NCS000392_OTHER_20160525

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
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❑FINAL PERMIT
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Pickle, Ken
From: Elizabeth M. Wike <[e-mail]>
Sent: Wednesday, May 25, 2016 7:58 PM
To: Pickle, Ken
Subject: RE: DAK Cape Fear Site NPDES Stormwater Permit Renewal Fees
Ken,
Thanks so much for such a good update on our permit status. We are in no particular hurry, just want to know the
status. Thank you.
Elizabeth Wike
Sr. Environmental Engineer
DAK Americas LLC
1205 Culbreth Drive I Suite 200
Wilmington, NC 28405
Office: [phone]
Cell: [phone]
Fax: [phone]
From: Pickle, Ken [mailto:[e-mail]]
Sent: Wednesday, May 25, 2016 11:23 AM
To: Elizabeth M. Wike
Cc: Bennett, Bradley
Subject: FW: DAK Cape Fear Site NPDES Stormwater Permit Renewal Fees
Oops,
Actually addressed to you, this time.
Ken
Ken Pickle
Stormwater Program Specialist
DEMLR Stormwater Permitting Program
Department of Environmental Quality
919 807 6376 office
ken.pickle@)ncdenr.gov
1612 Mail Service Center, Raleigh, NC 27699-1612
512 N. Salisbury St, Raleigh, NC 27604
l: "Nothing Compares
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
1

From: Pickle, Ken
Sent: Wednesday, May 25, 2016 11:21 AM
To: Pickle, Ken <[e-mail]>
Cc: Bennett, Bradley <bradle .bennett ncdenr. ov>
Subject: RE: DAK Cape Fear Site NPDES Stormwater Permit Renewal Fees
Hi Elizabeth,
Nice to hear from you. I heard yesterday's voice message just now. Our status on the renewal of NCS000392 is as
follows.
• The permit expires 5/31/2016 (in one week); we received your renewal application 12/10/2015. We consider
your renewal application as timely made.
Our billing records show that DAK is current through 7/31/2016; as in past years, billing will occur August.
Our database shows that the application reviewer is my supervisor, Bradley Bennett. However, Bradley doesn't
typically review renewal applications. This database entry should be understood to mean that Bradley is holding
the permit until staff time is available to work on it. When staff time is available, Bradley will assign it to one of
us. At that time the first thing our reviewer will do is contact DAK to let you know we have begun processing the
renewal application. At this point in time it is a certainty that we will be late in delivering your continued permit
coverage.
Federal rules establishing the NPDES program anticipate these circumstances explicitly. Under federal rule if the
permittee has made timely application for renewal, but the agency (us) is late in delivering the requested
renewal, the existing, expired permit continues in effect as long as the permittee complies with it. Please
continue to abide by your current permit even after the expiration date at the end of this month. Federal rules
protect DAK from "discharging without a permit" due simply to our delay as long as you abide by the permit.
Please do not interpret our delay as indicating a problem with the DAK renewal application. This circumstance is
not particular to DAK, as we have a substantial backlog of other renewals presently.
Unfortunately, I cannot give you a reliable estimate of when we will be able to pick up the DAK renewal and
issue the renewed coverage.
Ken
Ken Pickle
Stormwater Program Specialist
DEMLR Stormwater Permitting Program
Department of Environmental Quality
919 807 6376 office
ken. pickle(d)ncdenr.gov
1612 Mail Service Center, Raleigh, NC 27699-1612
512 N. Salisbury St, Raleigh, NC 27604
r • --> `Nothing Compares--,,,
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
From: Pickle, Ken
Sent: Friday, December 04, 2015 9:55 AM

To: 'Elizabeth M. Wike' <[e-mail]>
Subject: RE: DAK Cape Fear Site NPDES Stormwater Permit Renewal Fees
Hi Elizabeth,
Please contact Deborah Reese in our Division if you need a duplicate invoice. Her phone number is [phone].
If Deborah is not available contact Laura Alexander at [phone]. Laura can also put together a duplicate invoice
for you.
Ken
From: Elizabeth M. Wike [_mailto:[e-mail]]
Sent: Friday, December 04, 2015 9:37 AM
To: Pickle, Ken <[e-mail]>
Subject: FW: DAK Cape Fear Site NPDES Stormwater Permit Renewal Fees
Ken,
I mailed DAK's application to renew its NPDES Stormwater Permit yesterday. I am just following up on the unpaid
invoice. Can you help?
Elizabeth Wike
Sr. Environmental Engineer
DAK Americas LLC
1205 Culbreth Drive I Suite 200
Wilmington, NC 28405
Office: [phone]
Cell: [phone]
Fax: [phone]
From: Elizabeth M. Wike
Sent: Monday, November 30, 2015 5:26 PM
To: 'Pickle, Ken'
Subject: RE: DAK Cape Fear Site NPDES Stormwater Permit Renewal Fees
Ken,
Thank you for your response. I need to get another copy of the invoice for the $860 annual fee that is overdue. Can you
please send me a copy or tell me who I need to contact to get one? Thank you.
Elizabeth Wike
Sr. Environmental Engineer
DAK Americas LLC
1205 Culbreth Drive I Suite 200
Wilmington, NC 28405
Office: [phone]
Cell: [phone]
Fax: [phone]
3

From: Pickle, Ken [mailto:ken. pickle6l ncdenr. ov]
Sent: Thursday, November 19, 2015 4:53 PM
To: Elizabeth M. Wilke
Cc: Bennett, Bradley
Subject: RE: DAK Cape Fear Site NPDES Stormwater Permit Renewal Fees
Hi Elizabeth,
My apologies for being late getting back to you.
No, we don't consider the changes discussed as a 'major modification.'
Typically there is no fee associated with the stormwater permit renewal. What typically happens is our accounting folks
stay on the same billing schedule that they had before. For example, if they originally billed you in July, they will forever
continue to bill you in July each year, until the permit is eventually rescinded. The renewal action itself has no fee, and is
not typically tied to the billing account.
For NCS000392 our database is showing that your most recent billing period is 81112015 through 713112016, with a
nominal billing due date of 81712015. Our database is showing that the $860 annual fee for that period is overdue. All
previous years back to 2004-2005 are shown as paid up. So, it looks like we have just the one bill which is " 3 months
past due.
It is not necessary to submit this year's annual fee along with the renewal application. In our system the two actions are
viewed separately. But please make payment on the overdue bill. Let me know if I can help with that.
Ken
From: Elizabeth M. Wilke [mailto:[e-mail]
Sent: Tuesday, November 10, 2015 12:59 PM
To: Pickle, Ken <[e-mail]>
Subject: DAK Cape Fear Site NPDES Stormwater Permit Renewal Fees
Ken,
Thank you for discussing the permit renewal process with me for DAK Americas' Cape Fear NPDES Stormwater Permit
No. NCS000392. What is the fee that should be submitted with the renewal application? Is what we discussed on
Friday a "major modification"?
Thanks.
Elizabeth Wike
Sr. Environmental Engineer
DAK Americas LLC
1205 Culbreth Drive I Suite 200
Wilmington, NC 28405
Office: [phone]
Cell: [phone]
Fax: [phone]
ewikeedakamericas.com

,t . .
www.dakamericas.com
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1.M
September 26, 2013
Mr. Ken Pickle
Division of Energy, Mineral, and Land Resources
Stormwater Permitting Program
512 N. Salisbury St.
Raleigh, NC 27604
RE: DAK Americas LLC - Cape Fear Site
Permit Revision Request for NPDES Stormwater Permit No. NCS000392
FILE: 14974\50406
Dear Mr. Pickle:
19 @Rowg
OCT 1 6 2013
DAK Americas LLC (DAK) requests revision to NPDES Stormwater Permit No. NCS000392 to reflect changing
conditions, due to decommissioning and demolition activities, at the DAK Cape Fear Site. This permit revision
request was prepared based on our September 25, 2013 telephone discussion with you. Per your request, this
letter provides a summary of the stormwater permit revisions that were requested in our September 6, 2013
letter to the Division of Water Resources/Water Quality Programs.
DAK requests five revisions to the stormwater permit as a result of decommissioning and demolition activities at
the Cape Fear Site. The requested revisions involve diverting stormwater that is currently treated at the on -site
wastewater treatment plant (WWTP) to other existing surface water outfalls. The North Carolina Department of
Environment and Natural Resources (NCDENR) and DAK have discussed that implementation of each revision
will be contingent upon DAK's completion of specific triggering events. Table 1 summarizes the requested
revisions and the triggering events associated with each request.
Table 1. Requested Revisions to NCS000392 and Corresponding Triggering Events
Diversion of surface runoff from the
m Demonstration to NCDENR that the stormwater will not impact
two closed spray fields (West and
surface water
South of the solids disposal unit) to
Note: DAK has completed this triggering event and has demonstrated to
Outfall 004
NCDENR that the stormwater is not expected to impact surface water
quality. DAK is ready to implement this permit revision upon receipt of
the revised permit.
Diversion of stormwater from
Shutdown of industrial activity and removal of industrial materials
Monomers production area to Outfall
that were exposed to stormwater in the Monomers production area
002
o Complete cleaning of the industrial trench drains in the Monomers
area
Stormwater inspection conducted by NCDENR Wilmington Regional
Office personnel
2610 Wycliff Road, Suite 104, Raleigh, NC 27607 1 p 919-783-7777 1 f 919-783-0757 1 www.obg.com
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September 26, 2013
Page 2
O 2013 O'Brien & Gere. All Rights Reserved.
Diversion of stormwater from Fibers & ■ Shutdown of industrial activity and removal of industrial materials
Resins production area to Outfall 002 that were exposed to stormwater in the Fibers & Resins production
and/or Outfall 003 area
■ Complete cleaning of the industrial sewer in the Fibers and Resins
production area.
■ Most of this system is underground, and floor drains are under roofs,
however it is possible that de minimis quantities of stormwater could
enter the system (through infiltration or errant connections), and
produce an overflow at the lift station for this system, which would
runoff to Outfall 002.
a Stormwater inspection conducted by NCDENR Wilmington Regional
Office personnel
Diversion of stormwater from BACA ■ Shutdown of industrial activity and removal of industrial materials
pits to Outfall 002 that were exposed to stormwater in the BACA pits
■ Complete cleaning of the surfaces and trench drains in the BACA pits
Diversion of stormwater that falls on ■ Individual basin in Monomers WWTP or Fibers WWTP is removed
individual WWTP basins to Outfall 006 from service, emptied, and cleaned
Nate: Request that this revision be Note: This triggering event may be completed separately for each basin;
implemented far individual basins as therefore, it may be completed multiple times.
each basin is closed
DAK understands that, should this permit revision request be approved, NCDENR would revise the permit to
note that each revision is contingent upon DAK's completion of triggering events. The revised permit would
allow for DAK to notify NCDENR by email when a triggering event is completed, receive approval from NCDENR
to proceed with implementation of the revision, and then DAK would implement the permit revision.
DAK appreciates the Stormwater Permitting Program's consideration of this request and we look forward to
your review and approval. Should you have any questions regarding this request, please feel Free to contact me
at [phone] at your convenience.
Sincerely,
O'BRIEN & GERE ENGINEERS, INC.
A�o
Michael S. Hall, PG
Division Manager 2
DAK AMERICAS LLC
Penn ahoney
Director of Sustainability, Cape Fear Site
2610 wycliff Road, Suite 104, Raleigh, NC 27607 1 p 919-783-7777 1 f 919-783-0757 I www.obg.com
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September 6, 2013
Mr. Jim McKay
North Carolina Division of Water Resources\Water Quality Programs
NPDES Complex Permitting Unit
512 N. Salisbury St.
Raleigh, NC 27604
RE: DAK Americas LLC, Cape Fear Site (CF)
NPDES Permit No. NC0000663
NPDES Stormwater Permit No. NCS000392
Permit No. WQ0418067-Surface Disposal of Residual Solids
FILE: 14974\50406
Dear Mr. McKay:
The North Carolina Division of Water Resources (DWR) requested the estimated raw wastewater Flows and
loads DAK Americas LLC (DAK) expects to receive as influent to the on -site WWTP during decommissioning and
demolishing activities at their Cape Fear Site. DWR requested this information during meetings held on July 30
and August 16, 2013 in order to develop new NPDES wastewater and stormwater permits for the Cape Fear Site.
The objective of this letter is to provide information to facilitate renewal of DAK's NPDES permit and to provide
a description of the decommissioning tasks which must be completed in order to effect changes in wastewater
flows and loads. The changes in flows and loads associated with the completion of these tasks are provided.
In addition to flow and loading information, DWR requested that DAK perform acute toxicity testing on two
sources of wastewater to be treated at the on -site WWTP. The results of these tests are provided.
Once you have had a chance to review this information, i will call you to determine the next step needed in order
to adjust the permit for the upcoming changes.
I would be happy to answer any questions and you can reach me at 919-783-7777.
SincerelyWS.Hall,
NE R5, INC.
Division Manager 2
Attachments: Attachment A
DAK AMERICAS LLC
/Penny ahoney
Dire r of Sustainability
Cape Fear Site
Attachment B
Tables
cc: Tom Belnick, NPDES Complex Permitting Unit Supervisor
Ken Pickle, Stormwater Permitting Unit
2610 wycliff Road, Suite 104, Ralesgh, NC 27607 1 p 919.733-7777 1 f 9 t9-783-0757 I www.0bg.com
1W' End,naenmg Im! Prul«,;t u-1ro-r, �Uh,W)ns

Jim McKay
September 6, 2013 0 2013 O'Brien & Gere. All Ripts Reserved
Page 2
CAPE FEAR SHUTDOWN
DAK Americas requests revisions to its NPDES wastewater permit (NC0000663) and NPDES Stormwater permit
(NCS000392) as described in the 11 items below.
NPDES WASTEWATER PERMIT NO. NC0000663
1. The existing NPDES permit limits for Outfall 001 remain effective until the treatment of the wastewater
accumulated during the production shutdown and decontamination period has been completed and the
Monomers wastewater treatment plant (WWTP) has been shut clown and drained.
2. Reclassification of the facility from a Major Source to a Minor Source.
a. Attachment A shows DAK's evaluation of this determination.
3. New permit limits for Outfall 001 based on the effluent guidelines used in the development of the
existing permit and on the anticipated wastewater flows during the period when closure activities are
underway.
a. The three sources of wastewater during the period when closure activities are underway are:
i. leachate from the Surface Disposal Unit (SDU)
ii. stormwater that comes in contact with the terephthalic acid (TPA) in the Monomer's
WWTP North Polishing Pond and the Equalization Basin and
iii. stormwater from the trenches in the former manufacturing areas and stormwater that
falls on the footprint of the WWTP
b. See Table 1 for estimated wastewater flow and for proposed permit limits.
c. See Table 2 for an estimate of wastewater characteristics (BOD, TSS and COD) and Attachment B
for acute toxicity following shutdown of the Monomers WWTP but prior to treatment and
subsequent discharge at Outfall 001.
4. New effluent limits at Outfall 001 become effective when DWR receives notification that the following
decommissioning tasks have been completed.
a. The Monomers WWTP Emergency Basin, four aeration basins, two clarifiers and South Polishing
Pond are taken out of service and emptied. The Emergency Basin holds raw process
wastewater, the aeration basins are heavily loaded with mixed liquor, the clarifiers are heavily
loaded with activated sludge, and the South Polishing Pond holds process related wastewater.
These basins and tanks will be cleaned and drained as the load from the production areas
decrease.
b. TPA stored in the Monomers WWTP Equalization Basin and North Polishing Pond is drained to
remove standing liquid.
c. Loading at the Fibers WWTP drops to below normal production levels.
Shutdown of production at the Cape Fear Site will be complete by the end of September. This will be
followed by a period where tanks, lines, process vessels, and industrial sewers are purged and cleaned.
During the immediate post -shutdown period DAK expects the load to the WWTP to remain similar in
characteristic to wastewater produce during operation until the above three decommissioning tasks are
complete. DAK is uncertain of the exact completion date for these tasks because they are not routine
and unpredictable setbacks may arise both in the wastewater treatment plant operation and site closure
activities. It is anticipated that these activities will be completed in the first half of 2014.
S. A change in the classification of the WWTP from a Class IV system to a Class 11 system and the associated
reduction in testing frequency. See Table 3.
a. DAK requests this change because the Flow will be reduced from 2.3 million gallons per day to
0.5 million gallons per day and will therefore be reclassified as a Minor Source.
6. Elimination of Outfall 002 and Outfall 003 as wastewater outfalls and elimination of the sampling and
testing associated with these outfalls.
a. Outfall 002
2610 Wycllff Road, Suite 104, Raleigh, NC 27607 E p 919-783-7777 1 f 919-783-0757 1 www.obg.com
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Jim McKay
September 6, 2013 ® 2013 O'Brien & Gere. All Rights Reserved.
Page 3
i. Currently permitted for direct discharge of non -contact, once -through cooling water,
cooling tower and boiler blowdown, water treatment filter backwash, coal pile runoff
and stormwater.
ii. After production shutdown, non -contact, once -through cooling water, cooling tower and
boiler blowdown, and water treatment filter backwash will be eliminated.
iii. Coal pile runoff flows to a runoff basin prior to discharge through Outfall 002. It is
anticipated that the coal pile will be removed and the coal pile runoff basin closed by
December 2014. This stormwater has not been specifically characterized, but will not
differ pre- and post -shutdown. It is also a minor portion of the volume of stormwater
for Outfall 002 since the area of the coal pile and coal pile runoff basin represents only
2.3% of the total drainage area to Outfall 002.
b. Outfall 003
i. This outfall is currently permitted for direct discharge of non -contact once through
cooling water, cooling tower and boiler blowdown and stormwater runoff.
H. After production shutdown, cooling water, cooling tower and boiler blowdown will he
eliminated. It is anticipated that these sources of wastewater will be eliminated within a
few days of when manufacturing ceases.
iii. After shutdown, the only discharge from Outfall 003 will be stormwater from Drainage
Area 003.
c. For these two outfalls, DAK proposes to eliminate all NPDES Wastewater sampling and testing
and begin semiannual stormwater sampling when production shutdown and cleaning activities
have been completed.
7. Bypass of the Fibers WWTP when the wastewater characteristics have been reduced so that it meets the
newly calculated permit limits without treatment.
a. Upon completion of the shutdown of the manufacturing areas and the Monomers WWTP,
anticipated to be early 2014, wastewater will be treated in the Fibers WWTP.
b. The Fibers WWTP consists of a retention basin, an aeration basin, and two clarifiers with only
one clarifier normally in service. If necessary, chlorination will be provided to reduce the
potential presence of fecal coliform in discharge from the SDU. If necessary, dechlorination will
also be provided to meet the total residual chlorine effluent limit.
c. Flows are expected to decrease throughout the closure period as:
i. the SDU is closed
ii. the TPA is removed from the basins, and
iii. stormwater from other areas is diverted to stormwater outfalls upon completion of
decontamination.
d. As closure activities are completed, the wastewater flow will gradually decrease to very little.
DAK proposes that when the wastewater meets the new permit limits without treatment that
the Fibers WWTP be shutdown, cleaned, and demolished.
e. DAK Americas will notify DENR when measured untreated wastewater characteristics are
compliant with all permit limits for a period of six consecutive weeks. At that time DAK
proposes to bypass the Fibers WWTP and discharge any residual water without treatment.
8. Closure of the site's NPDES permit when wastewater discharges have been eliminated.
a. DAK Americas will notify DEN to request that the permit be rescinded when the discharges
have been eliminated for a period of six consecutive weeks.
NPDES STORMWATER PERMIT NO. NCS000392
1. Diversion of the stormwater from the production areas to a stormwater outfall
2610 Wydlff Road, Suite 104, Raleigh, NC 27607 1 p 919-783-7777 1 f 919-783-0757 1 www,obg.com
360' Engineering and Project Delivery Solutions Ph— I-Eng-s!u\Cnrrrt\Prrmd Mpd, IcytI Suppn« lrttrr`submatal VAK P,,mit 4"qu st docv

Jim McKay
September 6, 2013
Page 4
© 2013 O'Brien & Gere. All Rights Reserved.
a. Historically, stormwater from the manufacturing areas has accumulated in trenches and been
pumped to the WWTP. DAK proposes that this water continue to be treated in the WWTP until
all decontamination activities have been completed and then be allowed to discharge through.a
stormwater outfall. Stormwater from the Monomers Manufacturing area would be diverted to
Outfall 002 and from the Fibers and Resins Manufacturing area to either Outfall 002 or Outfall
003.
b. DAK Americas will notify DEN when the trenches have been decontaminated and the runoff
diverted to a stormwater outfall.
2. Diversion of the surface runoff from the two closed spray fields west and south of the SDU to Outfall 004,
a stormwater outfall. See characterization of the stormwater from these fields in Table 4. DAK would
like to divert this stormwater to the stormwater outfall as soon as possible.
3. Diversion of stormwater that falls on WWTP basins after they have been emptied and cleaned.
a. Currently the stormwater that falls on the WWTP basins is treated with the wastewater. As
basins are taken out of service during the closure period they will be emptied and cleaned. At
that point, for each basin, DAK proposes to divert the stormwater away front the WWTP to
percolate either to the groundwater or to be discharged at a stormwater outfall.
2610 Wycliff Road, Suite 104, Raleigh, NC 27607 1 p 919-783-7777 1 f 919-783-0757 1 www.obg.com
360° Engineering and Project Delivery 5olutions Mod,fiot—soPPoni.aw,\Sub ttaI\DnKP-9R"—t.d..

NPDES Permit Rating
Work Sheet
More than Engineering Solutions r--ry O BRIEN 6 GCRC

r r
NPDES Permit Rating Work Sheet o Regular Addltton
Cl Discretionary Addition
0 Scow change, but no
NF.DE5 No.: I_ NCO000663 _I_Irl_I status change
❑ Deletion
Facility Name:
I DAK Americas, LLC �t_1_I �I_1_L.�L . I _ 1 ^I_I�I_t_I_I�li►`I_i_ _I_I_I_h1_I�I_I
City: I- Leland, NC
Receiving water: 1. Cape Fear River
Reach Number. I_I_hI^I_I_I_i_I^1_I_i
is this facility a steam electric power plant (SIC=4911) Is this permit for a municipal separate storm sewer
with one or more of the following characterlstla7 serving a population greater than 100, 0007
1. Power output 500 MW or greater (not using a cooling pond/lake)
2. A nuclear power plant ❑ YES; score is 700 (stop here)
3. Cooling water discharge greater than 2596 of the receiving stream's 7Q10 Bow rate X NO (continue)
❑ YES; score is 600 (stop here) I X NO (continue)
FACTOR 1: Toxic Pollutant Potential
PCS SIC Code: 1_I_I_I�I
Primary SIC Code: I_ 2865.11
Other SIC Codes: 12824 _1_I
1_ 2821 _I__I I�I _ I_I_I
I�I_1
_I_I
Industrial Subcategory Code: 1001
1 (Code 000 If no subcategory)
Determine the Toxicity potential from Appendix A. Be sure to use the TOTAL
toxicity potential column and check one)
Toxicity Group Code Paints
Toxicity Group Code
Points
Toxicity Group
Code
Points
❑ No process
❑ 3_ 3
15
❑ 7_
7
35
waste streams 0 0
❑ 4. 4
20
❑ 8.
8
40
Cl 1. 1 5
Cl 5. 5
25
X 9.
9
45
❑ 2. 2 10
❑ 6. 6
30
❑ 10.
10
So
Code Number Checked: 1_19 i
Total Points Fador 1: 145 1
FACTOR 2: Flow/Stream Flow Volume (Cortploto 911hor5oction A or Sochon 5; chock only ono)
Section A —Wastewater Flow Only Considered
Wastewater type
Code
Points
(See instructions)
Type I: Flow < 5 MGD
❑
11
0
Flow 5to10MGD
❑
12
10
Flow >10 to 50 MGD
❑
13
20
Flow > 50 MGC)
❑
14
30
Type If. Flow <1 MGD
21
10
Flaw 1 to 5 MGD
❑
22
20
Flow >5 to 10 MGD
❑
23
30
Flaw >10 MGD
❑
24
50
Type ill: Flow <1 MGD
❑
31
0
Flow 1 to 5 MGD
❑
32
10
Flow >5 to 10 MGD
❑
33
20
Flow>10 MGD
❑
34
30
Section B Wastewater and Stream Flow Considered
Wastewater Type
Percent of In; trea m
Code
Points
(See Instructions)
Wastewater Concen.
tratlon at Receiving
Stream Low Flow
TYPE I11II:
< 109b
❑
41
0
2 10%to <50%
❑
42
10
2 50%
❑
43
20
Type II:
< 1 D%
X
51
0
2 10% to <50%
❑
52
20
� 50%
❑
53
30
Code Checked from Section A or 8: 1 51 1
Total Points Factor 2: 1 1 0 1

t r
NPOFS Permit Rating Work Sheet
FACTOR 3: Conventiond Pollutants NPDES No.: I, NCO000663
(only whop A mttt;ad by VL)Q pormil)
A C,x�,gv. C,r-ianding Pollutan<• Ler.:: one) XI 800 ❑ COD ❑ Other:
Code
Points
i•ennit U-ni4: (cog-1 °tie,, i 1
<100 lbs/day
1
0
X
'00 to 10001bs/day
2
5
❑
�1000 to 1000 lbs/day
3
15
0
>3000lbs/day
4
20
Code
points
Permit !.1m1,.s: 'r s�:I' ;K
e100 Ibs/day
1
4
X
f CO 10 1000 Ibs/day
2
5
U
-1Ono to 5000 Ibs/day
3
15
Q
'>5000lbs/day
4
20
C. Ftit=r-qen Pol!L-, - f17N,- I' ., ❑ Ammonia i X Other... TKN
Nitmgen Equimlenr
Permit Urr , ti_seok one; n -300 ibs/day
X 100 to 1000 Ibs/day
U 0 000 to 30001bs/day
s7 >3000 f5s/day
Cade AoWs
1 0
2 5
3 15
4 20
Code Checked: 12 1
Pants Scored: I 05 1
Code Checked: 12 1
Points Scored. l 05 1
Code Checked: 1 21
Points Scored: 1 05 1
Total points Factor 3:1— 15 1
'A(-7CP 4: PuNic Heattl7 Impolct
I. fire, e u pAtIr r�rinl;rty'water supply lac -)fed within SO miles downstream of the effluent d/scharge (this Includes any body of
•;;tier to wh;rb the receiving water Is a frihutary)T d public drinking water supply may Include Infiltration gallerler, or other
,elhods v-oineyance Ihat ultimately get tvater from the abaw referenced supply.
; yes, cheer, toxi.;...'otential number below)
X .) I;` no, 4c to Factor : ,
-7etermine :-.he human heahh toxicity patendal from Appendix A. Use the same SIC code and subcategory reference as in Factor 1. (Be
trrr• tc ;)sr: L!ie hUnla,tl h.�ztilh toxicity group column •• • .heck one below)
;'r• Jrft/ ,v�up
Cafe Points
'roxlcity Group
Code
Points
Toxicity Group Code
Points
t� -*-
Cl 3.
3
0
❑ 7. 7
15
�z. -2sir.!am:
0 0
(] 4.
4
0
Cl 8. 8
20
❑
a
❑ S.
5
5
Cl 9. 9
25
u 2.
2 0
i
b
10
❑ 10. 10
30
Code Number Checked: 11
1
Total Points Factor 4: 1
1 0 1
2

NPDES Permit Rating Work Sheet
FACTOR 5: Wator Quality factors NPDES No.: I_ Nca000663
A. is (or will) one or more of the effluent discharge limits based on water quallty factors of the receiving stream (rather than
technology -based federal effluent guidelines, or technology -based state effluent guidelines), or has a wasteload allocation
been assigned to the discharge?
Code Points
X Yes 1 10
❑ No 2 0
R. is the rrcelving water In compliance with appilcabk water quality standards for pollutants that are water quality limited in
the permit?
Code Points
❑ Yes 1 0
X No 2 5
C. Does the effluent discharged from this facility exhibit the reasonabk potential to violate water qualitystandards due to whole
effluent toxicity?
Code Points
❑ Yes 1 10
X No 2 0
Code Number Checked: Al 1 1 e i 21 C 1 2 1
Points Factor S: All 10 _t + B I, 5 1 + c 1 a j 1_ 15 I roTAL
FACTOR 6: Proximity to New Coastd Waters
A. Base Score: Enter flow code here (from Factor 2): 1, 51 _I Enter the muldpllcation factor that corresponds
to the flow code: 11 1
Check appropriate facility HPRI Code (From PCS):
HPRI a
Code
HPRI Score
Row Code
Multlprrcatlon Factor
0 1
1
20
11,31,or41
0.00
❑ 2
2
0
12, 32, or 42
0.05
13, 33, or 43
0.10
X 3
3
30
14 or 34
0.15
❑ 4
4
0
21 51
0.10
22 or
0.30
❑ 5
5
20
23 or 53
0.60
HPRI code checked: { 3.1
24
1.00
Base Score: (HPRI Score) _
30
, x (motipiication Factor) _ 0.1 0 _
— 3.0 _
(TOTAL POINTS)
B. Additional Points — NEP Program
For a facility that has an HPRI code of 3, does the facility
discharge to one of the estuaries enrolkd in the National
Estuary Pro tectfan (NEP) program (see Instructions) or
the Chesapeake Bay?
Code Points
❑ Yes 1 10
X No 2 0
C. Additional Points —Great Lckes Area of Concern
For a facility that has an HPRI code of S, does the facility
discharge any of the pollutants of concern into one of the
Great takes' 31 areas of concern (see instructions)
Code Number Checked: A 131 B 12 1 C 12 1
Points Factor 6: A 1--1, 31 + B i_l. 0.1 + C i_I. 0 1
Code Points
O Yes 1 1.0
X No 2 0
1 3.0 1TOTAL
3

NPDES Permit Rating Work Sheet
SCORE SUMMARY
NPDES No.: I NCO000663
Factor
Description
Total Points
1
Toxic Pollutant Potential
—45 _
0
2
Flow/Streamflow Volume
_ _
15
3
Conventional Pollutants
4
Public Health Impacts
__ 0 _
5
Water Quality Factors
_ 15
6
Proximity to Near Coastal Waters
3 _
78
TOTAL (Factors 1 through 6)
Si. Is the total score equal to or greater than 807 ❑ Yes (Facility is a major) X No
$2. 1f the answer to the above question is no, would you like this facility to be discretionary major?
X1 No
❑ Yes (Add 500 pants to the above score and provide reason below:
R ea son:
NEW SCORE:
OLD SCORE:
Permit Reviewer's Name
Phone Number
Date
4

Acute Toxicity Testing
Results
Test Procedure for Discharge
from the SDU
• Laboratory Report for
Discharge from the SDU
• Test Procedure for
Stormwater from Basins in
which TPA had Accumulated
Laboratory Report for
Stormwater Basins in which
TPA has Accumulated
More than Engineering Salutior�s
CrBRIEN 6 GERE

TEST PROCEDURE FOR DISCHARGE FROM THE SDU
Acute Toxicity testing was performed in accordance to section A. (7) of the current NPDES permit NC0000663.
The grab sample was collected directly from the sump at the discharge of the SDU.
350' Engineering and Project Delivery Solutions C0 (YORIEN 6 IGERE

Effluent Aquatic Toxicity Report Form - Acute Pass/Fail Date � `q - l 3
!a.}IEre- r�
Facility — L r NPDES# NC00 Pipe# County ,[firV"5w iok;
Laboratory Performing Test__ bYeritech, Inc. Comments
x
Signature of Operator in Responsible Charge �� L+ d./y,
Signature of Laboratory Sup
a dim „ , __ _ -W-_„-U Environmental Services
Toxicity Testing Laboratory Report for Discharge from the SDU
North Carolina Acute Pass/Fail Toxicity Test
Collection Date: -7' / 3
Collection Time: q 30�
Test Start Date: g' / 3
Sample_Type/Duration
Grab
Comp.
Duration
Y . i.
Aail RR
h, NC 2
Organism Tested
Pimephales promelas
r
V
PH Control 7611
Treatment
m
v �
� Q
D Control 7, `7 EL03
Treatment
Mortali Replicate Mean Mortality
Treatment 1 (Control) A B C D
1 6 0101 D 0/01 0 0101
Treatment 2 (exposure) A B C D
Concentration no% �0 %
FeStedCJD
(NOTE: If mean control mortality exceeds 10%, the test is considered invalid)
Calculate using Calculated Student's t PASS
Arc -Sine Square Root
Transformed data Tabular Student's t 3 �� FAIL
(ONE TAILED)
If the absolute value of the calculated t is less than or equal
to the absolute value of the tabular t, check PASS.
If the absolute value of the calculated t is greater than the
If the absolute value of the tabular t, check FAIL.
If all vessels within each treatment have the same response
but the treatment two response is greater than the control, check FAIL,
PH Control 7611
Treatment
m
v �
� Q
D Control 7, `7 EL03
Treatment
Mortali Replicate Mean Mortality
Treatment 1 (Control) A B C D
1 6 0101 D 0/01 0 0101
Treatment 2 (exposure) A B C D
Concentration no% �0 %
FeStedCJD
(NOTE: If mean control mortality exceeds 10%, the test is considered invalid)
Calculate using Calculated Student's t PASS
Arc -Sine Square Root
Transformed data Tabular Student's t 3 �� FAIL
(ONE TAILED)
If the absolute value of the calculated t is less than or equal
to the absolute value of the tabular t, check PASS.
If the absolute value of the calculated t is greater than the
If the absolute value of the tabular t, check FAIL.
If all vessels within each treatment have the same response
but the treatment two response is greater than the control, check FAIL,

Client: L4 i1 :i?,
NPDES#:NC !- I `L
s
Test Initiated by: V)l
Dilution Water: 10% Dilute Mineral Water Batch #
Randomization?:}Yes
Incubator#:
t.
Meritech. Inc.
Data Sheet for 24 Hour Acute PIF
Fathead Minnow
No. of Organisms per Chamber: 10
Test Vessel Size: 250 ml
Test Solution Volume: 200ml
No. of Replicates per Treatment-. 4
Temp. of Stock: - to 1 °C
Reference run on:
Start: Date:
End: Date: / _'3 Time:
[ J-
Test Organism: Pimephales promeias Age: days
Organism Source: Aquatox, Inc.
O �
Born: Date: - -�°3 Time:
Test Terminated by: /t,V—'
Reviewed by:
Number Exposed
Mortality after 24 Hrs.
Dissolved
Temperature
Conduc-
Residua!
Total
Hardness
Concen-
Total
No
pH
Oxygen (mg/L)
(°C)
tivity
(umhos/cm)
Chlorine
(mg/L)
(mg1L of
tration
Rep
Rep
Rep
Rep
Rep
Rep
Rep
Rep
Dead
CaCO3)
A
B
C
D
A
B
C
D
0
24
0
24
0
24
0
0
0
Control
10
10
10
10
%. f�!
%, QLj
7. (�(7
7p3
n
90%
10
10
10
10
/ C
t' ��
/ rr�
Ci
�L�
�. 7
S �
�,,�(`�
��U)
(-- . v
��z li
�7 ��}
U . j
pHrof100%
Conductivity of 100%,
(umhos/cm)
Residual Chlorine of
100%/ (mg1L)
! C�
Date and time fed prior to test initiation: ' • .�OND Fed by:
ee-r" v o-
�Lt�,i� C�

RHEA u ECHI INC. r0ehta�hSample IDr:
Sioassay Sanwle Chan oFCustodL,
642 Tamco Rd, Reidsville NC 27320
Phony: 1-336-342-4748 Fax: [phone]
Toni city Supe rvisor email: Web Site: wvrm.merltech-labs.com
CLIENT MFORMATION
Client: _ 4 [_ - � S - — PO#: 2A l ! `7-5 s
Contact Person: Z z f9—' Al) e �n c4A—j <' _ NPDES#: NC �V
Address: �Q 4�. , �_� Phone: �Z/d �26q_ ".2SZnV1
City: ti3 /1) Pipe #:: /-'2—_/`f <!'� Ll--- a�
County: ��.JSL.c.II � State: c Zip:
cry
n SAMPLE R1=ORWA7I011,I
Sample 5tt2: /���
Sample Type: L�Grab ❑ Composite # of containers:
Sampling Time: Start Date: 817 1 Start Time: D-5 AM PM
End Date: End Time: AM PM
S.t.WPLE CONTAINERS FeUST BE COfJPLETELY FULL (no sir spike), CHILLED AND OVERED VVi�TH tCE *— A
Collector's Name. Print: / ��L t r /�� �(JG�A�(� Signatu�� � %��-✓t
Test Required: �❑lCCh�ric (7 days)
!acute (24-48 hours)
1w. C: %
Comment-:
TOXICITY TEST WFORIl ATION
Test Organism: Ceriodephnia dubia (water f€ea)
2r"Plimephafes prorrrelas (fathead minnow)
❑ Vysidopsis bahia (shrimp)
Test Concentrations (if multiple dilutions):
SlHiPPING INFORMATION
Relinquished b� �', Date:
Received by: Bate:
Relinquished by:
Received by:
Relinquished by:
Received by:
Relinquished by:
Received by:
Date:
Date:
Date:
Date:
Date:
Date:
Time:C7 AM PM
Time: AM PM
Time:
TFme.
Time:
Time:
Time:
Time:
Sample Temperature (°C):
Method of Shipment: ❑LIPS 2rred EX ❑ Nieritech Pick-up [] Delivered [] Other
AM PM
AM PM
AM PM
AM PM
AM PM
AM PM
Samples shipped on Friday must be Fed Ex and must be clearly labeled for 5aturdey delivery, NO SIGNATURE REQUIRED —
SAMPLE RECEii ING (Labaratonf Use Onh!
r
Relinquished by:1
Received by: ! Date: ` �� Time: �• i `AM PM
Sample Temperatures (°C Sample '
WHITE = Labor4tor�� copy YELLMY = Client copy

CLIENT: DAK -12 Acre Lagoon
CONTROL
TRANS
VALUE
Rep 1
1.412
Rep 2
1.412
Rep 3
1.412
Rep 4
1.412
MEAN= 1.412
Std. Dev.= 0
Std. Dev.^2= 0
sp= 0.00000
90%
TRANS
VALUE
Rep 1
0
Rep 2
0
Rep 3
0
Rep 4
0
MEAN= 0.0000
Std. Dev.= 0.00000
Std. Dev.12= 0,00000
*** Tabular Student's t = 3.14
Calculated
Student's t: #DIV/O!
Result: #DIV/0!
NPDES: NC00 NIA
MORTALITY
TRANS
VALUE
0
1.412
1
1.249
2
1.1071
3
0.9912
4
0.8861
5
0.7854
6
0.6847
7
0.5796
8
0.4636
9
0.3218
10
0
Printed: 819120 13

IN
TEST PROCEDURE FOR STORMWATER FROM BASINS IN WHICH TPA HAS ACCUMULATED
Acute Toxicity testing was performed in accordance with section A. (7) of the current NPDES permit
NC0000663. The tested sample was derived from a benchtop study designed to model the procedure for forced
flushing the TPA and the conditions by which stormwater will contact TPA and accumulate in the TPA holding
basins. The benchtop study consisted of the steps listed below.
1. A sample of TPA was collected from the Monomers WWTP North Polishing Pond.
2. The sample was washed twice by spraying deionized water over the TPA in a bucket fitted with holes in
the bottom and lined with heavy duty filter cloth. Spraying the water over the TPA simulated how
forced flushing and rain may displace the wastewater surrounding the TPA grains. Each wash used a
volume of deionized water equal to 100% theoretical displacement of the pore space in the sample of
TPA.
3. The rinsate from the first two washings was discarded.
4. A third quantity of deionized water equal to 100% theoretical displacement was sprayed over the TPA
and collected for acute toxicity testing. The third rinse represents stormwater that will comingle with
the TPA and be sent to the Fibers WWTP for treatment.
360' Engineering and Project Delivery Solutions (� GGBRIEN 6 GERE

Effluent Aquatic Toxicity Report Form - Acute Pass/Fail Date � - �? - / 3
Grab
Comp.
Duration
Facility✓A K — I v P NPDES# NC00Itf/4._ Pipe# lVf', County frw1�
Laboratory Performing Test Meritech. Inc:_
x
Signature of Operator in Responsible Charge
x,;�� _
Signature of Laboratory Supervisor
omments
1 FIRM,��
Acute Toxicity Testing Laboratory Report for Stormwater from Basins in which TPA has
Accumulated I
North Carolina Acute Pass/Fail Toxicily Test
Collection Date: R %- 1 3
Collection Time:
Test Start Date:
Sample Type/Duration
o
— x
0
Hardness (mg/1)
I
Spec. Cond. (pmhos)
Chlorine (mg/1)
Sample temp, at receipt (°C)
Mortality
Treatment 1 (Control)
"i
h, NC 27699-162
Organism Tested
Pimephales promelas
pH Control 7, 1i 11
Treatment
rn m
CL
D.O. Control
Treatment
A B C D
Treatment 2 (exposure) A B C D
Concentration
Tested ° a �? 01a / Q 0 ��) v�
(NOTE: It mean control mortality exceeds 10%, the test is considered invalid)
7 �� 7�3
S, �J /r
Calculate using Calculated Student's t PASS L�
Arc -Sine Square Root
Transformed data Tabular Student's t FAIL
(ONE TAILED)
If the absolute Value of the Calculated t is less than or equal
to the absolute value of the tabular t, check PASS.
If the absolute value of the calculated t is greater than the
If the absolute value of the tabular t, check FAIL.
If all vessels within each treatment have the same response
but the treatment two response is greater than the control, check FAIL.
Calculate using Calculated Student's t PASS L�
Arc -Sine Square Root
Transformed data Tabular Student's t FAIL
(ONE TAILED)
If the absolute Value of the Calculated t is less than or equal
to the absolute value of the tabular t, check PASS.
If the absolute value of the calculated t is greater than the
If the absolute value of the tabular t, check FAIL.
If all vessels within each treatment have the same response
but the treatment two response is greater than the control, check FAIL.

ti-
Client: I
NPDES #:NC A) /A- Pb P 601�
Test Initiated by:
Dilution Water: 10% Dilute Mineral Water, Batch 4
Randomization?: Yes
Incubator#: Lf
Meritech. Inc.
Data Sheet for 24 Hour Acute PIF
Fathead Minnow
No. of Organisms per Chamber: 10
Test Vessel Size: 250 ml
Test Solution Volume: 200ml
No. of Replicates per Treatment: 4
Temp. of Stock: ,_q_ i °C
Reference run on: I —Al-, I
',. i�
Start: Date-1-0 { n Time: )Lilcv-
End: Date: ; t�' / ' % �� Time:
Test Organism: Pimephates promelas Age: a days
Organism Source: Aquatox, Inc._
Barn: Date: 7' "?� t Time
Test Terminated by: �h
Reviewed by:
Number Exposed
Mortality after 24 Hrs.
Dissolved
Temperature
Conduc-
Residual
Total
Hardness
Concen-
Total
No
pH
Oxygen (mg/L)
CC)
tivity
(umhos/cm)
Chline
(mgor/L)
(mg/L of
tration
Rep
Rep
Rep
Rep
Rep
Rep
Rep
Rep
Dead
CaCO,)
A
B
C
D
A
B
C
D
0
24
0
24
0
24
0
0
0
Control
10
10
10
10
0�
0�-,q
r
7,Q
7 {c.�}
03
90%
10
10
10
10
pH of 100%
Conductivity of 100%,
(umhos/cm)
Residual Chlorine of
100% (mg/L)
31
Date and time fed prior to test initiation: Fed by:
�I 1� j�i ` • r `'
Te5� � L7.rir'.�t'•��TC17%��!'✓1 Ui�111�
r f Irr� l ' j j �� i 1 a �'1 . �+"- �.�r -11•tiZ b u:.1� — C l!%� h� c'_ �j� `} e 1'_
11,ov� ,— X

M ER b ECH, INC. Meritech Sample ID
Woassor Sampee Chain of Cusfod
642 Tamco Pd, Reidsville NC 27320
Phone: [phone] Fax:[phone]
Toxicity Supervisorerriaii: Web Site: unnnv.merifech-iabs.com
(�}� CLIENT INFORMATION
Client: DA K - / / i1E— `�..__. PC#: 4 ��
Contact Person: ! r ,�. [ � 2 (r( /L2 C:; NPDES#: NC •v
Address: 4 . _ _� Z 6, s') Phone: ?/A-2 — �pz(a
City: 0 L_ /L.1 F�-- - - Pipe #: / /0)
County: �1,L1.2-1b( C,G'� State: L_ Zip: sS 05z=�
SAMPLE INFORHATION
Sample $Ko:
Sample Type: ICJ Grab ❑ Composite # of containers:_
Sampling Time: Start Date: 9/ / Stara Time: AM PM
End Date: End Time: AM PM
SAWIFLE CONTAIMERS 1,6USTT BE COWPL_E/TELY FULL (no air space), CHILLED h' ,OVERED 40i H ICE '•`
Collector's tame: Print: /c iK C./ �t1 r �I%C��[r, Signatur-. % U��,
TOXICITY TEST INFORMATION
Test Required:❑,,
Comments:
Chromic (7 days)
LGf�ce,te (24-48 `lours)
ENVCe: %
Test Organism: [] Cerfodaphnia dubia (water flea)
[;;4imephaias, promelas (fathead minnow)
Mysidopsls bahia (shrimp)
Test Concentvaiions (if multiple dilutions):
SHIPPING WFORMATION
Relinquished by:
L , �'`1
Date: f!
Time: �'� AM PM
Received by:
Date:
Time: Ali PM
Relinquished by:
Date:
Time: AM PM
Received by:
Date:
Time: AM PM
Relinquished by:
Date:
Time: AM PM
Received by:
Date:
Time: AM PM
Relinquished by:
Date:
Time: AM PM
Received by:
Date:
Time: AM PM
i r
b
Sample Temperature (°C):
V
Method of Shipment: �apS
red EX � Meritech Pick-up � Delivered
❑ Other
" Samples shipped
on Friday must be Fed -Ex and must be clearly labeled for Saturday delivery, NO
SIGNATURE REQUIRED "
SAMPLE RECEIVING (Laboratory Use OM
Relinquished by: ��C-� C -14: f )
received by/� / Date: �' � � i Time:
Sample Temperatures (°l) / ! 1 Sample Condition: r C
WKTE = Laboratory Copy YELLOkY = Client copy - � TM

CLIENT: DAK - NPP
CONTROL
TRANS
VALUE
Rep 1
1.412
Rep 2
1.412
Rep 3
1.412
Rep 4
1.412
MEAN= 1.412
Std. Dev.= 0
Std. Dev.^2= 0
sp= 0.00000
90%
TRANS
VALUE
Rep 1
0
Rep 2
0
Rep 3
0
Rep 4
0
MEAN= 0.0000
Std. Dev.= 0.00000
Std. Dev.12= 0.00000
*** Tabular Student's t = 3.14
Calculated
Student's t: #DIVIO!
Results #D IV/O r
NPDES: NC00 NIA
MORTALITY
TRANS
VALUE
0
1.412
1
1.249
2
1.1071
3
0.9912
4
0.8861
5
0.7854
6
0.6847
7
0.5796
8
0.4636
9
0.3218
10
0
Printed: 8/9/2013

,I r
Tables
More Ulan Engineering Solutions
o O'BRICW 6 GCRC

Table 1 Estimated Wastewater Flow and Proposed Permit Limits for Outfall 001
Flow 0.5 MGD
BOD, 5-day, 20°C 103.4 Ibs/day 273.3 Ibs/day
Total Suspended Solids (TSS) 167.1 Ibs/day 536.7 Ibs/day
pH Not more than 9.0 S.U. nor less than 6.0 S.U.
Total Residual Chlorine (TRC) 28 µg/I
Dissolved Oxygen (DO) Not less than 5.0 mg/l, daily average
DAK requests that the testing requirement for OCPSF chemicals be
OCPSF Chemicals waived based on a demonstration made previously by DAK in accordance
with 40 CFR 122.44(afi21(i)

Table 2 Estimated Raw Wastewater Flow and load to WWTP
Flow
BOD, 5-day
Total Suspended Solids (TSS)
0.5 MGD
4.15 MGD
220 Ibs/day 267 Ibs/day
166 Ibs/day 780 Ibs/day
COD 570 Ibs/day 2034 Ibs/day

. . k
Table 3 Proposed Measurement Frequency at Outfall 001
Flow Continuous
BOD, 5-day, 20°C Weekly
Total Suspended Solids (TSS) Weekly
pH 3/Week
Temperature, °C 3/Week
Conductivity, umhos/cm
3/Week
Total Residual Chlorine (TRC)
Weekly
Dissolved Oxygen (DO)
2/Month
Fecal Coliform
Monthly
(geometric mean)
Total Nitrogen, mg/I
Quarterly
TN = (NO7-N+NO3-N) + TKN
Nitrite/Nitrate Nitrogen, mg/l
Quarterly
(N OZ-N+N 03-N )
Total Kjeldahl Nitrogen, mg/I
Quarterly
(TKN)
Total Phosphorus, mg/I (TP)
Quarterly
Ammonia as Nitrogen, mg/I
Quarterly
(NH3 as N)
Total Copper, pg/I
Quarterly
Acute Toxicity Annually
DAK requests that the testing
requirement for OCPSF chemicals be
OCPSF Chemicals waived based on a demonstration
made previously by DAK in accordance
with 40 CFR 122.44(a)(2)(i)

. . t
Table 4 Characterization of Stormwater from the Two Closed Spray Fields
6/24/2013 8.8 4 72 1.30 1.3 0.54
7/15/2013 15.0 4 37 2.50 2.6 0.47
8/12/2013 7.8
8/19/2013 8.2
pH was not measured during these initial sampling events, therefore, pH was measured on subsequent dates

S',+e- S -'a- { t ,� 1119120t3
June 7, 2013
Mr. Tom Tharrington
Wastewater- Consultant
NCDENR DWQ - Wilmington Regional Office
127 Cardinal Drive Extension
Wilmington, NC 28405
cCCJ(_were� e,,,,drfion' Fl(111{ A�PrA�rOn�l
L
([ C[ C1Crno`1 + +fin � Gt�ClSro� f-'��t.le� M1�CrE
RE: NCS000392 and NCO00663 - Request for revision to required monitoring for Outfali 002 and
Outfall 003
FILE:14974\50406
Dear Mr. Tharrington:
DAK Americas LLC (DAK Americas), and O'Brien & Gere are submitting this request to revise the required
discharge monitoring stipulated in NPDES wastewater (NC000663) and stormwater (NCS000392) permits to
reflect changing conditions at the DAK Americas Cape Fear Facility in Leland, NC. As described during our
meeting with you on April 15, and in our May 1, 2013 letter to Mr. Ted Bush of the Division of Water Quality
(DWQ), DAK Americas is considering the potential shutdown, decontamination, and demolition of the DAK
Americas Cape Fear Facility. Although DAK Americas has not made the final decision to shut down, this request
is being made in anticipation of the potential for this eventuality.
Based on our meetings with the directors of the DWQ Division of Air Quality (DAQ) and Division of Waste
Management (DWM) on April 15, 2013 and April 30, 2013, we understand that since the permitted processes
will no longer be active, the new requirements during this period maybe implemented through submittal, and
subsequent NCDENR approval, of a written description of the proposed revision.
EXISTING MONITORING REQUIREMENTS FOR OUTFALLS 002 AND 003
Discharges from Outfalls 002 and 003 are covered by both the NPDES wastewater (NC000663) and stormwater
(NCS000392) permits. Authorized discharges include process -related sources and stormwater runoff. Figure 1
identifies the stormwater drainage area for Outfalls 002 and 003. The existing monitoring requirements for
these outfalls are summarized below, for reference.
NPDES PERMIT NCO000663 - OUTFALLS 002 AND 003
The NPDES wastewater permit (NC0000663) provides coverage for discharge of process-reiated wastewater
sources and stormwater, as summarized in Table 1. Weekly and monthly monitoring is required at these outfalls
because of the process -related flow.
Table 1, Existing NCO000663 Monitoring Requirements for outfalls 002 and 003
002 Non -contact once through cooling water
Cooling tower blowdown
Boiler blowdown
Water treatment filter backwash
Coal pile runoff
Stormwater runoff
003 Norr-contact once through cooling water
Coiling tower blowdown
Boner blowdown
Stcrmwater runoff
2610 Wycljff Road, Suite 104, Raleigh, NC 27607 1 ,; 919-783-7777 1 f 919-783.0757 1 www.obg.com
360" Engineering and Project Delivery Solutions IADA.Am! icas.14974,50406.Phase-i-Eng-Stu\Corfes1Permit Revision Request\Request for permit revision 6.7-2013.doc

Mr, Tom Tharrington
June 7, 2013 02013 O'Brien & Gere. Ali Rights Reserved.
Page 2
NPDES PERMIT NCS000392 — OUTFALLS 002 AND 003
NPDES Permit NCS000392 provides coverage for discharge of stormwater. Semi-annual monitoring is required
at Outfalls 002 and 003.
REQUESTED REVISIONS
Discharge of wastewater from process -related sources at Outfalls 002 and 003 will cease should the
manufacturing process shut down and discharge from the outfail would become intermittent (i.e., related to
stormwater events). The discharge areas for Outfalls 002 and 003 include developed area of the Cape Fear
Facility and monitoring of the stormwater discharges for these outfalls will be appropriate until a demonstration
of no -exposure to industrial activities can be made. Table 2 summarizes the discharges that would cease should
( b) production shutdown and those that would cease at some point during a facility decontamination and
Cc ) demolition process.
Water treatment filter backwash
003 Non -contact once through cooling water Stormwater runoff from areas exposed to
Cooling tower blowdown industrial activity
Boiler blowdown
Based on this understanding, DAK Americas requests approval to revise monitoring requirements to reflect
changing discharge conditions should they decide to shutdown manufacturing operations and corresponding
cessation of non-stormwater discharges at Outfalls 002 and 003. Under this event, the proposed monitoring
modifications requested are as listed below:
13 DAK Americans requests that once all non -storm water discharges cease from Outfalls 002 and 003 that
monitoring and reporting at Outfalls 002 and 003 under NPDES wastewater permit NCO000663 be
discontinued.
DAK Americas requests that semi-annual monitoring and reporting at Outfalls 002 and 003 under NPDES
Stormwater Permit NCS000392 be implemented once monitoring and reporting under NC0000663 has
ceased. Table 3 lists the requested monitoring parameters and monitoring frequency. The parameters listed
in Table 3 are consistent with the monitoring currently required for Outfalls 002 and 003 under NC0000663.
The intent of this request is to reduce the monitoring frequency to semi-annual, consistent with typical
stormwater monitoring requirements. Note that the list of analytical parameters currently required to be
monitored are proposed to be maintained.
Table 3. Requested Monitoring Parameters and Frequency for NCS000392
TSS (mg/L) Grab sample collected semi-anrivally Grab sample collected semi-annually
BOD (mg/L) Grab sample collected semi-annually Grab sample collected semi-annually
COD (mg/L) Grab sample collected semi-annually Grab sample collected semi-annually
TKN (mg/L) Grab sample collected semi-annually Grab sample collected semi-annually
TN Jmg/L) Grab sample collected semi-annually ^ Grab sample collected semi-annually
2610 Wycliff Road, Suite 104, Raleigh, NC 27607 1 p 919-783-7777 1 f 919-783-0757 1 www.obg.com
360' Engineering and Project Delivery Solutions I:\Dak•Americas.14974\50406.Phase-I-Fng-Stu\Corres\Permlt Revision Request\Request for permit revision 6-7-2013.doc

