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NCS000330_MONITORING INFO_20170811
STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. DOC TYPE ❑ FINAL PERMIT 9- MONITORING- REPORTS— - -- - --- - - -- ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ 2dl"] • 0`6 • �� YYYYMMDD August 8, 2017 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files: RECEIVED fkfy'� -TE 11 2017 CENTRAL FILES DWR SECTION OATI P.O. Box 5030 2020 Ashcrafl Avenue Monroe, NC 281 l 1-5030 Phone: (704) 2894511 Fax: (704)290-5194 Email: Joe. Hinkle a@atimetals.com Attached, please find stormwater monitoring data for Permit No NCS000330. The originals and one copy are included. The monitoring data is for the following monitoring schedule: Monitoring Period Sample Number Start I End Year 8 — Period 2 16 March 1, 2017 1 August 31, 2017 Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall through prior correspondence. If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sincerely, 0t Jo Hinkle EHS Manager Allvac Monroe Plant —*ATI Alivac Stormwater Monitoring Report Form Sample Date: ` / 77-J 7- _ Sample Time: _ 7:y O Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Stormwater Discharge Outfall #2 Drainage Area = 272,590sq ft. = 6.25 acres % Impervious = MN �t4fY1ES �QS��' 40 CFR Part 136 Parameter Results (mg/1) Benchmark Values (mg/l) BOD a 6 30 COD a. 120 TSS a 6 100 Cadmium D 0.001 Chromium, total recoverable 0,6107 1 Lead, total recoverable 0.03 Nickel, total recoverable 0.0 7 4/F 0.26 Zinc, total recoverable Q 416 9 O 0.067 Oil and Grease O 30 pH 7.3 (std units) 6-9 (std units) Storm Date: - 7— / 7 Storm Duration: 0-7-4 (firs.) Inches of Rainfall: 0 - a 0 Duration of time preceding rain event exceeding 4.1": _ 160 (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 6.25 acres x .64) + .9 x inches rain/12inches/ft. x 6.25 x .36) Q(Total, cfs) = .I333 x 0 O (Inches of rain) + .1688 x Q • 02 d (Inches of rain) =0.0606cfs .. f-�.. .� rZ e _f ' �� __ ✓ .. J' : � � - - - . M� - STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number. NC IS 000 33 U or Certiflcate of Coverage Number: NCG FACILITY NAME ZIG PERSON COLLECTING SAMPL S) -12 CERTIFIED LABORATORY(S) Lab # Lab # Part A: Specific Monitoring Requirements Date 1 'Sample Collected I ' SAMPLES COLLECTED DURING CALENDAR YEAR: 1 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Unf I �2 .✓ _ PHON O. (74"y} (SIGNATURE oqERmrrWoR DESIGNEE) By this signature, I certify that' is report is accurate complete to the best of my knowledge. Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? — yes zo (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow Oil and Grease Total Suspended Solids pH New Motor Oil Usage mo/dd! r A MG I mg4 m unit allmo Form SWU-246-051100 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date 7— /7- / 7 Total Event Precipitation (inches): Event Duration (hours): O , 7S (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the posVibility of fines and imprisonment for knowing violations." — ,,- L21,�Zw (Signature of Permittee) (Date) Form SWU-246-051100 Page 2 of 2 rI Ir 7 NCDENIR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: htt&/112orta1.ncdennorgf web jwg1wsIsuInptlesNw#tab-4 Permit No.: �l /�/�/ O/Q/ D/•3 Facility Name: A9 7-= X/I County: ' nJ Inspector: Date of Inspection: 7 - a 3 Time of Inspection: 4 : lJ/ 0/ or Certificate of Coverage No.: Total Event Precipitation (inches): /. 70 i � Phone No. 701/- Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) [gYes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfalI. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatur , I certify that thi report is accurate and complete to the best of my knowledge: O? ti 1. Outfall Description: Outfall No. � Structure (pipe, ditch, etc.) + Receiving Stream: v Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the disch (light, medium, dark) as descriptors: /i' afof using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 6ZONe3 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 (0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 lD 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 60 9. Is there evidence of erosion or deposition at the outfall? C es No 10. Other Obvious Indicators of Stormwater Pollution: List and describe ..SOME �'l"O.�ronl f} f _Ei✓c� d ��D SAC TO bed _ r'C,orsr'rc _ Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 e ��A NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http://portal.ncdenr.org/web/wa/ws/su/npdessw#tab-4 Permit No.: or Certificate of Coverage No.: Facility Name: 4 7= 4&VAc. County: T (Jiy,'oN Phone No. 7041 — oz 89- Z/// Inspector: `SAMd-4-4 /'Y1 as,6C1 Date of Inspection: 7 - 02 3 / 7 Time of Inspection: Total Event Precipitation (inches): 1, 9 0 " Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatureA certify that this report is accurate and complete to the best of my knowledge: r s A 1. Outfall Description: Outfall No. W 0 a Receiving Stream: r•C� re (pipe, ditch, etc.) Describe the industrial activities that occur within the outfalJ drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: A7gsO , wf" !Ti"AU 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): N&V 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 Q 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 0 4 5 7. Is there any foam in the stormwater discharge? Yes 0 8. Is there an oil sheen in the stormwater discharge? Yes 0 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. SWU-242, Last modified 10/25/2012 Page 2 of 2 x ja NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance onfflling out this form, please visit: http://portal.ncdenr.org/web/wq/ws/s u/nndessw#tab-4 Permit No.: N, Facility Name: County: _C or Certificate of Coverage No.: N/C/G/_/—/—/—/_/_/ Inspector: --s Aln16.S t f ! CtSE'Az Date of Inspection: 7 - oZ 3 ` / 7 Time of Inspection: 6 : q 9 ogM _ Total Event Precipitation (inches): 0 t l Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatureyl certify that this import is accurate and complete to the best of my knowledge: {I Z. Outfall Description: Outfall No. w 3 Structure (pipe, ditch, etc.) A ZV& 12 Receiving Stream: &i?