NCS000329_MONITORING INFO_20181212

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
D�Z�
DOC TYPE
❑ FINAL PERMIT
-�-MON#TORING REPORTS-- - - - - -- - -
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ vy • IZ- lZ
YYYYM M D D

AAT1
November 28, 2018
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
RECEIVED
DEC 12 2018
CENTRAL FILES
DWR SECTION HARD
Y.O. Box 5030
2020 Ashcraft Avenue
Monroe, NC 28111-5030
Phone: [phone]
Fax: [phone]
Frnail: [e-mail]
Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period
Sample Number
Start
End
Year 9 — Period 2
18
September 1, 2018
February 28, 2018
Analytical monitoring includes:
• Outfall #01 (B), commingled stormwater
• Outfall #02 (B), non -commingled stormwater
• Outfall #03 (B), non -commingled stormwater
• Non Contact Cooling Water #1 - 48
If you have any questions or need additional information, please contact me at 704-289-45 11.
Thank you.
Sincerely,
Sc yan
Environmental Manager

AllVae - Bakers Plant ATI. A(Ivac
Siminwa.ter Monitoring Report. )~ omi
Sample Date. � I/'3Y2
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Resents of Sample Analysis:
Sample Time: (o -/�.
torrnwater Discharge Outfail #01 (Commune
Drainage Area = 2,9I 5A70N. ft. = 69 acres
% Impervious = 34%
P~:e? Pa���/ate C/o�fa
�ac2 �aTuf'ca�
40 CFR Part 136
Parameter
Results (mg/i)
Benchmark Values (mg/1)
BOD
D
30
COD
120
TSS
y
100
Cadmium
D
0.001
Chromium, total recoverable
D
1
Copper, total recoverable
a
0.007
Nickel, total recoverable
Qs
0.26
Zinc, total recoverable
O Q
0.067
Oil and Grease
20
Temp (receiving stream)
(deg C)
32 (deg C)
Total Residual Chlorine
S
0.017
pH
(std units)
6-9 (std units)
Storm Date:1/_ -s-/� Storm Duration: 3• S (Hrs.) Inches of Rainfall: AS
Duraflon of time preceding rain event exceeding 0.1": Aga (Hrs.)
Estimated flow Calcination:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) = (A x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches raWl2inches/fi. x 69 x .34)
Q(Total= cis) = 1.5 180 x /. 8 (Inches of rain) + 1.7595 x AS (Inches ©f rain)

aceAnalytrcal "
www.pacWbs.cw
November 14, 2018
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Dear Scott Ryan:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Joe Hinkle, Allvac
David Pope, Allvac
REPORT OF LABORATORY ANALYSIS
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(�IacAe.Analytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
CERTIFICATIONS
Project SW OUTFALL #01(8)
Pace Project No.: 92405880
Charlotte Certlification IN
9800 KinceyAve. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NEtAP Certification # LA170028
FloridaINELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification M 84
North Carolina Field Services Certification #: 5342
V rginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification ID8
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: SW OUTFALL #01{B}
Pace Project No.: 92405880
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID
Sample lb
Method
Analysts
Reported
Laboratory
92405880001
8SW01
EPA 200.7 Rev 4.4 1994
SH1
5
PASI-A
92406880002
BSW01
EPA 1664B
JMS
1
PASI-C
92405880003
8SW01
SM 5220D-2011
GC
1
PASI-A
92406880004
BSW01
SM 521OB-2011
SMK
1
PAS1-A
92405880005
BSW01
SM 254OD-2011
CEH
1
PAS1-A
92405880006
BSW01
SM 4500-CI G-2011
MDW
1
PASI-A
f
REPORT OF LABORATORY ANALYSIS
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aceAnalj cal
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #01(8)
Pace Project No.: 92405880
Sample: BSW01 Lab Il]: 92405880001 Collected: 11/05/18 06:21 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Cadmium
ND
uglL
1.0 1
11/06/18 05:44
11/08/18 23:46
7440-43-9
Chromium
ND
uglL
5.0 1
11/06118 05:44
11/08/18 23:46
7440-47-3
Copper
45.2
ug/L
5.0 1
11/06/18 05:44
11/08/18 23:46
7440-50-8
Nickel
5.1
uglL
5.0 1
11/06/18 05:44
11/08/18 23:46
7440-02-0
Zinc
12.7
ug1L
10.0 1
11/06/18 05:44
11/08/18 23:46
7440-66-6
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvil$e, NC 28078
[phone]
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Sample: BSW01 Lab ID: 92406880002 Collected: 11/05/18 06:19 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data
Collected By
Collected Date
Collected Time
pH
Temperature
HEM, Oil and Grease
Oil and Grease
Date: 11/14/2018 04:06 PM
Analytical Method:
DPJ
11/05/18
06:14
6.8 Std. Units
16.1 deg C
Analytical Method: EPA 1664E
ND mglL
1
11/05/18 06:21
1
11/05118 06:21
1
11/05/18 06:21
0.10 1
11/05/18 06:21
0.50 1
11/05/18 06:21
4.8 1
11114/1805:03
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW01 Lab ID: 92405880003 Collected: 1110511 a 06:18 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 522OD-2011
Chemical Oxygen Demand 33.1 mg1L 25.0 1 11/08/18 19:11 11/09/18 00:07
Date: 11/14/2018 04:06 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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(�Iacmnaljftal"
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #01(9)
Pace Project No.: 92405880
Sample: BSW01 Lab lD: 92405880004 Collected: 11/05/18 06:17 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
52108 BOD, 5 day Analytical Method: SM 521OB-2011
BOD, 5 day NO mg1L 2.0 1 11/06/18 19:07 11/11/18 13:37 B3
Date: 11/14/2018 04:06 PM
REPORT OF LABORATORY ANALYSIS
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(�IaneMalXicale
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ANALYTICAL RESULTS
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Pace Analytical Services. LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW01 Lab ID: 92405880005 Collected: 11/05/18 06:15 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 254OD-2011
Total Suspended Solids 16.4 mg/L 5.0 1 11/08/18 00:47 D6
Date: 11/14/2018 04:06 PM
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SW OUTFALL #01(8)
Pace Project No.: 92405880
Pate Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW01 Lab ID: 92406880006 Collected: 11105/18 06:22 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500CL G Chlorine, Residual Analytical Method: SM 4500-Ci G-2011
Chlorine, Total Residual 0.045 mg/L 0.024 1 11/07/18 18:21 7782-50-5 H3
Date: 11/14/2018 04:06 PM
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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QUALITY CONTROL DATA
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
OC Batch: 442144 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92405880002
METHOD BLANK: 2427246
Associated Lab Samples: 92405880002
Parameter Units
Oil and Grease mg/a_
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 4.8 11/14/18 04:51
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2427247
Spike LCS
LCS
% Rea
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg1L
38.5 36.8
96
78-114
MATRIX SPIKE SAMPLE:
2427248
92405492004 Spike
MS
MS
% Rea
Parameter
Units
Result Conc.
Result
% Rea
Limits Qualifiers
Oil and Grease
mg/L
NO 38.5
39.0
101
78-114
Results presented on this page are In the units indicated by the "Units' column except where an aPoemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
QC Batch: 440463
QC Batch Method: EPA 200.7 Rev 4.4 1999
Associated Lab Samples: 92405880001
METHOD BLANK: 2419374
Associated Lab Samples: 92405880001
Parameter
Cadmium
Chromium
Copper
Nickel
Zinc
QUALITY CONTROL DATA
Analysis Method: EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET
Matrix: Water
Units
Blank
Result
Reporting
Limit
Analyzed
ug1L
ND
1.0
11/08/18 23:12
ug1L
ND
5.0
11/08/18 23:12
ug1L
ND
5.0
11/08/18 23:12
ug1L
ND
5.0
11/08/18 23:12
ug1L
ND
10.0
11/08/18 23:12
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2419375
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Cadmium
ug1L
500
480
96
85-115
Chromium
ug1L
500
484
97
85-115
Copper
ug1L
500
499
100
85-115
Nickel
ug1L
500
478
96
85-115
Zinc
ug1L
500
467
93
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2419376
2419377
MS
MSD
92405896001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug1L
ND
500
500
503
500
101
100
70-130
1
Chromium
ug1L
ND
500
500
506
504
101
100
70-130
0
Copper
ug/L
0.0053
500
500
521
519
103
103
70-130
0
mg1L
Nickel
ug1L
ND
500
500
493
490
98
97
70-130
1
Zinc
ug1L
0,011
500
500
502
499
98
98
70-130
1
mg1L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2419378
2419379
MS
MSD
92405904001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug1L
NO
500
500
498
501
100
100
70-130
1
Chromium
ug1L
NO
500
500
503
504
101
101
70-130
0
Copper
ug1L
NO
500
500
510
514
102
103
70-130
1
Nickel
ug1L
NO
500
500
490
494
98
98
70-130
1
Zinc
ug1L
0.014
500
500
497
499
97
97
70-130
0
mg/L
Results presented on this page are in the units Indicated by the -Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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lacmnalyfical"
www.pacelabs,con;
QUALITY CONTROL DATA
Project: SW OUTFALL#01(B)
Pace Project No.: 92405880
Pate Analytical $orvices, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 440996
Analysis Method: SM 254OD-2011
QC Batch Method: SM 2540D-2011
Analysis Description: 25401) Total Suspended Solids
Associated Lab Samples: 92405880005
METHOD BLANK: 2421944
Matrix: Water
Associated Lab Samples: 92405880005
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND 2.5
11/08/18 00:38
LABORATORY CONTROL SAMPLE: 2421945
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 244
98 90-110
SAMPLE DUPLICATE: 2421946
92405900003 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg1L
27.8 31.0
11 D6
SAMPLE DUPLICATE: 2421947
92405880005 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg1L
16A 18.2
10 D6
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
QC Batch: 440961
QC Batch Method: SM 4500-CI G-2011
Associated Lab Samples: 92405880006
METHOD BLANK: 2421856
Associated Lab Samples: 92405880006
Parameter Units
Chlorine, Total Residual mg/L
QUALITY CONTROL DATA
Analysis Method: SM 4500-CI G-2011
Analysis Description: 4500CL G Chlorine, Total Residual
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.024 11/0711815:16
SAMPLE DUPLICATE: 2421857
92405880006 Dup
Parameter Units Result Result
Chlorine, Total Residual mg/L 0.045 0,041
RPD Qualifiers
9 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this pegs are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 11 J14f2018 04:06 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
OC Batch: 440600 Analysis Method: SM 521OB-2011
QC Batch Method: SM 521 OB-2011 Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 92405880004
METHOD BLANK: 2420066
Associated Lab Samples: 92405880004
Parameter Units
BOD, 5 day mg1L
LABORATORY CONTROL SAMPLE: 2420067
Parameter Units
BOD, 5 day mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 11/11/18 13:26 B3
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 192 97 84.6-115 B3
SAMPLE DUPLICATE: 2420068
92405881001 Dup
Parameter Units Result Result
BOD, 5 day mg/L ND ND
RPD Qualifiers
B3
Results presented on this papa are In the units indicated by the 'Units' column except where an pltemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/14/2018 04:06 PM without the written consent of Pace Analytical Services, LLC,
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acmnalytical
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QUALITY CONTROL DATA
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Pace Analytical Services, i_LC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 441148
Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011
Analysis Description: 5220D COD
Associated Lab Samples: 92405880003
METHOD BLANK: 2422559
Matrix: Water
Associated Lab Samples: 92405880003
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0
11/09/18 00:04
LABORATORY CONTROL SAMPLE: 2422560
Spike
LCS
LCS % Rec
Parameter Units
Cone.
Result
% Rec Limits
Qualifiers
Chemical Oxygen Demand mg/L
750
757
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422561
2422562
MS
MSD
92406236003
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Cone,
Cone. Result
Result % Rec
% Rec
Limits
RPD Qual
Chemical Oxygen Demand mg1L 107
100
100 216
216 109
109
90-110
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422563
2422564
MS
MSD
92405876001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rec
% Rec
Limits
RPD Qual
Chemical Oxygen Demand mg1L ND
100
100 130
133 113
116
90-110
2 M1
Results presented on this page are in the units Indicated by the 'Units- column except where an alternate unit Is presented to the right of the result_
REPORT OF LABORATORY ANALYSIS
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Date: 11/14/2018 04:06 PM without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
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aceAnalyifical ® 9800Hun ersv Ile, NC 28078
wwwpacalabs.cam [phone]
QUALIFIERS
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit,
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a speck matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DU - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B3 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW OUTFALL #01(13)
Pace Project No.: 92405880
Lab ID
92405880002
92405880002
92405880001
92405880005
92405880006
92406880004
92405880003
Sample ID
BSW01
BSWo1
BSWo1
BSW01
BSW01
BSWo1
BSW01
Date: 11/14/2018 04:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
QC Batch Method QC Batch Analytical Method Batch
EPA16649
442144
EPA 200.7 Rev 4.4 1994
440463
SM 2540D-2011
440996
SM 4500-CI G-2011
440961
SM 52109-2011
440600
SM 5220D-2011
441148
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
EPA 200.7 Rev 4.4 1994 440492
SM 521OB-2011 440712
SM 5220D-2011 441293
Page 17 of 20

