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NCS000329_MONITORING INFO_20140306
STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. /�C�60C�Zj2� DOC TYPE El FINAL PERMIT __�..MONITORINGREPORTS__.._......................_......__- ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ 2o1 �• D'y �6 WYYMMDD February 28, 2014 ecovED Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center GENTRP,LFILES Raleigh, NC 27699-1617 OWnjgOG Central Files: 3*ATI Ali.a< P.O. Box 5030 2020 Asheraft Avenue Monroe, NC 281 11-5030 Phone: (704) 289-451 l Fax: (704)290-5194 Email: ioe.hinkleg)atimetals.com Attached, please find stormwater monitoring data for Permit N6-NCS000329. The originals and one copy are included. The monitoring data is for.the following monitoring schedule: Monitoring Period Sample Number I Start I End Year 4 — Period 2 8 1 September 1, 2013 1 February 28, 2014 Analytical monitoring includes: • Outfall #01 (B), commingled stormwater • Outfall #02 (B), non -commingled stormwater • Outfall #03 (B), non -commingled stormwater • Non Contact Cooling Water #1 - #8 If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sincerely, e Hinkle Environmental Manager 1 Allvac - Bakers Plant -OATI Allvac Stormwater Monitoring Report Form Sample Date: ' _ Sample Time: I?, Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Stormwater Discharge Outfall #01 (Comminaled Drainage Area = 2,915,470sq. ft. = 69 acres % Impervious =34% D TinIy Zdna�I r 4 Y6tj ,fi�aac1od 111�cr` 40 CFR Part 136 Parameter Results (mg/1) Benchmark Values (mg/1) BOD Q 30 COD 120 TSS 100 Cadmium 0.001 Chromium, total recoverable 1 Copper, total recoverable 0.007 Nickel, total recoverable 0.26 Zinc, total recoverable 0.067 Oil and Grease 20 Temp (effluent) q� I (deg C) n/a Temp (downstream) 4 v (deg C) D n/a Temp (upstream) 9� (deg C) n/a Total Residual Chlorine ,, 0.017 pH (std units) 6-9 (std units) Storm Date: Storm Duration: 9 (Hrs.) Inches of Rainfall: 0,56 6 r Duration of time preceding rain event exceeding 0.1": YDa (Hrs.) Estimated Flow Calculation: Q = CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) _ (A x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches rain/12inches/ft. x 69 x .34) Q(Total, cfs) = 1.5180 x -5D (Inches of rain) + 1.7595 x __ _Q, 50 �_ (Inches of rain) m fi 0 ATI alvaz Allvac - Bakers Plant Stormwater Monitoring Re ort Form Sample Date: a; ._ _ Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods Results of Sample Analysis: Sample Time: .3:3 i Pry Stormwater Discharge Outfall #02 (Non -Commingled) Drainage Area = 212,952N. ft. = 4.9 acres % Impervious = 12% V �n 2n1y%w 091eul 1vr1 �;11 Xcr 40 CFR Part 136 Parameter Results (mg/1) Benchmark Values (mg/1) BOD o� 3 30 COD �� O 120 TSS 100 Cadmium N� 0.001 Chromium, total recoverable Q116 qi Copper, total recoverable Q J Y5 0.007 Nickel, total recoverable Q, 033 0.26 Zinc, total recoverable Q 0.067 pH s 7 (std units) 6-9 (std units) Storm Date:. —& Storm Duration: � Mrs.) Inches of Rainfall: Duration of time preceding rain event exceeding 0.1": �Y90 (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 4.9 acres x .88) + .9 x inches rain/12inches/ft. x 4.9 x .12) Q(Total, cfs) = 0.1437 x , S0 (Inches of rain) + 0.0441 x 0, s0 (Inches of rain) = 0' 0UI _ cfs fir- 9141, u. 'Ac, f f, OATI al.az Allvac - Bakers Plant Stormwater Monitoring Report Form Sample Date: '- 7 - "T__ _ Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Sample Time: C" Stormwater Discharge Outfall #03 (Non -Commingled) Drainage Area = 336 580sq. ft. = 7.8 acres % Impervious = 15% 'Q�n� `�`�1�rIvJ40 �dcz 44a it tiCa 40 CFR Part 136 Parameter Results (mg(l) Benchmark Values (mg/1) BOD g 30 COD 120 TSS 100 Cadmium 0.001 Chromium, total recoverable /V D 1 Copper, total recoverable O ; 0.007 Nickel, total recoverable610079 0.26 Zinc, total recoverable 0.067 pH 64. 9 (std units) 6-9 (std units) Storm Date: — J " / 7 Storm Duration: �Y (Hrs.) Inches of Rainfall: Q.50 Duration of time preceding rain event exceeding 0.111: �� (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) = (.4 x inches rain/12 inches/ft. x 7.8 acres x .85) + .9 x inches rain/12inches/ft. x 7.8 x .15) Q(Total, cfs) = 0.2210 x , ,5 (Inches of rain) + 0.0878 x a 5L (Inches of rain) — cfs �1 Ki -t ."V r"� SN Lll j": PI I C 'i t Q 'io Fit,, `Jl ;;I ol t. c ATI AM Sample Location: Person Collecting Samples: Laboratory Performing Analysis Analytical Techniques and Methods: Results of Sample Analysis: Allvac - Bakers Plant Stormwater Monitoring Report Form Non -Contact Cooling Wastewater T•41nv11O/) k/76/✓Ylow AVndy/1 ✓�cl PPc JT ac:e 17al �Cal 40 CFR Part 136 Non -Cunt Cool Water Sampling Date Sampling Time Estimated Flow (MGD) Total Res Chlorine (hl) Temperature pH (std. units) Effluent Downstream Upstream I �/sue/ l J .,� !/l� • 1 D Qo� I /�c !I � ° 5 �(/s Llqb , i5 _ 3 . OD 1,10 , LI - :s i o;5-3 576 , DO A),/9 � .1 6 o 1 , D � 9, 9 , 7, / 97 U STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number: NCS06013 --...or or Certificate of Coverage Number: NCG FACILITY NAME 1 14110dl PERSON COLLECTING SAMPLEIS) On a i �cr CERTIFIED LABORATORY(S) Lab ll_(9__ Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: &—'1 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) ,ICOUNTY f �tJ1JPoPc �r PHONE NO. V S (SIGNATURE OF PERMITTEE OR DESIGNEE) By this signature, I certify that this report is accurate complete to the best of my knowledge. Date Sample Collected • �_ i NOW= -� Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? — yes /no (if yes, complete Part B) Part B: Vehicle Maintenance Ac vity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow Oil and Grease Total Suspended Solids pH New Motor Oil Usage mo/dd/ r MG m me unit gavmo Form SWU-246-051100 Page 1 of 2 STORM EVENT CHARACTERISTICS: Date - //-7 ,, Total Event Precipitation (inchp): DaSy Event Duration (hours): r (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): Mail Original and one copy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, includjpg the possibility of fines and imprisonment for knowing violations." -C�9 - l — C4 I-H , (111 j (Si f tare of Permittee) (Date) Form SWU-246-051100 Page 2 of 2 NA N4SrATZ �� aw. Stormwater Discharge Oatfal (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http:llh2o.enr.state.nc.us/su/Forms Docuznmts.htm#n-dSdorms Permit No.: N!I j/Q 1D131�1 `� I or Certificate of Coverage No.: NIGGI 1_ _I_I 1 1 I Facihty Name: L - County: A i nA _ _ Phone No. Inspector. Date of Inspection: :g -1 3 _ Time of inspection: AVS P __-- — Total Event Precipitation (inches): lla.s Was this a Representative Storm Event? (See information below) ,ErYes ❑ No Please check your permit to verify if Qualitative Monitoring must be perforrned during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfaE and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred_ A single storm event may contain up to 10 consecutive hours of no precipitation. By this signat*, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permitt6or Desi ) 1. Outfall Description: 4utfall No. Structure ipe, ditch, etc.) _ 3 Receiving Stream: Describe the industrial ac «ties that occur within the outfall drainage area:Aoirajc- 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: I r I A ±" rro+ - 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 110 Page I of 2 SIVU-242-I 12609 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 (D 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 G 3 4 5 7. Is there any foam in the stormwater discharge? Yes oNo 8. Is there an oil sheen in the stormwater discharge? Yes ON 9. Is there evidence of erosion or deposition at the outf0? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 E WTJ-242-112608 St®rmwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: hU:I/h2o.enr.state.Lic.us/su[Forms DDcumBrns.h=*miscforms Permit No.: N/Ck5/t)14 Facility Name:L County: Inspector. Date of Inspection: Time of inspection: / OkL,2-111 or 4rtificate of Coverage No.: NICIGI I 1 I_I 1 I ,.I a P rr Total Event Precipitation (inches): _ Was this a Representative Storm Event? (See information below) 2,Y—es ❑ No Please check yourpermit to verif if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours Q days) in which no storm event measuring greater than 0.1 inches has occurred_ A single storm event may contain up to 10 consecutive hours of no precipitation. By this signa.41re, I cerdfy that this report is accurate and complete to the best of my knowledge: (Signature of Permit 4 or L GutfaD Description: Outfall No. ijW - Receh ing Stream: Describe the industrial actA-t etc.) r L that occur within the outfall drainage area: .2. Color: Describe the color of the disc arge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: � _{L f D►�l rL _ _ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chioxine odor, etc.)- in One __— Page I of 2 S WU-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 0- 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the storrnwater discharge, where 1 is no solids and 5 is extremely muddy: 1 (2� 3 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes Do IQ. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Paae 2 of 2 5WU-242-112608 Stormwater Discharge Outfail (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: httn://h2o.enr.state.o;.asisulForms Docurroentshtm-rniscforms Permit No.: NlC/S/ 010l 03 lo? I7 I of Certificate of Coverage No.: NIGG/— / / / I 1 I Facility Name: County: _� Inspector. Date of Inspection: Time of Inspection: ,urn. srr Total Event Precipitation (inches): No. Was this a Representative Storm Event? (See information below) Yes ❑ No Please check yourpermit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this siggAture, I certify tkat this report is accurate aQd complete to the best of tuy ImDwledge: (Signature of Permi�eNor 1. Out€all Description: outfap No, 500 Receiving Stream: Describe the industrial acti �t f Aare".. ! oT me Structure (pipe, ditch, etc.) For K= IL 2. Color: Describe the color of the (light, rnadiuni, dazh) as descriptors: _dl+ within the outfall drainage area: f,t a c using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil weak chiorine odor, etc.): A o ll e Page I of 2 5.wi3-242-I 12608 j 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 4 5 a. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 2 4 5 7. Is there any foam in the stormwater discharge? Yes No S. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes (No J 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of poIlutant exposure. These conditions warrant further investigation. . Page 2 of 2 5 WU-242-1 12608 aceAnalytical www.p&celebs.com February 11, 2014 Mr. Joe Hinkle Allvac RE: Project: BAKER STORMWATER SW01 Pace Project No.: 92188821 Dear Mr. Hinkle: Pace Analytical Services, Inc. 9800 Nncey Ave. Suite 100 Huntersvilte, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on February 05, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, M U)4 r� Erin Waters erin.waters@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 14 Pace Analytical Services, Inc. nno��+- lt��m 9800 Kincey Ave. Suite 100 AL+ei rJl!`I Huntersville, NC 28078 wvw.pecalabs.corn (704)875-9092 CERTIFICATIONS Project: BAKER STORMWATER SW01 Pace Project No.: 92188821 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersvil le, NC 28078 FloridalNELAP Certification* E87627 North Carolina Drinking Water Certification M 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification #: 460221 South Carolina Certification M 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 14 aceAnaVkale www.pwwbs.com SAMPLE ANALYTE COUNT Pace Anatytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: BAKER STORMWATER SW01 92188821 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92188821001 BAKERS STORMWATER SW01 GRAB EPA 1664E CLW 1 FASI-C EPA200.7 SH1 5 PASI-A SM 2540D WRC 1 PASI-A SM 4500-CI G AES2 1 PASI-A SM 5210B DAS 1 PASI-A SM 5220D EWS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 14 aceAnalytical. www.pecelahs oom ANALYTICAL RESULTS Project: BAKER STORMWATER SW01 Pace Project No.: 92188821 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BAKERS STORMWATER Lab ID: 92188821001 Collected: 02/04/14 14:58 Received: 02/05/14 17:00 Matrix: Water SW01 GRAB Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Oil and Grease 200.7 MET ICP Cadmium Chromium Copper Nickel Zinc 2540D Total Suspended Solids Total Suspended Solids 4500CL G Chlorine, Residual Chlorine, Total Residual 5210E BOD, 5 day BOD, 5 day 5220D COD Chemical Oxygen Demand Analytical Method: EPA 1664B - ND mg1L 5.0 1 02/06/14 08:45 Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 ND uglL 1.0 1 02/06/14 08:50 02/11/14 11:52 7440-43-9 ND ug1L 5.0 1 02/06/14 08:50 02/09/14 16:52 7440-47-3 18.5 uglL 5.0 1 02/06/14 08:50 02/09/14 16:52 7440.50-8 ND uglL 5.0 1 02/06/14 08:50 02/09/14 16:52 7440-02-0 25.0 uglL 10.0 1 02/06/14 08:50 02/09/14 16:52 7440-66-6 Analytical Method: SM 2540D 8.2 mglL 5.0 1 02/10114 16:13 Analytical Method: SM 4500-Cl G 0.068 mg1L 0,024 1 02/06/14 09:322 7782-50-5 H3 Analytical Method: SM 5210B 3.0 mg1L 2.0 1 02/07/14 07:09 02/11/14 09725 Analytical Method: SM 5220D 33.0 mg1L 25.0 1 02/07/14 13:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 14 aceAnalytical xww.pacelabs.00m Project: BAKER STORMWATER SW01 Pace Project No.: 92188821 QC Batch: GCSVI16595 QC Batch Method: EPA 1664B Associated Lab Samples: 92188821001 METHOD BLANK: 1133931 Associated Lab Samples: 92188821001 Parameter Units Oil and Grease mg/L LABORATORY CONTROL SAMPLE: 1133932 Parameter Units Oil and Grease mg1L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 02/06114 08:39 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 40 37.6 94 78-114 MATRIX SPIKE SAMPLE: 1133933 92188301001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 41.7 40A 88 78-114 Date: 02/11/2014 05:27 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 14 acmnalytica! www..pwelebs.com Project: BAKER STORMWATER SW01 Pace Project No.: 92188821 QC Batch: MPRP115194 QC Batch Method: EPA 200.7 Associated Lab Samples: 92188821001 METHOD BLANK: 1133916 Associated Lab Samples: 92188821001 Parameter Units Cadmium Chromium Copper Nickel Zinc uglL ug1L uglL uglL ug1L QUALITY CONTROL DATA Analysis Method: EPA200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed ND 1.0 0211111411:25 ND 5.0 02/0911416:15 ND 5.0 02/09/1416:15 ND 5.0 02/09/14 16:15 ND 10.0 02109/1416:15 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)8759092 LABORATORY CONTROL SAMPLE: 1133917 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug1L 500 516 103 85-115 Chromium uglL 500 494 99 85-115 Copper ug1L 500 522 104 85-115 Nickel uglL 500 504 101 85-115 Zinc ug1L 500 489 98 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1133918 1133919 MS MSD 92188808001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc, Result Result % Rec % Rec Limits RPD Qual Cadmium ug1L ND 500 500 487 480 97 96 70-130 1 Chromium ug1L ND 500 500 480 486 95 96 70-130 1 Copper ug1L 114 500 500 640 640 105 105 70-130 0 Nickel ug1L 7.9 500 500 480 488 94 96 70-130 2 Zinc ug1L 303 500 500 776 784 95 96 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1133920 1133921 MS MSD 92188777001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cana Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium uglL NO 500 500 516 514 103 103 70-130 1 Chromium uglL 0.53J 500 500 496 488 99 98 70-130 2 Copper ug1L 5.1 500 500 535 532 106 105 70-130 1 Nickel uglL NO 500 500 506 495 101 99 70-130 2 Zinc uglL 195 500 500 693 670 100 95 70-130 3 Date: 02/11/2014 05:27 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 14 (�IacleAnalytical w wwpecelabs.00m