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Home My WebLink AboutWQ0012980_Residual Annual Report 2014_20150129For Better results. Naturally. Milorganite January 28, 2015 Information Processing Unit Division of Water Quality Department of Environment and Natural Resources 1617 Mail Service Center Raleigh, North Carolina 27699 -1617 Subject: Milorganite°Ann ual Report Good day: JAN 2 9 M5 watarousli bean$ g SeC On To demonstrate the quality of the Milorganite® sold in North Carolina during 2014, a report is enclosed. The report shows that Milorganite® continues to be an exceptional quality biosolids product, according to the applicable regulations (40 CFR 503 and 15A NCAC 2T.1106 and 2T.1107). The report includes the following sample results: Parameter Frequency As, Cd, Cu, Fe, Pb, Mo, Ni, P, K, Se, Zn Daily Al, B, Cr Monthly Hg Weekly Fecal Coliform 3 per month PCB Aroclors Daily Toxic Equivalents: Dioxins, Furans, and PCBs Monthly Priority Pollutants Semi-annually Solids Daily Also, the Residual Report Form, a report showing distributors and sales, and reports showing representative dryer exit temperature are enclosed. Milorganite° continues to be registered as a fertilizer with the North Carolina Department of Agriculture. If you have questions, please contact me at 414-225-2243 or tnowicki@mmsd.com. If you have no interest in continuing to receive this report, then please notify me. Thanks for your cooperation. Sincerely yours, Thomas A. Nowicki Staff Attorney Enclosures Milorganite - MMSD 260 W. Seeboth Street Milwaukee, WI 53204 u Phone: (414) 221-6810 (800) 287-9645 Fax: (414) 221-6818 Sustaining TurfgrassResearch info@milorganite.com www.milorggnite.com FOUN� o n North Carolina Department of Environment and Natural Resources ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ 00 12980 No Discharge Laboratory: Facility Name: Milwaukee Metro Sewerage District Residual Source WQ # or NPDES #: WWTP Name: Residual Analysis Data WPDES WI 0036820 Jones Island 1) Milwaukee Metro Sewerage District ;L 2) - 3) 4) 5) Parameter Parameter Limit LimitJanuary (mg/kg) Sample or Composite Date (monthly average) February March April May June July August September October November December Percent Solids %) NA 94 94 95 94 94 94 93 94 95 93 93 93 Arsenic 41 9.7 9.3 9.9 12 14 4.8 6.2 2.0 6.7 7.3 7.7 5.7 Cadmium 39 2.2 2.1 1.8 1.5 1.3 0.64 1.0 1.2 1.5 2.8 3.7 2.8 Chromium NA 220 220 230 180 210 220 200 230 380 300 230 240 Copper 1,500 280 260 260 250 260 240 260 230 290 280 280 280 Lead 300 54 42 38 45 45 63 59 49 47 48 31 27 Mercury 17 0.39 0.25 0.2 0.10 0.23 0.24 0.26 0.24 0.11 0.3 0.26 0.38 Molybdenum 75 12 10 9.0 9.5 8.9 9.2 10 9 12 13 13 12 Nickel 420 45 36 32 48 36 35 36 33 36 38 32 33 Selenium 100 <2.8 <2.8 <2.8 0.29 0.48 2.7 0.96 0.27 <2.6 0.85 <2.6 0.37 Zinc 2,800 560 540 630 550 490 540 590 570 660 770 640 570 Total Phosphorus NA 24,000 23,000 22,000 21,000 20,000 21,000 22,000 23,000 26,000 24,000 24,000 25,000 Total Nitrogen(%) NA 6.1 6.4 6.2 6.2 5.9 5.8 5.2 5.7 5.7 5.5 5.6 6.1 Ammonia -Nitrogen % NA 0.20 0.22 0.20 0.20 0.15 0.17 0.15 1 0.18 0.17 0.17 0.18 0.18 Nitrate Nitrogen(%) NA 1.1 0.6 0.85 0.72 0.76 0.95 0.62 1 0.7 2.7 0.70 1.3 1.2 Sampling frequency: Arsenic, cadmium, copper, lead, molybdenum, nickel, selenium, and zinc are daily; Mercury is weekly; Ammonia, chromium, nitrate, and nitrogen are monthly "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that of Preparer * *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) MILWAUKEE METROPOLITAN SEWERAGE DISTRICT Marketing Division Tonnage Tax Listing 01/01/2014 - 12/31/2014 Invoice/ State County ShipDate Sales Order Product Tons Distributor Run Date: 1/5/2015 Sage 103 of 177 Ship To City NC ----------------------------------------------------------------------------------------------- --------------------------------------- Watauga 02/11/2014 17742 Classic Grade 50# Potash Delete 02/11/2014 17742 Greens Grade 50# Potash Delete 03/21/2014 17938 Classic Grade 50# Potash Delete 03/21/2014 17938 Greens Grade 50# Potash Delete 04/21/2014 18248 Classic Grade 50# Potash Delete 04/21/2014 18248 Greens Grade 50# Potash Delete 05/19/2014 18413 Classic Grade 50# Potash Delete 05/19/2014 18413 Greens Grade 50# Potash Delete 06/20/2014 18640 Classic Grade 50# Potash Delete 06/20/2014 18640 Greens Grade 50# Potash Delete 07/02/2014 18702 Classic Grade 50# Potash Delete 07/02/2014 18702 Greens Grade 50# Potash Delete 07/10/2014 18730 Classic Grade 50# Potash Delete 07/10/2014 18730 Greens Grade 50# Potash Delete 07/24/2014 18787 Classic Grade 50# Potash Delete 07/24/2014 18787 Greens Grade 50# Potash Delete 07/24/2014 18787 Bulk Classic Grade 2000# Totes 08/28/2014 18920 Greens Grade 50# Potash Delete Watauga County Total: 3.00 Southern Agricultural Insecticides BOONE 18.00 Southern Agricultural Insecticides BOONE 6.00 Southern Agricultural Insecticides BOONE 15.00 Southern Agricultural Insecticides BOONE 4.00 Southern Agricultural Insecticides BOONE 17.00 Southern Agricultural Insecticides BOONE 2.00 Southern Agricultural Insecticides BOONE 19.00 Southern Agricultural Insecticides BOONE 6.00 Southern Agricultural Insecticides BOONE 15.00 Southern Agricultural Insecticides BOONE 6.00 Southern Agricultural Insecticides BOONE 15.00 Southern Agricultural Insecticides BOONE 12.00 Southern Agricultural Insecticides BOONE 9.00 Southern Agricultural Insecticides BOONE 15.00 Southern Agricultural Insecticides BOONE 5.00 Southern Agricultural Insecticides BOONE 1.00 Southern Agricultural Insecticides BOONE 21.00 Southern Agricultural Insecticides BOONE 189.00 NC State Total: 252.00 MILWAUKEE METROPOLITAN SEWERAGE DISTRICT Marketing Division Tonnage Tax Listing 01/01/2014 - 12/31/2014 Invoice/ State County ShipDate Sales Order Product Tons Distributor Run Date: 1/5/2015 Sage 102 of 177 Ship To City NC ---------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- Iredell 07/18/2014 18762 Classic Grade 50# Potash Delete 10.00 Southern States Cooperative, Inc. -VA Statesville 07/18/2014 18762 Greens Grade 50# Potash Delete 11.00 Southern States Cooperative, Inc. - VA Statesville Iredell County Total : 21.00 - --------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- Mecklenburg 06/12/2014 18541 Milorganite 36# Potash Delete 21.00 Pennington - NC Central Div. Charlotte Mecklenburg County Total : 21.00 ---------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- Robeson 10/20/2014 19053 Greens Grade 50# Potash Delete 21.00 Helena Chemical Robeson County Total: 21.00 ROWLAND HOURLY DRYER PRODUCT TEMPERATURE DATA DateTime I ( DRYER NUMBER) 10/1/14 0:00 190 189 184 187 98 193 196 196 104 194 80 190 10/1/14 1:00 185 185 185 184 98 190 190 178 105 196 80 178 10/1/14 2:00 179 185 183 184 98 189 182 171 99 176 162 10/1/14 3:00 180 186 187 186 99 191 186 183 102 185 170 10/1/14 4:00 177 183 187 186 193 189 184 104 183 180 10/1/14 5:00 173 177 178 175 98 178 177 178 103 176 177 10/1/14 6:00 173 177 175 177 175 176 177 179 181 10/1/14 7:00 172 180 176 179 177 177 174 102 182 184 10/1/14 8:00 176 181 179 181 99 182 180 115 99 174 181 10/1/14 9:00 179 181 187 185 186 183 104 91 187 192 10/111410:00 160 183 186 180 100 181 185 88 182 191 10/1/14 11:00 163 184 178 178 99 176 180 102 179 81 185 10/1/14 12:00 161 193 192 183 84 181 179 102 86 178 83 183 10/1/1413:00 176 187 181 180 178 183 179 102 87 179 84 187 10/1/14 14:00 197 208 188 188 188 171 179 103 88 184 85 174 10/1/1415:00 188 190 182 186 199 177 168 99 9T 175 85 174 10/1/1416:00 168 170 175 181 198 159 178 103 167 175 84 175 10/1/1417:00 159 180 177 175 169 189 185 106 190 206 84 197 10/1/14 18:00 182 177 187 178 183 183 191 109 145 180 81 189 10/1/1419:00 198 178 193 188 190 194 184 177 163 80 178 10/1/14 20:00 183 183 188 188 194 197 182 175 175 185 10/1/14 21:00 193 177 185 183 192 193 182 185 185 189 10/1/14 22:00 201 181 187 186 193 195 186 108 187 188 81 189 10/1/14 23:00 202 185 183 185 195 194 183 107 190 189 82 186 10/2/14 0:00 173 181 198 200 195 183 184 107 181 181 83 179 10/2/141:00 178 183 168 182 183 191 185 106 185 186 82 182 10/2/14 2:00 177 182 177 176 184 184 184 105 185 188 82 186 10/2/14 3:00 183 186 187 184 190 187 185 104 187 187 80 184 10/2/14 4:00 178 185 187 185 185 192 185 103 183 182 81 180 10/2/14 5:00 175 181 172 176 176 172 176 102 179 179 176 10/2/14 6:00 178 182 179 184 183 176 154 100 178 182 80 183 10/2/14 7:00 182 185 192 180 185 188 141 98 179 179 81 183 10/2/14 8:00 178 202 190 192 191 191 195 187 198 82 197 10/2/14 9:00 175 170 195 173 181 175 172 96 186 179 84 176 10/2/1410:00 189 184 159 185 177 180 180 185 185 84 180 10/2/1411:00 150 170 175 179 182 182 185 95 186 184 84 187 10/2/1412:00 176 178 180 179 183 183 185 95 185 186 86 187 10/2/1413:00 186 183 188 190 188 187 184 94 183 184 86 181 10/2/14 14:00 185 184 186 183 186 186 176 183 181 87 181 10/2/1415:00 188 194 192 192 191 193 184 93 188 188 89 189 10/2/14 16:00 188 190 188 186 188 190 160 187 191 88 187 10/2/1417:00 186 188 184 183 185 187 174 191 190 91 188 10/2/1418:00 183 185 185 184 183 185 193 188 186 91 198 10/2/1419:00 184 178 183 187 183 184 183 187 185 92 186 10/2/14 20:00 186 183 183 185 121 181 163 92 180 177 181 10/2/14 21:00 180 183 183 181 111 178 157 180 180 91 177 10/2/14 22:00 188 195 187 192 111 187 162 91 188 191 90 189 10/2/14 23:00 194 194 195 197 110 195 173 90 194 198 91 199 10/3/14 0:00 190 189 191 186 110 192 179 91 190 190 92 193 10/3/141:00 186 185 185 184 110 187 157 90 187 188 92 173 10/3/14 2:00 184 183 183 181 103 185 189 89 185 181 90 166 10/3/14 3:00 182 182 183 181 100 183 173 88 183 184 88 164 10/3/14 4:00 151 146 182 182 99 180 168 87 182 183 87 169 HOURLY DRYER PRODUCT TEMPERATURE DATA DateTime I ( DRYER NUMBER 10/3/14 5:00 109 149 181 183 116 179 171 86 193 193 83 173 10/3/14 6:00 102 155 185 186 102 168 186 81 198 196 190 10/3/14 7:00 103 186 184 185 103 178 187 196 197 190 10/3/14 8:00 102 130 188 184 182 185 192 182 182 184 10/3/14 9:00 103 136 191 189 193 194 186 186 185 181 10/3/14 10:00 100 127 190 186 197 188 184 186 183 181 10/3/1411:00 99 119 188 186 143 185 185 183 184 183 10/3/1412:00 98 112 186 188 126 182 184 80 184 187 80 187 10/3/1413:00 96 106 184 186 115 182 188 80 187 188 80 189 10/3/1414:00 88 101 181 185 108 183 186 187 185 188 10/3/14 15:00 135 135 183 187 150 185 184 185 187 184 10/3/1416:00 184 199 186 187 201 190 185 186 185 186 10/3/14 17:00 191 169 198 191 202 191 186 186 183 187 10/3/14 18:00 174 175 188 181 186 175 185 185 185 182 10/3/14 19:00 184 189 182 182 182 178 187 187 186 181 10/3/14 20:00 187 182 187 185 184 186 188 185 185 185 10/3/14 21:00 193 190 186 190 189 189 188 187 192 189 10/3/14 22:00 180 181 188 174 185 178 182 182 179 181 10/3/14 23:00 182 182 192 183 180 177 178 180 183 180 10/4/14 0:00 185 184 186 182 182 181 181 80 181 181 80 185 10/4/141:00 179 181 186 176 178 178 182 80 182 176 80 179 10/4/14 2:00 182 172 183 172 174 174 178 180 176 172 10/4/14 3:00 178 172 174 181 175 175 184 184 177 179 10/4/14 4:00 179 175 172 194 189 189 187 187 187 184 10/4/14 5:00 195 190 190 199 195 193 193 193 187 194 10/4/14 6:00 174 156 158 162 183 151 184 188 176 185 10/4/14 7:00 161 154 149 146 145 153 178 182' 170 179 10/4/14 8:00 158 153 160 154 158 159 183 184 170 182 10/4/14 9:00 161 156 163 172 163 170 187 186 175 191 10/4/14 10:00 169 166 165 184 177 178 187 185 178 193 10/4/14 11:00 181 178 177 174 184 186 191 187 180 189 10/4/14 12:00 178 185 181 183 192 185 191 80 187 181 80 184 10/4/1413:00 175 177 179 178 140 188 185 80 180 176 80 183 10/4/14 14:00 174 177 175 173 104 167 183 182 180 181 10/4/14 15:00 182 181 179 181 177 183 187 183 184 10/4/1416:00 192 195 206 203 102 194 144 186 188 202 10/4/1417:00 199 195 201 203 104 202 169 176 122 199 10/4/1418:00 196 190 198 193 103 198 191 186 99 190 10/4/1419:00 191 186 194 189 102 195 179 177 97 195 10/4/14 20:00 179 180 183 179 101 186 169 164 163 200 10/4/14 21:00 180 183 169 165 101 175 178 185 144 141 10/4/14 22:00 185 191 175 169 102 176 166 175 187 147 10/4/14 23:00 196 198 201 194 101 197 199 195 197 187 10/5/14 0:00 165 207 191 192 98 183 194 80 193 187 80 193 10/5/141:00 197 151 202 197 100 194 197 80 194 185 80 196 10/5/14 2:00 179 155 164 162 97 185 185 189 182 187 10/5/14 3:00 191 182 181 176 98 166 186 185 182 186 10/5/14 4:00 187 186 187 190 182 182 182 183 184 10/5/14 5:00 193 192 191 185 97 190 183 183 185 184 10/5/14 6:00 187 185 185 185 185 184 184 183 185 10/5/14 7:00 183 182 186 185 185 183 186 181 183 10/5/14 8:00 186 185 183 185 185 185 186 187 202 10/5/14 9:00 187 192 189 185 186 188 187 184 183 OOZ L6L L% 66 L Z L L 86 L 98L 96 L 00:V 4 t UL/O L 08 08 66 L Z6 L 08 EOZ Z6 L 4 L L 98L 98 VOL 99L 00:£ L tr L/L/O L 08 08 98L 68 L 08 E8 L 06 L E L 4 V8 L 98 ELL 08 L OO:Z L K/L/O L 9LL Z8L LLL L8L 844 98L 98 9LL LLL 00:LL bL/L/OL 8LL L8L ELL VOL VzL L8L 9L4 V8L 00:04 bL/L/OL L8L 06 L 6LL 96 L Z91 LLL V8 OL L 99 L 00:6 t, L/L/0 4 L6L L64 Z8L WL LZL M 96L 09L 00:8 VL/L/04 98L 98L Z8L 68L Z8 E64 68 8ZL OO:L 17L/L/OL VOL 98L 6LL VS L8 L% 86 Lt,L 00:9 VUL/OL t'8L b8L L8L 984 L8 46L Z9L V94 00:9 VLIL/OL 98L 98L L8 L L8 L Z8 96 L E8 E8 L Z8 L 00:V 17 L/L/O L 984 Z8L 484 tILL V9 98L Z84 L8L 00:£VWL/OL E8L V8L 9LL 9LL 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00:8 t, L/9/0 L 08L 9LL Z8 L 8L 4 96 9LL 96 LLL EL L OO:L V L/9/0 L 48L Z8L Z8L L8L L6 9LL 60L M Z84 00:9 tiL/9/0L 9L4 LLL 484 ZLL VL4 LEL t18L 484 00:9 tL/9/0L L6 OL L 99L 99L ZL L 86 OL L Z6 L E8 L V8 L OO:tl t, 4/9/0 4 ZO L 9L L VL L 9LL 98L 66 E8 L ZOZ 08 L 9L 4 OO:E t, L/9/0 L 04L 8LL Z8L 6LL ti8L LOL 98L L% L8L 99L 00:Z174/9/OL 6LL 08 . 69 L E8 L 09 Z8 L VL 4 L6 LLL 69 4 £9 L LLL 00: L b L/9/0 L EZ 4 08 06 L 9L L 08 LLL ELL L6 9L L VL L 99L 89 4 00:0 ti L/9/0 L 9E L EOZ t'8 L 98 L 9LL 86 09L 8L L 9LL 6LL OO:EZ b L/9/0 L ZO L L8 L L6L Z6 L 68 L 86 9LL OL L 9LL 9LL OO:ZZ V L/9/0 4 80 L 99L L6L 6LL L 8 L L6 ELL 9LL 89 L LL L 00: L Z t, 4/9/0 L 9ZL 98L E8L 98L SOL 96 VLL 6L4 ZLL L8L OO:OZ t,4/9/0L 984 98L 484 98L 68L 48 9L4 08L VLL V84 00:% K/9/OL 99L 98L V8L E84 98L E8L L8L L94 08L 00:8L VU9/04 t8 L Z84 99L 98L ELL ELL ELL 69 L 89 L OO:L L K/9/0 4 L8L L8L 98L Z8 L Z8 4 9LL 6L 4 L9 L 6LL 00:9 4 K/9/O L L8L 98L Ve L 98L 98L 9LL 09L V6 L Z8 4 00:9 L K/9/O L 99L L8L 99L L8 L 88 L 6LL 08 L ELL ESL 00:K K/9/0 L 69L 08 L64 88L 08 984 V6L 08 98L 984 ELL WL OO:EL tL/9/OL L8 L 08 L8L i78 L 08 99L 98L 08 98L 90 L ELL 98L OO: Z L V L/9/O L L8L L8L Z84 E8L LLL L8L ZLL 99L L8L 00:4L VU9/04 LL4 08L E8L 8LL L8L 48L 1 684 1 894 I LLL I 00:04 17L/9/OL ( iosw 1N b3AIJa ) I GMIJLBIea diva 3mnivu3dW31 iona0Ud 213A21a Aiun0H 1 T J r- k HOURLY DRYER PRODUCT TEMPERATURE DATA DateTime I ( DRYER NUMBER 10/7/1415:00 184 174 87 210 105 195 183 187 183 10/7/1416:00 146 166 201 102 200 172 172 187 10/7/14 17:00 175 143 193 101 184 173 162 178 10/7/14 18:00 183 198 88 186 103 183 169 174 174 10/7/1419:00 173 179 87 193 103 182 172 186 182 10/7/14 20:00 178 183 179 101 174 182 190 186 10/7/14 21:00 177 183 87 179 99 191 188 192 192 10/7/14 22:00 179 182 185 100 188 188 191 197 10/7/14 23:00 181 181 183 189 185 193 194 10/8/14 0:00 175 177 87 183 99 181 183 80 185 192 10/8/141:00 176 181 86 179 98 173 170 80 184 191 10/8/14 2:00 186 178 85 175 174 150 176 188 10/8/14 3:00 176 178 84 184 96 189 190 178 186 10/8/14 4:00 179 179 83 184 95 186 171 185 191 10/8/14 5:00 182 180 122 94 186 171 183 192 10/8/14 6:00 178 178 82 104 92 178 162 169 194 10/8/14 7:00 182 180 88 190 187 188 201 10/8/14 8:00 185 182 81 83 187 187 190 203 10/8/14 9:00 181 182 82 84 188 188 192 201 10/8/1410:00 177 180 82 98 187 189 193 205 10/8/1411:00 176 178 105 92 185 200 198 200 10/8/1412:00 176 174 82 106 91 182 191 80 190 192 10/8/1413:00 187 184 82 107 92 184 179 80 177 190 10/8/14 14:00 181 179 107 182 168 169 184 10/8/1415:00 181 183 84 108 93 180 163 158 183 10/8/1416:00 183 183 95 94 188 203 152 182 10/8/14 17:00 175 177 85 89 95 182 186 162 187 10/8/14 18:00 177 177 141 94 177 184 181 190 10/8/1419:00 179 179 86 144 95 184 189 180 187 10/8/14 20:00 179 182 191 94 183 186 183 187 10/8/14 21:00 181 181 85 185 82 188 185 179 195 10/8/14 22:00 180 180 84 178 183 187 185 189 10/8/14 23:00 179 176 83 177 184 186 185 196 10/9/14 0:00 178 179 83 180 80 187 186 80 184 201 10/9/141:00 178 179 82 179 80 184 184 80 184 197 10/9/14 2:00 185 175 177 184 181 187 181 10/9/14 3:00 180 180 81 180 185 181 183 185 10/9/14 4:00 179 176 177 182 181 180 179 10/9/14 5:00 180 179 80 180 184 188 186 184 10/9/14 6:00 177 175 179 186 186 187 190 10/9/14 7:00 180 182 181 187 186 188 185 10/9/14 8:00 183 182 184 189 189 200 194 10/9/14 9:00 182 180 180 186 187 183 188 10/9/14 10:00 179 179 178 183 183 183 180 10/9/14 11:00 180 178 178 183 185 185 183 10/9/1412:00 180 181 80 180 80 184 184 80 186 187 10/9/1413:00 180 179 80 181 80 186 182 80 186 186 10/9/1414:00 181 183 181 185 182 93 184 186 10/9/14 15:00 182 181 81 182 186 185 182 188 10/9/1416:00 182 181 81 180 185 185 81 186 186 10/9/14 17:00 186 184 184 188 189 128 191 187 10/9/14 18:00 185 181 184 189 191 169 192 191 10/9/14 19:00 180 179 175 185 189 184 195 191 80 80 80 80 m Zim 80 80 80 80 80 80 80 80 r C4 00 00 00 00 0 00 00 co CC) 00 co 00 00 00 00 00 00 00 0 00 00 00 co 00 co co 00 co 0 LO CO M N V' CO LO P- CO 0 LC) M CO O P- 00 r, 0 N N CO � N r- CO IT 0 IT CM h r O 0 h to r r O r- Ln N O r N 0 f- f- M G M ti 0 0 w w 0 00 00 00 00 00 00 00 Co 00 co 0 0 0 0 O O O 0, co co 00 co 00 co 00 00 00 O 00 V N r O O O O 0 0 r C`') Lc) 0 CA r- CO P- 00 CA r r r r r r r r T r r r r r r T r r r N N N r r r r r r r r r r r r r r r r r r r r T r r r r r r N O 0 Cn a Cn CO O ti M N ct �- to 0 t' N d r M 00 00 to CO CO L(7 to l() f� CO N O 00 CO N O d 0 00 0 N O O M 0 00 OOOMMMO W 00000000MOD0OO00000000000CC)0000000000 000CA000000Ot`t`0O000�00O T T r r r r r r r r r r r r r r r N N ———— N N N r T T r r r r r r r r r r r r r r r r r r T r r N r r r r r LL OM0000L00000MNN0Mr-0rN V 0LC)0MNNNMq-MLo000n"td'N0ON0NM0f-0N d I-N00t- oo rnLnvLntil�hhhl�r�hr�I�OOOO00000O000OOrnOOoOaoowaocoa000coaoao�aoa�a)aoaoa000ao W vr-0N0N0r-000vMNwwwLnf-00tN000NCOI,-r%-0(D 0Ln000NaI-NMhLomwwmr-mwO0 I- 00OOa0haO00000pOp000pOpOp00000pOpOpcO0pO1�000pOp00a00pCA000pOhO1�0000000000o0h hf�000000o0f�0000 r r T T T r r r r r T T T r r r r T r T T r r r r T T T r r r r r r T r r r r r r T r r r r r r r r T r r Nt d O 0 N d 0 0 0 0 fl- d 0 0 T T W LC) 0 1* LO M M M f- M M 0 0 M 0 0 N 0 N r Lo N 0 LC) 0 N N M M 0 O M 0 0 r- M 00OOMCA0000000000O�00000O0CC)0000CAO0000(A W 00000M0000000CA00000000a00000CA000000OCA0J�f�00 00 00 00 00 0 co 00 00 00 00 00 00 00 00 0 t-�00cor-r-coODoo�r-(or-�0000co00co�0000r-��to00co0000000000000000cocom00)0000coco(M0)a)0)00co00 T T T r r r r r r r r r T T r T r T r r r r T T T r r r r r ------------------ 0 00 O'O 00 rO 00 0 00 Co co 00 00 co 00 00 00 00 00 co co 0000Tfl-CO00 tM0000000rOCl) NMMOT0000000�rOrT00LLBNr0oCV) 000000LnLOLC)MCO00LoOOLO000 r- I,-00001,- r-ti0000P-P,P-r-000000000000000000I-I,-r-f`00000000r-00000000fl-0000000000000000000000000000000000 r r r r r r r r T r T T r r r T r r r r r T r T r r r r r r r r T T T T r r r r T r r r T r T T T r r r r O0Nr000NN00O00C0ONMMrONrOO f�I�00000OrOT�'00t`ONMLnf�ln�"c1"cl'COOI�rNMtC)O �000CC)��0000�h��t`M0p0000000000NO ti�00OtiO0000000000n�ti00000000MM00O0CC)O000000000O r r r T T T T r r r r r r r r r r r T T r r r r r r r r r T r r T T r r r r r r r T r r r T T T r r T r r C_ O�NMOrNMd'LC)O�00OOrNfM,tLT0 Of--COOOrNM34663 o0O0TNM7tL)—— —OONNM� N N N N r r r T r r r r r N N N NC76 6ir r r r T r T r r r N N N N �.' "tv T't �� cF�P �t'qTv'I IqvvIt It It r r T T \ \ \ \ \ \ \ \ \ \ r r r r r r r r T T T T r r \ \ \ \ \ \ \ \ \ \ r r r r r r r T T r T r r r \ rrr -T \r -r -T T -T r -T rT -r -r\ -r\ -T\ -T\ N000 0 0 0 00000 0 0 0 0 0 0rrrrr r r r r r r -r r r r r r rrTTTrrrrTrrrrT\ \ \ \ \ \ \ \ \ \\\ \\ 0 00 0OO CD OOOOO O O O O O O 0 00000000000 r r r r r T r 0 0 0 0 0 \ \ 0 0 0\ r\r r r r r r T T r r r r r r r HOURLY DRYER PRODUCT TEMPERATURE DATA DateTime I ( DRYER NUMBER 10/12/141:00 188 191 80 187 80 185 196 186 187 202 80 10/12/14 2:00 189 187 191 188 165 203 188 200 10/12/14 3:00 187 186 194 187 191 184 187 202 10/12/14 4:00 184 183 187 181 186 183 182 196 10/12/14 5:00 184 183 184 183 184 181 182 184 10/12/14 6:00 186 186 187 186 176 186 181 176 10/12/14 7:00 186 185 185 183 175 186 186 178 10/12/14 8:00 185 181 183 183 168 183 184 175 10/12/14 9:00 181 178 181 181 161 176 182 166 10/12/14 10:00 185 189 184 185 160 181 185 163 10/12/14 11:00 188 189 190 190 171 190 191 175 10/12/1412:00 187 188 80 187 80 188 170 182 182 173 80 10/12/1413:00 187 185 80 185 80 184 167 182 188 167 80 10/12/14 14:00 185 184 186 185 151 187 180 169 10/12/14 15:00 185 183 185 183 183 193 186 176 10/12/1416:00 183 183 82 186 184 179 181 193 179 81 10/12/1417:00 183 184 81 185 185 177 186 187 172 10/12/1418:00 184 185 184 182 172 184 181 172 80 10/12/14 19:00 185 190 182 185 171 185 189 173 10/12/14 20:00 201 202 191 199 173 184 186 171 10/12/14 21:00 182 176 187 189 173 182 183 172 81 10/12/14 22:00 177 175 186 181 177 184 186 172 80 10/12/14 23:00 182 182 184 184 178 189 187 177 10/13/14 0:00 186 185 82 186 80 187 176 186 185 173 80 10/13/141:00 188 182 82 189 80 187 175 184 186 173 80 10/13/14 2:00 182 183 182 180 174 187 185 176 10/13/14 3:00 185 186 185 184 177 185 183 174 10/13/14 4:00 176 175 166 180 176 185 183 172 10/13/14 5:00 181 179 190 182 171 178 176 168 10/13/14 6:00 185 183 182 185 173 190 192 174 10/13/14 7:00 185 177 83 179 184 187 181 185 183 81 10/13/14 8:00 184 182 82 185 186 186 185 168 152 10/13/14 9:00 184 184 181 187 172 179 165 152 82 10/13/1410:00 186 190 183 186 180 185 168 162 80 10/13/1411:00 179 187 181 185 183 185 181 177 81 10/13/1412:00 186 185 83 180 80 187 189 190 186 180 82 10/13/1413:00 190 188 83 186 80 189 189 184 183 192 82 10/13/1414:00 187 185 84 184 187 183 176 177 177 83 10/13/14 15:00 184 185 181 182 175 170 173 171 81 10/13/1416:00 183 185 83 183 184 171 174 165 185 81 10/13/1417:00 182 188 84 186 185 188 181 183 185 10/13/1418:00 183 187 84 177 182 187 166 169 171 10/13/1419:00 179 186 160 165 179 189 155 155 81 10/13/14 20:00 185 182 85 188 182 187 197 174 173 84 10/13/14 21:00 192 188 191 188 196 200 176 187 85 10/13/14 22:00 191 188 86 187 188 184 185 169 182 86 10/13/14 23:00 188 189 87 184 185 181 170 168 183 87 10/14/14 0:00 179 184 87 180 80 180 137 130 176 180 87 10/14/141:00 175 182 87 184 80 185 152 143 167 164 87 10/14/14 2:00 187 190 183 176 152 149 165 159 10/14/14 3:00 178 188 88 188 182 163 155 174 165 10/14/14 4:00 187 186 87 185 181 163 158 176 168 10/14/14 5:00 197 185 87 194 190 191 190 194 189 80 80 80 81 82 82 83 84 HOURLY DRYER PRODUCT TEMPERATURE DATA DateTime I ( DRYER NUMBER 10/14/14 6:00 195 189 87 192 189 196 184 185 191 86 10/14/14 7:00 183 178 87 182 184 173 176 176 184 10/14/14 8:00 182 174 182 182 175 180 184 179 87 10/14/14 9:00 181 182 186 176 187 180 188 186 87 10/14/1410:00 184 186 193 183 193 190 191 190 87 10/14/1411:00 188 186 179 183 185 186 186 184 85 10/14/1412:00 188 188 87 191 80 188 187 186 186 185 80 10/14/1413:00 187 185 87 186 80 188 186 185 188 187 80 10/14/14 14:00 183 184 180 181 186 187 185 183 10/14/14 15: 00 184 182 182 179 188 187 187 184 10/14/14 16:00 183 183 184 179 183 187 187 191 10/14/1417:00 186 188 85 186 185 187 187 185 191 10/14/14 18:00 188 187 187 187 187 188 185 190 10/14/1419:00 186 186 84 184 185 156 195 182 193 10/14/14 20:00 185 185 181 184 161 188 183 189 10/14/14 21:00 185 186 182 186 193 186 185 195 10/14/14 22:00 186 184 83 188 189 196 186 185 190 10/14/14 23:00 185 184 185 185 194 184 187 188 10/15/14 0:00 192 192 83 186 80 185 192 178 184 188 80 10/15/141:00 188 190 83 188 80 186 201 188 187 192 80 10/15/14 2:00 191 194 190 187 203 182 184 191 10/15/14 3:00 189 191 187 186 186 182 186 189 10/15/14 4:00 181 182 180 183 206 180 185 192 10/15/14 5:00 173 168 175 180 186 183 181 185 10/15/14 6:00 176 180 171 181 176 185 185 190 10/15/14 7:00 183 185 179 182 189 186 188 194 10/15/14 8:00 187 188 82 186 188 188 188 187 195 10/15/14 9:00 192 194 82 192 190 190 187 188 191 10/16/1410:00 193 196 83 184 169 188 168 174 183 10/15/1411:00 139 145 82 143 137 144 99 101 97 10/15/1412:00 187 193 82 178 80 177 186 181 121 116 80 10/15/1413:00 185 191 82 207 80 198 187 207 143 135 80 10/15/1414:00 187 188 193 199 - 195 193 183 172 10/15/14 15:00 185 181 189 188 180 180 194 179 10/15/14 16:00 186 184 185 185 184 184 197 199 10/15/1417:00 185 187 187 187 187 188 201 206 10/15/1418:00 184 185 185 186 199 189 196 200 10/15/1419:00 183 185 189 194 211 204 201 204 10/15/14 20:00 187 187 189 194 211 207 199 205 10/15/14 21:00 184 183 190 196 197 200 198 200 10/15/14 22:00 186 188 187 195 198 195 194 195 10/15/14 23:00 185 189 188 196 186 181 190 192 10/16/14 0:00 187 185 82 188 80 198 182 178 181 185 80 10/16/141:00 194 194 82 195 80 204 177 173 177 182 80 10/16/14 2:00 199 193 81 204 205 180 173 181 184 10/16/14 3:00 186 179 82 200 198 176 171 179 179 10/16/14 4:00 172 170 178 181 177 171 178 178 10/16/14 5:00 175 179 178 177 178 169 180 181 10/16/14 6:00 182 188 182 190 178 169 181 180 10/16/14 7:00 185 181 188 191 178 173 185 187 10/16/14 8:00 187 188 80 185 190 146 189 188 191 10/16/14 9:00 183 182 185 181 175 194 193 198 10/16/1410:00 189 188 191 201 202 195 200 198 83 83 81 80 80 80 80 ti: HOURLY DRYER PRODUCT TEMPERATURE DATA DateTime I ( DRYER NUMBER 10/16/14 11:00 184 182 184 189 201 198 197 196 10/16/1412:00 182 181 80 178 80 180 203 200 195 195 81 10/16/1413:00 180 185 80 190 80 193 203 188 194 193 81 10/16/1414:00 188 183 201 195 189 179 191 189 10/16/14 15:00 177 175 172 174 173 180 190 182 10/16/1416:00 178 177 184 190 179 178 188 184 82 10/16/14 17:00 184 180 183 185 182 179 190 183 10/16/14 18:00 185 184 185 189 187 181 187 181 10/16/1419:00 184 187 185 193 200 199 191 185 10/16/14 20:00 187 187 186 190 192 200 199 190 10/16/14 21:00 185 188 184 190 184 191 198 191 81 10/16/14 22:00 186 185 185 186 182 188 196 194 81 10/16/14 23:00 184 181 184 190 182 185 195 188 10/17/14 0:00 184 186 80 184 80 188 183 183 191 184 81 10/17/141:00 177 172 80 179 80 186 183 183 190 183 81 10/17/14 2:00 178 176 178 181 184 181 187 178 10/17/14 3:00 183 184 184 186 190 186 186 179 10/17/14 4:00 190 186 187 196 188 204 190 199 10/17/14 5:00 185 179 177 180 193 201 205 203 10/17/14 6:00 180 181 182 183 189 199 192 190 10/17/14 7:00 182 184 181 188 181 193 188 189 10/17/14 8:00 186 189 188 192 188 193 188 188 82 10/17/14 9:00 191 195 194 198 190 198 193 191 82 10/17/14 10:00 184 183 181 187 180 165 187 189 10/17/14 11:00 178 182 181 186 186 182 180 182 10/17/1412:00 177 173 80 178 80 180 182 176 176 180 82 10/17/1413:00 167 169 80 173 80 172 170 171 175 175 82 10/17/1414:00 175 182 180 175 182 180 178 178 80 10/17/14 15:00 190 192 196 192 174 195 192 190 10/17/14 16:00 198 198 194 199 115 177 190 195 10/17/14 17:00 192 190 186 189 100 160 179 189 10/17/14 18:00 182 182 176 179 119 155 176 182 10/17/14 19:00 175 177 172 174 179 181 186 181 10/17/14 20:00 174 178 145 181 206 190 187 191 10/17/14 21:00 145 189 182 201 203 184 192 201 10/17/14 22:00 171 198 191 202 194 175 193 201 10/17/14 23:00 192 185 192 195 189 177 188 193 10/18/14 0:00 194 174 80 192 80 188 184 177 189 188 80 10/18/141:00 187 175 80 182 80 175 178 177 184 182 80 10/18/14 2:00 180 177 178 172 189 179 184 182 10/18/14 3:00 175 176 178 176 195 177 187 186 10/18/14 4:00 178 181 181 181 201 183 189 188 10/18/14 5:00 184 191 187 187 203 182 191 194 10/18/14 6:00 187 184 188 192 207 182 196 199 10/18/14 7:00 183 182 185 181 201 173 187 195 10/18/14 8:00 179 183 182 179 188 179 178 177 10/18/14 9:00 181 185 182 179 185 182 177 181 10/18/14 10:00 186 185 187 189 184 182 182 179 10/18/14 11:00 191 187 194 198 189 181 182 186 10/18/1412:00 192 189 80 193 80 196 176 175 178 179 80 10/18/1413:00 187 186 80 188 80 192 184 185 176 174 80 10/18/14 14:00 179 180 180 182 186 174 178 178 10/18/14 15:00 177 182 178 172 181 181 174 178 80 80 W HOURLY DRYER PRODUCT TEMPERATURE DATA DateTime I ( DRYER NUMBER) 10/18/14 16:00 180 182 183 180 177 178 181 180 10/18/14 17:00 185 184 185 185 182 179 179 182 10/18/14 18:00 186 189 186 186 187 180 183 182 10/18/14 19:00 186 185 184 185 176 168 174 182 10/18/14 20:00 184 183 185 184 167 170 172 188 10/18/14 21:00 185 188 187 186 167 174 173 177 10/18/14 22:00 185 184 183 184 139 190 181 178 10/18/14 23:00 184 183 184 186 179 193 192 199 10/19/14 0:00 186 185 80 186 80 185 191 193 191 191 10/19/141:00 189 187 80 188 80 188 192 197 192 189 10/19/14 2:00 188 187 187 189 191 189 176 189 10/19/14 3:00 187 185 186 184 184 188 183 185 10/19/14 4:00 185 186 185 184 183 178 178 182 10/19/14 5:00 184 184 185 185 185 180 185 183 10/19/14 6:00 186 184 184 184 188 183 191 186 10/19/14 7:00 185 186 186 188 190 188 192 194 10/19/14 8:00 184 187 185 188 190 191 190 10/19/14 9:00 186 185 185 186 188 194 182 194 10/19/14 10:00 185 183 185 185 186 193 179 193 10/19/14 11:00 189 188 188 185 125 192 187 194 10/19/1412:00 191 188 80 191 80 190 124 189 188 197 10/19/1413:00 187 184 80 189 80 186 112 194 181 197 10/19/14 14:00 181 180 185 182 104 193 181 193 10/19/14 15:00 181 184 182 178 122 188 179 192 10/19/14 16:00 182 187 185 185 179 186 183 192 10/19/14 17:00 181 181 184 185 187 194 187 191 10/19/14 18:00 181 185 182 181 188 198 187 193 10/19/14 19:00 186 186 185 182 184 197 186 193 10/19/14 20:00 185 187 186 184 182 196 185 189 10/19/14 21:00 184 181 184 184 185 196 185 185 10/19/14 22:00 184 183 184 186 181 194 185 189 10/19/14 23:00 183 187 184 185 185 198 184 189 10/20/14 0:00 187 184 80 184 80 185 186 189 184 183 10/20/141:00 185 181 80 184 80 185 184 190 182 186 10/20/14 2:00 126 181 183 183 184 190 183 183 10/20/14 3:00 154 184 187 187 185 186 185 184 10/20/14 4:00 113 127 184 181 186 187 186 185 10/20/14 5:00 152 173 187 187 187 186 186 185 10/20/14 6:00 178 187 190 191 186 183 187 193 10/20/14 7:00 186 189 190 187 187 185 175 179 10/20/14 8:00 187 186 191 189 185 190 179 188 10/20/14 9:00 179 182 189 188 117 191 177 189 10/20/1410:00 182 187 188 183 98 187 174 188 10/20/14 11: 00 182 186 189 185 117 190 175 185 10/20/1412:00 183 187 80 192 80 192 176 192 179 187 10/20/1413:00 183 187 80 194 80 193 187 195 185 186 10/20/1414:00 181 184 195 194 163 203 188 192 10/20/14 15:00 181 183 195 193 148 193 189 192 10/20/14 16:00 176 180 188 181 120 191 179 184 10/20/14 17:00 176 182 185 179 106 191 179 182 10/20/14 18:00 168 174 184 181 101 188 181 182 10/20/14 19:00 179 183 186 187 99 188 183 185 10/20/14 20:00 179 184 188 185 96 191 187 186 80 80 80 80 E:I] 80 80 ME 80 80 00 00 r crr0"trrNO'1'0r00O00I`(OIn"tNrrLOU')M�000rOLO It IT '-T O 0 Q o t` 0 I- LO 0 CO r r O M M O 00 t- LO O O LO N r 0 0 0 0 0 0 0 0 0 0 00 00 0)r r r r r r r r r N N N r r r r r r N N r r r r r r r 0 CD ❑ 0 00 cc)000 000 000 coO000 000 000 00 LWN/ I.I. 0 CO f-- Lo 00 r- r r"t 0 CO LC) r O r 0 N t, t N r- N N d' CO r r 0 CO LO r T O r N 00 M 00 0 0 f- � 'ch th M O f- It LO O M OOOO000000O000000'V'O)0,0,CAOLC)0000O000000O0000cc) 00000000000000000000000000000000O r r T T r r r r r r T r r r T T r r r r r r r r r r r r r r — r r r r r r T r T r r r N N N N O Li) M ItO M M M O' r O r O r — L O C O 0 LO M O 0 M r LO CO O O O O d' CO Ln CO O CDf� CO 0 M N CA r 0 0 O 0 cD Cq 00 0 CA 00 t` 0 CO O O 00 O O N Cfl r 0 0 O r- LO 0 00 I,- CO CO (0 � CO � r- (0 �� 00 00 00 00 0) 0)O 00 00 00 (M CD O r CDr T T r r r T r r r T T T N r r r 0 0 0 r r N r r r r r r r r r r r r r r T r r r r r r r r r r r N N N N N WC -O—O OONO OOOOrM rNmO W OOOMO0w000 � �0r0I- 0000)000000000 W 0000000M LO 0)000000OMLO O000000000)OO 0 �a W r r r r r r r r r r r N N N r 0 0 0 0 r r r N N r r r r r r r r r r r r r r r r r r r r r r r r r r N N W� O00O00O Orl-'ItOOO OO OO OO ` O O O 0 0 m0 moD m CO mM w0 w0 0 0 0 0 CD 0 0 0 0 V Z N 0 Li Lf0 Ln V CA M N 00 O O M L20 O a0 1� CA CA CO Ln r M Ln Ln r CA O f� O0 00 Cp M N a0 CA CA CA M M N M O M M M O M M O 00 I- Lo 00 'I M 000000GO0000-00-00-0000—CO00—O--0000000000 00000000a0-00000000O00-----0000000-0000—O `W r r r T r r r r r r r r r r r r r r r r r r r r r r r r r r r r r T r T T r r r r r r r r r r r r T r r r a coOD co00 �OD 0000 co00 W 0 M M M LC) LO r It O '-t I,- N 0 It M 0 M N �t 0� 0 h CO O 1q' LO CO CO r- r O O 00 00 fl- 00 O f- O r O O O O 0 0 0 0 fl- M G M 00 CO 0 CO O O O 0 0 0 O CO 0 0 0 O O O O 0 00 0 0 0 0 0 0 0 0 0 0 00 CO CO CO CO 00 O O CO O 00 00 00 00 0 0 0 O r r r r r r r r r r — r r r — r r r r T r r T r r r r r r r r r r r r r r r r r r r r r r r r — r r r r r r r r fir// iL ❑ 0 0 00 0 0 0 0 00 00 00 00 0 00 00 00 00 0 00 J a/ LO CM co CO N t� M ti 1- O CO O O P It CO ED f` r N O LO ',T (0 U) r O O M M M 0 O 0� W 00 O Orr O r-- 00 f- 00 CA (fl O 00 LC) LO 0000000)0)00001-fl-00000)0000000000000)0)00000000CD 0000)00000000000000000000000000000000000000O00000) r r r T r r r r r r r r r r r r T r r r r r r r r N r T r r r r r r r r r r r r r r r r r r r r r r r r r N O W LO It N O 0 LO O m O 0 f- O M r 0 O T r O LO It 0 0 0�� 0 LC) CO LO M LO O f� f� f� 0 LO 'It M N r O O — — 0 I --CO CO CO t` f� 00 00 0 CO CO CO 0 00 0) 0) 0 0 CO 0)0 O O O O O 0 00 0 0000 0 000 00 00 00 00 00 00 00 r r r r r r r r r r r r r r T r r T r r r r T r r r r O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O W O O O O O O O O O O O OO. Q O 99 O O O O O O O O O O O O O O O O O O O O O O O O O O O 99 O O O O O O r N M O r N C'M tt LC) CO � 00 O O r N M O r N M 1q' LCj CO f-- 00 O O r N CO N N N O r N MF V tf) 0 ti CO Or+r+ r r r r r r r r N N N N O r N co ti lO CO f� 00 O+ r r—F r r r r r r r N N N N O r `Y CI' r V V ";r Cf' t 'V' V' t d' V' Cf' f V V't 't 't 't V 'P V' 't r r r T r r r r T r r r r r r r r r r r +� C) C) r r r r r r r r r r-------- N N N N N N N N N N—— — ————— M M O O O r r r r r r r r r r r r r N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N � C N N a a C) C) C C) C) C) 23 0 N N N N N N N N N N N N N N CD 6 6 6-0-0 c C) C, 0 N N N N N N N N N N N N N N -- Q 6 C) C) O O O O O O O O O O a CD C) C) C) 0 0 0 0 Q C) 0 a C) O O O O O O O O O O C) CD 0 C) 0 C) ') C)— C) O 0 O O O 0 0 0 0 0 0 00 0 0 0 0 0 0 O O O O O O O O O O O O O O T T T r r r r r r r r r r r r r T T r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r ,$ - HOURLY DRYER PRODUCT TEMPERATURE DATA DateTime I ( DRYER NUMBER) 10/23/14 2:00 191 192 199 199 206 196 10/23/14 3:00 189 192 200 181 203 198 10/23/14 4:00 190 191 199 210 197 192 10/23/14 5:00 177 185 193 200 192 184 10/23/14 6:00 187 187 190 192 180 182 10/23/14 7:00 188 187 189 177 183 185 10/23/14 8:00 187 186 176 190 178 179 10/23/14 9:00 187 189 180 190 182 191 10/23/14 10:00 190 190 189 190 186 188 10/23/14 11:00 189 190 186 193 190 187 10/23/1412:00 80 188 80 191 80 187 80 195 188 189 10/23/1413:00 80 188 80 188 80 173 80 199 189 188 10/23/1414:00 122 188 178 200 191 188 10/23/1415:00 102 185 180 200 192 191 10/23/1416:00 90 189 186 197 192 191 10/23/1417:00 90 190 187 198 191 195 10/23/14 18:00 110 187 187 193 189 191 10/23/14 19:00 109 189 185 196 186 194 10/23/14 20:00 111 189 185 202 193 198 10/23/14 21:00 110 184 181 198 193 194 10/23/14 22:00 108 184 180 185 176 181 10/23/14 23:00 105 184 183 182 168 180 10/24/14 0:00 80 103 80 187 80 187 80 177 162 180 10/24/141:00 80 101 80 189 80 188 80 190 174 186 10/24/14 2:00 99 192 190 188 171 188 10/24/14 3:00 96 194 190 185 172 184 10/24/14 4:00 93 194 187 193 172 182 10/24/14 5:00 181 174 170 159 178 10/24/14 6:00 91 182 179 179 168 181 10/24/14 7:00 90 186 185 188 176 185 10/24/14 8:00 88 191 192 186 171 192 10/24/14 9:00 193 187 185 175 181 10/24/1410:00 87 185 184 186 178 185 10/24/1411:00 85 185 182 114 180 186 10/24/1412:00 80 85 80 185 80 182 80 115 168 172 10/24/1413:00 80 84 80 188 80 184 80 117 190 191 10/24/1414:00 190 186 88 188 194 10/24/14 15:00 184 182 183 183 10/24/14 16:00 187 188 178 182 10/2411417:00 83 188 191 184 185 10/24/14 18:00 188 186 186 188 10/24/1419:00 82 188 185 86 183 183 10/24/14 20:00 81 187 185 185 181 10/24/14 21:00 187 183 184 185 10/24/14 22:00 80 188 184 85 183 181 10/24/14 23:00 187 185 85 182 180 10/25/14 0:00 80 80 80 188 80 185 80 85 185 181 10/25/141:00 80 80 80 191 80 183 80 85 181 183 10/25/14 2:00 187 184 86 186 183 10/25/14 3:00 186 185 85 183 185 10/25/14 4:00 192 189 189 195 10/25/14 5:00 192 190 188 187 10/25/14 6:00 190 189 184 183 92 90 88 86 85 83 82 80 80 80 80 81 83 81 80 80 80 80 80 80 80 80 80 81 106 168 182 204 202 181 182 199 186 186 183 187 186 181 185 184 185 188 187 183 187 0 - e DateTime HOURLY DRYER PRODUCT TEMPERATURE DATA ( DRYER NUMBER) 10/25/14 7:00 81 189 188 85 184 190 184 10/25/14 8:00 188 183 85 185 183 185 10/25/14 9:00 186 181 182 183 185 10/25/14 10:00 188 185 187 191 184 10/25/1411:00 187 186 86 185 185 187 10/25/1412:00 80 80 80 188 80 184 80 86 180 182 80 182 10/25/1413:00 81 80 80 187 80 185 80 86 186 182 80 183 10/25/1414:00 84 186 183 87 183 183 184 10/25/14 15:00 188 183 183 185 187 10/25/1416:00 189 185 88 192 190 184 10/25/1417:00 83 193 190 188 186 192 10/25/1418:00 82 190 186 185 186 196 10/25/14 19:00 189 183 189 186 196 10/25/14 20:00 81 187 182 87 183 181 181 10/25/14 21:00 80 185 179 86 184 185 179 10/25/14 22:00 180 180 184 191 183 10/25/14 23:00 188 187 85 184 181 185 10/26/14 0:00 80 80 80 204 80 199 80 85 181 193 80 185 10/26/141:00 80 80 80 193 80 198 80 85 186 179 80 182 10/26/14 2:00 183 183 83 184 184 186 10/26/14 3:00 179 179 187 188 185 10/26/14 4:00 184 187 185 184 183 10/26/14 5:00 198 185 82 185 182 184 10/26/14 6:00 197 190 81 187 185 185 10/26/14 7:00 189 185 80 136 162 181 10/26/14 8:00 187 181 134 140 193 10/26/14 9:00 186 184 147 132 193 10/26/14 10:00 191 189 101 92 190 10/26/14 11:00 189 188 174 150 174 10/26/1412:00 80 80 80 187 80 184 80 80 191 183 80 183 10/26/1413:00 80 80 80 182 80 180 80 81 187 183 80 190 10/26/14 14:00 198 184 182 177 186 10/26/14 15:00 185 186 180 179 177 10/26/1416:00 183 185 82 186 184 185 10/26/14 17:00 205 195 198 198 196 10/26/1418:00 194 194 81 156 167 178 10/26/14 19:00 179 168 163 158 170 10/26/14 20:00 184 179 82 185 183 177 10/26/14 21:00 190 188 194 193 188 10/26/14 22:00 192 191 194 193 193 10/26/14 23:00 190 191 83 195 192 191 10/27/14 0:00 80 80 80 189 80 186 80 83 195 195 80 192 10/27/141:00 80 80 80 188 80 187 80 83 196 195 80 190 10/27/14 2:00 192 186 82 197 196 189 10/27/14 3:00 193 185 82 200 199 193 10/27/14 4:00 196 193 199 201 197 10/27/14 5:00 194 194 83 201 201 193 10/27/14 6:00 192 186 83 197 200 190 10/27/14 7:00 191 187 198 199 188 10/27/14 8:00 186 181 192 197 187 10/27/14 9:00 184 175 84 194 189 185 10/27/14 10:00 184 184 84 194 188 184 10/27/1411:00 185 183 83 155 152 178 ,i a HOURLY DRYER PRODUCT TEMPERATURE DATA DateTime I ( DRYER NUMBER) 10/27/14 12:00 183 180 163 160 191 10/27/1413:00 80 80 80 187 80 188 80 84 157 185 80 186 10/27/1414:00 190 196 86 203 199 189 10/27/1415:00 129 127 87 187 194 190 10/27/1416:00 99 109 90 188 188 81 189 10/27/14 17:00 93 102 150 153 133 185 10/27/1418:00 81 92 99 171 164 108 82 184 10/27/1419:00 80 94 103 183 204 153 193 10/27/14 20:00 92 158 182 191 191 178 184 10/27/14 21:00 88 186 168 196 177 183 185 10/27/14 22:00 152 195 196 168 179 175 182 10/27/14 23:00 191 196 199 182 182 182 83 180 10/28/14 0:00 196 193 190 193 182 186 83 185 10/28/141:00 80 175 80 189 80 184 80 183 146 193 83 185 10/28/14 2:00 168 186 181 188 121 193 188 10/28/14 3:00 208 186 184 187 115 195 190 10/28/14 4:00 175 192 188 189 114 198 82 189 10/28/14 5:00 185 192 187 192 129 199 81 190 10/28/14 6:00 183 190 183 191 114 198 80 189 10/28/14 7:00 179 188 180 185 106 198 185 10/28/14 8:00 183 181 179 181 101 192 182 10/28/14 9:00 178 181 113 174 98 189 177 10/28/1410:00 183 181 125 175 96 187 179 10/28/14 11:00 196 192 104 184 192 184 10/28/14 12:00 182 195 100 196 94 194 190 10/28/1413:00 80 179 80 183 80 100 80 192 94 195 80 190 10/28/1414:00 179 183 98 200 198 190 10/2811415:00 81 193 177 99 196 196 187 10/28/1416:00 80 188 185 99 193 192 183 10/28/1417:00 192 186 101 192 94 193 184 10/28/1418:00 198 185 100 172 94 174 160 10/28/14 19:00 199 182 183 182 161 166 10/28/14 20:00 193 194 190 201 94 198 185 10/28/14 21:00 174 199 183 167 93 190 199 10/28/14 22:00 170 173 191 185 92 194 184 10/28/14 23:00 194 196 192 191 93 192 186 10/29/14 0:00 203 207 205 195 202 186 10/29/141:00 80 178 80 193 80 179 80 183 93 197 80 183 10/29/14 2:00 176 184 184 181 91 191 182 10/29/14 3:00 183 183 185 180 90 189 184 10/29/14 4:00 185 184 182 184 89 187 186 10/29/14 5:00 186 185 189 186 192 192 10/29/14 6:00 185 189 194 191 196 194 10/29/14 7:00 185 184 189 206 90 197 197 10/29/14 8:00 188 194 194 188 89 199 191 10/29/14 9:00 188 194 198 184 193 185 10/29/1410:00 186 193 197 188 88 192 184 10/29/14 11:00 182 195 196 193 195 192 10/29/14 12:00 188 197 198 196 197 191 10/29/1413:00 80 188 80 200 80 203 80 197 88 198 80 194 10/29/1414:00 188 202 204 204 89 205 199 10/29/1415:00 10/29/1416:00 186 176 201 190 201 191 204 203 90 89 210 194 205 194 B Q CO - O 00 d t` ti CO M r 0 CO t� r 0 00 O r M cf CO CO d V M N N r N r r r M N N M d ti ti CO OD O In N T O O CA W 00 00 O 00 M O O O O 0) 0) 0) O O O O O O O O 0) O O O O O O O 0)T T r r N r r r ® 00 00 00 00 �W/ LL CO O CO 00 O O CO co W M to N Lo O LO O It 1` O t` LO LO CO CO M N Cl) 00 1� O M M M N CO CO I�t M LO r M N OD 1- N M r N LO 'V' N r- C0 00 W 00 00 00 M h 00 00 00 r- r- OD 00 00 00 00 t� O O C0 O O r- 1- O O O0 O O M I- r- 1- M O 00 00 OD 00 00 00 00 00 co CA O O O O r r T r r r r T r r r r r r r r T r r r T r r r r r T r T r r r T r r r r r T r T T T T T r r T r T r r T Co O 00 00 C0 LO LO r N M N 00 r N r LO 00 N O LO LO Ln 00 O r N 0) CO 00 CO '[- N r N r M N CO ti CO M T (0 0)0 CO 0)O 0) r- r- 0 0 0 m w I- 0 00 w 00 O wO 00 00 M M O O CO M O O CO O O 00 M OD Co co M M M M r r N r T T r r T N r N r r r r r r r r r r r r r r N r r r N N r N N WIL N CO co0)O r-� t- M N r M M 0 r CO 1- N It N M CO v Lo N Cr) 00 N r 0)N 0) 0 00 r- 'd' 00 LO 0) 'It CO O 0) 0) Cl) 0) d' LO LO fl- CO 00 CO 0) 0) 0) 1- CO r- O 00 1- r- tl- Cfl r- 00 00 CO M M O O M M M r- O � O O Mt- t- M M M M M M Cb I- 0000 O 00 t_ W O O O O O G W r T r r T N N r r T r T T r — — r T r r r T r T r r r N r T r r r r — — r r r r r r r r T r r r r r r T r W In co 00 00 00 D A/ V 00 LO IT LO O f- CO M— Cn 00 Cl) 0) 0) 00 00 0)N r N LO CO O� Ln CO N M LO N N't 0) LO CD d' O CO r I-- O It 00 LO CO 1� N N N N f- I- 0 w f-00000000O0C0000)00fl-000)LO000000m0)0)m0)0)m0000000000000000 0000Il-tl- 00000 fl-000Y)I-00f-0000O00)00I- 0 W r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r N N T r r IL r M O W W O N r r O O O a ® co N CO LO t- (0 O 0) 0) O co M 00 r r r T r T N W LL') qP O LO 'It r LO M M M CO O T r (D 0 M t- O O O O N 00 1- N r N LO OD Lo V LO 00 0) LLB t- LO qT CO O Cl) O M N Ln O CO 'I* LO t- cr) P- oo 00 OD 00 M O 00 00 M OD 00 00 00 00 00 00 00 00 0) 00 00 O O CA 00 M O0 00 00 M 00 OD O0 00 00 00 1,- co 0) 00 rl- 00 O O 00 I- CD 00 O O 00 00 P- C) O O O 00 00 00 00 J I- co Lo CO LA co O W O qt O r CO O d O Ln d' O Lo 00 O"t O co O Lo O M M LO M r LC) N r N O In r Il- M M V' O m 00 O t O N r- M 00 M M OD M M O 00 00 00 r, 00 C0 00 C0 C0 00 00 00 O 00 00 O rl- t- t- m N w M M W 00 tl- tl- O0 O 00 tl- t` 00 00 O O0 Cfl 00 O O O 00 00 T T T r r T r T r r r T r r r r r T r r r r r r r T r r r T r T T r r r T r N T r T r r r r T r T r r T r O co 00 m 00 Q: 0000000 O O O O O O O O O O O O O O O O O O O O O O O O O O 0OoOOOOOOo OoOOOOoOOo O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O 00 O O c- N M p r N M' i C2 CO t` 00 6 O r N M't m CO I- wO O c- N co O r N co 4 U) CO M O CD N CO 'IT L() CO I� CO � O T r N N N N T T r r T T r r r T N N N N r r r r r r r r r r N N 'd' . . . r .. ... .a..a..a. �' � r � � r 'd' V' V' V' Z � r T r r r T r \ \ \ \ \ \ \ \ \ \ T ..r r ..r T r T . r r r T \ \ \ \ \ \ \ \ \ \ r r r r r T T r T r r \ \ \ \ \ +d \ \ \ \ \ \ \ O O O O O O O O O O \ \ \ \ \ \ \ \ \ \ \ \ \ \ r r r r r r r r r r \ \ \ \ \ \ \ O O O O O O O MM M M MMMMMM O O O O O O O O O O O O O O r r r r r T r r r r r r M M M M M M M M M M � N N N N N N N\\\\\\\\\\ M M M M M M M M M M M M M M\\\\\\\\\\ M CM M M M M M M M M M M Q \ \ \ \ \ \ \ O O O O O O O O O O O O O O O \ \ \ \ \ \ \ \ \ \ \ \ \ \ O O O O O O O O O O \ \ \ \ \ \ \ \ \ \ \ \ O O O O O O CD CD O O O O CD O O O O O O O O O O O O r T r r r r T r r r T r r r T r r r r r r r r T T r T T r T r r T T r T r T r T r r T r T r T r r r r T T HOURLY DRYER PRODUCT TEMPERATURE DATA DateTime I ( DRYER NUMBER 10/31/14 23:00 I I 188 I I 190 I I 190 I I 197 I 193 I 190 I I 94 For Better Results. `Naturally. Milorganite Milorganite® North Carolina Exceptional Quality Biosolids Certification Permit for Distribution of Class A Residuals WQ0012980 We, Thomas A. Nowicki, Staff Attorney, Milwaukee Metropolitan Sewerage District, and Robert Moser, P.E., Operations Manager, Veolia Water Milwaukee LLC, certify that we have personally examined and are familiar with the submitted information. Based upon our inquiry of those individuals immediately responsible collecting the info . n, we believe the information is true, accurate, and complete. EDIDENRIDWR We certify that Milorganite®: BAN 2, 9 2015 (1) complied with the limits of 40 CFR 503.13(b).