-b 6rc "Al Describe the industrial activities that occur n the outfall drainage area: 2. Color: Describe the color of the discharge (light, medium, dark) as descriptors: Z?W[ basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): ,n 12A le 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 © 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? Yes B. Is there an oil sheen in the stormwater discharge? Yes Io 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe / - OAI Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. SWU-242, Last modified 10/25/2012 Page 2 of 2 .0 M LT i�-K WA NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: hap: ortal.ncdenr. r web w ws u n w#tab-4 Permit No.: ZV/C/.S/ D/O/ 0/3/3/ O/ or Certificate of Coverage No.: Facility Name:,, /'qrZ 1911 VA C _ County: V-V Inspector: Phone No. /0 `/ Date of Inspection: 7-.23 -17 _ Time of Inspection: 7 : 0 !Y aln Total Event Precipitation (inches): 1.3oll Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, certify that this re ort is accurate and complete to the best of my knowledge: s 1. Outfall Description: / Outfall No. Jr' W O Structure (pipe, d��� -OZ4�&b Receiving Stream: Lh1grz foM Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the di (light, medium, dark) as descriptors: —A rge using basic colors (red, brown, blue, etc,) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _ n1OA1j:!6-,,, 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and S is very cloudy: 1 Q 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 7. B. 9. 1 0 3 Is there any foam in the stormwater discharge? 4 5 Yes Is there an oil sheen in the stormwater discharge? Yes Is there evidence of erosion or deposition at the outfall? Yes 10, Other Obvious Indicators of Stormwater Pollution: List and describe LION Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. SWU-242, Last modified 10/25/2012 Page 2 of 2 NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: hUp;-J/portal.ncdenr,org/webJwq/ws/s uJnpdessw#tab-4 Permit No.: Vrl/C/J/0/D / 0/-4/3/ O/ or Certificate of Coverage No.: N/C/./_/T/_/�/_/_/ Facility Name: A T = Alt VA c County: _ Inspector: fly,,OAI Phone No. _ 701q- 0'18 4 - q,511 Date of Inspection: 7 a 3 -_/ 7 Time of Inspection: _�_34 ,aM Total Event Precipitation (inches): / # 9 Q " Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) +" Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I Sotify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. ,5w a55 Structu a (pipe, ditch, etc.) �i4-c h Receiving Stream: i*c. k tNr ..SOn.i Cnc c C Describe the industrial activities that occur within the outfall drainage area:��e��M/rhD�u 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Fr� �'v.+�, br au►�y1J 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): IVyAo 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: ^ 1 �J 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: !� 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 (C.J 3 4 5 7. Is there any foam in the stormwater discharge? Yes A o a. Is there an oil sheen in the stormwater discharge? Yes Q 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Grro.s,; ' , `. / - - --- ' Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 i a .� NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out thisform, please visit: http://portal.ncdenr.orp-lweb/wq/ws/sulnpdessw#tab:4 Permit No.: �[/C/,�/Q/4/�/,�/3/Q/ or Certificate of Coverage No.: N/C/-G/_/._._/_/—/_/_/ Facility County: Phone No. --70!V - 122 9 - 4/2U/ Inspector: frIQ5,eEg Date of Inspection: 7-23 - 17 Time of Inspection: _ 6 :I A am _ Total Event Precipitation (inches): ll Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Q Xes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for Iocal storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this Keport is accurate and complete to the best of my knowledge: 1. Outfall Description: �/ 1G� 0utfall No. JQ6 Structure (pipe, ditch, etc.) T _ Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: M 61LAL -.-Ov n9 91 d 6E.1,," 7`r�h Z?W/ r�FF 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: /r'a M- browAl 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 S S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 0 3 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? Yes B. Is there an oil sheen in the stormwater discharge? Yes 9. is there evidence of erosion or deposition at the outfall? Yes 0 10. Other Obvious Indicators of Stormwater Pollution: List and describe /V'ONGE Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 Allvac - Monroe Plant 1--kAT, I Allvac Stomy ter Monitoring Report Form Sample Date: 7 - / 7 - ,% 7 _ Sample Time: 7 % 6 O O—Q/Y? Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Stormwater Discharge Outfall_ #2 Drainage Area = 272,590sa. ft. = 6.25 acres % impervious = 36% ;�ffi&s mAgc ° _ Ae'e 40 CFR fart 136 Parameter Results (mg/1) Benchmark Values (mglt) BOD a 6 30 COD 120 TSS a 6. 100 Cadmium D 0.001 Chromium, total recoverable 10,6107 1 Lead, total recoverable 0 0.03 Nickel, total recoverable 0.0 7 I/ $ 0.26 Zinc, total recoverable O- T S g O 0.067 Oil and Grease O 30 PH 7 3 (std units) 6-9 (std units) Storm Date: - 7-! 7 Storm Duration: Q. (Hrs.) Inches of Rainfall: a - a O Duration of time preceding rain event exceeding 0.1": 16 $ (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 6.25 acres x .64) + .9 x inches rain/12inches/ft. x 6.25 x .36) Q(Total, cfs) = .1333 x 0.20 (Inches of rain) + .1688 x 6.02 O (Inches of rain) = o. D 6 0.