NCS000329_MONITORING INFO_20180618

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
DOC TYPE
❑ FINAL PERMIT
..__L-�-MONITORING- REPORTS---- ---._--..---
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑
YYYYM M DD

June 07, 2018
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
JUN 18 2018
ATI
P.O. Box 5030
2020 Ashcraft Avenue
Monroe, NC 28 E 11-5030
Phone: [phone]
Pax: (704) 290-5 194
Email: joe.hinklena?atimetals.com
Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period
Sample Number Start
IEnd
Year 9 — Period l
17 March 1, 2018
August 31, 2018
Analytical monitoring includes:
• Outfall #01 (B), commingled stormwater
• Outfall #02 (B), non -commingled stormwater
• Outfall #03 (B), non -commingled stormwater
• Non Contact Cooling Water #1 - #8
If you have any questions or need additional information, please contact me at 704-289-4511,
Thank you.
Sincerely,
Scott an
Environmental Manager
f

Allvac - Bakers Plant OATI Allvac
Y Stormwater Monitoring Report_Form
Sample Date: .5--L:�_ Sample Time: .3 - Ylo4=
I.,,.
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Stormwater Discharge Outfall #01 Commingled)
Drainage Area = 2,915,470sq. ft. = 69 acres
% Impervious = 34%
- CLV d PePe, XAJ d—I'm ezoo f t
40 CFR Part 136
--
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
02.930
COD
�l 0
120
TSS
100
Cadmium
D
0.001
Chromium, total recoverable
1
Copper, total recoverable
A
0.007
Nickel, total recoverable
01
0.26
Zinc, total recoverable
D
0.067
Oil and Grease
NP
20
Temp (receiving stream)
4 (deg C)
32 (deg C)
Total Residual Chlorine
0.017
pH
(std units)
6-9 (std units)
Storm Date: _S =/S /F� Storm Duration: / - 05' (Hrs.) Inches of Rainfall: O . aS
Duration of time preceding rain event exceeding 0.1": 8— Mrs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) _ (A x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches rain/12inches/ft. x 69 x .34)
Q(Total, cfs) = 1.5180 x _ Q • a? 6- (Inches of rain) + 1.7595 x (Inches of rain)
�I• $19� cis

aleemalytical
wwwpecelabs.com
May 29, 2018
Mr. Joe Hinkle
Allvac
RE: Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvitle, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on May 16, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy long, Allvac
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC,
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a I 'Ow ytical
..pecebbacom
Project: SW 0UTFALL #01 (B)
Pace Project No.: 92385030
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
LouisianalNELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FloddalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florid alNELAP Certification #: E87627
Kentucky UST Certification #: 84
VrginialVELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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ladmnalRicale
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SAMPLE ANALYTE COUNT
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2BO78
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92385030001 SW OUTFALL #01(B) EPA 16648
JMS
1
PASI-C
EPA200.7
SH1
5
PASI-A
SM 2540D
WC
1
PASI-A
SM 4500-CI G
EWS
1
PASI-A
SM 5210B
RLO
1
PASI-A
SM 5220D
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW OUTFALL #01(B)
Parameters
Lab la: 92385030001 Collected: 05/15/18 15:54
Results Units Report Limit DF
Received: 05/16/18 08:18 Matrix: Water
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
05/15/18 15:53
Collected Date
05/15/18
1
05/15/18 16:63
Collected Time
15:46
1
05/15/18 15:53
pH
7.8 Std. Units
0,10
1
05/15/18 15:53
Temperature
28.4 deg C
0.50
1
05/15/18 15:53
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L
5.0
1
05/24/18 05702
200.7 MET ICP
Analytical Method: EPA200.7 Preparation Method: EPA200.7
Cadmium
ND ug1L
1.0
1
0512411815:10
0512511815:04 7440-43-9
Chromium
ND ug1L
5.0
1
051241i815:10
05125/1815iO4 7440-47-3
Copper
10.9 uglL
5.0
1
051241i815:10
05/2511815:04 7440-50-8
Nickel
6.5 uglL
5.0
1
0512411815:10
05125/1815iO4 7440-02-0
Zinc
ND ug1L
10.0
1
0512411815:10
0512511815:04 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
6.3 mg/L
2.5
1
05/21/18 20:54
4500CL G Chlorine, Residual
Analytical Method: SM 4500-CI G
Chlorine, Total Residual
0.044 mg/L
0.024
1
05/22/18 10:40 7782-50-5 H6
6210B BOD, 5 day
Analytical Method: SM 5210B
BOD, 5 day
2.8 mg/L
2.0
1
05/17/18 07:38
05/22/18 02:55
52200 COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
31.0 mg1L
25.0
1
05/25/18 16:38
REPORT OF LABORATORY ANALYSIS
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Date: 05/29/2018 04A1 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 15

laomnal�-Ncal
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QUALITY CONTROL DATA
Project: - SW OUTFALL 901 (B)
Pace Project No.: 92385030
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 412124
Analysis Method:
EPA 1664E
QC Batch Method: EPA 1664B
Analysis Description:
1664 HEM, Oil and Grease
Associated Lab Samples: 92385030001
METHOD BLANK: 2286233
Matrix: Water
Associated Lab Samples: 92385030001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Oil and Grease
mg/L
ND 5.0 05/24/18 04:56
LABORATORY CONTROL SAMPLE:
2286234
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Oil and Grease
mg1L
38.5 36.9
96 78-114
MATRIX SPIKE SAMPLE:
2286235
92385786001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Oil and Grease
mg1L
ND 38.5
39.5 103 78-114
Results presented on this page ere in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalXcal
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QUALITY CONTROL DATA
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
QC Batch: 412205 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 2003 MET
Associated Lab Samples: 92385030001
METHOD BLANK: 2286655
Matrix: Water
Associated Lab Samples: 92385030001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug1L
NO
1.0
05/2511817:41
Chromium
uglL
NO
5.0
05/2511817:41
Copper
ug1L
NO
5.0
05/2511817:41
Nickel
uglL
NO
5.0
0512511817:41
Zinc
uglL
NO
10.0
0512511817:41
Pace AnalyUcal Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2BD78
[phone]
LABORATORY CONTROL SAMPLE:
2286556
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
uglL
500
491
98
85-115
Chromium
ug1L
500
524
105
85-115
Copper
uglL
500
548
110
85-115
Nickel
ug1L
500
509
102
85-115
Zinc
uglL
500
476
95
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2286557
2286558
MS
MSD
92384986001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
uglL
ND
500
500
515
523
103
104
70-130
2
Chromium
uglL
NO
500
500
546
555
109
111
70-130
2
Copper
uglL
2030
500
500
2580
2610
110
117
70-130
1
Nickel
uglL
5.1
500
500
532
541
105
107
70-130
2
Zinc
uglL
159
500
500
653
662
99
101
70-130
1
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE:
2286559
2286560
MS
MSD
92385205002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone,
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Cadmium
ug1L
ND
500
500
504
491
100
98
70-130.
2
Chromium
uglL
5.7
500
500
6080
5940
71
44
70-130
2 M6
mg/L
Copper
ug1L
0.88
500
500
1390
1380
103
100
70-130
1
mg1L
Nickel
uglL
0.13
500
500
650
630
104
100
70-130
3
mg1L
Zinc
ug1L
12.6
500
500
13400
13300
163
158
70-130
0 M6
mg1L
Results presented on this page are In
the units Indicated by the
"Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 15