Project: BAKER STORMWATER SW01 Pace Project No.: 92188821 QC Batch: WETI29471 OC Batch Method: SM 2540D Associated Lab Samples: 92188821001 METHOD BLANK: 1136199 Associated Lab Samples: 92188821001 Parameter Units Total Suspended Solids mg1L QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 02/10/14 16:08 LABORATORY CONTROL SAMPLE: 1136200 Spike Parameter Units Conc. Total Suspended Solids mg1L 250 SAMPLE DUPLICATE: 1136201 92188644001 Parameter Units Result Total Suspended Solids mg/L 6.9 SAMPLE DUPLICATE: 1136202 Parameter Total Suspended Solids Date: 02/11/2014 05:27 PM Pace Analytical services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS LCS % Rec Result % Rec Limits Qualifiers 248 99 80-120 Dup Result RPD Qualifiers 6.7 3 92188815001 Dup Units Result Result mg1L 44.3 45.3 RPD Qualifiers 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 14 (�IaneAnalytrcal www.pacWb&WM Project: BAKER STORMWATER SW01 Pace Project No.: 92188821 QC Batch: WET129440 QC Batch Method: SM 4500-CI G Associated Lab Samples: 92188821001 METHOD BLANK: 1134928 Associated Lab Samples: 92188821001 Parameter Units Chlorine, Total Residual mg/L SAMPLE DUPLICATE: 1134929 Parameter Chlorine, Total Residual Date: 02/11/2014 05:27 PM QUALITY CONTROL DATA Analysis Method: SM 4500-CI G Analysis Description: 45000L G Chlorine, Total Residual Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.024 02/06/14 09:32 92188325001 Dup Units Result Result mg1L 0.033 0.034 RPD Qualifiers 3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the wriften consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 14 aceAnalytical" www!pecelebacom QUALITY CONTROL DATA Project: BAKER STORMWATER SW01 Pace Project No.: 92188821 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvllle, NC 28078 (704)875-9092 QC Batch: WET129408 Analysis Method: SM 52108 QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 92188821001 METHOD BLANK: 1133903 Matrix: Water Associated Lab Samples: 92188821001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg1L ND 2.0 02/11/14 09:25 LABORATORY CONTROL SAMPLE: 1133904 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mglL 198 173 87 84.5-115.4 SAMPLE DUPLICATE: 1133905 92188706001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mglL 378 339 11 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/11/2014 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 14 aceAnalytical wwwpecefahscom QUALITY CONTROL DATA Project: BAKER STORMWATER SW01 Pace Project No.: 92188821 QC Batch: WETAN7985 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92188821001 METHOD BLANK: 1134191 Associated Lab Samples: 92188821001 Parameter Units Chemical Oxygen Demand mg1L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 02107/1413:30 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1134192 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 736 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1134193 1134194 MS MSO 92188713001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 461 750 750 1050 1060 79 80 75-125 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1134195 1134196 MS MSD 92188710001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 2220 3000 3000 5100 5180 96 99 75-125 2 Date: 02/11/2014 05:27 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 14 aceAnalytrcal® WWW..paoefabtcom QUALIFIERS Project: BAKER STORMWATER SW01 Pace Project No.: 92188821 DEFINITIONS PaceAnalytical Services, Inc. 9B00 KinceyAve. Suite too Hunlersville, NC 28078 (764)B75-9492 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenytamine using Method 8270, The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI•A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/11/2014 0627 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 14 IaclaViAnalyfical (�waW.PacelaUmn QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BAKER STORMWATER SW01 Pace Project No.: 92188821 Lab ID Sample ID 92188821001 BAKERS STORMWATER SW01 GRAB 92188821001 BAKERS STORMWATER SW01 GRAB 92188821001 BAKERS STORMWATER SW01 GRAB 92188821001 BAKERS STORMWATER SW01 GRAB 92188821001 BAKERS STORMWATER SW01 GRAB 92188821001 BAKERS STORMWATER SW01 GRAB Date: 02/11/2014 05:27 PM Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch Method QC Batch Analytical Method EPA 16648 GCSV116595 EPA 200.7 MPRP115194 EPA 200.7 SM 2540D WET129471 SM 4500-CI G WET129440 SM 5210B WETl29408 SM 5210B SM 5220D WETA117985 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch ICP113792 1►i►l�If��'L•1c1.1 Page 12 of 14 l P7C0Atlatylid Condition Upon Receipt JSCILIRPage 1 of 2 Document Number: Issuing Authority: F-CHR-CS-03-revA3 Pace Huntersville Quality Office Client Name: � Z C Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commerciae pace Other Pro f11DiJe,Qate: ".1.':` Custody Seal on Cooler/Box Present: ❑ yes �o Seals intact: ❑ yes ❑ no s"�.f Proj Na`me:� ry . .,.a.. •..,a,.... ,,; it eintii4.aya,::a. Packing Material: ❑ Bubble Wrap ❑ Bubble Bags ❑ NonDWe Other T1 Thermometer Used: IR Gun T1102 01 Type of Ice: Blue None ❑�les on ice, cooling process has begun Temp Correction Factor I 1 3No Correction T1301. No Correction Biological Tissue is Frozen: Yes No NIA Data` d Initia f p r on examining Corrected Cooler Temp.: 'C g c n n Temp should be above freezing to 6'C Comments: Chain of Custody Present: Yes DNo ❑NIA 1. Chain of Custody Filled Out: Yes ❑No ❑NIA 2. Chain of Custody a in uis e s LTNo ❑Niti g, Sampler Name & Signature on COC: 0>6 ❑No ❑NIA 4. Samples Arrived within Hold Time: El>ds ❑No ❑NIA 5, Short Hold Time Analysis f<72hrY Dyes pNo ❑NIA 6. Rush Turn Around Time Requested: ❑Yes ❑No ❑NIA 7. Sufficient Volume: 1KYes ❑No ❑NIA 6. Correct Containers Used: -Pace Containers Used: s ❑No Z'es❑No ❑NIA ©NIA g, Containers Intact: Ye ❑No ❑NIA 10. Filtered volume received for Dissolved tests ifIL11No ❑NIA 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: es ❑No IINIA 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. Yes ❑No ❑No ❑N1A ❑NIA 13. exceptions: VOA, coliform, TOG, 0&G, WI•DRO (water) ❑Yes ❑No Samples checked for dechlorination: ❑ s ❑No ❑N/A 14. Headspace in VOA Vials >6mm : Dyes ONO/ ❑NIA 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # it purchased): ❑Yes ❑Yes [--]No ❑No C)NIA /9NIA 16. Client Notification/ Resolution: Person Contacted: Comments/ Resolution: Field Data Required? Y I N Date/Time: SCURF Reviewl YIM2gate: SRF Review: Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of (his form will be sent to the North Carolina DEHNR Certification Office (i.e out of hold, incorrect preservative, out of temp, incorrect containers) ranei.nere_�_ WO# : 92188521 I II11I�lll��llllllll111 � 92188821 ' Page 13 of 14 G Z.-1'aceAna1Xical' CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. M refevanl fields must be completed accurately. 11111 V. pdG 6lLYS. GOIII Section A Section B Section C Page: of cc Required Client Information: Required Project Information: Invoice Information: Company; Report To: Attention: 1727339 p r1 C.• O Alloy wav! Copy TO: ,� , I Com ! /� REGULATORY AGENCY plop SCOO AT,)e_A[ r NPOES r GROUND WATER r DRINKING WATER UST [- RCRA OTHER Purchase Order No.: Pace Ouo[e Refererroe: P Fax: Project Name: PartePm Site Location STATE: Requested Due Date1TAT: Project Number. Para Pmftle 4: Requested Analysis Filtered (YIN) Section 6 Matrix Codes s r z Required Gient Infornalw MATRIX I CODE S M COLLECTED Preservatives Y Drinkirlq Water DW ffi O o Water WT Waste Water WW U cor,T�wo7tTE w _ Product P s rsnrGaAae Soivsolid SL J L) v SAMPLE ID Oil oL - _ �; H t °' c Wipe WP (A-Z. 0-9 9l;) Air AR w r a C a tu z a- m H a S=plo IDS MUST BE UNIQUE Tissue TS pO U w Other OT `- Z ~ Q. a L m a O U) O O w ~ yCG DATE I TIME DATE I TIME rn a :D _ _ = z z I O Q 1 Pace Project No.! Lab I.D. 1 ers ?