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NCS000330_MONITORING INFO_20181126
STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. k)C�S(�OC� DOC TYPE ❑ FINAL PERMIT --�4- MONITORING- REPORTS-- - ----- -- REPORTS- 0 APPLICATION APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ ZDl 1� -tit • YYYYM M DD November 15, 2018 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files: ,OATI P.O. Box 5030 2020 Asheraft Avenue Monroe, NC 28111-5030 Phone: (704) 289-451 1 Fax: (704)290-5194 RECEIVEDEmail: Joe.Hinkle@atimetals.com NOV 2 6 2018 CEN-1 NAL FILES 11WR sl:cno' mo Attached, please find stormwater monitoring data for Permit No NCS000330. The originals and one copy are included. The monitoring data is for the following monitoring schedule: Monitoring Period Sample Number Start I End Year 10 — Period 1 19 September 1, 2018 1 February 28, 2019 Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall through prior correspondence. If you have any questions or need additional information, please contact me at 704-289-451 1. Thank you. Sincerely, k' (9 V�� J e Hinkle EHS Manager t 'A Allvac Monroe Plant !k. 1 Ajhrac Stormwater Monitoring Report Form Sample Date: ! D - a 6 - / ? Sample Time: —5 : /d2 rarn _ ^_ Sample Location: ,Sw o a Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analvsis: S ortnwater Pi:Khne NtWl #2 Drainage Area = 272 590s . ft. = 6.25 acres % Impervious = 360/9 40 CFR Eqq 13 Parameter Results (mg/1) Benchmark Values (mg/1) BOD 30 COD 6 120 TSS 38. 6 100 Cadmium ND 0.001 Chromium, total recoverable 0, Ca1 Lead, total recoverable 0.03 Nickel, total recoverable 0.26 Zinc, total recoverable 0,355 0.067 Oil and Grease 30 pH 7,0 (std units) 6-9 (std units) Storm Date: /0 -d 6. 19 Storm Duration: I R , 7.5 (Hrs.) Inches of Rainfall: _ 1__._qD Duration of time preceding rain event exceeding 0.1": 19 a (Hrs.) Estimated Flow Calculation: Q = CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cis) = (A x inches rainA 2 inches/ft. x 6.25 acres x .64) + .9 x inches min/12inches/ft. x 6.25 x .36) Q(Total, cfs) = .1333 x I . q (inches of rain) + .1688 x 1 - 4 D (Inches of rain) = 6 - q,2 3 cfs STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 0C)03,30 SAMPLES COLLECTED DURING CALENDAR YEAR: pC Q / 8 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME AT Z 4pcci/9(feti M!}'�Gat' IS PERSON COLLECTING SAMPLES) �AMG�f % Ai / dA✓� Fif�1/'i dt�E CERTIFIED LABORATORY(S) /f/q[F ,vim } i'"1 Lab # /01 Lab # Part A: Specific Monitoring Requirements COUNTY UN r ON PHONE NO. (71)y) a5 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall Date 50050 No. Sample Collected Total Flow if a Total Rainfall mo/dd/yr MG inches ca o a 10- A6 ` IT o, o Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oii per month? Qyes (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-"EM), if appl. Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG inches m /l m /l unit al/mo Form SWU-247, last revised 611212015 Pagel of 2 STORM EVENT CHARACTERISTICS: Date /0- 2-6-18 Total Event Precipitation (inches): Event Duration (hours): _ 19 , 7.5 (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are ant penalties for submitting false information, Including the possiboty of fines and imprisonment for knowing violations." (Signature of Permittee) 6 d (Date) Form SWU-246-051100 Page 2 of 2 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling our this form, please visit https://deg.ne.�,,oy/about/divisions/energy-mineral-land- resources/energy-m inera1-1and- permits/stormwater-perm itslnpdes-industrial-sw#tab-4 Permit No.: NIC/J/-O/0/0/313/0/ or Certificate of Coverage No.: N/C/G/ 1 /_I / l l Facility Name: A T.L—623ffc-- kj f�1�}�6/l r1} 15 County: 1'Phone No. lay -a 89 - q�,f fI Inspector: —JA- M 3.S mwzx - Date of Inspection: /r - 9 - a Time of Inspection: 8 : / 3 Am _ Total Event Precipitation (inches): Q - 1- 5 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or 1. Outfall Description: Outfall No. .Sw a r Structure (pipe, ditch, etc.): - Receiving Stream: �J !!