NCS000223_FINAL PERMIT_19941209

STORINIINATER DIVISION CODING SHEET
PERMIT NO.
NC S (;oO 22,3
DOC TYPE
tA. FINAL PERMIT
❑ MONITORING INFO
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ [ q_q q �Z
YYYYMMDD

State of North Carolina
Department of Environment
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
December 9, 1994
Mr. Jetty P Deakle
Envirochem Environmental Service
Investment Blvd.
Apex, NC 27502
Subject: Permit No. NCS000223
Envirochem Environmental Service
Wake County
Dear Mr. Deakle:
In accordance with your application for a stormwater discharge permit received on April 30,
1993, we are forwarding herewith the subject state - NPDES permit. This permit is rued
pursuant to the requirements of North Carolina General Statute 143-215 .1 and the MemorMdum
of Agreement between North Carolina and the US Environmental Protection agency Bated
December 6, 1983.
Cn 0
If any parts, measurement frequencies or sampling requirements contained in thi4e m are
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unacceptable to you, you have the right to an adjudicatory hearing upon written re st�vttn
thirty (30) days following receipt of this letter. This request must be in the form -a w tten
petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed wi the
Office of Administrative Hearings, Post Office Drawer 27447, Raleigh, North Carolina 2 11
-7447. Unless such demand is made, this decision shall be final and binding.
Please take notice this permit is not transferable. Part II, B.2. addresses the requirements to
be followed in case of change in ownership or control of this discharge.
This permit does not affect the legal requirements to obtain other permits which may be
required by the Division of Environmental Management or permits required by the Division of
Land Resources, Coastal Area Management Act or any other Federal or Local governmental
permit that may be required.
If you have any questions concerning this permit, please contact Aisha Lau at telephone
number 919/733-5083.
Siticerely,
1.
es oward, Jr, P. E.
cc: Mr. Jim Patrick, EPA
Raleigh Regional Office
Wake County
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DMSION OF ENVIRONMENTAL MANAGEMENT
S.
TO DISCHARGE STORMWATER UNDER THE
NATLONAL POLLUTANT DISCHARGE ELIMINATION -SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management Commission,
and the Federal Water Pollution Control Act, as amended,
EnviroChem Environmental Services, Inc.
is hereby authorized to discharge stormwater from a facility located at
EnviroChem Environmental Services, Inc.
1005 Investment Blvd.
Apex
Wake County
to receiving waters designated as Middle Creek, a class C NSW stream, in the Neuse River9.3�`sinjl
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in accordance with the discharge limitations, monitoring requirements, and other conditions fo in
Parts I, II, I1I, and IV hereof.
This permit shall become effective January 1, 1995.
This permit and the authorization to discharge shall expire at midnight on December 31, 1999.
Signed this day December 9, 1994.
* Pieston/H6ward, Jr., P.E., Director
Division of Environmental Management
By the Authority of the Environmental Management Commission

Permit No. NCS000223
PERMITTED ACTTVITIES
Until this permit expires or is modified or revoked, the permittee is authorized to discharge
stormwater to the surface waters of North Carolina or separate storm sewer system which has been
adequately treated and managed in accordance with the terms and conditions of this Permit. All
discharges shall be in accordance with the attached schedules as follows:
Part I: Monitoring, Controls, and Limitations for Permitted Discharges
Part II: Standard Conditions for NPDES Stormwater Permits
Part III: Limitations Reopener
Part IV: Administering and Compliance Monitoring Fee Requirements
Any other point source discharge to surface waters of the state is prohibited unless covered by
another permit, authorization or approval.
This permit does not relieve the permittee from responsibility for compliance with any other
applicable federal, state, or local law, rule, standard, ordinance, order, judgement, or decree.
I
Page 2

Permit No. NCS000223
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Page 3

Permit No. NCS000223
PART I
MONITORING, CONTROLS, AND LIMITATIONS FOR PERMITTED
DISCHARGES
During the period beginning on the effective date of the permit and lasting until expiration, the
Permittee is authorized to discharge stormwater associated with industrial activity. Such
discharges shall be controlled, limited and monitored as specified below.
The Permittee shall develop a Stormwater Pollution Prevention Plan, herein after referred to as the
Plan. This Plan shall be considered public information in accordance with Part II, Standard
Conditions, Section EX of this permit. The Plan shall include, at a minimum, the following
items:
a. Site Plan. The site plan shall provide a description of the physical facility and the potential
pollutant sources which may be expected to contribute to contamination of stormwater,
discharges. The site plan shall contain the following:
(1) A general location map (USGS quadrangle map or appropriately drafted equivRnt
map), showing the facility's location in relation to transportation routes and surface
waters. the name of the receiving water(s) to which the stormwater outfall(s) -J
discharges, or if the discharge is to a municipal separate storm sewer system, tb
name of the municipality and the ultimate receiving waters; and accurate latitudF
and longitude of the point(s) of discharge.
(2) A narrative description of storage practices, loading and unloading activities,
outdoor process areas, dust or particulate generating or control processes, and
waste disposal practices.
(3) A site niap drawn to scale with the distance legend indicating location of industrial
activities (including storage of materials, disposal areas, process areas and loading
and unloading areas), drainage structures, drainage areas for each outfall and
activities occurring in the drainage area, building locations and impervious surfaces,
and the percentage of each drainage area that is impervious. For each outfall, a
narrative description of the potential pollutants which could be expected to be
present in the stormwater discharge.
(4) A list of significant spills or leaks of pollutants that have occurred at the facility
during the 3 previous years and any corrective actions taken to mitigate spill
impacts.
(5) Certification that the stormwater outfalls have been evaluated for the presence of
non-stormwater discharges. The certification statement will be signed in
accordance with the requirements found in Part II, Standard Conditions, Section
B.9,
Page 4