*14L2,'_5YN hi I KI I I I I I 00 3 1 -50ol 'T G 1' :L�dfA � X :x `r s �'Nj1a` [f Z i -4-' 3,W,,1^ s r -S W D -- of 'vd1- -, I r s 9 10 11 12 ADDITIONAL COMMENTS ELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY! AFFILIATION DATE TIME SAMPLE CONDITIONS Q 1 o,ec_/ T o1,"SSPM / f X to Aql : 0 eOM 1 1 SAMPLER NAME AND SIGNATURE U o` U z b S ORIGINAL PRINT Name of SAMPLER: Lt� rAjr O 1 o ~ _ Ix ) m U � in SIGNATURE of SATE �� i {MMlDDIYYp •^ 'Important NDW BY SQnulg this fp you are accepting Pace's NET 30 dey payment loans ano Agreeing to Ia:e rhaged of 1-5% per monN'or ah invo"I— i Nrt[hm ylj •� F-ALL-O-020rev.07, 15-May-2007 lacmnalyticalo www.pacekiftoom February 11, 2014 Mr. Joe Hinkle Allvac RE: Project: Bakers Stormwater SW02 Pace Project No.: 92188809 Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Hunlersvitle, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on February 05, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, yG mo Erin Waters erin.waters@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac INC" �o et REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 Pace Analytical Services, Inc. aceAnalytrcal� 9840 Kincey Ave. Suite 140 Huntersville, NC 28078 www Pubs -cm (704)875-9092 CERTIFICATIONS Project: Bakers Stormwater SW02 Pace Project No.: 92188809 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification M M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 Virginia/VEL4P Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page.2 of 12 (� aceAnalj6cal www.pncelabi.com SAMPLE ANALYTE COUNT Project: Bakers Stormwater SW02 Pace Project No.: 92188809 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytts Reported Laboratory 92188809001 Bakers StormwaterSW02 EPA200.7 SH1 5 PASi-A SM 2540D WRC 1 PASI-A SM 5210B DAS 1 PASi-A SM 5220D EWS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 IceAna1jfta1 * www.pecelahi.mm ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bakers Stormwater SW02 Pace Project No.: 92188809 Sample: Bakers Stormwater SW02 Lab ID: 92188809001 Collected: 02/04/14 15:31 Received: 02105/14 17:00 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qua] 200.7 MET 1CP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium NO uglL 1.0 1 02/06/14 08:50 02/11/14 11:44 7440-43-9 Chromium 40.9 ug1L 5.0 1 02/06/14 08:50 02/09/14 16:40 7440-47-3 Copper 245 uglL 5.0 1 02/06/14 08:50 02/09/14 16:40 7440-50-8 Nickel 33.2 uglL 5.0 1 02/06/14 08:50 02/09114 16:40 7440-02-0 Zinc 283 uglL 10.0 1 02/06/14 08:50 02/09/14 16A0 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 122 mg1L 8.3 1 02/10/14 16:12 5210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 2.3 mg1L 2.0 1 02/07/14 07:09 02/11/14 09:25 5220D COD Analytical Method: SM 52200 Chemical Oxygen Demand 28.0 mg1L 25.0 1 02/07/14 13:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, Dale: 02/11/2014 05:28 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 a leAnalytical1 www.pacebb&oem QUALITY CONTROL DATA Project: Bakers Stormwater SW02 Pace Project No.: 92188809 QC Batch: MPRP115194 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92188809001 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 METHOD BLANK: 1133916 Matrix: Water Associated Lab Samples: 92188809001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium uglL ND 1.0 0211111411:25 Chromium uglL ND 5.0 0210911416:15 Copper uglL ND 5.0 0210911416:15 Nickel uglL ND 5.0 02/09/1416:15 Zinc ug1L ND 10.0 0210911416:15 LABORATORY CONTROL SAMPLE: 1133917 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Cadmium uglL 500 516 103 85-115 Chromium ug1L 500 494 99 85-115 Copper ug1L 500 522 104 85-115 Nickel ug1L 500 504 101 85-115 Zinc ug1L 500 489 98 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1133918 MS 92188808001 Spike Parameter Units Result Conc. Cadmium uglL ND 500 Chromium ug1L ND 500 Copper ug1L 114 500 Nickel ug1L 7.9 500 Zinc ug1L 303 500 1133919 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 487 480 97 96 70-130 1 500 480 486 95 96 70-130 1 500 640 640 105 105 70-130 0 500 480 488 94 96 70-130 2 500 776 784 95 96 70-130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1133920 1133921 MS MSD 92188777001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Cadmium ug1L NO 500 500 516 514 103 103 70-130 1 Chromium ug1L 0.53J 500 500 496 488 99 98 70-130 2 Copper ug1L 5.1 500 500 535 532 106 105 70-130 1 Nickel ug1L ND 500 500 506 495 101 99 70-130 2 Zinc ug1L 195 500 500 693 670 100 95 70-130 3 Date: 02/11/2014 05:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qual Qual Page 5 of 12 leAnalytical www.pac&bs.00m QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bakers Stormwater SW02 Pace Project No.: 92188809 QC Batch: WET129471 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92188809001 METHOD BLANK: 1136199 Matrix: Water Associated Lab Samples: 92188809001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 02/10/14 16:08 LABORATORY CONTROL SAMPLE: 1136200 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 250 248 99 80-120 SAMPLE DUPLICATE: 1136201 92188644001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 6.9 6.7 3 SAMPLE DUPLICATE: 1136202 92188815001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 44.3 45.3 2 Date: 02/11/2014 05:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 laceAnaIj4icaI www.pacelabs.com QUALITY CONTROL DATA Project: Bakers Stormwater SW02 Pace Project No.: 92188809 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 1 OD Huntersville, NC 28078 (704)875-9092 QC Batch: WET129408 Analysis Method: SM 52108 QC Batch Method: SM 5210E Analysis Description: 5210B BOD, 5 day Associated Lab Samples: 92188809001 METHOD BLANK: 1133903 Matrix: Water Associated Lab Samples: 92188809001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg]L ND 2.0 02/11/14 09:25 LABORATORY CONTROL SAMPLE: 1133904 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg1L 198 173 87 84.5-115.4 SAMPLE DUPLICATE: 1133905 92188706001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 378 339 11 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02111/2014 05:28 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 (�55'aeAnalj&,al$ wxwpacef&b&wm QUALITY CONTROL DATA Project: Bakers Stormwater SW02 Pace Project No.: 92188809 QC Batch: WETAI17985 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 52200 COD Associated Lab Samples: 92188809001 METHOD BLANK: 1134191 Associated Lab Samples: 92188809001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 1134192 Parameter Units Chemical Oxygen Demand mglL Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 02/0711413:30 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 736 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1134193 1134194 MS MSD 92188713001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 461 750 750 1050 1060 79 80 75-125 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1134195 1134196 MS MSD 92188710001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 2220 3000 3000 5100 5180 96 99 75-125 2 Date: 02/11/2014 05:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 12 lacmnalyfical* www.pacefebs.com QUALIFIERS Project: Bakers Stormwater SW02 Pace Project No.: 92188809 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02111 /2014 05728 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 laneAnalyfical" www.paoelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Bakers Stormwater SW02 Pace Project No.: 92188809 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92188809001 Bakers Stormwater SW02 EPA 200.7 MPRPI15194 EPA 200.7 ICPI13792 92188809001 Bakers Stormwater SW02 SM 2540D WETI29471 92188809001 Bakers Stormwater SW02 SM 5210B WET129408 SM 5210B WETI29437 92188809001 Bakers Stormwater SW02 SM 5220D VVETAl17985 Date: 02/11/2014 05:28 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 �d Sample Condition Upon Receit SCUR uVVM V V Page 1 oft . •�7ceAnr�ly�iG3f • Document Number: Issuing Authority: F-CHR-CS-03-rev.13 Pace Huntersville Quality Office I Client Name: C, Courier: ❑ Fed Ex ❑ UPS❑ l.1SPS❑ Client❑ Comma vial❑ Pace Other Custody Seal on Cooler/Box Present: ❑ yes �6 no Seals intact: ❑ yes ❑ no RTo1 s �Ue Date r' ` « Packing Material: ❑ Bubble Wrap ❑ Bubble Bags Ej'� None ❑ Other Thermometer Used: IR Gun T1102 T 30 Type of Ice;-W Blue None El samples on ice, cooling process has begun Temp Correction Factor T1102: No Correction T4(6. No Correction / 1 Biological Tissue tS Frozen: Yes No NIA Date an In�aog Corrected Cooler Temp.: C g conton Temp should be above freezing to 6° Comments: i r Chain of Custody Present: Yes ❑No ❑NIA 1, Chain of Custody Filled Out: Xes ❑No ❑NIA 2. r�hnin Af r.1letnriv w inm iic a • ri4z r7gf irwr Sampler Name & Signature on COC: CTYes ❑No ❑NIA 4. Samples Arrived within Hold Time: es ❑No ❑NIA 5. 