_ LL CF 1C h !3 a1 jf D Al t°rGC14 _ Describe the industrial activities that occur within the outfall drainage area: MeAllfor E Page 1 of 2 SWU-242, Last modified 07/2812017 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: ✓G444 /,'A-Ip h f' Ar'AW 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 1116nI E _ 4. Clarity: Choose the number which best describes the clarity of the discharge, where l is clear and 5 is very cloudy: 1 O2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where l is no solids and 5 is the surface covered with floating solids: Q 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 © 3 4 5 7. Is there any foam in the stormwater discharge? () Yes eNo. 8. Is there an oil sheen in the stormwater discharge? ()Yes K0. 9. Is there evidence of erosion or deposition at the outfall? O Yes 0'No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 �i Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit htt s:llde .nc. rov/about/divisions/ener -mineral-land- resources/energy-mineral-land-perm_ its/stormwater-permitslnpdes-industrial-sw#tab-4 Permit No.: NlCl,ll OIQI & 31J10 or Certificate of Coverage No.: N/C/GI_l_l_I_I_I 1 Facility Name: A % .S- ;-,Tf hu nA",A15 — — County: U,y � 1z41 Phone No. 70 4 -a89 - 4.S'IJ Inspector: %y%af C-,e Date of Inspection: //- Cl — [9 Time of Inspection: 8 . 9.1 qM Total Event Precipitation (inches): Q . 4/5 All permits require qualitative monitoring to be performed during a "measurable storm event." - A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or 1. Outfall Description: Outfall No. W 0 Structure (pipe, ditch, etc.): Receiving Stream: n r Describe the industrial activities that occur Within the outfall drainage area: M -,cr -4 ) -fkrrA Cx Page 1 of 2 SWIJ-242, Last modified 07/J' /2017 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: .11� f �7�'Oca�nf _ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): MO AIS 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 Q 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with Floating solids: 1 2 Q3 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: I �£ 3 4 5 7. Is there any foam in the stormwater discharge? () Yes Qr-N-o. 8. Is there an oil sheen in the stormwater discharge? ()Yes Gr�o. 9. Is there evidence of erosion or deposition at the outfall? o Yes �No. t0. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last moditicd 07/29/2017 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out ibis form, please visit https:Hdeg.nc.gov/about/divisions/energy-mineral-land- resourceslenerey-m i neral-1and -perm itslstormwater-perm its/npdes- industrial -sw#tab-4 Permit No.: N/C/ f IQIQI 01313/ 0 or Certificate of Coverage No.: NICIGI 1 I-1 I 1 1 Facility Name: 19 �Z .fa' ',cI& MA.�-�1e,f�... --- County: L& I.QAe Phone No. %D 4 -ab7°i - 415/ 1 Inspector: Z-AMO„S M6S64 Date of Inspection: 9 - / S Time of Inspection: .' 02 % ,qm Total Event Precipitation (inches): 6 -'4-5 All permits require qualitative monitoring to be performed during a `measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or i. Outfall Description: Outfall No. sw o 3 Structure (pipe, ditch, etc.): g2 e6r d 1 �c 11 Receiving Stream: A i G h RA.rj s aA1 Gre-.47k Describe the industrial activities that occur within the outfall drainage area: - ' Page 1 of 2 5WU-242, Last modified 07/28/2017 2. Color: Describe the color of the (light, medium, dark) as descriptors: _ using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4)pN G 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: w 1 3 4 5 5. Floating Solids: Choose the number which best describes the arnount of floating solids in the stormwater discharge, where l is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the arnount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 3 4 5 7. Is there any foam in the stormwater discharge? Q Yes �No. 8. Is there an oil sheen in the stormwater discharge? ©Yes (? No. 9. Is there evidence of erosion or deposition at the outfall? 