(�;a7cdimnaVical
www.pacelabs.co 1
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
QC Batch: 411695 Analysis Method: SM 2540D
OC Batch Method: SM 2540D Analysis description: 2540D Total Suspended Solids
Associated Lab Samples: 92385030001
METHOD BLANK: 2284017
Associated Lab Samples: 92385030001
Parameter Units
Total Suspended Solids mg1L
LABORATORY CONTROL SAMPLE: 2284018
Parameter Units
Total Suspended Solids mg1L
SAMPLE DUPLICATE: 2284019
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 2284020
Parameter
Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed ' Qualifiers
ND 2.5 05/21118 20:49
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 256 102 90-110
92384724001 Dup
Units Result Result RPD Qualifiers
mg/L ND ND
92384905001 Dup
Units Result Result RPD Qualifiers
mg1L ND ND
Results presented on this page are In the unite indicated by the "Units" column except where an aRemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalXical
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QUALITY CONTROL DATA
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
QC Batch: 411753 Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92385030001
METHOD BLANK: 2284194
Associated Lab Samples: 92385030001
Parameter Units
Chlorine, Total Residual mg1L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.024 05122/1810:40
SAMPLE DUPLICATE: 2284195
92384160004 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg1L 0.41 0.45 8 H6
SAMPLE DUPLICATE: 2284196
92385030001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg1L 0.044 0.046 4 H6
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 26078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 15

aU11; 1010,31
www.p9miabs.com
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
QC Batch: 411072
QC Batch Method. SM 5210B
Associated Lab Samples: 92385030001
METHOD BLANK: 2280664
Associated Lab Samples: 92385030001
Parameter Units
BOD, 5 day mg/L
LABORATORY CONTROL SAMPLE: 2280665
Parameter Units
BOD, 5 day mg1L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 5210B
Analysis Description: 52108 SOD, 5 day
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 05/22118 02:12
Spike LCS LCS % Rec
Conc, Result % Rec Limits Qualifiers
198 169 85 84.6-115.4
SAMPLE DUPLICATE: 2280666
92385027001 Dup
Parameter Units Result Result
BOD, 5 day mg/L 10.5 11.5
RPD Qualifiers
9
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 15

lanbAnalX-ical
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a
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL#01 (B)
Pace Project No.: 92385030
QC Batch: 412405
Analysis Method: SM
5220D
QC Batch Method: SM 5220D
Analysis Description: 5220D COD
Associated Lab Samples: 92385030001
METHOD BLANK: 2287604
Matrix: Water
Associated Lab Samples: 92385030001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg1L
ND 25.0
05/25/18 16:38
LABORATORY CONTROL SAMPLE: 2287605
Spike
LCS
LCS % Rea
Parameter Units
Conc.
Result
% Rec Limits - Qualifiers
Chemical Oxygen Demand mglL
750
741
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287606
2287607
MS
MSD
92384807001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg1L 272
100
100 360
363 88 91
90-110 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287608
2287609
MS
MSD
92385152001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits RPD Qual
Chemical Oxygen Demand mg1L 298
100
100 386
395 88 97
90-110 2 M1
Results presented on this page are in the units Indicated by the "Unlls" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
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acMnaly_Vcal
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QUALIFIERS
Project: SW OUTFALL#01 (B)
Pace Project No.: 92385030
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical QuantitaGon Limit.
RL - Reporting Limit.
Pace Anatytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(A) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonilrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA required holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
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lacmnal�-fica(
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #01 (B)
Pace Project No.: 92385030
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92385030001
SW OUTFALL #01 (B)
92385030001
SW OUTFALL #01(B)
EPA 16646
412124
92385030001
SW OUTFALL #01(B)
EPA 200.7
412205 EPA 200.7 412413
92385030001
SW OUTFALL #01(B)
SM 2540D
411695
92385030001
SW OUTFALL #01(B)
SM 4500-CI G
411753
92385030001
SW OUTFALL #01(8)
SM 5210B
411072 SM 5210B 411089
92385030001
SW OUTFALL #01(B)
SM 5220D
412405
REPORT OF LABORATORY ANALYSIS
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Document Name: Document Revised: February 7, 2018
'_• _ h,, Sam le Condition Upon Recel t SCUR Page 1 of 2
Ana& al • Document No.: I Issuing Authority:
Laboratory receiving samples:
Asheville ❑ Eden[-] Greenwood ❑
Pace Carolinas Quality Office
Huntersville Raleigh[ Mechanicsville❑
ConditionSample Client Narne-
Upon Receipt
Project #:
Courier: (Caed Ex PS CUSPS []Client
❑ Commercial `ace ❑Other: 912385030
CustodV Seal Present? [:]Yes Seals Intact? ❑Yes 7" oY
7`— Date/Initials Person ExamzingC�
Packing Material: ❑Bubble Wrap ubble Bags []None❑ Other Biological Tissue Frozen?
Thermo et • )10 []Ye ❑N/A
Gun ID:
92T040 Type of lee: wet ❑Blue [—None
Cooler Temp {'C): Correction Factor: Add/Subtract ('Cj +0.4
Temp should be above freezing to 6'[
Cabler Temp Corrected ('C): (]samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soi N/A, water sample)
Did samples o%nat in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did simples originate from a foreign source (int tionally,
❑Ye- j]�o including Hawaii and Puerto Rico)? []Yes �o
Comments/Discrepancy:
Chain of Custody Present?
C Y
No
N/A
I.
Samples Arrived within Hold Time?
[]No
❑N/A
2,
Short Hold Time Analysis (<72 hr.?
es
N/A
3.
Rush Turn Around Time Requested?
myeA
a
N/A
4.
5.
Sufficient Volume? es No NIA
Correct Containers Used?
-Pace Containers Used?
es
C es
[]NO'
1771NO
❑N/A
N/A .
6.
Containers Intact?
es
❑No
N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
ONO
/A
8.
Sample Labels Match COCl
-Includes Datefrime/ID/Anal is Matrix:
149A
[:]No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
Yes •
UNG
LIMIA
10.
Trip Blank Present?
Trip BlankCustody Seals Present?
❑Yes
ves
o
No
N/A
/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Tlme:
Field Data Required? ❑Yes []NO
Project Manager SCURF Review: Date: r
Project Manager SRF Review: "C Date: 5 f
Page 13 of 15

Document Name:
Document Revised: February 7, 2018
— -- aE@Aftalj�ttgl
Sample Condition Upon Recei tISCUR)
Page 1 of 2
-Document No.,
F-CAR4S-033-Rev.06
lswingAuthorlty:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, D110/8015 (water) DOC, tLHg
"Bottom half of box is to list number of bottle .
Project # - Wp# : 92385030'
PM: MW6 Due Date: 05/25/18
-CLIENT:-82-Allvac-NC-- -- - — - -
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot p
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of tnls mrrn will oe sent to the nvru, %armew ulna «�.�,��a��.,.� �..��� ,•s.
Out of hold, incorrect preservative, out of temp, incorrect containers,
Page 14 of 15

Stormwater Monitoring
Chain of Custody Record
Project Number/Name: SW Outfall #01(B)
Project Location: AT[ SM - Bakers
Sample Is-Siature:_
AAI
Date:-; S B —
z
a, v
e
6
L
ao',
F,
Requested Test Parameters
O
C.
T
G
-/®
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc
G
G /(D
HNO3
Y
Cadmium 0 Q
G
Q / P
HCL
Y
Oil & Grease
'
G
G /0
H2SO4
Y
COD 1
G
G /®
None
Y
BOD -
G
G /(D
None
Y
TSS (!�
3:
G
G /(D
None
Y
Residual Chlorine Cho L
Onsite
Vield pH,Anallsis
Onsite Field Temperature Anal sis
pH: ���(s.a.)
Sample Time: y
Temp: a8. y M) Sample Time:
Analysis Time:
3 'S�,...
Analysis Time: e.
Meter Calibrated: j�G
Thermometer Calibrated: ( / N
Sampling and field analysis completed by:
Relinquished By:
Received By: `ctA-k
Date: ,T—f
Time: 7 • ,�,�
Date: ,S _
Time ';; t
Relinquished By:
vrr act.
Receive Ord1�-
Date: A4
ITime:
Date: U
Time:
EHS-SW-Chain of Costody Outfall 01-Rev 001
Page 15 of 15