Mr. Tom Tharrington
June 7, 2013
Page 3
TP (mg/L) Grab sample collected semi-annually
Cobalt (mg/L) Grab sample collected semi-annually
1,4-Dioxane (mg/L) Grab sample collected semi-annually
O 2013 O'Brien & Gere. All Rights Reserved.
Grab sample collected semi-annually
None ,.
Grab sample collected semi-annually
pH ISM.) Grab sample collected semi-annually Grab sample collected semi-annually
For further clarity, Attachment 1 provides markups detailing the proposed deviations from monitoring
requirements, as described on pages from the existing NPDES wastewater (NC0000663) permit and Attachment
2 shows the associated changes to the stormwater (NCS000392) permit.
Currently, the timing for DAK Americas to decide on an operational change for the Cape Fear Facility is
unknown. Should DAK Americas decide to pursue a facility shutdown, DWQ will be notified of this decision and
of the anticipated facility shutdown date.
DAK Americas appreciates the DWQ's consideration of this request and we look forward to your review and
approval. Should you have any questions regarding this request, please feel free to contact me at (919) 783-
7777, extension 26, at your convenience.
Sincerely,
OBRIEN & GERE ENGINEERS, INC.
)�4aA I ige
Michael S. Hail, PG
Scientist III
DAK AMERICAS LLC
Penny rhoney
Direct ofSustainability
Cape Fear Site
Attachments: Figure 1-- Outfall 002 and Outfall 003 Drainage Areas .
Attachment 1 - Proposed Revisions to NPDES NC0000663
Attachment 2 - Proposed Revision to Stormwater Permit NCS000392
cc: Gary McCullen, O'Brien & Gere
Jim Gregson, DWQ Wilmington Regional Office, Surface Water Protection Supervisor
Charles Wakild, DWQ Director
jrn oin lac -,/if s�iu_c>/o� s �ndf7a2Ci11r;7 4dS CeV)S,-r, .r0C&�'p/5 a74 rde�) M13 ee 1
�a re Ce 9 S&d /"0/7 Ye 117/0 o { ialS is d��/etr w �✓
/oHxs c�2S�J �t����°fi� o'��/'d.ra✓tIG,�, �idJ C�BS�d' /ir ,-dr`[�cr f`o ��r��i� eJl1�n mGnr�brlti�y
2610 Wycliff Road, Suite 104, Raleigh, NC 27607 1 p 919-783-7777 1 f 919-783-0757 1 www.obg.com
360' Engineering and Project Delivery volutions 1;1Uak-Americas,14914\50406.Phase•I-Eng-Stu\[orres\Permit Revision Request\Request for permit revision 6.7-2013.doc

FIGURE 'I
H
LEGEND
Q Outfall
® Drainage Areas
DAK AMERICAS LLC
CAPE FEAR FACILITY
OUTFALL 002
AND
OUTFALL 003
DRAINAGE AREA
0 250 sw 1,D00
Feet
aO'ORIEN G GERE =e'

Attachment 1
Proposed Revisions to
NPDES NC0000663
9 UBRIEN 6 GERE

Permit NC000066 ..
A. (5) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS-OUTFA 002
Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized
to discharge non -contact once through cooling water,. cooling tower and boiler blowdown, water
treatment filter backwash, coal pile runoff and stormwater runoff through outfall 002. Such
rlierhnrriac chair hn 33mifnel nnrl mnniFnrnrl her fhn Dnrm;+eo ennr43o 41 holnw•
.......,' ... v� DAK Americas requests approval to discontinue the
reporting of Outfall 002 monitoring under NC0000663.
i FLUENT Monitoring will be reported under NCS000392. REQUiREME
CHARA 1STIC am Sample
Average Average Maximum Frequency e. Location
Flow, MGD
Weekly
Instantaneous
Effluent
Total Suspended Solids (TSS)
7 /l
150 mg/I
6 ekfy
Grab
Effluent
Temperature, °C 1
Weekly
Continuous
Effluent
Total Residual Chlorine (TRC) Z
17 µ9/1
Weekly
Grab
Effluent
PH
Not more than U. nor les an
Os. U.
2/Month
Grab
Effluent
Total Phosphorus mgh (TP)
ly
Composite
Effluent
Total Nitrogen, gel TN)
TN = (NO2-N 3 ) N
Monthly
alcWited
Effluent
NltriteJNitrate gen mg/l
(NO2-N -N)
Monthly
Composite
Effluent
To>Keloahl Nitroge mg_/l -
Monthly
Composite
Effluen
lW )
Footnotes:
1. The discharge shall not cause the temperature of the receiving water to exceed �2.8 4C above
background and in no case exceed 32 "C.
2. Total Residual Chlorine compliance is required for chlorine or chlorine derivative used for disinfection.
The Division shall consider all effluent TRC values reported below 50 ug/I to be in compliance with the
permit. However, the Permittee shall continue to record and submit all values reported by a North
Carolina certified laboratory (including field certified), even if these values fall below 50 ug/l.
There shall be no chromium; z1hc or copper added ta'the cooling'water except as pre -approved
additives to biocidal corhpounds.
There shall be no discharge of floating solids or visible foam in other than trace amounts
The permittee shall obtain authorization from the Division prior to the use of any chemical additive in
the discharge. The permittee shall notify .the Division' in writing at least ninety days prior to
instituting use of any additional additive in the discharge potentially toxic to aquatic life (other than
additives previously approved by the Division). Such notification shall include completion of Biocide
Worksheet Form 101 (if applicable), a copy of the MSDS for the additive and a map indicating the
discharge point and receiving stream.
Submit requests for approval to: NC DENR / DWQ / Aquatic Toxicology Unit
1621 Mail Service Center
Raleigh, North Carolina .27699-1621

PermitNCO000663
A. (6) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS-OUTFA 403
Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized
to discharge non -contact once through cooling water, cooling tower and boiler blowdown and
stormwater runoff through outfall 003. Such discharges shall be limited and monitored by the
flar.,.,ittuc n �narifiar! Fcl.-....'
DAK Americas requests approval to discontinue the
reporting of Outfall 003 monitoring under NC0000663.
EFFLUENT Monitoring will be reported under NCS000392. G REQUIREM
CHIA TER ISTI ---r---monrnjy weeKlyy Meas1JreM9M= Sam Sample
Average Average Maximum Frequency pe Location
Flow, MGD
Weekly
Instantaneous
Effluent
Temperature, °C
ekly
Continuous
Effluent
Total Residual Chlorine (TRC) 2
17 p
Weekly
Grab
Effluent
pH
Not more than 9, ess than
2/Month
Grab
Effluent
6.0 S
Total Phosphorus mg/ (TP) 3
Monthly
Grab
Effluent
Total Nitrogen mg/l N) 3
hI
Calculated
Effluent
TN (NO2-N + a- ) + TKN
Nitrite/Nitrate Nltroge 11
(NO2 N + NO3 N) 3
Monthly
Grab
Effluent
Total KjeldptKtroge , DI
Monthly
Grab
(fluent
(TKN
Footnotes; `
1. The discharge shall not cause the temperature of the receiving water to, exceed 2.8 °C above
background and in no case exceed 32 °C.
2. Total Residual Chlorine compliance Is required for chlorine or chlorine derivative used for disinfection. The
Division shall consider all effluent TRC values reported below 50 ug/l to be in compliance with the permit.
However, the Permittee shall continue to record and submit all values reported by'a North Carolina
certlfled laboratory (Including field certifled), even if these values fall below 50 ug/l.
3. The permlttee may petition to have the sampling frequency reduced to quarterly after 12 consecutive
samples analyses have submitted.
There shall be no chromium, zinc or copper added to the cooling water except as pre -approved
additives to biocidal compounds.
There shall be no discharge of floating solids or visible foam in other than trace amounts.
The perrnittee shall notify the Division in writing at least ninety days prior to instituting use of any
additional additive in the discharge potentially toxic to aquatic life (other than additives previously
approved by the Division). Such notification shall include completion of Biocide Worksheet Form 101
(if applicable), a copy of the MSDS for the additive and a map indicating the discharge point and
receiving stream.
Submit requests for approval to: NC DENR / DWQ / Aquatic Toxicology Unit
1621 Mail Service Center
Raleigh, North Carolina 27699-1621

Attachment 2
Proposed Revision to
Stormwater Permit NCS000392
a (YORIEN 6 GERE

P a to, fo;,+s
soil — %013
OOZ 00?j
1 0 0* 4-
4- 4-
4— 4
20+ 20+
20+ 20�
4
4- 4-
4-0 4' 4 0'-
Permit No. NCS000392
SECTION B: ANALYTICAL MONITORING REQUIREMENTS
Analytical monitoring of stormwater discharges shall be performed as.specified in Tablc 1. All
analytical monitoring shall be performed during a representative storm event. The required
monitoring will result in a minimum of ten analytical samplings being conducted over the term
of the permit at each stormwater discharge outfall (SDO).
A representative storm event is a storm event that measures greater than 0.1 inches of rainfall. The time
between this storm event and the previous storm event measuring greater than 0.1 inches must be at least
72 hours. A single storm event may have a period of no precipitation of tip to 10 hours. For example, if
it ruins but stops before producing any collectable discharge, a sample may be' collected if the next rain
producing a discharge begins within 10 hours. _ T
Table 1. Analytical Mooitorinti Reouirements
;� yr� r r,;ti c. r
1
ppOWN
Y
T
.r.,.��
tj�
-+' k
'�a, t : ri � x'v { - � c
i', r. f �G i
F-_T �1
,� f t ✓�tw"icpfc0.
'F6 �` r• 5 s �y i� ! . • �ti�} y
Total Suspended Solids
mg/L
semi-annual
Grab
All SDOs exce t 001� -
Biochemical Oxygen
Demand
mg/L
semi-annual
Grab ;
All SDOs except 001
Chemical Oxygen
Demand
mg/L
semi-annual
Grab.
All SDOs except 001
Total Kjeldahl
Nitro en
mglL
semi-annual
Grab
All SDOs except 001,-002 and-003
Total Nitrogen TN
mg1l,
semi-annual
Grab
All SDOs except 001, 002-u► d-W
Total Phos horus P
mg/L
semi-annual
Grab
All SDOs exce t 001, VW-wni-00
Cobalt4
m eL
semi-annual4
Grab
Outfall002
1,4 — Dioxane`t
m
semi-annual4
Grab
Outfalls 002 and 003
H
standard .
semi-annual
Grab
All SDOs exce t 001, 002 rind-003
Total Rainfalls
inches
semi-annual
Rain Gauge
-
ootnotcs:
I Measurement Frequency: Twice per year during a representative storm event.
2 Grab samples shall be collected within the first 30 minutes of discharge.
---�� Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) unless representative outfall
status has been granted. //We71-1>rlas •eot raci%V� ty
4 The permittee shall monitor Cobalt and 1,4 Dioxane for the first two full years of the permit, At that time, the permittee
may petition DWQ in writing to reduce or remove one of both of these parameters. To make that request, the permittee
shall send two summaries of data slid two written requests (an original and a copy) to the DWQ Central Office for review.
Each WWI shall be considered on an individual basis.
5 For each sampled representative storm event the total precipitation must be recorded. An on -site rain gauge or local rain
gauge reading must be recorded.
Part II Page 5 of 10

Proposed TIMELINE for Shutdown and losure of OAK America's Cape Fear Plant in Leland, NC
Sep-13 Oct-13I No,13I Dec-13I Jan-14 Feb-14I Mar-14I Apr-14I May-14I Jun-14I Jul-14I Aug-14 I Sep-14I Oct-14I Nov-14I Dec-14 f Jan-15I Feb-15I Mar-15I Apr-15I May-15I Jun-ISI Jul-15I Aug-15I Sep-15I Oct-15I Nov-15I
9/30/2U13 1/31/2014 12/31/2014
Production W TVN P
Cease Shut Down EC
sure
TPA
L.�i I,crt—p
kJ
C,Xr
Dec-15
12/31/2015
Decontam-
ination
WWTP
Complete
r/6las
<vYI
K8n

Proposed TIMELINE for Shutdown and Closure of DAK America's Cape Fear Plant in Leland, NC
Sep-13 l Oct-13I Nov-13I Dec-13I Jan-14 1 Feb-14I Mar-14I Apr-141 May-141 Jan-14I Jul-14I Aug-14I Sep-141 Oct-14I Nov-141 Dec-14 f Jan-15I Feb-15 1 Mar -IS I Apr-15I May-15I Jun-15I Ju1-15I Aug -IS I Sep -IS I Oct-15 i Nov-15 I Dec-15
9/30/2013
1/31/2014
12/31/2014
12/31/2015
,i���'-
_
Decontam-
!nation
Production VJWiP
Cease Shut D�
• �_ - wwTP
�5DU Closure Complete
I

DAK Cape Fear Facility NPDES
Stormwater/Wastewater Permit
30 July 2013.
QN
Tube V r E

Agenda
❑ Overview of facility closure
❑ Status of existing NPDES wastewater permit (NCO000663)
❑ NPDES wastewater closure transition
❑ NPDES stormwater closure transition (NCS000392)
❑ Surface Disposal Unit closure transition (WQ0018087)
❑ Path forward
© 2012 O'Brien & Gere o0 CYBRIEN 6 GERE

3
Estimated Closure Sequence
❑ September 30, 2013—Production ceases
❑ December 2013-January 2014—WWTP ceases operation
❑ January 2014-December 2015—Decontamination/Demolition
� Including closure of WWTP
❑ December 2 014--Surface Disposal Unit Closure
© 2012 O'Brien & Gere
( 05 CYBRIEN 6 GERE

NPDES Wastewater Permit Status
❑ Permit expired November 30, 2011
❑ Application for renewal dated June 1, 2011
© 2012 O'Brien & Gere 9 013RIEN G G E R E

NPDES Wastewater Closure Transition
❑ September 30, 2013—Discharge of noncontact cooling water from
Outfalls 002 and 003 ceases
Modify frequency/scope of monitoring to reflect stormwater
discharge only
❑ October 1, 2013 to December 2013/January 2014—WWTP completes
treatment of final discharges from shutdown/cleanout
❑ Continue discharge of fluid from Surface Disposal Unit to Outfall 001
5 © 2012 O'Brien & Gere On GBRICN G GERE

DAK Cape Fear Facility'NPDES SW/WW Permit
% n
*t
0

7
NPDES Stormwater Closure Transition
❑ Transition from mixed wastewater/stormwater discharge, to
stormwater discharge only
� Divert closed spray field stormwater from WWTP to stormwater
outfall / fesfs s� -7"--h-5.
❑ Transition discharge from WWTP to stormwater
� Remove sludge/clean surfaces
� Breach containment to allow drainage
� Removal of TPA solids
> January to December 2014
> Flush wastewater —discharge continuing runoff as stormwater
* Identify requirements for discharge
© 2012 O'Brien & Gere
EYBRICN G GCRC

8
Surface Disposal Unit Transition
❑ Route discharge directly to Outfall 001 following termination of WWTP
operations in December 2013/January 2014
� Chlorinate to address fecal coliform
� Identify monitoring frequency and parameters
� Modify requirement for Grade 4 ORC
❑ December 2014—close Surface Disposal Unit
❑ Terminate discharge once underflow is eliminated, or reduced
sufficiently to cap drains
© 2012 O'Brien & Gere
L` ='J D'ORICN 6 SERE

DAK Cape Fear Facility NPDES SW/WW Permit
v
4f o"6
ig MR,
gni-
g wggg,
5M
-S. I
r!Surface Di posal Un
�001 -� AAA
LIN-
0.0
Lo
:TL
tit'

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Path Forward/Schedule
a Agreement on approach
o Identify vehicle to memorialize specifics of agreement
❑ Identify schedule milestones
© 2012 O'Brien & Gere
a CY13RIEN 6 GERE

90 O'DRICN 6 GCRC
11

THANK YOU
Tube V E

I
TO:
Tom Belnick
cc: Jim Gregson
FROM:
Jason Lewandowski
Jim McKay
RE:
DAK-DWQ Meeting 7/30/13
Ken Pickle
FILE:
50406
Penny Mahoney
DATE:
August 9, 2013
Elizabeth Wike
Michael Hall
This memorandum provides a summary of the topics discussed during the meeting held between member s of
DWQ DAK Americas and O'Brien & Gere on July 30, 2013 at the NCDENR Archdale Building, Room 917. The
purpose of the meeting was to discuss wastewater and stormwater closure proposals DAK and O'Brien & Gere
developed for the closure and demolition of the Cape Fear Site in Leland, NC. Attendees included:
Tom Belnick, NPDES Complex Permitting Unit Supervisor
Jim Gregson, DWQ Wilmington Regional Office, Surface Water Protection Supervisor
Jim McKay, NPDES Complex Permitting Unit
Ken Pickle, Stormwater Permitting Unit
Penny Mahoney, DAK Americas
Elizabeth Wike, DAK Americas
Michael Hall, O'Brien & Gere
Jason Lewandowski, O'Brien & Gere
DISCUSSION POINTS
The following provides a summary of the topics discussed during the meeting:
ESTIMATED CLOSURE SEQUENCE
a September 30, 2013 - production ceases
m December 2014 - completion of Surface Disposal Unit (SDU) closure (SDU is capped so stormwater has no-'
exposure and leachate pipes are capped to prevent flow),
e December 2013 -January 2014 - WWTP ceases operation/
January 2014 - December 2015 -decontamination/demolition (includes closure of WWTP - breaching basin
berms)
EXPIRED WASTEWATER NPDES PERMIT
DAK is currently operating under a wastewater NPDES permit that expired November 30, 2011. DAK applied
for renewal of this permit on June 1, 2011. The following points were discussed at the meeting regarding the
wastewater NPDES permit:
n Tom Belnick indicated that the expected amount of time between when production ceases to when wastewater
stops being discharged to surface water is large enough to require a new wastewater NPDES permit. Tom Belnick
indicated that the EPA will not allow the expired permit to be modified or renewed. Because production is stated
to cease, a new permit cannot continue to use the production -based limits in the expired permit, and new limits
will need to be established.
o DAK estimates that the Cape Fear Site will continue to produce large volume, high chemical oxygen demand
(COD) wastewater flows for several months following the cessation of production. Elizabeth Wike asked what
lag -time there will be between when production ceases and new NPDES permit limits become effective.
a Tom Belnick indicated that he will review and answer this question.
9 GBRIEN 6 GERE

Tom Belnick
August 9, 2013
Page 2
WASTEWATER NPDES MONITORING AND REPORTING FOR OUTFALLS 002 AND 003
Discharges from Outfalls 002 and 003 include both process -related sources and stormwater, and are therefore
covered by both the NPDES wastewater and stormwater permits. Outfall 002A is only covered by the NPDES
stormwater permit. Outfall 002A receives discharge from Outfall 002 in addition to stormwater runoff from
industrial drainage area 002A (Figure 1). Outfall 003A receives discharge from Outfall 003 in addition to
stormwater runoff from industrial drainage area 003A. The following points were discussed at the meeting with
regard to the wastewater discharges from Outfall 002 and 003:
m After production ceases wastewater related discharges will be discontinued from Outfalls 002 and 003. Ken
Pickle emphasized that coal pile runoff must also be eliminated from Outfall 002 in order to discontinue the
monitoring and reporting required by the wastewater NPDES permits.
0 Ken Pickle indicated that once wastewater related discharges at Outfalls 002 and 003 are eliminated, wastewater
and stormwater monitoring and reporting can be discontinued for Outfalls 002 and 003, with stormwater
monitoring and reporting to continue from Outfalls 002A and 003A. Further, he indicated that DWQ approval of
this modification can be obtained with submittal of a letter request.
CLOSED SPRAY FIELDS STORMWATER RUNOFF
There are two closed spray fields west and south of the SDU (Figure 2). These fields were originally used to land
apply waste activated sludge from the site's aerobic biological wastewater treatment process, and have not been used
since 1983. The permit for operation of the spray fields (No. WQ0012759) was rescinded in 2010. Currently,
stormwater runoff from these fields in directed through ditches to a sump which also collects surface runoff from the
SDU. The surface runoff sump is pumped to the WWTP. Currently, shallow underdrain pipes collect and directwater
infiltrating these fields to second sump which also collects leachate from the underdrains in the SDU. The underdrain
sump is pumped to the WWTP.
The entire footprint of the west field is within the drainage area contributing runoff to Outfall 004. The footprint of
the south field is split between drainage areas contributing runoff to Outfall 004 and 005. The following items were
discussed at the meeting with regard to the runoff from the closed sludge spray fields:
n DAK would like to divert surface runoff from both fields to discharge through Outfall 004 in order to reduce
hydraulic loading to the WWTP. This would be accomplished by closing the underdrain pipes beneath both fields,
removing portions of the surrounding berms and ditches, and allowing stormwater runoff from both fields to
discharge through Outfall 004. Ken Pickle indicated that water quality data for surface runoff from the fields
would benefit the evaluation of discharging surface runoff from the field through Outfall 004.
e Elizabeth Wike offered to test stormwater runoff from the closed spray fields for the water quality parameters
that are tested semi-annually at Outfall 004 (TSS, BOD, COD, TKN, TN, TP and pH).
a Ken Pickle indicated that two separate samples will be sufficient to evaluate the option of discharging field runoff
at Outfall 004.
TPA SOLIDS STORMWATER RUNOFF
During production, residual grains of terephthalic acid (TPA) leave the manufacturing process and enter the process
wastewater drains. Over many years, this TPA has accumulated into a large quantity in the first two basins they
encounter in the WWTP. TPA is a white, solid organic chemical (C8H504) used as a precursor to plastic in water
bottles with a consistency somewhat like talc. It has a low solubility in water (17 mg/L), it is not toxic to aquatic
organisms within this solubility limit, and it is readily biodegradable in soil and water'. TPA is one of the main
1 TPA reported as readily biodegradable by the OECD/SIDS (Organization for Economic Cooperation and Development/Screening
Information Data Set)
®� O'®RICNI G GERE

Tom Belnick
August 9, 2013
Page 3
products manufactured and sold by DAK. DAK has removed and sold this material in the past, and intends to pull the
accumulated TPA out of these basins and sell it. Prior to loading and shipping, it is necessary to dewater the TPA.
During closure of the WWTP, DAK intends to pump off the residual wastewater from the basins containing TPA, and
treat it in the WWTP. Following this, DAK will flush the TPA with potable water to push out residual wastewater
trapped in the pore -space, and then drain the rinse water from the basin. This rinse water will also be treated in the
WWTP.
The process of draining, containerizing and shipping the TPA will be done incrementally and is expected to take
approximately 1-year to complete. During this process, stormwater that accumulates in the TPA -containing
basins will need to be pumped off periodically, and discharged as stormwater or wastewater. The following
items were discussed at the meeting regarding the discharge of storm water that accumulates in the basins
containing TPA:
o Michael Hall asked if stormwater exposed to this accumulation of TPA can be discharged as stormwater under the
NPDES stormwater permit. Ken Pickle indicated that this was problematic, and would be difficult to accomplish.
The next question asked was if the water could be discharged from Outfall 001, along with the water from the SDU
underdrain.
Q Ken Pickle indicated that the water would need to be characterized to evaluate the viability of this option. %
Elizabeth Wike offered to evaluate the characteristics of the water that accumulates in the TPA basins by
performing testing of water derived from a bench scale test. Water to be tested will be obtained by collecting a
sample of TPA from the WWTP, washing it twice with deionized water equal to 100% theoretical displacement by
spraying the water over the TPA in a bucket fitted with holes in the bottom and lined with heavy duty filter cloth.
Spraying the water over the TPA will simulate how rain will displace the wastewater surrounding the TPA grains.
The rinsate from the first two washings will be discarded. Then a third quantity of deionized water equal to '
100% theoretical displacement will be sprayed over the TPA and collected for analysis. Water will be tested for
TSS, BOO, COD, and acute toxicity.
Ken Pickle indicated that this level of testing will be adequate for evaluating the option of discharge through
Outfall 001, and requested an estimate of the flowrate generated during the TPA draining and removal process.
DISCHARGE FROM THE SDU
DAK currently has three inputs to the onsite WWTP: (1) process wastewater (2) sanitary wastewater and (3)
discharge from the SDU. After production ceases, and after the several months of lag -time DAK needs to treat
process clean -out fluid, all process and sanitary wastewater will be eliminated from the site, at which point, DAK
will need to close the majority of their wastewater treatment processes. DAK would like to identify an
alternative approach for the discharge from the SDU from the time process clean out finishes until the SDU is
closed.
o Ken Pickle indicated that continued discharge under a wastewater NPDES permit sounds appropriate. Discharge
under a stormwater permit is not appropriate.
o Tom Belnick indicated that the discharge from the SDU could be included under the new wastewater NPDES
permit. In support of this, he requested a general characterization of the wastewater generated by the SDU,
(including the quality as well as acute toxicity) and the expected flowrate from the SDU.
m Elizabeth Wike described the material in the SDU as waste activated sludge from aerobic biological treatment
processes in the WWTP, and consisting of dead bacteria cells that once fed on influent wastewater constituents,
and the higher forms of microorganisms that fed on the bacteria. Discharge from the SDU includes surface runoff
that flows over the solids, and leachate that is collected in underdrain pipes at the bottom of the SDU.
o Jason Lewandowski explained that the discharge flowrate currently measured from the SDU includes stormwater
from abandoned spray fields to the west and south ofthe SDU. If the flow from these fields is routed to Outfall
U0 O'BAICW S GEAC

Tom Belnick
August 9, 2013
Page 4
004, then discharge will only be generated as a result of rainfall into the SDU itself Discharge must be pumped
out of the SDU in order to be routed to Outfall 001, as it is now. Therefore, the discharge rate is controlled by the
discharge pump capacity. The existing pumps have a maximum discharge capacity of 1.8 MGD. Using the area of
the SDU and historical rainfall data, the projected maximum monthly discharge rate is 0.290 MGD. A 24-hour, 25-
year rainfall event would add 3.8 MG to the SDU, however, the discharge pumps would control the rate at which
this water is discharged.
Jason Lewandowski explained that samples of SDU discharge have been tested for several water quality
parameters approximately 2-times per week since mid -April 2013. Tested parameters include, BOD, TSS, fecal
Coliform, nitrite/nitrate, TKN, orthophosphate, and ammonia nitrogen. Jason provided meeting attendees a copy
of the water quality results (Table 1).
o Elizabeth Wike offered to have acute toxicity testing performed on the SDU discharge.
�+ Based on the existing water quality data and projected flowrate, Jason Lewandowski indicated that he expects the
discharge to be chlorinated prior to discharge at Outfall 001. Jim McKay indicated that dechlorination will likely
be required to accompany the chlorination process.
SDU PHYSICAL CLOSURE
m Tom Belnick asked if there is a plan for the physical closure of the SDU.
Michael Hall explained that samples of the SDU solids are being tested to determine the most cost effective
method of closure. One of the closure options being considered is to cap the SDU and close it in place. Mike Hall
indicated that the Division of Water Quality is overseeing the physical closure process.
No. Action Item
Water quality testing on runoff from abandoned spray
1 fiel- 2 separate samples ds
DAK — Elizabeth Wike
August 31, 2013
- Test TSS, BOD, COD, TKN, TP and pH
Water quality testing on TPA drainage water generated in
2 a bench -scale study
DAK -- Elizabeth Wike
August 31, 2013
- Test TSS, BOD, COD and acute toxicity
3 Acute toxicity testing of SDU discharge
DAK — Elizabeth Wike
August 31, 2013
4 Projected flowrate of TPA drainage
O'Brien & Gere —
August 31, 2013
Jason Lewandowski
Determine the time-lag of WWTP operation under
5 existing permit during process clean out, after production DWQ— Tom Belnick
ceases and before a new permit is active
B Provide feedback on the type of permit and limits DAK DWQ—Tom Belnick
can expect to have in a new wastewater NPDES permit
t O'®RIEN 6 GERE

FIGURE 1
1�
NC Siormwater Permit Areas
DAK Americas LLC
Cape Fear Facility
OVERVIEW OF
STORMWATER
SYSTEM
0 250 sw 1.000 1,500
Fmt
o IWA
woe
O'BRIEN 6 GER[

Table l'.=r -x= "_ y 'Surface Disposal Ulriit Disci"arge'Analytical Data RF:
f e 4�
including stormwater runoff from spray fields
Fecal
BOO
TSS
COD
NITRATE
NITRITE
NH3-N
TKN
O-PHOS
Coliform
m IL
m /L
m /L
m L
m /L
m L
m L
m /L
#/100 ml
Max
57.2
170
168
<0.02
5,63
225.0
359
42.9
24,000
Average
22.8
37
123
<0.02
1.79
53.2
163
23.0
939
Min
4.1
8
66
<0.02
0.27
0.5
38
2.1
10
BOD
TSS
COD
NITRATE
NITRITE
NH3-N
TKN
O-PHOS
Fecal
Coliform
Rain
Flow
From
Sludge
Lagoon
BOD
TSS
k1b1da
NITRATE
NITRITE
NH3-N
TKN
O-PHOS
DATE
m 1L
m 1L
m /L
m L
m 1L
m L
m L
m /L
#/100 ml
in
gallons
lb/daylb/day
lblda
Iblda
lb/da
Ib/da
Ib/da04/16/2013
14.1
8
115
<0.02
0.55
29.0
0
72,264
8.5
59.3
0.33
17.5
04/18/2013
22.4
170
145
<0.02
0.85
16.7
0
29,679
5.5
42
35.9
0.21
4.1
04/19/2013
14.1
64.
0
48,189
5.7
04/23/2013
18.3
11
136
<0.02
2.17
28.4
0
-
04/25/2013
22.4
13
142
<0.02
0.33
2A
10
0
37,109
6.9
4
43.9
0.10
0.7
04/29/2013
4.1
75
66
<0.02
0.64
5.2
0.06
51,349
1.8
32
28.3
0.27
2.2
05/02/2013
43.6
51
153
1.44
1,50
34.9
262
0.13
144,115
52.4
61
193.9
1.7
1.80
41.9
05/06/2013
5.5
30
80
<0.02
1.14
9.6
0.09
57,157
2.6
14
38.1
0.54
4.6
05/09/2013
22.6
62
135
<0.02
2.21
27.8
0
69,261
13.1
36
78.0
1.28
16.1
05/13/2013
22.7
24
151
<0.02
3.93
41.5
0
35,827
6.8
7
45.1
1.17
12.4
05/16/2013
57.2
39
168
<0.02
5,63
359
42.9
3,270
0
-
-
-
-
-
05/21/2013
39.0
38
147
<0.02
3,78
330
41.5
3,300
0.07
11,353
3.7
4
13.9
0.36
31
3.9
05/23/2013
46.6
36
146
<0.02
3.75
256
38.0
0-17
11,647
4.5
3
14.2
0.36
25
3.7
05/28/2013
17.3
73
145
<0.02
1.94
135
16.9
226
0
24,991
3.6
15
30.2
0.40
28
3.5
05/30/2013
32A
59
165
<0.02
4.56
291
40.1
0
-
-
-
-
06/0312013
5.0
66
135
<0.02
0,52
64
2.9
4,000
0,15
23,689
1.0
13
26.7
0.10
13
0.6
06/06/2013
46.0
63
146
<0.02
1,42
255
40.0
0.43
62,152
23.8
33
75.7
0.74
132
20.7
06111 /2013
19.0
17
110
<0.02
0.63
0.5
38
12.2
2,180
0.36
720,909
114.2
102
661.4
3.79
3.0
227
73.4
06/13/2013
20.5
23
104
<0.02
1.12
95.4
100
20.7
0
533,502
91.2
102
462.7
4.98
424.5
445
92.1
06/18/2013
32.6
13
120
<0.02
2.43
225.0
222
35.4
24,000
0.43
38,059
10.3
4
38.1
0.77
71.4
70
11.2
06/20/2013
16.7
13
108
<0.02
0.49
0.9
93
16.7
0.3
502,749
70.0
55
452.8
2.05
3.8
389
70.0
06/24/2013
8.9
12
83
0.88
0,27
47.5
62
9.5
4,600
0.35
507,574
37.7
51
351.4
1.14
201.1
261
40.0
06/27/2013
14.2
10
112
<0.02
0.52
1.2
38
6.6
0.24
343,905
40.7
29
321.2
1.49
3.4
108
18.9
07/0212013
6.7
14
75
<0.02
0.70
1.9
41
9.9
1,270
07/05/2013
13
98
07/09/2013
18.7
32
138
07/11/2013
8
136
07/16/2013
39
107
07/18/2013
16
91
DAK Americas LLC
Cape Fear Site
8/6/2013

Pickle, Ken
From: Pickle, Ken
Sent: Friday, August 09, 2013 2:57 PM
To: 'Jason Lewandowski'; Belnick, Tom
Cc: Gregson, Jim; Mckay, James; '[e-mail]'; '[e-mail]';
Bennett, Bradley
Subject: RE: DAK Meeting Memo for July 30th
Hi Jason,
I'm making my way through the notes from our July 30, 2013 meeting, which are nicely put together. Thanks for taking
on that task.
While I am willing to be corrected by others attending the meeting, I believe that the discussion of whether the TPA
drainage can be permitted under the existing stormwater permit goes beyond what was specifically covered in our
meeting together. Specifically,
• The report that I contributed to the discussion about a bench scale simulation of rainfall and TPA residuals
washing;
The report that I commented on whether, 'this level of testing will be adequate for evaluating the option of
discharge through 0utfa11001'. It may be that others from DWQ commented to that effect, but I am pretty sure
that I did not. Jim, Tom — did you guys comment on either of these points?
My sincere apologies if others remember the meeting this way, and I have just forgotten it.
have just had a memory lapse on these points. Can you double-check your notes, and check
see how they remember the related discussion on these points?
All - - will someone please copy Elizabeth? ! can't find her email.
Thanks,
Ken
Ken Pickle
Environmental Engineer
NCDENR I DEMLR I Stormwater Permitting Program
1612 Mail Service Center, Raleigh, NC 27699-1612
512 N. Salisbury St, Raleigh, NC 27604
Phone: [phone]
Fax: [phone]
Email: ken. [e-mail]
Website: httA:llportal.ncdenr.orglweb[Ir/stormwater
It certainly is possible that I
with others attending to
** Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulations.**
From: Jason Lewandowski Finailto:[e-mail]]
Sent: Friday, August 09, 2013 1:33 PM

To: Belnick, Tom
Cc: Gregson, Jim; Pickle, Ken; Mckay, James
Subject: DAK Meeting Memo for July 30th
Tom,
Good afternoon. As you requested, I have attached a memo that summarizes the discussion, and the resulting action
items we had from the meeting held about DAK on July, 30th.
DAK and I are well on our way to providing the deliverables we agreed on during the meeting. we look forward to
hearing back on the items you all were you looking into.
Have a nice weekend,
CYGRICNGGERE
Jason Lewandowski
ENGINEER 2
O'BRIEN & GERE
2610 Wycliff Road, Suite 104
Raleigh, NC 27607
p 919-783-7777 XT 12 1 f 919-783-0757
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Pickle, Ken r-
To: Bennett, Bradley
Cc: Georgoulias, Bethany; Belnick, Tom
Subject: DAK decommissioning and demolition and NCS000392
Bradley,
Meeting summary: I don't think there are any insurmountable issues with what OAK wants to do wrt modifying our
stormwater permit monitoring requirements.
We have some coordination tasks with Tom's program, and we have some work in identifying crisp transition points
during the decommissioning/demolition.
Attending: Penny Mahoney, DAK Operations Director; Elizabeth Wike, DAK Environmental Engineer; Mike Hall, O'Brien &
Gere Raleigh; Jason Rodowski (sp?) 0&G; Tom Belnick, Jim McKay, Jim Gregson (by phone), kbp
DAK target schedule:
o 9/30/2013 - Cease production. Begin routing process liquids and wash waters through the on -site WWTP
(NC0000663); estimate 90 days duration.
o 1/1/2014 - Cease WWTP operation.
o 1/1/2014—12/31/2015 — Decontamination and demolition duration.
o 12/31/2014 — Close out Surface Disposal Unit (Sludge lagoon receiving sludge from the WWTP.)
Looks like four outfalls at the site, although it appears there are two additional 'internal' outfalls, but their purpose is
unclear presently. Outfalls #01, #02A, #03A, and #04. Unclear now why there are also Outfalls #02 and #03 since these
two feed Outfalls #02A and #03A respectively. Perhaps some historic condition or perspective prompted these.
Special circumstances:
a. Currently supernotant from the sludge lagoon is returned to the WWTP. Once the WWTP is shut down, rain will
accumulate in the WWTP sludge lagoon, and must be removed so that the lagoon can be closed out
permanently, either by excavation and landfilling off site, or by capping in place. OAK proposed to have this rain
driven flow considered a stormwater discharge.
b. Two other WWTP lagoons have bottom sediments rich in TPA, which DAK would like to recover and sell. After
initially draining the lagoons, DAK proposed that any subsequent drainage from these bottom sediments
considered a stormwater discharge.
c. DAK currently has two legacy sludge spray fields on the property, with runoff being returned to the head of the
WWTP. They haven't been operated since the 80's or 90's (some uncertainty on when they were last operated.)
DAK proposed that that the runoff be considered a stormwater discharge.
Current conditions:
#01— WWTP discharge. Contains process ww and heavy process area stormwaters routed to the WWTP. Covered by
the ww permit.
#02 — Non -contact cooling water and similar flows; coal pile runoff; stormwater. Covered in the ww permit; ALSO
covered for BOD, COD, cobalt, and 1,4-dioxane in the sw permit. (Again, not sure why #02 rather than #02A was
picked.)
#03 — Non -contact cooling water and similar flows; stormwater. Covered in the ww permit; ALSO covered for TSS, BOD,
COD, and 1,4-dioxane in the sw permit. (Again, not sure why #03 rather than #03A was picked.)
#04 — Apparently sw only discharges, although not specifically named in the stormwater permit, this discharge point
would be captured by the standard wording in our permit which requires sampling at, "All SDO's" . Not included in the
ww permit.

After some discussion I think we arrived at the following proposed conditions in response to the D&D activities:
#01—Contrary to the initial proposal, sludge lagoon drainage (see special item a. above) during the demolition and close
out will be routed to the WWTP. I expect that will prolong the WWTP life an extra year beyond the 1/1/2014 target,
although with reduced functionality — i.e., it's probably not going to be necessary to operate the system as a full
activated sludge WWTP — it can convert to a simpler, cheaper physical -chemical plant.
#01— Contrary to the initial proposal of washing the TPA sediments in place until they are, 'clean', and then allowing the
discharge of any accumulated liquids as a stormwater, I cited 40CFR122.2 definition of 'Process wastewater, and
indicated that it would be difficult for us to permit this as a stormwater.
#01— So, when all these flows are
Ken Pickle
Environmental Engineer
NCDENR I DWQ I Stormwater Permitting Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
512 N. Salisbury St, Raleigh, NC 27604
Phone: [phone]
Fax: [phone]
Email: [e-mail]
Website: http://po,rtal.ncdenr.org/web/wq/wslsu
** Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulations.**

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Pickle, Ken
From: Pickle, Ken
Sent: Monday, July 28, 2014 9:12 AM
To: Sams, Dan
Cc: Bennett, Bradley; Gregson, Jim; Tharrington, Tom; Belnick, Tom
Subject: RE: Stormwater permit modification; DAK decommissioning
Hi Dan,
FYI, No Action
KBP summary of conference caft far stormwater issues:
Conferees: Jim Gregson, Tom Tharrington, Tom Belnick, KBP
-Che conference call information indicates that DAK progress so far sounds consistent with the November 201.3
permit addendum and transmittal letter: KBP concluded that no change to the stormwater permit addendum is
indicated based on DWR WIRO report of their site visit. Also, no change to the permit appears necessary based
on our understanding of DAK actions contemplated in the near term.
KBP opened a short discussion about the current state of the coal pile area.
o The stormwater permit does not authorize the discharge of runoff from the coal pile area.
o The extent of the removal of the coal could be significant in determining whether or not Outfall 002
could be switched over to a stormwater-only outfall.
o KBP made DAK aware of this issue since the beginnings of our discussions with them (June and
September 2013), and the issue is specifically addressed in the November 2013 transmittal letter that
accompanied the permit addendum.
WIRO DWR next site visit to include invitation to WIRO DEMLR to accompany them.
Ken Pickle
Environmental Engineer
NCDENR I DEMLR I Stormwater Permitting Program
1612 Mail Service Center, Raleigh, NC 27699-1612
512 N, Salisbury St, Raleigh, NC 27604
Phone: [phone]
Fax: [phone]
Email: ken.yickle@)-ncdenr.aoy
Website: http://Rortai,ncdenr,ol9/web/1rLStQrmwat;
** Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulations.**
From: Pickle, Ken
Sent: Friday, July 25, 2014 12:41 PM
To: Sams, Dan
Cc: Bennett, Bradley; Gregson, Jim
Subject: RE: Stormwater permit modification
Oops,'1:30] not 1:00.

kbp
Ken Pickle
Environmental Engineer
NCDENR I DEMLR I Stormwater Permitting Program
1612 Mail Service Center, Raleigh, NC 27699-1612
512 N. Salisbury St, Raleigh, NC 27604
Phone: [phone]
Fax: [phone]
Email: ken. i kle nc enr. ov
Website: http://portal.ncdQnr.org/web/Ir/stormvvater
** Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulations.**
From: Pickle, Ken
Sent: Friday, July 25, 2014 12:06 PM
To: Sams, Dan
Cc: Bennett, Bradley; Gregson, Jim
Subject: FW. Stormwater permit modification
Hi Dan,
I didn't see your name on the distribution of recent emails pertaining to a 00 confere �'.nce"call this afternoon about the
decommissioning activity at DAK Americas. Jim Gregson's group has the most interest in this call, but we in the
stormwater program are also involved to a lesser degree. I'm not sure if your participation is necessary, but just FYI.
Ken
Ken Pickle
Environmental Engineer
NCDENR I DEMLR I Stormwater Permitting Program
1612 Mail Service Center, Raleigh, NC 27699-1612
512 N. Salisbury St, Raleigh, NC 27604
Phone: [phone]
Fax: [phone]
Email: [e-mail]
Website: http://portal,ncdenr.org/web/­ir/stQrmwater
** Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulations.**
From: Pickle, ken
Sent: Friday, July 25, 2014 11:44 AM
To: Gregson, Jim; Tharrington, Tom
Cc: Bennett, Bradley; Belnick, Tom
Subject: FW: Stormwater permit modification
Tom, Jim,

r
4
Back in November 2013 we issued an addendum to our stormwater permit, along with a transmittal letter. Together the
two documents established our agreement with DAK on the stormwater concerns associated with the decommissioning
of DAK. I've included it here for our ready reference in today's phone call.
Ken
Ken Pickle
Environmental Engineer
NCDENR I DEMI-R I Stormwater Permitting Program
1612 Mail Service Center, Raleigh, NC 2769971612
512 N. Salisbury St, Raleigh, NC 27604
Phone: [phone]
Fax: [phone].
Email: [e-mail]
Website: tUD//oortalncdenr.org/web/Ir/`stormwa.ter
** Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulations.**
From: Pickle, Ken
Sent: Monday,. December 30, 2013 2:09 PM
To: '[e-mail]'
Subject: RAI: Stormwater permlt modification
Fll Elizabeth,
It has been a month since we revised_ the stormwater permit. 1 assume the permit is ok for the circumstances, but let
me know if difficulties with the stormwater permit arise during decommissioning.
Ken
Ken Pickle
EnvirQnment;al Engineer
NCDENR I DEMLR I Stormwater Permitting Program
1612 Mall Service Center, Raleigh, NC 27699-1612
512 N. Salisbury St, Raleigh, NC 27604
Phone: [phone]
Fax [phone]
Email: ken.. oickleQncdgnr..Qo_v
Website: j tttl2l//oortcil,nQdenr.orgLw�b/Ustormwater
** Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulations.**
From: Pickle, Ken ,
Sent: Friday, November 22, 2013 12:39 PM
To: '[e-mail]'
Cc: Bennett, Bradley
Subject: Stormwater permit modification

Hi Elizabeth, nice to hear from you.
Please see attached transmittal letter and Permit Addendum 1, as per my understanding of DAK's requests.
Please contact me if there are problems with the scope or detail of the letter and addendum.
Ken
<< File: DAK Americas Permit Addendum 1.docx >>
<< File: DAK Americas permit monitoring revision 11212013.docx >>
Ken Pickle
Environmental Engineer
NCDENR I DEMLR I Stormwater Permitting Program
1612 Mail Service Center, Raleigh, NC 27699-1612
512 N. Salisbury St, Raleigh, NC 27604
Phone: [phone]
Fax: [phone]
Email: [e-mail]
Website: htta://portal.ncdenr.org/web/Ir/stormwater
** Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulations.**

pnc Ken
From:
Belnick, Tom
Sent:
Monday, July 28, 2014 10:11 AM
To:
Gregson, Jim; Tharrington, Tom; Meadows, Susan; Pickle, Ken; Sams, Dan
Cc:
[e-mail]
Subject:
NCO000663 DA.K Notification
Attachments:
NCO000663 Mod 2014.pdf
Attached is NPDES Permit Notification for DAK, which provides notification to facility on which Effluent Sheets are
applicable effective August 1, Facility Is transitioning to closure/permit rescission during permit term, Let me know if
any questions.
Tom Belnick
Supervisor, NPDES Complex Permitting Unit
NCDWR/Water Quality Programs
919-807-6390
E-mail correspondence to and from this address may be subject to the
North Carolina Public Records Law and may be disclosed to third parties

09
A
�
MCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory
Governor
Ms. Penny C. Mahoney
Director of Sustainability
DAK Americas LLC
P.O. Box 2260
Leland, NC 28451
Dear Ms. Mahoney:
John E. Skvarla, III
Secretary
July 28, 2014
Subject: NPDES Permit Notification
Permit NCO000663
DAK Leland Plant
Brunswick County
Class II WWTP
The current NPDES permit provides for various transition effluent sheets, as the facility
progresses toward permanent closure and ultimata permit rescission during this permit term.
Following a site visit conducted by our Wilmington Regional office and review of data, the
Iivision is notifying you of its approval to transition to the following permit requirements:
Outfall 001. Effective August 1, 2014, void Effluent Sheets A(1) and A(2), and activate
requirements in Effluent Sheet A(7).
Outfall 002. No changes at this time. Facility is still subject to requirctnents specified in
Effluent Sheet A(3).
Outfall 003. Effective August 1, 2014, void Effluent Sheet A(4). Monitoring will
continue in accordance with Stortnwater Permit NCS000392. ✓;,evo-
If any parts, measurement frequencies, or sampling requirements contained in this permit are
unacceptable, you have the right to an adjudieutory hearing upon written request within thirty
(30) days after receiving this letter. Your request must take the form of a written petition
conforming to Chapter 150B of the North Carolina General Statutes, and must be filed with the
Office of Administrative Hearings, 6714 Mail Service Ccntcr, Raleigh, North Carolina 27699-
6714. Unless such demand is made, this permit remains final and binding.
This permit is not transferable except after notifying the Division of Water Resources. The
Division may modify and re -issue, or revoke this permit. Please notice that this permit does not
1617 Mail Service Center, Raleigh. North Caroline 27699-1617
Location: 512 N, Salisbury St. Raleigh, North Carolina 27604
Phone: [phone] Fax: [phone]
Internet: www.ncwaterc tali r
An Eq!jal opportunityWirmelive Action Employe(

Wr
affect your legal obligation to obtain other permits required by the Division of Water Resources
or other federal, state, or local governments.
If you have questions, or if we can be of further service, please contact Tom Belnick at
toirl.bclnick(:a)iicclenr.�ov or call [phone].
Sincerely,
Original Signed by Tom Belnick
Thomas A. Reeder
NC DENR, DWR Director
Email: DWRIWilmington Regional Office
DWR/Aquatic Toxicity- Susan Meadows
DEMLR/Ken Pickle, Dan Sams
US EPA Region 4
Hardcopy:
NPDES Permit File NC0000663
Central Files

Pickle, Ken
From: Tharrington, Tom
Sent: Monday, July 21, 2014 11:44 AM
To: Belnick, Tom; Pickle, Ken
Cc: Gregson, Jim; King, Morella s; Bennett, Bradley
Subject: RE: DAK Site Status (NC0000663)
Attachments: DAK Americas WWTP&SDU.pptx; DAK Americas Trenches&Stormwater.pptx
I threw together some of the pictures from the DAK site, they might give you an idea of what the site looks like when we
talk about it.
From: Belnick, Tom
Sent: Friday, July 18, 2014 3:37 PM
To: Tharrington, Tom; Pickle, Ken
Cc: Gregson, Jim; King, Morelia s; Bennett, Bradley
Subject: RE: DAK Site Status (NC0000663)
I think a phone call would help, to go over each outfall status. I'll get with Ken on Monday and get back with you's.
Tom Belnick
Supervisor, NPDES Complex Permitting Unit
NCDWR/Water Quality Programs
919-807-6390
E-mail correspondence to and from this address may be subject to the
North Carolina Public Records Law and may be disclosed to third parties
From: Tharrington, Tom
Sent: Friday, July 18, 2014 10:18 AM
To: Pickle, Ken; Belnick, Tom
Cc: Gregson, Jim; King, Morelia s; Bennett, Bradley
Subject: RE: DAK Site Status (NC0000663)
Hello Ken and Tom, just wanted to touch base with you and see how you wanted to proceed with the DAK permitting
issue. Jim Gregson and I visited the site on the 1S1h and toured the process areas and reviewed the new wastewater
treatment plant configuration (I have some photos if you would like to see them). We are pleased with the progress they
have made in both areas and the following items are what we need to discuss with you.
on in the sampling requirements of Outfall 003 which is now a stormwate , my outfall to State X
SIQLij monitoring levels ..___ �— ,.,..
ove the 'u'ffall'0G1'to f e reduced monitorin levels as of.August_I" as they are ready to move to this level.
Discuss the possible reduction of Qutfall 002 to State Stormwater monitoring levels after DAK provides us some
sampling data of the water quality from the recently c eaned process areas. 7K r. Co f,4
Don't know if you want to do this via email or try to have a conference tail. Let me know if you have any comments.
From: Pickle, Ken
Sent: Monday, June 16, 2014 7:42 AM
To: Belnick, Tom; Tharrington, Tom
Cc: Gregson, Jim; King, Morelia s; Bennett, Bradley
Subject: RE: DAK Site Status (NC0000663)

Thanks for including me on this email string. I'll have comments on Elizabeth's request about my stormwater discharges
in a day or so. I'm returning today from two weeks' vacation, and I also need to refresh myself on the degree of
flexibility on the stormwater discharges that we talked about together with Elizabeth.
Right now I do recall that our conversations, (and 1 think a written permit mod ?, or maybe transmittal letter ?), included
the provision that if WIRO thought any particular DAK proposal on the timing of various stages of the decommissioning
were OK, we in the stormwater group would start with an amenable initial reaction with respect to stormwater permit
conditions. But, I need to go back in the file and be sure of what we were generally contemplating when we talked
about this with Elizabeth and her boss, Penny.
Tom, if we can wait a couple of days more to respond to WIRO, that would be good for me.
kbp
Ken Pickle
Environmental Engineer
NCDENR I DEMLR I Stormwater Permitting Program
1612 Mail Service Center, Raleigh, NC 27699-1612
512 N. Salisbury St, Raleigh, NC 27604
Phone: [phone]
Fax: [phone]
Email: ken_ pickleCcDncdenr.gov
Website: http://portal.ncdenr.org/web/lr/stormwater
** Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulations.**
From. Belnick, Tom
Sent: Wednesday, June 11, 2014 4:44 PM
To: Tharrington, Tom; Pickle, Ken
Cc: Gregson, Jim; King, Morella s
Subject: RE: DAK Site Status (NC0000663)
Tom- this is a very complicated permit for ultimate facility closure, and unfortunately the main permit writer (Jim
McKay) has retired. I have copied Ken Pickle, who was involved in the stormwater portions. Forgive me for responding
with more questions, but I'm trying to get myself oriented to where the facility is at with regard to their permit
conditions, and what they are requesting at this time:
�Outfall 003.
• This Outfall is subject to Effluent Sheet A(4).
• Effluent Sheet A(4), Footnote 3, provides for Permittee to petition for reduced sampling frequency after 12
consecutive samples have been submitted.
• Ultimately Outfall 003/Effluent Sheet A(4) will be voided, and' monitoring will continue under Stormwater Permit
NCS000392.
• Question- is DAK requesting reduced monitoring per Effluent Sheet A(4) Footnote 3 (to Quarterly frequency)?
Outfall 002.
This Outfall is subject to Effluent Sheet A(3).
• following production shutdown and DWR approval, move to Effluent Sheet
• Following coal pile removal and DWR approval, void Effluent Sheet A(8), and continue under Stormwater Permit
NCS000392.
0 Question- is DAK requesting move to A(8) at this time?