0 Yes C�lo. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5WU-242, Last modified 0712R12017 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this firm, please visa https:Hdeg.ne.i�,ov/about/divisions/energy-mineraL-land- resources/energy-m inera I-1and-perm its/storm water- Perm its/npdes-industrial-sw#tab-4 Permit No.: or Certificate of Coverage No.: NICIGI_l—l—l—l_I_I FacilityName: A Tl rjl�taCr�9 ��N %���G2i i2�S County: U ,M Phone No. 70 N- Inspector: Date of Inspection: Time of Inspection: K: V y a,-,m Total Event Precipitation (inches): 0. 4-%.3 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowlcdge„ (Signature of Permittee or 1. Outfall Description: OutfalI No. ;5t� o e,✓ Structure (pipe, ditch, etc.): Receiving Stream: Describe the industrial activities that occur within the outfaJll drainage area: �/j . pQ i i1J c.�� I .N a1 r _. �"r-yG� �d19 0 � N G .,_ Lin/ • S _ S �e rI�C7� !s Page 1 of 2 SWIJ-242, Last modified 07/28/2017 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: ./ j'gh f bro m>Ai � 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _/fnA1,6 4. Clarity: Choose the number which best describes the clarity of the discharge, where l is clear and 5 is very cloudy: Q 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: l Q 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: I © 3 4 5 7. Is there any foam in the stormwater discharge? () Yes i► O. S. Is there an oil sheen in the stormwater discharge? ()Yes !o 9. is there evidence of erosion or deposition at the outfall? O Yes G;-1 o. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Q Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 F Environmental Quality Stormwater Discharge Out fall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit htt s:Hde .ne. L)v/about/divisions/ener -mineral-land- resources/ener -mineral-land- ermitslstormwater- ermitsln des-industrial-sw#tab-4 Permit No.: NIC/SIAIQI o 1,11-3 01 or Certificate of Coverage No..: NICIGI_I_l l_ _l—h/ Facility Name: County: CiV ,'6AJ Phone No. %0 q - QR9 - q-511 Inspector: !�j Amc-J Orel Date of Inspection: /f - 9 - % Time of Inspection: _ _X ; 6 6 4 ry!i Total Event Precipitation (inches): 0. L/5 All pen -nits require qualitative monitoring to be performed during; a "measurable storm event." A "treasurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the pennittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. - By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Deknee) 1. Outtall Description: r_ Outfal l No. S'A) 0 5 Structure (pipe, ditch, etc.): Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Pagel of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: /,- f- bra sW_� 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): IVOAl G 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where l is no solids and 5 is the surface covered with floating solids: 4D 2 3 4 5 6. Suspended Solids: Choose the number which best describes the arnount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? O Yes No. 8. Is there an oil sheen in the stormwater discharge? OYes erNo. 9. Is there evidence of erosion or deposition at the outfall? o Yes "0. to. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242. Last modified 07/2812017 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit httpsa/deg.ne._: ov/about/divisions/energy-mineral^ land- resources/energy-mineral-land-perm its/stormwater-perm itslnpdes-industrial-sw#tab-4 Permit No.: NIC/ 5/ 0/O 10 /3 / 3101 or Certificate of Coverage No.: NICIGI—I—I_I_I_I_l Facility Name: 19T I „ ,0 L.i 14I C/I-y MIA671ZI'015 — — — County: LJAII�QW Phone No. Inspector: lz Date of Inspection: it - 9 - / 4? w Time of Inspection: 9:.33 qm Total Event Precipitation (inches): O All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during; the sampling period, and the permittee obtains approval from the local DEMLR onal Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or D)kignee) 1. Outfall Description: Outfall No. _5W 0 6 Structure (pipe, ditch, etc.): Receiving Stream: „ f 111 Describe the industrial activities that occur within the outfall drainage area: / Page 1 of 2 SWU-242, Last modified 07I2WO17 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: , . 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): %I/Qe G 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: l © 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 © 3 4 5 7. Is there any foam in the stormwater discharge? Q Yes No. 8. Is there an oil sheen in the stormwater discharge? ()Yes GKO. 9. Is there evidence of erosion or deposition at the outfall? O Yes c7No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 aceAnalytical wwwPacelabs.mm November 06, 2018 Mr. Preston Baucom Allvac 2020 Ashcraft Ave Monroe, NC 28110 RE: Project: MONROE STORMWATER Pace Project No.: 92404952 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Baucom: Enclosed are the analytical results for sample(s) received by the laboratory on October 26, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Mr. Joe Hinkle, Allvac Mr. Tommy Long, Allvac Scott Ryan, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 lacmnalyticalo www.paceiabs.com Project: MONROE STORMWATER Pace Project No.: 92404952 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IQs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 LouisianalNELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification Ids 2225 Riverside Drive, Asheville, NC 28804 Florida]NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #; 84 Virginia/VELAP Certification #: 460221 Norlh Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuli, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 laneAnalytical' %ww.pacefebs.com SAMPLE ANALYTE COUNT Project: MONROE STORMVVATER Pace Project No.: 92404952 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytts Reported Laboratory 92404952001 SW02 EPA 1664B JMS 1 PASI-C EPA 200.7 Rev 4A 1994 DS 5 PASI-A SM 254OD-2011 CEH 1 PASI-A SM 521OB-2011 RLO 1 PASI-A SM 5220D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 aceAnalytical wwwpacelabs.cw ANALYTICAL RESULTS Pace Analytical Services, LLC 9a00 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: MONROE STORMWATER Pace Project No.: 92404952 Sample: SW02 Lab ID: 92404952001 Collected: 10/26/18 05:20 Received: 10126/18 10:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By JM 1 10126/18 05:21 Collected Date 10126/18 1 10/26/18 05:21 Collected Time 05:10 1 10/26118 05:21 pH 7.0 Std. Units 0.10 1 10/26118 05:21 Temperature 14 deg C 0.50 1 10/26/18 05:21 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease 5.1 mg1L 4.8 1 11/06/18 05:16 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Cadmium ND ug1L 1.0 1 10/27/18 05:34 10/29118 03:07 7440-43-9 Chromium 21.6 ug/L 5.0 1 10/27118 05:34 10/29/18 03:07 7440-47-3 Lead ND ug/L 5.0 1 10/27/18 05:34 10/29/18 03:07 7439-92-1 Nickel 109 ug/L 5.0 1 10/27/18 05:34 10/29/18 03:07 7440-02-0 Zinc 355 ug/L 10.0 1 10/27118 05:34 10/29/18 03:07 