NCS000329_MONITORING INFO_20180320

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
NC,, -7jZl�
DOC TYPE
0 FINAL PERMIT
-)(- MONITORING REPORTS ------ --
❑ APPLICATION
El
�] COMPLIANCE
❑ OTHER
DOC DATE
❑ ZO
YYYYMMDD

I�
March 13, 2018
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
RECEIVED
MAR 2 0 2018
CEN I r�AL FILES
r)VVR SECTION
3*ATI
P.O. Box 5030
2020 Ashcraft Avenue
Monroe, NC 281 11-5030
Phone: [phone]
Fax: [phone]
Email:.i oe.hinkl<a?atimetals.com
Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period
Sample Number
Start
I End
Year 8 — Period 2
16
September 1, 2017
1 Februa 28, 2018
Analytical monitoring includes:
• Outfall #01 (B), commingled stormwater
• Outfall #02 (B), non -commingled stormwater
• Outfall #03 (B), non -commingled stormwater
• Non Contact Cooling Water #1 - #8
1f you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerely,
Scott R
Environmental Manager

Allvac - Bakers Plant *ATIAllvac
Stormwater Monitoring Report Form
Sample Date: - a? 4 -Z8
Sample Location:
I Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Sample Time: -I-•
Stormwater Discharge Outfall #01 (Commingled)
Drainage Area = 2,915,470sg. ft. = 69 acres
% Impervious = 34%
Pace nad✓frCa/
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
Sd
30
COD
120
TSS
100
Cadmium
No
0.001
Chromium, total recoverable
1
Copper, total recoverable
0.007
Nickel, total recoverable
0.26
Zinc, total recoverable
AV
0.067
Oil and Grease
20
Temp (receiving stream)
(deg C)
32 (deg C)
Total Residual Chlorine
0.017
pH
- (std units)
6-9 (std units)
Storm Date: _a - /9 /R Storm Duration:. f • d 5- (Hrs.) Inches of Rainfall: 89. 3d
Duration of time preceding rain event exceeding 0.1": _ g!YiP (14rs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) = (A x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches rain/12inches/ft. x 69 x .34)
Q(Total, cfs) = 1.5180 x D •3d (Inches of rain) + 1.7595 x
©-so
(Inches of rain)

aceAnalyfical
www.pecelebs.ow
March 02, 2018
Mr. Joe Hinkle
Allvac
RE: Project: SIN OUTFACE_#01(Bj�
Pace Project No.: 92373887
Dear Mr. Hinkle:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 20078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 19, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
David Pope, Allvac
Scott Ryan, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 17

aceftljftal
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Project: SW OUTFALL #01(B)
Pace Project No.: 92373887
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certtfication IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
South Carolina Certification M 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VrginiaNELAP Certification #: 460221
North Carolina Wastewater Certification M 40
South Carolina Certification M 99030001
VrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
(704)B75-9092
Project:
SW OUTFALL #01(B)
Pace Project No.:
92373887
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92373887001
OUTFALL 1
EPA 200.7
SER
5
PASI-A
SM 2540D
MVC
1
PASI-A
SM 4500-CI G
MVC
1
PASI-A
SM 5210B
CDC
1
PASI-A
SM 5220D
NAL
1
PASI-A
92373887002
OUTFALL 1 O&G
EPA 1664B
JMS
1
PASI-C
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
98001(inceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #01(B)
Pace Project No.: 92373887
Sample: OUTFALL 1 Lab ID: 92373887001 Collected: 02/19/18 06:02 Received: 02/19118 12:14 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
02/19/18 06:01
Collected Date
02/19/18
1
02/19/18 06:01
Collected Time
05:55
1
02/19/18 06:01
pH
7.5 Std. Units
0,10
1
02/19118 06:01
Temperature
14.5 deg C
0.50
1
02/19/18 06:01
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA
200.7
Cadmium
ND ug/L
1.0
1
02/22/18 05:30
03/01/18 15:20
7440-43-9
Chromium
ND ug/L
5.0
1
02/22/18 05:30
03101/18 15:20
7440-47-3
Copper
15.3 ug/L
5.0
1
02/22/18 05:30
03101/18 15:20
7440-50-8
Nickel
ND ug/L
5.0
1
02122/1805:30
03/01/1815:20
7440-02-0
Zinc
ND ug/L
10.0
1
02/22/18 05:30
03/01/18 15:20
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
7.6 mg1L
5.0
1
02/23/18 01:37
4500CL G Chlorine, Residual
Analytical Method: SM 4500-CI G
Chlorine, Total Residual
0.084 mg1L
0.024
1
02/21/18 03:00
7782-50-5 D6,H1
5210E BOD, 5 day
Analytical Method: SM 5210B
BOD, 5 day
3.2 mg1L
2.0
1
02/20/18 18:14
02/25/18 17:07
B2,1-2
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
35.0 mg1L
25.0
1
02/22/18 14:45
R1
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SW OUTFALL #01(R)
Pace Project No.: 92373887
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: OUTFALL 1 O&G Lab ID: 92373887002 Collected: 02/19/18 06:04 Received: 02/19/18 12:14 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. 4ual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 02127/18 04:35
Date: 03/02/2018 12:12 PM
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SW OUTFALL #01(B)
Pace Project No.: 92373887
QC Batch: 399799 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92373887002
METHOD BLANK: 2217332
Associated Lab Samples: 92373887oo2
Parameter Units
Oil and Grease mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 02/27/18 04:29
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2217333
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 37.1
93
78-114
MATRIX SPIKE SAMPLE:
2217334
92373315004 Spike
MS -
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
38.2
96
78-114
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SW OUTFALL #01(B)
Pace Project No.: 92373887
QC Batch: 399194
QC Batch Method: EPA 200.7
Associated Lab Samples: 92373887001
Analysis Method:
Analysis Description:
EPA 200.7
200.7 MET
METHOD BLANK: 2214191
Matrix: Water
Associated Lab Samples: 92373887001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Cadmium
ug1L
ND
1.0
0310111814:23
Chromium
ug1L
ND
5.0
0310111814:23
Copper
ug1L
ND
5.0
03/0111814:23
Nickel
ug1L
ND
5.0
0310111814:23
Zinc
ug/L
ND
10A
03/0111814:23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2214192
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
ug/L
500
488
98
85.115
Chromium
ug1L
500
492
98
85-115
Copper
ug1L
500
500
100
85-115
Nickel
ug1L
500
487
97
85-115
Zinc
ug1L
500
493
99
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2214193
2214194
MS
MSD
92373852001
Spike
Spike
MS
MSD
MS
MSD
% Rea
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug1L
<0.0010
500
500
537
528
107
106
70-130
2
mg1L
Chromium
ug/L
<0.0050
500
500
482
473
96
95
70-130
2
mg1L
Copper
ug/L
0.050
500
500
553
540
101
98
70.130
2
mg1L
Nickel
ug1L
<0.0050
500
500
510
506
101
101
70-130
1
mg1L
Zinc
ug1L
0.075
500
500
559
555
97
96
70-130
1
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2214195
2214196
MS
MSD
92373647003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Cadmium
ug1L
ND
500
500
515
516
102
102
70-130
0
Chromium
ug1L
124
500
500
545
648
104
105
70-130
0
Capper
ug1L
ND
500
500
623
627
105
106
70-130
1
Nickel
ug1L
ND
500
500
572
570
98
98
70-130
0
Results presented on this page are in
the units Indicated by the
"Units" column except where
an alternate unit is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnaIXical
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QUALITY CONTROL DATA
Project: SWOUTFALL#01(B)
Pace Project No.: 92373887
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2214195 2214196
MS MSD
92373647003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Zinc ug/L 57200 500 500 59000 59800 360 528 70-130 1 M6
Results presented on this page are in the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC.
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aceAnalj&al
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QUALITY CONTROL DATA
Project: SW OUTFALL #01(5)
Pace Project No.: 92373887
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 399417
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92373887001
METHOD BLANK: 2215409
Matrix: Water
Associated Lab Samples: 92373887001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND
2.5 02/23/18 01:18
LABORATORY CONTROL SAMPLE: 2215410
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 262
105 90-110
SAMPLE DUPLICATE: 2215411
92374343001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
188
218 15 D6
SAMPLE DUPLICATE: 2215412
92374169002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg1L
6.2
6.8 9 D6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnaiytical
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Project: SW OUTFALL #01(B)
Pace Project No.: 92373887
QC Batch: 398980
QC Batch Method: SM 4500-CI G
Associated Lab Samples: 92373887001
METHOD BLANK: 2212953
Associated Lab Samples: 92373887001
Parameter
Chlorine, Total Residual
QUALITY CONTROL DATA
Analysis Method: SM 4500-CI G
Analysis Description: 4500CL G Chlorine, Total Residual
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mgJL ND 0.024 02/21/18 03:00
SAMPLE DUPLICATE: 2212954
92373887001 Dup
Parameter Units Result Result
Chlorine, Total Residual mg1L 0.084 0.051
RPD Qualifiers
49 DB,H1
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units indicated thy the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: SW OUTFALL #01(B)
Pace Project No.: 92373887
QC Batch: 398880 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day
Associated Lab Samples. 92373887001
METHOD BLANK: 2212480
Associated Lab Samples: 92373887001
Parameter Units
BOD, 5 day mg1L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 0212511817:07
LABORATORY CONTROL SAMPLE: 2212481
Spike LCS
Parameter Units Conc. Result
BOD, 5 day mglL 198 114
SAMPLE DUPLICATE: 2212482
92373898001 Dup
Parameter Units Result Result
BOD, 5 day mglL ND ND
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
58 84.8-115A 1-2
RPD Qualifiers
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/02/2018 12A 2 PM without the written consent of Pace Analytical Services, LI.C, Page 1 i of 17

