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NCS000329_MONITORING INFO_20170825
STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. ocd DOC TYPE ❑ FINAL PERMIT -- MONITORING REPORTS---- ----- - ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ 016 " i, YYYYM M D D August 23, 2017 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files: *ATI P.O. Box 5030 2020 AshcraA Avenue Monroe, IBC 28111-5030 Phone: (704) 289.4511 Fax: (704)290-5194 Email: joe.hinkle(a)atimetals.com Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and one copy are included. The monitoring data is for the following monitoring schedule: Monitoring Period Sample Number Start End Year 8 — Period 1 15 March 1, 2017 August 31, 2017 Analytical monitoring includes: • Outfall #01 (B), commingled stormwater • Outfall #02 (B), non -commingled stormwater • Outfall #03 (B), non -commingled stormwater • Non Contact Cooling Water #1 - #8 If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sincerely, Joe Hinkle Environmental Manager on X a� c(- C^ - �:2 r'a < orn Q M Allvac - Bakers Plant ATI Allvac Stormwater Monitoring Report Form Sample Date: T g �g %� _ Sample Time: /a? • •�� Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analvsis: Stormwater Discharge_Outfall #0.1_ (Commingled) Drainage Area = 2915,470sq. ft. = 69 acres % Impervious = 34% 40 CFR Part 136 Parameter Results (mg/l) Benchmark Values (mg/1) BOD 7.02 30 COD a? 120 TSs joa l 100 Cadmium ND 0.001 Chromium, total recoverable ND 1 Copper, total recoverable D• 6023 0.007 Nickel, total recoverable AID 0.26 Zinc, total recoverable AP 0.067 Oil and Grease Ail? 20 Temp (receiving stream) 9. 9 (deg C) 32 (deg C) Total Residual Chlorine 0.017 pH O (std units) 6-9 (std units) Storm Date: 8'8__L? Storm Duration: airs.) Inches of Rainfall:O Duration of time preceding rain event exceeding 0.111: Z90? airs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(impervious Area) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches rain/12inches/ft. x 69 x .34) Q(Totai, cfs) = 1.5180 x Q . {&_© (Inches of rain) + 1.7595 x __ Q . (oD (Inches of rain) 1• q6�s c-�J *ATI Allvac Allvac - Bakers Plant Stormwater Monitoring Report Form Sample Date: Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Sample Time: /� -�WW+4 Stormwater Discharge Outfall #02 (Non -Commingled) Drainage Area = 212.9524. ft. = 4.9 acres % Impervious = 12% 40 CFR Part 136 r Parameter Results (mg/1) Benchmark Values (mg/1) BOD 6.6 30 COD 5�2Q 120 TSS 100 Cadmium ND 0.001 Chromium, total recoverable Q 1 Copper, total recoverable Q.0.007 Nickel, total recoverable O. DO 0.26 Zinc, total recoverable p3S 0.067 pH 6.8 (std units) 6-9 (std units) Storm Date: g Storm Duration: - - J • S (firs.) Inches of Rainfall: Duration of time preceding rain event exceeding 0.1 ": 9/ rZ- (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., efs) = (A x inches rain/12 inches/ft. x 49 acres x .88) + .9 x inches rain/ I 2inches/ft. x 4.9 x .12) Q(Total, cfs) = 0.1437 x (Inches of rain) + 0.0441 x 0. 60 (Inches of rain) 0.113 cfs 0ATIA11vac Allvae - Bakers Plant Stormwater Monitoring Report Form Sample Date:S-e:zz Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Sample Time: la? Sag Stormwater Discharge Outfall #03 (on —Commingled) Drainage Area = 336.580sa. ft. = 7.8 acres % Impervious = 15% 2!!!id _ r0 —z &e/yfca./ 40 CFR Part 136 Parameter Results (mg/1) Benchmark Values (mg/l) BOD s- 30 COD a?� D 120 TSS S a 100 Cadmium 0.001 Chromium, total recoverable I Copper, total recoverable ©Da 0.007 Nickel, total recoverable 0.26 Zinc, total recoverable D 0.067 pH 9 (std units) 6-9 (std units) Storm Date: Storm Duration: _.� _ (Hrs.) Inches of Rainfall t9. /f> Duration of time preceding rain event exceeding 0.I": .2?d _ (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) _ (A x inches rain/12 inches/ft. x 7.8 acres x .85) + 9 x inches rain/12inches/ft. x 7.8 x .15) Q(Total, cfs) = 0.2210 x jQ.40 (Inches of rain) + 0.0878 x D • (dam_ (Inches of rain) 19• /B.S- cfs Allvac - Bakers Plant Stormwater Monitoring Report Form Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Non-ContactCooling Wastewater r.6w.:d Pope Z-r, AAA GJon 4Z Pace ._�nalyfca% 40 CFR Part 136 -OATI Spedaity MWertais Non- Contact Cooling Water # Sampling Date Sampling Time Estimated Flow(MGD) Total Residual Chlorine (mg/L) Temperature pH (std. units) Effluent Downstream Upstream 30 . S°` 0?9 0'` z -31-17 oa.- D. 0007 D• 7 OV .3Oe a78.8` a (9 IF °e •3 3 , Doas p.is o?3•0°r or8.8'� 8.s°` 7.6 4 D, Ow-r 0.08s )9. 7°° 0?8. Yoe 0?8. 6'` S. 0 5 7'3/- 7 8.02.-- 0• 00a9 0.61?7 8,` 0a. YOe- 028, ?a` 7. 7 s '3/ /7 `., O,OD9 40.031 0?9 C)°G o?8•Soa J.B'� s' 4•007a -o ai3o� a �,8�a a8•I°� s 8 '7-3//7 0.0a10 .o 9.,r I STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS s-4000.342(F FACILITY NAME T.� �9��vQG �e/S PERSON COLLECTING SAMPLE ) i T7C e. CERTIFIED LABORATORY(S) 5LQ.,e Lab # /a?_ Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 4WI (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY � SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. DateII Sample Collected I Total Flow Total WI-3FJI 1' Iwl���� I Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage moldd/yr MG inches m MgA unit al/mo Form SWU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date,?-8 l7 Total Event Precipitation (inches): �- Q Event Duration (hours): /• T (only if applicable —see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ' 441-br1 17 (Signature of Perm' tee) (Date) Form SWU-247, last revised 21212012 Page 2 of 2 LWKWA NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http�/portal.ncdenr.grglw(- wgfws/su/npdessw#tab -4 Permit No.: N/C/3"/o/ o/Q/,�/�/�/ or Certificate of Coverage No.: Facility Name: At1' 41&xe, - J.Cerr County: !.!„siva _ Phone No. 7� S Inspector: 2,L, aW Date of Inspection: Time of Inspection: Wao, _ Total Event Precipitation (inches): 49• 64 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) F Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred.' A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. Si✓o Structure (pipe, ditch, etc.) T'V/ / L4W Receiving Stream: D Cr e�C Describe the industrial activj ies that occur within the outfall drainage area: 2. Color: Describe the color of the d (light, medium, dark) as descriptors: using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.). / 4917 e 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: Q 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: © 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: Q 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes V� 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe _1✓D/7 e- Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5WU-242, Last modified 10/25/2012 LTXWW 'Al NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out thisform, please visit. http://portal.ncdenr.org.IwLbkw—q/ws/su/ni2dessw#tab-4 Permit No.: N/Q;r/ D/ O/Q/,j/d/j/ or Certificate of Coverage No.: N/C/G/_/—/_/_/_/_/ Facility Name: " &LUe -A-X�s _ County: _ Inspector: Phone No. Date of Inspection: _ 8 8/7 Time of Inspection: 1023�.- Total Event Precipitation (inches): e-4 0 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) 101`�Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event' or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for Iocal storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: :f Y 1. Outfall Description: .� Outfall No. -sWG- Structure (pipe, ditch, etc.) _ R Receiving Stream: eel Describe the industrial activities that occur within the outfall drainage area: ate rxl__s,���e 2. Color: Describe the color of the di (light, medium, dark) as descriptors: asic colors (red, brown .blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /a0/111e, 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: ri 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 ©1 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes 6 10. Other Obvious Indicators of Stormwater Pollution: List and describe Ille/l6 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. SWU-242, Last modified 10/25/2012 Page 2 of 2 4 v k NCDENR Stormwater Discharge autfall (SDU) Qualitative Monitoring Report Forguidance on filling out this form, please visit. http://portal.ncdenr,org/web/wg/ws/su./nl2dessw#tab-4 Permit No.: or Certificate of Coverage No.: N/L/.Qx/_/_/_/_/_/_/ Facility Name: County: G Phone No. 74y AO- !YXI/ -- Inspector: .1/4yid _&pG__J�L Date of Inspection: Time of Inspection: •'.S(pa..- _ ,_,, Total Event Precipitation (inches): & - Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) 2/Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. 5W63 Structure (pipe Receiving Stream: ,�rll ,ia' Describe the industrial activities tha of ccur ditch, etc.) n the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: T e Ca/ _ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): y4VAe 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: ® 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 6) 3 4 5 G. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: p 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes B. Is there an oil sheen in the stormwater discharge? Yes (� 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe z 4o& e , Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further Investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 laneAnalyticalc www.paceiebs.com August 18, 2017 Mr. Joe Hinkle Allvac RE: Project: Bakers Stormwater Pace Project No.: 92350554 ,gswol Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2807B (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on August 08, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 20 Pace Analytical Services, LLC laneAnalyficalf 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pecelabe,com (704)875-9092 CERTIFICATIONS Project: Bakers Stormwater Pace Project No.: 92350554 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification M 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Flodda/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 South Carolina Certification #: 99006001 Flodda/NELAP Certification #: E87627 Kentucky UST Certification #: 84 UrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VrginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 2 of 20 1c aceAnalytical www.peceletr� cam SAMPLE ANALYTE COUNT Project: Bakers Stormwater Pace Project No.: 92350554 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)675-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92350554001 BSW01 SM 2540D SLB 1 PASI-A 92350564002 BSW01 SM 52108 ECH 1 PASI-A 92350554003 BSW01 SM 5220D NAL 1 PASI-A 92350554004 BSW01 EPA 1664E JMS 1 PASI-C 92350554005 BSW01 EPA 200.7 SER, SH1 5 PASI-A 92350554006 BSW01 SM 4500-CI G MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 20 laneAnalytical" www.pocelabs,com ANALYTICAL RESULTS Project: Bakers Stormwater Pace Project No.: 92350554 Pace Analytical Services, LLC 9800 KinceyAve, Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BSW01 Parameters Lab ID: 92350554001 Collected: 08/07/17 00A2 Results Units Report Limit DF Received: 08/08/17 11A2 Matrix: Water Prepared Analyzed CAS No,' Qual Field Data Analytical Method: Collected By DPJ 1 08/08/17 00:40 Field pH 8 Sid. Units 0.10 1 08/08/17 00:40 Field Temperature 29.9 deg C 0.50 1 08/08/17 00A0 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 32.4 mg1L 10.0 1 08/10/11 14:27 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in futt, Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 20 e 5aceAnalXical 1�lwww.pecelebs,MM I ANALYTICAL RESULTS Project: Bakers Stormwater Pace Project No.: 92350554 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 kuntersville, NC 28078 (704)875-9092 Sample: BSW01 Lab ID: 92350564002 Collected: 08/08/17 00:43 Received: 08/08/17 11:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5210B BOD, 5 day Analytical Method: SM 5210B SOD, 5 day 7.2 mg1L 2.0 1 08/09/17 20A5 08/14/17 15:12 Date: 0811812017 06:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 20 aceAnalytical www.pacebbs.com ANALYTICAL RESULTS Project: Bakers Stormwater Pace Project No.: 92350554 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )875-9092 Sample: BSW01 Lab ID: 92350554003 Collected: 08/08/17 00:45 Received: 08108/17 11:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5220D COI] Analytical Method: SM 5220D Chemical Oxygen Demand 82.0 mg1L 25.0 1 08/14/17 14:05 Date: 08/18/2017 06:37 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC. Page 6 of 20 c aceAnalytical www.pscel9b3.0DM ANALYTICAL RESULTS Project: Bakers Stormwater Pace Project No.: 92350554 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BSW01 LAID: 92350564004 Collected: 08/08/17 00:46 Received: 08/08/17 11:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 08/16/17 05:30 Lsh3Ca[rI:Iff:I��riil�I'i[c3>l�] REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 20 e aceAnalytical www.pacelatrs.00m ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huniersville, NC 28078 (704)875-9092 Project: Bakers Stormwater Pace Project No.: 92350554 Sample: BSW01 Lab ID: 92350554005 Collected: 08/08/17 00:47 Received: 08/08/17 11:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug1L 1.0 1 08/14/17 23:30 08/18/17 16:40 7440-43-9 M1 Chromium ND ug1L 5.0 1 08/14/17 23:30 08/17/17 20:26 7440-47-3 Copper 22.8 ug1L 5.0 1 08/14/17 23:30 08/17/17 20:26 7440-50-8 Nickel ND uglL 5.0 1 08/14/17 23:30 08/18/17 16:40 7440-02-0 M1 Zinc ND ug1L 10.0 1 08/14/17 23:30 08/18/17 16:40 7440-66-6 M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08118/2017 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 20 aceAnalytrcal ~.peeeleDt.caw ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Project: Bakers Slormwater Pace Project No.: 92350554 Sample: BSW01 Lab ID: 92350554006 Collected: 08/08/17 00:49 Received: 08/08/17 11:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua! 4500CL G Chlorine, Residual Chlorine, Total Residual Date: 0811812017 06:37 PM Analytical Method: SM 4500-CI G 0.071 mg1L 0.024 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 08/1511714:22 7782-50-5 H1 Page 9 of 20 aceAnalytical wm..pambbs,corn QUALITY CONTROL DATA Project: Bakers Stormwater Pace Project No.: 92350554 Pace Analytical Services, LLC 9Boo KinceyAve. Suite too Huntersville, NC 28078 (704)875-9092 QC Batch: 373538 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92350554004 METHOD BLANK: 2069811 Matrix: Water Associated Lab Samples: 92350554004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 08/16/17 05:18 LABORATORY CONTROL SAMPLE: 2069812 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 37.1 93 78-114 MATRIX SPIKE SAMPLE: 2069813 35329509001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL 54.5 40 92.9 96 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit in presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 20 aceMalytical www.pacelabs.com QUALITY CONTROL DATA Project: Bakers Stormwater Pace Project No.: 92350554 QC Batch: 373202 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis, Description: 200.7 MET Associated Lab Samples: 92350554005 METHOD BLANK: 2067775 Matrix: Water Associated Lab Samples: 923,90554005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium ug1L ND 1.0 08/17/17 20A0 Chromium ug1L ND 5.0 08/17/17 20:10 Copper ug1L ND 5.0 08/17/17 20:10 Nickel ug1L ND 5.0 08f17117 20:10 Zinc ug1L ND 10.0 08/17/17 20:10 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvi0e, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2067776 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug1L 500 472 94 85-115 Chromium ug1L 500 473 95 85-115 Copper uglL 500 492 98 85-115 Nickel ug1L 500 463 93 85-115 Zinc uglL 500 484 97 85-115 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2067777 2067778 MS MSD 92350554005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPI] Qual Cadmium ug1L ND 500 500 307 305 61 61 70-130 0 M1 Chromium ug1L ND 500 500 477 478 95 95 70-130 0 Copper uglL 22.8 500 500 505 515 96 99 70-130 2 Nickel uglL ND 500 500 306 305 61 60 70-130 0 M1 Zinc uglL ND 500 500 323 323 64 64 70-130 0 M1 Reauits presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0811812017 06:37 PM without the written consent of Pace Analytical Services. LLC. Page 11 of 20 laneAnalyficals wwwpacelabs.cam QUALITY CONTROL DATA Project: Bakers Stormwater Pace Project No.: 92350554 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 372690 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92350554001 METHOD BLANK: 206488E Matrix: Water Associated Lab Samples: 92350554001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 08/10/17 14:24 LABORATORY CONTROL SAMPLE: 2064889 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 248 99 90-110 SAMPLE DUPLICATE: 2064890 92350492003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 20W91 92350554001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 32.4 32.4 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/18/2017 06:37 PM without the written consent of Pace AnalyticaS Services, LLC. Page 12 of 20 is aceAnalytical wwwpsoelebs.com Project: Bakers Stormwater Pace Project No.: 92350554 QC Batch: 373303 QC Batch Method: SM 4500-Ci G Associated Lab Samples: 92350554006 METHOD BLANK: 2068370 Associated Lab Samples: 92350554006 Parameter Units Chlorine, Total Residual mg1L QUALITY CONTROL DATA Analysis Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.024 08/151171422 SAMPLE DUPLICATE: 2068371 92350405001 Dup Parameter Units Result Result Chlorine, Total Residual mg1L ND ND RPD Qualifiers H1 Pace Analytical Services, LLC 9800 Kircey Ave. Suite too Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 20 aceAnalytical worw.pacofabS.cvm Project: Bakers Stormwater Pace Project No.: 92350554 QC Batch; 372626 QC Batch Method: SM 5210B Associated Lab Samples: 92350554002 METHOD BLANK: 2064396 Associated Lab Samples: 92350554002 Parameter Units GOD, 5 day mg1L LABORATORY CONTROL SAMPLE: 2064397 Parameter Units GOD, 5 day mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 5210B Analysis Description: 52108 GOD, 5 day Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2,0 08/14/17 14:57 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 206 104 84.6-115.4 SAMPLE DUPLICATE: 2064398 92350649008 Dup Parameter Units Result Result GOD, 5 day mg1L 3,1 3.4 RPD Qualifiers 9 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/16/2017 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 20 aceAnalytical www.pecelabs.