(3); Pe VNatgrQualitg� RjSec jon (2) was dried to achieve a pellet temperature exceeding 176'F/80`C when less than 10% moisture, as required for Class A pathogen destruction, according to 40 CFR § 503.32, Appendix B, B.2, and 15A NCAC 2T.1106(b)(3)(F); and (3) was dried to achieve greater than 90% solids, as required for vector attraction reduction, according to 40 CFR § 503.33(b)(8) and 15A NCAC 2T.1107(a)(8). We made this determination according to an environmental management system designed to ensure that qualified personnel properly gather and evaluate information regarding pollutant concentrations, pathogen reduction, and vector attraction reduction. We are aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment. Certified January 15, 2015: Thomas A. Nowicki, Staff Attorney Certified January /S-, 2015: Robert Moser, P..E., Operations'Manager Milorganite - MMSD 260 W. Seeboth Street Milwaukee, WI 53204 Phone: (414) 221-6810 (800) 287-9645 Fax: (414) 221-6818 www.milorganite.com ypG\p1NIENpFH� "OJ Noer s - - •Researcl�,Toundation - �AMFRFT rCS Parameter Units Highest. Day -Annual Average Federal Limit Arsenic mg/kg .21 .: 7.9 41 Cadmium mg/kg. 5.3 1.9 ..39 Chromium mg/kg: 380 238 Copper mg/kg :.340. 267 1,500 Lead..... mg/kg. 210 46 300 Mercury mg/kg: 0.84 10.25 17 Molybdenum mg/kg 18 11 75 Nickel... mg/kg. 120 37 420 Selenium mg/kg 5.9 0.5 100 Zinc mg/kg 11200 583 _ 2,800 TEQ* pg/g 23 9.8 PCB.Aroclors (total) mg/kg: 0.64 0.18 Milwaukee Metropolitan Sewerage District 260 West See6oth: Street, Milwaukee, Wl 53204 zj 1�► P A1NIN IRA. CIEW MEOW ALUMINUM ICP Dry wt. e 01/11/14 WMC2/14000475 4200 mg/kg D.W. e 7 e e 110 e B8. Annual IVl.ilorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 02/08/14 WMC6/14001578 5200 mg/kg D.W. 7 110 B8. SW846: 6010C MMSD 03/08/14 WMC10/14003247 6000 mg/kg D.W: 7 110 B8. SW846: 6010C MMSD 04/12/14 WMC15/14005643 5400 mg/kg D.W. 7 110 B8. SW846: 6010C MMSD 05/10/14 '" WMC19/14007579 11000 mg/kg D.W. 12 110 B8. SW846: 6010C MMSD 06/07/14 WMC23/14009882 10000 mg/kg D.W. 15 110 B8. SW846: 6010C MMSD 07/12/14 WMC28/14013005 8000 mg/kg D.W. 12 110 B8. SW846: 6010C MMSD 08/09/14 WMC32/14015986 5000 mg/kg D.W. 12 110 B8. SW846: 6010C MMSD 09/27/14 WMC39/14020976 5600 mg/kg D.W. 12 110 B8. SW846: 6010C MMSD 10/11/14 WMC41/14021279. 7300 mg/kg D.W. 12 110 B8: SW846: 6010C MMSD 11/08/14 WMC45/14023769 8100 mg/kg D.W. ]2 110 B8. SW846: 6010C MMSD 12/13/14 WMC50/14026279 4800 mg/kg D.W. 12 110 138. SW846: 6010C MMSD Avg: 6700 mg/kg D.W. (Milo) Ammonia in Fertilizer � . n Max: LOQ 11000'mg/kg D.W. e• Flags Analytical Method Lab 01/11/14 WMC2/14000475 0.2 % 0.11 0.37 AOAC (13) 2.065 MMSD 02/08/14 WMC6/14001578 0.22 % 0.11 0.37 AOAC (13) 2.065 MMSD 03/08/14 WMC10/14003247 0.2 % 0.11 0.37 AOAC (13) 2.065 MMSD 04/12/14 WMC15/14005643 0.2 % 0.11 0.37: AOAC (13) 2.065 MMSD 05/10/14 WMC19/14007579 0.15'% 0.11 0.37 . AOAC (13) 2.065 MMSD 06/07/14 WMC23/14009882 0.17 % 0.11 0.37 AOAC (13) 2.065 MMSD 07/12/14 WMC28/14013005 0.15 % 0.11 0.37,. AOAC (13) 2.065 MMSD 08/09/14 WMC32/1401,5986 0.18 % 0.11 0.37 " AOAC (13) 2.065 MMSD 09/27/14 WMC39/14020976 0.17 % 0.11 0.37 AOAC (13) 2.065 MMSD 10/11/14 WMC41/14021279 0.17 % 0.11 0.37 AOAC (13) 2.065 MMSD 11/08/14 WMC45/14023769 0.18 % 0.11 0.37 AOAC (13) 2.065 MMSD 12/13/14 WMC50/14026279 0.18 % 0.11 0.37 AOAC (13) 2.065 MMSD Avg: 0.18.6/0 Max: 0.22 j. Page 1 of 106 SYS/rptlMiloMonthly 1110113 tj Printed.• 1/8/1510:48 t - k 1 bu PAIN SlotACMINIMINNINT ARSENIC ICP METHOD Sample Date S I ample ID 01/01/14 DMO101/14000012 Result 11 mg/kg DM. LouoQ 1.8 Q. 2 Annual Milorganite Report January 1 tb December 31, 2014 ed SW846: 6010C MMSD 01/02/14 DMO102/14000039 it mg/kg DM. 1.8 2 SW846: 6010C MMSD 01/03/14 DM0,103/14000088 11 mg/kg D.W. 1.8 2 SW846:"6010C MMSD 01/04/14 DMO104/14000103 9.7 mg/kg D.W. 1.8 2 SW846: 6010C MMSD Ol/05/14 DM0105/14000122 M mg/kg D:W. 1.8 2 SW846: 6010C MMSD 01/06/14 DM0106/14000135 8.5 mg/kg D.W. '1.8 2 SW846: 6010C MMSD 01/07/14 DMO107/14000162 8.6 mg/kg D.W: 1.8 2 SW846: 6010C MMSD 01/08/14 DMO108/14000188 9.9 mg/kg D.W. 1.8 2 SW846: 6010C MMSD .Oi/b9/]4 DM0109/14000207 8.3 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/10/14 DM0110/14000430 11 mg/kg D.W. 1.8 2 SW846: 6010C : MMSD 01/11/14 DM0111/14000441 9.6 mg/kg D.W. 1.8.1 2 SW846: 6010C MMSD 01/12/14 DMO112/14000460 :10 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01%13/14 DM0113/14000473 10 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/14/14 DM0114/14000500 _ 10 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/15/14 DMO115/14000526 9.1 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/16/14 DM0116/14000545 8,6 mg/kg D;W. 1.8 2 SW846: 6010C MMSD 01/17/14 DMO117/14000560 9.5 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/18/14 DM0118/14000571 10 mg/kg D.W: 1.8 . - 2 SW846: 6010C MMSD 01/19/14 DM0119/14000590 11 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/20/14 DMO120114000603 9 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/21/14 DMO121/14000630 9 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/22/14 DM6122/14000656 9.1 mg/kg D.W. 1.8 2 Q21 SW846: 6010C MMSD 01/23/14 DMO123/14000675 9.8 mg/kg D.W. 1.8 2 "' SW846: 6010C MMSD 01/24/14 DMO124/14000690 9 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/25/14 DMO125114000923 9.5 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/26/14 DM0126/14000942 8.4 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/27/14 DMO127/14001095 10 mg/kg D.W. 1.8 2, SW846: 6010C MMSD 01/28/14 DMO128/14001122 12 mg/kg D.W. 1.8 2 SW846: 6010C MMSD, 01/29/14 DM0129/14001148. 11 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/30/14 DM6130/14001167 10 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 01/31/14 DMO131/14601182 8.2 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/01/14 DM0201/14001193 9.8 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/02/14 DM0202/14001430 12 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/03/14 DM0203/14001443 8.6 mg/kg D.W. 1.8 2 SW846: 6010C MMSD , 02/04/14 DM0204/14001470 -10 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/05/14 DM0205/14001498 9.8 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/06/14 Dmb206/14001517 8.1 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/07/14 DM0207/14001532 9.3 mg/kg D.W. 1.8 2 SW846: 6010C •MMSD 02/08/14 DM020,8114001543 11 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/09/14 DM0209/14001562 11 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/10/14 bM0210/14001576 11 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/i1/14 _ DM0211/14001811 9.6 ing/kg D.W. 1.8 2 SW846: 6010C MMSD 02/12/14 DM0212/14001837 7.8 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/13/14 DM0213/14001856 8.2 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/14/14 DM0214/14001871 9 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/15/14 DM0215/14001882 8.8 mg/kg D.W. 1.8 2 " SW846: 6010C MMSD 02/16/14 DM0216/14001893 8.6 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 5Y51rptlMi/oMontW Y 1/10/13 tj Page 2 of 106 Printed:1/8/1510:48 'MSD AMN'fps IRA ftwik U116,'ho ARSENIC ICP METHOD sample, Date sample ID 02/17/14 DM021W14001914 Re�ult 9 mg/kg D.W. LOP 1.8 LOO 11-Aflasts 2 Annual Milorganite Report January 1 to December 31, 2014 Analytical Method Lab SW846: 6010C MMSD 02/18/14 DM0218/14002002 8.9 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/19/14 DM0219/14002028 6.7 mg/kg D.W; 1.8 2 SW846:, 6010C MMSD 02/20/14 DM0220/14002101 9 mg/kg D.W. 1.8 2 SW846: 6010C MMSD o2/21/14 DM0221/14002181 9.5 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/22/14 DM0222/14002192 9.1 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/23/14 DM0223/14002211. 7.9 mg/kg D.W: 1,8 2 SW846:: 6010C MMSD 02/24/14 DM0224/14002224 11 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/25/14 DM0225/14002251 9.2 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/26/14 DM0226/14002310 8.8 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/27/14 DM0227/14002329 9.3 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 02/28/14 DM0228/14002350 10 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/O1/14 DM0301/14002921 10 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/02/14 DM0302/14002940. 8.9 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/03/14 DM0303/14002953' 11 mg/kg D.W.' 1.8 2 SW846: 6010C MMSD 03/04/14 DM0304114002986 9.6 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/05/14 03/06/14 DM0305/1400301'2 DM0306/14003182- 10 mg/kg D.W. 11 mg/kg D.W. 1.8 1.8 2 2 T SW846: 6010C - SW846' 6010C MMSD MMSD 03/07/14 DM0307/14003197 10 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03?08/14 DM0308/14003208 7.7 mg/kg D.W. 1.8 2 . SW846: 6010C MMSD 03/09/14. DM0309/i4003232 8.8 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/10/14 DM0310/14003245 9.4 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/11/14 DM0311/14003272 11 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/12/14 DM0312/14003300 9.3 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/13/14 DM0313/14003871 8.5 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/14/14 DM0314/14003886 10 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/15/14 DM0315/14003899 9.2 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/16/14 DM0316/14003918 9.1 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/17/14 DM0317/14003936 9.5 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/18/14 DM0318/14003963 9.5 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/1.9/14 DM0319/14004217 8.9 mg/kg D.W. 1.8 2., SW846: 6010C MMSD 03/20/14 DM0320/14004315 9.9 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/21/14 DM0321/14004330 9.6 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/22/14 DM0322/14004341 11 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/Z3/14 DM0323/14004360 9.2 m9/kg D.W. 1.8 2' SW846: 6010C MMSD 03/24/14 DM0324/14004461 8.7 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/25/14 DM0325/14004638 7.5 mg/kg D.W. :1.8 2 SW846: 6010C MMSD 03/26/14 DM0326/14004664 12 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/27/14 DM0327/1.4004683 If mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/28/14 DM0328/14004698 12 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/29/14 DM0329/14004889 11 mg/kg D.W. 1.8 2 w SW846: 6010C MMSD 03/30/14 DM0330/14004908 11 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 03/31/14 DM0331/14004921 13 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/61/14 DM0401/14004948 12 mg/kg D.W. ...1.8 2 SW846: 6010C MMSD 04/02/14 DMO402/14004974 14 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/03/14 DM0403/14004993 11 ring/kg D.W. 1.8 2. Q2. SW846: 6010C MMSD 04/04/14 DM0404/14005195 15 mg/kg D.W. 1.8 2 Q2. SW846: 6010C MMSD Page 3 of 106 SY5/rptIfOoMonthly 1110113 tj Printed., 11811510:46 Annual Milorganite Report f January 1 to December 31, 2014 iMSD PAW lu A C11W [VO WNBU ARSENIC ICP METHOD Sample Date Sample ID Result LOD LOQ Q. Flags Analytical Method Lab 04/05/14 DM0405114005206 13 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/06/14 DM0406/14005226 14 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/07/14 DM0407/14005240 13 mg/kg D.W. 1.8 2 Q2. SW846: 6010C MMSD 04/08/14 DM0408/14005267 12 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/09/14 DM0409/14005397 13 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/10/14 DM0410/14005416 14 mg/kg D.W. 1.8 2 Q2. SW846: 6010C MMSD 04/11/14 DM0411/14005434 14 mg/kg D.W. 1.8 2 Q2. SW846: 6010C MMSD 04/12/14 DM0412/14005605 13 mg/kg D.W. 1.8 2 AO. SW846: 6010C MMSD 04/13/14 DM0413/14005627 14 mg/kg D.W. 1.8 2: AO. SW846: 6010C MMSD 04/14/14 DM0414/14005641 15 mg/kg D.W. 1.8 2 AO. SW846: 6010C: MMSD 04/15/14 DM0415/14005668 2.6 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/16/14 DM0416/14005791 2.3 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/17/14 DM0417/14005815 3.3 mg/kg D.W 0.86 2 SW846: 6010C MMSD 04/18/14 DM0418/14006027 . 15 mg/kg D.W. 1.8 2 Q2. SW846: 6010C MMSD 04/19/14 DM0419/14006038 3.7 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 04/20/14 DM0420/14006057 3.3 mg/kg D.W. 0.86 2. SW846: 6010C MMSD 04/21/14 DM0421/14006127 3.1 mg/kg D.W. 0.86 2 SW846: 6010C„ MMSD 04/22/14 DM0422/14006154 16 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/23/14 DM0423/14006180 15 mg/kg.D.W. 1.8 2 SW846: 6010C MMSD 04/24/14 DM0424/1.4006339 .15 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/25/14 D.M0425/14006354 12 mg/kg D.W. 1.8 2 Q2. SW846: 6010C MMSD 04/26/14 DM0426/14006365 13 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/27/14 DM0427/14006384 14 mg/kg.D.W. 1.8 2 SW846: 6010C MMSD 04/28/14 DM0428/14006397 13 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 04/29/14 DM0429/14006454 13 mg/kg D.W. 1.8 2 Q2- SW846: 6010C MMSD 04/30/14 DM0430/14006482 16 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 05/01/14 DM0501/14006976 14 mg/kg D.W. 1.8 2 Q2. SW846: 6010C MMSD 05/02/14 DM0502/14006991 14 mg/kg D.W. 1.8 2 Q2. SW846: 6010C MMSD 05/03/14 DM0503/14007150 15 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 05/04/14 DMO504/14007169 14 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 05/05/14 DM0505/14007182 17 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 05/06/14 DM0506/14007209 16 mg/kg D.W. 1.8 2 SW846: 6010C MMSD 05/07/14 DMO507/14007235 17 mg/kg D.W. 1.8 2 Q2. SW846: 6010C MMSD 05/08/14 DMO508/14007254 15 mg/kg D.W. 1.8 .2 SW846: 6010C MMSD 05/09/14 DMO509/14007269 18 mg/kg D.W. 1.3 2 . SW846: 6010C MMSD 05/10/14 DM0510/14007280 4.1 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 05/11/14 DMO511/14007456 4 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 05/12/14 DM0512/14007469 3.1 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 05/13/14 DM0513114007551 15 mg%kg D.W. 1.3 2 Q2. SW846: 6010C MMSD 05/14/14 65 5114 DMO514/14007577 D-M0515/14007665 13 mg/kg D.W., 17 mg/kg D.W. 1.3 1.3 T 2 2 SW846: 6010C SW846: 6010C MMSD MMSD 05/16/14 DMO516114007680 18 mg/kg D.W. 1.3 2 Q2. SW846: 6010C MMSD 05/17/14 DM0517/14007691 14 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 05/18/14 DM0518/14007710 18 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 05/19/14 DMO519/14007764 16 mg/kg D.W. 1.3 2 AO. SW846: 6010C MMSD 05/20/14 DMO520/14007997 18 mg/kg D.W. 1.3 2.: SW846: 6010C MMSD 05/21/14 DM0521/14008023 15 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 5Y5/rptlMiloMonthly 1110113 JV Page 4 of 106 Printed. 11811510.48 J r Annual Milorganite Report MSDJanuary 1 to December 31, 2014 PAPIPS [I* A etWiR 1 11MU19 ARSENIC ICP METHOD Sample DaOD LOQ QA Flags Analytical Method Lab 05/22/14 DMO522/14008042 4.9 mg/kg D.W. 0.86 2' SW846: 6010C MMSD 05/23/14 DMO523/14008057 21 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 05/24/14 DM0524/14008291 18 mg/kg D.W. 1.3 2 SW846:6010C MMSD 05/25/14 DM0525/14008310 16 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 05/26/14 DMO526/14008323 17 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 05/27/14 D100527/14008646 16 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 05/26/14 DM0528/14008672 17 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 05/29/14 DM0529/14008691 17 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 05/36/14 DMO530/14008845 5.8 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 05/31/14 DM0531/14008856 5.8 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/01/14 DM0601/14009580 5.3 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/02/14 DM0602/14009593 5.8 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/08/14 DM0603/14009620 6.5 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/04/14 DM0604/14009635 4.1 mg/kg D.W. 1.4 2 SW846: 6010C MMSD 06/05/14 DM0605/14009654 5 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/06/14 DM0606/14009669 4.9 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/07/14 DM0607/14009844 4.7 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/08/14 DM0608/14009867 5.2 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/09/14 DM0609/14009880 5.4 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/10/14 DM0610/14009907 4.5 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/11/14 DM0611114010237 5.2 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/12/14 DMO612/14010256 5.1 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/13/14 DM0613/14010271 3.8 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/14/14 DM0614/14010282 3.7 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/15/14 DM0615/14010301 3 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/16/14 DM0616/14010319 2.6 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/17/14 DM0617114010346 3.6 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/18/14 DM0618/14010687 3.6 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/19/14 DM0619/14010706 4.5 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/20/14 DMO620/14010721 3.5 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/21/14 DM0621/14010732 3.3 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/22/14 DM0622/14010751 5.3 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/23/14 DM0623/14011513 4.5 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/24/14 DM6624/14011540 6 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/25/14 DM0625/14011566 7 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/26/14 DM0626/14011766 6.4 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/27/14 OM0627/14011781 5.3 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/28/14 DM0628/14011792 4.5 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/29/14 DM0629/14011811 5.4 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 06/30/14 DM0630/14011824 5.1 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 07/01/14 DM0701/14011851 4.9 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 07/02/14 DM0702/14011879 3.5 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 07/03/14 DM0703/14011898 3.8 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 07/04/14 DM0704/14011911 4.9 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 07/05/14 DM0705/14011924 5.2 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 07/06/14 DM0706/14011943 4.6 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 07/07/14 DM0707/14012196 5.4 mg/kg D.W. 0.86 2 SW846: 6010C MMSD Page 5 of 106 SY5/rptlMi/oMonth/y 1110113 tj Printed.- 1/8/1510:48 ti j m S D. P,s�i�tir3 (Gi d.Cllr�itk L9f�ll�HHi}fil ARSENIC ICP METHOD Sample bate gample ID Result LOD LOQ QA Flags Annual Milorganite Report January 1 to December 31, 2014 Afial�tical Method Lab 07/D8/14 DM0708/14012898 2.7 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 07/09/14 DM0709/14012926 3.9 mg/kg D.W. 0.86 2 SW846: 6010C MMSD . 07/10/14 bM0710/14012945 3 mg/kg D.W. 0.86 2 SW846: 601k: MMSD 07/11/14 DM0711/14012961 3.8 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 07/12/14 DM0712/14012971 < 1,3 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 07/13/14 DM0713/1401299,1 < 1.3 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 07/14/14 DM6714/14013004 < 1.3 mg/kg D.W. 1.3 2 Q3. SW846:M1.6t MMSD 07/15/14 DM0715/14013031 15 mg/kg D.W. 1.3 2, SW846: 6010C MMSD 07/16/14 DM0716/14013059 15 mg/kg D:W. 1.3 2. SW846: 6010C MMSD 07/17/14 DM0717/14013078 17 mg/kg D.W. ..1.3 2 SW846: 6010C MMSD 07/18/14 DM6718/14013295 13 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 07/19/14 DM0719/14013305 14 mg/kg D.W. 1.3 2.: SW846: 6610C 'MMSD 07/20/14 DM0720114013324 16 mg/kg D.W. 1.3 2 SW846: 6010C 'MMSD ' 07/21/14 DM0721/14013337 15 mg/kg D.W. 1.3 2 SW846: 60100 MMSD 07/25/14 DM0725/14013997 4.3 mg/kg D.W. 1.3 2 Q3. SW846: 6010C MMSD 07/26/14 DM0726/14614008 < 1.3 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 07/27/14 DM0727/14014027 4.2 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 07/28/14 DM0728/14014040 5.3 mg/kg D.W. 1.3 2 SW846:.6010C MMSD 07/29/14 DM6729/14014895 2.4 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 07/30/14 DM0730/14614923 4.7 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 07/31/14 DM0731/14014942 3.4 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 08/01/14 DMO801/14014957 4 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 08/02/14 DM0802/14014968 2.2 mg/kg D.W. 0.86 . 2 .. SW846: 6010C MMSD 08/03/14 DM0803/14014987 1.9 mg/kg D:W. 0.86 2 J. SW846: 6010C MMSD 08/04/14 DM0804/14015000 1.9 mg/kg D.W. 0..86 2 1. SW846: 6010C MMSD 08/05/14 DM0805/14015027 < 1.3 mg/kg D.W. 1.3 2 AO. SW846: 6010C MMSD 08/06/14 DMO806/14015405 < 1.3 mg/kg D.W. 1.3 2 AO, Q3. SW846: 6010C MMSD 08/67/14 DM0807/14615456 11 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 08/08/14 DM0808/14015471 < 1.3 mg/kg D.W. 1.3 2 AO. SW846: 6010C MMSD 08/09/14 DM0809/14015482' < 1.3 mg/kg D.W. 1.3 2 AO. SW846: 6010C MMSD 08/10/14 DM0810/14015966 1.4 mg/kg D.W. 1.3 2 AO, J. 'SW846: 6010C MMSD 08/11/14 DMO811/14015984 < 1.3 mg/kg D.W. 1.3 2 A0. SW846: 6010C MMSD 08/12/14 DM0812/14016011 4 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 08/13/14 DM0813/14016039 < 1.3 mg/kg D.W. 1.3 2 AO. SW846: 6010C MMSD 08/14/14 DM0814/14016058 < 1.3 mg/kg D.W. 1.3 2 AO, Q3. SW846: 6010C -MMSD 08/15/14 DM0815114016181 < 1.3 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 08/16/14 DMO816/14016192 < 1.3 mg/kg D.W. 1.3 2 A0. SW846::0010C MMSD 08/17/14 DM0817/140.16211 < 1.3 mg/kg D.W. 1.3 2 A0. SW846: 6010C MMSD 08/18/14 DM0818/14016290 < 1.3 mg/kg D.W. 1.3 2 A0. SW846: 6010C MMSD 08/19/14 DM0819/14016319 2.4 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 08/20/14 DMO820/14016347 < 1.3 mg/kg D.W: 1.3 2 AO. SW846: 6010C MMSD 08/21/14 DMO821/1.4016366 4 mg/kg D.W. 1.3 2.. AO, Q3. SW846: 6010C MMSD 08/22/14 DM0822/14016381 1.7 mg/kg D.W. 1.3 2 ]. SW846: 6010C MMSD 08/23/14 DMO823/14016392 1.4 mg/kg D.W. 1.3 2 J. _ SW846: 6010C MMSD 08/24/14 DM0824114016411 2.2 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 0$/25/14 DM0825%14016488 1.4 mg/kg D.W. 1.3 2: 3. SW846: 6010C MMSD OS/26/14 DM0826/14016515 1.4 mg/kg D.W. 1.3 2 A0, J. SW846: 6010C MMSD SYS/rptlM110Mo17th/y 1110113 of Page 6 of 106 Printed, • 11811510.48 M:SD P,i�1Nff3 f(t9A flfl�fR 0;1ir3:4fftffif ARSENIC ICP METHOD 08/28/14 DM0828/14016907 2.9 mg/kg D.W. 1.3 2 Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 08429/14 DM0829/14017671 5.5 mg/kg D.W. 1.3 2 Q3. SW846: 6010C MMSD 08/30/14 DM0830/14017682 6.5 mg/kg D.W. 1.3 2 SW846:.6010C MMSD 08/31/14 DMO831/14017701 4.3 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09/01/14 DMO901/14017714 5.8 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09/02/14 DM0902/14017871 6.3 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09/03/14 DM0903/14017886. 6.1 mg/kg D.W. 1.3 2 SW846:, 6010C MMSD 09/04/14 DM0904114017920 5 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09%05/14 DM0905/14017901 5.6 mg/kg D.W. 1.3 2 Q3. SW846: 6010C MMSD '09/16/14 DM0916/14019167 5.5 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09/17/14 DMO917/14019195 4.6 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09/18/14 DM0918/14019229 10 mg/kg D.W. 1.3 2. Q3. SW846: 6010C MMSD 09/19/14 DM0919/14019244 7.9 mg/kg DM. 1.3 2 SW846: 6010C MMSD 09/20/14 DM0920/14019255 6.6 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09/21/14 DMO921/14019274 7.9 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09/22/14 DM0922114019287 6.6 mg/kg D.W. 1.3 2. ..:SW846: 6010C MMSD 09/23/14 DM0923/14019778 5 mg/kg D:W. 1.3 2 SW846: 6010C MMSD 09/24/14 DM0924/14019806 6.2 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09/25/14 DM0925/14019825 4.6 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09/26/14 DM0926/14019840 7.6 mg/kg D.W. 1.3 2. Q3. SW846: 6010C MMSD 09/27/14 DM0927/14019851 6.2 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09/28/14 DMO928/14019870 6 mg/kg D.W.. 1.3 2 SW846:.6010C MMSD 09/29/14 DMO929/14019883 9.3 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 09/30/14 DM0930/14019909 12 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 10/01/14 DM1001/14019927 8 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 10/02/14 DM1002/14020572: 8.9 mg/kg D.W, 1.3 2 SW846: 6010C MMSD 10/03/14 DM1003/14020587 12 mg/kg D.W. 1.3 2 Q3. SW846: 6010C MMSD 10/64/14 DM1004/14020598 3.4 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 10/05/14 DM1005/14020617 4.4 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 10/06/14 DM1006/14020630- 3.7 mg/kg D.W, 0.86 2 SW846: 6010C MMSD 10/07/14 DM1007/14021108 3.4 mg/kg D.W. 0.86 2. SW846: 6010C MMSD 10/08/14 DM1008/14021160 2.2 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 10/09/14 DM1009/14021179 5 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 10/10/14 DM1010/14021194 _ 6.1 mg/kg D.W.. 0.86 2 SW846: 6010C MMSD 10/11/14 DM1011/14021244 6.4 mg/kg D.W. 1.3 •2:. AO. SW846: 6010C MMSD 10/12/14 DM1012/14021263 5 mg/kg D.W. 1.3 2 A0. SW846: 6010C MMSD 10/13/14 DM1013/14021276 5.9 mg/kg D.W. 1.3 2 A0, Q3. SW846:, 6010C MMSD 10/14/14 DM1014/14021304 6.7 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 10/15/14 DM1015114021332 7.4 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 10/16/14 DM1016/14021351 11 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 10/17/14 DM1017/14021787- 9.5 mg/kg D.W. 1.3 2 Q3. SW846: 6010C MMSD 10/18/14 DM1018/14021798 7.8 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 10/19/14 DM1019/14021817 8.5 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 10/20/14 DM1020/14021830 10 mg/kg D.W. 1.3 2 Q3. SW846: 6010C MMSD 10/21/14 DM1021/14021857 6.7 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 10/22/14 DM1022/14021885 8.6 mg/kg D.W. 1.3 2. SW846: 6010C MMSD 10/23/14 DM1023/14022266 6.9 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 5YS/rptimiloMonthly 1/10/13 tj Page 7 of 106 Printed: 1/8/1510:48 kMSD PAN'm lot A Rump woof ARSENIC.ICP: METHOD �adiple Datd �Sampfel I D 10/24/14 DM1024/14622273 l0/25/14 DM1025/14022286 8.3 mg/kg D.W. 1.3 2 id mg/kg D.W. 1.3 2 Annual Milorganite R6 port January 1 to December 31, 2014 SW846: 6010C MMSD SW846: 6010C MMSD 10/26/14 DMI:026/14022305, 8.8 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 10/27/14 DMI027/14022318 9.7 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 10/28/14 DM1028/14022409 7.4 -m"g/kg D.W. 1.3 2 Q3. SW846: 6010C MMSD 10/29/14 DM1.029/14022439 7.3 mg/kg D.W. .1.3 2 SW846: 6010C MMSD 10/30/14 DMI030/14022510 6.9 mg/kg D.W: :: :1.3 2 Q3. SW846: 6010C MMSD 10/31114 DM1031/14022525 9.5 mg/kg D.W. 1.3 2.. Q3. SW846: 6010C MMSD 11/01/14 DM1 1 bi/14022536 9.6 mg'/kg DM. 1.3 2 SW846: 6010C MMSD 11/02/14 DM1.102/14022555 10 mg/kg D.W., ...:1.3 2 .... . SW846: 6010C MMSD 11/03/14 DMI1103/14022568 9.1 mg/kg D.W: 13 2 SW846:-6010C MMSD 11/04/14 DMI104/14023111 9.3 mg/kg D.W. 1.3 2:. Q3. SW846: 6010C MMSD 1 1/d5/14 W110.5/14023139 10 mg/kg D.W. 1.3 2 SW846: 6010C -MMSD 11/06/14 DM1,106/14023158 8 mg/kg D.W. ::,1.3 2 SW846:.6010C MMSD 11/07/14 DM1:107/14023173 8.9 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 11/08g4 DM 1108/14023164 9.1 mg/kg D.W. 1.3 2 8W846: 6010C mMsb 11/09/14 DM1 i b9/14023203 9.2 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 11/10/14 DM1:1 10/14023767 10 mg/kg D.W, 13 2 SW846: 6010C MMSD 11/11/14 DMI:1 11/14023796 11 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 11/12/14 DM1112/14023876 8.9 mg/kg D.W. 1.3 2 SW846: 6010C MMSD I1/13/14 DMI 113/14023895 8.6 mg/kg D.W. 1.3 2 Q3. SW846: 6010C MMSD 11/14/14 bm.1.1 14/14023910 10 mg/kg D.W, 1.3 2 Q3. SW846: 6010C MMSD 11/15/14 DM1 115/14023929 8.3 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 11/16/14 DMI 116/1402394.8 9.5 mg/kg D.W. 1.3 2 SW846: 6010C MMSD MSD 11/17/14 DM1.1 17/14023961 11 mg/kg D.W. 1.3 2 Q3. SW846: 6010C MMSD 11/18/14 DMII 18/14024236 3.9 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 11/19/14 DMI 119/1402426.4 5.5 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 11/20/14 DM1 120/14024283 7.2 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 11/21/14 DM1121/14024302 8.5 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 11/22/14 DM1;122/14024313 6 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 11/23/14 DM1 123/14024393 2.8 mg/kg D.W. 1.3 2:. :'SW846: 6010C MMSD 11/24/14 DMI124/14024414 6.6 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 11/25/14 bm1:125/14024441. 7.5 mg/kg D.W. :::1.3 2 SW846: 6010C MMSD 11/26/14 bm1'126/14024469 4 mg/kg D.W. 1.3 2 SW846: 6010'C MMSD 11/27/14 DM1 127/1.4024529 6 mg/kg D.W. 1.3 .2 :'SW846: 6010C MMSD lf/28/14. DMI128/14024544 3.9 mg/kg D.W. 1.3 2. SW846: 6010C MMSD 11/29/14 DM.1129/14024555: 5.3 mg/kg D.W 1.3 2 SW846::6010 C MMSD 11/30/14 DM1 130/14024574 3.91 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 12/W/14 DM1201/1402460I 4.5 rh&g D.W. 1.3 2 SW846: 6010C MMSD 12/02/14 12/03/14 DMI.202/14025299 bm1.203/14025327. 5.1 mg/kg DM. 4.6 mg/kg D.W. 1.3 1.3 2 2 Q3. AO, 'Q3. 7 SW846: 6010C SW846: 6010C MMSD MMSD .12/04/14 DM1204114025346 3.7 mg/kg D.W. 1.3 2 AO. SW846: 6010C MMSD 12/05/14 DM1205/140253151 8.1 - mg/kg D.W. 1.3 2 AO, Q3. SW846: 6010C MMSD 12/06/14 DM1206/14025872 4.6 mg/kg D.W. :1.3 2 AO. SW846: 6010C MMSD 12/07/14 DM I I . 207/14025391 4.5 mg/kg D.W. 1:3 2 A6. SW846: 6010 . C MMSD 12/08/14 DM1208/14025404 5.8 mg/kg D.W. 1.3 2:: AO, Q3. SW846: 6010C MMSD 12/09/14 DM1209/14026170 3.7 mg/kg D.W. 1.3 2 AO, Q3. SW846: 6010C MMSD SYSIrptimlloMonthly 1110113 tj Page 8 of 106 Printed.• 11811510:48 pUlu Palms lot A awiP fV1Iian ARSENIC ICP METHOD Annual Milorganite Report January 1 to December 31, 2014 Sainple Date 12/10/14 Sampie 1p DM1210/14026198 Result 16 mg/kg D.W. &Ao 1.3 a� 2 e• SW846: 6010C MMSD 12/11/14 DM1211/1402621:7 2.4 mg/kg D.W. 1.3 2 AO. SW846: 6010C MMSD 12/12/14 DM1212/i4b26232 8 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 12/13/14 DM1213/14026243 9.1 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 12/14/14 DM1214/14026262 7.8 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 12/15/14 DM121.5/1402627:7 6.3 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 12/16/14 DM1'216/14026475 6.1 mg/kg D.W. 1.3 2 AO. SW846: 6010C MMSD 12/17/14 DM1217/14026503 7.2 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 12/18/14 DM1218/14026522 6.4 mg/kg D.W. 1.3 2 AO, Q3. SW846: 6010C MMSD 12/19/14 DM1219/14026537 9.3 mg/kg D.W. 1.3 2 AO, Q3. SW846: 6010C MMSD 12/20/14 DM1220/14026653 5.3 mg/kg D.W. 1.3 2 AO. SW846: 6010C MMSD 12/21/14 DM1221/14026672 5.4 mg/kg D.W. 1.3 2 _, AO. SW846: 6010C MMSD 12/22/14 DM1222/14026685 5.2 n4kg DX 1.3 2 AO, Q3. SW846: 6010C MMSD 12/23/14 DM1223/14026713 9.1 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 12/24/14 DM1224/14026741 5.3 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 12/25/14 DM1225/14,026760 6.7 mg/kg D.W. 1.3 2- SW846: 6010C MMSD 12/M/14 DM1226/14026777 5.8 mg/kg D.W. 1.3 2 SW846: 6010C MMSD 12/27/14 DM1221/14026788 < 0.86 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 12/28/14 DM1228/14026807 2.6 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 12/29/14 DM1229/14027031 2.4 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 12/30/14 DM1230/14027058 < 0.86 mg/kg D.W. 0.86 2 SW846: 6010C MMSD 12/31/14 DM1231/14027086 5 mg/kg D.W. A.3 2 SW846: 6010C MMSD Avg: 8 mg/kg D.W. BORON ICP Dry wt. lebate Samole ID Result Max: LOD LOQ 21 mg/kg D.W. 01/11/14 WMC2/14000475 15 mg/kg D.W. 1 5.1 6010B tAmerica Chia 02/08/14 WMC6/14001578 13 mg/kg D.W. 0.97 4.9 6010B ;tAmerica Chia 03/68/14 WMC10/14003247 15 mg/kg D.W. 1.2 5.9 6010E ;tAmerica Chia 04/12/14 WMC15/14005643 12 mg/kg D.W. 0.94 4.7 6010B ;tAmerica Chia 05/10/14 WMC19/14007579 10 mg/kg D.W. 1 5.1 6010B ;tAmerica Chia 06/07/14 WMC23/14009882 12 mg/kg D.W. 0.96 4.8 6010B ;tAmerica Chia 07/12/14 WMC28/14013005 13 mg/kg D.W. 0.99 5 6010B ;tAmerica Chia 08/09/14 WMC32/14015986 14 mg/kg D.W. 1 5.2 6010E ;tAmerica Chia 09/27/14 WMC39/14020976 17 mg/kg D.W. 1 5.2. 6010B ;tAmerica Chia 10/11/14 WMC41/14021276 16 mgkg D.W. 1 5 6010E ItAmerica Chia 11/08/14 WMC45/14023769 17 mg/kg D.W. 1.1 5.3 6010E ;tAmerica Chia 12/13/14 WMC50/14026279 19 mg/kg D.W. 1.1 5.3 6010B ;tAmerica Chia Avg: 14 mg/kg D.W. Max: 19.mg/kg D.W. 5Y51rpt1M11oMonth1y 1110113 tj Page 9 of 106 Printed., 1/8/1510:48 i PAtiTlW [ok A C[['t.'tk [68V:NNi[91 CADMIUM ICP METHOD Sample D. 01/61/14 DM0101/14000012 2.1 mg/kg D.W. .D 0.64 OQQ• 2 Flags Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 01%02/14 DM0102/14000039 2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/03/14 DM0103/14000088 2 mg/kg D.W. 6.64 2 J. SW846:;6010C MMSD 01/04/14 DM0104/14000103 2.1 mg/kg D.W. 0.64 2 SW846: 6010C MMSD Ol/65/14 DMO105/14000122 2.1mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/06/14 D100106/14000135 2 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 01/07/14 DM0107/14000162 2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD Ol/08/14 DMO108/14000188 1.9 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 01%09/14 DMO109/14000207 1:8 mg/kg D.W. 0.64 2' J. SW846: 6010C MMSD 01/10/14 DM0110/14000430 1.8 mg/kg D.W. 0.64 2 J. SW846: 6010C. MMSD 01/11/14 DM0111/14000441 2.2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/12/14 DM0112/14000460 2 nib/kg D.W. 0.64 2 SW846: 6010C MMSD, 01/13/14 DM0113/14000478 2.2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/14/14 DM0114/14000500 2.2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/15/14 DM0115/14000526 2.1 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/16/14 DMO116/14000545 2.1 mg/kg D.W. 0.64 2 SW846: 6010C MMSD Ol?17/14 DM0117/14000560 2:2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/18/14 DM0118/14000571 2.2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/19/14 DM0119/14000590 2.1 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/20/14 DMO120114000603 2,4 rrig/kg D.W. 0.64 2 SW846: 6010C MMSD 01/21/14 DMO121/14000630 2.2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/22/14 DMO122/14000656 2.3 mg/kg D.W. 0.64 - 2 SW846:.6010C MMSD 01123/14 DMO123/14000675 2.3 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01124/14 DMO124/14000690 2:3 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/25/14 DMO125/14000923 2.3 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/26/14 DM6126/14000942 2.2 mg/kg D.W. 0.64 2 " SW846: 6010C MMSD 01/27/14 DM0127/14001095 2.3 mg/kg D.W. 6.64 2, SW846: 6010C MMSD 01/28/14 DMO128114001122 2.4 rhg/kg D.W. 0.64 2 SW846: 6010C MMSD 01/29/14 DMO129/14001148 2.4 mg/kg D.W., 0.64 2 SW846: 6010C MMSD 01/30/14 DMO130/14001167 " 2.4 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 001/14 DM0131/14001182 2.2 mg/kg D.W. 0.64 .2 = SW846: 6010C MMSD 02/01/14. DM0201/14001193 2.2 ing/kg D.W. 0.64 2 SW846: 6010C MMSD 02/02/14 OM0202/14001430 2.2 mg/kg D.W. 0.64 2 SW846::6010C MMSD 02/03/14 DM0203/14001443 2.3 mg/kg D.W. 0.64 2 SW846: 6010C MMSD M/04/14 DM0204/14001470 2.1 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/05/14 DM0205/14001498 2.4 mg/kg D.W. 0.64 2 SW846: 6010C. MMSD 02/06/14 DM0206/14001517 2.1 mg/kg D.W. 0.64 2 SW846::6010C MMSD 02/07/14 DM0207/14001532 2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/08/14 DM0208/14001543 2.1 Mg/kg D.W. 0.64 2' SW846: 6010C MMSD 02/09/14 DMO209/14001562 2.2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/10/14 DM0210/l4001576 2.2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/11/14 DM02l l/14001811 2.2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/12/14 DM0212/14001837 2.3 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/13/14 DMO213/14001856 2.1 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/14/14 DM0214/14001871 2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/15/14 DM0215/14001882 2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/16/14 DM0216/14001893 SYS/rptiMi/oMonth/y 1/10/13 of 1.9 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD Page 10 of 106 Printed. 1/8/1510:48 r + PdAINIPS IN A CLLMR IN11480 CADMIUM ICP METHOD i 02/17/14 DM0217/14001914 Restsk, 2.1 mg/kg D.W. Y 0.64 • 0 2 Annual Milorganite Report January 1 to December 31, 2014msa SW846: 6010C MMSD 02/18/14 DM0218/14002002 2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/19/14 DM0219/14002028 1.9 mg/kg D.W., 0.64 2 it SW846: 6010C MMSD 02/20/14 DMO220/14002101 2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/21/14 DM0221114002181 2.2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/22/14 DM0222/14002192 2.1 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/23/14 DM0223/14002211 . 2.2 mg/kg D.W., 0.64 2 SW846:.6010C MMSD 02/24/14 DM0224/14002224 2.3 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/25/14 DM0225/14002251 2 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 02/26/14 DM0226/14002310 2.2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 02/27/14 DM0227/14002329 1.9 mg/kg D.W., 0.64 2 it SW846: 6010C MMSD 02/28/14 DM0228/14002350 2.1 mg/kg D.W. 0.64 2, SW846: 6010C MMSD 03/01/14 DM0301/14002921 2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 03/02/14 DM0302/14002940 2.1 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 03/03/14 DM0303/14002953 2.4 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 03/04/14 DM0304/14002986 2 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 03/05/14 DM0305/14003012 1.8 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/06/14 .. DM0306/14003182 1.8 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/07/14 DM0307/14003197 1.9 mg/kg D.W. 0.64 2 J. _ SW846:6010C MMSD 03/08/14 DM0308/14003208 1.7 mg/kg D.W. 0.64 2. J. SW846: 6010C MMSD 03/09/14 DM0309/14003232 1.9 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/10/14 DM0310/14003245 1.9 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/11/14 DM0311/14003272 2.1 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 03/12/14 DM0312/14003300 1.9 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/13/14 DM0313114003871 2.1 mg/kg D.W. 0.64 2 SW846: 6010C MMSD 03/14/14 DM0314/14003886 1.9 mg/kg D.W. 0.64 2 J. SW846:: 6010C MMSD 03/15/14 DM0315/14003899 1.8 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/16/14 DM0316/14003918 2 mg/kg D:W. 0.64 2 SW846: 6010C MMSD 03/17/14 DM0317/14003936 1.8 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/18/14 DM0318/14003963 1.7 mg/kg D.W. 0.64 .. 2 J. SW846: 6010C MMSD 03/19/14 DM0319/14004217 1.9 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/20/14 DM0320/14004315 1.7 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/21/14 DM0321/14004330 1.8 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/22/14 DM6322/14004341 1.8 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/23/14 DM0323/14004360 1.7 mg/kg D.W. 0.64 2, J. SW846: 6010C MMSD 03/24/14 DM0324/14004461 1.3 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/25/14 DM0325/14004638 1.3 mg/kg D.W. 0.64 2 J. SW846: 6016C MMSD 03/26/14 bm0326/14004664 1.3 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/27/14 DM0327114004683 1.4 Ong/kg D.W. 0.64 2' J. SW846: 6010C MMSD 03/28/14 DM0328/14004698 1.3 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/29/14 DM0329/14004889 1.5 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 03/30/14 DM6330/14004908 1.5 mg/kg D.W. 0.64 2 1 SW846: 6010C MMSD 03/31/14 DM0331/14004921 1.5 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/01/14 DM0401/14004948 1.6 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/02/14 DM0402/14004974 1.5 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/03/14 DM0403/14004993 1.9 mg/kg D.W. 0.64 2, J. SW846: 6010C MMSD 04/04/14 DM0404/14005195 1.7 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD SYS/rptlmmonth/y 1/10/13 tj Page 11 of 106 Printed., 11811510.48 VAINk3lot A CIDA R CiJU MINI CADMIUM ICP METHOD Samplia Date, Sample XD : 04/05/14 DM0405114005206 1.8 mg/kg D.W. 0.64 OQ 2:: Q& fl6gs 7. Annual Milorganite Report January 1 to December 31, 2014 Analytical Method- SW846: 6010C MMSD' 04/06/14 DM0406/i4OO5226 2 mg/kg D.W. 0.64 2 .3. SW846: 6010C MMSD 04/07/14 DMO407/14005240 1.8 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/08/14 DM0408/14005267 1.6 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD, 04/09/14 DM0409/14005397 1.6 mg/kg D.W. 0.64 2' J. SW846: 6010C MMSD 04/10/14 D.M0410/14oO5416 1.4 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/11/14 DMO411/14005434' 1.8 mg/kg D.W.• 0.64 2 J.. SW846: 6010C MMSD 04/12/14 DM0412/14005605 1,8 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/13/14 DM0413/14005627 1:6 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/14/14 DM0414/14005641 1.6 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/15/14 DMO415/14005668 1.6 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 01/16/14 DM0416/14005791 1.7 rrig/kg D.W. 0.64 2 _ . J. SW846: 6010C MMSD 04/17/14 DM0417/14005815 0.66 rr g/kg D.W. 0.14 2 J. SW846: 6010C MMSD 04/18/14 DM0418/14006027 1.5 mg/kg D.W. 0:64 2 J. SW846: 6010C MMSD 04/19/14 DM0419/14006038 0.62 mg/kg D.W. 0.14 2 1 SW846: 6010C MMSD 04/20/14 DM0420/14006057 0.65 mg/kg D.W. 0.14 2;.: J. SW846: 6010C MMSD 04/21/14. DM0421/14006127 0.66 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 04/22/14 DMO422/14006154 . 1.4 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/23/14 DMO423/14006180 1.6 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/24/14 DM0424/14006339 1.5 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/25/14 DM0.425/14006354 1.7 mg/kg D.W. 0.64. 2 J. SW846: 6010C• MMSD 04/26/14 DM0426114006365 1.7 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/27/14 DM0427/14006384 1.7 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/28/14 DM0428/14006397 1.8 mg/kg D.W. 0.64 2_ J. SW846: 6010C MMSD - 04/29/14 DM0429/14006454 1.3 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 04/30/14 DM0430114006482 1.4 mg/kg D.W. 0.64 2 J: SW846: 6010C MMSD OS/91/14 DM0501/14.006976 1.5 mg/kg D.W. 0.64 2.. .J. .SW846: 6010C MMSD 05/02/14 DM0502/14006991 1.3 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 05/03/14 DM0.503/14007150 1.5 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 05/04/14 DM6504/14007169 1.4 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 05/0/14 DM0505/14007182 1.3 mg/kg D.W. 0.64 2.: J. SW846: 6010C MMSD 05/06/14_ DM0506/14007209 1.3 rrig/kg D.W. 0.64 2 '1. SW846: 6010C MMSD 05/07/14 DM0507/14007235: 1.4 mg/kg D.W, 0.64 2 J. SW846: 6010C MMSD 05/08/14 DM0508/14007254 1.3 mg/kg D.W. 0.64 2 J. SW846: 6010C MMSD 05/09/14 D100509/14007269 1.3 mg/kg D,W. 0.22 '2 J. SW846: 6010C MMSD 05/10/14 DM0510/14007280 0.55 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 05/11/14 DM0511/14007456 0.61 mg/kg D.W. 0.14 2 J: SW846: 6010C MMSD 05/12/14 DM0512/14007469 0.7 mg/kg D.W. 0.14 2. .J. SW846: 6010C MMSD 05/.13/14 1)100513/14007551 1.2 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 05/14/14 DM0514/14007577 1.3 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 05/15/14 DM0515/14007665 1.4 mg/kg D.W: 0.22 2 J. SW846: 6010C MMSD 05/16/14 DM0516/14007680 1.7 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 05/17/14 DM0517/14007691 1.2 mg/kg D.W. 0.22 2 ]. SW846: 6010C MMSD OS/18/14 DM0518/14007710 1.2 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 05/19/14 DM0519/14007764 1.2 mg/kg D.W. 0.22 2 A01 J. SW846: 6010C MMSD 05/20/14 DM0520/14007997 1.4 mg/kg D.W. 0.22 2:. J. SW846: 6010C MMSD 05/21/14 DM0521/14008023 1.2 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD SY5/rptiftoMonth/y 1/10/13 tj Page 12 of 106 Printed: 11811510.48 MSD PdAINks f tit 4 CRIB OiAWNW1111 CADMIUM ICP METHOD Sample Date Sample ID 05/22/14 DMO522/14008042 kesult 0.67 mg/kg D.W. f6l) 0.14 • e 2 J. Annual Miaorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 05/23/14 DM0523/14008057 2 mg/kg D.W. 0.22 2 -1. SW846: 6010C MMSD 05/24/14 DM0524/14008291 2 mg/kg D.W._ 0.22 2 J. SW846: 6010C _ MMSD 05/25/14 DMO525/14008310 2 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 05/26/14 DM0526M4008323 2.2 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 05/27/14 DMO527/14008646 2 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 05/28/14 DM0528114008672 1.5 mg/kg D.W. 0.22 2 J: SW846:.6010C MMSD 05/29/14 DM0529/14008691 1.2 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD O5/30/14 DM0530/94008845 0:52 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD .. 