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HomeMy WebLinkAboutNCS000329_MONITORING INFO_20150128STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. C<�) boo DOC TYPE ❑FINAL PERMIT --X.- MONITORING REPORTS- ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑/L�6 YYYYMMDD STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS FACILITY NAME PERSON COLLECTING SAMPLE S) L J,� CERTIFIED LABORATORY(S) Lab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 12 LL' ! (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) E GNATURE OF PERMITTEE OR DESIGNEEEQUIRED ON PAGE 2.-1 1 : DateII Sample, Collected- 1 ; Rainfall WgNnlwhMWAWOMEN Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes /no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH' New Motor Oil Usage mo/dd/ r I MG linches mztl men unit gaumo Form SWU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Mail Original and one copy to: /q Division of Water Quality Date /r[ 'A/ Attn: Central Files Total Event Precipitation (in es): Q.�1617 Mail Service Center Event Duration (hours): (only if applicable — see permit.) Raleigh, North Carolina 27699-1617 (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) (Date) Form SWU-247, Iasi revised 21212012 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS IQ 3I(Q FACILITY NAME04 1� PERSON COLLECTING SAMPLEAS) j CERTIFIED LABORATORY(S) Lab #11_L_ Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: Z6 ty (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. r Date Sample Collected Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes Zo (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar •O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids PH' New Motor Oil Usage mo/dd/ r MG inches m m unit gallmo Form SWU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Mail Original and one copy to: ',' ''J Division of Water Quality Date Ld� L Attn: Central Files Total Event Precipitation (inches):1617 Mail Service Center Event Duration (hours): _4JA (only if applicable — see permit.) Raleigh, North Carolina 27699-1617 (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including thylpossibility of fines and imprisonment for knowing violations." (Date) Form SWU-247, last revised 21212012 Page 2 of 2 January 27, 2015 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 R CIE/vEt) JA N 3 0 2015 i.! OATI P.O. Box 5030 2020 Ashcraft Avenue Monroe, NC 2911, 1-5030 Phone: (704) 289-451 l Fax: (704)290-5194 Email: joe.hinkle(a),atimetals.com Central Files: DW R SECFIL 5 N Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and one copy are included. The monitoring data is for the following monitoring schedule: Monitoring Period Sample Number I Start I End Year 5 — Period 2 10 1 September 1, 2014 1 February 28, 2015 Analytical monitoring includes: • Outfall #01 (B), commingled stormwater • Outfall #02 (B), non -commingled stormwater • Outfall #03 (B), non -commingled stormwater • Non Contact Cooling Water #I - #8 If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sincerely, Dt f t�u J e Hinkle Environmental Manager ATI - Bakers Plant Stormwater Monitoring Report Form Sample Date: /1 r2U `1'i Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: 0 Sample Time: 7'. %1.2 0 /`tm Stormwater Discharee Outfall #01 (Commingled Drainage Area = 2,915,470sq. ft. = 69 acres % Impervious = 34% J ' �! ..Jr 4 40 CFR Part 136 Parameter Results (mg/1) Benchmark Values (mg/1) BOD 1,30 COD 120 TSS 100 Cadmium 0.001 Chromium, total recoverable 1 Copper, total recoverable Q� Q " 0.007 Nickel, total recoverable 0.26 Zinc, total recoverable 0.067 Oil and Grease 20 Temp (effluent) g, g (deg C) n/a Temp (downstream) gj (deg C) n/a Temp (upstream) 9(deg C) n/a Total Residual Chlorine 0.017 pH (std units) 6-9 (std units) Storm Date: - Storm Duration: �� (Hrs.) Inches of Rainfall: Q0 o�J Duration of time preceding rain event exceeding 0.1 ": (Hrs.) Estimated Flow Calculation: Q = CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches rain/12inches/ft, x 69 x .34) Q(Total, cfs) = 1.5180 x {Inches of rain) + 1.7595 x Ads (Inches of rain) FHR—M—MnnitnrinnRr. rtFnm—Rr 1 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS_ e)06329 FACILITY NAME / y /// PERSON COLLECTING SAMPLES) a �T CERTIFIED LABORATORY(S) Lab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) EREO ATURE OF PERMITTEE OR DESIGNEE UiRED ON PAGE 2. i I Date Sample CollectedI I'Total 1 Rainfall Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes Zno (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) I Non -polar O&G/TPH (Method 1664 SGT-HEM), if a 1- Total Suspended Solids pH New Motor Oil Usage moldd/ r MG inches mo m unit al/mo Form SWU-247, last revised 21212012 Page 1 of 2 STORM EVENT CHARACTERISTICS: Mail Original and one copy to: ,q-qq— Division of Water Quality Date /0 Attn: Central Files Total Event Precipitation (inc es): Q� as 1617 Mail Service Center Event Duration (hours): Y (only if applicable — see permit.) Raleigh, North Carolina 27699-1617 (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Permittee) /-pop-�s (Date) Form SWU-247, last revised 21212012 Page 2 of 2 "ATI Allvac - Bakers Plant Stormwater Monitoring Report Form Sample Date: a "U -/7 Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods Results of Samule Analvsis: Sample Time: Stormwater Discharge Outfall #02 (Non -Commingled) Drainage Area = 212,952sq. ft. = 4.9 acres % Impervious = 12% 11111111111 1 t 111 /_ 40 CFR Part 136 Parameter Results (mgll) Benchmark Values (mgll) BOD J-S 30 COD Hy 120 TSs 100 Cadmium 0.001 Chromium, total recoverable 1 Copper, total recoverable 6 ) ' 0.007 Nickel, total recoverable 0.26 Zinc, total recoverable Q v 0.067 pH (std units) 6-9 {std units} Storm Date: jr� Storm Duration: (Hrs.) Inches of Rainfall: Duration of time preceding rain event exceeding 0.1": (Hrs.) Estimated Flow Calculation: Q = CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 4.9 acres x .88) + .9 x inches rain112inches/ft. x 49 x .12) Q(Total, cfs) = 0.1437 x ,v S (Inches of rain) + 0.0441 x (Inches of rain) Allvac - Bakers Plant Fliq — v W — MnnitnrinP Rr rt Fnr — Rev 1 16 ATI Stormwater Monitoring Report Form Sample Date: Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Sample Time: I ., Y.YAA Stormwater Discharge Outfall #03 (Non -Commingled) Drainage Area = 336,580sq. ft. = 7.8 acres % Impervious = 15% 40 CFR Part 136 Parameter Results (mg/1) Benchmark Values (mg/1) BOD AID30 COD ND 120 TSS / 100 Cadmium 0.001 Chromium, total recoverable 1 Copper, total recoverable 0 0.007 Nickel, total recoverable D 0.26 Zinc, total recoverable 59 0.067 pH (std units) 6-9 (std units) Storm Date: Storm Duration: (Hrs.) Inches of Rainfall: 0"71u Duration of time preceding rain event exceeding 0.1": //5 (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 7.8 acres x .85) + .9 x inches rain/ I 2inches/ft. x 7.8 x .15) Q(Total, cfs) = 0.2210 x , 0?5 (Inches of rain) + 0.0878 x (Inches of rain) FHR — SW — Mnnitnrino Rp.r " Fnrm — RPv 1 ATI Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods Results of Sample Analysis: Allvae - Bakers Plant Stormwater Monitoring Report Form Non -Contact Cooling Wastewater /1!