6 Short Hold Time Analysis <72hr): pygs ❑No ❑NIA 6. Rush Turn Around Time Requested: ❑Yes 16No ❑NIA 7. Sufficient Volume: R4s ❑No ❑NIA 8. Correct Containers Used: xfYes ©No ❑NIA g. -Pace Containers Used: OYe ❑No ❑NIA Containers Intact: Yes ❑No J21NIA 10. Filtered volume received for Dissolved tests ❑Yes ❑No ❑NIA 11. Sample Labels match COG: ❑Yes ❑No ONIA 12, -Includes date/time/ID/Analysis Matrix: All containers needing preservation have been checked. /Comes ❑No ❑N1A 13. All containers needing preservation are found to be in 9 "s ❑No ❑N/A compliance with EPA recommendation. exceptions: VOA, colitorm,TOC,O&G,WI•DRO(water) ❑Yes ❑No Samples checked for dechlorination: ❑ s ❑No ❑N/A 14, Headspace in VOA Vials (>6mm): Yes ❑No ❑NIA 15. ,Trip Blank Present: [--]Yes ❑No 4�11A 16. Trip Blank Custody Seals Present ❑Yes ❑No ❑NIA ` Pace Trip Blank Lot ff (if purchasedl. Client Notification/ Resolution: Field Data Required? Y I N Person Contacted: Datef ime: Comments/ Resolution: samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, incorrect preservative, out of temp, incorrect containers) wo# : 92188809 If I1I111111If11luIInII i Page 11 of 12 . _2 i aceAr�alytical' e.lat. ,..,m CHAIN -OF -CUSTODY 1 Analytical Request Document The Chairs -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C cc Pape: of EL Required Client Information; Required Project Information: Invoice Information: �a ` Company: I� Report To' Attention: 1/ 4 O �� { /I Jed (Q CopyTo:� �L ,t Compa n Ne:._r REGULATORY AGENCY Addressp n j,0.50 flrlrCt r NPDES r GROUNDWATER r DRINKING WATER ('" UST j— RCRA I OTHER mail To: Purchase Order No.. Pace Quote Reference, ' .. Fax: Project Name: } I Pars Project Site Location - [�r Manager. STATE. Requested Due DatWTAT: f rvjeu Number: Papa Prohte -: Requested Analysis Filtered (YIN) Section D Matrix Codas 8 y z Regrtired Chent tnformetiurn MATRIX I CODIF a COLLECTED Preservatives } Dnrddng Water DIN g OU z Water VY7 Water WW WasteTART m TE O t Produt P .� SCL4.IPt�rr£ ENDGRAn W Z SoiYSofd SL SAMPLE ID WIIpe w°LP - " UJ � s g t Sample IDs MUST BE UNIQUE Tits" TS O a. m of Z Other OT O r rz m g a a LL @p'Q = D r y C t a In I DATE TIME DATE T1ME t`too 4& 0 zxzzZo a C Pace Project No.1 Lab LD- 1 1 l O _1 0i rK2—` i !� -1{-(qf :3 .•1 1 Xis � s 7 B 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION DATE TIME SAMPLE CONDMONS % low;.• :� <.� 9> o--!v al-h o17 -5 11A 7 sa SAMPLER NAME AND SIGNATURE rJ E ro ORIGINAL PRINT Name of SAMPLER.l - Z � 1. SIGNATURE of SAM F.. (MldlDDdi 9-1 lYY)_ U U to N -Inponanl Note: by signing Un form you are accepting Pace's NET 30 day payment tents enci agreeing to late charges of 1.5% per mon:tt 8.4:- nib n4. F-ALL-0-020rev.07, 15-May-2007 1aceAnalytical www.p9ce18bacom February 11, 2014 Mr. Joe Hinkle Allvac RE: Project: Bakers Stormwater SW03 Pace Project No.: 92188808 Dear Mr. Hinkle: Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 2BO78 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on February 05, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, m u,)n� Erin Waters erin.waters@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac NCCR,16/ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 12 aceAnalytical wwpecefebs.00m Project: Bakers Slormwater SW03 Pace Project No.: 92188808 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 12 laceAnalyfical* www.pacefabs.cw SAMPLE ANALYTE COUNT Project: Bakers Stormwater SW03 Pace Project No.: 92188808 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 A nalytes Lab ID Sample ID Method Analysts Reported Laboratory 92188808001 Bakers Stormwater SW03 EPA 200.7 SH1 5 PASI-A SM 2540D WRC 1 PASI-A SM 5210E DAS 1 PASI-A SM 5220D EWS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 12 aeeAnalytical"P xww.pecalahs.oan ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bakers Stormwater SW03 Pace Project No.: 92168808 Sample: Bakers Stormwater SW03 Lab ID: 92188808001 Collected: 02/04/14 15:40 Received: 02/05/14 17:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug1L 1.0 1 02106/14 08:50 02/11/14 11:32 7440-43-9 Chromium ND ug1L 5.0 1 02/06/14 08:50 02/09/14 16:31 7440-47-3 Copper 114 ug1L 5.0 1 02/06/14 08:50 02/09/14 16:31 7440-50-8 Nickel 7.9 ug1L 5.0 1 02/06/14 08:50 02/09/14 16:31 7440-02-0 Zinc 303 ug1L 10.0 1 02/06/14 08:50 02/09/14 1631 7440-66-6 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 16.3 mg1L 2.5 1 02/10/14 16:11 6210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 5.8 mglL 2.0 1 02/06114 14:48 02111114 12:30 L2 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 107 mglL 25.0 1 02107/14 13:30 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in lull, Date: 02/11/2014 04:47 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 12 aceAnalytical wmPacelabLcom QUALITY CONTROL DATA Project: Bakers Stormwater SW03 Pace Project No.: 92188808 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: MPRP115194 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92188808001 METHOD BLANK: 1133916 Matrix: Water Associated Lab Samples: 92188808001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium ug/L ND 1.0 0211111411:25 Chromium ug1L ND 5.0 0210911416:15 Copper ug/L ND 5.0 02/09/1416:15 Nickel ug1L ND 5.0 0210911416:15 Zinc ug1L ND 10.0 02/0911416:15 LABORATORY CONTROL SAMPLE: 1133917 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug1L 500 516 103 85-115 Chromium ug/L 500 494 99 85-115 Copper ug/L 500 522 104 85-115 Nickel ug1L 500 504 101 85-115 Zinc ug/L 500 489 98 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1133918 MS 92188808001 Spike Parameter Units Result Conc. Cadmium ug/L ND 500 Chromium ug/L ND 500 Copper ug1L 114 500 Nickel ug/L T9 500 Zinc ug/L 303 500 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1133920 MS 92188777001 Spike Parameter Units Result Conc. Cadmium uglL ND 500 Chromium ug1L 0.531 500 Copper ug1L 5.1 500 Nickel uglL ND 500 Zinc ug/L 195 5o0 Date: 02/1112014 04:47 PM 1133919 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 487 480 97 96 70-130 1 500 480 486 95 96 70-130 1 500 640 640 105 105 70-130 0 500 480 488 94 96 70-130 2 500 776 784 95 96 70-130 1 1133921 MSD Spike MS MSD MS MSD % Rec Conc, Result Result % Rec % Rec Limits RPD 500 516 514 103 103 70-130 1 500 496 488 99 98 70-130 2 500 535 532 106 105 70-130 1 500 506 495 101 99 70-130 2 500 693 670 100 95 70-130 3 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qual Qual Page 5 of 12 aceAnalyticalo www.pec&Wbs.com QUALITY CONTROL DATA Project: Bakers Stormwater SW03 Pace Project No.: 92188808 Pace Anatytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: WET129471 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92188808001 METHOD BLANK: 1136199 Matrix: Water Associated Lab Samples: 92188808001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 02/10/14 16708 LABORATORY CONTROL SAMPLE: 1136200 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 248 99 80-120 SAMPLE DUPLICATE: 1136201 