05/31/14 DM0531/14008856 0.59 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/01/14 DM0601/14009580 0.68 mg/kg D.W. 0.14 2 1 SW846: 6010C MMSD 06/02/14 DM0602/14009593 0.5 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/63/14 DM0603/14009620 061 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/64/14 DM0604/14009635 0.47 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 06/05/14 DM0605/14009654 0.42 mg/kg D.W. 0.22 2 J. SW846:-6010C MMSD 06/06/14 DM0606/14009669 0.48 mg/kg D.W. 0.22 2. J. SW846: 6010C MMSD 06/07/14 DM0607/14009844 0.54 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 06/08/14 DM0608/14009867 0.4 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 06/09/14 DM0609/14009880 0.33 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 06/10/14 DM0610/1.4009907 0.41 mg/kg D.W. 0.22 2: J. SW846: 6010C MMSD .06/11/14 DM061.1/14010237 0.69 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/12/14 DM6612/14010256 0.77 mg/kg D.W.' ''0.14 2 J. SW846: 6010C MMSD 06/13/14 DM0613/14010271 0.7 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/14/14 DM0614/14010282 0,69 ing/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/15/14, DM0615/14010301 1.1 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/16/14 DM0616/14010319 0.61 mg/kg D.W: 0.14 2 J. SW846: 6010C MMSD 06/17/14 DM0617/14010346 0.53 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/18/14 _ DM0618/14010687 0,69 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/19/14 DM0619/14010706 0.78 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/20/14 DM0620/14010721 0.59 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/21/14 DM0621/14010732 0.63 mg/kg D.W. 0.14 2 1 SW846: 6010C MMSD 06/22/14 DM0622/14010751 0:72 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/23/14 DM0623/14011513 0.67 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/24/14 DMO624/14011540 0.82 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/25/14 DM0625/140115a6 0.68 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/26/14 DM0626/14011766 0.86 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/27/14 DM0627/14011781 0.63 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/28/14 DM0628/14011792 0.74 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/29/14 DM0629/14011811 0.66 rng/kg D.W. 0.14 2 J. SW846: 6010C MMSD 06/30/14 DM0630/14011824 0.73 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 07/01/14 DM0701/14011851 0.63 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 07/02/14 DM0702/14011879 0.71. mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 07/03/14 DM0703/14011898 0.68 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 07/04/14 DM0704/14011911 0.71 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 07/05/14 DM0705/14011924 0.69 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 07/06/14 DM0706/14011943 0.74 mg/kg D.W. 0.14 2. J. SW846: 6010C MMSD 07/07/14 DM0707/14012196 0.66 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD SYSIrptSMiloMonthly 1110113 g Page 13 of 106 Printed: 11811510.48 r-,iMSD. VAIN06 101 A Elite [VOINNIIII CADMIUM ICP METHOD SaM pie. D -ate samplew 0/69/14 DM0708/14012898 07/69/14 DM0709/14012926 0.76 mg/kg D.W. 0.14 0.88 Mg/kg D.W. 0.14 2 1 Anh.uad. MilorganiteReport January 1 to December 31, 2014 iiiWii 6010C SW846: 6010C MMSD 07/10/14 DM0710/14012945 .0.69 mg/kg D.W.. 0.14 2 J. SW846: 6010C MMSD 07/11/14 DMO711/14012961 0.84 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 07/12/14 DM0712/14 . 012971 1 mg/kg D.W. 0.22 2.' :]. SW846: 6010C mkm 07/13/14 D.MO.713/14012991 0.96 mg/kg D.W. .0.22 2 1 SW846: 60.10.C. MMSD 07/14/14 DM0714/14013004 1 mg/kg D.W.: 0.22 2 1.: SW846: 6010C MMSD 07/15/14 DM0715/14013031 0.93 mg/kg D.W. 0.22 .2 . . . SW846: 6010C MMSD 0/16/14 DM0716/14-013059 0.98 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 07/17/14 QM0.717/14013078 0.84 mg/kg D.W. :0.22, 2 J. SW846: 601-0C: MMSD 07/18/14 DM0718114013295 1.1 mg/kg D.W.= 0.22 2 J. SW846::60WC MMSD 07/19/14 DM0719/14013305 1.3 mg/kg D.W. 0.22' 2:_ .3. :,:SW846: 6010C MMSD .07/20/14 DM0720/i4613324 1.2 mg/kg D.W. 0.22 2 ::3. SW846: 6010C MMSD 07/21/14 'DM0721/14013337 1.6 mg/kg D.W. .0.22 2 1.. SW846: 6010.C. MMSD 07/25/14 DM0725/14013997 1.5 mg/kg D.W. 0.22 2 1., SW846: 6010C MMSD 07/26/14 DM0726/14014008 1.8 mg/kg D.W. 0.22 2:, SWI 846: 6010C MMSD 07/27/14 DM0727/14014027 1.3 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 07/28/14 bM0.728/14014040 1.3 mg/kg D.W. 0.22 2 1 SW846: 6010C MMSD 07/29/14 DMO729/14014895 1.5 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD .07/30/14 DM0730/14014923 1.3 mg/kg D.W. 0.22 2 .3. sw846: 6010C MMSD 07131/14 DM0731/14014942 I mg/kg D.W. 0.22 SW846: 6010C MMSD 08/01/14 bm0.801/14014957 1.4 mg/kg D.W. 0.22 2 3. SW846: 6010C MMSD 08/02/14 DMO802114014968 0.7,mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 08/03/14 DM0803/14014987 0.64 mg/kg D.W. 0.14 2:- J. SW846: 6010C MMSD 08/04/14 DM0804/14015000 0.71 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 08/05/14 DM0805/14015027 0.95 mg/kg D.W. 0.22 2 J. SW846: 6016C MMSD 08/06/14 DM0806/14015405 0.86 mg/kg D.W. 0.22 2. J. ..SW846: 6010C MMSQ. 08/07/14 DMO807/14015456 1 mg/kg DA 0.22 2 J. sw846: 6010C MMSD 08/08/14 DMO808/14015471 1.2 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 08/09/14 DM0809/14015482 1.7 mg/kg D.W. 0.22 2 3: SW846:'6010C MMSD 08/10/14 DMO810/14015966 1.2 mg/kg' D.W. 0.22 2 J. !.SW846: 6010C MMSD 08/il/14 DM0811/14ol5984 1.2 mg/kg D.W. 0.22 SW846: 6010C MMSD 08/12/14 DMO812/14016011 1.1 mg/kg D.W. b.22 2 J. SW846:.6010C MMSD 08/13/14 DM0813/14016039 1.1 mg/kg D.W. 0.22. 2 J. SW846: 6010C MMSD 08/14/14 DMO814/14016058 1.3 mg/kg D.W. 0.22 2:. 'j. ':SW846: 6010C MMSD 08/15/14 DM0815114016181 1.3 mg/kg D.W. 0.22 2 . J. SW846: 6010C MMSD 08/16/14 bM0816/14016192 1.4 mg/kg D.W. 0.22 2 J. SW846:-6010t MMSD 08/17/14 DM0817/14.016211 1.3 mg/kg D.W. 0.22. 2 1 SW846: 6010C MMSD, 08/18/14 DM0818/1401,6290 1.2 mg/kg DW 0.22 2' J. SW846: 6010C MMSD 08/19/14 DM0819/140I6319 1.3 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 08/20/14 bM0820/14016347 1.3 mg/kg D.W. 'b.22 2 J. SW846:-6016t MMSD 08/2I/14 DM0821/14016366 1.4 mg/kg D.W. 0.22 .2.:: J. ::SW846: 6010C MMSD 08/22/14 DM0822/14016381 1.1 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 08/23/14 DMO823/14016392 1.4 mg/kg D.W. :.0.22 2 J. SW846: 6010C MMSD 08/24/14 DMO824/14016411 1.5 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 08/25/14 DM0825/14016488 1.4 mg/kg D.W. 0.22 2 :3. SW846: 6010C MMSD 08/26/14 DM0826/14016515 1.3 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD SY51rptmlomonthly 1110113 Y Page 14 of 106 Printed: 11811510.48 df Annual Milorganite Report January 1 to December 31, 2014 w P.4118113In A CtRu tolmsw1hr CADMIUM ICP METHOD Sample D. ao �� •• 08/28/14 DM0828/14016907 1.4 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 08/29/14 DM0829114017671 1.3 mg/kg D:W. 0.22 2 J. SW846: 6010C MMSD 08/30/14 DM0830/14017682 1.7 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 08/31/14 DM0831/14017701 1.7 mg/kg D.W. 0.22 2 J: SW846: 6010C MMSD 09/01/14 DM0901/14017714 1.9 mg/kg D.W. 0.22 2J. SW846: 6010C MMSD 09/02/14 DMO902/14017871 1.6 mg/kg D:W. 0.22 2 J. SW846: 6010C MMSD 09/03/14 DM0903/14017886. 1.5 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/04/14 DMb904/14017920 1.6 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/05/14 DM0905/14017901 1.4 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/16/14 DMO916/14019167 1.8 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/17/14 DMO917/14019195 1.5 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/18/14 DM6918/14019229 1.4 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/19/14 DM0919/1401.9244 1.5 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/20/14 DMO920/14019255 1.4 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/21/14 DM0921/14019274 1.4 mg/kg D.W. 0.22 2 J: SW846::6010C MMSD 09/22/14 DM0922/14019287 1.5 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/23/14 DM0923/14019778 1.4 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/24/14 DM0924/14019806 1.2 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD T 09/25/14 DM0925/14019825 1.4 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/26/14 DM0926/14019840 1.5 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/27/14 DM0927/14019851 1.6 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/28/14 DM0928/14019870 1.6 mg/kg D.W., 0.22 2 J. SW846: 6010C MMSD 09/29/14 DMO929/14019883 1.7 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 09/30/14 DMO930/14019909 1.4 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 10/01/14 DM1001/14019927 1.4 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 10/02/14 DM1002/14020572 1.5 mg/kg D.W. 0.22 2 J. SW846: 6010C MMSD 10/03/14 DM1003/14020587 2.9 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 10/04/14 DM1004/14020598 0:46 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 10/05/14 DM1005/14020617 0.6 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 10/06/14 DM1006/14020630 0.59 mg/kg D.W: 0.14 2 J. SW846: 6010C MMSD 10/07/14 DM1007/14021108 0.62 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 10/08/14 DM1008/14021160 0.64 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 10/09/14 DM1009/14021179 0.73 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 10/10/14 DM1010/14021194 0.69 mg/kg D.W: 0.14 2 J: SW846: 6010C MMSD .10/11/14 DM9011/14021244 3.8 mg/kg D.W. 0.22 2. SW846: 6010C MMSD 10/12/14 DM1012/14021263 3.9 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 10/13/14 DM1013/14021276 3.9 mg/kg D.W, 0.22 2 SW846: 6010C MMSD 10/14/14 DM1014/14021304 4 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 10/15/14 DM1015/14021332 3.6 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 10/16/14 DM1016/14021351 3.9 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 10/17/14 DM1017/14021787 3.6 mg/kg D.W. T0.22 2 SW846: 6010C MMSD 10/18/14 DM1018/14021798 3.3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 10/19/14 DM1019/14021817 3.7 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 10/20/14 DM1020/14021830 3.5 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 10/21/14 DM1021/14021857 3.7 mg/kg D.W: 0.22 2 SW846: 6010C MMSD 10/22/14 DM1022/14021885 3.6 mgft D.W. 0.22 2 SW846: 6010C MMSD 10/23/14 DM1023/14022256 3J mg/kg D.W. 0.22 2 SW846: 6010C MMSD Page 15 of 106 SY5/fptlM1/oMonth1y 1110113 tj Printed., 1/8/1510:48 4 Annual Milorganite Report January 1 to December 31, 2014 Pn*as Jut A. MOR C1i044r CADMIUM ICP METHOD Sample p p Result LOD LOQ 1 Flags Analytical Mettsod 10/24/14 DM1024/1:4022273 3.8 mg/kg D.W. 0.22 2_ SW846: 6010C MMSD 10/25/14 DM1025/14022286 3.8 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 10/26/14 DM.1026/14022305 3.7 mg/kg D.W. . 0.22 2 SW846: 6010C MMSD 10/27/14 DM1027/14022318 3.2 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 10/28/14 DM1028114022409 3.1 mg/kg D:W. 0.22 2 SW846: 6010C MMSD 10/29/14 DM 1 029/14022439 3 mg/kg D-.W. 0.22 2 SW846: 6010C. MMSD 10/30/14 DM1-030/14022510 3.4 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 10/31/14 DM1031/14022525 4mg/kg D.W. 0.22 2• SW846: 6010C MMSD 11/01/14 DM1101/14022536 3.6 mg/kg D:W. 0.22 2 SW846: 6010C MMSD 11/02/14 DM1102/14022555 3.6 mg/kg D.W.. .. 0.22 2 SW846: 6010C MMSD 11/03/14 DM1103/14022568 3.9 mg/kg D.W: 0.22 2 SW846: 6010C MMSD 11/04/14 DM1104/14023111 3.7 mg/kg D.W. 0.22 ?;; SW846: 6610C MMSD 11/05/14 DM1105/14023139 3.5 mg/kg D.W. 0.22 2 SW846: 6010C " MMSD 11/06/14 DM1106/14023158 3.7 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 11/07/14 DM1107/14023173 3.6 mg/kg D.W. 0.22 Z SW846: 6010C MMSD 11/60/14 DM1108/14023184 3.7 m4/kg D.W. 0.22 2' SW846: 6010C MMSD 11'/09/14 .. DM1109/14023.203 3.7 mg/kg D.W. 0.22 2. SW846: 6010C MMSD . 11/10/14 DM1110/14023767 3.8 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 11/11/14 DM.1111/14023796 3.9 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 11j1'2/14 DM1112/14023876 4 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 11/13/14 DM1,113/14023895 3.6 mg/kg D.W. 0.22 2 SW846: 60.10C MMSD 11/14/14 DM1114/14023910 4 mg/kg D.W; . 0.22 2 SW846: 6010C MMSD 11/15/14 DM1115/14023929 3.4 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 11'/16/14 DM1 1 16/14023948 3.3 mg/kg D.W. 0.22 2' SW846: 6010C MMSD 11/17/14 DM1.117/14023961 5.3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 11/18/14 DM4118/14024236 3.8 mg/kg D.W. : 0.22 2 SW846: 6010C MMSD 11/19/14 DM1119/14024264 3.5 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 11/26/14 DM1120/1.4024283 3.7 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 11/21/14 DM11121/14024302 3.6 mg/kg D.W. O.Z2 2 SW846:.6010C MMSD 11/22/14 DM1.122/14024313 4.2 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 11/23/14 DM1123/14024393 3.9 mg/kg D.W. 0.22 2: SW846: 6010C MMSD 11%24/14 DM1I24/14024414 4.2 mg/kg D.W. 0.22 '2 SW846: 6010C MMSD 11/25/14 DM1125/14024441- 3.8 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 11/26/14 DM1126/14024469 3.2 mg/kg D.W. 0.22. 2 SW846: 6010C MMSD 11/27/14 DM1127/14024529 3.3 mg/kg D.W. 0.22 .2 SW846: 6010C MMSD .: 11/28/14 DM1128/14024544 3.4 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 11/29/14 " DM1,129/14024555 3.2 mg/kg D.W. 0.22 2 SW846::6010C MMSD 11/30/14 DM1130114024574 3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD inbi/m DM1201/14024601 3.2 mg/kg D.W. 0.22 2 SW846: 6010C MMSD :. 12/02/14 DM1202/14025299 2.9 mg/kg D.W., 0.22 2 SW846: 6010C MMSD 12/03/14 DM1203/14025327 3 mg/kg D.W: 0.22 2 SW846: 6010C MMSD 12/04/14 DM1204/14025346 3.3 mg/kg D.W. 0.22 2. ... SW846: 6010C MMSD nm/14 DM1205/14025361 3.1 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/06/14 DM1206/14025372 3.5 mg/kg D.W. '.0.22 2 SW846:, 6010C MMSD 12/07/14 DM1207/14025391 3.3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/oB/14 DM1208/14025404 3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/09/14 DM1209/14026170 3.3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 5Y5/rpt1Ni10M0nth/y 1110113 tj Page 16 of 106 Printed: 11811510:48 a f MSD PAINIiS IAt A C[[sx�tk [eiEt�atllNl CADMIUM ICP METHOD Sample Date sample ID 12/10/14 DM1210/14026198 Result 3.1 mg/kg D.W. ibDLOP 0.22 2 ®• Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 12/11/14 DM1211/14026217 2.8 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/12/14 DM1212/14026232 3.3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/13/14 DM1213/14026243 3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/14/14 DM1214/14026262 3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/15/14 DM1215/14026277 3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/16/14 DM1216/14026475 3 mg/kg D.W., 0.2Z 2 SW846:.6010C MMSD 12/17/14 DM1217/14026503 3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/18/14 DM1218/14026522 3 mg/kg D.W. 0.22 2-: SW846: 6010C MMSD 12/19/14 DM1219114026537 3.5 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/20/14 DM1220/14026653 • 3.1 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/21/14 DM1221/14026672 3.1 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/22/14 DM1222/14026685 3.3 m0/kg D.W. 0.22 2 SW846: 6010C MMSD 12/23/14 DM1223/14026713 3.3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/24/14 DM1224/14026741 3.6 mg/kg D.W. '0.22 2 SW846: 6010C MMSD 12/25/14 DM1225/14026760 3.2 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/M/14 DM1226/14026777 3.3 mg/kg D.W. 0.22 2 SW846: 6010C MMSD 12/27/14 DM1227/14026188 0.62 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 12/28/14 DM1228/14026807 0.68 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 12/29/14 DM1229/14027031 0.79 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 12/30/14 DM1230/14027058 0.67 mg/kg D.W. 0.14 2 J. SW846: 6010C MMSD 12/31/14 DM1231/14027086 3.2 mg/kg D.W. 0.22 2 SW846: 6010C MMSD Avg: 1.9 mg/kg D.W. CHROMIUM ICP Dry wt: SampleDate Sample IDResult Max: LOD LOQ 5.3 mg/kg D.W. " QA Flags Analytical Lab 01/11/14 WMC2/14000475 220 mg/kg D.W. 0.58 2.1 SW846:'6010C MMSD 02/08/14 03/08/14 WMC6/14001578 WMC10/14003247 220 mg/kg D.W. 230 mg/kg D.W.0.58 0.57 2.1 2.1 SW846: 6010C SW846: 6010C MMSD MMSD 04/12/14 WMC15/14005643 180 mg/kg D.W. 0.57 2.1 SW846: 6010C MMSD 05/10/14 06/07/14 WMC19/14007579 WMC23/14009882 210 mg/kg D.W. 220 mg/kg D.W. '0.62 0.26 2.1 2.1 SW846: 6010C SW846: 6010C MMSD MMSD 08/09/14 09/27/14 10/11/14 11/08/14 12/13/14 WMC28/14013005 200 mg/kg D.W. 0.62 2.1 WMC32/14015986 WMC39/14020976 WMC41114021279 WMC45/14023769 WMC50/14026279 Avg: :240 mg/kg D.W. SYS/rptlMi/oMonth/y 1/10/13 tj SW846: 6010C MMSD 230 mg/kg D.W. 0.63 2.2 SW846: 6010C MMSD 380 mg/kg D.W. 0.62 2.1 SW846: 6010C MMSD 300 mg/kg D.W. 0.62 2.1 SW846: 6010C MMSD 230 mg/kg D.W. 0.62 2.2 SW846: 6010C MMSD 240 mg/kg D.W. 0.62 2.1 SW846: 6010C MMSD Max: 380:mg/kg D.W. Page 17 of 106 Printed., 1/8/I510:48 Annual Milorganite Report M 5 D January December ry 1 to De m er 31, 2014: Pd�1MfR3 f 4h d SlC49fk t�'dlei.WNthT COBALT ICP Dry wt. Sample D, .o Oo e• Flags Analytical Method 'Lab OS/11/14 .. WMC2/14000475. 370 mg/kg D.W. 0.12 If , B8, Q2, Q3. SW846: 6010C MMSD 02./08/14. wmm14001578 130 mg/kg D.W. 0.12 2.1. B8, Q2. SW846: 6010C MMSD m/OR/14 WMC10/14003247 52 ma/ka D.W. 6.12 2.1 B8, Q2. SW846:'6010C MMSD 05/10/14 WMC19/14'1007579 26 mg/kg D.W. 0.17 2.1' B8, Q3. SW846: 6010C MMSD 06/07/14 WMC23/14009882 20 mg/kg D:W. 0.41 2.1 B8. SW846: 6010C . MMSD 07/12/14 WMC28/14013005 12 mg/kg D.W. "6.17 : 2.1 B8, Q2.,: SW846::6010C MMSD 08/09/14 WMC32/14015986 16 mg/kg D.W. 0.17" 2.2; B8, Q2. SW846: 6010C MMSD 09/27/14 WMC39114020976 7.4 mg/kg DA 0.17 2.1 ' 68, Q2. SW846: 6010C MMSD 10/11/14 WMC41/14021279 8.9 mg/kg D.W. 0.17 2.1 B8, Q3. .: SW846: 6010C MMSD 11/08/14 WMC45/14023769 5.9 mg/kg D.W. 0.17 2.2 B8, Q2.: SW846: 6010C MMSD 12/-13/14 WMC50/14026279 7.3 mg/kg D.W. 0.17 2A:- B8. SW846: 6010C MMSD Avg: 60 mg/kg D.W. .. SYS/rptlMi/oMonth/y 1/10/13 tj Max: 370 mg/kg D.W. Page 18 of 106 Printed* 11811510:48 m j NO m L PdAIN(B IRA C.((g (10 iteNM(N( COPPER ICP METHOD Date 4amplo,IP Result Lbb LOQ QAPla`gs Annual Milorganite Report January 1 to December 31, 2014 Analytical Method LAb 01/01/14 DM0101/14000012 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/02/14 DMO102/14600039 270 mg/kg D.W. 1.4 41 SW846: 6010C MMSD 01/03/14 DMO-103/14000088 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/04/14 DMO104/14000103 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD Ol/05/14 DM0105114000122 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/06/14 DM0106/14000135 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/07/14 DM0107/14000162 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/08/14 DM0108/14000188 290 mg/kg D.W. 1.4 4 SW846: 6016C MMSD 01/09/14 DM0109/14000207 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/10/14 DM0110/14000430 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/11/14 DM0111/14000441 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/12/14 DM0112/14000460 290 mg/kg D.W. 1.4 .4 SW846: 6010C MMSD 01/13/14 DM0113/14000473 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/14/14 D.M0114/14000500 300 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/15/14 DM0.115/14000526' 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/16/14 DM0116/14000545 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/17/14 DM0117/140o0560 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/18/14 DM0118/14000571 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/19/14 DMO119/14000590 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD OS/20/14 DMO120/14000603 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/21/14 DMO121/14060630 270 mg/kg D.W. 1.4 4 A0. SW846: 6010C MMSD 01/22/14 DMO122/14000656 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/23/14 DMO123/14000675 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD . OS/24/14 DMO124/14000690 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/25/14 DMO125/14000923 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/26/14 DMO126/14000942 270 mg/kg D.W.. 1.4 4 SW846:.6010C MMSD 01/27/14 DMO127/14001095 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/28/14 DM0128/14001122 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/29/14 DMO129/14001148 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/30/14 DMO130/14001167 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 01/31/14 DMO131/14001182 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/01/14 DM0201/14001193 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/02/14 DM0202/14001430 286 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/03/14 DM0203/14001443 280 mg/kg.D.W. 1.4 4 SW846: 6010C MMSD 02/04/14 DM0204/14.001470 250 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/05/14 DM0205/14001498 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/06/14 bw.206/14001517 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/07/14 DM0207/14001532 260 mg/kg D.W. 1.4. 4 SW846: 6010C MMSD 02/08/14 DM0208/14001543 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/09/14 DM0209/14001562 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/10/14 DM0210/14001576 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/11/14 DM0211/14001811 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/12/14 DM0212/14001837 270 n4kg D.W. 1.4 4 SW846: 6010C MMSD 02/13/14 DM0213/14001856 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/14/14 DM0214/14001871 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/15/14 DM0215/14001882 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/16/14 DM0216/14001803 5Y5/rpt1Mi10Month1y 1110113 tj 250 mg/kg D.W. 1.4 4 SW846: 6010C MMSD Page 19 of 106 Printed- 1/811510:98 MS PAIN' ruq k ctwik mamma COPPER ICP METHOD 02/17/14 DM0217/14001914 240 mg/kg D.W. 1.4 4:' Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 02/18/14 DM0218/14002002 240 mg/kg D.W. 1.4 4 SW846: 6010C MMSD, 02/19/14 DM0219/14002028. ... 240 mg/kg D.W.. 1.4 4 SW846: 6010C MMSD 02/20/14 DM0220/14002101 240 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/21/14 DM0221/14002181 260'mg/kg D.W. 1.4 4: SW846: 6010C MMSD 02/22/14 QM0222/14002192 260 mg/kg DM. 1.4 4 SW846: 6010C MMSD 02/23/14 DM0223/14002211 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/24/14 DM022.4114002224 270 mg/kg D.W. 1.4 4., SW846: 6010C MMSD 02/25/14 : DM0225/14002251 260 mg/kg DM. 1.4 4'- SW846: 6010C MMSD 02/26/14' DM0226/14002310 .... . 250 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/27/14 DM0227/14002329; :250 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 02/28/14 DM0228/14002350 250 mg/kg D.W. 1.4 4.: .::SW846: 6010C MMSD 03/01/14 DM0301/1400292;1 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 03/02/14 DM0302/14002940 290 mg/kg D.W., 1.4 4 SW846: 60100 MMSD 03/03/14 DM0303/14002953 .280 mg/kg D.W.. 1.4 4 SW846: 6010C MMSD 03/04/14 DM0304/14002986 290 mg/kg D.W. 1.4 4 :SW846: 6010C MMSD 03/05/14 DM0305/14003012 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD, 03/06/14 DM0306/14003182 i 290 mg/kg D.W. :1.4 T 4 SW846: 6010C MMSD 03/07/14 DM0307/14003197 280 mg/kg D.W. . 1.4 4 SW846: 6010C MMSD o /08/14 DM0308/14003208 270 mg/kg D.W. 1.4 4 A0. SW846: 6010C MMSD 03/09/14 DM0309/14003232 280 mg/kg D.W. 1.4 4 AO. SW846: 6010C MMSD 03/10/14 DM0310/14003245. 290 mg/kg D.W. 1.4 4 AO. SW846: 6010C MMSD 03/11/14 DM0311/14003272 290 mg/kg D.W. 1.4 4. AO. ..SW846: 6010C MMSD 03/12/14 DM0312/14603300 300 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 03/13/14 DM0313/14003871 310 mg/kg DM. 1.4 4 SW846: 6010C MMSD" 03/14/14 DM0314/14003886 280 mg/kg D.W: 1.4 : 4 A0: SW846:•6010C MMSD 03/15/14 DM0315/14003899 250 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 03%16/14 DM0316/14003918 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 63/17/14 " DM0317/14003936 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 03/18/14 DM0318/14003963 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 03/19/14 DM0319/14004217 300 mg/kg D.W. 1.4 4:, :.SW846: 6010C MMSD 03/20/14 DM0320/14004315 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 03/21/14 DM0321/14004330 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 03/22/14 DM0322/14004341 300 mg/kg D.W. 1.4. 4 SW846: 6010C MMSD 03/23/14 DM0323/14004360 270 mg/kg D.W. 1.4 4:: SW846: 6010C MMSD .: 03/24/14. DM0324/14004461 210 mg/kg D.W. 1.4 4 SW846: 6010C MMSD . 03/25/14 DM0325/14004638, 210 mg/kg D.W.. 1.4 4 SW846: 6010C MMSD 03/26/14 DM0326/14004664 200 mg/kg D.W. 1.4 4. SW846: 6010C MMSD 03/27/14 DM0327114004683 200 mg/kg DA 1.4 4: SW846: 6010C MMSD 03/28/14' DM0328/14004698 200 mg/kg D:W. 1.4 4 SW846: 6010C MMSD 03/29/14 DM0329/14004889 210 mg/kg D.W. 1.4 4 T SW846: 6010C MMSD 03/30/14 DM0330/14004908 210 mg/kg D.W. 1.4 4. SW846: 6010C MMSD 03%h/14 DM0381/1400492.1 210 mg/kg D:W. 1.4 .4 SW846: 6010C MMSD 04/01/14 DM0401/14004948 260 mg/kg D.W. 1.4 4 Q3. SW846: 6010C _ MMSD 04/02/14 DM0402/14004974 210 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/03/14 DM0403114004993 260 m9/kg D.W. 1.4 4 SW846: 6010C MMSD 04/04/14 DM0404/14005195 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD SY5/rptImi/oMonthly 1110113 tj Page 20 of 106 Printed., 1/811510.48 { M&q Pi�iNE�fARdCl�tfRCtiaECCMbfNI COPPER ICP METHOD D. 04/05/14 DM0405/14005206 290 mg/kg D.W. .. 1.4 .. 4, .• IFIA-qs Annual Milorganite Report January 1 to December 31, 2014 Analytical kath-od" 'Lab SW846: 6010C MMSD 04/06/14 DM0406/14005226 280 mg/kg DX 1.4 4 SW846: 6010C MMSD 04/67/14 DM0401/14005240 290 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/08/14 DM0408/14005267 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/09/14 DM0409114005397 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/10/14 DM0410/14005416 240 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/11/14 DM6411114005434 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/12/14 bM0412/14005605 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/13/14 DM0413/14005627 280 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/14/14 DM0414/14005641 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/15/14 bM0415/14005668 250 mg/kg D.W. 1.4 4 SW846:-6010C MMSD 04/16/14 DM0416/14005791 240 mg/kg D.W. 1.4 4., SW846: 6010C MMSD 04/17/14 DM0417/14005815 230 mg/kg D.W. 0.58 4, Q3. SW846: 6010C MMSD 04/18/14 DM0418/14006027 240 mg/kg D:W. 1.4 4 Q2. SW846: 6010C MMSD 04/19/14 DM6419/14006038 200 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 04/20/14 DM0420/14006057 220 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 04/21/14 DM0421/144006127 210 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 04/22/14 DM0422/14006154 250 mg/kg D.W. 1.4 4 AO. SW846: 6010C MMSD 04/23/14 DM0423/14006180 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/24/14 DM0424/14006339 240 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/25/14 DM0425/14006354 250 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/26/14 DM0426/14006365 250 mg/kg D.W. 1.4 4 SW846:.6010C MMSD 04/27/14 DM0427/14006384' 240 mg/kg D.W. 1.4 4 SW846: 6016C MMSD 04/28/14 DM0428/14006397 250 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/29/14 , DM0429/14006454 270 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 04/30/14 DM0.430/14006482 250 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 05/01/14 DMO501/14006976 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD OS/02/14 DM0502/14006991 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 05/03/14 DM0503/14007150 280 mg/kg D.W. 1.4 4 AO. SW846: 6010C MMSD 05/04/14 DM0504/14007169 260 mg/kg D.W. 1.4 4 AO. SW846: 6010C MMSD 05/05/14 DM0505/14007182 260 mg/kg D.W. 1.4 4 AO. SW846: 6010C MMSD 05/66/14 DMO506/14007209 250 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 05/07/14 DMO507/14007235 260 mg/kg D.W. 1.4 4 SW846: 6010C MMSD 05/08/14 DMO508/14007254 240 mg/kg D.W. 1.4 4 SW846:'6010C MMSD 05/09/14 DM0509/14007269 260 mg/kg D.W. 6.42 4 SW846: 6010C MMSD 05/10/14 DM0510/14007280 230 mg/kg D.W. 0.58 4 SW846: 6010C MMSD OS/11/14 DM0511/14007456 210 mg/kg D.W. 0.58 4 SW846:.6010C MMSD 05/12/14 DM0512/14007469 210 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 05/13/14 DMO513/141007551 260 mg/kg D.W. 0.42 4 AO. SW846: 6010C MMSD 05/14/14 DM0514/14.0075.77 250 mg/kg D.W. 0.42 4 AO. SW846: 6010C MMSD 05/15/14i DMO515/14007665 260 mg/kg D.W. 0.42 4 AO. SW846:.6010C MMSD 05/16/14 DM0516/14007680 280 mg/kg D.W. 0.42 4 AO. SW846: 6010C MMSD 05/17/14 DM0517/14007691 220 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 05/18/14 DMO518/14007710 230 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 05/19/14 DM0519/14007764 250 mg/kg D.W: 0.42 4 AO. SW846: 6010C MMSD 05/20/14 DM0520/14007997 270 mg/kg D.W. 0.42 4 A0, SW846: 6010C MMSD 05/21/14 DMO521/14608023 250 mg/kg D.W. 0.42 4 SW846: 6010C MMSD SYS/rptIlOoMonthly 1110113 tj Page 21 of 106 Printed:11811510.48 pa�T�f�i fU� A ClE+.� ik/I�NNENi COPPER ICP METHOD sampipbate Samplia ID . 05/22/14 DM0522/14008042 Res ult 230 mg/kg D.W. L6b 0.58 LOQ, 4 Annual Klorganite Report January 1 to December 31, 2014, SW846: 6010C MMSD. 05/23/14 ., DMO523/14008057 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 05/24/14 DM0524/14008291 260 mg/kg D.W.. 0.42 4 SW846: 601OC MMSD 05/25/14 DM0525/14008310 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD OS/26/14 DM0526/14008323 300 mg/kg D.W. 0.42 4 :' SW846: 6010C MMSD 05/27/14 QM0627/14008646 300 mg/kg D.W. 0.42 4 • SW846: 6010C MMSD 05/28/14 OM0528114008672 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 05/29/14 DMO529114008691 270 mg/kg D.W. 0.42 4... A0. SW846: 6010C MMSD 05/30/14 DM0530/14008845 240 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 05/31/14" DM0531/14008856 250 mg/kg D.W. _ 0.58. 4 SW846: 6010C. MMSD 06/01/14 DM0601/14009580 240 mg/kg D.W. .0.58 4 SW846: 6010C MMSD 06/02/14 DM0602/14009593 230 mg/kg D.W. 0.58 4'::' SW846: 6010C MMSD 06/03/14 62 DM0663/140090 240 mg/kg D.W. 0.58 4: SW846: 6010C MMSD 06/04/14 QM0604/14009635 240 mg/kg D.W., '0 42 4 SW846: 601OC: MMSD 06/05/14 DM0605/14009654 260 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 06/06/14 DM0606/14009669 240 mg/kg D.W. 0.42 4.1. SW846: 6010C MMSD. 06/67/14 DM0607/14.009844 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 06/08/14 DM0608114009867 - 260 mg/kg D.W. 0:42 4 SW846: 601OC: MMSD 06/09/14 DM0609/14009880 260 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 06/16/14 DM0610/14009907 260 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 06/11/14 DM0611/14010237 230 mg/kg D.W. 0,58 4 SW846: 6010C MMSD 06/12/14 " DM0612/14010256 230 mg/kg D.W. 0:58 4 SW846:6010C MMSD 06/13/14 DM0613114.010271 240 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 06/14/14 DM0614/14010282 230 mg/kg D.W. 0.58 4.' SW846: 6010C MMSD 06/15/14 DM0615/14010301 220 mg/kg D.W. 0.58 4 SW846: 6010C MMSD ' 06/16/14 DM0616/14010319 220 mg/kg D.W. 0.58 4 SW846:'6010C' MMSD 06/17/14 DM0617/14.010346 240 mg/kg D.W. 0.58' 4 .. SW846: 6010C MMSD 06/18/14 DM0618/14010687 240 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 06/19/14 DM0616/14010706 : 250 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 06/20/14 DM06.20/14010721, . 230 mg/kg D.W. 0.58 4 SW846: 6010C " MMSD 06/21/14 DM0621/14.010732 220 mg/kg D.W. 0.58 .4... SW846: 6010C MMSD, 06/22/14 DM0622/1401'0751 2.30 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 06/23/14 DM0623/14011513 230 mg/kg D.W. _ 4.58 4 SW846: 6010C MMSD 06/24/14 DM0624/14011540 240 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 06/25/14 DM0625/14.011566 220 mg/kg D.W. 0.58 9.:. SW846: 6010C MMSD .: 06/26/14, DM0626/14011766 240 mg/kg D.W. 0.58 4 SW846: 6010C MMSD .. 06/27/14 DM0627/14011781 _ _ _ :: _ 240 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 06/28/14 DM0628114011792 220 mg/kg D.W. 0.58 4.. SW846: 6010C MMSD 06/29/14 DM0629/1401.1811 220 mg/kg D.W. 0.58 .4 SW846: 6010C MMSD 06/30/14 DM063b/14011824 230 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 07/01/14 DM0701/14011851 230 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 07/02/14 DM0702/14011879 240 mg/kg D.W. 0.58 4. , SW846: 6010C MMSD, 07/03/14 DM0703/14011898 240 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 67/04/14 DM0704/14011911 230 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 07/05/14 DM0705/14011924 ' . 240 mg/kg D.W:. 0.58 4 SW846: 6010C MMSD 07/06/14 DM0706/14.011943 230 mg/kg D.W. 0.58 4 :. ' SW846: 6010C MMSD 07/07/14 DM070W14012196 230 mg/kg D.W. 0.58 4 SW846: 6010C MMSD SYS/rptlMiioMontbiy 1110113 tJ Page 22 of 106 Printed: 118115 10:48 P�<I3Ati5IRAC tIONIVANIN! COPPER ICP METHOD Sample Date Sample ID 07/08/14 DM0708/14012898 Result 230 mg/kg D.W. 0.58 :Lo� Qik, 4 Annual Milorganite Report January 1 to December 31, 2014 lCaj,ML SW846: 6010C MMSD 07/09/14 DM0709/14012926 230 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 07/10/14 DM0710/14012945 240 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 07/11/14 DM0711/14012961 270 mg/kg D.W: 0.58 4 SW846: 6010C MMSD 07/12/14 DM0712/14012971 280,Mg/kg D.W. 0.42 4, SW846: 6010C MMSD 07/13/14 DM0713/1401299.1 260 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/14/14 DM0714/14013004 260 mg/kg D.W. 0.42 4 SW846:.6010C MMSD 07/15/14 DM6715/14013031 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/16/14 DM0716/14013059 290 mg/kj D.W. 0.42 4 SW846: 6010C MMSD 07/17/14 DM0717/14013078 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/18/14 DM0718/14013295 270 mg/kg D.W. 0.42 4 SW846:.6010C MMSD 07/19/14 DM0719/14013305 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/20/14 DM0720/14013324 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/21/14 DM0721/14013337 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/25/14 DM0725/14013997 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/26/14 DM072.6/14014008 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/27/14 DM0727/14014027 250 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/28/14 DM0728/14014040 240 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/29/14 DM0729/14014895 250 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/30/14 DM0730/14014923 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 07/31/14 DM0731/14,014942 250 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/01/14 DM0801/14014957 260 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/02/14 bM0802/14014968 240 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 08/03/14 DM0803/14014987 240 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 08/04/14 DM0804/14015000 240 Mg/kg D.W. 0.58 4 SW846: 6010C MMSD 08/05/14 DM0805/14015027 260 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/06/14 DMO806/14015405 250 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/07/14 DM0807/14015456 260 mg/k6 D.W. 0.42 4 SW846: 6010C MMSD 08/08/14 DM0808/14015471 240 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/09/14 DMO809/14015482 250 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/10/14 DM6810/14015966 240 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/11/14 DM0811/14015984 250 mg/kg DM. 0.42 4 SW846: 6010C MMSD 08/12/14 DMQ812/14016011 240 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/13/14 DMO813/14016039 240 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/14/14 DM0814/14016058 260 mg/kg D.W. 0.42 4 - SW846: 6010C MMSD 08/15/14 DM0815/14016181 250 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/16/14 DMO816114016192 240 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/17/14 DM0817/14016211 240 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/18/14 DM0818/14016290 230 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/19/14 DMO819/14016319 240 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/20/14 DM0820114016347 210 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/21/14 DM0821/14016366 190 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/22/14 DM0822/14016381 1.70 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/23/14 DM0823/14016392 190 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/24/14 DM0824/14016411 220 mg/kg D.W: 0.42 4 SW8466010C MMSD 08/25/14 DM0825114016488 250 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/26/14 DM0826/14616515 250 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 5Y5/rpt1M110Month1y 1110113 y Page 23 of 106 Printed:1/8/1510:48 .-„ PbPENEta Eta a Clk+.�Ui L}tll6f HNEfB ONSD COPPER ICP METHOD Sample,Qate 08428/14 DM0828/14016907 220 mg/kg D.W. 0.42 4:' Annual Milorganite Report January 1 to December 31, 2014 Analytical Method l.ab :'SW846: 6010C MMSD 08/29/14 DMO829/14017671 180 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 08/30/14 DM0830/14017682 210 mg/kg D.W.' ..0.42 4 . . SW846: 6010C MMSD 08/31/14 DM0831/14017701 260 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/61/14 DM0901/14017714 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/02/14 DM0.902/14017871 260 mg/kg D.W. . 0..42 4 SW846: 6010C MMSD 09/03/14 DM0903/14017886 270 mg/kg D.W: 0.42 4 SW846:.6010C MMSD 09/04/14 DM0904/14017920 280 mg/kg D.W. 0.42' 4 SW846: 6010C MMSD 09/05/14 DM0905/14017901 260 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/16/14 DM0916/14019167 300 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/17/14 DM0917/14019195 300 mg/kg D.W: 0.42 4 SW846: 6010C MMSD 09/18/14 DM0918/14019229 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/19/14 DM0919/14019244 310 mg/kg D.W. 0.42 4 SW846: 6010C MMSD nannna nnnnagn/ldnlagSF ion mnikn n W_ ' n-47 4 SW846: 6010C MMSD 09/21/14 DM0921/14019274 320 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/22/14 DM0922/14019287 310 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/23/14 DM0923/14019778 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/24/14 DM0924/14019806. 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/25/14 DMO925/14019825 270 mg/kg D.W. 0.42 4 SW846: 60iOC MMSD 09/26/14 DM0926/14019840 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/27/14 DM0927/14019851 310 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/28/14 DM0928/14019870 310 mg/kg D.W.: 0.42 4 SW846: 6010C MMSD 09/29/14 DM0929/140.19883 340 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 09/30/14 DMO930/14019909 320 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/01/14 DM1001/14019927 320 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/02/14 DM1,002/14020572 310 mg/kg D.W. 10.42 4 SW846: 6010C MMSD 10/03/14 DMI003/14020587 300 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/04/14 DM1004/94020598 270 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 10/05/14 DM1005/14020617 256 mg/kg D.W. O.S8 4 SW846: 6010C MMSD 10/06/14 DM1',006/14020630 270 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 10/07/14 DM1007/14021108 260 mg/kg D.W. 0.58 4: SW846: 6010C MMSD 10/08/14 DM1008/14021160 250 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 10/09/14 DM1'009/14021179, 270 mg/kg D.W, 0.58 4 SW846::6010C MMSD 10/10/14 DM1010/14021194 270 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 10/11/14 DM1011/14021244 290 mg/k6 D.W. 0.42 4 SW846: 6010C MMSD 10%12/14 DM1012/14021263 300 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/13/14 DM1013/14021276 300 mg/kg D.W:, _ 0.42 4 SW846`•6010C MMSD 10/14/14 DM1014/14021304 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/15/14 DM1015/14O2l332 290 m9/kg DM. 0.42 4 SW846: 6010C MMSD .. 10/16/14 -DM1016/14021351 310 mg/kg D.W. 0.42 4 "SW846: 6010C MMSD 10/17/14 DM1017/14021787 300 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/18/14 10/19/14 10/20/14 10/21/14 DM1018/14021798 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD DM1019/14021817 MO mg/kg D.W. 0.42 4 SW846: 6010C MMSD DM1020/14021830 286 mg/kg D.W. 0.42 4 SW846: 6010C MMSD DM1021114021857 280 mg/kg D.W.' ' 0.42 4 SW846: 6010C MMSD 10/22/14 DM1022/14021885 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/23/14 DM1023/14022256 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD Page 24 of 106 SYS/rptlMi/oMonthly 1/10/13 tj , Printed.1/8/1510:48 .p M: S D RdRMPS ro d CLUAIR Wits wfiff . COPPER ICP METHOD Sample Date Sample XD 10/74/14 DM1024/1.4022273 Ult 290 mg/kg D.W. LbD 0.42 00 O. Flags 4 7 Annual Milorganite Report January 1 to December 31, 2014 Analytical Method Lab SW846: 6010C MMSD 10/25/14 DM1025/14022286 280 mg/kg DM. 0.42 4 SW846: 6010C MMSD ]0/26/14 DM1026/14022305 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/27/14 DM1027/14022318 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/.28/14 DM1028/1:4022409 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/29/14 DM1029/14022439 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/30/14 DM1030/14022510 260 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 10/31/14 DM11031/14022525 310 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/01/14 DM1101/1.4022536 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/02/14 DM1102/14022555 290 mg/kg.D.W. 0.42 4 SW846: 6010C MMSD 11/03/14 DM1103/14022568 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/04/14 DM1104/14023111 280, mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/05/14 DM1105/14023139 280 mg/kg D.W. 0.42 4' SW846: 6010C MMSD 11/06/14 DM1106/14023158 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/07/14 DM1107/14023173 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/08/14 DM1108/14023184 300 mg/kg D.W. 0.42 4.. SW846: 6010C MMSD 11/09/14 DM1109/14023203 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/10/14 DM1.110/14023767 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/11/14 DM1111/14023796 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/12/14 DM1112/14023876 280 mg/kg D.W. 0.42 4 _ SW846: 6010C MMSD 11/13/14 DM1113/14023895 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/14/14 DM! 114/14023910 290 mg/kg D.W. '0.42 4 SW846: 6010C MMSD 11/15/14 DM1.115/14023929 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/16/14 DM1116/14023948 250 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/17/14 DM1117/1402396.1 260 mg/kg D.W. 0.42 4 SW846: 6010C MMSD, 11/18/14 DM1118/14024236" 250 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/19/14 DM1119/14024264 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/20/14 DM1120/14024283 300 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/21/14 DM1121/14024302 310 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/22/14 DM1122/14024313 310 mg/kg D.W. 0.42 4 SW846: 6010-C MMSD 11/23/14 DM1123/14024393 300 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/24/14 DM1124/14024414 320 mg/kg D.W. 0.42 4 'SW846: 6010C MMSD 11/25/14 DM1125/14024441 300 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/26/14 DM1126/14024469 260 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/27/14 DM1'127/14024529 290 mg/kg D.W. 0.42 4' SW846: 6010C MMSD 11/28/14 DM1128/14024544 300 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/29/14 DM1,129/14024555. .290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 11/30/14 DM1130/14024574 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 12/OS/14 DM1201/14024601 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 12/02/14 DM1202/14025299 280 mg/kg D.W. 0.42 4. SW846: 6010C MMSD 12/03/14 DM1203/14025327 i280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 12/04/14 DM1204/14025346 290 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 12/05/14 DM1205114025361 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 12/06/14 DM1206/14025372 310 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 12/07/14 DM1207/14025391 310 mg/kg D.W. 0.42 4 SW846: 6610C MMSD 12/08/14 DM1208/14025404 310 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 12/06/14 DM1209/14026170 300 mg/kg D.W. 0.42 4 SW846: 6010C MMSD SYS/rptiMi/oMonth/y 1/10/13 tj Page 25 of 106 Printed, 1/8/1510:48 i,r k MSD: PARias Ift 4 Ctwa flowow . COPPER ICP METHOD Sample e.te SamOle'Ia e o e e W 12/10/14 DM1210/14026198 300 mg/kg D.W. 0.42 4= 12/11/14 DM1211/14026217 280 mg/kg D.W. 0.42 4 Annual Milorganite Report January 1 to December 31, 2014 SW846:6010C MMSD SW846: 6010C MMSD 12/12/14 DM1212/14026232. 290 mg/kg D.W; 0.42 ." 4 SW846::6010C MMSD 12/13/14 DM1.213/14026243 : 280 mg/kg D.W. 0.42. 4 SW846: 6010C MMSD 12/1'4/14 DM12.14/14026262 260 mg/kg D.W. 0.42 4" SW846: 6010C MMSD 12/15/14 DM1215/1402627-7 270 mg/kg D.W. 0,.42 4 SW846: 6010C MMSD 12/16/14 DM1216/14026475 240 mg/kg D.W.. :0.42 4 SW846:.6010C MMSD 12/17/14 DM1217/14026503 270 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 12/18/14 DM1218/14026522 260 mg/kg DM. 0.42 4 SW846: 6010C MMSD 12/19/14 DM1219/14026537 . 270 mg/kg D.W.. ..0.42 4 SW846: 6010C MMSD 12/20/14 DM1220/14026653 250 mg/kg D.W: 0.42 4 SW846::6010C MMSD 12/21/14 DM1221/14026672 250 mg/kg DM. 0.42 4.: ::SW846: 6b10C MMSD 12/22/14 DM1222/14026685 260 mg/kg D:W. 0.42 4 SW846: 6010C MMSD 12/23/14 DM1,223/14026713 270 mg/kg D.W. :0.42 4 SW846: 6010C MMSD 12/24/14 DM1224/14026741 280 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 12/25/14 DM1225/14026760 290 Mg/kg D.W. 0.42 4: ." SW846: 6010C MMSD 12/26/14 DM1226/14026777 300 mg/kg D.W. 0.42 4 SW846: 6010C MMSD 12/27/14 DM1227/14026788 T 260 mg/kg D.W.: 0.58T 4 SW846: 6010C MMSD 12/28/14 DM1228/14026807 250 mg/kg D.W. " 0.58 4 SW846: 6010C MMSD 12/29/m DM1229/14027031 260 mg/kg D.W. 0.58 4 SW846: 6010C MMSD 12/30/14 DM1230/14027058 260 mg/kg D.W. 0.58 4. SW846: 6010C MMSD 12/31/14 DM1:231/14027086 290 mg/kg D.W: 0.42 4 SW846: 6010C MMSD Avg: 260 mg/kg D.W. SYS/rptlMiioMonthiy 1110113 tj Max: 340 mg%kg D.W. Page 26 of 106 Printed.