� �Iv I' j 2 7/ - , 'I'a In, f S /Al. 0 _. Ica/ 40 CFR Part 136 Non -Coat Cool Water Sampling Sampling Estimated Sample Location =Effluent Total Res # Date Time Ti Flow (MGD) Chlorine Temperature (deg C) pH (std. units) m 2 3 i- /5 9-'2 D 0. D59 35, d 4574D aoN 905L ,3 r L There are no discharges of air compressor condensate. Benchmark value for Total Res Chlorine = 0.017 mg/L. FPS —SW — Mnnitnrina Rennrt Fn — Rev 1 A � NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: http_//12ortal.ncdenr.or2/web/wQ/ws/su/npdessw#tab-4 Permit No.: N&ISI&Q/ /a/ / or Certificate of Coverage No:: N/C/Q/_/,/__/_ Facility Name: County: LL/I i OA Phone No. Inspector: ; - ✓ G art 41 Date of Inspection: /D--3i- /4 Time of Inspection: /I ,,Sv,4A Total Event Precipitation (inches): _a. LLB' Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) V Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or)ftsignee) Pagel of 2 5WU-242, Last modified 10/25/2012 r w � 1. Outfall Descri tion , Outfall No. S Structure (pipe, ditch, etc.) Receiving Stream: , VD Describe the industrial 1a ivides that o cur witjn the utfall drainage area: A1,9A1 --D/1 TQGT G'oo/�'/I�i � 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: c�l� i e— _ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 20 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 10 2 3 4 5 b. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 O 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes (S 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe — V r_' 4e Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 'k, NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http://portal.ncdenr.or2/web/wq/ws/su/npdessw#tab-4 Permit No.: N Facility Name: County: —(� or Certificate of Coverage No.: Inspector: 7,9m12N 4 Date of Inspection: Time of Inspection: ly?,'Od AA Total Event Precipitation (inches): 6, 66 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) PfYes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permitter Design SWU-242, Last modified 10/25/2012 Page 1 of 2 1. Outfa 1 Description: Outfall No. Structure (pipe, ditch, etc.) Receiving Stream: 04lGC Describe Xhe jndustrial activif ies that occur within the outfall drainage area: 2. Color: Describe the color of the (light, medium, dark) as descriptors: ng basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): AMA 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 O _3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1@ 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 t`J 3 4 5 7. Is there any foam in the stormwater discharge? Yes No B. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe 41'20e— Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 i * ; fi � j;h NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform, please visit. http;//portal.ncdenr,orp-lweb/wq/ws/su/nl2dessw#lgb-4 Permit No.: NIC/%� Facility Name: County: 11r1 4,o Inspector: ZIO/Pt Date of Inspection: Time of Inspection: or Certificate of Coverage No.: Phone No. Total Event Precipitation (inches): � S// Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) IVYes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittk or DesigfiVe) SWU-242, Last modified 10/25/2012 Pagel of 2 1. Outf4jI Descri Dutfall No. Receiving Stream: Describe the industrial et re (pi?e, ditch, etc.) —AIL vities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: AW I- - 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /AD/1� 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 Q 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 Q 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe /if c—&- Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5WU-242, Last modified 10/25/2012 1aceAnalytical o wwwpecelab3.00m December 30, 2014 Mr. Joe Hinkle Allvac RE: Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on December 22, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Laura J Cooper Iaura.cooper@paceIabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac )qeWIF REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 14 lacieAnalybcalo mvw.pecWbs.c= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 Charlotte Certiflcation IDs 9800 Kincey Ave. Ste 100, Huntersvil le, NC 28078 North Carolina Drinking Water Certification M 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification 10s 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87W Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Flodda/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia[VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification M 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 14 aceAnalytical. wxwpecelabs.com SAMPLE ANALYTE COUNT Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92230659001 BAKERS STORMWATER SW01 EPA 16648 CLW 1 PASI-C EPA 200.7 SH1 5 PASI-A SM 2540D MDW 1 PASI-A SM 4500-CI G MAB 1 PASI-A SM 5210B MLS 1 PASI-A SM 5220D EWS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 14 leAnalytical" wwwpacelaba.oam ANALYTICAL RESULTS Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BAKERS STORMWATER Lab ID: 92230659001 Collected: 12/22/14 04:50 Received: 12/22/14 12:30 Matrix: Water SW01 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 12/22/14 16:42 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND uglL 1.0 1 12/23/14 1510 12/23114 22:30 7440-43-9 Chromium ND uglL 5.0 1 12/23/14 15:10 12/23/14 22:30 7440-47-3 Copper 24.3 ug/L 5.0 1 12/23/14 15710 12/23/14 22:30 7440-50-8 Nickel ND uglL 5.0 1 12/23/14 15:10 12/23/14 22:30 7440-02-0 Zinc 15.9 ug1L 10.0 1 12/23/14 15:10 12/23/14 22:30 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 4.6 mg1L 3.6 1 12/26/14 17:10 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.060 mg1L 0.024 1 12/23/14 10:50 7782-50-5 H1 5210E BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 2.6 mg1L 2.0 1 12/23114 15:45 12/28/14 16:10 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand ND mg1L 25.0 1 12/30/14 08:30 Date: 12/30/2014 01:51 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written Consent of Pace Analytical Services, Inc.. Page 4 of 14 aceAnalytical www.pecelabs com QUALITY CONTROL DATA Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: GCSV119881 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92230659001 METHOD BLANK: 1358035 Matrix: Water Associated Lab Samples: 92230659001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg1L ND 5.0 12/22/14 16:40 LABORATORY CONTROL SAMPLE: 4358036 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 38.0 95 78-114 MATRIX SPIKE SAMPLE: 1358037 92230565001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 39.0 94 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an attemate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 01:51 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 14 leAnalytical* www.pecnlaha.own QUALITY CONTROL DATA Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 QC Batch: MPRP117612 Analysis Method: EPA200.7 QC Batch Method: EPA200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92230659001 METHOD BLANK: 1358768 Matrix: Water Associated Lab Samples: 92230659001 Parameter Units Blank Result Cadmium ug1L NO Chromium ug1L NO Copper ug1L NO Nickel ug1L NO Zinc ug1L NO Reporting Limit Analyzed Qualifiers 1.0 12/23114 21:56 5.0 12/23/14 21:56 5.0 12/23/14 21:56 5.0 12/23/14 21:56 10.0 12/23/14 21:56 Pace Analytical Services, Inc. 9B00 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1358769 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug/L 500 462 92 85-115 Chromium ug1L 500 438 88 85-115 Copper ug1L 500 459 92 85-115 Nickel ug1L 500 462 92 85-115 Zinc uglL 500 439 88 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1358770 1358771 MS MSD 92230489001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug1L ND 500 500 475 460 95 92 70-130 3 Chromium ug1L 575 500 500 1010 974 87 80 70-130 4 Copper ug1L 31.9 500 500 492 466 92 87 70-130 5 Nickel ug1L 193 500 500 636 615 89 84 70-130 3 Zinc uglL 392 500 500 816 804 85 82 70-130 