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 38.6 mg1L 5.0 1 10/3011 B 01:59 5210B BOD, 5 day Analytical Method: SM 521 OB-2011 BOD, 5 day 16.0 mg1L 2.0 1 10/27/18 01:32 11/01118 02:12 L2 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 73.6 mg/L 25.0 1 10131/18 15:00 11/01/18 17:23 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, LLC- Page 4 of 14 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92404952 QC Batch: 440476 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92404952001 METHOD BLANK: 2419432 Associated Lab Samples: 92404952001 Parameter Units Oil and Grease mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 4.8 11/06/18 05:13 Pace Analytical Services, LLC 9600 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2419433 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 38.5 36.4 95 78-114 MATRIX SPIKE SAMPLE: 2419434 92404994002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 38.5 37.6 97 78-114 Results presented on this page are In the units Indicated by the "llnits" column except where an alternate unit Is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 laceAnallyfical" www.pacefabs.com QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92404952 QC Batch: 438752 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92404952001 METHOD BLANK: 2412034 Matrix: Water Associated Lab Samples: 92404952001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium ug1L ND 1.0 10/29/18 03:51 Chromium ug1L ND 5.0 10/29/18 03:51 Lead ug1L ND 5.0 10/29118 03:51 Nickel ug1L ND 5.0 10/29118 03:51 Zinc ug1L ND 10.0 10/29/18 02:14 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2412035 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Cadmium ug1L 500 497 99 85-115 Chromium ug1L 500 491 98 85-115 Lead ug/L 500 497 99 85-115 Nickel ug/L 500 496 99 85-115 Zinc ug/L 500 516 103 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2412036 2412037 MS MSD 92404821001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Cadmium ug1L ND 500 500 486 483 97 96 70-130 1 Chromium ug1L NO 500 500 476 476 95 95 70-130 0 Lead ug1L ND 500 500 472 470 94 94 70-130 0 Nickel ug1L 7.4 500 500 480 476 94 94 70-130 1 Zinc ug1L 379 500 500 862 852 97 95 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2412038 2412039 MS MSD 92404952001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua[ Cadmium ug1L ND 500 500 493 484 99 97 70-130 2 Chromium ug1L 21.6 500 500 505 497 97 95 70-130 1 Lead ug1L ND 500 500 485 476 97 95 70-130 2 Nickel ug1L 109 500 500 602 588 99 96 70-130 2 Zinc ug1L 355 500 500 853 850 100 99 70-130 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 aoAnalytical viwwpacelabs.com QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92404952 Pace Analytical Services, LLC 9600 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 439068 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-201i Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92404952001 METHOD BLANK: 2413197 Matrix: Water Associated Lab Samples: 92404952001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 10/30/18 01:57 LABORATORY CONTROL SAMPLE: 2413198 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 254 101 90-110 SAMPLE DUPLICATE: 2413199 92404991002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 10.4 13.4 25 D6 SAMPLE DUPLICATE: 2413200 92404958002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 40.8 41.6 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, l.t.C. Page 7 of 14 acmnalytical **W pacelabs.WM Project: MONROE STORMWATER Pace Project No.: 92404952 QC Batch: 438745 QC Batch Method: SM 52108-2011 Associated Lab Samples: 92404952001 METHOD BLANK: 2412018 Associated Lab Samples: 92404952001 Parameter BOD, 5 day QUALITY CONTROL DATA Analysis Method: SM 52108-2011 Analysis