1/
Outfall 001.
o This Outfall is subject to Effluent Sheets A(1) and A(2). ✓ / ��/4
• Following production shutdown and DWR approval, move to Effluent Sheet A(7).
• Permittee will ultimately request permit rescission after all discharges cease.
• Question- I'm not sure of what DAK is requesting regarding bypass and interim step. Are they requesting to stay
at Effluent Sheet A(1) while pilot testing the modified monomer WWTP, then move to Effluent Sheet A(7)? If
yes, how long would trial period last.
Once again, sorry for the questions. I can tail you tomorrow to go over. If WiRO/CO concur with any of these requests,
it would be probably be best for CO to formally acknowledge the permit change, and make updates to BIMS so that we
are tracking compliance with the correct Effluent Sheets.
Tom Belnick
Supervisor, NPDES Complex Permitting Unit
NCDWR/Water Quality Programs
919-807-6390
E-mail correspondence to and from this address may be subject to the
North Carolina Public Records Law and may, be disclosed to third parties
From: Tharrington, Tom
Sent: Wednesday, June 11, 2014 10:52 AM
To: Belnick, Tom
Cc: Gregson, Jim; King, Morelia s '
Subject: DAK Site Status (NC0000663)
Hello Tom,
I have a couple of updates from the DAK site to make you aware of. The first is during my last site inspection the staff
at DAK asked for t fission to drop back to the basic stormwater monitoring parameters for Outfall 003. All mist
wastewaters associated with boiler and cooling tower operations have cease and the site is seeing only site stormwater
at this time. We in the Regional"Office are in agreeme t that r�educfion of'ttie required sampling at this Outfall would be
acceptable. I didn't kno if errmissssio� Ito go to this level of monitoring should be issued from this office or from the
CO. '
/`� � �` G 4�SY` fhd �' _/�.4�� a� p�.a�s %ra.�� if a 1.<.G aS�v �/ cz/is�'�.�+►�'
I have scheduled another visit to the site on July 15t" to inspect areas served by the 002 Outfall which should have
been completely cleaned and decommissioned at that point. At the time of my last visit the process equipment and
vessels had been cleaned and those suitable for salvage had been removed, the remaining task was to clean the process
area wastewater trenches.of-any'resid'ual sediments: This•acti�ity is near or at completion now. After my i sn pection in
July they would like to also have permission to reduce the monitoring at Outfall'002-as•vdel{. � wcsova
The last issue is Elizabeth Wike (DAK) contacted me this week and would like permission from the Wilmington Office
to conduct a trial period of operation where they by-pass the remaining Fibers Wastewater equipment and directly
discharge from the Monomers Wastewater System. At the time of my last inspection I toured the modified Monomers
System.and it appeared to be working well for them. Recent data show nitrogen removal rates of about 98% with the
total effluent BOD now running about 10 lbs/BOD/day or less. So as an interim step they would like to shutdown the
equipment and bypass the Fibers WWTP while continuing to gather data of directly discharged Monomers WWTP
effluent. This data would be' presented to me during the planned July inspection and from that point, request the
NPDES Permit reduction if results are as planned. I would like to send them an email confirming this Fibers WWTP by-
pass by the end of the week if it is acceptable to you. Call me if you have questions.

i also attached a few images for you
• 046 is the modified aeration basin with the curtain installed to create the anoxic section, they are currently
adding about 100 gallons per day of MicroC for carbon supplementation
• 055 is the new inclined plate clarifier, media filter and bag filter components
• 070 is the new activated carbon filters and new flowmeter located at the modified effluent point
• 076 is an overview of the Outfall 003 discharge point.
Tom Tharrington
Wastewater Treatment Plant Consultant
Division of Water Resources- Surface Water Protection Section
North Carolina Department of Environment and Natural Resources
Wilmington Regional Office
910-796-7324
torn.tha-rri n@ncde r. v
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Caw and may be disclosed to
third parties.

NCS000392 Addendum 1
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
PERMIT Addendum 1
TO DISCHARGE STORMWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other
lawful standards and regulations promulgated and adopted by the North Carolina
Environmental Management Commission, the Federal Water Pollution Control Act, as
amended, and the North Carolina Administrative Code at NCAC 15A 02H .0114(b)(1),
DAK Americas LLC
is hereby authorized to discharge stormwater from a facility located at
DAK Americas LLC - Caper Fear Site
3500 Daniels Road
Leland, NC
Brunswick County
in accordance with the discharge limitations, monitoring requirements, and other
conditions set forth in the NPDES stormwater discharge permit NCS000392, as amended in
this Addendum 1.
Amended conditions
1. This Permit Addendum 1 is an enforceable part of the permit.
2. In accordance with 15A NCAC 021-1.0114(b)(1), the monitoring program in Part II
Section B Table 1 Analytical Monitoring Requirements of this permit is amended
as follows:

NCS000392 Addendum 1
Table 1. Analytical Monitoring Requirements
Discharge
Characteristics
Units
Measurement
Fre uenc l
Sample
Type2
Sample
Location3
Total Suspended Solids
mg/L
semi-annual
Grab
All SDOs except 001
Biochemical Oxygen
Demand
mg/L
semi-annual
Grab
All SDOs except 001
Chemical Oxygen
Demand
mg/L
semi-annual
Grab
All SDOs except 001
Total Kjeldahl
Nitro en TKN
mg/L
g
semi-annual
Grab
All SDOs except 001
Total Nitrogen TN
mg/L
semi-annual
Grab
All SDOs except 001
Total Phosphor —us TP
mg/L
semi-annual
Grab
All SDOs except 001
Cobalt4
mg/L
semi-annual4
Grab
Outfall 002
1,4 — Dioxane4
mg/L
semi-annual4
Grab
Outfalls 002 and 003
H
standard
semi-annual
Grab
All SDOs except 001
Total Rainfalls
inches
semi-annual
Rain.Gauge
-
Footnotes:
I Measurement Frequency: Twice per year during a representative storm event.
2 Grab samples shall be collected within the first 30 minutes of discharge.
3 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) unless representative outfall
status has been granted.
4 The permittee shall monitor Cobalt and 1,4 Dioxane for the first two full years of the permit. At that time, the permittee
may petition DWQ in writing to reduce or remove one of both of these parameters. To make that request, the permittee
shall send two summaries of data and two written requests (an original and a copy) to the DWQ Central Office for review.
Each outfall shall be considered on an individual basis.
5 For each sampled representative storm event the total precipitation must be recorded. An on -site rain gauge or local rain
gauge reading must be recorded.
This permit addendum shall become effective December 1, 2013.
This permit addendum does not change the current expiration date for NCS000392.
Signed this day, November 21, 2013.
for Tracy Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission

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NCDENR
North Carolina Department of Environment and Natural Resources
Division of Energy, Mineral, and Land Resources
Land Quality Section,
Tracy E. Davis, PE, CPM
Director
November 21, 2013
Ms. Penny C. Mahoney
DAK Americas LLC
3500 Daniels Road, N.E.
Leland, NC 28451
Pat McCrory, Governor
John E. Skvarla, III, Secretary
Subject: Permit revision for NCS000392
DAK Americas - Cape Fear Site
Brunswick County
Dear Ms. Mahoney:
We have considered your requests for modifications to the subject NPDES stormwater
permit in O'Brien & Gere's September 26, 2013 letter on your behalf, and in prior
communications. As per our discussions during a couple of meetings and follow-up
conversations, we are providing this letter and the attached revised permit addendum as
our positive response to your requests.
The North Carolina Administrative Code at NCAC 15A 02H .0114 authorizes the Division to
make li'mi iced types of revisions to individual stormwater permits without going through the
full procedural requirements that would'otherwise accompany the issuance, renewal, or
modifications of those permits. We view your requested revisions as either not requiring a
formal revision to the permit in some cases, or as one of the types of revisions specifically
authorized by 02H .0114 in one case.
Your requested revisions:
1. 9/26/2013 O&G letter: You requested a permit revision to divert surface runoff from
the two closed spray fields in order to discharge through stormwater-only Outfall
004. The triggering event was to demonstrate to the Division that the flow from
those fields had a chemical character that did not suggest any out of the ordinary
pollutant risk. You have already made that demonstration to our satisfaction. We
also note your report that the spray fields have been inactive for some number of
years, exceeding 10 years.
However, please note that the text of NCS000392 does not currently specify which
areas of the facility would generate stormwater flows. It seems expeditious to note
that a revision to the permit text is not required. Our permit authorizes the
discharge of stormwater from all on -site industrial activity areas, and the two
dormant spray fields seem to qualify as such. Pending any contrary
determinations due to new site condition discoveries, the current permit,
unmodified, authorizes the discharge of surface runoff from these areas,
already. No change to the current permit is required. We appreciate your
willingness to take samples to establish the current character of the runoff from
those areas.
1612 Mail Service Center, Raleigh, North Carolina 27699-1612 • Telephone [phone] / FAX: [phone]
512 North Salisbury Street, Raleigh, North Carolina 27604 • Internet: httpa/portal.ncdenr.org/web/lr/land-quality
An Equal Opportunity 1 Affirmative Action Employer - 50% Recycled 110% Post Consumer Paper

Ms. Penny C. Mahoney, DAK Americas
November 21, 2013
Page 2of3
2. 9/26/2013 O&G letter: You requested a permit revision to divert surface runoff from
the Monomers production area to Outfall 002. You propose that the triggering
events would be the removal of exposed industrial materials in Monomers; the
completed cleaning of the industrial trench drains; and a stormwater inspection by
DEMLR staff in the Wilmington office. These arrangements are acceptable to us.
Upon the Regional Office inspection and approval of site conditions in the
area, those flows may be discharged under NCS000392, without
modification to the permit text: Please note again that the text of NCS000392
does not specify the point of origin for stormwater flows. No change to the current
permit is required.
However, please note that our stormwater-only permit does not authorize the
discharge of coal pile runoff. Have you made progress since our last discussion on a
plan to manage that flow to Dutfall 002 during the shutdown?
3. 9/26/2013 O&G letter: You requested a permit revision to divert stormwater flow
from the Fibers & Resins production area to Outfall 002 and/or to stormwater-only
Outfall 003. You propose that the triggering events are to be the removal of
exposed industrial materials in Fibers & Resins; the completed cleaning of the
industrial sewer; and a stormwater inspection by DEMLR staff in the Wilmington
office. These arrangements are acceptable to us. Upon the Regional Office
inspection and approval of site conditions in the area, those flows may be
discharged under NCS000392, without modification to the permit text. No
change to the current permit is required.
A. 9/,26/2013 O&G letter: You requested a permit revision to divert surface runoff from
the BACA Pits area to Outfall 002. You propose that the triggering events are to be
the removal of exposed industrial materials; and the completed cleaning of the
surfaces and trench drains. We think that a stormwater inspection by the DEMLR
staff in the Wilmington office will also be appropriate for this phase of the shutdown.
Upon the Regional Office inspection and approval of site conditions in the
area, those flows may be discharged under NCS000392, without
modification to the permit text. No change to the current permit text is required.
5. 9/26/2013 O&G letter: You requested a permit revision to divert stormwater runoff
from the several individual WWTP basins to Outfall 006. You propose that the
triggering events for each basin are to be the decommissioning, emptying, and
cleaning of each individual basin. We think that a stormwater inspection by the
DEMLR staff in Wili-nington office will also be appropriate for this phase of the
shutdown. Upon the Regional Office inspection and approval of site
conditions in the area, the stormwater-only flows from each individual basin
may be discharged under NCS000392, without modification to the permit
text. No change to the current permit text is required.
6. 6/7/2013 O&G letter: In June of this year, you requested a revision to the permit
text at Part II Section B Table 1 Analytical Monitoring Requirements. The Division is
authorized to change the monitoring requirements under the provisions of NCAC 15A
021i .0114. The revisions you propose in the June 7 letter are consistent with our
understanding of the physical changes planned during shutdown and
decommissioning of the facility. The revised Table 1 is attached to this letter as

/ Ms. Penny G. Mahoney, OAK Americas
/ November 21, 2013
Page 3 of 3
// Permit Addendum 1, for permit NCS000392. The Addendum 1 is an enforceable
part of the permit.
Please contact the Wilmington Regional Office approximately two weeks ahead of the day
that you anticipate needing their site inspections. Also, please contact me or the DEMLR
Wilmington Regional Office if developments during the decommissioning present difficulties
with the revised stormwater permit that we may not have anticipated.
Sincerely,
Ken Pickle
DEMLR Stormwater Permitting Program
[phone]
cc: Michael S. Hall, O'Brien & Gere, 2610 Wycliff Road, Suite 104, Raleigh, NC 27607
Jim Gregson, DWR WIRO
Dan Sams, DEMLR WIRO
Bradley Bennett, DEMLR Stormwater Permitting Program, RCO
DWR Central Files, NCS000392

NCS000392 Addendum 1
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF ENERGY, MINERAL, AND LAND RESOURCES
PERMIT Addendum 1
TO DISCHARGE STORMWATER UNDER THE
NATIONAL POLLUTANT DISCHARGEELIMiNATIM SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other
lawful standards and regulations promulgated and adopted by the North Carolina
Environmental Management Commission, the Federal Water Pollution Control Act, as
amended, and the North Carolina Administrative Code at NCAC 15A 02H .0114(b)(1),
DAK Americas LLC
is hereby authorized to discharge stormwater from a facility located at
DAK Americas LLC - Caper Fear Site
350u Daniels Road
Leland, NC
Brunswick County
in accordance with the discharge limitations, monitoring requirements, and other
conditions set forth in the NPDES stormwater discharge permit NCS000392, as amended in
this Addendum 1.
Amended conditions
1. This Permit Addendum 1 is an enforceable part of the permit.
2. In accordance with 1.5A NCAC 02H .0114(b)(1), the monitoring program in Part II
Section B Table 1 Analytical Monitoring Requirements of this permit is amended
as follows:

NCS000392 Addendum 1
Table 1. Analytical Monitoring Requirements
�, t R n' ,., ,Y i F'1
Dyscharge f�"a
s�-r f" � i--:�,
x r r
i.- rd; 3:
Measurement
it e r mr
k�Sample`1 ��
r w -..t r-:: r-
; s ttwg�� „�'�Sam-P.c . . s
.�-� tip: i;. ri .,r. ?&`. av �•.i,�i�f'r7
_
FSy Y • w `
Units
i�. = �'v3J..,,r�T �:5�,-�r fir•`],
. Fire 1
;, }fir •T �t+� ellI
T Ne2
,r`�
Locahnn3_..,
,xa.,Cha>ractertstics : ,,�_.
,
uenc
, erg;
•��:, x_�, t.�i".. :�
Total Suspended Solids
m L
semi-annual
Grab
All SDOs except 001
Biochemical Oxygen
All SDOs except 001
m L
semi-annual
Grab
Demand
Chemical Oxygen
All SDOs except 001
mg/L
semi-annual
Grab
Demand
Total Kjeldahl
All SDOs except 001
m L
semi-annual
Grab
Nitrogen TKN
Total Nitrogen TN
m
semi-annual
Grab
All SDOs except 001
Total Phosphorus TP
m /L
semi-annual
Grab
All SDOs except 001
Cobalt4
m L
semi-annua14
Grab
Outfall002
1,4 — Dioxane4
m L
semi-annual4
Grab
Outfalls 002 and 003
1-I
standard
semi-annual
Grab
All SDOs exce t 001
Total Rainfalls
inches
semi-annual
Rain Gauge
-
Footnotes:
I Measurement Frequency: Twice per year during a representative storm event.
2 Grab samples shall be collected within the first 30 minutes of discharge.
3 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) unless representative outfall
status has been granted.
4 The permittee shall monitor Cobalt and 1,4 Dioxane for the first two full years of the permit. At that time, the permittee
may petition DWQ in writing to reduce or remove one of both of these parameters. To make that request, the permittee
shall send two summaries of data and two written requests (an original and a copy) to the DWQ Central Office for review.
Each outfall shall be considered on an individual basis.
5 For each sampled representative storm event the total precipitation must be recorded. An on -site rain gauge or local rain
gauge reading must be recorded.
This permit addendum shall become effective December 1, 2013.
This permit addendurn dues not change the current expiration date for NCS000392.
Signed this day, November 21, 2013.
for Tracy Davis, P.E., Director
Division of Energy, Mineral, and Land Resources
By the Authority of the Environmental Management Commission

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality
January 25, 2007
DAK AMERICAS - CAPE FEAR PLANT
ATTN: PENNY MAHONEY, OR SUCCESSOR
PO BOX 2260
LELAND, NC 28451
Subject: NPDES Stormwater Permit Renewal
DAK Americas - Cape Fear Plant
Permit Number NCS000392
Brunswick County
Dear Permtttee:
Your facility is currently covered for stormwater discharge under NPDES Permit NCS000392. This permit expires
on April 30, 2007. North Carolina Administrative Code (15A NCAC 2}1.0105(e)) requires that an application for
permit renewal be filed at least 180 days prior to expiration of the current permit. In order to assure your continued
coverage under your permit, you must apply to the Division of Water Quality (DWQ) for renewal of your permit.
To make this renewal process easier, we are informing you in advance that your permit will be expiring. Enclosed
you will find an individual permit renewal application form, supplemental information request, and Stormwater
Pollution Prevention Plan certification.
Filing the application form along with the requested supplemental information will constitute your application for
renewal of your permit. As stated above, the application form must be completed and returned along with all
requested information by March 4, 2007 in order for the permit to be renewed by April 30, 2007.
Failure to request renewal by March 4, 2007 may result in a civil assessment of at least $500.00. Larger penalties
may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility without
coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and could
result in assessments of civil penalties of up to $25,000 per day.
If you have any questions regarding the permit renewal procedures please contact Mike Randall of the Stormwater
Permitting Unit at [phone], ext. 545.
Sincerely,
t� 161
Bradley Bennett, Supervisor
Stormwater Permitting Unit
cc: Central Files
St rmwatet'Permitting�Unit•F'iles�
Regional Office
One
NpnCarolina
turaly
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-161.7 Pltone [phone] Customer Service
Internet: www.ncwateMuality.ort, Location: 512 N. Salisbury St. Raleigh, NC 27604 Fax [phone]
An Equal Opportunity/Affirmative Action Employer — 50 % Recycled110% Post Consumer Paper

DAKAmericas
May 11, 2011
Nis. Jennifer Jones
Environmental Engineer
Stormwater Permittin., Unit
L NC DNR - DWQ
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: Draft NPDES Stormwater Permit No. NCS000392 !!� �
DAK Americas I_1_C — Cape Fear Site [lWW
3500 Daniels Road; N.E. M" 1 2
Leland, NC 28451 2�1�
Brunswick Countv DEMR - qy�
a a H &er,�,
Dear Ms. Jones:
DAK Americas received the draft NPDES stormwater permit on April 11, 2011. DAK is askin�0
that the draft permit be modified to drop the testing requirements for cobalt and for 1,4-dioxane.
The draft permit lists semi-annual analytical monitoring requirements for cobalt for Outfall 002.
While cobalt is used in DAK's manufacturing process, process wastewater that fray contain trace
amounts of cobalt arc discharged through the wastewater treatment plant, not throe<"ll a stormwa-
ter outfall. Attached are copies of EPA Form vhich were submitted to DENR as part of the
NPDES permit renewal application in 2006 for permit No. NCO000663 and in a request fora
permit modification in 2009. Both times, the level ofcobalt was less than 0.005 parts per million,
the lowest level at which cobalt can be detected. For this reason DAK requests that analytical
monitoring requirements for cobalt be dropped from the stormwater permit.
The draft permit also lists semi-annual.analytical monitoring requirements for 1,4-dioxane from
all stormwater discharge out[ails. Any chemicals from Out tal100I,which discharges the effluent
from the wastewater treatment plant, should be covered under the NPDES Permit No.
NC0000663. 'There is no patt j �yay for I A-dioxane to make its way into the stormwater dis-
ehar<red throe<,11 any of the stormwater outfalls. OutFatl 002 is permitted for the discharge of norl-
contact once through cooling water, cooling tower and boiler blowdown, water treatment fitter
backwash, coal pile runoff and stormwater. Outfall 003 is permitted for the discharge of' non -
contact once through cooling water, cooling tower and boiler blowdown and stormwater. The
only industrial activity in the drainage area for Outfall 003E is for the freshwater intake pond and
PUMPS. The only industrial activity located in the drainage area for Outfall 006 is railcar storage.
All other out falls (002A, 003A, 004, 005, 007, and 008) are undeveloped wooded areas. For
these reasons DAK requests that the analytical monitoring requirements for I A-dioxane be
dropped from the permit.
If you have any questions, please call me at [phone].
Sincerely,
El abeth Nike
Environmental langincer
Cape Fear Site • 3500 Daniels Road NE • P.O. Box 2260 • Leland, NC 28451
877-432-2766 (toll -free) • 910-371-4000 (phone) • 910-371-4179 (fax)
www.dakamericas.com

EPA ID Number (Copy from Item 1 of Form 1) Form Approved
Please type or print in the unshaded areas only
NCD047369046 OMB No, 2040-0086
Approval ex ires 8-31-98
Form U.S. ENVIRONMENTAL PROTECTION AGENCY
2 C APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
at� EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURAL OPERATIONS
NPDES ���'� Consolidated Permits Program
1. Outfall Location
For this outfall, list the latitude and longitude, (degrees, min.xxxx) and name of the receiving water(s)
Outfall
Latitude
Longitude
Receiving Water (name)
Number list
Deg
Min
Sec
Deg
Min
Sec
001
340
19,
05"N
780
01'
40"W
Cape Fear River
002
340
19,
28"N
780
02'
28"W
Machine Pond Branch
Cape Fear River
003
340
19,
14"N
780
03,
04"W
Unnamed tributary to Bay Branch
Cape Fear River
II. Flows, Sources of Pollution, and Treatment Technologies
A. Attach a line drawing showing the water Flow through the facility. Indicate sources of intake water, operations contributing wastewater to
the effluent, and treatment units labeled to correspond to the more detailed description in Item B. Construct a water balance on the line
drawing by showing average flows between intakes, operations, treatment units, and outfalls. It a water balance cannot be determined
(e.g., for certain mining activities), provide a pictoral description of the nature and amount of any sources of water and any collection or
treatment measures.
B. For each outfall, provide a description of (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary
wastewater, cooling water, and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received
by the wastewater. Continue on additional sheets if necessary.
1. Outfall No.
2. Operations Contributing Flow
3. Treatment
(list)
a. OPERATION (list)
b. AVERAGE FLOW
a. DESCRIPTION
b. LIST CODES FROM
(include units)
TABLE 2C-1
001
Discharges directly from the
2.0 MGD
Sedimentation (Settling)
1-U
wastewater treatment plant to the
Chemical Oxidation
2-13
Cape Fear River. NPDES
Coagulation
2-D
permitted discharge of treated
Activated Sludge
3-A
process wastewaters, sanitary
Aerated Lagoons
3-13
wastewater, and non-OCPSF
Stabilization Ponds
3-Cy
waters. The only stormwater
Discharge to Surface Water
4-A
discharged through this outfall
Aerobic Digestion
5-A
comes from stormwater co-
Flotation Thickening
5-.1
mingled with process wastewater
Land Application
5-P
I n sonic of the process areas and
Sludge Lagoons
5-T
stormwater from the sludge
application fields and sludge
pond. Stormwater from the
sludge disposal areas is collected,
treated, and ultimately discharged
through this outfall.
002
Non -contact once through
3.4 NTGD
Discharge to Surface Water
4-A
cooling water, cooling tower and
boiler blowdown, water treatment
filter backwash, coal pile runoff
and stormwater runoff are
discharged through Outfall 002.
003
Non -contact once through
0.2 MGD
Sedimentation (Wet Detention
1-U
cooling water, cooling tower and
Basin)
boiler blowdown and stormwater
Discharge to Surface Water
4-A
runoff are discharged through
Outfall 003.
EPA Form 3510-2C (8-90) Page 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items 11-A or B intermittent or seasonal?
❑ YES (complete the following table) ❑X NO o to Section !rr
1. OUTFALL
NUMBER
(list)
2. OPERATION(s)
CONTRIBUTING FLOW
(list)
3. FREQUENCY
4. FLOW
a. DAYS
PER WEEK
(specify
a
average)
b. MONTHS
PER YEAR
(specify
avera a
g)
a. FLOW RATE
in m d(specifywith
b. TOTAL VOLUME
units
c. DUR-
ATION'
(in days)
1. LONG TERM
AVERAGE
2. MAXIMUM
DA1LY
I
1. LONG TERM
AVERAGE
2. MAXIMUM
DAILY
III. PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
Q YES (complete Item 11I-8 ❑ NO (go to Section IV)
B. Are the limitations in the applicable effluent guideline. expressed in terms of production (or other measure of operation)?
0 YES (complete Item 1I1-C ❑ NO (go to Section IV)
C. If you answered "yes" to Item III-B, list the quantity which represents an actual measurement of your level of production, expressed in the terms
and units used in the a licable effluent guideline, and indicate the affected outfalls.
1. AVERAGE DAILY PRODUCTION
2. AFFECTED
a, QUANTITY PER DAY
b. UNITS OF MEASURE
t. OPERATION, PRODUCT. MATERIAL, ETC.
(specify)
OUTFALLS
(list outfall numbers)
1.288
MGD
Intermediates Monomers
001
0.264
MGD
Polyethylene Tere hthalate Fibers
001
0.448
MGD
Polyethylene Tere hthalate Resins
001
IV, IMPROVEMENTS
A. Are you now required by any Fedefal, State, or local authority to meet any implementation schedule for the construction, upgrading, or
operation of wastewater treatment equipment or practices or any other environmental programs which may affect the discharges described in
this application? This includes, but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance
schedule letters, stipulations, court orders, and grant orloan conditions.
❑ YES (complete the following table) X❑ NO o to Item W-B
1. IDENTIFICATION OF CONDITION,
AGREEMENT, ETC.
2. AFFECTED OUTFALLS
3. BRIEF DESCRIPTION OF PROJECT
4. FINAL
COMPLIANCE DATE
a. No
b. SOURCE OF DISCHARGE
a. REO-
UIRED
b. PRO-
JECTED.
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects
which may affect your discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned,
and indicate your actual or planned schedules for construction.
❑ MARK -X- IF, DESCRIPTION OF ADDITIONAL CONTROL PROGRAM IS ATTACHED
EPA FORM 3510-2C (Rev. 2-85) Page 2 of 4 CONTiNUED ON PAGE 3

EPA ID Number (Copy from Item 1 of Form 1)
CONTINUED FROM PAGE 2 NCD047369046
V.-INTAKE AND'EFFLUENT CHARACTERISTICS
A, B, 8 C: See instructions before proceeding - Complete one set of tables or each outfall - Annotate the outfall number in the space provided.
NOTE: Tables V-A, V-8, and V-C are included on separate sheets number V-1 through V-9. .
D: Use the space below t list any of the pollutants listed in Tables 2c43 of the instructions, which you know'or have reason to believe is discharged on
may be discharged from any outfall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical
data in your possession..
1. POLLUTANT
2. SOURCE
1. POLLUTANT
2. SOURCE
Acetaldehyde
Monomers manufacturing
X lene
Monomers manufacturing
Butyl acetate
Monomers manufacturing
VI. POTENTIAL DISCHARGES NOT -COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final
product or byproduct?
❑X YES list all suchpollutants below ❑ NO (go to Item VI-B)
Pollutants listed in Item V-C which are used as an intermediate or final product or byproduct were analyzed for and summarized in
Table V-C.
EPA FORM 3510-2C (Rev. 8-90) Page 3 of 4 CONTINUED ON REVERSE

CONTINUED FROM THE FRONT
�Vli" BIOLOGICALStTOXICITYisTESTING;DATA�i
y v.
�D6 you have any k Rowledg o w eason toy eliave that!a y�biofogical'.test;fnr acute;or chranii 'tozicity;has�beewmadeon anyof your discligrges-o�;ona gs.--N;
receiving;waterin relation ta: our drscharge�within th'e las€ 3 years' `�``�
IF fa_ 'tt
ask, 'r1'�" 'aE.,
,�,r. �. u x 7rw,ik r,{�u!+:r41- ' Na4`.%, t ,�w4 :x I�,l'$` '.f ' �� .�
''r -`�x •.4•'-'ai..;l�vl, r., .r.. w �+t- ,F..,'h� -:.:'z �Iu.....r,cM,��:.§":9 `.7�R .NDt o'"fo'Sectran`:,1%111,,''.
0.11
L^J _.n:..a.rtL...er__ i,YES,(rdentr ;fhe;tests anddescnbertherr." ur osebelow.�_,"+,s r,z.___(g
See Toxicity section of this application.
I.V,IfIitCONTRACTiA'NAI�YS.IS INFORMATION r T' A `
W..,.., ,...,�
e anaI— s reported rn fterii�U perfcinned:!?y a cant�actila6o�afbryor lm? Were anyof tli
;.� �'..W ®rdNOgoffo Sectron 1�
YI*S lrst hone
theaname, address andtele number tan
nal ibeacch,a(ioratom`bela?
A. NAME
3 ' `
l3. ADDRESS•
jBI I
W C, TEI!EPHONE
D. PQt_"I_'UTANTS%NALYZED
�s List
.�s,,.
a M
area:code;&rno.
Environmental Chemists
6602 Windmill Way
Wilmington, INC 28405
[phone]
See attached list
Maritech, Inc.
624 Tamco Road
Riedsville INC 27320
[phone]
Toxicity
NX- CERTIIFICATION �.
Jr that"this'°cf me and a!I`atfach iaerifs�werejprepari3d'under=rriy;"directionror._'super_vision in"'accordance'with"!a`system
o
�ce
desrgned;toga'ssuthaf,qualrfiersonnelrproperly■gaiiierandrevaluate`•ithe,nformatio subniitted. Based'oniny;inqurryoftheperso p rsans .4;
'ai..-A �R6 FF9A 1i.4' .�.^4fjBR� Ste• !:1 so nelj o "C,. Y�ik'a.lYf-g V `.r'gte the:in'LT,:IF ^RW �°,;, Mon,rr CN.: i 7
w'm�anage-„thesystern�,or;,,tlr�ose'persondrrectly'rp�onsrbte for¢gathensng the"fnformafron,the.rrifarmatron submrtted-isto3the'besf.pfamy
- -
,•.M--,ar,.�.�.s--x.v^z:=+'-
�knowledgeiandtielref'true?}�accurate; and�`completel;amtaware fhatathere are srgnrficanfpena{ties forsubmrftrng false rnformahonrncludinghe:
no,�
ossrbrlr ,of frne.and rm rrsonmenf,for,kwrn vfolatrons.,,,,'�
A. NAME & OFFICIAL TITLE (type or print)
B. PHONE NO. (area code no.)
Matthew Warrick, Cape Fear Site Manager
[phone]
C. SIGNATURE
D. DATE SIGNED
- 1Ao
(3-0 '
EPA FORM 3510-2C (Rev. 8-90) Page 4 of 4

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or EPA I.D. NUMBER (copy from Item 1 of Form 1) Qutfall 001
all of this information on separate sheets (use the same format) instead of completing NCD047369046
these oaaes. SEE INSTRUCTIONS.
V. INTAKE AND EFFLUENT CHARACTERISTICS continued from page 3 of Form 2-C
PART A - You must provide
the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
2. EFFLUENT..
3. UNITS
4. INTAKE (optional)'
1. POLLUTANT
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERMAVRG.
(specify if blank)
a. LONG TERM
VALUE
(ifavadawe)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
ifavailaMe
ANALYSIS
ANALYSES
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCE'NTRATI
(2) MASS
a. CONGEN-
TRA7[ON
b. MASS
.(s) 2 MASS
CONCENTRATION �)
ON
a. Biochemical Oxygen
66
624
28
313
13
141
252
lb/day
NA
NA
NA
Demand 800
ppm
b. Chemical Oxygen
574
5429
161
1769
574
5429
249
lb/day
NA
NA
NA
Demand COD
ppm
c. Total Organic Carbon
17.1
NA
NA
NA
NA
1
lb/day
NA
NA
NA
TOC
ppm
d. Total Suspended Solids
200
1748
65
725
28
307
252
lb/day
NA
NA
NA
TSS
ppm
e. Ammonia (as N)
.3
3
.6
7
.3
3
12
ppm
lb/day
NA
NA
NA
f. Flaw
Value
3.323
Value
1.767
Value
1.387
Continuous
MC�D
Value
NA
recording
NA
g. Temperature (winter)
Value 21
Value 18
Value 16.6
62
oC
Value
NA
NA
h. Temperature (summer)
Value
Value
Value
Value
NA
31
29
27.6
64
Qc
NA
Minimum
Maximum
Minimum
Maximum
i. pH
7.7
$
7.7
8
252
STANDARD UNITS
PART B - Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you
mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitation guideline, you must provide the results of at least
one analysis for that pollutant. For other pollutants for which you: mark column 2a, you must provide quantitative data or an explanation of their presence in your
dischar e. Complete one table for each outfall. See the instructions for additional details and re uirements.
1. POLLUT-
2. MARK W
3. EFFLUENT
4. UNITS
5. INTAKE o tional .
e. SE.
e, BE -
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
ANT
ANT AND
(specify if blank)
CAS NO. (if
LIEVE
0
L[EVE
GAB-
VALUE
(favaiaWe)
(Aavairable)
d. NO. OF
AVERAGE VALUE
b. NO. OF
CONCCENTRA
(2)hIA55
11)
CONCENTRATION
( 2WAS5
a.CONCEN,
TRATION
b-MASS
available
PEENT•
SENT
(I) 2)MASS
CONCENTRATION (.
ANALYSIS
cavrt%'-rlrunaa Ixl�u55
ANALYSES
TION
..
... ..
..
-
a. Bromide
❑
NA
NA
NA
NA
1
MG1L
LB/DAY
NA
NA
0
(24959-Fi7-9
.067
.004
b. Chlorine,,
Total Residual
ElX
<.200
<4.0
<.200
<4.0
<.200
<4.0
23
PPM
LBIDAY
NA
NA
0
C. Color
❑
X
40
NA
NA
NA
NA
NA
1
pcu
NA
NA
NA
0
d. Fecal
Coliform
❑
319
NA
319
NA
24
NA
13
#1100 ml
NA
NA
NA
0
( Fluoride
16984-48s)
X❑
0.3
.019
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
f. Nitrate -
Nitrite (as lv)
0
❑
28.1
366.3
28.1
366.3
8.1
94.2
12
PPM
LB/DAY
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT
Outfall 001
1. POLLUT-
2. MARK 'x'
3. EFFLUENT
4. UNITS
5. INTAKE (optional).
•. BE-
B. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
ANT AND
(specify if blank)
CAS NO. (if
LIEVE
LIEVE
VALUE
fdavaiable)
(ifavailable)
d. NO. OF
AVERAGE VALUE
b. NO, OF
fU
CONCENTRA
42) MASS
I1)
CONCENTRATI
42) MASS
a. CONCEN-
TRATIO14
b. MASS
available)
PR
ENT
SENT
0)
CONCENTRATI t2) MASS
ANALYSIS
0)
CONCENTRATI 42) MASS
ANALYSES
PON
ON
ON
ON
g. Nitrogen,
Total Organic
❑
30.1
392.4
30.1
392.4
7.7
20
12
PPM
LBIDAY
NA
NA
0
as N
h. Oilandand
Grease
❑
X❑
<5
<,325
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
I. Phosphorus
(as P). Total
[]
6.9
76.5
6.9
76.5
2.2
22.9
12
PPM
LBIDAY
NA
NA
0
7723-14-0
j. Radioactivity
(1) Alpha,
Total
❑
0
5.1
NA
NA
NA
NA
NA
1
pCi1L
NA
NA
NA
0
(2)tal Beta,
To
El10.2
NA
NA
NA
NA
NA
1
1
pCi1L
pCi1L
NA
NA
NA
0
(3)tal Radium,
To
❑
<1
NA
NA
NA
NA
NA
NA
NA
NA
0
(4) Radium
226, Total
❑
X
❑
<1
NA
NA
NA
NA
NA
1
p Ci1L
NA
NA
NA
0
k. Sulfate (as
$04)
Q
❑
11
169.2
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
14808-79-8
I. Sulfide
as S
❑
Fxj
0,01
.154
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
M. Sulfite (as
S03X
❑
"
<0.1
<1.54
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
14265-45-3
n. surfactants
X
❑
.059
.908
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
0. Aluminum,
Total
❑X
❑
.269
4.139
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7429-90-5
p. Barium,
Total
❑
O
10.005
<0.077
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-39-3
q. Boron,
Total
❑
.013
.200
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-42-8
r. Cobalt,
Total
E]
.487
7.494
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-48-4
s. Iron, Total
( 7439-89-4)
El.007
1 .108
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
t. Magnesium,
Total
❑
12.6
193.9
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-95-4
u. Molybdenum,
Tolal
❑
.007
.108
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-98-7
v. Manganese.
Tolat
❑
.086
1.323
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-96-5
w, Tin, Total
7440-31-5
❑
F
<0.05
10.769
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
x. Titanium,
,
Total
❑
Q
<0.01
<0.154
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-32-6
EPA FORM 3510-2C (Rev. 8-90) Page V-2 CONTINUE ON PAGE V-3

CONTINUED FROM PAGE 3 OF FORM 2-C
EPA I.D. NUMBER (copy from Item i of Form 1) OUTFALL NUMBER
NCD047369046 1 001
PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GCIMS fractions you must test for. Mark "X" in column 2-a for all such GCIMS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfaffs, and non -required GC/MS
fractions), mark "X- in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe Is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant. If you know or have reason to believe it will be
discharged In concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinilrophenol, or 2-methyl-4, 6 dinitrophenot, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge In concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for
additional details and requirements.
1. POLLUT-
2. MARK 'x'
3. EFFLUENT
(57) UNITS
5. INTAKE (optional
..
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
(57) LONG TERM AVRG.
-
(57) LONG TERM
ANT AND
(specify if blank)
ING RE-
LIEVED
LIEVED
(ifavalable)
VALUEd.
NO, OF
AVERAGE VALUE
b. NO. OF
CAS NO. ( If
QUIRED
PRE -SENT
ABSENT
rfava'able)
ANALYST
ANALYSE
available)
S
(1)CONCLNT-
RATION
(2)MASS
(1)CONCENT-
RATION
(2)MASS
(1)GONCENT-
RATION
(2)MASS
S
a.
CONCEN-
b. MASS'
(1}
CONCLNTR4
(2)MASS
TRATIRN
TION
METALS, CYANIDE, AND TOTAL PHENOLS
1m. Antimony,
Total
X❑
❑X
❑
.148
2.277
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-36-0
2M. Arsenic,
total
❑
0
<0.002
<0.031
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-38-2
3M. Beryllium,
Total
X❑
❑
0
10.001
<0.015
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-41-7
4M. Cadmium,
Total
X❑
❑
❑X
<0.001
<0.015
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-43-9
5M Chromium,
Total
X❑
❑
❑X
<0.005
0.077
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-47-3
6M Copper,
Total
X❑
^1
El0.001
0.008
.001
.008
.001
.006
5
PPM
LBIDAY
NA
NA
0
7440-50-8
7M lead, Total
X❑
❑X
❑
031
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
(7439-9P-1)
.477
8M Mercury,
Total
❑X
❑
X❑
<0.0002
<0.003
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-97-6
9M Nickel,
Total
❑X
❑X
❑
.012
0.185
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-02-0)
10M Selenium,
Total
X❑
❑
❑X
<0.005
<0.077
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7782-49-2
11 M Silver,
Total
Q
❑
❑X
<0.005
<0.077
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-22-4
12M Thallium,
Total
❑
<0.001
<0.015
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-28-0
13M Zinc,
Total
❑
.026
0.400
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-66-6
14M Cyanide,
Total
X❑
❑
❑X
<0.005
<0.077
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
57-12 5
15M Phenois,
Total
XL�
XC_
❑
.147
2.262
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
2,3,7,8-Teira-
DESCRIBE RESULTS
chlorodibenzo-
❑
❑
NA
P;pioxin
1764-01-6)
EPA FORM 3510-2C (Rev. 8-90) Page V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfall 001
1.'POLLUT
_ = 2.MARK X
3'.EFFLUENT
4:.UNITS :
5: INTAKE(o tiona!
TEST.,;:
,-;b:.BE ,.
;.;c BE _,.�.6
;G-�.a..MAXIMLIM.DAILY .c:,
6._MAXIMlfM,30,DAY,VALU£
,_c,LONGTERMAVRG _�.
_
ra. LONG:TERM
-- via
ANT�AND r
:'., S eCif �f.tj�ank
i p.
..CASNNO
-1NGRE
LIEVEp :.IIEVED
—.
VALUE' �'`."flavadaole)'VAWE"
�:
.,
'_.
d. NO:OF
-:'
-
'AVERAGE.VALUE
b: NO OF
fif"
-'''OUIRED_..
.PRE -SENT::
..ABSENT
ifavailable
.ANALYST
:.
-"ANALYSE
«-c'�... RAF10N
_.._. ..._.;
",.(2)MASS:rt,
".
F.(,)CONCEN7
- -:r,
RATION
:::_ :.::.;_. ,.
(2j"SS :x.:
;:(1).CONCENT,.-_:
RATION
'."
- 2 MA55.
:. ()
�
":-$
.
._ a. '.- _
C E
:. b. MASS
:zts.
.�.
-_l.-::-°11)CONCENT
1.: '+ ,'
-:.=.
(11..:__-*,
2-MASS
ONT
-
.5 V.-
:.a.
�.•-•,.hn-a.r.?x;14'
..,...
:-
.r.:.:'E.,-"`-%' ":si`
«.. °;'... .�
.'s
Ks'".' -=
,5, .y,x
::. :..
-:sc.>.,.
-
`'"
-
.CON
�: TRA ION}
OIN4TRA
-GCIMS", VOLATILE COMPOUNDS"
ry
=oz-a)
El0
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
- e
2V AWk nitnlle "E
{ta7 i31)
❑
FXI
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
3v 3�a
❑
x
<1 A
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
:AV. ais{ChWso-'__;::+
ymetltyl)Ethet (Sd2-.
0
❑
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
1
sv a o ,won
(7szs2)=
❑
❑X
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
6V Carbon
..Felradiollde� '.
❑
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
Ssz3s1
Iv, chlnmisenzene' _
n
❑
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
;eV Chlo_mc
Prb
0
❑
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
BV: Chlaoathena"=
(75-OCO) T.�.'.--"
El
FXI
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
,.
wthyh
❑X
❑
0
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
770.75-8==
11V Ghlorotorm
,(sr�crr3)
❑
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
: 12V OKt,loro-
t.e�hane
❑X
El
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
75-27d H-
' , 3v Dichloro-
-dn omelhane q,;
❑
X
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
:. 14V 11-Dchloro-.
❑X
El
❑X
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
T5-27 3 _:''.
(75
15V , 2-Dichlo—,
�ena�
❑
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
; 1(iV 3 t-0ichlo of
❑X
❑
FXI
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
Oichbro xk
❑
❑
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
oroayle�e =:
El<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
. 542 7S8 `:....
- 19V EthylhbnZunb �.
(10041-4
❑
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
2OV Methyl
7 � -
Elrxl
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
21V Methyl."
7 ��3 "
❑
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
N C D 047369046 1 001
1. POLLUT-
2. MARK W
3. EFFLUENT
4. UNITS
5. INTAKE (optional
a. TEST-
b. BE.
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. GONG TERM AVRG.
a. LONG TERM
ANT AND
(specify if blank)
CAS NO. (if
ING RE-
LIEVED
LIEVED
VALUE
(d avaeaue)
VALUE
it available
d. NO. OF
ANALYSI
AVERAGE VALUE
b- NO. OF
OUiRED
PRE-
ABSENT
ANALYSE
(1(CONCENT-
RATION
(2)MASS
(1)CONCENT-
RATION
(?)MASS
(1)CONCLNT-
RATION
(2)MtASS
S
e.
CONCEN.
b. MASS
available)
SENT
111
CONCENTRATI (2)MASS
$
TRATIO N
ON
GC/MS - VOLATILE COMPOUNDS (continued)
eerr
V. Y 22 Mylena
22e
L
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
75-0&2
23V. 1,1,2,2•TeL.
Ctrlomeuh ep9-
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
3&5
ich
yleneroo-
❑
0
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
,27-1&S
(108a&-3)ne
<1,0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
26V, 1,2-Treee-
DGhbNelhytefre866
15&
❑
1
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
D
2TVo.1.1,1 �d
❑
❑X
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
71-ss.s
2hlo 1,ne 2-1Y-
chbroeihn
❑
❑
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
7&00-5
2W. TriWom-
.Lhyi ne
❑
❑X
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
"1-0
30V. TkWro-
,_remelhano
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
7s-6o-4
-31V. Vinyl Chloride
(7-1014)
X❑
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
GCIMS FRACTION - ACID COMPOUNDS
1A. 2-
�7phon0l
�
❑
X❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
- 2A. 2,4'OIchbro
0.1
❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
ppht l •Oimelhy�
❑
❑
NI
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
t D5 87-9
4A. 4,6-�irdrPQ
-CA
0
❑
0
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
SA. 2,4-Oinilro-
ph
0
❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
al5
BA. 2-Nitro-phenol
(8&7°.r5) -
❑
x
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
7A. 4.N'amprernl
(100-02-7)
0
El<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
BA. P�rroro-Ml-
re
❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
%A. Penh
ct
❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
87-8&5rbrMphemi
10A. Phenoi
t1o0-95-2)
❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
chbmpherlW
<5.0
<0.077
NA
NA
NA
NA.
1
PPB
LBIDAY
NA
NA
0
86-06-2
EPA FORM 3510-2C (Rev. 8-90) Page V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfal 1001
1. POLLUT-
2. MARK X
-3. EFFLUENT :_,.;. —
4 UNITS, :.
5 :INTAKE' o bona!
a TEST,.:..
- ..b. BE
.,c. BE- -
a, MAXIMUM. DAILY .,
b. MAXIMUM 30 DAY, -.
c,c. LONG TERM AVRG. :.::_
ai.LONG TEftM'<
ANT<AND
�Sp2Clfy !f blank)
CAS NO. if.
-. ING RE-
LIEVED
'. LIEVED
VALUE'
VALUE'
eVALUE
d. NO.:OF
AVERAGE VALUE
'b: NO. OF':.
..
GUIRED::.;.
PRE -SENT'
--:ABSENT-
- -
---'FfavaiaWe
ffavailabfe
ANALY51
-
`.:ANALYSE-.
f11 CONCENT
RATION
'_:.- - _ . .:.
:. {2) MASS �:
(1)CONCENT;
RATION -
: ,_: _.-.. �..�
f2) MASS ._ -
-
f1)CONCENT-..
RATION
;..: -y y.
-. (il MASS -
$;'
.-, a -
.. "r«..:..,.
b MA$$
>..aYi37Ii3bIB
I7) _
CONCENTRATI . f21
3--`;
`S
;
"TRATION`
f
GCIMS:FRACTION - BASE/NEUTRAL COMPOUNDS
16 Acenphlhene --..
(83-32-9) -
<5.0
<0.077
NA
NA
ILIA
NA
1
PPB
LB/DAY
NA
NA
0
�.2B. Acenephlowu
(�g"l;;--.::-
[]
X❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
38. Anlhracene
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
- 4B Benndnm _
<5 0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
SB. Bonin fa) .
Anmracene[....
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
50,
, 58. eenza (a).:,.: :.
Pyre (so-32$) -.-_
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
78 3 4Ber,m- -
nuoiumfiarie�
X
❑
�
�
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
==98 Benxa Is�l
P rnene -s_
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
i 181 24 2 ,:::..
d W. Benin (k)
luorantheneEl
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
'-
108. Big (2-::.
Cilerneu exy)
I: Malhene i".t:."rf-.
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
„B: 8ie (2CMoro-"
'.:elhyl)E,her_-.,,--;,,.
❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
;cnwmsouiocsl)
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
Elhor 10ti60-1
,.138. Bie(2Cihyh _ ,
he.�)Phlaala--
❑X
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
14 B, 4.Bnn
-;:pnenylPyl ,;
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
-Ether 101553
-. I5B Butyl Benryl
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
-.t6B 2Chlaro-
Phlnnlene
El
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
rig 5&7 _'_ ..
178.CCWd
. phenyl Phenyl>;'.' -
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
Ether 70-72-3
05
=108 Chrys e:.
❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
10B. Dibeuo (ah)
:a,Chrecene:,q,-..
El
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
s37aa
`.20B,.t.2-DicfJoro-
❑
<5.0
<0A77
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
21 B..1,30iWoro-
b mom. .
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
1541-73-1)­
EPA FORM 3510-2C (Rev. 8-90) Page V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
N C D 04736904fi 1 001
1. POLLUT-
2. MARK'X'
3. EFFLUENT
4 if blank)
5. INTAKE (optional
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAX#MUM 30 DAY VALUE
(621) LONG TERM AVRG.
(621) LONG TERM
-
ANT AND
-ING RE-
LIEVED
LIEVED
VALUE
(davadable)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. (If
OUIRED
PRE -SENT
ABSENT(if
avaifablo
ANALYSI
ANALYSE
I1I RATIONNT
(2)MASS
(1)RATIONNT
(2}MASS
{1}RATIONNT
(2)MASS
S
aTRATIO N-
TRATION
b,MASS
available)
LN 2 MASS
CONCLNTHArI ( }
S
ON
GC/MS _ BASEINEUTRAL COMPOUNDS (continued)
226. 1,4.[Xchk ro-
b"ena
X❑
❑
X❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
Wd&7
236. 3,3'-Olcmfo
benzidine
X❑
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
9t-94-I
24B. Oielhyl
Phthalate
X❑
El
x<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
84-6G2
25B. Canelhyl
Phlharale
X❑
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
13,-t t-3
26B. Oi-N'Bulyt
Phthalate
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY 1
NA
NA
0
84 7L2
276- 2,4-Din'tro-
,alaene
X❑
El❑X
<5.0
<0-077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
12,-142
286,2,6-0iait-
,eluene
X❑
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
60B-2P2
29B- Oi-N-C CIA
P1dhalale
❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
„7-8"
30B, 1,2_fkphenyl-
Az
n
❑
bhydanrrazine)(m
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
,22£6-7
319, F€wranthene
I206.44-0)
❑
❑X
<5A
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
i0&73-7)
0
❑
Q
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
338. He=e
thlniobenzena
O
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
„&74-,
34B, Hex
rxn�naeia�
XD
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
67-68-3
35a. He:achlora-
cyclopentad,one
x
❑
X❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
77-0L
368. He
chloroelhane
x
❑
Q
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
s742-,
378. Indem (1,2.3.
c,d)Py-
❑X
❑
X❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
19&315
3813. 59-1) 11B
Q
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
39B. Napthalena
pl-26.3)
El<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
40B- Narobw-ene
(9aQ5-3)
Q
❑
x
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
d1B. N-NA-
sodimelh,lam e_
❑X
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
ez-7s9
429. N-Naraendi-N-
P,o
%a�rre
❑X
❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfall 001
1. POLLUT-
2. MARK'X'
2. EFFLUENT
3. UNITS
4. INTAKE (opt onal
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(Specify if blank)
CAS NO. i(
{
ING RE-
DUIRED
LIEVED
PRE -SENT
LIEVED
ABSENT
(if available)
VALUE
fWayai)ab)e
d. NO, OF
ANALYSIS
AVERAGE VALUE
b.00.OF
ANALYSES
available)
(1)CONCENT-
RATION
I2)MASS
(+)CONCENT-
RATION
12)MASS
(1)CONCLNT-
RATION
(2)MASS
a,CONCEN-
TRATION
b.MASS
(1)
CONCENTRA (2)MASS
TION
GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued)
438. N-Nd-
sodlphanylarNoe
❑X
❑
X❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
ea3M
440. Phenanthr
(85-0+-7
❑X
❑
X❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
45B. Pyr n
(,zam o}
Q
❑
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
a6B. t.2.a-Tri-
calorohenlena
Q
❑
0
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
12a 92-1
GC/MS FRACTION - PESTICIDES
(309A42)
❑
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
2P. a.BHC
(3+984-6 -
❑X
❑
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
- 3P. It Bhc
(3+¢asT)
❑X
❑
❑X
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
4P. y.BHC
f5"%'J)
Q
❑
0
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
5P, e-BHC
pl"&a)
❑X
❑
❑X
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
OP. ChbrGaae
+57.74-9)
X❑
❑
❑X
<1.0
<0.015
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
7P. 4A'-ODT
(5029-3)
a
❑
0
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
6P. a,a'-ODE
172s5-e)
X❑
❑
❑X
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
OP. 414'-DDD
(72-54$)
❑
❑X
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
lop, DwIddn
(60-57-+)
X❑
❑
❑X
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
t+P. a-Endp-ardtan
(115-29-7)
Q
❑
F
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
12P. p-ErKI mWfan
(115-29-7
❑
Q
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
13P, EndosWfan
sWlala
❑X
Elx
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
1631-67-e
. (izzaa)dn _
❑X
❑
❑X
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
15P. Erdan
Aldehyde
❑X
❑
❑X
<0A
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
7421-93-4
16P. Hepl.&Jar
(7&44-e)
❑
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-8 CONTINUE ON PAGE V-9

EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-6 NCD047369046 1 001
1 POLLUT
try z: nnaRK x,3:EFFLUENT
.�.1:
4' UNITS
5`:`INTAKE' o fional ,
LONGTERM
a. LON
ANT,AND
r �a TEST : b: BE �`c BE- '-
� ,a: MAXIMUM DAILY -b. MAXIMUM 30 DAY t- LONG TERM AVRG
',NQ_
�Sp@Cleft' if nh
CAS NO (!f;
. s,..
:--'
ING RE-: .-.. LIEVED ::,aLIEVED:?;
r
; -VALUE _ , -:: VALUE `' _ - VALUE,-0, d OF
ma.y... {lravada6fe : i
1ANALY51
t� .,
*wKAVERAGE VALUE 1
�:
b"NO OFF
ANALYSESsF
.f y�NY
Vdlfc7lJlB)".
i PREP ABSENT'
:SENT - .,._o _-
IR4.1
_ If°available > . _
:.=(1}CONCEN7
.{11 CONCENT-':5
-'-..v:f1YCONLCNT
:�
M455.
5.
a CONCEN,;.
-x._: '� �-'RATION�•-
{2JMAS$e-
•'i'CONCIZ
{2)MASS 'Y:^
RATION
.:12J ,.
n.
..€TRATION ;:
• b.MASS -
CONCENTRA
.
:� �...-.-�..* •i a� .-'9::.
x_.n-..-�¢:,. _a±..;-t
x*3, .`3:
_... „4g _�:.>
-'_T
TION::
:GCIMSlPESTICIDES'(coniinued)
r
:-77P Heptar3Jor '
L EPONdars'?z
�
❑
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
30P PCB 12k2
(534W21-9)
❑
❑X
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
19P PCB 1254 ,,:
f"°g7eatJ F' -'
❑X
❑
❑X
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
-28P PCB-7221s ®.
{„tw2a2J
El
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
21P PCU1232
In141 36-sy
❑
a
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
22P ; PCB 1248
I,2672:256�:
❑X
❑
❑X
<O.l
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
a23P PCB i260 :
I't6safiz-sy
_..,
❑X
El
0
<0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
($2674-1 �By2'16 W
❑X
El
❑X
< 0.1
<0.002
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
25P To o-plrena
ss-2y,
❑X
❑
❑X
<5.0
<0.077
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-9