Document Name:
Document Revised: February 7, 2018
c�CB�ficir<�,tlCcijn
1+
Sam ie Condition Upon Recei t(SCUR)
-Page 1 of 2
Document No.:
issuing Authority:
F•CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[_Greenwood ❑
Client Name:
Courier: ❑Fed Ex UPS []LISPS
❑ Commercial []Pace [-]Other:
—
Custody Seal Present? Dyes ❑No Seals Intact? Oyes
Huntersvllle ❑" Ralelgh❑ ❑ Mecchanicsville
Project p WO : 92405880
]Client
�1�
.❑i ND �•
Date/Initials Person Examining Contents:
Packing Material: []Bubble wrap ❑Bubble Bags ©None ❑ Other Biological Tissue Frozen?
[]Yes❑No QN/A
Thermometer:/ 92TO45 Type of Ice: j]wet ❑eiue ❑None
�IR Gun 10:
n
Cooler Temp I'Cj: '- . '] Correction Factor: Add/Subtract ('C)
Tem
p should be above freezing to 6'C
Cooler Temp Corrected ('Cl: --' ( , ) ❑Samples out of temp crileria. Samples on ice, cooling proce5s
hasLegun
USDA Regulated Sall ( N/A, water sample)
Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? DId samples originate from a foreign source (internationally,
i—iVPc nNn inrindina Hawaii And PaPrtn Rirel? rlYnc Finn
Comments/0iscre ane :
Chain of Custody Present?
Ov
QN0
N/A
1.
Samples Arrived within Hold Time?
Yeas
ONO
NIA
2.
Short Hold Time Analysis Jc72 hr.?
QYes
No
❑N/A
3.
Rush Turn Around Time Requested?
QYes
F
QNo
❑N/A
4.
Sufficient Volume?
� . Yes
Na
❑NIA
S.
Correct Containers Used?
i{:Xes
[]No
❑NIA
6,
-Page Containers Used?
M Yes
[]No
❑N/A
1
Containers intact?
Dyes Yes
NO
N/A
7.
Dissolved analysis; Samples field Filtered?
Oyes
QNO
. !A
S.
Sample Labels Match COC?
❑Yes
[]No
❑NJA
4.
iJ
✓ehl)/Ana1
-includes Date/Timsis Matrix:
Heads pace in VOA Vials (?5.6mm)?
OYes
QNo
r
0N A
10.
Trip Blank Present?
❑Yes
❑No
[Jh/A
11.
Trip Blank Custody Seals Present?
❑Yes
No
NJA
COMMENTS/SAMPLE DISCREPANCY field Data Required? []Yes [-]No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: kt Date:
Project Manager SRF Review: Date: r
Page 18 of 20

Document Name:
document Revised: February 7, 2018
aceArjWical •
Sample Condition Upon Recel t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is Project It Wp# : 92405880
verified and within the acceptance range for preservation PM: rives Due Dale: 11/14/18
samples.
Exceptions: VOA, Whim, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg CLIENT: 92-A 11 vae NC
"Bottom calf of ox s to list number of bottle
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon recelpt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 0
Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Cenifleatlon Office (Le.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 19 of 20