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1358772 1358773 MS MSD 92230486001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium uglL NO 500 500 465 458 93 92 70-130 2 Chromium ug1L NO 500 500 437 434 87 87 70-130 1 Copper uglL 3.2J 500 500 464 457 92 91 70-130 2 Nickel ug1L NO 500 500 462 457 92 91 70-130 1 Zinc ug1L 4.8J 500 500 442 435 87 86 70-130 2 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 01:51 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 114 (�5a'cmnalyfical"` WWW..pacelebscom QUALITY CONTROL DATA Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 QC Batch: WET134994 Analysis Method: SM 25400 QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92230659001 METHOD BLANK: 1360241 Associated Lab Samples: 92230659001 Parameter Units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: 1360242 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1360243 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1360244 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 12/26/14 17:08 Spike LCS Conic. Result 250 230 92230657001 Dup Result Result 11.1 13A 92230718001 Dup Result Result ND ND Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 LCS % Rec % Rec Limits Qualifiers 92 90-110 RPD Qualifiers 19 D6 RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 01:51 PM without the wntten consent of Pace Analytical Services, Inc,. Page 7 of 14 (�Iacmnalyficalo wwwpacetehs.cam QUALITY CONTROL DATA Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 QC Batch: WET134933 Analysis Method: SM 4500-CI G QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual Associated Lab Samples: 92230659001 METHOD BLANK: 1358408 Associated Lab Samples: 92230659001 Parameter Units Chlorine, Total Residual mg/L SAMPLE DUPLICATE: 1358409 Parameter Units Chlorine, Total Residual mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.024 12123/1410:50 92230659001 Dup Result Result RPD Qualifiers 0.060 0.058 3 H1 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 12/30/2014 01:51 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 14 aceAnalytical WWW'Paoefaba.wm QUALITY CONTROL DATA Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 QC Batch: WET134942 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210B BOD, 5 day Associated Lab Samples: 92230659001 METHOD BLANK: 1358934 Associated Lab Samples: 92230659001 Parameter Units BOD, 5 day mglL LABORATORY CONTROL SAMPLE: 1358935 Parameter Units BOD, 5 day mg1L SAMPLE DUPLICATE: 1358936 Parameter Units BOD, 5 day mglL Pace Analyticai Services, Inc. 9800 Kinccy Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 12/28/14 16:10 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 184 93 84.5-115.4 92230700001 Dup Result Result RPD Qualifiers 3340 2970 12 D6,1-13 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fug, Date: 12/30/2014 01:51 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 14 aceAnalyrical wwwpecefabscom QUALITY CONTROL DATA Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 QC Batch: WETA121408 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92230659001 METHOD BLANK: 1359896 Associated Lab Samples: 92230659001 Parameter Units Chemical Oxygen Demand mg1L LABORATORY CONTROL SAMPLE: 1359897 Parameter Units Chemical Oxygen Demand mg1L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 12/30114 08:30 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 750 776 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1359898 1359899 MS MSD 92230124003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 223 750 750 932 929 95 94 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1359900 1359901 MS MSD 92229858002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L ND 750 750 768 756 102 101 90-110 2 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 01:51 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 14 leAnalytical www.psoelaCscom QUALIFIERS Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. H1 Analysis conducted outside the EPA method holding time. H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 01:51 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 14 lacieAnallytical" w*w.pecelaftcam QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BAKERS STORMWATER SW01 Pace Project No.: 92230659 Lab ID Sample ID 92230659001 BAKERS STORMWATER SW01 92230659001 BAKERS STORMWATER SW01 92230659001 BAKERS STORMWATER SW01 92230659001 BAKERS STORMWATER SW01 92230659001 BAKERS STORMWATER SW01 92230659001 BAKERS STORMWATER SW01 Date: 12/30/2014 01:51 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch Method QC Batch Analytical Method EPA 1664B GCSV119881 EPA200.7 MPRPI17612 EPA200.7 SM 2540D WET/34994 SM 4500-CI G WETI34933 SM 5210B WET134942 SM 52103 SM 5220D WETA121408 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch ICPI15865 WET134946 Page 12 of 14 acoArkMlcal• Sample Condition Upon Receipt SCUR) Page 1 of.2 Document Number: Issuing Authority: F.CHR-CS-003-06.15 Pace Huntersville Qualit Office Client Name: 4Tl spge, A1� N44e,,, , (AUVAC- Courier: ❑ Fed Ex ❑ UPS❑ USP40 Client❑ Commercial[] Pace Other, 6 Ibrtal . ..., r�. kv Custody Seal on Cooler/Box Present: ❑ yes W no Seals intact: El - yes ❑ no iin-?I'(�'�4 , �D>1te,,�, "� � ,IfoJ1 Packing Material: ❑ Bubble V❑p ❑ Bubble Bags ❑ None 0 Other 7A e— Thermometer Used: IR Gun T1401 Type of Ice:(kep Blue None %Samples on tee, cooling process has begun Temo Correction Factor T1401 No Correction Corrected Cooler Tem.:7+ •C p Temp should be above freezing to 6°C Biological Tissue is Frozen: Yes fto N!A Comments: Date and Initials of per on ramtning contents:— !� t / Chain of Custody Present: es ❑No ❑NIA 1 • Chain of Custody Filled Out: Wes ❑No ❑NIA 2. Chain of Custody Relinquished: es ❑No ❑NIA 3, Sampler Name & Signature on COC: es ONO ❑NrA 4. Samples Arrived within Hold Time: Kies ONO ❑NfA 5. Short Hold Time Analysis <72hr : Yes ONO ❑NIA 6, Rush Turn Around Time Requested: es ❑No ©NIA 7. Sufficient Volume: pOes ❑No ❑NIA g. Correct Containers Used: -Pace Containers Used: Plyes ❑No es ❑No ❑NIA ©NIA 9, Containers Intact: es ❑No ❑NIA 10. Filtered volume received for Dissolved tests es ❑No ❑NIA 11, Sample Labels match COC: -Includes dale/time/0/Analysis Matrix: es ❑No ❑NIA 12. All containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. exceptions: VOA, coliform, TOC. O&G,1M-SRO (water) �les; ❑No *19 ❑No es ❑No El NIA ❑N1A 13. Samples checked for dechlorinatlon: []Yes 1SINo IA 14. Heads ace in VOA Vials >Bmm : ❑Yes ❑No IA 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot !f if purchased): ❑Yos P%o ❑Yes ❑Noi ❑NIA trA 16. Client Notification/ Resolution: Field Data Required? Y I N Person Contacted: Datefrime: Comments/ Resolution: SCURF Review: Date: D�JzACgyp: ; 92�30659 SRF Review: Date: Note: Whenever there is a dis pancy affecting North Ca ollns compliance 1111111111111,1111111-111 samples, a copy of this form will be sent to the North Carolina DEHNR ` Certification Office ( Le out of hold, Incorrect preservative, out of temp, 92230559 Incorrect containers) Page 13 of 14 CHAIN -OF -CUSTODY 1 Analytical Request Document ....)