Permit No. NCS000223
b. Stormwater Management Plan. The stormwater management plan shall contain a narrative
description of the materials management practices employed which control or minimize the
exposure of significant materials to stormwater, including structural and nonstructural
measures. The stormwater management plan, at a minimum, shall incorporate the
following-
(1) A study addressing the technical and economic feasibility of changing the methods
of operations and/or storage practices to eliminate or reduce exposure of materials
and processes to stormwater. Wherever practicable the permittee shall cover all
storage areas, material handling operations, manufacturing or fueling operations to
prevent materials exposure to stormwater. In areas where elimination of exposure
is not practicable, the stormwater management plan shall document the feasibility of
diverting the stormwater runoff away from areas of potential contamination.
(2) A schedule to provide secondary containment for bulk storage of liquid materials,
storage of Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) water priority chemicals, or storage of hazardous
materials to prevent leaks and spills from contaminating stormwater runoff. If the
secondary containment devices are connected directly to stormwater conveyance
systems, the connection shall be controlled by manually activated valves or other
similar devices [which shall be secured with a locking mechanism] and any
stormwater that accumulates in the containment area shall be at a minimum visually
observed for color, foam, and visible sheens, prior to release of the accumulated
stormwater. Accumulated stormwater shall be released if found to be
uncontaminated. Records documenting the individual making the observation, the
description of the accumulated stormwater and the date and time of the release shall
be kept for a period of five years.
m
(3) A narrative description shall be provided of Best Management Practices (BMf� to
be considered such as, but not limited to, oil and grease separation, debris co wol,
vegetative filter strips, infiltration and stormwater detention or retention, whe&6
necessary. The need for structural BMPs shall be based on the assessment oV
potential of sources to contribute significant quantities of pollutants to stormwater
discharges and data collected through monitoring of stormwater discharges.
(4) Inspection schedules of stormwater conveyances and controls and measures to be
taken to limit or prevent erosion associated with the stormwater systems.
c. Spill Prevention and Response Plan. The Spill Prevention and Response Plan shall
incorporate a risk assessment of potential pollutant sources based on a materials inventory
of the facility. Facility personnel (or team) responsible for implementing the plan shall be
identified in the plan. A responsible person shall be on -site at all times during facility
operations that have the potential to contaminate stormwater runoff through spills or
exposure of materials associated with the facility operations.
d. Preventative Maintenance and Good Housekeeping Program. A preventative maintenance
program shall be developed. The program shall document schedules of inspections and
maintenance activities of stormwater control systems, plant equipment and systems.
Inspection of material handling areas and regular cleaning schedules of these areas shall be
incorporated into the program.
e. Employee Training. Training schedules shall be developed and training provided at a
minimum on an annual basis on proper spill response and cleanup procedures and
preventative maintenance activities for all personnel involved in any of the facility's
Page 5

Permit No. NCS00{1223
operations that have the potential to contaminate stormwater runoff. Facility personnel (or
team) responsible for implementing the training shall be identified in the Plan.
f. Responsible Party. The Stormwater Pollution Prevention Plan shall identify a specific
position(s) responsible for the overall coordination, development, implementation, and
revision to the Plan. Responsibilities for all components of the Plan shall be documented
and position(s) assignments provided.
g. Plan Ammendment. The permittee shall amend the Plan whenever there is a change in
design, construction, operation, or maintenance which has a significant effect on the
potential for the discharge of pollutants to surface waters. The Stormwater Pollution
Prevention Plan shall be reviewed and updated on an annual basis.
The Director may notify the permittee when the Plan does not meet one or more of the
minimum requirements of the permit. Within 30 days of such notice, the permittee shall
submit a time schedule to the Director for modifying the Plan to meet minimum
requirements. The permittee shall provide certification in writing (in accordance with Part
II, Standard Conditions, Section B, #9) to the Director that the changes have been made.
h. Facility Inspections. Inspections of the facility and all stormwater systems shall occur at a
minimum on a semiannual schedule, once in the fall (September -November) and once
during the spring (April - June). The inspection and any subsequent maintenance activities
performed shall be documented, recording date and time of inspection, individual(s)
making the inspection and a narrative description of the facility's stormwater control
systems, plant equipment and systems. Records of these inspections shall be incorporated
into the Stormwater Pollution Prevention Plan. n
v .
Visual monitoring as required in LA.2.g.(3) shall be performed in addition to facilit}1gmc
inspections. cF 0
i. Implementation. Implementation of the plan shall include documentation of all monito g,
measurements, inspections and maintenance activities and training provided to emploes,23
-
including the log of the sampling data and of activities taken to implement BMPs associated r
with the industrial activities, including vehicle maintenance activities. Such documentation £�
shall be kept on -site for a period of five years and made available to the Director or his
authorized representative immediately upon request.
Page 6

Minimum monitoring and reporting requirements are as follows unless otherwise approved in
writing by the Director of the Division of Environmental Management.
If a facility has multiple discharge locations with substantially identical stormwater
discharges that are required to be sampled, the permitt.ee may petition the Director for
representative outfall status. If it is established that the stormwater discharges are
substantially identical and the permittee is granted representative outfall status, then
sampling requirements may be performed at a reduced number of outfalls.
b . Visual monitoring for color, odor, solids, foam, outfall staining, visible sheens and dry
weather flow shall be performed at all stormwater discharge outfall locations. All visual
monitoring shall be documented and records maintained with the Stormwater Pollution
Prevention Plan. The initial visual monitoring event shall be performed simultaneously
with the first analytical monitoring event and documentation of only this initial visual
monitoring event shall be submitted along with the required analytical monitoring submittal.
C. For purposes of the stormwater sampling required in this permit, all samples shall be
collected from a discharge resulting from a representative storm event (See Part II,
Standard Conditions, Section A). Failure to monitor storm events in accordance with the
specified frequency shall constitute a violation of this permit. If the stormwater runoff is
controlled by a detention pond, the following sampling requirements shall apply:
(1) If the detention pond detains the runoff generated by one inch of rainfall for 24
hours, visual observations for color, foam, outfall staining, visible sheens, and dryQ
weather flow are required, but analytical sampling shall not be required. rn
(2) If the detention pond discharges only in response to a storm event exceeding at?5-
year, 24-hour storm (See Part II, Standard Conditions, Section A), the pond scull
be considered a non -discharging stormwater control system and not subject tom r
NPDES requirements, unless the discharge causes a violation of water qualityx' F_
standards. P;
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d. Samples analyzed in accordance with the terms of this permit shall be submitted no Iater
than January 31 for the previous year in which sampling was required to be performed.
e. Analytical results from sampling during the final year of the permit term shall be submitted
with the permit renewal application.
This permit regulates stormwater discharges. Non-stormwater discharges which shall be
allowed in the stormwater conveyance system are:
(1) All other discharges that are authorized by a non-stormwater NPDES permit.
(2) Uncontaminated groundwater, foundation drains, air -conditioner condensate
without added chemicals, springs, discharges of uncontaminated potable water,
waterline and fire hydrant flushings, water from footing drains, flows from riparian
habitats and wetlands.
(3) Discharges resulting from fire -fighting.
If the storm event monitored and reported in accordance with this permit coincides with a
non-stormwater discharge, the permittee shall separately monitor and report all parameters
Page 7