*AT1 Allvac
Allvac - Bakers Plant
Stormwater Monitoringport Form
Sample Date:
Sample'Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Sample Time: �3a T�---
Stormwater Discharge Outfall #02 (Lion -Commingled)
Drainage Area = 212,952sq.ft. = 4.9 acres
% Impervious = 12%
cariaC _Aloe,
/mace z4na
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
O
120
TSS
a3 y. O
100
Cadmium
0.001
Chromium, total recoverable
S
1
Copper, total recoverable
D. / 7
0.007
Nickel, total recoverable
O Oy
0.26
Zinc, total recoverable
?A1
0.067
pH
9 (std units)
6-9 (std units)
Storm Date: S �l5"-/B Storm Duration: Z - 05' (Hrs.) Inches of Rainfall: O. aS
Duration of time preceding rain event exceeding 0.1 ": � (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., efs) = (A x inches rain/] 2 inches/ft. x 4.9 acres x .88) + .9 x inches rain/12inches/ft. x 4.9 x .12)
Q(Total, cfs) = 0.1437 x S (Inches of rain) + 0.0441 x 0- a6- {Inches of rain)
40. OY6 9 cfs

ll
e Analytical
www.pm*lebs.corn
May 29, 2018
Mr. Joe Hinkle
Allvac
RE: Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
Dear Mr. Hinkle:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 16, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, '
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

Iacl
nalyfical
(�
www.p9celebs.o0m
Project: SW OUTFALI_ #02 (B)
Pace Project No.: 92386032
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HuntersvUle, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
LouisianalNELAP Certification # L,A170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87M
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florid a/N ELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, LLC, Page 2 of 13

ladieAn.aIX"rcal
www.pn[ebbs-wm
SAMPLE ANALYTE COUNT
Pace AnatyticaI Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
SW OUTFALL #02 (B)
Pace Project No.:
92385032
Analytes
Lad ID
SamplelD
Method
Analysts
Reported
Laboratory
92385032001
SW OUTFALL #02
EPA 200.7
SH1
5
PASI-A
SM 2540D
MVC
1
PASI-A
SM 5210B
RLO
i
PASI-A
SM 5220D
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13

(� acMnalyfical
w".peceisb&o=
ANALYTICAL RESULTS
Pace Analytical Services, LLC
98aa Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
Sample: SW OUTFALL #02 Lab ID: 92385032001 Collected: 05/15/18 15:30 Received: 05/16118 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
Field Data
Analytical Method:
Collected By
DPJ
1
05/15/18 15:30
Collected Date
05115/18
1
05/15/18 15:30
Collected Time
15:24
1
05/15/18 15:30
pH
6.9 Std. Units
0.10
1
05/.15/18 15:30
Temperature
26.1 deg C
0.50
1
05/15/18 15:30
200.7 MET tCP
Analytical Method: EPA 200.7 Preparation Method: EPA
200.7
Cadmium
ND ug1L
1.0
1
05/24/1815:10 05125/1815:07
7440-43-9
Chromium
44.6 ug/L
5.0
1
05124/1815:10 05125/1815:07
7440-47-3
Copper
170 ug1L
5.0
1
05/2411815:10 05125/1815:07
7440-50-8
Nickel
41.0 ug1L
5.0
1
05/2411815:10 05125/1815:07
7440-02-0
Zinc
194 ug1L
10.0
1
05/2411815:10 05125/1815:07
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
234 mg1L
25.0
1
05/21/18 20:54
521013 SOD, 5 day
Analytical Method: SM 5210B
BOD, 5 day
4.6 mg1L
2.0
1
05/17/18 07:38 05/22/18 02:47
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
57.0 mg1L
25.0
1
05125/18 16:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 13

laciMnaly­tkal
www.Peceisbs.cont
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
QC Batch: 412205
QC Batch Method'. EPA 200.7
Associated Lab Samples: 92385032001
METHOD BLANK: 2286555
Associated Lab Samples: 92385032001
Parameter
Cadmium
Chromium
Copper
Nickel
Zinc
QUALITY CONTROL DATA
Analysis Method: EPA200.7
Analysis Description: 200.7 MET
Matrix: Water
Units
Blank
Result
Reporting
Limit
Analyzed
ug/L
NO
1.0
0512511817:41
uglL
NO
5.0
0512511817:41
uglL
NO
5.0
05/2511817:41
ug1L
NO
5.0
0512511817:41
uglL
NO
10.0
0512511817:41
Qualifiers
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2286556
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
uglL
500
491
98
85-115
Chromium
uglL
500
524
105
85-115
Copper
ug1L
500
548
110
85-115
Nickel
uglL
500
509
102
85-115
Zinc
ug1L
500
476
95
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2286557
2286558
MS
MSD
92384986001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
NO
500
500
515
523
103
104
70-130
2
Chromium
ug1L
ND
500
500
546
555
109
111
M130
2
Copper
ug1L
2030
500
500
2580
2610
110
117
70-130
1
Nickel
uglL
5.1
500
500
532
541
105
107
70-130
2
Zinc
uglL
159
500
500
653
562
99
101
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2286559
2286560
MS
MSD
92385205002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Cadmium
ug1L
ND
500
500
504
491
100
98
70-130
2
Chromium
ug1L
5.7
500
500
6080
5940
71
44
70-130
2 M6
mg1L
Copper
ug1L
0.88
500
500
1390
1380
103
100
70-130
1
mglL
Nickel
ug1L
0.13
500
500
650
630
104
100
70-130
3
mg1L
Zinc
ug1L
12.6
500
500
13400
13300
163
158
70-130
0 M6
mglL
Results presented on this page are in
the units Indicated by the
"Units" column except where an alternate unit Is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 13

laneAnalyiical
W"..pacefabs.cont
QUALITY CONTROL DATA
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
QC Batch: 411695
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2 540 D Total Suspended Solids
Associated Lab Samples: 92385032001
METHOD BLANK: 2284017
Matrix:
Water
Associated Lab Samples: 92385032001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND
2.5 05121/18 20:49
LABORATORY CONTROL SAMPLE: 2284018
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250
256
102 90-110
SAMPLE DUPLICATE: 2284019
92384724001
Oup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg1L
ND
ND
SAMPLE DUPLICATE: 2284020
92384905001
Dup
Parameter
units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg1L
ND
ND
Results presented on this page are In the units Indicated by the "Unite" column except where an atfernate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

lacmnalyiical.
www.pa[ B1eW.com
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
QC Batch: 411072
QC Batch Method: SM 5210B
Associated Lab Samples: 92385032001
METHOD BLANK: 2280664
Associated Lab Samples: 92385032001
Parameter
BOD, 5 day
QUALITY CONTROL DATA
Analysis Method: SM 52108
Analysis Description: 5210E BOD, 5 day
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg1L ND 2.0 05/22/18 02:12
LABORATORY CONTROL SAMPLE: 2280665
Spike LCS
Parameter Units Conc. Result
BOD, 5 day mg1L 198 169
SAMPLE DUPLICATE: 2280666
92385027001 Dup
Parameter Units Result Result
BOD, 5 day mg/L 10.5 11.5
Pace Anatytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
85 84.6-115.4
RPD Qualifiers
9
Results presented on this page are In the units Indicated by the "units" column except where an alternate unit In presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13

laceAnalytrcal e
www.paoelahs.cam
QUALITY CONTROL DATA
Project: SW OUTFALL #02 (B)
Pace Project No.: 92385032
Pace Anatytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 412405
Analysis Method: SM 5220D
QC Batch Method: SM 5220D
Analysis Description: 5220D COD
Associated Lab Samples: 92385032001
METHOD BLANK: 2287604
Matrix: Water
Associated Lab Samples: 92385032001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0
05/25/18 16:38
LABORATORY CONTROL SAMPLE: 2287605
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits
Qualifiers
Chemical Oxygen Demand mg1L
750
741
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287606
2287607
MS
MSD
92384807001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Chemical Oxygen Demand mg/L 272
100
100 360
363 88
91
90-110
1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287608
2287609
MS
MSD
92385152001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Chemical Oxygen Demand mg1L 298
100
100 386
395 88
97
90-110
2 M1
Results presented on this page are In the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC,
Page 8 of 13

