt11
ag em ployee-owned-company
0512912014 11:52
This report tray not be reproduced, except in full, without written permission front Rogers & Calkolt, Inc.

�oeers,&
e
`rrrr r
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Metals
�- Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result °/ REC Limits RPD Limit Flags
Batch B4E0534 - EPA 7470A
Matrix Spike Dup (B4E0534-MSDI)
Source: 4050181-01
Mercury
0.116 0.0040
1 Post Spike (B4E0534-PSI)
Source: 4050181-01
i Mercury
0.148 0.0040
Batch B4E0543 - EPA 3005A
Blank (B4E0543-BLK1)
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
ti
Blank (B4E0543-BLK2)
Arsenic
Barium
Cadmium
Chromium
L -- Lead --- —
Selenium
Silver
1 ^�
Blank (B4E0543-BLK3)
r�
Arsenic
Barium
Cadmium
Chromium
r
Lead
Selenium
Silver
mg/L 0.0500 0.0648 103 75-125 0.06 20
mg/L 0.0800 0.0648 104 80-120
ND
6.05
mg/L
ND
0.50
mg/L
ND
0.01
mg/L
ND
0.02
mg/L
ND
0.05
mg/L
ND
0.05
mg/L
ND
0.02
mg/L
ND
0.25
mg/L
ND
2.50
mg/L
ND
0.05
mg/L
ND
0.10
mg/L
ND ---0.25
— mgt —
ND
0.25
mg/L
ND
0.10
mg/L
ND
0.25
mg/L
ND
2.50
mg/L
ND
0.05
mg/L
ND
0.10
mg/L
ND
0.25
mg/L
ND
0.25,
mg/L
ND
0.10
mg/L
r
?Q Box 5655 1 Greenville, SC 29606 1 426 Fairfores't Way I_ Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] roger" aildtakotCxom
an'employee-owned company- =
0512912014 11:52 This report may not be reproduced eccept in full, without written permission from Rogers & Callcolt, Inc. .. ..

'} • ► ®�Ic
�s
�� ■uan�
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
l �
TCLP Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0543 - EPA 3005A
` LCS (B4E0543-BSI)
Arsenic
0.52
Barium
0.51
Cadmium
0.51
Chromium
0.50
Lead
0.51
Selenium
0.50
Silver
0.51
Matrix Spike (B4E0543-MS1)
Source: 4050350-01
Arsenic
2.47
Barium
3.20
Cadmium
2.49
Chromium
2.40
Lead
2.44
Selenium
2.44
` Silver
2.52
Matrix Spike (B4E0543-MS2)
Source: 4050141-01
Arsenic
Barium
f- Cadmium
t - --Chromium-- - -- ----- -- ----
Lead
- Selenium
i
Silver
i
Matrix Spike (B4E0543-MS3)
Arsenic
Barium
I Cadmium
Chromium
r '
Lead
j Selenium
Silver
0.05
mg/L
0.500
103
80-120
0.50
mg/L
0.500
102
80-120
0.01
mg/L
0.500
102
80-120
0.02
mg/L
0.500
99
80-120
0.05
mg/L
0.500
101
80-120
0.05
mg/L
0.500
99
80-120
0.02
mg/L
0.500
103
80-120
0.25
mg/L
2.50
ND
97
75-125
2.50
mg/L
2.50
ND
98
75-125
0.05
mg/L
2.50
ND
99
75-125
0.10
mg/L
2.50
ND
96
75-125
0.25
mg/L
2.50
ND
98
75-125
0.25
mg/L
2.50
ND
95
75-125
0.10
mg/L
2.50
ND
101
75-125
2.56
0.25
mg/L
2.50
ND
101
75-125
3.09
2.50
mg/L
2.50
ND
102
75-125
2.51
0.05
mg/L
2.50
ND
100
75-125
----- 2.48----0:10------mg/L-
2:50---ND-----99---
75-125--
2.51
0.25
1119/L
2.50
ND
100
75-125
2.42
0.25
mg/L
2.50
ND
95
75-125
2.85
0.10
mg/L
2.50
0.25
104
75-125
Source: 4050191-01
2.55
0.25
m9/L
2.50
ND
101
75-125
3.09
2.50
mg/L
2.50
ND
100
75-125
2.52
0.05
mg/L
2.50
ND
101
75-125
2.44
0.10
mg/L
2.50
ND
98
75-125
2.48
0.25
mg/L
2.50
ND
99
75-125
2.57
0.25
mg/L
2.50
ND
100
75-125
2.57
0.10
m9/L
2.50
ND
103
75-125
PO Box 5655 1 Greenville, SC 29606 1.426 Fairibrest Way I Greenville, SC 296071 main 864.232.1556-1 fix 864.232,6146 rogersa-McallCOtum -
an employee -owned company,•
0512912014 11:52 This report may not be reproduced, except in full, without written permission from Rogers B• Callcon, Inc.