Description: 5210E BOO, 5 day Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers mg/L NO 2.0 11/01/18 02:08 LABORATORY CONTROL SAMPLE: 2412019 Spike LCS Parameter Units Conc. Result BOO, 5 day mg/L 198 153 SAMPLE DUPLICATE: 2412021 92405075001 Dup Parameter Units Result Result BOD, 5 day mglL 685 676 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS % Rec % Rec Limits Qualifiers 77 84.6-115 L2 RPD Qualifiers 1 B1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Tull, Date: 11I0612018 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 1�55'ne Analytical f wuw.peceJeba.corrt I Project: MONROE STORMWATER Pace Project No.; 92404952 QC Batch: 439481 QC Batch Method: SM 5220D-2011 Associated Lab Samples: 92404952001 METHOD BLANK: 2415039 Associated Lab Samples: 92404952001 Parameter Units Chemical Oxygen Demand mg1L QUALITY CONTROL DATA Analysis Method: SM 5220D-2011 Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 11101/18 17:20 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2415040 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 748 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2415041 2415042 MS MSD 92404515005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 92.2 100 100 193 186 101 93 90-110 4 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE; 2415043 2415044 MS MSD 92405151001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 52.2 100 100 151 140 99 88 90-110 7 M1,R1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 aceAnalytrcal www.pacelabs.com QUALIFIERS Project: MONROE STORMWATER Pace Project No.: 92404952 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosod iphenyl a mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyles. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS B1 Less than 1.0 mglL DO remained for all dilutions set. The reported value is an estimated greater than value and is calculated for the dilution using the least amount of sample. D6 The precision between the sample and sample duplicate exceeded laboratory control limits. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 IeAnalytical www.pmlitbs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 26078 (704)875-9092 Project: Pace Project No.: MONROE STORMWATER 92404952 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92404952001 SW02 92404952001 SW02 EPA1664B 440476 92404952001 SW02 EPA 200.7 Rev 4.4 1994 438752 EPA 200.7 Rev 4.4 1994 438781 92404952001 SW02 SM 2540D-2011 439068 92404952001 SW02 SM 521OB-2011 438745 SM 521OB-2011 438770 92404952001 SW02 SM 5220D-2011 439481 SM 5220D-2011 439841 Date: 11/06/2018 01:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 Document Name: Document Revised: February 7, 2018 aceAnalyfical''_ Sam ie Condition Upon Recei t(SCUR) Page 1 of 2 No.: issuing Authority: _Document F•CAR-CS-033-Rev,06 Pace�Camllrias Qualit Office Laboratory receiving samples: Asheville ❑ Eden[—] Greenwood ❑ Huntersville Q Raleigh[] Mechanicsville[] ` n Receipt project fr T Client Narae: W # : 92404952 Courier: ❑Fed Ex UPS ❑LISPS — 'QClient ❑ Commercial ❑Pace ❑Other: 92404952 Custody Seal Present? QYes ❑No Seats Intact? ❑Yes ❑No 0a1eJlniUsfs Person Erramining Contents: Ll�li• ��+�1��• Packing Material: ❑Bubble wrap QBubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermometer: Dyes QMo ❑N/A [did Gun Ill: 92TO45 Type of Ice: ©wet ❑Blue []None Cooler Temp ('C): '? Correction Factor: Add/Subtract ('C) _0 I 11 Temp should be above freezing to 6'C Cooler Temp Corrected VC): ' Lr ❑samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soh ([] N/A, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or SC {check maps)? Did samples originate from a foreign source (internationally, eyes nNa inctudina Hawaii and Puerto Ricoi> rives nNo Comments/Discrepancy: Chain of Custody Present? ❑yes ONO NIA 1. Samples Arrived within Hold Time? O vies ONO EINIA 2. Short Hold Time Analysis 1<72 hr.)