Pace Analytical Services, LLC
c^nAml j'nare 9800 KinceyAve, Suite 100
rY( li ! Huntersville, NC 28078
WWW..pacelabS cam
(704)8759092
QUALIFIERS
Project: SW 0UTFALL #02 (B)
Pace Project No.: 92385032
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not he appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

ladieAnalyiical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW OUTFALL 02 (B)
Pace Project No.: 92385032
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92385032001
SW OUTFALL #02
92385032001
SW OUTFALL 902
EPA200.7
412205 EPA200.7
412413
92385032001
SW OUTFALL #02
SM 2540D
411695
92385032001
SW OUTFALL #02
SM 5210E
411072 SM 5210B
411089
92385032001
SW OUTFALL #02
SM 5220D
412405
Date: 05129/2018 04:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 13

Document dame: Document Revised: February 7, 2018
_ Sample Condition Upon Recelpt(SCURj Page 1 of 2
aceArrafyal Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ HuntersvillRaleigh[] Mechanicsville(]
Client Name: '''���Wiii O# : 92385032
Sample
UpoAT(
n ReceiptProject #: Ill II
Courier: Fed Ex UPS ❑US PS ❑Cllent
❑ Commercial Pace ❑Other: ` 92385032
Custody Seal Present? []Yes a Seals Intact? Dyes ( !0
+' Date/tnitiats Person Examin C {�
Packing Material: []Bubble Wrap ❑Bubble Bags one ❑ Other Bioioglca sue Frozen?
qt
❑Yes OW❑NIA
ThermOme C Type of Icc: ❑81ue ❑N[ne�R Gun ID: 92T040
Cooler Temp C). ,2 Correction Factor: Add/Subtract (•C) +0.4 Tempshould be above freezing to 6•C
Cooler Temp Corrected ('C): ' []Samples out of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Soil (ON/A, water sample)
Did samples onat( n quarantine zone within the United States: CA, NY, or SC (check maps)? old samples originate from a foreign source me tlonally,
ilYes r o 3nrn,dn¢ Flawan and Puerto Rica)? nYes o
Comments Discrepan :
Chain of Custody Present?
Y s
Na
N/A
1.
Sameles Arrived within Hold Time?
No
EJNiA
2.
Short !told Time Analysis 02 hr.)?
es
NIA
3.
Rush Turn Around Time Requested?
Elyes
N/A
4.
Sufficient volume?
s '❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
es
[_-]No
❑No
[]NIA
❑N/A
6.
Containers Intact?
No
On/A
7.
DISsolvedana sis: Samples Field Filtered?
Yes
[-]NO
/A
8.
Sample Labels Match COV
-Includes Date/Time/ID/Analysis Matrix:
(PCs
''TT'
❑No
❑N/A
9.
Headspace in VOA Vials (>S-6mm)?
❑Yes -
❑No
/A
10.
Trip Blank Present?
Tri Blank Custod Seals Present?
[]Yes
ves
o
❑Na
❑N/A
11.
7
COMMENTS/SAMPLE DISCREPANCY
Lot ID ofs lit containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
!vL
Date/Time:
Field Data Required? ❑Yes []NO
Date: 5~ f I G I I L
Date:
Page t t of 13

rJ
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10
cc
Remit
BP4U-125 mL Plastic Unpreserved (N/A) (0-)
BP3U-250 mL Plastic Unpreserved (N/A)
SPZU-500 mL Plastic Unpreserved (N/A)
BP1U-1 liter Plastic Unpreserved (N/A)
BP4S-125 mL Plastic H2SO4 (pH < 2) (CI-)
aP3N-250 mL plastic HNO3 (pH < 2)
SP4Z-125 mL Plastic ZN Acetate & NaOH (>9)
8P4C-12S mt Plastic N30H (pH > 12) (CI-)
WGFU-Wide-mouthed Glass jar Unpreserved
AG1U-1 liter Amber Unpreserved (N/A) (Cl-)
AG1H-1 liter Amber HCI (pH <2)
AG3U-250 mL Amber Unpreserved (N/A) (0-)
XxAG1S-1
liter Amber H2SO4 (pH < 2)
AG3S-250 mL Amber H2504 (pH < 2)
A63A(DG3A)-25D mL Amber NH40 (N/A)(CI-)
DG9H-40 mL VOA HCI (N/A)
VG9T-40 mL VOA Na25203 (N/A)
VG..-40 mL VOA Unp (N/A)
D69P-40 mL VOA HSP04 (N/A)
VOAK (fi vials per kit)-5035 kit (N/A)
V/GK (3 vials per kit)-VPH/Gas kit (N/A)
SPST-125 mL Sterile Plastic (N/A - tab)
SP2T-250 mL Sterile Plastic (N/A - lab)
I�
f
BP3A-Z50 ml. Plastic (NH2)ZSO4 (9.3-9.7)
AGOU-100 mL Amber Unpreserved vials (N/A) I
VSGU-20 mt Scintillation vials (N/A)
I
DG9U-40 mL Amber Unpreserved vials (N/A)
�► n �
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Stormwater Monitoring
Chain of Custody Record
Project-Number/Name: SW Outfall #02(B)—
Project Location: ATI-SNi = Bakers -
Sample 's Signature:
Date:
CL
z
G,,
6
>
'
u
C
Requested Test Parameters
k
CIO
A
H
...
c
7 2-
Wj-
,Lj E-
:3
G
G l0
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc
G
G AD
HNO3
Y
Cadmium Ov
G
G /0
H2SO4
Y
COD ('
G
G /®
None
Y
BOD (-)
3�
G
G /&
None
Y
TSS
Onsite field pH Analysis
Onsite Field Temperature Anal sis
PH: eq (s.u.) . Sample Time:
Temp: Q?;1 (°C) Sample Time:
Analysis Time: 3 �3
Analysis Time: 3d..
i
Meter Calibrated: Yes
Thermometer Calibrated: 6) / N
Sampling and field analysis completed b -
Relinquished B
Received -Lc
Date: S 6-
Time: •o25;�•.
Date:
Relinquished By:
Received
Date: �`�
Time:
Date:
Time: iQLtL
EFTS -SW -Chain of Costody Outfall 02-Rev 001
Page 13 of 13

ikATI Allvac
AIlvac - Bakers Plant
Stormwater Monitoring Report Form
Sample Date: S /S-/B
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analvsis:
Sample Time: .3 :9
Stormwater Discharge Outfall 403 (Non -Commingled)
Drainage Area = 336,580sg. ft. = 7.8 acres
% Impervious = 15%
pacea�v�;ca�
40 CFR Part 136
Parameter
Results (mg/i)
Benchmark Values (mg/1)
BOD
. 5-
30
COD
�O O
120
TSS
100
Cadmium
D
0.001
Chromium, total recoverable
D
1
Copper, total recoverable
0 O1P
0.007
Nickel, total recoverable
0. QQ 6
0.26
Zinc, total recoverable
, 0,15'-
0.067
pH
7 (std units)
6-9 (std units)
Storm Date: �T-ZS � Storm Duration: ) - 0 5- (Hrs.) Inches of Rainfall: D - aS'
Duration of time preceding rain event exceeding 0.1": _ 87, (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) = (A x inches rain/12 inches/ft. x 7.8 acres x .85) + .9 x inches rain/12inches/ft. x 7.8 x .15)
Q(Total, cfs) = 0.2210 x S (Inches of rain) + 0.0878 x _ Q _02 S _ (Inches of rain)
= a. O %7l cfs

aceAnalytical
wwiw.pecela6s.com
May 29, 2018
Mr. Joe Hinkle
Allvac
RE: Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on May 16, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

Pace Analytical Services, LLC
a 980o Kincey Ave. acmnalyfical Hunte sville, NC'28078
w wPecelabscom [phone]
CERTIFICATIONS
Project: SW DUTFALL #03 (B)
Pace Project No.: 92385033
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #; 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaAtELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 13