=n QUALITY CONTROL DATA Project: Bakers Stormwater Pace Project No.: 92350554 QC Batch: 373047 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5224D COD Associated Lab Samples: 92350554003 METHOD BLANK: 2067169 Associated Lab Samples: 92350554003 Parameter Units Chemical Oxygen Demand mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 08/14/17 14:05 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hurtersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2067170 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 722 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067171 2067172 MS MSD 92350458005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 115 750 750 879 867 102 100 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067173 2067174 MS MSD 92350498001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 32.0 750 750 789 797 101 102 90-110 1 Results presented on this page are In the unite indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 20 1aceAnalyfical e www.pwelabs com QUALIFIERS Project: Bakers Stormwater Pace Project No.: 92350554 b]4;C11110RI-9 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hurtersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 20 aceAnalyticat wwwpecelabs,cam QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Bakers Stormwater Pace Project No.: 92350554 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92350554001 BSW01 92350554004 BSW01 EPA 1664B 373538 92350554005 BSW01 EPA200.7 373202 EPA200.7 373510 92350554001 BSW01 SM 2540D 372690 92360554006 BSW01 SM 4500-CI G 373303 92350554002 BSW01 SM 5210B 372626 SM 5210B 372670 92350554003 BSW01 SM 5220D 373047 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/18/2017 06:37 PM without the written consent of Pace Analytical Services, LLC, Page 17 of 20 Document Name: Document Revised: August 4, 2017 Sam le Condition Upon Receipt(SCUR) Page 1 or 2 Document No.: Issuing Authority: aceAnalytical, F-CAR-CS-033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ HuntersvilIQ Raleigh❑ Mechanicsville[] Client Name: WO# : 92350554 .. U ----Praject#;Courier: []Fed Ex❑UPS ❑LISPS ❑Client ❑ Commercial 11_(jpace ❑Other: 92330934 I111 I + Custody Seal Present? Dyes �lo Seals Intact? Dyes o ``CC Date/Initials Person Examining Canter 1 " Packing Material: [—]Bubble Wrap ❑Bubble Bags 14QNDne ❑ Other Biolo is sue Frozen? ThermoMeter: ❑yes ❑N/A Gun 10:j et [—]Blue ❑None Type of Ice: ILO Correction Factor: Cooler Temp Corrected ('C): Temp should be above freezing to 6'C ❑Samples out of temp criteria. Samples on ice, tooting process has begun USDA Regulated Soil,(j�N/A, water sample) Did sample or g ate inkquarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source tint nptlonally, I—IM rincluding Hawaii and Puerto RicoI7 FIYes o Comm ents/Discrepancy: Chain of Custody Present? es No N/A 1. Samples Arrived within Hold Time? s ❑No ❑N/A 2. Short Hold Time Anal sis <72 hr.)? es ONO ❑NJA 3. Rush Tum Around Time Requested? M Yes CINIA 4. sufficient volume? ONO ❑NJA 5. Correct Containers Used? -Pace Containers Used? es ❑No No ❑N/A 171111A 6. Containers Intact? s ❑Na ❑NJA 7. Dissolved analysis: Samples Field Filtered? Oyes ❑No A a. Sample Labels Match COC? -includes Date/Time/ID/Analysis Matrix: \-�Ys ❑No N/A 9. Headspace in VOA Vials (>5-6mm)? ❑Yes ❑No )f§;/A 10, Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes []Yes � )b []NO ❑N/A A 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Lot 10 of split containers: Project Manager SCURF Review: Project Manager SRF Review: Field Data Required? L_JYes LJNo DateMme: Hate: �C/p / l �7 Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of This form will be sent to the North Carolina DEHNR Certification Office (Le. Out of hold, incorrect preservative, out of temp, Incorrect containers) Page 18 of 20 m 3 0 v m m x b n -a n Q O Y C LA is m H m O �y ^• O a � O n n m m 3 r2o re b tl 9 to iv a u � o tD � N 0 Y w A M a � n K n 0 a Itemll BP41.1-125 mL Plastic Unpreserved (N/A) (Cl-) 811313-250 mL Plastic Unpreserved (N/A) BP2U-500 mL Plastic Unpreserved (N/A) 81,111-1 liter Plastic Unpreserved (N/A) BP45-125 mL Plastic H2SO4 (pH < 2) (CI-) BP3N-250 mL plastic HNO3 (pH < 2) AZZBP4Z-125 mL Plastic ZN Acetate & NaOH (>9) BP4C-125 mL Plastic NaOH (pH > 12) (CI-) WGFU-Wide-mouthed Glass Jar Unpreserved AGIU-1 liter Amber Unpreserved INN (C1-) AGIH-1 liter Amber HCl (pH < 2) AG3U-250 mL Amber Unpreserved (N/A) (CI-) AG1S-1 liter Amber H2SO4 (pH < 2) AG3S-250 mL Amber H2SO4 (pH < 2) AG3A(DG3A)-250 mL Amber NH4C1 (N/A)(CI-) DG9H-40 mL VOA HCI (N/A) V69T-40 mL VOA Na25203 (N/A) V69U-40 mL VOA Unp (N/A) DG9P-40 ml VOA H3PO4 (N/A) VOAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/Aj SPST-125 mL Sterne Plastic (N/A— lab) SPZT-250 mL Sterile Plastic (N/A —lab) BP3A-250 mL Plastic tNH2)2SO4 {9.3-9.7) Cubitainer VSGU-20 mL Scintillation vials (N/A) G11 w � u s -' t ? Op t,+ mp =r O w H, d � o h 3 s tT -q S = m x H 3 a O ffb Cr tu 0 -+ tm, 7 Cr Of m 01 O O� Cr � m O � y� O m T � o Agra ° m 3 W 8 i7 Z 0 a ro o c p 3 m � O � � A L to n � n 3t -O r s 3 3 N m OC ro n anw d > ro —� ^ G N n 0 Zt R > N OCO c Cif C 10 /� A O � p 8 .10 r+ J r J p PaceAnalytical' .rr_suelaM.mm CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain-of-Cuslody is a LEGAL DOCUMENT. All relevant trelds must be completed accurately. Section A Section 8 Section C Page: of Required Client Inromtaum Required Projectation; InformInvoice Information• company: �, _ Report To* 2177354 Address s. %1C Copy To..., G �[ Company Name ► REGULATORY AGENCY `' AddressMllo NPDES I— GROUND WATER i DRINKING WATER UST r RGRA OTHERof Email To: Purchase Order No.: Para Q" e me: P / Fax: Projetl Name: r e ace Prc}ea Ivtanagar: Site Lrxarion STATE. /�J r •' v Requested Due DatolTAT: Project Number- Paw PfolYe e' Requested Analysis Fittered (YMj Section D Matrix coders c z Requlmd Chant Information MATRIX f CODE E o COLLECTED Preservatives i D6*ing Water OW 0 0 Water WT waste Water WW Product P * 6 Sc TMtT E COMPm EnPOSITE tQtr V — Z SOVSpld SL C1 0 } SAMPLE ID a. OL a m e Wipe WP (A-Z, 6.91,-) Air AR lL 0 �- ur Q Z ` Sample IDS MUST BE UNIQUE Tissue TS O 0 a �: H z m m U Other OT x a w a Ui a O m 0 F < O c« O Z U p= m ni m L Q m — DATE TIME GATE TIME = Z Z Z Z O y tY Pace Project No.! Lab I.O. SWOT c3- �,f 1 z W 0 G /1 .7 3 swo 1 w 6 = � a s wO tiIJ ev 8-8� ¢ I y s SWo 1 6 g-17 = Ir 6 swa! 877 ,�: Y o 7 9 J10 it ,z ADDITIONAL COMMENTS RELINQUISHED BY 1 AFFIUATION DATE TIME ACCEPTED BY I AFFILIATION HATE TIME SAMPLE CONDITIONS a9 �4fdt�— B.oAAd i 14 1't LLB)3-�- r&Alf '18� SAMPLER NAME AND SIGNATURE c `e Un ORIGINAL N PRINT Name of SAMPLER: �, t � : > .� o g z` q '= z 5- p DA Slgned SIGNATURE of SAMPLER., ' E r m m `—' K m� O `m N p N � 'lmpnnant 14M,: By Sran'ma It- loan YOU -W �PIXV P,w 'S NET 30 day paymanf tenmy and agrepetg tO lain hirges of 1.5%9er month W any inverses rot paid wdhit 30 dit" " F-ALL-"20rev.07, , 5-May-2007 aceAnalytical www.poulabs.com I August 17, 2017 Mr. Joe Hinkle Allvac RE: Project: Bakers Stormwater Pace Project No.: 92350557 gswoa? Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on August 08, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures CC: Mr, Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shag not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 or 16 Pace Analytical Services, LLC 6 aceAnalytica! 