aceMalytical
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f
Project: SW OUTFALL #01(B)
Pace Project No.: 92373887
QC Batch: 399148
QC Batch Method: SM 5220D
Associated Lab Samples: 92373887001
METHOD BLANK: 2214027
Associated Lab Samples: 92373887001
Parameter
Chemical Oxygen Demand
QUALITY CONTROL DATA
Analysis Method: SM 5220D
Analysis Description: 5220D COD
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg1L ND 25.0 0212211814:45
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2214028
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg1L 750 747 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2214029 2214030
MS MSD
92373205001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 238 100 100 348 348 110 110 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2214031 2214032
MS MSD
92373887001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 35.0 100 100 128 141 93 106 90-110 10 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
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aceMalytica! 9800 Kincey Ave. Suite 100
Huntersvifle, NC 28078
—pacelab co" [phone]
QUALIFIERS
Project SW OUTFALL #01(B)
Pace Project No.: 92373887
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation limit.
RL - Reporting Limit.
S - Surrogate•-
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenxene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H1 Analysis conducted outside the EPA method holding time.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
SW OUTFALL #01(B)
92373887
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92373887001
OUTFALL 1
92373887002
OUTFALL 1 O&G
EPA 1664B
399799
92373887001
OUTFALL 1
EPA 200.7
399194 EPA 200.7
399266
92373887001
OUTFALL 1
SM 2540D
399417
92373887001
OUTFALL 1
SM 4500-CI G
398980
92373887001
OUTFALL 1
SM 5210B
398880 SM 5210B
398953
92373887001
OUTFALL 1
SM 5220D
399148
REPORT OF LABORATORY ANALYSIS
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Document Name:
Document Revised: February 7, 2018
aCeAna! fC81
Semple Condition Upon Recei t(SCUR)
Page 1 of 2
Document No.;
Issuing Authority:
F-M-CS-033•Rev.06 I
Pace Carolinas QuallN Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ HuntersvillC2__1__ Raleigh❑ Mechanicsville❑
client Name: WO# : 92373887
Courier: Fed x ❑UPS USPS a Project
❑ Commercial ❑Pace ❑Qther; 92373887
Custody Seal Present? Elves f5go' Seals Intact? ❑Yes B116—_ c
Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap ❑Bubble Bags []None .-B- Offier Biological Tissue Frozen?
Thermometer: ❑Yes [:]No NNW'
r; 1— 92TO36 Type once: wet ❑Blue ❑None
Cooler Temp I'Q: 3, '7Correctlon Factor: Add/Subtract ('Cj +0,
Cooler Temp Corrected i'Q: ,
USDA Regulated Soll Jf5-147A, water sample)
Did samples original n a quarantine zone within the United States: CA, NY, or SC (check maps)?
Fly. s o
Temp should be above freezing to 6'C
[]Samples out of temp criteria. Samples on ice, cooling process
has begun
Dld ssmpW originate from a foreign source (internationally,
including Hawall and Puerto Rim)? nYes 49lrff--
Commenq Discre a
Chain of Custody Present?
es
Na
N/A
1.
Samples Arrived within Hold Time?
es
No
N A
2.
Short Hold Time Analysis e72 hr. ?.
a
No
N A
3.
Rush Tum Around TimeRequested?
Oyes
J2<o
N/A
4.
Sufficient Volume?
es
Nv
[INIA
5.
Correct Containers Used?
-Pace Containers Used?
es
[:]No
No
[]N/A
N A
6.
Containers Intact?
Yes
Na
N A
7.
Dissolved analysis- Samples Fleld Filtered?
pro
KO
NIA
B.
Sample labels Match COO
-includes Date/rime/ID/Analysis Matrix:
/
[]No
❑N/A
9.
Heads ace in VOA Vials >S-6mm ?
QYes
QNo
N/A
10,
Trip Blank Present?
Trip Blank Custodv Seals Present?
❑Yes
Yes
ONO
014o
A
t A
11,
COMMENTSISAMPLE DISCREPANCY
Field Data Required? []Yes ONO
Lot ID of split containers; _
CLIENT NDTIFICATN]N/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: li�i _ Date:
Project Manager 5RF Review: rt"' Date:
i
Page 15 of 17

Document Name:
Document Revised: February 7, 2018
IceAnalytica!
Sample Condition Upon Recel t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F•CAR-CS•033-Rev.05
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Eacapuona: VOA, Coliforrn, TOC, Oil and Grease, DRO/8015 (water) ODC, LLHS
**Bottom half of box Is to list number of bottle
Project # Wp# : 92373887
PH.- KWB Due Dale: 02/28/18
CLIENT: 82—Allvae NC
ri
0
61,
0
0
ME,
180,
61,
0
ME,
0
MEN
0
0
0
0
0
0
0
MINE
M
164L
0
0
MOORE
04
0
0
11 1
M
MEMO
0
0
0
0
0
0
0
0
61104
0
0
0
HE,�Ga��nai°a�aii�
0
i��i
WEL,iiaM�
10
0
0Ci�
iii
ii164LiMaai0
- - ---- - --- , -- -- -pH Adjustment Log for Preserved Samples -
Sample ID
Type of Preservathre
pH upon recelpt
Date prefervatlors adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot a
Note: Whenever there is a discrepancy affecting North Carolina Compliance sampres, a Copy al this lorm will W sent to the North Caroline OEHN8 Certincatlon urrlce tr.e.
Out of hold. Incorrect preservative, out of temp, Incorrect containers.
Page 16 of 17

Stormwater Monitoring
Chain of Custody Record
Project Number/Name:
SW Outfall #01(B)
1project Location: AT[ SM - Bakers
Sample 'S Sign
ure:
Date: 4
d
d
z Ir
Ey
`
Q
,.
_
Requested Test Parameters
E N
H
0
Cd
�
O
03
-14 /S
:00,-
G
G /0
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc
:per
G
G /®
HNO3
Y
Cadmium . �t
:p
G
/ P
HCL
Y
Oil & Grease
G
G /d)
H2SO4
Y
COD f,r
G
G 1
None
Y
BOD AA
:T
G
G /®
None
Y
TSS �
G
G /
None
Y
Residual Chlorine 6
Onsite Field
eH Analysis
Onsite Field Temperature Analysis
PH: 17. S (s.u.)
Sample Time:
Temp: /y.S (°C) Sample Time: s.•ss...
Analysis Time: 6 : 0
Analysis Time:
Meter Calibrated: Yel
Thermometer Calibrated: / N
Sampling and fieldAnalysis
completed by:
Relinquished B
Received
Date: � - - /,;"
Time:
Date: Z, 1 li- $'
Time: 1,21 i-/
By:
Received By:
Ii'•:elinquished
Date:
Time:
Date:
Time:
EH5-SW-Chain of Costody Outfall 01-Rev 001
Page 17 of 17

ATIAlihc
Allvac - Bakers Plant
Stormwater Monitoringport Form
Sample Date:
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis.
Sample Time:
Stormwater Discharge Outfall #02 (Non -Commingled)
Drainage Area = 212 952s . ft. = 4.9 acres
% Impervious = 12%
i4 c enQ �YTiGa�
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
3� D
120
TSS
D a
100
Cadmium
0.001
Chromium, total recoverable
I
Copper, total recoverable
0.007
Nickel, total recoverable
0. DO8
0.26
Zinc, total recoverable
D D 7
0.067
pH
(std units)
6-9 (std units)
Storm Date: -/9 4 Storm Duration: /• o?S (Hrs.) Inches of Rainfall: 0.,,3Q
Duration of time preceding rain event exceeding 0.1 ": a?yD (Hrs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(impervious Area)
Q(tot., cfs) _ (A x inches rain/12 inches/ft. x 4.9 acres x .88) + .9 x inches rain/ 12 inches/ft. x 4.9 x .12)
Q(Total, cfs) = 0. l 437 x 0- -?0 ^ (Inches of rain) + 0.0441 x (:0 - 34 (Inches of rain)
V. A;q cfs

s
aceAnalytical
WWW,peoelabs corn
March 02, 2018
Mr. Joe Hinkle
Allvac
RE: Project: SW OUTFALL #02(B
Pace Project No.: 92373888
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on February 19, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
David Pope, Allvac
Scott Ryan, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page i of 14

le
Analytical e
Yrrw.psoelads tom
Project: SW OUTFALL #02(B)
Pace Project No.: 92373888
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FtoridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
V rginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 2 of 14

c
aceAnalytical
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SAMPLE ANALYTE COUNT
Project: SW OUTFALL 902(B)
Pace Project No.: 92373888
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytos
Reported
Laboratory
92373888001 OUTFALL 2 COMP EPA 200.7
SER
5
PASI-A
SM 2540D
MVC
1
PASI-A
SM 5210B
CDC
1
PASI-A
SM 5220D
NAL
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 14