� cfs STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number: NC or Certificate of Coverage Number: NCG FACILITY NAME G PERSON COLLECTING SAMPL S) �-W CERTIFIED LABORATORY(S) A&A Lab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2 Ot 7 (This monitoring report shall be received by the Divislon 'no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY PHON O. (7y4) — (SIGNATURE OqERmnrTWoR DESIGNEE) By this signature, I certify tha his report is accurate complete to the best of my knowledge. r is ii r ' �P Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes je6 o (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow Oil and Grease Total Suspended Solids pH New Motor OR Usage mold!/ r MG m MRA unit 9211mo, Form SWU-246-051100 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date -7-/Z' l 7 Total Event Precipitation (inches): Q a d Event Duration (hours): Q • 7.S (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the po ibility of fines and imprisonment for knowing violations." (?-ZW -/ I (Signature of Permittee)6 (Date) Form SWU-246-051100 Page 2 of 2 4 h 41 �0 MCDENR Stormwater Discharge Qutfall (SDQ) Qualitative Monitoring Report Forguidance on filling out this form, please visit. http:f/portal.ncdenr.org/web/wq/ws/su/npdessw#tab- Permit No.: or Certificate of Coverage No.: Facility Name: County. --tL inspector: Z Phone No. 70Y- Date of Inspection: �Z " 3 — 17 _ Time of inspection: _ 44 : 3_,1�_, Total Event Precipitation (inches): O { Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Eg"Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this sign I certify that thi report is accurate and complete to the best of my knowledge: 4YZ J ea= r r� 1. Outfall Description: ' Outfall No..lW a I Structure (pipe, ditch, etc.) Receiving Stream: 4i Cr- - Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the di (light, medium, dark) as descriptors: using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): —,.,V4 e 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 (D 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 O 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes �o 9. Is there evidence of erosion or deposition at the outfall? es No 10. Other Obvious Indicators of Stormwater Pollution: List and describe _ .SOMEL_ 6COSrc�.v f} ENcf d �A A0 b,- Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. SWU-242, Last modified 10/25/2012 Page 2 of 2 l NC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http:1/nortal.ncdenr.orgf web/wq/ws/su/nodessw#tab-4 Permit No.: NXI.' Facility Name: --Z County: UN.'� inspector:yAi Date of Inspection: Time of Inspection 6 : y3 ,om or Certificate of Coverage No.: Phone No. 7041 — v2 $9- Total Event Precipitation (inches): 1. 90 1t Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature,/] certify that thi§ report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. 3W O a Structure (pipe, ditch, Receiving Stream: i+c� Ar�-6CA) Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: t7 Q , v,1 A-AC4 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /VCvV�_ 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 O 3 4 5 5. FIoating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 p 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 0 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes O 9. Is there evidence of erosion or deposition at the outfall? Yes LO 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 LTIFWA -Ar*'Ar NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http;/L12ortal.ngdenr.org/web/wq/ws/sulnndessw#tab-4 Permit No.: or Certificate of Coverage No.: Facility Name: jA County: iyr'. Inspector: Date of Inspection: _ _7- 9.3 ` / 7 Time of Inspection: Total Event Precipitation (inches): r 0 I l Phone No. Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature/I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. w Q.3 Structure (pipe, ditch, etc.) 6 Z4)11 Receiving Stream: >J41"ds�.►1 _Gd'�Ei� Describe the industrial activities that occur within the outfall drainage area: _1 _ . .r _ _ .. ., . If _ . i/ I .i_ _ 'In I . , _ 2. Color: Describe the color of the discharge usin basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: ' 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): n/D.✓E _ 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 © 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 (0 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes 6D 10. Other Obvious Indicators of Stormwater Pollution: List and describe / ✓ OW Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 r� RC®ENR Stormwater Discharge autfall (00) Qualitative Monitoring Report Forguidance onfilling out thisform, please visit: http://portal.ncdenr.org/web/wq/ws/su/nodessw#€tab-4 Permit No.: 0/3/2/� or Certificate of Coverage No.: Facility Name: /9 X 1711 VA C County: UAJ, ,0N Phone No. 70 Inspector: l lQSEAZ Date of Inspection: �7 —,r2,3_17 Time of Inspection: 7 O i1 Total Event Precipitation (inches): Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, certify that this re ort is accurate and complete to the best of thy knowledge: _ —T 1. Outfall Description: ' / Outfall No. Jr w O Structure (pipe, ditch, etc.) �4 6 %c// �t_'G�1 Receiving Stream: A/ zclDN . Cr' iF Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the di (light, medium, dark) as descriptors: using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): IVO I- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 Q 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 ® 3 4 5 7, Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes L'�! 