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or EPA I.D. NUMBER (copy from Item 1 of Form 1) Outfall 002
all of this information on separate sheets (use the same format) instead of completing NCD047369046
these Daaes. SEE INSTRUCTIONS.
V. INTAKE AND EFFLUENT CHARACTERISTICS continued from page 3 of Form 2-C
PART A - You must provide
the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
2. EFFLUENT
3. UNITS
4. INTAKE o tional
1: POLLUTANT
(specify if blank)
a, MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
VALUE
(davaPable)
(ffavaifabfe)
d. NO. OF
AVERAGE VALUE
b. NO. OF
(t)
CONCENTRATI (�) MASS
ANALYSIS
(t) .
CONCENTRATI - (2) MASS
ANALYSES
-
(1)
CONCENTRATI
(2) MASS
It)
CONCENTAATI
(2) MASS
a. CONCEN-
TRATION�
b. MASS
ON
ON
ON
ON
Oxygen
Da. mand BOD
Demand BOD
6
185.8
NA
NA
NA
NA
1
PP m
lb/day
Y
NA
NA
NA
Chemical Oxygen
D
Demand GOD
49
1518
NA
NA
NA
NA
1
PP m
lb/day
Y
NA
NA
NA
c. Total Organic Carbon
TOC
18.3
567
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
d. Total Suspended Solids
TSS
67
1926
51.2
1230
41.4
1019
52
PP m
lb/day
Y
NA
NA
NA
e. Ammonia (as N)
<2
<6.195
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
Value
Value
Value
Value
NA
f. Flow
4.452
3.773
2.992
56
MGD
NA
g. Temperature (winter)
Value 21
Value 19.3
Value 19.1
12
DC
Value
NA
NA
h. Temperature (summer)
Value
Value
Value
Value
NA
30
27.8
27.3
15
oC
NA
Minimum
Maximum
Minimum
Maximum
i. pH
6.4
$.3
NA
NA
24
STANDARD.UNITS _
PART B - Mark "X" in column
2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you
mark column 2a
for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitation. guideline, you must provide the results of at least
one analysis for
that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your
discharge Complete
one table for each outfall.. See the instructions for additional details and re uirements.
1. POLLUT-
2. MARK'X'
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
-
1. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
ANT AND
(specify if blank)
CAS NO. (if
tIEV
o
0AA•
VALUE
(davadabia)
(rlavailabfe)
d. NO. OF
AVERAGE VALUE
b. NO, OF
It)
CONCENTRA
(2)MASS
lt]
CONCENTRATIO
(2)MASS
a. CONCEN•
TRAT(ON
b. MASS
available)
PRES-
ENT
SENT
(tl
CoNCENTRATIO (2)MASS
ANALYSIS
nF
eorveEem:hT wl flluss
ANALYSES
TION
N
Na.
(2 Bromide
24959-67-9
❑
0.145
4.491
NA
NA
NA
NA
1
PP m
lb/day
Y
NA
NA
b. Chlorine.
Total Residual
0
❑
0.630
13.9
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
H
c. Color
❑
X
10
NA
NA
NA
NA
NA
1
pcu
NA
NA
NA
0
d. Fecal
Caliform
X❑
El37
NA
NA
NA
NA
NA
1
Col/100 ml
NA
NA
NA
0
e. Fluoride
�sssa-as-a
❑
0A
12.390
NA
NA
NA
NA
1
PP m
lb/day
Y
NA
NA
0
f. Nitrato- --
X❑
Nitrite (as N)
1.11
31.1
1.11
31.1
0.63
16.3
12
ppm
lb/day
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-1 CONTINUE ON REVERSE

ITFM V.R CONTINUED FROM FRONT
Outfal1 002
1. POLLUT-
2. +MARK 'X'
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
"-BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
t. LONG TERM AVRG. VALUE
a. LONG TERM
ANT AND
(specify if blank)
CAS NO. (if
LIEVE
D
g.0E-
LIEVE
VALUE
(ifavagable)
(rfavailable)
d. NO. OF
AVERAGE VALUE
b. NO. OF
ANALYSES
(1)
CONCENTRA
(2F MASS
(t)
CONCENTRATI
(21 MASS
a. CONCEN-
TRATION
b. MASS
available)
PErES-
o AB-
SENT
(t)
CONCENTRATI (2) MASS
ANALYSIS
(U
CONCENTRATI (2) MASS
TION
ON
ON
ON
g. Nitrogen,
Total Organic
❑
1.7
52.657
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
as N
h. Oil and
Grease
❑
7
216.8
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
i. Phosphorus
(as P), Total
❑
0.1
3.097
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7723-14-0
j. Radioactivity
❑
FRI
<3
NA
NA
NA
NA
NA
1
pCi1L
NA
NA
NA
0
Tolpha,
tal
(2) Beta.
Total
❑
10.2
NA
NA
NA
NA
NA
1
pCi1L
NA
NA
NA
0
adium,
❑
<1
NA
NA
NA
NA
NA
1
pCi1L
NA
NA
NA
0
Total
226, Total
22 , Total
❑
X
❑
<1
NA
NA
NA
NA
NA
1
p Ci1L
NA
NA
NA
0
k. Sulfate (as
SO4)
❑
104
3221
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
14808-79-8
I. Sulfide
as S
❑X
❑
0.04
1.239
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
m: Sulfite (as
SO,X
❑
❑X
<1
31.0
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
14265-45-3
n. Surfactants
X
❑
0.057
1,766
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
o. Aluminum,
Total
❑
1.97
61.0
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
ra29-90-s
p. Barium,
Total
❑
0.036
1.115
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-39-3
q. Boron,.
Total
❑
0.104
3.221
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-42-8
r. Cobalt,
Total
❑
<0.005
<0.155
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-48-4
( Iron, Tota9-4)
7439 -89-4
❑
0.602
18.6
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
t- Magnesium,
Total
❑
6.12
190
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-95-4
u. Molybdenum,
Total
❑
0.015
0.465
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-96-7
V. Manganese,
Total
O
❑
0.174
5.390
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-96-5
w. Tin, Total
7440-31-5
❑
0
<0.05
<1.549
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
x. Titanium,
Total
1-1
<0.01T0,310
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440 -32�)
_
EPA FORM 3510-2C (Rev. 8-90) Page V-2 CONTINUE ON PAGE V-3

CONTINUED FROM PAGE 3 OF FORM 2-C
EPA I.D. NUMBER (copy from Item I of Form i) OUTFALL NUMBER
N C D047369046 1 002
PART C — If you are a primary industry and this outfall contains process wastewater, refer to Table 20-2 in the instructions to determine which of the GCIMS fractions you must lest for. Mark "X" in column 2-a for all such GCIMS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and non -required GC/MS
fractions), mark -X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant. If you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant Is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (a11.7 pages) for each outfall. See instructions for
additional details and requirements,
1. POLLUT-
2. MARK °x'
3. EFFLUENT
(sal UNITS
5. INTAKE (OPtional
a. TEST-
b. BE-
c, BE-
a, MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
(58) LONG TERM AVRG.
(58) LONG TERM
ANT AND
(specify if blank)
NO. if
ING RE-
LIEVED
LIEVED
(Javadaole)
VALUE
d. NO. OF
AVERAGE VALUE
b, NO. OF
CAS
QUIRED
PRESENT
ABSENT
ifavailable
ANALYSI
ANALYSE
available)
(1)
CONCENTRA (2)MASS
$
(1)CONCENT-
RATION
(2)MASS
(1)CONCENT-
RATION
(2)MASS
11)CONCENT-
RATION
(2)MASS
S
�,
CONCIEN-
b. MASS
RATI
TRATION-
TION
METALS, CYANIDE, AND TOTAL PHENOLS
1 m. Antimony,TolaI
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-36-0
2M, Arsenic.
Total
❑
[]
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-38-2
3M. Beryllium,
Total
❑
❑
XQ
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-41-7
4M. Cadmium,
Total
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-43-9
5M Chromium,
Totat
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-47-3
6M Copper,
Total
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
744a-So-B
7M lead, Total
❑
❑
n
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7439-92-1
SM Mercury,
Total
❑
El❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
T439-97-6
9M Nickel,
Total
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-02-0
14M selenium,
Total
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7782-49-2
11M Silver,
Total
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-22-4
12M Thallium,
Total
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-28 0
13M zinc,
Total.
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-66-6
14M Cyanide,
Total
❑
❑
XD
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
57-12-5
15ta Phenols,
LiElNA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
Total
UIIUAIN
2,3,7,8-Tetra-
DESCRIBE RESULTS
.itenzo-
❑
❑
NA
P-Diochlor
P-Dio
(1764xin
�]1-8)
EPA FORM 3510-2C (Rev. 8-90) Page V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfall 002
1. POLLUT-
2. MARK 'X'
3. EFFLUENT
4. UNITS
INTAKE a tional
a. TEST-
b. BE.
G. BE.
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
e. LONG TERM AVRG.
_ _5.
a. LONG TERM
ANT AND
(specify if blank)
ING RE-
LIEVED
LIEVED
VALUE
(ifavadabfe)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. if
OUIRED
PRE -SENT
ABSENT
ifavalfable
ANALYST
ANALYSE
(1)CONCTNT-
(1)CONCENT•
{1)CONCENT-
5
8.
b. MASS
available)
(1)
S
RATION
(2)MASS
RATION
(2)MASS
RAPON
(2)MASS
CONCEN-
CONCENTRA (2)MASS
TRATION
TION
GC/MS - VOLATILE COMPOUNDS
1V. Aadan � 107-
❑
02-8]
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2V, Acrybntrille
El
ElX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3V. Benzene
(71-4321
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
s (Chtoro-
`4V. V. Bi] Elhar (542•
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
B&1
SV. Brarlwform
❑
(75-25.2)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
6V, Ca bon
Telro&&orida
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
5&23-5
W. 04=benzene
❑
(IM90-7)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
-. 8V, Chlorodi-
hro=Z1t)Kene
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
124-48-1
W. Chlaraerhana
❑
as-a�)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
-1 OV. 2-C"o -
arhy wwI Elhw
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
11a75-B
11 V. ChIo.tovn
❑
(67-66-3)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
12V. Dichloro-
tromoethana
❑
El
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
75-27 4
13V, Dir Wd
dilluoromalhane
❑
❑
.
75-71A
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
14V. 1,1-Mchbo
orfwna
❑
❑
75-27-3
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
15V, 1,2-MOdoro-
emena
El
1o7-0fi-2
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1EV. 1,1-Dichhra
ethyl°"a
❑
7535-4
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
72 17V, -Olrhbro-
17V, i.e
❑
7Bsls
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
18V. 1,3-D&Aor
propylene
❑
542-75 fi
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
19V. EUryibenz
❑
(10"174)
❑
X
TVA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2W. MM1 l
sr9rn;da
El
ElX❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
74.839
21V. Itla"
hbnd
El
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(74.7-3
EPA FORM 3510-2C (Rev. 8-90) Page V-4 CONTINUE ON PAGE V-5

EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-4 NCD047369046 1 002
1. POLLUT-
2. MARK'X4
3. EFFLUENT
4, UNITS
5. INTAKE (optional)
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(specify if blank)
ING RE-
LIEVED
LIEVED
VALUE
(ifavadable}
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. (!(
QUIRED
PRE-
ABSENT
if available
ANALYSI
ANALYSE
11)CONCENT-
(2)MASS
(I)CONCENT•
(2)MASS
(I)CONCENT-
(2)MASS
S
a.
b. MASS
available)
SENT
(1)
(2)MASS
S
RATION
RATION
RATION
CONCEN-
GONCENTRATI
TRATION
�N
i
GCIMS - VOLATILE COMPOUNDS (continued)
22 V. Methylene
z
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
23V. 1.1.2.2-Tetre-
Chierne,hnne(79-
❑
34.5)
ElX❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
24V- Tetrachbro-
ahylena(
❑
127-18a
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
25V. Tnttlene
(IMW 3)
❑
❑
X�'j
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
29V, 1.2-Trgne-
OichWmelhylerle
El
El
F
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
150-60.5
27V. 1, 1, 1-Tri-
c,b,h roee�
❑
❑
XD
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7,-sse
28V. 1,1,2-Tn-
cNo m
❑
❑
X�
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
79oas
29V- TnchWro-
"�1a e
❑
79 01-6
❑
XQ
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
30V. Triclr Z
Iluom-4)hane
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
75-r-%
1
31V- Vuryl CNoMe
{75-01-4)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
GC/MS FRACTION - ACID COMPOUNDS
1A. 2-
_ Chlomphenol
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
9557-8
A. 2.4- 2picNoro-
ph.ml
❑
❑
❑X
120 632
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3A, 2,4-Dimethyl-
°'
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
106-87-9
aA. A,&pintro-0-
crew
El
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
534-52-1
5A. 2,4-Dneho-
❑
El❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(181' 51-2&5)
5A. 2-Mtro-O.W1
(W75-5)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7A. 4-Rt pllenol
❑
(1no-e2:7)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
8A_ P-Chbro-M-
C°tee'
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
s0-0-7
9A. Penta-
chlorophenol
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
B7-0&51
10A. Phenol
(10&05-2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
11A. 2.4,a-Trl-
''°°��'°'
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
ae-oaz
EPA FORM 3510-2C (Rev. 8-90) Page V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfall 002
1. POLLUT-
2. MARK'X'
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
a. TEST-
b. BE-
C. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(specify if blank)
ING RE-
LIEVED
LIEVED
VALUE
VALUE
VALUE
d. NO. OF
AVERAGE VALUE
b- NO. OF
CAS NO. if
QUIRED
PRE -SENT
ABSENT
W avadabla
if available ..
ANALYSI
ANALYSE
(1)CONCBNT-
(1)CONCENT-
(1)CONCENT-
S
a.
available)
(1)
S
RATION
(2) MASS
RATION
(2) MASS
RATION
(2) MASS
CONCEN•
b. MASS
CONCENTRATI (2) MASS
TRATION
ON
GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS
1 B. Acw+phlhene (V-0)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
28. A—"Wylerar
(2WV-B)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
313. ANttracene
�120-12-7)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
413. 9enzldine
{92-87-5)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
5B. Benz° (a)
Anlhracene
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
55-55-3
6B. eenry (e)
Py,aae(5a32-a)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
713. 3,4-9arry
tiueramn°"e
❑
2059&2
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
813, Be"zo ON)
Peryl�
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
191-24-2
9B. Berizo (k)
°°e
El❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(z�lntho7-os-9°°ra
109. Bis(2C'hl-
M.Ih.....h°xy)
Methane
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
111-91-1
1 S8. Bis (2-Chloro-
ethyl)Ether
111.414
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
12B. Bis (2-
ChIom1w I't)
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
er Eth10�&o661
130. Bis(2-Ethyl
heryl) Phthalate
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1,7-8t-7
14 B,4-13o
pth.,101.55
❑
❑
. Elh°r 101.55-3
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
155 Bulyt Benzyt
Phlhalele
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
SSBB 7
16B. 2-04oiu-
naphlh°lane
❑
❑
91-58-7
❑X
NA
NA
NA
NA
NA-
NA
0
NA
NA
NA
NA
0
11B. 4,ct,40 -
phenyl Ph -VI
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
Ether 7005-72.3
16B. Chrysene
❑
(21"1-9)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
196. Diheriza (a.h)
A"
❑
s3-7o-3 ...
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
208. 1.z-Blchlero-
e"e
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
es-so-t
218. 1,3-achloro-
❑
El❑X
NA
NA
NA
(541ia3 -73-,)
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
EPA I.D. NUMBER (copy from item 1 of Form 1) OUTFALL NUMBER
N C D047369046 1 002
1. POLLUT-
2. MARK'X'
3. EFFLUENT
4 if blank)
5. INTAKE (opt' nal
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
(822) LONG TERM AVRG.
(622) LONGTERM -
ANT AND
ING RE-
LIEVED
LIEVED
VALUE
(davapable)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. ( if
QUIRED
PRE -SENT
ABSENT
ifavallable)
ANALYSI
ANALYSE
(1)CONCENT.
(1)CONCENT-
(1)CONCENT-
S
a. CONCEN-
available)
(11
S
RATION
(2) MASS
RATION
(2) MASS
RATION
(2) MASS
TRATION
b. MASS
CONCENTA►.n (2) MASS
ON
GC/MS — BASE/NEUTRAL COMPOUNDS {continued}
22B. 1,4-Dlddero-
t,OM a
❑
OB 46-7
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
236. 3,3'-Dichiwo-
w ni°ine
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
24B, piethyl
P413, a1e
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
S4-Bfi2
256. Dimelhyl
Phthalate
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
131-11-3
26B_ IIIN-Butyl
htha
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(84- 4.le'e2
2713. 2.4-Oind—
tntrleoe
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
121-14-2
288. 2,B-Dintm-
t°I°e"a
❑
606.20-2
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
296. Di-n-Odyi
.Phthalate
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
117-84 0
30B. 1.2-Diphenyl-
Fryduazine(asAw-
benzene)
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
122�8-7
31B. Flwmnthene
❑
(20644-0)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3213. Fl—w
❑
(Bu-73-7)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
33B Hexer
ct1
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
74-1)
348. Hexer
chleivbutatliene
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
B7-BB9
35a. Heachfwo-
cyclnpertadiana
El
El
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
77a7 4
308. Hwa-
r3llomelhane
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
07-72-,
370. Ind—(1,2,3-
cd)P,'�en e
El
E83�3B-51
El
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
ma. laapho-ne
❑
(7"4.1)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3913, Naplhalene
❑
(91.20-3).
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
408, Wmbenz
❑
(WG6-3)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
418. N-Wt
s°a'amitre
El
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
sz�7s-methyls
428, N-Nafoadl-N.
PmWy ine
❑
❑
621,64.7
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-7 CONTINUE ON REVERSE

�7i7►IIRif] *1i01&0]TANt;IX;l:0]►tI
Outfall 002
1, POLLUT-
2. MARK'X'
2. EFFLUENT
3. UNITS
4. INTAKE (opt onal
a. TEST-
b, BE-
c. BE-
a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
c, LONG TERM AVRG.
a. LONG TERM
ANT AND
{Specify if blank)
ING RE-
LIEVED
LIEVED
(it available)
VALUE
d- NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. if
OUIRED
PRE -SENT
ABSENT(if
ova llable
ANALYSIS
_
ANALYSES
available)
(1)
i+ICONCLNT•
(1)CONCENT-
(1)CONCENT-
a.CONCEN-
b.MASS
RATION
2 MASS
(J
I
RATION
(2)MASS
RATION
(2)MASS
TRATION
CONCENTRA (2)&%SS
TION
GC/MS FRACTION - BASEINEUTRAL COMPOUNDS (continued)
438. N-N,lro-
sod[phenylamine
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
8630 6
448. Phenanthrene
(M-014
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
45B. P7rane
r29 99 9J
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
4913. 1,2,4-Tn-
dibrob"e
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
126d2-,
GC/MS FRACTION PESTICIDES
1 P, Aldan
(309-M2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2P-o.BHC
4319-84.6
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3P t4anc
{3t9-ti�7J
❑
El
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
4P:y-BHC
(5B 0-9)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
5P. &BHC
(319AB-8)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
eP. cnbma�a
6P.
❑
El
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7P. 4,4.-DDT
(50-29-3)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
aP- 4,4'-DDE
c7255-9)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
9P. 414'-DDD
(72-54-8)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
19P, Dieldnn
(sos7-n
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
11P. u-Endo-wllan
❑
(115-29-7)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
12P. II -Endo -sultan
❑
(115-2D-7
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
13P. Endaaullan Sulfate
So lfa
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
-A
14P. Lnddn
❑
(72-2")
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
15P, Endnn
❑
❑
X❑
NA
NA
NA
NIA
NA
NA
0
NA
NA
NA
NA
0
(74
7421-93 4
16P. Halxachbr
-
❑
J76-44-e)
Cl I
NA
NA
NA
NA
NA
NA
0
NA
NA
NA I
NA I0
EPA FORM 3510-2C (Rev. 8-90) Page V-8 CONTINUE ON PAGE V-9

EPA I.D. NUMBER (copy from Item 1 of Form 1)
OUTFALL NUMBER
CONTINUED FROM PAGE V-6
INCDO47369046
002
1. POLLUT-
2. MARK X
3. EFFLUENT
4. UNITS
5. INTAKE o fional
a• TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(specify 1f blank)
CAS(if
ING RE-
LIEVED
LIEVED
VALUE
VALUE
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. u7
ANALYSE:
QUIRED
PRE-
ABSENT
tf available
(if available)
ANALYSI
.NO.
available)
SENT
(1) CONCENT-
(1)RATIONNT
I1)RRAAFONNT
S
;a. CONCEN-
(11
-
-
RATION
(2)MASS
(21 MASS
I2)MASS
TRATION
b. MASS
CONT
( 21MAS5
t
OENTRA
GCIMS - PESTICIDES (continued)
17P. Heptacidar
❑
El
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(ExpxJde
10245 7-3
1024-
1BP, PCB-1242
(534e9-21-9)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
19P. PC8-1254
(11097-69-1)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
20P. PC13-1221
(11104-28-2)
El❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
21P. PCB-1232 -
(11141-1B-5)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
22P. PCB-1248
(12B72-29-6)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
23e. PCB-1260
(1100&82-5) :'
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
zaP. Pca-1a1B
(12e7an-10
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
25P. Tcs&W*ne
(WOO-35-2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-1 CONTINUE ON REVERSE

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or EPA I.D. NUMBER (copy from Item 1 of Form 1) Outfail 003
all of this information on separate sheets (use the same format) instead of completing NCD047369046
these pages. SEE INSTRUCTIONS,
V. INTAKE AND EFFLUENT CHARACTERISTICS continued from page 3 of Form 2-9
PART A - You must provide
the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
2. EFFLUENT
3. UNITS
4. INTAKE (opt! nal
1. POLLUTANT
(specify if blank)
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONGTERM
VALUE
(ifavaitable)
(ifavailable)
d. NO. OF
AVERAGE VALUE
b. NO. OF
(1)
ANALYSIS
[tl
ANALYSES
(1)
- a. CONCEN-
b. MASS
-
CODiCE'NTRATI
ICI MASS
CONCENTRATI
(2) MASS
(
x
CONCENTRATI (� MASS
TRATION
- CONCENTRATI 42) MASS
ON
ON
ON
ON
a. Biochemical Oxygen
<2
<2,769
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
Demand BOD
b. Chemical Oxygen
22
30.458
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
Demand COQ
c. Total Organic Carbon
5.9
8.168
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
TOC
d. Total Suspended Solids
<2
2.769
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
TSS
e. Ammonia (as N)
<0.2
<0.277
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
Value
Value
Value
NA
f. Flow
Value O 166
NA
NA
1
MGD
NA
g, Temperature (winter)
Value 20
Value 18.3
Value 18
12
aC
Value
NA
NA
h. Temperature (summer)
Value
Value
Value
Value
NA
29
24.5
24.2
13
oC
NA
Minimum Maximum Minimum Maximum
I. pH 6.6 7.6 NA NA 1 STANDARD UNITS
PART B - Mark "X" in column 2-a foreach pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you
mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitation guideline, you must provide the results of at least
one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your
dischar e. Complete one table for each outfall. See the instructions for additional details and requirements.
1. POLLUT-
2. MARK W
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
ANT AND
a. BE.
B. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
(specify if blank)
a. LONG TERM
CAS NO. (if
LIEVE
n
L1EVE
OAa-
VALUE
(Wavailable)
(ifavaifable)
d. NO. OF
AVERAGE VALUE
b. NO. OF
(1)
CONCENTRA
(2) MASS
(�y
CONCENTRATIO
(2) MASS
a.CONCEN-
TRATION
b-MASS
available)
PRES-
ENT
SENT
{I)
CONCENTRATIO (2) MASS
ANALYSIS
ill
CCNC�Tr T� q 01 1�55
ANALYSES
TION
N
N
a. Bromide
0.066
0.404
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
0
24959-67-9
b. Chlorine,
Total Residual '
❑
X❑
<0.2
0.277
<0.2
0.277
<0.2
0.277
30
ppm
lb/day
NA
NA
0
c. Color
Q
Q
10
NA
NA
NA
NA
NA
1
pcu
NA
NA
NA
0
d. Fecal
26000
NA
NA
NA
NA
NA
1
Co11100 ml
NA
NA
NA
0
Coliform
Fluoride
0.1
0,138
NA
NA
NA
NA
1
ppm
lblday
NA
NA
0
( 16984-48-8)
f. Nitrate-
.75
1-038
0.75
1.038
.383
.530
1
ppm
lb/day
NA
NA
0
Nitrite (as N)
1
EPA FORM 3510-2C (Rev. 8-90) Page V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT
Outfal 1003
1. POLLUT-
2. MARK 'X'
3. EFFLUENT
4. UNITS
5. INTAKE o tional
a, Br-
s. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONG TERM
ANT AND
(specify if blank)
CAS NO. (if
LIEVE
o
LIEVE
VALUE
(davarlat#e)
(iiavailahle)
d. NO. OF
AVERAGE VALUE
b. NO. OF
(t)
CONCENTRA
(�) MA55
[+)
CONCENTRATI
(2) MASS
a. CONCEN-
TRATIDN
tr. MASS
available)
PENT
oAs-
SENT
fl)
CONCENTRATI (2) MASS
ANALYSIS
fll
LONCENTRATI 42) MASS
ANALYSES
TION
ON
ON
ON
g. Nitrogen,
Total Organic
❑
0.4
0.554
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
as N
h. Oil and
❑
0
<5
<6.922
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
Grease .
i. Phosphorus
(as P), Total
❑
<0.04
0.055
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7723 14-0
j. Radioactivity
(1) Alpha,
❑X
<3
NA
NA
NA
NA
NA
1
pCi1L
NA
NA
NA
0
Total
(2) Beta,
❑
X
4.5
NA
NA
NA
NA
NA
1
pCi/L
NA
NA
NA
0
Total
(3) Radium,
El
0
<1
NA
NA
NA
NA
NA
1
p CK
NA
NA
NA
0
Total
(4) Radium
0
<1
NA
NA
NA
NA
NA
1
p Ci/L
NA
NA
NA
0
226, Total
k. Sulfate (as
So,)
❑X
❑
35
48.5
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
i 4808a9-8
I. Sulfide
❑X
❑
.01
0.014
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
as S
m. Sulfite (as .
SOA
❑
X❑
<0.1
<0.138
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
14265-45-3
n. Surfactants
❑X
❑
0.043
0.060
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
o. Aluminum.
Total
❑
0,147
0.204
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7429-90-5
p. Barium,
Total
❑
0,017
0.024
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7440-39-3
q. Boron,
Total
❑
0.042
0.058
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7440-42.8
r. Cobalt,
Total
❑
❑X
<0.005
<0.007
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7440-48-4
s. Iron, Total
X
❑
0.588
0.814
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7439=89-4
t. Magnesium,
Total
Fx_j
❑
2.76
3.821
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7439-95-4
u. Molybdenum,
Total
❑
<0.005
<0.007
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7439-98-7
Y. Manganese,
Total
❑
0.013
0.018
NA
NAF'N
NA
NA
1
PPM
LB/DAY
NA
NA
0
7439-96-5
W. Tin, Total
❑
<0.05
0.069
NA
NANA
NA
1
PPM
LB/DAY
NA
NA
0
7440-31-5
x. Titanium,
Total
El
<0.01
<0.014
NA
NA
A
NA
1
PPM
LB/DAY
NA
NA
0
7440-32-6
EPA FORM 3510-2C (Rev. 8-90) Page V-2 CONTINUE ON PAGE V-3

CONTINUED FROM PAGE 3 OF FORM 2-C
EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
NCD047369046 1 003
PART C — If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC1MS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and non -required GC/MS
fractions), mark "X' in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant. If you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. if you mark column 2b for acroleln, acrylonitrile, 2,4 dinitrophenol, or 2-methyt-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for. each outfall. See instructions for
additional details and requirements.
1. POLLUT-
2• MAIM[ IX'
3. EFFLUENT
(59) UNITS
5. INTAKE (Opt
onal
a. TEST.
b. BE-
c. BE-
a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
(59) LONG TERM AVRG.
(59) LONG TERM
ANT AND
(specify if blank)
ING RE-
LIEVED
LIEVED
(dava�"able)
VALUE
d. NO. OF
AVERAGE VALUE
- b. NO. OF
CAS NO. (if
QUIRED
PRE -SENT
ABSENT
lfavailable)
ANALYST
ANALYSE
available)
(11CONCENT.
RATION
(2)MASS
I1)CONCENT-
RATION
(2)MASS
(1)CONCENT-
RATION
(2)MASS
5
a.
CO NCEN-
b. MASS
(1)
CONCENTRA
(2}MASS
TRATIQN
TION
METALS, CYANIDE, AND TOTAL PHENOLS
1 m. Antimony,
Total
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-36-0
2M. Arsenic,
Total
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-38-2
3M_ Beryllium,
Total
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-41-7
4M. Cadmium,
Total
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-43-9
5M Chromium,
Total
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-47-3
6M Copper,
Total
❑
❑
XQ
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-50-8
7M lead, Total
❑
❑
DX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7439-92-1
8M Mercury,
Total
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7439-97-6
9M Nickel,
Total
❑
❑
nC
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-02 0
TOMalSelenium,
El
El0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7782-49-2
11M Silver,
Total
El
❑
XD
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-22-4
12M Thallium,
Total
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-28 0
13M Zinc,
Total
❑
❑
XO
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-66 6
14M Cyanide,
Total
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
TVA
0
57-12-5
Phenols,
El
El
IX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
Total
Total
DIOXIN
2,3,7,8-Tetra-
❑
❑ X
DESCRIBE RESULTS
chlonxlibenzo-
NA
P-Dioxin
(1764--01-61
EPA FORM 3510-2C (Rev. 8-90) Page V-3 CONTINUE ON REVERSE

rONTINIIFO FROM THE FRONT
Outfall 003
1. POLLUT-
2. MARK •X•
3: EFFLUENT
4. UNITS
5. INTAKE (opt nal
a. TEST-
b. FIE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(Specify if blank)
ING RE-
LIEVED ,
LIEVED
VALUE
(d avadable)
VALUE
d. NO. OF
AVERAGE VALUE
•b. NO. OF
CAS NO. if
QUIRED
PRE -SENT
ABSENT
if available
ANALYSI
ANALYSE
available 1
(11CONCENT-
(1)CONCENT•
(1)CONCENT-
S
a.
b. MASS
111
S
RATION
2 MASS
()
RATION
121 MASS
RATION
(21 MA55
CONCEN-
CONCENTRA 12j MA55..
TRATION
TION
GCIMS - VOLATILE COMPOUNDS
1 V, Aodan (f 07-
0�e1
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2V. Awy mVille
(107-13.11
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3V. Benzene
471-43-21
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
W. Bla (Chlolo-
mut")Etrw(542-
8&I
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
sV. Bromolonn
(75.25-2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
6V. Caroon
Telrec 58-2,r,5)
❑
El
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7V- Chlomb-o
(IWW7)
❑
❑
Fx_1
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
ov. Chlolodl
0
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
( 2=:hane
9V. Chloroethane
(75�M3)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1 VV. 2-0h01a-
elhyW4* Ether
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
f 1a75.s
11 V, Chlorolonn
(67.r�3)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
12V. DicNoro-
6fO11Oatha"
75.27-4
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
13V. Dit*l
dfluolm ethane
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(75.71-8
14V. 1,1-Dichloro-
�'.
❑
rs-z7-a
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
15V. 1.2-Dwhl r
ethane
El❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
07-06-2
16v. 1.1-Dichbro-
ethylene
❑
7535 4
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
17v. 1.2-Dlchk ro-
p°v'm
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
w7-5
i,3-Dirtka
1"W "e
El❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
sa2.75•s
19V. Elhylbenzene
(100-41-0)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2GV. Methyl
[3romWe -
El
ElX❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
74-ea-s-W-9
21v. Memyi
C1i1onde
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. B-90) Page V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
NCD047369046 1 003
1. POLLUT-
2. MARK 'X•
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(Specify if blank)
CAS NO. (!f
ING RE-
LIEVED
LIEVED
VALUE
(davadabte)
VALUE
ifavatI ble
d. NO. OF
ANALYSI
AVERAGE VALUE
b. NO. OF
Ql1IRED
PRE-
ABSENT
ANALYSE
(1)CONCENT-
(IICONCENT-
(1)CONCENT-
a.
b. MASS
(1)
(2)MAS5
available)
S
SENT
RATION
(2)MASS
RATION
(21MASS
RATION
(21MASS
CONCEN•
CONCENTRATI
-
TRATION
. ON
GC/MS - VOLATILE COMPOUNDS (Continued)
22 V. Methytere
h"fide
El
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7 2
23V. 1,1,2,2-Tetra
uranel79
❑
El0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
34-5
3a-s
24V. Tett chbro-
elhyle�(
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
127-11i-0
25V. T,9w
(ID"W-31
❑
❑
X
NIA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
26V. 1,2-Tra"s-
°iGhl"me,hyl—
,58 80.5
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
27V. t,t.t-7ri-
ch'°roAe
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
71-55-6
28V. 1,7,2-Tri-
°"e
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
79.OD-5
nV, Trictioro-
ahyle""e
❑
❑
XO
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
79-0
WV. TnCNoro-
11mm—thane
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
75844
3,V.Vi"yl Chloride
(75-014)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
GCIMS FRACTION - ACID COMPOUNDS
IA. 2-
Chlarophewl
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
95 57-8
2A. 2,4-0lcW-
0--d
❑
❑
X❑
NA
NA
NIA
NA
NA
NA
0
NA
NA
NA
NA
0
12o-sz-z
3A. 2,4-0n,,Ih*
phew'
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
,OS-87-9
4A. 4,6# "tso-O-
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1534 5z-1
34
2 5A. ,4-Oirvtro-
5A.
❑
❑
n
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
51-28-5
eA. z-NRro-phend
(as-7s5)
El
El
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7A. 4-Nho-phe l
(100-M-7)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NIA
NA
NA
NA
0
&A. P-CtJoro M-
cfe t
Cl
sl}sa7
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
SA, Pe d,
chlorophenol
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
87$8-8
,OA. Pheml
loe ss-2)
❑
1XI
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
11A. 2,4,6-T,$-
a11vMPheA°'
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
88-118.2
EPA FORM 3510-2C (Rev. 8-90) Page V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outtall 003
1::PdLLUT-
2. MARK x',:..
:_:.:..... 3 EFFLUENT '::
4. UNITS
5 INTAKE(optional),....:
!`a. TEST-.:
---, 6.8E
-
c. BE-
a: MAXIMUM DAILY
h MAXIMUM 30 DAY
c. LONG TERM AVRG
-:.-a.;CONG:TERM..
ANT AND
ECi !f rbiafliC
iSA fY J
'CAS-NO.;(if
AB5ENOT
VALUE' .
O
AVERAGE VALUE
. NO OF
A
,ouIRED
PRE --SENT
-
favaiable
if available
AN A Si
NALYSE._
available).,:.,:
,.
.:,
:.. r. '.
(1) b��.m...
pit i45
-.
- $ '-
:, ...:.:
41) CONCENT..
..:`
..(I)CONCENT
s`-;•- :-'
`�'
n,-::.5;
'-_
�_
•:.4 -<=
..::I7}CONCENT
RATIONa •;-[2}MPSS
.RATION*`
+-:?f2)MA35."!"
r -RATION
;12)A1ASS :?''
b. MASS
CONCENTRATE
—.*i__r
-
x-_T,
TRATION
„
- ON .
GCIMS"FRACTION BASElNEUTRAL COMPOUNDS
1B Aconphlh°ne -;
sB332,91-.:
El
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
,.28: Acenaphlyfene„,.
`120&96-8i -..: .:;:.:
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
30. Arthrarene
s1291za);'
El
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
43- Botawine
s92�7•s�,,;
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
5a Benzo (a) .
a AntNacene [' *_
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
56dS3 -.!;:'a- .
❑
I Pyrenu(50-3249).;
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
-76 34•Be�o- _
nuorsmhena
El
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
zos99 z -,
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
195.242 "ir' �'
"99-aerrzo(kl
"Flux mh°"e-�'"=`
❑
El
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
207-089
-106 Bie<2 -�
kieth thoMy)
Atemsn°�.'-.
❑
El
F
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
111-81-1 u:
11 B. IN. (2-Chloro-:.
elnyl)Elhe:..
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
12B. Bie (2- .
Chlgaoieopmpyl) ..
-Elhar
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
108-66=-'-
=38- B-s(2-Ethyl .
h yly Phlhalale ``.
El❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
" _14 13 4-Bo1=q-
phe ylP1
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
`Ether 101-55-3
- 158 auly, Bono
Phth l ,a °.
.,
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
AS-88-7:
1 fig ; 2-Chloro-
naphthalene
❑
❑
a
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7 91 5&7 ^>
578:-4-Chloro- -
phenyl Phenyl
El❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
Ether 1005-72a
19e clay�e
❑
El
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
19B Dlhenzo{ah)e
Arllhracene :,
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
53-7a3
- 20B 1 2 Dichluro- _.
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
9b561 .:
0
❑
❑
�X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(413
5 41-73 f
EPA FORM 3510-2C (Rev. B-90) Page V-6 CONTINUE ON PAGE V-7

EPA I.D. NUMBER (copy from Item 1 of Farm 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-6 1 NCD047369046 1 003
1. POLLUT-
2• MARK W
3. EFFLUENT
4 if blank)
5. INTAKE (optional)
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
(023) LONG TERM AVRG.
(a23) LONG TERM
ANT AND
CAS NO.
ING RE-
LIEVED
LIEVED
VALUE
{davadabfe)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
(if
QUIRED
PRE -SENT
ABSENT
ifavai)abfe)
ANALYSI
ANALYSE
HT-
(1)CTION
S])CONCENT-
(1)CONCE,4T-
s
a. CONCEN-
available)
(1)
5
(2)N7PSS
RATION
(2) MASS
,. RATION
(2)MASS
TRATION.
b- MASS
CONCENTRATI (2) MASS
ON
GCIMS — BASE/NEUTRAL COMPOUNDS (continued)
226. $,3DICh10 r
El
Da 457
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
238. 3,3'-Oldbro-
°
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
e1-s4. n
-1.11
24B. DIOMO
Phlhwate
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
acca-2
2513. DlmethA
Pnu,alele
❑
El
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
134-11-3
26B. Di-N-2u1y4
Phthalate
❑
a4-74-2
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2713. 2,4-0iretn
'0'uene
❑
121114-2
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
28B. 2,6-0inar
'°"°"°
❑
aaB 2(�2
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
298, Oi-N-Cctyl
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1117 0
17414-D
308.1,2-Oiphenyl- -
-hydraz;°e(-Am.
benzene)
❑
ElNA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
,22-s6-7
318. FWra"Ihene
-
❑
(206A4-0)
❑
IX-1
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
329- FI°o,ene
❑
(e0-73-7)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3313 Ff
G'T
❑
ElX❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
74-11ZB1B
l ia7d-,
340. Hess
chlemh°,adiene
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
e7-sa-3
359 Fi x chlor
��opei°ad1Bne
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7-a7a
W. Ha I
. chlomelha"e
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
fl7-72-,
378.: Imam (1,2,3-
m)P
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1fl3-39-5'3 )
El
(7a5a,>WPM-
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
39D. Nepihalene
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
40B. Ndrot� nzene
(sass-3)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
419, N44Sro-
so
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
.75-91ylarlune
s2ass
429. N-Nuoadl-N-
amine
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
fi21-fi4-7
(621-
EPA FORM 3510-2C (Rev. 8-90) Page V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfall 003
2. MARK X
2. EFFLUENT
3. UNITS
4. INTAKE (OPtional
1. POLLUT-
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(specify) if blank)
ING RE-
LIEVED
LIEVED
(if available)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. if
QUIRED
PRE -SENT
ABSENT
. ifava;table
ANALYSIS
_
ANALYSES
available)
IIICONCENT-
(1)CONCENT-
(1)CONCENT-
0.CONCEN-
b.MASS
0)
RATION
(2)MASS
RATION
(2j R1A55
RATION
(2IMASS
TRATION
CONCENTAA (2)MASS
TION
GC/MS FRACTION - BASEINEUTRAL COMPOUNDS (Continued)
-N N 438. clp-
ao8, .N^an 1Pe
El❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
8¢368
448. Phettanthrerse
(1�
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
ASB, Py*ene
(12&O0.0)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
D
488, 1,2,4-Try
dawobe ene
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
D
520-82-F
GCIMS FRACTION - PESTICIDES
1P. Aldnn
(309-00-2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2P. a-8HC
El(311I-8a6
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3P I-
S7
(319-85-7)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
4P. r6HC
(5"9-01
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
6P e8Uhc
(31 ��Hc
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
OP. Chlordane
(57-74-e)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7P_ 414'-DDT
(50-29-3)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
8P. 4,4'ADE
In-5�B)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
UP. 4 4,-DDD
(72-54-a)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
,OP_ Dieldrin
reo-s7-,s
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
11F1a-Endo-wllan
{7152a71
ID❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
12P. (4-E�n
(115-2a7
❑
❑
IX-1
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
13P. Endo"an
SWata
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
10314 8
14P. Endcin
(72-20-e)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
15P. Endnn
A1d21-B3-0a1�e
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
74
16P. Heptachlor
(764441)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-8 CONTINUE ON PAGE V-9

EPA I.D. NUMBER (copy from Item 1 Of Farm 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-6 1 NCD047369046 1 003
1. POLLUT-
2. MARK W
3. EFFLUENT
4. UNITS
5. INTAKE (opt nal)
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY
c- LONG TERM AVRG.
a. LONG TERM
ANT AND
(specify if blank)
CAS NO. (if
ING RE-
LIEVED
LIEVED
VALUE
i VALUE
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
ANALYSES
QUIRED
PRE-
ABSENT
if available
afavailable)
ANALYST
available)
(1)CONCENT-
RATION
(21MASS
{ f CONCENT-
)RATION
(21MASS
1 CONCENT-
)RATION
(2)MASS
S
aN-
TRATION
TRATIO
b. MASS
SENT
CONCENTRA (21MASS
FION
GC/MS - PESTICIDES (continued)
17P. H.V.. .,
E„�Iaa -
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
5024-57 -33
18P. PCB-1242
(530a21-9} .
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1W. PCB-1254
(I roa7-ag +)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
20P. Pce-1221
(11104.2&2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
21 P- PCB-1232
(11141-1&5)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
22P. PCB-1248
(12672-2ae)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
23P. PCB-1260
(11090-62-6)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
-24P_ PCB-1610
(12674-11.2) -.
❑
ElX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
25P. To.Wane
(aWI-35-2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-9

EPA ID Number (Copy from Item 1 of Form 1)
Form Approved
Please type or print in the unshaded areas only
NCD047369046
OMBo
o , e 040-0 8 31 5$
Form U.S. ENVIRONMENTAL PROTECTION AGENCY
APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
2Cj EXISTING MANUFACTURING, COMMERCIAL, MINING AND 51LVICULTURAL OPERATIONS
EPA
�0 Consolidated Permits Program
NPDES �
I. Outfall Location
For this outfall, list the latitude and longitude, (degrees, rnin.xxxx) and name of the receiving water(s)
Outfail
Latitude
Longitude
Receiving Water (name)
Number List
Deg
Min
Sec
De
:Min
Sec
001
340
19'
05"N
780
01'
40"W
Cape Fear River
002
340
19,
28"N
780
02'
26"W
Machine Pond Branch
Cape Fear River
003
340
19,
14"N
780
03,
04"W
Unnamed tributary to Bay Branch
Cape Fear River
II. Flows, Sources of:Pollution, and Treatment Technologies
A. Attach a line drawing showing the water flow throughthefacility. Indicate sources of intake water, operations contributing wastewater to
the effluent, and treatment units labeled to correspond to the more detailed description in Item B. Construct a water balance on the line
drawing by showing average flows between intakes, operations, treatment units, and outfalls. If a water balance cannot be determined
(e.g., for certain mining activities), provide a pictoral description of the nature and amount of any sources of water and any collection or
treatment measures.
B. For each outfall, provide a description of (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary
wastewater, cooling water, and storm water runoff; (2) The average flow contributed by each operation;: and (3) The treatment received
by the wastewater. Continue on additional sheets if necessa .
1.: Outfall No.
2. Operations Contribu ng Flow
'3. Treatment
(fist)
a. OPERATION (fist)
b. AVERAGE FLOW
a. DESCRIPTION
b. LIST CODES FROM
(include units)
TABLE 2C-1
001
Discharges directly from the
2.0 MGD
Sedimentation (Settling)
I-U
wastewater treatment plant to the
Chemical Oxidation
2-B
Cape Fear River. NPDES
Coagulation
2-D
permitted discharge of treated
Activated Sludge
3-A
process wastewaters, sanitary
Aerated Lagoons
3-13
wastewater, and non-OCPSF
Stabilization Ponds
3-G
waters. The only stormwater
Discharge to Surface Water
4-A
discharged through this outfall
Aerobic Digestion
5-A
comes from stormwater co-
Flotation Thickening
54
mingled with process wastewater
Land Application
5-P
in some of the process areas and
Sludge Lagoons
5-T
stormwater from the sludge
application fields and sludge
pond. Stormwater from the
sludge disposal areas is collected,
treated, and ultimately discharged
through this outfall.
002
Non -contact once through
3.4 NIGD
Discharge to Surface Water
4-A
cooling water, cooling tower and
boiler blowdown, water treatment
filter backwash, coal pile runoff
and stormwater runoff are
discharged through Outfall 002.
003
Non -contact once through
0.2 MGD
Sedimentation (Wet Detention
l-U
cooling water, cooling lower and
Basin)
boiler blowdown and stormwater
runoff are discharged through
Discharge to Surface Water
4-A
Outfall 003.
EPA Form 3510-2C (8-90) Page 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items II -A or B intermittent or seasonal?
❑ YES (complete the following table) — ' 0 IN o'to Section III)
1. OUTFALL
NUMBER
(list)
2, OPERATION(s)
CONTRIBUTING FLOW
(list)
3. FREQUENCY
4.,FLOW
a. DAYS
PER WEEK
(specify
average)
b. MONTHS
PER YEAR
(specify
average)
a. FLOW RATE
in m d
b. TOTAL VOLUME
s eci( with units
c. DUR-
ATI ON
(in days)
1. LONG TERM
AVERAGE
2. MAxWUM
DAILY
1. LONG TERM
AVERAGE
2. MAXIMUM
DAILY
III. PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply,to your facility?
❑X YES (complete Item III-B) ❑ NO (go to Section IV)
B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)?
❑X YES (complete Item IlLa. NO (go to Section IV)
C. If you answered "yes" to Item III-B, list the quantity which represents an actual measurement of your level of production, expressed in the terms
and units used in the applicable effluent guideline. andindicate the affected outfalls.
1. AVERAGE DAILY PRODUCTION
2. AFFECTED
a. QUANTITY PER DAY
b, UNITS OF MEASURE
c. OPERATION, PRODUCT, MATERIAL, ETC.
(specify)
OUTFALLS
(list outfall numbers)
1.288
MGD
Intermediates Monomers
001
0.264
MGD
Polyethylene Tere hthalate Fibers
001
0,448
MGD
Polyethylene Tere hthalate Resins
001
IV. IMPROVEMENTS
A. Are you now required by any Federal, State, or local authority to meet any implementation schedule for the construction, upgrading, or
operation of wastewater treatment equipment or practices or any other environmental programs which may affect the discharges described in
this application? This includes, but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance
schedule letters, stipulations, court orders, and grant or loan conditions.
YES (complete the following table) ❑X NO o to Item IV-S
1. IDENTIFICATION OF CONDITION,
AGREEMENT, ETC.
2. AFFECTED OUTFALLS
3. BRIEF DESCRIPTION OF PROJECT
4. FINAL
COMPLIANCE DATE
a. No
b. SOURCE OF DISCHARGE
a. REQ-
UIRED
b. PRO-
JECTED
B. OPTIONAL: You may attach additional sheets describing any, additional water pollution control programs (or other environmental projects
which may affect your discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned,.
and indicate your actual or planned schedules for construction. .
❑ MARK "X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAM IS ATTACHED "
EPA FORM 3510-2C (Rev. 2-85) Page 2 of 4 CONTINUED ON PAGE 3

EPA ID Number (Copy from Item 1 of Form 1)
CONTINUED FROM PAGE 2 NCD047369046
V. INTAKE AND EFFLUENT"CHARACTERISTICS
A, B, & C: See instructions before proceeding - C6hnplete one set of tables or each outfall - Annotate the outfall number in the space provided.
NOTE: Tables V-A, V-B, and V-C are included on separate sheets number V-1 through V-9.
D: Use the space below t list any of the pollutants fisted in Tables 2c-3 of the instructions, which you know or have reason to believe is discharged or
may be discharged from any outfall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical
data in your possession,
1. POLLUTANT
2. SOURCE
1. POLLUTANT
2. SOURCE
Acetaldehyde.
Monomers manufacturin
X lene
Monomers manufacturin
Butyl acetate
Monomers manufacturin
VI, POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final
product or byproduct?
YES list al! such pollutants below ❑. NO (go to Item V1-8)
Pollutants listed in Item V-C which are used as an intermediate or final product or byproduct were analyzed for and summarized in
Table V-C.
EPA FORM 3510-2C (Rev. 8-90) Page 3 of 4 CONTINUED ON REVERSE

CONTINUED FROM THE FRONT
VII. BIOLOGICAL -TOXICITY,TESTI NG DATA-�,­.
Do you have any knowledge or reason to'believe that any biological test for acute or chronic toxicity has been'rnade.on any of your discharges or on a! -
receiving water in relation to y"ou'-.r discharge -'­ within the last .3
YES fiden tiFy the s dejcdh6 their purpose'
below
See Toxicity section of this application.
re . a . n . y� of.the.an I sesTrep ortediri'lt6mV-pdrf6rni6dbya'66ntractlaboratory.or:cohsuftf . ng , firm
'Section 1) 41�tdl*l
:(fist e-,nameL,,acd ss,; t and releprionepumber ot,:ana .,I!dv:to, 4
�U4
Z
e eac �.tP. - a� N
QT- TW, C JELEPHONE-��I_�,�;�,77M
`q'i'D., POLLUTANTS -ANALYZED
t ?.!"j
W YM
Environmental Chemists
6602 Windmill Way
[phone]
See attached list
Wilmington, NC 28405
Florida Radiochemistry
Hoffner Ave., Suite 201
Services, Inc.
Orlando, FL, 32812
[phone]
See attached list
1316 S. Fifth St
Oxford Labs
[phone]
See attached list
Wilmington, NC 28401
624 Tamco Road
Maritech, Inc.
Riedsville, NC 27320
[phone]
Toxicity
-IX CERTIFICATIO
"I certify under,penally, of law thatsystem this docurrient and bll:att��7hr6e�nts�wers-,'prLpared-u-nder.'i7�k-directibn or supervi�i6n:in.accordance.,,.w4h,.aI
.
'desi�ned to assu��, that'qii�ii6d'�6i�q�4'�­ h­ " d d "t d 'o'­f.'th'e' p'ei'son or �ersons'.,�.
YL ather an evaluate the infba�66h 1submitte', Based oq.My 'P'qyy'
.-rope
who q. manage t a system or t ose -persons trec theJftrination 'subrhitt�d' h th e in6nnation, best, of
-li' f complete significant pena ies information,including Chef
knt5��)eag'6 And be e ac"cluirake, and omp ete,-,,,, 'am"a"w'a"rethat
'-�gessi&fity'of fi&��nd impns�nrnantstoiknowinviolations.'?_-'!`%l
A. NAME & OFFICIAL TITLE (type or print)
B. PHONE NO. (area code & no.)
Leroy Butler, Cape Fear Site Manager
[phone]
C. SIG RE
D. DATE. SlGt4ED_L
EPA FORM 3510-2C (Rev. 8-90) Page 4 of 4

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or EPA I.D. NUMBER (copy from Item 1 of Form I) Outfal 1001
all of this information on separate sheets (use the same format) instead of completing NCD047369046
these nacres- SEE INSTRUCTIONS.
V. INTAKE AND EFFLUENT CHARACTERISTICS continued from page 3 of Form 2-C
PART A - You must provide the results of at feast one analysis for every pollutant in this table. Complete one table for each outfall. See instructions
for additional details.
2. EFFLUENT
3. UNITS
4, ttVTAKE. optional
1. POLLUTANT
(specify If blank)
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
VALUE
(Wavadabla)
VALUE
d. NO. OF
AVERAGEVALUE
b. NO. OF
1fava blej
ANALYSIS
ANALYSES
CONCENTRATION
III MASS
CONCENTRATION
..
(2) MASS
CONCE'NTRATI
(2) MASS
a. CONCEN-
TRATION
b. MASS
CONCENTRATION (2) MASS
ON
a. Biochemical Oxygen
20J
368
10.5
154
6.5
105
251
lb/day
NA
NA
NA
Demand BOD
ppm
b. Chemical Oxygen
Demand COD
119
1,945
NA
NA
NA
NA
i
ppm
lb/day
NA
NA
NA
c. Total Organic Carbon
16.1
231.1
NA
NA
NA
NA
1
lb/day
NA
NA
NA
TOC
ppm
d. Total Suspended. Solids
48
822
23
343
12
201
251
lb/day
NA
NA
NA
TSS
ppm
e. Ammonia (as N)
0.1
2
0.1
2
0.1
2
12
ppm
lb/day
NA
NA
NA
f. Flow
Value
4.311
Value
2.5
Value
2.0
Continuous
MGD
Value
NA
recording
NA
g. Temperature (winter)
Value 23
Value 17.2
Value 16.8
62
cc
Value
NA
NA
h. Temperature (summer)
Value
Value
Value
Value
NA
32
30.5
29.0
64
C
NA
Minimum
Maximum
Minimum
Maximum
i, pH
7.5
8.4
7.5
8.4
251
STANDARD UNITS
PART B - Mark "X" in column
2-a for each pollutant you know or have reason to believe is present. Marie "X" in column 2-b for each pollutant you believe to be absent.-.-- If you
mark column 2a
for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitation guideline, you must provide the results of at.least
one analysis for
that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your
dischar e. Complete
one table for each outfall. See the instructions for additional details and requirements. 2
1. POLLUT-
2. MARK'X'
3. EFFLUENT
4. UNITS
5. INTAKE o tional >,
aIEVE
BIEYE
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONGTERM
ANT AND
(specify if blank)
CAS NO. (if
o
OAe-
VALUE
(lava➢able)
(ifavailable)
d. NO. OF
AVERAGE VALUE
b. NO. OF
[�I
CONCENTRA
(Z)IAASS
(t)
CONCENTRATION
(2)MASS
a. CONCEN.
TRATION
b. MASS
available)
PRES-
ENT
SENT
(1)
CONCENTRATION (2)MASS
ANALYSIS
ICI
coNMNTRAnm IaI"SS
ANALYSES.
TION
a. Bromide
24959-(37-9
❑
37.0
531.1
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
b. Chlorine,
Total Residual
❑
X
<0.100
<2.138
<0.100
<2.138
<0.096
<1.653
12
PPM
LB/DAY
NA
NA
'' 0
c. Color
❑
X
8
NA
NA
NA
NA
NA
1
pcu
NA
I NA
NA
0
d. Fecal
Coliform
❑
1,200
NA
420
NA
14
NA
15
##/100 ml
NA
NA
NA
0
o. Fluoride
❑
0.3
0.431
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
t6984-48-8
f. Nitrate- .
Nitrite (as N)
X
❑
❑
11.4
219.2
11.4
219.2
2.40
40.6
11
PPM
LBIDAY
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-1 CONTINUE ON REVERSE