Stormwater Monitoring
Chain of Custody Record
Project Number/Name:
SW Outfall #Q1(B)
Project Location: ATI SM - Bakers
Sample 's Si nature:
Date: /-
e.
o
v
c
aV
U
F
Fr
y
Requested Test Parameters
E k
E-
U
>
U
..
F.,
a.
G
G /®
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc
G
G /(D
HNO3
Y
Cadmium
G
/ 1'
HCL
Y
Oil &-, Grease o
G
G /�O
H2SO4
Y
ICOD t,o
G
G Im
None
Y
BOD U
G
G /d)
None
Y
TSS Jv
G
I G /d)
None
Y
Residual Chlorine
Onsite Field eH Analysis
Onsite Field Temperature Anal sis
pli: _�.8 (s.u.)
Sample Time: (•/y,..
Temp: 16. r (*Q Sample Time: 6% ,�
Analysis Time:
.a%.
Analysis Time:
Meter Calibrated: es
Thermometer Calibrated: / N
Sampling and field an, lysis completed by:,
Relinquished By: 6 I7
Received y. k-t-rf.A
Date: /`
Time: r'.` v
!
Date: j j- ;- t Y
Time: (� fU
Relinquished By-.
Received By:
Date:
Time:
Date:
Time:
EHS-SW-Chain of Costody Outfall 01-Rev 001 Page 20 of 20

OATI AElvac
Alivac - Bakers Plant
Stornlwater Monitoring Re ort Form
Sample Date:
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Sample Time: A D.�a..-
Stormwater Discharge Outfall#02 (Non-Commin led
Drainage Area = 212 952s . ft. = 4.9 acres
% Impervious = 12%
Doviol &t Tr X&a rkah
Race
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
-ALD
30
COD
3Ot
120
TSS
a
100
Cadmium
ND
0.001
Chromium, total recoverable
605,
1
Copper, total recoverable
, OS
0.007
Nickel, total recoverable
D
0.26
Zinc, total recoverable
,y
0.067
pH
(std units)
6-9 (std units)
Storm hate: //-;A Storm Duration: 347 "s.) Inches of Rainfall: 1
Duration of time preceding rain event euceeding 0.1": / U - (Hrs.)
Estimated Flow Calculation:
Q=CM
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) = (A x inches rain/12 inches/ft. x 4.9 acres x .88) + .9 x inches rain/12inches/R. x 4.9 x. 12)
Q(Total, cfs) = 0.1437 x _ /. 8_ (Inches of rain) + 0.0441 x AS (Inches of rain)
cfs

e
aceAnalytical
mnvpace+a6stom
November 12, 2018
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW OUTFALL #02(B)
Pace Project No.: 92405881
Dear Scott Ryan:
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNVNELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me_
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Joe Hinkle, Allvac
David Pope, Allvac
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of Pace Analyticat Services, LLC.
Page 1 of 13

s
aceAnalytical
mvwpaculabs.com
Project: SW OUTFALL#02(B)
Pace Project No.: 92405881
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification A 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NEIAP Certification #: E87627
Kentucky UST Certification M 84
VirginiaNELAP Certification M 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification M 99030001
VirginiaNELAP Cert[fication #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 2 of 13

9
aceAnalytical
—Pacelabs cam
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 knceyAve, Suite 100
Huntersville, NC 28078
[phone]
Project: SWOUTFALL#02(B)
Pace Project No.: 92405881
Analysts
Lab ID Sample ID Method Analysts Reported Laboratory
92405881001 BSW02
EPA 200.7 Rev 4.4 1994
SH 1
5 PASI-A
SM 254OD-2011
CEH
1 PASI-A
SM 521OB-2011
SMK
1 PASI-A
SM 52200.2011
GC
1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC, Page 3 of 13

w
aceAnalytical
ww�vpateiabs.torrr
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #02(B)
Pace Project No.: 92405881
Sample: BSW02 Lab ID: 92405881001 Collected: 11/05/18 06:07 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
Field Data
Analytical Method
Collected By
DPJ
1
11/05118 06:10
Collected Date
11105118
1
11/05118 0610
Collected Time
06:04
1
11/05/18 06:10
pH
6.9 Std. Units
0.10
1
11/0511806:10
Temperature
16.6 deg
0.50
1
11/0511806:10
200.7 MET ICP
Analytical Method: EPA 2003 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Cadmium
ND ug1L
1.0
1
11/06/15 05:44
11/05/18 2149
7440-43-9
Chromium
5.0 uglL
5.0
1
11/0611805:44
11/081182149
7440-47-3
Copper
50.0 ug1L
5.0
1
11/06/18 05:44
11/08/18 23:49
7440-50-8
Nickel
ND uglL
5.0
1
11/06/18 05:44
11/08118 23:49
7440-02-0
Zinc
42.2 uglL
10A
1
11/0611805:44
11/0811823749
7440-6"
2640D Total Suspended Solids
Analytical Method: SM 25400-2011
Total Suspended Solids
21.8 mg1L
2.5
1
11/08118 WAS
5210E BOD, 5 day
Analytical Method: SM 521 OB-2011
BOD, 5 day
ND mg1L
2.0
1
11/06/18 19:07
11/11/18 13:33
133
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
30.8 mg1L
25.0
1
11/08/18 19:11
11/09/18 00:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 13

ceAnalytical
wwwpacelabs.com
I
QUALITY CONTROL DATA
Project, SW OUTFALL 902(8)
Pace Project No.: 92405881
Pace Analytical Services, LLC
9800 KinceyAve. Suite t00
Huntersville, NC 28078
[phone]
QC Batch: 440463
Analysis Method:
EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Description:
200.7 MET
Associated Lab Samples: 92405881001
METHOD BLANK: 2419374
Matrix:
Water
Associated Lab Samples: 92405881001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug/L
NO
1.0
11/08/18 23:12
Chromium
ug/L
NO
5.0
11/08/18 23:12
Copper
ug/L
NO
5.0
11/08/18 23:12
Nickel
ug/L
NO
5-0
11/08118 23:12
Zinc
ug/L
NO
10.0
11/08/18 23:12
LABORATORY CONTROL SAMPLE:
2419375
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Cadmium
ug/L
500
480
96 85-115
Chromium
ug/L
600
484
97 85-115
Copper
ug/L
500
499
100 85-115
Nickel
ug1L
500
478
96 85-115
Zinc
ug/L
500
467
93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419376
2419377
MS
MSD
92405896001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result % Rec % Rec
Limits
RPD Qual
Cadmium
ug/L
NO
500
500
503
500 101 100
70-130
1
Chromium
ug/L
NO
500
500
506
504 101 100
70-130
0
Copper
ug/L
0-0053
500
500
521
519 103 103
70-130
0
mg/L
Nickel
ug/L
NO
500
500
493
490 98 97
70-130
1
Zinc
ug/L
0.011
500
500
502
499 98 98
70-130
1
mg1L
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2419378
2419379
MS
MSD
92405904001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Resuft
Result % Rec % Rec
Limits
RPD Qual
Cadmium
uglL
NO
500
500
498
501 100 100
70-130
1
Chromium
ug/L
ND
500
500
503
504 101 101
70-130
0
Copper
ug/L
ND
500
500
510
514 102 103
70-130
1
Nickel
ug/L
ND
500
500
490
494 98 98
70-130
1
Zinc
ug/L
0.014
500
500
497
499 97 97
70-130
0
mg/L
Results presented on this page are In the units indlcatsd by the'Untis' column except when an ahemete unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 13

aceAnalytical
trww.pacelaW.oam
QUALITY CONTROL DATA
Paco Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL 902(S)
Pace Project No.: 92405881
QC Batch: 440996
Analysis Method:
SM 254OD-2011
QC Batch Method: SM 254OD-2011
Analysis Description:
25400 Total Suspended Solids
Associated Lab Samples: 92405881001
METHOD BLANK: 2421944
Matrix: Water
Associated Lab Samples: 92405881001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 11/08/18 00:38
LABORATORY CONTROL SAMPLE: 2421945
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 244
98 90-110
SAMPLE DUPLICATE: 2421946
92405900003 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
27.8
31.0 11 D6
SAMPLE DUPLICATE: 2421947
92405880005 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
16.4
18.2 10 D6
Results presented an thin papa are In the units Indicated by the'Unils' column except where an alternate unit Is presented to the right of the result
.REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