10. Other Obvious Indicators of Stormwater Pollution: List and describe D/V Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 RC®ER Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform, please visit: http_//l2ortal,ncdenr.orglweblwglwsisulnpdessw# wb-4 Permit No.: or Certificate of Coverage No.: Facility Name: C County: #* AI Phone No. 7a - _ 8 Q - yS 1 / Inspector: MA as6w _ Date of Inspection: _7 - r, 3 -1 7 Time of inspection: 6 : 30 ,om Total Event Precipitation (inches): I , 9 D " Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) R"Y'es ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event". or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permitee obtains approval from the local DWQ Regional Office. By this signature, I gertify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. ,> W D.5 Structu a (pipe, ditch, etc.) - k1 i IT- h Receiving Stream: 1,C b r r —C ':E _ Describe the industrial activities that occur within the outfall drainage area: e,ow GrriD 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: zjjeei ym brase.361 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): lVoly47 _. 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 6D 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1� 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 (0 3 4 5 7. Is there any foam in the stormwater discharge? Yes A o 8. Is there an oil sheen in the stormwater discharge? Yes Q 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe No Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 WWA RC®ENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfilling out thisform,please visit: http://portal.ncdenr.org/webjwq/wsIsufnodessw#tab-4 Permit No.: �i/�/,�/Q/4/�/,�/3/Q/ or Certificate of Coverage No.: Facility Nam County: Inspector: _ Phone No. Date of Inspection: 7-23 - / _ Time of Inspection: 6 :SA 4Lm Total Event Precipitation (inches): ll Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) [w]Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Mbst permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this geport is accurate and complete to the best of my knowledge: 1. Outfall Description: 1 Outfall No. ,JU0-6 Structure (pipe, ditch, etc.) Receiving Stream: z-dzk Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Jr o 4- 6jro sue.✓ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Al&, lC _ 4. - Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 ,? 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 Q 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes 00 10, Other Obvious Indicators of Stormwater Pollution: List and describe A10,46F Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SwU-242, Last modified 10/25/2012 a' 13Ce Analytical www.pacelabs.com July 27, 2017 Mr. Joe Hinkle Allvac RE. PiujeuL Monroe Stormwater Pace Project No.: 92348113 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on July 18, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless ullleiwise holed Ili llle hotly or llle ieputL. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac David Pope, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 aceAnalytical www.pacelatrs.cam Project: Monroe Stormwater Pace Project No.: 92348113 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Asheville Cellifleallwt IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginialVELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 Y Pace Analytical Services, LLC aceAnalytical 980D KinceyAve. Suite 100 Muntersville, NC 28078 ww,vpaaefabs.cnm (704)875-W92 SAMPLE ANALYTE COUNT Project: Monroe Stormwater Pace Project No.: 92348113 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92348113001 MSW 02 EPA 1664E JMS 1 PASI-C EPA 200.7 SEP 5 PASI-A SM 2540D NAL 1 PASI-A SM 521 OB ECH 1 PASI-A SM 522015 NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 0 !t aceAnalytical www.pacelabs.mm ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Monroe Stormwater Pace Project No.: 92348113 Sample: MSW 02 Lab lD: 92348113001 Collected: 07117117 07:00 Received: 07/18/17 11:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual Field Data Analytical Method: Collected By JM 1 07/17/17 07:02 Field Temperature. 28-3 dP0 C 0.50 1 07/17/17 07.02 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NU mglL 5.0 1 0'1125117 06:08 200.7 MET iCP Analytical Method: F-PA 2W./ Preparation Method: LPA2O0./ Cadmium ND ug1L 1.0 1 07/19/17 15:30 07/23/17 08:14 7440-43.9 Chromium 10.7 uglL 5.0 1 07/19/17 15:30 07/23/17 08:14 7440-47-3 Lead ND ug1L 5.0 1 07/19/17 15:30 07/23/17 08:14 7439-92-1 Nickel 74.8 ug/L 5.0 1 07/19/17 15:30 07123/17 08:14 7440-02-0 Zinc 459 ug1L 10.0 1 07/19/17 15:30 07/23/17 08:14 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 26.2 mglL 8.3 1 07/19/17 18:17 5210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 26.9 mglL 2.0 1 07/19/17 06:30 07/24/17 09:13 D6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 124 mg1L 25.0 1 07/20/17 20:39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 a aoAnalytical www.pecolabs.com Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 370347 QC Batch Method: EPA 1664B Associated Lab Samples: 92348113001 METHOD BLANK: 2052116 Associated Lab Samples: 92348113001 Parameter Oil and Grease QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporthig Units Result Limit Analyzed Qualifiers mg1 NL) 5.0 U/125117 06:07 Pace Analytical Services, LLG 9800 Kincey Ave. Suile 100 Huntersvilie, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2052117 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 36.8 92 78-114 MATRIX SPIKE SAMPLE: 2052118 92348428001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 38.0 95 78-114 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 acmnalytical wrvw.paeerebs.com QUALITY CONTROL DATA A Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersvNe, NC 28078 (704)875-9092 Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369581 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92348113001 METHOD BLANK: 2047905 Matrix: Water Associated Lab Samples: 92348113001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium u IL ND 1.0 07/23/17 07;03 Chromium uglL ND 5.0 07/23/17 07:03 Lead uplL ND 5.0 07/23/17 07:03 Nickel uglL ND 5.0 07/23/17 07:03 Zinc uglL ND 10.0 07/23/17 07:03 LABORATORY CONTROL SAMPLE: 2047906 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Cadmium uglL 500 478 96 85-115 Chromium ug/L 500 470 94 85-115 Lead ug/L 500 468 94 85-115 Nickel ug/L 500 468 94 85-115 Zinc ug1L 500 476 95 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2047907 MS 92347968019 Spike Parameter Units Result Cone. Cadmium ug/L ND 500 Chromium ug/L ND 500 Lead uglL ND 500 Nickel ug1L ND 500 Zinc uglL ND 500 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2047909 MS 92347941003 Spike Parameter Units Result Cone. Cadmium uglL ND 500 Chromium uglL ND 500 Lead uglL ND 500 Nickel uglL ND 500 Zinc uglL ND 500 2047908 MSD Spike MS MSD MS MSD % Rec Cone, Result Result % Rec % Rec Limits RPD 500 482 471 96 94 70-130 2 500 493 464 99 93 70-130 6 500 494 459 99 92 70-130 7 500 474 462 95 92 70-130 3 500 499 463 100 92 70-130 8 2047910 MSD Spike MS MSD MS MSD % Rec Cone. Result Result % Rec % Rec Limits RPD 500 453 465 91 93 70-130 2 500 447 458 89 92 70-130 2 500 441 450 88 90 70-130 2 500 442 453 88 90 70-130 2 500 451 461 90 92 70-130 2 Results presented on this page are In the units indicated by the "Units- column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shMI not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Qual Qual Page 6of14 ''• aceAnalytical www.pacslabs.com Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369720 QC Batch Method: SM 2540D Associated Lab Samples: 92348113001 METHOD BLANK: 2048785 Associated Lab Samples: 92348113001 Parameter Units Tutal 8uspeiided Sulids iny1L LABUkA1 UkY CUN I FtUL SAMPLE: 2048786 Parameter Units Total Suspended Solids mglL Pace Analytical Services, LLG 9800 KinceyAve. Suite too Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water plank Reporting Result Limit Analyzed Qualifiers ND 2.5 OT119117 18:14 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 24B 99 90.110 SAMPLE DUPLICATE: 2048787 92348128001 Parameter Units Result Total Suspended Solids mg/L ND SAMPLE iLIPLICATE: 2048788 9234811B001 Parameter Units Result Total Suspended Solids mg/L ND Dup Result ND RPD Qualifiers Dup Result RPD Qualifiers ND Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 lacmnalyticale www.pacelabs.com Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369591 QC Batch Method: SM 5210B Associated Lab Samples: 92348113001 METHOD BLANK: 2047932 Associated Lab Samples: 92348113001 Parameter Units BOD, 5 day mg/L LABORATORY CONTROL SAMPLE: 2047933 Parameter Units BOD, 5 day mg/L SAMPLE DUPLICATE: 2047934 Parameter Units BOD, 5 day mg1L } Pace Analytical Services, LLC 11 9800 KinceyAve, Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM. 5210B Analysis Description: 5210B BOD, 5 day Matrix: Water Rlank Rpportin0 Result Limit Analyzed Qualifiers ND 2.0 07/24/17 09:13 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 197 99 84.6-115.4 92348113001 Dup Result Result RPD Qualifiers 26.9 35.3 27 D6 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 aceAnalytical mvw.pasolabs.com Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369924 QC Batch Method: SM 5220D Associated Lab Samples: 92348113001 METHOD BLANK: 2049917 Associated Lab Samples: 92348113001 Parameter Chemical Oxygen Deniand QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers rug/L ND 25.0 07/20/17 20:39 Pace Analytical Services, LLG 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 {704)875-9092 LABORATORY CONTROL SAMPLE: 2049918 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 773 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2049919 2049920 MS MSD 92347277007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 31.0 750 750 813 BOB 104 104 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2049921 2049922 MS MSD 92348319001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc- Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 642 750 750 1380 1360 98 96 90-110 1 Results presented on this page are in the units Indicated by the "Units" column except whore an alternate unit Is presented to the right at the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 aceAnalytical www.pacelabs.com QUALIFIERS Project: Monroe Stormwater Pace Project No.: 92348113 0:(;11i!I111116 IK Pace Analytical Services, LLC 9800KinceyAve. Suite100 Huntersville, NC 28078 (704)87&9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrog2tQ 1,2 Diphonylhydrazine docompocoe to and cannot be ceparated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and 12PD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 f • aceAnaljdical o www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Monroe Stormwater Pace Project No.: 92348113 Pace Analytical Serviees, LLC 9800 Kincey Ave. Suite100 I luntersville, NC 28078 (704)875.9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92348113001 MSW 02 92348113001 MSW 02 EPA1664B 370347 92348113001 MSW02 EPA200.7 369581 EPA200.7 370082 92348113001 MSW 02 SM 2540D 369720 92348113001 MSW 02 SM 5210B 369591 SM 5210B 369608 02340113001 MSW 02 SM 6220D 360024 Date: 07/2712017 05:03 PM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 �a,CeAnalj4ical' Laboratory receiving samples: Asheville ❑ Eden❑ Document Name: Document Revised: Sept,21, 2016 Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.01 Pace Quality Office Greenwood ❑ Huntersville.Q Raleigh❑ Mechanicsville❑ . Client Name; WO 9234811:3 Project III: _ 'Courier: Commercial ❑Fed Ex ❑UPS ❑USPS ❑Client ❑ ._Qpace ❑other: 923481111113 11I 1 11 Custody Seal Present? ❑Yes QNo Seals Intact? ❑Yes --[]No Date/Initials Person Examining Contents: 7 Packing Material: ❑Bubble wrap ❑Bubble Bags ❑None .