5ac
(
eAmlyfiml*
www.p&ceiabi.com
ANALYTICAL RESULTS
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #02(B)
Pace Project No.: 92373888
Sample: OUTFALL 2 COMP Lab ID: 92373888001 Collected: 02/19/18 05:50 Received: 02/19/18 12A4 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
02/19/18 05:51
Collected Date
02/19118
1
02/19/18 05:51
Collected Time
05:45
1
02/19/18 05:51
pH
6.8 Std. Units
0.10
1
02/19/18 05:51
Temperature
12.9 deg C
0.50
1
02/19/18 05:51
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA
200.7
Cadmium
ND ug1L
1.0
1
02/22/18 05:30 03/01/18 15.23
7440-43-9
Chromium
12.5 uglL
5.0
1
02/22/18 05:30 03/01/18 15:23
7440-47-3
Copper
17.3 ug1L
5.0
1
02/22/18 05:30 03/01/18 15:23
7440-50-8
Nickel
8.1 ug1L
5.0
1
02/22/18 05:30 03/01/18 15:23
7440-02-0
Zinc
77.0 uglL
10.0
1
02/22/18 05:30 03/01/18 15:23
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
10.2 mg1L
5.0
1
02/23/18 01:38
5210B BOD, 5 day
Analytical Method: SM 5210B
BOD, 5 day
2.0 mg1L
2.0
1
02/20/18 18:14 02/25/18 17:07
B2, L2
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
31.0 mg1L
25.0
1
02/22/18 14:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/0212018 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14

IeAnalytical
rnrw.pacehlbs cam
QUALITY CONTROL DATA
Project: SW OUTFALL #02(B)
Pace Project No.: 92373888
OC Batch: 399194 Analysis Method: EPA 200.7
OC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92373888001
METHOD BLANK: 2214191 Matrix: Water
Associated Lab Samples: 92373888001
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
Cadmium
ug/L
ND
1.0
0310111814:23
Chromium
ug1L
ND
5.0
0310111814:23
Copper
ug1L
ND
5.0
03/0111814:23
Nickel
ug1L
ND
5.0
03/01/1814:23
Zinc
ug1L
ND
10.0
03/0111814:23
Pace Aaatytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2214192
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Cadmium
ug1L
500
488
98
85-115
Chromium
ug1L
500
492
98
85-115
Copper
ug1L
500
500
100
85-115
Nickel
ug1L
500
487
97
85-115
Zinc
ug1L
500
493
99
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2214193
2214194
MS
MSD
92373852001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug1L
<0.0010
500
500
537
528
107
106
70-130
2
mg1L
Chromium
ug1L
<0.0050
500
500
482
473
96
95
70-130
2
mg1L
Copper
ug1L
0,050
500
500
553
540
101
98
70-130
2
mg1L
Nickel
ug1L
<0.0050
500
500
510
506
101
1101
70-130
1
mg1L
Zinc
ug1L
0.075
500
500
559
555
97
96
70-130
1
mg1L
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE;
2214195
2214196
MS
MSD
92373647003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc,
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug1L
ND
500
500
515
516
102
102
70-130
0
Chromium
ug1L
124
500
500
645
648
104
105
70.130
0
Copper
ug1L
ND
500
500
623
627
105
106
70-130
1
Nickel
ug1L
ND
500
500
572
570
98
98
70-130
0
Results presented on this page are In
the units Indicated by the
"unite" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/0212018 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14

aceAnalytical
www.pacelabscom
QUALITY CONTROL DATA
Project- SW OUTFALL #02(B)
Pace Project No.: 92373888
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE; 8 MATRIX SPIKE DUPLICATE: 2214195 2214196
MS MSD
92373647003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Zinc ug/L 57200 500 500 59000 59800 360 528 70-130 1 M6
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in f0,
Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLG.
Page 6 of 14

aceAnalytical
�
wwwpecalabs.com
QUALITY CONTROL DATA
Project: SW OUTFALL #02(B)
Pace Project No.: 92373888
QC Batch: 399417 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92373888001
METHOD BLANK: 2215409
Associated Lab Samples: 92373888001
Parameter
Units
Total Suspended Solids
mg1L
LABORATORY CONTROL SAMPLE: 2215410
Parameter
Units
Total Suspended Solids
mg1L
Pace Anatytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 02/23/18 01:18
Spike LCS LCS % Pee
Conc. Result % Rec Limits Qualifiers
250 262 105 90-110
SAMPLE DUPLICATE: 2215411
92374343001
Dup
Parameter
Units
Result
Result
Total Suspended Solids
mg1L
188
218
SAMPLE DUPLICATE: 2215412
92374169002
Dup
Parameter
Units
Result
Result
Total Suspended Solids
mg/L
6.2
6.8
RPD Qualifiers
15 D6
RPD Qualifiers
9 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03102/2018 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14

aceAnalj6dal
www psceiabs can
Project: SW OUTFALL #02(B)
Pace Project No.: 92373888
QC Batch: 398880
QC Batch Method: SM 5210B
Associated Lab Samples: 92373888001
METHOD BLANK: 2212480
Associated Lab Samples: 92373888001
Parameter
BOD, 5 day
QUALITY CONTROL DATA
Analysis Method: SM 52106
Analysis Description: 5210B BOD, 5 day
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg1L ND 2.0 02/2511817:07
LABORATORY CONTROL SAMPLE: 2212481
Spike LCS
Parameter Units Conc, Result
BOD, 5 day mg/L 198 114
SAMPLE DUPLICATE: 2212482
92373898001 Dup
Parameter Units Result Result
BOD, 5 day mg1L ND ND
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
58 84.6-115.4 L2
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 14

1aceAnalytical "
»ww.pacelalis tarn
QUALITY CONTROL DATA
Project: SW OUTFALL #02(B)
Pace Project No.: 92373888
QC Batch: 399148 Analysis Method: SM 5220D
OC Batch Method: SM 5220D Analysis Description: 52200 COD
Associated Lab Samples: 92373888001
METHOD BLANK: 2214027
Associated Lab Samples: 92373888001
Parameter Units
Chemical Oxygen Demand mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 0212211814:45
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2214028
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 747 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2214029 2214030
MS MSD
92373205001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 238 100 100 348 348 110 110 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2214031 2214032
MS MSD
92373887001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 35.0 100 100 128 141 93 106 90-110 10 R1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 14

Pace Analytical Services, LLC
(�5aceAwlyfical" 9800 Kiney Ave. Suite 100
Hunsersville, NC 28078
078
wNw.pacebbs carry
[phone]
QUALIFIERS
Project: SW OUTFALL#02(8)
Pace Project No.: 92373888
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantization Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

(�IacleAnalytical
wwwpexelabs ODM
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 2BO78
[phone]
Project: SW OUTFALL #02(B)
Pace Project No.: 92373888
Analytical
Lab lD Sample ID QC Batch Method QC Batch Analytical Method Batch
92373888001
OUTFALL 2
COMP
92373888001
OUTFALL 2
COMP
EPA 200.7
399194 EPA 200.7 399266
92373888001
OUTFALL 2
COMP
SM 25400
399417
92373888001
OUTFALL 2
COMP
SM 521013
398880 SM 5210B 398953
92373888001
OUTFALL 2
COMP
SM 52200
399148
REPORT OF LABORATORY ANALYSIS
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Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 14

Document Name:
Document Revised: February 7, 2018
.
Sam le Condition Upon Recel t SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
aCBArta fCaf
'Y`
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvllleld' Raleigh[] Mechanicsville❑
the t N
WO# : 92373888
Upon Receipt Project #:
UPCourier. F ❑5 DUSPS lient
❑ Commercial ❑Pace ' ❑Qther: I
92373888
Custody Seal Present? ❑Yes No Sealslntetti ❑Yes �� GG
Date/Initials Perron Examining Contents;�.„l'
Pecking Material: ❑Bubble Wrap []Bubble Bags ❑None ,_E5 Other
Thermometer: n,Type of let: et ❑Blue
D2,92T036
Cooler Tamp I'C): �J 13 Correction Factor: Add/Subtract ('CI +0.1
Cooler Temp Corrected ('C):
USDA Regulated SoIIAff"NIA, water sample)
old samples originate in'a quarantine zone within the United States: CA, NY, or SC (check maps}?
hype rlssw---
Biological Time Frozen?
[]Yes ❑No ❑N/A
❑None
Temp should be above freezing to 6'C
[]Samples out of temp criteria. Samples an ice, cooling process
has begun
Did samples originate from a foreign source {internatlana
i—fi Acne I4aw211 and Puerto ItIm1711Yes
Comments Dlscre a
Chain of Custody Present?
er
nN.
N A
1.
Samples Arrived within Hold Time?
Yes
L3110
N/A
2.
Short Hold Time Ana Is L02 hr.?
es
ONO
N A
3.
Rush Turn Around Time Requested?
Oyes
No
N/A
4.
SuHiclent Volume?
No
ONJA
5.
Correct Containers Used?
-Pace Containers Used?
fJr95
Jye&
ONO
QNo
❑N/A
ONLA
6.
Containers intact?
Yes
ON.
N A
7.
Dissolved analysis: Sam !es Field Filtered?
QY
No
N/A
S.
Sample Labels Match COC7
-includes Date/Time/ID/Analysis Matrix:
JdYes
❑No
[_-]N/A
9.
Heads ace in VOA Vials >S•fimm 7
OYRS
ONO
NLAII
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
OYes
❑No
1771NO
N/A
rl/A
11.
COMMENTS/SAMPLE [DISCREPANCY
Field Data Required? Dyes ❑Na
Lot ID of split containers:
— _CLIENT, NOTIFICATION/RESOLUTION--
Person contacted: Date/Time: _
Project Manager SCURF Review: • L
Project Manager SRF Review:
i,
Date: 4 i `' 11 b
Date: :2 1 Z.0 1
Page 12 of 14