aceAnalytical
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1
i
QUALITY CONTROL DATA
Project: SW OUTFALL #02(6)
Pace Project No.: 92405881
QC Batch: 440600 Analysis Method: SM 521 OB-2011
QC Batch Method: SM 521 OB-2011 Analysis Description: 521OB BOD, 5 day
Associated Lab Samples: 92405881001
METHOD BLANK: 2420066 Matrix: Water
Associated Lab Samples: 92405881001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
BOD, 5 day mg/L ND 2.0 11/11/18 13:26 B3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2420067
Spike LCS LCS % Roe
Parameter Units Cone. Result % Rec Limits Qualifiers
BOD, 5 day mg/L 198 192 97 84.6-115 B3
SAMPLE DUPLICATE: 2420068
92405B81001 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg/L ND ND B3
Results presented on this page are in the units indicated try the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 13

aceAnaIXical e
www.pecelabs.cw
I
Project: SW OUTFALL 002(B)
Pace Project No.: 92405881
OC Batch: 441148
QC Batch Method: SM 5220D-2011
Associated Lab Samples: 92405881001
METHOD BLANK: 2422559
Associated Lab Samples: 92405881001
Parameter Units
Chemical Oxygen Demand mg/L
QUALITY CONTROL DATA
Analysis Method: SM 5220D-2011
Analysis Description: 5220D COD
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 25.0 11/09/18 00:04
Pace Analytical Services, LLC
9800 IGncey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2422560
Spike LCS LCS °% Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 757 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422561 2422562
MS MSD
92406236003 Spike Spike MS MSO MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result e% Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 107 100 100 216 216 109 109 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422563 2422564
MS MSD
92405876001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L ND 100 100 130 133 113 116 90-110 2 M1
Results presented on this page are In the units Indicated by the'Unh' column except where an alternate unit is presented to the right of the reaulL
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full.
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, LLC
Page 8 of 13

aceAnalytical e
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I �
QUALIFIERS
Project: SW OUTFALL #02(B)
Pace Project No.: 92405881
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroelhylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Arralylical is TNI accredited. Contact yuur Pace PM rut lire current list ur accredited w alytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B3 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M/ Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

Pace Analytical Services, LLC
1�55'cieARalytr'cals 9800lGnceyAve. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
( i
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW OUTFALL#02(B)
Pace Project No.: 92405881
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92405881001
BSW02
92406881001
BSW02
EPA 200.7 Rev 4A 1994
440463
EPA 200.7 Rev 4.4 1994
440492
92405881001
BSW02
SM 2540D-2011
440996
92405881001
BSW02
SM 521OB-2011
440600
SM 521OB-2011
440712
92405881001
BSW02
SM 5220D-2011
441148
SM 5220D-2011
441293
IeFi{�iiliF7fItSGItiifiill,T,
REPORT OF LABORATORY ANALYSIS
This report shag not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC,
Page 10 of 13

aLCAV641Cal
Documem Name:
Sam a Condltlen tl Rrcel t(SCl1Ri
Dow"M ReNscd: Febrvasv 7, 2018
PM 1 o1 ]
Doctsmeet No:
IswinSAvtherity:
'CAR-CS-033�1ev.06
Pace O.Mat Q.a6 OHice
•Check mark top haft of box if pH and/or dechtorfnation Is
verified and within the acceptance ranee for preservation
samples.
E.ceptienr. VOA, [alifolm, TOC, as and Grease, DROlrA15 SwatI fR]C, like
•*Bottom half of box is to list number of battle
Praiet WO# 92405881
PM: MNB Due hate: 11/14/10
CLIENT: 92-AiLvao NC
gas
a
0
an
on
ME
OPEN
0
11
NO
so
LEINE
Boom
M
M
0
mi.
ON
M
WON
ME
on
Monson
on
PH Adjustment log for Preserved Samples
taeple la
Typo of PrlselYatMa
PH yppn ttcelpt
WnPnNtealWa WOW
rYnepraemtba
wlwt.f
Pmeunt Or►m"—Uw
.dried
left
Hete: Whtnrer three lcad.tM.Myaftalnt HannCarobnacen+P"—nnyn,acopy or lmt.orm n., uexn�w the
Ore hold, umnaa pr _rin. wl of wM% IKprntt T¢nuwr .
Pepe 12 of 13

66
1
Stormwatcr Monitories
C-hain-of-Custody Record__
Project Number/Name:
SW Outfall #02 B
Project Location: ATI SM - Bakers
Sample 's Sinature:
Date: ^S^
BA
Q
Requested Test Parameters
[—
i
O
n ,�
C6
c
l-S- B
G
G 1
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc
ID._
G
G /0
HNO3
Y
Cadmium
G
G I43
H2SO4
Y
COD
-'D7�
G
G /d}
None
Y
BOD
6 OS
G
G !4)
None
Y
TSS
Onsite Field pH Analysis
Onsite Field 'I'em erature Analysis
pll: 6. 9 - (s.u-)
Sample Time: G -,o
Temp: s s _ (*Q Sample Time: 6 03�
Analysis Time: 6.-10—
Analysis Time: 6 ;03,
Meter Calibrated:
Thermometer Calibrated: / N
Sampling and field anal sis completed bv:
� '
Relin uished By:
Received
Date: - /
Time: G?A
Date: H- ci-t Y Time: `l Sl=
Relinquished 13 :
Received By:
Date:
'rime:
Date: Time:
EHS-SW-Chain o1 Costody Outten 02•Rav 001 page 13 or 13

Docunstrn Name:
Sa le CmeAtlan 1.4mon fltcd t(SCURJ
Document Rt"fed: February 7, 2019
Psige l M 2
4pcumene Na-:
F-CAR-CS•0i3-Rty.03
Issuing Authority:
Pace "Its," ds Qwnty Omre
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvitleg Raleigh❑ Mechardesville❑
Pr_tl_Wa WO# : 9lf2405881
❑Commerdal ❑PKeEN Uvs ❑aOUSPS
her:_ 'Client �92405881
Custody Simi Pretest] ❑Yes ❑LNo Se41a1s118ct7 ❑res ❑no I1-r
onelssmaa Pawn FrAntmay Ca.senp''-`t 1 f 1 �/
►aekN Matertal: [3Bubble Wrap ©Subtle gas' D14one ❑ Other Btoogk2i Tlque Rgien?
Thermomertj - ❑yes Cye9 ❑H/A
{7IR 91T045 FYaeeflrr Owes ❑awe Off"
Coder Temp(*Qj l�'l 5 Correction Fartor:AddjSubvact CC1 -nl Tempshould tx atwrt freeanR so 6'C
Coder Temp C—eeted M: - r_ L I-_ ❑smn�aL wr ettemvern:rta. sFmP4e on ir:, wel�nt wean
his "sun
USDA Regilated FP If (E] NIA watr samptel
dd Famrvres mipnate In a 9uaimme zone witldn the Untied lutes: CA, NY, er SCicbeck maps)? Did saNpat s W"sne Irnm a f.Wip, soLece ItmIna0-11v,
F-11— M.. I l— FINS.
Cammenlf/dscrew
r
Chain alCustod Present?
- n
nP
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L.
/
Sam las lamed khi. Hold Time?
ON.
DWIA
2.
Short Held ttme Ana b 102 In.?
era
Nc
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1
Rush Turn Around Time untetl7
-
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i
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'17rn
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-Para CPRtanrerT Lh d?
YO
N9
xIA
Containers knta[t?
Oh,
UNIA
7.
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- NIA
a.
Sample iahels Makeh CDC?
�I�,d
cl4-
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❑WA
9.
•InUudet Oate/Time Dona is M.0m
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s WA
10
Trip Buns Present?
01.
LDR.
terQWA
11.
Tr Blink CisSeats Resent?
f3y.
No
DhIA
COMMFNTSISAMPLE DISCAFPANCY Field Oar Ra9Wred? []Yet CINo
Lot 10 xf ,plit WM1uifKrs:
CLITNT ROUFICATIONIRTSOLUT10R
Ptoon contacted: Date/Fime:
Project Manager SCURF A&Wm:
Pmlea Manager SRF Reldew:
Dale:
Deu:
Page 110113