•[Other: Thermorrieter: � cadet ❑❑ Blue None 05amples on ice, cooling process has begun —'❑ tR Gun ID: �_ Type of Ice: Correction Factor: Cooler Tamp Corrected CO _ , l • Biological Tissus Froxon? [:]Yes .[]No-- []N/A Term shnuld he above freeing to 6°C USDA Regulated Soil (,Q•N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, rlyeS lat,>n indudinQ Hawaii and Auprtn Ricol? MYes J_INA Comments/Discrepancy: Chain of Custody Present? .--E > a []NO ❑N/A I. Samples Arrived within Hold Time? V6s ❑No ❑N/A 2• Short Hold Time Analysis (<72 hr.)? .-Oyes ❑No ❑NIA 3• Rush Turn Around Time Requested? Oyes No ❑NIA 4• SufficiontVoltimo?' .(r]i(fea []No ❑N/A Correct Containers Used? -Pace Containers Used? JDYes -Yes ❑No ❑No ❑NIA ❑N/A Containers Intact? ,Dies ONO ❑NIA 7. Samples Field Filtered? []Yes Milo ❑N/A 8. Note if sediment is visible in the dissolved container . Sample Labels Match COO -Includes Date/iime/ID/Analysis ,QYes _l Matrix: j []No ❑NIA 9. Headspace in VOAViafs (>5-6mm)? ❑Yes []No -AgN%A 10. Trip Blank Present? Trip Blank Custody Seals Present? []Yes ❑Yes ❑No [:]No ©Wa/A ❑WIA' 11, rtIFNT NOTIFICATION/RE50LUTtON Person Contacted: Comment_/Sample Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: Field Data Roquirod? ❑YOL [--]No Date/Time: pate: Date: Note: Whenever there is -a discrepancy affecting North Carolina compliance samples, a copy of this form will be sentto the North Carolina DEHNR Certification Office (i.e: but of hold, incorrect preservative, out of temp, incorrect containers) .. . Page 12 of 14 b m m w 0 ~ Item# zzzzzzzBP4U-125 mL Plastic Unpreserved (N/A) (Cf-) BP3U-25C mL Plastic Unpresmed (N/A) BPZU-SOD mL Plastic Unpreserved (N/A) BP1U-1 liter Plastic Unpreserved (N/A) BP3S-250 mL Plastic H2504 (pH < 2) (CI-) BP314-250 mL plastic HNO3 (pH < 2) 13P3Z-250 mL Plastic ZN Acetate & NaOH (>9) BP3C-250 mi Plastic rJa7H (pH > 12) (Cl-) WGFU-Wide-meuth2d Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (NIA) (CI-) 'ZZZ" AGiH-1 liter Amber F.CI (pH < 2) AG3U-250nLAmber Cnpreserved(N/A)(Ci-) AG15-1 liter Amber H2SO4 (pH < 2) AG3S-250 rwL Arnber-H'_SO4 (pH < 2) AG3A(DG3A)-250 mLAmber NH4Cl (N/A)(CI-) VG9H-40 mL VOA MCI IN/A) vG9T-40 mL VOA Na2Sz03 (N/A) VG9U-40 rrr_ VC•A Unp iN/A) DG9P-40m,VCA H3PG4 (N/A) VOAK (6 vials per k1C,-5035 kit (N/A) V/GK (3 vials per kit)AMR/Gas kit (N/A) r SPST-225 mL Sterile Plastic (N/A — lab) SP2T-25C inLSterilePlastic (N/A— lab) BP3A-250 rr:L Plastic (NIH2)2504 (9.3-9.7) Cubitainer VSGU-20 ntL5c ntillaticn vials (N/A) GN 17 O Cr G S O m X D' S O. .r ro Cr O 0 in n X ru � w 2 3 v rD O ro ro ee � w � a Cr M CL m � v� 0 3 N 0 7 n' tA 3 T n O a' v 0 O + n n• F C w r a Zu 3 C m @ O n .. v 0 c 3 A CM M C > rn m O 0- N ro � � N N A v PaceAnalytical. ..Facelabsxom CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be Cornpleted :lccurate!y. Section A Section B Section C Page: of Required Client information: Required Project Inro—alion: Invoice Inlorn tin: Com �1 :rt/l�./ _ RepartTo: f Attention: /rJ 2176538 f /� i T� I� TI of m fy, Q �r ,[ t sO./ I Adtb 2 0 A spy To: ^, — cam n Narca: M / REGULATORY AGENCY' Addry3: . jeo,)e Q O j NPDES F GROUND WATER i DRINKING WATER r UST I-J RCRA i- OTHER Email To: Purchase Orclee No.: Paco Oeolo Reference: Project Na Pacc Projecyy}� I I' Site Lowlion / 7 Q�/rd E dr Manager, r h �r STATE: G Requested Due DaterrAT: FTolecl Number Pace Pr me n: Regtieste:d'Analysis Filtered (YIN) Section D Matrix Codes — E z Roqulradciioni Inlw tion MATRIX I CODE COLLECTED Preservatives s - Drinking Water DW U zO Water WT Waste Water WW Ia COtittvstTE cosnPuslYE U I i Product P siarrt �+mctva us J ~ Z SoillSolid SL m O' O Ui y V SAMPLE ID orl� QS�L v �; m N 0 (A-Z, 0.9 1,1 Air AR p � 4 4 Z I q/ Sample IDS MUST BE UNIQUE Tissue TS O U n- w ~ z Z �' A— U Other OT r O n of a �ALI' a a E a z tL a> g O c5 0 O v s ~ rn, DATE TIME DATE I TIMEN = S T z O '�' D= Pace Project No.) Lab I.D. wal wy Cr 1 7-)-6: V lit"t XI I I 1 11x z w Cr 7- 314x O Cr7- al 1 X X 4 w 0 �L I x srrbw 0 a. ;1 4 00__Albc Vj rr I X 1 6 7- 8 9 10 •1Z 12 A13DITIONAL COMMENTS RELINQUISHED BY / AFFILIATfON- DATE - TIME- -ACCEPTED BY I AFFILIAT.Ok DATE- TIME SAMPLE CONDITIONS S 1 r ��, d `� : a m Ir moon. ,04 4--13- 7: o ...�- ,� js;, t:[ � fi_ ��� y� ri F!r// Z.G. Y �� �1. ✓ F` 3-r%� ! i", I t: f � 61 m SAMPLER NAME -AND SIGNATURE U o u A ORIGINAL PRINT Name of SAMPLER: o 2. r m `—' } V u Y E d SIGNATURE of SAMPLER DATE Signed (MMIDD'YYt: — 7 a �, 'Important Note: gy sit ning taus IOttn you arc accepting P.xe's NET 30 day psyment tears rind agreeing to Into charges of 1.51. per mpIi for arty iweicrs Rol paid wiIN1. 30 days. F-ALL-0-020rev.07, 15-May-2D07 « a C `> aceAnalytical o www.pacelabs.com July 27, 2017 Mr. Joe Hinkle Allvac RE: Project: Monroe Stormwater Pace Project No.: 92348113 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on July 18, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of tho report. If you have any questions concerning this report, please feel free to contact me. Sincerely, F Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac David Pope, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 lacceAwn!1XicaI wwwpacelabs.cmi Project: Monroe Stormwater Pace Project No.: 92348113 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater CertiFlcation #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 Not tli Caiuliiia DiliMiig Walel CeiUncaduri #: 37712 .... ...... ...... ..... ....... ... ,..... ,...... CERTIFICATIONS South Carolina Certification #: 99006001 FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Cei tificatiui i #. 