Document Name:
Document Revised: February 7, 7018
JCai�
Sample Condition UM Recel t{SLUR}
Page 1 of 2
Document No.:
Issuing Authority:
ceAMI
F•CAR-CS-033-Rev.05
Pace Carolinas Quality Office
*Check mark top half of box if PH and/or dechlorination Is Project N
verified and within the acceptance range for preservation
samples.
6teeptlons: VOA, Coliform, TOC, Oil and Grease, DAD/8015 (water) DOC, L1Hg
**Bottom half of box Is to list number of bottle
W0#:923 3888
PH: ffNB We Date: 02/Z8~ /tg
CLIENT: 82-Allvee NC
0000001110
60
MEM
060
60
ilk
No
ONE
on
MOMEN
M
pH -Adjustment Log for Preserved'Samptes -- ---- -- -- - - -
Sample ID
Type of Preservative
pH upon recelpt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot e
Note: whenever there is a oiscrepancy arfecling North Carolina compliance samples, a COPY at this form will tie sent to the North Carolina UFHNR Certirrtatron Unrce If.e.
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 13 of 14

Stormwater Monitoring
Chain of Custody Record
Project Number/Name: SW Outfall #OZ(B)
jProject Location: ATI SM - Bakers
Sample 's Si nature:
Date: e2
II
V
E�
G
C
y
,
N
c
Requested Test Parameters
,�
6
U
T
- -
fa,,
G
G IdD
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc r1
G
G I®
HNO3
Y
Cadmium c
G
0/0
H2SO4
Y
COD
' ,. ,
G
G /®
None
Y
BOD y
.YZ.
G
G I0
None
Y
TSS
.Onsite Field pH Analysis
Onsite Field Temperature Analysis
pH: 1p- 8_ __
(s.u.) Sample Time: �•'Y�
Temp: fa, Q (°C) Sample Time: S•'y�,r,,.
Analysis Time:
Analysis Time:
Meter Calibrated:
Yex
Thermometer Calibrated: 1 N
Sampling
and field anal sis com leted by:
Relinquished By:
Received B : %
Date:
ITime:
Date: 2—-r
Time: 2.1
Relinquished By:
lReceived B
Date:
Time:
Date:
Time:
EHS-SW-Chain of Costody Qutfall 02-Rev 001
n
Page 14 of 14

Allvac - Bakers Plant
Stormwater Monitoriniz Report Form
Sample Date: off- / 9 -/e
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
OATI Allva
Sample Time:. 5�,36�r•-- __ _
Stormwater Discharge Outfall #03 (Non -Commingled)
Drainage Area = 336,580s__ A. ft. = 7.8 acres
% Impervious = 15%
_00 /�� Tk.
Ace
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/l)
BOD
30
COD
120
TSS
100
Cadmium
P
0.001
Chromium, total recoverable
D
1
Copper, total recoverable
O S
0.007
Nickel, total recoverable
. DO f
0.26
Zinc, total recoverable
D
0.067
pH
,f- ,a (std units)
6-9 (std units)
Storm Date: a -/ 9 -18 Storm Duration: _ / • a S (Hrs.) inches of Rainfall: 0.30
Duration of time preceding rain event exceeding 0.1 ": �_ (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) _ (.4 x inches rain/12 inches/ft. x 7.8 acres x .85) + .9 x inches rain/ 12 inches/ft. x 7.8 x .15)
Q(Total, cfs) = 0.2210 x Q. 3D (Inches of rain) + 0.0878 x Q • 34 (Inches of rain)
0 9 cfs

4
acmna pical
www.peNAabs.com
March 02, 2018
Mr. Joe Hinkle
Allvac
RE: Project: SVV OUTFACE #03(B)
Pace Project No.: 92373890
Dear Mr. Hinkle:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 19, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucorrl, Allvac
David Pope, Allvac
Scott Ryan, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC,
Page 1 of 14

leac,AmIXical*
Pace Analytical Services, LLC
9800 Kincey Ave, Suite
Huntersville, NC 28078
0788
W com
[phone]
CERTIFICATIONS
Project: SW OUTFALL #03(13)
Pace Project No.: 92373890
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
LouisianalNELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification A 84
North Carolina Field Services Certification #: 5342
VrginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
VrginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 14

•
IeAnalj cal
www4woews.com
SAMPLE ANALYTE COUNT
Project: SW OUTFALL #03(B)
Pace Project No.: 92373890
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilfe, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92373890001 OUTFALL 3 COMP EPA 200.7
SER
5
PASI-A
SM 2540D
MVC
1
PASI-A
SM 5210B
CDC
1
PASI-A
SM 5220D
NAL
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 14

le
aceAnalyfr'cal
wsrw.lpoc& s.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL#03(8)
Pace Project No.: 92373890
Sample: OUTFALL 3 COMP
Lab ID: 92373890001 Collected: 02/19/18 05A1
Received: 02/19/18 12A4 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
02/19/18 05:41
Collected Date
02119/18
1
07-119/18 05:41
Collected Time
05:34
1
02/19/18 05:41
pH
7.2 Std. Units
0.10
1
02119/18 05:41
Temperature
13.3 deg C
0.50
1
02/19/18 05:41
200.7 MET ICP
Analytical Method: EPA 200.7
Preparation Method: EPA 200.7
Cadmium
ND ug1L
1.0
1
02122/1805:30
03101/1815:26
7440-43-9
Chromium
19.1 ug1L
5.0
1
02122/18 05:30
03/01/18 15:26
7440-47-3
Copper
25.7 ug1L
5.0
1
0212211805:30
03/01/1815:26
7440-50-8
Nickel
5.2 ug1L
5.0
1
02/22/18 05:30
03/01/18 15:26
7440-02-0
Zinc
16.2 ug1L
10.0
1
02/22/18 05:30
03/01/18 15:26
7440-66.6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
6.8 mg/L
5.0
1
02/23/18 01:39
5210B BOD, 5 day
Analytical Method: SM 5210B
BOD, 5 day
2.0 mg1L
2.0
1
02/20/18 18:14
02/25/18 17:07
B2,1-2
52201) COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
33.0 mg1L
25.0
1
02/22/18 14:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14

IeAnaljftal
uww.peceleba corn
QUALITY CONTROL DATA
Project: SW OUTFALL #03(B)
Pace Project No.: 92373890
QC Batch: 399194
QC Batch Method: EPA 200.7
Associated Lab Samples: 92373890001
Analysis Method:
Analysis Description:
EPA 200.7
200.7 MET
METHOD BLANK: 2214191
Matrix: Water
Associated Lab Samples: 92373890001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Cadmium
ug1L
NO
1.0
03/01/1814:23
Chromium
ug1L
NO
5.0
0310111814:23
Copper
ug1L
NO
5.0
03/0111814:23
Nickel
ug1L
NO
5.0
0310111814:23
Zinc
ug1L
NO
10.0
0310111814:23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2807E
[phone]
LABORATORY CONTROL SAMPLE: 2214192
Spike
LCS
LCS
% Rec
Parameter Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
uglL
500
488
98
85-115
Chromium
uglL
500
492
98
85-115
Copper
uglL
500
500
100
85-115
Nickel
ug1L
500
487
97
85-116
Zinc
ug1L
500
493
99
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2214193
2214194
MS
MSD
92373852001
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
Cadmium
ug1L <0.0010
500
500
537
528
107 106
70-130
2
mg1L
Chromium
ug1L <0.0050
500
500
482
473
96 95
70-130
2
mg1L
Copper
uglL 0.050
500
500
553
540
10140 98
70-130
2
mg1L
Nickel
ug1L <0.0050
500
500
510
506
101 101
70-130
1
mg1L
Zinc
u91L 0.075
500
500
559
555
97 96
70-130
1
mg1L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2214195
2214196
MS
MSD
92373647003
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
Cadmium
ug1L NO
500
500
515
516
102 102
70-130
0
Chromium
ug1L 124
500
500
645
648
104 105
70-130
0
Copper
ug1L NO
500
500
623
627
105 106
70-130
1
Nickel
ug1L NO
500
500
572
570
98 98
70-130
0
Results presented on this page are In the units Indicated by the "Units"
column except where
an ahemate
unit Is presented to the right
or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 031021201811212 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14

aceAnalyfical
wlrw.peoef b&CGM
QUALITY CONTROL DATA
Project: SW OUTFALL #03(8)
Pace Project No.: 92373890
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2214195 2214196
MS MSD
92373647003 Spike Spike MS MSD
Parameter Units Result Conc. Conc. Result Result
Zinc uglL 57200 500 500 59000 59800
Pace Anatytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MS MSD % Rec
% Rec % Rec Limits RPD Qua[
360 528 70-130 1 M6
Results presented on this page are in the unite indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 14