• 1/8/1510.48 N,SD- WINO ItaAtltWWIl£'li IXT FECAL COLIFORM SLUDGE 'Sample o. 01/05/14 MF/14000281 < 0.22 MPN/g TS �� 0.22 �e logS 0.73. B Annual Milorganite Report January 1 to December 31, 2014 EPA 1680 MMSD 01/12/14 MF/14000893 0.21 MPN/g TS 0.21 0.7 EPA 1680 MMSD 01/20/14 MF/14001250 < 0.21 MPN/g TS 0.21 0.7 EPA 1680 MMSD 02/14/14 MF/14002911 < 0.22 MPN/g TS 0.22 0.73 EPA 1680, MMSD 02/17/14 MF/14003047 < 0.22 MPN/g TS 0.22 .0.73 EPA 1680 MMSD 02/24/14 MF/14003138 < 0.22 MPN/g TS 0.22 0.73 EPA 1680 MMSD 03/07/14 MF/14004378 < 0.22 MPN/g TS 0.22 0.73 EPA 1680 MMSD 03/09/14 MF/14004426 < 0.22 MPN/g TS 0.22 0.73 EPA 1680 a MMSD 03/16/14 MF/14004744 < 0.22 MPN/g TS 0.22 0.73 EPA 1680 MMSD 04/07/14 MF/14006115 < 0.21 MPN/g TS 0.21 0.7 EPA 1680 MMSD 04/14/14 MF/14006564 < 0.22 MPN/g TS 6.22 0.73 EPA 1680 • MMSD 04/21/14 MF/14007114 < 0.21 MPN/g TS 0.21 0.7. EPA 1680 MMSD 05/04/14 MF/14008425 0.21 MPN/g.TS 0.21 0.7 EPA 1680 MMSD 05/11/14 MF/14008787 0.21 MPN/g TS 0.21 0.7 EPA 1680 .. MMSD 05/18/14 MF/14009431 0.21 MPN/g TS 0.21 0.7 EPA 1680 - MMSD 06/02/14 MF/14010891 . < 0.22 MPN/g TS 0.22 0.73: EPA 1680 MMSD 06/09/14 MF/14011493 < 0.21 MPN/g TS 0.21 0.7 EPA 1680 MMSD 06/16/14 MF/14012167 < 0.21 MPN/g TS 0.21 0.7 EPA 1680 MMSD 07/06/14 MF/14014180 < 0.22 MPN/g TS 0.22 0.73 EPA 1680 MMSD 07/14/14 MF/14014642 < 0.21 MPN/g TS 0.21 0.7.. EPA 1680 MMSD 07/26/14 MF/14015263 < 0.21 MPN/g TS 0.21 0.7 EPA 1680 MMSD 08/04/14 MF/14016731 < 0.22 MPN/g TS 0.22 0.73 EPA 1680 MMSD 08/11/14 MF/14017429 < 0.21 MPN/g TS 0.21 0.7 EPA 1680 MMSD 08/18/14 MF/14018002 <-0.21, MPN/g TS 0.21 0.7' EPA 1680 MMSD 09/02/14 MF/14019423 0.21 MPN/g TS 0.21 0.7 EPA 1680 MMSD 09/16/14 MF/14020820 0.21 MPN/g TS 6.21 0.7 EPA 1680 MMSD 09/24/14 MF/14021446 < 0.22 MPN/g TS 0.22 0.73 EPA 1680 MMSD 10/06/14 MF/14022464. <-0.21 MPN/g TS 0.21 0.7 EPA 1680 MMSD 10/13/14 MF/14023066 < 0.21 MPN/g TS 0.21 0.7 EPA 1680 MMSD 10/27/14 MF/14024179 < 0.22 MPN/g TS 0.22 0.73 EPA 1680. MMSD 11/03/14 MF/1402471.2 < 0.22 MPN/g TS 0.22 0.7.3. EPA 1680 MMSD 11/10/14 MF/14025198 < 0.21 MPN/g•TS 0.21 0.7 EPA 1680 MMSD 11/17/14 MF/14025811 0.22 MPN/g TS 0.22 0.73 EPA 1680 . MMSD 12/02/14 MF/i4026563 < 0.21 MPN/g TS 0.2. 0.67 EPA 1680: MMSD 12/08/14 MF/14026987 14 MPN/g TS 0.21 0.7 EPA 1680 MMSD 12/15/14 MF/14027309 < 0.22 MPN/g TS 0.22 0.73 EPA 1680 MMSD Page 27 of 106 SYS/rptlM110Month/y 1110113 tj Printed.• 11811510;48 s t� MSD PAWFS lod.UwIR w1vo IRON ICP METHOD, ,Sample Date i 01/01/14 DMO101/14000012 Resuli 39000 mg/kg D.W. LOD 16 / 120 Annual Milorganite Report January 1 to December 31, 2014 e i SW846: 6010C MMSD 01/02/14 DMO102/14000039 38000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/03/14 DM0103/14000088 43000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/04/14 DM0104/14000103 45000 mg/kg D.W. 16 120 „SW846: 6010C MMSD 01/05/14 DMO105114000122 50000 mg/kg D.W. 16 120' SW846: 6010C MMSD 01/06/14 DMO106/14000136 52000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/07/14 DM0107/14000162 53000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/08/14 DM0108/14000188 56000 mg/kg D.W. 16 120. SW846: 6010C MMSD 01109/14 DMO109/14000207 54000 mg/kg D.-W. 16 120 SW846: 6010C MMSD 01/10/14 DM0110/14000430 51000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/11/14 MI 49000 mg/kg D.W. 16 120 SW846: 6016C MMSD 01/12/14 DM0112/14000460 46000 mg/kg D.W. 16 120: SW846: 6010C MMSD 01/13/14 DMO113/14000473 47000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/14/14 DM0114/14000500 47000 mg/kg D.W.. 116 120 SW846:.6010C MMSD 01/15/14 DM0115/14000526 44000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/16/14 DM0116/14000545 42000 mg/kg D.W. 16 120 ' SW846: 6010C MMSD 01/17/14 DM0117/14000560 43000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/18/14 DM0118/14000571 48000 mg/kg D.W.. 16 120 SW846: 6010C MMSD 01/19/14 DM0119/14000590 _ 49000 mg/kg D.W. 16 120 SW846: 6010C MMSD :'01po/14 DMO120/14000603 54000 mg/kg D.W. 16 120 :'SW846: 6010C MMSD 01/21/14 DMO121/14000630 54000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/22/14 DM0;122/14000656 49000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/23/14 DMO123/14000675 _ 51000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/24/14 DM0124/14000690 48000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/25/14 DM0125/14000923 49000 mg/kg D.W. 16 120' SW846: 6010C MMSD 01/26/14 DM0.126/14000942 47000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/27/14 DMO127/14001095 47000 mg/kg D.W. 16 120 SW846: 6010C MMSD 01/28/14 DM0128/14001122 49000 mg/kg D:W. 16 120 SW846: 6010C MMSD 01/29/14 DMO129/14001148 50000 mg/kg D.W. 16 120 SW846: 6010C_ MMSD 01/30/14 DMO130114001167 49000 mg/kg D.W. 16 120 SW846: 6610C MMSD 0i/31/14 DM0131/14001182 48000.mg/kg D.W. 16 120' SW846: 6010C MMSD 02/01/14 DM0201/14001193 44000 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/02/14 DM0202114001430 46000 mg/kg D.W., 16 120 SW846: 6010C• MMSD 02/03/14 DM0203/14001443 45000 mg/kg D.W. 16 120 SW846:. 6010C MMSD 02/04/14 02/05/14 DM0204/14001470 DM0205/1400149b 42000 mg/kg D.W. 45000 mg/kg D.W. 16 _ _ _ 16 120. 120 _ SW846: 6010C SW846: 6010C MMSD .. MMSD 02/06/14 DM0206/14001517 40000 mg/kg D.W. 16 120 SW846:.6010C MMSD 02/07/14 DM0207/14001532 30000 mg/kg D.W. 16 120.1 SW846: 6010C MMSD 02/08/14 DM0208/14001543 39000 mg/kg D.W. 16 120' SW846: 6010C MMSD 02/09/14 DM0209/14001562 41000 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/10/14 DM0210/14001576 44000 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/11/14 DM0211/1400181.1 47000 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/12/14 DM0212/14001837 45000 mg/kg D:W. 16 120 SW846: 6010C MMSD 02/13/14 DM0213/14001856 44000 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/14/14 DM0214/14001871 . 42000 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/15/14 DM0215/14001882 44000 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/16/14 DM0216/14001893 42000 mg/kg D.W. 16 120 SW846: 6010C MMSD SYS/rptimi/omonthiy 1110113 tj - Page 28 of 106 Pr117ted.-1/8/1510:48 0 M M t1AS, UWk P,tN]NtN3 f 4d� d CE4>xttR EBiIE�NgENi IRON ICP METHOD • e , o o LOO Annual Milorganite Report January 1 to December 31, 2014 02/17/14 DNl10217/14001914 42000 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/18/14 DM0218114002002 42000 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/19/14 DM0219/14002028 42000 mg/kg D.W., 16 120 SW846: 6010C MMSD 02/20/14 DM0220114002101 42000 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/21/14 DM0221/1400218.1 45000,mg/kg D.W. 16 120 SW846: 6010C MMSD 02/22/14 DM0222/14002192 43600 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/23/14 DM0223/14002211 46000 mg/kg D.W. 16 120 SW846:.6010C MMSD 02/24/14 DM0224/14002224 42000 mg/kg D.W. 16 120 SW846: 6010C MMSD 02/28/14 DM0225/1400225.1 44000 mg/kg D.W. 16 ..120 SW846: 6010C MMSD 02/26/14 DM0226/14002310 44000 mg/kg D.W. 16 126 SW846: 6010C MMSD 02/27/14 DM0227/14002329 48000 mg/kg D.W. 16 120 SW846::6010C MMSD 02/28/14 DM0228/14002350 46000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/61/14 DM0301/14002921 50000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/02/14 DM0302/1400294b 50000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/03/14 DM0303/14002953 49000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/04/14 DM0304/14002986 45000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/05/14 DM03b5/14003012 45000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/06/14 DM0306/14003182 39000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/07/14 DM0307/14003197 39000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/08/14 DM0308/14003208 39000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/09/14 DM0309/14003232 40000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/10/14 DM0310/14003245 39000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/11/14 DM0311/14003272 41000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/12/14 DM0312/14003300 47000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/i3/14 DM0313/14003871 44000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/14/14 DM0314/14003886 37000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/15/14 DM0315/14003899 37000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/16/14 DM0316/14003918 41000 mg/kg D:W. 16 120' SW846: 6010C MMSD 03/17/14 DM0317/14003936 39000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/18/14 DM0318/14003963 "' 36000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/19/14 DM0319/14004217 46000 mg/kg D.W. 16 120„ SW846: 6010C MMSD 03/20/14 DM0320/14004315 43000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/21/14 DM0321/14004330 42000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/22/14 DM6322/14004341 40000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/23/14 DM0323/14004360 38000 mg/kg D.W. 16 120: SW846: 6010C MMSD 03/24/14 DM0324/14004461 30000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/25/14 DM0325/14004638 33000 mg/kg D.W. 16 120 SW846:.6010C MMSD 03/26/14 DM0326/14004664 32000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/27/14 DM0327/14004683 34000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/28/14 DM0328/14004698 36000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/29/14 DM0329/14004889 36000 mg/kg D.W. 16 120 SW846: 6010C MMSD 03/30/14 DM0330/14004908 38000 mg/kg D.W. 16 120 _ SW846: 6010C MMSD 03/31/14 DM0331/14004921 39000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/01/14 DM0401/14004948 39000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/02/14 DM0402/14004974 _ 44000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/03/14 DM0403/14004993 53000 mg/kg D.W. 16 120, SW846: 6010C MMSD 04/04/14 DM0404/14005195 54000 mg/kg D.W. 16 120 SW846: 6010C MMSD SY5/rpt-Wi/oMonth/y 1110113 tj Page 29 of 106 Printed; 1/8/1510:48 F , r MSD eliNtt51NA Ct4AqR 19111ANUff IRON ICP METHOD .. Sp - D I ate i e 04/OS/14 DM0405%14005206 50000 mg%kg D.W. o 16 eLab 120 Annual Milorganite Repot# January 1 to December 31, 2014 SW846: 6010C MMSD 04/06/14 DM0466/14005226 47000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/07/14 DM0.407/14005240. 42000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/08/14 DM0408114005267 45000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/09/14 DM0409/14006397 46000 Mg/kg D.W. 16 120 SW846: 6010C MMSD 04/10/14 DM0410/14005416 41000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/11/14 DM0411/14005434. 46000 mg/kg D.M. 16 120 SW846:.6010C MMSD 04/12/14 DM0412/14005605 44000 mg/kg D.W. 16 120... .SW846: 6010C MMSD 04/13/14 DM0413/14005627 44000 mg/kg D:W. 16 120 SW846: 6010C MMSD '- 04/14/14 DM0414/14005641 43000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/15/14 DM0415/14005668 42000 mg/kg D.W.. "' 16 120 SW846:'6010C MMSD 04/16/14 DM0416/1400579.1 41000 mg/kg D.W. 16' 120:: SW846: 6010C MMSD 04/17/14 DM0417/14005815 42000 Mg/kg D:W. 9.6 120 SW846: 6010C MMSD 64/f8/14 DM0418/14006027 43000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/19/14 DM0419/14006038 43000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 04/20/14 DM0420/14006057 43000 mg/kg D.W. 9.6 120: SW846: 6010C MMSD 04/21/14 DM0421/14006127 42000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 04/22/14 DM0422/14006154, 43000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/23/14 DM0423/14006180 43000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/24/14 DM0424/14006339 39000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/25/14. DM0425/14006354 43000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/26/14 DM6426114006365, 43000 nig/kg D.W. 16 120 SW846:.6010C MMSD 04/27/14 DM0427/14006384 44000, mg/kg D.W. 16 120 SW846: 6010C MMSD 04/28/14 DM0428/14006397 48000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/29/14 DM0429/14006454 44000 mg/kg D.W. 16 120 SW846: 6010C MMSD 04/30/14 DM0430/14006482 42000 mg/kg D.W. 16 120 SW846:6010C MMSD 05/01/14 DMO501/1.4006976 41000 mg/kg D.W. 16 120.. SW846: 6010C MMSD 05/02/14 DM0502/1400699.1 39000 mg/kg D:W. 16 120 SW846: 6010C MMSD 05/03/14 DM0503/14007150 36000 mg/kg D.W. 16 120 SW846: 6010C MMSD 05/04/14 DM6504/14007169 38000 mg/kg D.W. 16 120 SW846: 6010C MMSD OS/95/14 DMO505/14007182 38000 mg/kg D.W. 16 120: SW846: 6010C MMSD 05/06/14 DMO506/14007209 40000 mg/kg D.W. 16 120 SW846: 6010C MMSD 05/07/14 DM0507/14007235 41000 mg/kg D.W. 16 120 SW846:.6010C MMSD 05/08/14 DM0508/14007254 39000 mg/kg D.W. 16 120 SW846: 6010C MMSD 05/09/14 DM050,9/14007269 41000 }n9/kg D.W. 24 120: SW846: 6010C MMSD 05/10/14. DM0510/14007280 52000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD. 05/11/14 DM0511/14007456: " 47000 mg/kg D.W. 9.6 .. 120 SW846:.6010C MMSD 05/12/14 DM0512/14007469 47000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 05/13/14 DM05.13/1400755.1 43000 mg/kg DM. 24 120 SW846: 6010C MMSD 05/14/14 DM0514114007577 40000 mg/kg D.W. 24 120 SW846: 6010C MMSD - 05/15/14 DM0515/14007665 43000 mg/kg D.W. 24 120 SW846:, 6010C MMSD 05/16/14 DMO516/14007680 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD 05/f7/14 DM0617114007691 38000 rpg/kg D.W. 24 120 SW846: 6010C MMSD O5/18/14 DM0518/14007110 37000 mg/kg D.W. 24 120 SW846: 6010C MMSD 05/19/14 DM0519/14007764 38000 mg/kg D.W. 24 120 AO. .. SW846: 6010C MMSD 05/20/14 DM0520/14007997 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD OS/21/i4 DM0521/14008023 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD SYS/rptlMi/oMonthiy 1110113 tj Page 30 of 106 Printed.• 11811510,48 P,lR]MCRS (D�d'41f�� [1TJI�IN�fHJ IRON ICP METHOD ;Sample DatxF. Sampleo 05/22/14 DM0522/14008042 Pesult 44000 mg/kg D.W. L60 9.6 120, B8. • � I l Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 05/22/14 DM0522114008042 47000 mg/kg D.W. 24 120 SW846: 6010C MMSD 05/23/14 DM0523/14008057 41000 mg/kg D.W. 24 120 SW846: 6010C MMSD 05/24/14 DM0524/14008291 37000 mg/kg D.W. 24 120 SW846: 6010C MMSD 05/25/14 DM0525/14008310 42000 mg/kg D.W. 24 120 SW846: 6010C MMSD 05/26/14 DM0526/14008323 48000 mg/kg D.W. 24 120 SW846: 6010C MMSD 05/27/14 DM0527/14008646 49000 mg/kg D.W. 24 120 SW846: 6010C MMSD 05/28/14 DM0528/14008672 46000 mg/kg D.W. 24 120 SW846: 6016c MMSD 05/29/14 DM0529/14008691 49000 mg/kg D.W. 24 120. SW846: 6010C MMSD 05/30/14 DM0530114008845 51000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 05/31/14 DM6531/14008856 49000 mg/kg D.W. 9.6 120 SW846:.6010C MMSD 06/01/14 DM0601/14009580 49000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/02/14 DM0602/14009593 45000,mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/03/14 DM0603/14009620 48000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/04/14 bM0604/14009635 43000 mg/kg D.W. 24 120 SW846: 6010C MMSD 06/05/14 DMO605/14009654 38000 mg/kg D.W. 24 120 SW846: 6010C MMSD 06/06/14 DM0606/14009669 41000 mg/kg D.W. 24 120 SW846: 6010C MMSD 06/07/14 DM0607/14009844 42000 mg/kg D.W. .24 120 SW846: 6010C MMSD 06/08/14 DM0608/14009867 40000 mg/kg D.W. 24 120 SW846: 6010C MMSD 06/09/14 DMO609/14009880 38000 mg/kg D.W. 24 120 SW846: 6010C MMSD 06/10/14 DM0610/14009907 39000 mg/kg D.W. 24 120 SW846: 6010C MMSD 06/11/14 DM0611/14010237 36000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/12/14 DM0612/14010256 42000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/13/14 DM0613/14010271 47000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/14/14 DMO614/14010282 44000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/15/14 DM0615/14010301 44000 mg/kg D.W. 9.6 120 SW846:.6010C MMSD 06/16/14 DM0616/14010319 43000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/17/14 DM0617/14010346 43000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/18/14 DM0618/14010687 41000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/19/14 DMO619/14010706 45000 mg/kg D.W. 9.6 120 SW846:;6010C MMSD 06/20/14 DMO620/14010721 43000, mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/21/14 DM0621/14010732 40000 mg/kg D.W. 9.6 in SW846: 6010C MMSD 06/22/14 DIM0622/14010751 41000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/23/14 DM0623/14011513 41000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/24/14 DM0624/14011540 42000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/25/14 DM0625/14011566 40000 mg/kg D.W. 9.6 120 SW846: 6010C T MMSD 06/26/14 QM0026/14011766 43000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/27/14 DM0627/14011781 42000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/28/14 DMO628114011792 42000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/29/14 DM0629/14011811 43000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 06/30/14 DM0630/14011824 42000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 07/01/14 DM0701/14011851 44000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 07/02/14 DM0702/i4011879 46000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 07/03/14 DM0703/14011898 46000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 07/04/14 DM0704/14011911 41000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 07/05/14 DMO705/14011924 41000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 07/06/14 DM0706/14011943 45000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD SY5/rptlMiloMonthly 1110113 tj Page 31 of 106 Printed. • 1/8/1510:48 Annual Milorganite Report January 1 to December 31, 2014 MSD ` . . PRRIffis W b_Cll AR IWAKNkEN( IRON ICP METHOD bate,o 0 0 QA'Flags; 4hakfi:�i Method Lab 07/07/14 DM0707/14012196 43000.mg/kg D.W. 9.6 120 SW846: 6010C MMSD 07/08/14 DM0708/14.012898 44000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 07/09/14 DM0709/14012926 . 48000 mg/kg D.W.. 9.6 120 SW846: 6010C: MMSD 07/10/14 DM0710/14012945 .44000 mg/kg D.W. 9.6 120 AO. SW846: 6010C MMSD 07/1'1/14 DM0711/14012961 47000 mg/kg D.W. 9.6 120:: AO. SW846: 6010C MMSD 07/12/14 DM0712/14012971 45000 mg/kg D.W. 24 120 SW846: 6010C, MMSD 07/13/14 DM0.713/14012991 45000 mg/kg D.W. 24 120 SW846: 6010C MMSD 07/14/14 DM0714/140.13004 47000 mg/kg D.W. 24 120 SW846: 6010C MMSD 07/15/14 DM0715/14013031 49000 mg/kg D.W. 24 120 SW846: 6010C MMSD 07/16/14 DMQ716/14013059 48000 mg/kg D.W. 24 120 SW846: 6010C, MMSD 07/17/14 DM0717/14013078 48000 mg/kg D.W: 24 120 SW846: 6010C MMSD 07/18/14 DM6718/14013295 45000 mg/kg D.W. 24 120 SW846: 6010C MMSD 07/19/14 DM0719/14013365 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD 07/20/14 DM0720/14013324 44000 mg/kg D.W. -1:;24 120 SW846: 6010C. MMSD 07/21/14 DM0.721/14013337 44000 mg/kg D.W. 24 120 SW846: 6010C MMSD 07/25/14 DM0725/14o13997 38000 mg/kg D.W. 24 120 ...SW846: 6010C MMSD 07/26/14 DM0726/14014008 45000 mg/kg D.W. 24 120 SW846: 6010C MMSD 07/27/14 DM0727/14014027 , 43000 mg/kg D.W. 24 120 SW846:.6010C: MMSD 07/28/14 DMO728/14014040 43000 mg/kg D.W. 24. 120 SW846: 6010C MMSD 07/29/14 DM0729/14014895 50000 mg/kg D.W. 24 120' SW846: 6010C MMSD 07/30/14 DM07301i4014923 49000 mg/kg D.W. 24 120 SW846: 6010C MMSD 07/31/14 DMO731/14014942. 46000 mg/kg D.W. 24 120 SW846::6010C MMSD 08/01/14 DM0801/14014957 50000 mg/kg D.W. 24 120 - SW846: 6010C MMSD 08/62/14 DM0802/14014968 50000 mg/kg DX 24 120 SW846: 6010C MMSD 08/03/14 DMO803/14014987 51000 mg/kg D.W. 24 120 SW846: 6010C MMSD 08/04/14 DM6804/14015000 45000 mg/kg D.W. 24 : 120 SW846::6010C MMSD 08/05/14 DMO805114015027 45000 mg/kg D.W. 24 120.. SW846: 6010C MMSD 08/66/14 DM0806/14015405 45000 mg/kg D:W. 24 120 SW846: 6010C MMSD 08/67/14 DM0807/14015456 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD 08/08/14 DM0808/14015471 43000 mg/kg D.W. 24 120 SW846: 6010C MMSD 08/09/14 DMO809/14015482 46000 mg/kg D.W. 24 120, SW846: 6010C MMSD 08/10/14 DM081.W14015966 44000 mg/kg D.W. 24 120 SW846: 6010C MMSD 08/11/14 DM0811/14015984 43000 mg/kg D.W. 24 120 bSW846:.6610C MMSD 08/12/14 DM0812/14016011 41000 mg/kg D.W. 24 : 120 SW846: 6010C MMSD 08/13/14 DMO813/14016039 40000 m6/kg D.W. 24 120 :'SW846: 6010C MMSD 08/14/14 DM0814/14016058 41000 mg/kg D.W. 24 120 SW846: 6010C MMSD 08/15/14 :" DMO815/14016181 40000 mg/kg D.W. 24 .: 120 SW846::6010C MMSD 08/16/14 DM0816/14016192 36000 mg/kg D.W. 24 120 SW846: 6010C MMSD 08/17/14 DM0817/1.4016211 36000 mg/kg DA 24 120 SW846: 6010C MMSD 08/18/14 ... DMO818114016290 38000 mg/kg D.W. 24 120 SW846: 6010C MMSD 08/19/14 bmd819/14016319 44000 mg/kg D.W. 24 _ 120 SW846:.6610C MMSD 08/20/14 DM0820/14016347 31000 mg/kg D.W. 24 120 SW846: 6010C MMSD 08/21/14 DM0821/14016366 36000 mg/kg DA 24 120 SW846: 6010C MMSD 08/22/14 DM0822/14016381 38000 mg/kg D.W. .24 120 SW846: 6010C MMSD 08/23/14 DM0823/14016392 40000 mg/kg D.W: 24 120 SW846: 6010C MMSD 08/24/14 DM0824/1401641:1 48000 mg/kg D:W. 24 120: SW846: 6010C MMSD 08/25/14 DM0825/14016488 50000 mg/kg D.W. 24 120 SW846: 6010C MMSD SYS/rptiMiloMonthly 1110113 tj Page 32 of 106 Printed. • 1/8/1510:48 ... M.$D: pANTN(P3 f Df & CtLAAR Lk;fMMINT IRON ICP METHOD 08/26/14 DM0826/14016515 47000 mg/kg D.W. 24 120 s � I I Annual Milorganite Report January 1 to December 31, 2014 iLab SW846: 6010C MMSD 08/28/14 DM0828/14016907 37000 mg/kg D:W. 24 120 SW846: 6010C MMSD 08/29/14 DM0829/14017671 29000 mg/kg D.W. 24 120 SW846: 6010C MMSD 08/30/14 DM0830/14017682 34000 mg/kg D.W. 24 120 SW846: 6010C MMSD 08/31/14 DMO831/14017701 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/01/14 DMO901/14017714 53000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/02/14 DM0902/14017871 42000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/03/14 DM0903/14017886 41000 mg/kg D.W. 24 120 SW846: 6016C MMSD 09/04/14 DM0904/14017920 45000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/05/14 DM0905/14017901 36000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/16/14 DMO916/14019167: 44000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/17/14 DM0917/14019195 44000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/16/14 DM0918/14019229 38000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/19/14 DM0919/14019244 42000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/20/14 DM0920/14019255 46000 mg/kg D.W. 24 120 SW846:,6010C MMSD 09/21/14 DM0921114019274 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/22/14 DM0922/14019287 45000 mg/kg D.W. 24 120 SW846: 6010C 'MMSD 09/23/14 DM0923/14019778 40000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/24/14 DMO924/14019806 36000 mg/kg D.W. 24 120 SW846:6010C MMSD 09/25/14 DM0925114019825 36000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/26/14 DM0926/14019840 40000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/27/14 DM0927/14019851 . 39000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/28/14 DMO928/14019870 43000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/29/14 DM0929/14019883 45000 mg/kg D.W. 24 120 SW846: 6010C MMSD 09/30/14 DM0930/14019909 40000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/01/14 DM1001/14019927 35000 mg/kg D.W. 24 120 SW846::6010C MMSD 10/02/14 DM1002/14020572 33000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/03/14 DM1003/14020587 42000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/04/14 DM1004/14020598 42000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 10/05/14 DM1005/14020617 40000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 10/06/14 DM1006/14020630 43000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 10/07/14 DM1007/14021108 46000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 10/08/14 DM1008/14021160 39000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 10/09/14 DM1009/14021179 44000 mg/kg D.W. 9.6 120 SW846:6010C MMSD 10/10/14 DM1010114021194 47000 mg/kg D.W. 9.6 120 SW846: 6010C MMSD 10/11/14 DM1011/14021244 41000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/12/14 DM1012/14021263 42000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/13/14 DM1013/14021276 42000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/14/14 DM101'4/14021304 42000 mg/kg D.W. 24 126. SW846: 6010C MMSD 10/15/14 DM1015/14021332 42000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/16/14 DM1016/14021351 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/17/14 DM1017/14021787 44000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10%18/14 DM1018/14021798 36000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/19/14 DM1019/14021817 39000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/20/14 DM1020/14021830 39000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/21/14 DM1021/14021857 42000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/22/14 DM1022/14021885 43000 mg/kg D.W. 24 120 SW846: 6010C MMSD SYS/rpt.tMiloMonthly 1/10/13 tj Page 33 of 106 Printed, 1/8/1510:48 14 5 U PAEMPS (14 A CLEW EXtIi KUM IRON ICP METHOD sainple e. a 10/23/14 DM1023/14022256 43000 mg/kg D.W. ee 24 LOQ e• 120 Anhual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 10/24/14 DM1024/14022273 48000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/25/14 OM1025/14022286 44000 mg/kg D.W.. 24 .: 120 SW846: 6010C: MMSD 10/26/14 DM1026/14022305 42000 mg/kg D.W. 24 120 SW846: 6010C MMSD 10/27/14 DM1027/14022318 36000 mg/kg D.W. 24 120: SW846: 6010C MMSD 10/28/14 DM1028/14022409 30000 mg/kg D.W. 24 120 SW846: 6010C.. MMSD 10/29/14 DM1029/14022439 30000 mg/kg D.W. 24 .. 120 SW846: 6010C MMSD 10/30/14 DM1030/14022510 M000 mg/kg D.W. 24 120 .. SW846: 6010C MMSD 10/31/14 DM1031/14022525 49000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/01/14 DM1101/14022536 43000 mg/kg D.W. 24 120 SW846: 6010C. MMSD 11/02/14 DM1102/14022555 44000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/03/14 DM1103/14022568 46000 mg/kg D.W. 24 120 . - SW846: 6010C MMSD. 11/04/14 DM1104114623111 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/05/14 DM1105/14023139 45000 mg/kg D.W., ''24 120 SW846: 6010C MMSD 11/06/14 DM1.106/14023158 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/07/14 DM1107/14023173 45000 mg/kg D.W. 24 120 :: 'SW846: 6010C MMSD. 11/68/14 DM1108/14023184 48000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/09/14 DM1109/14023203 45000 mg/kg D.W., 24 120 SW846: 6010C, MMSD 11/10/14 DM1:110/14023767 47000 mg/kg D.W. .24. 120 SW846: 6010C MMSD 11/11/14 DM1111/14023796 49000 mg/kg D.W. 24 120 'SW846: 6010C MMSD 11/12/14 DM1112/14023876 49000 mg/kg D.W. 24 126 SW846: 6010C MMSD 11/13/14 DWI 13114023895 . 45000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/14/14 DM1114/14023910 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD il/15/14 DM1115/14023920 42000 mg%kg D.W. 24 120 SW846: 6010C MMSD 11/16/14 DM1116/14023948 42000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/17/14 DM1117/14023961 41000 mg/kg D.W. 24 120 SW846:'6010C' MMSD 11/18/14 DM1118/14.024236 44000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/19/14 DM1119M4024264 44000 mg/kg D.W. 24 126 SW846: 6010C MMSD 11/26/14 DM1120/14024283 48006 mg/kg D.W. 24 120 SW846: 6010C. MMSD 11/21/14 DM1121/14024302' 48000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/22/14 DM1122/14024313 50000.i ig/kg D.W. 24 120 : ,' SW846: 6010C MMSD 11/23/14 DM1123/14024393 47000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/24/14 DM1124/14024414. 50000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/25/14 DM1125/14024441 48000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/26/14 DM1126/14024469 40000mj/kg D.W. 24 12-0 ; .:':'SW846: 6010C MMSD 11/27/14 DM1127M4024529 42000 mg/kg D.W. 24 126 SW846: 6010C MMSD 11/28/14 DM1,128/14024544 41000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/29/14 DM1129/14024555 38000 mg/kg D.W. 24 120 SW846: 6010C MMSD 11/30/14 :: DM1130/14024574 38000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/Ol/14 DM1201/14024601 40000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/02/14 DM1202/14025299 39000 mg/kg D.W: 24 120 SW846: 6010C MMSD .12/03/14 DM1203/14025327 40000 mg/kg D.W. 24 120. SW846: 6010C MMSD 12/04/14 DM1204114025346 43000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/05/14 DM1205/14025361 43000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/06/14 DM1-206/14025372 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/07/14 DM1207/14025391 42000 mg/kg D.W. 24 120'' SW846: 6010C MMSD 12/08/14 DM1208/14025404 38000 mg/kg D.W. 24 120 SW846: 6010C MMSD SY5/,PtIMi/oMonthly 1110113 t1' _ Page 34 of 106 Punted: 11811510:48 PdRINif6 tp2 d CtE+�9fit 0<�I�YiIltHi IRON ICP METHOD i. i 12/09/14 DM1209/14026170 Result- 39000 mg/kg D^ L0b 24 LOQo 120 i � f t Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 12/10/14 DM1210/14026198 39000 mg/kg D:W. 24 120 SW846: 6010C MMSD 12/11/14 DM1211/14026217 36000 mg/kg D.W. 24 120 SW646: 6010C MMSD 12/12/14 DM1212/14026232 40000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/13/14 DM1213/14026243 40000 mg/kg D.W. 24 120,; SW846: 6010C MMSD 12/14/14 DM121.4/14026262 40000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/15/14 DM1215/14026277 41000 mg/kg D.W. 24 120 aSW846: 6010C MMSD 12/16/14 DM1216/14026475 39000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/17/14 DM1217/14026503 40000 ing/kg D.W. 24 120:: SW846: 6010C MMSD 12/18/14 DM1218/14026522 38000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/19/14 DM1219/14026537 41000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/20/14 DM1220/14026653 39000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/21/14 DM1221/14026672 39000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/22/14 DM1222/14026686 42000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/23/14 DM1223/14026713 44000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/24/14 DM1224/14026741 46000 mg/kg D.W. 24 120 SW846: 6010C MMSD 12/25/14 DM1225114026760 41000 mg/kg D.N. 24 120 SW846: 6010C MMSD 12/26/14 DM1226114026777 12/27/14 DM1227/14026788 12/28/14 DM1228/14026807 12/29/14 DM1229/14027031 12/30/14 DM9230/14027058. 12/31/14 DM1231/14027086 Avg: 43000 mg/kg D.W. SY5/rptlMiloManthly 11-101-13 tj 42000 mg/kg D.W. 24 120 46000 mg/kg D.W. 9.6 120 48000 mg/kg D.W. 9.6 120 49000 mg/kg D.W. 9.6 120 48000 mg/kg D.W. 9.6 120 38000 mg/kg D.W. 24 120 Max: 56.000 mg/kg D.W. SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD SW846: 6010C MMSD Page 35 of 106 Printed.• 11811510:48 Q' t ;�- Pd0w, f{* A Cticia CA10RINf LEAD ICP METHOD. ample ►. 01%01/14 DM0101/14000012 210 tng/kg D.W. .n 0.96 .. .•Anafitical 4: Annual Milorganite Report January 1 to December 31, 2014 Method' SW846: 6010C MMSD 01/02/14 DM0102/14000039 28 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/03/14 DM0103/14000088 30 mg/kg D.W. 6.96 4 SW846: 6010C MMSD 01/04/14 DMO104/14000103 34 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/05/14 DM010511.4000122 98 mg%kg D.W. 0.96 4 SW846: 6010C MMSD Ol/06/14 DMO106/14000135 38 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/07/14 DMO107/14000162 29 mg/kg D.W. 6.96 " 4 SW846: 6010C MMSD 01/08/14 DM0108/14000188 28 mg/kg D:W. 0.96 4. SW846: 6010C MMSD 01/09/14 _ DMO109114000207 27 mg/kg DA 0.96 4' SW846: 6010C MMSD 61/SO/14 :' DM0110/14000430 28 mg/kg D.W. ..0.96 4 SW846: 6010C MMSD 01/11/14 DM0111/14000441 33 mg/kg D.W: 0.96 4 SW846: 6010C MMSD 01/12/14 DM0112/14000460 31 mg/kg D.W. 0.96 4. SW846: 6010C MMSD Oi/13/14 DM0113/14000473 31 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/14/14 DM0114/14000500. 100 mg/kg D.W. 0.96 4 D2, Q3. SW846:.6010C MMSD 01/15/14 DM0115/14000526 34 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/16/14 DM0116/14000545 .38 mg/kg D.W. 0.96 4, SW846: 6010C MMSD O1/17/14, DM0117114000560 34 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/18/14 DM0118/14000571 41 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/19/14 DM0119/14000590 210 mg/kg D.W. 0.96 4 SW846: 6016C MMSD 01/20/14 DM0120/14000603 34 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/21/14 DMO121/14000630 36 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/22/14 DM0122/14000656. 33 mg/kg D.W. 0.96 4 SW846:.6010C MMSD 01/23/14 DMO123/14000675 29 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/24/14 DM0124/14000690 40 mg/kg D:W. 0.96 4 SW846: 6010C MMSD 01/25/14 DMO125/14000923 40 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/26/14 DMO126/14000942 200 mg/kg D.W. 0.96 4 SW846:=6010C MMSD 01/27/14 DM0127/14001095 32 mg/kg D.W. 0.96 4. SW846: 6010C MMSD 01/28/14 DMO128/1.4001122 34 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 01/29/14 DMO129/14001148 29 mg/kg D.W. 0.96 4 SW846:.6010C MMSD 01/30/14 DMb130/14001167 27 mg/kg D.W. 0.96 4 SW846:6010C MMSD O1/31/14 DM0131/14001182 29 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/01/14 DM0201/14001193 140 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/02/14 DM0202/14001430 170 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/03/14 DM0293/14001443 64 mg/kg.D.W. 0.96 4 Q2. SW846: 6010C MMSD 02/04/14 DM0204/i'4001470 36 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/05/14 DM0205/14001498 28 mg/kg D.W. 0.96 4 SW846: 6010C. MMSD 02/06/14 DM0206/14001517 26 mg/kg D.W. 0.96 4 SW846::6010C MMSD 02/07/14 DM0207/14001532 37. mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/08/14 : - DM0208114601543 36 mg/kg D:W. 0.96 4` SW846: 6010C MMSD 02/09/14 DM0209/14001562 39 mg/kg D.W. . 0.96 4 SW846: 6010G MMSD 02/10/14 DM0210/14001576 40 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/11/14 DM0211/14001811 35 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/12/14 DM0212/14001837 33 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/13/14 DM0213/14001856 37 mg/kg D.W. 0.96 4 SW846:, 601QC MMSD 02/14/14 DM0214/14001871 30 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/15/14 DM0215/14001882 30 mg/kg D.W. 0.96 4' SW846: 6010C MMSD 02/16/14 DM0216/14001893 26 mg/kg D.W. 0.96 4 SW846: 6010C MMSD - SY5/rpt1Ni1bMonth/y 1/10/13 tj - Page 36 of 106 Printed.• 11811510:48 + ,t P'OTNIki In s Ciw a umi€ NaT LEAD ICP METHOD 02/17/14 DM0217/14001914 29 mg/kg D:W. 0.96 4 Annual Milorganite Report January 1 to December 31, 2014 Ew SW846: 6010C MMSD 02/18/14 DM0218/140020b2 26 mg/kg D.W. 0.96 4 D2, Q2. SW846: 6010C MMSD 02/19/14 DM0219/14002b28 27 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/20/14 DM0220/14002101 29 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/21/14 DM0221/14002181 31 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/22/14 DM0222/14002102 39 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/23/14 DM0223/14002211 _ 33 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/24/14 DM0224/14002224 36 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/25/14 DM0225/14002251 32 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/26/14 DM0226/14002310 32 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 02/27/14 DM0227/14002329. 31 mg/kg D.W. _ 0.96 4 SW846: 6010C MMSD 02/28/14 DM0228/14002350 25 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/01/14 DM0301/14002921 32 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/02/14 DM0302/14002940 32 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/03/14 DM0303/14002953 35 mg/kg D.W. 6.96 4 SW846: 6010C MMSD 03/04/14 DM0304/,14002986 33 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/05/14 DM0305114003012 37 mg/kg D:W. 0.96 4 SW846: 6010C MMSD 03/06/14 DM0306/14003182 41 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/07/14 DM0307/14003197 41 mg/kg D.W. 6.96 4 SW846: 6010C MMSD 03/08/14 DM0308/14003208 39, mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/09/14 DM0309/14003232 37 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/10/14 : bM0310/14003245 96 mg/kg D.W. 0.96 4 Q3. SW846: 6010C MMSD 03/11/14 DM0311/14003272 43 mg/kg D.W. 0..96 4 SW846: 6010C MMSD 03/12/14 DM0312/14003300 40 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/13/14 DM0313/14003871 47 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/14/14 DM0314/14003886 44 mg/kg D.W. 0.96 4 A0. SW846: 6010C MMSD 03/15/14 DM0315/14.003899 45 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/16/14 DM0316/14003918 43 mg/kg D.W. 0.96 4 SW846-.6010C MMSD 03/17/14 DM0317/14003936 40 mg/kg D.W. 0.96 4 SW846: 6010C. MMSD 03/18/14 DM0318/14003963 35 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/19/14 DM0319/14004217 33 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/20/14 DM0320/14004315 37 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/21/14 DM0321/14004330 40 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/22/14 DM0322/14004341 36 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/23/14 DM0323/14004360 39 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/24/14 DM0324/14004461 35 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/25/14 DM0325/14004638 25 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/26/14 DM0326/14004664 27 mg/kg D.W. 0.96 4 SW846: 6610C MMSD 03/27/14 DM0327/14004683 23 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/28/14 DM0328/14004698 20 mg/kg D.W. 0.96 -4 SW846: 6010C MMSD 03/29/14 CiM0329/14004889. 32 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/30/14 DM0330/14004908 30 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 03/31/14 DM0331/14004921 49 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 04/01/14 DM0401/14004948 31 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 04/02/14 bM0402/14004974 33 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 04/03/14 DM0403/14004993 38 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 04/04/14 DM0404/14005195 36 mg/kg D.W. 0.96 4 SW846: 6010C MMSD SY5/rptlMi1bMonth1y 1/10/13 tj Page 37 of 106 Printed., 11811510:48 4 mbu P,t'aw(U�AClEkt{ L��I�itlkfNl LEAD ICP METHOD 04/05/14 DM0405/14005206 35 mg/kg D.W. 0.96 4 Annual Milorganite Report January 1 to December 31, 2014. SW846: 6010C MMSD 04/06/14 DM0406/14005220 35 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 04/07/14 DM0407/14005240. 35 mg/kg D.W: 6.96 4 SW846:.6010C MMSD 04/08/14 DM0408114005267 36 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 04/09/14 DM0409/14005397 31 mg/kg D.W. 0.96 4: SW846: 6010C MMSD 04/10/14 DM0410/14005416 35 mg/kg D.W. 0.96 4 SW846: 6010C.. MMSD 04/11/14 DM0411/14005434: 25 mg/kg D.W. 0.96 4 SW846::6010C MMSD 04/12/14 DM0412/14005605 28 mg/kg D.W. 0.96 4 .. SW846: 6010C MMSD 04/13/14 DM0413/14005627 24 mg/kg D:W. 0.96 4 SW846: 6010C MMSD 04/14/14 DM0414/14005641 . 44 mg/kg D.W. 0.96 4 SW846: 6010C MMSD' 04/15/14 DM0415/14005668 53 mg/kg D.W: 0.96 4 SW846: 6010C MMSD 04/16/14 DM0416/14005791 59 mg/kg DM. 0.96 4: SW846: 6010C MMSD 04/17/14 DM0417/14005815 68 mg/kg DX 1.6 4 SW846: 6010C MMSD 04/18/14 DM0418/14006027. 55 mg/kg D.W. 0.96 4 SW846:,6010C MMSD 04/19/14 DM0419/14006038 61 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 04/20/14 DM0420/14006057 99 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 04/21/14 DM0421/14006127 67 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 04/22/14 DM0422/14006154 53 mg/kg D.W, 0.96 4 SW846: 6010C MMSD 04/23/14 DM0423/14006180 44 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 04/24/14 DM0424/14006339 47 mg/kg D.W. 0.96 4 SW846: 6010C MMSD .. 04/25/14 DM0425/140063544 44 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 04/26/14 DM0426/14006365, 52 mg/kg D.W: 0.96 4 SW846:.6010C MMSD 04/27/14 DM0427/14006384 44 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 04/28/14 DM0428/14006397 44 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 04/29/14 DM0429/14006454 36 mg/kg D.W. 0.96 4 SW846: 6010C _ MMSD 04/30/14 " DMQ430/14006482 46 mg/kg D.W. 0.96 - 4 SW846: 6010C MMSD 05/O1/14 DM0501/14006976 55 mg/kg D.W. 0.96 4.: SW846: 6010C MMSD 05/02/14 DM0502/14006901 51 mg/kg D.W. 0.96 .4 SW846: 6010C MMSD 05/03/14 DM0503/14007150 46 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 05/04/14 DMO504/14007169 46 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 05/05/14 DMO505/14007182 41 mg/kg D.W. 0.96 4: SW846: 6010C MMSD 05/06/14 : DMO506/14007209 45 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 05/07/14 bm05O7/14007235 45 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 05/08/14 DM0508/14007254 41 mg/kg D.W. 0.96 4 SW846: 6010C MMSD 05/09/14 DM0509/14007269 42 mg/kg D.W. 0.86 .4 SW846: 6010C .MMSD .: O5j10/14 DM0510/14007280 48 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 05/11/14 : DM0511/14007456:. ," 44mg/kg D.W. 1.6 4 SW846:6010C MMSD 05/12/14 DM0512/14007469 43 mg/kg D.W. 1.6 4.. SW846: 6010C MMSD 05/13/14 DM0513/1:4007551 42 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 05/14/14 DM0514/14007577 39 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 05/15/14 DM0515/14007665 43 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 05/16/14 DM0516/14007680 56 mg/kg D.W. 0.88 4, SW846: 6010C MMSD 05/17/14 DM0517/14007691 52 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 05/16/14 DM0518/14007110 45 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 05/19/14 DM0519114007764 42 mg/kg D.W. 0.88 4 A0. SW846: 6010C MMSD 05/20/14 DM0520/1.4007997 50 mg/kg D.W. 0.88 4: SW846: 6010C MMSD 05/21/14 DM0521/14008023 45 mg/kg D.W. 0.88 4 SW846: 6010C MMSD SYM/rptlMMOMonthiy 1110113 tj Page 38 of 106 Printed- 1/8/I510:98 � MSD �dPiNIF314�.b` ClUi1� Ck6lb;Mhtpii LEAD ICP METHOD Sample Diate 05/22/14 DMO522/14008042 56 mg/kg D.W. lt= 1.6 IOQ Q• 4 � e � r Annual Milor anite Re ort 9 p January 1 to December 31, 2014 SW846: 6010C MMSD 05/23/14 DM0523/14008057 42 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 05/24/14 DMO524/14008291 43 mg/kg D.W. 9.88 4 SW846: 6010C MMSD 05/25/14 DMO525/14008310 43 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 05/26/14 DM0526/14008323 38 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 05/27/14 _ DM0527/14008646 36 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 05/28/14 DM0528/14008672. 37 mg/kg D.W. 9.88 4 SW846: 6010C MMSD 05/29/14 DMO529/14008691 35 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 05%30/14 DM0530/14008845 .53 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 05/31/14 DM0531/i4008856 51 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/01/14 DM0601/14009580 52 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/02/14 DM0602/14009593 49 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/03/14 DM060 ?14009620 51 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/04/14 DM0604/14009635 53 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 06/05/14 DM0605/14009654 55 mg/kg D.W. 0.88 4 SW846:6010C MMSD 06/06/14 DM0606/14009669 53 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 06/07/14 DM0607/14009844 51 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 06/08/14 DM0608/14009667 58 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 06/09/14 DM0609/14009880 47 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 06/10/14 DM0610/1.4009907 46 mg/kg D.W. 0.88 4 . SW846: 6010C MMSD 06/11/14 DM061,1/14010237 96 mg/kg D.W. 1.6 4 Q3. SW846: 6010C MMSD 06/12/14 bM0612/14010256 58 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/13/14 DM0613/14010271 59 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/14/14 DM06.14/14010282 :55 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/15/14 DM0615/14010301 52 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/16/14 DM0616/14010319 54 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/17/14 DM0617/14010346 56 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/18/14 DM0618114010687 58 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/19/14 DM0619/14010706 63 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/20/14 DM0620/14010721 68 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/21/14 DM0621114010732 74 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/22/14 DMO622/14010751 76 rung/kg D:W. 1.6 4 SW846: 6010C MMSD 06/23/14 DM0623/14011513 72 mg/kg D.W. .1.6 4 SW846: 6010C MMSD 06/24/14 DM0624/14011540 73 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/25/14 DM0625/14011566 80 mg/kg D.W. 1.6 4, SW846: 6010C MMSD 06/26/14 DM0626/14011766 84 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/27/14 DM0627/14011781 78 mg/kg D.W. .1.6 4 SW846: 6010C MMSD 06/28/14 DM0628/14011792 70 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/29/14 DM0629/14011811 67 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 06/30/14 DM0630/14011824 72 mg/kg,D.W. 1.6 4 SW846: 6010C MMSD 07/01/14 DM0701/14011851 68 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 07/0,2/14 DM0702/14011879 66 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 07/03/14 DM0703/14011898 68 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 07/04/14 DM0704/14011911 71 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 07/05/14 DM0705/14011924 73 mg/kg D.W. 1.6 4 SW846: 6016C MMSD 07/06/14 DM0706/14011943 76 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 07/07/14 DM0707/14012196 71 mg/kg D.W. 1.6 4 SW846: 6010C MMSD SYS/rptlMiloMontbly 1/10/13 tj Page 39 of 106 Printed.-1/8/1510.48 46 Y r� MS- PdAipif� IU? � C1k7.'�tR (�7i��NNfH1 LEAD ICP METHOD. Sample o. i 07/08/14 _' DM0708/14012898 Result 71 mg/kg D.W. Lob 1.6 LbQ QA Flags 4 Annual Milorganite' Report January 1 to December 31, 2014 Analytical Method Lab SW846: 6010C MMSD 07/09/14 DM0709/14012926 65 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 07/10/14 DM0710/14012945. 