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NCS000329_MONITORING INFO_20140818
STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. /�CS(�DD LJZy DOC TYPE ❑FINAL PERMIT $--MONITORINGREPORTS-- _ ...._..._.___.._._ __. ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ �,p� ' 0 �j • �u YYYYMMDD August 11, 2014 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files: RECEIVED AUG 18 2014 CENTRAL FILES DWQ180G OATI P.O. Box 5030 2020 Ashcrati Avenue Monroe, NC 281 1 1.5030 Phone: (704) 289-4511 Fax: (704)290-5194 Finail; .j oe.hinkicoo,atimeta Is.com Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and one copy are included. The monitoring data is for the following monitoring schedule - Monitoring Period Sample Number Start I End Year 5 — Period 1 9 March 1, 2014 1 August 31, 2014 Analytical monitoring includes: • Outfall #01 (13), commingled stormwater • Outfall #02 (13), non -commingled stormwater • Outfall #03 (13), non -commingled stormwater • Non Contact Cooling Water #1 - #8 If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sine ely, 4 V� Jo Hinkle Environmental Manager I Allvac - Bakers Plant ATI Allvac Stormwater Monitoring Report Form Sample Date: �`��"�7 Sample Time: _ 'y�li/ij Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Stormwater Discharge Outfall #01 (Commingled Drainage Area = 2. 915,470sq. ft. = 69 acres % Impervious = 34% Xcr 40 CFR fart 136 Parameter Results (mg/l) Benchmark Values (mg/1) BOD 30 COD 120 TSS 100 Cadmium 0.001 Chromium, total recoverable 1 Copper, total recoverable 0.007 Nickel, total recoverable 141D 0.26 Zinc, total recoverable A 0.067 Oil and Grease 20 Temp (effluent) (deg C) n/a Temp (downstream) elez(deg C} n/a Temp (upstream) IV (deg C) n/a Total Residual Chlorine 0.017 PH (std units) 6-9 (std wets) Storm Date: Storm Duration: _ (Hrs.) Inches of Rainfall: � Duration of time preceding rain event exceeding 0.1": (Hrs.) Estimated Flow Calculation: Q = CIA Q(Total) = Q(Pervious Area) + Q(impervious Area) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches rain/ I2inches/ft. x 69 x .34) Q(Total, cfs) = 1.5180 x o�J� (Inches of rain) + 1.7595 x Z P (inches of rain) /) 9/0 g cfs -4 in end A t 3kAT1 Allv,c Allvae - Bakers Plant Stormwater Monitoring Report Form Sample Date: / Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample AnaIvsis: Sample Time: — 6 . e?t��. Stormwater Discharge Outfall #02„(Non-Commingled) Drainage Area = 212 952sa. ft. = 4.9 acres % Impervious = 12% 40 CFR Part 136 Parameter Results (mg/1) Benchmark Values (mg/l) BOD 30 COD 1,33 120 TSS 41�J 100 Cadmium 141D 0.001 Chromium, total recoverable Copper, total recoverable 8 0.007 Nickel, total recoverable • ,1� 0.26 Zinc, total recoverable ' 0.067 pH ` (std units) 0 6-9 (std units) Storm Date: Storm Duration: _l (Hrs.) Inches of Rainfall: Duration of time preceding rain event exceeding 0.1 ": (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) _ (A x inches rain/12 inches/ft. x 4.9 acres x .$$) + 9 x inches rain/12inches/ft. x 4.9 x .12) Q(Total, cfs) = 0.1437 x a 5'' (Inches of rain) + 0.0441 x la?J5 (Inches of rain) -- cfs Jh f -i.! "Y Raja A ve 6. OATI Allvac Allvac - Bakers Plant Stormwater Monitoring Report Form Sample Date: _ / "�S�f7 _ Sample Time: -Z*/) MW Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analvsis: Stormwater Discharge Outfall #03 (Non-Commineled) Drainage Area = 336,5804. ft. = 7.8 acres % Impervious = 15% rl)IIntl ZQA d �- &917�011 Z i'l X'ICr 40 CFR Part 136 Parameter Results (mgtl) Benchmark Values (mgA) BOD / l0 30 COD ,Cf,1� 120 TSS 100 Cadmium A 0.001 Chromium, total recoverable 1 Copper, total recoverable 0.007 Nickel, total recoverable 0.26 Zinc, total recoverable 0.067 pH (std units) 6-9 (std units) Storm Date: -�S / Storm Duration:_ (Hrs.) Inches of Rainfall: Duration of time preceding rain event exceeding 0.1": _ 2y (Hrs.) Estimated Flow Calculation: Q = CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) _ (A x inches rain/l2 inches/ft. x 7.8 acres x .85) + .9 x inches rain/ 12inches/ft. x 7.8 x .15) Q(Total, cfs) = 0.2210 x .j (Inches of rain) + 0.0878 x 0�s (Inches of rain) cfs •! . fl Ali ;p ON j i I'll '�!