980D KinceyAve. Suite 100 Huntersville, NC 28078 sww.Pecelabs.wm (704)875-9092 CERTIFICATIONS Project: Bakers Stormwater Pace Project No.: 92350557 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 worth Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification* E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 South Carolina Certification #: 99006001 Florida/NELAP Certification #; E87627 Kentucky UST Certification #: 84 VrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VrginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 16 Pace Analytical Services, LLC aceAnalyticals 9800 Kincey Ave. Suite 100 Huniersvi0e, NC 28078 Ww,pecelabs com (704)875-9092 SAMPLE ANALYTE COUNT Project: Bakers Stormwaler Pace Project No.: 92350557 Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92350557001 BSW02 SM 2540D WC 1 PASI-A 92350557002 BSW02 SM 5210E ECH 1 PASI-A 92350557003 BSW02 SM 5220D NAL 1 PASI-A 92350557004 BSW02 EPA 200.7 SER 5 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 16 Pace Analytical Services, LLC leac,AnalXical saoo KinceyAve. Suite toa Muntersville, NC 28078 www.pacatabs.00m (704)875-9092 ANALYTICAL RESULTS Project: Bakers Stormwater Pace Project No.: 92350557 Sample: BSW02 Lab iD: 92350557001 Collected: 08/08/17 00:32 Received: 08/08/17 11:12 Matrix; Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method; Collected By DPJ 1 08/08/17 12:30 Field pH 6.8 Sid. Units 0.10 1 08/08/17 12:30 Field Temperature 26.5 deg C 0.50 1 08/08/17 12:30 2S40D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 70.0 mg1L 12.5 1 08/10/17 23:58 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 08/17/2017 10:09 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 16 aceAnalytical www,p&cebbs,cam ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bakers Stormwater Pace Project No.: 92350557 Sample: BSW02 Lab ID: 92350557002 Collected: 08/08/17 00:34 Received: 08/08/17 11:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 62108 BOD, 5 day BOD, 5 day Date: 08/17/2017 10:09 AM Analytical Method: SM 5210B 6.6 mg1L 2.0 1 08/09117 20:45 08/14/17 15:09 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 16 laneAnalyfical' www.pecelab3.0om ANALYTICAL RESULTS Project: Bakers Starmwater Pace Project No.: 92350557 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BSW02 Lab ID: 92350557003 Collected: 08/08/17 00:35 Received: 08/08/17 11:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qual 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 52.0 mg1L 25.0 1 08/14/17 14:05 Date: 08/1712017 10:09 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 16 laneAnalyfical" www.pecowin.cam ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bakers Stormwater Pace Project No.: 92350557 Sample: BSW02 Lab 1D: 92350557004 Collected: 08/08/17 00:37 Received: 08/08117 11:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug1L 1.0 1 0811411714:10 08/15/1715:54 7440-43-9 Chromium 7.3 ug1L 5.0 1 0811411714:10 08/1511715:54 7440-47-3 Copper 140 ug1L 5.0 1 0811411714:10 08/15/1715:54 7440-50-8 Nickel 6.4 ug1L 5.0 1 08114/1714:10 08/15/1715:54 7440-02-0 Zinc 35.4 ug1L 10.0 1 08114/1714:10 08115/1715:54 7440-66-6 Date: 08/17/2017 10:09 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 16 aceAnalytical " WWW..PK*il t*.corn QUALITY CONTROL DATA Project: Bakers Stormwater Pace Project No.: 92350557 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 372824 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92350557004 METHOD BLANK: 2065686 Matrix: Water Associated Lab Samples: 92350557004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium uglL ND 1.0 08/1511714:26 Chromium uglL ND 5.0 0811511714:26 Copper uglL ND 5.0 08115/1714:26 Nickel ug1L ND 5.0 08/15117 14:26 Zinc uglL ND 10.0 08115/1714:26 LABORATORY CONTROL SAMPLE; 2065687 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug1L 500 478 96 85-115 Chromium ug1L 500 482 96 85-1115 Copper ug1L 500 507 101 85-115 Nickel ug1L 500 481 96 85-115 Zinc ug1L 500 499 100 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2065688 2065689 MS MSD 92350542001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua] Cadmium ug1L ND 500 500 473 464 95 93 70-130 2 Chromium uglL ND 500 500 490 473 96 95 70-130 1 Copper ug1L 0.017 500 500 521 515 101 100 70-130 1 mg1L Nickel ug1L ND 500 500 476 469 95 94 70-130 1 Zinc uglL ND 500 500 496 489 98 96 70-130 1 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2065690 2065691 MS MSD 92350498001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug1L ND 500 500 460 453 92 91 70-130 2 Chromium uglL ND 500 500 469 462 94 92 70-130 2 Copper uglL ND 500 500 513 505 102 101 70-130 2 Nickel uglL ND 500 500 467 461 93 92 70-130 1 Zinc ug1L ND 500 500 491 485 97 96 70-130 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0811712017 10:09 AM without the written consent of Pace Ana4ytical Services, LLC. Page 8 of 16 e aceAnap cal www.p&celabs.com QUALITY CONTROL DATA Project: Bakers Stormwater Pace Project No.: 92350557 QC Batch: 372821 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 254OD Total Suspended Solids Associated Lab Samples: 92350557001 METHOD BLANK: 2065670 Associated Lab Samples: 92350557001 Parameter Units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: 2065671 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 2065672 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 2065673 Parameter Total Suspended Solids Pace Analytical Services, LLC 9800 KinceyAver Suite 100 Huntersville, NC 2B078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 08/10/17 23:50 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 258 103 90-110 92350737001 Dup Result Result RPD Qualifiers 183 D6 92350675001 Dup Units Result Result mg/L 34.7 37.3 RPD Qualifiers 7 D6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the resuh. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fult, Date: 08/17/2017 10:09 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 16 O aceAnalytical www.pecetabs.com QUALITY CONTROL DATA Project: Bakers Stormwater Pace Project No.: 92350557 QC Batch: 372626 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 92350557002 METHOD BLANK: 2064396 Associated Lab Samples: 92350557002 Parameter Units BOD, 5 day mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 08/14117 14:57 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2064397 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg1L 198 206 104 84.6-115A SAMPLE DUPLICATE: 2064398 92350649008 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg1L 3.1 3.4 9 Results presented on this page are In the units Indicated by the "Un%s" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/1712017 10:09 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 16 5ceAna1j#ical wsw.pecelebs.cam QUALITY CONTROL DATA Project: Bakers Stormwater Pace Project No.: 92350557 QC Batch: 373047 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92350557003 METHOD BLANK: 2067169 Associated Lab Samples: 92350557003 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 2067170 Parameter Units Chemical Oxygen Demand mg1L Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 08114/1714:05 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 722 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067171 2067172 MS MSD 92350458005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 115 750 750 879 867 102 100 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067173 2067174 MS MSD 92350498001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 32.0 750 750 789 797 101 102 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/1712017 10:09 AM without the written consent of Pace Analytical Services, LI-C. Page 11 of 16 Pace Analytical Services, LLC Iaclmalyfical", 9800 KineyAve. Suite 100 Huntersville, NC 29078 (�www.pscelabs.com (704)875-9092 QUALIFIERS Project Bakers Stormwater Pace Project No.: 92350557 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL -Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/1712017 10:09 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 16 leAnalytrca! www.pecefa6s.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Bakers Stormwater Pace Project No.: 92350557 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92350557001 BSW02 92350557004 BSW02 EPA 200.7 372824 EPA 200.7 373300 92350567001 BSW02 SM 2540D 372821 92350557002 BSW02 SM 5210B 372626 SM 52106 372670 92350557003 BSW02 SM 5220D 373047 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/1712017 10:09 AM without the wntten consent of Pace Analytical Services, LAC- Page 13 of 16 Document Name: Document Revised: August 4, 2017 aceAna! !Ca!' Sample Condition Upon Recei t(SCUR) Page 1 of 2 Document No,: Issuing Authority: F-CAR-CS•033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville� Ralelgh❑ Mechanicsville[] Sample.. Client Nam e: : WOW 92350557 Project Courier: FlEed Ex UPS USPS ❑❑ ❑ Client 11111111111111111111111 Commercial p ❑ c ate ❑Other. i 92350557 Custody Seal Present? ❑Yes 4A0 Seals Intact? ❑Yes Ile Date/Initials Person Examining Packing Material: ❑Bubble Wrap ❑Bubble Bags one ❑ Other Biological Tissue Frozen? Thermomet r: ` Gun ID: Typ�t cf Ic 'C ❑Yes QlAo ❑N/A ❑Blue []None Correction Factor: Cooler Temp Corrected ('C): Temp should be above freezing to VC ❑Samples out of temp criteria. Samples on ice, cooling process USDA Regulated Soil /A, water sample} has begun Did samples or mate In a quarantine zone within the United States: CA, NY, or SC (check Ayes (Io maps)? Did samples originate from a Foreign source iinternationatiy, indudine Hawaii and Puerto Ricoi? nYes . Mo Comments/Discrepancy: Chain of Custody Present? sLas No N/A 1. Samples Arrived within Hold Time? No N/A 2. Short Hold Time Analysis (02 hr.)