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 aceAnalytical WW.pacelebs.c= SAMPLE ANALYTE COUNT Project: Monroe Stormwater Pace Project No.: 92348113 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 {704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92348113001 MSW 02 EPA 1664E JMS 1 PASI-C EPA200.7 SER 5 PASI-A SM 2540D NAL 1 PASI-A SM 52104 ECM 1 PASI-A SM 5220D NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in futl, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 0 Pace Analytical Services, LLC aceAnalytieal ® 9800 Kincey Hunte svfle, NC128076 www.pacetabs.com (704)875-9092 ANALYTICAL RESULTS Project: Monroe Stormwaler Pace Project No.: 92348113 Sample. MSW 02 Lab ID: 92348113001 Collected: 07117/17 07:00 Received: 07/18/17 11:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By JM 1 07/17/17 07:02 Field Temperature 28.3 deg C 0.50 1 07/17/17 07:02 HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 07/25/17 06:08 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug/L 1.0 1 07/19/17 15:30 07/23117 08:14 7440-43-9 Chromium 10.7 ug/L 5.0 1 07/19/17 15:30 07/23/17 08:14 7440-47.3 Lead ND ug/L 5.0 1 07/19/17 15:30 07/23/17 08:14 7439-92-1 Nickel 74.8 uglL 5.0 1 07/19/17 15:30 07/23/17 08:14 7440-02-0 Zinc 459 ug1L 10.0 1 07/19/17 15:30 07/23/17 08:14 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 26.2 mg/L 8.3 1 07/19/17 18:17 5210B BOD, 5 day Analyticol Mellicid: SM 6210B BOD, 5 day 26.9 mg/L 2.0 1 07/19/17 06:30 07/24/17 09:13 06 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 124 mg/L 25.0 1 07/20/17 20:39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Hate: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 acMnalytical www.pacelabs.corn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 370347 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92348113001 METHOD BLANK: 2052116 Associated Lab Samples: 92348113001 Parameter Units Oil and Grease moll LABORATORY CONTROL SAMPLE: 2062117 Parameter Units Oil and Grease mglL Matrix: Water Blank Reporting Result limit Analyzed Qualifiers ND 5.0 07/25/17 06:07 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 40 36.8 92 78-114 MATRIX SPIKE SAMPLE: 2052118 92348428001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 38.0 95 78-1114 Results presented on This page are In the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aceAnalytical wwwpacelabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369581 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92348113001 METHOD BLANK: 2047905 Matrix: Water Associated Lab Samples: 92348113001 Blank Repuil.i Parameter Units Result Limit Analyzed Qualifiers Cadmium ug1L NO 1.0 07/23/17 07:03 Cluuuliurn uy1L NO 6.0 07/23/1707,03 Lead uglL NU 6.0 U1123111 0/:03 Nickel ug1L NO 5.0 07/23/17 07:03 Zinc ug1L NO 10.0 07/23/17 07:03 3_ Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersviRe, NC 26078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2047906 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium uglL 500 478 96 85-115 Chromium uglL 500 470 94 85-115 Lead uglL 500 468 94 85.115 Nickel uglL 500 468 94 85-115 Zinc uglL 500 476 95 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2047907 MS 92347968019 Spike Parameter Units Result Conc. Cadmium uglL NO 51 Chromium uglL NO 51 Lead uglL NO 51 Nickel uglL NO 51 Zlut: uy1L ND 51 2047908 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 482 471 96 94 70-130 2 500 493 464 99 93 70-130 6 500 494 459 99 92 70-130 7 500 474 462 95 92 70-130 3. 500 499 463 100 92 70-130 8 Qual MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2047909 2047910 MS MSD 92347941003 Spike Spike M5 MSD MS MSD °/a Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium uglL NO 500 500 453 465 91 93 70-130 2 Chromium uglL NO 500 500 447 458 89 92 70-130 2 Lead uglL NO 500 500 441 450 88 90 70-130 2 Nickel uglL NO 500 500 442 453 88 90 70-130 2 Zinc uglL NO 500 500 451 461 90 92 70-130 2 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the renult. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 r aceAnalj cal www.pecelabs.=n QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch; 369720 Analysis Method: SM 2540D QC Balch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92348113001 METHOD BLANK: 2048785 Associated Lab Samples: 92348113001 Parameter - Units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: 2048786 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 2048787 Parameter Units Total Suspended Solids mglL SAMPLE DUPLICATE: 2048788 Parameter Units Total Suspended Solids mglL Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (7C4)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 07/19/1718:14 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 248 99 90-110 92348128001 Dup Result Result ND ND 92348118001 Dup Result Result NO ND RPD Qualifiers RPD Qualifiers Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 acmnalytical www.pacefabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369591 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 92349113001 METHOD BLANK: 2047932 Matrix: Water Associated Lab Samples: 92348113001 Blank Repoi Lilly Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 07/24/17 09:13 1 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2047933 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 197 99 84.6-115.4 SAMPLE DUPLICATE: 2047934 92348113001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 26.9 35.3 27 D6 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 aceAnalXical www.pacetabs.mrn Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369924 QC Batch Method: SM 5220D Associated Lab Samples: 92348113001 METHOD BLANK: 2049917 Associated Lab Samples: 92348113001 Pairamoter Unite Chemical