ITFM V-R C0NTINI1Fn FROM FRONT
Outfal l 001
1. POLLUT-
2. MARK *X'
1 3. EFFLUENT
4. UNITS
5. INTAKE (optional):
+ BE -
a. "'
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
ANT AND
(specify if blank)
CAS NO. {if
LfEVE
LIEVE
VALUE
fr(avarl'abfe)
(if available)
d. NO. OF
AVERAGE VALUE
b. NO. OF
ANALYSES
to
CONCENTRA
(2)MASS
(I)
CONCENTRATI
(2)MASS
a. CONCEN•
TRATION
b. MASS
available)
PRES-
ENT
SENT
(t)
CONCENTRATI (2)MASS
ANALYSIS
(I)
CONCENTRATI (2)MASS
I
TION
ON
ON
ON
g. Nitrogen,
Total Organic
❑
14
265
14
265
5
85
12
PPM
LB/DAY
NA
NA
0
as N
h. Oil and
Grease
❑
<1
<0.144
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
i. Phosphorus
(as P), Total
❑
3.8
74
3.8
74
2.3
38
12
PPM
LBIDAY
NA
NA
0
7723-14-0
j. Radioactivity
Alpha,
❑
<3
NA
NA
NA
NA
NA
1
pCi/L
NA
NA
NA
0
Total
To
El
NA
NA
NA
NA
NA
1
pCi/L
NA
NA
NA
0
To)taleta
)Radium,
❑
FRI
0.8
NA
NA
NA
NA
NA
1
pCi/L
NA
NA
NA
0
Total
(4) Radium
❑
X
0.3
NA
NA
NA
NA
NA
1
P Ci/L
NA
NA
NA
0
226, Total
k. Su4tale (as
Soo)
QX
❑
74
1,062.1
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
14808-79-8
I. Sulfide
as S
❑
0
0.01
0.144
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
m. Sulfite (as
SOA
❑
0
<1
<14.35
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
14265-45-3
n. Surfactants
X
❑
0.043
0.061
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
o. Aluminum,
Totai
❑
0.103
1.478
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7429-90-5
p. Barium,
Total
❑
0.009
0.129
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-39-3
q. Boron,
Total
❑
❑X
<0.005
<0.072
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-42-8
F. Cobalt,
Total
❑
0.070
1.005
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
7440-48 4
10
S. Iron, Total 7439-89.4
El
[
<0.005
10,09
<0.005
1 <0.09
<0.005
<0.076
4
PPM
LB/DAY
NA
NA
0
t. Magnesium, -
Total
❑
8.01
115.0
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-95-4
u. Molybdenum,
Total
❑
X❑
0.005
0.072
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-98-7
v. Manganese,
Total
El0.059
0.847
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7439-96:5
W. Tin, Total
7440 31-5
❑
X❑
<0.05
<0.718
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
x. Titanium,
Total
El
<0_01
<0.144
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-32-6
EPA FORM 3510-2C (Rev. 8-90) Page V-2 CONTINUE ON PAGE V-3

CONTINUED FROM PAGE 3 OF FORM 2-C
EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
NCD047369046 1 001
PART C — If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 In the instructions to determine which of the GCIMS fractions you must test for. Mark "X" in column 2-a for all such GCIMS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and non -required GC/MS
fractions), mark "X' in column 2-b for each pollutant you know or have reason to believe is present. Mark -X" in column'2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the resuits of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant. If you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenal, or 2-methyl-4, 6 dinitrophenol, you must provide the results of al least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (att 7 pages) for each outfall. See instructions for
additional details and requirements.
1. POLLUT-
2. MARK'X'
3. EFFLUENT
(57) UNITS
5. INTAKE (opt onal
a: TEST-
b. BE-
c. BE.
a. MAXIMUM DAILY VALUE
b. MAXIMUM30 DAY VALUE
(57) LONG TERM AVRG.
(57) LONG TERM
ANT AND
(specify if blank)
CAS NO.
ING RE-
LIEVED
LIEVED
fit available)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
(if
QUIRED
PRE -SENT
ABSENT
ifavailable
ANALYSE
°ANALYSE
available)
(11
CONCENTRA (2)MASS
g
(1)CONCENT-
RATION
(2)MASS
(1)CONCENT
RATION-
(2)MA55
41)CONCENT•
RATION
(2)MASS
S
a.
NC
COEN-
b. MASS
TRATION-
TION
METALS, CYANIDE, AND TOTAL PHENOLS
1 m. Antimony,
Total
❑X
X❑
❑
0.16
2.297
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7440.36 0
2M. Arsenic,
Total
❑
❑X
<0.005
<0.072
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-38-2
3M. Beryllium,
Total
❑X
❑
0
10.001
<0.014
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-41-7
4M. Cadmium,
Total
❑X
❑
❑?l:
<0.001
<OA14
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-43-9
5M Chromium,
Total
❑X
❑X
❑
0.066
0.947
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-47-3
6M Copper,
Total
❑X
❑
0.028
0.502
0.028
0.502
0.013
0.232
4
PPM
LBIDAY
NA
NA
0
7440-50-8
7M lead, Total
(7439-92-1)
�
El
X0.005
<0.072
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
8M Mercury,
Total
❑X
❑
X❑
0,0002
0.00287
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-97-6
9M Nickel,
Total
X❑
❑X
❑
0.009
0.129
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-02-0
10M Selenium,
Total
X❑
❑
<0.005
<0.072
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7782-49-2
11 M Silver,
Total
X❑
❑
X❑
10.005
<0.072
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-22-4
12M Thallium,
Total
X❑
❑
X❑
<0.001
<0.014
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-28-0
13M Zinc,
Total
XD
❑X
❑
0.225
3,229
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-66-fi
14M Cyanide,
Total
X❑
❑
X❑
<0.005
<0.072
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
57-12-5
Phenols,
Total
X❑
❑
X❑
<0.010
10.1435
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
2,3,7,8-Tetra-
DESCRIBE RESULTS
chlorodibenzo
❑
ElNA
P-Dioxin
1764-0l -6)
EPA FORM 3510-2C (Rev. 8-90) Page V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfall 001
1. POLLUT-
2. MARK W
3. EFFLUENT
4. UNITS
5, INTAKE o bona!
a. TEST-
I b. BE-
C. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(Specify if blank)
CAS NO.
ING RE-
LIEVED
LIEVED
VALUE
{davadable)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
!f
QUIRED
PRE -SENT
ABSENT
fitavailabre
ANALYSI
ANALYSE
available)
(1)CONCENT-
RATION
{z]MASS
(1)CONCENT-
RATION
Iz)MASS
(t)CONCENT•
RATION
{2J MASS
S
a.
CONCEN-
b. MASS
11)
CONCENTRA (2) MASS
S
TRATION
TION
GCIMS - VOLATILE COMPOUNDS
02-Sjerr en{1Q7
Fv--i
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
2V. AerfkWlille
(107-13-1)
Ej
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
3V. fl eu e
(71-43.2)
❑
n
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
4v. HIS (Qitor-
methyl}Ethw(542-
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
ea ,
5V. Bnue "l
(75-25.2)
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
6V. Calton
ssaa,brid
X❑
❑X
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
7V. ChbroLenzene
(10s-9o-7F
x
F
<1,0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
SV. Chbrod,
euwm
Q
0
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
9V. Chbl thane -
r7soo-s>
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
16V, 2-Chloeo-
her
1-1elhyNinyt
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
lEl
„oas.s
11V_ Chbldd-
El
1.59
0.023
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
V doro-
Dkx "o
bmmoethane
❑
❑
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
rsv�
ltn Dic -flm
❑
❑
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
(75-71m,ethane
75-71-5
14V. 1,1-Dichloro-
ethane
❑X
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
75-27-3
15V. 1,2-Dlchbro-
es07o�2
❑
<1.0
<0.014
NA
NA
NA
ILIA
1
PPB
LBIDAY
NA
NA
0
WhIA ow�oro-
R
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
7535 4
acle�
<10
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
7&87-s
111V. 1,3-Dlddaro-
Pmpylene
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
542-75-6
19V. Ethylbe wo
(:EE-41-4)
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
20V. Mettryl
Er4o�g
<1,0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
21V. Methyl
Q
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
$3
EPA FORM 3510-2C (Rev. 8-90) Page V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
NCD047369046 1 001
1. POLLUT-
2. MARK W
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
a. TEST-
b. BE-
C, BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG.
a. LONG TERM
ANT AND
(specify if blank)
CAS NO. (!f
lNG RE-
LIEVED
LIEVED
VALUE
(davailable)
VALUE
ifavaltable)
d. NO. OF
ANALYSI
AVERAGE VALUE
b. NO. OF
QUIRED
PRE-
ABSENT
ANALYSE
(1)C-ONCENT-
RATION
(2)MASS
(1)CONCLNT-
RATION
(2)MASS
(,)CONCEIT-
RATION
(2)MASS
5
a.
CONCEN-
e. MASS
available
SENT
nr
CONCENTRATI`• (2)MASS
S
TRATION
ON
GC/MS - VOLATILE COMPOUNDS (continued)
22 V. Methylene
CNoride
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
75-0&2
23V. 1. 2-Tetre-
C
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
34-5h1aroethaneIn-
.thwa-ice
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
127-18-4
25V. Tolusoe
(10&88-31
Q
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
20V. 2-Trani
Diw,0..Ihy1ene
O
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
686 155
27V. 1,1,1-Tri-
chloroethne
❑
x❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
7,-55-e
28V. 1, 1.2-Tri-
1-1cJYoroelhane
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
- 76{145
edwe�
Elx❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
7s o, s
llwroree
❑
<1.0
<0.014
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
75-%4
31v,+Arrylchlor+ne
<
<0.014
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
GCIMS FRACTION - ACID COMPOUNDS
1A. 2.
CNarophanal
a
El
O
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
2A. 2.a-pidrlonr
°h,2aa
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
3A. 2,4-Dinlelhys-
phenol
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
SOS-8T-9
aBei6Drn(flo
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
53452-s
5A. 2,a-pintro-
p51 l
❑x
❑
x❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
6A. 2-Atr phenol
{a675-5)
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
7A. 4,Nitro-phenol
#106-02-7)
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
6craan� lcMoo-
❑x
❑
X❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
5&5P7
OA. Perva-
e�6o-s�
Q
❑
0
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
.10A. Phe [
{soe-s5.2)
❑
1XI
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
11A_ 2.4.6-r
apheml
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfall 001
1. POLLUT-
2. MARK •X
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
a. TEST-
b. BE-
c. BE.
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(specify if blank)
CAS NO.
ING RE-
LIEVEG
LIEVED
VALUE
VALUE
VALUE
d. NO. OF
AVERAGE VALUE
d. NO. OF
(if
QUIRED
PRE -SENT
ABSENT
lfavadable
ifava'ab;e
ANALYSI
ANALYSE
available)
{1)CONCLNT-
(1)CONCENT-
(1)CONCENT-
rJ
g;
(1)
RATION
(2) MASS
RATION!
(2) MASS
RATION
(2) MASS
CO NCEN-
b. MASS
CONCENTRATI (2) MASS
TRATION
GClM5 FRACTION - BASEINEUTRAL'COMPOUNDS
, B. Acenphl"_
(83-32-9)
❑
0
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
2B. Acenapldylene
(208-98-8)
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
313. Anthraoene
{120-12-7)
❑
x
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
- 46. Benndm
{92-W-5)
❑
x]
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
5B. 8enm (a)
Anthrstene
❑
❑
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
56�3
�a a 5042-8)
El<5.D
<DA72
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
D
7B. 3,4-13enno-
naoratnhene
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
2059&2
,.BB Benxa (9NI
p
V2",e
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
I9t-2a-2 _
93. Benno{k)
_Ehprenthene
❑
❑
❑
<5.0
<0.072
NA
NA
NA
NA
1
PP8
LBIDAY
NA
NA
0
zm ua9
108.8+s (a
Metha
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
,me"neao
111-91-1
11 B. Bis (2Chloio-
ethyl)Ethe,
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
444
126. Bis (2.
Cnloroiwpmpyl)
❑
<5.0
.07
<02
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
Ether ,oB-6a,
heBNgP^Ma� ie
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
1, 7-81-7
14 B. 4.13mt11a
Phenyl phenyl
El�
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
'Ether 101-55-3
158 Br474 BennyF
Ph,halste
❑
❑
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
95AB-7
76B. 2-Chbro-
- nephlhalene
❑
x]
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
915&7
17B. 4-C Od
Pherryl Phenyl
❑
Fx_1
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
Ether 7005-72-3
186. Chrysene
(216-01-9)
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
1913. Mbe (a,h)
Anlhm ne
1-1
X❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
gene-Oichbro-
❑
X❑
` 5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
ss-so-,
21 B. 1,3-Oichloro-
El<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
��} �
EPA FORM 3510-2C (Rev. 8-90) Page V-6 CONTINUE ON PAGE V-7

EPA I.D. NUMBER (copy from Item 1 of Form l) OUTFALL NUMBER
CONTINUED FROM PAGE V-S 1 NCD047369046 1 001
1. POLLUT-
2, MARK'X'
I EFFLUENT
4 if blank)
5. INTAKE o fional
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
(e2i) LONG TERM AVRG.
(e21) LONG TERM
ANT AND
iNG RE-
LIEVED
LIEVED
VALUE
(iavabble)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO, OF
if CAS NO.
(
QUIRED
PRE -SENT
ABSENT
if available
ANALYSI
ANALYSE
(1)CONCENT-
RATION
I2}MASS
11)CONCENT-
RATION
(2) tiU1S3
(1)CONCENT-
RATION
'(2) MASS
S
a.CONCEN-
TRATION
b. MASS
available)
(1)
CONCENfRATI (2) MASS
g
QN
GC/MS - BASEINEUTRAL COMPOUNDS (continued)
22B, 1,4-Oichlero-
��ena .
0
❑
Q
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
108-4G7
238. 3,3'-Dktlloro-
ce'lolne
❑X
❑
❑X
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
PNW.t.
hlhalate
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
ea•eaz
zsB. Oenetlly,
Plw�ate
❑X
❑
0
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
131-11-3
26B, DI-N-Butyl
Phthalate
X❑
❑
Q
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
84-74-2
27B. 2,4-D.WW
toluene
❑X
❑
X❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
,21-14-2
288, 2,&Dinuro-
toluene -
X❑
❑
X❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
8M2P2
P�a°>;te°"N
X❑
❑
X❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
17-U-0
306. 1,2-Olphenyl-
❑
bbet¢){aeAm-
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
,22m)
310. Flwranthene
(2.)
X❑
❑
❑X
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
32B. Flwrem
(8d73-7)
X❑
❑
❑X
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
338. H-r
chlorobanzena
X❑
❑
❑X
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
1174-i
34B. Hexat3&3
tad-
0
❑
X❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
Y-
toe"t
358. Hexarhlaro-
eyclopantadiena
❑X
ElX❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
77-07-0
38B. Hexa
7,am�nana
0
Cl
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
87-72-1
310. Indew (1,2,3-
c,d)Pyrene
❑X
❑
X❑
<5.D
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
,93 39 s
398. lsophomm
(7B-s9,)
❑
Q
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
30B. Naplhalene
(9,-zasl
❑
X❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
4DB. ilmherizene N
(�-�)
Q
ElQ
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
41B, N-Nitr
Zmelhylamine
❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
82-75-0
420, N-Ndro &N-
Pmpylxlnrle
❑X
El
X❑
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
021-64a
EPA FORM 3510-2C (Rev. 8-90) Page V-7 CONTINUE ON REVERSE

CONTINIJFD FROM THE FRONT
Outfall 001
1. POLLUT-
2.MARKX
2. EFFLUENT
3. UNITS
4. INTAKE (opt onal
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
specify if blank)
CAS NO. (if
ING RE-
QUIRED
LIEVED
PRESENT
LIEVED
ABSENT
(if available)
VALUE
ifova flahla)
d. NO. OF
ANALYSIS
AVERAGE VALUE
b. NO. OF
ANALYSES
(1)RATOFNIIT
12)MASS
(I)RATON T
(2)MASS
(1)RATION T
(2)MASS
aTRATION N-
TRATIO
b. MASS
available)
CONC NTRA (2)MASS
TION
GC1MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued)
43B.N.NG-
-di�Ylamine
X
El❑X
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
(E&30-fl
448. Phe ntrdor
(85.014
❑X
❑
❑X
<5.0
10.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
458. Pyraoe
(12"")
X❑
❑
❑X
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
46F1. 1,2.4-Tn•
a-A-b�ana
❑
❑X
<5.0
<0.072
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
i26-82-,
GC/MS FRACTION - PESTICIDES
1P. Alddn
(soeoo-2)
�
❑
<0.I
<0.001
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
2P. o.BHC
(31484-6
❑
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
(rahc
[3
(314857)
❑X
❑
❑X
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
4P_ )-BHC
(5"9-9)
❑X
❑
❑X
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
5P, t BHC
(3113-8s-8)
x
❑
❑X
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
6P.
(57-74-97-74-O)
El
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
� 2a3)DT
❑X
❑
❑X
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
BP. 4,4'- DE
(7255-9)
❑
❑X
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
2645)00
0
❑
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
1 OP. Olaldnn
IBas7-,)
❑X
❑
❑X
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
I 1 P. a End_�kfan
1115-29-7)
❑X
❑
❑X
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
115-2,a-I llan 1
❑
a
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
13P_ E�.Wfan
Saua,a
❑X
El0<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
,031-G711
14P. Endrin
172-2a8) -,
❑X
❑
❑X
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
15P. Endrin
Ald�,yda
❑X
❑
❑X
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
7421-83-4
,OP. Heptachlor
(7114")
❑X
❑
❑X
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-8 CONTINUE ON PAGE V-9

EPA I.D. NUMBER (copy from Item I of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-6 1 NCD047369046 1 001 1
1 POLLUT;'
W _,jQ1
:.XF
MaNJEST jp! 4 ��,BE
%a��MAXIMUWDAILYA
-3AEFFLUEN J
b.-MAXIMUM 30 DAY—'" -�4­ c� LONGTER
od� -OF�
4ku I
s eci yJ,:'6hink),,,;
MNTAKU(6�' o 1. niff�
a LON&TERM. 9k 6 ?"b NO F
C AS
.1 `�
VX
RE4`�',�' jELIEVED, ;ALIEVEW�j
PRE- N 7
1221RED41 ��
„VALUE
AL ii
VALUE
'
�;mj�bl
(ifavaif;rbll, e)ANALYST_
��ERM
A E4
AV GENALUE
V LU
L
;A L �'�'E�S4q.
__,4,
�N
�a
tF WE
SENT
*111) CONCENT
MT�
CONCENITA p CEN x
W�l RATION (2 1�(I) CON
":RATION
�—iaTCONCEN:i?�
RA ]ON' PNIb.-MASE
t�A
�-CONC"4' !S
­45-
L
z6
tj,
--T 10 N
g
;!�j
A
7EP0 do'
Ll
x
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
(I B12 -9)
0-1
<O.oc)l
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
Mup. PCB-1254
El
X
<0.1
<O.Ool
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
,00P.'PCB-1221j�'-_-
F-I
[X
<0A
10.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
,21p. pCs_I
rx]
❑
[x]
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
Q_22P�PC!31248
am
x
❑
X
<0.1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
'60
!jAff
X
El
Xx
<0.1
<0,001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
ff 2 p PCB " , 6 -
142'6'14-_I 1�1)'
—1
❑<0.
[X
1
<0.001
NA
NA
NA
NA
1
PPB
LB/DAY
NA
NA
0
25P.! Toxa-phem
e0, 1
<0.001
NA
NA
NA
NA
1
PPB
LBIDAY
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-9

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or EPA I.D. NUMBER (copy from Item 1 of Form 1) O utfa 11002
all of this information on separate sheets (use the same format) instead of completing NCD047369046
these pages. SEE INSTRUCTIONS.
V. INTAKE AND EFFLUENT CHARACTERISTICS continued from page 3 of Form 2-C
PART A - You must provide
the results of at least one analysis for every pollutant
in this table. Complete one table for each outfall. See instructions for additional details.
2. EFFLUENT
3. UNITS
4. INTAKE (optional)
1. POLLUTANT
(specify if blank)
a. MAXIMUM DAILY
b. MAXIMUM 3D DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONG TERM
VALUE.
fdavadable)
flfavailablo)
d. NO. OF
AVERAGE VALUE
b. NO. OF
(1) 2 MA55
CONCENTRATT (M
ANALYSIS
(1) 2 Mass
CONCENTRATI ( )
ANALYSES
coNcelNrRAn
t2) Mass
(1)
CONCEHTRATI
( 2) Mass
a. CONCEN-
TRATION
b. MASS
ON
ON
ON
ON
Biochemical Oxygen
D
Demand BOD
3
72.8
NA
NA
NA
NA
1
PP m
lb/day
Y
NA
NA
NA
Chemical Oxygen
D
Demand GOD
101
2,451.2
NA
NA
NA
NA
1
PP m
lb/day
Y
NA
NA
NA
c. Total Organic Carbon
TOC
21 5
521.796
NA
NA
NA
NA
1
PP m
lb/day
Y
NA
NA
NA
d. Suspended Solids
TSStaI
125
5,1137
72
2,342
61
1,760
101
ppm
lb/day
NA
NA
NA
e. Ammonia (as N)
0.1
2.427
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
f. Flow
Value 9.003
Value 4.136
Value 3.419
102
MGD
Value
NA
NA
g. Temperature (winter)
Value 24
Value NA
Value NA
1
oC
Value
NA
NA
h. Temperature (summer)
Value
Value
Value
Value
NA
32
NA
NA
NA
oC
NA
Minimum
Maximum
Minimum
Maximum
i. pH
6.3
8m
NA
NA
1
STANDARD UNITS
I
M
I
PART B - Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you
mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitation guideline, you must provide the results of at least
one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your
dischar e. Complete one table for each outfall. See the instructions for additional details and requirements.
1. POLLUT-
2. MARK W
3. EFFLUENT
4. UNITS
5. INTAKE o tional
+• eE-
a• BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. -LONGTERM AVRG. VALUE
a. LONG TERM
ANT AND
(specify if blank)
CAS NO. (if
LIEVE
0
LIEVE
pAR
VALUE
(ifavadabfeJ
(if available)
d. NO. OF
AVERAGE VALUE
6 N0. OF
(1)
CONCENTRA
12)A1A55
(1)
CONCENTRATIO
(211 wss
a. CONCEN-
TRATION
b. MASS
available)
PRES-
EMT
SENT
(t)
CONCENTPATiO (2)MASS
ANALYSIS
I+�
Cm CENTRAT*N SZI S
ANALYSES
TlON
N
N
_
-
a. Bromide
tza959.6�
❑
0.264
6.407
NA
NA
NA
NA
1
PP m
lb/day
Y
NA
NA
0
b. C.hlonne, -
Total Residua{
❑
0.740
17.347
NA
NA
NA
NA
1
ppm
Iblday
NA
NA
0
c. Color
❑X
17
NA
NA
NA
NA
NA
1
pcu
NA
NA
NA
0
d. Fecal
El
-Coliforrn .
5
NA
NA
NA
NA
NA
1
Col/100 ml
NA
NA
NA
0
e. Fluoride
�s9sa-as-s
0 2
4,854
NA
NA
NA
NA
1
PP m
lb/day
Y
NA
NA
0
f. Nitrate -
❑
Nitrite as N
0.42
10.193
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-1 CONTINUE ON REVERSE

197Tva:1r*T*1I II III la III a 6Id *101 I*,19 *14NI I1
Outiall 002
POLLUT.;=
2.-MARCx
.
i
g1. INTAKE o lions!
a. aE=
a. MAXIMUM,DAILY ,':
b MAXIMUM 30 DAY,VALUE
a LONG TERM AVRG. VALUE
LONGTERM
ANT AND,
bJa
(specify if hkjl
CAS'NO. if.
LIEVE
U
B. BE
"LIEVE'
F---.VALUE
_- (davaiable) =
{iiavaelable}.`
-
d NO OF
AVERAGE VALUE
b NO OF
ANALYSES
(1)
CONCENTRA
;,{2)MA55
S+1
CONCENTRAT!
,,: 12j MA55
n,
a.CONCEN__,
b MASS
.,
-,avadab(ej.
..
ARES
0AB_ .
SENT:,,
S+) {a)MAss
� CONCENTRATIr- `
ANALYSIS
'.coNce�irRAr!-, n `h1MAss _
.
ENT,, :
.>... _?
°i.:... TION
ON _...
-'::i _
::.- ON-.-TRA7ION
.:-—ON
:.9, Nitrogen;,_---'
Totall bro6jc
❑
2.2
53.393
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
,h:.0ll and
❑
n
<1
24.269
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
i.,Fhosphorus
(as 0?Total'
❑
3.71
90.039
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7723-14-0
;(1.} Alpha
Total..,..
❑
X
❑
3.2
NA
NA
NA
NA
NA
1
p Ci1L
NA
NA
NA
0
Beta , .
❑
X
❑
6.3
NA
NA
NA
NA
NA
1i
P Ci1L
NA
NA
NA
0
.::Total_._.... '"_;'
To
(3)Rad, lLIT ,
❑
0.4
NA
NA
NA
NA
NA
1
pCi/L
NA
NA
NA
0
aTotal�= '.
(4);Radlurn
ElX
<1.0
NA
NA
NA
NA
NA
1
P CilL
NA
NA
NA
0
k Sulfate (as
so4)�r
❑
56
1,359.1
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
14808=70-8-_
15ulfide ,.
a§ 5 . '
❑
❑x
0.01
0.243
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
m. Sulfite (as
soax ;
❑
Q
<1
24,269
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
14265-45-3
n: Surfactanis 2
X
❑
0.059
1,432
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
o'Aluminum; -.
Total
❑
4.09
99.262
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7a29-90-5
p:' Badum, :
Total
❑
Q.039
0.947
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
744D 39 3
?,q;,Boron,--,
A.Tole
❑
a
<0.005
0.121
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
' 7440-42-8
r: Cobalt's -
.Total
[]
rX
<O.OQS
0.121
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-48-4
s. Iron,(743989-4)Total.'
7439-89-4 ..
�
❑
1.15
27.910
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
t Magnesium,':
T�I
❑X
❑
5.20
126.201
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-95-4 , -
u. Miolybdenum -
Total
El❑X
<0.005
0.121
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-98-7
V. Manganese,
Total -
❑
0.156
3.786
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7439-96-5
W.-Tin Total
.(7440 =31-5
El
<0.05
1.213
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
x. Titanium,
Total -._
[]
<0.01
0.243
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-32-8
EPA FORM 3510-2C (Rev. 8-90) Page V-2 CONTINUE ON PAGE V-3

EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C 1 NCD047369046 1 002
PART C — If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC1MS fractions you must test for. Mark "X" in column 2-a far all such GCIMS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater ouffalls, and non -required GC/MS
fractions), mark -X" in column 2-b for each pollutant you know or have reason to believe is present. Mark W in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 210 for any pollutant, you must provide the results of at least one analysis for that pollutant. If you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acryionitriie, 2.4 diNtrophenol, or 2-methyl-4, 6 dlnitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instnrctions for
additional details and requirements,
1. POLLUT-
2. MARK'X'
3. EFFLUENT
(58) UNITS
5. INTAKE (optional)
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
(58) LONG TERM AVRG.
(58) LONG TERM
ANT AND
AN
(Specify if blank)
ING RE-
LIEVED
LIEVED
fifavadable)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS 1f .
QUIRED
PRE -SENT
ABSENT
fitaya'table
ANALYST
ANALYSE
available)
S
(I)CONCENT-
RATION
(2)MASS
(i)CONCENT•
RATION
(2)MASS
(t)CONCENT-
RATION
(2)MASS
S
a.
CONCEN-
h.MASS
(t)
CONCENTRA
(21MASS
TRATION
TION
METALS, CYANIDE, AND TOTAL PHENOLS
1m.Amimony, ,
Total
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-36-0
2M. Arsenic,
Total
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-38-2
3M, Beryllium,
Total
El
ElX❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-41-7
4M. Cadmium,
Total
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-43.9
5M Chromium,
Total
El❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-47-3
6M Copper,
Total
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-50-8
7M lead, Total
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7439-92-1
SM Mercury,
Total
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7439.97.E
9M Nickel,
Total .
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-02-0
Selenium,
Total
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7782-49-2
11M Silver,
Total -
❑
❑
XD
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-22-4
t 2M Thallium,
Total
❑
ElX❑
NA
NA
NA
NA
NA
NA
D
NA
NA
NA
NA
0
7440-26-0
Tottaa ZIP'
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-66-8
14M Cyanide,
Total
❑
❑
X❑
NA
NA
NA
NA
NA
NA
D
NA
NA
NA
NA
0
57-12.5
Phenols,
❑
ElX❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
Total ..
o[a
LJIUAIN
2,3,7,8-Tetra-
DESCRIBE RESULTS
chiorodibenzo-
❑ ❑
NA
P-Dioxin
(1764-01=6
EPA FORM 3510-2C (Rev. 8-90) Page V-3 CONTINUE ON REVERSE

W*Pk1111 1lil�:Zil �all. lN117:141211
Outfall 002
1. POLLUT-
2. MARK W
3. EFFLUENT
4. UNITS
5. INTAKE a fional
-a. TEST-
b. BE-
C. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(Specify if blank)
ING RE-
LIEVED
LIEVED
VALUE
(Ifavatabfe)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. if
OUIRED
PRE -SENT
ABSENT(it
avaffabla
ANALYSI
ANALYSE
available)
11)
S
(1)CONCENT-
(1)CONCENT-
(1)CONCENT-
5
a,
b. MASS
RATION
(2)IUASS
RATION
(2)MASS
RATION
12)MASS
CONCEN•
CONCFNTRA 2)hAASS
TRATION.
TION
GC/MS - VOLATILE COMPOUNDS
1V. Arddein (107-
ar-8)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2V. Aoryturrtrile
(107-13-11
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
ay. Banzena
(71-432)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
4V. BLS (Chbra-
me4hy1)Elhw(542_
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
Wit
5V. Bromobrm
(75-25-2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
sv. Cerbe"
T
El❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
s0-23so-23-onde
T7. Chlombenzena
El{10&90-7)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
eV. Chbm&
brornema
El
ElX❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
tea-a9.1lhene
QV- CH —Vane
(75-M3)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1ov. 2Lhbro- -
el I.h yl Ether
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
51475-8
11V. Chlaloloml
El(67-06-3)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
12V, 1]i NUa
"oln7sv-aane
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
cl,n,ranethlme
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7s-7,-e
14V. 1,l-D hkre-
❑
(75a.27-3
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
15V. 1,2-1)lrhbm-
o1ha—
❑
107
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
I ev. 1.1-Dmh$e
5N°ne
El
ElX❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(7535-4
17V. 1,2-1)trhtor
or°pone
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7s-ars
1BV, i3-Oicnkro-
°
El
5a
(.2-12asc
El
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EthyIhenzerte
❑
(100-41-4)
El1SV.
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
20V. 2ov. ,.,lalny,.
a
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
r4-as0
21V. Methyl
Chk1We
El
El
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
"1-3
EPA FORM 3510-2C (Rev. 8-90) Page V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
NCD047369046 1 002
1. POLLUT-
2. MARK 'xr
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
a. TEST-
b. BE-
c. BE.
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
e. LONG TERM AVRG.
a. LONG TERM
ANT AND
(Specify If blank)
ING RE-
LIEVED
LIEVED
VALUE
(davadable)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. (if
QUIRED
PRE-
ABSENT
if&V fable
ANALYST
ANALYSE
11)PC,AONCE T
(1ICONCENT-
(1)CONCENT-
(2)MASS
S
a,
b. MASS
available)
SENT
(+)
(2)MASS
g
{zjMASS
RATION
42)MASS
RATION
CONCEN-
CONCENTRATI
TRATION
ON
GC/MS - VOLATILE COMPOUNDS (continued)
22 V- Melhyl—
Chlorl
❑
Ts-0s-2
-z
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
23V. 1,122-Tw -
cWroeL"(TY
❑
34-5
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
24V. Teirechlora
alhyiene(
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
,zT-19-4
25V. Td—
(+O-W-3)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
26V.1.2-Trap
Dichloroelhylene
❑
❑
156-605
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
27V. 1 I. I. -Tr4
chbroeI.-T
El❑
T1u5-6
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2BV. 1,1,2-Tn-
28V. 1,1,2- e
❑
❑
Taao-s
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2W. TncMoro-
alhylo
❑
❑
�e-o,-6
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
30V. Tnrfilaro-
n—methane
❑
❑
7s-6aa
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
31V_ Virro Chloride
❑
(T�1-4)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
GCIMS FRACTION ACID COMPOUNDS
tA_ 2-
ChImph
❑
❑
X�
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
95_57'a-5T-8
24.. 2,4-Dlcltloro-
�'
❑
❑
1;7 z
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3A. Zj_up eth*
❑
El0
(t05-6 -e
os-eT
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
4A. 4.r,0Wro-O-
.—t
❑
❑
s34-S2-1
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
5A. 2,4-Dinlro-
011
❑
❑
51-2&5
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
6A- 2-Wro-pher l
❑
(ea-7s5)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
4-M� ph l
❑
(10
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
8A. P-CFJora-hb
Cresol
El
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
59 1,T
9A. Porda-
tll.phefol
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
aT-eas
10A. Pheml
nas-95-?I
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
11A. 2.4,6Trr
11A 2.4,&T
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
ea-o�x
EPA FORM 3510-2C (Rev. 8-90) Page V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfall 002
2. MARK'X•
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
t. POLLUT-
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(specify if blank)
ING RE-
LIEVED
LIEVED
VALUE
VALUE
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. (if
QUIRED
PRESENT
ABSENT
_
_ rfab10
fliavalrable)ANALYST
ANALYSE
{+)CONCENT-
RATION
(2) MASS
{,)CONCENT-
RATION
r2) MASS
(1)CONCENT•
RATION
(2) MASS
S
a.
CONCEN-
b. MASS
available)
(+)
CONCENTRATI (2) MASS
S
TRATION
ON
GCIMS FRACTION - BASElNEUTRAL COMPOUNDS
W. Acanpra—
($0_32-e)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
213. ACanaphlylene
()
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3B. Anthracene
t+20�12-7)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
4B. Benndune
(02-s7-5)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
5B. 90nzo (a)
A^.
El
El
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
5&55-3
. BB. Henzo la)
ryene(sa3z$)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7B. 3,4-6emz
fl oranthene
❑
❑
XD
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2(X,W2
BB. eenm (gM)
P
721.
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
tg1�24�2
9B. Benzo M
'FI—anthene
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
207-OB-S
Im Bia(2- -
`NDfOe1hv�Y)
Methane
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
f I1-0I-}
118_ Bls {2-Cnloro-
-0
(111 4-0)
El❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
12B. Sis (2-
Ch,aroleoprapyl)
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
Ether 108841
138. Bis(2-Elhyl-
Phthe'ala
❑
El
❑X
NA
NA
NA
NA
NA
NA
0
NA
TVA
NA
NA
0
117-
(I 7-e,-r
1413 4-Dr
phenyl Phenyl
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
TVA
NA
NA
0
E[her 1a1-55�
15B BUY Benzyl
PNhala7t0)
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
ar0&
16B. 2_04 ro
'ph lharene
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
gt-W
17B. 4-Chlnra-
Et
El❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
Ether.r(7005-Phefr
. 72-]
188. Chryaene
(z1ao1-es
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1913. D.nenzo (a,h)
Aruhracena
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
53-70-3
20B. 1,2-DKhbo
e
El
ras-so-benzen1
El
n
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
210. 1,3-[hc"Ortr
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-6 CONTINUE ON PAGE V-7

EPA I.D. NUMBER (copy from Item 1 of Form I) OUTFALL NUMBER
CONTINUED FROM PAGE V-6 1 NCD047369046 1 002
1. POLLUT-
2. MARK 'X'
3. EFFLUENT
4 if blank)
S. INTAKE (optional)
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXtMVM 30 DAY VALUE
(622) LONG TERM AVRG.
(im) LONG TERM
ANT AND
CAS NO. if
ING RE-
LIEVED
LIEVED
VALUE
(rlavaiable)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
(
OUIRED
PRE -SENT
ABSENT
iiavailabfe
ANALYSI
ANALYSE
(1)CONCENT-
(1)CONCENT-
(i)CONCENT-
c�
it.CONCEN-
available)
(1)
S
RATION
(2) MASS
RATION
(?I MASS
RATION
(2) MASS
TRATION
b. MASS
CONCENTRATI (2) MASS
ON
GCIMS — BASE/NEUTRAL COMPOUNDS (continued)
226. 1.4-DkAYoe
l'.
❑
,oe a5-7
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
23& 3,T-Dkbfm,
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
9t-B4-t1
24B. Diethyl
Phthalate
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
94-6&2
250. Dimothyl
PnthBlete
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
131-11-3
269. Di-N-Butyi
Phthalate
❑
[�
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
84-74-2
toluene
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
121-144
- 268. 2.&#kMiro-
to'"�
❑
6a&2a2
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
M. Di-N-OGyl
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
0Phthadale
1, 7-a4-0
17-11"
306- ,,2-Diphenyl-
hyd,wbe—.ine(asAw
hen�nna) .
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
122-6&7
318. Fluoranlhene
❑
(2ow,4-0)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
329. Fluomne
❑
(M73-7)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
338, Hexe-
`"° p!4 �—
El❑
QX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1,8-74-,
348. H-.
G1b1aM1tad'eno
❑
El
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
07�8�3
358, H—to.—
(7'd°P'W°1B e
❑
7�7-41.
ElOX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
36B. Hera-
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(-72-1) 6
7-7z•,
37nden
nden I 378. o [,,z,3-
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
193-39-5
28B,
76B, IsopFn�"na
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
39B. Napthalene
❑
(91-20-3)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
406. Nbobe-wo
❑
(9&95.3)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
416. N-Nrll
mdime9)
❑
❑
Q
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
ls9426.
4ENA
dd
N-Ndroadl-N-
❑
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(621-8amin❑
fi2184-7
EPA FORM 3510-2C (Rev. 8-90) Page V-7 CONTINUE ON REVERSE

rnMTINI IFn FROM TI-IF FRONT
Outfall 002
2, MARK X
2. EFFLUENT
3. UNITS
4. INTAKE (opt onal
1. POLLUT-
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
specify if blank)
ING RE-
LIEVED
LIEVED
(if available)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. (if
QUIRED
PRESENT
ABSENT
tifava!lable)
ANALYSIS
ANALYSES
(1)CONC T
{2JMSS
(1)CONCENT-
(2)MASS
(1)CONCENT-
(2)MASS
a. CONCEN-
b. MASS
available)
(1)
42)MASS
RATION
RATION
TRATION
CONCENTRA
TION
GCIMS FRACTION - BASE/NEUTRAL COMPOUNDS (continued)
43B. N-Nd—
Be16yIa^�^°
86-30.61
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
44B. P^ena4l+rane
(85-01.4
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
45B.. Pyres°
1129-oo-o)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
408. 1,2,4-Tn-
dwoeenzene
❑
❑
XC
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
GC/MS FRACTION - PESTICIDES
1 P. Aldnn
(30a0'2)
❑
❑
X
NA
INA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2P. a-BHC
(318'8'1-6
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(31 W )
(319-aS7
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
aP. I-RHC
(S�g9r
❑
❑
IX-1
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
SP. MBHC
(31-
El0-66.8)
❑
)(
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
6P. Chlordane
(57-74.0) -
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
IT. 4,4'-nor
(60.219a)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
BP. 4,4•-DDE
(72s5-9)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
9P. 4.4•-DDD
(72-54a)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
- 10F. Dieldrin
(so-57 u
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
11P, u Endo-swfan
El(11529-7)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
12P. I7-Endo-sUlm
(115S29•7
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
13P. EndoO Ul
1fate
El
ElX❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(103%-
14P. Endrin
2
(72-0-01
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
16P. EMnn
A'^°^y^°
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7a2,-93-4
16P. HeoacWr
❑
(7"4-81
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-8 CONTINUE ON PAGE V-9

EPA I.D. NUMBER (copy from Item 1 of Form J)
OUTFALL NUMBER
CONTINUED FROM PAGE V-fi
INCDO47369046
002
9. POLLUT-
2. MARK 'X,
3. EFFLUENT
4. UNITS
5ANTAKE (optfonal I
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY
C. LONG TERM AVRG.
a. LONG TERM
ANT AND
Specify if blank)
CAS NO. (if
ING RE-
LIEVED
LIEVED
VALUE
VALUE
VALUE
d. NO. OF
AVERAGE VALUE
D. NO.OF
QUIRED
PRE-
ABSENT
If available
fifavailable)
ANALYSI
ANALYSE
available)
SENT
S
(1)
-(I)CONCENT-
(17CONCENT-
(1)CONCENT-
a.CONCEN-
RATION
{2)MA55
RATION
.12)MA.S
RATION
(2)MASS
TRATION...
b. MASS
CONCENTRA -.121 A1A55
I
TION
+
GC/MS - PESTICIDES (continued)
17P. Haptetldor
Exp ide
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1024.57-3
18P. PC13-1242
(53469-21-11)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
19P_ PCR-1254
(110e7.69.1)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
20P. PC13-1221
(11104-28-7)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
21P.PCB-1232
❑
(11141-10-5)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
22P- PCB-1246
(12672-2")
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
23P. PC6-1260
(nosrre2-5s
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
24P. PCB-4016
(12674-11-2)
❑
ElX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
25P. Toxa-oe e
{sw1-35-2s
El
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-1 CONTINUE ON REVERSE

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or EPA I.D. NUMBER (copy from Item 1 of Form 1) Qutfall 003
all of this information on separate sheets (use the same format) instead of completing NCD047369046
these paqes. SEE INSTRUCTIONS.
V. INTAKE AND EFFLUENT CHARACTERISTICS continued from page 3 of Form 2-C
PART A - You must provide the results of at least one analysis for eve ollutant
in this table. Complete one table for each outfall. See instructions
for additional details.
2. EFFLUENT
3. UNITS
4. INTAKE (optional)
i POLLUTANT
(specify if blank)
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONGTERM
.
VALUE
(jlavadable)
fifavallable)
d. NO. OF
AVERAGE VALUE
b. NO. OF
(I)
CONCENTRATI I2) MASS
ANALYSIS
(+1
CONCENTRATI (2) MASS
ANALYSES
(+)
CONCENTRAT_ I
(2) MASS
(0
CONCENTRATI
(2) MASS
a. CONCEN-
TRATION.
b. MASS
ON
ON
ON
ON
a. Biochemical Oxygen
<2
a2.769
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
Demand BOD
b. Chemical Oxygen
11
15.229
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
Demand COD
c. Total Organic Carbon
7.1
9.830
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
TOC
d. Total Suspended Solids
4
5.538
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
TSS
e. Ammonia (as N)
0.1
0.138
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
NA
Value
Value
Value
Value
NA
f. Flaw
0,166
NA
NA
MGD
NA
g. Temperature (winter)
Value 19.0
Value NA
Value NA
1
oC
Value
NA
NA
h. Temperature (summer)
Value
Value
Value
Value
NA
28 0
NA
NA
NA
oC
NA
Minimum
Maximum
Minimum
Maximum
I. pH
6.9
8.0
NA
NA
1
STANDARD UNITS
PART B - Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you
mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitation guideline, you must provide the results of at least
one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your
dischar e. Complete one table for each outfall. See the instructions for additional details and re uirements.
1. POLLUT-
2. MARK W
3. EFFLUENT
4. UNITS
5. INTAKE o tional
OLIEVE
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
ANT AND
(specify if blank)
CAS NO. (if
LIEVE
SENT
VALUE
(+!evadable)
(ifavailable)
d. NO. OF
AVERAGE VALUE
b. NO. OF.
f11
CONC1)
12)MA$5
(1)
CONCENTRATIO
12)P.IASS
a. CONCEN-
TRATION
b. MASS
available)
PRESS
ENT
01
CONCENTRATIO (2I MA55
ANALYSIS
01
CONCENTRATION izl'uss
ANALYSES
noN
N ,
N
Bromide
❑
0.292
0.404
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
0
( 24959-67-9)
b. Chlonne
TotalReslal
❑
❑X
0,150
0.208
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
0
c. Color
❑
❑X
37
NA
NA
NA
NA
NA
1
pcu
NA
NA
NA
0
d. Fecal
❑
270
NA
NA
NA
NA
NA
1
C011100 ml
NA
NA
NA
0
Coliform
e. Fluoride
❑
0,2
0.277
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
0
16984-48-8
f, Nitrate -
❑
0.10
0.138
NA
NA
NA
NA
1
ppm
lb/day
NA
NA
0
Nitrite (as N)
EPA FORM 3510-2C (Rev. 8-90) Page V-1 CONTINUE ON REVERSE

ITEM V-0 CONTINUED FROM FRONT
Outfall 003
1, ROLLUT-
2. MARK W
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
•. BE-
B. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
C. LONG TERM AVRG. VALUE
a. LONG TERM
ANT AND
(specify if blank)
CAS NO. (if
LIEVE
D
LlEVE
VALUE
(itavatable)
(ifavailable)
d. NO. OF
AVERAGE VALUE
b. NO. OF
1)
CONCENTRA
(2)11ASS
S t
CONCENTRATI
J2)MASS
a. CONCEN-
TRATION
b. MASS
available)
PRES-
Das
SENT
1 1
CONCENTRATI (2)MASS
ANALYSIS
11
CONCENTRATI (21MASS
ANALYSES
ENT
TFON
ON
ON
ON
g, Nitrogen,
Total Organic
❑
0.5
0.692
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
as N
Oilh. andand
❑
<1
<1.384
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
Grease
G
i. Phosphorus
(as P), Total
❑
0.10
0,138
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7723-14-0
j. Radioactivity
(1) Alpha
❑
❑X
<3
NA
NA
NA
NA
NA
1
p Ci/L
NA
NA
NA
0
Total
(2) Beta,
❑
<4
NA
NA
NA
NA
NA
1
p Ci1L
NA
NA
NA
0
Total
(3) Radium,
❑
X
0.6
NA
NA
NA
NA
NA
1
pCi1L
NA
NA
NA
0
Total
(4) Radium
❑
X
❑
<1
NA
NA
NA
NA
NA
1
pCi1L
NA
NA
NA
0
226, Total
k. Sulfate (as
SO4)
❑
30
41,533
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
,aaoe-79-s .
1. Sulfide
❑
❑
0.02
0,028
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
aSS)
m. Sulfite (as
SO,X
❑
❑X
<1
<1.384
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
14265-45-3
n. Surlactanis
❑
❑X
0.048
0,066
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
o. Aluminum,
Total
❑
0,289
0.400
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7429-90-5
p. Barium,
Total
O
❑
0.020
0.028
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7440-39-3
q. Boron,
Total
El<0.005
<0.007
NA
NA
NA
NA
1
PPM
LSIDAY
NA
NA
0
7440-42-8
r. Cobalt,
Total
❑
X❑
<0.005
<0.007
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7440-48-4
PPM
LB/DAY
NA
NA
0
s. Iron, Total
%�
❑
❑
0,434
0.601
NA
NA
NA
NA
1
7439-89,4
L Magnesium,
Total
❑
2.85
3,946
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7439-95.4
u- Molybdenum,
Total
❑
<0.005
<0.007
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7439-98-7
v. Manganese.
Total
❑
0,038
0,053
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7439-96-5
w. Tin, Total
❑
❑X
<0.05
0.069
NA
NA
NA
NA
1
PPM
LBIDAY
NA
NA
0
7440-31-5
x. Titanium,
Total
❑
<0.01
<0.014
NA
NA
NA
NA
1
PPM
LB/DAY
NA
NA
0
7440-32-fi
EPA FORM 3510-2C (Rev. 8-90) Page V-2 CONTINUE ON PAGE V-3