8
laneAnalytical
..pacelabs.carn
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
SW OUTFALL #03 (8)
Pace Project No.:
92385033
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92385033001
SW OUTFALL #03
EPA 200.7
SH1
5
PASI-A
SM 2540D
MVC
1
PASI-A
SM 5210B
RLO
1
PASI-A
SM 5220D
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13

aceAnalytrcal
www.pecebbs cam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
Sample: SW OUTFALL #03 Lab ID: 92385033001 Collected: 05/15/18 15:42 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
Field Data
Analytical Method:
Collected By
DPJ
1
05/15/18 15A1
Collected Date
05/15/18
1
05115/18 15:41
Collected Time
15:34
1
05/15/18 15:41
pH
7.2 Std. Units
0.10
1
05/15/48 15:41
Temperature
27.5 deg C
0.50
1
05/15/18 15:41
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA
2003
Cadmium
ND ug/L
1.0
1
0512411815:10
05/25/1815:09 7440-43-9
Chromium
ND ug1L
5.0
1
0512411815:10
05/2511815:09 7440-47-3
Copper
65.6 ug1L
5.0
1
0512411815:10
05/2511815:09 7440-50-8
Nickel
5.7 ug/L
5.0
1
0512411815:10
05/2511815:09 7440-02-0
Zinc
45.3 ug1L
10.0
1
05/2411815:10
05/2511815:09 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
22.2 mg1L
5.0
1
05/21118 20:55
5210E BOD, 5 day
Analytical Method: SM 5210B
BOD, 5 day
6.5 mg/L
2.0
1
05/17/18 07:38
05/22/18 02A9
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
50.0 mg/L
25.0
1
06125/18 16:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05129/2018 04:41 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 13

kmnalyitrcal
www.paoelebs, oom
QUALITY CONTROL DATA
Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 412205
Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92385033001
METHOD BLANK: 2286555
Matrix: Water
Associated Lab Samples: 92385033001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Cadmium
uglL
ND 1.0
05/2511817:41
Chromium.
ug1L
ND 5.0
05/2511817:41
Copper
uglL
ND 5"0
0512511817:41
Nickel
ug1L
ND 5"0
05125/1817:41
Zinc
ug1L
ND 10.0
06/25/1817:41
LABORATORY CONTROL SAMPLE:
2286556
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Cadmium
ug1L
500
491
98
85-115
Chromium
ug1L
500
524
105
85-115
Copper
ug1L
500
548
110
85-115
Nickel
ug/L
500
509
102
85-115
Zinc
ug1L
500
476
95
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2286557
2286558
MS
MSD
92384986001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter
Units
Result
Conc"
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Cadmium
uglL
ND
500
500 515
523
103 104
70-130
2
Chromium
ug1L
ND
500
500 546
555
109 Ill
70-130
2
Copper
ug1L
2030
500
500 2580
2610
110 117
70-130
1
Nickel
ug1L
5.1
500
500 532
541
105 107
70-130
2
Zinc
ug1L
159
500
500 653
662
99 101
70-130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2286559
2286560
MS
MSD
92385205002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Cadmium
ug1L
ND
500
500
504
491
100
98
70-130
2
Chromium
ug1L
5.7
500
500
6080
5940
71
44
70-130
2 M6
mg1L
Copper
ug1L
0.88
500
500
1390
1380
103
100
70-130
1
mg/L
Nickel
ug1L
0,13
500
500
650
630
104
100
70-130
3
mg1L
Zinc
uglL
12.6
500
500
13400
13300
163
158
70-130
0 M6
mg1L
Results presented on this page are In
the units Indicated by the
"Units" column except where an alternate unit Is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 13

lacbAnalyiical
WWW.PB elabs.com
QUALITY CONTROL DATA
Project: SW OUTFALL#03 (8)
Pace Project No.: 92385033
QC Batch: 411695 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description'. 2540D Total Suspended Solids
Associated Lab Samples: 92385033001
Pace Analytical Servlcee, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875r9092
METHOD BLANK: 2284017
Matrix: Water
Associated Lab Samples: 92385033001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND 2.5
05/21/18 20:49
LABORATORY CONTROL SAMPLE: 2284018
Spike LCS
LCS % Rec
Parameter
Units
Cone. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 256
102 90-110
SAMPLE DUPLICATE: 2284019
92384724001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L ND ND
SAMPLE DUPLICATE: 2284020
92384905001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L ND ND
Results presented on this page are in the units Indicated by the "Untis" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 13

le
Analytical
wwwpac&bS.com
QUALITY CONTROL DATA
Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 411072
Analysis
Method:
SM 5210B
QC Batch Method: SM 5210B
Analysis
Description:
5210B BOD, 5 day
Associated Lab Samples: 92385033001
METHOD BLANK: 2280664
Matrix: Water
Associated Lab Samples: 92385033001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
BOD, 5 day
mg1L
ND 2.0 05/22/18 02:12
LABORATORY CONTROL SAMPLE: 2280666
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
BOD, 5 day
mg1L
198
169
85 84.6-115.4
SAMPLE DUPLICATE: 2280666
92385027001 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg1L 10.5 11.5 9
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/2912018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 13

laneAnalytical
wwwpecelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
[phone]
Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
QC Batch: 412405
Analysis Method: SM 5220D
QC Batch Method: SM 5220D
Analysis Description: 5220D COD
Associated Lab Samples: 92385033001
METHOD BLANK: 2287604
Matrix: Water
Associated Lab Samples: 92385033001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg1L
ND 25.0
05/25/18 16:38
LABORATORY CONTROL SAMPLE: 2287605
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits
Qualifiers
Chemical Oxygen Demand mg1L
750
741
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287606
2287607
MS
MSD
92384807001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Chemical Oxygen Demand mg1L 272
100
100 360
363 88
91
90-110
1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2287608
2287609
MS
MSD
92385152001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Chemical Oxygen Demand mg1L 298
100
100 386
395 88
97
90-110
2 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC,
Page 8 of 13

e
(�IaneAnalytical
www.pacelebs com
QUALIFIERS
Project: SW OUTFALL #03 (B)
Pace Project No.: 92385033
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
Mt Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/29/2018 04:41 PM without the written consent of Pace Analytical Services, LLC, Page 9 of 13

156e.,1,W1ytrcal
Nw.pecelabs WM
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
SW OUTFALL #03 (B)
Pace Project No.:
92385033
Analytical
Lab ID
Sample ID
QC Batch Method
GC Batch Analytical Method
Batch
92385033001
SW OUTFALL #03
92385033001
SW OUTFALL #03
EPA 200.7
412205 EPA 200.7
412413
92385033001
SW OUTFALL #03
SM 2540D
411695
92385033001
SW OUTFALL #03
SM 5210E
411072 SM 5210B
411089
92385033001
SW OUTFALL #03
SM 5220D
412405
Date: 05/29/2018 04:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 13

Document Name:
Document Revised: February 7, 2018
C8/ir'18iC3�
Sam !e Condition U on Recei t SCUR
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Qualily Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville(V Raleigh[] Mach anicsville❑
ConditionSampip Client Name:
Upon Receipt�r Project #•WO# ■-92385033F
Courier: Fed Ex ❑UP5 ❑LISPS ❑Cllent II I II� I I I� I�Ir I I II I �II
❑ Commercial ace ❑Other: I
— — 92385033
Custody Seat Present? []Yes o Sealslntact? Oyes QMWo
Date/initials Person Examining Con nts: Vl {�
Packing Material: []Bubble Wrap ❑Bubble Bags �ne ❑ Other 9lologfc I Tissue Frozen?
Thermomet �' ❑YeWNo []N/A
927+O4d Type of Ice: Vet et ❑Blue ❑None
Gun lD:� �■k�
Cooler Temp j'C): �1. 1 _ Correction Factor: Add/Subtract ('C) +0.4 Temp should be above freezing to fi'C
Cagier Temp Corrected ('C):
❑Samples out of temp criteria. Samples on Ice, coaling process
has begun
USDA Regulated Soil N/A, water sample)
Did samples oIn �Inat arantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {Internationally,
Oyes, go Including Hawaii and Puerto Ricoi? ❑yes
Camments/Discre an :
Chain of Custody Present?
es
❑No
❑NIA
1.
Sam les Arrived within Hold Time?
es
No
N/A
2.
Short Hold Time Analysis 42 hr.)?
QNO
N/A
3.
Rush Turn Around Time Requested?
❑Yes
o
n N/A
4.
Sufficient Volume?
es
❑No
❑N/A
$.
Correct Containers Used?
-Pace Containers Used?
es
❑No
[]No
❑N/A
N/A .
6.
ContalnerS Intact?
UYes
❑No
N/A
7,
Dissolved analysis: Samples Field Filtered?
Yes
❑No
NIA
g.
Sample Labels Match COC?
-Includes Date/Inme/ID/Anal is Matrix:
Y
❑Na
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
ao
N/A
10.
11.
Trip Blank Present? []yes o ❑
Trip BlankCustody Seals Present? Yes ❑No
COMMENTS/SAMPLE DISCREPANCY
Lot ID of s lit containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
Field Data Requlred7 ❑Yes []NO
Project Manager SCURF Review: Date:
Project Manager SRF Review: / Date:
Page 11 of 13