g
(1)
If the storm event monitored and reported in accordance with this permit coincides with a
non-stormwater discharge, the permittee shall separately monitor and report all parameters
as required under the non-stormwater discharge permit and provide this information with
the stormwater discharge monitoring report.
Specific Stormwater Monitoring Requirements
The specific stormwater monitoring requirements includes both analytical and visual monitoring of
stormwater samples. Specific monitoring requirements are defined below.
Analytical Monitoring
Operators of new facilities discharging stormwater must provide quantitative data for
the parameters listed below once within two years after commencement of the discharge
from the facility. Based on a review of this data the Division may amend the
monitoring requirements of this permit,
1) The following parameters must be tested for; oil and grease, pH, BOD5, COD,
TSS, total phosphorus, total Kjeldahl nitrogen, and nitrate plus nitrite nitrogen.
2) A pollutant analysis of the effluent must be completed using EPA approved
methods for the following analytic fractions: (a) purgeables (i.e., volatile
organic compounds); (b) acid extractables; (c) base/ neutral extractables;
(d) organochlorine pesticides and PCBs; (e) herbicides; (f) metals and other
organics, and (g) the pollutants in Table V of the attached list. The attached
Annual Pollutant Analysis Monitoring (APAM) Requirement Reporting Form A v
describes the sampling and analysis requirements and lists chemicals to be co o0
included in the pollutant analysis. except for those listed in Table V. cam-, 0
1 ty
3) The type of sample to be taken is defined in Part II, Standard Conditions, `4 M
Section A. t
4) Samples are to be taken at each stormwater discharge outfall unless N
representative outfall status has been granted.
5) For each sampled representative storm event the total precipitation, storm
duration, and total flow must be monitored. Total flow shall be either;
(a) measured continuously, (b) calculated based on the amount of area draining
to the outfall, or.(c) estimated by the measurement of flow at 20 minute intervals
during the rainfall event.
Page 8

(2) ' Visual Monitoring
Visual monitoring requires a qualitative visual inspection of each stormwater outfall. regardless
of representative outfall status, for the purpose of evaluating the effectiveness of the
Stormwater Pollution Prevention Plan (SPPP) and assessing new sources of stormwater
pollution. No analytical tests are required. Visual monitoring of stormwater outfalls does not
need to be performed during a representative storm event.
Stormwater Discharge
Characteristics
r n l
Monitoring
2
Monitoring
Location3
Color
Semi -Annual
Visual
SDO
Odor
Semi -Annual
Visual
SDO
Clan
Semi -Annual
Visual
SDO
Floating Solids
Semi -Annual
Visual
SDO
Suspended Solids
Semi -Annual
Visual
SDO
Foam
Semi -Annual
Visual
SDO
Oil Sheen
Semi -Annual
Visual
SDO
Other obvious indicators
of stormwater pollution
Semi -Annual
Visual
SDO
Footnotes:
l Frequency: The first visual monitoring event during the term of the permit must be
peifornted during the hiitial analytical monitoring event. All subsequent visual
monitoring will be performed twice per year, once in the spring and once in the fall.
2 Monitoring Type: Visual monitoring requires a qualitative visual observation of +each
stormwater outfall. No analytical testing or sampling is required. v
r*�
3 Sample Location: Stormwater Discharge Outfall (SDO)
Page 9

Individual Stormwater Page Al
PART li
STANDARD CONDITIONS FOR NPDES STORNIWATER PERMITS
The Federal Water Pollution Control Act, also known as the Clean Water Act, as
amended, 33 USC 1251, et. seq.
Schedules of activities, prohibitions of practices; maintenance procedures, and
other management practices to prevent or reduce the pollution of waters of the
United States. BMPs also include treatment requirements, operation procedures,
and practices to control plant site runoff, spillage or leaks, sludge or waste
disposal, or drainage from raw material storage.
Means shall be calculated according to the following definitions:
a. Arithmetic Mean: The arithmetic mean of any set of values is the summation
of the individual values divided by the number of individual values.
b . Geometric Mean: The geometric mean of any set of values is the Nth root
of the product of the individual values where N is equal to the number of
individual values. The geometric mean is equivalent to the antilog of the
v
a-ridmebc mean of the logarithms of the individual values. For purposes oq
2Z
calculating the geometric mean, values of zero (0) shall be considered to berg
n
one (1). ,r
m
C. Weighted b y Flow Value: Weighted b flow value means the summation o .
g } g Y i�
each concentration times its respective flow divided by the summation of the
flows.
respective
4. Bulk Stora, of f Liquid Products
Liquid raw materials, manufactured products, waste materials or by-products with a
single above ground storage contasner having a capacity of greater than 660 gallons
or with multiple above -ground storage containers having a total storage capacity of
greater than 1,320 gallons.
5. Calendar Day
The period from midnight of one day until midnight of the next day. However, for
purposes of this perrait, any consecutive 24-hour period that reasonably represents
the calendar day may be used for sampling.
The rainfall runoff from or through any coal storage pile.

Individual Stormwater Page A3
container, roLi=ng stock, or concentrated animal feeding operation from which
pollutants are or may be discharged to waters of the state.
A storm event that is between 0.2 and 0.8 inches of rainfall and which bas a
duration of greater than 3 hours and that is preceded by at least 72 hours in which
no storm event measuring greater than 0.1 inches has occurred.
rr
The fraction of total rainfall that is not infiltrated into or otherwise retained by the
soil, concrete, asphalt or other surface upon which it falls that will appear at the
conveyance as runoff.
r• �r rrr'r
Spill containment for the contents of the single largest tank within the containment
structure plus sufficient freeboard to allow for the 25-year, 24-hour storm event-
aMOMWITTOOM.
A chemical or chemical category which:
a. Is listed in 40 CFR 372.65 pursuant to Section 313 of Title III of the
Superfund Amendments and Reauthorization Act (SARA) of 1986, also
titled the Emergency Planning and Community Right -to -Know Act of 1986;
b . Is present at or above threshold levels at a facility subject to SARA title III, n
Section 313 reporting requirements; and o
c-
c. That meet at least one of the following criteria: � �'
0
(1) Is listed in appendix D of 40 CFR art 122 on either Table II ` M .
PPe P �
(organic priority pollutants), Table III (certain metals, cyanides, and M
phenols) or Table IV (certain toxic pollutants and hazardous
substances);
(2) Is listed as a hazardous substance pursuant to section 311(b)(2)(A)
of the CR'A at 40 CFR 116.4; or
(3) Is a pollutant for which EPA has published acute or chronic water
quality criteria.
Kilm-71WOM, -r.
Includes, but is not limited to: raw materials; fuels; materials such as solvents,
detergents, and plastic pellets; finished materials such as'metalhc products; raw
materials used in food processing or production; hazardous substances designated
under section 101(14) of CERCLA; any chemical the facility is required to report
pursuant to section 313 of Tine III of SAR.A; fertilizers; pesticides; and waste
products such as ashes, slag and sludge that have the potential to be released with
storm,A-ater discharges.