CONTINUED FROM PAGE 3 OF FORM 2-C
EPA I.D. NUMBER (copy from Item i of Form 1) OUTFALL NUMBER
NCD047369046 1 003
PART C — If you are a primary industry and this eutfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GCIMS fractions you must test for. Mark "X' in column 2-a for all such GCIMS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and non -required GC/MS
fractions), mark "X' in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant. If you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 &nitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analyslS or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table fall 7 pages) for each outfall. See instructions for..
additional details and require ents.
1. POLLUT-
2. MARK'X'._
3. EFFLUENT
(59) UNITS
5. INTAKE. o #Iona!
a. TEST-
b. BE-
C. BE.
a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
(59) LONG TERM AVRG.
(59) LONG TERM
ANT AND
(specify if blank)
CAS NO.
ING RE-
. LIEVED-
LIEVED
(davadabte)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
(if
OUIRED
PRE -SENT
ABSENT
ifavartable .
ANALYSI
'ANALYSE
available)
(1)
CONCENT A (2)M.ASS
S
(t)CONCEEi
(2(2)MASSNT
(1)CONCLNY-
RATION(71M+SS
(1)CONCENT-
ELATION
(2)MAS5
S
a.
b, MASS
CONCEN-
nON
TRATION
METALS, CYANIDE, AND TOTAL PHENOLS
1m. Antimony,
Total
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-36-0
NA
NA
0
2M. Arsenic,
Total
❑
❑
0
NA
NA
NA
NA
NA
NA
NA
NA
0
7440-38-2
3M. Beryllium,
Total
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-41-7
4M. Cadmium,
Total
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-43-9
5M Chromium,
Total
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-47-3
6M Copper,
Total
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440.50.8
7M lead, Total
El
❑
F
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7439-92-1
8M Mercury,
Total
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7439-97-6
9M Nickel,
Total
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-02-0
10M Selenium,
Total
[]
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7782-49-2
11M Silver,
Total
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-22-4
12M Thallium,
Total
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-28-0 . ..
13M Zinc,
Total
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7440-66-0
14M Cyanide,
Total
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
57-12-5
15M Phenols,
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
Total
2,3,7,8-Tetra-
❑
❑
X
DESCRIBE RESULTS
chlorodibenzo-
NA
P-Dioxin
-(1764-01-6)
EPA FORM 3510-2C (Rev. 8-90) Page V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfall 003
1. POLLUT-
2. MARK'X'
3. EFFLUENT
4. UNITS
5. INTAKE (optional
a. TEST-
b. BE.
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(Speafy it blank)
ING RE-
LIEVED
LIEVED
VALUE
(davedable)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF;
CAS NO. (!f
OUIRED
PRE -SENT
ABSENT
0favalable)
ANALYSI
...
-
ANALYSE
IucONCENT-
{2j MASS
(t)CONCENT-
(2j MASS
(1(CONCLNT-
(2)MASS
- S
a.
b. MASS
available)
(1) 2 nnA
(1 SS
$
RAT40N
RATION
RATION
CONCEN-
CONCENTRA
TRATION.
TION
GC/MS - VOLATILE COMPOUNDS
IV. Aaolein (107-
02-8)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2V. Aetybrtitnlle
no7-?}v
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(7,�a(7 Benzene s-z)
❑
❑
Fx_1
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
4V. Sis (Chloro-
melhyl)Elh-(542_
❑
❑
Q
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
se-+
5V. Bmmoform
-(75-25-2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
BV. Carbon
TelracWndo
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
58 215
7V-Chlwobenzena
(10a90-7)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
BV. CNot
°ion1OT th.n°
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
- 323-48-1 -
(75 Chloroethane
{7s� 3s
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
10V. 2-010ra
.thvi yl Ett-
❑
i1i47$ B
El❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
,1 V. Chloroform
(87-5 )
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
12V. cichloro-
bm
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7s27m
13V. Oichb—
diewrra-He ne
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
75-71-8
14V. 1,14kct*oro-
a
❑
v-
75-s27-a
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
15V. 1,2-0icMoro-
shanB
❑
1o7�z
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
16V. 1;14]itlltoro-
❑
ElX❑
7535-4
QSM-4)
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
17V. 1,24)kl it
❑
Tl
f1
❑
X❑
NA
NA
NA
NA
NA
NA
D
NA
NA
NA
NA
0
tBV. 1.3-131,04oro-
-propylene
El❑
Sat-75 6
NA
NA
NA
NA
NA
NA
D
NA
NA
NA
NA
0
❑
10041-4lbenzene
(+�+-+s
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
M-hyt
El
❑
X❑
NA
NA
NA
NA
NA
NA
D
NA
NA
NA
NA
0
(74-8374A3o8
21V. hlelhyl
cNonae
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA j
NA
NA
NA
0
74-87-3
EPA FORM 3510-2C (Rev. 8-90) Page V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
NCD047369046 1 003
1. POLLUT-
2• MARK'X'
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(specify If blank)
GAS NO. ( 1f
ING RE-
LIEVED
LIEVED
VALUE
(ifava#ahle)
VALUE
rtavaitable
d. NO. OF
ANALYSI
AVERAGE VALUE
b. NO. OF
QUIRED
PRE-
ABSENT
ANALYSE
11)CAOTN iii
("RATION T
{i)RATIONNT
S
°,
b. MASS
available)
5
SENT
{2)MASS
(2)MASS
(2)MASS
CONCEN-
CONCEINTRATI {2)M4SS
TRATION
ON
GCIMS - VOLATILE COMPOUNDS (continued)
22 V. Methylene
ode
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7s-os-z
k,2,2-Telra-
ctrwd°usne(7�
❑
34S
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
24V. Tetiachloro-
ethylene(
❑
❑
QX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
in.18-4
. 2sv. Tntuen°
(10E,.13 -3)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
26v. 1.2-Tr°
M.Nomelhyi°n°
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
156-sa s
27V. +1111-Tri-
chloroethane
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
71-SSfi
2SV. 1,1.2-Tn-
chleraethane
❑
79 865 -
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
29V. TridVnn>
�"Y'B B
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7&8t-fi
3W. TrioNaro-
❑
75-ea4
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
31V. Vinyt Chlonde
(7$-01-4)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
GC/MS FRACTION - ACID COMPOUNDS
1A. 2-
Chlnol
El
El0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
= 0
95-57-8
57-8)
2A 2,4'DicMioro-
ph-1❑
12n-e3�z
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3A. 2,4.DM"l% F
ph0O0l
❑
ies-67-e
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
4A. 4,5-0iritra-O-
-�l
❑
s34s2.1
❑
X�
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
5A. 2,4-Dimm. P'
L
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
51-285
6A. 2-1v1tF0­0enol
❑
(88-75a)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7A. 4-Mro-phenol
❑
(100.02a)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
BA. PCrd._?l•
Crawl
❑
5950.7
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
9A- Panin-
chlbrophenol
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
87-86-5
Phenol
❑
X
NA
NA
NA
NA
NA
NA2,4,6-Tri-
LOW
°p"_
❑
❑X❑
2
EPA FORM 3510-2C (Rev. 8-90) Page V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfall 003
1. POLLUT-
2. MARK W
3. EFFLUENT
4, UNITS
5. INTAKE o tiona!
a. TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
h. MAXIMUM 30 DAY
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
specify if blank)
ING RE.
LIEVED
LIEVED
VALUE .
VALUE
VALUE
d, NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. (if
QUIRED
PRE -SENT
ABSENT
rfavadabte)
tiravailable
ANALYSI
ANALYSE
(,)CONCENT-
RAT,ON
{2j MASS
(1)CONCENT-
RATION
(2) I''u`
{1)CONCENT-
RATION
(2) MASS
S
a,
CONCEN-
b. MASS
available)
(1) 2
CONCENTRATI () MASS
$
TRATION
ON
GClMS FRACTION - BASEINFUTRAL COMPOUNDS
%B. Acen".m
ID&W-9)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
20. Acan. Nylene
(206.9&8)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
38. Arttlreceno
1120-12-7)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
4B. 13—ndi"e
(92-87-5)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
58. Benzo (a)
❑
❑
OX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
58. Benzn (e)
Pyrene(50-32-8)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
713. 3,4-Remo-
ftuoranthene
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2D5 99-2
08. Remo (9N)
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
(191-24- 2
191-24-
90. Remo (k)
Fluerar,thene
❑
El
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
207=1
1013. Sts 12-
ChloroeiYgxy> .-
Methane
❑
El
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
11I-91-1
,1 B. Bis 12LFdwo-
.t",) Ether
1 f 1-44-0
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
126. Bis(2-
Chlom"opropy')
er Eth109-BD_,
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
13B Sis(2-Ethyl-
f7) °
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
n7a,a
11- 1-7
t4 B. a-erolno-
pM1e"y' �"°nyl
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
Ether 101-55-3
1513 Butyl Be"
Ph":1118
❑
El
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
a�as-7
10B, 2-Chlo—
,e0th 1ene
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
St-50 7
178. 4-Chloro-
Ph_yi Phenyl
❑
Ether 7005-72-3
❑
X�
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
' ap Chrysene
(21"1-0)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
199�
19B, Oibenzn (e.h)
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
5 I
209 1,2-Dchloro-.
Muene
❑
9s�o-1
❑
X[]
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
276, ,,3.Oicldoro-
�°"e
❑
541.73-,
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
N C D047369046 1 003
2• MARK'X
3. EFFLUENT
4 if blank)
5. INTAKE (optional)
1. POLLUT-
a. TEST•
b. BE,
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 3U DAY VALUE
(623) LONG TERM AVRG.
(623) LONG TERM
ANT AND
tNG RE-
LIEVED
LIEVED
VALUE
(davaiable)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. (if
QUIRED
PRE -SENT
ABSENT
lfavaitable
ANALYSI
ANALYSE
available)
(1)CO pNNT-
(2)MASS
fl)CONCENT
(2(Ie,g55
(1)CONCLNT-
(2F'`e`SS
sr
a.CONCEN-
N
(2l MASS
S
RATION
RATION
TRATION
b. MASS
CONCENTFt.4TE
ON....
.....
GC/MS — BASEINEUTRAL COMPOUNDS (continued)
229 1,4-OiflUmo- -
h°"�B^°
❑
❑
OX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
,OB-46-7
238. 3,T-DkMmo-
heu°
❑
❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
sld.!
,-o4-,
24B. Diethyl
Phthalata
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
64.6&2
256. Dimethyi _
Phh,slat°
El❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
i31-11-3
268, DI-N-Bwyl
Phtha1a1
El
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
84-74-2)
27B. 2,4AinMo-
mluone
,21-14.2
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2aB, 2.&DRndh
nlnene
❑
❑
QX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
298. Di-N- W
Phtha'a,°
❑
ElQ
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
n 7-e4-o
308. 1.2-Oiphre yV-
hycreane(a,nro-
benz�)
El❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
122-6&7
31B. FIu nthene
(zos ")
❑
❑
FRI
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
32B. Flwaene
(a&73-7).
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
33B.Heea-
ah1oro°ewe"°
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
„=-1
34B. Hello-
chioro Zjene
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
07-68.3
358, Nara J jmr
�p-dadi—
❑
77A7-4
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
368. Hello-
d'ko etlw.
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
67-72.1
378, hdeno (1.2,3-
°diPyre"°
❑
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1s3-3as
386. mne Impho
(78-59-1)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
39B. NaMhalene
(s1-�)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
40B. Nitrobenzene
(9&95.3F
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
416. N-NVr
wd-nelhylamine
❑
ElX❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
6275-9
4213. N.NkroWm-
Propylamine
❑
621-64-7
❑
X❑
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev, 8-90) Page V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
Outfall 003
1. POLLUT-
2. MARK x
2. EFFLUENT
3. UNITS
4. INTAKE (opt onal
a -TEST•
b. BE-
C. BE-
a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
ANT AND
(specify If blank)
ING RE- •
LIEVED
LIEVED
(if available)
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
CAS NO. (if
i
QUIRED
PRE -SENT
ABSENT
ilavellabla
ANALYSIS
ANALYSES
available)
I7f CONRATION
{1J
(1)gAT10NNT
a.GONCEN-
b. MASS
(2)MASS
RATION
(2)MASS
12)MASS
TRATION
CONCENTRA (2) MASS
iION
GCIMS FRACTION - BASEINEUTRAL COMPOUNDS (continued)
438-N-N&—
sodlphanytamina
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
B1r30-61
-449. Phenardhre
(�1 !
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
45a. Pyrene
(129ma)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
468. 1,2,4-Tri-
himb
° °" °
❑
❑
QX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
i
GC/MS FRACTION - PESTICIDES
1P. Afdfin
(2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
2P. a-BHC
(319r84.li
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
3P. Ii-ahc
(31&&S7)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
4P. y-BHC -
(5e%9)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
s,ael
(319-e&a-SI
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
6P. Chlordane
El(57-74-9)
ElX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7P. 4,4'•DDT
(5&29-3)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
W. 4,4•-DOE
(72-5&9)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
9P, 4,4'-DDD
(72-54-e1
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
10P. Didtlrin
(60.57-1)
❑
❑
FX1
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
11 P, ,,-Endo-w1fan
(t155-29-7)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
12P. 8-Erdo-sllfen
El(I1S2!Y7
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
13P, Erdo®alan
srnlale
❑
❑
0
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1o31-07•e
14P, End in
(72-2ae)
❑
Cl
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
15P. Endrin
Aldehyde
❑
❑
QX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
7421-93A
16P, Heaacl o
El(76-14$)
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-8 CONTINUE ON PAGE V-9

EPA I.D. NUMBER (copy from Item i of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-6 NCD047369046 1 003
1. POLLUT-
2. MARK W
3. EFFLUENT
4. UNITS
5. INTAKE (opt onal
a- TEST-
b. BE-
c. BE-
a. MAXIMUM DAILY
b. MAXIMUM 30 DAY
c. LONG TERM AVRG.
a- LONG TERM
ANT AND
(specify if blank) :
if CAS NO.
(
ING RE-
LIEVED
LIEVED
VALUE
VALUE
VALUE
d. NO. OF
AVERAGE VALUE
b. NO. OF
ANALYSES
QUIRED
PRE-
ABSENT
it available
(ifavailable)
-
ANALYST
available)
SENT
(1)
(1)CCONICOEINT,
(1)CONCENT-
(Ij CONCENT-
_S
a. CONCEN-
.
(2)MA5S
- RATION
(2) MASS
RATION
(2) MASS
TRATION
b. MASS.
- CONCENTRA (2) MASS
TCN
GC/MS - PESTICIDES (continued)
17P. Heptact4o[
4.ide
❑
❑
❑X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
1024-57-3
18P. PCB-1242
(5346921-0)-
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
19P. PCB-1254
(110s7-69-1)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
20P. PCB-1221
(11104-28-2) '
❑
ElX
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
21P,PCR-1232
(11141-16-5)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
22P. PCB-1248.
(12672-29-6) -
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
23P. PCB-12W
(11OW82s)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
24P. PCB-1010
(12674-11-2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
25P. Toxa-phone
(eoo1 2)
❑
❑
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
0
EPA FORM 3510-2C (Rev. 8-90) Page V-9

Attachment IV. Narrative Description of Pollutant Sources
A. For each outfall, provide an estimate of the area (include units) of impervious
surfaces (including; paved areas and building roofs) drained to the outfall, and an
estimate of the total surface area drained by the outfall.
A.
outfall
Number
o List
Area of
Impervious
Surface
Total Area
Drained
Portion ofjlropqrty Drained
001
NA
NA
Outfall 001 discharges treated wastewater from the
site's wastewater treatment plant. It is covered under
NPDES permit NC0000663.
002
40 acres
138 acres
Monomers manufacturing areas
002A
<1 acre
32 acres
Northwest portion of the property
003
15 acres
66 acres
West and southwest portion of property
003A
4.7 acres
23 acres
West portion of property
003B
<1 acre
18 acres
Freshwater intake pond and pump station
004
7:2 acres
195 acres
South portion of the property
005
<I acre
58 acres
Southeast portion of property
006
9 acres
65 acres
Eastern portion of property, new rail storage area
007
<1 acre
9 acres
Northeast portion of property
008
<2 acres
18 acres
Southwest portion of property
B. Provide a narrative description of significant materials that are currently or in the past
three years have been treated, stored, or disposed in a manner to allow exposure to
storm water; method of treatment, storage, or disposal; past and present materials
management practices employed, in the last three years, and frequency in which
pesticides, herbicides, soil conditioners, and fertilizers are applied.
No significant materials, (as defined in the instruction of this form), have been treated,
stored, or disposed of at this facility in the last three years in a manner that would allow
exposure to storm water. The management practices at the facility prevent signicant
materials from entering the stone water discharges.
As defined by the United States Environmental Protection Agency (U.S. EPA) in the
Federal Regulations under 40 CFR 122.26(b)(12), "Significant Materials" include, but
are not limited to: raw materials, fuels; materials such as solvents, detergents, and plastic

pellets; finished materials such as metallic products; raw materials used in food
processing or production; hazardous substances designated under Section 101(14) of the
Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA);
any chemical the facility is required to report pursuant to Section 313 of Title III of the
Superfund Amendments and Reauthorization Act; fertilizers, pesticides, and waste
products such as ashes, slag, and sludge that have a potential to be released with storm
water discharges.
Materials representing a possibility of contact with storm water are:
• AFFF Liquid Foam Concentrate
• Cal -Shield
• Coal (Bituminous)
• No. 2 Diesel Fuel
• Dyed Diesel Fuel
• Ethylene Glycol
• No. 6 Fuel Oil
c Gasoline, Regular Unleaded
• Hydrogen Peroxide
• Magnesium Chloride (35%)
• Novus CE 2688
• Paraxylene
o Sodium Hypochlorite (15%)
• Solcst 68 Oil
• Terephthalic Acid (All Grades)
• Transformer Oil
Potential sources (storage tanks, site areas, and operations) that may be reasonably
expected to add pollutants to storm water discharges or that may result in the discharge of
pollutants to the storm water drainage system are listed below by the outfall through
which the pollutant would discharge.
1.1 DRAINAGE AREA 002
Description
Quantity Volume, gal
Type
Acetic acid
2 375,000
AST
Caustic
1 88,200
AST
Cobalt slurry
1 61,000
AST
Diesel fuel
1 175
AST
Diesel fuel
1 650
AST
Diesel fuel
1 500
AST
Diesel fuel
1 10,000
AST

Description
uanti
Volume al
Type
DRL-6
1
40,000
AST
Finish oil
7
10,000
AST
Finish oil
3
1,500
AST
Finish oil/water
2
5,000
AST
Florence non -white
1
40,000
AST
Gasoline, regular unleaded
1
10,000
AST
Glycol, refined
1
150,000
AST
Glycol, refined and loading rack
1
40,000
AST
Glycol, spent
2
40,000
AST
Glycol, virgin
1
300,000
AST
KP-1
1
40,000
AST
Lube oil
1
1,870
AST
Lube oil
1
395
AST
Magnesium Chloride
1
6,150
AST
Methanol, distilled and loading rack
1
179,148
AST
Methanol, Recovered
1
872,000
AST
No. 2 Fuel oil
1
5,000
AST
No. 6 Fuel oil
2
50,000
AST
No. 6 Fuel oil
1
150,000
AST
No. 6 Fuel oil
1
414,000
AST
Paraxylene, Exxon
t
1,000,000
AST
Paraxylene
1
250,000
AST
Paraxylene
1
1,260,000
AST
Phosphoric Acid
1
6,650
AST
TEG
1
25,000
AST
TRIM #1
1
80,000
AST
Uran
1
8,700
AST
Waste oi1
1
20,000
AST
Waste oil
1
10,000
AST
Waste oil
1
8,000
AST
Coal yard
Compressors
3
Cooling tower
Drum storage areas
Numerous
Gas, oil, and lube mobile truck
1
690
Oil/water separator
2
Transformers
38
The drainage area for Outfall 002 receives the majority of the storm water runoff from
the monomers, fibers, and resins production plants, which includes, at a minimum,
numerous above -ground storage tanks (ASTs) for POL and raw materials, unloading and
loading operations, coal storage, and transfer operations for piping between the ASTs and
the buildings. An absorbent boom is located at the discharge point of this outfall as an
additional preventive measure against a release of POL to the environment.

Secondary containment structures have been provided for all petroleum ASTs at the
plant. The SPCC plan documents the volume of these secondary containment structures.
Each secondary containment structure is constructed to contain the entire volume of all of
the tanks located within that containment area plus sufficient freeboard to allow for
precipitation. Should a containment structure fail resulting in a spill, DAK personnel are
properly trained to access the outfalls and contain the spill. A 1.4-aerc retention pond is
located to the southeast of Outfall 002 within this drainage area. This pond can be used
to divert and store any spills until appropriate clean up and disposal can be perfonned.
Dikes and manually operated valves are located in the ditches along the railroad
unloading area and the rail spur to contain any spills that may occur during unloading
operations. Sandbags are located at strategic locations near the coal-fired power plant to
contain any spills that may occur until clean up and disposal can be performed.
Another retention pond is located southwest of Outfall 002. This pond is used to retain
any storm water runoff from the coal storage area. Periodically the accumulated coal
dust sediment is dredged from the pond and disposed properly.
1.2 DRAINAGE AREA 002A
Storm water pollutant sources were not identified within this drainage area.
1.3 DRAINAGE AREA 003
Description Quantity Volume, gal Type
Ethylene glycol 1 20,000 AST
Dowthenn A in piping system 7,000
Compressors containing Solest 68 oil 2
Parking lot
Outfall 003 receives the storm water runoff from the parking lots, the resin's plant rail
loading and storage area, and the western portion of the fiber production building where
Dowthenn A and ethylene glycol, which are components that are utilized in the
production processes, are used.
In addition, Solest 68 oil is contained within two compressors located on the roof'of the
fiber production building.
The resin's plant was constructed in 2006-2007. This new construction, which added
impervious surface to this area, required a State Storrs Water Permit. As part of the
requirements for the State Storm Water Pen -nit (Pen -nit No. SW$ 060138), Storm Water
Pond Number 002R was constructed. It drains to Outfall 003. The permanent pool depth
is maintained at 3 feet. The forebay volume is approximately 20% of the basin volume.

The temporary pool controls runoff from the 1" storm event. The temporary pool draws
down in two to five days.
1.4 DRAINAGE AREA 003A
Description Quantity _ Volume, gal Type_
Polymer 1 2,000 AST
Railcar storage area and transportation
of raw materials (including terephthalic
acid (TPA) and ethylene glycol)
Railcars containing liquid raw materials, including ethylene glycol and TPA, pass
through this drainage area or are temporarily stored in this drainage area until unloading
or loading of the liquid raw materials can be performed. There is a potential for leaks or
spills from these railcars, but there is no containment provided in this area to contain any
spills or leaks before discharging to the outfall. In addition, polymer is stored in a
secondarily contained AST in this drainage area.
1.5 DRAINAGE AREA 003B
Description Quantity Volume, gal Type
Sodium hypochlorite
River water and fresh water pond
pumphouse
10,000 AST
A river water pumphouse is used to pump water from a tributary to the Cape Fear River
to the fresh water pond. A fresh water pumphouse located at the fresh water pond is used
to pump water from the fresh water pond to the plant. These two pumphouses are not
covered; therefore, any leaks from these pumps could be contacted by storm water. To
address this, the pumps are contained within a sandbag perimeter.
One 10,000-gallon sodium hypochlorite AST is located in this drainage area. This AST
is located within a concrete containment structure.
1.6 DRAINAGE AREAS 004 AND 005
Description Quantity Volume, gal Typeu
Land application fields
Sand blasting and painting operations
Railcar maintenance area
Wastewater sludge lagoon

Two land application fields and a wastewater sludge lagoon are located on the
southeastern corner of the property. The land application fields are permitted under
Permit No. WQ0012759 for the Land Application of Residual Solids (503 exempt). This
permit requires annual monitoring in every December of three groundwater wells located
in this drainage area. The wastewater sludge lagoon is permitted under Pen -nit No.
WQ0018087 for the Surface Disposal of Residual Solids (503 exempt).
Railcar maintenance occurs in the drainage area for Outfall 004. No POLs are used in
this area.
1.7 DRAINAGE AREA 006
Description -Quantity Volume, gal Type
Wastewater Treatment Plant
Hydrogen peroxide 1 7,500 AST
Emergency response fire training
AFFF, high expansion foam 1 1,000 AST
TPA, new monomers railcar storage area
The on -site wastewater treatment plant, monomers' rail car storage tracks, and the on-
side emergency fire training are located in the drainage area for Outfall 006. Hydrogen
peroxide and AFFF Liquid Foam are stored in this area. Hydrogen peroxide is stored in a
7,500 gallon AST and AFFF is stored in a 1,000-gallon plastic AST. Neither of these �° t See' '
ASTs have secondary containment. Secondary containment is not required for these 40 %U
tanks since neither of these products contain Section 313 Water Priority Pollutants. k.
�4x
A new monomers railcar storage area was constructed in 2006-2007. This new
construction, which added impervious surface to this area, required a State Storm Water
Permit. As part of the requirements for the State Storm Water Permit (Permit No. SW8
060138), Storm Water Pond Number 002R was constructed. It drains to Outfall 003.
The permanent pool depth is maintained at 3 feet. The forebay volume is approximately
20% of the basin volume.
The temporary pool controls runoff from the 1" storm event. The temporary pool draws
down in two to five days.
An absorbent boom is located at the discharge point of this outfall as an additional
preventive measure against POL releases to the environment
1.8 DRAINAGE AREA 007
Storm water pollutant sources were not identified within this drainage area.

1.9 DRAINAGE AREA 008
Storm water pollutant sources were not identified within this drainage area.
1.10 OTHER
Process sludge from the biological treatment plants is disposed of in a 12-acre sludge
lagoon. The runoff from the sludge lagoon and from two spray fields (which have been
out of service for years) is collected in a holding pond and pumped through the treatment
plant before release through NPDES regulated Outfall 001.
1.11 MANAGEMENT PRACTICES
The management practices used to protect storm water discharges are extensive. These
practices are covered in five documents that contain specific policies and procedures
regarding safety, health, and environmental matters. The entire documents are available
to NC DENR if required, but are too thorough to include as part of this application. The
documents can be summarized as follows:
Storm Water Pollution Prevention Plan
This document describes the outfalls, control measures, inspections, and other
information to prevent unpennitted discharges to storrn water outfalls.
Safety Manual
Cape Fear Site
This document defines DAK's approach to reducing transportation incidents involving
hazardous materials. The work defines hazardous materials, reviews the materials on
site, provides a list of contacts, details worker training requirements, references
publications, and covers shipping requirements, packaging, marking, labeling, placarding.
Railcar inspection, tank truck inspection, and loading and unloading procedures with
checklists are included. The inspection checklists are very explicity and written with the
primary focus of protecting workers and the environment from exposure to hazardous
substances.
Spill Prevention Control and Countermeasure Plan
This document establishes the procedures and prevention plans for preventing and
controlling spills. The focus of the document is related to petroleum products, but the
practices have a bearing on other chemicals at the site. A full inventory of petroleum
products at the site is presented, with location by location contingency plans and

countermeasures. Inspection frequencies and safeguards are discussed. Specific
attention is given to keeping spills and products from beign discharges through the storm
drains.
Hazardous Waste Permit Application
This document discusses the following subject areas: general security provisions,
inspection schedule; preparedness and prevention requirements; spill prevention,
containment, and countermeasures plan; and prevention of accidental ignition of ignitable
wastes. Specific procedures and policies relating to storm water runoff are discussed. In
summary, areas of activity relating to chemical transfer or storage are bermed and diked,
and transfer activities are prohibited in pending or actual precipitation conditions.
NPDES Permit No. 0000663 Renewal Application
This application includes specific details about the wastewater discharges from Outfall
001, Outfall 002, and Outfall 003. A facility description is provided, as well as treatment
schematics and analytical results pertaining to the outfalls. Since outfalls 002 and 003
correspond with storm water discharges, the permit conditions and the management
practices pertain to the storm water permit application.
A maintenance contractor provides lawn and landscaping services. Annually (in March)
fertilizer in a 8-8-8 or 10-10-10 ratio of nutrients is applied to approximately five acres at
roughly 200 pounds per acre. The only area of application is around the Administration
Building, Guard House, and Training Center. Most grassy areas are not maintained other
than mowing. Lime is applied in the sludge field on occasion, but this would not impact
the storm water since the drainage is collected and treated in the on -site wastewater
treatment facilities.
"Rodeo", a commercial herbicide, is used on the maintained areas, curbs, and fence lines
at an approximate rate of 1-1.4 ounces/gallon of water. Application of herbicide is two to
three times per year.
A small amount of pesticide (six ounces) was applied to ornamental shrubs near the plant
entrance in February 2008. Orkin provides control for fire ants and wasps upon request.
No other pesticides have been used within the last three years.
This limited use of lawn maintenance is significantly less than that practiced at most
urban commercial properties and does not have a tangible impact on the storm water
discharges from the facility.
C. See section above for a description of the existing structural and nonstructural control
measures to reduce pollutants in storm water runoff.
Oud'all Number I List of Codes from Table 2F- I

Outfall Number
(List)
List of Codes from Table 2F-1
001
1L, I-U, 2-D, 3-A, 3-13, 3-G, 4-A, 5-A, 5-J, 5-P
002
4-A
002A
4-A
003
4-A
003A
4-A
00313
4-A
004
4-A
005
4-A
006
4-A
007
4-A
008
4-A

EPA ID Number (copy from item f of Form 1) Form Approved. OMB No. 2040-0086
CC047369046 outfall oat 1 Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F)
Part A —You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grah Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
<5
NIA
Biological Oxygen
Demand (GODS)
13
Chemical Oxygen
Demand (COD)
35
Total Suspended
Solids (TSS)
54
Total Nitrogen
4.2
Total Phosphorus
0,51
pH
Minimum 7.4o
Maximum 7.40
Minimum
Maximum
Part B — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
{il available)
Maximum Values
(includo units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
EPA Form 3510-2F (1-92) Page VII-1 Continue on Reverse

EPA ID Number (copy from Item f of Form f) I Farm Approved. OMB No. 2040-0086
VCD047369046 Outfall 002A Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F)
Part A —You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(it available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
<5
NIA
Biological Oxygen
Demand (BOD5)
14
Chemical Oxygen
Demand (COD)
57
Total Suspended
Solids (TSS)
30
Total Nitrogen
3 . c
Total Phosphorus
0.36
pH
Minimum 6.50
Maximum 6.50
Minimum
Maximum
Part B — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(ifavailable)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
EPA Form 3510-2F (1-92) Page VII-1 Continue on Reverse

EPA ID Number (copy from Item I of Form 1 ) Form Approved. OMB No. 2040-0086
C0047369046 outfall 003 1 Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F)
Part A —You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details,
Pollutant
and
CAS Number
(if available)
Maximum Values
(includo units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
5
NIA
Biological Oxygen
Demand (BODS)
43
Chemical Oxygen
Demand (COD)
68
Total Suspended
Solids (TSS)
5
Total Nitrogen
1.4
Total Phosphorus
0,05
pH
Minimum 6.7o
Maximum 6,70
Minimum
Maximum
Part B— List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
GAS Number
(ifavaifable)
Maximum Values
{include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
EPA Form 3510-2F (1-92) Page VII-1 Continue on Reverse

EPA ID Number (copy from Item 1 of Form 1) Form Approved. OMB No. 2040-0085
CDO47369046 Outfall 003A I Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F)
Part A -- You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
a
NIA
Biological Oxygen
Demand (BODS)
2
Chemical Oxygen
Demand (COD)
13
Total Suspended
Solids (TSS)
2
Total Nitrogen
1.4
Total Phosphorus
. oz
PH
Minimum 6.6o
Maximum 6.60 1
Minimum
Maximum
Part 8 — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
EPA Form 3510-2F (1-92) Page VII-1 Continue on Reverse

EPA ID Number (copy from Item f of Form f) Form Approved. OMB No. 2040-0086
CDO47369046 Outfall 003B 1 Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F)
Part A — You must provide the results of at least one analysis for every pollutant in this table. Camplele one liable for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(ifavadabfe)
Maximum Values
finciude units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
<5
NIA
Biological Oxygen
Demand (BODS)
`�
Chemical Oxygen
Demand (COD)
25
Total Suspended
Solids (TSS)
2
Total Nitrogen
0.17
Total Phosphorus
o-02
pH
Minimum 6,70
Maximum 6,70
Minimum
Maximum
Part B — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
EPA Form 3510-2F (1-92) Page VII-1 Continue on Reverse

EPA ID Number (copy from Item 1 of Form 1) Form Approved. OMB No. 204MO86
CDC47369046 Outfall 004 I Approval expires5-31-92
VII. Discharge information (Continued from page 3 of Form 2F)
Part A — You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
Pollutant
and
GAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
<5
NIA
Biological Oxygen
Demand (BOD5)
a2
Chemical Oxygen
Demand (COD)
34
Total Suspended
Solids (TSS)
4
Total Nitrogen
1.4
Total Phosphorus
0.04
PH
Minimum 6,-70
Maximum 6.70
Minimum
Maximum
Part B — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each oullall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
EPA Form 3510-2F (1-92) Page VII-1 Continue on Reverse

EPA ID Number (copy from /tern 1 of Form 1) Form Approved. OMB No. 2040-0086
CDO47369046 Outfall 005 1 Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F)
Part A — You must provide the resuffs of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(1f available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
NIA
No flow
Biological Oxygen
Demand (BOD5)
Chemical Oxygen
Demand (COD)
Total Suspended
Solids (TSS)
Total Nitrogen
Total Phosphorus
pH
Minimum
Maximum
Minimum
Maximum
Part B — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the fddlity is operating undei an exisliny NPDES permit). Complete one table for each outfall. See the insbucliows for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
EPA Form 3510-2F (1-92) Page VII-1 Continue on Reverse

EPA ID Number (copy from Item f of Form f) Form Approved. OMB No. 2040-0086
cD047369046 outfall 006 1 Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2FJ
Part A — You must provide the resuhs of at least one analysis for every pollutant in this table. Complete one (able for each outfatl. See instructions for additional details.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grat> Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
a5
NIA
Biological Oxygen
Demand (BOD5)
2
Chemical Oxygen
Demand (COD)
2B
Total Suspended
Solids (TSS)
21
Total Nitrogen
1.5
Total Phosphorus
0.12
pH
Minimum 7.3o
Maximum 7.30
Minimum
Maximum
Part B — List each pollutant that is limited in an effluent guideline which the tacility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
{include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flaw -weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
EPA Form 3510-2F (1-92) Page VII-1 Continue on Reverse

EPA ID Number (copy from Item f of Form 1) Farm Approved, OMB No. 2040-0086
CDO47369046 Outfall 007 1 Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F)
Part A -- You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details,
Pollutant
and
CAS Number
(rfavailable)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
<s
NIA
Biological Oxygen
Demand (BOD5)
4
Chemical Oxygen
Demand (COD)
40
Total Suspended
Solids (TSS)
47
Total Nitrogen
1.4
Total Phosphorus
0.18
pH
Minimum 7.20
Maximum 7.20
Minimum
Maximum
Part B — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
EPA Form 3510.2F (1.92) Page VII-1 Continue on Reverse

EPA ID Number (copy from Item 1 of Form 1) Form Approved. OMB No. 2040-0086
NCD 047369046 outfall Doe 1 Approval expires 5-31-92
VII. Discharge information (Continued from page 3 of Form 2F)
Part A — You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 2D
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
<5
NIA
Biological Oxygen
Demand (BOD5)
2
Chemical Oxygen
Demand (COD)
35
Total Suspended
Solids (TSS)
5
Total Nitrogen
1.5
Total Phosphorus
0.04
pH I
Minimum 6,5a
Maximum 6.50
Minimum
Maximum
Part 6 — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each outfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
EPA Form 3510-2F (1-92) Page VII-1 Continue on Reverse

Continued from the Front
Part C - List each pollutant shown in Tattle 2F-2, 2F-3, and 2F-4 that you know or have reason to believe is present. See the instructions for additional details and
requirements. Complete one table for each outfaff.
Pollutant
and
CAS Number
(d available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Part D — Provide data for the storm event(s) which resulted in the maximum values for the flow weighted composite sample-
1.
Date of
Storm
Event
2.
Duration
of Storm Event
(in minutes)
3.
Total rainfall
during storm event
(in inches)
4.
Number of hours between
beginning of storm measured
and end of previous
measurable rain event
5.
Maximum flow rate during
rain event
(gallons/minufe or
specify units)
6.
Total flow from
rain event
(gallons or specify units)
02/13/00
160 minutes
0.75 inches
264 hours
7. Provide a description of the method of flow measurement or estimate.
All outfalls were sampled during the 2/13/08 rain event.
EPAForm 3510-2F (1-92) Page VII-2

'�
',envirochem:n�r
Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (lax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE N94, DLS CIiRTIFICNFE #37729
Customer:
DAK - AMERICAS —CAPE FEAR PLANT
Post Office Box 2260
Leland, NC 28451
Attn: Bertha Bland
REPORT OF ANALYSIS
Date Sampled: 02/13/08
Sampled By: Larry Young / James I-Iines
STORMWATER:
Date of Report: February 22, 2008
Purchase Order No.: 4500064371
Report Number:
Report To:
Project No:
8- 1460
Bertha Bland
Page 1 of 2
Parameter
008
003
003A
003B
Date
# 2817
# 2818
# 2819
# 2820
Analyzed
Biochemical Oxygen Demand,
2
43
2
< 2
2/13/08
BOD5 as 02 mg/L SM 52.10 B
Chemical Oxygen Demand, COD mg/L
35
68
13
25
2/18/08
SM 5220 D
Oil & Grease, mg/L
< 5
5
8
< 5
2/18/08
EPA 1664 A
Total Suspended Solids, TSS mg/L
5
5
2
< 2
2/19108
SM 2540 D
Nitrate + Nitrite Nitrogen,
0.02
0.10
0.07
0.03
2/.18/08
NO3+NO2-N mg/L SM 4500 NO3-E
Total Kjeldahl Nitrogen, TKN mg/L
1.5
1.3
1.3
0.7
2/21/08
SM 4500 NH,-B-C
Total Nitrogen, as N mg/L
1.5
1.4
1.4
0.7
2/21/08
SM 4500 NO3-E & SM 4500 NH3-B-C
Total Phosphorus, as P mg/L
0.04
0.05
0.02
0.02
2/19/08
SM 4500 P-B-E
Comments:

ANALYTICAL & CONSULTING
CHEMISTS
Customer: DAK Americas
STORM WATER:
Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsutown Road • Manteo, NC 27954
[phone]
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Report 8-1460
Page 2 of 2
Parameter
002A
002
007
006
004
Date
# 2821
# 2822
# 2823
# 2824
# 2825
Analyzed
Biochemical Oxygen Demand,
14
13
4
2
< 2
2113/08
RODS as Oi mg/L SM 5210 B
Chemical Oxygen Demand, COD mg/L
51
35
40
28
34
2/18/08
SM 5220 1)
Oil & Grease, mg/L
< 5
< 5
< 5
< 5
< 5
2/18/08
EPA 1664 A
Total Suspended Solids, TSS mg/L
30
54
47
21
4
2/19/08
SM 2540 D
Nitrate + Nitrite Nitrogen,
0.82
1.11
0.05
0.09
0.05
2/18/08
NO3+NO2-N mg/L SM 4500 NO3-E
Total Kjeldahl Nitrogen, TKN mg/L
2.2
3 1
13
1.4
1.3
2/21/08
SM 4500 Nt13-B-C
Total Nitrogen, as N mg/L
3.0
4.2
1.4
1.5
1.4
2/21/08
SM 4500 NO3-E & SM 4500 NH3-B-C
Total Phosphorus, as P mg/L
0.36
0.51
0.18
Oa l2
0-04
2/19/08
SM 4500 P-B-E
Comments:
Reviewed by: r

nv rochem.
t-onectea isy• _�,g ���{�„ yocc•v4
CSmnle Tvne! 1 = Influent_ F. = FM;
ENVIRONMENTAL CHEMISTS, INC
Sample Collection and Chain of Custody
W =Wall_ CT=Rtrpam_ C(1 =Cnil CI.= Clnrlup n*hpr-
6602 Windmill Way
Wilmington, NC 28405
Phone: [phone]
Fax [phone]
No: () —
Sample Identification
m
X
z
Collection
a d
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0 0
96
U"
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= E
U
PRESERVATION
ANALYSIS REQUESTED
Wz
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x
p
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DATE
TIME
TEMP
Outfali.�d 8 PH:
C
'O,�i
X
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0&G$0D,C0D,T9S,Tot91
N,Total P
od
M?l S
outfall: pH
bd� • 7
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X
X
O&G,BOD,COD,TSS,Total
N,Total P
6
Outfall:
Q�iJ�f% pH:
Z� of
C
X
X
O&G,BOD,COD,TSS,Total
N,Total P
Outfall .6-)03B pH: 6, 7
Z Zp
4
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X
X
O&G,BOD,COD,TSS,Total
N,Tatal P
Q Y.P7
OutfalL•6w,0i pH: �v C
C9"&-7I
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b
Outfoll �a pH.
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O&G,BOD,COD,TSS,Total
N,Total P
Outfall: r� pH:
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of 93
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X
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O&G,BOD,COD,TSS,Total
N,Total P
o > a
(05
Outfall:
Od sa pH: 73
a$a�
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X
X
O&G,BOD,COD,TSS,Total
N,Total P
D Fq7
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Outfall:�a r{ pH: 6, 7
^�
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, X-N,Total
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O&G,BOD,COD,TSS,Total
P
d E6
Outfall: pH:
C
X
X
O&G,BOD,COD,TSS,Total
N,Tatal P
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
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2.
Temperature wh n ceived: •�{= Acc ted: ✓ Rej ted: Resample Requ sted:
Delivered By• 7z Received B ' Date• Time::
Alai�i L
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y

SIC S 000 39 a
DAK Americas
Cape Fear Site
PO Box 2260
Leland, NC 28451
February 1, 2011
Ms Coleen Sullins
Division of Environmental Management
North Carolina Department of Environment,
& Natural Resources
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Dear Ms Sullins:
In accordance with DAK Americas procedures, and pursuant to 40CFR 270.11 (a)(1)(ii),
and (b) and 40CFR 122.22 (a)(1)(ii) and (b), and all applicable State Regulations, I,
Leroy N. Butler, Manager of the DAK Americas Cape fear Site in Brunswick County,
North Carolina, delegate my authority to sign all routine reports required by permits, and
provide other information requested by the State and/or Federal Regulatory Agencies to
the Operations Director of Sustainability.
My delegation of this authority is consistent with the normal responsibility of these
positions with DAK Americas.
Sincerely,
Od
�D
Leroy N. But]
D� 2�11 Ca e Fear Site Manager
9 p �
FHB �
R
Cape Fear Site • 3500 Daniels Road NE • P.O. Box 2260 • Leland, NC 28451
877-432-2766 (toll -free) • 910-371-4000 (phone) • 910-371-4179 (fax)
www.dakamericas.com

l'?1KVe,J; - e2 imS
DAK Americas
FIBERS, MONOMERS & RESINS
March 4, 2008
50
Mr. Bradley Bennett I
Environmental Program Supervisor
Stormwater Permitting Unit C. ;� d
Division of Water Qualityg
North Carolina Department of Environment and Natural Resources `}
1617 Mail Service Center j
Raleigh, North Carolina 27699-1617 ll
v
Subject: Renewal Application for Stormwater Discharge Permit 0
Permit No. NCS000392
DAK Americas LLC
Cape Fear Site y -�
3500 Daniels Road (P.O. Box 2240)
Leland, Brunswick County, North Carolina 28451 (28451) g CD
Jo
Dear Mr. Bennett: k
This application is to request that stormwater discharge permit NCS000392 which
expires August 31, 2008 be renewed. As a part of this submittal, US EPA Forms I and
2F are attached. This permit covers ten outfalls that discharge to the Cape bear River or
its tributaries.
If you have any questions please call Elizabeth Wilke at [phone].
Sincerely,
l
Matt Warrick
Cape Fear Site Manager
DAK Americas LLC
3500 Daniels Road, N.E. • Leland, NC 28451
1-877-432-2766

Form
U.S. Environmental Protection Agency
EPA I.D. Number
EPA General Information
1
General
Consolidated Permits Program
NCD047369046
Read the "General Instructions"
before starting)
\\ \\ \\L\a' 61"1tBni3\\\\ \
General Instructions
�l\EPA�I�D�Niatnber \\\\\\\�
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If a preprinted label has been provided, affix it in the designated
space. Review the information carefully; if any of it is incorrect,
;Name \\\\\\\
cross through it and enter the correct data in the appropriate fill-
�l II\Facilit
\\�\
\D`AWAmeri1cas�ELC
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in area below. Also, if any of the preprinted data is absent (the
area to the left of the label space lists the information that
�Ma�lln .Address\\\\
\
\\\DAWAmeri1casELC
N:E:
should appear), please provide it in the proper fill-in area(s)
below. If the label is complete and correct, you need not
complete Items, 1, II, V, and VI (except V!-B which must be
ffi\
\
Leland-ACW451 \
\
\
completed regardless). Complete all items if no label has been
\Vl,\Faclllty\,Locatt6
provided. Refer to the instructions for detailed item descriptions
\\ \\\
\\\\\\\\\
and for the le al authorizations under which this data is
g
collected htt :Ilwww.epa.gov/npdesipubs/form 1, d€ .
II. Pollutant Characteristics
Instructions: Complete A through J to determine whether you
need to submit any permit application forms to the EPA. If you
answer "yes' to any questions, you must submit this form and the supplemental form listed in the parenthesis following the
question. Mark "X" in the box in the third column if the supplemental
form is attached. If you answer "no" to each question,
you need not submit any of these forms. You may answer
"no" if your activity is excluded from permit requirements; see
Section C of the instructions. See also, Section D of the instructions for definitions of bold-faced terms.
Specific Questions
Mark X
Specific Questions
Mark 'X'
Yes
No
Form
Yes
No
Form
Attached
Attached
A. Is this facility a,publicly owned treatment
_ _
B. Does or will this facility (either existing or
works which results in a discharge to waters
proposed) include a concentrated animal
of the U.S.? (Form 2A)
❑
XC�
❑
feeding operation or aquatic animal
❑
❑X
❑
production facility which results in a
discharge to waters of the U.S.? Form 213
C. Is this a facility which currently results in
D. Is this a proposed facility (other than those
discharges to waters of the U.S. other than
XO
❑
described in A or above) which will result in a
❑
❑X
❑
those described in A or B above? Form 2C
discharge to waters of the U.S.? Form 2D
E. floes or will this facility treat, store, or
F. Do you or will you inject at this facility
dispose of hazardous wastes? (Form 3)
❑
XC�
❑
industrial or municipal effluent below the
lowermost stratum containing, within one
❑
❑X
❑
quarter mile of the well bore, underground
sources of drinking water? Form 4
G. Do you or will you inject at this facility any
H. Do you or will you inject at this facility fluids
produced water or other fluids which are
for special processes such as mining of sulfur
brought to the surface in connection with
by the Frasch process, solution mining of
conventional oil or natural gas production, inject
❑
❑X
❑
minerals, in situ combustion of fossil fuel, or
❑
0
❑
Fluids used for enhanced recovery of oil or
recovery of geothermal energy? (Form 4)
natural gas, or inject fluids for storage of liquid
hydrocarbons? Form 4
I. Is this facility a proposed stationary source
J. Is this facility a proposed stationary source
which is one of the 28 industrial categories
which is NOT one of the 28 industrial
listed in the instructions and which will
categories listed in the instructions and which
potentially emit 100 tons per year of any air
❑
❑X
❑
will potentially emit 250 tons per year of any air
❑
❑X
❑
pollutant regulated under the Clean Air Act and
pollutant regulated under the Clean Air Act and
may affect or be located in an attainment
may effect or be located in an attainment
area? Form 5
area? Form 5
III. Name of Facilit
DAK Americas LLC Cape Fear Site
1V. Facility Contact
A. Name & Title last first & title
B. Phone area code & no.
Elizabeth Martin Environmental Engineer
910 371-0448
V. Facility Mailing Address
A. Street or P.O. Box
PO Box 2260
B. City or Town
C. State D. Zip Code
Leland, NC 28451
VI. Facility Location
A. Street, Route No. or Other Specific Identifier
3500 Daniels Road, N.E.
B. County Name
Brunswick
C. City or Town
D. State
E. Zip Code
F. County Code
Leland
NC
28451
019
EPA Form 3510-1 (Rev. 10-80)

Continued From The Front
VI I. SIC Codes (4-digit, in order of priority)
A. First
B. Second
2865
Cyclic Organic Crudes and Intermediates, and
Organic Dyes and Pigments
2824
Manmade Organic Fibers, Except Cellulosic
C. Third
D. Fourth
2821 Plastic Materials, Synthetic Resins, and Non-
vulcanizable Elastomers
VIII. Operator Information
A. Name
B. Is the name listed
DAK Americas LLC
in Item VIII-A also
the owner?
❑X Yes ❑ No
C. Status of Operator Enter the appropriate letter into the answer box; if "0ther", specify.)
D. Phone area code & no.
F = Federal M = Public (other than federal or state)
S = State O = (specify) P
P = Private
(specify) Private
[phone]
E. Street or P.O. Box
3500 Daniels Road, N.E.
F. City or Town
G. State
H. Zip Code
IX. Indian Land
Leland
NC
28451
Is the facility located on Indian lands?
❑ Yes ❑X No
X. Existinq Environmental Permits
A. NPDES Dischar es to Surface Water
D. PSD Air Emissions from Proposed Sources
NCO000663
B. U I C (Underground Injection of Fluids)
E. Other (specify)
(specify)
See attached table for complete list of permits.
C. RCRA (Hazardous Wastes)
XI. Ma
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show
the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its hazardous waste
treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs, rivers and other surface
water bodies in the map area. See instructions for precise re uirements.
XII. Nature of Business rovide a brief descri tion
The Cape Fear Site has three production operations: (1) Monomers, (2) Fibers, and (3) Resins. The monomers production
area supplies raw materials to the Fibers and Resins operations.
Monomers is divided into terephthalic acid (TPA) production lines and an Ingredient Recovery process for the separation
and recovery of raw materials for reuse. In addition, there is a Glycol Recovery Unit.
The Direct Couple Oligomer (DCO) area, followed by the continuous polymerization (CP) production lines, convert TPA into
polymer (PET -polyethylene terephthalate). Product from DCO and CP is further processed in the Fibers and Resins areas.
The Fibers area (also called Staple area) produces PET fiber and packages the fibers into bales.
The Resins operation manufactures polyester chips, which DAK's customers use to produce various plastic items for
industrial and/or consumer use. The polyester chips are manufactured in a solid state polymerization process.
XIII. Certification see instructions
1 certify under penalty of law that 1 have personally examined and am familiar with the information submitted in this application and all
attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in the
application, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for submitting
false information including the possibilit of fine and imprisonment.
Name & Official Title (type or print)
Matt Warrick
Cape Fear Site Manager
B. Signature C. Date Signed
k�/' I - 7
EPA Form 3510-1 (Rev. 10-80) Reverse

DAK Americas LLC
Cape Fear Site
List of Permits
Issuing Agency
Type of Permit
ID Number
NCDENR
NPDES
NC0000663
NCDENR
Stormwater Permit
NCS000392
NCDENR
Land Application of Wastewater
Residuals
WQ0012759
NCDENR
Erosion and Sediment Control
Permit
Bruns-2006-372
NCDENR
NC State Stormwater Permit
SW8 060138
NCDENR
NC DENR Air Permit
03033T36
NCDENR
RCRA
NCD047369046
USCOE
Outfall Permit
Channel No. 12-67

EPA ID Number (copy from Item f of Form 1) Form Approved. OMB No. 2040-0086
Please orintortvoe in the unshaded areas only. kCD047369046 Approval expires 5-31-92
FORM
ZF
NPDES
U.S. Environmenta€ Protection Agency
®� Washington, DC 20460
Application for Permit to Discharge Storm Water
Discharges Associated with Industrial Activity
Paperwork Reduction Act Notice
Public reporting burden for this application is estimated to average 28.6 hours per application, including time for reviewing instructions, searching existing data sources,
gathering and maintaining the data needed, and completing and reviewing the collection of information. Send comments regarding the burden estimate, any other aspect
of this cotiection of information, or suggestions for improving this form, including suggestions which may increase or reduce this burden to: Chief, Information Policy
Branch, PM-223, U.S. Environmental Protection Agency, 1200 Pennsylvania Avenue, NW, Washington, DC 20460, or Director, Office of Information and Regulatory
Affairs, Office of Management and Budget, Washington, DC 20503,
I. Outfall Location
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. Outfall Number
(list)
B. Latitude
C. Longitude
D. Receiving Water
(name)
See Attachment I.
II. Improvements
A. Are you now required by any Federal, Slate, or local authority to meet any implementation schedule for the construction, upgrading or operation of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited
to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions.
1. Identification of Conditions,
Agreements, Etc.
2. Affected Outfalls
3. Brief Description of Project
4, Final
Compliance Hate
number
source of discharge
a. req.
b. proj.
See Attachment II.
B: You may altach additional sheets describing any additional water pollution (or other environmental projects which may affect your discharges) you now have under
way or which you plan. Indicate whether each program is now under way or planned, and indicate your actual or planned schedules for construction.
III. Site Drainage Map
Attach a site map showing topography (or indicating the outline of drainage areas served by the outfalls(s) covered in the application if a topographic map is unavailable)
depicting the facility including: each of its inlake and discharge structures; the drainage area of each storm water outfall; paved areas and buildings within the drainage
area of each storm water outfall, each known past or present areas used for outdoor storage of disposal of significant materials, each existing structural control measure
to reduce pollutants in storm water runoff, materials loading and access areas, areas where pesticides, herbicides, soil conditioners and fertilizers are applied; each of
its hazardous waste treatment, storage or disposal units (including each area not required to have a RCRA permit which is used for accumulating hazardous waste
under 40 CFR 262.34 ); each well where fluids from the facility are injected underground; springs, and other surface water bodies which received storm water discharges
from the facility.
EPA Form 3510-2F (1-92) Page 1 of 3 Continue on Page 2

Continued from the Front
IV. Narrative Description of Pollutant Sources
A, For each outfall, provide an estimate of the area (include units) of imperious surfaces (Including paved areas and building roofs) drained to the curtail, and an estimate of the total surface area
drained by the outfall.
outfall
Area of Impervious Surface
Total Area Dminetl
Outfarl
Area of Impervious Surface
Total Area Drained
Number
(provide units)
(provide units)
Number
(provide units)
(provide vnits)
see attachment IV.
B. Provide a narrative description of significant materials that are currently or in the past three years have been treated, stored m disposed in a manner to allow exposure
to storm water; method of treatment, storage, or disposal; past and present materials management practices employed to minimize contact by these materials with
storm water runoff; materials loading and access areas, and the location, manner, and frequency in which pesticides, herbicides, soil conditioners, and Terlilizers are
applied.
see attachment IV.
C. For each outfall, provide the location and a description of existing structural and nonstructural oontrol measures to reduce pollutants in storm waler runoff; and a
description of the treatment the storm water receives, including the schedule and type of maintenance for conlrvt and treatment measures and the ultimate disposal
of any solid or fluid wastes other than by discharge.
outfall
List Codes from
Number
Treatment
Table 2F-1
See attachment IV.
V. Nonstormwater Discharges
A. I certify under penally of law hat the outfall(s) covered by this application have been tested or evaluated for the presence of nonstormwater discharges, and that all
nonstormwater discharged from these outfaii(s) are identified in either an accompanying Form 2C or From 2E application for the outfall.
Name and Official Title (type or print)
Signature
Date Signed
Matt Warrick, Site Manager
!+
+�� 1 f
iw�! WWW
% ?5,cy—l' .er\�-
v CCC/// ___]]] vLJC]
8. Provide a description of the method used, the dale of any testing, and the onsiite drainage points that were directly observed during a test,
outalls covered by this application were evaluated for non-stormwater discharges by dry weather observations of outfalls and
other appropriate observation locations and the analysis and validation of accurate piping schematics. outfalls 001, 002, and
003 are covered by NPDES permit; although as much or maore attention was devoted to these outfals due to the association of
these outfalls with the industrial activity. outfalls 002A, 003A, 003B, 004, 005, 006, 007 were carefully inspected on several
occasions. No industrial activities that would be associated with a discharge take place in the regions of Outfalls 002A, 003a,
005, 007, or 006 were observed. outfall 003A, 004, and 005 had no perceptible dry weather flow and outfall oo6 showed no
indication that the natural seepage was related to the treatment plant located nearby.
I. Significant Leaks or Spills
Provide existing information regarding the history of significant leaks or spills of toxic or hazardous pollutants at the facility in the last three years, including the
approximate date and location of the spill or leak, and the type and amount of material released,
None.
EPA Form 3510-2F (1-92) Page 2 of 3 Continue on Page 3

EPA36ID 90a6umber(copyfromltem 1 of Form f)
Continued from Page 2 INCO047
VII. Discharge Information
A, B, C, & D: See instructions before proceeding. Complete one set of tables for each outfall. Annotate the outfall number in the space provided.
Table VII-A, VII-B, VII-C are included on separate sheets numbers VII-1 and VII-2.
E. Potential discharges not covered by analysis — is any toxic pollutant listed in table 2F-2, 2F-3, or 2F.4, a substance or a component of a substance which you
currently use or manufacture as an intermediate or final product or byproduct?
0 Yes (list all such pollutants below) Q No (go to Section IX)
Ill. Biological Toxicity Testing Data
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to our discharge within the last 3 years?
Yes (list all such pollutants beiow) ✓❑ No (go to Section IX)
IX, Contract Analysis Information
Were any of the analyses reported in Item VI performed by a contract laboratory or consulting firm?
© Yes (list the name, address, and telephone number of, and pollutants JE:]No (go to Section X)
analyzed by, each such laboratory or firm below)
A. Name
B. Address
C. Area Code & Phone No.
D. Pollutants Analyzed
Environmental Chemists
6602 windmill way
1910) 392-0223
GODS, COD, Oil s Grease,
Wilmington, NC 28405
TSS, Nitrate + Nitrite
Nitrogen, Total Kjeldahl
Nitrogen, Total Nitrogen as
N, Total Phosphorus as P
X. Certification
1 certify under penalty of law that this document and all attachments were prepared under my direction or supervision in occordance wrlh a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that
there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations,
A. Name & Official Title (Type Or Print)
B. Area Code and Phone No,
Matt Warrick, Site Manager
[phone]
C. Signature
D, Date Signed
—^
R �.�
l / rL / r V
EPA Forrx 3510 2F (1-92) v Page 3 of 3

EPA ID Number (copy from item 1 of Form 1) Form Approved. OMB No. 2040-0086
CD047369046 I Approval expires 5.31.92
VIL Discharge information (Continued from page 3 of Form 2F)
Part A — You must provide the results of at least one analysis for every pollutant in this table_ Complete one (able for each outfall. See instructions for additional details.
Pollutant
and
CAS Number
(ifavailable)
Maximum Values
{include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Oil and Grease
N/A
see Attachment vzr,
Biological Oxygen
Demand (BOD5)
Chemical Oxygen
Demand (COD)
Total Suspended
Solids (TSS)
Total Nitrogen
Total Phosphorus
pH
Minimum
Maximum
Minimum
Maximum
Part B — List each pollutant that is limited in an effluent guideline which the facility is subject to or any pollutant listed in the facility's NPDES permit for its process
wastewater (if the facility is operating under an existing NPDES permit). Complete one table for each oulfall. See the instructions for additional details and
requirements.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
EPA Form 3510-2F (1-92) Page VII-1 Continue on Reverse

Continued from the Front
Part C - List each pollutant shown in Table 2F-2, 2F-3, and 2F-4 that you know or have reason to believe is present. See the instructions for additional details and
requirements. Complete one table for each ouffall.
Pollutant
and
CAS Number
fifavairable)
Maximum Values
(include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Grab Sample
Taken During
First 20
Minutes
Flow -Weighted
Composite
Part D — Provide data for the storm evert(s) which resulted in the maximum values for the flow weighted composite sample.
1.
Date of
Storm
Event
2.
Duration
of Storm Event
(in minutes)
3.
Total rainfall
during storm event
(in inches)
4.
Number of hours between
beginning of storm measured
and end of previous
measurable rain event
5.
Maximum flow rate during
rain event
(gallonsJminufe or
specify units)
6,
Total flow from
rain event
(gallons or specify units)
7. Provide a description of the method of flow measurement or estimate.
EPA Form 3510-2F (1-92) Page VII-2

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Outfall 001 DAK Americas
Latitude : 34019'05"N CAmericas LLC
Longitude: 78001'40"W 3500 Cape Fear Site
Stream Class: C Daniel Road, N.E.
Lela
Receiving Stream: Cape Fear River Leland, NC 28451 FIBERS,MONOMERSB RESINS

Attachment I. Outfall Location
All storm water from the property drains to one of ten outfalls (Outfalls 002, 002A, 003, 003A, 003B, 004, 005, 006, 007, or 008), all
of which ultimately discharge to the Cape Fear River. The outfall number, the area that drains to the outfall, and the receiving stream
are listed below:
A.
Outfall
Number
D. Receiving Water
Total Area
o (List)
B. Latitude
C. Longitude
(name)
Drained
Portion of Property Drained
001
34"
19'
05"
780
01'
40"
Cape Fear River
NA
Outfall 001 discharges treated wastewater
from the site's wastewater treatment plant. It
is covered under NPDES permit NC0000663.
002
340
19'
28"
780
02'
26"
Dalliscn's-Swamp
138 acres
Monomers manufacturing areas
002A
340
19'
41"
780
02'
32"
Doll' wamp
32 acres
Northwest portion of the property
003
340
19'
14"
780
03'
04"
Tributary to Bay Branch
V 66 acres
West and southwest portion of property
003A
340
19'
23"
78"
02'
57"
Tributary to Bay Branch
/ 23 acres
West portion of property
003B
340
19'
57"
78"
03'
04"
Bay Branch ;/
18 acres
Freshwater intake pond and pump station
004
340
18'
35"
78"
02'
12"
Otter Branch j
195 acres
South portion of the property
005
34°
18,
42"
78°
01,
55"
Dollison's Swamp 1 /
58 acres
Southeast portion of property
006
34"
18,
35"
78°
02'
12"
r
Dollison's Swamp V
65 acres
Eastern portion of property, new rail storage
area
007
340
19,
19"
780
02'
03"
Doll isori Wamp
9 acres
Northeast portion of property
008
340
18'
53"
78°
03'
12"
Mulberry Branch
18 acres
Southwest portion of property

Attachment 11.
The site's NPDES Permit No. NC0000663 became effective February 1, 2008. 1n this recently
renewed permit, the site is required to meet a Total Suspended Solids limit of 75 mgll for the
monthly average and 150 mg/L for the daily maximum for Outfall 002. This new limit will
become effective August 1, 2009. A copy of the permit is attached.