? • ves QNa ❑N/A 3. Rush Turn Around Time Requested? Yes BND ❑NJA 4. Sufficient Volume? ves ONO ❑N/A 5. Correct Containers Used? -Pace Containers Used? Eyes ElYes ONO ONO ❑NIA ❑N/A 6. Containers Intact? Eyes C3NO N/A 7, Dissolved analysis: Samples Field Filtered? ❑Yes E3NO Q N/A 8. Sample'Label% Match COC? -Includes Datejrime/ID/Analysis Matrix: QYcs '" ❑ND ❑N/A 9. Heads ace in VOA Vials (�P5-6mm)? ❑ves QNO - NJA 20. Trip Blank Present? Trip Blank Custody Seals Present? ❑ves ❑ves QNo H ❑N/A ❑N/A 11. COMMENTS/SAMPLE DISCREPANCY Field Data Required? Oyes ONO Lot ID of spfit containers: CLIENT NOTIFICATION%RESOLUTION Person Contacted: Date/Time: Project Manager SCURF Review: Date: Project Manager SRF Review: L/i Date: Vf Page 12 of 14 Document Name: Document Revised: February 7, 2018 �ceAnalyftcal' Sample f onditlon Upon R"el t(5CUR) Pale 1 of 2 Document Na.: Issuing Authority: r - — F.CAR-CS-033-Rev.06 Pace Carolinas Quad Office_ -- *Check mark top half of box if pH and/or dechlorination Is verified and within the acceptance range for preservation samples, Except€om: VOA, Collform, TOC, Oil and Grease, DRO/9015 (water) DOC, LLHg "Bottom half of box Is to list number of bottle Project Wp# : 92404952 I,M: MWB Due Date: 11/06/18 CLIENT: 82-Allvae NC Ift E u 0. Y a E a a u a ,fin 7 a E on_ H d m C W G ' v N a m d N v m m p ? = V n M ee as m y� Q N y m n O Z a ry a ca a b a E 3 3 _ $i a ? `a E .; 47 a ry a U = `., z CL C a E 4 N l7 a v gpr ✓1 S m A E ,zA l7 a v Jp� N a E ¢ "J,' t7 a -- i �C �i J E Sa ry a� Z .�. V = 0 Y ' Q 0 N 2 Z ¢ O q l�7 S Z A C 4 0 9 l7 5 Z Ri = a 0 V'0`r l�3 Z N r y a 6 x t7 a ¢ .Z ?; e .L' a y ?; rr 1� S z U '� E ' Z c 7 E E z i q .5 in E mar O E E q q 1 2 I 3 a i I s 6 7 8 10 71- 1 N 12 N NN\� pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon recelpt Date preservatlan adjusted Time preservstlon adjusted Amount of Preservative added Lot tt Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the Nonh Carolln0 ULHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 13 of 14 Ie, f PaceAnalytical' wwr.oacalahs.cam CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must he complaled accurately. Section A Section S Section C Page: of , Required Client Information: Required Project Information' lnvujm Information: _ Report To: ,r Aft nt -f�AZ 1790377 Address; r Copy r is _ To; Jv - C� a r y REGULATORY AGENCY /trc. rL� rile A 2F� e - -5'0jz] j/::yd fVL NPUES GROUND WATER ( DRINKING WATER (-- UST (- RCFiA OTHER Emait To: Purchase OfdCr No: p'nm Ounfp Refcrenar; J Fax: Proiect Name: j Paco P 4 Site Location L4!z�e— STATE: Requestod Due DaterTAT; Project Number: Pace Profde e. Requested Analysis Filtered (Y/Nj Section D Matrix Codes ❑ it Req.IrodOwnt,nf—wm. MATRix r CODS e COLLECTED Preservatives > Drinking Water OW - O) z Y{atcr VY'T WW 4 ] corosn: START r)LrdT( ENGiANV{a51e _Z Proiuet P 501VS0110 SL a rj p Y SAMPLE ID ° °p �? r (A-Z. 48l,•1 Air AR w 0 w a o. z m t" Sampie IDs MUST BE UNIQUE Tissue TS p EL Fa- m Vr U Other OT x a a ILL a 0 O u] L = y �zfcy�iZ ~ L DATE 71ME DATE TIME pace Project No./ Lab I.D. la 1 D13 ! 2 . { a ' S;!`fyI dU� s 7 8 I 9 14 11 12 a ADDITIONAL COMMENTS RELINQUISHED BY; AFFILIATION DATE TIME ACCEPTED BY ! AFFILIATION DATE TIME SAMPLE CONDITIONS .4 Sa SAMPLER NAME AND SIGNATURE ORIGINAL PRINT Name of SAMPLER: �pt,.�� /7 GEC-Q � � :�i,�-lam E m 7 o n A PATE Signed ) SIGNATURE D1 $AM R: ._/,!1 �Gt-� G '" (� in 'n G (MMIDDNY): 'imlxal,u i Noi, Ry ,lj.inq,hi 1— lnni px.f•s .CIE 130 day I.Y—V I' mrtv nne:xirn,(.tin!, to III,, dm T!. or 15%p;�unlh tnr any urvrJice:-Wt rx'rN -thin 30 0ys, F-ALL-0-020rev.07. 15-May-2007