! / % A aceAnpacelabs.wm The Chain -Custody is a LEGAL DOCUMENT. All relevant fields mutst be competed accurately. -ofalyti%al Section A Section B Section C Page. of Required C5ent Information; Required Project Infomla5on: Report To: Invoice Infonrw on: Attention: 9 1886856 i 8 8 6 8 5 6 `T Coay7o� ` REGULATOFtYAGENCY Bfir I NPQES •GROUND WATER r DRINKING WATER Email To: Purchase Ordor No.: Peon Quote r UST RCFIA i OTHER Referm ysiFax: Project Name Pace PMWI Site Location Requested Due DatalTAT: Project Number. Pepe Prone a,57A7E: Requested Analysis. Filtered Section D Matrix Codes RequlredCWft iefomuUM MATRIX I CODE o COLLECTED Preservatives Onrdcing Water OW p2 O Z water WT Waste Water WW g U cc rAItP06riECOMPOSITE U Product P — START ENorcfue SGIVS06d SL o x U SAMPLE ID Qd OL m' Wipe WP (A-Z.0-91:) Air AR C' a z Sample IDS MUST BE UNIQUE Tissue TS O d i'_ w Other OT U X W W -O, IN H g8 dg LL 4 (� a ~ H DATE TIME DATE• TIME' y _ _ = Z Z O t..,,Pace Project Lab l.D/. 1 I. �v rr C' ,,No.l 7iZ VtfrS I z -f �1 a r cr iJ 7 i 'S� �r 7 9 i0 ti 12 ADDITIONAL COMMENTS RELl lul8M BY I AFFILIATION DATE TIM�E/ ACCEPTEDBYtAFRUATION DATE TIME SAMPLE CONDITtOHS 4 -'7 7•S� � �'3U. ` PA��' `." '!1 � V230 Z`'s� _:✓ hf � r Svc slc OR-iG'INA SAMPLER NAME AND SIGNATURE— a� fD PRINT Name of SAiePLER: ¢j✓/� �,• a m �• 8 " d A o SIGNATURE of PLE DATE Sref[tBtl E A 9mpeawt Now By agrung this form you are woeixrg Paces NET 30 day w=nt Iorms and agreeing to Late charges of 1.5% per month for any paid -Mm 30 ftyve F-ALL-0420rBv.07. 15-iMay-2007 lace Analytical www.pecelab&com December 30, 2014 Mr. Joe Hinkle Allvac RE: Project: BAKERS STORMWATER SW02 Pace Project No.: 92230660 Dear Mr. Hinkle: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 Enclosed are the analytical results for sample(s) received by the laboratory on December 22, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, ,4 a L wr Laura J Cooper taura.cooper@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 laceAnalj6cal" wrrw.psoe7eb3-mm Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER SW02 Pace Project No.: 92230660 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florid a/NE LAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virg inialVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 lacieAnalj6cal" www pecelahs.aom SAMPLE ANALYTE COUNT Project. BAKERS STORMWATER SW02 Pace Project No.: 92230660 Pace Analytical Services, Inc. 9800 Kiocey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92230660001 BAKERS STORMWATER SW02 EPA 2003 SH1 5 PASI-A SM 2540D MDW 1 PASI-A SM 5210B MLS 1 PASI-A SM 5220D EWS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 leAnalyticalo wnvw.pecelabamm ANALYTICAL RESULTS Project: BAKERS STORMWATER SW02 Pace Project No.: 92230660 Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BAKERS STORMWATER Lab ID: 92230660001 Collected: 12/22/14 04:25 Received: 12/22/14 12:30 Matrix: Water SW02 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug1L 1.0 1 12/23/14 15:10 12/23/14 22:33 7440-43-9 Chromium 15.2 ug1L 5.0 1 12/23/14 15:10 12/23/14 22:33 7440-47.3 Copper 142 ug1L 5.0 1 12/23/14 15:10 12/23/14 22:33 7440-50-8 Nickel 8.5 ug1L 5.0 1 12/23/14 15:10 12/23/14 22:33 7440-02-0 Zinc 182 ug1L 10.0 1 12/23/14 15:10 12/23/14 22:33 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 5210E BOD, 5 day BOD, 5 day 5220D COD Chemical Oxygen Demand aFSiafY]kIrl6�ri[lf fifil_1�T' 22.2 mg/L Analytical Method: SM 52108 3.5 mg/L Analytical Method: SM 52200 194 mg1L 6.2 1 12/26/14 17:10 2.0 1 12/23/14 15:45 12/28/14 16:10 25.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 12/30/14 08:30 Page 4 of 12 acMnalytrcal wnrw!pecslebs.cam QUALITY CONTROL DATA Project: BAKERS STORMWATER SW02 Pace Project No.: 92230660 QC Batch: MPRP117612 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92230660001 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 1358768 Matrix: Water Associated Lab Samples: 92230660001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium uglL ND 1.0 12/23/14 21:56 Chromium uglL ND 5.0 12/23/14 21:56 Copper ug1L ND 5.0 12/23/14 21:56 Nickel ug1L ND 5.0 12/23/14 21:56 Zinc ug1L ND 10.0 12/23/14 21:56 LABORATORY CONTROL SAMPLE: 1358769 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug1L 500 462 92 85-115 Chromium ug1L 500 438 88 85-115 Copper ug1L 500 459 92 85-115 Nickel uglL 500 462 92 85-115 Zinc uglL 500 439 88 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1358770 MS 92230489001 Spike Parameter Units Result Conc. Cadmium ug1L ND 500 Chromium ug1L 575 500 Copper uglL 31.9 500 Nickel uglL 193 500 Zinc uglL 392 500 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1358772 MS 92230486001 Spike Parameter Units Result Conc. Cadmium ug1L ND 500 Chromium ug)L ND 500 Copper ug1L 3.2J 500 Nickel ug1L ND 500 Zinc ug1L 4.8J 500 1358771 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 475 460 95 92 70-130 3 500 1010 974 87 80 70-130 4 500 492 466 92 87 70-130 5 500 636 615 89 84 70-130 3 500 816 804 85 82 70-130 2 1358773 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 465 458 93 92 70.130 2 500 437 434 87 87 70-130 1 500 464 457 92 91 70-130 2 500 462 457 92 91 70-130 1 500 442 435 87 86 70-130 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 11:11 AM without the written consent of Pace Analytical Services, Inc.. Qual Qual Page 5 of 12 IeAnalytical to wwwpacefebs.com Project: BAKERS STORMWATER SW02 Pace Project No.: 92230660 QC Batch: WET134994 QC Batch Method: SM 2540D Associated Lab Samples: 92230660001 METHOD BLANK: 1360241 Associated Lab Samples: 92230660001 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: 1360242 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1360243 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 1360244 Parameter Units Total Suspended Solids mg1L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 12/26/14 17:08 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 250 230 92 90-110 92230657001 Dup Result Result RPD Qualifiers 11.1 13.4 19 06 92230718001 Dup Result Result RPD Qualifiers ND ND Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12130/2014 11:11 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 IeAnalytical www.pecelatiLcom QUALITY CONTROL DATA Project: BAKERS STORMWATER SW02 Pace Project No.: 92230660 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: WETI34942 Analysis Method: SM 5210E QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 92230660001 METHOD BLANK: 1358934 Matrix: Water Associated Lab Samples: 92230660001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg1L NO 2.0 12/28/14 16:10 LABORATORY CONTROL SAMPLE: 1358935 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOO, 5 day mg1L 198 184 93 84.5-115.4 SAMPLE DUPLICATE: 1358936 92230700001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg1L 3340 2970 12 D6,H3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 11:11 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 1aceAnalXical avrw.pecelab&wn QUALITY CONTROL DATA Project: BAKERS STORMWATER SW02 Pace Project No.: 92230660 QC Batch: WETAI21408 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92230660001 METHOD BLANK: 1359896 Associated Lab Samples: 92230660001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 1359897 Parameter Units Chemical Oxygen Demand mg1L Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 12130/14 08:30 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 776 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1359898 1359899 MS MSD 92230124003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 223 750 750 932 929 95 94 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1359900 1359901 MS MSD 92229858002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L ND 750 750 768 756 102 101 90-110 2 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 11:11 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 (�15'neAnalytical" www.pecw4com QUALIFIERS Project: BAKERS STORMWATER SW02 Pace Project No.: 92230660 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (827D listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines. unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 11:11 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 laxAnalyfica( www.pftWabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BAKERS STORMWATER SW02 Pace Project No.: 92230660 Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92230660001 BAKERS STORMWATER SW02 EPA 200.7 MPRP117612 EPA 200.7 ICP115865 92230660001 BAKERS STORMWATER SW02 SM 2540D WET134994 92230660001 BAKERS STORMWATER SW02 SM 5210B WET134942 SM 5210B WET134946 92230660001 BAKERS STORMWATER SW02 SM 5220D WETN21408 Date: 12l3012014 11:11 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 coAlkilytical• Sample Condition Upon Receipt Document Number: F-CHR-CS-003-rev.16 Page 1 of 2 _ Issuing Authority: Pace Huntersville Quality Office Client Name: ATZ r'J-A.Is (AMIXf- Courier: ❑ Fed Ex ❑ UPS❑ USPSM Client❑ Commerclal❑ Pace Other Q"OMl M'NrY" M)'`� ``' Custody Seal on Cooler/Box Present: El yes rd no Seals intact: ❑ yes ❑ no R.,};D` a 81tt9t Packing Material: ❑ Bubble V❑p ❑ Bubble Bags ❑ None 4 Other ' et C Thermometer Used: IR Gun T1401 Type of Ice: Blue None Samples an Ice, cooling process has begun Temp Correction Factor T1401 No Correction Corrected Cooler Temp" "2, T •C Temp should be above freezing to VC Biological Tissue Is Frozen: Yes Nola Comments: Date and Initials of.pe son pxamlnlng contents•-rt- Chain of Custody Present: Wes ONO ❑NIA 1. Chain of Custody Filled Out: es ONO ❑NIA 2. Chain of Custody Relln uished: t�(es ❑No ❑NIA 3. Sampler Name & Signature on COC: *es ❑No ONIA 4. Samples Arrived within Hold Time: ges ONO ❑NIA 5. Short Hold Time Anal sis <72hr : pas ONO ❑NIA 6. Rush Turn Around Time Requested: 119'es ❑No ❑NIA 7. Sufficient Volume: Oes ONo ❑NIA 8. Correct Containers Used: -Pace Containers Used: 00es ONO gks ONO El NIA ❑NIA 9. Containers Intact: Oes ONO ❑NIA 10. Filtered volume received for Dissolved tests 06Z ONO ❑NIA 11. Sample Labels match COC: -Includes datelllmellDlAnat sis Matrix: res Ono ❑NIA 12. All containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. exceptions: VOA, colirorm, TOC. O&G,1M-DR0 (water) lees ONO 14ves ONO OYes RO ❑NIA ❑NIA 13, Samples checked for dechlorination: ❑Yes ONO IA 14. Heads ace in VOA Vials >6mm : ❑Yes ONO ' e/A 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # if purchased): ❑Yes 110 ❑Yes I❑No I ❑NIA ?uA 16. Client Notification/ Resolution: Field Date Required? Y 1 N Person Contacted: Datelrime: Comments/ Resolution: SCURF Review: TvvAo Date: I G as 11-1Wo� :..9223066.0 SRF Review: Date: Note: Whenever there is a discrepancy affectingNorth Carolina compliance I samples, a copy of this form will be sent to the North Carolina DEHNR �� 11[11 j I Certification Office (Le out of hold, incorrect preservative, out of temp, 82230680 Incorrect containers) Page 11 of 12 P A CHAIN-Of-CUSTODY 1 Analytical Request Document � n__rf�'. The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed accurately. Section A - Section it Section C. Page of Required Client InfoRnetidn: Required Project Information: Invoice Information: I Repent To• ttentidn- "If If PprrII r f ti j/ Gopy To REGULATORY 'AGENCY G _ Add � ` 30 L74r2 F NPDES F_ GROUNDWATER j DRINKING WATER i UST j RCRA i OTHER Small To: Purchase Order No.: Pace pears FIewo+ce. Fax: ProjeaN— �/�WL's.. Q Site location .SI Lf STATE: Requested Due Dat&rTAT. - Project Number, Par-0 Pro04 - Requested Analysis Filtered (YIN) - - Section D _ - matrix Codes "- c _ - x RoqulreeCFen k0ormatlon MATnlx I ODE_ Dnnking water OW o - -COLLECTED - Preservatives •� _ Water wT oz Waste Water WW u m tsrif Z _ Product P Soig9ow St.} s _ l SAMPLE ID Oil a m x�m (A-Z•o-41:) Air, AR o tu: 0. I- o Sample IDs MUST BE UNSOLIE Ttssue TS O U a- M ' z m Z.• yr a -- - Qttter OT r _ x J r w U m •' - O m ., ~ - - - l -. �. 0. �. - 4• a t�A -ir Q z _ U � Co rn t6 L m m L C a w 0 . a l6rl DATE TIME DATE' TIME rn a 2. z 2 2 Z Z OPace -Jul Project NoJ Lab I.D. 1 e C- i zz3 0 "0 Ov 2 s ) c ,l a . rir7 �c ircJd 2 .i �!•rl 1 s 7 8 9 7o It 12 ADDITIONAL COMMENTS RELINDU D SY t AFFiL1ATiON DATE TIME ACCEPTED BY f AFFILIATION DATE TIME SAMPLE CONDITIONS o Da �+ GFY�4Z3itr L SAMPLER NAME AND SIGNATURE z a e 0 -0 8 5 c PRINT NarnoofSAMPL£ li./!!J�/ e ,fP� E ~ n `-g s V w ✓, E N SIGNATURE of DATE Signed _ 'J i7 - i�4Jt /y / jMMfDDrM: 'Important Note: By &grtirg this form you are accepting Pace's NET 30 day payment tenor mid agreeing la late changes of 1.5% Per mOrYM for f trn—f- pad M.th n 30 days. � 1 -.A „L-'_'uzVrev, V r . z a-May-N- r 1aceAnalyitrcal' www.pecefebs cw December 30, 2014 Mr. Joe Hinkle Allvac RE: Project: BAKERS STORMWATE=R SW03 Pace Project No.: 92230666 Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on December 22, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Laura J Cooper laura.cooper@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac 6 pRO�` REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 aceAnalyrrcal® wwwpacelabs.com Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)8759092 Project: BAKERS STORMWATER SW03 Pace Project No.: 92230666 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 12 IeAnalytioal tiww,pecw4com SAMPLE ANALYTE COUNT Project: BAKERS STORMWATER SW03 Pace Project No.: 92230666 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analyses Reported Laboratory 92230666001 BAKERS STORMWATER SW03 EPA200.7 SH1 5 PASI-A SM 2540D MDW 1 PASI-A SM 5210B MLS 1 PASI-A SM 5220D EWS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 aceAnalytical® www.pwdab.00m ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER SW03 Pace Project No.: 92230666 Sample: BAKERS STORMWATER Lab ID: 92230666001 Collected: 12/22/14 04:45 Received: 12/22114 12:30 Matrix: Water SW03 Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 200.7 MET IC Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium NO uglL 1.0 1 12/23/14 15:10 12/23/14 22:39 7440-43-9 Chromium NO ug1L 5.0 1 12/23/14 15:10 12/23/14 22:39 7440-47-3 Copper 51.3 ug1L 5.0 1 12/23/14 15:10 12123/14 22:39 7440-50-8 Nickel ND ug1L 5.0 1 12/23/14 15:10 12/23/14 22:39 7440-02-0 Zinc 75.8 ug1L 10.0 1 12/23/14 15:10 12/23/14 22:39 7440.66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 11.4 mg1L 2.8 1 12/26/14 17:11 5210E BOD, 5 day Analytical Method: SM 5210B BOD, 5 day NO mg/L 2.0 1 12/23/14 15:45 12/28/14 16:10 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand NO mg/L 25.0 1 12/30/14 08:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 11:12 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 1aceAnalytk wwwpecatebs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER SW03 Pace Project No.: 92230666 QC Batch: MPRP117612 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92230666001 METHOD BLANK: 1358768 Matrix: Water Associated Lab Samples: 92230666001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium ug1L ND 1.0 12/23/14 21:56 Chromium ug1L ND 5.0 12/23/14 21:56 Copper ug1L ND 5.0 12/23/14 21:56 Nickel ug1L ND 5.0 12/23/14 21:56 Zinc ug1L ND 10.0 12/23/14 21:56 LABORATORY CONTROL SAMPLE: 1358769 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Cadmium ug/L 500 462 92 85-115 Chromium ug/L 500 438 88 85-115 Copper ug/L 500 459 92 85-115 Nickel ug/L 500 462 92 85-115 Zinc ug/L 500 439 88 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1358770 1358771 MS MSD 92230489001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD oval Cadmium ugfL ND 500 .500 475 460 95 92 70-130 3 Chromium ugfL 575 500 500 1010 974 87 80 70-130 4 Copper ug1L 31.9 500 500 492 466 92 87 70-130 5 Nickel ug1L 193 500 500 636 615 