Document Name:
Document Revised: February7, 2018
h�
ciCB�!)Ci'y `lC�•
Sample Condition Upon Recei t{SCUR)
Page 1 of 2
Document'Na.:
Issuing Authority:
1
F-CAR-0-033-Rev.06
Pace Carolinas Quality office
*Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box Is to list number of bottle
Project #; WO# 2385033
PM: MWB Due Date: 09/25/18_
CL I Elf T : 92-IA 11 vac NC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjuted
Amount of Preservative
added
Lot M
Note: Whenever there is a discrepancy attecting North Carolina compliance samples, a copy or rnis Worm wui oe sent to the Norco taruunu ucnlrn �c uu�nu� �•• �_,••�•
Out of hold, lncorrtct preservative, out of temp, incorrect containers.
Page 12 of 13

Stormwater Monitorin
Chain of Custody Record
Project-Number/Name:
SW Outfall #03 B
Project Location: ATI SM - Bakers
Sample 's Si nature:
v
Date: S ,� Lif
z II
U
E-4
VRequested
Test Parameters
w•�
A
E"
L
O
`a
a
H
c
d
T
- f
G
G !®
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc
3
G
G I O
HNO3
Y
Cadmium G�a�
G
G /0
H2SO4
Y
COD {
•' 9
G
G 10
None
Y
BOD �� r
3 r3
GI
G /&
I None
Y
TSS
Onsite INU2H Analysis
Onsite Field Temperature Analysis
pH: 7. a (s.u.)
Sample Time:
Temp: (°C) Sample Time:
Analysis Time:
.�
Analysis Time: 3•:3
Meter Calibrated: yo
Thermometer Calibrated: 0 1 N
Sarneling and field analysis completed b
Relinquished B :
Received wv�►�- r' .�,
Date: 6•-/6 -
Time:
Date:
Relinquished B
�>r cL,.c;,-
IReceiveqBh
III f)/Ij2( ;
Date: �f (; -% (,
Time: Z
Date:
ime:
EHS-SW-Chain of Costody Outfall 03-Rev 001
Page 13 of 13

Allvac - Bakers Plant
Stormwater Monitoring_ Report Form
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Non-ContactCooling Wastewater
_ j)a,,4 Pole. J9 - , e .r Dion
lace }�r+a �V i'rca.l
40 CFR Part 136
OATI
Non-
Contact
Cooling
Water # ,
Sampling
Date
i
Sampling
Time
Estimated
Flow(MGD)
Total
Residual
Chlorine
(mg/L)
Temperature
pH (std. units]
Effluent
Downstream
Upstream
1
s
140Da..
oo s-8
0.03
30 . Y
d 8. a
8. S
. S
2
s-
= 000.
©• aoaa
0.03
2 2 70c
2A .30'-
. 30r
2. 3
3
S-
-'p?3,h=
A9,09
Q • DS
3.8`-
. 3°',
48.100
7• Y
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0?6. 9 "`
, y °C
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0"26.904
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O D1'Yy
a• aS
o? 3°`
a?8'Y
d8.3°G

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000312? 9
FACILITY NAME 0�Tr A1IJ14C, QXers
PERSON COLLECTING SAMPLE ) rw.o( a
CERTIFIED LABORATORY(S) JacC 2yC4 Lab
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: g"
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY (ZA,r 0
PHONE NO. ( lay )���15//
SIGNATURE OF PERMI WEE OR DESIGNEE
REQUIRED ON PAGE 2.
•
Date
Sample
Collected-
!! E
otal
Rainfall
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes _no
(if yes, complete Part B)
Part B. Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
aVDI.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mold r
MG
inches
MgA
m9A
unit
gaumo
Form SWU-247, last revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date S �-
Total Event Precipitation (inches):
Event Duration (hours): i. os- (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable -- see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permi ee) (Date)
Form SWU-247, last revised 21212012
Page 2 of 2

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling oul this form, please visit https://dea.nc.t;ov/about/divisions/energy-mineral-land-
resources/ener mineral -land- ernits/stormwater- ermitsln des-industrial-sw#tab-4
Permit No.: NIC1S1_01 1_01_jIAIQI or Certificate of Coverage No.: NICIGI_I 1_I_I_I_I
Facility Name: /9rx Allpa.c —2?4,krrs
County: _ GtAIOA Phone No. 'f0Y-vZ89—AI.171
Inspector: aviQ% /a e up
Date of Inspection:
Time of Inspection: 3 : S
Total Event Precipitation (inches): 0. o�'.�i
All permits require qualitative monitoring to be perfonned during a "treasurable storm event."
A "measurable storm event" is a stone event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the pernittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the pernittee obtains approval from the local DEMLR
Office.
By this signature, 1 certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. . Structure (pipe, ditch, etc.):
Receiving Stream:
SPd t IV&U
Dry Creek
Describe the industrial activities that occur within the outfall drainage area:
- /v? Brio, I Sfony e
Page 1 of 2
SWU-242, last modified 07/28/2017

2. 'Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: G%ea.lr
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): /VOA e
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
© 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stonnwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
© 2 3 4 5
b. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
7.
8.
9.
0 2 3 4 5
Is there any foam in the stormwater discharge? O Yes O©No.
Is there an oil sheen in the stormwater discharge? OYes E?)No. _
Is there evidence of erosion or deposition at the outfall? O Yes B No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe 1Vd
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. 'These conditions warrant further investigation.
Page 2 of 2
S W U-242, Last modi lied 0712812617

K�'Ir-v.
Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling ow this form, please visit https:Hdeq.nc.gov/about/divisions/energy-mineral-land-
resou rces/energy-mineral-1and- perm its/stormwater-permitslnpdes-industrial-sw##tab-4
Permit No.: NICI51 D 10101J I,1.Q1 or Certificate of Coverage No.: NICIGI—I—I—I I_I I
Facility Name: AT�_ A161,4kG -I&Ars
County: &Al.;9 ! Phone No. 7291Y07"-'t/S//
Inspector: D'.411d Age 31 t
Date of Inspection: 4r::
Time of Inspection:
Total Event Precipitation (inches): LO. a S
All pennits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the pennitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the pennittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. Outfall Description:
Outfall No. 95h6cU Structure (pipe, ditch, etc.): _ Pipe
Receiving Stream: _
Describe the industrial activities that o6cur within the outfall drainage area:
Page 1 of 2
SWU-242, Lasl modified 07/28/2017

2. 'Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: Clear
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.); /✓one,
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 © 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 ® 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 © 3 4 5
7. is there any foam in the stonnwater discharge? O Yes e)No.
8. Is there an oil sheen in the stormwater discharge? OYes (DNo.
9. Is there evidence of erosion or deposition at the outfall? O Yes ONo.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe &oI7 e
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https://deg.ne.gov/about/divisions/eiiergy-mineral-land-
resou rces/energy-mineral_land -nermits/storm water-permits/npdes-industrial-sw#tab-4
Permit No.: 01j1d1�1 or Certificate of Coverage No.: NIC/GI 1_I_I
Facility Name: A77- Al/yQC-2?AK&-x
County: &A4� /r Phone No. 'jQ�- �9 �•a/S/%
Inspector: 21?4Wt, A a --YR.
Date of Inspection:
Time of Inspection: .3 'S�l�.o•.r
Total Event Precipitation (inches): e . o?$'
All permits require qualitative monitoring to be perfonned during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local stone events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Pennitfee d besignee)
1. Outfall Description:
Outfall No. SW Structure (pipe, ditch, etc.)
Receiving Stream:
i e �
Describe the industrial activities [hat occur within the outfall drainage area:
Page 1 of 2
SWEI-242, Last modified 07,2812017