Individual Storrnwater Page A5
g-. Steam electric power generating facilities, including coal handling sites;
h . Transportation facilities classified as Standard Industrial Classifications 40,
41, 42, 44, and 45 which have vehicle maintenance shops, equipment
cleaning operations, or airport deicing operations. Only those portions of
the facility that are either involved in vehicle maintenance (including vehicle
rehabilitation, mechanical repairs, painting, fueling and lubrication),
equipment cleaning operations, airport deicing operations, or which are
otherwise identified under (a)-(g) or (i)-(k) of this definition are associated
with industrial activity;
Treatment works treating domestic sewage or any other sewage sludge or
wastewater treatment device or system, used in the storage treatment,
recycling, and reclamation of municipal or domestic sewage, including
lands dedicated to the disposal of sewage sludge that are located within the
confines of the facility, with a design flow of 1.0 mgd or more, or required
to have an approved pretreatment program under 40 CFR part 403. Not
included are farm lands, domestic gardens or lands used for sludge
management where sludge is beneficially reused and which are not
physically located in the confines of the facility, or areas that are in
compliance with section 405 of the CWA;
Construction activity including clearing, grading and excavation activities
except: operations that result in the disturbance of less that five acres of total
land area which are not part of a larger common plan of development or
sale;
k. Facilities under Standard Industrial Classifications 20, 21, 22, 23, 2434,'
25, 265, 267, 27, 283, 285, 30, 31 (except 311), 323, 34 (except 3441),'r=n
35, 36, 37 (except 373), 38, 39, 4221-25, (and which are not otherwise _'
included within (a)-O) of this definition). ..,
For the categories of industries identified in (a) through 0) of this definition the 10,
term includes, but is not limited to, stornwater discharges from industrial plant
yards: immediate access roads and rail lines used or traveled by carriers of raw
materials, manufactured products, waste material, or by-products used or created
by the facility; material handling sites; refuse sites; sites used for the application or
disposal of process wastewaters; sites used for the storage and maintenance of
material handling equipment; sites used for residual treatment, storage, or disposal;
shipping and receiving areas; manufacturing buildings; storage areas (including tank
farms) for raw materials, and intermediate and finished products; and areas where
industrial activity has taken place in the past and significant materials remain and are
exposed to stormwater. For the categories of industries identified in (k), the term
includes only stormwater discharges from all areas listed in the previous sentence
(except access roads) where material handling equipment or activities, raw material,
intermediate products, final products, waste material, by-products, or industrial
machinery are exposed to stormwater.
Material handling activities include the: storage, loading and unloading,
transportation, or conveyance of any raw material, intermediate product, finished
product, by-product or waste product. The term excludes areas located on plant
lands separated from the plant's industrial activities, such as office buildings and
accompanying parking lots as long as the drainage from the excluded areas is not
mixed with stormwater drained from the above described areas.

Individual Stormwater Page A7
30. u
Any non -containerized accumulation of solid, non -flowing waste that is used for
treatment or storage.
_-•M061414WIP
The maximum 24-hour precipitadon event expected to be equaled or exceeded, on
the average, once in 25 years.
A

Individual Stormwater Page A9
Nothing in this permit shall be construed to preclude the institution of any legal
action or relieve the permittee from any responsibilities, liabilities, or penalties to
which the permittee is or may be subject to under NCGS 143-215.75 et seq. or
Section 311 of the Federal Act, 33 USC 1321. Furthermore, the permittee is
responsible for consequential damages, such as fish kills, even though the
responsibility for effective compliance may be temporarily suspended.
The issuance of this permit does not convey any property rights in either real or
personal property, or any exclusive privileges, not does it authorize any injury to
private property or any invasion of personal rights, nor any infringement of
Federal, State or local laws or regulations.
6,Several,iljz-
The provisions of this permit are severable, and if any provision of this permit, or
the application of any provision of this permit to any circumstances, is held invalid,
the application of such provision to other circumstances, and the remainder of this
permit, shall not be affected thereby.
The permirtee shall furnish to the Director, within a reasonable time, any
information which the Director may request to determine whether cause exists for
modifying, revoking and reissuing, or terminating this permit or to determine o
compliance with this permit The permittee shall also furnish to the Director upM
request, copies of records required to be kept by this permit. c) 0
4 rn
8. F.-,.^:r2:IOr1 Of Pe?iFili
to.
The permittee is not authorized to discharge after the expiration date. In order to
receive automatic authorization to discharge beyond the expiration date, the
permittee shall submit such information, forms, and fees as are required by the
agency authorized to issue permits no later than 180 days prior to the expiration
date. Any permittee that has not requested renewal at least 180 days prior to
expiration, or any permittee that does not have a permit after the expiration and has
not requested renewal at Ieast 180 days prior to expiration, will be subjected to
enforcement procedures as provided in NCGS § 143-2153.6 and 33 USC 1251 et.
seq.
All applications, reports, or information submitted to the Director shall be signed
and certified.
a. All applications shall be signed as follows:
(I) For a corporation: by a responsible corporate officer. For the purpose of
this Section, a responsible corporate officer means: (a) a president,
secretary, treasurer or vice president of the corporation in charge of a

Individual Stormwater Page A11
This permit may be modified, revoked and reissued, or terminated for cause. The
notification of planned changes or anticipated noncompliance does not stay any
permit condition.
y�• r• : • �r r � • •• ��r • r:r
Titre permittee shall at all times properly operate and maintain all facilities and
systems of treatment and control (and related appurtenances) which are installed or
used by the permittee to achieve compliance with the conditions of this permit.
Proper operation and maintenance also includes adequate laboratory controls and
appropriate quality assurance procedures. This provision requires the operation of
back-up or auxiliary facilities or similar systems which are installed by a perrittee
only when the operation is necessary to achieve compliance with the conditions of
the permit.
.Need to Halt or Reduce not a DCfense
It shall not be a defense for a permittee in an enforcement action that it would have
been necessary to halt or reduce the permitted activity in order to maintain
compliance with the condition of this permit-
v,
Definitions
"Bypass"
(1) means the known diversion of stormwater from any portion of a
stormwater control facility including the collection system, which is notF
designed or established or operating mode for the facility. e1
(2) "Severe property damage" means substarttia] physical damage to proper ,
damage to the control facilities which causes them to become inoperable
substantial and permanent loss of natural resources which can reasonably be
expected to occur in the absence of a bypass. Severe property damage does
not mean economic loss caused by delays in production.
b. Bypass Not Exceeding Limitations.
The perminee may allow any bypass to occur which does not cause limitations to be
exceeded, but only if it also is for essentialmaintenance to assure efficient
operation. These bypasses are not subject to the provisions of Paragraphs c. and d.
of this section.
C. Notice
(I} Anticipated b}lpass. If the perminee ]mows in advance of the need for a
bypass, it shall submit prior notice, if possible at least ten days before the
date of the bypass; including an evaluation of the anticipated quality and
affect of the bypass.