? Yes ❑No EINIA 3. Rush Turn Around Time Requested? Yes a NIA 4. Sufficient Volume? s No N/A 5. Correct Containers Used? -Pace Containers Used? es ❑No No ❑N/A N/A 6. Containers Intact? KP s No ❑NIA 7. Dissolved analysis: Samples Field Filtered? Des 0140 t/A 8. Sample Labels Match COC? -Includes Date�me/ID/Anal sis Matrix: f1 j� r*Y i V V�''t'�� [-]No N/A 9. Heads ate in VOA Vials (>5.6mml? ❑yes ❑N /A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑ves ❑Yes ❑No ❑N/A LELA 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Lot ID of split containers: Project Manager SCURF Review: s Date/Time: Date: of ii Field Data Required? []Yes []No Project Manager SRF Review: (�(� Date: LY /-? } __ NOW Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out or hold, incorrect preservative, out of temp, incorrect containers) Page 14 of 16 03 to m m 0 v 3 a O n v A A c m `m x v A -o z n a v b C N 3 m M d —' r O CrOl � c Oa � m o. ro to tD 3 rD d CL a Ln e's � c rp 3 r3. n n v m � R M N d A 0 u i.+ O w to v of N A w N r Item# BP4U-125 mL Plastic Unpreserved (N/A) (Cl-) BP3U-250 mL Plastic Unpreserved (N/A) BP2U-SOO mL Plastic Unpreserved (N/A) BP1U-1 liter Plastic Unpreserved (N/A) BP45.125 mL Plastic H2504 (pH < 2) (CI-) BP3N-2SO mL plastic HNO3 tpH < 2) SP4Z-125 mL Plastic ZN Acetate & NaOH (>9) 111134C-125 mL Plastic NOOK (pH > 12) (CI-) WGFU-Wide-mouthed Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (CI-) AG1H-1 liter Amber HCI (pH < 2) AG3U-250 mL Amber Unpreserved (N/A) (CI-) AGiS-1 liter Amber H2SO4 (pH < 2) ZXVAG3S-250 mL Amber H2SO4 (pH < 2) AG3A(DG3A)-250 mL Amber NH4C1 (N/A)(CI-) DG911-1-40 mL VOA HCI (N/A) VG9T-40 mL VOA Na25203 (N/Al VG9U-40 mL VOA Unp (N/A) DG9P-40 mt VOA H3PO4 (N/A) VOAK (6 vials per kit)-5035 kit (N/A) V/GX (3 vials per kit)-VPH/Gas kit (N/A) SPST-125 mL Sterile Plastic (N/A — lab) SPZT-250 mt Sterile Plastic (N/A — tab) BP3A-250 mL Plastic (NH2)2504 (9.3-9.7) Cubttaincr VSGU-20 mL Scintillation vials (N/A) GN o � < D 3 S O or m � 3 a Q 13 S 0 N 3 N � S .. ro D � W n R ro 3 R C 3 Cr n ro ro D w 7 Cr O ro rR+ O rn � N n S ro 3 6r x D S N 0 Cr O X tv 3 D. 0 IL ro n z 0 Cu 0 3 O QD N CAW V A 9 A MC V I j rn FaceAnalytical" r.. eaeelahe eem CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain-af-Custody is a LEGAL DOCUMENT. AN relevant fields must be competed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company' Ret T�s� Attention: 2177355 yy�4hr � 1 tt -5aezt�At kv b; o� Address 7�yr�ri/Q/WT�+��c,l� Copy J Ve Tv: ,� /y G d i CompanylVamc: C ��f� REG LATORYAGENCY N muVp� �EVMon2 Ae NPDES r GROUNDWATER j- DRINKING WATER F UST r RCRA i OTHER Email To: Purchase Order No.: gO14ioie Fiaferer�e: Fax•. Project Name: L P.O praged Manager: Site Location STA TE: /j�/ ! �L, 11 k Iji Requested Due DatofrAT: Project Number- Pa°° 'b A Requested Analysis Filtered (Y/N) 11 J Section D Matrix Codas E. z Required Client Inlormatan MATRIX ! CODE o 3 COLLECTED Preservatives > j Drinking water Dw :! U Oz water wT Wastewater WW :$f .H m S11 TART couPos B w Z_ Product P Soil/Solid St. o s 0 � ..► SAMPLE ID oil OL � a m IA-z, Q9 ! :) Air AR O w o. n H - t7 Sample IDs MUST BE UNIQUE Tissue TS O a � w @ 411 U Other 07 U X w � w O N 0 m Ta 41 0. w moa z�rm q� 9�350557 uy DATE TIME DATE TIME N U _ = 2 z Z M L Q y D: Pace Project Nod Lab I.U. + 51+10 Mf Cr -B J7 "' oa I z oa w .8 �� rX I I 3 shroa err a- -a 17 X I Id oC�03 a S wo r Cr 6- -! 5 6 7 8 9 10 11 12 RTIME ADDITIONAL COMMENTS RELINQUISHED BY / AFFILIATION DATE ; ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS S-8 / I e d • 364, ORIGINAL SAMPLER NAME AND SIGNATURE � p z _`v b S A E PRINT Name of SAMPLER; r ,' C m .a o} ; y Z �Y 2 aEi FOf `—' U a to a •� E rn SIGNATURE of SAMPLER. OAT Igned tMM/DD1YYi: �� ! •Imparam N Wa: By suing Ifns lorm yea are acceotin{I Pace's NET 30 day payetent Lamas and agromrg to Late charges of i.5% Per manth for any In0061 fte Paid eilhn 30 days. f- F-ALL-"20rev.07, 15-May-2007 IacleAnalytical (� wyrw.pettle6s.mm August 16, 2017 Mr. Joe Hinkle Allvac RE: Project: Bakers Stormwater Pace Project No.: 92350558 & VO-9 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NO 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on August 08, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac pk,C r REPORT OF LABORATORY ANALYSIS 1FN� This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 16 laneAnalytical www.pacelabs.com Project: Bakers Stormwater Pace Project No.: 92350558 Pace Analydcal Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersviile, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloddalNELAP Certification #: E87648 Massachusetts Certification #; M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 VrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 16 Iacmnalytica( Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 wwwpwefbs cm (704)875-9092 SAMPLE ANALYTE COUNT Project: Bakers Stormwater Pace Project No.: 92350558 Analytes Lab ID Sample 1D Method Analysts Reported Laboratory 92350558001 BSW03 SM 2540D SLB 1 PASI-A 92350558002 BSW03 SM 52108 ECH 1 PASI-A 92350558003 BSW03 SM 5220D NAL 1 PASI-A 92350558004 BSW03 EPA200.7 SER 5 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 16 Pace Analytical Services, LLC _ 1ce1 Analytical 9800 Kincey Ave. Suite 100 Huniersville, NC 28078 'vww.pacebbs,mm (704)875-9092 1 ANALYTICAL RESULTS Project: Bakers Stormwater Pace Project No.: 92350558 Sample: BSW03 Parameters Lab ID: 92350558001 Collected: 08/08/17 00:55 Results Units Report Limit DF Received: 08/08117 11:12 Matrix: Water Prepared Analyzed CAS No, Qual Field Data Analytical Method: Collected By DPJ 1 08/08/17 12:52 Field pH 6.9 Std. Units 0.10 1 08/08/17 12:52 Field Temperature 27.6 deg C 0.50 1 08/08/17 12:52 2540D Total Suspended Solids Analytical Method: SM 25400 Total Suspended Solids 5.2 mg/L 5.0 1 08/13/17 10:44 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/16/2017 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 16 leAnalytical www.pscelahs oom ANALYTICAL RESULTS Project: Bakers Stormwater Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Project No.: 92350558 Sample: ; BSW03 Lab ID: 92350558002 . Collected: 08/08/17 00:57 Received: 08/08/17 11:12 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5210B SOD, 5 day BOO, 5 day Analytical Method: SM 5210B 2.5 mglL 2.0 1 08/09/17 20:45 08/14/17 15:16 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/16/2017 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16 aceAnalytical www.pacelabs.corn ANALYTICAL RESULTS Project: Bakers Stormwater Pace Project No.: 92350558 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BSW03 Lad ID: 92350558003 Collected: 08/08/17 00:58 Received: 08/08/17 11:12 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 25.0 mg/L 25.0 1 08/14/17 14:05 Date: 08/16/2017 06:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 16 Pace Analytical Services, LLC e aceAnal. t6cal 9800 Kincey Ave. Suite 100 Huntersvllle, NC 28078 www.pacelabs oom (704)875-9492 ANALYTICAL RESULTS Project: Bakers Stormwater Pace Project No.: 92350558 Sample: BSW03 Lab ID: 92350558004 Collected: 08/08/17 01:00 Received: 08/08/17 11:12 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium NO ug/L 1.0 1 081141171410 08/15/1716A0 7440-43-9 Chromium NO ug/L 5.0 1 0811411714:10 0811511716:10 7440-47-3 Copper 23.5 ug/L 5.0 1 0811411714:10 0811511716:10 7440-50-8 Nickel ND ug/L 5.0 1 0811411714:10 0811511716:10 7440-02-0 Zinc 14.7 ug1L 10.0 1 08/14/1714:10 08/1511716:10 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/1612017 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16 acmnalytical wwwpecelabs com Project: Bakers Stormwater Pace Project No.: 92350558 QC Batch: 372824 QC Batch Method: EPA 200.7 Associated Lab Samples: 92350558004 METHOD BLANK: 2065686 Associated Lab Samples: 923,90558004 Parameter Units Cadmium Chromium Copper Nickel Zinc ug/L uglL uglL ug1L uglL QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 08/15/1714:26 ND 5.0 08115/1714:26 ND 5.0 08/15/1714:26 ND 5.0 08115/1714:26 ND 10.0 08115/1714:26 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2065687 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug1L 500 476 96 85-115 Chromium uglL 500 482 96 85-115 Copper ug1L 500 507 101 85-115 Nickel uglL 500 481 96 85-115 Zinc ug1L 500 499 100 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2065688 . MS 92350542001 Spike Parameter Units Result Conc. Cadmium uglL ND 500 Chromium ug1L ND 500 Capper uglL 0.017 500 mg1L Nickel uglL ND 500 Zinc uglL ND 500 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2065690 MS 92350498001 Spike Parameter Units Result Conc. Cadmium uglL ND 500 Chromium ug/L ND 500 Copper ug/L ND 500 Nickel ug/L ND 500 Zinc uglL ND 500 2065689 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 473 464 95 93 70-130 2 500 480 473 96 95 70-130 1 500 521 515 101 100 70-130 1 500 476 469 95 94 70-130 1 500 496 489 98 96 70-130 1 2065691 MSD Spike MS MSD MS MSD % Rec Conc, Result Result % Rec % Rec Limits RPD 500 460 453 92 91 70-130 2 