(�IaceAnalyfical�
wwwpeoalebs cam
QUALITY CONTROL DATA
Project: SW OUTFALL #03(B)
Pace Project No.: 92373890
QC Batch: 399417 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92373890001
METHOD BLANK: 2215409
Associated Lab Samples: 92373890001
Parameter
Units
Total Suspended Solids
mg1L
LABORATORY CONTROL SAMPLE: 2215410
Parameter
Units
Total Suspended Solids
mglL
SAMPLE DUPLICATE: 2215411
Parameter
Units
Total Suspended Solids
mglL
Pace Analytical Services, LLC
9800 Kircey Ave, Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 02/23/18 01:18
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 262 105 90-110
92374343001 Dup
Result Result RPD Qualifiers
188 218 15 D6
SAMPLE DUPLICATE: 2215412
92374169002 Dup
Parameter Units Result Result
Total Suspended Solids mg1L 6.2 6.8
RPD Qualifiers
9 D6
Results presented on this page are In the units indicated by the"Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14

5aceAnalytical"
(�ttwwpeoelebs.cam
QUALITY CONTROL DATA
Project: SW OUTFALL 903(B)
Pace Project No.: 92373890
QC Batch: 398880 Analysis Method: SM 52108
QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 92373890001
METHOD BLANK: 2212480
Associated Lab Samples: 92373890001
Parameter Units
BOD, 5 day mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 02/2511817:07
LABORATORY CONTROL SAMPLE: 2212481
Spike LCS
Parameter Units Conc, Result
BOD, 5 day mg/t_ 198 114
SAMPLE DUPLICATE: 2212482
92373898001 Dup
Parameter Units Result Result
BOD, 5 day mg/L ND ND
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2807B
(704 )875-9092
LCS % Rec
% Rec Limits Qualifiers
58 84.6-115A L2
RPD Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 14

•
lacieAnalytical
www. Rifts .com
QUALITY CONTROL DATA
Project: SW OUTFALL #03(B)
Pace Project No.: 92373890
QC Batch: 399148 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92373890001
METHOD BLANK: 2214027
Associated Lab Samples: 92373890001
Parameter Units
Chemical Oxygen Demand mg1L
LABORATORY CONTROL SAMPLE: 2214028
Parameter Units
Chemical Oxygen Demand mg1L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 02/2211814:45
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
750 747 100 90-110
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2214029 2214030
MS MSD
92373205001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Cone. Result Result % Rec % Rec Limits RPD Quai
Chemical Oxygen Demand mg1L 238 100 100 348 348 110 110 90.110 0
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2214031 2214032
MS MSD
92373887001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 35.0 100 100 128 141 93 106 90-110 10 R1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0310212018 12:12 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 14

I
Pace Analytical Services, LLC
aceArialytrcal @ 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
N'wbsCom [phone]
QUALIFIERS
Project: SW OUTFALL ft03(B)
Pace Project No.: 92373890
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14

+
Pace Analytical Services, LLC
aceAnalytr'cale
9800Kincey Ave. Suite 100
Huntersville, NC 28078
wwwpeoefaba.Cortr
(704 )875-9092
QUALITY CONTROL DATA CROSS REFERENCE
TABLE
Project: SW OUTFALL#03(B)
Pace Project No.: 92373890
Analytical
Lab ID Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92373890001 OUTFALL 3 COMP
92373890001 OUTFALL 3 COMP
EPA 200.7
399194 EPA 200.7
399266
92373890001 OUTFALL 3 COMP
SM 2540D
399417
92373890001 OUTFALL 3 COMP
SM 5210B
398880 SM 52108
398953
92373890001 OUTFALL 3 COMP
SM 5220D
399148
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/02/2018 12:12 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 14

Document Name:
Document Revised: February 7, 2a1B
aceAflaf ?Cal`
Sam le Condition Upon Recel t SCURj
Page 1 of 2
Document No.:
Issuing Authority:
F.CAR-0-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersvilk•ff' Raleigh[] Mechanicsville❑
-Saniffli! Condition Client Name: WO# : 92373890
Project M.
Courier. F Ex ❑UPS j USPS ent
❑ Commercial ace QQther: 82373880
2''�'I��,,� ,__,�`
Custody Seel Present? []Yes )Jiro Seals Intact? Oyes E o
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None Other
Thermometer Type of ke: e/t ❑Blue
IR 6un lo: 92TO36 �"
Cooler Temp ('Cj: 3 - 3 - Correction factor: Add/Subtract (*C) +0,1
Coder Temp Corrected ('C):
USDA Regulated Soil (E MA, water sample)
LAB sainples orlgln- a quarantine tone within the United States: CA, NY, or SC {check mapsl?
rlYes nl
Date/Initlals Person Examining Contents: [ ' Z L $ I
Biological Tlssu 7
❑Yes ❑N N/A
[]None
Temp should be above freezing to 6'C
❑Samples out of temp criteria. Samples on lee, cooling process
has begun
Did samples originate from a foreign source jlntermt Y,
Indudina Hawaii and Puerto Ricol? nYes No
Comments/??Isere an .
Chain of Custody Present?
Na
[INIA
1.
Samples Arrived within Hold Time?
es
ONO
N A
2.
Short Hold Time Analysis c72 hr.)?
yes
No
N A
3.
Rush Turn Around TimeRequested?
Ye,
o
N/A
4.
Sufficient Volume?
Yesycr
No
N A
S.
Correct Containers Used?
-Pace Containers Used?
A! Yp
&fej
❑No
No
❑N/A
[:INIA
6.
Containers Intact?
Yes
ONO
N A
7.
Dissolved ana sis: Samples Field Filtered?
Yn
0No
N/A
B.
Sample labels Match COC?
-Includes Date/Time/iD/Ana is Matrix:
)243—
ONO
❑N/A
9.
Heads ace in VOA Vials >5-6mm ?
Oves
ONO
N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Des
ONO
ONO
A
I A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CUENT.N0TIFiCATFON/AES0LUTii3N
Field Date Required? Des []No
Person contacted: % Date/Time: r
Project Manager SCURF Review: Date:
Project Manager SRF Review: �,� Date:
Page 12 of 14

Document Name:
Document Revised: February 7, 2018
.
I�
�naryt
Sample Condition U RecN t(SCUR
Page 1 of 2
Document No.:
issuingauttlority:
N
lFe
F-CAR-CS-033-0ev.06
Pace Carolinas Quality Office
'Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Eximptlons: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, UHS
••Bottom half of box is to list number of bottle
Project # Wp# : 92373890
lem: f1WB Due Dale: 02/26/18
CLIENT: 92-pllvao NC
--- - - — - -- -pH AdIustment Lo—g for Preserved Samples---- -- - ------ --- ----
Semple 10
Type of Preservative
pH upon receipt
Date preservation adjusted
Time presuvatlon
edjusled
Amount of Preservative
added
Lot a
Note. whenever there is a discrepancy affecting North Carolina compliance samples, a COPY of this form will ae sent to the North Cilrollne DEHNR Certification CnAC! it.e.
Out of hold, incorrect preservative, Out of temp, incorrect containers.
Page 13 of 14

Stormwater Monitoring
Chain of Custody Record
Project Number/Name:
SW Otttfall #03 B
Project Location: ATI SM - Bakers
Sample 's Signature:
Date:
c.
GO
z "
U
H
;�a
�,
Requested Test Parameters
CI
G
0
W*r.•
/
G
G /0
HNO3
Y
Total Recoverable: Chromium, Nickel, Copper, Zinc
,j•'+�/,,..
G
G /d)
HNO3
Y
Cadmium
G
G I V
H2SO4
Y
COD W}
G
G 10
None
Y
BOD cv
G
G /d)
None
Y
TSS
Onsite Field pH Analysis
Onsite Field Temperature Analysis
pH: a (s.u.)
Sample Time:
j�',?,c,'
Temp: _ fIJ (°c) Sample Time:
-
Analysis
Time: ,.,y/a,,.
Analysis Time:
Meter Calibrated: Le-
Thermometer Calibrated: 1 N
.X
Saineling and field .analysis com leted by:
Q�9
Relinquished By:
Received B
Date: 2-9 -/ Er
Time:
Date: Time'. Q
Re"n uished By:
Received By:
Date:
Time:
Date:
Time:
=77-
i
I
EHS•SW-Chain of Costody Outfall 03-Rev 001
Page 14 of 14