*ATIA11vac
Allvac - Bakers Plant
Stormwater Monitgd Re ort Form
Sample Date. "S-
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Sample Time:
Stormwater Discharge Outfall #03 (Non -Commingled)
Drainage Area = 336,580sc�ft. = 7.8 acres
% Impervious = 15%
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
D
30
COD
120
TSS
5�
100
Cadmium
0.001
Chromium, total recoverable
I
Copper, total recoverable
0.007
Nickel, total recoverable
.D
0.26
Zinc, total recoverable
Q Q!
0.067
pH
% (std units)
6-9 (std units)
Storm Date: /- f � i� Storm Duration: 3,:r' (Hrs.) Inches of Rainfall: Z. 8
Duration of time preceding rain event exceeding 0.1 ": 29a (firs.)
Estimated Flow Calculation:
Q—CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) = (A x inches.rain/I2 inches/ft. x 7.8 acres x .85) + .9 x inches min/I2inches/ft. x 7.8 x .I5)
Q(Total, cfs) = 0.2210 x _ /. (Inches of rain) + 0.0878 x /. �- --(Inches of rain)
. Q• S3/0'0 cfs

(�Iacmnalyfical*
wwwpacelahs.=
November 12, 2018
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW OUTFALL #03(13)
Pace Project No.: 92405879
Dear Scott Ryan:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Joe Hinkle, Allvac
David Pope, Allvac
ACC$f0'
THE
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

laneAnalyticals
www.pscelabs,cam
CERTIFICATIONS
Project: SW OUTFALL#03(8)
Pace Project No.: 92405879
Charlotte Certification 09
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Flodda/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky USTCertifiication * 84
North Carolina Field Services Certification #: 5342
V rginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 16

acmnalytical
wwwpatelabs.00m
SAMPLE ANALYTE COUNT
Project: SW GUTFALL #03(B)
Pace Project No.: 92405879
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
An alytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92406879D01
BSW03
EPA 200.7 Rev 4.4 1994
SH1
5
PASI-A
92405879002
BSW03
SM 5220D-2011
GC
1
PASI-A
92405879D03
BSW03
SM 521013-2011
SMK
1
PASI-A
924058790D4
BSW03
SM 254OD-2011
CEH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 3 of 16

IeAnalytical o
wvwpacetabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
Sample: BSW03 LAID: 22405879001 Collected: 11/05/18 06:31 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
Field Data Analytical Method
Collected By
DPJ
1
11/05/18 06:32
Collected Date
11105/18
1
11/05/18 06:32
Collected Time
06:25
1
11/05/18 06:32
pH
7.2
Std. Units
0.10
1
11/05/18 06:32
Temperature
15.7
deg C
0.50
1
11/05/18 06:32
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Cadmium
ND
ug1L
1.0
1
11/06/18 05:44
11/08/18 23:43
7440-43-9
Chromium
ND
ug1L
5.0
1
11/06/18 05:44
11/08/18 23:43
7440-47-3
Copper
11.8
ug1L
5.0
1
11/06/18 05:44
11/08/18 23:43
7440-50-8
Nickel
ND
ug1L
5.0
1
11/06/18 05A4
11/08/18 23A3
7440-02-0
Zinc
17.4
uglL
10.0
1
11/06/18 05:44
11/08/18 23:43
7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:09 PM without the written consent of Pace Analytical Services, LLC,
Page 4 of 16

(�Iacmnalyfical"
wwpacelabs corn
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL 903(B)
Pace Project No.: 92405879
Sample: SSW03 Lab ID: 92405879002 Collected: 11/05/18 W30 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
5220D COD
Chemical Oxygen Demand
Date: 11/12/2018 06:09 PM
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
33.1 mg1L 25.0 1 11/08/18 19:11 11/09/18 00:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L.L.C.
Page 5of16

s
acmnalXical
www.pacelabs.com
ANALYTICAL RESULTS
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2BO78
[phone]
Sample: BSW03 Lab ID: 92405879003 Collected: 11/05/18 06:28 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210E BOD, 5 day Analytical Method: SM 521 OB-2011
SOD, 5 day ND mg/L 2.0 1 11/06/18 19:07 11/11/18 13:38 B3
Date: 11/12/2018 06:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 16

(�5a'cmnalyfical*
w w .pacelebs.corn
ANALYTICAL RESULTS
Project: SW OUTFALL #03(13)
Pace Project No.: 92405879
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW03 Lab ID: 924058713004 Collected: 11/05/18 06:26 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D-2011
Total Suspended Solids 15.3 mg1L 2.5 1 11/08/18 00:44
Date: 11/12/2018 06:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 16

aceAnalyfical
www.pacalahs.oan
QUALITY CONTROL DATA
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 440463
Analysis Method:
EPA 2003 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4A 1994
Analysis Description: 200.7 MET
Associated Lab Samples: 92405879001
METHOD BLANK: 2419374
Matrix: Water
Associated Lab Samples: 92405879001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug1L
ND
1.0
11/08/18 23:12
Chromium
ug1L
ND
5.0
11/08/18 23:12
Copper
ug1L
ND
5.0
11/08/18 23:12
Nickel
ug1L
ND
5.0
11108/18 23:12
Zinc
uglL
ND
10.0
11/08/18 23:12
LABORATORY CONTROL SAMPLE:
2419375
Spike
LCS
LCS % Rec
Parameter
Units
Cone.
Result
% Rec Limits Qualifiers
Cadmium
ug1L
500
480
96 85-115
Chromium
ug1L
500
484
97 85-115
Copper
ug/L
500
499
100 85-115
Nickel
ug1L
500
478
96 85-115
Zinc
ug1L
500
467
93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419376
2419377
MS
MSD
92405896001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units Result
Cone.
Cone.
Result
Result % Rec % Rec
Limits
RPD Qual
Cadmium
uglL ND
500
500
503
500 101 100
70-130
1
Chromium
ug1L ND
500
500
506
504 101 100
70-130
0
Copper
ug1L 0.0053
500
500
521
519 103 103
70-130
0
mg1L
Nickel
ug1L ND
500
500
493
490 98 97
70-130
1
Zinc
ug1L 0.011
500
500
502
499 98 98
70-130
1
mg1L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419378
2419379
MS
MSD
92405904001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units Result
Cone.
Conc.
Result
Result % Rec % Rec
Limits
RPD Qual
Cadmium
ug1L ND
500
500
498
501 100 100
70-130
1
Chromium
ug1L ND
500
500
503
504 101 101
70-130
0
Copper
ug1L ND
500
500
510
514 102 103
70-130
1
Nickel
ug1L ND
500
500
490
494 98 98
70-130
1
Zinc
ug1L 0.014
500
500
497
499 97 97
70-130
0
mglL
Results presented on this page are in the units Indicated by the'Uniht' column except where an aRemate unit is presented to the right at the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:09 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16

aceAnalytical a
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QUALITY CONTROL DATA
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
QC Batch: 440996 Analysis Method: SM 254OD-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92405879004
METHOD BLANK: 2421944 Matrix: Water
Associated Lab Samples: 92405879004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mgll_ NO 2.5 11108t18 00:38
LABORATORY CONTROL SAMPLE:
2421945
Parameter
Units
Total Suspended Solids
mglL
SAMPLE DUPLICATE: 2421946
Parameter
Units
Total Suspended Solids
mg1L
SAMPLE DUPLICATE: 2421947
Parameter
Units
Total Suspended Solids
mglL
Spike LCS LCS
Conc. Result % Rec
250 244 98
92405900003 Dup
Result Result
27.8 31.0
92405880005 Dup
Result Result
16.4 18.2
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
90-110
RPD Qualifiers
11 D6
RPD Qualifiers
10 D6
Results presented an this page are In the units Indicated by the 'Units- column except when, an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/1212018 06:09 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16

laneAnalyfical"
www.pace4bs.c=
QUALITY CONTROL DATA
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
QC Batch: 440600 Analysis Method: SM 521 OB-2011
QC Batch Method: SM 5210B-2011 Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 9240587SO03
METHOD BLANK: 2420066
Associated Lab Samples: 92405879003
Parameter Units
BOD, 5 day mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 11/11/18 13:26 B3
LABORATORY CONTROL SAMPLE: 2420067
Spike 1-CS
Parameter Units Conc. Result
BOD, 5 day mg1L 198 192
SAMPLE DUPLICATE: 2420068
92405881001 Dup
Parameter Units Result Result
BOD, 5 day mg/L ND ND
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
97 84.6-115 B3
RPD Qualifiers
B3
Results presented on this page ere In the units Indicated by the'ttnits' column except when an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:09 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 16