f
xMr i �Pgers, & Callcott
IV...-af�lt
�4��EtEENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0543 - EPA 3005A
t Matrix Spike (B4E0543-MS4)
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
i Silver
Matrix Spike (B4E0543-MS5)
Arsenic
�i Barium
Cadmium
1
Chromium
Lead
Selenium
Silver
Matrix Spike (B4E0543-MS6)
Arsenic
Barium
Cadmium
_. -Chromium --- -------
Lead
Selenium
Silver
Matrix Spike (B4E0543-MS7)
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Source:4050230-02
2.52
0.25
m9/L
2.50
ND
100
75-125
3.11
2.50
mg/L
2.50
ND
96
75-125
2.45
0.05
mg/L
2.50
ND
98
75-125
2.35
0.10
m9/L
2.50
ND
94
75-125
2.42-
0.25
m91L
2.50
ND
96
75-125
2.45
0.25
mg/L
2.50
ND
94
75-125
2.56
0.10
mg/L
2.50
ND
102
75-125
Source:4050333-01
2.45
0.25
mg/L
2.50
ND
97
75-125
ND
2.50
mg/L
2.50
ND
96
75-125
2.46
0.05
mg/L
2.50
ND
98
75-125
2.36
0.10
mg/L
2.50
ND
94
75-125
2.39
0.25
mg/L
2.50
ND
95
75-125
2.36
0.25
mg/L
2.50
ND
92
75-125
2.44
0.10
mg/L
2.50
ND
98
75-125
Source:4050333-03
2.55 0.25
mg/L
2.50
ND
101
75-125
3.12 2.50
mg/L
2.50
ND
101
75-125
2.52 0.05
mg/L,
2.50
ND
100
75-125
-------2:44----0:10------mg/L---2.50---ND--
--97--
-75-125 -
2.46 0.25
mg/L
2.50
ND
98
75-125
2.45 0.25
mg/L
2.50
ND
95
75-125
2.55 0.10
mg/L
2.50
ND
102
75-125
Source: 4050419-01
2.49
0.25
mg/L
2.50
ND
98
75-125
4.63
2.50
mg/L
2.50
ND
96
75-125
2.48
0.05
mg/L
2.50
ND
99
75-125
2.42
0.10
mg/L
2.50
ND
97
75-125
2.44
0.25
mg/L
2.50
ND
97
75-125
2.46
0.25
mg/L
2.50
ND
96
75-125
2.54
0.10
mg/L
2.50
ND
101
75-125
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232:1556 1 fax 864.232.E 140 rogersandcallcott.com
an employee -owned company
0512912014 11:52 This report may not be reproduced except in full, without written permission front Rogers d Callcott, Inc.'

�o • "tt
Hft
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0543 - EPA 3005A
Matrix Spike Dup (B4E0543-MSDI) Source: 4050350-01
.
s_.
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Post Spike (B4E0543-PSI)
2.55
3.24
2.52
2.44
2.46
2.48
2.54
Source: 4050350-01
0.25
2.50
0.05
0.10
0.25
0.25
0.10
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
2.50
2.50
2.50
2.50
2.50
2.50
2.50
ND
ND
ND
ND
ND
ND
ND
100
100
101
97
98
97
102
75-125
75-125
75-125
75-125
75-125
75-125
75-125
3 20
1 20
2 20
1 20
0.6 20
2 20
0.8 20
Arsenic
2.44
0.25
mg/L
2.50
ND
95
80-120
Barium
3.15
2.50
mg/L
2.50
ND
96
80-120
Cadmium
2.41
0.05
mg/L
2.50
ND
96
80-120
Chromium
2.35
0.10
mg/L
2.50
ND
94
80-120
Lead
2.37
0.25
mg/L
2.50
ND
95
80-120
Selenium
2.40
0.25
mg/L
2.50
ND
94
80-120
Silver
2.44
0.10
mg/L
2.50
ND
98
80-120
i
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforen Way I Greenville, SC 296071 main 864.232.1556
,I fax [phone]
r9geC'Sr1ndcaIICOtt.00171
an employee owned company,
'
This report may not be reproducer,, except in full, without written permission front Rogers & Callcait; Inc.
,
0512912014 11:52

ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0933 - EPA 5030
Blank (B4E0933-BLKI)
Benzene
ND
2-Butanone (MEK)
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
1,2-Dichloroethane
ND
_
1,1-Dichloroethene
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surrogate: 1, 2-Diehloroethane-D4
Surrogate: Toluene-D8
`
Surrogate: 4-Brontofluorohenzene
' - Blank (B4hU933-BLKL)
0.00200 mg/L
0.00400 mg/L
0.00200 mg/L
0.00200 mg/L
0.00200 mg/L
0.00200 mg/L
0.00200 mg/L
0.00200 mg/L
0.00200 mg/L
0.00200 mg/L
Benzene
ND
0.100
mg/L
2-Butanone (MEK)
ND
0.200
mg/L
Carbon tetrachloride
ND
0.100
mg/L
Chlorobenzene
ND
0.100
mg/L
Chloroform
ND
0.100
mg/L
1,2-Dichloroethane
ND
0.100
mg/L
" -`-1,l-Dichl5-r—oethene----
Tetrachloroethene
ND
0.100
mg/L
- Trichloroethene
ND
0.100
mg/L
Vinyl chloride
ND
0.100
mg/L
Surrogate: 1, 2-Dichloroethane-D4
Surrogate: Toluene-D8
Surrogate: 4-Brontofluorobenzene
LCS (B4E0933-BSI)
88 70-'130
102 70-130
116 70-130
83 70-130
94 70-130
115 70-130
Benzene
0.0192
0.00200
mg/L
0.0200
96
70-130
2-Butanone (MEK)
0.0184
0.00400
mg/L
0.0200
92
60-140
' Carbon tetrachloride
0.0203
0.00200
mg/L
0.0200
102
70-130
Chlorobenzene
0.0193
0.00200
mg/L
0.0200
97
70-130
Chloroform
0,0170
0.00200
mg/L
0.0200
85
70-130
1,2-Dichloroethane
0.0177
0.00200
mg/L
0.0200
88
70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 I fax 864.232,6140" r6gersahidCallcott.C011l
an employee -owned company
0512912014 11:52 This report may not be reproduced, ercept in full, without written permission front Rogers & Callcolt, Inc.