� .r ; ..:I I�•�:YIj'�;l1 Is: �? Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods Results of Sample Analysis: Allvac - Bakers Plant Stormwater Monitoring Report Form Non -Contact Cooling Wastewater �Q 40 CFR Part 136 ATIAlh Non -Coat Cool.Water Sampling Date Sampling Time Estimated Flow (MGD) Total Res 4m'�)e Temperature pH (std. units) Effluent Downstream U stream p 2 1A1 3 ow3A 6DO-5 5iy � DJ4 CO- 3v, i 79 6 z� a �,92 a 7,,,/ 40 U , , g STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number: NC 'OQ�� or SAMPLES COLLECTED DURING CALENDAR YEAR: A"T Certificate of Coverage Number: NCG (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the so npling results from the laboratory.) FACILITY NAME I COUNTY r PERSON COLLECTING SAMPLE ), ✓'d Ply, : r PHONE NO. 1 CERTIFIED LABORATORY(S) &e2 &2VLab #_ZZl�/4r)ctl�/ j''irJ Lab # Part A: Specific Monitoring Requirements (SIGNATURE OF PERMIiTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. f FSampleI Date CoIlected I' ■ ! 1 1 1 _- 164 WARAMA -. 5 R S Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? — yes Vireo (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow Oil and Grease Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG I MgA I MPA I unit I zavmo Form SWU-246-051100 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date �/t Total Event Precipitation (in hes): 0�5 Event Duration (hours):__ (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possi_biiity of fines and imprisonment for knowing violations." L-J a- (YU 1-JU-41L (Signature of Per ttee) (Date) Form SAU-246-051100 Page 2 of 2 `T a Stormwater Discharge Outfall (SDO) Quailitative Monitoring Report Forguidance on filling out this form, please visit: htw:ilh-3o.enr-state.ne.us/su/Forms Dggurnenmhun#UjsCf0rMS Permit No.: tj1g&61&DI-.�1z11. or Certificate of Coverage No.: N/C/G/ I I I 1 I I Facility Name: County: Insr)ector: Date of Inspection: Time of Inspection: / Total Event Precipitation (inches): 6"?& r 1 No. , 762 Was this a Representative Storm Event? (See information below) � Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed duffing a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0-1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signattje, I certify that this report is accurate and complete to the best of my knowledge: (Signature of 1. Outfall Descrinlion: Outfall No. 'Swo1 Receivinz Stream: Describe the industrial ditch, etc-) J 41 ties that occur within the outfall drainage area: 2. Color: Describe the color of the disco (light, medium, dark) as descriptors: 1'' Al using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (Le., smells strongly of oil, weak chlorine odor, etc.): _4g2Z2e Page 1 of 2 SWU-242-112609 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very c'oudy: 1 2 � 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 0 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 7. ' Is there any foam in the stormwater discharge? Yes . No & Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfali? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 swu 2a2-t 126es 6 Stormwater Discharge ®utfall (SDO) Qualitative Monitoring Report For guidance on filling out this forrn, please visit. htm://h2o.car.sLate.ne.us/su/Forms Documents.bmiftisgforms Permit No.: wcd/ Faciliry Name: County: Inspecto Date of ] _ Time of Inspection: V Total Event Precipitation (inches): v.7 �t of Coverage No.: NIGGI 1 1 1 1 l/ Was this a Representative Storm Event? (See information below) Z Yes ❑ No Please check yourpermit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signattye, I certify that this report is accurate and complete to rbe best of my knowledge: (Signature of Permiti� or Desigae) 1. OutiaR Description: Outfali No. store pe, ditch, etc.) ReceiNinz Stream - Describe the industriaUv�ities that occur within the outfall drainage area: 2. Color: Describe the