(�IaoAnalyfical*
www pacelabs.com
QUALITY CONTROL DATA
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 441148
Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011
Analysis Description: 5220D COD
Associated Lab Samples: 92405879002
METHOD BLANK: 2422559
Matrix: Water
Associated Lab Samples: 92405879002
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0
11/09/18 00:04
LABORATORY CONTROL SAMPLE: 2422560
Spike
LCS
LCS % Rec
Parameter Units
Cone.
Result
% Rec Limits
Qualifiers
Chemical Oxygen Demand mg(L
750
757
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422561
2422562
MS
MSD
92406236003
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rec
% Rec
Limits
RPD Qual
Chemical Oxygen Demand mglL 107
100
100 216
216 109
109
90-110
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422563
2422564
MS
MSD
92405876001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Cone.
Cone, Result
Result % Rec
% Rec
Limits
RPD Qual
Chemical Oxygen Demand mg/L ND
100
100 130
133 113
116
90-110
2 M1
Results presented on this page are In the units Indicated by the *Units' column except when an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:09 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 16

Pace Analytical Services, LLC
ilcale 9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
l
wwwr bs.ow [phone]
QUALIFIERS
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Olphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-N itrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B3 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg1L.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /12/2018 06:09 PM without the written consent of Pace Analytical Services, LLC, Page 12 of 16

aceftlytical s
www.pacefabs.cw
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
SW OUTFALL #03(B)
92405879
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92405879001
BSW03
92405879001
BSW03
EPA 200.7 Rev 4.4 1994
440463
EPA 200.7 Rev 4.4 1994
440492
92405879004
BSW03
SM 254OD-2011
440996
92405879003
BSW03
SM 521OB-2011
440600
SM 521 OB-2011
440712
92405879002
BSW03
SM 5220D-2011
441148
SM 5220D-2011
441293
UFSi7�i)i1fY���tII�I�I•'i[t�'l�ul
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 16

Document Name:
Document Revised: February 7, 2018
iC8�i1c3ildlCslr'n
c
Semple Condition Upon Recei t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033•Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑
Client Name:
Courier: ❑Fed Ex [-]UPS
❑ Commercial ❑Pace
Greenwood ❑ Huntersville Raleigh[) Mechanicsville[]
Custody Seal Present? ❑Yes .❑i No seals Intact? []Yes \❑No
F
Project w0# ' 924058 1 J
11111117111111111111I
; I
Date/initials Person Examining [ontents;'—,t , 1 r �
Packing Material: ❑Bubble wrap ❑Bubble Bags ❑J None ❑ Other Biological Tissue Frozen?
Thermometer [:]Yes❑No ON/A
92Ta45 Type of Ice: 0wet ❑Blue ❑None
,0IR Gun ID: V
Cooler Temp ('Cl: (� , Correction Factor: Add/Subtract VQ 1
`` Temp should be above freezing to 6'C
Cooler Temp Corrected ('Q [ 1 Dimples out of temp criteria. Samples an ice, cooling process
has begun
USDA Regulated Soil L❑ N/A, water w mple)
Did samples originate in a quarantine zone vlithin the United States. CA, NY, or SC (check maps)? Dld samples originate from a foreign source (internationally,
hlvpc 1 1fin inrinrilne Wawaa —1 Pnprrn riirn17 f,Vnc 11Hn
Cam ments/Discre anc ;
Chain of Custody Present?
L❑Yes
©No
N/A
1.
Samples Arrived within Hold Time?
Yes
❑No
N/A
2.
Short Hold Time Analysis (<72 hr.?
, Yes
No
N/A
3.
Rush Turn Around Time Requested?
Yes
D Na
❑N/A
4.
Sufficient Volume7
l cs
QN0
N/A
5.
Correct Containers Used?
i
;QYes
❑No
❑N/A
6.
-Pace Containers Used?
13YeS
[]NO
❑N/A
/
Containers Intact?
Yes
No
CINJA
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
QNo
rs/A
S.
Sample labels Match COC?
O+Yel
❑No
[]N/A
9.
�J l
-Includes Date/Time/IO/Anal sis Matrix:
Heads ace in VOA Vials (>5.6mm)?
❑Yes
No
U N/A
10.
Trip Blank Present?
❑Yes
❑No
QN/A
11,
!A
Trip Blank Custody Seats Present?
❑Yes
No
COMMENTS/SAMPLE DISCREPANCY Field Data Requlred7 []Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: 'L Date:
Page 14 of 16

Document Name:
Document Revised: February 7, 2018
26AMIXidal `
Sam le Condition Upon Recel tiSCURi
Pa e 1 of 2
Document No.:
issuing Authority:
F-CAR-CS-033-Rev.05
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is Project" �®� ; �� 4 0����
verified and within the acceptance range for preservation
samples. 111M: MWB Dire Date: 11/14/18
.._Exceptions: VOA._Collform,TOC, Oil and Grease, ORO/BOSS (water) DOC, LLHg r1,IEN_TL. 92gJJ
o NC
"Bottom half of box is to list number of bottle
$
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w
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pH Adjustment Log for Preserved Samples
Sample 10
Type of Preservative
pH upon recelpt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
tot U
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wilt be sent to the North Carolina OEKNR Certification Office V. e.
Out of hold, intorrect preservative, out of temp, incorrect containers.
Page 15 of 16

60�
uLZ.
Stormwater Monitorin
C-haiwofCustody-Record
Project Number/Name- SW Outfall #03(B)
jProject Location: ATl SM - Bakers
Sample 's Sign
re:
JDate:
It
U_
F
icy
>
1
r
a V
sa
•
Requested Test Parameters
E Y
?
p
U
rl Z11b r
!L
')
j-,S-
G
G
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc
„r
G
G Im
HNO3
Y
Cadmium
3
G
G lIg
H2SO4
Y
COD
G
G /0
None
Y
BOD
6 •' („4
G
G /m
None
Y
TSS
Onsite Field eH Analysis
Onsite Field Temperature Analysis
pH: %•� (s.u.) Sample Time: .as,.,
Temp: /S' q (°C) Sample Time: /,A�
Analysis Tillie-,
Analysis Time: 6�
Meter Calibrated: Y8.5
Thermometer Calibrated: (9 1 N
Sampling and field analysis completed b j:
ffi
Relinquished B 44-1
Received y:
Date: / - 5 '%9" Time: (,//z�
Date: Time: �l
Relinquished By:
Received By:
Date:
Time:
Date:
Time:
EHS-SW-Chain of Costody Qutfall 03-Rev 001 Page 16 of 16

Allvac - Bakers Plant
Stormwater Monitoring Report Form
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Non-ContactCooling Wastewater
Pa.c e 4fia.ly
40 CFR Part 136
AT I
Spedalty Maxertaks
Non-
Contact
Cooling
Water # ,
Sampling
Date
Sampling
Time
Estimated
Flow(MGD)
Total
Residual
Chlorine
(mg/L)
Temperature
pH (std. units)
Effluent
Downstream
Upstream

lacieAnalj4icale
www.pacelabs.com
October 31, 2018
Scott Ryan
Allvac
Monroe, NC
RE: Project: NonContact Cooling Water
Pace Project No.: 92403862
Dear Scott Ryan:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 17, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Joe Hinkle, Allvac
David Pope, Allvac
A�Rbr��
TNI
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

Pace Analytical Services, LLG
aceAnafytical a
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
www.pacews.com
[phone]
CERTIFICATIONS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Nuntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification M 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VrginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida1NELAP Certification M E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
VrginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 19

accAnalytical
www.pacebbs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
NonContact Cooling Water
92403862
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92403862001
NonContact #1
EPA 1664B
JMS
1
PASI-C
SM 4500-Cl G-2011
MDW
1
PASI-A
92403862002
NonContact #2
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92403862003
NonContact#3
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92403862004
NonContact #4
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PAS1-A
92403862005
NonContact #5
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92403862006
NonContact #6
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92403862007
NonContact #7
EPA 16648
JMS
1
PASI-C
SM 4500-Cl G-2011
MDW
1
PASI-A
92403862008
NonContact#8
EPA16648
JMS
1
PASI-C
SM 4500-a G-2011
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 19