89 84 70-130 3 Zinc ug1L 392 500 500 816 804 85 82 70-130 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1358772 1358773 MS MSD 92230486001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug1L ND 500 500 465 458 93 92 70.130 2 Chromium ug1L ND 500 500 437 434 87 87 70-130 1 Copper ug1L 3.2J 500 500 464 457 92 91 70.130 2 Nickel ug/L ND 500 500 462 457 92 91 70-130 1 Zinc ug1L 4.8J 500 500 442 435 87 86 70-130 2 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 11:12 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12 aceAnalytical WWW.pacwW t orn QUALITY CONTROL DATA Project: BAKERS STORMWATER SW03 Pace Project No.: 92230666 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: WET134994 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92230666001 METHOD BLANK: 1360241 Matrix: Water Associated Lab Samples: 92230666001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 12/26/14 17:08 LABORATORY CONTROL SAMPLE: 1360242 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 230 92 90-110 SAMPLE DUPLICATE: 1360243 92230657001 Dup Parameter Units Result Result RP❑ Qualifiers Total Suspended Solids mglL 11.1 13A 19 D6 SAMPLE DUPLICATE: 1360244 92230718001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L ND ND Results presented on this page are in the unite indicated by the "Units" cotumn except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12130/2014 11:12 AM without the written consent of Pace Analytical Services, Inc,. Page 6 of 12 (�Iacmnalyficajf" www.pacelabs.00m Project BAKERS STORMWATER SW03 Pace Project No.: 92230666 QC Batch: WET134942 QC Batch Method: SM 5210B Associated Lab Samples: 92230666001 METHOD BLANK: 1358934 Associated Lab Samples: 92230666001 Parameter Units SOD, 5 day mg1L QUALITY CONTROL DATA Analysis Method: SM 5210B Analysis Description: 5210B BOD, 5 day Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 12/28/14 16:10 LABORATORY CONTROL SAMPLE: 1358935 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits SOD, 5 day mg1L 198 184 93 84.5-115.4 SAMPLE DUPLICATE: 1358936 92230700001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mglL 3340 2970 12 D6,H3 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/30/2014 11:12 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 0 aoAnalytical wwwpeoelabs.com QUALITY CONTROL DATA Project: BAKERS STORMWATER SW03 Pace Project No.: 92230666 QC Batch: WETA121408 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92230666001 METHOD BLANK: 1359896 Associated Lab Samples: 92230666001 Parameter Units Chemical Oxygen Demand mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 12/30/14 08:30 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hvntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1359897 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 776 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1359898 1359899 MS MSD 92230124003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 223 750 750 932 929 95 94 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1359900 1359901 MS MSD 92229858002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 750 750 768 756 102 101 90-110 2 Results presented on this page are in the unite indicated by the "Units" column except where an alternate untt Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12l3012014 11.12 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 aceAnalytical' www.pscelabs.00m QUALIFIERS Project: BAKERS STORMWATER SW03 Pace Project No.: 92230666 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilte, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration, Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12I30I2014 11:12 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 acMnalj&al wmpacelebs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BAKERS STORMWATER SW03 Pace Project No.: 92230666 Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92230666001 BAKERS STORMWATER SW03 EPA 200.7 MPRPl17612 EPA 200.7 ICP115865 92230666001 BAKERS STORMWATER SW03 SM 2540D WETI34994 92230666001 BAKERS STORMWATER SW03 SM 5210B WET134942 SM 5210B WET134946 92230666001 BAKERS STORMWATER SW03 SM 5220D WETA/21408 I+FfiaifragI�If���>iC!<iiliF�lul REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 ceAnalyfl alp Sam le Condition Upon Receipt S Document Number: F-CHR-CS-003-rev.15 Client Name: Ci+cl�/,i,� Page 1 of 2 Issuing Authority: Pace Huntersville Quality Office Courier: ❑ Fed Ex ❑ UPS[] USPSO Client❑ Commercial[] Pace Other Custody Seal on CoolerlBox Present: ❑ yes no Seals intact: ❑ yes ❑ no g e 'at !174 -PI- 101111-21 Packing Material: ❑ Bubble IIDp ❑ Bubble Bags ❑ None 10 Other ZPLL Thermometer Used: IR Gun T1401 Type of Ice: et Blue None Samples on Ice, cooling process has begun Temp Correction Factor T1401 No Correction Corrected Cooler Temp.: Z.. •C Temp should be above freezing to TC Biological Tissue Is Frozen: Yes No Comments: Date and Initials of p Mo. examining contents-: rZ re L Chain of Custody Present: 2hs ONO ❑N!A 1. Chain of Custody Filled Out: es ©No ❑NIA 2. Chain of Custodm Relinquished: 50ea ONO ❑N!A 3. Sampler Name & Signature on COC: PQ, ❑No ❑N!A 4. Samples Arrived within Hold Time: es ONO ❑NIA 5. Short Hold Time Analysis <72hr : es ❑No ❑NIA 6. Rush Turn Around Time Requested; es ❑No ❑NIA 7. Sufficient Volume: es ❑No ❑NIA 8. Correct Containers Used: -Pace Containers Used: i'es ONO es ❑No ❑NIA ❑NIA 9. Containers Intact: es ❑No ❑NIA 10. Filtered volume received for Dissolved tests ILpfes ❑No ❑NIA 11. Sample Labels match COC: -includes date/lime/ID/Analysis Matrix: -res ❑No 1 ❑NIA 12. All containers needing preservation have been checked. All containers needing preservation are found to be In compliance with EPA recommendation. exceptions: VOA, colitorm, TOC, O&G, WI�DRO (water) —.6'es ❑No Wes ❑No Dyes ONO ❑N1A ❑N!A 13. Samples checked for dechlorination: Dyes ONO !A 14. Heads ace In VOA Vials >6mm : Dyes ❑No IA 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # if purchased): Dyes 106ho Dyes ONo ❑NIA W1IlA 16. Client Notification) Resolution: Field Data Required? y I IN Person Contacted: DatelTime: i Comments/ Resolution: SCURF Review: Date: �zZ/ SRF Review: Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, incorrect preservative, out of temp, Incorrect containers) (W0f1:92P30666 n911�1191111111111W 1 Page 11 of 12 2ceAnaloical* wwwr.cacelabs.com 4,sA CHAIN -OF -CUSTODY 1 Analytical Request Document The Chainof-CusWdy is a LEGAL DOCUMENT. All relevant fields must be completed accurately. s w G Section A Section 8 Section C. Page: of Required Cliont Information: Required Proje°i UfF°mration: - Invoice Informatiow. %'' - -' - Report To: � A¢e j w + f8 l i A J Jl- i ti� A j A r a _ Copy T°' J ^� , Co r �� REGULATORY AGENCY - AftC F NPDES I GROUNDWATER DRINKING WATER i UST I' RCRA i OTHER Email To: Purchase Order. No.: Pam Duo;e Project N /' {' 1 �03 pxa Pmlea Site LCC2tfGn .s i G� �_ '' STATE: _ Requested Due DatdTAT: - Project Nvmber: Proeb A: Requested Analysis Filtered (YIN) Section D Matxitc Codas r '• -Z I't"Wred Cttaru trdnii�itapon - - - hM,TRix f CooE _ - .. COLLECTED- - ... Preservatives s DnWrlg Water Im- Water WT Waste Water WW m mPOSITE COSTART �ENOIGAAS Product P ., SoiVSofd SL �. .