General Permit
Part 8 — Sector -Specific Requirements for Industrial Activity
Subpart C — Sector C — Chemical and Allied Products Manufacturing, and Refining.
You must comply with Part 8 sector -specific requirements associated with your primary
industrial activity and any co -located industrial activities, as defined in Appendix A. The sector -
specific requirements apply to those areas of your facility where those sector -specific activities
occur. These sector -specific requirements are in addition to any requirements specified
elsewhere in this permit.
8.C.1 Covered Stormwater Discharges.
The requirements in Subpart C apply to stormwater discharges associated with industrial
activity from Chemical and Allied Products Manufacturing, and Refining facilities, as identified
by the SIC Codes specified under Sector C in Table D-1 of Appendix D of the permit.
8.C.2 Limitations on Coverage.
8.C.2.1 Prohibition of Non .Slorrn4raler Discharges. (See also Part 1.1.4) The following are not
covered by this permit: non-stormwater discharges containing inks, paints, or
substances (hazardous, nonhazardous, etc.) resulting from an onsite spill, including
materials collected in drip pans; washwater from material handling and processing
areas;'and washwater from drum, tank, or container rinsing and cleaning.
8.C.3 Sector -Specific Benchmarks
Table 8.C-1 identifies benchmarks that apply to the specific subsectors ol'Sector C.
These benchmarks apply to both your primary industrial activity and any co -located industrial
activities.
Stormwater Discharges Associated with Industrial Activity —Sector C
t,,,AjVMAA, A -
SODcioo� O
51

t/
General Permit
Table 8.C-1.
Subsector
(You may be subject to requirements for
more than one sector/subsector)
Parameter
Benchmark Monitoring
Concentration
Subsector C1. Agricultural Chemicals (SIC
2873-2879)
Nitrate 2lus Nitrite Nitrogen
0.68 mg/L
Total Lead
Hardness Dependent
Total Iron
1.0 mg/L
Total Zinc'
Hardness Dependent
Phos horns
2.0 mg/L
Subsector C2. Industrial Inorganic Chemicals
(SIC 2812-2819)
Total Aluminum
0.75 m L
Total Iron
1.0 mg/L
Nitrate plus Nitrite Nitrogen
0.68 mg/L
Subsector C3. Soaps, Detergents, Cosmetics,
and Perfumes (SIC 2841-2844)
Nitrate plus Nitrite Nitrogen
0.68 mg/L
Total 'Zinc'
Hardness Dependent
Subsector C4, Plastics, Synthetics, and Resins
(SIC 2821-2824)
Total Zinc'
Hardness Dependent
The benchmark values of some metals are dependent on water hardness. For these parameters, permittees must
determine the hardness of the receiving water (see Appendix J, "Calculating Hardness in Receiving Waters for
Hardness Dependent Metals," for methodology), in accordance with Part 6.2,1,1, to identify the applicable `hardness
range' for determining their benchmark value applicable to their facility. The ranges occur in 25 mg/L increments.
Hardness Dependent Benchmarks follow in the table below:
Water
Hardness
Range
Lead
(mg/L)
Zinc
(mg/L)
0-25 mg/L
0.014
0.04
25-50 mg/L
0.023
0.05
50-75 mg/L
0.045
0.08
75-100 mg/L
0.069
0.11
100- l 25 mg/L
0.095
0.13
125-150 mg/L
0.122
0.16
150-175 mg/L
0.151
0.18
175-200 mg/L
0.182
0.20
200-225 mg/L
0.213
0.23
225-250 mg/L
0.246
025
250f mg/L
0.262
0.26
8.C.4 Effluent Limitations Based on Effluent Limitations Guidelines (See also Part 6.2.2.1
of the permit.)
Table KC-2 identifies effluent limits that apply to the industrial activities described
below. Compliance with these effluent limits is to be determined based on discharges from these
industrial activities independent of commingling with any other wastestreams that may be
covered under this permit.
Stormwater Discharges Associated With Industrial Activity — Sector C 52

General Permit
Table S.C-2'
Industrial Activity
Parameter
Effluent Limit
Runoff from phosphate fertilizer
manufacturing facilities that comes into
contact with any raw materials, finished
product, by-products or waste products
(SIC 2874)
Total Phosphorus (as P)
105.0 m > L, daily maximum
35 mg/L,
30-dayavg.
Fluoride
75.0 mg/L
daily maximum
25.0 mglL,
30-day avg.
1 Monitor annually.
Stormwater Discharges Associated With Industrial Activity — Sector C
53

6 -pa-1 -1
2/xr1/2011 EPA I Envirofa b4u�_F[1LILLRQ..
http:l/oaspub.epa.g o�lenvirolmultlsys 2.get_list_lri7tri_fac_itl=28a51 DpN7Wo205TA TE
a ifti Envirofacts Data Warehouse Last updated on Friday, February 11, 2011
5
You are here: EPA Home Env irofacts Mull Report
'i Ma+tcl
(�_ f MultiSystem Report
Erwiia?acts r—DAK MONOMERS LLC
,3500-DANIELS-ROAD-NORTHEAS
LELAND, NC 28451
Map this taclity
F[PA Faccl Information
This query was executed on FEB-11-2011
Toxic Releases for Reporting Year 2009
TRI FACILITY ID: 284SIDPNT STATE
There were no SIC Codes reported to EPA for this facility.
Chemicals Transferred to other Sites
RELEASE
RELEASEBASIS
I
CHEMICAL NAME
TRI CHEMI
UCUMENT�
j
AMOUNTS
11
I
TYPE OF WASTE MANAGEMENT
TRANSFE_R__SITE NAME
TRANSFER
ID
COD
XA
0001239L1;1309207852904II
16
GIANT RESOURCE IHARLEYVILLE
RECOVERY
ACETALDEHYDE
000075070
1309207852916'
38.75
([RECOVERY
INC SUMTER JSUMTER
A ALDEHY
000075070
1309207852916
_
84 15
(ENERGY
- - _ -_
RECOVERY
GIANT RESOURCE
RECOVERY
HARLEYVILLE
.. _
IMETAL$
SOLIDIFICA
TMETAL ijGIAN
.
N
N010I13092078529301
����
1
AND COIMPO NIDS IRECOVERYDURCE
HARLEYVILLE
ONLY
00744039331D9207852942�
1
F�
HEADWATERS RESOURCE
INC
SOUTH
IORDAN
I
—
I
I
----
SAMPSON COUNTY'
-
C BALT
1309207853019
124483
DISPOSAL WASTE
ROSEBORO
COMPOUNDS
�
INDUSTRIES
INDUSTRIES INC...._ _.
IDIDXIN AND
COMPIOE-IiKEUNDS
N150j
13Q9207853021i
_ 52416I
-- I1NCDWATERS
RESOURCEi
SOUTH I
ORDAN
ETHYLENE GLYC
000107211
1309207853033i
12917�
1RECOVERY
INC SUI TER_-IISUMTER
ETHYLENE
_HYLENEGLYCOL
000107211�
1309207853033
-
40967�-ENERGYRECDVERY
�JGIANT
RECOVERYOURCE IHARLEYV[LLE
LEAD MP- NDS
COMPUR
NDS
N4ZD,
N456
1309207853458
13D9207853072
k844
�
14�
�
,4
- -
- .. ... - - - .. ........ .. ... ....._
h
RESOURCE{
NG
HEADWATERS RRCE,
ESOU
INC .......... ..._....._........_ _ .....j
JOWATERS ITH
O DA
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SOUTH
JORDAN
Chemicals Released to Air
CHEMICAL NAME ID
DOCUMENT
LESSYR _
CODS J
INDICATOR
1.1 4- I XAN ;000123911�L309207852904i
2811
STACK OR POINT
EMISSIONS
1.4-DIOXANE 1000123911i
1309207852904
9770
FUGITIVE OR NON POINT
EMISSIONS
,AC ALDEHYDE
- -
000075070i1309207852916�
J
17651
__ - _- -- -
(FUGITIVE
_ _ --
OR NON POINT
EMISSIONS_._._
AC ALDEHY
000075070�1309207852916i
23814
�EM
STACK OR
SSIONSPOINT
AMMONIA 1007664417
130920785292H'
3979
FUGITIVE OR NON POINT
EMISSION$
;AM IA 1
--
0076644 17
1309207852928�
5644
-
STACK OR POINT
NTIM NY COMPOUNDS
- --' — J
A - -- -- --I.
-N010
��
13092078529370
__..._
35
--
STACK DR PRINT
EMISSIONS --------I
BA I M
007440393i1309207852942�
16
4EMISSIONSPOINT
(STACK OR
BEN N
1
_[EMISSIONS
IVE OR NON-POINT07143239207852955�112OOD
(BEN NE
000071432
1309207852955
21576
_. ...
STACK OR POINT
EMISSIONS - -
100009252411309207852979 Ill- STACK OR POINT
___.--.___..... -...... .._..
J EMISSIONS I
BIPH NYL 000092524 1309207852979i 71830.39 FUGITIVE OR NON -POINT
oaspub.epa.gov/.../multisys2.get—list—tr... 1/18

2/11/2011 EPA j Envirofacts Warehouse I ENVIRO...
BR MOMETHANE
�000074839'I1309207852981'1
4
IIFUGITIVE
E ISSION�R NON POINT
BROMOMETHANE
U40074839'
1309207852981l
126102
JSTACKOR
POINT
EMI`
CHLORINE
007782505i1309207852993
1
10
....
FUGITI VE OR NON -POINT
EMISSIONS
CHLORODIFLUOROMETHANE
000075456
1309207853007
8400
EMISS[ E OR NON -POINT
COBALT COMPOUNDS
- N046�
13092076530191
- 49
_
STACK OR
EMISSIONSPOINT
_
DIOXIN AND p[OXIN-LIKE COMPOUNDS
_..------._. - ---
N150
1304207653021
.1251976
- -- -
- --
STACK OR POINT
EMISSIONS - ...
ETHYLENE GLYCOL
00010721 L
1309207853033
-' 8838
i
STACK OR POINT
EMISSIONS
ETHYLENE GLYCOL
00010721I11309207853033i
I�
45771)
�^
FUGITIVES NON -POINT
EMISSIONS
HYDROCHLORIC ACID (1995 AND AFTER "ACID
0076470101
1309207853045I
_ _ .....__
150987
..__....-.__-- - __...--__.
STACK O R POINT
AEROSOLS" ONLY i _- - ---__..... --._ . f
LEAD COMPOUNDS
N420
1309207853058
67
lSTACK
-
OR O EMISSIONS
MAN ANESE COMPOUNDS
N450
1309207853060
49.03F-�MASSIONSPOINT
MERCURY COMPOUNDS
- _
N4581'
1309207853072
2.89
... ... .......
STACK OR POINT
EMISSIONS...... _.
M HAN L �D0006756111309207853084
- _ ---- ---- --..._.- -
11536
FUGITIVE OR NON POINT
' METHANOL
000067561'i1309207653084;
��
10315fi
IEMISSIONSPOINT
STACK OR
N BUTYL ALCOHOL
_
'[N-BUTYLA HOL -
D000713631
000071363',1309207853096
1309207853096i
517
_.._...._. -
- 154961
(STACK
FUGITIVE OR NON -POINT
EMISSIONS
OR POINT
EMISSIONS
O-XYLENE
_ _........ --..__.... --__.
o00095476'1309207B53110!
2605
- ---
iFUGITIVE
---EMI55[ON_S_�
OR NON -POINT
_.
P-XYLENE
00010642311309207853146�
6544
:FUGITIVE
OR NON -POINT
EMISSIONS.
P-XYLENE
_- - _ -_
000106423'1309207853146�
�I_
- .._._ -J
131814
_ ___ -
_
STACK OR POINT
EMISSIONS
POLYCYCLIC AROMATIC COMPOUNDS �'
-T_ N590
1309207853161�
2��
�EM[SSIONSISTACK
OR PDINT
-
SULFUR[C ACIQ (1994 AND AFTER "ACID
AEROSOLS" ONLY
007664939
13092078531851
55875
;
_
STACK OR POINT
EMISSIONS
TOL ENE
0001088E
1309207853197
I..
2654
FUGITIVE OR NON -POINT
EMIS5-IONS
- . .... ...... __ .--_-__
TOLUENE
000108663
- ___. ... .__
T
1 8 1 71
__ ..... __._. _
20653
_ -
.... --.. __J
_-
STACK OR POINT
EMISSIONS
Chemicals Released to the Land Surface
CHEMICAL NAME Cam_ DOCUMENT IRELEASE AMOUNTS
LBS7YRFRE LEASLBAS.IS
CODE LAND DISPOSAL .................... ............
ANTIMONY COMPOUNDS N010 130920 852930 , ...-__
23i
LAND TREATMENT/,APPLICATION FARMING_
__
COBALT COMPOUNDS N096. 13092E 078530t9 T
_
65 T-
AND TREATMENT/APPLICATION FARMING
MANGANESE COMPOUNDS N450 IF3092078530601
9981
LAND TREATMENT/APPt-ICATION.FARMING
Chemicals Released to Surface Water
CHEMICAL NAME
. -. _
......,
TRI CHEM,
..... ....._
DOCUMENT- RELEAL5AYRUNTS ',
RELEASE
STORM LITY WATER
APPLICABIFLAG
STORM WATER
PERCENTAGE
ID _J_
_ -_CODE
1 4-DIOXANE _ ._... _:
000123911;
1309207852904 ---.._. .........__.... 36
-- .... _ .,.0..,.... -_ _._,..
0'
ACETALDEHYDE ........
000075D70
1309207852916 301
IF
I,— .........
6.
AMM NIA___ _;
ANTIM NY rF
CQMPOUNDS
007664417'
N010
1309207852928 _... 528.�..-__.
1309207852930 1780
_.._.._�
0 .
0
_. D'
0
CHLORINE T
COBALT COMPOUNDS
007782505
N096;
1309207852993--_
1309207853014
F 1102
0
0
ETHYLENE GLYCOL
000107211
1309207853033
175.14
0
0.
MP UND
MERCURY
C MPOUNDS
N450
N458
1309207853072
.8
-MANGANE
04
D
0C .
0'
F.
METHANOL _
NITRATE
MPOUND
000067561,
N511
1309207853084
13092D7853108
_ 22 24.
351496
........
_ !
......... .110 ..... ........
0
0
-XYLENE
000095476
1309207853110
18
I
0...............
P-XYLENE _ _ -
000106423
1309207853146
_ _18
—2202
,. -IF
SODIUM NITRITE ,
007632000
1309207853173
0
0
;TOLUENE-__,OOgLOBB83;1309207853197
---- 6
;.,
0 -
D
Chemicals Released via Underground Injection
There was no data of this type reported for this facility.
oaspub.epa.gov/.../multisys2.get list tr... 2/18

2/11/2011 EPA I Envirofacts Warehouse ]'ENVIRO...
Additional Information can be obtained from the Toxics Release Inventory System ® Query:
Additional links for TRI:
This information resource is not maintained, managed, or owned by the Environmental Protection Agency (EPA) or the Envirofacts Support Team. Neither
the EPA nor the Envirofacts Support Team is responsible for their Content or site operation. The.Envirofacts Warehouse provides this reference only as a
convenience to our Internet users.
• National Library of Medicine (NLM) �J TOXMAP
• The Environmental Defense Fund's (EDF) Chemical Scorecard has on-line environmental information regarding this =0 ili reported TRI
releases.
Water Discharge Permit Information (PCS)
Pending migration to a new system, the data for the Permit Compliance System (PCS) will remain frozen in Envirofacts for the following
states and territories as of the below listed dates:
Frozen as of June 6th, 2006: MA,NH,RI,VI,PR,OC,MD,IN,NM,UT,HI,AK,ID
Frozen as of August, 2006: AS,AT,CT,C2,FM,GA,GB,GU,JA,MH,MP,MT,MW,NE,NI,NN,NV,NY,PA,PW,SD,SR,TT,UM
Frozen as of April 24th, 2008: IL
Frozen as of August 26th, 2008: AR CA,CO,OK,TN,WI
Frozen as of June 17th, 2009: TX, LA, GM, AL
Please refer to the ECHO Clean Water Act Query Screen to retrieve updated data for the states frozen in Envirofacts.
NPOES: N00000663
SIC CODE: 2821 SIC DESCRIPTION: PLASTICS MATERIALS, SYNTHETIC RESINS, AND NONVULCANIZABLE ELASTOMERS
This facility has permits to discharge the following chemical/substances through the points (pipes) listed in the table below:
PARAMETER CODE
PARAMETER DESCRIPTION JINUMBER OF DISCHARGE POINTS
ACRYLONITRILE_-____-...
_ __344.18
34469 ILYRENE
34536 7 j1..Z-Q.ICHLOROBENZENE.-
00530
LIDS TOTAL SUSPENDED�_
2
T
34626
2,6-D[NITROTOLUENE ___..._
00300
OXYGEN. DISSOLVEDfD01 j
L
00610
NITROGEN. AMMONIA TOTAL fA5 N1,
,
39100 IBIS.
_._._._ _..
(2-ETHYLhEXYL) PHTHALATE ........ .........
I
34447
NITROBENZENE
1
34657...,_.-.,_,_4,6-DINITRO-0-CRE5OL.--
_
OL042
----
COPPER. TOTAL (AS CU) �.
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1
34371
ETHYLSENZENE
1
34205
ACENAPHTHENE
1
34586_..
2 CHLOROPHENOL._._._......---....
00630 INITRITE
PLUS NITRATE TOTAL I DET, (A5 N)
3
00665
PHOSPHORUS. TOTAL (AS P}
3
TGE6C_- ;
P/F_STAT 24HR ACU PIMEPHALES_
I
34461 IPHENANTHRENE
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1
34591 '
i ITROPHENOL.... _ _
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342:W ;
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34526
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I I
__00094
34200 JACENAPHTHYLENE
1
34180
R L Y N I
1
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CHLORINE, TOTAL RESIDUAL
3 j
31616OLIFORM,
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32106
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_....___00400 _
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3
321[02
CARBON TETRACHLORIDE
1
3401p -
TOLUENE---1-
39702
34541
HEXACHLOROBUTAWENE
1.2-DICHLOROPROPANE
1
I
39175
VINYLCHLQR[DE
34561
1DLCHLOROPRQPENE. TOTAL WEIGHT i
L
34694
PHEN LSINGLE COMPOUND
34247
BENZO A PYRENE
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34571
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1.4-DICHLOROBENZENE ._...... i
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346N
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IDIMETHYL PHTHALATE
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34616
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34376 IFLUORANTHENE
1
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2/11/2011 EPA EnVirofacts Warehouse ENVIRJ...
f 34601 12,4-DICHLOROPHENOL 1
_-34546 1,2-TRANS-DICHLORO _ETHYLENE _ IF 1
__ 34311 —. 'CHLOROETHANE. TOTAL WEIGHT.—_
00010 iTEMPERATURE W.TA ER Dom. CENTIGRADE .3
34242 BENZO(K)FLUORANTHENE 1
00600
In T TAL AS N 1
3
r- 34566 }
1 3-DICHLOROBENZENE
1
34396
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IMETHYLENF CHLORIDE i
1
34501............ .:
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1-N- TY PHTHALATE
34403
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34531
1.2-DICHLOROETHANE, TOTAL WEIGHT
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34496 _ill,
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34556 _ ;DIBFNZQ
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34475
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Additional Information can be obtained from Water Discharge Permit Infomation ® Query.
AFS Information
O eratinStatus:
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OPERATING
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Noncellulosic Organic Fiber
pate Plant Information Last Updated: 01/03/2011
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2/11/2011
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Action Kev
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Results
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NumberNumbers
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TITLE V
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LIST OF PROCESS UNIT INFORMATION FOR GROUP CONTAINE
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2/11/2011 EPA j Envirofacts Warehouse I ENVIRO...
PROCESS CODE /
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Facility Mailing Addresses
Affiliation Delive PoinPoint— Cit Name State- postal Code lInfonnation-
AUT H CON0 ACTD?. D ENE____.-_ LS LELAND j NC _ 28451 I NC -FITS
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This information resource is not maintained, managed, or owned by the Environmental Protection Agency (EPA) or the Eovirofacts Support
Team. Neither the EPA nor the Envirofacts Support Team is responsible for their content or site operation. The Envirofacts Warehouse provides
this reference only as a convenience to our Internet users.
• National Library of Medicine (NLM) OT XMAP
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2.11112011
Environmental Releases for DAK AMERI...
Investigate
Pollution Topics
► Toxic Chemical Releases
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/ Superfund
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.hernical_Releases I Reports
Environmental Release Report: DAK AMERICAS
L.L.C. CAPE FEAR SITE
• Map Locating Toxic Chemical Releases
• 2002 Rankings: MaiorChemical Releases or Waste
Generation at this Facility
• 2002 TRI Pollution Releases Ranked by Ozone Depleting
Potential
• 2002 TRI Pollution Releases_ Ranked by Potential Human
Health Risks
• 2002 TRI Pollution Releases Sorted by Health Effect
• What We Don't Know About Chemical -Safety and Harm
• TRY Data Summary
+ Dioxin Compounds Summary
• Facility Information
• Links
• Map Locating Toxic Chemical Releases
• DAK AMERICAS L.L.C. CAPE FEAR SITE LELAND NC
[t0Qi
• 2002 Rankings; Maior Chemical Releases or Waste Generation at This Facility*
Cleanest/Best Facilities in US Percentile Dirtiest/Worst Facilities in US
0% 10% 20% 30% 40% 50% 60% 70% 80% 90% 1000/b
scorecard.goodguide.com/.../facility.tcl... 1/5

2/11/2011 Environmental Releases for DAK AMERI...
i ��ni ciivviicio�PiC IC PDCJ
Cancer risk score air and water releases):
. t �
Noncancer risk score air and water releases
Air releases of recognized carcinogens:
Air releases of recognized developmental toxicants:
Air releases of recognized reproductive toxicants:
See how this facility ranks on other chemical release and waste management attributes tracked by
Scorecard
Rank facilities in NORTH CAROLINA or in BRUNSWICK County by chemical releases or waste generation
*Note: These rankings are based on chemical releases and transfers reported by industrial facilities to
the Toxics Release Inventory, and do not take into account major sources of pollution or toxic chemicals
that are not covered by TRI.
[ too I
• 2002 TRI Pollution Releases Ranked by Ozone Depleting Potential
Top Ranked Ozone Depleting Chemical: METHYL BROMIDE
List chemicals contributing to ozone depletion
[ too i
• 2002 TRI Pollution Releases Ranked by Potential Human Health Risks
Top Ranked Cancer Risk: BENZENE
List chemicals contributing to cancer risk
Top Ranked Noncancer Risk: COBALT COMPOUNDS
List chemicals contributing to noncancer risk
See Scorecard's estimates of the health risks associated with outdoor air pollution for this area
[Lg-p-i
• 2002 TRI Pollution Releases Sorted by
Health Effect*
Air Releases
Water Releases
{Pounds from TRI
(Pounds from TRI
sources)
sources
RecognizedCarcinogens
75,233
87
Suspected Carcinogens
3,812
2,041
Suspected Cardiovascular or Blood
602,436
95,619
Toxicants
Recognized Developmental Toxicants
115,805
7
Suspected Developmental Toxicants
494,211
2,252
Suspected Endocrine Toxicants
18,959
Suspected Immunotoxicants
350,801
2.169
Suspected Kidney Toxicants
608,519
5,867
Suspected Gastrointestinal or Liver
865,820
6,479
Toxicants
Suspected Musculoskeletal Toxicants
209,316
Sus ected Neurotoxicants
768,803
13,259
Recognized Reproductive Toxicants
12,867
scorecard.goodguide.com/.../facility.tcl... 2/5

2,111/2011 Environmental Releases for DAK AMERI...
Suspected_ Reproductive Toxicants 438,120 9,545
Suspected Respiratoryy Toxicants 981,907 15,298
Suspected Skin or Sense Organ Toxicants '972,823 7,869
*Note: Some chemicals are associated with more than one health effect, so their release may be
counted multiple times in this table. Therefore, it is not appropriate to sum releases sorted by health
effect. Total reported releases to air and water are provided in the data summary below.
[I2R]
• What We Don't Know About Chemical Safety and Harm
Air Releases
6 TRI chemicals released to air in the United States lack the risk assessment values required
for safety assessment
218 TRI chemicals released to air in the United States lack the exposure estimates required for
safety assessment
Water Releases
5 TRI cherr6 released to water in the United States lack the risk assessment values required
for safety assessment
172 TRI chemicals released to water in the United States lack the exposure estimates required
for safety assessment
I tOD I
• TRI Data Summary
Environmental Releases, Transfers, and Production -Related Waste (Pounds from TRI sources)
Air
Water
Land
Underground Total Environmental
Total off -Site
Total Production -
Year
Releases
Releases
Releases
Infection
Releases
Transfers
Rea dd Waste
1988
7,156,490
34,430
3,069,490
0
10,260,410
421, t43
NA
1989
7,199,632
183,432
2,459
0
7,385,523
383,266
NA
1990
6,445,155
248,198
2,520
0
6,695,873
311,412
NA
1991
5,704,412
18,284
13,344
0
5,736,040
1,219,310
15,592,687
1992
14,437,452
19,B60
40,641
0
14,497,953
301,901
11,695,244
1993
3,815,000
15,456
24,854
0
3,855,310
118,580
10,576,687
1994
3,797,152
48,322
70,976
0
3,916,450
8,610,382
17,917,965
1995
2,827,971
449,407
376,234
0
3,653,612
9,244,279
23,460,582
1996
2,271,238
533,319
2,413
0
2,806,970
5,806,303
11,515,548
1997
1,777,363
556,889
205,199
0
2,539,451
11,490,168
12,660,482
1998
1,676,202
590,355
2,383
0
2,268,940
5,523,259
12,814,567
1999
1,240,234
483,750
1,795
0
1,725,779
3,345,934
6,881,227
2000
1,227,650
343,143
1,812
0
1,572,605
2,012,808
5,964,083
2001
1,010,055
303,677
1',402
0
1,315,134
1,475,250
4,484,350
2002
981,927
101,941
1,521
0
1,085,389
886,070
3,718,896
"NA" means that no data are available because 'Total -Production Related Waste" was not reported
until 1991.
ItoDI
Dioxin Compounds Summary
Environmental Releases, Transfers, and Production -Related Waste (Grams of Dioxin Compounds
from TRI sources)
Year Air Wa er Land Underground Total Environmental Total Off -Site ToLal_Production-
Releases Releases Releases Injection Releases Transfers Related Waste
scorecard.goodguide.com/.../facility.tci... 3/5

2/1.1/2011 Environmental Releases for DAK AMERI...
2000 .183 0 0 0 .183 .4734 .6564
2001 .163 0 0 0 .163 .4242 .5872
2002 .155 0 0 0,155 0 .633
[tom)
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Send a FAX to the management of this facility. (free)
'f Email EPA
loin an online discussion about this facility
to Join Together
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€rie nd
i Network with environmental groups
4 Learn how to use Scorecard to Find out about
toxics in your community
I. to 1) l
Support Us
Contribute to Environmental Defense
Volunteer with environmental groups in your
community
• Facility_Information
2002 Facility Name: DAK AMERICAS L.L.C. CAPE FEAR SITE
Mailing Address: 3500 DANIELS RD. N.E., LELAND, NC 28451
Public Contact: PENNY C. MAHONEY
Phone:[phone]
SIC Code: 28 Chemicals And Allied Products
2002 Parent Company: DAK AMERICAS L.L.C.
Latitude: 34.31833
Longitude:-78.02889
Facilities are encouraged to respond to the information presented in Scorecard.
Itoo l
• Links
• Scorecard's Criteria -air pollutants report for this facility
• See EPA Envirofacts report for this facility for information about regulatory compliance,
hazardous waste handling processes, Superfund status, and permitted air and water emissions.
• RTK NET report for this facility, which includes its complete Form R report to EPA's Toxics
Release Inventory
Scorecard's report for BRUNSWICK County on:
• Chemical releases from industrial facilltie-s_(TRIJ
• Hazardous air pollutants
• Criteria air pollutants
ItoQ I
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.N��Soowsq SD
�e
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
STAFF REVIEW AND EVALUATION
NPDES Stormwater Permit
Facility Name:
�~"a
�r
b r''oTFacility
NPDES Permit Number:CNCSZ0003
Location:
car Creek Road, I-ayetteville, NC (Cumberland County)
Type of Activity:
Plastic Manufacture
SIC Code:
2821
Receiving Streams:
See Figure 1
River Basin:
Cape Fear River Basin, Sub -basin 03-06-15
Stream Classification:
WS-IV; CA
Proposed Permit Requirements:
See attached draft permit.
Monitoring Data:
See Table 1
Response Requested by (Date:):
Central Office Staff Contact:
Return to: Brian Lowther, [phone]
Special Issues:
!Issue
Rating Scale: 1(easy) to
10 hard
Compliance history
6
Benchmark exceedance
6
Location ("I'MDL, T&E
7
species, etc)
Other Challenges:
Y
• licnchniark f()I' I A
Dioxane:
• Fi"ur'irlc out the Mkk
XV1111 3 owllcrs
Difficulty Rating:
27/40
Special Issues Explanation:
• l A-Dloxanc was deluded in the SW sample~. It is a kncmvn carcinogen and has human health
cauccrnS. More III l'orinatloll kw. this is below in the analytical Illoniloring section.
Page 1 of'9

NCS000389
Description of Onsite Activities:
• DAK is principally engaged in the; tlinnufacnlre of polyester chips. Which Will he used to prnduce
various plastic dents lix' industrial and/or consumer usc. The polyester chips at 111is facility are
marlufactured in <1 C0I1tinUOUS process which utilizes two primary process systems.
• 111C L11anllf,r]Ctl111112 operations occur in dIL: SouthWest portion oi'thc property in the continuous
polymerization (CI) and file solid state polymerization (SSP) plane. The railroads located oil the
southeastern portion nfthc property are for INad1112 ot'product and unloading ol'raw materials.
• DAK Americas LLC Ccdar Creck Sitc is located in the Ccdar Creek Industrial Complex. The complex
also houses Dupont I'eijin films; WC11nlan, Inc (no longer in operation). and the DAK Service Complex (a
utilities facility purchased front NIOnsanto ill Jarlliary 2004). The Service Center is located east of'lhe
Dupont TCijin film property and supplies utilities for both the DAK Reline Plant and the Dupont Teijitl Film
Plant. Utilities include steam. cooling water, demincralizcd water, and wastcwatcr treatment.
• Clear Path Recycling is now located on part.,of thr DAK f<icilit". Clear Path ', the lamest PET
(Polyethylene tci-ephthalate') recycling facility in the world. Clear Taal Ilecyclirig has obtained 53 acres
which was formerly part of DAK Americas 172 acre: tract.
Documents Reviewed:
• NPDI7S Stormwater Permit Application Materials
• National Heritage Program (NIIP)'I'hreatened and Endangered Species Database
• SPU File
• Central Files
• }SPA Sector -Specific Permit, 2008
• 303(d) List, 2008 draft, 2000 final
• 2U{}5 Cape ]car Basinwide Plan
• DuPont I'ilc NCS000056
• TRI Maps data and links.
History:
• August 15. 2003: Pertltit issued to DAK Resins LLC. Monitoring included 1,4-Dioxanc anti COD sampled
annually fbr the first three years and quarterly during year four.
• F(Alruary 2, 2005: Name chain-,c to DAK Americas. LLC
• ,lanuary 25, 2007: Renewal letter sent.
• iklarch 0. 2008; Renewal Application received. Asked fi)r SW outfall 003 to he included With their
xyastewater permit. This request was denied when the Nv isteNYater permit was renewed.
• August 10, 2009: Rcqucst to transfer OUtfalls front DAK to Clear Path,
Page 2 of 9

NC:S000389
Figure l: Map of Facility
I U
.:a.` _ =Y _ " ,.,._._. __ — _ —_ Tom' '. ,' r . —j'• _ —.._ .�—•.-------�.,— �-•• � — .—. � _._ -�.i=�
— e•- . - Ili '! '� I/ (� l _ `� �,� � •��
•� ' ',' '.I:. 4" i.� I i9�.rnch
i #' ,5 �`�y.i�.urP
ii L�
a in
r 41 1 SS ( '• 4
1 DAK America 11C Cedar Creek Site
.�I !
�� i�•`:� J 1 '+tr'i* ; '� `ray • �.i 1� �.'ty •.�vn�p .rlet F /' ,
-�• i rr''%i„ i'�., x�i.-'Lc } 1 _ 1, frS f }T,,; "Ay-
r.•- } 2 : �' S ./'. 1.- f l��-. -t.•. �J•a,R aAa�y
rd
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UZI}, ',�'•,•
^. 'ice --r l ::
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�a�� �5�i1' ,` � ' }` ��• jam, i x�f'.pmy'i1 , ,' ; `` e '�- 'sh"l; ! .1
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���\ y ' •J _I I
;'r l 11 .S�'�.���}
S,S
NCS000389
DAK America LLC
DAK America LLC Cedar Creek Site
�
Lab tud->: 341159' CO" N
de: 780 4730" \N
Longi
<r
County, Currberiand
;
Recaving Stream: Cme Fear River
Su-eam pass; WS-IV; CA
M�P Scale 1.24,DOO
Sub -barn; 03-06-15 (Crime Fear River basin)
Facility Location
Page 3 of 9

NCS00038N
Central Office Review Summary:
1. Owner's Other Permits: DAK America wastewater permit NCO003719, The effluent monitoring requirements
include flow, TSS, BOD, NI-13-N, Fecal Coliform, Total Residual Chlorine, Temperature, DO, p1-1, Total
Nitrogen, Total Phosphorus, Acute Toxicity, and Conductivity. Also, have OCPSF parameters.
o Air Quality Title V- 04319T18
o Synthetic Minor Air Permit — 04051 R30
o Permit to Discharge Wastewater Under the Public Works Commision's Industrial Pretreatment Program
(application pending) — 21 16RF
Notes on Wastewater permit: our discharge permit for DAK Americas, LLC (formerly Monsanto, Fayetteville) has
storm water conditions and boilerplate that will need updating for this renewal (unless covered by your permit
NCS000389). Update: the stormwater outfalls were not included in NC0003719 and need to be included in the SW
renewal.
2. General Observations:
• "Three companies located within the expansive property.
• The old 1` onsanto facility, now Clear Path Recycling, was used to manufacfurc 1Z01.111d-LJp.
• Site conditions arc such that DAK and Clear lath share one SW outfall (4001). DAK has
rcpresentativc outfall status for their single 4001 outl'ail. Clear' Path has nurncrotls others.
• The site is 26,1 Acres with 4.72 acres on impervious
• In the application, Cobalt is listed as a potential I)OHL1tant not covered by analysis. Cobalt is in the TRI
for being at the facility. "hhc Ccdar Crcck site used CoNilt as a toner additive. "fhc plirnt has reccnlly
discontinued its use; however. one 2000-1h totc bin rcrrlains on site. It is located inside in the Logistics
1Vareh0u1Ze and will be returned tit the manufacturer with the next Month.
3. Impairment: The 2006 303(d) includes the Cape Fear River 18426)c (frorl (iruvs Creek to Lock and Darn 3) fur
a C11101-01)hyll a violation and 18-(26)d (from Lock to Dam 3 to NC:41) fi r a Mercury Fish Advisory, Basinkvidc
Plan indicates the Cape Fear River ] 8-(2fi)b (front Peares Mill Creek to Gravy Creek) has turbidity and fecal
colifi�rm as stressors. "I'hc impairment language Was not added to tllc permil because these segments of the Cape
fear are not the same segment of the Cape Fear where the facility's discharges are located.
The City of Fayetteville water supply intake looks to be about 12 miles upstream based on the classified streams
layer is GIS. The stream segment is identified as "From City of Fayetteville water supply intake to mouth of
Hammond Creek."
4. Threatened and Endangered: Based on the Natural hleritage Virtual Workroom there are no federal protected
species within two miles of the facility.
5. Location: Six outfalls Ilo w to the Crape bear River:
• 001 — 34' 58' 08", -78' 46' 58" — SW from developed and undeveloped land including plant process
areas and cooling tower blowdown.
• 002 — 34 58' 08", -78' 46' 58" — Wastewater
• 003 — 34- 59' 02", -78 47' 26" -- Stormwater runoff from DAK resin plant.
• F — 34' 58' 42",-78-46' 50" - SW From developed and undeveloped land. Qverflow from SW001
• G — 34 58' 41 ", -79 46' 50" — SW from activities associated with wastcwater treatment basins, fuel
storage and paved roadways used for in -plant transportation. The outfall discharges onto a vegetative
strip prior to entering the waterway.
• 1-1 — 34' 58' 45", -79 47' 05" — SW from activities associated with the wastewater treatment plant. The
outfall discharges onto a vegetative strip prior to entering the waterway.
6. Industrial Changes Since Previous Permit: None provided.
Analytical Monitoring Notes: The analytical samples in central files are shown in Table 1. A letter -was included
to explain a 2040 rng/l COD value. They conducted a visual search for potential contamination and no visual
Page 4 of 9

NCS000389
contaminates were detected. Another sample was taken from the stormwater pond and the value was 13.3 mg/l.
The permittee believes the original sample was invalid.
1?PA 2008 Multi Sector -Specific Pe-mit, Sector C for Chemicals and Allied Products: Subsector C4 Plastics,
Synthetics, and Resins (SIC 2821-2:324) recommends monitoring for Total Zinc. Zinc will not be added to the
perrnit because it does not seem to be a pollutant of'concern based on the industrial activities of this site.
Based on the last staff report, 1,4 —Dioxanc was added to the requirements as the result of a previous spill on
7/1612002. The perrnit file included data taken for the pervious renewal and the last two samples indicated there
was some 1.4-Dioxane in the stormwater (sce Table 1).
1,4 —Dioxane is a known carcinogen and is a very persistent chemical that does not readily break down. In this
case, an aquatic life based storinwatcr benchmark would not be helpful because it has high human health
concerns. For example, the stormwater benchmark would be 1 100 mg/L (calculated �/2 FAV) compared to the
human hcalth based instrcam standards of 3.2 ug/L for water supplies and 730 ug/L for general liuman health
exposures (Class C waters). A 10 day child exposure rate has been developed for this chemical of 400 ug/L.
(Intbrmation based on an email from Nikki Remington 2/25/10)
The reviewer rccotnmctids that the facility should be aware of any 1,4 - dioxane levels that raise human hcalth
concerns, particularly with a discharge to WS-CA. Because of the previous spill, a benchmark will trigbcr more
investigation or more clean-up if needed. The Water Supply standard is not typically used even when receiving
waters are WS because it is not necessarily appropriate for a stormwater benchmark. This more stringent WS
value should be noted, but the reviewer recommends, the 10 day child exposure rate of 400 ug/L be used as the
benchmark. This benchmark reflects a time frame more consistent with storinwatcr events (10 days vs lifetime
exposure for the human health/water supply numbers) and would be protective of* the more sensitive population
(children); this values secins to be the most appropriate to prompt the facility to respond to a possible problem.
However, if future monitoring detects levels above the WS standard, DWQ may want to investigate potential
WQ standard violations.
Sample results from previous renewal:
Lead — 0.01 mg/1 (benchmark = 0.033 mg/1)
Oil anti Grease — 5 mg/1 (benchmark = 30 mg/1)
pl-1 — 7.35 (benchmark = 6-9 su)
TSS — 17 mg/1 (benchmark = 100 mg/1)
Data from the previous permit is in Table 1.
Monitoring for NCS000056 — DuPont Teijin Films included COD, Oil and Grease, and pl-I.
COD, 1,4 —Dioxanc, Oil and Grease, and pH have been added to the permit because they arc potential pollutants
onsite. Oil and Grease will be added to make the parameters consistent with the DuPont permit.
8. Qualitative Monitorin_y_Notes: NUnC I11C:ILICICC1 In the application.
Page 5 of 9

NCS000389
'cable l: Analytical Monitoring
Required
Sampling
Ran a
Sample
Date
TotalPrecipitation
Flow
MGD
(in)
Duration
(hours)
1.4- Dioxane
COD
Benchmark:
0.4 m IL*
Benchmark:
120 m IL*
Outfall 003
11/19/ 2003
0.71
1
2
<0.02 5
17
6/4/2004
0.218
0.3
0.67
<0.1
13.3
7/29/200
2.97
4.2
4
<0.005
�
10/6/2005
1.9
2.7
36
J _ BDL�
13.3
11/8/2006
1.2
1.8
24
2/1/2007
1.06
1.5
25.5 l
r. �[?.
13.3
t
FTOver Current Benchmark
Data Not Collected
* Benchmarks not in pervious permit
Page 6 of 9

NCS000399
Recommendations: Based on the documents reviewed, the application information submitted on March 6, 2008
sufficient to issue an Individual Stormwater Permit.
Prepared by (Signature)
Stormwater Permitting Unit Sup
Concurrence by Regional
RO Water Quality
Regional Office Staff' Comments (attach additional pages as necessary)
Date
Date 3 A0 Zv 1 I)
Date
Date
What ou falls need to be sampled for this permit? They were sampling only 003. Some of the outfalls were covered in
their waste/water permit but that is now not the case and need to be covered in this permit.
4
�✓; sl �Sct,. v Yr�tS wt % r � �3� s`e— r /a,,,xl /LvIG n A
��MY17/1
O03
loc-o rle ml -de f�r lwro,1114r� lnpnck�')
s
1
Page 9 of 9

NC:S000 3y9
Revised Permit Recommendations: Analytical Monitoring:
1. COD and 1,4—Dioxane have been ,Maintained in the permit. Oil and Grease and pl l have been added to the
analytical monitoring requirements. Parameters added because they are potential pollutants and they arc
consistent with NCS000056 DuPont which is on the same site.
2. All analytical monitoring has been set to scmi-annually during a representative storm event as defined in Part 11
Section B. The permittce must also document the total precipitation for each event. If'no discharge occurs
during; the sampling period, the pernnittee must submit a monitoring; report indicating "No Flow" within 30 days
of the end of the six-month sampling; period. Additionally, samples must be taken a minimum of'60 days apart,
as specified in Table 2.
3. Benchmarks for analytical monitoring have been added to this draft permit. I-Lxcccdanccs of benchmark values
require the permittce to increase monitoring, increase management actions, increase record keeping, and/or
install stormwater Best Management Practices (BMPs) in a tiered program. If the sampling results arc above a
benchmark value, or outside of the benchmark range, for any parameter at any outfall then the facility sliall
follow the Tier 1 guidelines which require a facility inspection within two weeks and implementation of a
mitigation plan within two months. If during the teen of this permit, the sampling results arc above the
benchmark values, or outside of the benchmark range, for any specific parameter at a specific discharge outfall
two times in a row (consecutive), then the facility shall follow the Tier 2 guidelines which require a repetition of
the steps listed for Tier 1 and also irnmediately institute monthly monitoring for all parameters at every outfall
where a sampling result exceeded the benchmark value for two consecutive samples.
4. "hhe permittce is required to collect all of the analytical and qualitative monitoring samples during representative
storm events as defined in fart 11 Section B. Qualitative monitoring is required regardless of representative
outfall status.
5. The permittce is responsible for all monitoring until the renewal permit is issued. See Footnote 1 of Tables 1, 4,
and 5.
6. The flow reporting requirement has been removed per DWQ revised strategy. (The total rainfall parameter is in
this permit, however.)
7. Vehicle maintenance monitoring; has been revised to scmi-annually in order to coincide with analytical and
qualitative monitoring.
Other Proposed Changes to the Previous Permit:
Additional guidance is provided about the Site Plan requirements. 'file site map must now identify if the
receiving stream is impaired and if it has a TMDL established. It must also describe potential pollutants in each
outfall. The map requirements are stated more explicitly. And, the site plan must contain a list of significant
spills that have occurred in the past three years and also must certify that the outfalls have been inspected to
ensure that they do not contain non-stormwatcr discharges. Additional information is provided in Part 11 Section
A.
2. Additional requirements for the Stormwater Management Plan have been specified in Part I1 Scction A. More
details regarding secondary containment are provided.
3. Additional requirements for the Stormwater Pollution Prevention Plan have been specified in Part II Section A.
The plan must also be updated annually to include a list of'significant spills and to certify that the outfalls do not
contain non-stormwatcr discharges.
4. The facility must now implement a scmi-annual Facility Inspection Program of the site's stormwater
management controls as specified in Part 11 Section A.
5. Information regarding the No Exposurc EXCIUSio[1 has been added to this dral't permit. if industrial materials and
activities are not exposed to precipitation or runoff as described in 40 CFR § 122.26(g), the facility may qualify
for a No I"xposure Exclusion from N11DES stormwater discharge permit requirements. Additional information
is provided in Part I Section A.
Page 7 of" 9

CNLCs0Q0-j1 9
Discussions with permittee: Elizabeth Wilke at DAK. Office: (910) 3,71-4498, Mobile: [phone],
e%vike@(Iakamericas.com
dakamericas.com
From email on 2/18/10: Beginning on the west end, the first tract is awned by DAK Americas. This area is the
location of DAK's Resins Plant. The area to the cast of DAK's Resins Pi.ant is the Dupont facility, Moving
further to the east is a large tract that reaches front Highway 53 on the north to the Cape Fear River on the south.
`file northern portion of this property contains DAK Americas Utilities, the southern portion contains DAK's
wastewater treatment plant. The tract of land on the north cast belongs to Clear Path Recycling.
Stormwater out falls were previously included in DAK's NPD1 S permit for the wastewater treatment plant for
the outfalls from the DAK Utilities Area, DAK Wastewater "treatment Plant Area, and what is now Cicar Path
RccN,cling, When DAK applied to renew its NPDFS permit, DI NR decided to remove these outfalls from the
NPDI S permit and have them included in the stormwater permit. The stormwater permit application for the
DAK Resins site was submitted a couple of years ago. it only included one outfall from the retention pond
shown on the south east corner of the property. I'll is stonnwater from this pond rarely discharges to the Cape
Fear River because most of the water either evaporates or infiltrates to the ground before reaching the overflow
from the pond. The DuPont facility is permitted separately.
Can You tell ine hoes, cobalt is used on the site? How much is on site and where it is stored?
From email on 3/23/10: The Cedar Creek site used cobalt as a toner additive. The plant has recently
discontinued its use; however, one 2000-lb tote bin remains on site. It is located insicie in the Logistics
Warehouse and will be returned to the manufacturer With the next month.
Elizabeth Wike Called on 4/23/10. She said she couldn't find any documentation on their representative
outfall status. She was fine if the permit was issued and in the future the facility apply for the representative
status again. She will continue to look for it though.
Page 8 of 9

Central Files: APS SWP
-
05/31/11
Permit Number NCSb00392
Permit Tracking Slip
Program Category
Status Project Type
NPDES SW
In draft Renewal
Permit Type
Version Permit Classification
Stormwater Discharge, Individual
Individual
Primary Reviewer
Permit Contact Affiliation
jennifer.jones
Coastal SW Rule
Permitted Flow
Facility
Facility Name
MajorlMinor Region
Cape Fear Manufacturing Facility
Minor Wilmington
Location Address
County
3500 NE Daniels Rd
Brunswick
Leland NC 28451
Facility Contact Affiliation
Owner Name
Owner Type
DAK Americas LLC
Non -Government
Owner Affiliation
Jorge P. Young
5925 Carnegie Blvd
Charlotte NC
28209
Dates/Events
Scheduled
Orig Issue App Received Draft Initiated Issuance
Public Notice Issue Effective
Expiration
08/15/03 03/12/08 02/14/11 05/31/11
04/15/11
'01111 .51311!1
6 Jf l,l
Regulated Activities
Requested/Received Events
Plastics & synthetics manufacturing
Region comments on draft requested
02/17/1 1
Additional information requested
02/17/11
Region comments on draft received
03/31/11
Additional information received
05/12/12
Outfall 002
Waterbody Name
CAPE FEAR RIVER
Stream Index Number Current Class Subbasin
18-(63) C;Sw 03-06-17

Permit No.
(to be provided by DWQ)
Trench Elevations
Bottom elevation
95.70
fmsl
OK
Storage/overflow elevation
98.20
fmsl
Top elevation
98.20
fmsl
Trench Dimensions
Length (long dimension)
20.00
it
Width (short dimension)
2.00
ft
Height (depth)
2.50
ft
OK
Additional Information
Maximum volume to each inlet into the trench?
0.00
ac-in
OK
Length of vegetative filter for overflow
30.00
ft
OK
Number of observation wells
1
OK
Distance to structure
15.00
ft
OK
Distance from surface waters
30.00
ft
OK for non -SA waters
Distance from water supply well(s)
1,000.00
ft
OK
Separation from impervious soil layer
6.00
ft
OK
Depth of naturally occuring soil above SHWT
6.00
ft
OK
Bottom covered with 4-in of clean sand?
y
(Y or N)
OK
Proposed drainage easement provided?
y
(Y or N)
OK
Capures all runoff at ultimate build -out?
y
(Y or N)
OK
Bypass provided for larger storms?
y
(Y or N)
OK
Trench wrapped with geotextile fabric?
_ y (Y or N)
OK
Pretreatment device provided
grass strip prior to trench
Form SW401-Intiltration Trench-Rev.4 Parts I. & 11. Design Summary, Page 2 of 2

X-S000392
Beverly Eaves Perdue
Governor
Facility Name:
NPDES Permit Number:
Facility Location:
Mailing Address:
Type of Activity:
SIC Code (if applicable):
Receiving Streams:
River Basin:
Stream Classification:
A����
ALI�
NCDENR LoJ'sL_
.North Carolina Department of Environment and Natural Resources C�
Division of Water Quality 3� 1 _ 4 -
CA-D-k_
Coleen H. Sullins Dee Freeman
Director Secretary Z `t'�
Proposed Permit Requirements:
Monitoring Data:
Response Requested by (Date):
Central Office Staff Contact:
Special issues:
STAFF REVIEW AND EVALUATION
NPDES Stormwater Permit; .
DAK Americas LLC
NCS000392
3500 Daniels Road, NC (Brunswick County)
P.O. Box 2240, Leland, NC 28451
Chemical (Polymer) Manufacturer
2865, 2824, 2821
See Figure 1
Cape Fear River Basin, Sub -basin 03-06-17
UTs to the Cape Fear River, Bay Branch, Otter Branch, and Mullberry
Branch C, Sw (All)
�V
See attached draft permit.(�� 011
See Table 1
March 18, 2011
Return to: Jennifer Jones, (919).807-6379
Issue
Rating Scale: 1(easy) to 10(hard)
Compliance history
5
Benchmark exceedance
5
Location (TMDL, T&E
species, etc)
9
Other Challenges:
5
Difficulty Rating:
24/40
LC��Qa�
MAR 3 1 2011
DENR - wATER AL
edandu & 8kwm—.&— d__ _
Special Issues Explanation:
The site EHS coordinator has not returned my phone calls, therefore I am proceeding with creating a preliminary
staff report and draft permit, and the RO staff review of this site. After RO Staff review and site visit, a draft
permit will be able to be issued. RO site visit is strongly recommended for issuance of this permit. After RO staff
review, staff report and Draft permit will have a 2Id central office individual permit review.
Description of Onsite Activities:
This site is a chemical polymer manufacturer with 3 production facilities (monomers, fibers and resins). The
Page l of i i.