&Cak6tt"
_ E:NVIR0: ME -TAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Volatile Organics
Quality Control Summary
Reporting
'Spike
Source
_
%REC RPD
V
Parameter
Result
Limit
Units
Level
Result
%REC
Limits RPD Limit Flags
Batch B4E0933 - EPA 5030
LCS (B4E0933-BSI)
1,1-Dichloroethene
0.0177
0.00200
mg/L
0.0200
88
70-130
Tetrachloroethene
0.0184
0.00200
mg/L
0.0200
92
70-130
Tricbloroethene
0.0175
0.00200
mg/L
0.0200
87
70-130
Vinyl chloride
0.0174
0.00200
mg/L
0.0200
87
60-140
Surrogate: 1,2-Dichloroethane-D4
92
70-130
Surrogate: Toluene-D8
91
70-130
Surrogate:4-Bromq/luorobenzene
90
70-130
Matrix Spike (B4E0933-MS1)
Source: 4050230-02
'
Benzene
1.05
0.100
mg/L
1.00
ND
105
70-130
}
2-Butanone (MEK)
0.699
0.200
mg/L
1.00
ND
69
60-140
Carbon tetrachloride
0.993
0.100
mg/L
1.00
ND
99
70-130 '
Chlorobenzene
0.992
0.100
mg/L
1.00
ND
99
70-130
Chloroform
0.910
0.100
mg/L
1.00
ND
91
70-130
1,2-Dichloroethane
0.830
0.100
mg/L
1.00
ND
83
70-130
1,1-Dichloroethee
0.905
0.100
mg/L
1.00
ND
90
70-130
Tetrachloroethene
1.07
0.100
mg/L
1.00
ND
107
70-130
Trichloroethene
0.835
0.100
mg/L
1.00
ND
84
70-130
Vinyl chloride
0.803
0.100
mg/L
1.00
ND
80
60-140
Surrogate: 1, 2-Dichloroethane-D4
Surrogate: Toluene-D8
- --
-- - - - ---Surrogate:
4-Bromofluorobenzene--------
Matrix Spike (B4E0933-MS2)
Source: 4050333-03
Benzene
1.07
0.100
2-Butanone (MEK)
0.738
0.200
Carbon tetrachloride
1.00
0.100
Chlorobenzene
1.00,
0.100
Chloroform
0.922
0.100
1,2-Dichloroethane
0.840
0.100
1,1-Dichloroethee
0.914
0.100
Tetrachloroethene
1.07
0.100
^,
Trichlomethene
0.923
0.100
'-
Vinyl chloride
0.782
0.100
Surrogate: 1,2-Dichlaroethane-D4
Surrogate: Toluene-D8
87 70-130
98 70-130
--85-----70-130
mg/L
1.00
ND
107
70-130
mg/L
1.00
ND
74
60-140
mg/L
1.00
ND
100
70-130
mg/L
1.00
ND
100
70-130
mg/L
1.00
ND
92
70-130
mg/L
1.00
ND
84
70-130
mg/L
1.00
ND
91
70-130
mg/L
1.00
ND
107
70-130
mg/L
1.00
ND
82
70-130
mg/L
1.00
ND
78
60-140
88 70-130
97 70-130
PO Box 5655 .I Greenville, SC 29606 1 426. Fairforest Way I Greenville,_SC 24607 I _main t364.2321556 I fax $64.232.5140 POg@rS�llldCaHCOl .COt71 _
an employee-owned_company
05129/2014 11:52
This report may not be reproduced, except in full, without written permission from Rogers B Callcon, Inc.

Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
arameter Result Limit units Level Result %REC Limits RPD Limit Flags
Batch B4E0933 -EPA 5030
Matrix Spike (B4E0933-MS2)
Source: 4050333-03
-
Surrogate:4-Bromofluorobenzene
89
70-130
Matrix Spike (B4E0933-MS3)
Source: 4050350-01
Benzene
1.07
0.100
mg/L
1.00
ND
107
70-130
2-Butanone QvIEK)
0.710
0.200
mg/L
1.00
ND
71
60-140
Carbon tetrachloride
0.948
0.100
mg/L
1.00
ND
95
70-130
Chlorobenzene
1.01
0.100
mg/L
1.00
ND
101
70-130
d Chloroform
0.916
0.100
mg/L
1.00
ND
92
70-130
1,2-Dichloroethane
0.822
0.100
mg/L
1.00
ND
82
70-130
1,1-Dichloroethene
0.874
0.100
mg/L
1.00
ND
87
70-130
" Tetrachloroethene
1.05
0.100
mg/L
1.00
ND
105
70-130
- Trichloroethene
0.829
0.100
mg/L
1.00
ND
83
70-130
Vinyl chloride
0.756
0.100
mg/L
1.00
ND
76
60-140
Surrogate: 1,2-Dichloroethane-D4
86
70-130
r
Surrogate: Toluene-D8
97
70-130
Surrogate:4-Brontafluorobenzene
94
70-130
Matrix Spike Dup (B4E0933-MSD1) Source: 4050230-02
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
0.990
0.100
mg/L
1.00
ND
99
70-130
0.766
0.200
1119/1-
1.00
ND
77
60-140
0.919
0.100
1119/1,
1.00
ND
92
70-130
0.938
0.100
mg/L
1.00
ND
94
70-130
0.870
0.100
mg/L
1.00
ND
87
70-130
0.819
0.100
mg/L
1.00
ND
82
70-130
0.842
0.100
mg/L
1.00
ND
84
70-130
0.980
0,100
mg/L
1.00
ND
98
70-130
0.776
0.100
mg/L
1.00
ND
78
70-130
0.725
0.100
mg/L
1.00
ND
72
60-140
Surrogate:l,2-Dichloroethane-D4
86
70-130
Surrogate: Toluene-D8
92
70-130
Surrogate: 4-Bromofluorobenzene
89
70-130
6
11
8
6
4
1
7
9
7
10
20
20
20
20
20
20
20
20
20
20
PO_ Box 5655 I Greenville, SC 29606 1 426 Fairforest`Way I Greenville, SC 29607 1 main 864.232.1556, I. fax,B64.232.6140.= rOgersandC1.IICOtt.COt11
an employee -owned company -
This report may not be reproduced, except in full, without written permission from Rogers & C'allco, nc.
• OS/29/20I411:52 ttIs ar