• - .. - p' SAMPLE ID O� " W t°OL (A-Z 0-91;) - Air AR to < z • .a m c Sample IDS MVST BE UNIQUE Issue . TS p o•' - 'w �. U Other OT U- r d U o rn O o } ELn O cr) O O O s Q ~ DATE' TIME .DATE- .TIME _ _ = 2 Z O y Pace Project Nol Lab I.D. w -� �' zz3 V1g&&4V Z�. Lic -r - 4 t' r Ott . e iU -- 4 4:4 1 5 6 6 9 70 ii iz ADDITIONAL COMMENTS 'REUNOU ED BY I AFFILLATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS �. Z; :F r.1 ✓ GJ /2v ok O?IGNAL SAMPLER NAME AND SIGNATURE PRIM Name of SAMPLE.ji' D 1 ' a > } m = DATE Signori SIGNATURE of P J J E o— U a m m r: {MMIDOIYYp �`:7` 00 'tmponara Noce. By sing Mis farm you are 30MV N Pa='s NET 30 day paym m rerun and agree'rrg to late d%ww of 1,5% par mom for a�y rctvoixs J Paid -a- 30 Dys a✓ F-ALL-Q-020rev.07. 7 5-May-ZUL17 (�IacleAnalytical www.paceAgbs.com January 14, 2015 Mr. Joe Hinkle Allvac RE: Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on January 08, 2015, The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Laura J Cooper laura.cooper@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 18 Pace Analytical Services, Inc. aceAnalyticaJ� 9800 KinceyAve. Suite 100 Huntersville, NC 28078 www.pKelableom (704)875-9092 CERTIFICATIONS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Charlotte Certification IDs 9800 KinceyAve. Ste 100, Huntersville, NC 28078 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification M M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 18 le Analytical www.pacefabs.wrn SAMPLE ANALYTE COUNT Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytts Reported Laboratory 92232628001 BAKERS NON CONTACT #1 EPA 1664B CLW 1 PASI-C SM 4500-CI G MAB 1 PASI-A 92232628002 BAKERS NON CONTACT #2 EPA 1664E CLW 1 PASI-C SM 4500-CI G MAB 1 PASI-A 92232628003 BAKERS NON CONTACT #3 EPA 1664B CLW 1 PASI-C SM 4500-Cl G MAB 1 PASI-A 92232628004 BAKERS NON CONTACT #4 EPA 1664E CLW 1 PASI-C SM 4500-CI G MAB 1 PASI-A 92232628005 BAKERS NON CONTACT #5 EPA 1664B CLW 1 PASI-C SM 4500-Cl G MAB 1 PASI-A 92232628006 BAKERS NON CONTACT #6 EPA 1664B CLW 1 PASI-C SM 4500-CI G MAB 1 PASI-A 92232628007 BAKERS NON CONTACT #7 EPA1664B CLW 1 PASI-C SM 4500-CI G MAB 1 PASI-A 92232628008 BAKERS NON CONTACT #8 EPA 1664B CLW 1 PASI-C SM 4500-CI G MAB 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 18 aceAnalytical ' www.pacedahacam ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BAKERS NON CONTACT Lab ID: 92232628001 Collected: 01/07/15 08:30 Received: 01/08/15 17:30 Matrix: Water #1 Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua[ HEM, Oil and Grease Analytical Method: EPA 16646 Oil and Grease NO mglL 5.0 1 01/14/15 08:36 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.14 mglL 0.024 1 01/09/15 14A5 7782-50-5 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/14/2015 03:48 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 18 (� aceAnalytical wwwpecelabs.com ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite t00 Huntersville, NC 28078 (704)875-9092 Sample: BAKERS NON CONTACT Lab IQ: 92232628002 Collected: 01/07/15 09:00 Received: 01/08/15 17:30 Matrix: Water #2 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 01/14/15 08:37 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.027 mg/L 0.024 1 01/09/15 14:15 7782-50-5 H3 Date: 01/14/2015 03:48 PM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 18 1aceAnalytical r`ww.pacelahacom ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BAKERS NON CONTACT Lab ID: 92232628003 Collected: 01/07/15 09:30 Received: 01/08/15 17:30 Matrix: Water #3 Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 01/14/15 08:37 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.059 mglL 0.024 1 01109/15 14:15 7782-50-5 H3 Date: 01/14/2015 03:48 PM REPORT OF LABORATORY ANALYSIS This report shall nat be reproduced, except in lull, without the written consent of Pace Analytical Services, Inc.. Page 6 of 18 aceAnalytical w w.pacefebs.com ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BAKERS NON CONTACT Lab ID: 92232628004 Collected: 01/07/15 09:40 Received: 01/08/15 17:30 Matrix: Water #4 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 01/14/15 08:37 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.24 mg/L 0.024 1 01/09/15 14:15 7782-50-5 H3 Date: 01/14/2015 03:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 18 IeAnalyticals wwwpecalabs com ANALYTICAL RESULTS Pace Analytical Services, tnc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Sample: BAKERS NON CONTACT Lab ID: 92232628006 Collected: 01/07/15 10:00 Received: 01/08/15 17:30 Matrix: Water #5 Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qua] HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 01/14/15 08:38 4500CL G Chlorine, Residual Anatytical Method: SM 4500-CI G Chlorine, Total Residual 0.10 mg1L 0.024 1 01/09/15 14:15 7782-50-5 H3 Date: 01/14/2015 03:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 18 laceAnalyiical xnvw.pacelabxcom ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Sample: BAKERS NON CONTACT Lab ID: 92232628006 Collected: 01/07/15 10:20 Received: 01/08/15 17:30 Matrix: Water 96 Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease NO mglL 5.0 1 01114/15 08:38 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.12 mg1L 0.024 1 01/09/15 14:15 7782-50-5 H3 Date: 01/14/2015 03:48 PM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc., Page 9 of 18 aceAnalytkal® wwwpacelab&oam ANALYTICAL RESULTS Pace Analytical Services, Inc.. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Sample: BAKERS NON CONTACT Lab IQ: 92232628007 Collected: 01/07/15 10:40 Received: 01/08/15 17:30 Matrix: Water #7 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 01/14/15 08:39 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.82 mg1L 0.12 5 01/09/15 14:15 7782-50-5 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 18 leAnalytical wwwpacelahs.com ANALYTICAL RESULTS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BAKERS NON CONTACT Lab ID: 92232628008 Collected: 01/07/15 11:00 Received: 01108/15 17:30 Matrix: Water #8 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg1L 5.0 1 01/14/15 08:39 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.062 mg1L 0.024 1 01/09/15 14:15 7782-50-5 H3 Date: 01/1412045 03:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 11 of 18 (�Iacmnalytical* www.peoelaUctlim QUALITY CONTROL DATA Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Pace Analytical Services, tnc. 980D Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: GCSV120059 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92232628001, 92232628002, 92232628003, 92232628004, 92232628005, 92232628006, 92232628007, 92232628008 METHOD BLANK: 1369584 Matrix: Water Associated Lab Samples: 92232628001, 92232628002, 92232628003, 92232628004, 92232628005, 92232628006, 92232628007, 92232628008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg1L ND 5.0 01/14/15 08:31 LABORATORY CONTROL SAMPLE: 1369585 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 36.0 90 78-114 MATRIX SPIKE SAMPLE: 1369686 35170500002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 5.7 47.6 48.8 90 78-114 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Hate: 01/14/2015 03:48 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 18 ac,Mnalyrlcal o wwwpecelabscom QUALITY CONTROL DATA Project: BAKERS NON CONTACT COOLING Pace Project No.: 922322628 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)87"092 QC Batch: WET135166 Analysis Method: SM 4500-CI G QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual Associated Lab Samples: 92232628001, 92232628002, 92232628003, 92232628004, 92232628005, 92232628006, 92232628007, 92232628008 METHOD BLANK: 1366954 Matrix: Water Associated Lab Samples: 92232628001, 92232628002, 92232628003, 92232628004, 92232628005, 92232628006, 92232628007, 92232628008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chlorine, Total Residual mglL ND 0.024 01/09115 14:15 SAMPLE