Allvac - Bakers Plant
Stormwater Monitoring; Report Form
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Non-ContactCooling Wastewater
2���w aoe. xx1 141a, c1o,�tz
Pace XnAIVficQl
40 CFR Part 136
3*ATI
specialty matertaft
Non-
Contact
Cooling
Water #
Sampling
Date
Sampling
Time
Estimated
Flow(MGD)
Total
Residual
Chlorine
(mg/L)
Temperature
pH (std. units)
Effluent
Downstream
Upstream
1
1 0?-6 8
grow-
.00
,31
OZ0'
eli 96
``
7s
2
4-08
/73°e-
90
4
oo
D • a il
1'1.1 °`
9 a°`
. 9&
a
5
�2 - G
o -'0? q ..
6. o
3. ec-
. 0 4
9.apc
7.0
6
a?-6
/d -`15;i-
A 019 9 YD.D
JD.aae,
.1
Q 00
./
7
a-6 -i8
os...Q
. OD s
4.03
a -0- / L
/a. ald
-8
8
a-6 �s
��=,���,
Fa.o
o.av
OW-3°G
io s�
�o a�
7 7

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 5'0663a 9 -
FACILITY NAME /0A t
PERSON COLLECTING SAMPLE ) d —TN
CERTIFIED LABORATORY(S) a C C a i Lab #__Z4_
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: D!
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY /
PHONf NQ — S
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
1
DateII
Samplei—Total
Collected
1
Rainfall
`
i
i
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&GITPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
moldd/vr
MG
inches
m
m I
unit
al/mo
Form SWU-247, last revised 21212012
Page I of 2

STORM EVENT CHARACTERISTICS:
Date 2 -If
Total Event Precipitation (inches): D• O
Event Duration (hours): Z. (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Per�ittee) (Date)
Form SWU-247, last revised 21212012
Page 2 of 2

A WA
NCURR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidon ce on filling out thisform, please visit. http://portal.ncdennorg/web/wQ jwsIsu/npdessw#tab-4
Permit No.: or Certificate of Coverage No.:
Facility Name: err &�Lev-s
County: —ALA /,l Phone No. �-AY 9-',�s /
Inspector: _ IZ� &e _�- Z/ea
Date of Inspection: o?-/9 /S
Time of Inspection: S•-s74-
Total Event Precipitation (inches): JO--W
Was this a "Representative Storm Event' or "Measureable Storm Event" as defined by the permit?
(See information below.)
['Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event' or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall, The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the hest of my knowledge:

1. Outfall Description:
Outfall No. � Structure
Receiving Stream:
Describe the industrial activities t at i
2. Color: Describe the color of the d
(light, medium, dark) as descriptors:
ditch, etc.) : S_ 'V11zh ay
�fe� _
r within the outfall drainage area:
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): _ >hJA61
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
® 2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
a 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
6 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious indicators of Stormwater Pollution:
List and describe e'
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

WDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance onfrllingout thisform,please visit: bttn://portal.ncdenr.orgjweb/wgjw�lsyjnndessw#tab-4
Permit No.: or Certificate of Coverage No.: NV/C/CG/_/—/—/—/_/_/
Facility Name: ,Qrr Al'lrac-BaKerf _
County: lln:on_ Phone No. O` za'B9 - ysll
Inspector: ^2�,V ?/41;Ln C/vn7�2 - -
Date of Inspection:
Time of Inspection:
Total Event Precipitation (inches): 40•3D
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
E Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no
I
recipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:

1. Outfall Description: n
Outfall No. X8 da Structure (pipe, ditch, etc.) _ I
Receiving Stream: G eelhl _
Describe the industrial activities pat occur within the outfall drainage area:
2. Color: Describe the color of the discharge ysing basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: C /e4.r
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): Ivo,4 G
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
() 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 D 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy.-
(1) 2 3 4 5
7. is there any foam in the stormwater discharge? Yes d�tQ
8. is there an oil sheen in the stormwater discharge? Yes
4. is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious Indicators of Stormwater Pollution:
List and describe _ /Vail
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

AN`
2= Awl5WA.
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit. htt�/portal.ncd�nr-org/web/wg/wslsu/­npdessw#tab-4
Permit No.: hj/C/,5-/Q/Q/o/3/2?/4/ or Certificate of Coverage No.:
Facility Name: r4Tr �A/1i14e - 0a..Xert
County: LLn: o., Phone No. 749 y ,&99 - yS// _.._
Inspector: _ Da.-.�Aae �'�, '4/a0, G/enfz
Date of Inspection: -
Time of inspection: S 3Ta.
Total Event Precipitation (inches): D -SO
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
dyes ❑ No
Please verify whether Qualitative Monitoring mast be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of rimy knowledge:

1. Outfall Description: ' n
Outfall No. 5, 49-? Structure (pi e, ditch, etc.) Y , 2 A, 74A
Receiving Stream: 12-11Dr G'rce
Describe the industrial activi�ie that occur within the outfall drainage area:
2. Color. Describe the color of the
(light, medium, dark) as descriptors: —
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): NOW G �^ _
4. CIarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
® 2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
® 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
(T 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes &
9. Is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious Indicators of Stormwater Pollution:
List and describe 6-
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242. Last modified 10/25/2012

aceAnalytical.
www.pne)abs.com
February 15, 2018
Mr. Joe Hinkle
Allvac
RE: Project:NonContact Cooling Water
Pace Project No.: 92312424
��� V fir• -ewe
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078.
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on February 07, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucotn, Allvac
David Pope, Allvac
Scott Ryan, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C.
Page 1 of 17

aceAnalXical
www.pambbs,tom
Project: NonContact Cooling Water
Pace Project No.: 92372424
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, H u ntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VrginiaNELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2807E
[phone]
Page 2 of 17

lacieAnaljtical'
www.pa01863.com
SAMPLE ANALYTE COUNT
Project: NonContact Cooling Water
Pace Project NO.: 92372424
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92372424001
NonContact #1
EPA 1664B
JMS
1
PASI-C
92372424002
NonContact #2
EPA 1664B
JMS
1
PASI-C
92372424003
NonContact #3
EPA 1664B
JMS
1
PASI-C
92372424004
NonContact #4
EPA 1664B
,iMS
1
PASI-C
92372424005
NonContact #5
EPA 1664E
JMS
1
PASI-C
92372424006
NonContact #6
EPA 1664E
JMS
1
PASI-C
92372424007
NonContact #7
EPA 1664B
JMS
1
PASI-C
92372424008
NonContact #8
EPA 1664E
JMS
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 17

Pace Analytical Services, LLC
IaclMalyfical* 9800 Kiney Ave. Suite too
Huntersville, NC 28078
78
(�»ww.pecalabu cam [phone]
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92372424
Sample: NonContact #1 Lab ID: 92372424001 Collected: 02/06/18 W10 Received: 02/07/18 15:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16648
Oil and Grease ND mg1L 5.0 1 02/15/18 04:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2018 02:08 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 17

aceAnapical
www.pacajahs Dom
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Analytical Services, LLC
9800 KinceyAve. Suite 1o0
Huntersville, NC 28078
t704j875-9092
Pace Project No.: 92372424
Sample: NonContact #2 Lab ID: 92372424002 Collected: 02/06/18 09:32 Recejved: 02107/18 15:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
HEM, Oil and Grease
Oil and Grease
Analytical Method: EPA 1664E
7.7 mg1L 5.0 1
REPORT OF LABORATORY ANALYSIS
02115/18 04:58
This report shall not be reproduced, except in full,
Date: 02/15/2018 02:08 PM without the written consent of face Analytical Services, LLC. Page 5 of 17

aceAnalyti+cal
www.pace)aW.com
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92372424
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, KC 28078
[phone]
Sample: NonContact #3 Lab ID: 92372424003 Collected: 02/06/18 09:47 Received: 02/07118 15:10 Matrix: Water
Parameters Results Units Reporl Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16648
Oil and Grease ND mg/L 5.0 1 02115/18 04:58
Date: 02115/2018 02:08 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 17

aceAnalytical'
www.pacelaba cvm
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92372424
Sample: NonContact #4 Lab 1i): 92372424004 Collected: 02/06/18 10:05 Received: 02/07118 15:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 02/15/18 05:02
Date: 02/15/2018 02:08 PM
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 17

Ie
Analytical
www.Pecalebi cam
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92372424
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #5 Lab ID: 92372424005 Collected: 02/06/18 10:24 Received: 02/07/18 15:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 02/15/18 05:02
Date: 02/15/2018 02:08 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLG.
Page 8 of 17

IeMaIXcale
www.pscebbs com
ANALYTICAL RESULTS
Project: NonContact Coaling Water
Pace Project No.: 92372424
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #6 Lab ID: 92372424006 Collected: 02/06/18 10:45 Received: 02107/18 15:10 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual
HEM, Oil and Grease
Oil and Grease
Date: 02/15/2018 02:08 PM
Analytical Method: EPA 1664B
ND mglL 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02115118 05:02
Page 9017