92188644001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 6.9 6.7 3 SAMPLE DUPLICATE: 1136202 92188815001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 44,3 45.3 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/11 /2014 04:47 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 12 aceAnalytical® wwMpecelaftco n Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Bakers Stormwater SW03 Pace Project No.: 92188808 QC Batch: WET129418 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210E GOD, 5 day Associated Lab Samples: 92188808001 METHOD BLANK: 1134290 Associated Lab Samples: 92188808001 Parameter Units GOD, 5 day mglL LABORATORY CONTROL SAMPLE: 1134291 Parameter Units GOD, 5 day mg1L SAMPLE DUPLICATE: 1134292 Parameter GOD, 5 day Date: 02111/2014 04:47 PM Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 02/11/1412:30 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 148 75 84.5-115.4 LO 92188808001 Dup Units Result Result mglL 5.8 5.8 RPD Qualifiers 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 12 aceAnalytical wwwPe0ald11&WM Project: Bakers Stormwater SW03 Pace Project No.: 92188808 QC Batch: WETA117985 OC Batch Method: SM 5220D Associated Lab Samples: 92188808001 METHOD BLANK: 1134191 Associated Lab Samples: 92188808001 Parameter Units Chemical Oxygen Demand mglL LABORATORY CONTROL SAMPLE: 1134192 Parameter Units Chemical Oxygen Demand mg1L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 25.0 0210711413:30 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 736 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1134193 1134194 MS MSD 92188713001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 461 750 750 1050 1060 79 80 75-125 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1134195 1134196 MS MSD 92188710001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc, Result Result % Rec % Rec Limits RPD Oual Chemical Oxygen Demand mg/L 2220 3000 3000 5100 5180 96 99 75.125 2 Date: 02/11/2014 04:47 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc,. Page 8 of 12 aceAnalytical wwiw.pacelahs.com QUALIFIERS Project: Bakers Slormwater SW03 Pace Project No.: 92188808 [DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyle is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville ANALYTE QUALIFIERS LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/11/2014 04:47 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12 IeAnalytical. www.pecelab3.Wm QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Bakers Stormwater SW03 Pace Project No.: 92188808 Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92188808001 Bakers Stormwater SW03 EPA 200.7 MPRP115194 EPA 200.7 ICP113792 92188808001 Bakers Stormwater SW03 SM 2540D WET129471 92188808001 Bakers Stormwater SW03 SM 5210B WET129418 SM 5210B WET129420 92188808001 Bakers Stormwater SW03 SM 5220D WETA117985 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02f 1112014 04:47 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 12 Sampler X"" /Alcr.Atolyfrcal' Sample Condition Upon Receipt (SCUR) Page 1 of Document Number: Issuing Authority: F-CHR-CS-03-rev.13 Pace Huntersville Quality Office Client Name: Courier: ❑ Fed Ex ❑ UPS❑ LISPS❑ Client❑ CommerciaK Pace Other O tional :.:, • :�•_:>:...:•; L'[ ❑ no Proi' DuetQater 4z J� 4 Custody Seal on CoolerlBox Present: ❑ yes no Seals intact: ❑ yes S PNt' Name::;,, Packing Material: ❑ Bubble Wrap ❑ Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1102 ol 01 Type of Ice:--ee Blue None ❑-Samples on ice, cooling process has begun Biolo ical Tissue is Frozen: Yes No NIA Date and initials of pe on examining Corrected Cooler Temp.: C g cone Temp should be above freezing to 6°C Comments: Chain of Custody Present: Yos ONO ❑NIA 1. Chain of Custody Filled Out: ids ❑No ❑NIA 2. I Name 8 Signature on COC: .wes ❑No ❑N1A 4. Samples Arrived within Hold Time: Y s ❑No ❑N1A 5. Short Hold Time Analysis <72hr): Yes ❑Na ❑N!A B. Rush Turn Around Time Requested: Dyes dNo ❑N!A 7. Sufficient Volume: es ❑No ❑N1A g, Correct Containers Used: -Pace Containers Used: 'p4es ❑No es ❑No ❑N!A ❑NIA j. Containers Intact: Yes ❑No ❑N!A 10, Filtered volume received for Dissolved tests Dyes ❑No l3 IA 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: ❑�w ❑No ❑NIA 12. All containers needing preservation have been chocked. exceptions: VOA, coGforrn, TOC, OE,G, VJf-SRO (water) Yes ❑No Samples checked for dechlorination: ❑Y ❑No ❑NrA 14. Headspace in VOA Vials >6mm : Yos ❑No ,15. Trip Blank Present: Dyes ❑No VWIA 16. Trip Blank Custody Seals Present Dyes ❑No ❑NIA Pace Trip Blank Lot # it purchased): Client Notification! Resolution: Field Data Required? Y 1 N Person Contacted: Date/Time: Comments) Resolution: SCURF Review: �t � Date: _ . __P_Yara lahPl.hpra._ _ .V SRF Review: Date: t W®# . 92188V08 I Note: Whenever there is a discrepancy affecting North Carolina compliance � samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e out of hold, incorrect preservative, out of temp, I 11 I 1 incorrect containers) 92186$08 Page 11 of 12 G �.- aceAnalytical' CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Page: of Section A Section S Seetlon C Required Client information: Required Pruiect Information: Invoice Information: ry y Company:. Report To: Attention: 1727347 Add Copy To: ��� r Company Name' / ,`G f REGULATORY AGENCY Address f} `t f r V dh� I NPDES r GROUND WATER r DRINKING WATER r UST iW RCRA (" OTHER Email To: Purchase Order No.: Pace Ouote Rrteren�. q Fax: Project Name Pace Praha Site Location STATE: Requested Due DaterPAT: Project Number: Pace Profile 4: Requested Analysis Filtered (YIN) Section 1) Matrix Codes a Z Requlrwcliem Intormaton MATRIX r CODE a COLLECTED Pressrvatives Y` Drinking Water DW O L) Water WT Wastewater WW a 6 d] COMI'05nE COMPOWTE o U Prmuct P y START FAYGRA9 Z SoYSolid SL q y } SAMPLE ID Oa OL 0) y Wipet WP (A-Z. 0-91:) Air AR OO a a z �• O Sample IDs MUST BE UN:QUE Tissue TS C- M o a 1 = U Diner OT U X w r LU Z 0 Z m C N a w p c O O ~ 0DATE S 2 Z O y d` Pace Proj d NOJ Lab I.D. THE DATE`/ iIME 2 Z y 2 + I -i :, ;vf .y 3 , g y-! 5 6 7 8 9 10 11 12 ADDITIONAL COMMENTS IJNQUISI1icD BY t AFFILIATION DATER ACCEPTED BY 1 AFFILL4TION DATE TIME SAMPLE CONDITIONS I -/ `So PM SAMPLER NAME AND SIGNATURE U § m ` v ORIGINAL PR1NTNaRNofSAMPLER:�� (�1 �� L. ! �_ � Z o 4 o o 0 > as renrle m DATE Signed SIGNATURE of SAM L 9 `-5 `/T m ¢ U w E (MMIDDtYY): N rn -imponant Note: By sigrong tnia form you are aooep" Pdce'S NET 30 day payment temp and sgreevg w late charges of 1.5% per m9atlr fo Ayr na aa;� wi�in'3b al s�f F-ALL-"20rev.07, 15-May-2007 (�Iacmnalyticalo wrvw.pacefa6s.cavn January 22, 2014 Mr. Joe Hinkle Allvac Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 RE: Project: Bakers Non Contact Cooling Pace Project No.: 92186793 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on January 16, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, m I. wta Erin Waters erin.waters@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 18 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. mA _�I�^'� 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 ca Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 www.pacelahscom (336)623-8921 (828)254-7176 (704)875-9092 CERTIFICATIONS Project: Bakers Non Contact Cooling Pace Project No.: 92186793 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 FloridalNELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification* 357 North Carolina Wastewater Certification #: 12 VirginiaNELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 as REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in Full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 18 7 c Pace Analytical Services, Inc. Pace Analytical Services, Inc. A,y __Iir'1� 205 East Meadow Road - Suite A 2225 Riverside Dr. m ica Eden, NC 27288 Asheville, NC 28804 www,peceobs.com (336)623-8921 (828)254-7176 SAMPLE ANALYTE COUNT Project: Bakers Non Contact Cooling Pace Project No.: 92186793 Pace Analytical Services, Inc. 980o Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 A nalytes Lab ID Sample ID Method Analysts Reported Laboratory 92186793001 Bakers Non Contact #1 EPA 1664B CLW 1 PASI-C SM 4500-CI G AES2 1 PASI-A 92186793002 Bakers Non Contact#2 EPA 1664E CLW 1 PASI-C SM 4500-CI G AES2 1 PASI-A 92186793003 Bakers Non Contact #3 EPA 1664B CLW 1 PASI-C SM 4500-CI G AES2 1 PASI-A 92186793004 Bakers Non Contact #4 EPA 1664E CLW 1 PASI-C SM 4500-CI G AES2 1 PASI-A 92186793005 Bakers Non Contact #5 EPA 1664B CLW 1 PASI-C SM 4500-CI G AES2 1 PASI-A 92186793006 Bakers Non Contact #6 EPA 1664B CLW 1 PASI-C SM 4500-CI G AES2 1 PASI-A 92186793007 Bakers Non Contact #7 EPA 1664B CLW 1 PASI-C SM 4500-Cl G AES2 1 PASI-A 92186793008 Bakers Non Contact #8 EPA 1664B CLW 1 PASI-C SM 4500-CI G AES2 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 18 Pace Analytical Services, Inc. Pace Analytical Services, Inc. leac, Analytical 205 East MeadoEden NC 27288 Ashevile,, NC 128804 www.pecerebs oom (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Bakers Non Contact Cooling Pace Project No.: 92186793 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Bakers Non Contact #1 Lab ID: 92166793001 Collected: 01/15/14 09:50 Received: 01/16/14 16:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 01/21/14 14:06 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.57 mg/L 0.024 1 01/21/14 13:56 7782-50-5 H3 Date: 01/22/2014 01:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 18 Iac ( e Analytic@ wwwpscelab.com Project: Baker Pace Project No.: 92186 Sample: Bakers Non Con Parameters HEM, Oil and Grease Oil and Grease 4500CL G Chlorine, Restd Chlorine, Total Residual Date: 01/22/2014 01:54 PM Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ® 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave, Suite 1 OD Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS s Non Contact Cooling 793 tact #2 Lab ID: 92186793002 Collected: 01/15114 10:10 Received: 01/16/14 16:20 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 1664B ND mg/L 5.0 1 01121/1414:07 ual Analytical Method: SM 4500-CI G 0.15 mg1L 0.024 1 01/21/14 14:09 7782-50-5 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc,. Page 5 of 18 Pace Anatytical Services, Inc. Pace Analytical Services, Inc. leac,Analytical 205 East Meadow Road - Suite A 2225 Riverside Dr, Eden, NC 27288 Asheville, NC 28804 www.pecwabi.corn (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Bakers Non Contact Cooling Pace Project No.: 92186793 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)B75-9092 Sample; Baker; Non Contact #3 Lab ID: 92186793003 Collected: 01/15/14 10:20 Received: 01/16/14 16:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 01/21/14 14:07 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.14 mg/1- 0.024 1 01/21/14 14:22 7782-50-5 H3 Date: 01/22/2014 01:54 PM REPORT OF LABORATORY ANALYSIS This report shati not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 18 lacmnalyfical" wnnvpecelahacom Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7178 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bakers Non Contact Cooling Pace Project No.: 92186793 Sample: Bakers Non Contact #4 Lab ID: 92186793004 Collected: 01/15/14 10:35 Received: 01116I14 16:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease 52.7 mg/L 5.0 1 01121/14 14:08 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.50 mg/L 0.024 1 01/21/14 14:56 7782-50-5 H3 Date: 01/22/2014 01:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 18 Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceMalXical* 205 East MeadowEden, NC 27 BB Asheville, NC 28804 WWW.P J8bS.WM (336)623.8921 (828)254-7176 ANALYTICAL RESULTS Project: Bakers Non Contact Cooling Pace Project No.: 92186793 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Sample: Bakers Non Contact #5 Lab ID: 92186793005 Collected: 01/15/14 10:50 Received: 01/16/14 16:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, 011 and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 01/21114 14:08 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.064 mg/L 0.024 1 01/21114 15:05 7782-50-5 H3 Date: 01/22/2014 01:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc,. Page 8 of 18 Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalytical ® 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 www.p&cWabs.cem (336)62M921 (828)254-7176 ANALYTICAL RESULTS Project: Bakers Non Contact Cooling Pace Project No.: 92186793 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Bakers Non Contact 96 Lab IQ: 92186793006 Collected: 01/15/14 11:05 Received: 01116/14 16:20 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 01/21114 14:08 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.042 mg1L 0.024 1 01/21/14 16:18 7782-50-5 H3 Date: 01/22/2014 01:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, inc.. Page 9 of 18 Pace Analytical Services, Inc. Pace Analytical Services, Inc. ® 205 East Meadow Road - Suite A 2225 Riverside Dr. aceMalytrcal Eden, NC 27288 Asheville, NC 28804 www.p&Wabs.com (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Bakers Non Contact Cooling Pace Project No.: 92186793 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Bakers Non Contact #7 Lab ID: 92186793007 Collected: 01/15/14 11:20 Received: 01/16/14 16:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 01/21/14 14:09 4SOOCL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.42 mg/L 0.024 1 01/21/14 15:45 7782-50-5 H3 Date: 01/22/2014 01:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc,. Page 10 of 18 aceAnalytical` www.pacelabsmm Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project: Bakers Non Contact Cooling Pace Project NO.: 92186793 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Bakers Non Contact #8 Lab ID: 92186793008 Collected: 01/15/14 11:40 Received: 01/16/14 16:20 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease 5.2 mg1L 5.0 1 01/21114 14:09 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.28 mg1L 0.024 1 01/21/14 15A9 7782-50-5 H3 Date: 01/22/2014 01:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 11 of 18 aceAnalytical xnYw.pecele4mm Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bakers Non Contact Cooling Pace Project No.: 92186793 QC Batch: GCSVi16474 Analysis Method: EPA 1664B QC Batch Method: EPA 16646 Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92186793001, 92186793002, 92186793003, 92186793004, 92186793005, 92186793006, 92186793007, 92186793008 METHOD BLANK: 1124651 Matrix; Water Associated Lab Samples: 92186793001, 92186793002, 92186793003, 92186793004, 92186793005, 92186793006, 92186793007, 92186793008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers ` Oil and Grease mg1L ND 5.0 01121/14 14:04 LABORATORY CONTROL SAMPLE: 1124652 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 33.8 84 78-114 MATRIX SPIKE SAMPLE: 1124653 92186786002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg1L ND 40 36.9 92 78-114 Date: 01122/2014 01:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 18 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. �aneMalytical 205 East MeadoEdRn, NC 27288 Asheville, NC 28804 980oHunersv le, NC128076 w'wwPacerabscorn (336)623-8921 (B28)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Bakers Non Contact Cooling Pace Project No.: 92186793 QC Batch: WET129188 Analysis Method: SM 4500-CI G QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual Associated Lab Samples: 92186793001, 92186793002, 92186793003, 92186793004, 92186793005, 92186793006, 92186793007, 92186793008 METHOD BLANK: 1125476 Matrix: Water Associated Lab Samples: 92186793001, 92186793002, 92186793003, 92186793004, 92186793005, 92186793006, 