Individual Stormwater Page A13
(2) The permitted facility was at the time being properly operated; and
(3) The perminee submitted notice of the upset as required in Part II, E. 5. (b)
(B) of this permit.
(4) The permiam complied with any remedial measures required under Part II,
A. 2. of this permit.
d. Burden of Proof
In any enforcement proceeding the permittee seeking to establish the occurrence of
an upset has the burden of proof.
y� � • • •; s ; •;s
I' - 1O M
Samples collected and measurements taken, as required herein, shall be
characteristic of the volume and nature of the permitted discharge. Samples shall be
taken on a day and time that is characteristic of the discharge. All samples shall be
taken before the discharge joins or is diluted by any other waste stream, body of
water, or substance. Monitoring points shall not be changed without notification to
and approval of the Director.
Duplicate signed copies of all reports required herein, shall be submitted to the
following address:
Division of Environmental Management rr" -0°t
Water Quality Section _J m
ATTENTION: Central Files 4
Post Office Box 29535
Raleigh, Noah Carolina 27626-0535
3. 'Floe MeaturCmen_t_s
Where required, appropriate flow measurement devices and methods consistent
with accepted scientific practices shall be selected and used to ensure the accuracy
and reliability of measurements of the volume of monitored discharges.
Test procedures for the analysis of pollutants shall conform to the EMC regulations
published pursuant to NCGS 143-215.63 et~ seq, the Water and Air Quality
Reporting Acts, and to regulations published pursuant to Section 304(g), 33 USC
13I4, of the Federal Water Pollution Control Act, as Amended, and Regulation 40
CFR 136.
To meet the intent of the monitoring required by this permit, all test procedures
must produce minimum detection and reporting levels that are below the permit
discharge requirements and all data generated must be reported down to the
minimum detection or lower reporting level of the procedure. If no approved

Individual Stormwater Page Al
a. Enter upon the permittee's premises where a regulated facility or activity is
located or conducted, or where records must be kept under the conditions of
this permit;
b . Have access to and copy, at reasonable times, any records that must be kept
under the conditions of this permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring
and control equipment), practices, or operations regulated or required under
this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit
compliance or as otherwise authorized by the Clean Water Act, any
substances or parameters at any location.
The permittee shall give notice to the Director as soon as possible of any planned
physical alterations or additions to the permitted facility. Notice is required only
when:
a. The alteration or addition to a permitted facility may meet one of the criteria
for determining whether a facility is a new source in 40 CFR Part 122.24
(b), or
b . The alteration or addition could significantly change the nature or increase
the quantity of pollutants discharged. This notification applies to pollutants
which are subject neither to effluent limitations in the permit, nor to A
notification requirements under 40 CFR Part 122.42 (a) (1). n
v
2. Ant cif d SQncomp]iano r�
CIO
The permittee shall give advance notice to the Director of any planned changes•ia m
the permitted facility or activity which may result in noncompliance with the pWit
requirements.
3. Tran 5 aa
4
This permit is not transferable to any person except after notice to and approval by
the Director. The Director may require modification or revocation and reissuance of
the permit to change the name and incorporate such other requirements as maybe
necessary under the Clean Water Act.
Monitoring results shall be reported at the intervals specified elsewhere in this
permit.
The permittee shall report to the central office or the appropriate regional office any
noncompliance which may endanger health or the environment Any information
shall be provided oral]}, within 24 hours from the time the permittee became aware

Individual Stormwater Page A17
PART III
LIMITATIONS REOPENER
This permit shall be modified or alternatively, revoked and reissued, to comply with any
applicable effluent guideline or water quality standard issued or approved under Sections
302(b) (2) (c), and (d), 304(b) (2) and 307(a) of the Clean Water Act, if the effluent
guideline or water quality standard so issued or approved:
a. contains different conditions or is otherwise more stringent than any effluent
limitation in the permit; or
b. controls any pollutant not limited in the perniL
The permit as modified or reissued under this paragraph shall also contain any other
requirements in the Act then applicable.
ADMINISTERING
PART IV
AND COMPLIANCE
REQUIREMENTS
MONITORING FEE
The perminee must pay the administering and compliance monitoring fee within 30 (thinny)
days after being billed by the Division, Failure to pay the fee in timely manner in
accordance with 15ANCAC 2H .0105(b)(4) may cause this Division to initiate action to
revoke the permit