Oxygen Demand mq/L LABORATORY CONTR01. SAMPLE: 2049918 Parameter Units Chemical Oxygen Demand mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilre, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Reoult Limit Analyzed Qualifiers ND 25 0 07120/17 20.39 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 750 773 103 90.110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2049919 2049920 MS MSD 92347277007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Couu. Culic. Result Result % Rec % Roc Limits kPD (dual Chemical Oxygen Demand mg/L 31.0 750 750 813 808 104 104 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2049921 2049922 MS MSD 92348319001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone, Cone. Result Result % Rec % Rec Limits RPD Qua] Chemical Oxygen Demand mg/L 642 750 750 1380 1360 98 96 90-110 1 Resu is presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 acmnalytical mvw.pacelebs.com QUALIFIERS Project Monroe Stormwater Pace Project No.: 92348113 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, LLG 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration, Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPIJ - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenytamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration, Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANAIYTF QUAI,IFIFRS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07127/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 10'of 14 Pace Analytical Services, LLC aceAnalytica! 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 wrvw.pacelabs.cam (704 )875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Monroe Stormwater Pace Project No.: 92348113 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92348113001 MSW 02 92348113001 MSW 02 EPA 1664B 370347 92348113001 MSW 02 EPA200.7 369581 EPA200.7 370082 02348113001 MSW 02 SM 2540D 309720 92348113001 MSW 02 SM 5210E 369591 SM 52108 369608 92348113001 MSW 02 SM 5220D 369924 Date: 07/27/2017 05:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 all �5'ceAnalyicai` Laboratory receiving samples: Asheville ❑ Eden[—] Document Name: Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS•D33-Rev,01 Pace Quality Office Greenwood ❑ HuntersviII49— Raleigh❑ Mechanicsville[] . ,. Client Name; project: WO#� 92348113 • -T _ _ I j 'Courier: ❑Fed Ex ❑TIPS ❑USPS ❑Client O I III I II I II I II I�I �II T❑ Commerclal _]Pace ❑Other: 92348113 Custody Seal Present? ❑Yes QNo Seals Intact? []Yes - 'QNo Date/Initials Person Examining Contents: r -i Packing Material: []Bubble Wrap ❑Bubble Bags ❑None 20ther:��� Thermometer:_ -awet ❑Blue ❑None-ElSamples on Ice, cooling process has begun —[Q IR Gun ID: Type of Ice: Correction Factor: Cooler Temp Corrected (`C): '--? Biological. Tissue Frozen? ❑Yes .❑No-- ❑N/A Temp should be above freezing to VC USDA Regulated Soil M-N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {internationally, nvps indudine Hnwaii and Puerto Rico)? MYes _I:lNo-- Comments/Discrepancy: Chain of Custody Present? --BY-e-s ❑No [I N/A 1. Samples Arrived within Hold Time? QYds [_-)No El N/A 2. Short Hold Time Analysis (<72 hr.)? -©Yes ❑No ❑NIA 3. Rush Turn Around Time Requested? ❑Yes No ❑NIA 4. Sufficient Volume?' Dges []NO ❑N/A 5. Correct Containers Used? -Pace Containers Used? QYe-s -Yes []No ❑No [I NIA El N/A 6. Containers Intact? ©'r.s [:]No (-]N/A 7. Samples Field Flitered? Dyes .[ l o ❑N/A 8. Note if sediment is visible in the dissolved container Sample Labels Match COC? -Includes Date/Time/lD/Analysis Matrix: I _2Yes ! - [:]No [--]N/A 9. Headspace in VOA Vials (>5-6mm)? ❑Yes ❑No __QN/A 10. Trip Blank Present? Trip Blank Custody Seals Present? Dyes ❑Yes ❑No ❑No [ kI/A ❑N/A 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comment:;/52mple Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: Field Data Required? ❑Yes ❑No Date/Time: date: I cl I I Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, Incorrect containers) ., Page 12 of 14 m ED Co w 0 LO Ln A �PaceAnalXical - WwW.Pac iI2b3,Cete CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be Comgleted accurarely. Section A Section B Section C Page: of Required Client Information: Required Project Information: tnvaice Infornalien: Com d! 4__ i RaportTo: f /� Attention:�r fF 2176538 M N /\ �A%s�A1 [, p/ ]_%Q,►lT !lJink CopyTa: �, r a Com q Namo: U /[ ,;�}REGULATORY-AGENCY. Addry ' �x a O f NPDES I GROUND WATER F DRINKING WATER f UST f- RCRA I-OTHERRole Email To: Purchase Order No.: Pace Ounta renw: Project Na rd � d j� P,1ce Pmj Man7�s: A A fJ Site Location TE; C. Requested Due DatefTAT: Project Nuper. m Paco Profile Regtuesled'Analysis'Filtered (YIN)' Section D Matrix Codes a z Roquired Client Inlonnalion MATRIX ! CODE _ - a. COLLECTED Preservatives 3-- Drinking Water DW U Oz Water WT Waste Water Ww $ �j m C�n��E Product P _ p�y,B Z Soil/Solid SL [7 ,p y } SAMPLE ID r �; h cr m ,mil pe ,OL (A-Z, 0.9 ! ,-} Air AIRz � m 1•- o Sample IDs MUST BE UNSO_UE Tissue TS O U a LU F Z H U Other OT r .� .8 o = ,,, O PN C ..�' .,� t' V tf+ 7 �a3�srlt3 I a a n D — O �; m r m N y z co s • ~ DATE TIME DATE TIME S S z Z 2 D & 0-1 pace Project No./ Lab I.D. �D �r 2 (0 0 ;L- G 7- - 1 I IX I I II I I I I II 3 rn3w o ;). G 7• .A 1 191 a W 0 .�L - :Od 1 X 6 7 8 9 t0 11 +fl+ 12, LL ADDITIONAL COMMENTS RELINQUISHED BY! AFFILIATION DATE TIME ACCEPTED BY.! AFFILIATI7N DATE' TIME SAMPLE CONDITIONS ir.T l$, o`aJ TPAOM Yr OR G -1 $- 7: 0 T lei? A = m SAMPLER NAME AND SIGNATURE m OF:IGWAL PRINT Name of SAMPLER: 'A A u '- E in SIGNATURE of SAMPLER DATE Sianed (mmmryy 7 ~ Ql 'Important Nele: By signing this form you are accepting Puce. NET 30 d.,,y pa�ment t- nrd a lr eing to t7ta chnrltos of 7.5:: Per mo# Ion airy :.tor n not paid AtFvn 30 days. F-ALL-Q-020rev.07, 15-May-2007 0