DUPLICATE: 1366955 92232628001 Dup Parameter Units Result Result RPD Qualifiers Chlorine, Total Residual mglL 0.14 0,14 2 H3 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01114/2015 03:48 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 18 aceAnalj&al° wwwpecelsbaoam QUALIFIERS Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. POL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) OUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration, Acid preservation may not be appropriate for 2-Chloroethylvinyi ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /1412016 03:48 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 18 6 amAnalytrcal www.pecelahs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BAKERS NON CONTACT COOLING Pace Project No.: 92232628 Lab 1D Sample ID QC Batch Method OC Batch 92232628001 BAKERS NON CONTACT#1 EPA 1664E GCSVI20059 92232628002 BAKERS NON CONTACT #2 EPA 1664B GCSV120059 92232628003 BAKERS NON CONTACT #3 EPA 1664B GCSVI20059 92232628004 BAKERS NON CONTACT 04 EPA 1664B GCSV120059 92232628005 BAKERS NON CONTACT #5 EPA 1664B GCSV120059 92232628006 BAKERS NON CONTACT 96 EPA 1664B GCSV120059 92232628007 BAKERS NON CONTACT 07 EPA1664B GCSV120059 92232628008 BAKERS NON CONTACT #8 EPA 1664B GCSV120059 92232628001 BAKERS NON CONTACT #1 SM 4500-Cl G WETl35166 92232628002 BAKERS NON CONTACT #2 SM 4500-CI G WETI35166 92232628003 BAKERS NON CONTACT #3 SM 4500-Cl G VVETI35166 92232628004 BAKERS NON CONTACT #4 SM 4500-CI G WET/35166 92232628005 BAKERS NON CONTACT #5 SM 4500-CI G WETI35166 92232628006 BAKERS NON CONTACT #6 SM 4500-CI G WETI35166 92232628007 BAKERS NON CONTACT #7 SM 4500-CI G WET135166 92232628008 BAKERS NON CONTACT #8 SM 4500-CI G VVET135166 Bate: 01/14/2015 03:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huniersville, NC 28078 (704)875-9092 Analytical Method Analytical Batch Page 15 of 18 .� acoAtkilylfcal' Client Name:_.Ar-r Document Name: Condition Upon Recei� Document Number:, F-CHR-CS-003-rev.16 Document Revised: September *22, ZU1 4 Page 1 of 2 + Issuing Authority: Pace Huntersville Quality Office Courier: ❑ Fed Ex ❑ UPS[] USPS❑ Client❑ Commercial❑ ac Other I .0 CustodySeal on Cooler/Box Present: es, I fib ( W-01 ❑_y ❑ no Seals intact: ❑yes [] no -! F� Packing Material: ❑ Bubble V[]p BBubble Baggy ❑ None ❑: Other_ / Thermometer Used: IR Gun 1401 Type of I6;E Wet 1 Blua None i Q Samples on Ice, cooling process has begun Temp Correction Factor T1401 No Correction g Tissue is Frozen: vas No I Date and Initial of person examining N' pBiological Corrected Cooler Tem.:•C contents: f %J� f `' Temp should be above freezing to VC Comments: Chain of Custody Present: 04, ON. ❑NIA 1. Chain of Custody Filled Out: ' 0'63 ONO ❑NIA 2. Chain of Custody Relinquished: 1 Yea ❑No ❑NIA 3. Sampler Name & Signature on COG: 9jas ON, ❑NIA 4. Samp lee Arrived within Hold Time: t ON, ❑NIA 5. Short Hold Time Analysis <72hr : <� es-T0o Rush Turn Around Time Requested: ❑Yes ©to ❑NIA 7. Sufficient Volume: I34es ❑No ❑NIA g, Correct Containers Used: [Rf es []No ❑NIA 9. -Pace Containers Used: Oyes ONO ❑NIA Containers Intact: es ONO ❑NIA 10. Filtered volume received for Dissolved tests ❑Yes ❑No 131A 11. Sample Labels match COC: 2S es ONO ❑NIA 12. -Includes date/tlmelID/Anal sis Matrix: A!I containers needing preservation have been checked. ❑Yes ❑No 04A 13. Ail containers needing preservation are found to be in ❑yes ❑No MA with EPA recommendation. 624 ON. exceptions: VOA. coliform, TOC, O&G, WI•DRO (water) Samples checked for dechlorination: ❑Yes ONO Dtgk 14, Headspace in VOA Vials >6mm : ❑Yes ONO aA 16, Trip Blank Present: Oyes ONO 71A 16. Trip Blank Custody Seals Present ❑Yea ONO Pace Trip Blank Lot # if purchaseft Client Notification/ Resolution: Field Data Required? Y I N Person Contacted: Datefrime: Comments/ Resolution: SCURF Review: It I Date: SRF Review:1 Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, Incorrect preservative, out of temp, Incorrect containers) Plara.lahpl.hprq WQ, : 92232626, 02232628 Page 16 of 18 CHAIN -OF -CUSTODY 1 Analytical Request Document kQQ ^^ „„ c The Chain -Of -Custody is a LEGAL_ DOCUMENT. AN relevant fields must be completed accuratey. � hhr�r.DaoelaM.com. 07 Section A Section B Section G Page: to Of d Rogvired Client tnformation: Required Pro_jW lnfomTaiion; Invoice Information: Attention: 178215 To: yM� / l f-- " Il Cow � OG �'yi �f E Company ��/Y' �'FC14 ����' REG TORY AGENCY dress• )90?eX .54a-3S %�ilr�•? r NPDES i GROUND WATER s DRINKING WATER Entail To: Purchase Order No.: Pace Rnoto - UST = RCRA - OTHER Ralarcrr: P g. CJy G? -yS P= Project Name: e'rS %l M LG�f C ✓ Pace m Prajecl site Location Requested Duo DaUUTAT: Project Nurnber• - _ P w Prdae s:' 1•'i L� ' .. STATE: /fl+�/ ' Requested Analysis Filtered (YIN) Section D Matrix Codes _ z RoquirodClient Information ' MATRIX I CODE - o • - - COLLECTED - Preservatives - Drinking water OW Water WT - $ cr C) z F Owastew � � � Z} ` � Product arts WIN ±In 00-POSITE START COMPOSITE ENorOzta J ••� O � T S0.40" SL Chi cx $ `� M�J m . SAMPLE ID Uj w (A M 1,} Air AR 58mp1* 10s MUSS T BE UNIQUE Tissue TS Q Q IL a a i`�, � m a d 3 q+ � • N t} C' V m OUher CT X w w Z o m m O= a�.�,��, W C I ca Q1 3% \ `KD \ 4J y ~ — - v4i DATE T[ME DATE TIME rn Z 7 2 = S Z Z .0 O Q .� \ Q [C Pace Project NpJ Lab I.D. I �7 .rG., k/ i�% i:. �,I . 7y I 1.dT /� 1—% 1 �; 31:--. Jtrr 1 I T- 7' a 10 st PrS cc". I - - 9. X crr wiI G - i V nn__ . �'�r1 /t/on (a S 1 car ry 1 � / � J yy�C -1742 ADDMONAL COMMENTS RELINQUISHED BY r AFFILIATION DATE TIME ACCEPTED BY r AFFILIATION DATE TIME SAMPLE CONDITIONS -=t,. Pic{ =1It i3� ;•� SAMPLER NAME AND SIGNATURE U o `a ORIGINAL PRINT Nam* of SAMPLER: � man. E SIGNATURE of SAMPLER m, (M.DD.Y): O/ O / ~ U y -Umonant Note: By signing this form you are aemPWV Pace•S NET 30 day wymcnt lama and agreeny to lam cnargea of 1.5% per mar^ amr inr net Dail wuhn Vday, FALL-"20rev.07, 15-May-2007 00 a .� 'aceAnalytical' ....pxetaEs.cmn CHAIN -OF -CUSTODY 1 Analytical Request Document The Chah-cf-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section 8 Section C Pago: of Required Ole+rt InforTnatkm: Required Project Wo&rkstion: Invoice Information: Com -: /. .i�a� �. RePottTo:....� ttantbn: y^ ^ "837F6 �,-Cl- V Adtlress: n' , C [ic i Copy To: t� P� f n/E�le Company N f s Z,G,r A 2/i2 < - REG TORY AGENCY e III Address'�G11X NPDES I DRINKING WATER = LEST j fiCF2A ! OTHER Email To: Purcft= Order No.: Pecs Quote Rolaronca Ph _ Fax Project N ,s l� �a/� ['a, J.� p Site Location - .. STATE, `--� . Requested Due DatWTAT: - Project Number ; . - _/t.� .. - Paw Praute r.. I I'7i ! ' � l L Requested Analysis Filtered (YIN) Sacfion n Matrix Codes -- x Regtdred merit Womiatim MATRIX ! CME -s �M - COLLECTED Preservatives s __ Drinking Water, DW V O,, Water v✓r WasteMTE Water + PW ,T,Rt �e L� SoiuSofd SL a� 0 SAMPLE ID m� OLL � T 0 (A-Z. 0-91;) Air AR . m 4 z ivo` m SampklDsMUST BEUWQUE Tissue' TS p' 'a m L Other Oi ZE J. - ul tpy ~ DATE TIME DATE. TIME N at D i S 2 Z z M D y \ IY Pace Project NO1 Lab I.D. t err /Uon G 1 G st-- 1 X SG Karl it�onGa G ! X = , s zrJ Qn , WT f7— s o� ���wc 8 Y s 6 ' 7 8 - 9 to _ 11 12 - ADDITIONAL COMMENTS VILINQUISHED BY J AFFILIATION DATE TIME ACCEPTED BY I AFFII.UiT10N DATE/ TI—M]E� "MPLE COND1'i1ON5 ^�' y n fZ r3flif ORIGINALSAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: C r n > �- $ o V U rn V m m SIGNATURE of SAMPLER: DATEAtgnedD/ O7 /� DrM: w.:ars r.ruc: uy 39*4 tns roan you are eaoettnng Pace's NET 30 Eatt payment t=W ace agr Vow g 10 late Chargm of 1.5% Der mvalc>r na ti o,te.e 30 B^r F-ALL-0-020rev.07. tSMay-2007