TABLE n--moAmc T ac POLLUTAwm
IN EACH OF FOUR PRAMONS 1?i
ANALYSJB BY GAS CHROMATOORAPHY/
NA B6 SpscrsosWPY (GS/MS)
volatile+
1V
scroleia
IYV
acrylonitrlls
3V
benzene
6V
bromoforrn
{V
carbon tetrachloride
TV
chlorobensene
OV
chlorodlbrwr*ornetbaoe
BV
chloroethane
1OV
7-chloroethylvinyl ether
11V
chloroform
12V
dichlombromomethane
14V
1,1-dlchlorvethaae
J6V
1,2-dicbJoroethane
1sV
1,I�lchlorrothylene
17v
1,Z-dich)nit,propi►ne
JDV
1,8-dichlorotropYlene
19V
ethylbenseae
IOV
methyl bromide
21V
methyl chloride
22V
methylene chloride
29V
1,13,24stracb1oroethane
24V
tatrach)oroethylene
25V
toluene
26V
1,2-trans-dlchloroethy lone
37V
1,1,1-trichloroethane
20V
1.1,2-trlchloroetbans
29V
trichlorooLbYlsae
$IV
vinyl chloride
Acid Comppoundr
IA
3-chlorophenol
2A
2,4-dichlorophenol
3A
2,4-dlmethylphenol
4A
4,6-dlniu0-o-cre60l
6A
2,4-dlnitrophenol
N
2-nitrophenol
7A
4-o•f unphenol
ILA
p-chloro-m-cresol
4A
pentach)oropbscOl
IOA
phenol
11A
2,4.6.trichlorophenol
&asr/Ntutral
IS acenaphtbene
2B acenapbchylens
3B anthracens
4B benxidine
6B benaolaknthrscene
OB beaso(a)pyrene
7B m,4-bensonuorant:hene
6B beaso(Qhi)peryleae
9B benzo(k)nuoranthene
JOB ble(2-Cbloroetboxy)methaae
11B ble(2-chloroethyDetber
12B bls(2-cblorolsopropy0other
13B bis (2-ethylhexyl)phthalat*
14B 4-bromophenyl phenyl ether
I&B butylbenxy] phthalate
16B 2-ch3oro1Laphtbalene
17B 4-chlorophenyl phenyl ether
JOB ohrysene
JOB dlbenzo(chAxtbracene
30B 1,2-dlchlorobenxens
21B 1,9-dlchlorobenxene
22B 1,4-dlchlorobenzene
23B 3,T-dichlorobenxldlne
24B diethyl pbthalsto
25B dimethy) phthalate
26B di-n-butyl phthalate
27B 2,4-41nitrotoluene
28B 2.6-d1nitrotoluene
29B dl-o-octy) pbtbaiate
30B 1,2-d1pheny1hydraslne (as eaobe•nssne)
318 flurorsrithOns
32B nuorene
mB hexr.chlorobenzene
34B bexachlorobutadJene
35B hexachlorocyclopentadlene
3H3 hexachloroethane
37B ladeno(1,2,3-OdWrons
38B
leopborone
36B
nnpthalene
40
nitrobensens
41B
N-nl:rosodimethylamine
42B
N nitrosodl-n-propylamine
4M
N-nitroeodiphenylamine
44B
pb enanthre ne
45B
pyrene
*6
1.2.4-trlchlorobemene
1P
P=Wsdes
aldrin
2P
alpha-BHC
3P
beta-BHC
4P
gamrna-BHC
AP
delta-BHC
6P
chlordane
7P
4.4'-DDT
6P
4,4'-DDE
!P
4,4'-DDD
lOP
dieldrin
11P
alpha-endceulfan
12P
beta-endoaulfaa
13P
endoeulfan sulfate
14P
endr•In
16P
endrla aldehyde
16P
heptachlor
17P
heptachlor epoxide
OP
PCB-1242
JOP
PCB-1264
20P
PCB-1221
21P
PCB -I=
22P
PCB-1248
23P
PCB-1280
34P
PCB-1010
UP
toxaphona
TABLE III--OTWM TOXIC POLLUTAM
(METAL$ AND CYANIDE) AND TOTAL
PwWoLB
Antimony. Total
Arsenic, Total
Beryllium. Total
Cadmium, Total
ChromlLim. Total
Copper, Total
Lead, Total
Mercury, Total
Nickel, Total
Selenium. Total
Silver, Total
Thallium, Total
Zinc. Total
Cyanide, Total
Phenols, Total
TABLE N—CONVEMnONAL AND
NONOONVENTIONAL POLLUTANTS Rs-
QUIRED TO' BE 71E9TED BY PjarrD4
D1SCX4RGERB IF EXPJiOnm TO w
PR82 Kn
Hromlde
Chlorine, Total Realdual
Color
Petal Coliform
Fluoride
N1 trzte-Ni trl to
Nitrogen, Total Orgazdc
Oil and Grease
Phosphorus, Total
RadloacUvJty
Sulfate
Sulfide
8ulnte
Surfactants
Aluminum, Total
Barium. Total
Boron, Total
Cobalt, Total
Iron, Total
JKLeneslum, Total
Molybdenum, Total
Manganese, Total
Tin, Total
Tltaalum, Total
• A • s via —W Jan.&
ARDOUR HUBI3TANcss �RVE•�Quum To
BE IDL TIFi11;D BY FAA&'O DI8-
CHARas" 17 RxP8cr&D To Bs
PRESENT
Asbestos
Toxic Poilulaats
Hamrdow s bstasors
Aostaldehyds
Ally] alcohol
Allyl chloride
Amyl acetate
Aniline
Bensonitrile
Benxyl chloride
Butyl acetate
Butylamine
Caplan
Carbaryl
Carbofuran
Carbon 4iaulride
Chlorpyrlfos
Coumapt"
Cresol
Crotonaldshyde
CYclobexane
2,4-D(2,4•Dlcbloropheooxy acetic acid)
Diasinon
Dlcam bs
Dichlobenll
Dichlons
2.2-Dlchloroproplonlc acid
Dlcblorvos
Dlethyl amine
Dimet.hyl amine
Dlotrobemans
Dlquat
Disulfoton
Diuron
Spl chlwcohydrin
Ctblon
Ethylene diamine
Ethylene dibroml4s
Formaldehyde
Purfural
Outhlon
Isoprene
Isopropenolam)ae Dodecylbonsenesuitonsts
Keltbane
Kepone
hwathion
Mercaptodlmethur C?
Methoxychlor {7
Methyl mercaptan f=
Methyl metbacry)ate-9 .�
Methyl parathion C-1 n
Mevinpbos an
Mexacarbate
Monoethyl LM1130
Monomethyl amine LD
Naled x'
Napthenlc acid
Nltrotoluene
Parathion GO
Phenolsulls,"te
Phowene
Propargite
Propylene oxide
Pyrethrlpe
qul Holies
Resorcinol
atrontl um
Strychnine
Styrene
2.4.5•T (2,4,6 'Hchlorophenoxy acetic acid)
TDE (Tetrachlorofthenylethane)
2,4,5-TP (2-0.4,5-Trichlomphenoxy) pro-
panolc acid]
Trlchlorofan
Trlethanolamine dodecylbensenesulfonate
Trietbylamine
Trimetbyla Une
Uranium
Vanadium
V113y1 acetate
Xylene
Xylenol
Zirconium