(�55'&Mnalyfical
wwwpacelabs.corn
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Nnrey Ave, Suite t00
Huntersville, NC 28078
[phone]
Sample: NonContact#1 Lab ID: 92403862DD1 Collected: 10/16/18 07:45 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 10131/18 03:39
4500CL G Chlorine, Residual Analytical Method: SM 4500-Cl G-2011
Chlorine, Total Residual 0.34 mg1L 0.024 1 10/18/18 23:12 7782-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 19

aceAnalytical e
wwwpaceAsbs-c=
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #2 Lab ID: 92403862002 Collected: 10/16/18 08:05 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/t_ 5.0 1 10/31/18 03:39
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual 0.038 mg1L 0.024 1 10/18/18 23:21 7782-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 19

laceAnalyficale
www.pace4bs.corn
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
Sample: NonContact#3 Lab ID: 92403862003 Collected: 10/16/18 08:27 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 10/31/18 03:39
4600CL G Chlorino, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual 0.49 mg1L 0.024 1 10/18/18 23:26 7782-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 19

laeAnalXical"
www.pacelabs.corn
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pee* Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #4 Lab la: 92403862004 Collected: 10/16/18 08:50 Received: 10117118 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 10/31118 03:40
4500CL G Chlorine, Residual Analytical Method: SM 4500-Cl G-2011
Chlorine, Total Residual 0.093 mg1L 0.024 1 10/18/18 23:30 7782-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7of19

(�Iacmnalyficale
www pacelabs.com
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact 95 Lab ID: 92403862005 Collected: 10/16/18 09:15 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. dual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 1 10/31/18 03:40
4500CL G Chlorine, Residual Analytical Method: SM 4500-Cl G-2011
Chlorine, Total Residual 0.46 mg1L 0024 1 10/18/18 23:35 7782-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 19

acmnalyiical s
www.pacelabs.com
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Mncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #6 Lab ID: 92403862006 Collected: 10/16/18 09:37 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16648
Oil and Grease ND mg/L 5 0 1 10/31/18 03:40
4600CL G Chlorine, Residual Analytical Method: SM. 4500-CI G-2011
Chlorine, Total Residual 0.028 mg1L 0.024 1 10/18/18 23:40 7782-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 19

aceftlXieal
w wpacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huniersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92403862
Sample: NonContact#7 Lab Ib: 92403862007 Collected: 10/16/18 10:00 Received: 10/17/18 06:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 1 10/31/18 03:41
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual 0.030 mgtL 0.024 1 101181182145 7782-50-5 H3
9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1013 t12018 03:28 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

(�55'cie Analytical
www.paoQbs.mm
ANALYTICAL RESULTS
Project: NonContacl Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9000 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #8 Lab ID: 92403862008 Collected: 10/16/18 10:23 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mglL 5.0 1 10131/18 03:41
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual 0.097 mg1L 0.024 1 10/18/18 23:50 7782-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/31/2018 03:28 PM without the written consent of Pace Analytical Services, I.I.C. Page 11 of 19

(�IaceAnalytical'
wwwpwelab9.com
QUALITY CONTROL DATA
Project: NonContact Cooling Water
Pace Project No.: 92403662
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 439353 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92403862001, 92403862002, 92403862003, 92403862004, 92403862005, 92403862006, 92403862007,
92403862008
METHOD BLANK: 2414537 Matrix: Water
Associated Lab Samples: 92403862001, 92403862002, 92403862003, 92403862004, 92403862005, 92403862006, 92403862007,
92403862008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L ND 4.8 10/31/18 03:37
LABORATORY CONTROL SAMPLE:
2414538
Spike LCS
LCS
e% Rec
Parameter
Units
Cone. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg1L
38.5 38.7
101
78-114
MATRIX SPIKE SAMPLE:
2414539
92403774004 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg1L
ND 38.5
38.4
99
78-114
Results presented on this page are In the units indicated by the 'Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/31/2018 03:28 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19

lacieAnalytical
w"pacelabs.mm
QUALITY CONTROL DATA
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 437083 Analysis Method: SM 4500-CI G-2011
QC Batch Method: SM 4600-CI G-2011 Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92403862001, 92403852002, 92403862003, 92403862004, 92403862005, 92403662006, 92403862007,
92403862008
METHOD BLANK: 2404409 Matrix: Water
Associated Lab Samples: 92403862001, 92403862002, 92403862003, 92403862004, 92403862005, 92403862006, 92403862007,
92403862008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine, Total Residual mg1L ND 0.024 10/18/18 23:08
SAMPLE DUPLICATE: 2404410
92403862001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg/L 0.34 0,34 1 H3
Results presented on this page are In the unite Indicated by the'V~ column except when an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 10/31/2018 03:28 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

aceAnalytical
WWW..paCerabs.WM
QUALIFIERS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Irl:111LIIII(LOR&9
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, Lt_C
9800 Kiincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10131 /2018 03:28 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19

aceAnalytical"
www.pao&Wbs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NonContact Cooling Water
Pace Project No.: 92403862
Lab ID Sample ID QC Batch Method QC Batch
92403862001
Non Contact#1
EPA16648
439353
92403862002
NonContact#2
EPA1664B
439353
92403862003
NonContact#3
EPA 16646
439353
924D3862004
NonContact#4
EPA16648
439353
92403062005
NonContact#5
EPA1664B
439353
92403862006
NonContact#6
EPA166413
439353
92403862007
NonContact#7
EPA1664B
439353
92403862008
NonContact#8
EPA 1664B
439353
92403962001
NonContact 91
SM 4500-Cl G-2011
437083
92403862002
NonContact #2
SM 4500-CI G-2011
437083
92403862003
NonContact 03
SM 4500-CI G-2011
437083
92403862004
NonContact #4
SM 4500-CI G-2011
437083
92403862005
NonContact #5
SM 4500-0 G-2011
437083
92403862006
NonContact#6
SM 4500-CiG-2011
437083
92403862007
NonContact #7
SM 4500-CI G-2011
437083
92403862008
NonContact #8
SM 4500-CI G-2011
437083
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9B00 Kinsey Ave. Suite too
Huntersville, NC 28078
[phone]
Analytical Method
Analytical
Batch
Page 15 of 19

s
aceAnaloical
Z i7_
Document Name:
Sample Condition Upon Recet t(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas qua i�Office
Laboratory receiving samples;
Asheville ❑ Eden[] Greenwood ❑ Huntersvill j�� Raleigh❑ Mechanicsville❑
Client Name: WO# : 92403862
Courier:
❑ Commercial
Custody Seal Present?
( � Project q:
[�Eed Ex ❑U S ❑USPS ❑Client
Q]Pace []Other: 92403862
"`❑Yes 40 Seals Intact? ❑Yes IL,QNo
1
Packing Material: ❑Bubble Wrap Bubble Bags ❑None ❑ Other
Thermometer: ,)
111ALn ID: 92TO45 Type of Ice: sLjwet []Blue
Cooler Temp ('C): 2 1 t � Correction Factor: Add/Subtract IT)
Cooler Temp Corrected
USDA Regulate
�So11 .� N/A, water sample)
Did samples o�i�irsate In quarantine zone within the United States: CA, NY, or SC (check maps)?
MY0, i1Nn
pate/Instlats Perron Examining Co tents: / t �' � 1
Blollsg . 1 Tissue Frozen?
❑YesNo ❑N/A
❑None
Temp should be above freezing to VC
❑Samples out of temp criteria. Samples on ice, tooting process
has begun
Did samples originate front a foreign source rote nationally,
inrhidlna Hawxii and Punrtn Rltol? FlYes MNn
Comments/Discrepancy:
Chain of Custody Present?
e6yes
No
N/A
1.
Samples Arrived within Hold Time?
C - yes
ON.
0 N/A
2.
Short Hold Time Analysis c72 hr.)?
#cly.
- Ilo
D N/A
3.
Rush Turn Around Time Requested?
Qy.
- b
❑N/A
4.
SufficientVolurne?
/-Qves
No
❑N/A
S.
Correct Containers Used?
Yes
❑No
[]NIA
5.
-Pace Containers Used?
ye}�
❑No
[]NA
Containers Intact?
Yes
No
EINJA
7.
Dissolved analysis: Samples Field Filtered?
� ❑Yes
No
� NIA
g.
Sample Labels Match COC?
/ Yes
❑Na
❑N/A
9.
-includes Date/Time/ID/Analysis Matrix:
/ Z
Heads ace in VOA Vials (}5.&mm)>
- No
/A
10.
Trip Blank Present?
-[]Yes
❑Yes C] 0
❑N/A
11.
I
Trip Blank CustodySeals Present?
[]Yes
[]No
r NIA
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
Field Data Required? []Yes []No
i ll
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
V
Page 16 of 19