72 mg/kg D.W. 1.6 4 SW846: 6oik: MMSD 07/11/14 DM0711/14012961 75 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 07/12/14 DM0712/14012971 61 mg/kg D.W. 0.88 .4' _ SW846: 6010C MMSD 07/13/14 DM0713/14012991 59 mg/kg D.W. 0.88 4 SW846: 6010C. MMSD 07/14/14 DM0714/14013004 55 mg/kg D.W. 6.88 :. 4 SW846: 6010c MMSD 07/15/14 DM0715/14013031 59 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 07/16/14 DM0716/14043059 56 mg/kg DM. 0.88 4 SW846: 6010C MMSD 07/17/14 DM0717/14013078 61 mg/kg D.W. .0.88 4 SW846: 6010C : MMSD 07/18/14 DM0718/14013295 56 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 07/19/14 DM0719/14013305 56 mg/kg D.W. 0.88 4.-, SW846: 6010C MMSD 07/20/14 DM0720/14013324 59 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 07/21/14 DM0721/14013337 55 mg/kg D.W. 0.88 4 SW846:.6010C MMSD 07/25/14 DM0725/14013997 55 mg/kg D.W.. 0.88 4 SW846: 6010C MMSD 07/26/14 _ DM0726/14014008 43 mg/kg D.W. 0.88 4: SW846: 6010C MMSD 07/27/14 DM0727114014027 39 ing/kg D.W. 0.88 4 SW846: 6010C MMSD 07/28/14 DM0728/14014040 35 mg/kg D.W.: . 6.88 4 SW846: 60fOC �. MMSD 07/29/14 DM0729/14014895 40 mg/kg D.W. 0.88 4 SW846: 60iOC MMSD 07/30/14 DM0730/14014923 42 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 07/31/14 DM0731/14014942 38 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 08/01/14 DM0801/14014957 39 mg/kg D.W. 0.88 4 SW846:;6010C MMSD 08/02/14 DM0802/140.14968 50 mg/kg D.W. 1.6 4. SW846: 6010C MMSD M/63/14 DM0803/14014987 51 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 08/04/14 DMO804/14015000 50 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 08/05/14 DM0805/14015027 35 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 08/06/14 DMO806/14015405 33 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 08/07/14 DM0807/14015456 38 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 08/08/14 DMO808/14015471 40 mg/kg D.W, 0.88 4 SW846: 6010C : MMSD 08/09/14 DM0809114015482 34 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 08/10/14 DM08.10/14018966 37 mg/kg D.W. 0.88 4:: SW846: 6010C MMSD 08/11/14 DMO811/1401598'4 35 mg/kg D.W. 0.86 4 SW846: 6010C MMSD 08/12/14 DM0812/14016011 37 mg/kg D.W, 0.88 4 SW846: 6010C MMSD 08/13/14 DMO813/14016039 42 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 08/14/14 DMO814/14016058 40 mg/kg D.W. 0.88 4: SW846: 6010C MMSD 08/15/14 DM0815/14016181 43 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 08/16/14 DM0816/14016192 43 mg/kg D.W. 0.88 4 SW846::6010C MMSD 08/17/14 DM08171140.16211 42 mg/kg D.W. 0.88 4. SW846: 6010C MMSD 08/18/14 DM0818/14016290 45 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 08/19/14 DM0819/14016319 51 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 08/20/14 DM0820/14016347 58 mg/kg D.W. 0.88 4 SW846:'6010C MMSD 08/21/14 DM0821/14016366 65 mg/kg D.W. 0.88 4.: SW846: 6010C MMSD 08/22/14 DM0822/14016381 60 mg/kg D:W. 0.88 4 SW846: 6010C MMSD 08/23/14 DM0823/14016392 72 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 08/24/14 DMO824/14016411 63 mg/kg D.W., 0.88 4 SW846: 6010C MMSD 08/25/14 DMO825/14016488 59 mg/kg D.W. 0.88 4 : ': SW846: 6010C MMSD 08/26/14 DM0826/14016515 62 mg/kg D.W. 0.88 4 SW846: 6010C MMSD SY5/rptlMi/oMonth/y 1110113 tj Page 40 of 106 Printed. • 1/8/1510:48 � 1 0 f 1, Tol, M S D P)MINIf3 f0k d CuMiR INOUNNINT LEAD ICP METHOD 08/28/14 DM0828/14016907 60 mg/kg D:W. 0.88 4 Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 08/2.9/14 DM0829/14017671 65 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 68/30/14 DM083b/14017682 65 mg/kg D.W., 01.88 4 SW846: 6010C MMSD 08/31/14 DM0831/14017701 52 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 09/01/14 DMO901/14017714 .53 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 09/62/14 DM0902/14017871 56 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 09/03/14 DMO903/14017886 _ 52 mg/kg D.W., 0.88 4 SW846:-6010C MMSD 09/04/14 DMO904/14017920 48 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 09/65/14 DM0905/1401790.1 45 mg/kg D.W. 0.88 '4 SW846: 6010C MMSD 09/16/14 DM0916/14019167 53 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 09/17/14 DMO917/14019195 45 mg/kg D.W: 0.88 4 SW846:-6010C MMSD 09/18/14 DM0918/14019229 47 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 09/19/14 DM0919/14019244 44.mg/kg D.W. 0.88 .4 ''SW846: 6010C MMSD 09/20/14 DM0920/14019255 44 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 09/21/14 DMO921/14019274 45 mg/kg D.W. 0.88 4 SW846-.6010C MMSD 09/22/14 DMO922/14019287 46 mg/kg D:W. 0.88 4 SW846: 6010C MMSD 09/23/14 DMO923/14019778 47 mg/kg D:W. 0.88 4 SW846: 6010C MMSD 09/24/14 DMO924/14019806 45 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 09/25/14 DMO925/14019825 47 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 09/26/14 DMO926/14019840 47 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 09/27/14 DMO927/14019851 44 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 09/28/14 DM0928/14019870 42 mg/kg D.W. 0.86 4 SW846: 6010C MMSD 09/29/14 DM6929/14019883 45 mg/kg D.W. 0..88 _ 4 SW846: 6010C MMSD 09/30/14 DMO930/14019909 50 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/01/14 DM1001/14019927 46 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/02/14 DM1002/14020572 49 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/03/14 DM1003/14020587 73 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/04/14 DM1004/14020598 60 mg/kg D:W. 1.6 4 SW846: 6010C MMSD 10/05/14 DM1005/14020617 59 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 10/06/14 DM1006/14020630 58 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 10/07/14 DM1007/14021108 58 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 10/08/14 DM1008/14021160 55 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 10/09/14 DM1009114021170 59 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 10/10/14 DM1010/14021194 54 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 10/11/14 DM1011/14021244 43 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/12/14 DM1012/14021263 39 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/13/14 DM1013/14021276 42 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/14/14 DM1014/14021304 42 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/15/14 DM1015/14021332 45 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/16/14 DM1016/14021351 51 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/17/14 DM1017/14021787 44 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/18/14 DM1018/14021798 47 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/19/14 DM1019114021817 48 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/20/14 DM1020/14021830 47 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/21/14 DM1021/14021857 48 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 10/22/14 DM1022/14021885 49 mg/kg D.W. 0.88 4; SW846: 6010C MMSD 10/23/14 DM1023/14022256 55 mg/kg D.W. 0.88 4 SW846: 6010C MMSD SYS/rptImlloMonth/y 1/10/13 tj Page 41 of 106 Printed.• 11811510:48 a P.USi�CRa (#i3 � ElL4�tli CKIID.NNt�' LEAD ICP METHOD Sample rate- r Result LOD r r r Annual Milorganite Report January 1 to December 31, 2014 10/24/14 DM1024/14022273 43 mg/kg D.W. 0.88 4 • .':SW846* 6010C MMSD 10/25/14, . DM1025/14022286 43 mg/kg D.W. 0.88 4. SW846: 6010C MMSD 10/26/14 DM1:026/14022305 43 mg/kg D.W. J6.88 .. 4 SW846: 6010C MMSD 10/27/14 DM1027/14022318 40 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 16/28/14 DM102.W4022409 43,mg/kgD.W. 0.88 4' SW846:6010C MMSD _ 10/29/14 DM1029/14022439 44 mg/kg D.W. Q.88 4 SW846: 6010C MMSD 10/30/14 DM1,030/14022510 35 mg/kg D.W.. 0.88 4 SW846:16010C MMSD 10/31/14 DM1031/14022525 37 mg/kg D.W. '0.88 4 SW846: 6010C MMSD il%OS/14 DM1101/14022536 39 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/02/14 DM1102/14022565 36 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/03/14 DM1:103/14022568 37 mg/kg D.W. :0.88 4 SW846: 6010C MMSD 11/04/14 DM1'104/14023111 31 mg/kg D.W. 0.88 4.. SW846: 6010C MMSD 11/OS/14 DM1105/14023139 32 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/06/14 DM1:106/14023158 33 mg/kg D.W., 0.88 4 SW846: 6010C MMSD 11/07/14 DM1:107/14023173 36 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/08/14 DM1108/14023184 34 mg%kg D.W. 0.88 4 SW846: 6010C MMSD 11/09/14 DM1109/14023203 33 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/10/14 DM1110/14023767 30 mg/kg D.W.: 0.88 4 SW846::6010C MMSD 11/11/14 DM1111/14023796 33 mg/kg D.W. 0.88 4 SW846: 6010C MMSD If/f2/14 DM1112/14023876 31 mg/kg D.W. 0.88 .4. " SW846: 6010C MMSD 11/13/14 DM1113/14023895 28 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/14/14 DM1:114114023910 29 mg/kg D.W. '0.88 4 SW846: 6010C MMSD 11/15/14 DM1115/14023929 28 mg/kg D.W. 0.88 4,. SW846: 6010C MMSD 11/16/14 DM1116/14623948 27 mg/kg D:W. 0.88 4 SW846: 6010C MMSD 11/17/14 DM1117/14023961 32 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/18/14 DM1.118/14024236 28 mg/kg D.W: 0.88 4 SW846: 6010C MMSD 11/19/14 DM1119/14024264 30 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/20/14 DM1120/14024283 27 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/21/14 DM1,121114024302, 25 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/22/14 DM1122/14024313 30 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/23/14 DM1123/14024393 .28 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/24J14 DM1124/14024414 28 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/25/14 DM1;125/14024441 31 mg/kg D.W., 0.88 4 SW846: 6010C MMSD 11/26/14 DM1,126/14024469 29 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/27/14 DM1127/14024529 31 mg/kg D.W. 0.88 4 :SW846: 6010C MMSD _ 11./28/14 DM1128/14024544 33 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 11/29/14 DM1:129/14024555 36 mg/kg D.W. 0.88 4 SW846:,6010C MMSD 11/30/14 DM1130/14024574 29 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/01/14 : DM1201114024601 30 mg/kg D:W. 0.88 4 SW846: 6010C MMSD 12/02/14 DM1202/14025299 31 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/03/14 DM1203/14025327 31 mg/kg D.W. T0.88 4 SW846: 6010C MMSD 12/04/14 DM1204/14025346 31 mg/kg D.W. 0.88 .4. SW846: 6010C MMSD 12/05/14 DM1205/14025361 28 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/06/14 DM1206/14025372 22 mg/kg D.W., 0.88 4 SW846: 6010C MMSD 12/07/14 DM1207/14025391 26 mg/kg D.W.. . 0.88 4 SW846: 6010C MMSD 12/08/14 DM1208/14025404 24 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/09/14 DM1209/14026170 26 mg/kg D.W. 0.88 4 SW846: 6010C MMSD SYS/rptimlloMonthly 1110113 tj Page 42 of 106 Printed. • 1/8/1510:48 -' MA OIL R�RINCF� EDP a Ctl��t'R Ct;iit�NNENi LEAD ICP METHOD Sample e. v 12/10/14 DM1210/14026198 29 mg/kg D.W. o e LOQe 0.88 4 Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 12/11/14 DM1211/14026217 28 ing/kg D.W. 0.88 4 SW846: 6010C MMSD 12/12/14 DM1212/14026232 29 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/13/14 DM1213/14026243 25 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/14/14 DM1214/14026262 28, mg/kg D.W. 0.88 4:, SW846: 6010C MMSD 12/15/14 DM1215/14026277 24 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/16/14 DM1216/14026475. 20 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/17/14 DM1217/14026503 20 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/18/14 DM1218114026522 23 mg/kg D.W. 0.88 .4 SW846: 6010C MMSD 12/19/14 DM1219/14026537 21 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/20/14 DM1220/14026653 19 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/21/14 DM1221/14026672 19 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/22/14 DM1222/14026685 '19 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/23/14 DM1223/14026713 20 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/24/14 DM1224/14026741 22 mg/kg D.W. 6.88 4 SW846: 601k MMSD 12/25/14 DM1225/14026760 24 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/26/14 DM1226/14026777 28 mg/kg D.W. 0.88 4 SW846: 6010C MMSD 12/27/14 DM1227/14026788 43 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 12/28/14 DM1228/14026807 43 mg/kg D.W: 1.6 4 SW846: 6016C MMSD 12/29/14 DM1229/14027031 41 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 12/30/14 DM1230/14027058 47 mg/kg D.W. 1.6 4 SW846: 6010C MMSD 12/31/14 DM1231/14027086 29 mg/kg D.W, 11.88 4 SW846: 6010C MMSD Avg: 46 mg/kg D.W. Max: 210 mg/kg D.W. Page 43 of 106 SYS/rptlMiloMonthly 1/10113 tj Printed.11811510:48 MSD p�i�t�3 ray p crt.�� rr<e�i��ar�r MERCURY by M.:7471 (sludge) Sample D. 0o 00 0 Annual Milorganite Report January 1 to December 31, 2014 . 01/04/14 WMC1114000137 0.52 mg/kg D.W. 0.038 0.081 7471A ;tAmerica Chic 01/11/14 WMC2/14000475 0.42 mg/kg D.W. 0.041 0.0M 7471A Mmerica Chic 01/18/14 WMC3/14000605 0.26 mg/kg D.W. 6.038 0.082 7471E ;tAmerica Chic 01/25/14 WMC4/14001097 0.37 mg/kg D.W. 0.039 0.083 7471A ;tAmerica Chic 02/0i/14 WMC8/14001445 0.31 mg/kg D.W. 0.041 0.088 7471A ;tAmerica Chic 02/08/14 WMC6/14001578 0.33 mg/kg D.W. 0.036 0.077 7471A _ ;tAmerica Chic 02/15/14 WMC7/14001916 0.32 mg/kg D.W. 0.014 0.035 7471A Mmerica Chic 02/22/14 WMC8/14002226 0.048 mg/kg D.W. 0.0062 0.016 7471A Mmerica Chic 03/01/14 WMC9/14bO2955 0.32 mg/kg D.W. 0.0062 0.016 7471A Mmerica Chic 03/08/14 WMC10/14003247 0.34 mg/kg D.W. 0.0084 0.021 7471A ;tAmerica Chic 03/15/14 WMC11/14003938 .0.28 mg/kg D.W. 0 0067 0.017 7471A tAmerica Chic 03/22/14 WMC12/14004463 0.018 mg/kg D.W. 0.0064 0.016 7471A ;tAmerica Chic 03/29/14 WMC13/14004923 0.035 mg/kg D.W. 0.0065 0.017 7471A ;tAmerica Chic 04/05/14 WMC14/14005242 0.26 mg/kg D.W. O'.0064 0.016 7471A ;tAmerica Chic 04/12/14 WMC15/14005643 0.053 mg/kg D.W. 0.0069 0.017 7471A Mmerica Chic 04/19/14 WMC16/14006129 0.066 rpg/kg D.W. 0.0068 0.017 7471A ;tAmerica Chic 04/26/14. WMC17/14006429 0.017 mg/kg D.W. 0.0066 0.017 7471A Mmerica Chic 05/03/14 WMC18/14007184 0.38 mg/kg D.W. '0:0065 0.017 7471A Mmerica Chia 05/10/14 WMC19/14007579 0.02 mg/kg D.W. 0.0069 0.018 7471A Mmerica Chic 05/17/14 WMC20/14007770 0.29 mg/kg D.W. 0.0069 0.018 7471A Mmerica Chia 05/24/14 WMC91/14008326 0.28 mg/kg D.W. 0.0061 0.016 7471A ;tAmerica Chia 05/31/14 1NMC22/14009595 0.2 mg/kg D.W. 00068 0.017 7471A Mmerica Chia 06/07/14 WMC23/14009882 0.0074 mg/kg D.W. 0.0066 0,017 J 7471A ;tAmerica Chic; 06/14/14 WMC24/14010321 0.28 mg/kg D.W. 0.0069 0.017 7471A tAmerica Chic 06/21/14 WMC25/14011615 0.33 mg/kg D.W. 0.0064 0.016 7471A Mmerica Chia 06/28/14 WM626/14011826 0.35 mg/kg D.W. 0.0066 0.017 7471A ;tAmerica Chic 07/05/14 WMC27/14012198 0.34 mg/kg D.W. 0.007 0.018 7471A ;tAmerica Chia 07/12/14 WMC28/14013005 0.12 mg/kg D.W. 0.0068 0.017 7471A Mmerica Chic 07/19/14 WMC29/14013339 0.43 mg/kg D.W. 0.0068 0.017 7471A Mmerica Chic . 07/26/14 WMC30/14014042 :0.17 mg/kg D.W. 0.0065 0.017 7471A Mmerica Chic 08/02/14 WMC31/14015002 0.4 mg/kg D.W. 0.007 0.018 7471A Mrhehca'Chia 09/09/14. WMC32/14015986 0.33 mg/kg D.W. 0.0065 0.017 7471A ;tAmerica Chia 08/16/14 . . WMC33/14016294 0.33 mg/kg D.W. 0.0064 .: 0.016 7471A ;tAmerica Chic; . 08/23/14 WMC34/14016490. 0.038 mg/kg D.W. 0.0067; 0.017 7471A Mmerica Chic ' 08/30/14 WMC35/14017716 0.099 mg/kg D.W. 0.0068 0.017 7471A ;tAmerica Chic 09/05/14 WMC36/14018081 0.13 mg/kg D.W. 0,0067 0.017 7471A ;tAmerica Chic 09/20/14 WMC 38/14020851 0.14 mg/kg D.W. 0.0064 .' 0.016 74tA ;tAmerica Chic 09/27/14 WMC39/14020976 0.066 mg/kg D.W. 0.0065 0.017 7471A Mmerica Chic; 10/04/14 WMC40/14021278 0.028 mg/kg D.W. 0.0061 0.016 7471A ;tAmerica Chia 10/11/14 WMC41/14021279 0.089 mg/kg D.W. 0.0068 0.017 AX. 7471A .: ;tAmerica Chic; 10/18/14 WMC42/14021832 0.84 mg/kg D.W. 0.034 0.088 AX. 7471A Mmerica Chic 10/25/14 WMC43/14022322 0.23 mg/kg D.W. 0.007 0.018 AX. 7471A Mmerica Chia 11/01/14 WMC44/14022570 0.1 mg/kg D.W. 0.0071 0.018 AX. 7471A tAmerica Chic 11/08/14 WMC45114023769 .0.19 mg/kg D.W. 0.0067 0.017 7471A Mmerica Chia 11/15/14 WMC46/14023963 0.061 mg/kg D.W. 0.0069 0.017 7471A Mmerica Chic; 11/22/14 WMC47/14024416 0.36 mg/kg D.W. 0.0065 0.017-'7471A ;tAmerica Chia 11/29/14 WMC48/14025406 0.59 mg/kg D.W. 0.014 0.035 7471A Mmerica Chic SYS/rptimlloMonth/y 1110113 U Page 44 of 106 Printed.1/8/1510:48 MMCR e s Annual Milorganite Report January 1 to December 31, 2014 PAPI NIN IDI A CILM1R INOWN(NT MERCURY by M..747i (sludge) Sample Date Samplie,113 Aet 12/06/14 WMC49/14025407 0.48 mg/kg D.W. 0.034 0.086 7471A Mmerica Chic 12/13/14 WMC50/14026279 0.1 mg/kg D.W. 0.0069 0.018 7471A ;tAmerica Chic 12/26/14 WMC51/14026687 0.36 mg/kg D.W. 0.067 0 7471A Mmerica Chia 12/27/14 WMC52/14027033 0.57 mg/kg D.W. 0.035 0.09 7471A tAmerica Chia Avg: 0:25 mg/kg D.W. Max: 0:84.mg/kg D.W. Page 45 of 106 5Y5/rptIN1/oMonth/y 1110113 tj Printed. • 1/8/1510:48 f� FAMRS fW A 6LW LkiIW[W MOLYBDENUM YCP METHOD sample Date Sample ID Result LOD WQ Annual Milorganite Report January 1 to December 31, 2014 lyeical Met d Lab 01/01/14 DMO101/14000012 11 mg/kg D.W. 0.18 1 SW846: 6010C MMSD O1/02/14 DMO102/14000039 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/03/14 DMO103/14000088 12 mg/kg D.W. 0'.18 1 SW846: 6010C MMSD 01/04/14 DMO104/14000103 12 mg/kg D.W. 0.18 1 SW846: 6010C MMSD . 01/05/14 DMO105/14000122 13 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/06/14 DM0106/14000135 14 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/07/14 DMO107/14000162 13 mg/kg D.W. 0.18 1 SW846: 6010C MMSD O1/08/14 DM0108/14000188 13 mg/kg D.W. 0.18 1 _ SW846: 6010C MMSD, 01%09/14 DMO109/14000207 12 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/10/14 DM0110/14000430 13 mg/kg D.W. 0.18 1 SW846:.6010C MMSD 01/11/14 DM0111/14000441 13 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/12/14 DM0112/14000460 13 mg/kg D.W. 0.18 1; SW846: 6010C MMSD 01/13/14 DM0113/14000473 13 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/14/14 DM0114/14000500 13 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/15/14 DM0115/14000526 12 mg/kg D.W. 0.1'8 1 SW846: 6010C MMSD 01/16/14 DM0116/14000545 11 mg/kg D.W. 0.18 1., SW846: 6010C MMSD 01/17/14 DM0117/14000560 11 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/18/14 DM0118/14000571 12 mg/kg D.W: 0.18 1 SW846: 6010C MMSD 01/19/14 DMO119/14000590 12 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/20/14 DMO120/14000603 13 rrig/kg DM. 0.18 1; SW846: 6010C MMSD 01/21/14 DMO121/14000630 12 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/22/14 DM0122/14000656 10 mg/kg D.W: 0.18 1 SW846: 6010C MMSD 01/23/14 DM6123/14000675 9.9 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/24/14 DMO124/14000690 10 Mg/kg D.-W. 0.18 1 SW846: 6010C MMSD 01/25/14 DM0.125/14000923 it mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/26/14 DMO126/14000942 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/27/14 DM0127/14001095 10 mg/kg D.W. 0.18 1 . SW846: 6010C MMSD 01/28/14 DMO128/14001122 .9 rig/kg D.W. 0.18 1 SW846: 6010C MMSD 01/29/14 DMO129/14001148 9.9 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/30/14 DM0130/14001167 9.6 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 01/31/14 DM0131/14001182 10 mg/kg D.W. 0.18 1 _ SW846: 6010C MMSD 02/01/14 DM0201/140011,93 11rrig/kg D.W. 0.18 1_ SW846: 6010C MMSD,, 02/02/14 DM0202/14001430 11 mg/kg D.W. 0.18 1 SW846:.6010C MMSD 02/03/14 DM6203/14001443 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/04/14 DM0204/14001470 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD .. 02/05/14 DM0205/14001498 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/06/14 DMO206/14001517 9.4 mg/kg D.W.' 0.18 1 SW846:.6010C MMSD 02/07/14 DM0207/14001532 9.2 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/08/14 DM0208/14001543 9.7 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/09/14 DM0209/14001562 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/10/14 DM0210114001576 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/11/14 DM0211/14001811 11 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/12/14 DM0212/14001837 9.7 mg/kg D.W. 0.18 1 SW846: 6010C MMSD UL/1.S/14 UIVIUL 10/ 1 fuu 1000 7.V II R1/ry U. VV. ' U.10 1 JVYo'tV. --u 02/14/14 DM0214/14001871 - 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/15/14 DM0215/14001882 10 mg/kg D.W. 0.18 1: SW846: 6010C MMSD 02/16/14 DM0216/144001893 9.8 mg/kg D.W. 0.18 1 SW846: 6010C MMSD Page 46 of 106 SYS/rptiMi/oMonthiy 1110113 0 Pr/nted.11811510:48 D ft P,#Rt�tA,f ID?A, L'l}�,41k tk�li�7NNItit MOLYBDENUM,YCP METHOD 02/17/14 DM0217/14001914 9.5 mg/kg D.W. 0.18 1 Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 02/18/14 DM0218/14002002 9.1 mg/kg DX 0.18 1 SW846: 6010C MMSD 02/19/14 DM0219/14002028 9.3 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/20/14 DM0220/14002101 9.7 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/21/14 DM0221/14002181 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/22/14 DM0222/14002192 9.6 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/23/14 DM0223/14002211 11 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/24/14 DM0224/14002224 12 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/26/14 DM0225/14002251 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/26/14 DM0226/14002310 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 02/27/14 DM0227/14002329 10 mg/kg D.W. 0.18 1 SW846: 60iOC MMSD 02/28/14 DM0228/14002350 it mg/kg D.W. 0.18 1 SW846: 6016C MMSD 03/01/14 DM030.1/i4002921 11 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/02/14 DM0302/14002940 11 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/03/14 DM0303/14002953 12 mg/kg D.W. 0.18 1 SW846:•6010C MMSD 03/04/14 DM0304/14002986 9.2 mg/kg D.W. 0.18 1 SW846: 6016C MMSD 03/O5/14 DM0305/14.003012 8.9 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/06/14 DM0306/14003182 8.3 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/07/14 DM0307/14003197 8.3 mg/kg D.W. :0.18 1 SW846: 6010C MMSD 03/08/14 DM0308/14003208 8 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/09/14 DM0309/14003232 8.7 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/10/14 DM0310/14003245 9.3 mg/kg D.W. 0.18 1 SW846:, 6010C MMSD 03/11/14 DM0311/14003272 10 mg/kg D.W. 0.18 1 SW846: 6610C MMSD 03/12/14 DM0312/14003300 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/13/14 DM0313/14003871 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/14/14 DM0314/14003886 10 mg/kg D.W: 0.18 1 SW846: 6010C MMSD 03/15/14 DM0315/14003899 8.8 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/16/14 DM0316/i4003918 9.8 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/17/14 DM0317114003936 8.9 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/18/14 DM0318/14003963 8.7 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/19/14 DM0319/14004217 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/20/14 '. DM0320/14004315 9.2 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/21/14 DM0321/14004330 9.7 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/22/14 DM0322/14004341 9.5 mg/kg D.W. 0.18 1 SW8466010C MMSD 03/23/14 DM6323/14004360 8.5 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/24/14 " DM0324/14004461 6.9 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/25/14 DM0325/14004638 6.3 mg/kg D.W.. 0.18 1 SW846: 6010C MMSD 03/26/14 DM0326/14004664 6.8 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/Z7/14 DM0327/14004683 6.6 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/28/14 DM0328/14004698 6.9 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/29/14 DM0329/14004889 8.9 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03/30/14 DM0330114004908 9.3 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 03%3i/14 DM0331/14004921 9.3 mg%kg D.W. 0.18 1 SW846: 6010C MMSD 04/61/14 DM0401/14004948 9.3 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 04/02/14 DM0402/14004974 9.2 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 04/03/14 DM0403/14004993 11 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 04/04/14 DM0404/140M195 10 mg/kg D.W. 0.18 i SW846: 6010C MMSD 5YS/rptlM11bMonth1y 1/10/13 tj Page 47 of 106 Printed.,1/8/1510:48 6 Annual Milorganite' Report M Sft D January 1 to December 31, 2014 WTAW ►UkA.WRU 1WIVXRDIi MOLYBDENUM ICP METHOD Sample Date Sample e o 04/05/14 DM0405/14005206 11 mg/kg D.W. 0.18 1 : SW846: 6010C MMSD 04/06/14 DM0406/14005226 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 04/07/14 DM0407/14005240 9.7 mg/kg D.W. 0.18 1 SW846: 6010C. MMSD 04/08/14 DM0408/14005267 9.8 mg/kg D.W. 0.18 1 SW846: 6010C, MMSD 04/09/14 DM0409/14005397 10 mg/kg D.W. 0.18 -1 SW846: 6010C MMSD 04/10/14 DM0410/14005416 8.1 mg/kg D.W. 0.18 1 .. SW846: 6010C MMSD 04/11/14 DM0411/14005434, 9 mg/kg D.W... 0.18 1 SW846: 6010C MMSD 04/1.2/14 DM0412/14005605 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 04/13/14 : DM0413/14005627 9.6 mg/kg D.W. 0.18 1 "SW846: 6010C 'MMSD 04/14/14 DM0414/14005641 9 mg/kg D.W. 0.18 1 SW846: 6010c MMSD 04/15/14 DM0415/14005668' 8.8 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 04/16/14 DM0416/14005791 8.5 mg/kg D.W. 0.18 1 . SW846: 6010C MMSD 04/17/14 DM0417/14005815 8.9 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 04/18/14 DM0418/14006027 9.5 mg/kg D.W. .0.18 1 SW846: 6010C MMSD 04/19/14 DM6419/14006038 8 mg/kg D.W. 0.32 1 A0. SW846: 6010C MMSD 04/20/14 DM0420/14.006057 8.1'mg/kg D.W. 0.32 1., A0. :SW846: 6010C MMSD 04/21/14 DM0421/14006127 8 mg/kg D.W. 0.32 1 A0. SW846: 6010C MMSD 04/22/14 DM0422/14006154 8.6 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 04/23/14 DM0423/14006180 9.1 mg/kg D.W. 0.18 1 SW846: 6010C, MMSD 04/24/14 DM0424/14006339 8.6 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 04/25/14 DM0425/14006354 8.9 mg/kg D.W. 0.18 1 . SW846: 6010C MMSD 04/26/14 DM0426/14006365 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 04/27/14 DM0427/114.006384 11 mg/kg D.W. 0.18 1- _ SW846: 6010C MMSD 04/28/14 DM0428/14006397 12 rrig/kg D.W. 0.18 1 SW846: 6010C MMSD 04/29/14 DM0429/14006454 9.7 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 04/30/14 DM0430/14006482: 11 mg/kg D.W. 6.18 1 SW846:-6010C MMSD 05/OS/14 DM0501/14.006976 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 05/02/14 DM0502/14006991 9.5 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 05/03/14 DM0503/14007150 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 05/04/14 Dmb504/14007169 ' 9.1 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 05/9S/14 DM0505/14007182 8.5 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 05/06/14 DM0506/144007209 8.8 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 05/07/14 DM0507/14007235 10 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 05/08/14 DM0508/14007254 8.9 mg/kg D.W. 0.18 1 SW846: 6010C MMSD 05/6W14 DM0509/14607269 8.8 mg%kg D.W. 0.12 1, • SW846: 6010C MMSD 05/10/14 DM0510/14007280 8.7 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 05/11/14 DM0511/14007456 . 8.2 mg/kg D.W. 0.32 1 SW846::6010C MMSD 05/12/14 DMO512/14007469 7.8 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 05/13/14 DM0513/14007551 8.9 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 05/14/14 DM0514/14007577 8.6 rrig/kg D.W. . 0.12 1 SW846: 6010C MMSD 05/15/14 DM0515/14007665 8 mg/kg D.W. . 0.12 1 SW846: 6010C MMSD 05/16/14 DM0516/14007680 9.1 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 05/17/14 DM0617/14007691 7.6 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 05/18/14 DM0518/14007710 8 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 05/19/14 DM0519/14007764 8.8 mg/kg D.W. : 0.12 1 A0. SW846: 6010C MMSD 05/20/14 DM0520/14007997 8.9 mg/kg D.W. 0.12 1:: SW846: 6010C MMSD 05/21/14 DMO521/14008023 8.6 rrig/kg D.W. 0.12 3: SW846: 6010C MMSD SYS/rptlMiloMonthly 1110113 of Page 48 of 106 Printed: 11811510.48 '"r 1 ..:, P9RiNiHS f4� A ttE+H& khAC�:�}tfffl MOLYBDENUM ICP METHOD 05/22/14 DM0522/14008042 9 mg/kg D.W. 0.12 1 Annual Milorganite Report January 1 to December 31, 2014 Yt SW846: 6010C MMSD 05/22/14 DM0522/1;4008042 9.4 mg/kg D.W. 0.32 1 B8. SW846: 6010C MMSD 05/23/14 DM0523/14008057 6.2 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 05/24/14 DM0524/14008291 7.9 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 05/25/14 DM0525/14008310 8.7 mg/kg D.W. 0.12 1. SW846: 6010C MMSD 05/26/14 DM0526/14008323 8.9 mg/kg D.M. 0.12 1 SW846: 6010C MMSD 05/27/14 DM0527/14008646 9.2 mg/kg D.W. 0.12 1 SW846:.6010C MMSD 05/28/14 DM0528/14008672' 9.3 mg/kg D.W. 0.12 1 SW846: 6010C MMSD OSy29/14 DM0529/14008691 4 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 05/30/14 DM0530/14008845 10 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 05/31/14 DM0531/14008856 10 mg/kg D.W. 0.32 1 SW846::6010C MMSD 06/01/14 DM0601/14009580 9.8 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/02/14 DM0602/14009593 9.3 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/03/14 DM0603/14009620 9.4 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/04/14 DM0604/14009635 11 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 06/05/14 DM0605/14009654 9.1 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 06/06/14 DM0606/14009669 9.8 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 06/07/14 DMO607/14009844 10 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 06/08/14 DM0608/14009867 9.9 mg/kg D.W: 0.12 1 SW846: 6010C MMSD 06/09/14 DM0609/14009880 9.2 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 06/10/14 DM0610/14009907 8.5 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 06/11/14 DM0611/14010237 9 mg/kg D.W. 0.32 1 SW846:.6010C MMSD 06/12/14 DM0612/14010256 9 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/13/14 DM0613/1401027.1 9.5 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/14/14 DM0614/14010282 9 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/15/14 D100615/14010301 9 mg/kg D.W. 0.32 1 SW846::6010C MMSD 06/16/14 DM0616/14010319 9.1 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/17/14 DM0617/14010346 9.4 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/18/14 DM0618/14010687 9.8 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/19/14 DM0619/14010706 9.7 mg/kg D.W: 0.32 1 SW846: 6010C MMSD 06/20/14 DM0620/14010721 9.1 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/21/14 DM0621/14010732 9 m4/kg D:W. 0.32 1 SW846: 6010C MMSD 06/22/14 DM0622/14010751 9.2 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/23/14 DM0623114011513 9 mg/kg D.W. 0.32 1 SW846:-6010C MMSD 06/24/14 DM0624114011540 9.3 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/25/14 DM0625/14011566 8 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/26/14 DM0626/14011766, 9.5 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/27/14 DM0627114011781 8.6 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/28/14 DM0628114011792 8.3 mg/kg D.W. 0.32 1. SW846: 6010C MMSD 06/29/14 DM0629/14011811 8.6 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 06/30/14 DM0630/14011824 8.6 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 07/01/14 DM0701/14011851 9 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 07/02/14 DM0702/14011879 8.7 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 07/63/14 DM0703/14011898 9.2 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 07/04/14 DM0704/14011911 9.1 mg/kg D.W. 0.32 1 SW846; 6010C MMSD 07/05/14 DM0705/14011924 8.7 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 07/06/14 DM0706/14011943 9 Mg/kg D.W. 0.32 1 SW846: 6010C MMSD SYS/rptimi/omonth/y 1/10/13 of Page 49 of 106 Printed. • 1/8/1510:48 MSD: PAINGS tot A CRAR [tA NN(11I MOLYBDENUM ICP METHOD sample Date Sample ID 07/07/14 DM0707114012196 8.9 mg/kg D.W. 0.32 • eMethod 1 Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 07/08/14 DM0708/14012898 8.7 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 07/09/14 DM6709/14012926 8.3 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 07/10/14 DM0710/14012945 8.5 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 07/11/14 DM0711/1401296.1 9.8 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 07/12/14 DM0712/14012971 10 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/13/14 DM0713/14012991 9.8 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/14/14 DM0714/14013004 10 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/15/14 DM0715/14013031 10 mg/kg D:W. 0.12 1 SW846: 6010C MMSD 07/16/14 DM0716/14013059 9.9 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/17/14 DM6717/14013078 10 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/18/14 DM0718/144013295 9.8 mg/kg D.W. 0.12 1. SW846: 6010C MMSD 07/19/14 DM0719/14013305 9.5 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/20/14 bM0720/14013324 9.7 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/21/14 DM0721/14013337 9.7 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/25/14 DM0725/14013997 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/26/14 DM0726/14014008 14 mg/kg D.W. 0.12 Y SW846: 6010C MMSD 07/27/14 DM0727/14014027. 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/28/14 DM6728/14014040 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/29/14 DM0729/14014895 13mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/30/14 DM0730/14014923 15 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 07/31/14 DM0731/14014942 12 mg/kg D.W. u. 1 SW846: 6610C MMSD 08/01/14 DM6801/14014957 14 mg/kg D.W. 0.12 1 SW846: 60i0C MMSD 08/02/14 DM0802/14014968 11 mg/kg D:W. 0.32 T SW846: 6010C MMSD 08/03/14 DM0803/14014987 it mg/kg D.W. 0.32 1 SW846: 6010C MMSD 08/04/14 DMb804/14015000 10 mg/kg D.W. 6.32 1 SW846: 6010C MMSD 08/OS/14 DM0805/14015027 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/06/14 DMO806/14015405 9.1 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/07/14 DMO807/14015456 9.3 mg/kg D.W. 0.12 '. 1 SW846: 6030C MMSD 08/06/14 DM0808/14015471 8.9 mg/kg D.W. 0.12 1 SW846: 6610C MMSD o8/66/14 DM0809/14015482 9 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 98/10/14. ; DMO810/14015966 8.8 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/11/14 DM0811/14015984 8.6 mg/kg D.W. , 0.12 1 SW846: 6010C MMSD 08/12/14 DM0812/14016011 7.9 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/13/14 DM0813/14016039 8.3 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/14/14 DM0814/14016058 8.2 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/15/14 DM0815/14016181 9 mg/kg D.W: 0.12 1 SW846: 6010C .' MMSD 08/16/14 DMO816114016192 8.1 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/17/14 DM0817/14016211 8.1 m4ft D.W. 0.12 1 SW846: 6010C MMSD 08/18/14 DM0818/14016290 8.2 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/19/14 DMO819/14016319 8.8 mg/kg D.W. . 0.12 1 SW846: 6010C MMSD 08/20/14 DMO820/14016347 6.8 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/21/14 DM0821/14016366 6.9 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/22/14 DMO822/14016381 6.9 mg/kg D.W. 0..12 1 SW846:.6010C MMSD 08/23/14 DM0823/14016392 7.9 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/24/14 DM0824/14016411 9.4 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/25/14 DM0825/14016488 10 mg/kg D.W. 0.12 1 SW846: 6010C MMSD SY5/rptlMdoMontMy 1110113 0 Page 50 of 106 Pnnted.• 11811510.48 D IHMSD P�kiACt� t%i.A Ct4�4iR C#itiL�klt}it MOLYBDENUM ICP METHOD ample ID 08/26/14 DM0826/14016515 Ite, suit 9.1 mg/kg D:W. 0.12 1. Annual Milorganite Report January 1 to December 31, 2014 Analytical Met o �Lab SW846: 6010C MMSD 08/28/14 DM0828/14016907 7.9 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/29/14 DM0829/14017671 6 mg/kg D.W., Q.12 1 SW846: 6010C MMSD 08/30/14 DM0830/14017682 . 8.8 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 08/31/14 DM0831/14017701 11, mg/kg D.W. 0.12 1. SW846: 6010C MMSD 09/61/i4 DM0901/14017714 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD . 09/02/14 DMO902/14017871 9.3 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/03/14 DM0903/14017886 9.1 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/04/14 DM0904/14017920 9.8 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/05/14 DM0905/14017901 8.6 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/16/14 DMO916/14019167 11 mg/kg D.W. 0.12 1 SW846::6010C MMSD 09/17/14 DMO917/14019195 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/18/14 DM0918/14019229 10 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/19/14 DM0919/14019244 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/20/14 DM0920/14019255 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/21/14 DMO921/14019274 13 mg/kg D.W. 0.12 .1. SW846: 6010C MMSD 09/22/14 DMO922/14019287 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/23/14 DMO923/14019778 12 mg/kg D.W. 0,.12 1 SW846: 6010C MMSD 09/24/14 DMO924/14019806 it mg/kg D.W. , 0.12 1 SW846: 6010C MMSD 09/25/14 DMO925/14019825 11 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/26/14 DMO926/14019840 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/27/14 DM0927/14019851 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/28/14 DMQ928/14019870 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/29/14 DMO929/14019883 .16 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 09/30/14 DMO930/14019909 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/01/14 DM1001/14019927 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/02/14 DM1002/14020572 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/03/14 DM1003/14020587 18 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/b4/14 DM1004/14020598 i2 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 10/05/14 DM1:005/14020617 11 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 10/06/14 DM1006114020630 12 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 10/07/14 DM1007/14021108 12 mg%kg D.W. 0.32 1 SW846: 6010C MMSD 10/08/14 DM1008/14021160 12 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 10/09/14 DM1009/14021179 13 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 10/10/14 DM1010/1402119.4 13 mb/kg D.W. 0.32 1 SW846: 6010C MMSD 10/11/14 DM1011/14021244 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/12/14 DM1012/14021263 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/13/14 DM1;013/14021276 15 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/14/14 DM1014/14021304 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/]5/14 DM1015/14021332 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/16/14 DM1'016/14021351 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/17/14 DM1017/14021787 16 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/18/14 DM1018/14021798 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/19/14 DM1019/14021817 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/20/14 DM1020/14021830 13 mg/kg D.W: 0.12 1 SW846: 6010C MMSD 10/21/14 DM1021/14021857 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/22/14 DM1022/14021885 15 mg/kg D.W. 0.12 1 SW846: 6010C MMSD SYS/rptimloMonthly 1110113 y Page 51 of 106 Printed: 11811510:48 , � e Annual Milorganite Report January 1 to December 31, 2014. -MSD: P,9Ai11(� f OP A LCU.1z� [k�lt�J4�%CNi : MOLYBDENUM ICP METHOD Sample o. a OD- L09 Analyficaumiihad Lab 10/23/14 DM1023/14022256 12 mg/kg D.W. 0.12 1' SW846: 6010C MMSD 10/24/14. DM1024/14022273 14 mg/kg D.W. 0.12 1 " SW846: 6010C MMSD 10/25/14 DMI025/14022286 14 mg/kg D.W. 0.12 .. 1 SW846: 6010C MMSD 10/26/14 DM1026/14022305 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 10/27/14 .. DM1027/14022318 .12 mg%kg D.W. 0.12 1 SW846: 6010C 10/28/14 DM1028/14022409 12 mg/kg D.W. 0.12 1 SW846: 6010C, MMSD 10/29/14 DM1:029/14022439 12 mg/kg D.W. 0.12 1 SW846::6010C MMSD 10/30/14 DM1030/14022510 12 mg/kg D.W. 012 1... SW846: 6010C MMSD 10/31/14 :' DM1031/14022525 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/01/14 DM1.101/14022536 ... 13 mg/kg D.W. 0.12 1 ' SW846: 601,OG MMSD 11/02/14 DM1102/14022555 13 mg/kg D.W. 0..2 1 SW846:'6010C MMSD 11/03/14 DM1103/14022568 13 mg/kg DX 0.12 1.: SW846: 6010C MMSD 11/04/14 DM1104/14023111 13 mg/kg D.W. 0.12 .1 SW846: 6010C MMSD 11/05/14 DM1:105/14023139 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/06/14 DM1:106/14023158 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD Sl/07/14 DM1107114023173 14 mg%kg D.W. 0.12 1:. SW846: 6010C MMSD 11/08/i4 DM1108/144023184 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/09/14 DM1;109/14023203 • 14 mg/kg D.W.. 0.12 1 SW846:16010C MMSD 11/10/14 DM1;110/14023767 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11)11/14 DM1111/1402379.6 .14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/12/14 DM1112/14023876 14 mg/kg D.W. 0.12 1 ..SW846: 6010C MMSD. 11/13/14 DM.1113/14023895: 13 mg/kg D.W. 0.12 1 SW846:.6010C MMSD 11/14/14 DM1114/14023910 15 mg/kg D.W. 0.12 1 - SW846: 6010C MMSD ll/15/14 DM1115/14023929 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/16/14 DM1116/14023948 11 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/17/14 "' DM1117/14023961 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/18/14 DM1118/14024236 it mg/kg D.W. 0.12 1 SW846: 6010C MMSD ll/19/14 DM1119/14024264 12 mg/kg DX 0.12 1 SW846: 6010C MMSD i1/20/14 DMI120/14024283 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/21/14 DM1121/14024302 14 mg/kg D.W., 0.12 1 SW846: 6010C MMSD ll/22/14 DM1122114024313 14 mg/kg D.W. 0.12 1:: SW846: 6010C MMSD 11/23/14 DM1123/14024393 13 mg/kg D.W. 0.12 i SW846: 6010C MMSD 11/24/14 DM1124/14024414 15 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/25/14 DMT125/14024441 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/26/14 DM1126/14024469 11 mg/kg D.W. 0.12 '1:: SW846: 6010C MMSD 11/27/14 DM1127/14024529 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/28/14 DM1128/14024544 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/29/14 DM1129/14024555 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 11/50/14 . DM1130/14024574 13 mg/kg D.W. 0.12 1 $W846: 6010C MMSD 12/01/14 DM1201/14024601 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/02/14 DMl202/14025299' 11 mg/kg D.W: 0.12 1 SW846: 6010C MMSD 12/03/14 DM1203114025327 11 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/64/14 DM1204114025346 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/05/14 DM1205/14025361 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/06/14 DM1206/14025372 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/07/14 DM1207/14025391 12 mg/kg D.W. 0.12 1.: SW846: 6010C MMSD 12/08/14 DM1208/14025404 11 mg/kg D.W. 0.12 1 SW846: 6010C MMSD SY5/rptlM110M0nth1y 1/M/13 tj Page 52 of 106 Printed., 11811510:48 14 PdRMW Ibk d CUM EW KNPIN? MOLYBDENUM ICP METHOD n. 12/09/14 DM1209/14026170 12 mg/kg D.W. .t)a� 0.12 1 Annual Milorganite Report January 1 to December 31, 2014 o• SW846: 6010C MMSD 12/10/14 DM1210/14026198 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/11/14 DM1211/14026217 11 mg/kg D.W. 0'.12 1 SW846: 6010C MMSD 12/12/14 DM1212/14026232 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/13/14 DM1213/14026243 11 mg%kg D.W. 0.12 i SW846: 6010C MMSD 12/14/14 DM1214/14026262 it mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/15/14 DM1215/14026277 10 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/16/14 DM1216/14026475 10 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/17/14 .. DM1217/14026503 11 mg/kg D.W. 0.12 1. SW846: 6010C MMSD 12/i8/14 DM1218/14026522 10 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/19/14 DM1219/14026537 12 mg/kg D.W., 0.12 1 SW846: 6010C MMSD 12/20/14 DM1220/14026653 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/21/14 .. DM1221114026672 11 mg%kg D.W. 0.12 1 SW846: 6010C MMSD 12/22/14 DM1222/14026685 12 mg/kg D.W. 0.12 i SW846: 6010C MMSD 12/23/14 DM1223/14026713 13 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/24/14 DM1224/14026741 14 mg/kg D.W. 0.12 1 SW846: 6010C MMSD 12/25/14 12/26/14 DM1225/14026760 DM1226/14026777 13 mg/kg D.W. 13 mg/kg D.W. 0.12 0.12 1 1 SW846: 6010C SW846: 6010C MMSD MMSD 12/27/14 DM1227/14026788 13 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 12/28/14 DM1228114026807 13 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 12/29/14 DM1299/14027031 13 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 12/30/14 DM1230/14027058 12 mg/kg D.W. 0.32 1 SW846: 6010C MMSD 12/31/14 DM1231/14027086 12 mg/kg D.W. 0.12 1 SW846: 6010C MMSD Avg: 11 mg/kg D.W. Max- 18 mg/kg D.W. Page 53 of 106 5Y5/rptIN110M0nth/y 1110113 tj Printed- 118/1510:48 a .,, ;, -' .. PARINIz IN A Cltle IwilvNef NICKEL ICP. METHOD sample o, 01/01/14 DM0101/14000012 85 mg/kg D.W. o m 0.14 LOQ 1 Annual Milorganite Report January 1 to December 31, 2014 QA Flags Anaiwcal Method. Lab. SW846: 6010C MMSD 01/02/14 DMO102/14000039 36 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/03/14 DM0103/14000088- 40 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/04/14 DMO104/14000103 40 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/65/14 DM0105/14000122 62 mg%kg D.W. 0.14 1' SW846: 6010C MMSD 01/06/14 DMQ106/14000135 43 mg/kg D.W. 0.14 1 SW846: 6010C, MMSD 01/07/14 DMO107/14000162 44 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/08/14 DMb108/14000188 42 mg/kg D.W. 0.14 1 . SW846: 6010C MMSD 01/09/14 DM0109/14000207 40 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/10/14 DMO110114000430 41 mg/kg D.W. 0.14 1 SW846:.6010C MMSD 01/11/14 DMO111/14000441 41 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/12/14 DM0112/14000460 43 mg/kg D.W. 0.14 1 SW846: 6010C MMSD Oi/13/14 DM0113/14000473 42 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/14/14 DMO114/14000500 64 mg/kg D.W. 0.14 1 D2, Q2, Q3'. " SW846: 6010C MMSD 01/15/14 DM0115/14000526 36 mg/kg D.W. 0.14 1 SW846: 6010C MMSD O1/16/14 DM01.16/14000545 34 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/17/14 DM0117/14000560 36 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/18/14 DM.0.118/14000571 , 39 mg/kg D.W., 0.14 1 "' SW846: 6010C MMSD 01/19/14 DM0119114000590 68 mg/kg D.W. 0.14 1 SW846: 6010C MMSD O1/20/14 DMO12W14000603 39 mg/kg D:W. 0.14 1" SW846: 6010C MMSD 01/21/14 DMO121/14000630 38 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/22/14 DMO122/14000656 37 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/23/14 DMO123114000675 34 mg/kg D:W. 0.14 1. SW846: 6010C MMSD ovj 4/14 DMO124/14000690 44 mg/kg D:W. 0.14 1 SW846: 6010C MMSD 01/25/14 DMO125/14000923 36 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/26/14 DMO126/14000942 120 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/27/14 DMO127/14001095 35 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/28/i4 DMO128/14001122 36 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/29/14 DMO129/14001148 36 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/30/14 DMO130/14001167 33 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 01/31/14 DMO131/14001182 33 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/Ol/14 DM0201/14001193 62 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/02/14 bM0202/14001430 51 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/03/14 DM0203/14001443 40 mg/kg D.W. 0.14 1 D2, Q2. SW846: 6010C MMSD 02/04/14 DM0204/14001470 38 mg/kg D.W. 0.14 i SW846: 6010C MMSD 02/05/14 DM0205/14001498 36 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/06/14 DM0206/14001517 32 mg/kg D.W: 0.14 : 1 SW846: 6010C MMSD 02/07/14 DM0207/14001532 32 mg/kg D.W. 0.14 1 .. SW846: 6010C MMSD 02/10/14 DM0210/14001576 34 mg/kg D.W: 0.14 1 SW846: 6010C MMSD 02/11/14 DM0211/14001811 35 mg/kg D.W. 0.14 1. SW846: 6010C MMSD 02/12/14 DM0212/14001837 32 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/13/14 DM0213/14001856 31 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/14/14 DM0214/14001871 32 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/15/14 DM0215/14001882 31 mg/kg D.W. 0.14 1 SW846: 6010C MMSD . - 02/16/14 DM0216/14001893 SYS/rptiMi/oMonthly 1110113 tj 29 mg/kg D.W. 0.14 1 SW846: 6010C MMSD Page 54 of 106 Printed:11811510.48 MSD PAWP3 flit A C IAS WORK Annual Milorganite Report January 1 to December 31, 2014 NICKEL ICP METHOD • e� .