92186793007, 92186793008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chlorine, Total Residual mg1L ND 0.024 01/21/14 13:56 SAMPLE DUPLICATE: 1125477 Parameter Chlorine, Total Residual Date: 01/22/2014 01:54 PM 92186793001 Dup Units Result Result mg1L 0.57 0.57 RPD Qualifiers REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 0 Page 13 of 18 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. w Road - Suite A 205 East Meadow 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 wwwpecdabscom (336)623-6921 (826)254-7176 (704)875-9092 QUALIFIERS Project: Bakers Non Contact Cooling Pace Project No.: 92186793 DEFINITIONS DF - Dilution Factor, if reported, represents the (actor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylarnine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute, LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/22/2014 01:54 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 18 aceAnalytkal www.pgcalabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 2BB04 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Bakers Non Contact Cooling Pace Project No.: 92186793 Lab ID Sample ID QC Batch Method QC Batch 92186793001 Bakers Non Contact #1 EPA 1664E GCSV116474 92186793002 Bakers Non Contact #2 EPA 1664E GCSV116474 92186793003 Bakers Non Contact #3 EPA 1664B GCSV116474 92186793004 Bakers Non Contact 44 EPA 1664E GCSV/16474 92186793005 Bakers Non Contact #5 EPA 1664B GCSVI16474 92186793006 Bakers Non Contact #6 EPA 1664B GCSVI16474 92186793007 Bakers Non Contact #7 EPA 1664B GCSV116474 92186793008 Bakers Non Contact #8 EPA 1664E GCSV116474 92186793001 Bakers Non Contact #1 SM 4500-CI G WET129188 92186793002 Bakers Non Contact #2 SM 4500-CI G WET129188 92186793003 Bakers Non Contact #3 SM 4500-CI G WET129188 92186793004 Bakers Non Contact #4 SM 4500-CI G WET129188 92186793005 Bakers Non Contact 05 SM 4500-CI G WET129188 92186793006 Bakers Non Contact #6 SM 4500-Cl G WET129188 92186793007 Bakers Non Contact #7 SM 4500-Cl G WET129188 92186793008 Bakers Non Contact #8 SM 4500-CI G WET129188 Date: 01122/2014 01:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Method Analytical Batch Page 15 of 18 ,1.W�7ct�Ar�alyficrtl Uocument Name: Condition Upon Receipt SCU Document Number: F-CHR-CS-03-rev.13 Uocument rtt;wseu. veuGnruci Iv, eu IJ Paae 1 of 2 issuing Authority: Pace Huntersville Quality Office Client Name: Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial Pace Other - Custody PI'oj`•De:Date:��`> �� F:r Custody Seat on Cooler/Box Present: yes C�r El Seals intact: ❑ yes no Nuame: Packing Material: ❑ Bubble Wrap ❑ ,Bubble Bags ❑ None ❑ Other Thermometer Used: IR Gun T1102 jiRp Type of Ice: a Blue None LJ Samples on ice, cooling process has begun Temp Correction Factor T 102: N"o Correction T130"o Correction Biolo )cal Tissue IS Frozen: Yes No NIA Date and in' ials of p e camining Corrected Cooler Temp.: C g contents: Temp should be above freezing to VC Comments: Chain of Custody Present: es ONO ❑NIA 1. Chain of Custody Filled Out; Zles ❑No ❑NIA 2, unaln or uustoay Keuncluished: .Ief]Yes LJNo UNIA 37 Sampler Name & Signature on COC: �,Yes ONO ❑NIA 4, Samples Arrived within Hold Time: Z Yes ONO ❑NIA 5. Short Hold Time Analysis (<72hr): Oyes 1160 ❑NIA 6. Rush Turn Around Time Requested: Dyes t,INo ❑NIA 7, Sufficient Volume: 9<s ONO ❑NIA g, Correct Containers Used: 0"Yes ONO ❑NIA -Pace Containers Used: Eyes ONO ❑NIA g, Containers Intact: Yes ONO ❑NIA .10, Filtered volume received for Dissolved tests Oyes ONO ❑NIA 11, Sample Labels match COC: No ❑N/A -includes dale/time/ID/Anaivsls Matrix: 12. All containers needing preservation have been checked. ❑Yes ❑No ❑NtA 13 All containers needing preservation are found to be in compliance with EPA recommendation. Oyes ONO ❑NJ exceptions: VOA, colifoim, TOC, O&G, WI-DRO (water) Dyes ONO Samples checked for dechlorination: Dyes ❑No NIA 14. Heads ace in VOA Vials (>6mm): ❑Yes ONO l�tr I( 15. Trip Blank Present: ❑Yes ONO ❑fern 16. Trip Blank Custody Seals Present Dyes ONO ❑NIA Pace Trip Blank Lot # (if purchased): Client Notification/ Resolution: Field Data Required? Y 1 N Person Contacted: DatelTime: Comments/ Resolution: F SCURF Review: L Date: I jW SRF Review: Dater 7 Note: Whenever there i rscrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i,e out of hold, incorrect preservative, out of temp, jincorrect containers) Place label here WOA:92186793 - -. !Iq,IIItiVtl - CHAIN -OF -CUSTODY ! Analytical Request Document cc �2aceAnalytical • The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed accurately. w .pacdatctom Page: of Section A Section B Section C ^ ^ /� Required Client Information: Required Project Information: Invoice Inferrnatiom Company; , Report To: 7 Q n Attention: ` m . L L 8 Addr !: & � jlo (!j [ [ Copy J { I/ iC fT Ij 1 GompanyName;/J 4 ki REGU!_470ItY AGENCY Address. [�� 6 �1'icrtresc NPOES j— GROUND WATER j— DRINKING WATER O - (J 1 .r {` UST r OTHER RCRA i Email To: Purchase Order No.: Pace Ovum Reference: P Fax: Project Nam /i? Pace Protect Manager. Site Location STA re_ l-r VL Requested Due Date1TAT: Project Number. Pace Prwae:r: Requested Analysis Filtered (YIN, Section D Matrix Cod" Required Client lnformatian MATRIX I CODE 9 COLLECTED Preservatives y Z Y Drinking Water DW Q V z C warar wr waste water W I a U START POSITE �WIN So�solid 5L O y y -� ,� J •U w r SAMPLE ID oil OL _ w C y A (A-Z 0-91; ► Aires AR Wp w a l V V r O Sample IDS MUST 6E UNIQUE Tissue 75 C:)EL U w Z U Other OT u W ¢ a o i� z 2U t m m m a' v y DATE TIME DATE TIME m _ = Z Z 20 D LY Pace Project No.I Lab I.D. y IYI ILI 4 Mewrj fac f '��Z % -IS r /r:11 I A&I C! 1-44t 03 G ieLg s- , x S- lee ! X X r 12 ' cic (T G--' - 5-1 •o b- 1 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS 7'Sv // i2- : ,n c�7fiC'I-le-lel f% SAMPLER NAME AND SIGNATURE v o w ORIGINAL PRINT Name of SAMPLER: / /i �1 Ll.(F J r d tl C. rt e y � } n 5 C SIGNATURE of SAMP ER: DATE Sig ed i fr r� •t (MWDDIYY): 'Important Now By sprang this form you are accepting Pace's NET 30 day payment ienrts and agreeing to Ute Uarges at 1.5% per month eny ter pa 30 F-ALL-0-020rev.07,15-May-2007 CHAIN -OF -CUSTODY 1 Analytical Request Document /-FaceAnalyiical • The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed aocurately. '- eetae:-eem 00 Page: of Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: ^ y ^ 'L1� Company: -� bL Report 70: r Attention: , l�'1'\ fl{! Address. J O` O� n t q lD !� I Copy To, o ; Company Name. Tz I =� ry 1REGULATORY IT 0. AGENCY aI Address:; P. e` i3000 s3 � NPDES (- GROUNDWATER � DRINKING WATER oyw G O 7 rn,,, lx LIST(- RCRA OTHER Email To: Purchase Order No.: PPace0 e6 Reference: Phone: _ i 1 Fax: Projp Na�e: r C:v �C 1� 0. C Co C i rl Peca Project htana9er- Site Location STA rE. Requested Due DdterTAT: Project Number. Pace Pyre n: Requested Analysis Filtered (YIN) Section 0 Matrix Cedes -- y _ Riqulretl CYent mlormauon MATRIX r CODE3 i COLLECTED Preservatives i Dnnking Water DW r O 41 Waver WT Wa5t0Water WW LOLWOSrTE START COMPOSITE ENDIGRAB U �, J t. Z Product P Soil/Soid SL — m 0 J O y V a b } SAMPLE ID O1l QL 3 Q rn � to WIPv (A-Z, 0-9 r r) Piro Ail to a a Lw Z 1 Sample IDS MUST BE UNIQUE Tissue TS O cD }} w Z Other OT X F r w O f LL c C O O L@ - w ~ N DATE TIME DATE TIME fn u rn Z = M z z f al 2 t O y ff Pace Project Nod Lab I.D. 1 z C G 115j I:i3 1 X 3 e%kCv`5 O COYZ C- WIT C—li-6-Ii 11;�{ 'm 7. X a +r Q C G "s -N r' : f 3n.m I X s 6 7 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS 1- -24D SAMPLER NAME AND SIGNATURE U o c a ORIGINAL a z_ >> (•QQ� ? BD} S g? ✓ Q PRINT Name of SAMPLER: �n �, I f Ur -Vel ~ m a u U y r N SIGNATURE of SAMPLER: A --, ft - (MMIDDlY o 1 Y - -Important NOW 6y signing Snn farm you am accepMg Pace'S NET 30 day payment Serm3 and agreeing to Into charges of 1.5X par month any m anal witnm F-ALL-0-020rev,07, 15-May-2007