2. 'Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: G%Bar- T_
3. ' Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): • AL -me,
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
C 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7.
8.
9.
© 2 3 4 5
Is there any foam in the stormwater discharge? O Yes ®No.
Is there an oil sheen in the stormwater discharge? OYes eNo.
Is there evidence of erosion or deposition at the outfall? O Yes (qNo.
to. Other Obvious Indicators of Stormwater Pollution:
List and describe eo e
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242. Last mmliGed 07/28/2017

Ip
Analyt cal
www.pawiabs.com
May 24, 2018
Mr. Joe Hinkle
Allvac
RE: Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Anatytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on May 16, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
pcm
a REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
B
Page 1 of 20

Pace Analytical Services, LLC
18c,Amlytical • 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabscom [phone]
CERTIFICATIONS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Charlotte Certification IDs
9800 Kincey Ave. Ste 100. Huntersville, NC 28078
LouisianalNELAP Certification # L.AI70028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, INC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification #: 37712
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELPAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

Pace Analytical Services, LLC
aceAmly Kcal a
9800 Kincey Ave. Suite 100
Huntersville,
NC 28078
www.pacelsAs.cmr
[phone]
SAMPLE ANALYTE COUNT
Project:
NONCONTACT COOLING WATER
Pace Project No.:
92385034
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92385034001
NONCONTACT #1
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92385034002
NONCONTACT #2
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92385034003
NONCONTACT #3
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92385034004
NONCONTACT #4
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92385034005
NONCONTACT #5
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92385034006
NONCONTACT #6
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92385034007
NONCONTACT #7
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
92385034008
NONCONTACT #8
EPA 16648
JMS
1
PASI-C
SM 4500-CI G
EWS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This reportshall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 20

lacmnalXicale
www.paoajabs.com
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Sample: NONCONTACT #1 Lab ID: 92385034001 Collected: 05/15/18 10:40 Received: 05116/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 1 05/24/18 05:02
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.036 mg1L 0.024 1 05/22/18 10:40 7782-50-5 H6
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 20

0
ac.eAnalytical
www.paeelab&com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Sample: NONCONTACT #2 Lab ID: 92385034002 Collected: , 05/15/18 11:00 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16648
Oil and Grease 14.9 mg1L 5.0 1 05/24/18 05:03
4500CL G Chlorine, Residual Analytical Method: SM 4500-Cl G
Chlorine, Total Residual 0.039 mg1L 0.024 1 05/22/18 10:40 7782-50-5 H6
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 20

laneAnalyfical"
www.pacelabs com
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NONCONTACT #3 Lab ID: 92385034DD3 Collected: 05/15/18 11:23 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 05124/18 05:06
4600CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.053 mg/L 0.024 1 05122/18 10:40 7782-50-5 H6
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 20

(�IacleAnalytical
wnrw.pecala8a,cam
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)87"092
Sample: NONCONTACT #4 Lab ID: 92385034004 Collected: 05/15/18 11:45 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 05/24/18 05:07
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.40 mg1L 0.048 2 05/22/18 10:40 7782-50-5 H6
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in futl,
without the written consent of Pace Analytical Services, LLC,
Page 7 of 20

1e
ace, Analytical
mvw.pacelatu.Com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Sample: NONCONTACT #7 Lab ID: 92385034007 Collected: 05/15/18 12:52 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 1 05/24/18 05:08
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.097 mg1L 0.024 1 05/22/18 10A0 7782-50-5 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/24/2018 06:42 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 20

•
.eAna0cal
www.pocelahacom
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: NONCONTACT #8 Lab ID: 92385034008 Collected: 05/15/18 13:15 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 166413
Oil and Grease ND mg1L 5.0 1 05/24/18 05:08
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.051 mg/L 0.024 1 05122/18 10:40 7782-50-5 H6
Date: 05/2412018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 20

(�IacloAnalyficale
www.pacelaba-com
QUALITY CONTROL DATA
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 412124
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664E
Analysis Description:
1664 HEM, Oil and Grease
Associated Lab Samples: 92385034001, 92385034002,
92385034003, 92385034004,
92385034005, 92385034006, 92385034007,
92385034008
METHOD BLANK: 2286233
Matrix: Water
Associated Lab Samples: 92385034001, 92385034002,
92385034003, 92385034004,
92385034005, 92385034006, 92385034007,
92385034008
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Oil and Grease mg/L
ND 5.0 05/24/18 04:56
LABORATORY CONTROL SAMPLE: 2286234
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Oil and Grease mg/L
38.5 36.9
96 78-114
MATRIX SPIKE SAMPLE: 2286235
92385786001 Spike
MS MS % Rec
Parameter Units
Result Conc.
Result % Rec Limits Qualifiers
Oil and Grease mg&
ND 38.5
39.5 103 78-114
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/24/2018 06:42 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 20

(�IacleAnaOcal
»ww.pecelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HurtersvNe, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
QC Batch: 411753 Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92385034001, 92385034002, 92385034003, 92385034004, 92385034005, 92385034006, 92385034007,
92385034008
METHOD BLANK: 2284194 Matrix: Water
Associated Lab Samples: 92385034001, 92385034002, 92385034003, 92385034004, 92385034005, 92385034006, 92385034007,
92385034008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine, Total Residual mg1L ND 0.024 05/22/18 10:40
SAMPLE DUPLICATE: 2284195
92384160004 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg1L 0.41 0.45 8 H6
SAMPLE DUPLICATE: 2284196
92385030001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mglL 0.044 0.046 4 H6
Results. presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/24/2018 06A2 PM without the written consent of Pace Analytical Services, LLC,
Page 13 of 20

(�IaceAnalytical*
www.pacebbs.com
QUALIFIERS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the' analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN - The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/24/2018 06:42 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 20

e
aceAnaly{tical
www.pscebbs m"
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Lab ID Sample ID OC Batch Method OC Batch
92385034001
NONCONTACT #1
EPA 1664B
412124
92385034002
NONCONTACT #2
EPA 1664E
412124
92385034003
NONCONTACT #3
EPA 1664B
412124
92385034004
NONCONTACT #4
EPA 1664B
412124
92385034005
NONCONTACT #5
EPA 1664E
'412124
92385034006
NONCONTACT #6
EPA 1664E
412124
92385034007
NONCONTACT #7
EPA 16646
412124
92385034008
NONCONTACT #8
EPA 16648
412124
92385034001
NONCONTACT #1
SM 4500-CI G
411753
92385034002
NONCONTACT #2
SM 4500-CI G
411753
92385034003
NONCONTACT #3
SM 4500-CI G
411753
92385034004
NONCONTACT #4
SM 4500-CI G
411753
92385034005
NONCONTACT #5
SM 4500-CI G
411753
92385034006
NONCONTACT #6
SM 4500-CI G
411753
92385034007
NONCONTACT #7
SM 4500-Cl G
411753
92385034008
NONCONTACT #8
SM 4500-CI G
411753
Oate: 05/2412018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical Method
Analytical
Batch
Page 15 of 20

leAnalyfical
wwwpeoelabs com
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NONCONTACT #5 Lab ID: 92385034005 Collected: 05/15/18 12:10 Received: 05/16/18 16:42 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 1 05/24/18 05:07
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.22 mg/L 0.024 1 05/22/18 10:40 7782-50-5 H6
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 20

aGeAnal0cals
wwwpscelab,cam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )8759092
Project: NONCONTACT COOLING WATER
Pace Project No.: 92385034
Sample: NONCONTACT #6 Lab ID: 92385034006 Collected: 05/15/18 12:30 Received: 05/16/18 16A2 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 05/24/18 05:07
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.044 mg/L 0.024 1 05/22/18 10A0 7782-50-5 H6
Date: 05/24/2018 06:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 20