color of the (light, medium, dark) as descriptors: using basic colors (red, brown, blue, etc.) and tint 3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weals chlorine odor, etc.): _ Z2017 e- Page 1 of 2 sWU-242-1L26D& 4. Clarity: Choose the number which best describes the clarity of the discharge, where l is clear and 5 is very c'oudy: � 1 (2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids- 1 0 3 4 5 6. Suspended Solids; Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 7. Is there any foam in the stormwater discharge? Yes . & Is there an oil sheen in the stormwater discharge? Yes oNo 9. Is there evidence of erosion or deposition at the outfall? Yes (9 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU 242-I12608 Stormwater Discharge Outfall (SD®) Qualitative Monitoring Report Forguidance on filling out this form, please visit: bttp://h2o.enr.state.nc.us/su/For-ms Documents.htm#miscforms Permit No.: NIG,-I Facility Name: County Inspector Date of Inspection: Time of Inspection: Total Event Precipitation (inches): •� of Coverage No.: NIGGI I I I 1 1 I Was this a Representative Storm Event? (See information below) ,['Yes ❑ No Please check your permit to verify if Qualitative Monitoring must he performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 clays) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this sgnatyre, i certify that_this report is accurate and complete to the best of my knowledge: (Signature of Permittior Design) 1. Outfall Description: Outfall No. 4103 Structure (pi e, ditch, etc.) � Receiving Stream: , Describe the industrial acti ties that occur within the outfal] drainage area: f 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: irf IV /i g j .�fO4L) 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak - chlorine odor, etc.): /?j2 j j e Page 1 of 2 S,WU-242-1 I2608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very c'oudy: 1 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids- 1 `J 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? Yes S.J S. Is there an off sheen in the stormwater discharge? Yes (N)o 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SW-242-112609 aceAnalytical ~pscafe6acam July 23, 2014 Mr. Joe Hinkle Allvac RE: Project: Bakers Stormwater BSW01 Pace Project No.: 92209547 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on July 16, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, �_u,l7— L ap,--. Laura J Cooper Iaura.cooper@paceIabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 14 Pace Analytical Services, Inc. aeeAnalytical ® 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 www.pscelabsxam (704)875-9092 CERTIFICATIONS Project: Bakers Stormwater BSW01 Pace Project No.: 92209547 Charlotte Certification IDs 9800 KinceyAve. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification #: 460221 South Carolina Certifcation #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 14 aceAnalyticalo www.paceiab&Mm SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bakers Stormwater BSVV01 Pace Project No.: 92209547 Analytts Lab ID Sample ID Method Analysts Reported Laboratory 92209547001 BSW01 EPA 16648 CLW 1 PASI-C EPA 200.7 JMW 5 PASI-A SM 2540D TEP 1 PASI-A SM 4500-CI G MDW 1 PASI-A SM 5210B MAB 1 PASI-A SM 5220D SMW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 Of 14 Pace Analytical Services, Inc. �l�G/1IlLrlytlCal ® 984D Kincey Ave. Suite 140 IrG iliR Huntersville, NC 28078 www.pacWabs.com (744)875.9492 ANALYTICAL RESULTS Project: Bakers Stormwater BSW01 Pace Project No.: 92209547 Sample: BSW01 Lab ID: 92209547001 Collected: 07/15/14 18:45 Received: 07/16/14 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual Field Data Analytical Method: Collected By TOMMY 1 07/15/14 18:40 LONG & BRANDON LINKER Field pH 8.9 Sid. Units 0.10 1 07115/14 18:40 Field Temperature 27.8 deg C 0.50 1 07/15/14 18:40 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 5.0 1 07/18114 13:01 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug1L 1.0 1 07/18/14 