�An�lyucaiMkh6d' Lab 02/17/14 DM0217/14001914 31 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/18/14 DM0218/14002002 32 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/19/14 DM0219/14002028 33 mg/kg D.W., 0.14 1 SW846: 6010C MMSD 02/20/14 DM0220/14002101 35 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/2i/14 DM0221/14002181 36 mg/kg D.W. 0.14 ] SW846: 6010C MMSD 02/22/14 DM0222/14002192 38 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/23/14 DM0223/14002211 . 37 mg/kg D.W. 0.14 1 SW846:.6010C MMSD 02/24/14 DM0224/14002224 36 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 02/25/14 DM0225/14002251 .34 mg%kg D.W. 0.14 i' " SW846: 6010C MMSD 02/26/14 DM0226/14002310 32 mg/kg D.W. 0.14 1 SW846: 60.10C _ MMSD 02/27/14 DM0227/14002329 33 mg/kg D.W.; 0.14 1 SW846: 6010C MMSD 02/28/14 DM0228/14002350 31 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/61/14 DM0301/14002921 '34 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/02/14 DM0362/14002940 37 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/03/14 DM0303/14002953 38 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/04/14 DM0304/14002986 31 mg/kg D:W. 0.14 1 SW846: 6010C MMSD 03/05/14 DM0305/14003012 30 mg/kg DA 0.14 i SW846: 6010C MMSD 03/66/14 DM0306/14003182 30 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/07/14 DM0307/14003197 34 mg/kg D.W.. 0.14 1 SW846: 6010C MMSD 03/08/14 DM0308/14003208 40 mg/kg D.W. 0.14 1 ... SW846: 6010C MMSD 03/09/i4 DM0309/14003232 31 mg/kg D.W. 0.14 i SW846: 6010C MMSD 03/10/14 DM0310/14003245 44 mg/kg D.W. 0.14 1 D2, Q2. SW846: 6010C MMSD 03/11/14 DM0311/14003272 37 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/'12/14 _ DM0312/14003300 35 mg/kg D.W. 0.14 1 SW846: 6010C MMSD .. 03/13/14 DM0313/14003871 35 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/14/14 DM0314/14003886 37 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/15/14 DM0315/14003899 33 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/16/14 DM0316/14003918 33 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/17/14 DM0317/14003936 32 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/18/14 DM0318/14003963 32 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/19/14 DM0319/14004217 34 mg/kg D:W. 0.14 1, SW846: 6010C MMSD 03/20/14 DM0320/14004315 31 mg%kg D.W. 0.14 1 SW846: 6010C MMSD 03/21/14' DM0321/14004330 33 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/22/14 DM6322/14004341 34 mg/kg D.W.. 0.14 1 SW846: 6010C MMSD 03/23/14 DM0323/14004360 32 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/24/14 DM0324/14004461 23 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/25/14 DM0325/14004638 23 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/26/14 DM0326/14004664 23 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/27/14 DM0327/14004683 24 mg/kg D.W. 0.14 1 " SW846: 6010C MMSD 03/28/14 . DM0328/i4004698 25 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/29/14 DM6329/14004889 25 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/30/14 DM0330114004908 28 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 03/31/14 DM0331/14004921 45 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/01/14 DM0401/14004948 26 mg/kg D.W. 0.14 ] SW846: 6010C MMSD 04/02/14 bM0402/14004974 27 mg/kg D.W. 6.14 1 SW846: 6010C MMSD 04/03/14 DM0403/14004993 33 mg/kg D:W. 0.14 1 SW846: 6010C MMSD 04/04/14 DM0404114005195 31 mg/kg D.W. 0.14 1 SW846: 6010C MMSD SYSIrptimlloMonthly 1170/13 tJ Page 55 of 106 Printed: 11811510:48 j . G. S D, P.18190IRA CO" INNINT . NICKEL ICP METHOD Date r 04/05/14 DM0405/14005206 34 mg/kg D.W. rr 0.14 ro r 1 Annual Milorganite' Report January 1 to December 31, 2014m .d Wb 'SW846: 6010C MMSD 04/06/14 DM0406/14005226 34'mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/07/14 DM0407114005240 32 mg/kg D.W: I1.14 1 SW846: 6010C MMSD 04/08/14 DM0408/14005267 30 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/09/14 DM0409/14005397 '29 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/10/14 DM0410/14005416 35 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/11/14 DM0411/14005434 59 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/12/14 DM0412/14005605 87 mg/kg D.W. 0.14 1 . SW846: 6010C MMSD 04/13/14 DM0413l14005627 87 mg/kg D.W. 0.14 1' SW846: 6010C MMSD 04/14/14 DM0414/14005641 82 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/15/14 DM0415/14005668 73 mg/kg D.W, : 0.14 1 SW846: 6010C MMSD 04/16/14 DM0416/14005791 60 mg/kg D.W. 0.14 .1:: SW846: 6010C MMSD 04/17/14 DM041,M4005815 54 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 04/18/14 DM0418/14006027 52 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/19/14 DM0419/14006038 48 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 04/20/14 DM0420/1'4006057 70 mg/kg D.W. 0.3 1.: SW846: 6010C MMSD 04/21/14 DM0421/14006127 49 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 04/22/14 �? DM0422/14006154 49 mg/kg D.W: 0.14 1 SW846:, 6010C MMSD 04/23/14 DM0423/14006180 47 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/24/14 DM0424/14006339 .44 mg/kg D.W. 0.14 1:: SW846: 6010C MMSD 04/25/14 DM0425/14006354 45 mg/kg D.W. 0.14 1 SW846: 6010C . MMSD 04/26/14 QM0426/14006365. 48 mg/kg D.W;, 0.14 1 SW846: 6010C MMSD 04/27/14 DM0427/14006384 46 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/28/14 DM0428/14006397 47 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/29/14' DM0429/14006454 46 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 04/30/14 DM0.430/14006482 43 mg/kg D.W, 0.14 1 SW846: 6010C MMSD 05/01/14 DM0501/1.4006976 44 mg/kg D.W. 0.14 1 SW846: 6010C MMSD OS/02/14 DM0502/14006991 40 mg/kg D.W. 0.14 .1 SW846: 6010C MMSD 05/03/14 DM0503/14007150 37 mg/kg D.W. 0.14 1 SW846:, 6010C MMSD 05/04/14 DM0504/14007169 34 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 05/05/14 DMO505114007182 35 mg/kg D.W. 0.14 1: ... SW846: 6010C MMSD 05/06/]4 DM05b6/14007209 38 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 05/07/14 DM0507/14007235 37 mg/kg D.W. 0.14 1 SW846: 6016C MMSD 05/08/14 DMQ508/14007254 34 mg/kg D.W. 0.14 1 SW846: 6010C MMSD 05/09/14 DMO509/14007269 .36 mg/kg D.W. 0.2 2 . SW846: 6010C MMSD 05/10/14 DM0510/14007280 36 mg/kg D.W. 0.3 1 .. SW846: 6010C MMSD 05/11/14 DM0511l14007456, 33 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 05/12/14 DM0512/14007469 32 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 05/13/14 .. DM0513/14007551 36 mg/kg D.W. 0.2 2 SW846: 6010C MMSD .. 05/14/14 DMO514/14007577 36 mg/kg D.W. 0.2 2' SW846: 6010C MMSD ' 05/15/14 DM0515/14007665 34 mg/kg D.W: 0.2 2 SW846: 6010C MMSD 05/16/14 DM0516/14007680 45 mg/kg D.W. 0.2 2.. SW846: 6010C MMSD OS/11/14 DM0517/1400760.1 31 mg/kg D.W. 0.2 2 SW846: 6010C MMSD OS/18/14 DM0518/1400Mb 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 05/19/14 DM0519/14007764' 32 mg/kg D.W. 0.2 2 A0. SW846: 6010C MMSD 05/20/14 DM0520/1400799.7 38 mg/kg D.W. 0.2 2 : SW846: 6010C MMSD 05/21/14 DMO521/14008023 36 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 5Y5/rpt1N110M0nth1Y 1110113 tj Page 56 of 106 Printed: 1/8/1510:46 p , MSD polos fig a Carat [f3/1oor NICKEL ICP METHOD Sampte Date Samplell) Result LODi Annual Milorganite Report January 1 to December 31, 2014 05/22/14 DMO522/14008042 33 mg/kg DM. 0.3 1. SW846: 6010C MMSD 05/23/14 DMO523/14008067 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 05/24/14 DMO524/14008291 33 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 05/25/14 DMO525/14008310 37 mg/kg D.W. 0.2 2 SW846: 6610C MMSD 05/M/14 DM0526114008323 39 mg/kg D.W. 0.2 2' 'SW846: 6010C MMSD 05/27/14 DM0527/14008646 39 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 05/28/14 DM0528/14008672. 37 mg/kg D.W: 0.2 2 SW846:.6010C MMSD 05/29/14 DM0529114008691 36 mg/kg D.W. 0.2 2 SW846: 6010C MMSD OS/30/14 DM0530/14608845 38 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 05/31/14 DM0531/14008856 37 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/01/14 DMO601/14009580 43 mg/kg D.W. 0.3 1 . SW846::6010C MMSD 06/02/14 DM0602/14009593 37 mg/kg D.W. 0.3 1 -SW846: 6010C MMSD 06/03/14 DM0603/14009620 36 mg/kg DM. 0.3 1 SW846: 6010C MMSD 06/04/14 DM0604/14009635 36 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 06/05/14 DM0605/14009654 37 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 06/06/14 DM6606/14009669 35 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 06/07/14 DM0607/14009844 38 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 06/08/14 DM0608/14009867 36 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 06/09/14 DM0609114009880 34 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 06/10/14 DM0610/14009907 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 06/11/14 DM0611/14010237 35 mg/kg D.W. 0.3 i SW846: 6010C MMSD 06/12/14 DM0612/14010256 33 mg/kg D.W. 0.3 1 SW846: 6010C = MMSD 06/13/14 DM0.613/14010271 34 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/14/14 DM0614/14010282 •34 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/15/14 DM0615/14010301 33 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/16/14 DM0616/14010319 34 mg/kg D.W: "'0.3 1 SW846: 6010C MMSD 06/17/14 DM0617/14010346 37 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/18/14 DM0618/14010687 34 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/19/14 DM0619/14010706 36 mg/kg D.W. 0.3 i SW846: 6010C MMSD 06/20/14 DM0620/14010721 33 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/21/14 DMO621/14010732 36 mg/kg D.W. 0.3 1. SW846: 6010C MMSD 06/22/14 DM0622/1401076.1 34 mg%kg DA 0.3 1 SW846: 6010C MMSD 06/23/14 DM0623/14011513 33 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/24/14 DM0624/14011540 34 mg/kg D.W.. 0.3 1 SW846: 6010C MMSD 06/25/14 DM0625/14011566 42 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/Z6/14 DM0626/14011766 37 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/27/14 DM0627/14011781 . 36 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/28/14 DM0628/14011792 34 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/29/14 DM0629/14011811 34 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 06/30/14 DM0630/14011824 36 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 07/01/14 DM0701/14011851 35 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 07/02/14 DM0702/14011879 38 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 07/03/14 DM0703%14011898 32 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 07/04/14 DM0704/14011911 33 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 07/05/14 DM0705/14011924 33 mg/kg D.W: 0.3 1 SW846: 6010C MMSD 07/06/14 DM0706114011943 36 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 07/07/14 DM0707/14012196 33 mg/kg D.W. 0.3 1 SW846: 6010C MMSD SYS/rptlMMoMonthiy 1/10/13 tj Page 57 of 106 Printed. • 1/8/1510:48 hMSD: PiRENEE�i f Gf A. flir.S1R l�ili+:RHEH1 NICKEL ICP METHOD Sample Da3 w/m/14 DM0708/14012898 33 mg/kg D.W. 0.3 1 Annual Milorganite Report January 1 to December 31, 2014 " . Lab SW846: 6010C MMSD 07/09/14 DM0709/14012926 32 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 07/10/14 DM0710/14012945 33 mg/kg D.W.; 0.3 1 SW846: 6010C MMSD 07/11/14 DM0711/14012961 37 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 07/12/14 DM0712/1401297.1 39 mg)kg D.W. 0.2 2 SW846: 6010C MMSD 07/13/14 DM0713/14012991 41 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 07/14/14 DM0714/14013004 41 mg/kg D.W. 0.2 2 SW846: 6010C MMSD .07/15/14 DM0715/14013031 39 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 07/16/14 DM0716/14013059 40 1r 9g kg DX 0.2 2 SW846: 6010C MMSD 07/17/14 DM0717/14013078 40 mg)kg D.W. 0.2 2 SW846: 6010C MMSD 07/18/14 DM0718/14013295 39 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 07/19/14 DM0719/14013305 38 mg/kg D.W. 0.2 2, SW846: 6010C MMSD 07/20/14 DM0720/14013324 37 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 07/21/14 DM0721/14013337 39 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 07/25/14 DM0725/14013997 34 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 07/26/14 DM0726/14014008 34 mg/kg D.W. 0.2 2 : SW846: 6010C MMSD 07/27/14 DM0727/14014027 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 07/28/14 DM6728/14014040 32 mg/kg D.W: 0.2' 2 SW846: 6010C MMSD 07/29/14 DM0729/14.014,895 35 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 07/30/14 DM0730/14014923 36 rrig/kg DX 0.2 2- SW846: 6010C MMSD 07/31/14 DM0731/14014942 34 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/01/14 DM0801/14014957 33 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/02/14 DM0802114014968 32 mg/kg D.W. 0.3 1, SW846: 6010C MMSD 08/03/14 DM0803/14014987 32 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 08/04/14 DM0804/14015000 32 mg/kg D.W. 0.3 1 SW846: 60100 MMSD 08/05/14 DM0805/14015027 34 mg/kg D.W. 0.2 2 SW846:'6010C MMSD 08/06/14 DM0806/14015405 31 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/07/14 DM0807/14015456 31 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/08/14 DMO808/14015471 32 mg/kg D.W. ..0.2 2 SW846: 6010C MMSD 08/09/14 DM0809114015482 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/10/14 DM0810/14015966 40 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/11/14 DM0811/14015984 31 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/12/14 DM0812/14016011 30 mg/kg D.W. 0.2 2 SW846r-6010C MMSD 08/13/14 DM0813/14016039 33 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/14/14 DM0814/14016058 30 mg/kg D.W. 0.2 2 "SW846: 6010C MMSD 08/15/14 QM0815/14016181 30 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/16/14 DM0816/14016192 30 mg/kg D.W. 0.2 2 SW846:6010C MMSD 08/17/14 DM0817/140.16211 28 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/18/14 DM0818/14016290 31 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/20/14 DM0820/14016347 32 mg/kg D.W. 0:2 2 SW846: 6010C MMSD 08/21/14 DM0821/14016366 32 mg/kg D.W. 0.2 2 _ SW846: 6010C MMSD 08/22/14 DMO822/14016381 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/23/14 DMO823/14016392 37 mg/kg D.W, 0.2 2 SW846: 6010C MMSD 08/24/14 DM0824/14016411 40 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/25/14 DM0825/14016488 40 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/26/14 DMO826/14016515 37 mg/kg D.W. 0.2 2 SW846: 6010C MMSD SYS/rpti iioMonthiy 1/10/13 tJ Page 58 of 106 Printed: 1/8/1510.48 � 0 i e l kMSD PdhlMCK3 (5k A Ct165�! L1iJ14:NHlN! NICKEL ICP METHOD e. r 08/28/14 DM0828/14016907 30 mg/kg D.W. 06 0.2 10Q e• 2 Annual Milorganite Report January 1 to December 31, 2014 iLab SW846: 6010C MMSD 08/29/14 DMO829/14017671 28 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/30/14 DM0830/14017682 30 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 08/31/14 DM0831/14017701 36 mg/kg D.W. 0.2 2 SW846: 6010C MMSD . 09/01/14 DMO901/14017714 37 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09102/14 DMO902/14017871 39 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/03/14 DM0903/14017886 32 mg/kg D.W.' ' 0.2 2 SW846:.6010C MMSD 09/04/14 DM0904/14017920 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/05/14 DMO905/14017901 29 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/16/14 DM0916/14019167 34 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/17/14 DM0917/14019195 32 mg/kg D.W. 0.2 2 SW846:.6010C MMSD 09/18/14 DMO918/14019229 31 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/19/14 DMO919/14019244 36 mg/kg D^ 0.2 2 SW846: 6010C MMSD 09/20/14 DMO920/14019255 39 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/21/14 DMO921/14019274 41 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/22/14 DMO922/14019287 40 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/23/14 DMO923/14019778 36 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/24/14 DMO924/14019806 33 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/25/14 DMO925/14019825 33 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/26/14 DMO926/14019840 35 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/27/14 DM0927/14019851 43 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/28/14 DM0928/14019870 . 42 mg/kg D.W.. 0.2 2 SW846: 6010C MMSD 09/29/14 DMO929/14019883 45 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 09/30/14 DM0930/14019909 39 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/01/14 DM1001/14019927 38 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/02/14 DM1002/14020572 41 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/03/14 DM1003/14020587 64 mg/kg D.W. 0.2 2 Q3. SW846: 6010C MMSD 10/04/14 DM1004/14020598 38 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 10/05/14 DM1005/14020617 35 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 10/06/14 DM1006/14020630 37 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 10/07/14 DM1007/14021108 36 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 10/08/14 DM1008/14021160 38 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 10/09/14 DM1009/14021179, 39 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 10/10/14 DM1010/14021194 39 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 10/11%14 DM1011/14021244 39 mg%kg D.W. 0.2 2 SW846: 6010C MMSD 10/12/14 DM1012/14021263 37 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/13/14 DM1013/14021276. 37 mg/kg D.W., 0.2 2 SW846:.6010C MMSD 10/14/14 DM1014/14021304 37 mg/kg D.W. 0.2 2 SW846: 6010C MMSD . 10/15/14 DM1015/14021332 38'mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/i6/14 DM1016/14021351 43 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/17/14 DM1017/14021787. 37 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/18/14 DM1018/14021798 38,mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/19/14 DM1019/14021817 39 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/20/14 DM1020/14021830 38 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/21/14 DM1021/14021857 38 mg/kg D.W: 0.2 2 SW846: 6010C MMSD 10/22/14 DM1022/14021885 38 mg/kg D.W. 0.2 2, SW846: 6010C MMSD 10/23/14 DM1023/14022256 39 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 5Y5/rptlM11bMonth/y 1110113 tj Page 59 of 106 Printed.• 11811510.48 j Annual. Milorganite Report MS January 1 W December 31, 2014 ra�a�ras r� a'ctt�;1� E�n��u�xr . NICKEL ICP METHOD sam- piee. - , e o o e e eA Fla , i 10/24/14 DM1024114022273 36 mg%kg D.W. 0.2 2'' SW846: 6010C MMSD 10/25/14 DM1025/14022286 36 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/26/14 " DM1026/14022305 38 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/27/14 DM1027/14022318 36 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/28/14 DM1028/14022409 34 mg"/kg D.W. 0.2 2 : SW846: 6010C MMSD .. 10/29/14 DM1029/14022439 35 mg/kg D.W. 0.2. 2 SW846:6010C MMSD 10/30/14 DM1030/14022510 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 10/31/14 DM1031/14022525 38 mg/kg D.W. 0.2 2 SW846: 6010C MMSD, 11J01/14 DM1101/14022536 35 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/02/14 DM1102/14022555. 34 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/03/14 DM1103/14022568 34 mg/kg D.W. , 0.2 2 SW846: 6010C MMSD li/04/14 DM1104M402311.1 31 mg/kg D.W. 0.2 2: AO. SW846: 6010C MMSD 11/05/14 DM1105/14023139 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/06/14 DM1:106/14023158: 32 mg/kg D.W.; 0.2 2 SW846: 6010C MMSD 11/07/14 DMI-107/14023173 33 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/68/14 DM1108/14023184 34 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/09/14 DM1109/140232M 34 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/10/14 DM1;110/14023767: 33 mg/kg D.W. 0.2 2 "' SW846:.6010C MMSD 11/11/14 DM1111/14023796 33 mg/kg D.W. 0.2 2, SW846: 6010C MMSD 11/12/14 DM1112/14023876 32,mg/k9 D.W. 0.2 2 SW846: 6010C MMSD 11/13/14 DM1113/14023895 28 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/14/14 DM1:114/14023910 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/15/14 DM1115/14.023929 27 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11%16/14 DM1116/14023948 27 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/17/14 DM1117M4023061 29 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/18/14 DM1118/14024236 29 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/19/14 DM1119/14024264 31 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/20/14 DM1120/14024283 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/21/14 DM1.121/14024302 32 mg/kg D.W. . 'O.2 2 SW846: 6010C MMSD 11/22/14 DM1122/14024313 34 mg/kg D.W. 0.2 2 SW846: 6016C MMSD 11/23/14 DM1123/14024393 33 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11%24/14 DM1124/14024414 34 mg/kg D.W. 0.2 2 SW846: 6010C MMSD,. 11/25/14 DM1125/14024441 .. 30 mg/kg D.W: . 0.2 2 SW846: 6010C MMSD 11/26/14 DM1126/14024469 25 mg/kg D.W. 0.2 2 SW846: 60i6C MMSD 11/27/14 DM1127/14024529 33 mg/kg D.W. 0.2 2' SW846: 6010C MMSD 11/28/14 DM1128/14024544 .. 33 mg/kg D.W. . 0.2 2 SW846: 6010C. MMSD 11/29/14 DM1'129/14024555: 36 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 11/30/14 DM1130/14024574 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/Ol/14 DM1201/1402460:1 34 mg/kg D:W. 0.2 2' SW846: 6010C MMSD 12/02/14 ' DM1202/14025299 30 mg/kg D.W.. 0.2 2 SW846: 6010C MMSD i2/03/14 DM1203/14025327' 33 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/04/14 DM1204/14025346 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/OS/14 DM1205/1.402536.1 31 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/06/14 DM1206/14025372 37 mg/kg D.W. :.:0.2 2 SW846:, 6010C MMSD 12/07/14 DM1207/14025391 39 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/98/14 DM1208/14025404 35 mg/kg D.W. 0.2 2'. SW846: 6010C MMSD 12/09/14. DM1209/14026170 36 mg/kg D.W. 0.2 2 SW846: 6010C MMSD SYS/rpttmil,wonthiy 1/10/13 tj Page 60 of 106 Printed.-11811510,48 I MS0 �,�g34iP3 f 0� A Ctf�ti'k �x7tE$il�[�1 NICKEL ICP METHOD Sample D. 12/10/14 DM1210/14026198 36 mg/kg D.W. 0.2 oQ 2 Annual Milorganite Report January 1 to December 31, 2014 o•ytica SW846: 6010C MMSD 12/11/14 DM1211/14026217 34 mg/kg D.W. 0.2 2 SW846: 6010C MMSD '. 12/12/14 DM1212/14026232 35 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/13/14 DM1213/14026243 33 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/14/14 DM121'4/14026262 33 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/15/14 DM1215/14026277 33 ing/kg D.W. 0.2 2 , . SW846: 6010C MMSD ' 12/16/14 DM1216/14026475 29 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/17/14 DM1217/14026503 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/18/14 DM1218/14026522 31 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/19/14 DM121'9/14026537 34 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/20/14 DM1220/14026653 32 mg/kg D.W: 0.2 2 SW846: 6610C MMSD 12/21/14 DM1221/14026672 31 mg/kg D.W. 0.2 2 SW846: 6016C MMSD 12/22/14 DM1222114026685 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/23/14 DM1223114026713 32 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/24/14 DM1224/14026741 34 mg/kg D.W. 0:2 2 SW846:'6010C MMSD 12/25/14 DM1225/14026760 35 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/M/14 DM1226/14026777 35 mg/kg D.W. 0.2 2 SW846: 6010C MMSD 12/27/14 DM1227/14026788 35 mg/kg D.W. 0.3 1 SW846: 6010C MMSD 12/28/14 DM9228/14026807 34 mg/kg D.W. 0.3 1 SW846: 6010c MMSD 12/29/14 DM1229/14027031 34 mg/kg D.W. 0.3 1' SW846: 6010C MMSD 12/30/14 DM1230/14027058 33 mg/kg D.W. 0.3 1 SW846: 6010C MMSD . 12/31/14 DM1231/14027086. 32 mg/kg D.W.. 0.2 2 SW846: 6010C MMSD Avg: 37 mg/kg D.W. NITRATE NITROGEN Sample Date Sample ID 01/11/14 WMC2/14000475 Result 1.1 % Max: Lob LOQ 0.5 1.7 120 mg/kg D.W: QA,Flags Analytical Method AOAC (16) 930.0 " Lab MMSD 02/08/14 WMC6/14001578 0.6 % 0.5 1.7 AOAC (16) 930.0 MMSD 03/68/14 WMC10/14003247 0.85 % 0.5 1.7 AOAC (16) 930.0 MMSD 04/12/14 WMC15/14005643 ; 0.72 % "0.5 1.7 AOAC (16) 930.0- MMSD 05/10/14 WMC19/14007579 0.76 % 0.5 1.7 AOAC (16) 930.0 MMSD 06/07/14 WMC23/14009882 0.95 % 0.5 1.7 AOAC.(16) 930.0 'MMSD 07/12/14 WMC28/14013005 0.62 % 0.5 1.7 AOAC (16) 930.0 MMSD 08/09/14 WMC32/14015986 0.66 % 0.5 1.7 AOAC (16) 930.0 MMSD 09/27/14 WMC39/14020976 2.7 % '0.5 1.7 AOAC (16) 930.0 MMSD 10/11/14 WMC41/14021270 0.7 % 0.5 1J AOAC (16) 930.0 .MMSD 11/08/14 WMC45/14023769 1.3 % 0.5 1.7 AOAC (16) 930.0 MMSD 12/13/14 WMC50/14026279 1.2 % 0.5 1.7 AOAC (16) 930.0 MMSD Avg: 1 % Max: 2.7 % Page 61 of 106 5Y5/rpt1M1/oMonth1y 1110113 0 Printed- 118115IONS - :N L) l . : : aa�ioi� rot n �rtr�; i�rt�neu[�r NITROGEN-Total(Manual) Sample Date Sample Ib Result LOD . - w LoQ QA �Flags Annual Milorganite Report ..January 1 W December 31, 2014 Analytipal Method, Lab 01/11/14 WMC2/14000475. 6.1 % 0.11 0.37 ,' AOAC (16) 955.4 MMSD 02/08/14 WMC6/14001578 6.4 % 0.11 0:37 AOAC (16) 955.4 MMSD 03/08/14 WM610/14003247 6.2 % 0.11 0.37 AOAC (16) 955.4 MMSD 04/12/14 WMC15/14005643 6.2 % 0.11 0.37 AOAC (16) 955.4 MMSD 05/10/14 WMC19/14007579 5.9' % 0.11 0.37' AOAC (16) 955.4 MMSD -' 06/07/14 WMC23/14009882 5.8 % 0.11 0.37 AOAC (16) 955A MMSD 07/12/14 WMC28/14013005 S.2 0/a 0.11 0.37 AOAC (16) 955.4 MMSD OS/09/14 WMC32/14015986 5.7 % 0.11 0.37:- AOAC (16) 955.4 MMSD 09/27/14 WMC39/14020976 5.7 % 0.11 0.37 AOAC (16) 955.4 MMSD " 10/11/14 WMC41/14021279 . 5.5 %, .0.11 0.37 AOAC (16) 955A MMSD 11/08/14 WMC45/14023769 5.6 % 0.11 0.37 " AOAC (16) 955.4 MMSD 12/13/14 WMC50/14026279 6.1 % 0.11 0.37 :AOAC (16) 955.4 MMSD Avg: 5.9 % NITROGEN-1Mate r'Insoluble Sampie-bate.. Max: LOO 6.14 % 01/11/14 WMC2/14000475. 4.2 % 0.5 1.7. AOAC 2.061 (13) 'MMSD 02/08/14 WMC6/14001578 5 % 0.5 1.7 AOAC 2.061 (13) MMSD 03/08/14 WMC10/14003247 4.8 % 0.5. 1.7 AOAC 2.061 (13) MMSD 04/12/14 WMC15/14005643 4.4 % 0.5 1.7: AOAC 2.061 (13) MMSD 05/10/14 WMC19/14007579 4.4 % O.S. 1.7 AOAC 2.061 (13) MMSD 06/07/14 WMC23/14009882 . 4.3 % 0.5 1.7 AOAC 2.061 (13) MMSD 07/12/14 WMC28114013005 4.1 % 0.5 1.7 AOAC 2.061 (13) MMSD 08/09/14 WMC32/14015986 4.6 % 0.5 1.7 AOAC 2.061 (13) MMSD 09/27/14 WMC39/14020976 2.5 % 0.5 1.7 AOAC 2.061 (13) MMSD 10/11/14 WMC41/14021279 ' 4.2 % 0.5 1.7 AOAC 2.061 (13) MMSD 11/08/14 WMC45/14023769 4 % 0.5 1.7.. AOAC 2.061 (13) MMSD 12%13/14 WMC50/14026279 4.2 % 0.5 1.7 AOAC 2.061 (13) MMSD Avg: 4.26/o s. SYS/rptlM110Month/y 1/10/13 tj Max: 5 % Page 62 of 106 Printed: 11811510.48 n 1 �.MS01 PAIim 161 A Chit f17It, HH[w pW.Solids o. 01/04/14 WMC1/14000131 5:96 Stnd. Units eo 0.1 LOQ 0.33 Annual Milorganite Report January 1 to December 31, 2014 .Lalf SW846: 9045D MMSD 01/11/14 WMC2/14000475 6.14 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 01/18/14 WMC3/14000605 6.26 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 01/25/14 WMC4/14001097 6.28 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 02/01/14 WMC5/14001445 6.21 Stnd: Units 0.1 0.33 SW846: 9045D MMSD 02/08/14 WMC6/14001578 6.22 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 02/15/14 WMC7/14001916 6.21 Stnd. Units 0.1 0.33 SW846:.9045D MMSD 02/22/14 WMC8/14002226 6.13 Stnd, Units 0.1 0.33. SW846: 9045D MMSD 03/O1/14 WMC9/14002955 6.13 Stand. Units 0.1 0.33 SW846: 9045D MMSD 03/08/14 WMC10/14003247 6.13 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 03/15/14 WMC11/14003938 6.24 Stnd. Units 0.1 0.33 SW846: 904SD MMSD ' 03/22/14 WMC12/14004463 6.17 Stnd, Units 0.1 0.33- SW846: 9045D MMSD 03/29/14 WMC13/14004923 5.81 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 04/05/14 WMC14/14005242 6.07 Stnd. Units 0.1 0.33 SW846: 904SD MMSD 04/12/14 WMC15/14005643 6.11 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 04/19/14 WMC16114006129 &04 Stnd, Units 0.1 .0.33. SW846: 9045D MMSD 04/26/14 WMC17114006429 6.07 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 05/03/14 WMC18/14007184 6.21 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 05/10/14 WMC19/14007579 6.28 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 05/17/14 WMC20/14007770 6.1 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 05/24/14. WMC21/14008326 6.23 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 05/31/14 WMC22/14009595 6.36 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 06/07/14 WMC23/14009882 6.38 Stnd. Units -� 0.1 0.33 SW846: 9045D MMSD . 06/14/14 WMC24/14010321 6,41 Stnd. Units 0.1 0.33 SW846: 9045D 'MMSD _ 06/21/14 WMC26/14011516 6.33 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 06/28/14 WMC26/14011826 6.36 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 07/05/14 WMC27/14012198 6.3 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 07/12/14 WMC28/14013005 6.36 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 07/19/14' ' WMC29/14013339 6.43 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 07/26/14 WMC30/14014042 6.37 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 08/02/14 WMC31/14015002 6:14 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 08/09/14 WMC32/14015986 6.01 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 08/16/14 WMC33/14016294 6.03 Stnd. Units 0.1 0.33 SW846: 9645D MMSD 08/23/14 WM634/14016490 5.85 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 08/30/14 WMC35/14017716 6 Stnd. Units 0.1 0.33 SW846: 9045D ..MMSD 09/05/14 WMC36/14018081 6.09 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 09/20/14 WMC 38/14020851. 6.18 Stnd. Units 0.1 0.33 SW846::9045D MMSD 09/27/14 WM639/14020976 6.18 Stnd. Units 0.1 0.33 SW846: %45D MMSD 10/04/14 WMC40114021278 6.41 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 10/11/14 WMC41/14021279 6.31 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 10/18/14 WMC42/14021832 6.31 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 10/25/14 WMC43/14022322 6.25 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 11/01/14 WMC44/14022570 6.31 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 11/08/14 WMC45/14023169 6.17 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 11/15/14 WMC46/14023963 6.14 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 11/22/14 WMC47/14024416 6.18 Stnd. Units 0.1 0.33 SW846: 9045D MMSD 11/29/14 WMC48/14025406 6,26 Stnd. Units 0.1 0.33 SW846: 9045D MMSD op SYS/rptimilwonthiy 1/10/13 fJ Page 63 of 106 Printed:1/8/1510:48 i • 1 re"iMSD P,1R1W W A CAI R tx UNNtK PHOSPHORUS ICP METHOD Annual Milorganite Report January 1 to December 31, 2014 Sample Date 01/01/14 sampie io DMO101/14000012 Aesum 27000 mg/kg DN. L-WL---LlV 2.6 10 AO. SW846: 6010C MMSD 01/02/14 DMO102114000039 25000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 01/03/14 DMO103/14000088 26000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 01/04/14 DM0,104/14000103 25000 mg/kg D.W. 2.6 10 A0: SW846: 6010C MMSD 01/05/14 DMO105/14000122 25000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 01/b6/14 DMO106/14000135 25000 mg/kg D.W. 2.6 lb AO. SW846: 6010C MMSD 01/07/14 bmb107/14000162 24000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 01/08/14 DM0108/14000188 25000_ mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 01/09/14 DMO109/14000207 24000 mg/kg MW. 2.6 10 . AO. SW846: 6010C MMSD 01/10/14 DM0l lbm4000430 23000 mg/kg D.W. 2.6 10 AO. SW846: 601PC MMSD 01/11/14 DM0111/14000441 ' 24000 mg/kg D.W: 2.6 10 AO, SW846:'6010C MMSD 01/12/14 DM0112/14000460 24000 mg/kg D.W. 2.6 10. AO. SW846: 6010C MMSD 01/13/14 DM0113114000473 24000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 01/14/14 DM0114/14000500 24000 mg/kg D.W. 2.6 10 A0. .. SW846: 6010C MMSD 01/15/14 DM0115/14000526 23000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 01/16/14 DMO116/14000545 22000mg/kg DN. 2.6 10: AO. SW846: 6010C MMSD 01/17/14 DM0117114000560 22000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 01/18/14 DM0.118/14000571 25000 mg/kg D.W. 12.6 10 AO. SW846: 6010C MMSD 01/19/14 DM0119/14000590 25000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 01/20/14 DMO120/14000603 26000 ing/kg D.W. 2.6 10- AO. SW846: 6010C MMSD 01/21/14, DMO121/14000630 24000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 01/22/14 DMO122/14000656 24000 mg/kg D.W. 2.6 10 AO, Q2:, SW846: 6010C MMSD 01/23/14 DMO123/14000675 24000 mg/kg D.W. 2.6 10 AO: SW846: 6010C MMSD 01/24/14 DMO124/14000690 24000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 01/25/14 DM0.125/14000923 25000 nig/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 01/26/14 DMO126/14000942 24000 mg/kg D.W. 2.6 10 A0. SW846:6010C MMSD 01/27/14 DMO127/14001095 24000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 01/28/14 DMO128/14001122 24000 mg/kg D:W. 2.6 10 AO. SW846: 6010C MMSD 01/29/14 DMO129/14001148 25000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 01/30/14 DM0130/14001167 24000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 01/31/14 DM0131/14001182 24000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 02/01/14 DM0201114001193 24000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 02/02/14 DM0202/14001430 25000 mg/kg D.W. 2.6 10 A0: SW846: 6010C MMSD 02/03/14 DM0203/14001443 25000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 02/64/14 DM0204/14001470 23000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 02/05/14 DM0205/14001498 25000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 02/06/14 DM0206/14001517, 24000 mg/kg D.W. 2.6 .. 10 AO. .. SW846: 6010C MMSD 02/07/14 DMO207/14001532 23000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 02/08/14 DM0208/14001543 23060 mg/kg D.W. 2.6 16 AO. SW846: 6010C MMSD 02/09/14 DM0209/14001562 23000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 02/10/14 DM0210/14001576 23000 mg/kg D.W. .. 2.6 10 A0. SW846:'6016C MMSD 02/11/14 DMO211/14001811 24000 mg/kg D.W. 2.6 10 AO. SW846: 6016C MMSD 02/12/14 DM0212/14001837 24000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 02/13/14 DM0213/14001856 23000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 02/14/14 DM0214/14001871 23000 mg/kg D.W. 2.6 10 A0: SW846: 6010C MMSD 02/15/14 DM0215/14001882 23000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 02/16/14 DM0216114001893 SYSIrptlM110Monthly 11101-13 U 23000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD Page 65 of 106 Printed., 1/8/1510:48 d _.. MSR PA.Ih[fi Iota Clkke ignu ull PHOSPHORUS:ICP METHOD 02/11/14 DM0217/i4001914 23000 mg/kg D.W. o 0 2.6 0 10 o • AO. Annual Milorganite Report :January 1 to December 31, 2014 . , SW846: 6010C MMSD 02/18/14 DM0218/14002002 23000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 02/19/14 DM0219/14002028 23000 mg/kg D.W. 2.6 10 AO. "' SW846:.6010C MMSD 02/20/14 DMO220/14002101 23000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 02/21/14 DM0221/14002181 23000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 02/22/14 DM0222114002192 22000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 02/23/14 DMG223/14002211 ' 23000 mg/kg D.W. 2.6 10 AO. SW846:'6010C MMSD 02/24/14 DM0224/14002224 21000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 02/25/14 DM0225/14002251 21000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 02/26/14 DM0226/14002310 22000 mg/kg D.W. -2.6 10 AD. SW846: 6010C: MMSD 02/27/14 DM0227/14002329 23000 mg/kg D.W. 2.6 10 AO.: SW846: 6010C MMSD 02/28/14 DM0228114002350 23000:rcig/kg D.W. 2.6 10. SW846: 6010C MMSD, 03/OS/14 DM030.1/14002921 24000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 03/02/14 DM0302/14002940 24000 mg/kg-D.W.:' 2.6 10 AD. SW846: 6010C: MMSD 03/03/14 DM0303/14002953 27000 mg/kg D.W. 2.6 10 AD, Q3.' SW846: 6010C, MMSD :03/04/14 DM0304/14002986 23000 mg/kg DX 2.6 10 : AD. SW846: 6010C MMSD 03/05/14 D.M0305/14003012 24000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 03/06/14 "' DM0306/14003182 24000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 03/07/14 DM0307/14003197 24000 mg/kg D.W. 2.6 10. AD. SW846: 6010C MMSD 03/08/14 DM0308/14003208 23000 mg/kg D.-W. 2.6 10 AD. 'SVV846: 6010C MMSD 03/09/14 DM0309/14003232 24000 mg/kg D.W. . 2.6 10 AD. SW846: 6010C MMSD 03/10/14 DMO310/14003245 24000 mg/kg D.W. 2.6 10 AO. SW846:'6010C MMSD 03/11/14 _ DM0311/14003272 24000 mg/kg D.W. 2.6 10,: AO. SW846: 6010C MMSD 03/12/14 DM0312114003300 25000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 03/13/14 DM0318/14003871 25000 mg/kg D.W. . 2.6 10 AD. SW846: 6010C MMSD 03/14/14 DM0314/14003886 24000 mg/kg D.W: 2.6 10 AO, Q2. SW846: 6010C MMSD 03/15/14 DM0315/14003899 22000 Mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 03/16/14 DM0316/14003918 24000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 03/17/14 DM0317/14003936 23000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 03/18/14 DM0318/14003963 22000 mg/kg D.W. 2.6 10 AD. SW846: 6610C MMSD 03/.19/14 DM0319/14004217 24000 tng/kg D.W. 2.6 10.:. AO. SW846: 6010C MMSD 03/20/14 . DM0320/14004315 23000 i 4kg D.W. 2.6 .10 AD, Q2. SW846: 6010C MMSD 03/21/14 DM0321/14004330 23000 mg/kg D.W. - 2.6 10 AD. SW846:.6010C MMSD 03/22/14 DMO322114004341 23000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 03/23/14 DM0323/14004360 22000.mg/kg D:W. 2.6 10' AD. SW846: 6010C MMSD 03/24/14 DM0324114004461 19000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 03/2S/14 DM0325/14004638 20000 mg/kg D.W: 2.6 10 AD. SW846:6010C MMSD 03/26/14 DM0326/14004664 20000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 03/27/14 DM0327/14004683 19000 mg/kg D.W. 2.6 10' AD. " SW846: 6010C MMSD 03/28/14 DM0328/14004698 18000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 03/29/14 DM0329/14004889 18000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 03/30/14 DM0330/14004908 17000 mg/kg D.W. 2.6 SO AO. SW846: 6010C MMSD 03/31/14 DM0331/14004921 17000 mg/kg D.W. 2.6 10 AD. SW846: 6010C MMSD 04/01/14 DM0401/14004948 17000 mg/kg D.W. 2.6 10 AD. SW846:.6010C MMSD 04/02/14 DM0402/14004974 19000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 04/03/14 DM0403/14004993 22000 mg/kg D:W. 2.6 10; A0. SW846: 6010C MMSD 04/04/14 DM0404/14005195 21000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD SY5/rptimi/oMonth/y 1110113 0 _ Page 66 of 106 Printed: 1%811510:48 MR P,tR1NIF3 fOR�:CIIt��GR IC'tti�l3ltafHl PHOSPHORUS ICP METHOD SampleeaSampleo 04/05/14 DM0405/14005206 23000 rrig/kg D.W. o. 2.6 10 A0. � t r P Annual Milorganite Report January 1 to December 31, 2014. SW846: 6010C MMSD 04/06/14 DM0406/14005226 23000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 04/07/14 DM6407/14005240 24000 mg/kg D.W. 2.6 10 AO. SW846:,6010C MMSD 04/08/14 DMQ408/14005267 22000 mg/kg D.W. 2.6 10 AO. SW846: 6010C. MMSD 04/09/14 DM0409/14005397 22000 r 6ft DA 2.6 10 AO. .:SW846: 6010C MMSD 04/i0/14 DM0410/14005416 21000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 04/11/14 DM0411/14005434 24000 mg/kg D.W., 2.6 10 AO, Q3. SW846: 6010C MMSD 04/12/14 DM0412/14005605 22000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 04/13/14 .. DM0413114005627 22000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 04/14/14 DM0414/14005641 21000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 04/15/14 bM0415/14005668 20000 mg/kg D.W. 2.6 10 AO, SW846: 6010C MMSD 04/16/14 DM0416/14005791 18000 mg/kg D.W. 2.6 10, A0. SW846: 6010C MMSD 04%17/14 DM0417/14005815 17000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 04/18/14 DM0418/14006021 18000 mg/kg D.W. 2.6 10 A0, Q2. .. - SW846: 6010C MMSD 04/19/14 DM6419/14006038 18000 mg/kg D.W. 6.94 10 SW846: 6010C MMSD 04/20/14 DM0420/14006057 19000 mg/kg D:W. 0.94 10 SW846: 6010C MMSD 04/21/14 DM0421/14006127 19000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 04/22/14 DM0422/14006154 21000 mg/kg D.W. 2.6 10 AO. SW846: 6610C MMSD 04/23/14 DMO423/14006180 20000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 04/24/14 DM0424/14006339 190.00 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 04/25/14 DM0425/14006354 21000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 04/26/14 bM0426/14006365 22000 mg/kg D.W. :2.6 10 AO. SW846::60i0C MMSD 04/27/14 DM6427/14006384 21000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 04/28/14 DM0428/14006397 22000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 04/29/14 DM0429/14006454 21000 mg/kg D.W. ..2.6 10 AO, Q2... SW846: 6010C MMSD 04/30/14 DM6430/14006482 21000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 05/01/14 DM0501/14006976 21000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 05/02/14 DM0502/14006991 20000 mg/kg D:W. 2.6 10 AO. SW846: 6010C MMSD 05/03/14 DMO503/14007150 19000 mg/kg D.W. 2.6 10 A0. SW846: 6010C MMSD 05/04/14 DM0504/14007169 19000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 05/9S/14 DM0505/14007182 19000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 05/06/14 DM0506/14007209 21000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 05/07/14 'DM0507/14007235 20000 mg/kg D.W. 2.6 10 A0: SW846:.6010C MMSD 05/08/14 DM0508/14007254 19000 mg/kg D.W. 2.6 10 AO. SW846: 6010C MMSD 05/09/14 DM0509/14007269 20000 mg/kg D.W. 1.7 10 ' AO. SW846: 6010C MMSD 05/10/14 `' DM0510/14007280 21000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD . 05/11/14 0100511/14007456 20000 mg/kg D.W.' 0.94 10 SW846::6010C MMSD 05/12/14 DM0512/14007469 20000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 05/13/14 DMO513/14007551 21000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 05/14/14 DMO514/14007577 19000 mg/kg D.W. 1.7 10 A0. SW846: 6010C MMSD 05/15/14 DM0515/14007665 20000 mg/kg D.W: 1.7 10 AO. SW846:.6010C MMSD 05/16/14 DM0516/14007680 21000 mg/kg D.W. 1.7 10 _ AO. SW846: 6010C MMSD 05/17/14 DMO517/14007691 18000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 05/18/14 DM0518/14007710 18000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 05/19/14 DM0519/14007764 18000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 05/20/14 DM0520/14007997 21000 mg/kg D.W. 1.7 10.: AO. SW846: 6010C MMSD 05/21/14 DMO521114008023 21000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD SYS/rptimlloMonthly 1/10/13 U Page 67 of 106 Printed- 1/8/1510:48 i M 5 D PAIN IN A tli 2 [#r'IONNINI PHOSPHORUSICP METHOD ,sample o OS/22/14 DM0522/14008042 20000 mg/kg D.W. o 0.94 10.. • Annual Milorganite Report January 1 to December 31, 2014. .. SW846: 6010C MMSD 05%23/14 DM0523/14008051 22000 mg/kg D.W. 1.7 to A0. SW846: 6010C MMSD 05/24/14 DM0524/14008291 . 