Document Name:
Document Revised: February 7, 2018
�alceft"a
Sample Condition Upon. Receipt(SCUR)_ _
Page 1 of 2
Document No.:
Issuing Authority:
I
F-CAR-CS•033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvil14 Raleigh❑ Mechanicsville El
SampleClient Name: W0E-;-9Z385034"Upon Receipt - -
Tr Project # j 11
Courier: ❑Fed Ex ❑UPS I (LISPS []Client
❑ Commercial t lace ❑Other: 92365034
Custody Seal Present? ❑Yes No Seals Intact? ❑Yes0
Date/initials Person Evamining ibnten
Packing Material: []Bubble Wrap q5bbie Bags []None❑ Other Blologtca ue Frozen?
Therrnom ❑Yes N/A
qte0. Gun ID:
92TO40 Type of Ice: t ❑Blue ❑None
Cooler Temp (•C): �, .1 I• I Correction Factor: Add/Subtract ('C) +0.4
'QQ�11 Temp should be above freezing to VC
Cooler Temp Corrected (•C). L� 05amples out of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Soil N/A, water sample)
Did samples o"ate in quarantine lone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (in er ionaily,
Myes n InAirrnir Hawaii and Puerto Rico)? nYes
Comm ents/Discrepancy:
Chain of CustodX Present?
es
CIA10
N/A
1.
Sam les Arrived within Hold Time?
54 6
[]No
N/A
2.
Short Hold Tlme Analysis (02 hr.)?
Yes
o
NIA
3.
Rush Turn Around Time Requested?
❑Yes
o
N/A
4.
Sufficient volume?
es
No
QNJA
5.
Correct Containers Used?
-Pace Containers Used?
es
❑ND
MN.
[]N/A
❑NIA .
6.
Containers Intact?
�742el
[]NO
[]N/A
7.
Dissolved analysis: Samples Field Filtered?
Yes
No
N/A
S.
Sample Ubels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
qes
[]No
❑N/A
5.
Heads ace In VOA Vials (>5-6mm)?
❑Yes
aD
10/A
1 10.
Trip Blank Present?
Trip Blank CustodySeals Present?
❑Yes
❑Yes
o
No
A
NIA
COMMENTSISAMPLE DISCREPANCY
:3 r
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Field Data Required? ❑Yes ❑No
Project Manager SCURF Review: Date:
Project Manager SRF Review: Data:
` t
Page 16 of 20

Document Name:
Document Revised: February 7, 2018
— — eeAlnalytkal•
Sample Condition Upon Recei t(SCUR)
Page 1 of 2
DacumentNo.:
tssuingAuthorW.
F-CAR-CS-033-Rev.06
Pace Carolinas Quallty Office
*Check mark top half of box if pH and/or dechlorination is Project #"WO# : 92385034
verified and within the acceptance range for preservation PM: MWB Oue Date: 05/25/18.
samples. 'CLIENT` S2-A11Vaa NC. "
Exceptions: VOA, Conform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot p
+vote: Whenever there is a discrepancy affecting north Carolina compliance samples, a copy or tins roan Will ne sent to the J—rn Lar „ a ��_ .� �••
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 17 of 20

'• ATI
Sntciahy h!alenari
Storm Water Mor�itorinQ
_ (NON CONTACT)
Bakers North
Chain of Custody Record
page 41
Project Number/Name: NonContact oling Water
Project Location: Allvac Bakers
Sampler's Signature:
Date:
o
a
"
G
°'
CL
s
0
CL
t?
a,
o
w
r
a
u
0
vs
QCIL
•
a
IJ
o
a
°
Requested Test
Parameters
G
Ge
None
Y
,3Q.
Residual Chlorine
tip
In..QQ,r.-
G
G,$
None
Y
Residual Chlorine
G
G/O
None
Y
7,
3. 8
Residual Chlorine
G
GAD
None
Y
7.,6
Residual Chlorine
S
G
G/p I
None
Y
Residual Chlorine
G
GM
None
Y
Residual Chlorine
G
G&
None
Y
Residual Chlorine
G
None
Y
72 5'
0?7.j
Residual Chlorine
_gZL
Meter Calibrated:
/ N
IThermometer Calibrated
®/ N
Sampling and Field analysis completed by:
Relinquished By:
JiFecelved
By:
,Date: S- 6 -
T1me:
p-
Date: -
Relinquished By:
c • [
Received
Date:
ITime:`
Date:
ICX
ITime:
EHS Baker South SW R6v p 2 5/10/2016
U,✓(
OeIL
Page 18 of 20

r
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3
w_
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0
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7
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0
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n v
n wa
n
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3
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R
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-
oa
14
rn
ut
a
w
N
,
hemp
BP4U-125 mL Plastic Unpreserved (N/A) (Cl-)
BP3U-250 mL Plastic Unpreserved (N/A)
MU-500 mL Plastic Unpreserved (N/A)
BPSU-1 liter Plastic Unpreserved (N/A)
BP4S-125 mL Plastic H2.SO4 (PH < 2) (Cl-)
BP3N-25O mt plastic HNO3 (pH < 2)
BP4Z-12S mL Plastic ZN Acetate & NaCH (>9)
BP4C-125 mL Plastic NaOH (pH > 12) (Cl-)
WGFU-Wide-mouthed Glass jar Unpreserved
AG1U-1 liter Amber Unpreserved (N/A) (CI-)
AG1H-1 liter Amber HCI (pH < 2)
AG3U-250 mL Amber Unpreserved (N/A) (CI-)
AG1S-1 liter Amber H2SO4 (pH < 2)
AG35-250 mL Amber H2SO4 (pH < 2)
AG3A(DGMA -250 mL Amber NH4CI (NJA)(CI-)
DG914-40 mL VOA HCI (N/A)
VG9T-40 mL VOA Na25203 (N/A)
VGDLJ-40 mk� VOA Unp (Fr/p.)
DG9P-40 mL VOA H3PO4 (N/A)
VOAK (6 vials per kit)-SO35 kit (N/A)
V/GK (3 vials per kit).VPH/Gas kit (N/A)
SPST-In mL Sterile Plastic (N/A— lab)
SP2T-250 mL Sterile Plastic (N/A— lab)
BP3A-250 mL Plastic (NH2)2SO4 (9.3-9.7)
AGOU-IDO mL Amber Unpreserved vials (N/A)
VSGU-20 mL Scintillation vials (NIA)
DG9U-40 mL Amber Unpreserved vials (N/A)

Storm Water Monitoring
(NON CONTACT)
Bakers North
Chain of Custody Record
4;: AT
Specialty Materials
page #2
Project Number/Name: NonContact Cooling Water
Project Location. Alivac Bakers
Sampler's Signature:
Date: ,s-
CIL
to
4J
o
°+
i
IE
ii
h
a
d
C
V
a
aa.
?
to
a
IO
a
°+
G
u
0
a
aE,
C
Requested Test
Parameters
ZZo
G
G
HCL
Y
,3p. y
Oil & Grease
G
G
HCL
Y
Oil & Grease
4,% ,,c
a,,.
G
G
HCL
Y
Oil & Grease
h(dwCeR
��.,
G
G
HCL
Y
Oil & Grease
S
0
G
G
HCL
Y
Oil & Grease
G
G
HCL
Y
Oil & Grease
414-twtI 7
G
G
HCL
Y
Oil & Grease
d.*
G
G
HCL
Y
d 7.3
Oil & Grease
Meter Calibrated: / N IThermorneter Calibrated: d / N
Sampling and field analysis completed by:
Relinquished By:
Relinquished By:
Date :5'/6 -
Time: 6 •;,yD�., pate ; -if -•[ �
Tfpie:
Relinquished 8 :
- 'FW 11104n4ulshed B :
Date: S• i (,' j :
Time , q-.
a
Ime:
EHS Baker South SW REV # 2 5/10/2016
rl
r_ia e�'
Page 20 of 20