12:50 07/19/14 05:01 7440-43-9 Chromium ND ug1L 5.0 1 07/18/14 12:50 07/19114 05:01 7440.47-3 Copper 12.2 ug1L 5.0 1 07/18/14 12:50 07/19/14 05:01 7440-50-8 Nickel ND ug1L 5.0 1 07/18/14 12:50 07/19/14 05:01 7440-02-0 Zinc ND ug1L 10.0 1 07/18/14 12750 07/19/14 05:01 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 12.0 mg1L 7.1 1 07/22/14 03:28 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.12 mg1L 0.024 1 07/18/14 11:47 7782-50-5 H1 5210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 39.8 mg/L 2.0 1 07/17/14 06:15 07/22/14 01:45 L1 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 75.0 mg1L 25.0 1 07/18/14 23:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:29 AM without the written consent of Pace Anatytical Services, Inc.. Page 4 of 14 aCeARalytical " wwwpecelabsoom QUALITY CONTROL DATA Project: Bakers Stormwater BSW01 Pace Project No.: 92209547 QC Batch: GCSV118268 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92209547001 METHOD BLANK: 1244684 Associated Lab Samples: 92209647001 Parameter Units Oil and Grease mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 07/18/1413:00 Pace Anatytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1244686 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg1L 40 37.9 95 78-114 MATRIX SPIKE SAMPLE: 1244686 92209628001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 36.5 91 78-114 Results presented on this page are In the unkts Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:29 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 14 lacmnalytioalo wnrw.patelebsco n QUALITY CONTROL DATA Project: Bakers Stormwater BSW01 Pace Project No.: 92209547 QC Batch: MPRPI16468 Analysis Method: EPA 200.7 QC Batch Method: EPA200.7 Analysis Description: 2003 MET Associated Lab Samples: 92209547001 METHOD BLANK: 1244780 Matrix: Water Associated Lab Samples: 92209547001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium uglL ND 1.0 07119/14 02:45 Chromium uglL ND 5.0 07119/14 02A5 Copper uglL ND 5.0 07119/14 02:45 Nickel ug1L ND 5.0 07/19114 02:45 Zinc uglL ND 10.0 07/19/14 02:45 Pace Analytical Services, Inc. 9600 Kincey Ave. Suite tD0 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1244781 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug1L 500 481 96 85-115 Chromium ug1L 500 482 96 85-115 Copper ug1L 500 487 97 85-115 Nickel ug1L 500 489 98 85-115 Zinc ug1L 500 471 94 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1244782 1244783 MS MSD 92209172001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qua] Cadmium uglL 2.1 500 500 452 498 90 99 70-130 10 Chromium ug1L 16.1 500 500 494 543 96 105 70-130 9 Copper ug1L 190 500 500 720 792 106 120 70-130 10 Nickel uglL 102 500 500 547 589 89 97 70-130 7 Zinc uglL 6050 500 500 6710 6790 131 148 70-130 1 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1244784 1244785 MS MSD 92209436001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug1L ND 500 500 472 472 94 94 70-130 0 Chromium ug1L ND 500 500 478 479 95 96 70-130 0 Copper ug1L 0.034 500 500 520 523 97 98 70-130 1 mglL Nickel ug1L ND 500 500 481 462 96 96 70-130 0 Zinc ug1L 0.023 500 500 484 483 92 92 70-130 0 mg1L Results presented on this page are In the units indicated toy the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:29 AM without the written consent of Pace Analytical Services, Inc,. Page 6 of 14 aceAnalytical wew.pacelahi.com QUALITY CONTROL DATA Project: Bakers Stormwater BSW01 Pace Project NO.: 92209547 QC Batch: WET132201 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92209547001 METHOD BLANK: 1246458 Associated Lab Samples: 92209547001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 1246459 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 1246460 Parameter Units Total Suspended Solids mg1L SAMPLE DUPLICATE: 1246461 Parameter Units Total Suspended Solids mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 2.5 07/22/14 03:24 Spike LCS Conc. Result 250 226 92209869001 Dup Result Result 273 292 92209553001 Dup Result