NCS000392
monomers production area supplies raw materials to the fibers and resins operations. Monomers: Monomer area
is divided in terephthalic acid (TPA) production lines and an ingredient recovery process for the separation and
recovery of raw materials for reuse. There is also a Glycol Recovery Unit, The Direct couple oligomer (DCO} area,
S , followed by the continuous polymerization (CP) production lines, convert TPA into polymer (PET-polytheylene
r.i 0 terephthalate). Product from -DCO and CP is further processed in the Fibers and Resins areas. The Fibers area
(also called the Staple area) produces PET fiber and packages the fibers into bales. The Resins area manufactures
polyester chips, which DAK's customers use to produce various plastic items for industrial and/or consumer use.
The polyester chips are manufactured in a solid-state polymerization process.
Documents Reviewed:
✓ NPDES Stormwater Permit Application Materials (EPA forms 1&2F).
✓ National Heritage Program (NHP) Threatened and Endangered Species Database
✓ SPU File
✓ Central Files — no files or data in central files.
✓ EPA Sector -Specific Permit, 2008
✓ 303(d) List, 2008 draft, 2006 final
✓ NC Secretary of State's website to check permit name
✓ 2003 permit
✓ EPA TRI database and Environmental Defense fund Scorecard
History:
• Date permit first issued: 8/15/2003
• Date permit re -issued: August 15, 2003—Aug. 15, 2008
• Date permittee submitted renewal application: 3/6/2008
Page 2 of I 1

?JCS'000392
Figure 1: Map of Facility
r.l •s..
♦' r "s 'J �•L. JJf r t ri•1C pie reJ'•.
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xk. DAK Americas LLC
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NCS000392
DAK Americas LLC
Leland, NC
N
Latitude: 3413 19' 10" N
f
Longitude: 780 02' 23" W
County: Brunswick
Receiving Stream: UT the Cape Fear River,
Bay Branch, Otter Branch, and Mullberry Branch
Map Scale 1:311,381)
Stream Class: All C, Sw) }•}CAW; PNA
Sub -basin: 03-06-17 (Cape Fear River Basin)
�r rrts���lw�;'-•''�i
r 1�rr =�rA`�r: Lj �
Facility Location
Wage 3 of l 1

NCS000392
Central Office Review Summary:
1_ Owner's. Other Permits:
NC0000663. (NPDES WW), WQ0012759 (Land application of WW), BRUNS-2006-372 (Erosion and
Sediment Control Permit), SW8060138 (NC State SW Permit), 03033T36 (NC DENR Air Permit),
NCD047369046 (RCRA), Channel No. 12-67 (Outfall Permit). � �
Zorn
General Observations:
1& 2F: Materials representing a possibility of contact with stormwater are: AFFF liquid foam concrete, cal-
n ^�shield, Coal, #2 Diesel fuel, dyed diesel fuel, ethylene glycol, No. 6 fuel oil, regular gasoline, hydrogen peroxide,
magnesium chloride, Novus CE 2688, paraxylene, sodium hypochlorite (15%), solest 68 oil, terphthalic acid, and
transformer oil.
Also potential sources are: , , oCL
1-CO
Yy
I�c Vy'
Outfall 2.
Acetic acid, cobalt slurry, diesel fuel, DRL-6, finish oil, Florence non -white, gasoline, glycol, KP-1,
lube oil MgCI, Methanol, No.2 fuel oil, Paraxylene, phosphoric acid, TEG, TRIM#1, Uran, Waste
-�
oil COAL YARD, ompressors, cooling tower, drum storage areas, gas, oil'and lube mobile truck,
ls�loil/water
separator, transformers.
Outfall 2A
No SW pollutant sources ID'd in this SW area.
Outfall 3
Ethylene glycol, dowtherm A in piping system, compressors containing SOlest 68 oil, Parking lot
Outfall 3A
Polymer, railcar storage area and transportation of raw materials (including TPA and ethylene
glycol)
Outfall 3B
Sodium hypochlorite, river water and fresh water pond,
Outfalls 4 & S
Land application fields (WQ permit - requ monitoring); sand blasting and painting, railcar
maintenance area, wastewater sludge lagoon,
Outfall 6
WWTP, . ydrogen peroxid { emergency response fire training, AFL FF highlexpansion foam, PA,
new monomers railcar storage area
Outfall /
No SW pollutant sources ID'd in this area.
Outfall 8
No SW pollutant sources ID'd in this area.
"ALSO - See attached PDF of information from EPA forms 1 & 2F for more information
3. Impairment:
o This section of the Cape Fear and other water bodies do not have a TMDL and are not on either the
2008 or the 2010 303D list. Further downstream (approx 10 miles by water), the Cape Fear is listed as
impaired for Copper, Turbidity, low pH, and low DO - however the Brunswick River also comes in at
this point and it is gVite far down the river.
4. Threatened and Endangered:
o The NHP web workspace was reviewed on Feb 11, 2011, it showed that the American Alligator was
found in Indian Creek. This is near the DAK Americas Cape Fear Site, however, the site does not drain
to this water body. Additionally, the accuracy of the NHP data was rated as low, and the alligator was
last seen here in 1978.
c3Nxt, 1aD_ pS�Q c 3 }� Q -Li'_ 4,L4- 6.�1-zz`-r�.- c�u.l�, _ � •
S. Location:
o The site drains to 4 receiving waters and is very large with many sub -drainage areas. In the previous
permit and in the applicant's EPA form 1 and 2F for renewal, they both state that Dollison's Swamp is
a receiving water, however, Dollison's swam is not a classified water body. These outfolls drain to the
Cape Fear River (18-(63)b) - which is the classified water body. There is no classification for Dollison's
Swamp in the GIS layer or in BIMS as of Feb 11, 2011.
6. Industrial Changes Since Previous Permit:
o See questions below.
Page 4 of] l
MR

NCS000392
' 7. Analytical Monitoring Notes:
o No data in files; previous permit did not require analytical monitoring. However rene�lal EPA forms 1
& 2F provided monitoring of all outfalls. No data was above benchmarks. The highest data points
were at outfalls 002A, 007 and 003.. See data below.
o EPA MSGP requires monitoring for Zinc for these SIC codes (2821 and 2824) . See questions asked to
the permittee below.
8. Qualitative Monitoring Notes: No data in files or with submission.
V.►-�DA. titti.. �e-u� o�-�.a�a.l c�9-9� c,�La_ra9�-a��r�, ,mom-ru��-���q
Page 5 of l 1

NCS000392
Table 1: Analytical Monitoring
Outfall
Outfall
Outfall" Outfall
1 Oufall
Outfall
Outfall
Outfall
Outfall I
All analyzed in Feb. 2008
008
003
003A 003E
002A
i
! 002
f007
006
004
BOD
2
43
2 <2 -
14
13
4
2
<2
COD
35
68 1
13 25
51
E 35
40
' 28
34 ,
O&G
<5
5
8 , <5
<5
<5
<5
I <5
TSS
5
5
2 '1 <2
30
54
1<5
47
21
J 4
Nitrate + Nitrite N
0.02
0.1
0.07 0.03
0.82
1.11
0.05
0.09
1 0.05 i
TKN
1.5
1.3
1.3 0.7
2.2
3.1
1.3
1.4
1.3
TN
1.5
1.4
1.4 0.7
3
4.2
1.4
1.5
1.4 -
TP
0.04
0.05
0.02 0.02
0.36
0.5.1
0.18
0.12
0.04
Above Benchmark
ata4Missin
Page 6 of 11

NCu000392
Discussions with permittee: Elizabeth Wike, 910-371-4498, Called February 15, 2011 & February 17, 2011. She
has not returned my calls. I will update this as soon as I hear from her and send this to the R0.
1. Have you had any name changes? We have your last name as DAK Americas LLC.
a. fL6
2. Have you had any industrial changes since your last permit or since you applied in 1008?
a.
3. On your application you stated that portions of the site drain to Dollison's swamp. That maybe true, but
Dollison's swampis not a classified water body. Do you know what water body they ultimately drain to -
the Cape Fear River?
C
'
4. Can you please describe what is in each dr nage area for each outfall: uo-� 4.} S W uQW
a. 001? Any SW data? &Nfl)
i. NoA/ij tAd x9Ht _#0-00- 6�u4,d ujW-rp
b. 002: Lists a lot of chemicals. Do they all have exposure to stormwater? Do the ASTs have secondary
containment? Please describe. 1
i. C7- 1'G3 S -arWu` !° ��a_ru a 2� -V
c. 002A : No SW exposure? Please describe what is in this drainage area.
0('a
�}
J �,)11
, d. 003: Please describe further what is in this drainage area. Is there the potential for ethylene glycol
& do wtherm.A.to- contact. SW? Have you ever tested for those in SW?
-�-
�b�✓ e. 003A: Please describe further what is in this drainage area. " potential for spills or leaks from
p railcar." What is in the railcars? Have you ever tested for that in SW?
(�&La-ek �2g- n,,
003B. Sodium hypochloriter does it have secondary,containment? Please describe.
i.
ooco
g. 004: This area seems to not be covered under NPDES? Do application field runoff and SW runoff
D�pQ commingle before exiting property? p
&0S ka,4 YWf c�2CQ--�e w( perilu °J -�4 e"
� G! ALP CQ-►�-��`� he y` � c� d c c �,c cG! CA 9,,0e.L -2cl.e4�. >< o
vW� h. 00.5 This area seems to not be covered under NPDES? Do application field runoff and'SW runoff L.4)0.)rP-
commingle before exiting property?tj1
L 006: You have no secondary containment for HzOz, however you permit actually does require that
`...secondary containment for bulk storage of liquid materials" Part 11, Section A, 2(b).
i. We.
Page 7 of 1 ]

NCS000392 , ,
j. 007. No SW exposure? Please describe what is in this drainage area
". GC v o_-G e 1Z0 u
k. 008: No SW exposure? Please describe what is in this drainage area
1. 008A? You have a drainage area an your map but no outfall located on the map.
i. %LQ-Q K_ .
5. Have you done qualitative monitoring per your permit? Please send me a copy of your qualitative
monitoring.
W-U-e. Vie-
6. Do you have any vehicle maintenance areas? _.
a. fJ
�cr� �►��.., , �-�.�-�ca C_� c_e_u-2�.n c_ ��-cre►--�'�`�-�GdcJ
a� 1 7. What area DR�, abshield, Paroxylene, TETRIM#1, G ran. Please describe and provide MSDS sheets.
C .= a. 4 - coo �r ,r
DfZ L 6 ! KP —1 inn_- Yu--r1-orx �D ec�v�_ . rnsDss v i�o9 6s�
8. Please describe how coal is exposed to stormwater and where that drains. ` `3es�C'�)
a. : (J
9. Does any of the cooling tower water go into the stormwater outfalls? If so, ore they monitored by NPDES WW
group? �pa� � � �� u •mac A V (Ck- SV,)
a. ^> `'Sew Ylj)0 Pt&rr�*
10. Are any of your stormwater outfalls covered in the NC wastewater NPDES permit?
a. /)_�_) '�-3 :
11. Are any SW and WW outfalls commingled? Are they monitored b NDDES WW permit?
.z � � � �� co o �, o_a a 0_ ., ` `l-P IUD trS .
12. Do you have any zinc or materials containing zinc exposed to stormwater on your site?
a . C', r9 —OU C�4 a Yu-� C7�4 0
13 Do you have any of the ollo wing materials exposed to storm water on your site -if so where, and how are they
used and contained? (See attached spreadsheet).
a.
Savo- w c44 '4-0_uSh;—1,.._� sL o. p� lu-► u xb ►• fl e3. 9s� c�v_e `WQ-
14. Where do you use or produce; -,`4 Dioxane onsite?i Where is it stated and is it exposed to st rmwater? If it is not s�i. ,
exposed to stormwater, how -is it different than the Fayetteville site?
a. E Y_� b�u 2 - ., I acf�ma. e �► 5 �:1-e�. , , , slt�
15. Is any of your stormwater area routed to your WWTP and have you ever had a wastewater overflow due to high
stormwater flow?
W W� Page 8 of 11 �oE o

NCS000392 `" � Z3 ZD� j CCU_ I fiy✓t
Discussions with permittee: Elizabeth Wike, 910-371-4498, Called F bruary 15, 2011 & February 17, 2011, She
4-
has not returned my calls. I will update this as soon as I hear from her and send this to the RO.
1. Have you had any name changes? We have your last name as OAK Americas LLC.
a. no
2. Have you had any industrial changes since your last permit or since you applied in 2008?
a. Nothing substantial
3. On your application you stated that portions of the site drain to Dollison's swamp. That may be true, but
Dollison's swamp is not a classified water body. Do you know what water body they ultimately drain to —
the Cape Fear River?
a. Cape Fear River
4. Can you please describe what is in each drainage area for each outfoll:
a. 001 ? An y SW data?
i. Only WW treatment plant— only sw that falls on ww treatment plant. Any sw will go into
treatment system.
b. 002: Lists a lot of chemicals. Do they all have exposure to stormwater? Do the ASTs have secondary
containment? Please describe.
c. 002A : No SW exposure? Please describe what is in this drainage area.
i. There is a road and some grassy areas, not really any industrial areas.
d. 003: Please describe further what is in this drainage area. Is there the potential for ethylene glycol
& dowtherm A to contact SW? Have you ever tested for those in SW?
e. 003A: Please describe further what is in this drainage area. "potential for spills or leaks from
railcar." What is in the railcars? Have you ever tested for that in SW?
i. It potentially could be all the chemicals that are brought into the facility. Bring it all in by rail.
ii. Have never had a spill from a railcar.
iii. She doesn't know if they have — she will check on that and get back to me.
iv. Part of site parking lot and big grassy field, road and rail line. No industrial activity. No spill,
so no need to test in past.
f. 003B: Sodium hypochlorite —does it have secondary containment? Please describe.
i. Yes.
ii. Pump water is just water from the river. No chemicals going into that.
g. 004 & 005: This area seems to not be covered under NPDFS? Do application field runoff and SW
runoff commingle before exiting property?
i. The industrial areas and the land application area — that would be commingled before exiting
Page 7 of 13

NCS000392
outfall.
ii. Since they have turned in the
iii. 2 permits: 1 for land app of sludge and 1 for surface disposal of sludge. Recently asked DEN
to close land app of sludge. This year they rescinded permit.
iv. The spray fields have not used the sprayfields since maybe the 1980s — many years.
v. The sludge lagoon permit is still active. Any drainage from sludge lagoon goes to wwtp.
vi. Now it is a big grassy field.
vii. So really only sandblasting and painting
viii. Some railcar maintenance is done there. Not under cover. The maintenance is sandblasting
and painting.
1. No.
2 •Lin'tla�Willis--ean youplease",take+a•look•�;at�wlien:youlda'a`�site visit'?
h. 00:5 This area seems to not be covered under NPDFS? Do application field runoff and SW runoff
commingle before exiting property?
i. Yes. See above. No more land application.
ii, Never had,a..spill from that area.
j. 007: No SW exposure? Please describe what is in this drainage area
i. Trees
k. 008: No SW exposure? Please describe what is in this drainage area
i. Trees. There is a part of 008 that was cleared as a borrow site, but most of that area is
wooded. The borrow site is inactive. This is all stabilized now.
L 008A? You have a drainage area on your map but no outfall located on the map.
i. She thinks they missed a dashed line when they created the map. Contains railcar storage,
don't load. They are either empty or filled with competed storage. All of that drains to a
stormwater pond that drains on the west end of that area. Now that area drains out to outfall
003. Just 008A drains to the SW pond, then it drains to 003 where it commingles and goes to
the 003 outfall. 008A is the drainage area between 008 and the road —the long skinny area.
5. Have you done qualitative monitoring per your permit? Please send me a copy of your qualitative
monitoring.
Page 8 of 13

NCS000392
W will send me a eo of the last 5 ears
6. Do you have any vehicle maintenance areas?
a. They don't do any vehicle maintenance — they send it out.
7. What are:
a. DRL-6, KP-1, cal -shield, Paraxylene, TEG, TRIMIf1, Uran.
b. Please describe and provide MSDS sheets.
M OR will et back to me on this
8. Please describe how coal is exposed to stormwater and where that drains.
a. 002A —in the center —there are two outfalls. The pile has a stormwater pond. That pond drains to outfall
002 through piping.
b. The treatment in that coal stormwater pond is just stetting.
c�Linda -- can you(p.leas'e take a look at tli� fhis:is,covered under NPDES WW permit — but not sure if all
SW in this outfall (002) is�eovered undeFWs. "Does not appear to be. See next question.
9. Does any of the cooling tower water go into the stormwater outfalls? If so, are they monitored by NPDES WW
group?
a. Outfalls 002 and 003 have cooling water blowdown. They are monitored
b. NPDES WW permit: 001, 002, 003 only
i. For outfall 002, they monitoring flow weekly, TSS weekly, Numerical Limits for TSS, temp weekly,
TRC weekly, Numerical limits, pH 2x/month, TKN, TN, and NO2-NO3-N
1. Discharge non -contact, water treatment filter backwash, coal pile runoff, and
ii. Outfall 003: noncontact cooling water, cooling tower and boiler blowdown, and stormwater
1. Flow, temp, TRC, (all weekly), pH 2x/month, monthly: TP, TN, TKN, NO2-NO3N
m
10. Are any of your stormwater outfalls covered in the NC wastewater NPDES permit?
a. Yes, 001, 002 and 003. See above.
11. Are any SW and WW outfalls commingled? Are they monitored by NDPES WW permit?
a. Yes 002 and 003. See above.
12. Do you have any zinc or materials containing zinc exposed to stormwater on your site?
a. Piping. Not a major part of their process.
13. Do you have any of the following materials exposed to stormwater on your site —if so where, and how are they
used and contained? (See attached spreadsheet).
ee attached sheet. EW will answer in returned email b March 15 2031
Page 9 of 13

NCS000392
14. Where do you use or produce 1,4 Dioxane onsite? Where is it stored and is it exposed to storm water? if it is not
exposed to stormwater, how is it different than the Fayetteville site?
15. is any of your storm water area routed to your WWTP and have you ever had a wastewater overflow due to high
stormwater flow?
a. Generally speaking a lot of the area is no. There are areas around the monomer system drain through
concrete -lined ditch to WWTP.
b. No overflows from WWTP.
16. Have you had any major spills?
a. Not one that ran off the site.
b. Some years ago they did have something but it was quite some time ago. They have lots of BMP, means
to block of ditches, they have a lot of containment and BMPs across the site.
17. Do you manufacture the some thing as the Fayetteville site?
a. They do, but they also manufacture some other things.
b. N. of railroad is monomers manufacturing area:
i. Terephthalic acid (TPA). That is then used on the other side of the plant or goes to the S side of
the plant.
c. Then on the south side of the plant in the two large shaded areas:
i. The one to the E: they manufacture polyester fibers.
ii. In the on to the W they make PET plastic (resins).
Page 10 of']',

NCS000392
Chemical Name Drainage Area Method chemical is stored in
1,4-DI OXAN E
ACETALDEHYDE
AMMONIA
ANTIMONY COMPOUNDS
BARIUM
BENZENE
BIPHENYL
BROMOMETHANE
CHLORINE
CHLORODI FLUOROM ETHANE
COBALT COMPOUNDS
DIOXIN AND DIOXIN -LIKE --P
COMPOUNDS
ETHYLENE GLYCOL
HYDROCHLORIC ACID (1995 AND
AFTER "ACID AEROSOLS" ONLY)
LEAD COMPOUNDS
MANGANESE COMPOUNDS
MERCURY COMPOUNDS
METHANOL
N-BUTYL ALCOHOL
NITRATE COMPOUNDS
O-XYLENE
POLYCYCLIC AROMATIC
COMPOUNDS
P-XYLE N E
SODIUM NITRITE
SULFURIC ACID (1994 AND
AFTER "ACID AEROSOLS" ONLY)
TOLUENE
Possible method of exposure to stormwater (put
none if none)
Page 9 of 1 1

NCS000392
Revised Permit Recommendations:
1. At this time (before speaking with the onsite representative and before the RO site visit), the permit reviewzr
suggests adding TSS, BOD, COD, TKN, TN, TP, Oil and Grease, and pH. Additionally, Cobalt, Ethylene Glycol,
and 1,4 Dioxane are also possibly recommended to be added. No analytical monitoring was included in the
previous permit (2003-2008). This list and draft permit will be re-evaluated after RO site visit.
2. All analytical monitoring has been set to semi-annually during a representative storm event as defined in Part
II Section B. The permittee must also document the total precipitation for each event. If no discharge occurs
during the sampling period, the permittee must submit a monitoring report indicating "No Flow" within 30
days of the end of the six-month sampling period. Additionally, samples must be taken a minimum of 60 days
apart, as specified in Table 2.
3. Benchmarks for analytical monitoring have been added to this draft permit. Exceedances of benchmark values
require the permittee to increase monitoring, increase management actions, increase record keeping, and/or
install stormwater Best Management Practices (BMPs) in a tiered program, If the sampling results are above a
benchmark value, or outside of the benchmark range, for any parameter at any outfall then the facility shall
follow the Tier 1 guidelines which require a facility inspection within two weeks and implementation of a
mitigation plan within two months. If during the term of this permit, the sampling results are above the
benchmark values, or outside of the benchmark range, for any specific parameter at a specific discharge
outfall two times in a row (consecutive), then the facility shall follow the Tier 2 guidelines which require a
repetition of the steps listed for Tier 1 and also immediately institute monthly monitoring for all parameters at
every outfall where a sampling result exceeded the benchmark value for two consecutive samples.
4. The permittee is required to collect all of the analytical and qualitative monitoring samples during
representative storm events as defined in Part II Section B. Qualitative monitoring is required regardless of
representative outfall status.
5. The permittee is responsible for all monitoring until the renewal permit is issued. See Footnote 1 of Tables 1,
4, and 5.
6. The flow reporting requirement has been removed per DWQ revised strategy. (The total rainfall parameter is
in this permit, however.)
7. Vehicle maintenance monitoring has been revised to semi-annually in order to coincide with analytical and
qualitative monitoring.
Other Proposed Changes to the Previous Permit:
1. Additional guidance is provided about the Site Plan requirements. The site map must now identify if the
receiving stream is impaired and if it has a TMDL established. It must also describe potential pollutants in each
outfall. The map requirements are stated more explicitly. And, the site plan must contain a list of significant
spills that have occurred in the past three years and also must certify that the outfalls have been inspected to
ensure that they do not contain non-stormwater discharges. Additional information is provided in Part II
Section A.
2. Additional requirements for the Stormwater Management Plan have been specified in Part II Section A. More
details regarding secondary containment are provided.
3. Additional requirements for the Stormwater Pollution Prevention Plan have been specified in Part 11 Section A.
The plan must also be updated annually to include a list of significant spills and to certify that the outfalls do
not contain non-stormwater discharges.
4. The facility must now implement a semi-annual Facility Inspection Program of the site's stormwater
management controls as specified in Part II Section A.
5. Information regarding the No Exposure Exclusion has been added to this draft permit. If industrial materials
and activities are not exposed to precipitation or runoff as described in 40 CFR §122.26(g), the facility may
qualify for a No Exposure Exclusion from NPDES stormwater discharge permit requirements. Additional
information is provided in Part I Section A.
Page 10 of 11

NICS000392
Recommendations: Based on the documents reviewed, the application information submitted on March 6, 2011
sufficient to_ issue a preliminary Individual Stormwater Permit for RO staff review. After RO staff review, staff
report and Draft permit will have a 2Id central office individual permit review.
Prepared by (Signature) 2I r 7 Date
Stormwater Permitting Unit Supervisor s f ze-e�'� Date
for Bradley
e� Bennett
Concurrence by Regional Offi Date WAAZ 2-10 ZO//
RO Water Quality Supervisor E�� �,.�( _.� ��� ��. Date h 7
Regional Office Staff Comments (attach additional pages as necessary)
� • • • " ! • 0� , � 1 • ♦ r is
! r
4-0 VJL
LAD
CN44-
• • ♦ • ��
Page 1 1 of 11

ex F IIbioPermit NC0000663
A. M EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS— OUTFALL 001
Beginning on the effective date of this permit and lasting until either the Authorization to Construct
approval by the Division and receipt of the Engineer Certificate for the approved expansion to 4.77
MGD, or expiration, the Permittee is authorized to discharge treated wastewater from cuffaH 001.
Such discharges shall be limited and monitored by the Permittee as specified below:
ti .,,.> x ;,
+4_EFFLUENT,,LIMITATIONSrA ii,' s
MONITORING REQUIREMENTS,
EFFLUENT Cg ��
3
A A r,,Sz �•�s
,z
r, r a.
L
�CHARACTE=R1$TICS
,b�;Measurement
+` •. _ " t
;Sam le
P
n `5amOle'
,.Monthly Average
?Daily Maximum
�
a Frequency, -
• . 1
T e
YP
,
Location .
;
h.f-,d...
Flow
3.5 MGD
Continuous
RecordingInfluent
or
Effluent
SOD, 5-day, 20oC
493.3 Ibslday
1283.5 Ibs/day
Daily
Composite
Effluent
Total Suspended Solids (TSS)
786.0 Ibs/day
2495.3 Ibslday
Daily
Composite
Effluent
PH
Not more than 9.0 S.U. nor less than 6.0
3/Week
Grab
Effluent
S.U.
Temperature, °C
3/Week
Grab
Effluent
Conductivity, µmhos/cm
3/Week
Grab
Effluent
Total Residual Chlorine (TRC) 1
28 µg/I
Weekly
Grab
Effluent
Dissolved Oxygen (DO)
Not less than 5.0 mg/l, daily average
2/Month
Grab
Effluent
Fecal Coliform
Monthly
Grab
Effluent
(geometric mean)
Total Nitrogen, mg/I
Monthly
Calculated
Effluent
TN = (NO2-N+NO3-N) + TKN
Nitrite/Nitrate Nitrogen, mg/I
Monthly
Composite
Effluent
(NO2-N+NO,-N)
Total Kjeldahi Nitrogen, mg/1
Monthly
Composite
Effluent
(TKN)
Total Phosphorus, mg/I (TP)
Monthly
Composite
Effluent
Ammonia as Nitrogen, mg/1
Quarterly
Composite
Effluent
(NH3 as N)
Total Copper, µg/l
Quarterly
Composite
Effluent
Acute Toxicity 2
Quarterly
Composite
Effluent
Footnotes:
1. Total Residual Chlorine compliance is required for chlorine or chlorine derivative used for disinfection.
The Division shall consider all effluent TRC values reported below 50 ug/I to be in compliance with the
permit. However, the Permittee shall continue to record and submit all values reported by a North
Carolina certified laboratory (including field certified), even if these values fall below 50 ugll.
2. Acute Toxicity, refer to A. (7).
Ibslday = pounds per day
There shall be no discharge of floating solids or visible foam in other than trace amounts.
When an approved analytical protocol with the appropriate minimum detection level is followed and a
result of "non -detectable" or "below quantitation limit" is obtained, the permittee will be considered
to be in compliance with the numerical permit limit for that pollutant.

Permit INIC000'0653
A.(2) EFFLUENT LIMITATIONS AND MONITORING REOUiREMENTS/OCPSF\-OUTFALL
001
Beginning on the effective date of this permit and lasting until either the Authorization to Construct
approval by the Division and receipt of the Engineer Certificate for the approved expansion to 477
MGO, or expiration, the Permittee is authorized to discharge O[PSF're|ated process wastewater from
ouhfall 001. Such discharges shall be limited and monitored by the Permittee as specified below:
MONITORING
REQUIREMENTS.
Benzene
0.708
2.602
Annually
Composite
Effluent
Bis(2-ethylhexyl) phthalate
1.971
5.338
Annually
Composite
Effluent
Carbon Tetrachloride
0.344
0.727
Annually
Composite
Effluent
Di-n-butyl phthalate
0.517
1.091
Annually
Composite
Effluent
Diethyl phthalate
1.550
3.884
Annually
Composite
Effluent
Dimethyl phthalate
0.364
0.899
Annually
Composite
Effluent
Methyl Chloride
1.645
3.635
Annually
Composite
Effluent
Methylene Chloride
0.765
1.703
Annually
Composite
�ff luent
Naphthalene
0.421
1.129 1
Annually
Composite
Effluent

Permit NCO000663
(continue A. (2) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS (OCPSF)-OUTFALL 001)
.EFFLUENT
CHARACTERISTIC...
" '?
-EFFLUENT
-Monthly
Average s
g
s/da)
LIMITATIONS
;Daily :Daily' f
-Maximum 'Maximum
(Ibs/da ). ( jj)
..MONITORING:;REQUIREMENTS
,-
Measurement �5arrmple r
z ti rF
Frequency �� ,;Type z �.'
�:.
Sample
Location
4-Nitrophenol
1.378
2.372
Annually
Composite
Effluent
Phenanthrene
0.421
1.129
Annually
Composite
Effluent
Phenol
0.287
0.497
Annually
Composite
Effluent
Pyrene
0.478 "
1.282
Annually
Composite
Effluent
Tetrachloroethylene
0.421
1.071
Annually
Composite
Effluent
Toluene
0.497
1.531
Annually
Composite
Effluent
1,2,4-Trichlorobenzene
1.301
2.678
Annually
Composite
Effluent
1,1,1-Trichloroethane
0.402
1.033
Annually
Composite
Effluent
1,1,2-Trichloroethane
0.402
1.033
Annually
Composite
Effluent
Trichloroethylene
0.402
1.033
Annually
Composite
Effluent
Vinyl Chloride
1.990
5.127
Annually
Composite
Effluent
Total PAH z
1.36
46.71
-Annually
Composite
Effluent
Benzo(a)anthracene
0.421
1.129
Annually
Composite
Effluent
. 3,4-Benzofluoranthene
0.440
1.167
Annually
Composite
Effluent
Benzo(k)fluoranthene
0.421
1.129
Annually
Composite
Effluent
Benzo(a)pyrene
0.440
1.167
Annually
Composite
Effluent
Chrysene
0.421
1.129
Annually
Composite
Effluent
Dibenz(a,h)anthracene
Annually
Composite,
Effluent
tndeno(1,2,3-ed)pyrene
Annually
Composite
Effluent
Footnotes:
1. Monitoring for the specified parameters has been waived based on a demonstration made, by the
Permittee in accordance with 40 CFR 122.44(a)(2)(i). This waiver is good only for the term of the
permit. Please note that any exceedence of the effluent limitations found herein shall be
considered a permit violation subject to appropriate enforcement action.
2. Total PAHs. are comprised of Benzo(a)anthracene, Benzo(a)pyrene, 3,4-Benzofluoranthene,
Benzo(k)fluoranthene, Chrysene, Dibenz(a,h)anthracene, and lndeno(1,2,3-ed)pyrene. The sum 'of
concentrations of these parameters shall not exceed the stated Total PAH limit.
Ibslday = pounds per day

Permit NC000b663
A. (3) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS — OUTFALL
Beginning on the Authorization to Construct by the Division and the receipt of the Engineer
Certificate for the approved expansion to 4.77 MGD, and lasting until expiration, the Permittee is
authorized to discharge treated wastewater from outfa/l 001. Such discharges shall be limited and
monitored by the Permittee as specified below:
r.;o} F�
Na
:EFFLUENTLIMITATIONSZ,�--=r
�MON(TO RENGREQEJIREMEiVTS
EFFLUENT
y�k
Maximum
Measurement
Sample
Sample
CH ARACTERISTICS
s
Montfiiy Average
q,Daily g
y Frequency
}n
Location
.f
R:Type
Flow
4.77 MGD
Continuous
Recordin g
Influent or
Effluent
BOD, 5-day,
198.91 lbs/day
298.36 lbs/day
Daily
Composite
Effluent
(April 1 _Octobeober 31)
BOD, 5-day, 203C
298.36 Ibs/day
449.54 Ibs/day
Daily
Composite
Effluent
(November 1 — March 31)
Total Suspended Solids (TSS)
786.0 Ibs/day
2495.3 Ibs/day
Daily
Composite
Effluent
pH
Not more than 9.0 S,.U. nor less than 6.0
3/Week
Grab
Effluent
S.U.
Temperature, °C
3/Week
Grab
Effluent
Conductivity, µmhos/cm
3/Week
Grab
Effluent
Total Residual Chlorine (TRC) 1
28 µg/I
Weekly
Grab
Effluent
Dissolved Oxygen (DO)
Not less than 5.0 mg/I, daily average
2/Month
Grab
Effluent
Fecal Coliform
Monthly
Grab
Effluent
(geometric mean)
Total Nitrogen, mg/1
Monthly
Calculated
Effluent
TN = (NO2-N+NO3-N) + TKN
Nitrite/Nitrate Nitrogen, mg/1
Monthly
Composite
Effluent
(NO2-N+NO,-N)
Total Kjeldahl Nitrogen, mg/I
Monthly
Composite
Effluent
(TKN)
Total Phosphorus, mg/l (TP)
Monthly
Composite
Effluent
Ammonia as Nitrogen, mg/1
Quarterly
Composite
Effluent
(NH3 as N)
Total Copper, µg/I
Quarterly
Composite
Effluent
Acute Toxicity 2
Quarterly
Composite
Effluent
Footnotes:
1. Total Residual Chlorine compliance is required for chlorine or chlorine derivative used for disinfection.
The Division shall consider all effluent TRC values reported below 50 ug/l to be in compliance with the
permit. However, the Permittee shall continue to record and submit all values reported by a North
Carolina certified laboratory (including field certified), even if these values fall below 50 ug/l.
2. Acute Toxicity, refer to A. (7).
Ibslday = pounds per day
There shall be no discharge of floating solids or visible foam in other than trace amounts.
When an approved analytical protocol with the appropriate minimum detection level is followed and a
result of "non -detectable" or "below auantitation limit" is obtained. the Permittee will he considered
to be in compliance with the numerical permit limit for that pollutant.

PermitNCO000663
A. (4) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS (OCPSF)-OUTFALL
001
Beginning on the Authorization to Construct approval by the Division and the receipt of the Engineer
Certificate for the approved expansion to 4.77 MGD, and lasting until expiration, the Permittee is
authorized to discharge OCPSF-related process wastewater from outfall 001. Such discharges shall
be limited and monitored by the Permittee as specified below;
' 'EFFLU
L; CiHARACTERISTIC'
�'=; EF;FLUENT.,;LIMITATIONS,
f�Fv,' °
"`"'''
' ;'i`'MONITORING REQUIREMENTS
'-NIdnthly
` �_ 'r�
Average ,�Maximum
v(IUS/da ),<
'` :�r;Daily < y
C R
(Ibslda ).
°� Daily
Maxirrtum
%," (
Measurement
F,Fregilency'-
Sample .
a Type
Sample
Location
Acenaphthene
0.57
1.53
Annually
Composite
Effluent
Acenaphthylene
0.57
1.53
Annually
Composite
Effluent
Acrylonitrile
2.49
6.28
Annually
Composite
Effluent
Anthracene
0.25
1.53
Annually
Composite
Effluent
Benzene
0.96
3.53
Annually
Composite
Effluent
Bis(2-ethyl hexyl) phthalate
2.67
7.24
Annually
Composite
Effluent
Carbon Tetrachloride
0.47
0.99
Annually
Composite
Effluent
Chlorobenzene
0.39
0.73
Annually
Composite
Effluent
Chloroethane
2.70
6.95
Annually
Composite
Effluent
Chloroform
0.54
1.19
Annually
Composite
Effluent
2-Chlorophenol
0.80
2.54
Annually
Composite
Effluent
Di-n-butyl phthalate
0.70
1,48
Annually
Composite
Effluent
1,2-Dichlorobenzene
2.00
4.23
Annually
Composite
Effluent
1,3-Dichlorobenzene
0.80
1.14
Annually
Composite
Effluent
1,4-Dichlorobenzene
0.39
0.73
Annually
Composite
Effluent
1,1-Dichloroethane
0.57
1.53
Annually
Composite
Effluent
1,2-Dichloroethane
1.76
5.47
Annually
Composite
Effluent
1,1-Dichloroethylene
0.41
0.65
Annually
Composite
Effluent
1,2-trans-Dichloroethylene
0.54
1.40
Annually
Composite
Effluent
2,4-Dichlorophenol
1.01
2.90
Annually
Composite
Effluent
1,2-Dichloropropane
3.97
5.97
Annually
Composite
Effluent
1,3-Dichloropropylene
0.75
1.14
Annually
Composite
Effluent
Diethyl phthalate
2.10
5,27
Annually
Composite
Effluent
2,4-Dimethylphenol
0.47
0.93
Annually
Composite
Effluent
Dimethyl phthalate
0.49
1.22
Annually
Composite
Effluent
4,6-Dinitro-o-cresol
2.02
7.18
Annually
Composite
Effluent
2,4-Dinitrophenol
1.84
2.19
Annually
Composite
Effluent
2,4-Dinitrotoluene
2.93
7.39
Annually
Composite
Effluent
2,6-Dinitrotoluene
6.61
16.63
Annually
Composite
Effluent
Ethylbenzene
0.83
2.80
Annually
Composite
Effluent
Fluoranthene
0.55
1.76
Annually
Composite
Effluent
Fluorene
0.57
1.53
Annually
Composite
Effluent
Hexachlorobenzene
0.13
0.73
Annually
Composite
Effluent
Hexachlorobutadiene
0.52
1.27
Annually
Composite
Effluent
Hexachloroethane
0.54
1.40
Annually
Composite
Effluent
Methyl Chloride
2.23
4.93
Annually
Composite
Effluent
Methylene Chloride
1,04
2.31
Annually
Composite
Effluent
Naphthalene
0.57
1.53
Annually
Composite
Effluent
Nitrobenzene
l2-Nitrophenol I
0.70
1.06
1.76
Annually
Composite
Effluent
1.79
Annually
Composite
Effluent

Permit NC000060,53 .
(continue A. (4) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS (OCPSF)-OUTFALL 001)
f isF.FLUENT
CHARACTERISTIC`
EFFLUENT LIMITATIONS _.
Monthly Daily �, Daily;
Average Maximum Maximum
;(lb`slda) (Ibs/da) ( jl)
E,: MONITORING, REQUIREMENTS
Measurement` Sample °
1 ; ,
Frequency Type
:.. .
5ampfe.
Location
4-Nitrophenol
1.87
3.22
Annually
Composite
Effluent
Phenanthrene
0.57
1.53
Annually
Composite
Effluent
Phenol
0.39
0.67
Annually
Composite
Effluent
Pyrene
0,65
1.74
Annually
Composite
Effluent
Tetrachloroethylene
0,57
1.45
Annually
Composite
Effluent
Toluene
0.67
2.07
Annually
Composite
Effluent
1,2A-TrichIorobenzene
1.76 -
3.63
Annually
Composite
Effluent
1,1,1-Trichioroethane
0.54
1.40
Annually
Composite
Effluent
1,1,2-Trichioroethane
0.54
1.40
Annually
Composite
Effluent
Trichloroethylene
0.54
1.40
Annually
Composite
Effluent
Vinyl Chloride
2.70
6.95
Annually
Composite
Effluent
Total PAH 1
1.36
34.28
Annually
Composite
Effluent
Benzo(a)anthracene
0.57
1.36
Annually
Composite
Effluent
3,4-Benzofluoranthene
0.60
1.36
Annually
Composite
Effluent
Benzo(k)fluoranthene
0.57
1.36
Annually
Composite
Effluent
Benzo(a)pyrene
0.60
1.36
Annually
Composite
Effluent
Chrysene
0.57
1.36
Annually
Composite
Effluent
Dibenz(a,h)anthracene
Annually
Composite
Effluent
lndeno(1,2,3-ed)pyrene_l
Annually
Composite
Effluent
Footnote:
1. Total PAHs are comprised of Benzo(a)anthracene, Benzo(a)pyrene, 3,4-Benzofluoranthene,
Benzo(k)fluoranthene, Chrysene, Dibenz(a,h)anthracene, and Indeno(1,2,3-ed)pyre ne. The sum of
concentrations of these parameters shall not exceed the stated Total PAH limit.
Ibslday = pounds per day
Should any annual monitoring result in detection of an OCPSF parameter contained in 40 CFR 414
Subpart I quarterly monitoring will begin immediately for the detected parameter(s). After four
consecutive quarterly samples resulting in non -detection are achieved, the monitoring frequency will
revert back to annually.
When an approved analytical protocol with the appropriate minimum detection level is followed and a
result of "non -detectable" or "below quantitation limit" is obtained, the permittee will be in
compliance with the numerical permit limit for that pollutant.

PermitNCO000663
A. (5) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS-OUTFALL 002
Beginning on the effective date of this per and lasting until expiration, the Permittee is authorized
to discharge non -contact once through cooling water, cooling tower and boiler blowdown, water
treatment filter backwash, coal pile runoff 'and stormwater runoff through outfall 002. Such
discharges shall be limited and monitored by the Permittee as specified below:
�.•yi, 2'4$M
Y3 '.
F : 'J' ; "fir ` 3• �T'] 7
*, t
r :EFFLUENT LIMITATIONS
`A
-.[
.. ��� MONITORING EQU a.
R IREMENTS
EFFLUENT�� .;�
,,, h � �
t ;.�
CHARACTERISTICS
Monthly ,'
;Weekly�Measuremerit
Sample : Y
r5ample
4
�erage
a
Average,
1`Max�nium
Frequency!?
Type dti
Location,'
S
y
t
Flow, MGD
Weekly
Instantaneous
Effluent
Total Suspended Solids (TSS)
75 mg/1
150 mg/I
Weekly
Grab
Effluent
Temperature, °C 1
Weekly
Continuous
Effluent
Total Residual Chlorine (TRC) Z
17 µg/1
Weekly
Grab
Effluent
Not more than 9.0 S.U. nor less than
pH
6.0 S.U.
2/Month
Grab
Effluent
Total Phosphorus, mg/I (TP)
Monthly
Composite
Effluent
Total Nitrogen, mg/I (TN)
Monthly
Calculated
Effluent
TN = (NO,-N + NO,-N) + TKN
Nitrite/Nitrate Nitrogen, mg/I
Monthly
Composite
Effluent
(NO2-N + NO3-N)
Total Kjeldahl Nitrogen, mg/I
Monthly
Composite
Effluent
(TKN )
Footnotes:
1. The discharge shall not cause the temperature of the receiving water to exceed 2.8'C above
background and in no case exceed 32 QC.
2. Total Residual Chlorine compliance is required for chlorine or chlorine derivative used for disinfection.
The Division shall consider all effluent TRC values reported below 50 ug/I to be in compliance with the
permit. However, the Permittee shall continue to record and submit all values reported by a North
Carolina certified laboratory (including field certified), even if these values fall below 50 ug/l.
There shall be no chromium, zinc or copper added to the cooling water except as pre -approved
additives to biocidal compounds.
There shall be no discharge of floating solids or visible foam in other than trace amounts
The permittee shall obtain authorization from the Division prior to the use of any chemical additive in
the discharge. The permittee shall notify the Division in writing at least ninety days prior to
instituting use of any additional additive in the discharge potentially toxic to aquatic life (other than
additives previously approved by the Division). Such notification shall include completion of Biocide
Worksheet Form 101 (if applicable), a copy of the MSDS for the additive and a map indicating the
discharge point and receiving stream.
Submit requests for approval to: NC DENR 1 DWQ / Aquatic Toxicology Unit
1621 Mail Service Center
Raleigh, North Carolina 27699-1621

Permit NC0006663•
M
A. (6) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS-OUTFALL 003
Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized
to discharge non -contact once through cooling water, cooling tower and boiler blowdown and
stormwater runoff through outfall 003. Such discharges shall be limited and monitored by the
Permittee as specified below:
>' sy
z
4 r35
a
t EFFLUENT
}^ N EFFLUI=NT LIMITATIONS`
�� MONITORING REQUIREMENTS
ur N P ✓ c ,. rr..... .., _ _ :..>— .,ice.... -r
` i off ..x �� v 1
CHARACTERIS TICSo��a
Monthlyr
Weekly,
�Darly
Measurement
rR 5ample
x Sample =-.
-
Average
Average'
Maxlmum
;Frequencyx
:, n�
u 'Location
rTYPe F
Flow, MGD
Weekly
Instantaneous
Effluent
Temperature, °C 1
Weekly
Continuous
Effluent
Total Residual Chlorine (TRC) z
17 pg/1
Weekly
Grab
Effluent
Not more than 9.0 S.U. nor less than
pH
6.o S.U.
2/Month
Grab
Effluent
Total Phosphorus, mg/I (TP) 3
Monthly
Grab
Effluent
Total Nitrogen, mg/i (TN) 3
Monthly
Calculated
Effluent
TN = (NO,-N + NO,-N) + TKN
Nitrite/Nitrate Nitrogen, mg/I
(NO2-N + NO3-N) 3
Monthly
Grab
Effluent
Total Kieldahl Nitrogen, mg/1
(TKN) 3
Monthly
Grab
Effluent
Footnotes:
1. The discharge shall not cause the temperature of the receiving water to exceed 2.8 'C above
background and in no case exceed 32 'C.
2. Total Residual Chlorine compliance is required for chlorine or chlorine derivative used for disinfection. The
Division shall consider all effluent TRC values reported below 50 ug/I to be in compliance with the permit.
However, the Permittee shall continue to record and submit all values reported by a North Carolina
certified laboratory (including field certified), even if these values fall below 50 ug/l.
3. The permittee may petition to have the sampling frequency reduced to quarterly after 12 consecutive
samples analyses have submitted.
There shall be no chromium, zinc or copper added to the cooling water except as pre -approved
additives to biocidal compounds.
There shall be no discharge of floating solids or visible foam in other than trace amounts.
The permittee shall notify the Division in writing at least ninety days prior to instituting use of any
additional additive in the discharge potentially toxic to aquatic life (other than additives previously
approved by the Division). Such notification shall include completion of Biocide Worksheet Form 101
(if applicable), a copy of the MSDS for the additive and a map indicating the discharge point and
receiving stream,
Submit requests for approval to:. NC DENR / DWQ / Aquatic Toxicology Unit
1621 Mail Service Center
Raleigh, North Carolina 27699-1621

endations: Based on the documents reviewed, the application information submitted on March 6, 2011
0mm .�.».
�jent'to issue a preliminary Individual Stormwater Permit for RO staff review. After RO staff review, staff
report and Draft permit will have a 2"d central office individual permit review.
! prepared by (Signature] 21 l i Date
Stormwater Permitting Unit Supervisor Date
for Bradley Bennett
Concurrence by Regional Office Date
RO Water Quality Supervisor.
Date
Regional Office Staff Comments (attach additional pages os necessary)
Page 11 of 1 1

Addendum to Staff Report
E. Wike & J. Jones - conversation - 5Z18/11:
1. Ask E. Wike about cobalt - she states in her letter dated May 12, 2011 that cobalt should be
removed from permit parameters. However, in Attachment IV of the permit application, it lists
"potential sources that may be reasonably expected to add pollutants to storm water discharges
or that may result in the discharge of pollutants to the storm water drainage system...". Under
Outfall 002 Cobalt Slurry is listed. In her May 12th letter, E. Wike has stated it was tested on EPA
form 2C, but not for other forms 2F.
a. Was it tested in outfalls for stormwater?
i. Yes -- in outfall 002. However E.W. does not know if that was tested on a day
when it was raining or per stormwater permit.
b. If it was listed in Attachment IV, why now do you not believe that it should be tested for
in outfall 2?
i. They probably listed that there because it is in that outfall (002), but does not
believe it is of significant concern.
ii. Would be willing to live with having it in the permit and then being able to
remove it after a certain amount of testing -
1. I suggested if test 4x, then would be able to petition to remove this
parameter.
1. Ask E. Wike about 1,4 dioxane:
a. What is different about this site than the'Fayetteville site?
i. 1,4 dioxane issue came up before DAK acquired the site, and was something to
do with the acquisition or at the same time as the acquisition by Monsanto. She
does not know the exact facts of the spill though or when it was.
ii. This has not been the case at the cape fear site.
b. Where is it stored and is it exposed to stormwater?
c. If it is not exposed to stormwater, how is it different than the Fayetteville site?
d. What
caused-th spi at the yefteVille-site-and-would t et be at this
b site?
,—E-Wike-would-be-a able-to=a-similar-testte-t*imust�2
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Jones, Jennifer
www
From: Willis, Linda
Sent: Friday, May 20, 2011 11:10 AM
To: Jones, Jennifer
Subject: RE: NCS000389 - DAK Americas Cape Fear Site - Final Permit revision
Sounds like you negotiated a good solution with Elizabeth. I have no objections to the direction you both have agreed
upon.
Linda
From: Jones, Jennifer
Sent: Wednesday, May 18, 2011 4:11 PM
To: Willis, Linda
Cc: Jones, Jennifer
Subject: NCS000389 - DAK Americas Cape Fear Site - Final Permit revision
Hey Linda,
I just spoke to Elizabeth Wike regarding their permit. She agreed to test for cobalt and 1,4 dioxane initially, and if low
levels, would be able to petition to stop testing (as in the case of Cobalt b/c no benchmark) OR could remove if < % of
the benchmark value (in the case of 1,4 dioxane). See wording below.
Let me know if you think this is ok.
I plan to issue the permit May 30"'—that is 15 days after the public notice is up.
Thanks!
Jen
SECTION B: ANALYTICAL MONITORING REQUIREMENTS
Analytical monitoring of stormwater discharges shall be performed as specified in Table 1. All analytical monitoring shall
be performed during a representative storm event. The required monitoring will result in a minimum of ten analytical
samplings being conducted over the term of the permit at each stormwater discharge outfall (SDO).
A representative storm event is a storm event that measures greater than 0.1 inches of rainfall. The time
between this storm event and the previous storm event measuring greater than 0.1 inches must be at least
72 hours. A single storm event may have a period of no precipitation of up to 10 hours. For example, if
it rains but stops before producing any collectable discharge, a sample may be collected if the next rain
roduci a discharge begins within 10 hours.

5. Floating Solids
Choose the number which best describes the amount of floating solids in the stormwater discharge where
I is no solids and 10 is the surface covered with floating solids:
2 3 4 5 G 7 8 9 10
b. Suspended Solids
Choose the number which best describes the amount of suspended solids in the stormwater discharge
where I is no solids and 10 is extremely muddy--
3 4 5 G 7 8 9 10
7. Foam
Is there any foam in the stormwater discharge? Yes
8. Oil Sheen '
Is there an oil sheen in the stormwater discharge'? Yes (To
9. Other Obvious Indicators of Stormwater Pollution List and describe P �� ( o )O� -� ° S1 - a(-�I & KXV
Note: Low clarity, high solids, and/or the Are�6nce of foam or oil sheen maybe indicative of pollutant
exposure. These conditions may warrant further investigation.
Page 2
S WU-242.101599

Table 1. Analytical Monitoring Requirements
Discharge
Measurement
Sample
Sample
Characteristics
Units
Frequencyl
Type2
Location3
Total Suspended Solids
mg/L
semi-annual
Grab
All SDOs except 001 and 002
Biochemical Oxygen
rng/L
semi-annual
Grab
All SDOs except 001
Demand
Chemical Oxygen
mg/L
semi-annual
Grab
All SDOs except 001
Demand
Total Kjeldahl Nitrogen
All SDOs except 001, 002
m g/ L
semi-annual
i l
Grab
(TKN)
and 003
Total Nitrogen (TN)
mg/L
semi-annual
Grab
All SDOs except 001, 002
and 003
All SDOs except 001, 002
Total Phosphorus (TP)
mg/L
semi-annual
Grab
and 003
'Cobalt4
mg/L
semi-annual
Grab
Outfall002
1,4 — Dioxane5
mg/L
semi-annual
Grab
Outfails 002 and 003
All SDOs except 001, 002
pH
standard
semi-annual
Grab
and 003
Total Rainfa116
inches
semi-annual
Rain Gauge
-
Footnotes:
I Measurement Frequency: Twice per year during a representative storm event.
2 Crab samples shall be collected within the first 30 minutes ol'discharge.
3 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) unless representative outfall status has
been granted.
4 The permittee shall monitor Cobalt for the first two full years of the permit. At that time, the permittee may petition DWQ in
writing to reduce or remove this parameter. To make that request, the permittee shall send two summaries of data and two written
requests (an original and a copy) to the DWQ Central Office for review.
5 Tlie permittee 'scontinue m nng aran r t c nainde pennit if rst four mp a nts, all
results re ow one-h of the benchmark value, Each outfal all be con ' on an ittdn' a basis.
6 For each sampled representative storm event the total precipitation must be recorded. An on -site rain gauge or local rain l;aug+
reading must be recorded.
The permittee shall complete the minimum ten analytical samplings in accordance with the sche ule specified below in
Table 2. A minimum of 60 days must separate Period l and Period 2 sample dates unless monthly monitoring has
been instituted under a Tier Two response.
Jennifer Jones
Environmental Engineer
NCDENR I DWQ I Stormwater Permitting Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
512 N. Salisbury St, Raleigh, NC 27604
Phone:
[phone]
Fax:
[phone]
Email:
[e-mail]

F:
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Permit No.: N/C/6 ID /8 /O /D /O /U / or Certificate -of: Coverage N6: ' NIClGIr�l lO
Facility Name: 5 er, , C,
County: (7' C 1 '4 Phone No.
Inspector: " i - in n
Date of Inspection: t
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
i v-
(Signature of Permittee or Designee)
2. Outfalll Description
Outfall No..
Structure (pipe,.ditch, tc.)
Receiving Stream: J < ) -
D scribe the industrial activiitie that occur ithin the outfa11 drainage area: j
2, Color
Describe the color of the disch ge us ag basic of rs {r d, brow , blue, etc.) and tint (light, medium,
dark) as descriptors: - ��r �I r ['
3. Odor
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor,
efc.) 11 11 0C.
4. Clarity
Choose the number which best describes the clarity, of the discharge where I is clear and :10 is very
cloudy:
1 2 (2 4 5 6 7 8 9 10
Page 1
SWU-242-101599