(�Iacmnalyfical �
www.p&cektu.com
ANALYTICAL RESULTS
Pace Ana lyt}caI Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92372424
Sample: NonContact #7 Lab ID: 92372424007 Collected: 02/06/18 11:05 Received: 02/07/18 15:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
Date: 02/15/2018 02:08 PM
Analytical Method: EPA 1664B
ND mg/L 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
02115/18 05:02
Page 10 of 17

(�IaceAnalytical
wwwPacelaha tam
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92372424
Pace Analytical Services, LLC
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #8 Lab ID: 92372424008 Collected: 02/06/18 11:30 Received: 02/07/18 15:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
Date: 02/15/2018 02:08 PM
Analytical Method: EPA 1664B
ND mglL 5.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02115118 05:03
Page 11 of 17

aceAnalytical.
www.pacefabs.00m
QUALITY CONTROL DATA
Project: NonContact Cooling Water
Pace Project No.: 92372424
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 398117 Analysis Method: EPA 1664E
OC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92372424001, 92372424002, 92372424003. 92372424004, 92372424005, 92372424006, 92372424007,
92372424008
METHOD BLANK: 2208140
Matrix: Water
Associated Lab Samples: 92372424001, 92372424002,
92372424003, 92372424004, 92372424005, 92372424006, 92372424007,
92372424008
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Oil and Grease
mg/L
NO 5.0
02/15/18 04:56
LABORATORY CONTROL SAMPLE & LCSD:
2208141
2208142
Spike LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units
Conc. Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
Oil and Grease
mg/L
40 38.0 37.7
95 94
78-114 1 30
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be teproduced, except in full,
Date: 02115/2018 02:08 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 17

laceAnalytical
www.peceiabs aom
QUALIFIERS
Project: NonContact Cooling Water
Pace Project No.: 92372424
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/15/2018 02:08 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 17

leAnalyfcal"
www.pscelab3 mm
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NonContact Cooling Water
Pace Project No.: 92372424
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
Analytical
QC Batch Analytical Method Batch
92372424001
Non Contact#1
EPA16646
398117
92372424002
NonContact #2
EPA 1664E
398117
92372424003
NonContact #3
EPA 1664E
398117
92372424004
NonContact#4
EPA1664B
398117
92372424005
NonContact #5
EPA 1664E
398117
92372424006
NonContact #6
EPA 1664B
398117
92372424007
NonContact #7
EPA 1664B
398117
92372424008
NonContact 98
EPA 1664E
398117
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 02/1512018 02:08 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 17

Document Name:
Document Revised: February 7, 2Dlg
5alce
Sam le Condition U on Recel t(SCUR)
Page i of 2Analytical
Document No.:
Issuing Authority:
F•CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[-] Greenwood ❑ Huntersvil Ralelgh❑ Mechanicsville[]
Sample Condition Client Name. Project a W0# : 92372424
Courier: ❑Eed Ex (]UPS USPS ❑Cllent
❑ Commercial lI )ace '[]Other:_
Custody Seal Present? []Yes �Icp Seals Intact? ❑Yes
Packing Material: ❑Bubble Wrap IL RBUbble Bags ❑None ❑ Othei
Thermom ter
n ID: 92TO36 Type of Ice: t (:]Blue
Cooler Temp 'Cj: � C_ Correction Factor: Add/Subtract ('Q +0.1
Cooler Temp Corrected ('C)-,
USDA Regulated SoSJeN/A, water sample)
Did samples or ate in'a quarantine zone within the United States: CA, NY, or SC (check maps)?
or ate
1111111111111111111111
Date/Initials Person Examinl (gCont
Biological Tissue Frozen?
❑None ❑Yes�o []N/A
Temp should be above freezing to 6'C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source ,(Int�er ytionally,
including Hawaii and Puerto Ricol? l lYes �Rfvo
Comments/D'iscre an :
Chain of Custody Present?
s
No
N/A
1.
Samples Arrived within Hold Time?
Na
Q N/A
2.
Short Hold Time Analysis c72 hr.)?
QYEA
N/A
3.
Rush Turn Around Time Requested?
Dyes
N/A
4.
Sufficient Volume?
Y
Na
N/A
S.
Correct Containers Used?
-Pace Containers Used?
Ay
❑No
No
❑N/A
N/A
6.
Containers Intact?
No
N/A
7:
Dissolved analysis: Samples Field Filtered?
byes
No
_
/A
a.
Sample Labels Match COO
-includes Date/Time/ID/Anal is Matrix:
1ev�t� s
v "
[]No
❑N/A
9.
Heads ate In VOA Viats >5-6mm)?
Dyes
QNo
N/A
10,
Trip Blank Present?
Trip Blank Custody Seals Present?
Dyes
QYes
a
No
❑N/A
,qA
11.
COMMENTS/SAMPLE DISCREPANCY
Field Data Required? Dyes []No
Lot ID of split containers`
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
Project Manager SCURF Review: / Date:
Project Manager SRF Review: Date:
Page 15 of 17

Document Name:
Document Revised: February 7, 2018
__ � aceAnalytrcal
Sample Condition Upon Recel t SCUR
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033•Rev.06
Pace Carolinas Quality Office
'Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project Wp# : 92372424
PM: MWB Due Date: 02/16/18
CLIENT: 92-pllvae NC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Bate preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot p
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEKNR Certification omce p.e.
Out of hold, Incorrect preservative, out of temp, Incorrect containers,
Page 16 of 17

Storm Water Monitoring
(NON CONTACT)
Bakers North
Chain of Custody Record
Ada AT
SpecWty Materials
nacn t12
Project Number/Name: No Contact Cooling Water
Project Location: Allvac Bakers
Sampler's Signature:
Date: a- (o -/
©
w
C
o
a+
iE
CL
o
i
QSL
`a
a►
CL
d
a
C
u
ro
C
d
C
°
Requested Test
Parameters
11)-7 ZqZ
oar f
.0?- /
/Om .
G
G
HCL
Y
Oil & Grease Ca -I
No
G
G
HCL
Y
Oil & GreaseOO 2-
6
G
HCL
Y
Oil & Greasecb
DirCei,
Q a�
G
G
HCL
Y
,/
Oil & Greasers
IVOA ad.v
Q a.
G
G
HCL
Y
Oil & Grease005
AI0AemALet4f4
G
G
HCL
Y
Q.
Oil & Grease
NO/?
'O
G
G
HCL
Y
p,
Oil & Greas
CojlAd
•'30a..
G
G
HCL
Y
Q,3
Oil & Greasec>*
Meter Calibrated: f / N
IThermometer Calibrated: ®/ N
Sampling and Field analysis completed by:
Relinquished By:
lRelinquished
By: ItJox�
Date : - 7-
Time: y: QQ,r,.,-
Date
Time: 9 2'3
Relin wished By:
IRelinquished
By:
Date : - Ti e: 1 5 [ 0 JDate
:
Time:
EHS Baker South SW REV # 2 5/10/2016
U
�f
Page 17 of 17

aceAnalytr'cal
www.Pecelabs Com
February 08, 2018
Mr. Joe Hinkle
Allvac
RE: Project:CNonContact Cooling Water
Pace Project No.: 92372431
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on February 07, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
David Pope, Allvac
Scott Ryan, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 17

leAnalytrcal�
www.pscelsD.i com
Project: NonContact Cooling Water
Pace Project No.: 92372431
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Asheville Certification lDs
2225 Riverside Drive, Asheville, NC 28804
FloddalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
UrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 17

•
IacleAnaljftal
(�www.pecelabs can
SAMPLE ANALYTE COUNT
Project: NonContact Cooling Water
Pace Project No,: 92372431
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)87"092
Lab ID
Sample ID
Method
Analysts
Analytos
Reported
Laboratory
92372431001
NonContact #1
SM 4500-CI G
NAL
1
PASI-A
92372431002
NonContact #2
SM 4500-CI G
NAL
1
PASI-A
92372431003
NonContact #3
SM 4500-CI G
NAL
1
PASI-A
92372431004
NonContact #4
SM 4500-CI G
NAL
1
PASI-A
92372431005
NonContact #5
SM 4500-Cl G
NAL
1
PASI-A
92372431006
NonContact #6
SM 4500-CI G
NAL
1
PASI-A
92372431007
NonContact #7
SM 4500-Cl G
NAL
1
PASI-A
92372431008
NonContact #8
SM 4500-CI G
NAL
1
PASi-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in cull,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 17

acemalj t&cal
_pacelabs.cam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite t00
Huntersville, NG 28078
[phone]
Project; NonContact Cooling Water
Pace Project No.: 92372431
Sample: NonContact #1 Lab ID: 92372431001 Collected: 02/06118 09:10 Received: 02107/18 15:10 Matrix: Water
Parameters Results Units Report limit DF Prepared Analyzed CAS No. Qual
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.31 mg1L 0.024 1 02/08/18 13:13 7782-50-5 H3
Date: 02/08/2018 06:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Lull,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 17

e
5aceAnalyfical
(�www.powlabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92372431
Sample: NonContact #2 Lab ID: 92372431002 Collecled: 02/06/18 09:32 Received: 02/07/18 15:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500CL G Chlorine, Residual
Chlorine, Total Residual
Date: 02/08/2018 06:53 PM
Analytical Method: SM 4500-CI G
0.080 mglL 0.024 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02108118 13:13 7782-50-5 H3
Page 5 of 17

laneAm,(Xical"
www.p&oelabs.corn
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite ID0
Huntersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92372431
Sample: NonContact #3 Lab ID: 92372431003 Collected: 02/06/18 09:47 Received: 02/07/18 15:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500CL G Chlorine, Residual
Chlorine, Total Residual
Date: 02/08/2018 06:53 PM
Analytical Method: SM 4500-CI G
0.27 mgfL 0.024 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02/0811813:13 7782-50-5 H3
Page 6 of 17