21000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 05/25/14 DMO525/14008310 21000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 05/26/14 DMO526/14008323 22000 mg/kg D.W. 1.7 10' AO. SW846: 6010C MMSD 05/27/14 DMO527/14008646 23000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 05/28/14 DM0528/14008672 22000 mg/kg D.W. 1.7 10 AO. SW846::6010C MMSD 05/29/14 DM0529/14008691 22000 mg/kg D.W. 1.7 to.. _ AO. SW846: 6010C MMSD 05/30/14 DMO530/14008845 22000 mg/kg D:W. 0.94 10 SW846: 6010C MMSD O5/31/14 DM0531/14008856 22000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/01/14 DM6601/14009580 MOO mg/kg D.W. 6.94 10 SW846: 6010C MMSD 06/02/14 DM0602/14009593 22000 mg/kg D:W. 0.94 10 SW846: 6010C MMSD .06/03/14 DM0663/14009620 220DO mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/04/14 :: bmb604/14009635 21000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 06/OS/14 DM0605/14009654 22000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 06/06/14 DM0606/14009669 22000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 06/07/14 DM0607/14009844 24000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 06/08/14 bmQ608/14009867 23000 mg/kg D.W. 1.7 10 AO. SW846:.60]OC MMSD 06/09/14 DM0609/14009880 23000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 06/,10/14 DM0610/14009907 24000 mg/kg D.W. 1.7 10' AO. SW846: 6010C MMSD 06/11/14 DM061'1/14010237 22000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/12/14 DMO612/14010256 22000 mg/kg D.W. 6.94 10 SW846: 6010C MMSD 06/13/14 DM0613/14010271 21000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/14/14 DM0614/14010282 210DO mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/15/14 DMO615/14010301 21000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/16/14 DMO616/14010319 21000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/17/14 DM0617/14010346 21000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/18/14 DM0618/14010687 210DO rang/kg D.W. 0.94 10 SW846: 6010C MMSD 06/19/14 DMO619/14010706 21000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/20/14 DMO620/14010721 19000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/21/14 DM0621/14010732 19000 mg/kg D.W. 0.94 10:: SW846: 6010C MMSD 06/22/14 DM0622/144010751 19000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/23/14 DM0.623/14011513 19000 mg/kg D.W. 0.94 10 SW846:.6010C MMSD 06/24/14 DM0624/14011540 20000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/25/14 DM0625/14011566 19060 mg/kg D.W. 0.94 16 SW846: 6010C MMSD 06/26/14 DM0626/14011766 20000 mg/kg D.W. 0.94 10 SW846: 6010C. MMSD 06/27/14 DM0627/14011781 20000 mg/kg D.W. 0.94 10 SW846 6010C MMSD 06/28/14 DM0628/14011792 20000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/29/14 DM0629/14011811 20000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 06/30/14 DM0630/14011824 20000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 07/01/14 DM0701/14011851' 2000D mg/kg D.W. 0.94 10 SW846: 6010C MMSD 07/02/14 DM0702/14011879 21000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 07/03/14 DM0703/14011898 21000 mg/kg D.W. 0.94 10 SW846: 6010C " MMSD 07/04/14 DM0704/14011911 21000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 07/05/14 DM0705/14011924 21000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 07/06/14 DM0706/14011943 21000 mg/kg DM. 0.94 10 SW846: 6010C MMSD 07/07/14 DM0707/14012196 21000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD. Page 68 of 106 SYS/rptlMi/oMonth/y 1110113 tj Printed, 11611510:48 �} polgiP.i lot a Clktu IvoltiNow PHOSPHORUS ICP METHOD 07/08/14 DM0708/14012898 22000 mg/kg D:W. 0.94 10 � 1 i 1 Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 07/09/14 DM0709/14012926 22000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 07/10/14 DM0710/14012945 21000 mg/kg D.W. 6.94 10 SW846: 6016C MMSD 07/11/14 DM0711/14012961 21000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 07/12/14 DM0712/14012971 22000 my/kg D.W. 1.7 10'' AO. SW846: 6010C MMSD 07/13/14, DM0713/14012991 22000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 07/14/14 DM0714/14013004 22000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 07/15/14 DM0715/14013031 23000. mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 07/16/14 DM0716114013059 23000 mg/kg D,W. 1.7 10 SW846: 6010C MMSD 07/17/14 DM0717/14013078 24000 mg/kg D.W. 1.7 10 A0. SW846: 6010C MMSD 07/18/14 DM0718/14013295: 23000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 07/19/14 DM0719/14013305 23000 mg/kg D.W. '1.7 101. AO. SW846: 6010C MMSD 07/20/14 DM0720/14013324 23000 mg/kg D:W. 1.7 10 AO. SW846: 6010C MMSD 07/21/14 DM0721/14013337 23000 mg/kg D.W. 1.7 10 AO. SW646: 6010C MMSD 07/25/14 DM0725/14013997 22000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 07/26/14 DM0726114014008 24000 mg/kg D.W. 1.7 10,; AO. "SW846: 6010C MMSD 07/27/14 DM0727/14014027 24000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 07/28/14 DM0728/14014040 23000 mg/kg D.W. A.7 10 AO. SW846: 6010C MMSD 07/29/14 DM0729114014895 23000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 07/30/14 DM0730114014923 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 07/31/14 DM0731/14014942 23000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 08/01/14 DM0801/14014957 25000 mg/kg D.W. 1.7 10 AO. SW846:.6016C MMSD 08/02/14 DM0802/14014968 25000 mg/kg D.W. 0.94. 10 SW846: 6010C MMSD 08/03/14 DM0803/14014987 25000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 08/04/14 DM0804/14015000 25000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 08/05/14 DM0805/14015027 24000 mg/kg D.W. 1.1 10 AO. SW846:6010C MMSD 08/06/14 DMO806/14015405 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 08/07/14 DM0807/14015456 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 08/08/14 DMO808/14015471 24000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 08/09/14 DMO809/14015482 26000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 08/10/14 DMO810/14015966 26000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 08/11/14 DM0811/14015984 27000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 08/12/14 DMO812/14016011 25000 mg/kg D.W, 1.7 10 SW846: 6010C MMSD 08/13/14 DM0813/14016039 25000 mg/kg D.W. 1.7 10 AO, Q2. SW846: 6010C MMSD 08/14/14 DM0814/14016058 24000 mg/kg D.W. 1.7 16 SW846: 6010C MMSD 08/15/14 DM0815/1401618:1 24000 ing/kg D.W. 1.7 10. ^AO. SW846: 6010C MMSD 08/16/14 DM0816/14016192 ... 24000 mg/kg D.W, ..1.7 10 SW846: 6010C MMSD 08/17/14 DM6817/14016211 23000 mg/kg D.W. .1.7 10 SW846: 6010C MMSD 08/18/14 DM0818/14616290 22000 mg/kg D.W. 1.7 16 SW846: 6010C MMSD 08/19/14 DM0819114016319 23000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 08/20/14 DM0820/14016347 21000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 08/21/14 DM0821/14016366 19000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 08/22/14 DM0822/1401638.1 17000 mg/kg D.W. 1.7 10 " SW846: 6010C MMSD 08/23/14 DM0823/14016392 19000 mg/kg D.W.. .1.7 10 SW846: 6010C MMSD 08/24/14 DM0824114016411 22000 mg/kg D.W. 1,7 10 SW846: 6010C MMSD 08/25/14 DM0825/14016488 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 08/26/14 DM0826/14016515 22000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD SYS/rptlMiloMonthly 1110113 lj Page 69 of 106 Printed- 118/1510:98 Annual Milorpnite Report January 1 to December 31, 2014 MSD- moir')fill k 00 fY IFN ENT PHOSPHORUS ICP. METHOD Sample,e o o • . 08/28/14 DMO828/14016907 20000 mg/kg D.W. 1.7 10, SW846: 6010C MMSD 08/29/14 DMO829/14017671 18000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 08/30/14 bM0830/14017682 20000 mg/kg D.W. 1.7 10 " SW846: 6010C MMSD 08/31/14 DMO831/14017701 22000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 09/01/14 DMO901/14017714 23000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 09/02/14 DMO902/14017871 23000 mg/kg D.W. . 1.7 10 SW846: 6010C, MMSD 09/03/14 DM0903/14017886 240DO mg/kg D.W. 1.7 10 SW846: 6010C MMSD 09/04/14 DMO904/14017920 25000.mg/kg D.W. 1.7 10 SW846: 60106 MMSD 09/05/14 DMO905/14017901 23000 mg/kg D.W. 1.7 10. SW846: 6010C MMSD 09/16/14 'DM0916/14019167 27000 mg/kg D.W.. .. 1.7 10 AO. SW846: 6010C:' MMSD 09/17/14 DM0917/14019195 ' 27000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 09/18j14 DMO918/14019226 26000 mg/k6 D.W. 1.7 10 SW846: 6010C MMSD 09/19/14 DMO919/14019244 28000 rng/kg D.W. 1.7 10 SW846: 6010C MMSD . , 09/20/14 .. DM0920/14019255 : 28000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 09/21/14 DM0921/14019274 28000 mg/kg D.W. 1.7 10 SW846: 6010C, MMSD 09/22/14 DM0922/14019287 28000'mg/kg D.W. 1.7 10 SW846: 6010C MMSD 09/23/14 DM0923/14019778 25000 Trig/kg D.W. 1.7 10 AO. SW846: 6010C, . MMSD 09/24/14 DM0924/14019806 23000 mg/kg D.W:. 1.7 10 SW846: 6010C MMSD 09/25/14 DM0925/14019826 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 09/26/14 DM0926/14019840 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 09/27/14 DM0927114019851 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD " 09/28/14 DM0928/14019870 26000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 09/29/14 DM0929/14019883 V000 mg/kg D.W. 1.7' 10.: SW846: 6010C MMSD 09/30/14 DM0930/14019909 26000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 10/01/14 DM1001/14019927 26000 mg/kg D.W._ 1.7 10 SW846: 6010C MMSD 10/02/14 DM1.002/14020572 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 10/03j14 DM1003/14020587 35000 mg/kg D.W. 1.7 10 . A0, Q3. SW846: 6010C ,MMSD 10/04/14 DM1004/14020598 22000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 10/05/14 DM1005/14020617, 21000 mg/kg D.W.. 0.94 10 SW846: 6010C MMSD 10/06/14 DM1006/14020630 22000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD SO/07/14 .. DM1007/14021108 22060 mg/kg D.W. 0.94 10:: SW846: 6010C MMSD 10/08/14 DM1008/14021160 22000 mg/kg D.W. 0.94 10 _ SW846: 6010C MMSD 10/09/14 DM1fl09/14021179 23000 mg/kg D.W.: 0.94 10 SW846: 6010C MMSD 10/10/14 DM1010/14021194 22000 mg/kg D.W. 0.94 10, SW846: 6010C MMSD 10/11/14 DM1011/14021244 23000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 10/12/14 DM1012/14021263 23000 mg/kg D.W. 1.7 10 SW846: 6010C. MMSD 10/13/14 DM1013/14021276 24000 mg/kg D.W. 1.7 10 SW846::6010C MMSD 10/14/14 DM1'01.4/14021304 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 10/15/14 DM1015/14021332 23000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 10/16/14 DM1;016/14021351 23000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 10/17/14 DM1017114021787 24000 mg/kg D.W. 1.7 T 10 SW846: 6010C MMSD 10/18/14 DM1018114021798 22000 mg/kg D.W. 1.7 10:: AO. SW846: 6010C MMSD 10/19/14 DM1019/14021817 23000 mg/kg D.W. 1.7 16 AO. SW846: 6010C MMSD 10/20/14 DM1020/14021830. 22000 mg/kg D.W.. 1.7 10 AO. SW846: 6610C : MMSD 10/21/14 DM1.021/14021857 23000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 10/22/14 DM1022/14021885 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD .. 10/23/14 DM1023/14022256 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD Page 70 of 106 SY51rptlMiloMonthly 1110113 tj Printed., 11811510:48 � f r 'MSDfa... , Pdh1NCka I� A Clk�i1R Ckd107A8IN1 PHOSPHORUS ICP METHOD sampleDatdo 10/24/14 DM1024/14022, ® 0o oQ 24000 mg/kg D.W. 1.7 15 Annual Milorganite Report . January 1 to December 31, 2014 e, 6010C MMSD 10/25/14 DM1025/14022286 23000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 10/26/14 DM1026/14022305 24000 mg/kg D.W. 1.7 10 AO. SW846:.6010C MMSD 10/27/14 DM1027/14022318 24000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 10/28/14 DM1028/14022409 24060 mg/kg D.W. 1.7 16 AO. SW846: 6010C MMSD 10/29/14 DM1029/14022439 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 10/30/14 DM1030/14022510 22000 mg/kg D.W. 1.7 10 SW846::6010C MMSD 10/31/14 DM1031/14022525 24000 mg/kg D.W. 1.7 10 ..SW846: 6010C MMSD 11/01/14 DM1101/14622536 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/02/14 D.M1102/14022555 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/03/14 DM1103/14022568 25000 mg/kg D.W. 1.7 10 AO. SW846:-6010C MMSD 11/04/14 DM1104/14023111 24000 mg/kg D.W. 1.7 10 . SW846: 6010C MMSD 11/95/14 DM1105/14023139 25000'mg/kg D.W. 1.7 1.0 SW846: 6010C MMSD 11/06/14 DM1106/14023158 24000 mg/kg D.W. 1.7 10 AO. SW846:.6010C. MMSD 11/07/14 DM1107/14023173 - 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/08/14 DM1108/14023184 25000,mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/09/14 DM1109/14023203 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/10/14 DM1110/14023767 26000 mg/kg D.W. 1.7 10 i SW846: 6010C MMSD 11/11/14 DM1111/14023796 .25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/12/14 DM1112/14023876 250.00 mg/kg D.W. 1.7 10, ::SW846: 6010C MMSD 11/13/14 DM1113/14023895 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/14/14 DM1114/14023910 25000 mg/kg D.W.: _ 1.7 10 A0, SW846:;6010C MMSD 11/15/14 DM1115/14023929 24000.mg/kg D.W. 1.7 10 ..,SW846: 6010C MMSD 11/16/14 DM1116/14023948 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/17/14 DM1117/14023961 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/18/14 DM1118/14024236 23000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/19/14 DM1119/14024264 24000 mg/kg D.W. 1.7 10 .SW846: 6010C MMSD ll/20/14 DM1120/14024283 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/21/14 DM1121/14024302 26000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/22/14 DM1122/14024313 26000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/25/14 DM1123/14024393 24000 mg)kg D.W. 1.7 10; SW846: 6010C MMSD il/24/14 DM1124/14024414 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/25/14 DM1125/14024441 . 24000 mg/kg D.W. 1.7 10 SW846:6010C MMSD 11/26/14 DM1.126/14024469 22000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 11/27/14 DM1127/14024529 24000 mg- ft D.W. 1.7 110. AO. SW846: 6010C MMSD .. ll%28/14 DM1128/14024544 24000 mg/kg D.W. 1.7 10. AO. ^ . SW846: 6010C MMSD 11/29/14 DM1129/14024555 , 24000 mg/kg D.W.:. 1.7 10 A0. SW846: 6010C MMSD 11/30/14 DM1'130/14024574 24000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 12/Oh/14 DM1201/14024601 24000 mg/kg D.W. 1.7 10 A0. SW846: 6010C MMSD 12/02/14 DM1202/14025299 25060 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/03/14 DM1203/14025327 25000 mg/kg D.W: 1.7 10 SW846 6010C T MMSD 12/04/14 DM1204/14025346 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/05/14 DM1205/14025361 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/06/14 DM1206/14025372 26000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/07/14 DM1207/14025391 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/08/14 DM1208/14025404 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/09/14 DM1209/14026170 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD SYS/rptimiloMonthiy 1110113 tj Page 71 of 106 Printed. • 11811510:48 r Annual Milorganite Report -January 1 to. December 31, 2014 MMSD r imm lot A CRIMR�►a� J�aExr PHOSPHORUS ICP METHOD Sample Date SamplelD Result o.d 12/10/14 DM1210/14026198 26060 mg/kg D.W. 1.7 10:- AO. SW846: 6010C MMSD 12/11/14 DM1211/14026217 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/12/14 DM1212/14026232 26000 mg/kg D.W. 3.7 10 AO.. SW846: 601OC MMSD 12/13/14 DM1213/14026243 26000 mg/kg D.W. 1.7 10 AO. SW846: 6010C MMSD 12/14/14 DM1214/14026262 26000. m- Wkg D.W. 1.7 10' A0. SW846: 6010C MMSD 12/15/14 DM1215/14026277 26000 mg/kg D.W. 1.7 10 AO., SW846: 6010C. MMSD 12/16/14 DM1216/14026475 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/17/14 DM1217/14026503 25000 mg/kg D.W. 1.7 10 . SW846: 6010C MMSD, 12/18/14 DM1218/14026522 24000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/19/14 DM1219/14026537. 24000 mg/kg D.W. 1.7 10 SW846: 6010C; MMSD 12/20/14 DM1220/14026653 23000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/21/14 DM1221114026672 23000 mg%kg D.W. 1.7 10 SW846: 6010C MMSD 12/22/14 DM1222/14026685 24000 mg/kg D.W. 1.7 10 Q2. SW846: 6010C MMSD 12/23/14 DM1223/14026713 25000 mg/kg D.W., :'1.7 10 SW846: 601OC: MMSD 12/24/14 DM1224/14026741 26000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/25/14 DM1225/14026760 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/26/14 DM1226/14026777 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD 12/27/14 DM1227/14026788 24000 mg/kg D.W. 0.94 10 SW846: 6010C MMSD 12/28/14 DM1228/14026807 23000 mg/kg D.W. 0.94 10. SW846: 6010C MMSD 12/29/14 DM1229/14027031 24000 m6%kg D.W. 0.94 16 SW846: 6010C MMSD 12/30/14 DM1230/14027058 24000 mg/kg D.W. 0.94 16 SW846: 6010C MMSD 12/31/14 DM1231/14027086 25000 mg/kg D.W. 1.7 10 SW846: 6010C MMSD Avg: 23000.mg/kg D.W. 5Y5/rptlMi/oMonthly 11101-13 tj Max: 35000 mg/kg D.W. Page 72 of 106 Printed: 11811510.48 PdAfATRS fU9 A• ClE�ttR [�dirY.I1Nflii POTASSIUM ICP METHOD 01/01/14 DM0101/14000012 4500 mg/kg D.W. 48 100 Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 01/02/14 DMO102/14000039 4300 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/03/14 DMO103114000088 3900 mg/kg D.W; 48 100 SW846:.6010C MMSD 01/04/14 DMO104/14000103 4000 mg/kg D.W. 48 100 SW846: 6010C MMSD 01j05/14 DM0105/14000122 3900 m6/kg D.W. 48 100_ SW846: 6010C MMSD 01/06/14 DMO.106/14000135 3800 mg/kg D.W. 48 100 Q3. SW846: 6010C MMSD 01/07/14 QM0107/14000162.. 3300 mg/kg D.W. " 48 100 SW846: 6010C MMSD 01/08/14 DM0108/14000188 3600 mg/kg D.W. 48 100 Q3. SW846: 6010C MMSD Ol/09/14 DM0109/14000247 3700 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/10/14 DM0110/14000430 ,; 3200 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/11/14 DM01 11 /14000441 3500 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/12/14 DM0112/14000460 3300 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/13/14 DM0113/14000473 3100 mg/kg D.W. 48 100 SW846: 6010C MMSD OS/14/14 DM0114/14000500 3200 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/15/14 DMO115/14000526 3200 mg/kg D.W. 48 100 SW846:' 6010C MMSD 01/16/14 DM0116/14000545 3500 mg/kg D.W. 48 S00 SW846: 6010C MMSD 01/17/14 DM0117/14000560 3400 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/18/14 DM0118/14000571 , 4100 mg/kg D.W. -48 100 SW846:; 6010C MMSD 01/19/14 DM0119/14000590 3900 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/20/14 DMO120/14000603 3900 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/21/14 DM0121/14000630 3800 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/22/14 DM0122/14000656: 3700 mg/kg D.W. 48 _ 100 SW846::6010C MMSD 01/23/14 DM0123/14000675 3700 mg/kg D.W. 48 too_-. SW846: 6010C MMSD O1/24/14 DMO124/14000690 4000 mg/kg D.W. 48 100 SW846: 6010C MMSD .. 01/25/14 DMO125/14000923 3800 mg/kg D.W. 48 100 SW846: 6010C MMSD' ' 01/26/14 DM0126/14000942' 3800 mg/kg D.W. 48 100 " SW846: 6010C MMSD 01/27/14 DMO127/14001095 3800 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/28/14 DM0128/14001122 3500 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 01/29/14 DMO129/14001148 3500 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 01/30/14 DMO130/14001167 3400 mg/kg D.W. 48 100 SW846: 6010C MMSD 01/31/14 DMO131114001182 3800 mg/kg D.W. 48 100 . SW846: 6010C MMSD 02/01/14 DM0201/14001193 3700 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/02/14 DM0202114001430 3700 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/03/14 DM0203/14001443 3600 mg/kg D.W. 48 100 SW846: 6010C - MMSD 02/04/14 DM0204/14001470 3600 mg/kg D.W. 48 100 SW846: 6010C .MMSD 02/05/14 DM0205/14001498 3300 mg/kg D.W. 48 100 . SW846: 6010C MMSD 02/06/14 DM0206/14001517 3200 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/07/14 DM0207/14001532 3700 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/08/14 DM0208/1.4001543 3500 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/09/14 DM0209/14001562 3300 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/10/14 DM0210/14001576' 3300 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/11/14 DM0211/14001811 3300 mg/kg D.W. 48 100 AO. .. SW846: 6010C MMSD 02/12/14 DM0212/14001837 3400 mg/kg DX 48 100 SW846: 6010C MMSD 02/13/14 DM0213/14001856 3500 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/14/14 DM0214/14001871 3300 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/15/14 DM0215/14001882 3700 mg/kg D.W. 48 100 SW846: 6010C MMSD .02/16/14 DM0216/14001893 5Y5/rpt1Mi/oM6nth/y 1110113 tj 3900 mg/kg D.W. 48 100 SW846: 6010C MMSD Page 73 of 106 Printed: 11811510.48 e , G P,IRiR{P3 (UP A CIE+.HR [�it�:tlAfNl POTASSIUM ICP METHOD Date Sample I I D Result LOD LQQ QA.Flags � Annual Milorganite Report January 1 to December 31, 2014 Analy.bcal Method Lab 02/17/14 DM0217/14001914 4000 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/18/14 DM0218/14002002 4000 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/19/14 DM0219/14002028 3800 mg/kg D.W.: 48 100 SW846: 6010C MMSD 02/20/14 DM0220/14002101 3700 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/21/14 DM0221/14002181 3300 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/22/14 DM0222/14002192 3300 mg/kg O.W.. 48 100 SW846: 6010C MMSD 02/23/14 DM0223/14002211 3300 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/24/14 DM0224/14002224 3500 mg/kg D.W. 48 100- SW846: 6010C MMSD 02/25/14 DM0225/14002251 3500 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/26/14 DM0226/14002310 3800 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/27/14 DM0227/14002329 4500 mg/kg D.W. 48 100 SW846: 6010C MMSD 02/28/14 DM0228/14o02350 4100 mg/kg D.W. 48 S00 SW846: 6010C MMSD 03/01/14 DM0301/14002921 4600 mg/kg D.W. 48 100 _ SW846: 6010C MMSD 03/02/14 DM0302/14002940 4100 mg/kg D.W. 48 100 SW846: 6010C MMSD 03/03/14 DM0303/14002953 4100 mg/kg D.W. 48 100 SW846: 6010C MMSD 03/04/14 DM0304/14002986 3900 mg/kg D.W. 48 100. . SW846: 6010C MMSD 03/OS/14 DM0305/14003012 4200 mg/kg D.W. 48 100 Q3. SW846: 6010C MMSD 03/06/14 DM0306/14003182 ' 4000 mg/kg D.W. 48 100 SW846:'6010C MMSD 03/07/14 DM0307/14003197 4000 mg/kg D.W. 48 100 .SW846: 6010C MMSD 03/06/14 DM0308/14003208 3800 m6/kg D.W. 48 100 A0. SW846: 6010C MMSD 03/09/14 DM0309/14003232 3800 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 03/10/14 DM0310/14003245' 3400 mg/kg D.W: 48 100 AO. SW846: 6010C MMSD 03/11/14 DM0311/14003272 3500 mg/kg D.W. 48 100.. AO. ..SW846: 6010C MMSD 03/12/14 DM0312/14003300 3800 mg/kg D.W. 48 100 SW846: 6010C MMSD 03/13/14 DM0313/14003871 4200 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 03/14/14 DM0314/14003886 4300 mg/kg D.W: 48 100 AO. SW846: 6010C MMSD 03/1S/14 DM0315/14003899 5500 mg/kg DN. 48 100. AO. SW846: 6010C MMSD 03/16/14 - DM0316114003918 5200 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 03/17/14 DM0317/14003936, 4900 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 03/18/14 DM0318/14003963 3900 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 03/19/14 DM0319/14004217 3900 mg/kg D.W. 48 100 A0. SW846: 6010C MMSD 03/20/14 DM0320/14004315 4200 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 03/21/14 DM0321/14004330 4100 mg/kg D.W. 48 100 AO. SW846: 6016C MMSD 03/22/14 DM0322/14004341 3800 mg/kg D.W. 48 100. AO. SW846: 6010C MMSD 03/23/14 DM0323114004360 4100 mg/kg D:W. 48 100 :AO. SW846: 6010C MMSD 03/24/14 DM0324/14004461 4400 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 03/25/14 DM0325/14004638 4600 mg/kg D.W. 48 100 AO. SW846: 6016C MMSD 03/26/14 DM0326/14004664 5000 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 03/27/14 DMO327/14004683 4400 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 03/28/14 DM0328/14004698 4100 mg/kg D.W. 48 100 A0. SW846: 6010C MMSD 03/29/14 DM0329/14004889 4200 mg/kg D.W. 48 100 A0. SW846: 6010C MMSD 03/30/14 DM0330/14004908 4100 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 03/31/14 DM0331/14004921 4300 mg/kg D.W. 48 100 AC. SW846: 6010C MMSD 04/01/14 DM0401/14004948 4400 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/02/14 DM0402/14004974 4900 mg/kg D.W. 48. 100 AO. SW846: 6010C MMSD 04/03/14 DM0403/14004993 4600 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/04/14 DM0404/14005195 4200 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD SYS/rptimi/oMonth/y 1110113 tj Page 74 of 106 Printed: 1/8/1510:48 MSD P11RIN115 (Ia. A CIL(* 191INNNINI POTASSIUM ICP METHOD Annual Milorganite Report January 1 to December 31, 2014 bampie iate 04/05/14 sampie io DM0405/14005206 ReSUlt 4500 mg/kg D.W. WD 48 LOQ 100 QA Flags, AO. Analytical MiAhdd SW846: 6010C Lab MMSD 04/06/14 DM0406/14005226 4500 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/07/14 DM0407/14005240 4600 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/08/14 DM0408/14005267 4100 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/09/14 DM0409/14005397 4500 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/10/14 DM0410/14005416 4400 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/11/14 DM0411/14005434 4500 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/12/14 DM0412/14005605 4200 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/13/14 DM0413/14005627 4200 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/14/14 DM0414/14005641 4300 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/15/14 DM0415/14005668 4100 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/16/14 DM0416/14005791 4200 mg/kg D.W. 48 100 AO, Q2. SW846: 6010C MMSD 04/17/14 DM0417/14005815 4800 mg/kg D.W. 46 100 SW846: 6010C MMSD 04/18/14 DM0418/14006027 4600 mg/kg D.W. 48 100 AO, Q2. SW846: 6010C MMSD 04/19/14 DM0419/14006038 4800 mg/kg D.W. 46 100 SW846: 6010C MMSD 04/20/14 DM0420/14006057 5000 mg/kg D.W. 46 100 SW846: 6010C MMSD 04/21/14 DM0421/14006127 4800 mg/kg D.W. 46 100 SW846: 6010C MMSD 04/22/14 DM0422/14006154 4500 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/23/14 DM0423/14006180 4300 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/24/14 DM0424/14006339 4000 mg/kg D.W. 48 100 SW846: 6010C MMSD 04/25/14 DM0425/14006354 4400 mg/kg D.W. 48 100 SW846: 6010C MMSD 04/26/14 DM0426/14006365 4300 mg/kg D.W. 48 100 SW846: 6010C MMSD 04/27/14 DM0427114006384 4400 mg/kg D.W. 48 100 SW846: 6016C MMSD 04/28/14 DM0428/14006397 4400 mg/kg D.W. 48 100 SW846: 6010C MMSD 04/29/14 DM0429/14006454 4200 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 04/30/14 DM0430/14006482 4500 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 05/01/14 DM0501/14006976 4200 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 05/02/14 DMO502/14006991 4600 mg/kg D.W. 48 100 AO, Q2. SW846: 6010C MMSD 05/03/14 DM0503/14007150 4300 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 05/04/14 DM0504/14007169 4200 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 05/05/14 DM0505114.007182 4400 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD OS/06/14 DM0506/14007209 4500 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 05/07/14 DM0507/14007235 4600 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 05/08/14 DM0508/14007254 4400 mg/kg D.W. 48 100 AO. SW846: 6010C MMSD 05/09/14 DM0509/14007269 43.00 mg/kg D.W. 46 100' AO. SW846: 6010C MMSD 05/10/14 DM0510/14007280 4500 mg/kg D.W. 46 100 SW846: 6010C MMSD 05/11/14 DMO511/14007456 4800 mg/kg D.W. 46 100 SW846: 6010C MMSD 05/12/14 DMO512/14007469 4900 mg/kg D.W. 46 100 SW846: 6010C MMSD 05/13/14 DMO513/14007551 4700 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 05/14/14 DM0514/14007577 4500 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 05/15/14 DM0515/14007665 4200 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 05/16/14 DM0516/14007680 5500 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD OS/17/14 DMO517/14007691 4900 mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 05/18/14 DM0518/14007710 4700 mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 05/19/14 DM0519/14007764 4700 mg/kg D.W. 46 100 AO, 88. SW846: 6010C MMSD 05/20/14 DM0520/14007997 5200 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 05/21/14 DMO521/14008023 4800 mg/kg D.W. 46 100 SW846: 6010C MMSD SYSIrpti iloMonthly 1/10/13 tj Page 75 of 106 Printed. 118115 10:48 P,iAIMS W A UYIVIR fiiAKKKKI POTASSIUM; ICP METHOD Sample Date Sample ID Result LOD LGQ Q• Flags Annual Milorganite Report January 1 to December 31, 2014 AnaWrical Method Lab 05/22/14 DM0522/1'4008042 4900 mg/kg D.W. 46 100 SW846: 6010C MMSD 05/23/14 DM0523/14008057 5100 mg/kg D.W. 46 100 AO, Q3. SW846: 6010C MMSD 05/24/14 DMO524/14008291 4800 mg/kg D.W: 46 100 AO. SW846: 6010C MMSD 05/25/14 DM0525114008310 4700 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 05/26/14 DM0526/14008323 4500 mg/kg D.W. 46 10b AO. SW846: 6010C MMSD 05/27/14 DM0527/14008646 . ., 4400 mg/kg D.W. 46 100 A0. SW846: 6010C MMSD 05/28/14 DM0528/14008672 4400 mg/kg D.W. 46 100 AO: SW846: 6010C MMSD 05/29/14 DM0529/14008691 4200 mg/kg D.W. 46' 100 AO. SW846: 6010C MMSD OS/30/14 DM0530/14008845 4300 mg/kg D:W. 46 100 SW846: 6010C MMSD 05/31/14 DMO531/14008856 4200 mg/kg D.W. 46 100 SW846: 6010C MMSD 06/01/14 DM0601/14009580 , 4200 mg/kg D.W. 46 100 SW846: 6010C MMSD 06/02/14 DM060211.4009593 4400 mg/kg DX 46 100 SW846: 6010C MMSD 06/03/14 DM06b3/14009620 4400 mg/kg D.W. 46 ibb SW846: 6010C MMSD 06/04/14 bM0604/14009635. 4000 mg/kg D.W. 46 100 AO. SW846:.6010C MMSD 06/05/14 DM0605/14009654 4000 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 06/06/14 DM0606/1.4009669 4000 mg/kg D.W. 46 100. AO. SW846: 6010C MMSD 06/07/14 DM0607/14009844 4200 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 06/08/14 DM0608/14009867:. 4200 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 06/99/14 DM0609/14009880 4200 mg/kg D.W. 46 100 AO. 5WB46: 6010C MMSD 06/10/14 DM06.10/1.4009907 4400 mg/kg D:W. 46 100 AO. SW846: 6010C MMSD .. 06/11/14 DM0611/14010237 4000 mg/kg D.W. 46 100 SW846: 6010C MMSD 06/12/14 DM0612/14010256 3700 mg/kg D.W. 46 100 A SW846:6010C MMSD 06/13/14 DM0613/14010271 3800 mg/kg D.W. 46 100 SW846: 6010C MMSD 06/14/14 DM0614/14010282 4500 mg/kg D.W. 46 100 SW846: 6010C MMSD 06/15/14 DM0616/14010301 4600 mg/kg D.W. 46 100 SW846: 6010C MMSD 06/16/14 DM0616/14010319 ' 4400 mg/kg D.W. 46 100 SW846:' 6010C MMSD 06/17/14 DM0617/14010346 4200 mg/kg D.W. 46 100 SW846: 6010C MMSD 06/18/14 DM0618/1.4010687 4300 mg/kg D.W. 46 100 SW846: 6010C MMSD 06/19/14 DMO619/14010706. 3700 mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 06/20/14 DM0620/14010721 3900 mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 06/21/14 DM0621/1401073.2 4200 mg/kg D.W. 46 100 B8. SW846: 6010C 'MMSD 06/22/14 DM0622/14010751 4300 mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 06/23/14 DM0623/14011513. 4500 mg/kg D.W. 46 100 B8, Q2. SW846: 6010C MMSD 06/24/14 DM0624/14011540 5400 mg/kg D.W. 46 100 SW846: 6010C MMSD 06/25/14 DM0625/14011566 4800 mg/kg D.W. 46 100 SW846: 6010C MMSD 06/26/14 DM0626/14011766 4800 mg/kg D.W. 46 100 SW846: 6010C MMSD 06/27/14 DM0627/14011781: 5100 mg/kg D.W: 46 100 SW846: 601bC MMSD 06/28/14 DM0628/14011792 4900 mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 06/29/14 DM0629/1401181"1 4800'mg/kg D'.W. 46 100 B8. SW846: 6010C MMSD 06/30/14 DMO630/14011824 4700 mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 07/01/14 DM0701/14011851 4700 mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 07/02/14 DM0702/14011879 4700 mg/kg D.W. 46 100. _ SW846: 6010C MMSD 07/03/14 DM0703/14011898 4800 mg/kg D.W. 46 100 SW846: 6010C MMSD 07/04/14 DM0704/14011911 5200 mg/kg D.W. 46 100 SW846: 6010C MMSD 07/05/14 DM0705/14011924 5100 mg/kg D.W. 46 100 SW846: 6b10C MMSD 07/06/14 DM0706/14011943 4900'mg/kg D.W. 46 100; SW846: 6010C MMSD 07/07/14 DM0707/14012196 4700 mg/kg D.W. 46 100 SW846: 6010C MMSD SYS/rpt.fMilomonthiy 1110113 tj Page 76 of 106 Printed. • 1/8/I510.48 MSDJanuary Pd118Ci5W A [tUIR 1911DAW[w POTASSIUM. ICP METHOD Sample.Date Sample ID Result LOD LOP .. 1 1 i Annual Milorganite Report 1 to December 31, 2014 07/08/14 DM0708/14012898 4300 mg/kg D.W. 46 100 SW846: 6010C MMSD 07/09/14 DM0709/14012926 4100 mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 07/10/14 DM0710/14012945 4400 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/11/14 DM0711/14012961 3800 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/12/14 DM0712/14012971 3300 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/13/14 DM0713/14012991 3500 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/14/14 DM0714/14013004 3600 mg/kg D.W. 46 100 AO. SW846:.6010C MMSD 07/15/14 DM0715/14013031 3400 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/16/14 DM0716/14013059 3400 mg/kg D.W. 46 100 SW846: 6010C MMSD 07/17/14 DM0717/14013078 3400 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/18/14 DM0718/14013295 3400 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/19/14 DM0719/14013305 3500 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/M/14 DM0720114013324 3600 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/21/14 DM0721/14013337 3600 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/25/14 DM0725/14013997 3600 mg/kg D.W. 46 100 SW846: 6010C MMSD 07/26/14 DM0726/14014008 3500 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/27/14 DM072,7/14014027 3500 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/28/14 DM0728/14014040 3500 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/29/14 DM0729/14014895 3500 mg/kg D.W. 46 100 SW846: 6010C MMSD 07/30/14 DM0730/14014923 3500 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 07/31/14 DM0731/140149.42 3200 mg/kg D.W. 46 100. SW846: 6010C MMSD 08/01/14 DMO801/14014957 3600 mg/kg D.W. 46 100 SW846: 6010C MMSD 08/02/14 DM0802/14014968 4200 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/03/14 DM0803/14014987 4300 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/04/14 DM0804/14015000 4500 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/05/14 DM0805/14015027 3600 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/06/14 DMO806/14015405 3800 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/07/14 DM0807/14015456 4400 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/08/14 DM0808/14015471 4300 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/09/14 DM0809/14015482 4600 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/10/14 DM081,0/14015966 4800 mg/kg D.W. 46 100, AO. SW846: 6010C MMSD 08/li/14 DM0811/14015984 4600 mg/kg D.W. 46 100 A0. SW846: 6010C MMSD 08/12/14 DM0812/14016011 4000 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/13/14 DMO813/14016039 3900 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/14/14 DM0814/14016058 3506 mg/kg D.W. 46 100. AO. SW846: 6010C MMSD 08/15/14 DM0815/14016181 3800 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/16/14 DM0816/14016192 3700 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/17/14 DM0817/14016211 3600 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/18/14 DM0818/14016290 3300 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/19/14 DMO819/14016319 3400 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/20/14 DM0820/14016347 4100 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/21/14 DMO821114016366 4700 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/22/14 DM0822/14016381 4100 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/23/14 DM0823/14016392 4500 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/24/14 DM0824/14016411 4300 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/25/14 DM0825/14016488 3800 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/26/14 DM0826/14016515 3300 mg/kg D.W. 46 100 A0. SW846: 6010C MMSD 5Y5/rptlM11bMonth1y 1/10113 tj Page 77 of 106 Printed., 11811510:48 i P,AINGS lie A Mfl% B ( AW-NNIN1 POTASSIUMt ICP METHOD Sample Date Sample o ResUlt LOD ILGQ QA Flags Annual Milorganite Report January 1 to December 31, 2014 Analytical Method 08/28/14 DM0828/14016907 3400 mg/kg D.W. 46 1 0: SW846: 6010C MMSD 08/29/14 DM0829/14017671 4200 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/30/14 DMO830/14017682 4100 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 08/31/14 DM0831/1401770.1 3400 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 09/01/14 DMO901/14017714 3400 mg/kg D.W. 46 100' AO. SW846: 6010C MMSD 09/02/14 DM0902114017871 3300 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD' 09/03/14 DM0903/14017886 3300 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 09/04/14 DMO904/14017920 3200 mg/kg D.W. 46 100 .. AO. SW846: 6010C MMSD 09/05/14 DM0905/14017901 3200 m6/kg D:W. 46 100 SW846: 6010C MMSD 09/16/14 DMO916/14019167 3800 mg/kg D.W. 46 100 AO. SW846:"6010C MMSD 09/17/14 DMO917114019195 3600 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 09/18/14 DM0918/14019229 3900 mg/kg DA 46 100.' A0. "SW846: 6010C MMSD 09/19/14 DM0919/14019244 3800 mg/kg D.W. 46 100 A0. SW846: 6010C MMSD 09/20/14 DM0920/14019255, 4000 mg/kg D.W., 46 100 AO. SW846: 6010C MMSD 09/21/14 DMO921/14019274 4000 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 09/22/14 DM0922/14019287 4000 mg/kg D.W. 46 100 : AO. SW846: 6010C MMSD 09/23/14 DM0923/14019778 4100 mg/kg D.W. 46 100 A0. SW846: 6010C MMSD 09/24/14 DM0924/14019806" 3800 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 09/25/14 DMO925/14019825 4100 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 09/26/14 DM0926114019840 3900 mg%kg D.W. 46 100 AO. SW846: 6010C MMSD 09/27/14 DM0927/14019851 4000 mg/kg D.W. 46 100 AO. "SW846: 6010C MMSD 09/28/14 DMO928/14019870 4000 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 09/29/14 DM0929/14019883 3800 mg/kg D,W. 46 100. AO, Q3. SW846: 6010C MMSD 09/30/14 DM0930/14019909 3600 mg/kg D:W. 46 100 'AO. SW846: 6010C MMSD 10/01/14 DM1001/1401992'7 4100 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 10/02/14 DM1002/14020572 3800 mg/kg D.W. 46 100 A01 SW846: 6010C MMSD 10/03/14 DM1003114020587 3400 mg/kg D.W. 46 100:: AO, Q3. SW846: 6010C MMSD 10/04/14 DM1004/14020508 3800 mg/kg D.W. 46 100 SW846: 6010C MMSD 10/05/14 DM1005/14020617 3900 mg/kg D.W. 46 100 SW846: 6010C MMSD 10/06/14 DMI006/14020630 3800 mg/kg D.W. 46 100 SW846: 6010C MMSD 10/07/14 DM1007/14021108 3800 mg/kg D.W. 46 100: , SW846: 6010C MMSD 10/08/14 DM1008/14021160 3400 mg/kg D.W. 46 166 B8. SW846: 6010C 'MMSD 10/09/14 DM1009/14021179 3200 mg/kg D.W. 46 100 AO, B8. SW846r6010C MMSD 10/10/14 DM1010114021194 3200 mg/kg D.W. 46 100 AO, B8, Q3. SW846: 6010C MMSD 10/11/14 DM1011/14021244 3400 mg/kg D.W. 46 100 SW846: 6010C MMSD 10/12/14 DM1012/14021263 3300 mg/k9 D.W. 46 100 SW846: 6010C MMSD 10/13/14 DM1013/14021276: 3500 mg/kg D.W: 46 100 SW846: 6010C MMSD 10/14/14 DM101,4/14021304 3900 mg/kg D.W. 46 500.. SW846: 6010C MMSD 10/15/14 DM1015/14021332 3400 mg/kg D:W. 46 100 SW846: 6010C MMSD 10/16/14 DM1016/14021351 3300 mg/kg D.W. 46 100 SW846: 6010C MMSD 10/17/14 DM1.017/14021787 3600 mg/kg D.W: 46 100 SW846: 6010C MMSD 10/18/14 DM1018/14021798 3300.mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 10/19/14 DM1019/14021817 3400 mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 10/20/14 DM1020/14021830. 3400 mg/kg D.W. 46 100 B8. SW846: 6010C MMSD 10/21/14 DM1021/14021857 3600 mg/kg D.W. 46 100 SW846: 6010C MMSD 10/22/14 DM1022/14021885 3700 m4/kg D.W. 46 100 SW846: 6010C MMSD 10/23/14 DM1023/14022256 4200 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD SYS/rptiMdoMonth/y 1110113 0 Page 78 of 106 Printed.11811510,48 �MMSD PAIN113 IN A Cty" [VANN191 POTASSIUM ICP METHOD 10/24/14 DM1024/14022273 10/25/14 DM1025/14022286 3700 mg/kg D.W. 46 3600 mg/kg D.W. 46 100 r r Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD SW846: 6010C MMSD 10/26/14 DM1026/14022305 3500 mg/kg D.W. 46 100 SW846: 6010C MMSD 10/27/14 DM1027/14022318 3500 mg/kg D.W. 46 100 SW846: 6010C MMSD 10/28/14 DM1028/14022409 3500 mg/kg D.W. 46 100 SW846: 6010C MMSD 10/29/14 DM1029/14022439 3800 mg/kg D.W. 46 100 SW846: 6010C MMSD 10/30/14 DMI030/14022510 3200 mg/kg D.W. 46 100 Q3. SW846: 6010C MMSD 10/31/14 DM1031/14022525 3200 mg/kg D.W. 46 100 Q3. SW846: 6010C MMSD 11/Ol/14 DM1101/14022536 3500 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/02/14 QW 102/14022555 3600 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/03/14 DM1103/14022568 3600 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/04/14 DM1104/14023111 3800 mg/kg D.W. 46 100 SW846: 6b10C MMSD 11/05/14 DM1105/14023139 3700 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 11/06/14 DM1106/14023158 3600 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/07/14 DM1107/14023173 4100 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/08/14 DM1108/14023184 3800 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/69/14 DM1109/14023203 4000 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/10/14 DM1110/14023767 4000 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/11/14 DM1111/14023796 3800 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/12/14 DM1112/14023876 3800 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/13/14 DM1113/14023895 4000 mg/kg D.W. 46 lob SW846: 6010C MMSD 11/14/14 DM1114/14023910 3900 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/15/14 DM1115/14023929 4100 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 11/16/14 DM1116/14023948 4400 mg/kg D:W. 46 100 AO. SW846: 6010C MMSD 11/17/14 DM1117/14023961 4200 mg/kg D.W. 46 100 A0. SW846: 6010C MMSD 11/18/14 DM1118/14024236 3900 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/19/14 DM1119/14024264 3800 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/26/14 DM1120/14024283 3500 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/21/14 DM1121/14024302 3900 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/22/14 DM1122/14024313 4000 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/23/14 DM1123/14024393 3700 mg/kg D.W. 46 100, SW846: 6010C MMSD 11/24/14 DM1124/14024414 3300 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/25/14 DM1125/14024441 3500 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/26/14 DM1126/14024469 3600 mg/kg D.W. 46. 100 AO. SW846: 6010C MMSD 11/27/14 DM1127/14024529 3700 in9/kg D.W. 46 100 SW846: 6010C MMSD 11/28/14 DM1128/14024544 3700 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/29/14 DM1129/14024555 3800 mg/kg D.W. 46 100 SW846: 6010C MMSD 11/30/14 DM1130/14024574 3800 mg/kg D.W. 46 100 SW846: 6010C MMSD 12/01/14 DM1201/14024601 3700 mg/kg D.W. 46 100' SW846: 6010C MMSD 12/02/14 i DM1202/14025299 4300 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/03/14 DM1203/14025327 4600 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/04/14 DM1204/14025346 3900 mg/kg D.W. 46 100. AO. SW846: 6010C MMSD 12/05/14 DM1205/14025361 3900 mg/kg D.W. 46 100 A0. SW846: 6010C MMSD 12/06/14 DM1206/14025372 4100 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/07/14 DM1207/14025391 4400 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/08/14 DM1208/14025404 4600 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/09/14 DM1209/14026170 4100 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 5Y5/rpt1Mi1bMonth/y 1/10/13 tj Page 79 of 106 Printed., 1/8/1510.