Result 255 244 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS % ReC % Rec Limits Qualifiers 90 80-120 RPD Qualifiers 7 RPD Qualifiers 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shad not be reproduced, except in full, Date: 07/23/2014 09:29 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 14 aceAnalytical wr wpeoWbs.com QUALITY CONTROL DATA Project: Bakers Stormwater BSW01 Pace Project No.: 92209547 QC Batch: WET132157 Analysis Method: SM 4500-CI G QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual Associated Lab Samples: 92209547001 METHOD BLANK: 1244589 Associated Lab Samples: 92209547001 Parameter Units Chlorine, Total Residual mgJL SAMPLE DUPLICATE: 1244590 Parameter Units Chlorine, Total Residual mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 0.024 07/1811411:47 92209547001 Dup Result Result 0.12 0.12 RPD Qualifiers 1 H1 Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the reeutt. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07123/2014 09:29 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 14 aceAnalytical wwwpecelabacom QUALITY CONTROL DATA • t Pace Ana lyticat Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Project: Bakers Stormwater BSW01 Pace Project No.: 92209547 QC Batch: WET132129 Analysis Method: SM 52108 QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 92209547001 METHOD BLANK: 1243591 Matrix: Water Associated Lab Samples: 92209547001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mgfL ND 2.0 07/22/14 01:45 LABORATORY CONTROL SAMPLE: 1243592 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg1L 198 256 129 84.5-115.4 L0,L1 SAMPLE DUPLICATE: 1243593 92209401001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 12.2 12.2 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:29 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 14 aceAnalytical www.pacelahacam Project: Bakers Stormwater BSW01 Pace Project No.: 92209547 QC Batch: WETA/19630 QC Batch Method: SM 5220D Associated Lab Samples: 92209547001 METHOD BLANK: 1245549 Associated Lab Samples: 92209547001 Parameter units Chemical Oxygen Demand mg1L QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 07/18/14 23:00 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1245550 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 776 103 90-110 MATRIX SPIKE R MATRIX SPIKE DUPLICATE: 1245551 1245552 MS MSD 92208517002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 351 750 750 776 769 57 56 75-125 1 M1 MATRIX SPIKE R MATRIX SPIKE DUPLICATE: 1245553 1245554 MS MSD 92209553001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 133 750 750 549 556 55 56 75-125 1 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:29 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 14 Pace Analytical Services, Inc. aceMalyrlcal • 9800 Kinney Ave. Suite 100 Huntersville, NC 2807878 wwwpecelebs.wrn (704)875-9092 QUALIFIERS Project: Bakers Stormwater BSWO1 Pace Project No.: 92209547 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. M DL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute, LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L1 Analyle recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/23/2014 09:29 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 14 Pace Analytical Services, Inc. ac$Analytical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 WWW. (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Bakers Stormwater BSW01 Pace Project No.: 92209547 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92209547001 BSW01 FLDI 92209547001 BSW01 EPA 1664E GCSV118268 92209647001 8SW01 EPA200.7 MPRP116468 EPA200.7 ICP114872 92209547001 BSW01 SM 2540D WET132201 92209547001 BSW01 SM 4500-CI G WET132157 92209547001 BSW01 SM 52106 WET132129 SM 5210B WET132132 92209547001 13SW01 SM 52201) WETA119630 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07123/2014 09:29 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 14 • Document Name: Document Revised: April 07. 