�� aceAnalytrca!
Document Name:
Sample Condition Upon Recel tISCURj
document Revised: February 7, 2018
I Page 1 of 2
Document No.:
F-CAR•CS-033-Rev.06
Issuing Authority:
--Pace Carolinas Quail _Office
'Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project W®# 92403862
PM: MWB Due Date: 10/31/18
CLIENT: 92-Allvae NC
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pH Adjustment Log for Preserved Samples
Sample 10
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservetlon
adjusted
—Amount of Preservative
added
—Cot'$
Nate: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certilication Office (I.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 17 of 19

Storm Water Monitorin
(NON CONTACT)
Bakers North
Chain of Custody Record
-0,4 AT
Specialty +.Wuiata
nave 42
Project Number/Name: No Contact Cooling Water
I Project Location: Allvac Bakers
Sampler's Signature:
;
Date: Q- �2
C
v►
U
C
�
o
V
a+
VIar
A
u
M
m
0
CL
a
o
Requested Test
Parameters
G Z
Aron �p1
&WAR5-
,,
G
G
HCL
Y
,rS
Oil & Grease
p 4LA a
:p j,...
G
G
NCL
Y
dy, f t
Oil & Grease
adConf
:� �,�
G
G
HCL
Y
8, •a
Oil & Grease
Ce.ecf
�SD._
G
G
HCL
Y
'e
Oil & Grease
G
G
HCL
Y
,(,'b
Oil & Grease
i
:,3
G
G
HCL
Y
a, 9g
Oil & Grease
&ACpAt&ct
D�DD�.
G
G
HCL
Y
-a
Oil & Grease
G
G
HCL
Y
Oil & Grease
Meter Calibrated: / N
IThermometer Calibrated: ®/ N
Sampling and Field analysis completed by: '
Relinquished By:
Relinquished By:�,�,;�
Date p- Time:
Uate : •-,-L7' ,JTii-ne:,'J
q�--
Relinquished By: f
Reli is gd By:'
Date Ljt.ltjTime:
l ` Date; {
}
Tithe:
EHS Baker South SW REV # 2 5/10/2016
Ctl
Page 18 of 19

Storm Water Monitorin
(NON CONTACT)
Bakers North
Chain of Custody Record
�ATI
Specialty 6131c,ials
oaee $11
Project Number/Name: NonConta t Cooling Water
Project Location: Allvac Bakers
Sampler's Signature:
.1=;
Date: Q o//, —/
i'
a
o
°'
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0
0
m
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}
~
m
z
L
a
U
u,
CL
H
a
M
"
y
0
~
a
a
..
y
O
Requested Test
Parameters
q
lie
Ca waf 1
a-
- 6
rl5,.,
G
G/10
None
Y
5'e-I
Residual Chlorine
„,�8
:65',
G
G/®
None
Y
7.1
3, 'c
Residual Chlorine
Alon 4
G
G/®
None
Y
ZJ
OV.3%
Residual Chlorine
:5'
G
GAS
None
Y
`e
Residual Chlorine
A-V
G
G/O
None
Y
'c
Residual Chlorine
ortC41t 6
..
G
G/®
None
Y
'c
iResidual Chlorine
emfu,�
Go
None
Y
. 7'4
Residual Chlorine
,rCoirfaoi
D•' ,3
G
G
None
Y
•e,
Residual Chlorine
Meter Calibrated:
/ N
IThermorneter Calibrated
/ N
Sampling and Field analysis completed by:
iuz&
Relinquished By:
Received By:
+
`� /
Date: -
Time:
p... /
Date:-
}
J Time:
Relinquished By:
/
Rec 1ved,By: f
Time:
\ _
daft
1
Time:
EHS Baker South SW REV # 2 5/10/2016
Page 19 of 19

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS O<X—Wg
FACILITY NAME .L"J4I!'�G ni9tX0,rr
PERSON COLLECTING SAMPLE ) ~ ,:d
CERTIFIED LABORATORY(S) a re Lab #1&_
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR:"
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY (aAM
PHONE NO. (7d Y) 4W - fW11
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Date
Sample
Collected
Total
Rainfall
i My
K)
i
i
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes /no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G1TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
moldd/ r
MG
inches
m 1
m
unit
allmo
Form SWU-247, last revised 21212012
Page I of 2

STORM EVENT CHARACTERISTICS -
Date
Total Event Precipitation (�inc�hes): B
Event Duration (hours): ._ _ (only if applicable —see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Pe mit e) (Date)
Form SWU-247, last revised 21212012
Page 2 of 2

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit liti s://de .nc. Gov/about/divisions/cncr -mineral-land-
resourceslenerey-mineral-land-permits/stormwater-permits/npdes-industrial-sw#tabA
Permit No.: NlCI 1fZIQl�l,�1 �l�l or Certificate of Coverage No.: NIGGI_I_I_I I_I_I
Facility Name: lafiMC •,5A.,t ew
County: Phone No.
Inspector: P"Wix %�p� TI
Date of Inspection: 'S-
Time of Inspection: •67Dar
Total Event Precipitation (inches): /.g
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the pennitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the penmittee obtains approval from the local DEMLR
Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or`Designee)
1. Outfall Description:
Outfall No. 95WI Structure (pipe, ditch, etc.): bpi// W!Y
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SW U-242, last modified 0729/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: ,f�eRr
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): NDAB
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
0 2 3 4 5
5. )Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
© 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stonnwater discharge, where l is no solids and 5 is extremely muddy:
7.
8.
9
© 2 3 4 5
Is there any foam in the stormwater discharge? o Yes (0)No.
Is there an oil sheen in the stonnwater discharge? OYes eNo.
Is there evidence of erosion or deposition at the outfall? 0 Yes ® No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe %i om B
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242, last modified 0712812017

rnsvonmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For• guidance on filling out this form, please visit httpsJ/deg.nc.gov/about/divisionslenew-mineral-land-
resourceslenergy-mineral-land-permits/storm wat er-permi t s/npdes-industrial-sw#tab-4
Pennit No.: NICI�I D/O /01,�1�1 �1 or Certificate of Coverage No.: NlCIGI—IWI—I—I—I l
Facility Name: //Y4G-geke*S
County: GL/l/OR Phone No. %Q f 4.W -3 1
Inspector: Z4y1W Qpe 3/,.
Date of Inspection:
Time of inspection:
Total Event Precipitation (inches): /.8
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour stonn
interval does not apply if the pernittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
onal Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. Outfall Description:
Outfall No, B5MOg Structure {pipe, ditch, etc.}: e
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SWU-242, fast inodified 07/28/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: G%
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): _ _Alow G
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stonnwater discharge, where I is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
0 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes ® No.
8. Is there an oil sheen in the stormwater discharge? OYes allo.
9. is there evidence of erosion or deposition at the outfall? O Yes ®No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe Are
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
5 W U•242, Last modified 07/28/2017

Entironmc+r+ta!
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit htt s:l/de .nc, ov/about/divisions/cner -mineral-land-
resources/eneray-m ineml-]and -pernijts/st orm wat er-permits/npdes-industrial-sw#tab-4
Permit No.: or Certificate of Coverage No.: NIC/GI_I_I_I_I_I_I
Facility Name: _ /ft�%{-aG ' ALA-'tr�r
County: &h/pit Phone No.
Inspector! &rzw Ape IT'-'
Date of Inspection:
Time of Inspection: ai%r.r
Total Event Precipitation (inches): /.8
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the pennittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee rrDesignee)
1. Outfall Description:
Outfall No. 65WO
Receiving Stream:
Structure (pipe, ditch, etc.): p e /D; .,&k _
Describe the industrial activities that, occur within the outfall drainage area:
Page t of 2
5WU-242, Last modified 07/28/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: c%ate
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): / '0"'j a
4. Clarity: Choose the number which best describes the clarity of the discharge, where l is clear
and 5 is very cloudy:
1 © 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
© 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
© 2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes tq No.
8
9.
Is there an oil sheen in the stormwater discharge? OYes (§No.
Is there evidence of erosion or deposition at the outfall? O Yes ®No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe ivoA e
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
swu-242, Last modified 07/28/2017