Ds.&l_coteCl
ENVnIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0741- EPA 3510C - GCMS
Blank (B4E0741-BLKI)
k 2-Methylphenol (o-Cresol)
3/4-Methylphenol (m,p-Cresol)
total Cresol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
-- 2,4,6-Trichlorophenol
Blank (B4E0741-BLK2)
ND 0.0100
ND 0.0100
ND 0.0200
ND' 0.0100
ND 0.0100
ND 0.0100
ND 0.0100
ND 0.0100
ND 0.0100
ND 0.0100
ND 0.0100
ND 0.0100
.Surrogate: Nitrobenzene-D5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fluorophenol
Surrogate: Phenol-D5
Surrogate: 2, 4, 6-Tribromophenol
Surrogate: Terphenyl D14
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
2-Methylphenol (o-Cresol)
ND
0.100
mg/L
3/4-Methylphenol (m,p-Cresol)
ND
0.100
mg/L
' total Cresol
ND
0.200
mg/L
2,4-Dinitrotoluene
ND
0.100
mg/L
Hexachlorobenzene
ND
0.100
mg/L
l Hexachlorobutadiene
ND
0.100
mg/L
r Hexachloroethane
ND
0.100
mg/L
Nitrobenzene
ND
0.100
mg/L
Pentachlorophenol
ND
0.100
mg/L
Pyridine
ND
0.100
mg/L
2,4,5-Trichlorophenol
ND
0.100
mg/L
2,4,6-Trichlorophenol.
ND
0.100
mg/L
80 35-114
80 43-116
54 21-110
34 10-110
86 10-123
86 33-141
'
Surrogate: Nitrobenzene-D5 72 35-114
Surrogate: 2-Fluorobiphenyl 79 43-116
Surrogate: 2-Fluorophenol 47 21-110
'
Surrogate: Phenol-D5 30 10-110
PO Sox 5655.1 Greenville, SC 29.606 14.26 Pairforest Way I Greenville, SC 29607 1 main 864.232,1556 I. fax [phone]
rogersandcalk tt.eom
}
an_employee-owned company
�`�
0512912014 11:52 This report may not he reproduced, except in full, without written permission from Rogers & Callcott, Inc.
.

Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0741- EPA 3510C - GCMS
Blank (B4E0741-BLK2)
Surrogate: 2,4, 6-Tribromophenol 85 10-123
Surrogate: Terphenyl-D14 92 33-141
LCS (B4E0741-BSI)
2-Methylphenol (o-Cresol)
0.592
0.100
mg/L
0.900
74
50-90
3/4-Methylphenol (m,p-Cresol)
1.10
0.100
mg/L
1.60
69
42-92
2,4-Dinitrotoluene
0.724
0.100
mg/L
0.800
90
65-104
Hexachlorobenzene
0.718
0.100
mg/L
0.800
90
72-116
Hexachlorobutadiene
0.651
0.100
mg/L
0.900
81
39-100
Hexachloroethane
0.645
0.100
mg/L
0.800
81
36-99
Nitrobenzene
0.665
0.100
mg/L
0.800
83
51-108
Pentachlorophenol
0.730
0.100
mg/L
0.800
91
49-111
•
Pyridine
0.374
0.100
mg/L
0.800
47
23-67
2,4,5-Trichlorophenol
0.723
0.100
mg/L
0.900
90
56-112
2,4,6-Trichlorophenol
0.723
0.100
mg/L
0.800
90
55-113
Surrogate: Nitrobenzene-D5
83
35-114
Surrogate: 2-Fluorobiphenyl
89
43-116
Surrogate: 2-Fluorophenol
59
21-110
Surrogate: Phenol-D5
33
10-110
Surrogate: 2,4,6-Tribromophenol
91
10-123
Surrogate: Terphenyl-DU
101
33-141
Matrix Spike (B4E0741-MS1) Source: 4050230-02
2-Methylphenol (o-Cresol)
0.537
0.100
mg/L
0.800
ND
67
35-100
3/4-Methylphenol (m,p-Cresol)
1.02
0.100
mg/L
1.60
ND
64
30-97
2,4-Dinitrotoluene
0.665
0.100
mg/L
0.800
ND
83
60-109
Hexachlorobenzene
0.572
.0.100
mg/L
0.800
ND
71
68-114
Hexachlorobutadiene
0.527
0.100
mg/L
0.800
ND
66
35-101
Hexachloroethane
0.513
0.100
mg/L
0.800
ND
64
37-93
Nitrobenzene
0.582
0.100
mg/L
0.800
ND
73
40-112
Pentachlorophenol
0.809
0.100
mg/L
0.800
ND
101
44-120
' Pyridine
0.348
0.100
mg/L
0.800
ND
44
14-68
2,4,5-Trichlorophenol
0.659
0.100
mg/L
0.800
ND
82
30-132
2,4,6-Trichlorophenol
0.662
0.100
mg/L
0.800
ND
83
40-123
Surrogate: Nitrobenzene-D5
70
35-114
Surrogate: 2-Fluorobiphenyl
73
43-116
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232,1556 1 fax 864.232A 140 rog&sandcallcottxorn.
an employee -owned company
0512912014 11:52 This report may not be reproduced, except in full, without written permission from Rogers & Calliott, Inc.