2014 ceArlalytrcal' Sample Condition Upon -Receipt SCUR) Page 1 of 2 Document Number: Issuing Authority: F-CHR-CS-003-rev-14 Pace Huntersville Quality Office Client Name: Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial❑ Other opti0f18i:cr Proj�t`ie - I ` Custody Seal on Cooler/Box Present: El yes ❑ Seals intact: El yes ❑ no�� j �- :Pr�jNar�e; Packing Material: ❑ Bubble Wrap ❑ Bubl�ags ❑ None ❑ Other Thermometer Used: IR Gun T1102 T1L4QA Type of Ice: � Blue None ]'Samples on ice, cooling process has begun Temp Correction Factor T1102: No Correction T1301'. No Correction Corrected Cooler Temp.:„r C Temp should be above freezing to 6°C ii Biological Tissue s Frozen: Yes No NIA 9 Comments: Date and Initi Is of erson examining contents: f (W-e-!i Chain of Custody Present: /❑Yes ❑No ❑NIA 1. Chain of Custody Filled Out: Yes ❑No ❑NIA 2. Chain of Custody Relinquished: ess ❑Na ❑N1A 3. Sampler Name & Signature on COC: Yes ❑No ❑N/A 4. Sam les Arrived within Hold Time: Yes ❑No ❑NIA 5. Short bold Time Analysis <72hr : es ❑No El NIA 6. Rush Turn Around Time Requested: []Yes 5amd--❑NIA 7. Sufficient Volume: -,BYes ❑No ❑NIA 8. Correct Containers Used: -Pace Containers Used: fires 0No Yes ❑No ❑NIA ❑NIA 9. Containers Intact: Yes ❑No ❑NIA 10, Filtered volume received for Dissolved tests ❑Yes ©No A 11. Sample Labels match COC: -Includes date/time/10/Anal sis Matrix: �-C]No ❑NIA 12, All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, ooliform, TOC, O&G, WI-DRO (water) Yes'❑No s No es Ohio ❑N!A ❑N1A 13. Samples checked for dechlorination: ❑Yes ❑No A 14. Headspace In VOA Vials (>6mm): Oyes ❑No A 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (ifpurchased): ❑Yes ONo ❑Yes ❑No ❑WA 16. Client Notification/ Resolution: Field Data Required? Y 1 N Person Contacted: Date/Time: Comments! Resolution: �������� �} ®Tr SCURF Review: M Date: VIA = 922®954? SRF Review: Ok Date: Note: Whenever there is a discrepancy affecting North Carolina compliance y `y samples, a copy of this form will be sent to the North Carolina DEHNR 92209547 - rn Certification Office (Le out of hold, incorrect preservative, out of temp, (if no label available) w incorrect containers) 0 A 0? �/-PkMnalytical` www.o>Icefabs.com CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain-Df-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Paga. of Required Client Information: Required Project Information: Invoice Information: �/ Cornpany: �-[ Report Tv_ Attention: i V c li vVI yyt —70 Vn r Address: a 0 c) I C L✓ n' Copy To: Company Name: ( �WC REGULATORY AGENCY t 1f[r N L Addrus,0. D a rtOln o C r NPDES r GROUND WATER r DRINKING WATER r UST ! RCRA OTHER Email To: Purchase Order No.: Pace Quote Reference: Phone: c Fax: Project Name: is5 Pace,lrPropct Site Location o - S) r r4 r w0 ftana0Per STATE. Requested Duo DMVTAT: Project Number: Paso Prr>Ffe k: Requested Analysis Filtered (YIN) Section O Matrix Codes E z Requiredpient }nrormalion MATRIX !CODE Y o 2 COLLECTED Preservatives 5 DdOing water Dw ;, ° Water WT Waste water VYW I Panosrue o ti Product P SoitlSalid 'aT�irre < cr EONr lUu j s Z SL SAMPLE ID Oil OL L) T Wipe VVP (A-Z. as r .•1 As AR C W J C Sample IOs MUST BE UNIQUE Tissue TS D 0- F m N i S , t r Other OT X O (D Om F A J 7 # V S N O Q H _= Z Q �} d7 to DATE TIME DATE TIME w a T Z `L O v 0 S. Ly Pace Project No./ Lab I.D. i✓O G 7 IS iy :V r Lit 2 ,/D WT % 7l5-1y b'rrilr L7.4 s vtlD WT (- -f5-f4 '.aep i7.4 X a f3 SI-10I C •i5-1V 'r50 17. 5 n WT 1S-IY ; ip- Z7.t X s n tJ 7-Is r 27. 7 s 9 10 11 12 ADDITIONAL COMMENTS 3ELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY ! AFFILIATION DATE TIME SAMPLE CONDITIONS .Z -1 . Lr is nrl �7 `r ��fr�-17 �rcy! k I 1 PH VI A p>4 f, 4 o SAMPLER NAME AND SIGNATURE U .. PRINT Norma of SAMPLER: (� n L, L� ORIGINAL £ m ro o ? g} n m $ 3 U `a E SIGNATURE of SAMPL DATE Signod Si ne (MTE Qnp %mponanl Note: By slgnng this farm you are accepting Pace's NET 30 day paymem terms and agroeing to late charges of t,5% Der month for any invoi q not DaidAkhin 304days. F-ALL-0-020rev.07, 15•May-20'07