II. Samplin
for main sample I grab sample
Date Sampled: (composite sample)
Sampling begun (date, time):
Sampling finished (date, time):
Date and time sampled (grab sample):
t. Facility information:
Annual Pollutant Analysis Monitoring Requirement
Reporting Form A
j (Revised June 1990)
NPDES Permit No: Discharge (Pipe) No:
Facility Name: Class:
Persons) Collecting Samples:
Status of facility wastewater treatment operation on
If no, explain briefly:
Analytical Laboratory:
for purgeable
County:
day of sampling: typical:
fraction
Page 1 of 9
Year:
Yes No
Corresponding sample taken for toxicity testing:
Yes
No
Instructions
The purpose of this document and the accompanying memo is to standardize the sampling, analysis and reporting procedures to be used
for the Annual Pollutant Analysis Monitoring (APAM) Requirement as described in the permit.
Sampling rC,PPF�r nI T� �.Or 3'fe: ►. �veh
1 - Take a sample from the final effluent during Collect a grab sample for the volatlle
organic fraction when collection of the 21--- —posrte sample is completed. Fdflow any other sampling instructions provided by the laboratory
performing the analysis. r^ tt
2 Indicate in the space provided at the top of this page whether a corresponding sample for toxicity testing was taken,
3 Make note of any unusual wastewater treatment operating conditions occurring on the day of sampling in the space provided on I form.
Analysis 0
4 . Analyze the effluent for pollutants listed on the APAM form, Including those to be identified and approximately quantif and the 10
significant peaks rule, using appropriate EPA -approved methods for each of the analytic fractions. Other analytical methods ca a sub lituted
only with prior, written approval of the Director of the Division of Environmental Management (DEM). Read and distribute totthe fa ratory
performing the analysis the accompanying memo (Tedder, October 1990) clarifying analytical requirements. J 71
5 - Identify chemicals to be analyzed for according to the 10 significant peaks rule (as described in Item 2 of the Annual Pqd9tant galysis.
Monitoring Requirement in the permit) using a GCIMS library search, Tentative identification is all that is required; confirmau n by standard
infection is not necessary. Estimate the concentration of each based on an internal standard having the closest retention time.
rn
Reporting
6 . Quantization Limit Targets that should be met are listed on this Revised APAM Reporting Form A, Report the use of any higher quantita-
tion limit and an explanation as to why the listed quantitation limit target could not be met. Examples of acceptable reasons for not meeting
a quantitation limit target could be high background concentrations in a sample, orthe necessity for sample fraction dilution to bring a chemical
to within a quantifiable concentration. List any quantitation limit differtent (whether higher or lower) from the target In the column provided
for this purpose.
7 - If a chemical is found to be below the quantitation limit, report the concentration detected as less than (or 'C') the quantitation limit
in the appropriate space. Provide a concentration estimate for chemicals detected in concentrations greater than the detection limit and less
than the quantitation limit. Enter the detection limit In parentheses beside the estimate. Chemicals detected in concentrations above the quan-
titation limits must be quantified. Quantization limit and detection limit are defined in the accompanying memo (Tedder, October 1990). Enter
the total number of peaks detected in each analytic fraction in the appropriate space on this Revised APAM Form A. Report all concentrations
in units of micrograms per liter (uglt) and metals as total recoverable metal. If'no peaks to be identified under the 10 significant peaks rule
are observed, enter "none" in the space provided for "other" compounds in each appropriate analytic fraction section. Provide the concentra-
tion estimate and retention time for "unknowns" as well as for "significant peaks" for which a structural assignment can be made.
8 • It "significant peaks" are found, provide probable molecular weight, library match probability, retention time,.identification basis, and
MS scan number for each. In addition, list internal standards and their retention times.
9 In the section labeled "Organic Analytical Information" (p. 9), include forleach organic fraction the method, extraction technique, GC
operating conditions, and surrogate recovery. Report the size of the GCIMS library being utilized in the appropriate space.
10 - Use copies of this Annual Pollutant Analysis Monitoring Revised Form A to report the results of the analysis. Both the analytical laboratory
representative and the facility operator in responsible charge should sign completed forms (last page).
11 • Mail two completed copies of the form (and the laboratory report; if submitted to the facility on a different form) to: ATTN: Central Files,
Division of Environmental Management, NC DEHNR, P.O. Box 27687, Raleigh, NC 27611. Mail the APAM form separately from Discharge Monitoring
Reports.

A. Purgeable (Volatile Organic) Fraction, EPA Method. Page 2 of 9
Number of chemicals detected in Fraction
Fraction STORET Number 84085
STORET Compound
Number
Ouantitation
Limit Target
0uantitation
I Limit'
Concentration
Delecled
GCIMS
Confirmation?
1. Pollutants to be analyzed for:
(ugll)
WWI)
(ug11)
Yes
No
34210
Acrolein
100
34215
Acrylonitrile
100
1
34030
Benzene
5
1
32101
Bromodichloromethane
5
1
32104
Bromoform
5
I
34413
Bromomethane
10
1
32102
Carbon tetrachloride
5
1
34301
Chlorobenzene
6
1
34311
Chloroethane
10
1
34576
2-Chloroethyl vinyl ether
10
1
32106
Chloroform
5
1
34418
Chloromethane
10
32105
Dibromochloromethane
5
1
34496
1,1-Dichloroethane
5
1
34531
1,2-Dichloroethane
5
1
34501
1,1-Dichloroethylene
5
1
34546
trans-1,2-Dichloroethylene
5
1
34541
1,2-Dichloropropane
6
1
34704
cis 1,3-Dichloropropene
5
{
34699
trans 1,3-Dichloropropene
5
1
34371
Ethylbenzene
8
1
34423
Methylene chloride
5
1
34516
1,1,2,2-Tetrachloroethane
7
1
M
34475
Tetrachioroethylene
5
1
34010
Toluene
6
-j
34506
1,1,1-Trichloroethane
5
1
up
34511
1;1,2-Trichloroethane
5
1
39180
Trichloroethylene
5
1
34488
Trichlorofluromethane
10
1
39175
Vinyl chloride
10
If different from quantitation limit target

Compound
Probable
Molecular
Weight
Estimated
Concentration
(ug11)
Library Match
Probability
(°!o)
Retention
Time (RT)
(Min)
Identification Basis
(Check all that apply)
Scan
Number
Library
Match
Manual
Interpretation
RT
Complete only It non -targeted compounds are present:
Retention
Internal Standard Time
(Min)
330
S3�I r z
N
O
w
v
e
to
m
m
v
M
W
C
O
1
Cr
a
CD
c9
N
CD
m
w
7r
41
CD

B. Acid Extractable Fraction, EPA Method
Page 4 of 9
Number of chemicals detected in Fraction
Fraction STORET Number 45582
STORET Compound
Ouantitation
Ouantltation
Concentration
GCIiMS
Number
Limit Target
I Limit-
Detected
Confirmation?
1. Pollutants to be analyzed for:
(ug11)
(ug11)
(ug11)
Yes
No
34452
4-Chloro-3-meth k henol
10
4
34586
2-Chloro henol
10
}
34601
2 4-Dichloro henoi
10
34606
2 4-Dimeth I henol
10
I
34616
2 4-Dinitro henol
50
4
34657
2-Meth I.4 6-dinitro henoi
50
4
34591
2-Nitrophenol
10
I
34646
4-Nitrophenol
50
}
39032
Pentachloro henoi
50
34694
Phenol
10
I
34621
2 4 6-Trichloro henoi
10
" If different from quantitation limit target
0
M
r7 n
m
r

Compound
Probable
Molecular
Weight
Estimated
Concentration
(uglt)
Library Match
Probability
(°/a)
Retention
Time (RT)
(Min)
Identification Basis
(Check all that apply)
Scan
Number
Library
Match
Manual
Interpretation
RT
Complete only if non -targeted compounds are present:
Retention
Internal Standard Time
(Min)
h6 L- 333
N
m
n
m
x
0 n
w
Cr
co
w
c
v
0
1
O
Z
m
m
N
w
cn
w
m
m
.r•7
to