ERVIRONMENTA
.....
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B4E0741- EPA 3510C - GCMS
Matrix Spike (B4E0741-MSl) Source: 4050230-02
Surrogate: 2-Fluorophenol 44 21-110
Surrogate: Phenol-D5 28 10-110
Surrogate: 2, 4, 6-Tribromophenol 82 10-123
Surrogate: Terphenyl-D14 68 33-141
Matrix Spike (B4E0741-MS2) Source: 4050333-01
2-Methylphenol(o-Cresol)
0.454
0.100
mg/L
0.800
ND
57
35-100
3/4-Methylphenol (m,p-Cresol)
0.930
0.100
mg/L
1.60
ND
58
30-97
2,4-Dinitrotoluene
0.746
0.100
mg/L
0.800
ND
93
60-109
Hexachlorobenzene
0.675
0.100
mg/L
0.800
ND
84
68-114
Hexachlorobutadiene
0.533
0.100
mg/L
0.800
ND
67
35-101
Hexachloroethane
0.508
0.100
mg/L
0.800
ND
64
37-93
Nitrobenzene
0:620
0.100
mg/L
0.800
ND
78
40-112
Pentachlorophenol
0.795
0.100
mg/L
0.800
ND
99
44-120
Pyridine
0.265
0.100
mg/L
0.800
ND
33
14-68
2,4,5-Trichlorophenol
0.715
0.100
mg/L
0.800
ND
89
30-132
2,4,6-Trichlorophenol
0.704
0.100
mg/L
0.800
ND
88
40-123
Surrogate: Nitrohenzenne-D5
75
35-114
Surrogate: 2-Fluorobiphenyl
80
43-116
Surrogate: 2-Fluorophenol
47
21-110
Surrogate: Phenol-D5
30
10-110
Surrogate: 2,4,6-Tribromophenol
89
10-123
Surrogate: Terphe»,vl-D14
92
33-141
Matrix Spike (B4E0741-MS3)
Source: 4050333-03
2-Methylphenol (o-Cresol)
0.570
0.100
mg/L
0.800
ND
71
35-100
3/4-Methylphenol (m,p-Cresol)
1.07
0,100
mg/L
1.60
ND
67
30-97
2,4-Dinitrotoluene
0.775
0.100
mg/L
0.900
ND
97
60-109
Hexachlorobenzene
0.710
0.100
mg/L
0.800
ND
89
68-114
Hexachlorobutadiene
0.576
0.100
mg/L
0.800
ND
72
35-101
Hexachloroethane
0.561
0.100
mg/L
0.800
ND
70
37-93
` Nitrobenzene
0.649
0.100
mg/L
0.800
ND
81
40-112
Pentacblomphenol
0.828
0.100
mg/L
0.800
ND
104
44-120
Pyridine
0.265
0.100
mg/L
0.900
ND
33
14-68
r 2,4,5-Trichlorophenol
0.757
0.100
mg/L
0.800
ND
95
30-132
2,4,6-Trichlorophenol
0.727
0.100
mg/L
0.800
ND
91
40-123
PO Box 5655 ( Greenville, SC 29606 1 426`.Nirforest Way I Greenville, 5C 29607 1 main 864.232,1556 1 fax [phone]
1'OgerSandCallC6ti.COC11,
_
an employee -owned company
0512912014 11:52
This report may oat be reproduced, except in full, without written permission from Rogers d Callcott, Inc.
d

h: tifCo
nitr�_ .a age.
! !!!!ENV-IR:0 EN
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting
Spike
Source
%REC
RPD
Parameter
Result
Limit
Units
Level
Result
%REC
Limits
RPD
Limit Flags
i
Batch B4E0741- EPA 3510C - GCMS
Matrix Spike (B4E0741-MS3)
Source: 4050333-03
Surrogate: Nitrobenzene-D5
78
35-114
i
Surrogate: 2-Fluorobiphenyl
84
43-116
Surrogate: 2-Fluorophenol
49
21-110
Surrogate: Phenol-D5
32
10-110
-
Surrogate: 2,4,6-Tribromophenol
93
10-123
Surrogate: Terphenyl-D14
96
33-141
Matrix Spike Dup (B4E0741-MSDI) Source: 4050230-02
2-Methylphenol(o-Cresol)
0.626
0.100
mg/L
0.800
ND
78
35-100
15
30
3/4-Methylphenol(m,p-Cresol)
1.19
0.100
mg/L
1.60
ND
75
30-97
15
30
2,4-Dinitrotoluene
0.796
0.100
mg/L
0.800
ND
100
60-109
18
30
Hexachlorobenzene
0.669
0.100
mg/L
0.800
ND
84
68-114
16
30
N,
Hexachlorobutadiene
0.633
0.100
mg/L
0.800
ND
79
35-101
18
45
Hexachloroethane
0.608
0.100
mg/L
0.900
ND
76
37-93
17
45
Nitrobenzene
0.684
0.100
mg/L
0.800
ND
86
40-112
16
30
i-
Pentachlorophenol
0.988
0.100
mg/L
0.800
ND
123
44-120
20
30 S
Pyridine
0.336
0.100
mg/L
0.800
ND
42
14-69
4
30
2,4,5-Trichlorophenol
0.777
0.100
mg/L
0.800
ND
97
30-132
17
30
2,4,6-Trichlorophenol
0.782
0.100
mg/L
0.800
ND
98
40-123
17
30
Surrogate: Nitrobenzene-D5
83
35-114
Surrogate:2-Flunrobiphenyl
88
43-116
Surrogate: 2-Fluorophenal
54
21-110
Surrogate: Phenol-D5
34
10-110
t
Surrogate: 2,4,6-Tribromophenol
101
10-123
Surrogate: Terphenyl-D14
68
33-141
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 I main 864,232.1556 1 fax.864.232,6140 rogersandcallcott.com
an employee=owned company -
0512912014 11:52 This report may not be reproduced, except in full, without written permission front Rogers & Callcott, Inc.

.�timger
m s
y
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Pesticides
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0743 - EPA 3510C - GC
• - 'Blank (B4E0743-BLKI)
Z
Gamma-BHC (Lindane)
ND
0.000050
mg/L
Chlordane
ND
0.00050
mg/L
Endrin
ND
0.000050
mg/L
Heptachlor
ND
0.000050
mg/L
Heptachlor epoxide
ND
0.000050
mg/L
Toxaphene
ND
0.00050
mg/L
Methoxychlor
ND
0.000050
mg/L
Surrogate: 2,4,5,6-Tetrachloro-m-xvlene
96
60-130
Surrogate: Decachlorobiphenyl
69
30-150
Blank (B4E0743-BLK2)
Gamma-BHC (Lindane)
ND
0.00050
mg/L
Chlordane
ND
0.0050
mg/L
Endrin
ND
0.00050
mg/L
Heptachlor
ND
0,00050
mg/L
Heptachlor epoxide
ND
0.00050
mg/L
Toxaphene
ND
0.0050
mg/L
Methoxychlor
S
ND
0.00050
mg/L
Surrogate: 2,4,5,6-Tetrachloro-m-cvlene
94
60-130
Surrogate: Decachlorobiphenyl
100
30-150
LCS (B4E0743-BS1)
Gamma-BHC (Lindane)
0.0041
0,00050
mg/L
0.00400
102
70-130
Endrin
0.0041
0.00050
mg/L
0.00400
104
70-130
Heptachlor
0.0041
0.00050
mg/L
0.00400
102
70-130
Heptachlor epoxide
0.0040
0.00050
mg/L
0.00400
101
70-130
Methoxychlor
0.0047
0.00050
mg/L
0.00400
117
70-130
Surrogate:2,4,5,6-Tetrachloro-m-xvlene
96
60-130
Surrogate: Decachlorobiphenyl
98
30-150
Matrix Spike (B4E0743-MS1)
Source: 4050230-02
Gamma-BHC (Lindane)
0.0042
0.00050
mg/L
0.00400
ND
105
60-140
Endrin
0.0042
0.00050
mg/L
0.00400
ND
106
60-140
Heptachlor
0.0040
0.00050
mg/L
0.00400
ND
99
60-140
Heptachlor epoxide
0.0042
0.00050
mg/L
0.00400
ND
104
60-140
' Methoxychlor
r
0.0036
0.00050
mg/L
0.00400
ND
90
60-140
PO Box 5655 1 Greenville, SC 29606.1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 6.864.232,6140 ro&rsan&alIC0tt.00171
--,an employee -owned company ;
0512912014 11:52 This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. _
i t':�0- ITI�. P

o CalicbU
• r,ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Pesticides
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags
Batch B4E0743 - EPA 3510C - GC
Matrix Spike (B4E0743-MS1) Source: 4050230-02
Surrogate: 2,4,5,6-Tetrachloro-m-xvlene 93 60-130
Surrogate: Decachlorobiphenyl 56 30-150
Gamma-BHC (Lindane)
0.0045 0.00050
mg/L
0.00400
ND
112
60-140
Endrin
0.0045 0.00050
mg/L
0.00400
ND
113
60-140
Heptachlor
0.0045 0.00050
mg/L
0.00400
ND
112
60-140
Heptachlor epoxide
0.0043 0.00050
mg/L
0.00400
ND
108
60-140
Methoxychlor
0.0043 0.00050
mg/L
0.00400
ND
108
60-140
Surrogate:2,4,5,6-Tetrachloro-m-xvlene
97
60-130
Surrogate: Decachlorobiphenyl
96
30-150
Matrix Spike (B4E0743-MS3)
Source: 4050333-03
Gamma-BHC (Lindane)
0.0041 0.00050
mg/L
0.00400
ND
102
60-140
Endrin
5
0.0044 0.00050
mg/L
0.00400
ND
110
60-140
Heptachlor
0.0040 0.00050
mg/L
0.00400
ND
100
60-140
Heptachlor epoxide
0.0042 0.00050
mg/L
0.00400
ND
105
60-140
Methoxychlor
0.0042 0.00050
mg/L
0.00400
ND
105
60-140
1
"
Surrogate: 2,4,5,6-Tetrachloro-m-xvlene
96
60-130
Surrogate: Decachlorobiphenyl
93
30-150
Matrix Spike Dup (B4E0743-MSD1) Source: 4050230-02
Gamma-BHC (Undone)
0.0042 0.00050
mg/L
0.00400
ND
106
60-140
0.4
20
Endrin
0.0044 0.00050
mg/L
0.00400
ND
110
60-140
4
20
Heptachlor
0.0042 0.00050
mg/L
0.00400
ND
105
60-140
6
20
Heptachlor epoxide
0.0043 0.00050
mg/L
0.00400
ND
106
60-140
2
20
Methoxychlor
0.0040 0.00050
mg/L
0.00400
ND
99
60-140
10
20
Surrogate: 2,4,5,6-Tetrachloro-m sylene
94
60-130
Surrogate: Decachlorobiphenyl
77
30-150
PO Box 5655 1 Greenville, SC 29606 1 426 Fairfoi est Way 1. Greenville,, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcottxom
an employee awned company
0512912014 11:52 This report may not be reproduced, except in fill, without written permission from Rogers & Callcott, Inc.

Rgrs & Cll®t't
- ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP Bottle Extraction
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result % REC Limits RPD Limit . Flags
Batch B4E0632 - EPA 1311
Blank-(B4E0632-BLKI)
TCLP Bottle Extraction Complete
Blank (B4E0632-BLK2)
TCLP Bottle Extraction Complete
.PO Sox 5655 1 Greenville, SC 29606 1 426 Fair(orest Way 1 Greenville, SC 29607 I main 864.232.1556 1 fax [phone] roger sandcallcott.com
an employee -owned company
0512912014 11:52 This report may not be reproduced, except in,hdl, without written permission from Rogers d& Callc»tt, Inc: _

Mgers & CaIbtott
ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WW IT
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: 05/29/14 11:52
TCLP ZHE Extraction
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4E0487 - EPA 1311 - ZHE
Blank (B4E0487-BLKI)
TCLP ZHE Extraction Complete
Sample Preparation Data
Parameter
Batch
Sample ED
Prepared
Analyst
EPA 3005A ICP Digestion
EPA 3005A
B4E0543
4050230-02
05/15/2014 12:50
MEC
EPA 3050B Metal Digestion
EPA 3050B
B4E0350
4050230-01
05/12/2014 12:55
MEC
EPA 3510 Extraction
EPA 3510C - GC
B4E0743
4050230-02
05/21/2014 09:12
DBB
EPA 3510 Extraction
EPA 3510C - GCMS
B4E0741
4050230-02
05/20/2014 10:30
DBB
EPA 7470A Mercury Digestion
EPA 7470A
B4E0534
4050230-02
05/15/2014 09:37
DER
EPA 7471B Mercury Digestion
EPA 7471B
B4E0494
4050230-01
05/14/2014 16:25
DER
TCLP Extraction Data
Extraction
Initial
Final
Parameter
Batch Sample ED Started Finished Fluid #
pH
pH
EPA 1311- TCLP Extraction
EPA 1311
B4E0632 4050230-02 5/13/14 at 1615 5/14/14 at 1200 2
12.31
11.72
EPA 1311- TCLP ZHE
EPA 1311 - ZHE
B4E0487 4050230-02 5/13/14 at 1705 5/14/14 at 0930 1
N/A
N/A
PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.com
an employee -owned company
0512912014 11:52 This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc.

R6 - brs &Caltc®tt
-ENVIRONMENTAL
Environmental Testing Solutions Project: Waynesville WWTP
351 Depot St. Work Order: 4050230
Asheville, NC 28801-4310 Reported: ' 05/29/14 11:52
Data Qualifiers and Definitions
ND Analyte NOT DETECTED at or above the reporting limit
NR Not reported
RPD Relative Percent Difference
PI The RPD between the sample / duplicate or matrix spike / spike duplicate was not within control limits due to matrix interference.
S The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits. The Laboratory Control Sample
(LCS) was within control limits.
S 1 The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits due to matrix interference. The
Laboratory Control Sample (LCS) was within control limits.
S3 Estimated value - the spike result exceeded the calibration range. The spike recovery was not evaluated against the control limits.
PO Sox 5655 1 Greenville, SC 29606 1 426 fairforest Way I Greenville, SC 29607 ( main 864,232,1556 1 fax [phone] rogersandcallcott.com
an employee -owned company
0512912014 11:52 This report may not be reproduced, except to full, without written permission from Rogers R Callcott, Inc. „ _ MIMAIT

5
. 4
ROGMS &. CA LLCUrT
pie
JABORATORY SMIACES
P.O. Box 5655, Greenville, SC 29606
Phone [phone] Fax [phone]
Shipping Address: 426 Fairforest Way
Greenville, SC 29607
Client Nome
Address
J�r
Report To:
6_
.,A
CHAIN OF CUSTODY RECORD PAGE OF
Filtered (Yes/N
Cooled ( No)
Container Type (Q/n
Telephone No. FAX No. c
0
PO No. Project No. v
Rogers do o
Yr._
Callcott Dote Time Sample Description
Lob No. �
9- q- i
0 `�.'
2 d - �,
tin 011,� k,mUrAo SlOdci-c�tu,o na � X x . �)[
SAMPLER
Date Time
ReceipO by (Sig.)
Date/Time
Relinquished by (Sig.)
��
Shippere�
06(GM
Relinquished by (Sig.)
Date/rime
Re ved )
at /Time
Shipp o
I
Relinquished by (Sig.)
Date/Time
Recdived ( g.)
Dote/Time
©
.
Shipper Nome do
Seal at'chd by Recd. Intact Sea] $ at'chd by Recvd. Intact I
Form Revised July 2008
Container Volume
Sample Type (2rob/Co posite
Sample Source (WW, GW, DW, tha
Sample Source Chlo d (Yes/Nc
Lab Receipt Cl, Ch k
Lob Receipt pH Check
Preserved (Code)
A -None D-NoOH G-Boric Acid
B-HNOi E-HCL H-Ascorbic Acid
C-H,SO, F-NNS,O, 1- _
COM MEN7&
AtAA 1� N oral KA
KNOWN HAZARDS ASSOCIA7ED WITH SAMPLES
Temperature of blank or repr entative sample
At time of collection 'C
At time of lob receipt "C

_. Rogers & Cakott
ENVIRONMENTAL
Sample Receipt Verification
Date (� work
Client:
Received:' w ' Order:
Carrier Name: Client FedEx
Tracking umber:
ZIPS
UPS% Ma'
(/
�A_
Cou ier
field Services
b
14b ca;?� 0
Other:
.Receipt Criteria
Y
e
s
o
A
Comments
Shipping container / cooler intact?
Damaged Leaking Other:
Custody seals intact?
COC included with samples?
COC signed when relinquished and received?
Sample bottles intact?
Damaged Leaking Other:
Sample ID on COC agree with label on bottle(s)?
Date / time on COC agree with label on bottle(s)?
Number of bottles on COC agrees with number of bottles received?
Samples received within holding time?
Sample volume sufficient for analysis?
VOA vials free of headspace (<6mm bubble)?
Temp at receipt recorded on COC
Samples cooled? Temp measured with IRthermometer -SN: 97050067
Ice Cold Packs Dry Ice None
Samples requiring pH preservation at proper pH?
Note: Samples for metals analysis may be preserved upon receipt in the lab.
If in-house preservation used — record Lot #
HCL
H3POa
H,SO4
NaOH
HNO,
Other
Comments:
• I were non-conformance issues noted at sample receipt?
Non -Conformance issue other than noted above:
Yes or
Revised January 2014 Completed by:

49 Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • (910) 392-"24 (Fax)
710 $owsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Environmental Testing Solutions, Inc.
Post Office Box 7565
Asheville NC 28802
Attention: Kelley Keenan (ETS)
Lab ID Sample ID:
14-12610 Site: 603 Lime Sludge
Test Method
Ignitability
Cyanide
Total Solids (%)
Sulfide
2,4,5-TP
2,4-D
Comment
Reviewed by:
Date of Report: May 30, 2014
Customer PO #•
Customer ID: 08100055
Report #: 2014-05238
Project ID: Waynesville WWTP
Collect DatelTime Matrix Sampled by
5/6/2014 9:15 AM . Solid/Sludge Client
EPA 1030
EPA 335.4
SM 2640 B
SM 4500 S 0
SW846 Method 8151A
SW846 Method 8151A
Results Date Analyzed
<0.8 mm/sec
05/16/2014
. <0.132 mg/kg
05/20/2014
45.4 %
05/07/2014
<0.264 mglkg
05/20/2014
<0.0003 mg/L
05/20/2014
<0.0003 mg/L
05/20/2014
Report #:: 2014-05238 Page 1 of 1

•
•
FMr
t a Environmental Testing Solutions, Inc.
CHAIN -OF -CUSTODY / Analytical Request
Client Name: / Q 63
Address:
PO Box 7565, Asheville, NC 28802
Phone: (828)
3500-9364,,Fax: [phone]
P—i—fNom-4, 1k)dUjrDOVVkLD 111 A�IL
Report to:
Phone:
PO Number:
Fax:
R....o.fM AnalwePC
Project'Number:
PH Checked Upon Recei
Cl, < 0.2 mo Upon Recei pt
Preservatives
Sample Identification
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V1Zl�l
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,DWO)
1 j
Received on Ice:
Y / N
`'-
Sealed Cooler:
Y / N�
Samples.lniacr
""Y / N
^_`1
AddlHonal Comments:
wv—�— hL/ O5-„� `. J , /
AAG1 l•r
J J
,
Printed
N of Satt��er
(J`
--_ •�
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Signature
of Sampler:

L
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Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
CHAIN -OF -CUSTODY / Analytical RequestPI 102-
Client Name: U),Agew51)t1 e
Address:Q(v l�)a�h<<; �tra,
)A.. i ale A)C d- 6795
If
Report to:' /14ar{G A . 16v,e5
Phone: Flag -ySa-1/( 8S Fax:
PO Number:
Rennp.-MA Analvses
Project Number-
J
L
pH Checked Upon Receipt
CIZ < 0.2 mg/1 Upon Receipt
Preservatives
A Sample Identification
y
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O / N
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Y / N
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Y / N
Additional Comments: Sa A 44o1CY�tit r I C E
Printed Name of Sampler:
Mark A. JcnQS
J apf 5inm,5
SSG//
Signatur a Qf SaQmple .

6��-
Aluminum pH
Ammonia -Nitrogen Phosphorus
Calcium Plant Available Nitrogen (by calculation)
Magnesium Potassium
Nitrate -Nitrite Nitrogen Sodium
% Total Solids TKN
After the residuals have been monitored for two years at the above frequency, the Permittee
may submit a request to the Division for a permit modification for the reduction of the
frequency of monitoring for pollutant concentrations and for the pathogen density
requirements, but in no case shall the frequency of monitoring be less than once per year
when residuals are sold or given away.
4. A Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the
Permittee annually. The TCLP analysis shall include the following parameters (please note
the regulatory level in mg/L in parentheses): o , / /n le s /- v j a r_-_ i Q- AP:
Arsenic (5.0)
Benzene (0.5)
Carbon tetrachloride (0.5)
Chlorobenzene (100.0)
Chromium (5.0)
m-Cresol (200.-0)
Cresol (200.0)
1,4-Dichlorobenzene (7.5)
1, 1 -Dichloroethylene (0.7)
Endrin (0.02)
Hexachlorobenzene (0.13)
Hexachloroethane (3.0)
Lindane (0.4)
Methoxychlor (10.0)
Nitrobenzene (2.0)
Pyridine (5.0)
Silver (5.0)
Toxaphene (0.5)
2,4,5-Trichlorophenol (400.0)
2,4,5-TP (Silvex) (1.0)
Barium (100.0) ---
Cadmium (1.0)
Chlordane (0.03)
Chloroform (6.0)
o-Cresol (200.0)
p-Cresol (200.0)
2,4-D (10.0)
1,2-Dichloroethane (0.5)
2,4-Dinitrotoluene (0.13)
Heptachlor (and its hydroxide) (0.008)
Hexachloro-1,3-butadiene (0.5)
Lead (5.0)
Mercury (0.2)
Methyl ethyl ketone (200.0)
Pentachlorophenol (100.0)
Selenium (1.0)
Tetrachloroethylene (0.7)
Trichloroethylene (0.5)
2,4,6-Trichlorophenol (2.0)
Vinyl chloride (0.2)
5. All residuals included in this permit must be monitored quarterly, from the date of permit
issuance, for compliance with condition 19 of this permit. Data to verify stabilization of
the residuals must be maintained by the Permittee. The required data is specific to the
stabilization process utilized, but should be sufficient to clearly demonstrate compliance
with the Class A pathogen requirements in 40 CFR Part 503.32(a) and the vector attraction
reduction requirements in 40 CFR Part 503.33. In addition, the EPA certification
statements concerning compliance with pathogen requirements, vector attraction reduction
requirements and management practices must be completed quarterly by the proper
authority or authorities if more than one is involved, either the person who generates the
residuals or the person who prepares the residuals to be sold or given away.
After the residuals have been monitored for two years at the above frequency, the Permittee
may request a permit modification for the reduction of the frequency of monitoring for
Pollutant concentrations and for the pathogen density requirements, but in no case shall the
frequency of monitoring be less than once per year when residuals are sold or given away.
0
WA00140

IWO
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Proiect Name: InJALA hp4Ib I I(7
CHAIN -OF -CUSTODY / Analytical Request Z.'? Z.
Client Name:
Address: �� (Q LZ✓A�a� u-�' 1 0�
Wa4 ww,` Il e , Ills a 8 78.5'
Reportto: Mp,r)C 4, Jone5
Phone: !8 LlSa- yGBS Fax: $a8-yS1�-•2013
PO Number:
Reauested Analvses
Project
Number:
pH Checked Upon Receipt
Preservatives
C12 < 0.2 mg/1 Upon Receipt
V
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o
Sample Identification
a
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U
s
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y
y
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(°C) Comments
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,l
Temperature (°C) S C Ma / '
.Joh�'S
W4 -CSv,JC -049h 7
�1 . 30 S Caur-C'✓
Received on Ice:
Y / N
rT5 ur, er
���-s
'C,15
os•o�-1�1
ly3
Sealed Cooler:
J / N
Samples Intact:
1 Y Y N
Additional Comments:
lqsr , G>.h ��Cu Cr Pb � � M® al; SDI �n� Fe�,l ��� �
r 9) / I
Printed Sampler:
- nature
Date
n MmD�t
I 1 !t t�-1v +ro3�e�l CAr Wl /V; ra+e-/0,`4rde Nidro ea��-fa A? Se%al
Name of
q f A, 1orICr
/�
JE�Y' St �st5
��� /
Signatur ofSamper:
41 �a���"�� pl�r�� Avg �abl��'�r®s�n(b�C4�Cu�4��dN1