500 469 462 94 92 70-130 2 500 513 505 102 101 70-130 2 500 467 461 93 92 70-130 1 500 491 485 97 96 70-130 1 Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/16/2017 06:44 PM without the written consent of Pace Analytical Services, LLC. Qua] Qual Page 8 of 16 le aceAnalytircal wwwpacefebs-cam QUALITY CONTROL DATA Project: Bakers Stormwater Pace Project No.: 92350558 QC Batch: 372880 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids, Associated Lab Samples:' 92350558001 METHOD BLANK: 2066136 Associated Lab Samples: 92350558001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 2066137 Parameter Units Total Suspended Solids m911- SAMPLE DUPLICATE: 2066138 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2066139 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 08113/1710:44 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 240 96 90-110 92350558001 Dup Result Result 5.2 ND 92350698002 Dup Result Result 30.6 27.2 RPD Qualifiers RPD Qualifiers 12 06 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/16/2017 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16 e IacleAnalytical (�wvw.pacefebs corn Project: Bakers Stormwater Pace Project No.: 92350558 QC Batch: 372626 OC Batch Method: SM 5210B Associated Lab Samples: 92350558002 METHOD BLANK: 2064396 Associated Lab Samples: 92350558002 Parameter BOD, 5 day QUALITY CONTROL DATA Analysis Method: SM 5210B Analysis Description: 5210B BOD, 5 day Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers mglL ND 2.0 0811411714:57 LABORATORY CONTROL SAMPLE: 2064397 Spike LCS Parameter Units Conc. Result BOD, 5 day mg/L 198 205 SAMPLE DUPLICATE: 2064398 92350649008 Dup Parameter Units Result Result BOD, 5 day mg/L 3.1 3.4 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS % Rec % Rec Limits Qualifiers 104 84.6-115.4 RPD Qualifiers 9 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/16/2017 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 16 aceAnalytical w»w.pacelabs.arn QUALITY CONTROL DATA Project: Bakers Stormwater Pace Project No.: 92350558 OC Batch: 373047 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92350558003 METHOD BLANK: 2067169 Associated Lab Samples: 92350558003 Parameter Units Chemical Oxygen Demand mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 0811411714:05 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2067170 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mglL 750 722 96 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067171 2067172 MS MSD 92350458005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 115 750 750 879 867 102 100 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067173 2067174 MS MSD 92350498001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mglL 32.0 750 750 789 797 101 102 90-110 1 Results presented an this page are In the unite Indicated by the "Unite" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/16/2017 06:44 PM without the written consent of Pace Analytical services, LLC. Page 11 of 16 lacieAnalyficale www.pecelebs,m n QUALIFIERS Project: Bakers Stormwater Pace Project No.: 92350558 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (7G4)875-9092 OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantilalion Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethytvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyse is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/16/2017 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16 aceAnalX cal www.pacefabs.ow QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Bakers Stormwater Pace Project No.: 92350558 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 26078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92350558001 BSW03 92350558004 BSW03 EPA 200.7 372824 EPA 200.7 373300 92350558001 BSW03 SM 2540D 372880 92350558002 BSW03 SM 5210B 372626 SM 5210B 372670 92350558003 BSW03 SM 5220D 373047 Date! 08/16/2017 06:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 16 Document Name: Document Revised: August 4, 2017 i .. MAnal i� lioal' Sample Condition Upon Recei t SCUR Page 1 of 2 Document No.: Issuing Authority: F•CAR-CS•033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville Raleigh[] Mechanicsville❑ Sample Condition Client Name;IRCLI Project ft WO 92350558 Courier: _❑Fed Ex ❑UPS ❑USPS ❑Client II III I II I �I III�� III ❑ Commercial ace []other: 92350598 CustodySea! Present? ❑Yes i�o Seals Intact? Yes `` ❑ Date/Initials Person Examining Contaa-�l 1 Packing Material: ❑bubble Wrap ❑bubble Bags ne ❑ Other Biological Tissue Frozen? Thermomen Gun ID: O � I Type t t ❑Blue ❑None LivesQ o ❑N/A ac Correctiotor: Confer Temp Corrected of {'C): •� Temp should be above freezing to 6'C ❑Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soil `ON/A, water sample) Did samples or' inate in MV rm? quarantine zone within the United States: CA, NY, or SC (check maps)? Oid samples originate from a foreign source (inteyCGl tionalty, inriudine Hawaii and Purrm Rito)7 11Yes %JfVo Comm ents/Discrepancy: Chain ofCustody Present? es ONO N/A 1. Samples Arrived within Hold Time? QZges No ❑N/A 2. Short Hold Time Analysis <72 hr.)? es MNo ❑NIA 3. Rush Turn Around Time Requested? Dyes N/A 4. Sufficient Volume? roYes ❑No ❑N/A S. Correct Containers Used? -Pace Containers Used? es _hs []No []No ❑N/A N/A 6. Containers Intact? K ❑No N/A 7. Dissolved ana sis: Samples Field Filtered? yes ❑No YA 8. Sample labels Match COC? -Includes Date/Time/ID/Analysis Matrix: s ❑No N/A 9. HeadspaceinVOA Vials (>5-6mm)? ❑Yes ❑No A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes qR ❑No NIA 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Lot 10 of split containers: Project Manager SCURF Review: Project Manager SRF Review: l Field Data Required? ❑Yes ❑No Date/Time: Date: Date: j `f Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, Incorrect preserva(ive, out of temp, Incorrect containers] Page 14 of 16 N w 0 0 a 3 0 0 0 v ei n Y m x b n m = p n 0- O C N Y 1"h n v m fD m .-r r t7 o CM Y n G 0 1 N n n � N 3 rip A c y a m � o t'p � N A 3 C n n n c w n 0 a N ~O W W - N . a w . .+ Itemtt zzzzzzzzzzzz BP4U-125 mL Plastic Unpreserved (N/A) (G-) SP3U-250 mL Plastic Unpreserved (N/A) BP2U-500 mL Plastic Unpreserved (N/A) SPiU-1 liter Plastic Unpreserved (N/A) BP45.125 mL Plastic H2SO4 (pH c 2) (CI-) 8P3N-250 mL plastic HNO3 jpH < 2) BP4Z-125 mL Plastic ZN Acetate & NaOH (>9) BP4C-125 mL Plastic NaOH (pH > 12) (CI-) WGFU-Wide-mouthedGlass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (0-) zzzz AGiH-1 liter Amber HCI (pH < 21 AG3U-250 ml.Amber Unpreserved (N/A) {CI-) AG1S-1 liter Amber H2SO4 (pH < 2) AG35-250 mt Amber H2SO4 (pH < 2) AG3A(DG3A).250 mL Amber NH4Cl (N/A)(CI-) D69H-4O mL VOA HCI (N/A) VG9T-40 mL VOA Na2S203 (N/A) VGSU-40 mL VOA Unp (N/A) DG9P-40 mL VOA H3PO4 (N/A) VOAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per kitj VPH/Gas kit (N/A) SPST-125 mL Sterile Plastic (N/A — lab) SPZT-250 mL Sterile Plastic (N/A — tab) BP3A-250 mL Plastic (NH2)2SO4 (9.3-9.7) Cubitainer VSGU-20 mL Scintillation vials (N/A) I—f I I GN * � N o ro <. O M 3 O1 CL S O ni y N CL M O S X N 3 N S 0 fD — n vi n rt rp 7 � C y 7 Cr t9 � 0 Cr t9 0 r9 ' N I� PaceAnalytical' r .oseelaas.cam CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company: Report To �. f.eft Attonlion: 2177356 AddresS7 / Copy To: may, C �Q. Company Nam '�✓ �l • / • r REGULATORY AGENCY Isf4Tu'DB t. 8��d Addres;* SD3O r NPDES r GROUND WATER I' DRINKING WATER r UST (— RCRA j— OTHER Email To: Purchase Order No.: Pa Owle Refer : P nn: Fax: Project Name: Px� Protect Site Location —&qe hAanagar. STATE: k Requested Due DatafTAT: Project Number, Requested Analysis Filtered (YIN} I Section D Matrix Codes a z Roppired Client Wwmatioo >,nn.TRIXf cooE s z COLLECTED Preservatives > Drinking Water OW Q zO Water WT Waste afar W W eTE U TE c N� l _ Product m START B Z SNYSofid St. o 0 p SAMPLE ID Oil OL - �_ UWipe WP (A-Z. 0.91:) Air AR tu w 4 w v V o Sample IDS MUST BE UNIQUE Tissue TS O U a 4: U Other OT Lu a O m T To a i o a N p ra fn t L = H 9�3�J45�0 ~ r rn DATE TIME DATE TIME 3 = x Z Z O y R Pace Project No./ Lab I.D. 1 Sj✓03 G g- 7am, X X I I C3 i 2 j✓03 is 3 sWo3 —17 a. tDC I I I I I ,✓ 1=03 4 y✓o3 wt er -s-» > >I X I DQ I I I I All 5 s 7 B 9 J12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILtAnON DATE TIME ACCEPTED BY! AFFILIATION DATE TIME SAMPLE CONDITIONS a 7. b% a -8 - .T: i a s•.6. �� -� 7 N s m SAMPLER NAME AND SIGNATURE e c ORIGINAL PRINT Names of SAMPLER:owd B�• o�AW ZA SIGNATURE of SAMPLER: fMhWOlYYi: r c7 N •hart Notes: By sgnmg itu fwm you are aomplwiq Pace's NET 30 an payment Icarus and vyccwg to late d wges o1 1.5 %per month to• any .rvoic Aot paid within 3a djys• F-ALL-0-020rev.07, 15-May-2007 1YO17 6o^7�4t C60l/"ci aceAnalytical wwnpecelebs,mn • e • August 04, 2017 Mr. Joe Hinkle Allvac RE: Project: NonContact Cooling Water Pace Project No.: 92349614 Pace Analytical $ervi4m, LLC 9800 Kircey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on August 01, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr, Tommy Long, Allvac David Pope, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 21 Pace Anatydcal Services, LLC a laceAnalyticaI 9800 neyAve. Suite I DO Huntersville, NC 2807878 wwwpecelahsmm (704)875-9092 • CERTIFICATIONS Project: NonContact Cooling Water Pace Project No.: 92349614 • Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E8764B Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 V rginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 21 Pace Analytical Services, LLC lac s eMalXical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 "°'"'PftV1ab3 com (704)875-9092 • SAMPLE ANALYTE COUNT Project: NonContact Cooling Water Pace Project No.: 92349614 Analytes, Lab ID Sample ID Method Analysts Reported Laboratory 92349614001 Non Contact Cooling #1 EPA 1664E JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A 92349614002 Non Contact Coaling #2 EPA 16648 JMS 1 PASI-C SM 4500-Cl G MDW 1 PASI-A 92349614003 Non Contact Cooling #3 EPA 1664E JMS 1 PAS1-C SM 4500-CI G MDW 1 PASI-A 92349614004 Non Contact Cooling #4 EPA 1664B JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A 92349614005 Non Contact Cooling #5 EPA 1664B JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A 92349614006 Non Contact Cooling #6 EPA 16648 JMS 1 PASI-C SM 4500-Ci G MDW 1 PASI-A 92349614007 Nan Contact Cooling #7 EPA 1664B JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A 92349614008 Non Contact Cooling #8 EPA 1664E JMS 1 PASI-C • SM 4500-CI G MDW 1 PASI-A • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 21 • 0 laneAnalj&cala www.pacelebs.00m ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project NonContact Cooling Water Pace Project No.: 92349614 Sample; Non Contact Cooling #1 Lab ID: 92349614001 Collected: 07/31/17 07:00 Received: 08101/97 11:21 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mglL 5.0 1 08/04/17 05:59 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.12 mg1L 0.024 1 08/02/17 17:49 7782-50-5 H3 Date: 08/04/2017 02:56 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 21 aceAnalylfical www.pwolabs.com • • • Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NonContact Cooling Water Pace Project No.: 92349614 Sample: Non Contact Cooling #2 Lab ID: 92349614002 Collected: 07/31/17 07:10 Received: 08/01/17 11:21 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease NO mglL 5.0 1 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.17 mg]L 0.024 1 Date: 08/04/2017 02:56 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Paco Analytical Services, LLC. 0810211717:49 7782-50-5 H3 Page 5 of 21 aceAnalyti+cala wwwpecelabs.com • • is Pace Analytical Services, LLC 9800 Kircey Ave. Suite 100 Hunterswre, NC 26078 (704)875-9092 ANALYTICAL RESULTS Project: NonContact Coaling Water Pace Project No.: 92349614 Sample: Non Contact Cooling #3 Lab ID: 92349614003 ' Collected: 07/31/17 07:25 Received: 08/01/17.11:21 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.15 mg1L 0.024 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full. Date: 08/04/2017 02:56 PM without the written consent of Pace Analytical Services, LLC. 08/04/17 06:00 08/02/1717:49 7782-50-5 H3 Page 6 of 21 Pace Analytical Services, LLC aceAnalytical 9800 Kinsey Ave. Suite 140 Huntersville, NC 2807B wwwpacelabs,cam (704)875-9092 • ANALYTICAL RESULTS Project: NonContact Cooling Water Pace Project No.: 92349614 Sample: Non Contact Cooling #4 Lab ID: 92349614004 Collected: 07/31/17 07:43 Received: 08/01/17 11:21 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 08/04/17 06:00 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.085 mg1L 0.024 1 08/02/17 17:49 7782-50-5 H3 • • Date: 08/04/2017 02:56 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of, Pace Analytical Services, LLC. Page 7 of 21 aceAnalytical www.paceobs.com • • Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NonContaci Cooling Water Pace Project No.: 92349614 Sample: Non Contact Cooling #5 Lab ID: 92349614005 Collected: 07/31/17 08:08 Received: 08101/17 11:21 Matrix: Water Parameters Results Units . Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mglL 5.0 1 08/04/17 06:00 4500CL G Chlorine, Residual Analytical Method: SM 4500-Cl G Chlorine, Total Residual 0.027 mg1L 0.024 1 08/02/17 17:49 7782-50-5 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/04/2017 02:56 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 21 laneAnalytical' www.pecelabs,corn • 0 • ANALYTICAL RESULTS Project: NonContact Cooling Water Pace Project No.: 92349614 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Non Contact Cooling #6 Lab ID: 92349614006 Collected: 07131/17 08:27 Received: 08/01/17 11;21 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 08/04/17 06:04 4500CL G Chlorine, Residual Analytical Method: SM 4500-Cl G Chlorine, Total Residual 0.031 mg1L 0.024 1 08/02/17 17:49 7782-50-5 H3 Date: 08/04/2017 02:56 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, w4houl the written consent of Pace Analytical Services, LLC. Page 9 of 21 • t Analytical mw.pecelaba.c= ANALYTICAL RESULTS Project: NonContact Cooling Water Pace Project No.: 92349614 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Non Contact Cooling #7 Lab ID: 92349614007 Collected: 07/31/17 08A5 Received: 08/01/17 11:21 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 16646 Oil and Grease ND mg1L 5.0 1 08/04/17 06:04 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.027 mg1L 0,024 1 08102/17 17:49 7782-50-5 H3 Date: 08/04/2017 02:56 PM REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 21 • s aceMalytical6 www.pacelabs oom ANALYTICAL RESULTS Project: NonContact Cooling Water Pace Project No.: 92349614 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Non Contact Cooling #8 Lab ID: 92349614008 Collected: 07/31/17 09:05 Received: 08/01/17 11;21 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua! HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mg1L 5.0 1 08/04/17 06:04 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.095 mg1L 0.024 1 08/02/17 17:49 7782-50-5 H3 Date: 0810412017 02:56 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 21 laceAnalytical"' wwwpacelabs com • QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: NonContact Cooling Water Pace Project No.: 92349614 QC Batch: 371874 Analysis Method: EPA 16W OC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92349614001, 92349614002, 92349614003, 92349614004, 92349614005, 92349614006, 92349614007, 92349614008 METHOD BLANK: 2060348 Matrix: Water Associated Lab Samples: 92349614001, 92349614002, 92349614003, 92349614004, 92349614005, 92349614006, 92349614007, 92349614008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 08/04/17 05:57 LABORATORY CONTROL SAMPLE: 2060349 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 38.8 97 78-114 MATRIX SPIKE SAMPLE: 2060350 92349575001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers • Oil and Grease mg/L ND 40 38.0 93 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. ® REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/04/2017 02:56 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 21 (�IaclMnalyfical' tvwwpacelabs.com • • Project: NonContact Cooling Water Pace Project No.: 92349614 QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 371637 Analysis Method: SM 4500-CI G QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual Associated Lab Samples: 92349614001, 92349614002, 92349614003, 92349614004, 92349614005, 92349614006, 92349614007, 92349614008 t METHOD BLANK: 2059096 Matrix: Water Associated Lab Samples: 92349614001, 92349614002, 92349614003, 92349614004, 92349614005, 92349614006, 92349614007, 92349614008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chlorine, Total Residual mg1L NO 0.024 08/02/17 17:49 SAMPLE DUPLICATE: 2059097 92348807001 Dup Parameter Units Result Result RPD Qualifiers Chlorine, Total Residual mg/L ND ND H1 Results presented on this page are In the units indicated by the "Units" column except where an alte hale unit is presented to the right of the result. • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/04/2017 02:56 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 21 le Analytrcal www.patefabs_=n • QUALIFIERS Project: NonContact Cooling Water Pace Project No.: 92349614 DEFINITIONS Pace Anatytical Services, LLC 9800 Kircey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyle is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-N itrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/04/2017 02:56 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 21 aceAnalytical ff w.pacelabs.com • QUALITY CONTROL DATA CROSS REFERENCE TABLE Paco Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: NDnContact Cooling Water Pace Project No.: 92349614 Analytical Lab ID Sample ID -QC Batch Method QC Batch Analytical Method Batch 92349614001 Non Contact Cooling #1 EPA 16648 371874 92349614002 Non Contact Cooling #2 EPA 1664B 371874 92349614003 Non Contact Cooling #3 EPA 1664B 371874 92349614004 Non Contact Cooling #4 EPA 1664B 371874 92349614005 Non Contact Cooling #5 EPA 1664B 371874 92349614006 Non Contact Cooling #6 EPA 1664B 371874 92349614007 Non Contact Cooling #7 EPA 1664B 371874 92349614008 Non Contact Cooling #8 EPA 1664E 371874 92349614001 Non Contact Cooling #1 SM 4500-CI G 371637 22349614002 Non Contact Cooling #2 SM 4600-CI G 371637 92349614003 Non Contact Cooling #3 SM 4500-CI G 371637 92349614004 Non Contact Cooling 04 SM 4500-CI G 371637 92349614005 Non Contact Cooling #5 SM 4500-CI G 371637 92349614006 Non Contact Cooling #6 SM 4500-CI G 371637 92349614007 Non Contact Cooling #7 SM 4500-CI G 371637 92349614008 Non Contact Cooling #8 SM 4500-CI G 371637 • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/04/2017 02:56 PM without the written consent of Pace Analytical Services, LtC. Page 15 of 21 �eAnaljlical' Laboratory receiving samples: Asheville ❑ Eden❑ ........•..un ,.wnc. UVL iJ1(1V11L nCV15t:u: aept. 41, Lult) Sam le Condition Upon Recelpt(SCURI Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev-01 Pace Quali 0 ice Greenwood ❑ Huntersvillen--l-*, Raleigh❑ Mechanicsville[] Samoi"to4iiion Upon Client Name: Project A WQ# : 92349614 _ f I 'Courier: ❑Fe d.0 ❑UPS ❑USPS ❑Client ❑ Commercial ace ❑Other: 92349614 1 Custody Seal Present? ❑Yes EJ<o Seals Intact? Des EfN o Date/Initials Person Examining Contents: C Packing Material: ❑Bubble Wrap Bubble Bags [—]None ❑Other: Thermometer: et []Blue []None Samples on ice, cooling process has begun ❑ IR Gun ID: TV Type f Ice: Correction Factor: Cooler Temp Corrected ('C): r Biological. Tissue Frozen? []Yes No Temp should be above free/Agwater to VC USDA Regulated Soil { sample) Did samples oropKe in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (lnterna lly, ❑Yes q including Hawaii and Puerto Rico)? ❑Yes o Chain of Custody Present? Fires ONO ❑NIA 1. Samples Arrived within Hold Time? ❑ es [—]No ❑N/A 2. Short Hold Time Analysis (c72 hr.? ❑yes 05No ❑NIA 3. Rush Turn Around Time Requested? Oyes o ❑N/A 4. Sufficient Volume?' Gifes [—)NO ❑N/A 5. Correct Containers Used? -Pace Containers Used? 12< es ON. ON- ❑N/A N/A 6, =ontalnerslntact7 2 es ❑No N A 7. Samples Field Filtered? ❑Ye No N/A S. Note if sediment is visible in the dissolved container'. . Sample Labels Match COC? / -Includes Date/Time/iD/Analysis Matrix: Yes ONO ❑N/A 9. Headspace in VOA Vials (>5-6mm)? ❑Yes [--]No N/ 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Des []NO [—]No N/A 11. CLIENT NOTIFICATION/RESOLUTION Field Data Required? ❑Yes ❑No Person Contacted: Commen,s/Sample Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date-:11'} Date: _ 8 L r Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) • Page 16 of 21 fik • A F' +•+ �+ �D Oo �1 ��V1 a to N r Items yi "VZZZ 44BP4U-125 mL Plastic Unpreserved (N/A) (Cl-) 05 n W 1 BP3U-250 mt Plastic Unpreserved (N/A) 0,< Q- 3 S t7 i BP2U-500 mL Plastic Unpreserved (N/A) Q G °. 3 ; o =1 BPSUliter Plastic Unpreserved (N/A) Cr 'a = S D m no x m BP35-250 mL Plastic H25(>4 (pH < 2) {CI-) u ' o BPSN-250 mi plastic HNO3 (pH < 2) O ro _ w Cr N A BP3Z-250 mL Plastic ZN Acetate & NaOH (>9) 0 aw 2 zzzz BP3C-250 mL Plastic NaOH (pH > 12) (Cl-) Q n ro ro WGFU-Wide-mouthed Glass jar Unpreserved 0. p Cr OQ 0 O n AGIU-1 liter Amber Unpreserved (N/A) (Cl-) zr Z//Izzzz z z AGIH-1 liter Amber HCI (pH < 2) G AG3U-250 mL Amber Unpreserved (N/A) (Cl-) 7 Cu O AG1S-1 liter Amber H2504 (pH < 2) ACM-250 mL Amber H2SO4 (pH < 2) AG3A(DG3A)-250 mL Amber NH4CI (N/A)(CI-) DG9H-40 mL VOA HCI (N/A) O VG9T-40 mL VOA Na25203 (N/A) h r► VG9U40 mL VOA Unp (N/A) ft .7.. D69040 ML VOA H3PO4 (N/A) r 3 M -• O VOAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) /p N 1 SPST-125 mL Sterile Plastic (N/A — lab) p SM-250 mt Sterile Plastic (N/A —lab) p In C A C2 a Cn zzz BP3A-ZSO ml. Plastic (NH2)2SO4 (9.3-9.7) m Cubitainer � VSGU-20 mL Scintillation vials (N/A) a GN -1 ,, weAnalylical Laboratory receiving samples: Asheville ❑ Eden[] s UULU111CM lVd(lic: uocumem Kevisea: bept• 41, zuio Sam le Condition Upon Recei tiSCUR) Page i of 2 Document No.: Issuing Authority: F-CAR-CS•033-Rev.01 Pace Quality Office Greenwood ❑ Huntersvilleg Raleigh[] Mechanicsville[] Samole!Con'd. ..® Client Name: : 92349614 • � I � Project q: WO# PM t MW9 Due Date. 08/ 10/ 17 'Courier: Fed Ex ❑ ❑LIPS I]Commercial ce ❑LISPS ❑other: Client CLIENT: 92-A l L vac NC . Custody Seat Present? ❑YesSeals Intact? ❑Yes Na Packing Material: ❑Bubble Wrap mellbble Bags []None ❑other: Date/Initials Person Examining Contents: Thermometer: ❑ IR Gun ID: `S 1 Typ of is : Pw�et ❑Blue ❑None Samples on ice, cooling process has begu Correction Factor: Cooler Temp Corrected VC): Biological Tissue Frozen? []Yes ❑No /A Temp should be above freezing to VC USDA Regulated Soft (121VA, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (intern naily, Yes o Including Hawaii and Puerto Rico)? ❑Yes LNo Comments/Discrepancy: Chain of Custody Present? dyes ONO ❑N/A 1, Samples Arrived within Hold Time? 0�1 ❑No ❑N/A 2. Short Hold Time Analysis (<72 hr.?_ ❑Yes 0No ❑N/A 3. Rush Turn Around Time Requested? oye Mll< ❑N/A 4. Sufficient Vol ume?• Yes ❑No ❑N/A 5. Correct Containers Used? E5Yes []No ❑N/A 6. -Pace Containers Used? ,Containers Intact? es les ❑No ❑No ❑N/A ❑H/A 7. Sam les Field Filtered? ❑Yes eNo []N/A 8. Note if sediment is visible in the dissolved container = . Sample Labels Match COC? ErY.% ON. ❑NIA 9. -Includes Date/Time/ID/Analysis Matrix: Iry Headspace In VOA Vials (>5-6mm)? [--)Yes ❑No N/A 10. Trip Blank Present? ❑Yes [:]No /A 11. Trip Blank Custody Seals Present? ❑Yes ❑No ❑ CLIENT NOTIFICATION/RESOLUTiON Field Data Required? [—]Yes ❑No Person Contacted: Date/Time: Comment>/Sample Discrepancy: Project Manager SCURF Review: Date: Project Manager SRF Review: Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 18 of 21 • rD 0 A ItemR BP4U-125 mL Plastic Unpreserved (N/A) (0-) BP3U-750ml. Plastic Unpreserved (N/A) — MU-500 mL Plastic Unpreserved (N/A) BP1U-1 liter Plastic Unpreserved (N/A) BP3S-250 mL Plastic H2504 (pH < 2) (CI-) BP3N-250 mL plastic HNO3 (pH < 2) BP3Z-250 mt. Plastic ZN Acetate & NaOH (>9) --ZV77zzz zV BP3C-250 mL Plastic NaOH (pH > 12) (CI-) WGFU-wide-mouthed Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (Cl.) Z_ . zzzzzvzzz AGIH-1 iker Amber HCI (pH < 2) AG3U-250 mL Amber Unpreserved (N/A) (Cl-) z/Z Z/,� Z Iz All AG1S-1 liter Amber HZS04 (pH < 2) AG35-250 mL Amber H2SO4 (pH < 2) AG3A(DG3A)-250 mL Amber NH4CI (N/A)(Cl-) OG9H-40 mL VOA HCI (N/A) VG9T-40 mt VOA Na25203 (N/A) VG9U-00 ml.VOA Unp (N/A) D690-40 mL VOA H3PO4 (N/A) VOAK (6 vials per kit)-5035 kit (N/A) V/GK (3 vials per kit} VPH/Gas kit (N/A) SP5T-125 mL Sterile Plastic (N/A — lab) SP2T-250 mL Sterile Plastic (N/A —lab) BP3A-250 mL Plastic (NH2)2SO4 (9.3-9.7) Cubitainer VSGU-20 mLScintiilatl, vials (NIA) GN 9 O M n u f� C� Storm Water Monitoring (NON CONTACT) Bakers North Chaln of Custody Record 4fATI Speciany MalenjI3 naen Nt Project Number/Name: Non Contact Cool in Water Project Location: Allvac Bakers Sampler's Signature: Date:7-21-17 C w c- �Ey yy c a rz a Q u 0 CL a, T � *' C v m a 1=�'3'' m � is a y 2 U! a . � � a W LL 9 c °1 . a r d H 0 Requested Test Parameters 99.)J496 14 - I- .AD G GID None Y 6.1 30.5 Residual Chlorine Cry 1 17.,104A." G G None Y . 3 a J,3 Residual Chlorine X- G G/V None Y 7.6 013. a Residual Chlorine G GAB None Y R, Q Residual Chlorine G G/O None Y 8,8 Residual Chlorine G GAB None Y . ,S a 9, 0 Residual Chlorine 5,.,. G G None Y 7.S a? .3 Residual Chlorine O,f.. G G None Y .g g.0 Residual Chlorine Meter Calibrated: J/ N IThermorneter Calibrated ®/ N Sampling and Field analysis completed by: Relinquished By: Received By: cs� Date: -/- Time: .'QQar Date: A+ i "74 me: Relinquished By: Received By: Date : * ` ` ` Time: Date: Time: EHS Baker South SW REV N 2 5 10/2016 =� l �2 ' o3 ooK CD-5 M(� von ,ao8 Page 21 of 21 • • • Storm Water Monitorin (NON CONTACT) Bakers North Chain of Custody Record frATI Specially Materials nave H2 Project Number/Name: NonContact Cooling Water Project location: Allvac Bakers Sampler's Signature: Date: -.3/-/ Ec LA iE CL Q .0 ci 0 ?, `m M c ( CIL a g Z u p V 0 3 M a as c 0 Requested Test Parameters �92) `6p lq L>ti -11- 7 G G HCL Y 30. f Oil & Grease .•/ji*- G G HCL Y a 1 .2 Oil & Grease G G HCL Y 023.0 Oil & Grease G G HCL Y A 7 Oil & Grease NM i T8--,08g= G G HCL Y Za. e Oil & Grease ot7.- G G HCL Y .D Oil & Grease if 7,,, G G HCL Y 071.3 Oil & Grease G G HCL Y Oil & Grease Meter Calibrated: / N IThermometer Calibrated: / N Sampling and Field analysis completed b/26w ME Relinquished By: Relinquished By: G�- Date 7 Time: d0o,. Date: Ob - 14 Time: Relinquished By: + vrc.t Relinquished By: Date : - -I 1,;flTime: Date : Time: EHS Baker South SW REV # 2 5/10/2016 col 002 a)3 ooq �5 oo� M-7 (-6� Page 20 of 21