C. Base/Neutral Fraction, EPA Method Page 6 of 9
Number of chemicals detected In Fraction
Fraction STORET Number 45583
STOAET Compound
Number
Quentitation
Limit Target
Quantitation
L51miv
Concentration
Detected
GClMS
Confirmation?
1. Pollutants to be analyzed for:
(ug11)
(ugli)
(ug11)
Yes
No
3405
Acena hthene
10
1
34200
Acena hth lene
10
1
34220
Anthracene
10
I
39120
Benzidine
50
l
34526
Benzo a anthracene
10
1
34247
Benzo_LaLpyrene
10
1
34230
Benzo b fluoranthene
10
I
34521
Benzo hi) perylene
10
I
34242
Benzo k fluoranthene
10
I
34278
Bis 2-chloroethox methane
10
I
34273
Bis 2-chloroeth I ether
10
I
34283
Bis 2-chloroiso ro i ether
10
l
39100
Bis 2•eth lhex Iphthalate
10
1
34636
4-Bromo hen I phenyl ether
10
I
34292
Butyl benz I phthalate
10
I
34581
2-Chlorona hthalene
10
I
34641
4-Chloro hen I phenyl ether
10
I
34320
Ch sene
10
1
34556
Dibenzo a,h anthracene
10
1
34536
1 2-Dichlorobenzene
10
1
34566
1 3-Dichlorobenzene
10
34571
14•Dichlorobenzene
10
l
v
•�
34631
3 3-Dichlorobenzidine
20
I
C"I
n
34336
Diethyl phthalate
10
l
34341
Dimeth I hthalate
10
I
39110
Di-n-but 1_phthalate
10
1In
34611
2 4-Dinitrotoluene
10
I
34626
2 6-Dinitrotoluene
10
I
34596
Di-n•oct ! phthalate
10
I
34346
1 2-Di hen Ih drazine
10
I
34376
Fluoranthene
10
I
34381
Fluorene
10
1
39700
Hexachlorobenzene
10
I
34391
Hexachlorobutadiene
10
I
34386
Hexachloroc clo entadiene
10
I
34396
Hexachloroethane
10
I
34403
Indeno 1 2 3-cd rene
10
l
34408
lso horone
10
l
34696
Naphthalene
10
I
34447
Nitrobenzene
10
1
34438
N-nitrosod imeth y famine
10
I
34428
N-niIroso-di-n ro pylamine
10
I
34433
N-nitrosodi hen lamina
10
I
34461
Phenanthrene
10
I
34469
P rene
10
I
34551
1,2,4•Trichlorobenzene
10
If different from quantitation target

Compound
Probable
Molecular
Weight
Estimated
Concentration
(ug11)
Library Match
Probability
(%)
Retention
Time (RT)
(Min)
Identification Basis
(Check all that apply)
Scan
Number
Library
Match
Manual
Interpretation
RT
Complete only if non -targeted compounds are present:
Retention
Internal Standard Time
(Min)
EMU IVU430
OSM
W,
0

I
G. Organochlorine/Orgagophosphorus Pesticides and PCB's Page 8 of 9
Number of chemicals detected in Fraction
Fraction STORET Number 00188
STORET Compound
Number
Quantitation
Limit Target
Quantitation
Limit"
Concentration
Detected
Confirmation?
Dual Column GC/MS
1. Pollutants to be analyzed for: (ug11)
Organochlorine Pesticides/PCB's: EPA Method
(U g11)
(ug11)
Yes
No
Yes
No
39330
Aldrin
0.05
I
39337
al ha-BHC
0.05
I
39338
Beta-BHC
0.05
I
34259
Delta-BHC
0.1
39340
Gamma-BHC Lindane
0.05
39350
Chlordane
0.2
39310
4 4'-DDD
0.1
I
39320
4 4'-DDE
0.1
4
39300
4 4'•DDT
0.1
39380
Dieldrin
0.02
34361
Endosulfan I (alpha)
0.1
34356
Endosulfan It beta
0.1
34351
Endosulfan sulfate
0.7
39390
Endrin
0.06
34366
Endrin aldehyde
0.2
39410
Heptachlor
0.05
39420
Heptachlor epoxide
0.8
I
39480
Methox chlor
0.5
39755
Mirex,
0.2
39400
Toxa hene
2.4
I
34671
PCB 1016
0.5
I
39488
PCB 1221
0.5
I
39492
PCB 1232
0.5
39496
PCB 1242
0.5
39500
PCB 1248
0.5
39504
PCB 1254
1.0
39508
PCB 1260
1.0
I
Organophosphorus Pesticides: EPA Method Fn
39560
Demeton
2.5
I
39540
Parathion (ethyl)
0.6
E. Herbicides, EPA Method
Number of chemicals detected In Fraction
Fraction STORET Number 00148
STORET Compound
Number
Quantitation
Limit Target
Quantitation
Limit*
Concentration
Detected
Confirmation?
Dual Column
1. Pollutants to be analyzed for:
(ug11)
I (ug11)
(ug11)
Yes
No
39730
2,4 D
12
39045
Silvex
2
I
39740
2,4,5-T
2
If different from quantitation limit target

Organic Analytical Information: Page 9 of 9
Organic Fraction
Method
Extraction
GC'' Operating Conditions
Column Description
Surrogates (Spikes)
Batch
Continuous
Compound
Recovery
%
Length X ID, Film Thickness,
Column Type, Carrier Gas & Flow
Rate, Temperature Program
Purgeable
Acid Extractable
Base/Neutral Extractable
Example: Acid Extractable
625
X
30m x40.25mm, 0.25um, D13•5,
He, 30 cmisec, 400C (4 min)
4 270°C, 10*1min
d5 • phenol
50
GC1MS Library size (number of reference spectra): 4
F. Metals and Other Chemicals
Number of Metals and Other Chemicals (as listed below) detected in Sample
Fraction STORET Number 78240
STORET Compound
Number
Ouantitation
Limit Target
` Oueniitation
I Limit'
Concentration
Detected
1. Pollutants
to be analyzed for:
(ug/1)
(ug11)
(ug11)
01104
Aluminum
50
I
01097
Antimony
50
I
01002
Arsenic
10
I
01012
Be Ilium
25
01027
Cadmium
2
I
01034
Chromium
5
I
01042
Copper
2
I
r
01051
Lead
10
I
71900
Mercury
0.2
l
01067
Nickel
10
01147
Selenium
5
I
01077
Silver
5
01092
Zinc
10
I
2. Other inor anics: 4
01007
Barium
500
00940
Chloride
1000
I
00720
Cyanide
20
I
00951
Fluoride
100
' if different from quantitation limit target
Analytical laboratory Representative: I
Signed: 4 Date:
Facility Operator in Responsible Charge (ORC): }
f certify that this report is accurate and complete to the best of my knowledge.
Signed: 4 Date: