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NCS000329_MONITORING INFO_20150825
STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. DOC TYPE ❑FINAL PERMIT --�MUNITURING REPORTS._._ ❑APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ Zoe S • � `6 •�-S YYYYMMDD k STORMWATER DISCHARGE OUTFALL (SDO) �. MONITORING REPORT Permit Number NCS O D O 3 7 SAMPLES COLLECTED DURING CALENDAR YEAR: ' (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACH,ITY NAME G PERSON COLLECTING SAMPL S) 711 CERTIFIED LABORATORY(S) Lab #�_ Lab # Part A: Specific Monitoring Requirements COUNTY 11f) ! Q II PHONE NO. (1 ) 9 - l/ SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. Date CollectedSample Total F. 7171r. i oil WRINA Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes _�t/no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH' New Motor Oil Usage mo/dd/ r MG inches m m unit al/mo Form SA U-247, last revised 21212012 Page 1 of 2 L STORM EVENT CHARACTERISTICS: Mail Original and one copy to: Division of Water Quality Date 7J3 -15 Attn: Central Files Total Event Precipitation (inches): , 1617 Mail Service Center Event Duration (hours): j ! - (only if applicable — see permit.) Raleigh, North Carolina 27699-1617 (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possjbitity of fines and imprisonment for knowing violations." (Signature of -Y-ZS - IS (Date) Form SWU-247, last revised 21212012 Page 2 of 2 August 25, 2015 Attn: Central Files RECM ED N.C. Division of Water Quality AUG 2 8 2015 1617 Mail Service Center Raleigh, NC 27699-1617 CENTRAL FILES DWR SECTION Central Files: OATI I1•0. Box 5030 2020 AsheraA Avenue Monroe, NC 28111-5030 Phone: (704) 289451 1 Fax: (704)290-5194 Email: ioe.hinklepalimetals.com Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and one copy are included. The monitoring data is for the following monitoring schedule: Monitoring Period Sample Number Start I End Year 6 •- Period 1 1 l March 1, 2015 1 August 31, 2015 Analytical monitoring includes: • Outfall #01 (B), commingled stormwater • Outfall #02 (B), non -commingled stormwater • Outfall #03 (B), non -commingled stormwater • Non Contact Cooling Water #1 - #8 If you have any questions or need additional information, please contact me at 704-289-4511, Thank you. Sincerely, qC't & Jo Hinkle Environmental Manager ,+ ATI ATI - Bakers Plant Stormwater Monitoring Report Form Sample Date: __ / a 3 "IS Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods Results of Sample Analvsis: Sample Time: ZO -5 P Stormwater Discharge Outfall #01 (Commingled) Drainage Area = 2 915 470s . ft. = 69 acres % Impervious = 34% AQ V 1' it- 40 CFR Part 136 Parameter Results (mg/l) Benchmark Values (mg/1) BOD 0 30 COD 120 TSS 100 Cadmium 0.001 Chromium, total recoverable AD 1 Copper, total recoverable 0,5 0.007 Nickel, total recoverable D 0.26 Zinc, total recoverable 8 0.067 Oil and Grease 20 Temp (effluent) (deg C) n/a Temp (downstream) n 3 (deg C) n/a Temp (upstream) (deg C) n/a Total Residual Chlorine 1 0.017 pH (std units) 6-9 (std units) Storm Date: 7,1 3 45 Storm Duration: (Hrs.) Inches of Rainfall: Duration of time preceding rain event exceeding 0.1":` (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Itnpervious Area) Q(tot., cfs) _ (A x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches rain/12inches/ft. x 69 x .34) C1(Total, cfs) = 1.5180 x 6, Rn (Inches of rain) + 1.7595 x (Inches of rain) cfs FNC - SW - MnnitriHna Rennrl Fnnm - Rew I ATI Allvac - Bakers Plant Stormwater Monitoring Report Form Sample Date: 7 j ) -i Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Sample Time: _ /; /o) pm Stormwater Discharge Outfall #02 (Non -Commie Ig gd) Drainage Area = 212,952sQ. ft. = 4.9 acres % Impervious = 12% 40 CFR Part 136 Parameter Results (mg/1) Benchmark Values (mg/1) BOD M 30 COD 120 TSS 100 Cadmium a 0.001 Chromium, total recoverable O 1 Copper, total recoverable D 0 0.007 Nickel, total recoverable 0.26 Zinc, total recoverable 0.067 pH (std units) 6-9 (std units) Storm Date: %3 l.5 Storm Duration: (Hrs.) Inches of Rainfall: Duration of time preceding rain event exceeding 0.1": (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) = (.4 x inches rain/] 2 inches/ft. x 4.9 acres x .88) + .9 x inches rain/] 2inches/ft. x 4.9 x .12) Q(Total, cfs) = 0.1437 x (Inches of rain) + 0.0441 x a Q (Inches of rain) IV .t A cfs Allvac - Bakers Plant F.I4C — CW _ Mlnnifnrina Rnmrr Fnrm — Rry I OATI r' 2 Stormwater Monitoring Report Form Sample Date: / -�J IS Sample Time: 7. 3 1 Q I✓L Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analvsis: Stormwater Discharge Outfall #03 (Non -Commingled) Drainage Area = 336,580sq. ft. = 7.8 acres % Impervious = 15% �GtV1 Pooe Jr P ld r' c cil - 40 CFR Part 136 Parameter Results (mg/1) Benchmark Values (mg/1) BOD 0 30 COD 0 120 TSS 14 100 Cadmium NP 0.001 Chromium, total recoverable A 1 Copper, total recoverable c U /l 0.007 Nickel, total recoverable 0.26 Zinc, total recoverableL2 LIE 0.067 pH (std units) a 6-9 (std units) Storm Date: Storm Duration: (Hrs.) Inches of Rainfall: Duration of time preceding rain event exceeding 0.111: /[� / (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) _ (A x inches rain/l2 inches/ft. x 7.8 acres x .85) + .9 x inches rain/12inches/ft. x 7.8 x .15) Q(Total, cfs) = 0.2210 x (Inches of rain) + 0.0878 x (Inches of rain) r 7 r 7 cfs FNC -.. SW — Mnnilminv Rerxxt Fnr — Rev 1 ATI Sample Location: Person Collecting Samples Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Allvac - Bakers Plant Stormwater Monitorinp, Report Form Non -Contact Cooling Wastewater 40 CFR Part 136 7 IG Non -Cant Cool Water # Sampling Date Sampling Time Estimated Flow (MGD) Sample Location =Effluent Total Res Chlorine m Temperature (deg C) (std.. u units) 1 -3 9: 56a-m ?. 9 2 -3- ,` /-/o . 3 3 4 5 -31 V %MdxIQ,O61LN40 r ' ?--5-15 LObam d.DON46 �3 , g - -15 1.4643 8♦ • There are no discharges of air compressor condensate. • Benchmark value for Total Res Chlorine = 0.017 mg/L. Ip VHS — SW — Mnnitraina Remrt Fnr — Rev F Ari'Ar NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http:l/portal,ncdenr.orp-/web/wQ/ws/sulnpdessw#tab:4 Permit No.: N&Al /j�Q/Q/0/,j/`-2/Q/ or Certificate of Coverage No.: Facility Name: County: Inspector: Date of Inspection:.5 /b'-, Time of Inspection: Phone No. Total Event Precipitation (inches): Q. IS Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) JzYes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatuV, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permitteeq Designee Pagel of 2 $WU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. Receiving Stream: Describe the industrial acti i etc.) UUUdl1 UI-d111d6V dl Ud. 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors:.- 'Xro,iit 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 170 4 e- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2O 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 6) 4 5 7. Is there any foam in the stormwater discharge? Yes No B. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Ahem e__ Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 ALIT MO� NCDENR Stormwater Discharge Outfail (SDO) Qualitative Monitoring Report Forguidance on filling out thisform, please visit: http:J/portal.ncdenr.org/webJwq JwsJsuJnp -dessw#tab-4 Permit No.: ly/�/,//Q/Q//.// or Certificate of Coverage No.: Facility Name: 127 1. / L County: ZZAtOri Phone No. Inspector:rri Date of inspection: Time of Inspection: IdA Total Event Precipitation (inches): 0-1 is Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) /Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of PerViftee or Page 1 of 2 SWU-242, last modified 10/25/2012 � 1< 1. OutfaU Description: Outfall No. Structure (pi e, Deceiving Stream: Ij T k I Describe the indu trial acti ities that occur 11-d 11' �. 2. Color: Describe the color of the c (light, medium, dark) as descriptors: etc.) —7V4 e- in th�j outfall drainage area: _57"o%r, c_ using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 01 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? Yes Vo B. Is there an oil sheen in the stormwater discharge? Yes /ko 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describeuwC Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. SWU-242, Last modified 10/25/2012 Page 2 of 2 A F-9AA 'ro'Ar NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit. http://portal,ncdenr.orp-lweb/wq/ws/su/npdessw#tab74 Permit No.: N/Q'S/!J/0/Q/,3/49/y/ or Certificate of Coverage No.: NXI-GI_/—/_/_/_/_/ Facility Name: /all✓d[, County: Phone No. 7DS10?yf-Y-s// Inspector: GC' " Date of Inspection: 4 /ff /S Time of Inspection: Total Event Precipitation (inches): 0,7,511 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) /VYes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signa,yure, I certify thpt this report is accurate and complete to the best of my knowledge: (Signature of Permiti{be or D Page 1 of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. ASIJO. St Receiving Stream: Describe the industrial a ivities cturee (pipe, ditch, etc.) ,0141' : occur within the outfall drainage area: 2:za/1' 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 121)4ef 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and S is very cloudy: 1 M 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1O 2 3 4 5 G. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2� 3 4 5 7. Is there any foam in the stormwater discharge? Yes No B. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 �acemalXical e ' www.p&cW&bs.com Pace Analytical Services, Inc. 9800KinceyAve. Suite100 Huntersville, NC 28078 (704)875-9092 July 31, 2015 Mr.'Joe Hinkle Allvac RE: Project: BAKERS STORMWATER Pace Project No.: 92260320 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, AlFn,--D Matthew Brainard matthew.brainard@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 20 aceAnalytical www.paoerab&=n Pace Analytical Services, Inc. 9800 Klncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: BAKERS STORMWATER Pace Project No.: 92260320 Charlotte Certification IDs 9800 Kincey Ave. Ste 100. Huntersville, NC 28078 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification M 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification M 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FtoridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification M 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In toll, without the written consent of Pace Analytical Services, Inc.. Page 2 of 20 aceAnalXical e www.pacelabsc0m Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvllle, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: BAKERS STORMWATER Pace Project No.: 92260320 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92260320001 SW01 SM 5220D MJP 1 PASI-A 92260320002 SW01 SM 5210B BRJ 1 PASI-A 92260320003 SW01 SM 2540D SAM 1 PASI-A 92260320004 SW01 EPA200.7 JDA 5 PASI-A 92260320005 SW01 SM 4500-Cl G MLS 1 PASI-A 92260320006 SW01 EPA 1664B JMS 1 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Without the written consent of Pace Analytical Services, Inc.. Page 3 of 20 aceAnalytical . wwwpacelah corn Pace Analytical Services, Inc. 9800 Klncey Ave. Suite 100 Nuntersvllle, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92260320 Sample: SW01 Lab ID: 92260320001 Collected: 07/23/15 18:50 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 50.0 mg1L 25.0 1 07/27/15 15:45 Date: 07/31/2015 02:22 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 20 aceAnalytical rwrw.pacWab&com Pace Analytical Services, Inc. 9800 KlnceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92260320 Sample: SW01 Lab ID: 92260320002 Collected: 07/23/15 18:51 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 52108 BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 26.4 mg1L 2.0 1 07/25/15 04:41 07/29/16 23:39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31 /2015 02:22 PM without the written consent of Pace Analytical Services, Inc., Page 5 of 20 6 aceAnalytical www.pacafaEs.com Pace Analytical Services, Inc. 9800KinceyAve. Suite100 Hunlersvllle, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92260320 Sample: SW01 Lab ID: 92260320003 Collected: 07/23/15 18:52 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit DI= Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 14.7 mg1L 8.3 1 07/29/15 11:30 Date: 07/31/2015 02:22 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 20 aceAnal ical" www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersvllle, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92260320 Sample: SW01 Lab ID: 92260320004 Collected: 07/23/15 18:53 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug/L 1.0 1 07/27/15 19:00 07/28/15 20:20 7440-43-9 Chromium ND ug/L 5.0 1 07/2711519:00 07/28/15 20:20 7440-47-3 Copper 33.6 ug/L 5.0 1 07127M5 19:00 07/28/15 20:20 7440-50-8 Nickel 6.6 ug/L 5.0 1 07/27115 19:00 07/28/15 20:20 7440-02-0 Zinc 19.8 ug/L 10.0 1 07/27/15 19:00 07/28/15 20:20 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 20 ace Analytical 1 wxwpacefahs.com Pace Analytical Services, Inc. 9800 Klncey Ave. Suite 100 Huntersvllle, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92260320 Sample: SW01 Lab ID: 92260320005 Collected: 07/23/15 18:54 Received: 07124M5 12:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.11 mg1L 0.024 1 07/27/15 12:55 7782-50-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in felt, Date: 07131 /2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 20 aceAnalyticale wxwPw81abscam Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92260320 Sample: SW01 Lab ID: 92260320006 Collected: 07/23/15 18:56 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Oil and Grease Date: 07/31/2015 02:22 PM Analytical Method: EPA 1664B ND mg1L 5.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 07/30/15 10:22 Page 9 of 20 a ce Analytical www.pecefahscom QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260320 QC Batch: GCSV/22117 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92260320006 METHOD BLANK: 1521896 Associated Lab Samples: 92260320D06 Parameter Units Oil and Grease mg1L LABORATORY CONTROL SAMPLE: 1521897 Parameter Units Oil and Grease mg/L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 07130M 5 10:14 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 40 35.6 89 78-114 MATRIX SPIKE SAMPLE: 1521898 92259903005 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 37A 94 78-114 Results presented on this page are In the units tndleated by the "Units" column except when an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 20 acemalX cal www.paaalaba.com Pace Analytical Services, Inc. 9800 Kinoey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260320 QC Batch: MPRPl19100 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92260320004 METHOD BLANK: 1518994 Matrix: Water Associated Lab Samples: 92260320004 Blank Reporting Parameter Units Result Limit Analyzed Cadmium ug1L NO 1.0 0712811519:37 Chromium uglL NO 5.0 07/2811519:37 Copper ug1L ND 5.0 07/28/1519:37 Nickel ug/L NO 5.0 07/28/1619:37 Zinc ug/L NO 10.0 07/2811519:37 LABORATORY CONTROL SAMPLE: 1518995 Parameter Units Cadmium uglL Chromium uglL Copper uglL Nickel uglL Zinc ug1L Qualifiers Spike Cone. LCS Result LCS % Rec % Rec Limits 500 451 90 85-115 500 467 93 85-115 500 464 93 85-115 500 448 90 85-115 500 441 88 85-115 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1518996 1518997 MS MSD 92260382008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug1L ND 500 500 448 449 90 90 70-130 0 Chromium ug/L ND 500 500 466 466 93 93 70-130 0 Copper ug/L ND 500 500 462 461 92 92 70-130 0 Nickel uglL ND 500 500 444 444 89 89 70-130 0 Zinc uglL 2.9J 500 500 435 436 86 87 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1518998 1518999 MS MSD 92260178001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug1L 2.3 500 500 457 453 91 90 70-130 1 Chromium uglL 13.0 600 500 475 473 92 92 70-130 1 Copper uglL 824 500 500 1340 1440 102 122 70-130 7 Nickel uglL 14.8 500 500 453 450 88 87 70-130 1 Zinc ug1L 608 500 500 1040 1060 86 89 70-130 2 Results presented on this page are In the units Indicated by the "Units" column except where an altemate unit Is presented to the right of the mutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc - Page 11 of 20 aceAnalyircal wwwpacelabacam Pace Analytical Services, Inc, 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260320 OC Batch: WET139159 Analysis Method: SM 2540D OC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92260320003 METHOD BLANK: 1520840 Matrix: Water Associated Lab Samples: 92260320003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 07129M5 11:24 LABORATORY CONTROL SAMPLE: 1520841 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 248 99 90-110 SAMPLE DUPLICATE: 1520842 92260085003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 177 200 12 D6 SAMPLE DUPLICATE: 1520916 92260247001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 6.4 6.4 0 Reautts presented on this page are in the units Indicated by the "units' column except where an alternate unit is presented to the right of the resun. REPORT OF LABORATORY ANALYSIS This report shag not be reproduced, except in full, Date: 07/3112015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 20 aceAnalytrcal www.pecelabs.com QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260320 QC Batch: WET139116 Analysis Method: SM 4500-CI G QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual Associated Lab Samples: 92260320005 METHOD BLANK: 1519021 Associated Lab Samples: 92260320005 Parameter Units Chlorine, Total Residual mgfL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.024 0712711512:55 SAMPLE DUPLICATE: 1519022 92260064001 Dup Parameter Units Result Result Chlorine, Total Residual rng1L 0.034 0.040 RPD Qualifiers 16 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on thks page are In the units Indicated by the "Units" column except where an attemate unit is presented to the rtght of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 20 aceAnal ical twww.pacela5acom Pace AnaWlcal Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260320 QC Batch: WET139092 Analysis Method: SM 5210B QC Batch Method: SM 52108 Analysis Description: 5210B BOD, 5 day Associated Lab Samples: 92260320002 METHOD BLANK: 1518626 Matrix: Water Associated Lab Samples: 92260320002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg1L ND 2.0 07/29/15 23:39 LABORATORY CONTROL SAMPLE: Parameter 1518627 Units Spike LCS LCS Conc, Result % Rec % Rec Limits Qualifiers BOD, 5 day mg/L 198 175 88 84.6-i15.4 SAMPLE DUPLICATE: 1518628 92260323002 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 20.4 19.9 2 Results presented on this page are In the units indicated by the 'Units" column except when an alternate unit is pratenttd to the right of the rasutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 20 aceAnalytical www.pacefahacam Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92260320 QC Batch: WETA123876 QC Batch Method: SM 5220D Associated Lab Samples: 92260320D01 METHOD BLANK: 1519000 Associated Lab Samples: 92260320001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 1519001 Parameter Units Chemical Oxygen Demand mg1L QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 0712711515:45 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 746 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1519002 1519003 MS MSD 92260042002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 250 1500 1500 578 578 22 22 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1519004 1519005 MS MSD 92260382006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua$ Chemical Oxygen Demand mg/L ND 750 750 76.0 76.0 9 9 90-110 0 M1 Results presented on this page are In the units Indicated by the "Units" catumn except when an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/3112015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 20 acemaly ml www.pacerabs.com Pace Analytical Services, Inc. 9800 KlnceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: BAKERS STORMWATER Pace Project No.: 92260320 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anatyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethyhrinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each anatyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited anatytes. TN - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07131I2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 20 aceftlytical. * w.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvllle, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BAKERS STORMWATER Pace Project No.: 92260320 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92260320006 SW01 EPA 1664E GCSV122117 92260320004 SW01 EPA 200.7 MPRP119100 EPA 200,7 ICP117179 92260320003 SW01 SM 2540D WET139159 92260320005 SW01 SM 4500-CI G WET139116 92260320002 SW01 SM 5210B WET139092 SM 5210B WET139095 92260320001 SW01 SM 5220D WETA123876 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc., Page 17 of 20 1�Cf?Ark'{PyrrlC�l • Condition Upon Receh Document Number: F-CHR-CS-003-rev.16 Page 1 of 2` Issuing Authority: Pace Huntersville Quality Office Client Name: Arc t Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial❑ ace Other• Custody Seal on CooleilBox Present: yes ❑ no Seals inlact: Byes Page 2 of 2 is for Internal Use Only ❑ no i•+-Si+,�,•�f va.c3 t--z. �.•:.P.If.e[Ya...�-•^^ Packing Material: ❑ Bubble V❑ip ❑ Bubble Bags wrNone Other Thermometer Used: IR Gun T1401 Type of Ice: Blue None Samples on ice, cooling process has begun Temp Correction Factor T1401 No Correction Lf l Corrected Cooler Temp.: r 17 •C Tamp should be above freezing to 6*C Biological Tissue Is Frozen: Yes No Comments: Date and Initlal of ers n e rpining contents: � �) dhbib , 'oi Custody Present:' retfes ON, ❑NIA 1. Chain of Custody Filled Out: ples ❑No ❑NIA 2. Chain of Custody Relinquished: Yes ON, ❑NIA 3. Sampler Name & Signature on COG. jpryes ONO ❑NIA 4. Samples Arrived within Hold Time: As ❑No ❑NIA 5. , Short Hold Time Analysis <72hr : P<ls ❑No ❑NIA 6, Rush Turn Around Time Requested: Dyes ENNo ❑NIA 7, Sufficient Volume: es ONO ❑NIA 8. . Correct Containers Used: - -Pace Containers Used: s ❑No es ©No ❑NIA ❑NIA 9. Containers Intact: es ONO ❑NIA 10. Filtered volume received for Dissolved tests PYes ❑No ❑NIA 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: �es ONO ❑NIA 12. Alf containers needing preservation have been checked. All containers needing preservation are found to be in comoliance with EPA recommendation. Y-as ONO /r�fve9 ❑No C ❑NIA ❑NIA 13. exceptions: VOA, coliform, TOC, O&G, WI-DRO (water) ❑Yes No Samples checked for dechlorination: ❑Yes ONO A!rNIA 14. Headspace In VOA Vials >6mm : [--]Yes ONO 641A 15. Trip Blank Present: ❑Yes ONO 1121IN1,11A 16. Trip Blank Custody Seals Present ❑Yes ❑No NIA Client Notification/ Resolution: Field Data Required? Y 1 N Person Contacted: Dalerrime: Comments! Resolution: SCURF Review: Date: -VW® : 9226�3, SRF Review: Date: f pp+ Note: Whenever there is a discrepancy affecting North Carolina compliance �� samples, a copy of this form will be sent to the North Carolina DEHNR Certlfication•Office ( I•e out of hold, incorrect preservative, out of temp, 92200320 Incorrect containers) — -- — H Page 18 of 20 Z*.F2aceAnalv6cal* CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. A11 relevant fields must be completed accurately. 0 N 0 rn • wrrrr.pacelaas.ceta — Page: of Section A Section B Section C 1egvired Client Information: - Requirod Project Information: tn% ice tnformation: ReportTo,- Attention: -77 887 866 As n llG n 3'0 4d Copy To: H P7Wa -1 /�. REGULATORY AGENCY ` G ���` `' NPDES I GROUNDWATER DRINKING WATER . F, UST j I RCRA i OTHER _mail To: Purchase Order No.: pace 4wm ��- Fa>C Project Name: C� peCe Pmfocl Site Location . _ srare: A ?equested Dtm OateITAT: Project Number. - Paw ProrAo M. - Requested Analysis Filtered (YIN) Section D Matrix Codes Y z. rteardred CIW4 Mrormaeoe MATRIX r CODE — COLLECTED Preservatives Drinking water DW 2 OU zz J water wT Waste Water Ww � m C STYE CFor L) I Product P > 3 Z SoilfSolid SL 1 aq 0 p y } °L SAMPLE !D wipe c? w Z ,� (A-Z. 0-9I.-). Air .. AR O to a Z 0 Sample IDS MUST BE UNIQUE Tissue TS O a w - z iCD Other OT x, 1 O t H + O c ayi „t d 7 - a a m p n 2 OR t° to a 4 C U m CD d — DATE. TIME DATE TIME y 5 � S S z z i O ,y Pace Project NOJ Lab I.D. Y, 4 ivo.i rSir 1ix s G • ��s ;s �. X b 63 ofr G 8 ' S' 10 1t rIME. 12 —4— --± — — ADDITIONAL COMMENTS LINQUISHED BY I AFFILIATION DATE ACCEPTED BY I AFFItJA ON DATE TIME i SAMPLE CONDITIONS oo ,>` :' r t� t G.. %: ORIGINAL SAMPLER NAME AND SIGNATURE I (> � c PRINT Name of SAMPLER: z E m DATE Signed SIGNATURE of SAMPLER: (MMIDDrM. rn w •Important Note: By s9ung this form you am axepdng Pam's NET 30 day payment ten. and agrocirM tD tala Crarees of 1.5% Def month for am invoices not said whin 34 days. 1 F-Al.I.-O-S)7tlrav rt7 I S-May.2r 117 ®D -.. CHAIN -OF -CUSTODY 1 Analytical Request Document N o The Chai" Custody is a LEGAL DOCUMENT. A I relevant fields muss be completed accurately. N // aceAnal•ytical' rrww.pacalaas.com s; ; :. _. _. = ; .. vi t ,.- • Section A i • . _.. ✓ c _ Seetion.6- f _ , . . .r. ". Section G_ , Y ._ . F.. '' .' ' Page of, ' - EL Rogtiired Ctierit lnfamatiori: Required Project Information: .. Invoice Information: -..: Report To:r . «. :.. .. ` . - - Attention: `SQy���lz'-�.. o a�drr M'7G X1X,',;1,)a- copy To, REGULATORY AGENCY / / ldc �.it�ClG % JDCC�I�Ii(//�IlcTCI��r/1 ` J _ jr : J �.L i .r'_' T,_i::. t1: �tltl.!%�v)[. 7D3QJ%/fGi!%dC �f� NPDES. ,F, GROUNDWATER } Email -To: Purcrt Order No.: pace Ovote i UST ( _RCRA yDRINKiNGWATER t : - .OFHER ReraKence: Fa:c. Project Name: �� .1C� Paw PfO Site Location I �� Requested Due DateITAT: y ti.:- . .i.. ProjeCt Number-; V �. _ _ .._ .+� t'_ � ..•.� _ _ - - .Paco ProLls C. _ f !ri -ti - -•� �• . • . � � � 37A 7E: " Y�' " - - • - '� � - . Requested Analysis Filtered((YIN)- - Section D _ Matrix Codes Rar{.tcdC7ienta<armutior - - 1 MATRrx-f'cooe� g ' COLLECTED -'• Preservatives z -- - Don dN wafer Dw- water WT Waste Water Procluct WW P. 'V U 9 V z Soillsofi0 . SL SAMPLE ID Oil Wipe oL WP C .Z m c L m (AZ!>9f:ft -Aires_,-_ Sample IDs MUST 6E UNIQUE ' Tasue ' AR: .. TS - a.rta. O a. S '; t: - :. , a ' IQ-., ry _ H ... ., Q ` c U '% r� ja ,� �- z v J V: j.•_ �'... 4. .I J 'OT sX• �. W. lw,.� _ .�..$ , ' - J ice' Z. O is v O C ..� a ? -r , ; , �! �� t, 1 l'� ✓ Q ,m+ • ': DATE TIME.- .DATE' ,-TIME i- rn x__ = Z Z O V sect NoJ Lab I.D. Pace'Pro' n 1 raj 3 WO 1 T C :2s /.r %' a. X �n '34 _S, l %v � �/ ' ...:.:°:�I.i ,....:s?i.",.:i' �' `�, :cam ��Jrys. ! ' f ''• S"` .s _ .� _ t � - - '''fiL ,6 .�/.) 1 1 4:.C�'/s -15 li��i:..G.0 1 10 4— + p I ADDITIONAL COMMENTS . RELINQUISHED BY! AFFILtATiON A. DATE TIME A ACCEPTED BY I AFFIIJA�ON DATE TIME SAMPLE CONDITIONS >frx-lc :cn,9'�li.L:GG.G:S,Bv� .,:,.ni�i(r� ��� 7�7y/� �_T..r..%% r ,, r✓, f.!,%.'r l rb% �f. v .4%i ' %,t c It SAMPLER NAME AND SIGNATURE�� r _ PRINT Name of SAMPLER:— �e n o a _ H z c z SIGNATURE of SAMPLER"��"G/ � DATE Signed (MMIDDlYY) / ~ U m E. vi 'hroon= Nete: av Stenine eua ram, ___ ---- aceAnalyticaI www.poesfabs.com July 30, 2015 Mr. Joe Hinkle Allvac RE: Project: BAKERS STORMWATER Pace Project No.: 92260323 Dear Mr. Hinkle: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 2807E (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, -� Matthew Brainard matthew.brainard@pacelabs.com Project Manager Enclosures 0c: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 16 (�55ne Analytical www.Paoefabs.wrn Project: BAKERS STORMWATER Pace Project No.: 92260323 Asheville Certification Ids 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification M M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 YirginialVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve, Suite 100 Huntersville, NC 2807E t704j875-9092 Page 2 of 116 (�5a'ne Analytical` WW..peaslabs.com SAMPLE ANALYTE COUNT Project: BAKERS STORMWATER Pace Project No.: 92260323 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analyses Reported Laboratory 92260323001 SW02 SM 5220D MJP 1 PASI-A 92260323002 SW02 SM 5210B BRJ 1 PASI-A 92260323003 SW02 SM 2540D SAM 1 PASI-A 92260323004 SW02 EPA200.7 JDA 5 PASI-A l REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fu 1, without the written consent of Pace Analytical Services, Inc.. Page 3 of 16 acmnalyfical www.pacoftcorn ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92260323 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SW02 Lab ID: 92260323001 Collected: 07/23/15 19:12 Received: 07124/15 12:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 57.0 mg1L 25.0 1 07/27/15 15A5 Date: 07/30/2015 02:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 16 Iac eAna1jftalc www.pacOftcom ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92260323 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite100 Huntersvllle, NC 28078 (704)875-9092 Sample: SW02 Lab ID: 92260323002 Collected: 07/23/15 19:13 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 52108 BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 20.4 mg1L 2.0 1 07125/15 04:41 07/29/15 23:39 a Date: 071301205 02:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 16 aceAnalyilcal. w+ww.pacembs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92260323 Sample: SW02 Lab ID: 92260323003 Collected: 07/23/15 19:14 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Total Suspended Solids 4 Date: 07/30/2015 02:30 PM Analytical Method: SM 2540D 82.0 mg/L 10.0 1 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 07/29/15 11:30 Page 6 of 16 (�5a'cmnalyfical* www.pecdeftow ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huniersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92260323 Sample: SW02 Lab ID: 92260323004 Collected: 07/23/15 19:16 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug1L 1.0 1 07/27/15 19:00 07/28/15 20:23 7440-43-9 Chromium 16.2 ug1L 5.0 1 07/27/15 19:00 07/28/15 20:23 744047-3 Copper 496 ug1L 5.0 1 07/27/15 19:00 07/28115 20:23 7440-50-8 Nickel 10 ug1L 5.0 1 07/27/15 19:00 07/28/15 20:23 7440-02-0 Zinc 74.7 ug1L 10.0 1 07/27/15 19:00 07/28/15 20:23 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 16 leAnalytical www.pacelabicom QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260323 QC Batch: MPRP119100 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92260323004 METHOD BLANK: 1518994 Associated Lab Samples: 92260323004 Parameter Units Cadmium uglL Chromium ug1L Capper ug1L Nickel ug1L Zinc ug1L LABORATORY CONTROL SAMPLE: 1518995 Parameter Units Cadmium ug/L Chromium ug1L Copper ug1L Nickel uglL Zinc uglL Matrix: Water Blank Result Spike Cone. 500 500 500 500 500 ND ND ND ND ND Reporting Limit Analyzed 1.0 07/28115 19:37 5.0 07/28115 19:37 5.0 07/28/1519:37 5.0 07128/1519:37 10.0 07/2811519:37 LCS LCS Result % Rec 451 90 467 93 464 93 448 90 441 88 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 (704)875-9092 Qualifiers % Rec Limits Qualifiers 85-115 85-115 85-115 85-115 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1518996 1518997 MS MSD 92260382008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Cadmium uglL ND 500 500 448 449 90 90 70-130 0 Chromium uglL ND 500 500 466 465 93 93 70-130 0 Copper uglL ND 500 500 462 461 92 92 70-130 0 Nickel uglL ND 500 Soo 444 444 89 89 70-130 0 Zinc ug1L 2.9J 500 500 435 436 86 87 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 151899E 1518999 MS MSD 92260178001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cane. Result Result % Rec % Rec Limits RPD Qual Cadmium ug1L 2.3 500 500 457 453 91 90 70-130 1 Chromium ug1L 13.0 500 500 475 473 92 92 70-130 1 Copper ug1L 824 500 500 1340 1440 102 122 70-130 7 Nickel uglL 14.8 500 500 453 450 88 87 70-130 1 Zinc uglL 608 500 500 1040 1060 86 89 70-130 2 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 16 IaceAnalyfical' (�www.paoelabs.com QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260323 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville. NC 28070 (704)875-9092 QC Batch: WET/39159 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92260323003 METHOD BLANK: 1520840 Matrix: Water Associated Lab Samples: 92260323003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 07/29/15 11:24 LABORATORY CONTROL SAMPLE: 1520841 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 248 99 90-110 SAMPLE DUPLICATE: 1520842 92260085003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 177 200 12 D6 SAMPLE DUPLICATE: 1520916 92260247001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 6.4 6.4 0 Results presented on thin page are in the units Indicated by the "Units" column except when an attempt* unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 16 aceAnalytical wwwpacWab&CoM QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260323 QC Batch: WET139092 Analysis Method: SM 52108 QC Batch Method: SM 5210B Analysis Description: 52108 BOO, 5 day Associated Lab Samples: 92260323002 METHOD BLANK: 1518626 Associated Lab Samples: 92260323002 Parameter Units BOD, 5 day mglL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 2A 07129M5 23:39 LABORATORY CONTROL SAMPLE: 1518627 Spike Parameter Units Conc. BOD, 5 day mglL 198 SAMPLE DUPLICATE: 1518628 92260323002 Parameter Units Result BOD, 5 day mg1L 20.4 LCS LCS % Rec Result % Rec Limits 175 88 84.6-115.4 Dup Result RPD Qualifiers 19.9 2 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 16 laeAnalyticaI www.pacobs.corn QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260323 Pace Anatytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704P75-9092 QC Batch: WETA123876 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92260323001 METHOD BLANK: 1519000 Matrix: Water Associated Lab Samples: 92260323001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg1L ND 25.0 07/27/15 15:45 LABORATORY CONTROL SAMPLE: 1519001 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 746 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1519002 1519003 M5 MSD 92260042002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Quai Chemical Oxygen Demand mglL 250 1500 1500 578 578 22 22 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1519004 1519005 MS MSD 92260382006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L ND 750 750 76.0 76.0 9 9 90-110 0 M1 Results presented on this page are In the units indicated by the "Units- column except where an altamate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 16 laneAnalyfical' www,paosfaftcorn QUALIFIERS Project: BAKERS STORMWATER Pace Project No.: 92260323 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Kuntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, inc.. Page 12 of 16 (�55ce Analytical� aww.psoma av" QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BAKERS STORMWATER Pace Project No.: 92260323 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)075-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92260323004 SW02 EPA 200.7 MPRP119100 EPA 200.7 ICP117179 92260323003 SW02 SM 2540D WET139159 92260323002 SW02 SM 5210B WET139092 SM 5210B WET139095 92260323001 SW02 SM 5220D WETA123876 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 16 (!2100 Af ly f al* Document Name: Condition Upon Receil Document Number: F-CHR-CS-003-rev.16 Document Revised: May 18, 2015 Pane 1 of 2* Issuing Authority: Pace Huntersville Qualitv Office Client Name. I S pecei Q ' Page 2 of 2 Is for Internal Use Only Courier: ❑ Fed Ex ❑ UPS❑ LISPS[] Client❑ Commercial❑ DPaOther +.�r��/^']]� 0 • .{{p'� V f,S y �lIV tF lie •iV i.�q y„t� ; S Custody Seal on CoofetlBox Present: yes ❑ no Seals intact:.0' yes ❑ no �,� Packing Material: ❑ Bubble V❑p ❑ Bubble Bags None%/..E]� Other Thermometer Used: IR Gun T1401 Type of Ice. ( Wet/ Blue None Samples on ice, cooling process has begun Temp Correction Factor T1�401 No Correction ���� Corrected Cooler Temp. -.Date and Initials of pore •C Biological Tissue Is Frozen: Yea No I I 1so e a Ining contents: Temp should be above freezing to 6'C Comments: ` Chatn'of Custody Present: es ONO ❑NIA 1. Chain of Custody Filled Out: fil'es ONO ❑NIA 2. Chain of CustodyRelinquished: Dyes ONO ❑NIA 3. Sampler Name & Signature on COC: Yes. ONO ❑NIA 4. Sam les Arrived within Hold Time: Yes ❑ o ❑NIA 5. Short Hold Time Analysis <72hr : e o ❑NIA 6. Rush Turn Around Time Requested: DYes o ❑NIA 7. Sufficient Volume: PK. ❑No ❑NIA 8. Correct Containers Used: -Pace Containers Used: !" `es..ONo i1Yes ONO ❑NIA ❑NIA 9. Containers Intact: es ❑No ❑NfA 10. Filtered volume received for Dissolved tests oes. ONO ❑NIA 11, Sample Labels match COC: -includes dateltimellD/Anal sis Matrix: P, r" ONO IN I ❑NIA 12. All containers needing preservation have been checked. All containers needing preservation are found to be in Yes ONO dYes ONO ❑NIA ❑NIA 13, compliance with EPA recommendation. exceptions: VOA, ooliform, TOC, O&G, VIA-ORO (water) Dyes JAo Samples checked for dechlorinalion: ❑Yes ONO NfA 14, Heads ece in VOA Vials >6mm : Dyes ONO 6NIA 15. Trip Blank Present: Dyes ONO t&NIA 16, Trip Blank Custody Seats Present Dyes ONO 21'NIA Pace_Tri .Blank;Lot.#: if. purchased):, - Client notification! Resolution., Field Data Required? Y 1 N Person Contacted: DetefTime: Comments! Resolution: SCURF Review: Date: ( - ; 9226®323 SRF Review: Data: Z O Note: Whenever there is a discrepancy affecting North Carolina compliance lilt 111111 samples, a copy of this form will be sent to the North Carolina DEHNR y 4 i ; Le out of hold Incorrect preservative, out of temp. � 60323 Certification Office ( p p. 822 Incorrect containers) Page 14 of 16 2. Anf?h/fit-ni' CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. AN relevant Gelds muss be completed accurately. ar�."cataas.com Cr. Page: CL of Section A Section S Section C Required Client Information: Required Project Information: I / Retort To:,�/17 Invoice Information" A o T �L WcL �jZo T e "? -1L a�!'eL � J r[(�rrf I�rCt'IGiGC .S REGULATORYAGENCY / re= NPOES UST i—] ij GROUNDWATER RCRA - DRINKING WATER i OTHER EmadTo: Purchase Ord" 140.: Paw Owte Rasarmroo: Fax Project Name: a ��s S or uJ cr POCK Prapa Site Location STATE, f �L Requested Due DatoITAT: Project NumCar. Papa PmrJe °: Requested Analysis Filteredf (Y!N) Section D Matrix Codes Z Roquahed CMnt rnfaon MATRIX r CODe s M COLLECTED Preservatives I Drinking Water DW Water WT U rj O zo waste Water WIN Product P IT —COMPOSITE Ui} SAMPLE !D Soivsolia SL Ott } x Is U W �, i G ,n°LrP (A-Z. 0-01;) Air AR a v 0. Z M O t �`yJ Sample tDs MUST 9E UNtOUE Tissue TS Other OT O Q. O m o H T Zvi m � 1� L`�' E T F_ M ° 0. GO O O vi an d v N l r In I DATE TIME DATE TIME = i i z z z O Pace Project NoJ Lab L.D. : D" ' G -3is X # s I Offs LS tt) FFF� _7 2 4 ` U 7 73et U NED BY 1 AFFIUAT10N DATE TIME ACCEPTED BY r AFFILIATION DATE }TtMe SAMPLE CONDITIONS a K 1 0t L1 X,t.._. SAMPLER NAME AND SIGNATURE S� I `o m PRINT Name of SAMPLER: J dd ' 5 e, z � �'. p$mp 8 U z ;, � c z � — SIGNATURE of SAMPLER: DATE Signed r (Mmmar : z,2 /J # F " � v E vi 'Imoonant Nor. By sgrwrp mis form yov aro aoaor++9 Pace's NET 30 day Mrrem twins One agreainp to We n w,;03 of 1.5% Per moam for any re o.= nei II&WO n 30 days. I F-ALL-O"020rev.07. 1 SMay-2007 r CHAIN -OF -CUSTODY 1 Analytical Request Document aceAnalytkal • The Chainof-Cuslody is a LEGAL DOCUMENT. All relevant fields must be Completed accurately. to I Section A' Section B - Section C - CL Page: of Required Client Information; Required Project Information: Invoice Inlw=l; en: - + 1;1= Repon Att TO: � nl,: k if R•; r r!(r r le";-, Add— ' J CopYTO Z J // // / r/!� n�P r=1Q r { r t REGULATORY AGENCY �,/ NPDES i GROUNDWATER i DRINKING WATER r— UST i RCRA - OTHERRerermm Ernail TO: Purchase Order NO:. Pace cl+0te ore / y-:�sr9 - 4 � /1 Fax' Projea Name' (�� �r S ; ���/� cJ�� c Pxo ftal- M Site Location STATE: Requested Due Date1TAT: Project Number. . Pam ProLle r. r Requested Analysis Filteredf (YfN) Section D Matrix Codes — E. z RmWlrod Q,enttrlforinatien •. MATRIX r CODE R _ � COLLEC MD Preservatives s Drinking Water DW Water W7 - U oz Waste Ater WW v m c T 1l ENMPAD w r - 1 z Product Soil/sclid St. C9 �' -e SAMPLE ID w F N C ,� (A Z 0 9 f; i Aires AR Sample IDS MUST SE UNIOUE ' Tessue TS 0- a w z Z U a 001er OT fC• W- r- to O y G C N T r� V 1:'1 l W r r f 1 1 tL q p 0. O H m r •y ' ~ DATE' TIME .DATE TIME �- , # = 2 T Z Z 2 O 1 Pace Project NoJ Lab I.D. -1=-4- { 1 r x -; s I s T - tf � 4 10 11 s� ! - 12 ADDITIONAL COMMENTS REUNOULSHF-D BY! AFF.3LU4TiON DATE TIME ACCEPTED BY f AFFILIATION DATE 'TIME SAMPLE CONDITIONS 5&r11 e?S,1v 119err. -. !JM I V i/ `vtiYS 1t tr it r� w !1 I 1 3I 1 V, y SAMPLER NAME AND SIGNATURE_ ,,� �� B m _ � PRINT Name of SAMPLER-z c Z c •ai•:_ r S1 SIGNATURE of SAMPLER: ;1 /J /� DATE Signed ,_, /� 7'2 -,�I n m � : -- rj �� c h {M.TE j; 7 y -1mPonam Note; By 6VftA9 trss form you aM acspurg PacaLs NET 30 day payment tends aN aWvc rg to tam charges of 1.5% per mach for airy rlvoce3 not D64J wcM 30 ears. I I--ALL-0-020reV.D7. 15-May-ZO07 Ie Analytical www.paoefab&com July 30, 2015 Mr. Joe Hinkle Allvac RE: Project: BAKERS STORMWATER Pace Project No.: 92260317 Dear Mr. Hinkle: Pace Analytical Services, inc. 9800KinceyAve. Suite100 Huntersville, NC 28078 (704 )875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 16 IeAinalyti�cal` rnuw.pacafamcom Project: BAKERS STORMWATER Pace Project No.: 92260317 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia[VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Hunlersville, NC 28078 (704)875-9092 This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc., Page 2 of 15 le aceAnalytical www.paoslabacom SAMPLE ANALYTE COUNT Project: BAKERS STORMWATER Pace Project No.: 92260317 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704 )87S9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92260317001 SW03 SM 5220D MJP 1 PASI-A 92260317002 SW03 SM 5210B BRJ 1 PASI-A 92260317003 SW03 SM 2540D SAM 1 PASI-A 92260317004 SW03 EPA 200.7 JDA 5 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Tull, without the written consent of Pace Analytical Services, Inc.. Page 3 of 15 IeAnalytical www.pacAbs.c= ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704j875-9092 Project: BAKERS STORMWATER Pace Project No.: 92260317 Sample: SW03 Lab ID: 92260317001 Collected: 07/23/15 07:31 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5220D COD Chemical Oxygen Demand Date: 07/3012015 02:30 PM Analytical Method: SM. 5220D ND mg1L 25.0 1 07127I15 15AS REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 15 aceAnalytrcal* www.paaal9b3.com ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92260317 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Sample: SW03 Lab ID: 92260317002 Collected: 07/23/15 07:32 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qual 5210E BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 4.9 mg1L 2.0 1 07/25/15 04:41 07129/15 23:39 I Date: 07/30/2015 02:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 15 laoeAnalyfical* www.pacelabs.cnm ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Project No.: 92260317 Sample: SW03 Lab ID: 92260317003 Collected: 07/23/15 07:33 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Total Suspended Solids Analytical Method: SM 2540D 14.0 mglL 3.6 REPORT OF LABORATORY ANALYSIS 07/29/15 11:30 This report shall not be reproduced, except in full, Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 15 acMnalyfical o www.psceiabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pars Project No.: 92260317 Sample: SW03 Lab ID: 92260317004 Collected: 07/23/15 07:35 Received: 07/24/15 12:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug1L 1.0 1 07/27/15 19:00 07/28/15 20:16 7440-43-9 Chromium ND ug1L 5.0 1 07/27/15 19:00 07/28/15 20:16 7440-47-3 Copper 31.0 ug1L 5.0 1 07/27/15 19:00 07/28/15 20:16 7440-50-8 Nickel ND u011- 5.0 1 07/27/15 19:00 07/28115 20:16 7440-02-0 Zinc 23.3 ug1L 10.0 1 07/27/15 19:00 07/28/15 20:16 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 15 laneAnalytical" Kwwlacewhs.sam QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260317 QC Batch: MPRP119100 Analysis Method: EPA 200.7 QC Batch Method: EPA200.7 Analysis Description: 200Y MET Associated Lab Samples: 92260317004 METHOD BLANK: 1518994 Matrix: Water Associated Lab Samples: 92260317004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium ug/L ND 1.0 0712811519:37 Chromium ug/L ND 5.0 07128/1519:37 Copper ug/L ND 5.0 07128/1519:37 Nickel ug/L ND 5.0 0712811519:37 Zinc ug/L ND 10.0 0712811519:37 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1518995 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Cadmium ug/L 500 451 90 85-115 Chromium ug/L 500 467 93 85-115 Copper ug/L 500 464 93 85-115 Nickel ugJL 500 448 90 85-115 Zinc ug/L 500 441 88 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1518996 1518997 MS MSD 92260382008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 448 449 90 90 70-130 0 Chromium ug/L ND 500 500 466 465 93 93 70-130 0 Copper ug/L ND 500 500 462 461 92 92 70-130 0 Nickel ug/L ND 500 500 444 444 89 89 70-130 0 Zinc ug/L 2.9.11 500 500 435 436 86 87 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1518998 1518999 MS MSD 92260178001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone, Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L 2.3 500 500 457 453 91 90 70-130 1 Chromium ug/L 13.0 500 500 475 473 92 92 70-130 1 Copper ug/L 624 500 500 1340 1440 102 122 70-130 7 Nickel ug/L 14.8 500 500 453 450 88 87 70-130 1 Zinc ug/L 608 500 500 1040 1060 B6 89 70-130 2 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the resutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 15 laxAnalyfical* www.peceltift om QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260317 QC Batch: WET139159 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92260317003 METHOD BLANK: 1520840 Associated Lab Samples: 92260317003 Parameter Units Total Suspended Solids mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 07/2911511724 LABORATORY CONTROL SAMPLE: 1520841 Spike Parameter Units Conc. Total Suspended Solids mg/L 250 SAMPLE DUPLICATE: 1520842 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 LCS LCS % Rec Result % Rec Limits Qualifiers 248 99 90-110 92260085003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 177 200 12 D6 SAMPLE DUPLICATE: 1520916 92260247001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 6.4 6.4 0 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 15 laneAnalytical" wwwpacelabasam QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260317 QC Batch: WET139092 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 92260317002 METHOD BLANK: 1518626 Associated Lab Samples: 92260317002 Parameter Units BOD, 5 day mglL Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 07/29/15 23:39 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvllle, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1518627 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg1L 198 175 88 84.6-115.4 SAMPLE DUPLICATE: 1518628 92260323002 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg1L 20.4 19.9 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right or the mull. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 07/30/2016 02:30 PM without the written consent of Paoe Analytical Services, Inc.. Page 10 of 15 leAnalyfical xnvw.pacabbs.com QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92260317 OC Batch: WETAl23876 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92260317001 METHOD BLANK: 1519000 Matrix: Water Associated Lab Samples: 92260317001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L NO 25.0 07/27/15 15:45 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville. NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1519001 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mglL 750 746 99 90-110 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1519002 1519003 MS MSD 92260042002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 250 1500 1500 578 578 22 22 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1519004 1519005 MS MSD 92260382006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone, Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 750 750 76.0 76.0 9 9 90-110 0 M1 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 15 ace Analytical WWW..Pecefab&CCWn QUALIFIERS Project: BAKERS STORMWATER Pace Project No.: 92260317 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot, NO - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875.9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyt chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 07/30/2015 02;30 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 15 aceAnalyticalo www.pacefabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BAKERS STORMWATER Pace Project No.: 92260317 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92260317004 SW03 EPA 2007 MPRP119100 EPA 200.7 ICP117179 92260317003 SW03 SM 2540D WET139159 92260317002 SW03 SM 5210B WET139092 SM 5210B WET139095 92260317001 SW03 SM 5220D WETA123876 l' Date: 07/30/2015 02:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 13 of 15 t Client Name: , ' z� Document Name: Document Revised: May 18, 2015 Condition Upon Receipt SCUR Page 1 of 2' Document Number: Issuing Authority: F-CHR-CS-003-rev.16 Pace Huntersville Quality Office Page 2 of 2 is for Internal Use Only r Courier: []Fed Ex ❑ UPS❑ USPSO Client❑ Commercial[] Pacer -,Other Custody Seal on Cooler/Box Present: , yes ❑ no Seals Intact: :I yes ❑ no O~« 0 1p CI�Ti} Packing Material: ❑ Bubble vL p ❑ Bubble Bags ❑ Nonerj Other Thermometer Used: iR Gun T1401 Type of Ice: & Blue None Samples on Ica, cooling process has begun Temn Correction Factor T1401 No Correction Date and Initial s f p rs n e� Inln9 Corrected Cooler Tenip,: ..7 •C Biological Tissue is Frozen: Yes No RI contents: Temp should be above freezing to 6'C Comments: Chs3 Wof Custody Present: ,!Zlfes ONO ❑NIA 1. Chain of Custody Filled Out: es ONO ❑NIA 2. Chain of Custody Relinquished: 2! . ONO ❑NIA 3. Sampler Name 8r Signature on COC: es ON' ❑NIA 4. Samples Arrived within Hold Time: es ZjNo ❑NIA 5, Short Hold Time Analysis <12hr ; Yeses_ oo ❑NIA B. Rush Turn Around Time Requested: ❑Yes .Joao ❑NIA 7. Sufficient Volume: Pyes ONO ❑NIA 8. Correct Containers Used: lyres ONO ❑N/A 9, -Pace Containers Used: Res CINo ❑NIA Containers Intact: des ONO ❑NIA 10. Filtered volume received for Dissolved tests Was ONO ❑NIA 11. Sample Labels match COC: es ONO ❑NrA 12. -includes dateltime/ID/Anal sis Matrix: All containers needing preservation have been checked. �es ❑No ONIA 13. All containers needing preservation are found to be in 14Yes ONO ❑NIA compliance with EPA recommendation. exceptions: VOA, oolirorm, TOC, 080, col-DRO (water) ❑Yes �Io Samples checked for dechlorination: ❑Yes ONO P<A 14. Heads ace in VOA Vials >6mm : ❑Yea ONO 121 A 15. Trip Blank Present: ❑Yes ONO 16. Trip Blank Custody Seals Present ❑Yes ONO NIA Pace Trip Blank Lot # if purchased): - - - . - . - - . — _ . . - - _' Client Notification/ Resolution: Field Data Required? Y I N Person Contacted: Dale/Time: Comments/ Resolution: SCURF Review:1 NDater SRF Review: Date: 2, Note: Whenever there is a discrepancy affecting North Carolina compliance —samples,, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, Incorrect preservative, out of temp. Incorrect containers) -iW0#:92260317 jII2260 AlIIIIIIIIIIIIIIII Page 14 of 15 X_2ara do_2hitirg1 CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed a=urately. iavar.paulaEs.Sem C Page: of ' Section A Section B Section C Required Client Information- Required Project lnfoem hi Invoice lnfo nation: Report Ta: Attention• E I 8 8 7 8 e f ! Coe -SPY O C 14i ,OC /� � 1 .] C`I /.t,71 ' Bf 3 REGULATORY ENCY J J Ci !/ OYi r0� NPDES F r UST - GROUND WATER ; DRINKING WATER RCRA OTHER Email To: Purchase Order No.: Pace OuoW Fax. ProjectName. r Pf Sit. Location STATE: Requested Due DaterrAT: Project Number. Pace J Requested Analysis Filtered !N} Suction D Matrix Codes -- " z A.qukw Cent lnfermation MATRtx1 cooE o COLLECTED Preservatives s 1 Drinking water DW 3 1 w Water WT waste waver ww 32 U m COMPOSME ° EMDAGRAD w Product P m SAMPLE ID O1"s'kd o� �_ � Wipe WP (A-z 0-91.) Air AR o ta, z D o Sampke Ds MUST BE UNIQUE Tissue TS Other OT O U n. Z m o to w O L L) C� w g� IL( O aCL O� L C L i ~ i N DATE TIME DATE TIME z x Y z z d rar Pace Project No1d„ab I.D. 1 w 0 I IX 2 O afE - rvy I I 6jr 3 VS 3 1 s 6 7 9 16 11 rTIME -TI tz ADDITIONAL COMMENTS NQUISHED BY t AFFILIATION DATE ACCEPTED BY f AFFILIATION DATE Ime SAMPLE CONDITIONS �+ • {� q t K r J 1'r'l 4�'I�'�� �JlJ �4}C ORjG{;ti.-.L SAMPLER NAME AND SIGNATURE L) o z $ PRINT Name of SAMPLER: S iZ oC7 z E F e — fr U rn o r SIGNATURE of SAMPLER: DATE $ignad (MMlDD1YY}: may- y •ia,mnant NOW By signing tris form you are xtneptiry Pxe's NET 30 day oaymcrs terns ere agn e % to I= verges of 1.5% per n M for any mows not'$" vkm 30 eay& I F.ALL-Q-OZUrev.67. 15-May-ZU U 7 ace Analytical rrww.pscefabacom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite100 Huntersville, NC 28078 (704)875-9092 August 07, 2015 Mr. Joe Hinkle Allvac RE: Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on August 04, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, 1�,—D Matthew Brainard matthew,brainard@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 18 aceAnalyticale wmpaceiahscom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite t oo HuntersAlle, NC 28078 (704)875-9092 CERTIFICATIONS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Charlotte Certlflcatlon IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida./NELAP Certification #: E87W Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification M 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 18 aceftlytical e www.pnW6b$.=n Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92261784001 BAKERS NONCONTACT #1 EPA 1664E JMS 1 PASI-C SM 4500-CI G MLS 1 PASI-A 92261784002 BAKERS NONCONTACT #2 EPA 1664B JMS 1 PASI-C SM 4500-CI G MLS 1 PASI-A 92261784003 BAKERS NONCONTACT #3 EPA 16646 JMS 1 PASI-C SM 4500-CI G MLS 1 PASI-A 92261784004 BAKERS NONCONTACT #4 EPA 16646 JMS 1 PASI-C SM 4500-Cl G MLS 1 PASI-A 92261784005 BAKERS NONCONTACT #5 EPA 1664E JMS 1 PASI-C SM 4500-CI G MLS 1 PASI-A 92261794006 BAKERS NONCONTACT #6 EPA 1664B JMS 1 PASI-C SM 4500-CI G MLS 1 PASI-A 92261784007 BAKERS NONCONTACT #7 EPA 1664B JMS 1 PASI-C SM 4500-CI G MLS 1 PASI-A 92261784008 BAKERS NONCONTACT #8 EPA1664B JMS 1 PASI-C SM 4500-CI G MLS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Anatytical Services, Inc.. Page 3 of 18 aceAnalytical • www,pacelahs.corn Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Sample: BAKERS NONCONTACT #1 Lab ID: 92261784001 Collected: 08/03/15 08:50 Received: 08/04/15 15A5 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 08/07/15 08:47 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.12 mg1L 0,024 1 08/05/15 10:35 7782-50-5 Date: 08/07/2015 03:02 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 18 aceAnalytical www.pacelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Sample: BAKERS NONCONTACT #2 Lab ID: 92261784002 Collected: 08/03/15 09:15 Received: 08104/1515:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 08/07115 08:48 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.17 mg1L 0.024 1 08/05/15 10:35 7782-50-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull, Date: 08/07/2015 03:02 PM without the written consent of Pace Anatytical Services, Inc.. Page 5 of 18 aceAnalytical www.pacefabscam Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Sample: BAKERS NONCONTACT #3 Lab ID: 92261784003 Collected: 08/03/15 09:35 Received: 08/04/15 15:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 08/07/15 08:48 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.41 mglL 0.12 5 08/05/15 10:35 7782-50-5 Date: 08/07/2015 03:02 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 18 d aceAnalyiical www.pacdabacom Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Kuntersville, NC 28078 (704)875-9092 Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Sample: BAKERS NONCONTACT" Lab ID: 92261784004 Collected: 08/03/15 10:00 Received: 08/04/16 15:45 Matrix: Water Parameters Results Units Report Limit ❑F Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 16648 Oil and Grease ND mg1L 5.0 1 08/07/15 08:49 4600CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.12 mg1L 0.024 1 08/05/15 10:35 7782-50-5 Date: 08/07/2015 03:02 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 18 aceAnalytical www.pacelah& WM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Sample: BAKERS NONCONTACT #5 Lab ID: 92261784005 Collected: 08/03/15 10:20 Received: 08/04/15 15:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 08/07/15 08:49 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.18 mg1L 0.024 1 08/05/15 10:35 7782-50-5 Date: 08/07/2015 03:02 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc„ Page 8 of 18 aceAnalytical wwwpacefaGacom Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Sample: BAKERS NONCONTACT #6 Lab ID: 92261784006 Collected: 08/03/15 10:45 Received: 08/04/15 15:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg[L 5.0 1 08/07/15 08:50 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.070 mg1L 0.024 1 08/05/15 10:35 7782-50-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 18 aceAnalytical. www.pacefabscom Pace Analytical Services, Inc. 9800 Kinoey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Sample: BAKERS NONCONTACT 97 Lab ID: 92261784007 Collected: 08/03/15 11:10 Received: 08104M5 15:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 08/07/15 08:50 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.093 mgfL 0.024 1 0810511510:35 7782-50-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 18 aceAnalytrcal www.pacelabsaom Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Sample: BAKERS NONCONTACT #8 Lab ID: 92261794008 Collected: 08/03/15 11:35 Received: 08/04/15 15:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 08/07/15 08:51 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine. Total Residual 1.3 mg1L 0.24 10 08/05/15 10:35 7782-50-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 18 aceAnalytical WW..pecelaba.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 QC Batch: GCSV122191 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92261784001,92261784002,92261784003,92261784004,92261784005,92261784006,92261784007, 92261784008 METHOD BLANK: 1528455 Matrix: Water Associated Lab Samples: 92261784001, 92261784002, 92261784003, 92261784004, 92261784005, 92261784006, 92261784007, 92261784008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mglL ND 5.0 08/07/15 08:46 LABORATORY CONTROL SAMPLE: 1528456 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 35.1 88 78-114 MATRIX SPIKE SAMPLE: 1529457 92261950002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/t_ ND 40 37.4 94 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 18 aceAnalytical www.pecelabs.com Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 {704�875-9092 QUALITY CONTROL DATA Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 QC Batch: WET139292 Analysis Method: SM 4500-CI G QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual Associated Lab Samples: 92261784001, 92261784002, 92261784003, 92261784004, 92261784005, 92261784006, 92261784007, 92261784008 METHOD BLANK: 1526178 Matrix: Water Associated Lab Samples: 92261784001, 92261784002, 92261784003, 92261784004, 92261784005, 92261784006, 92261784007, 92261784008 Blank Reporting Parameter Units Result Limit Anatyzed Qualifiers Chlorine, Total Residual mg/L ND 0.024 08/05/15 10:35 SAMPLE DUPLICATE: 1526179 92261784001 Dup Parameter Units Result Result RPD Qualifiers Chlorine, Total Residual mg1L 0.12 0.12 5 Reaufts presented on this page are In the units Indicated by the "Units" column except when an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 18 aceAnalytical" www.paoatabs.com Pace Analytical Services, Inc. 8800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit, RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 18 aceAnalytical ~.paoelehacom Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BAKERS NON CONTACT COOLING Pace Project No.: 92261784 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92261784001 BAKERS NONCONTACT #1 EPA 1664B GCSV122191 92261784002 BAKERS NONCONTACT 02 EPA 1664E GCSV/22191 92261784003 BAKERS NONCONTACT #3 EPA 16648 GCSV122191 92261784004 BAKERS NONCONTACT #4 EPA 1664B GCSV122191 92261784005 BAKERS NONCONTACT #5 EPA 1664B GCSVl22191 92261794006 BAKERS NONCONTACT #6 EPA 1664B GCSVl22191 92261794007 BAKERS NONCONTACT #7 EPA 1664B GCSVl22191 92261784008 BAKERS NONCONTACT #8 EPA 1664B GCSVl22191 92261784001 BAKERS NONCONTACT #1 SM 4500-CI G WET139292 92261784002 BAKERS NONCONTACT 92 SM 4500-CI G WET139292 92261794003 BAKERS NONCONTACT 03 SM 4500-CI G WET139292 92261784004 BAKERS NONCONTACT #4 SM 4500-CI G WETl39292 92261784005 BAKERS NONCONTACT #5 SM 4500-CI G WETl39292 92261784006 BAKERS NONCONTACT 96 SM 4500-CI G WET139292 92261784007 BAKERS NONCONTACT #7 SM 4500-CI G WET/39292 92261784008 BAKERS NONCONTACT #8 SM 4500-CI G WET139292 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 18 UOCUment Name: uocument htevisea: may its, u ra aCeAnnlytical' Sample Condition Upon Receipt (SCUR) Page 1 of 2` Document Number: Issuing Authority: F-CHR-CS-003-rev.16 Pace Huntersville Qualitv Office Client Name: L t ✓�t {- _ Page 2 of 2 Is for Internal Use Only Courier: ❑ Fed Ex [IUPS❑ LISPS❑ Client❑ Co erccial❑ � their0' `p 'ai Custody Seal on Cooler/Box Present: ❑ yes no Seals intact: El yes ❑ no *r sst t-'M r Packing Material: ❑ Bubble v❑tp ubble Bags ❑ bone ❑ Other Thermometer Used: IR Gun 1�40 Type of Ice: Wet Blue None amples on Ice, cooling process has begun Temp Correction Factor T1401 No orrection Biological Tissue is Frozen: Yes No lA Date and Initials of person ex �nlntng Corrected Cooler Temp.: 'C g contents:�� X' r' "_u Temp should be above freezing to 6°C Comments:. Chain -of Custody Present: es PfO ❑NIA 1. Chain of Custody Filled Out: es ❑NIA 2. Chain of Custody Relinquished: Dyl-row ❑NIA 3. Sampler Name & Signature on COC: ❑y s 0 ❑NIA 4, Samples Arrived within Hold Time: Of", ONO XNIA 5. Short Hold Time Analysis <72hr : Dyes o NIA 6. Rush Turn Around Time Reauested: ❑Yes o ❑NIA 7. Correct Containers Used: -Pace Containers Used: rQWesNo s o ❑NIA ❑NIA Containers Intact: Erfe, ❑No ❑NIA Filtered volume received for Dissolved tests ❑Yes No IA 11, Sample Labels match COC: -Includes date/lime/ID/Analysis Matrix: Yes , ❑o ❑NIA 12. All containers needing preservation have been checked. Dyes ONO ONIA 13. All containers needing preservation are found to be in compliance with EPA recommendation. ❑Yes C,iN1A j exceptions: VOA, conform, TOC, 09G, wi-DRO (water) Yes ONO Samples checked for dechlorination: Dyes ❑No IA 4. Heads ace in VOA Vials >6mm : Dyes ❑No ❑ 1 5. Trip Blank Present: Dyes ONO ❑Nl 1'6, 1 Trip Blank Custody Seals Present ❑Yea ❑No NIA - Pace Trip -Blank -Lot # if urchased :---- ---- - - --- - -- - - - ---- -- -- -- - -- - --- - - Client Notification/ Resolution: Field Data Required? Y 1 N Person Contacted: DatelTime: Comments/ Resolution: SCURF Review: Date: I mILCI WO# : 92261764 SRF Review: Date: EKC Note: Whenever there is a discrepa cy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR `a Z1i111411 fA 11! ttiillll Certification Office (i.e out of hold, incorrect preservative, out of temp, 817tl8 incorrect containers) Page 16 of 18 �. 'iceAralytical' CHAIN-0-CUSTODY 1 Analytical Request Document The Chain -of -Gus ndy is a LEGAL DOCUMENT. All relevant fields must t>e completed accurately. Section A Section B. Section C Page: of ioquired Client Information: Required Project Information: Prof Invoice Information: AttenWn� r 11883 5 0 ^_'Ael Report To: O� ` �� 4ddress Copy ; 1 '7 . W To:. : � /. /� C G� '• REGULATORY AGENCY ' Add O r NPDES GROUNDWATER 1= DRINKING WATER a UST ; RCRA F OTHER _mail To: Purchase Order. No.: Pam Doan Raera,ce: P Fax: Project Name Pepe Project Site Location �// J� O M` rs , r: STATE: Requested Due Date/TAT: Project Number - - - Pace Prefle 0: - { l - Requested Analysis Filtered (YIN) Section D Matrix Codes - z _ Regw.edcuan+ruorm,wn MATR+x r coDE. 3 2 COLLECTED r Preservatives °> Dnr*ing Water DW z J Water WT WaterWasta WW tj ay g C Product Sowsokd SL ' 01 START Ene6 J o -.0 ` 'J c t SAMPLE ID Oil �_ 0 w v0L (A-Z.0-91.•) Air AR Sample IDS MUST BE UNIQUE Tissue TS p O ur a a Z m H V v c L Other OT U w H m tl/ N S '•r O V �� L/ Ti Q U CL CCryz M L_ m C7 CD H- N rlMi anTt TIM x r z z OLL Pace Project NoJ Lab I.D. ix I I x) ,2 / 3 Ali Kers I c - , 4 ers #" r - s 1 Ix I I i 1xi 5 cr s No�J E 3-/ �.' !I 1XI It!b e �f Ohl v f�tc / 1I ix a. 6l Dn1 D fQG f C ,, S Id.l' g S 3;_/S ,.� •z ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION D TE TIME ACCEPTED BY AFFlLL4TION DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIC ORIGINAL NATURE PRINT Name of SAMPLE 1%1C r' CIO MPLER•' DATE Signed I SIGNATURE of m -m V = E (MfAlDDlYY): •Imoonant Now: By smwr o revs rpm you are aoeaavw Pam's NET 30 day oavmoa tom* and aar k e tD late onareos of i,5 oar merr& A wAnv&aWnda3z mA 3o daarr. --, i -N F-ALL-Q-020rev.07. 15-May-2007 /a • �r+n An�hrfir7l- CHAIN-O -CUSTODY 1 Analytical Request Document o The Chain-of-Cuswdy is a LEGAL DOCUMENT. All relevant fields must he completed accurately. ., uvt,i-u,a,yuvur tom. W uu6s.tam ection A Section B Section C Page: of equired Client Information: Required Project Information: Invoice Infomietion: Attention` JniQ�,e� Repon7o: Q/YI /►'i Q A CopyTo. I� Co N�C� REGULATORY AGENCY IJG D J D r �L ('� lit I S a G�, NPDES i GROUND WATER j DRINKING WATER s UST RCRA i OTHER mail To: Pui cnaso Order No.: Peoe Corte Rerer�wa: - - s// t3 W8,? IF Pro" LIrG� P� PM)w manaaar Site Location STATE: r, l equested Due Datr1TAT: Project Number: Paco Prof" A: .+l +� CJ Requested Analysis Filtered (YIN) Section D Matrix Codas g a. z RequImdC&ent Vdix sCon - MATRIX r CODE 3 COLLECTED Preservatives } Ddr*jng Water DW ct zO Water WT Waste Water VYVY tj m co�^rt> w z Product SoiuS0Ad SL b encrds:Aa L o g r SAMPLE ID w!� - �? a w in v w°P ;A-7- 0.9! :) Air AR a Z H o . Sample IDs MUST BE UNIQUE Tissue TS O a - Imo- le •:'�a '� Q=„er OT X z o m o 03. 71 ti R -• Q US U � W � .n Z (7in CE t p h - Q- O C _ z U _ rn DATE TIME _ DATE TIME v+ = y Z Z O .a.► Q Pace Project Not Lab E.D. I #r-J C 3LUS ILA,- li A( 5 i 7 Q/iI a G - , s r l I 0 z ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION IE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS 'D!A C .� Qnli Ei�:;� SAMPLER NAME AND SIC, TURE `o m 8 %a5- PRINT Name of PLER:' M rt Cow Y1T o1 1 a m z m m � � . a E m ~ o `-�' U Tii y SIGNATURE of SA:2 DATE Sig ned Q , ` ' `7 r� L &�&-1 (MMIDD(� cn impdnant Note: By signetg Mis tam you are aootrptuig Pace's NET 30 day paymeni terms and aoromm ID tata � .f 1 s c 4.....wti u..-... _41..—Lim. at, .,--- --