IeAnalj6dal
www.pwelabe.coam
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92372431
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact 04 Lab ID: 92372431004 Collected: 02/06/18 10:05 Received: 021071.18 15A0 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4600CL G Chlorine, Residual Analytical Method: SM 4500-Cl G
Chlorine, Total Residual 0.24 mg1L 0.024 1 02/08/18 13:13 7782-50-5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 06:53 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 17

aceAnalytical
Mww.peceJab cam
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92372431
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2807E
[phone]
Sample: NonContact #5 Lab ID: 92372431005 Collected: 02/06/18 10:24 Received: 02107118 15:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.96 mg/L 0.12 5 02 O8118 13:13 7782-50-5 H3
Date: 02/08/2018 06:53 PM
REPORT OF LABORATORY ANALYSIS
This"report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 17

le
Analytical
www.pecala6a com
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92372431
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #6 Lab ID: 92372431006 Collected: 02/06/18 10:45 Received: 02/07/18 15:10 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua]
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.030 mglL 0.024 1 02/08/18 13:13 7782-50-5 H3
Date: 02/08/2018 06:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 17

leAnalj tical
www.Pecelabs,com
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92372431
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #7 LabID: 92372431007 Collected: 02/06118 11:05 Received: 02/07118 15:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500CL G Chlorine, Residual Analytical Method>SM 4500-CI G i .
Chlorine, Total Residual 0.038 mg1L 0,024 1 02/08/18 13:13 7782-50-5 H3
Date: 02/08/2018 06:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 17

lacmnalyfical-
wwwpacelahs am
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92372431
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersv4e, NC 28078
[phone]
Sample: NonContact #8 Lab ID: 92372431008 Collected: 02/06/18 11:30 Received: 02/07/18 15:10 Matrjx: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua!
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.24 mgtL 0.024 1 02/08/18 13:13 7782-50-5 H3
Date: 02/08/2018 06:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 11 of 17

e
IacleAna,(Xical
(I�wwwpacelabs coal
QUALITY CONTROL DATA
Project: NonContact Cooling Water
Pace Project No.: 92372431
Pace Analytical Services, CLC
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
QC Batch: 397273 Analysis Method: SM 4500-Cl G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92372431001. 92372431002, 92372431003, 92372431004, 92372431005, 92372431006, 92372431007,
92372431008
METHOD BLANK: 2203060 Matrix: Water
Associated Lab Samples: 92372431001, 92372431002, 92372431003, 92372431004, 92372431005, 92372431006, 92372431007,
92372431008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine, Total Residual mg/L ND 0.024 02/08/18 13:13
SAMPLE DUPLICATE: 2203061
92372277001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg/L 0,54 0.56 3 H1
SAMPLE DUPLICATE: 2203084
92372431008 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg1L 0.24 0.24 2 H3
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 06:53 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 17

e•
IaceAnalytical
(�»ww.pecelebs com
QUALIFIERS
Project: NonContact Cooling Water
Pace Project No.: 92372431
117=17t:IrlI912&I
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting limit.
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 6270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260,
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 06:53 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 17

le
Analytrcal
nww.pacelaW.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NonContact Cooling Water
Pace Project No.: 92372431
Lab ID Sample ID QC Batch Method QC Batch
92372431001
Non Contact #1
SM
4500-CI G
397273
92372431002
NonContact #2
SM
4500-CI G
397273
92372431003
NonContact 03
SM
4500-0 G
397273
92372431004
NonContact #4
SM
4500-CI G
397273
92372431005
NonContact #5
SM
4500-CI G
397273
92372431006
NonContact #6
SM
4500-CI G
397273
92372431007
NonContact #7
SM
4500-CI G
397273
92372431008
NonContact #8
SM
4500-CI G
397273
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical Method
Analytical
Batch
This report shall not be reproduced, except in full,
Date: 02/08/2018 06:53 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 17

Document Name:
Document Revised: January 24, 2018
1! aceAnalytical �
Sample Condition Upon Recel t(SCUR
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.05
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ HuntersviUL6 Raleigh[] Mechanicsvill2❑
ConditionClient Na e: Project Wok ' 92372431
Courier: [:]Fed Ex [:]UPS ❑USPS ❑Client III III 11111111111111111
❑ commercial [ [ ce ❑Other:
�/ 92372431
Custody Seal Present? [—]yes jlo seats Intact? ❑Yes T
o
Date/initials Person Examfning me
Packing Material: []Bubble Wrap ❑Bubble BagsqQane ❑ Other Biologic ssue Frozen?
Thermometer: __,,tt 11 ❑Yes ❑N/A
92TO36 type of Ice: et ❑Blue [-]None'
}
�GunlO:
Cooler Temp ('C): W.V Correction Factor-, Add/Subtract {'Ci t0.1 Temp should be above freezing to VC
Cooler Temp Corrected ('C): []Samples out of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Sol N/A, water sample)
Did samples orig[nate lip, quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source [Internationally,
I—IY.s r1Q. Inehidlno Hawaii and Puerte R[enl? FlYes C-i Q)
Comments/Discrepancy:
Chain of Custody Present?
No
N/A
1.
Samples Arrived within Hold Time?
No
N/A
2.
Short Hold Time Analysis <72 hr.)?
Yes
%o
[]N/A
3.
Rush Turn Around Time Requested?
Dyes
ONJA
C.
Sufficient Volume?.
El No
N/A"
S.
Correct Containers Used?
-Pace Containers Used?
es
es
[]No
[]NO
❑N/A
❑N/A
6.
7.
Containers intact? 4�5No N/A
Dissolved analysis: Samples Field Filtered?
Yes
[IN.
JA
S.
Sample Labels Match COC?
-Includes Date/lime/ID/Analysisx:
Matrix:
c /l�'es
�lf-�
❑No
❑N/A
9.
Heads ace in VOA Vials >5-6mm)?
Yes
No
`{. A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
Yes
1 �Tn
❑No
❑N/A
/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of SDlit containers:
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? ❑Yes []NO
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
Page 15 of 17

Document Name:
Sample Condition Upon ReceE t SCURj
Document Revised: January 24, 2018
Page 2 of 2
Document No.:
F-CAR•CS-033-Rev.05
Issuing Authority:
Pace Carolinas Quality Office
.. aceAnalytical
*Check mark top half of box if pH and/or dechlorination is Project # WQ# ; 92372431
verified and within the acceptance range for. preservation w�+
PM: MWB we Dale: 02/16/18
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water} DOC, UHg CLIENT: 92—A I l vae NC
"Bottom half of box is to list number of bottle
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pH Adjustment tog for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: Whenever there is a discrepancy affecting North Carolina com pliance sam pies, a ropy of this form wm be sent to the north ,,aroma urn +� �• ••�
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 16 of 17

Storm Water Monitoring
(NON CONTACT)
Bakers North
Chain of Custody Retord
-rftfATI
SPecWm Materials
page #1
Project Number/Name: NonContaiU Cooling Water
Project Location: Alivac Bakers
Sampler's Signature:
L'
,
Date:vz -el /8
G
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ro
a
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E
1=
a
E
s
2
a
w
�'
aLA
>CL
a
U
C
r,
s
a
a
cc
a
u
r
w
Requested Test
Parameters
QnCa
G
G
None
Y
o??. 07
Residual Chlorine
AbeG
G/O
None
Y
3
Residual Chlorine
G
GA)
None
Y
. a
IY. 8
Residual Chlorine
/d 4*4,f 'i
D :0
G
GAD
None
Y
./
Residual Chlorine
din ConfKt
0: �.
G
GA
None
Y
7.0
J, 9
Residual Chlorine
o„CM&0b
G
G/9
None
Y
Q.
Residual Chlorine
o Co f
/,DS
G
G/a
None
Y
D.!
Residual Chlorine
Once f
'.�
G
G
None
Y
. 7
vtaj
Residual Chlorine
Meter Calibrated:
®/ N
IThermometer Calibrated
®/ N
Sampling and Field analysis completed by:
01
Relinquished By:
Received B
ze-
Date :
Time:
1,1d
te:
rRecelvedAy
Time: 7-
Relin wished By:
:
Date., n
Time:
Date:
Time;
EHS Baker South SW REv p 2 5110/2016
r
f YIUC
I'
i
�e t
Page 17 of 17