•48 ` � o r-� NS- D PbAIN05lot A CUMR 10KIN W. POTASSIUM. ICP METHOD Sample/ 1 1 Result LOD LQQ QA Flags Annual Milorganite Report January 1 to December 31, 2014 Analytical Method Lab 12/10/14 DM121,0114026198 4300 mg/kg D.W. 46 100' AO. SW846: 6010C MMSD 12/11/14 DM1211/14026217 4500 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/12/14 DM1212/14026232 5000 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/13/14 DM1213/14026243 5200 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/14/14 DM1214/14026262 5500 mg/kg D.W. 46 S00 AO. SW846: 6010C MMSD 12/15/14 DM1215/14026277 .5300 mg/kg D.W. 46 100 AO. SW846: 6010Q MMSD 12/16/14 DM1216/14026475 4200 mg/kg D.W. 46 100 SW846: 6010C MMSD 12/17/14 DM1217/14026503 4300 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/18/14 DM1218/14026522 4200 mg/kg D.W. 46 100 Q3. SW846: 6010C MMSD 12/19/14 DM1219/14026537 3800 mg/kg D.W. 46 100 SW846:,6010C MMSD 12/20/14 bM1220/14026653' '4100 mg/kg D.W. 46 100 SW846: 6010C MMSD 12/21/14 DM1221/14626672 3906 mg/kg D.W. 46 100 . _ SW846: 6010C MMSD 12/22/14 DM1222/14026685 3800 mg/kg D.W. 46 100 SW846: 6010C MMSD 12/23/14 DM1223/14026713 3800 mg/kg D.W: 46 100 SW846::6010C MMSD 12/24/14 DM1224/14026741 4200 mg/kg D.W. 46 100 SW846: 60]OC MMSD 12/25/14 DM1225/14026760 4000 mg/kg D.W. 46 100 SW846: 6010C MMSD 12/26/14 DM1226/14026777 4000 mg/kg D.W. 46 100 SW846: 6010C MMSD 12/27/14 DM1227/14026788 4100 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/28/14 DM1228/1.4026807 4200 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/29/14 DM1229/1:4027031 4100 mg/kg D.W. 46 100 AO. SW846: 6010C MMSD 12/30/14 DM1230/14027058 4400 mg/kg D.W. 46 100' SW846: 6010C MMSD 12/31/14 DM1231/14027086 4200 mg/kg D.W. 46 100 SW846: 6010C MMSD Avg: 4000 mg/kg D.W. Max: 5500 mg/kg D.W. 5Y5/rpt1M11bMonth/y 1110113 tj Page 80 of 106 Printed: 118115 10:48 r r i ��;, P'1119(}3 f fi A CAA wiviviv SELENIUM ICP METHOD Sample o.te Sample Io Result LOD LOQ QA Flags Annual Milorganite Report January 1 to December 31, 2014; Analytical MethodLab 01/01/14 DMO101/14000012 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 01/02/14 DMO102/14000039 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 01/03/14 DMO103/14000088 < 2.8 mg/kg D.W. 2.8 4 Q3. SW846: 6010C MMSD 01/04/14 DMO104/14000103 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 01/05/14 DMO105/14000122 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 01/06/14 DMO106/14000135 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 01/07/14 DMO107/14000162 < 2.8 mg/kg D.W. 2.8 4 B8. SW846:6010C MMSD 01/08/14 DMO108/14000188 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 01/09/14 DMO109/14000207 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 01/10/14 DMO110/14000430 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 01/11/14 DMO111/14000441 < 2.8 mg/kg D.W. 2.8 4 B7. SW846: 6010C MMSD 01/12/14 DMO112114000460 < 2.8 mg/kg D.W. 2.8 4 B7. SW846: 6010C MMSD 01/13/14 DM0113/14000473 < 2.8 mg/kg D.W. 2.8 4 B7. SW846: 6010C MMSD 01/14/14 DM0114/14000500 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 601bC MMSD 01/15/14 DM0115/14000526 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 01/16/14 DM0116/14000545 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 01/17/14 DM0117/14000560 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 01/18/14 DMO118/14000571 < 2.8 mg/kg D.W. 2.8 4 A0, B8. SW846: 6010C MMSD 01/19/14 DMO119/14000590 < 2.8 mg/kg D.W. 2.8 4 A0, B8. SW846: 6010C MMSD 01/20/14 DMO1210/14000603 < 2.8 mg/kg D.W. 2.8 4 A0, B8. SW846: 6010C MMSD 01/21/14 DMO121/14000630 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 01/22/14 DMO122/14000656 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 01/23/14 DMO123/14000675 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 01/24/14 DMO124/14000690 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 01/25/14 DMO125/14000923 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 01/26/14 DMO126/14000942 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 01/27/14 DMO127/14001095 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 01/28/14 DMO128114001122 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 01/29/14 DMO129/14001148 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 01/30/14 DMO130/14001167 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 01/31/14 DMO131/14001182 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/01/14 DM0201/14001193 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 02/02/14 DM0202/14001430 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 02/03/14 DM0203/14001443 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/04/14 DM0204/14001470 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/05/14 DM0205/14001498 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/06/14 DM0206114001517 < 2.8 mg/kg D.W. 2.8 4 BB, Q3. SW846: 6010C MMSD 02/07/14 DM0207114001532 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/08/14 DM0208/14001543 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 02/09/14 DM0209/14001562 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 02/10/14 DM0210/14001576 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/11/14 DM0211/14001811 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/12/14 DM0212/14001837 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/13/14 DM0213/14001856 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/14/14 DM0214/14001871 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/15/14 DM0215114001882 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 02/16/14 SYS/rptiNlIoMontMy DM0216/14001893 1110113 q < 2.8 mg/kg D.W. 2.8 4 68. SW846: 6010C MMSD Page 81 of 106 Printed., 1/8/1510:98 ti �dll1M[f3 (U� � Lll4vtk Gb�i�'NNfHf SELENIUM ICP METHOD Sample Date Sample ID 02/17/14 DM0217/14001914 Result < 2.8 mg/kg D.W. LOD 2.8 1 LOQ 4 QA Flagis B8, Q3. Annual Milorpnite Report January 1 to December 31, 2014 AnalAicail Method Lab SW846: 6010C MMSD 02/18/14 DM0218/14002002 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/19/14 DM0219/14002028 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 02/20/14 DM0220/14002101 < 2.8 mg/kg D.W. 2.8 4 _ B8, Q3. SW846: 6010C MMSD 02/21/14 DM0221/14002181 < 2.8 mg/kg D.W. 2.8 4 B8; Q3. SW846: 6010C MMSD 02/22/14 DM0222/14002192 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 02/23/14 DM6223/14002211 < 2.8 mg/kg D.W. 2.8 4 H. SW846: 6010C MMSD 02/24/14 DM0224/14002224 < 2:8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/25/14 DM0225/14002251 < 2,8 mg/kg D.W. 2.8 4 BB; Q3. SW846: 6010C MMSD 02/26/14 DM0226/14002310 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 02/27/14 DM0227/14002329 < 2.8 mg/kg D.W. 2.8 4 68, D2, Q3. SW846: 6010C MMSD 02/28/14 DM0228/14002350 < 2.8 mg/kg D.W. 2.8 4. ' SW846: 6010C MMSD 03/01/14 DM0301114002921 < 2:8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 03/02/14 bM0302/14002940 . < 2.8 mg/kg D.W.. 2.8 4 B8. SW846: 6010C MMSD 03/03/14 DM0303/14002953 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 03/04/14 DM0304/14002986 < 2.8 mg/kg D.W. 2.8 4' Q3. SW846: 6010C MMSD 03/05/14 DM0305/14003012 < 2.8 mg/kg D.W. 2.8 4 BB, D2, Q3. SW846: 6010C MMSD 03/06/14 DM0306/14003182 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 03/07/14 DM0307/14003197 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 03/08/14 DM0308/14003208 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 03/09/14 DM0309/14003232 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 03/10/14 DM0310/14003245 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 03/11/14 DM0311/14003272 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 03/12/14 DM0312/14003300 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 03/13/14 DM0313/14003871 . < 2.8 mg/kg D.W., 2.8 4 B8, Q3.. SW846:,6010C MMSD 03/14/14 DM0314/14003886 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 03/15/14 DM0315/14003899 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 03/16/14 DM0316/14003918 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 03/17/14 DM0317/14003936 . < 2.8 mg/kg D.W. 2.8 4 68, Q3. SW846:,6010C MMSD 03/18/14 DM0318/14003963 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 03/19/14 DM0319/14004217 < 2.8 mg/kg D.W. 2.8 4 BB, Q3. SW846: 6010C MMSD 03/20/14 DM0320/14004315 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 03/21/14 DM0321/14004330 < 2.8 mg/kg D.W. 2.8 4 B8, Q31 SW846: 6010C MMSD 03/22/14 DM0322/14004341 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 03/23/14 DM0323114004360 < 2.8 mg/kg D:W. 2.8 4 B8. SW846: 6010C MMSD 03/24/14 DM0324/14004461 < 2.8 mg/kg D.W. .2.8 4 B8, D2, Q3. SW846: 6010C MMSD 03/25/14 DM0325114004638 < 2.8 mg/kg D.W. 2.8 4 Q3. SW846: 6010C MMSD 03/26/14 DM0326/14004664 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 03/27/14 DM0327/14004683 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 03/28/14 D.M0328/14004698 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 03/29/14 DM0329/14004889 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 03/30/14 DM0330/14004908 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 03/31/14 DM0331/14004921 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/01/14 DM0401/14004948 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/02/14 DM0402/14004974 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 04/03/14 DM0403/14004993 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 04/04/14 DM0404/14005195 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD SYS/rptlMi/oMonth/y 1/10/13 tj Page 82 of 106 Printed: 1/8/1510:48 �� ' MSD t P.tBiNER3 EU4 A t1E1,4EfI Ek'Ef6iNNiM SELENIUM ICP METHOD samole Date Sample ID Result LOD LOQ IQA Pla f Annual Milorganite Report January 1 to December 31, 2014 Analytical Method 01/05711 DM0405/14005206 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C ;Lab 'MMSD 04/06/14 DM0406/14005226 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 04/07/14 DM0407/14005240 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/08/14 DM0408/14005267 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 04/09/14 DM0409/1.4005397 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 04/10/14 DM0410/14005416 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/11/14 DM0411/14005434 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846:, 6010'C MMSD 04/12/14 DM0412/14005605 < 2.8 mg/kg D.W. 2.8 4 AO, B8. SW846: 6010C MMSD 04/13/14 DM0413/14605627 < 2.8 mg/kg D.W. 2.8 4 AO, B8. SW846: 6010C MMSD 04/14/14 DM0414/14005641 < 2.8 mg/kg D.W. 2.8 4 AO, B8, Q3. SW846: 6010C MMSD 04/15/14 DM0415/14005668 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/16/14 DM0416/14005791 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 04/17/14 DM0417/i4005815 3.5 mg/kg D.W. 2.2 4 B9, I SW846: 6010C MMSD 04/18/14 DM0418/14006027 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/19/14 DM0419/14006038 2.6 mg/kg D.W. 2.2 4 B7, J. SW846: 6010C MMSD 04/20/14 DM0420/14006057 < 2.2 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 04/21/14 DM0421/14006127 2.5 mg/kg D.W. 2.2 4 B7, I SW846: 6010C MMSD 04/22/14 DM0422/14006154 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/23/14 DM0423/14006180 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/24/14 DM0424/14006339 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/25/14 DM0425/i4006354 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/26/14 DM0426114006365 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 04/27/14 DM0427/1.4006384 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 04/28/14 DM0428/14006397 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/29/14 DM0429/14006454 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 04/30/14 DM0430/14006482 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 05/01/14 DMO501114006976 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 05/d2/14 DM0502/14006991 < 2.8 mg/kg D.W. 2.8 4 B8, Q3. SW846: 6010C MMSD 05/03/14 DM0503/14007150 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 05/04/14 DM0504/14007169 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 05/05/14 DMO505114007182 < 2.8 mg/kg D.W. 2.8 4 B8. SW846: 6010C MMSD 05/06/14 DM0506/14007209 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 05/07/14 DMO507/14007235 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 05/08/14 DM0508/14007254 < 2.8 mg/kg D.W. 2.8 4 B8, D2, Q3. SW846: 6010C MMSD 05/09/14 DMO509/14007269 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 05/10/14 DM0510/14007280 IS mg/kg D.W. 2.2 4 B7, J. SW846: 6010C MMSD 05/11/14 DM0511/14007456, < 2.2 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 05/12/14 DM0512/14007469 < 2.2 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 05/13/14 DM0513/14007551 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 05/14/14 DM0514/14007577 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 05/15/14 DMO515/14007665 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 05/16/14 DMO516/14007680 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 05/17/14 DM0517/14007691 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 05/18/14 DM0518/14007710 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 05/19/14 DM0519/14007764 < 2.6 mg/kg D.W. 2.6 4 AO, B8, D2, Q3. SW846: 6010C MMSD 0S/20/14 DM0520/14007997 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 05/21/14 DMO521/14008023 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD SYS/rptlMi/oMonth/y 1110113 OF Page 83 of 106 Printed. • 11811510.48 Annual Milorganite Report January 1 to December 31, 2014 P,+.AiM(F2 fGi 9 ClE�sfii f�il�;#NINI SELENIUM ICP METHOD Sample 'Date SamplelD Res6ft OD b5j22/14 DM0522/14008042 3.4 mg/kg D.W. 2.2 4 B7, I SW846: 6010C MMSD nrn�i,n nnena,),�i1AnnsnG7 I r -A- n Xh/ 1) r 4 aR 01. SW846: 6010C MMSD 05/25/14 DM0525/14008310 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 05/26/14 DMO526/14008323 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 05/27/14 DM0527/14008646 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3... SW846: 6010C MMSD 05/28/14 DM0528/14008672 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD OS/29/14 DMO529/14008691 < 2.6 mg/kg D.W. 2.6 4.. B8, Q3. SW846: 6010C MMSD 05/30/14 DM0530/14008845 3:3 mg/kg D.W. 2.2 4 J. SW846: 6010C MMSD 05/31/14 DM0531/14008856 4.7 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/01/14 DM0601/14009580 2.7 mg/kg D.W. 2.2 4 B7, J. SW846: 6010C MMSD 06/02/14 DM0602/14.009593 4:6 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/03/14 DM0603/14009620 4.1 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/04/14 DM0604/14009635 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 06/05/14 DM0605/14009654 < 2.6 mg/kg D.W. 2.6 4 AO, B8, Q2: SW846: 6010C MMSD 06/06/14 DM0606/14009669 < 2.6 mg/kg D.W. 2.6 4 'AO, Q2. SW846: 6010C MMSD 06/07/14 DM0607/14009844 < 2.6 mg/kg D.W. 2.6 4 AO. SW846: 6010C MMSD 06/08/14 bM0608/14009867 < 2.6 mg/kg D.W. 2.6 4 AO. SW846: 6016C MMSD 06/09/14 DM0609/14009880 < 2.6 mg/kg D.W. 2.6 4 AO. SW846: 6010C MMSD 06/10/14 DM0610/14009907 < 2.6 mg/kg D.W. 2.6 4 AO, BB, Q2. SW846: 6010C MMSD 06/11/14 DM0611/14010237 4.9 mg/kg D.W. 2.2 4 67. SW846: 6010C MMSD 06/12/14 DM0612/14010256 2.6 mg/kg D.W. 2.2 4 B7, J. SW846: 6010C MMSD 06/13/14 DM0613/14010271 < 2.2 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/14/14 DM0614/14010282 2.7 mg/kg D.W. 2.2 4, B7, J. SW846: 6010C MMSD 06/15/14 DMO615/14010301 4.3 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/16/14 DMO616/14010319 2.3 mg/kg D.W. 2.2 4 B7, J. SW846: 6016c MMSD 06/17/14 DM0617/14010346 < 2.2 mg/kg D.W. 2.2 4 B8. SW846: 6010C MMSD 06/18/14 DM0618/14010687 5.1 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/19/14 DM0619/14010706 3.2 mg/kg D.W. 2.2 4 B7, J. SW846: 6010C MMSD 06/20/14 DM0620/14010721 5.3 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/21/14 DM0621/14010732 5.3 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/22/14 DM0622/14010751 5.9 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/23/14 DM0623/14011513 4.8 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/24/14 DM0624/14011540 3 mg/kg D.W. 2.2 4 B7, J. SW846: 6010C MMSD . 06/25/14 DMO625/144011566 4,8 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/26/14 DM0626/14011766 3.1 mg/kg D.W. 2.2 4 B7, J. SW846: 6010C MMSD 06/27/14 DM0627/14011781 4.2 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 06/28/14 DM0628114011792 < 2.2 mg/kg D.W. 2.2 4- B7. SW846: 6010C MMSD 06/29/14 DMO629/14011811 4:9 mg/kg D.W. 2.2 4 " B7. SW846: 6010C MMSD 06/30/14 DM0630/14011824 4 mg/kg D.W. 2.2 4 B7, J. SW846: 6010C MMSD 07/01/14 DM0701/14011851 4.1 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 07/02/14 DM0702/14011879 3.4 mg/kg D.W. 2.2 4 _ ; J. SW846: 6010C MMSD 07/03/14 DM0703/14011898 4.2 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 07/04/14 bM0704/14011911 < 2.2 mg/kg D.W. 2.2 4 B8. SW846: 6010C MMSD 07/05/14 DM0705/14011924 < 2.2 mg/kg D.W. 2.2 4 B8. SW846: 6010C MMSD 07/06/14 DM0706/14011943 < 7.2 mg/kg D.W. 2.2 4 B8. SW846: 6010C MMSD 07/07/14 DM0707/14012196 < 2.2 mg/kg D.W. 2.2 4 B8. SW846: 6010C MMSD SY5/rptiMi/oMonth/y 1/10/13 4i Page 84 of 106 Printed., 1/8/1510:4B M S D PdRiafk3 fUiA CtWip (ylfV401 SELENIUM ICP METHOD Sample Date Sample ID Result LOD LOQ .. Flags Annual Milorganite Report January 1 to December 31, 2014 Analytical Method Lab 07/08/14 DM0708/14012898 3.5 mg/kg D.W. 2.2 4 B8, J. SW846: 6010C MMSD 07/09/i4 D100709/14012926 4.4 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 07/10/14 DM0710/14012945 4.4 mg/kg D.W. 2.2 4 SW846: 6010C MMSD 07/11/14 DM0711/14012961 2.8 mg/kg D.W. 2.2 4 J. SW846: 6010C MMSD 07/12/14 DM0712/14012971 < 2.6 mg/kg D.W. 2.6 4 A0, B8. SW846: 6010C MMSD 07/13/14 DM0713/14012991 < 2.6 mg/kg D.W. 2.6 4 A0, B8. SW846: 6010C MMSD 07/14/14 DM0714/14013004 < 2.6 mg/kg D.W. 2.6 4 A0, B8, Q3. SW846: 6010C MMSD 07/15/14 DM0715/14013031 < 2.6 mg/kg D.W. -2.6 4 A0, B8, Q3. SW846: 6010C MMSD 07/i6/14 DM0716/14013059 < 2.6 mg%kg D.W. 2.6 4 A0, M, Q3. SW846: 6010C MMSD 07/17/14 DM0717/14013078 < 2.6 mg/kg D.W. 2.6 4 A0, 88, Q3. SW846: 6010C MMSD 07/18/14 DM0718/14013295 < 2.6 mg/kg D.W. 2.6 4 A0, B8, Q3. SW846:.6010C MMSD 07/19/14 DM0719/14013305 < 2.6 mg/kg D.W. 2.6 4 A0, B8. SW846: 6010C MMSD 07/20/14 DM0720/14013324 < 2.6 mg/kg D.W. 2.6 4 A0, B8. SW846: 6010C MMSD 07/21/14 DM0721/14013337 < 2.6 mg/kg D.W. 2.6 4 A0, B8, Q3. SW846: 6010C MMSD 07/25/14 DM0725/14013997 < 2.6 mg/kg D.W. 2.6 4 A0, B8, Q3. SW846: 6010C MMSD 07/26/14 DM0726/14014008 < 2.6 mg/kg D.W. 2.6 4 A0, B8. SW846: 6010C MMSD 07/27/14 DM0727114014027 < 2.6 mg/kg D.W. 2.6 4 A0, B8. SW846: 6010C MMSD 07/28/14 DM0728/14014040 < 2.6 mg/kg D.W. . 2.6 4 A0, B8, Q3. SW846: 6010C MMSD 07/29/14 DM0729/14014895 < 2.6 mg/kg D.W. 2.6 4 A0, B8, Q3. SW846: 6010C MMSD 07/30/14 DM0730/14014923 < 2.6 mg/kg D.W. 2.6 4 A0, B8, Q3. SW846: 6010C MMSD 07/31/14 DM0731/14014942 < 2.6 mg/kg D.W. 2.6 4 A0, B8, Q3. SW846: 6010C MMSD 08/01/14 DMO801/14014957 < 2.6 mg/kg D.W. 2.6 4 A0, B8, Q3. SW846: 6010C MMSD 08/02/14 DM0802/14014968 < 2.2 mg/kg D.W. 2.2 4 SW846: 6010C MMSD 08/03/14 DM0803/14014987 4 mg/kg D.W. 2.2 4 J. SW846: 6010C MMSD 08/04/14 DMO864/14015000 4 mg/kg D.W. 2.2 4 SW846: 6010C MMSD 08/05/14 DM0805/14015027 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 08/06/14 DM0806/14015405 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 08/07/14 DMO807/14015456 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 08/08/14 DM0808/14015471 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 08/09/14 DMO809/14015482 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 08/10/14 DM0810/14015966 < 2.6 mg/kg D.W. 2.6 4, B8. SW846: 6010C MMSD 08/11/14 DM0811114015984 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 08/12/14 DMO812/14016011 < 2.6 mg/kg D.W. .'2.6 4 B8, Q3. SW846: 6010C MMSD 08/13/14 DM0813/14016039 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 08/14/14 DM0814/14016058 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 08/1S/14 DMO815/14016181 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD. 08/16/14 DMO816/14016192 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 08/17/14 DMO817/14016211 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 08/18/14 DM0818/14016290 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 08/19/14 DMO819/14016319 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 08/20/14 DM0820/14016347 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 08/21/14 DM0821/14016366 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 08/22/14 DMO822/14016381 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 08/23/14 DM0823/14016892 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 08/24/14 DM0824/14016411 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 08/25/14 DM0825/14016488 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 08/26/14 DM0826/14016515 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 5Y5/rpt1M11bXonth1y 1110113 tj Page 85 of 106 Printed.• 1/8/1510.48 "AMSD tl PAkINIPS f�4A CLEtttR [lilEdHHiNi SELENIUM. ICP METHOD Sample Date �Sample ID Result LOD LO I Q QA Flags Annual Milorganite Report January 1 to December 31, 2014 Analytical Method Lab. 08/28/14 DM0828/14016907 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 08/29/14 DM0829/14017671 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 08/30/14 DMO830/14017682 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 08/31/14 DM0831/14017701 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 09/O1/14 DM0901/14017714 < 2.6 mg/kg D:W. 2.6 4 B8. SW846: 6010C MMSD 09/02/14 DM0902/14017871 < 2.6 mg/kg D.W. 2.6 4 68, D2, Q3. SW846: 6010C MMSD 09/03/14 DMO903/14017886 _ < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 09/04/14 DMO904/14017920 < 2.6 mg/kg DX 2.6 4. BB, D2, Q3. SW846: 6010C MMSD 09/05/14 DMO905/1401790.1 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 09/16/14 DMO916/14019167. < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 09/17/14 DM0917/14019195 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 09/18/14 DMO918/14019229 < 2.6 mg/k9 D.W. 2.6 4 _ : B8, Q3. SW846: 6010C MMSD 09/19/14 DM0919/14019244 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 09/20/14 DM0920/14019255 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 09/21/14 DMO921/14019274 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 09/22/14 DMO922114019287 < 2.6 mg/kg D,W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 09/23/14 DMO923/14019778 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 09/24/14 DM0924/14019806 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 09/25/14 DM0925/14019825 < 2.6 mg/kg D.W. 2.6 4 68, Q3. SW846: 6010C MMSD 09/26/14 DMO926/14019840 < 2.6 ing/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 09/27/14 DMO927/14019851 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 09/28/14 DM0928/14019870 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 09/29/14 DMO929/14019883 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 09/30/14 DMO930/14019909 < 2.6 mg/kg D.W. 2.6 4 Q3. SW846: 6010C MMSD 10/O1/14 DM1.001/14019927 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846:.6010C MMSD 10/02/14 DM1'002/14020572 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 10/03/14 DM1003/14020587 < 2.6 mg/kg D.W. 2.6 4. B8, Q3. SW846: 6010C MMSD 10/04/14 DM1004/14020598 5.3 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 10/05/14 DM1005/14020617 3.9 mg/kg D.W. 2.2 4 B7,,3. SW846: 6010C MMSD 10/06/14 DM1006/14020630 4.6 mg/kg D.W. 2.2 4 B7. SW846: 6010C MMSD 10/07/14 DM1007/14021108 2.3 mg/kg D.W. 2.2 4 B7, ]. SW846: 6010C MMSD 10/08/14 DM1008/14021160 3.8 mg/kg D.W. 2.2 4 B8. SW846: 6010C MMSD 10/09/14 DM1009/14021179 2.7 mg/kg D.W: 2.2 4 B8, J. SW846: 6010C MMSD 10/10/14 DM1010/14021194 3.7 mg/kg D.W. 2.2 4 SW846: 6010C MMSD 10/11/14 DM1011/14021244 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 1O/12/14 DM1012/14021263 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 10/13/14 DM1013/14021276 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 10/14/14 DM1014/14021304 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 1O/1.5/14 DM1015/14021332 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 10/16/14 DM1016/14021351 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 10/17/14 DM1017/14021787 . < 2.6 mg/kg D.W. 2.6 4 BB, D2, Q3. SW846: 6010C MMSD 10/18/14 DM1018114021798 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 10/19/14 DM1019/1402181,7 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 10/20/14 DM1020/14021830 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 10/21/14 DM1021/14021857 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 10/22/14 DM1022/14021885 < 2.6 mg/kg D.W. 2.6 4' B8, Q3. SW846: 6010C MMSD 10/23/14 DM1023/14022256 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD SYS/rptlMi/oMonthly 1/10/13 h' Page 86 of 106 Printed.,11811510.48 M S D AiK1KENS f [r3 A CIED,itR ❑'JIG�KklIHi SELENIUM ICP METHOD o.te Sample Io Result LOD LQQ e• Flag s Annual Milorganite Report January 1 to December 31, 2014 Analytical Metttod Lab 10/24/14 DM1024/14022273 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 10%25/14 DM1025/14022286 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 10/26/14 DM1026/14022305 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 10/27/14 DM1027/14022318 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 10/28/14 DM1028/14022409 < 2.6 rrig/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 10/29/14 DM1029/14022439 < 2.6 mg/kg D.W. 2.6 4 68, Q3. SW846: 6010C MMSD 10/30/14 DM1030/14022510 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 10/31/14 DM1031/14,022525 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 11/01/14 DM1101/14022536 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/02/14 DM1102/14022555 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/03/14 DM1103/14022568 < 2.6 mg/kg D.W. 2.6 4 68, Q3. SW846: 6010C MMSD 11/04/14 DM1104/14,023111 < 2.6 rrig/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/05/14 DM1105/14023139 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 11/06/14 0101106/14023158 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 11/07/14 DM1107/14023173 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6016C MMSD 11/08/14 DM1108/14023184 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/09/14 DM1109/14023203 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/10/14 DM1110/14023767 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 11/11/14 DM1111/14.023796 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/12/14 DM1112114023876 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 11/13/14 DM1113114023895 < 2.6 mg/kg D.W. 2.6 4 68, Q3. SW846: 6010C MMSD 11/14/14 DM1114/14023910 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 11/15/14 DM1115/14023929 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/16/14 DM1116/14023948 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/17/14 DM1117114023961 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3, SW846: 6010C MMSD 11/18/14 DM1118/14024236 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD .11/19/14 DM1119/14024264 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 11/20/14 DM1120/14024283 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 11/21/14 DM1121/14024302 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/22/14 DM1122/14024313 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/23/14 DM1123/14024393 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/24/14 DM1124/14024414 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 11/25/14 DM1125/14024441 < 2.6 mg/kg D.W. 2.6 4 B8, Q3: SW846: 6010C MMSD 11/26/14 DM1126/14024469 <, 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/27/14 DM1127/14024529 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/28/14 QM1128/14024544 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 11/29/14 DM1.129/14024555 < 2.6 mg/kg D.W. 2.6 .: 4 B8. SW846: 6010C MMSD 11/30/14 DM1130/14024574 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 12/01/14 DM1201/14024601 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 12/02/14 DM1202/14025299 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 12/03/14 DM1203/14025327 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 12/04/14 DM1204/14025346 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 12/05/14 DM1205/14025361 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 12/06/14 DM1206/14025372 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 12/07/14 DM1207/14025391 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 12/08/14 DM1208/14025404 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 12/09/14 DM1209/14026170 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 5Y5/rpt.tR!1oMonth1y 1110113 tj Page 87 of 106 Printed: 1/8/1510:48 1 1 ;-; '- D PAIN S 1W 1 CLL1XR BRIMMNINT SELENIUM ICP METHOD Sample 1- Sample ID Result LOD LOQ QA Flags Annual Milorganite Report January 1 to December 31, 2014 Analytical Method Lab 12/10/14 DM1210/14026198 < 2.6 mg/kg D:W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 12/11/14 DM1211/14026217 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3. SW846: 6010C MMSD 12/12/14 DM1212/14026232 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 12/13/14 DM1213/14026243 < 2.6 mg/kg D.W. 2.6 4 88. SW846: 6010C MMSD 12/14/14 DM1214/14026262 < 2.6 mg/kg D.W. 2.6 4, 'B8. SW846: 6010C MMSD 12/15/14 DM1215114026277 < 2.6 mg/kg D.W. 2.6 4 B81 D2,.Q3: SW846: 6010C MMSD 12/16/14 DM1216/14026475 < 2.6 mg/kg D.W. 2.6 4 B8, D2. SW846: 6010C MMSD 12/17/14 DM1217/14026503 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 12/18/14 DM1218/14026522 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 12/19/14 ... DM1219/14026537 < 2.6 mg/kg D.W. 2.6 4 B8, Q3. SW846: 6010C MMSD 12/20/14 DM1220/14026653 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 12/21/14 DM1221/14026672 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 12/22/14 DM1222/14026085 < 2.6 mg/kg D.W. 2.6 4 B8, D2. SW846: 6010C MMSD 12/23/14 DM1223/14026713 < 2.6 mg/kg D.W. 2.6 4 B8, D2, Q3.. SW846: 6010C MMSD 12/24/14 DM1224/14026741 < 2.6 mg/kg D.W. 2.6 4 B8. SW846: 6010C MMSD 12/251/14 DM1225/14026760 < 2.6 mg/kg D.W. 2.6 4:' B8. SW846: 6010C MMSD 12/26/14 DM1226/14026777 < 2.6 mg/kg D.W. 2.6 4 B8, D2., SW846: 6010C MMSD 12/27/14 0M1227/14026788 3.6 mg/kg D.W.. 2.2 4 B8, J. SW846: 6010C MMSD 12/28/14 DM1228/14026807 < 2.2 mg/kg D.W. 2.2 4 BB. SW846: 6010C MMSD 12/29/14 DM1229/14027031 4.3 mg/kg D.W. 2.2 4 B8. SW846: 6010C MMSD 12/30/14 DM1230/14027058 3.7 mg/kg D.W. 2.2 4 B7, J. SW846: 6010C. MMSD 12/31/14 DM1231/14027086 < 2.6 mg/kg D.W. 2.6 4 SW846: 6010C MMSD Avg: 0.51 mg/kg D.W. Max: 5.9 mg/kg D.W. Page 88 of 106 SYS/rptSMi/oMonth/y 1110113 tf Printed: 11811510:48 MSD PA11IiiS IN A. CLUMR Lf,ION(Ni Solids (% Moisture) Sample Date Sample ID Result LOD LOQ Q• Flags Annual Milorganite Report January 1 to December 31, 2014 Daily Composite 01/01/14 DM0101/14000012 5.4 % 0.1 0.33 SM(20) 254OG MMSD 01/02/14 DMO102/14000039 6.8 % 0.1 0.33 SM(20) 254OG MMSD 01/03/14 DMO103/14000088 5.8 % 0.1 0.33 SM(20) 254OG MMSD 01/04/14 DMO104/14000103 6.2 % 0.1 0.33 SM(20) 2540G MMSD 01/05/14 DMO105/14000122 7.3 % 0.1 0.33 SM(20) 2540G MMSD 01/06/14 DMO106/14000135 7.7 % 0.1 0.33 SM(20) 254OG MMSD 01/07/14 DMO107/14000162 6 % 0.1 0.33 SM(20) 254OG MMSD 01/08/14 DM0108/14000188 5.3 % 0.1 0.33 SM(20) 2540G MMSD 01/09/14 DMO109/14000207 6.7 % 0.1 0.33 SM(20).2540G MMSD 01/10/14 DM0110/14000430 6.3 % 0.1 0.33 SM(20) 2540G MMSD 01/11/14 DM0111/14000441 5.3 % 0.1 0.33 SM(20) 254OG MMSD 01/12/14 DM0112/14000460 5.5 % 0.1 0.33 SM(20) 2540G MMSD 01/13/14 DM0113/14000473 5.6 % 0.1 0.33 SM(20) 254OG MMSD 01/14/14 DM0114/14000500 5.2 % 0.1 0.33 SM(20) 254OG MMSD 01/15/14 DMO115/14000526 5.8 % 0.1 0.33 SM(20) 254OG MMSD 01/16/14 DM0116/14000545 4.7 % 0.1 0.33 SM(20) 254OG MMSD 01/17/14 DM0117/14000560 5.3 % 0.1 0.33 SM(20) 2540G MMSD 01/18/14 DM0118/14000571 6.4 % 0.1 0.33, SM(20) 254OG MMSD 01/19/14 D100119/14000590 5.9 % 0.1 0.33 D1. SM(20) 254OG MMSD 01/20/14 DMO120/14600603 5.4 % 0.1 0.33 SM(20) 254OG MMSD 01/21/14 DMO121/14000630 6.9 % 0.1 0.33 SM(20) 254OG MMSD 01/22/14 DMO122/14000656 8.1 % 0.1 0.33 SM(20) 254OG MMSD Ol/23/14 DMO123/14000675 7.5 % 0.1 0.33 SM(20) 2540G MMSD 01/24/14 DMO124/14000690 6 % 0.1 0.33 SM(20) 254OG MMSD 01/25/14 01/26/14 DMO125/14000923 DMO126/14000942 7 % 8 % 0.1 . 0.1 0.33 0.33 SM(20) 2540G SM(20) 2540G MMSD MMSD 01/27/14 DMO127114001095 8.1 % 0.1 0.33 SM(20) 254OG MMSD 01/28/14 DMO128/14001122 5.7 % 0.1 0.33 SM(20) 254OG MMSD 01/29/14 DMO129/14001148 4 % 0.1 0.33 DI. SM(20) 254OG MMSD 01/30/14 DMO130/14001167 3.6 % 0.1 0.33 SM(20) 254OG MMSD 01/31/14 DMO131/14001182 4.1 % 0.1 0.33 SM(20) 254OG MMSD 02/01/14 DM0201/14001193 6.3 % 0.1 0.33 SM(20) 254OG MMSD 02/02/14 DM0202/14001430 6.4 % 0.1 0.33 SM(20) 254OG MMSD 02/03/14 DM0203/14001443 5.7 % 0.1 0.33 SM(20) 254OG MMSD 02/04/14 DM0204/14001470 7.5 % 0.1 0.33 SM(20) 2540G MMSD 02/05/14 DM0205/14001498 3.9 % 0.1 0.33 SM(20) 254OG MMSD 02/06/14 DM0206/14001517 4.1 % 0.1 0.33 SM(20) 254OG MMSD 02/07/14 DM0207/14001532 7.4 % 0.1 0.33 SM(20) 2540G MMSD 02/08/14 DM0208/14001543 6.4 % 0.1 0.33 SM(20) 254OG MMSD 02/09/14 DM0209/14001562 6.5 % 0.1 0.33 SM(20) 254OG MMSD 02/10/14 DM0210/14001576 6.8 % 0.1 0.33 SM(20) 2540G MMSD 02/11/14 DM0211/14001811 4.7 % 0.1 0.33 SM(20) 2540G MMSD 02/12/14 DM0212/14001837 6.9 % 0.1 0.33 SM(20) 2540G MMSD 02/13/14 DM0213114001856 6.3 % 0.1 0.33 SM(20) 254OG MMSD 02/14/14 DM0214/1400187.1 7.1 % 0.1 0.33'' SM(20) 2540G MMSD 02/15/14 DM0215/14001882 6.6 % 0.1 0.33 SM(20) 254OG MMSD SYSIrptlMi/oMonthiy 1110113 tJ Page 89 of 106 Printed,11811510-48 J •� PARTNO IRA CI1mg EaAF/AWIRi Solids (% Moisture) Sample .. 02/16/14 DM021,6/14001893 5.5 % .o 0.1 LOQ .. Flags 0.33 Annual Milorganite Report January 1 to December 31, 2014 Analytical Method Lab SM(20) 254OG MMSD 02/17/14 DM0217/14001914 6 % 0.1 0.33 SM(20) 254OG MMSD 02/18/14 DM0218/14002002 6 % 0.1 0.33 SM(20) 2540G MMSD 02/19/14 DM0219/14002028 7.3 % 0.1 0.33 SM(20) 254OG MMSD 02/20/14 DM0220/1400210'.1 5.5 % 0.1 0.33 SM(20) 254OG MMSD 02/21/14 DM0221/14002181 5.9 % .0.1 0.33 SM(20) 2540G. MMSD 02/22/14 DM0222/14002192 8 % 0:1 0.33 SM(20) 2540G MMSD 02/23/14 DM0223/14002211 3.2 % 0.1 0.33 SM(20) 254OG MMSD 02/24/14 DM0224/14002224 6 % 0.1 0.33 SM(20) 254OG MMSD 02/25/14 OM0225/14002251 6.1 % 0.1 0.33 SM(20) 254OG MMSD 02/26/14 DM0226/14002310 5.7 % 0.1 0.33 SM(20) 254OG MMSD 02/27/14 DM0227/14002329 6.8 % 0.1 0.33 SM(20) 254OG MMSD 02/28/14 DM0228/14002350 6.5 % 0.1 0.33 SM(20) 254OG MMSD 03/01/14 DM0301/14002921 5.1 % 0.1 0.33 SM(20) 2540G MMSD 03/02/14 DM0302/14002940 5.9 % 0.1 0.33 SM(20) 2540G MMSD 03/03/14 DM0303/14002953 5.1 % 0.1 0.33 SM(20) 254OG MMSD 03/04/14 DM0304/14002986 5 % 0.1 0.33 SM(20) 2540G MMSD 03/05/14 DM0306/14003012 7.4 0% 0.1 0.33 SM(20) 2540G MMSD 03/06/14 DM0306114003182 6.1 % 0.1 0.33 SM(20) 254OG MMSD 03/07/14 DM0307/14003197 6.9 % 0.1 0.33 SM(20) 254OG MMSD 03/08/14 DMO308/14003208 8.2 % 0.1 0.33 SM(20) 2540G MMSD 03/09/14 DM0309/14003232 5.7 % 0.1 0.33 SM(20) 254OG MMSD 03/10/14 DM031.0/14003245 6.2 % 0.1 0.33 SM(20) 2540G MMSD 03/11/14 DM031.1/1;4003272 7.5 % 0.1 0.33 SM(20) 254OG MMSD 03/12/14 DM0312/14003300 4.8 % 0.1 0.33 SM(20) 2540G MMSD 03/13/14 DM0313/14003871 3.1 % 0.1 0.33 SM(20) 254OG MMSD 03/14/14 DM0314/14003886 4.2 % 0.1 0.33 SM(20) 2540G MMSD 03/15/14 DM0315/1'4003899 7.6 % 0.1 0.33 SM(20) 2540G MMSD 03/16/14 DM0316/14003918 4.5 % 0.1 0.33 SM(20) 2540G MMSD 03/17/14 DM0317/14003936 7.5 % 0.1 0.33 SM(20) 254OG MMSD 03/18/14 DM0318/14003963 6.9 % 0.1 0.33 SM(20) 2540G MMSD 03/19/14 DM0319/14004217 4.1 % 0.1 0.33 SM(20) 254OG MMSD 03/20/14 DM0320/14004315 6.2 % 0.1 0.33 SM(20) 2540G MMSD 03/21/14 DM0321/14004330 5.2 % 0.1 0.33 SM(20) 254OG MMSD 03/22/14 DM0322/14004341 4.3 % 0.1 0.33 SM(20) 2540G MMSD 03/23/14 DM0323/14004360 4.7 % 0.1 0.33 SM(20) 2540G MMSD 03/24/14 DM0324/14004461 3.7 % 0.1 0.33 SM(20) 254OG MMSD 03/25/14 DM0325/14004638 4 % 0.1 0.33 . SM(20) 2540G MMSD 03/26/14 DM0326/14004664 5.5 % 0.1 0.33' SM(20) 254OG MMSD 03/27/14 DM0327/14004683 4.1 % 0.1 0.33 SM(20) 2540G MMSD 03/28/14 DM0328/14004698 4 % 0.1 0.33 SM(20) 254OG MMSD 03/29/14 DM0329/14004889 5.1 % 0.1 0.33 SM(20) 254OG MMSD 03/30/14 DM0330/14004908 3.2 % 0.1 0.33 SM(20) 2540G MMSD 03/31/14 DM0331/14004921 3.4 % 0.1 0.33 SM(20).2540G MMSD 04/01/14 DM0401/14004948 3.4 % 0.1 0.33 SM(20) 2540G MMSD 04/02/14 DM0402/14004974 7.4 % 0.1 0.33 SM(20) 2540G MMSD 04/03/14 DM0403/14004993 6.9 % 0.1 0.33 SM(20) 2540G MMSD SYS/rptimoMonthty 1/10/13 tj Page 90 of 106 Printed.,1/8/1510.48 ; " ,� i'MS-D .... pmg,if51DIACaw LYIIit, Kw I Solids (% Moisture) Sample Date Sample ID Result LOD LOQ � � r Anliu ' l Milorganite Report January 1 to December 31, 2014: Lab 04/04/14 DM0404/14005195 5.2 % 0.1 0.33. SM(20) 254OG MMSD 04/05/14 DM0405/14005206 4.2 % 0.1 0.33 SM(20) 2540G MMSD 04/06/14 DM0406/14005226 7.8 % 0.1 0.33 SM(20) 254OG MMSD 04/97/14 DM0407/14005240 5.7 % 0.1 0.33 SM(20) 254OG MMSD 04/08/14 DM0408/14005267 5.9 % 0.1 0.33 SM(20)2540G MMSD 04/09/14 DM0409/14005397 6.2 % 0.1 0.33 SM(20) 2540G., MMSD' 04/10/14 DM0410/14005416 5.8 % 0.1 0.33 SM(20) 2540G MMSD 04/11/14 DM0411/14005434 6.2 % 0.1 0.33 SM(20) 2540G MMSD 04/12/14 DM0412/14005605 6.1 % 0.1 0.33 SM(20) 2540E MMSD 04/13/14 DM0413/14005627 4.2 % 0.1 0.33 SM(20)254OG MMSD 04/14/14 DM0414/14005641 6.8 % 0.1 0.33 SM(20) 2540G MMSD 04/15/14 DM0415/14005668 7.6 % 0.1 0.33 SM(20) 2540G MMSD 04/16/14 DM0416/14005791 9.1' % 0.1 0.33 SM(20) 2540E MMSD 04/17/14 DM0417/14005815 8 % 0.1 0.33 SM(20) 2540G MMSD 04/18/14 DM0418/14006027 9.4 % 0.1 0.33 SM(20) 254OG MMSD 04/19/14 DM0419/14006038 8.9 % 0.1 0.33 SM(20) 254OG MMSD 04/20/14 DM0420/14006057 4.7 % 0.1 0.33 SM(20) 254OG MMSD 04/21/14 DM0421/14006127 . 6.3 % 0.1 0.33 SM(20) 254OG MMSD 04/22/14 DM0422/14006154 4.4 % 0.1 0.33 SM(20) 254OG MMSD 04/23/14 DM0423/14006180 6.4 % 0.1 0.33 SM(20) 2540G MMSD 04/24/14 QM0424/14006339 6.4 % 0.1 0.33 SM(20) 2540G. MMSD 04/25/14 DM0425/14006354 . 5.3 % 0.1 0.33 SM(20) 254OG MMSD 04/26/14 DM0426114.006365 4.7 % 0.1 0.33 . . SM(20) 2546G MMSD 04/27/14 DM0427/14006384 5.2 % 0.1 0.33 SM(20) 254OG MMSD 04/28/14 QM0428/14006397 4.2 % 0.1 0.33 SM(20) 254OG MMSD 04/29/14 DM0429114006454 - 4.8 % 0.1 0.33 SM(20) 2540E MMSD 04/30/14 DM0430/14006482 4.9 % 0.1 0.33 SM(20) 254OG MMSD .' OS/01/14 D100501/14006976 3.7 % 0.1 0.33 SM(20) 254OG MMSD ' 05/02/14 DMO502/14006991 4.9 % 0.1 0.33 SM(20) 2540G" MMSD 05/03/14 DMO503114007150 7.8 % 0.1 0.33 SM(20) 254OG MMSD 05/04/14 DM0504/14007169 4.4 % 0.1 0.33 SM(20) 2540G MMSD OS/05/14 DM05051/14007182 4.5 % 0.1 0.33 SM(20) 254OG MMSD 05/06/14 DM0506/14007209 6.8 % .'0.1 0.33 SM(20)254OG MMSD 05/07/14 DM0507/14007235 7.1 % 0.1 0.33 SM(20) 2540G MMSD 05/08/14 DM0508/14007254 9.4 % 0.1 0.33. SM(20) 254OG MMSD 05/09/14 DM0509/14007269 6.7 % ... 0.1 0.33 SM(20) 2540G MMSD 05/10/14 DM0510/14007280 4.1 % 0,1 0.33 SM(20) 2540G MMSD 05/11/14 DM0511/1,4007456 6.6 % 0.1 0.33 SM(20) 254OG MMSD 05/12/14 DM0512/14007469 7.2 % 0.1 0.33' SM(20)254OG MMSD 05/13/14 DM0513/14007551 5.6 % 0.1 0.33 SM(20) 2540G. MMSD 05/14/14 DM0514/14007577 ' 5.4 0% 0.1 0.33 SM(20) 254OG MMSD 05/15/14 DM0515/14007665 4.8 % 0.1 0.33 SM(20) 254OG MMSD 05/16/14 DM0516/14007680 4.5 % 0.1 0.33 SM(20) 2540G MMSD OS/17/14 DM0517114007691 6.1 % 0.1 0.33 SM(20) 254OG. MMSD 05/18/14 DM0518/14007710 6.8 % 0.1 0.33 SM(20) 254OG MMSD 05/19/14 DM0519/14607764 7.5 % 0.1 0.33 SM(20) 2540G MMSD 05/20/14 DM0520/14007997 7.8 % 0.1 0.33 „ SM(20) 254OG MMSD SYS/rptlMilaMonthly 1/10/13 tj Page 91 of 106 Printed.11811510.48 L • ., MSD pjnfP in A ILWtR [R wiHw[w, Solids (% Moisture) Sample Date Sample ID 05/21/14 DM0521/14008023 Result 5.8 % LOD 0.1 LOQ QA Flags 0.33 Annual Milorganite Report :January 1 to December 31, 2014 Analytical Method Lab SM(20) 254OG MMSD 05/22/14 DMO522/14008042 4 % 0.1 0.33 SM(20) 2540G MMSD 05/23/14 DMO523/14008057 4.2 % 0.1 0.33 SM(20) 2540G MMSD 05/24/14 DM0524/14008291 6.1 % 0.1 0.33 SM(20) 254OG MMSD 05/25/14 DM0525/14008310 7.2 % 0.1 0.33 SM(20) 2540G MMSD 05/26/14 DM0526/14008323 6 % 0.1 0.33 SM(20) 2540G, MMSD OS/27/14 DM0527/14008646 6.2 % 0.1 0.33 SM(20) 254OG MMSD 05/28/14 DM0528/14008672 5.4 % 0.1 0.33 SM(20) 254OG MMSD 05/29/14 DM0529/14008691 5.3 % 0.1 0.33 SM(20) 254OG MMSD 05/30/14 DM0530/14008845 6.6 % 0.1 0.33 SM(20) 2540G MMSD 05/31/14 DM0531/14008856 5.6 % 0.1 0.33 SM(20) 2540G MMSD 06/01/14 DM0601/14009580 6.1 % 0.1 0.33 SM(20) 2540G MMSD 06/02/14 DM0602/14009593 7 % 0.1 0.33 SM(20) 254OG MMSD 06/03/14 DM0603/14009620 7.1 % 0.1 0.33 SM(20) 254OG MMSD 06/04/14 DMO604/14009635 6.8 % 0.1 0.33 SM(20) 2540G MMSD 06/65/14 DM0605/14009654 6.2 % 0.1 0.33 SM(20) 254OG MMSD 06/06/14 DMO606/14009669 7 % 0.1 0.33 SM(20) 254OG MMSD 06/07/14 DM0607/14009844 5.4 % 0.1 0.33 SM(20) 254OG MMSD 06/08/14 DM0608/14009867 5.1 % 0.1 0.33 SM(20) 2540G MMSD 06/09/14 DM0609/14009880 5.2 % 0.1 0.33 SM(20) 254OG MMSD 06/10/14 DM0610/14009907 5.5 % 0.1 0.33 SM(20) 254OG MMSD 06/11/14 DM0611/14010237 5.8 % 0.1 0.33 SM(20) 2540G MMSD 06/12/14 DM0612114010256 6.2 % 0.1 0.33 SM(20) 2540G MMSD 06/.13/14 DM0613/14010271 5.1 % 0.1 0.33 SM(20) 2540G MMSD 06/14/14 DM0614/14010282 5.1 % 0.1 0.33 SM(20) 2540G MMSD 06/15/14 DMO615/14010301 6.9 % 0.1 0.33 SM(20) 254OG MMSD 06/16/14 DM0616/14010319 6.5 % 0.1 0.33 SM(20) 2540G MMSD 06/17/14 DM0617/14010346 7 % 0.1 0.33 DI. SM(20) 2540G MMSD 06/18/14 DM0618/14010687 6.3 % 0.1 0.33 SM(20),2540G MMSD 06/19/14 DM0619/14010706 6.6 % 0.1 0.33 SM(20) 254OG MMSD 06/20/14 DM062oh4b10721 5.3 % 0.1 0.33 SM(20) 2540G MMSD 06/21/14 DM0621/1'4010732 6.3'% 0.1 0.33 SM(20) 254OG MMSD 06/22/14 DM0622/14010751 5.2 % 0.1 0.33 SM(20) 2540G MMSD 06/23/14 DM0623/14011513 4.2 % 0.1 0.33. SM(20) 2540G MMSD 06/24/14 DM0624M.4011540 5.4 % 0.1 0.33 SM(20) 254OG MMSD 06/25/14 DM0625/14011566 7.1 % 0.1 0.33 SM(20) 2540G MMSD 06/26/14 DM0626/14011766 4.8 % 0.1 0.33 SM(20) 254OG MMSD 06/27/14 DMO627/14011781 6.7 % 0.1 0.33 SM(20) 2540G MMSD 06/28/14 DM0628/14011792 8.1 % 0.1 0.33 SM(20) 254OG MMSD 06/29/14 DM0629114011811 8.3 % 0.1 0.33 SM(20) 2540G MMSD 06/30/14 DM0630/14011824 7.6 % 0.1 0.33 SM(20) 254OG MMSD 07/01/14 DM0701/1401.1851 8.9 % 0.1 0.33 . SM(20) 254OG MMSD 07/02/14 DM0702/14011879 8.1 % 0.1 0.33 SM(20) 254OG MMSD 07/03/14 DM0703/14011898 5.7 % 0.1 0.33 SM(20) 2540G MMSD 07/04/14 DM0704/14011911 6 % 0.1 0.33 SM(20) 2540G MMSD 07/05/14 DM0705/14011924 5 % 0.1 0.33 SM(20) 254OG MMSD 07/06/14 DM0706/14011943 5.8 % 0.1 0.33 SM(20) 254OG MMSD SmlrptimiloMonthly 1110113 q' Page 92 of 106 Printed.• 11811510.48 is MSD Pal IMS lilt A CLtkgR frO NANT Solids (% Moisture) - D. a .o LOQ Q. Flags Annual Milorganite Report January 1 to December 31, 2014 Analytical Method Lab 07/07/14 DM0707114012196 7.7 % 0.1 0.33 SM(20) 254OG MMSD 07/08/14 DM0708/14012898 6.5 % 0.1 0.33 SM(20) 254OG MMSD 07/09/14 DM0709/14012926 6.7 % 0.1 0.33 SM(20) 2540G MMSD 07/10/14 DM0710/14012945 7.3 % 0.1 0.33 SM(20) 254OG MMSD 07/11/14 DM0711114012961 6.9 % 0.1 0.33 SM(20) 2540G MMSD 07/12/14 DM0712/14012971 6.1 % 0.1 0.33 SM(20) 2540G MMSD 07/13/14 DM0713/14012991 6 % 0.1 0.33 SM(20) 254OG MMSD 07/14/14 DM0714/14013004 5.2 % 0.1 0.33 . SM(20) 254OG MMSD 07/15/14 DM0715114013031 4.6 % 0.1 0.33 SM(20) 2540G MMSD 07/16/14 DM0716/14013059 4.7 % 0.1 0.33 SM(20) 254OG MMSD 07/17/14 DM0717/14013078 5.6 % 0.1 0.33 SM(20) 2540G MMSD 07/18/14 DM0718/14013295 6.8 % 0.1 0.33 SM(20) 254OG MMSD 07/19/14 DM0719/14013305 7.9 % 0.1 0.33 SM(20) 2540G MMSD 07/20/14 DM0720/14013324 7.2 % 0.1 0.33 SM(20) 2540G MMSD 07/21/14 DM0721/14013337 8.1 % 0.1 0.33 SM(20) 2540G MMSD 07/75/14 DM0725/14013997 3.7 % 0.1 0.33 SM(20) 2540G MMSD 07/26/14 DM0726/14014008 4.4 % 0.1 0.33 SM(20) 2540G MMSD 07/27/14 bM0727/14014027 6.9 % 0.1 0.33 SM(20) 2540G MMSD 07/28/14 DM0728/14014040 10 % 0.1 0.33 SM(20) 254OG MMSD 07/29/14 DM0729/14014895 7 % 0.1 0.33 SM(20) 2540G MMSD 07/30/14 DM0730/14014923 6.8 % 0.1 0.33 SM(20) 2540G MMSD 07/31/14 DM0731/14014942 7.9 % 0.1 0.33 SM(20) 2540E MMSD 08/01/14 DM0801/14014957 7.5 % 0.1 0.33 SM(20) 254OG MMSD 08/02/14 DM0802/14014968 5.9 % 0.1 0.33 SM(20) 2540G MMSD 08/03/14 DM0803/14014987 5 % 0.1 0.33 SM(20) 254OG MMSD 08/04/14 DMO804/14015000 6.9 % 0.1 0.33 SM(20) 2540G MMSD 08/05/14 DMO805/14015027 8.6 % 0.1 0.33 SM(20) 2540G MMSD 08/06/14 DM0806/14015405 7.6 % 0.1 0.33 SM(20) 2540G MMSD 08/07/14 DM0807/14015456 8.2 % 0.1 0.33 SM(20) 254OG MMSD 08/08/14 DM0808/14015471 8.4 % 0.1 0.33 SM(20) 254OG MMSD 08/09/14 DM0809/14015482 7.3 % 0.1 0.33 SM(20) 2540G MMSD 08/10/14 DM0810/14015966 5.3 % 0.1 0.33 SM(20)254OG MMSD 08/11/14 DMO811/14015984 5.1 % 0.1 0.33 SM(20) 254OG MMSD 08/12/14 DM0812/14016011 6.5 % 0.1 0.33 SM(20) 254OG MMSD 08/13/14 DMO813/14016039 8.9 % 0.1 0.33 SM(20) 2540G MMSD 08/14/14 DM0814/14016058 4.6 % 0.1 0.33 . SM(20) 2540G MMSD 08/15/14 DMOS15/14016181 5.2 % 0.1 0.33 SM(20) 2540G MMSD 08/16/14 DM0816/14016192 5.6 % 0.1 0.33 SM(20) 254OG MMSD 08/17/14 DMO817/14016211 4.5 % 0.1 0.33 SM(20) 2540E MMSD 08/18/14 DMO818/14016290 7.5 % 0.1 0.33 SM(20) 2540G MMSD 08/19/14 bM0819/14016319 4.2 % 0.1 0.33 SM(20) 2540E MMSD 08/20/14 DMO820/14016347 4.1 % 0.1 0.33 SM(20) 2540G MMSD 08/21/14 DM0821/14016365 4.3 % 0.1 0.33 SM(20) 2540G MMSD 08/22/14 DMO822/14016381 6.4 % 0.1 0.33 SM(20) 254OG MMSD 08/23/14 DM0823/14016392 4.8 % 0.1 0.33 SM(20) 2540G MMSD 08/24/14 DM0824114016411 4.9 % 0.1 0.33 SM(20) 254OG MMSD 08/25/14 DM0826114016488 6.3 % 0.1 0.33 SM(20) 2540G MMSD 5Y5/fpttM11bMonth1y 1110113 tj Page 93 of 106 Pnnted:11811510.-98 +, Annual Milorganite Report January 1 to December 31, 2014 MSD PdPTMiY3fDPA'CILI ABUROKN[Ai Solids (% Moisture) Sam.ple'Date Sample ID Result LOD 08/26/14 DMO826114016515 4.5 % 0.1 0.33 SM(20) 254OG MMSD 08/28/14 DM0828/14016907 15 6/0 0.1 0.33 SM(20) 254OG MMSD 08/31/14 DMO831/14017701 5.4 % 0.1 0.33 SM(20) 254OG MMSD 09/01/14 DMO901/14017714 4.6 6/° 0.1 0.33 SM(20) 2540G MMSD 09/02/14 DMO902114017871 6.4 % 0.1 0.33 SM(20) 254OG MMSD 09/03/14 DM0903/14017886 5.8 % 0.1 0.33 SM(20) 254OG MMSD 09/04/14 DM0904/14017920 3.8 % 0.1 0.33 SM(20) 254OG MMSD 09/05/14 DMO905/14017901 3.6 % 0.1 0.33 SM(20) 254OG MMSD 09/16/14 DMO916/14019167 3.5 % 0.1 0.33 SM(20) 254OG MMSD 09/17/14 DMO917/14019195 3.4% 0.1 0.33, SM(20) 2540G MMSD 09/18/14 DMO918/14019229 3.8 % 0.1 0.33 SM(20) 254OG MMSD 09/19/14 DM0919/14019244 4.4 % 0.1 0.33 SM(20) 254OG MMSD 09/20/14 DM0920/14019255 5 % 0.1 0.33 SM(20) 254OG MMSD 09/21/14 DMO921114019274 5 % 0.1 0.33 SM(20) 254OG MMSD 09/22/14 DMO922/14019287 4.3 % 0.1 0.33 SM(20) 254OG MMSD 09/23/14 DMO923/14019778 6.4 % 0.1 0.33 SM(20) 2540G MMSD 09/24/14 DM0924/14019806 7.6 % 0.1 0.33 SM(20) 2540G MMSD 09/25/14 DM0925/14019825 5.2 % 0.1 0.33. SM(20) 254OG MMSD 09/26/14 DMO926/14019840 4.1 % 0.1 0.33 SM(20) 254OG MMSD 09/27/14 DM0927/14019851 6.9 % 0.1 0.33 SM(20) 2546G MMSD 09/28/14 DM0928/14019870 6.5 % 0.1 0.33 SM(20) 2540G MMSD 09/29/14 DM0929/14019883 4.1 % 0.1 0.33 SM(20) 2540G MMSD 09/30/14 DM0930/14019909 4.6 % 0.1 0.33 SM(20) 2540G MMSD 10/01/14 DM1001/14019927 6 % 0.1 0.33 SM(20) 2540G MMSD 10/02/14 DM1002/14020572 6.1 % 0.1 0.33 _ SM(20) 254OG MMSD 10/03/14 DM1003/14020587 4.4 % 0.1 0.33 SM(20) 2540G MMSD 10/04/14 DM1004/14020598. 5 % 0.1 0.33 SM(20) 2540G MMSD 10/OS/14 DM1005/14020617 7.2 % 0.1 0.33 SM(20) 254OG MMSD 10/06/14 DM1006/14020630 3.6 % 0.1 0.33 SM(20) 254OG MMSD 10/07/14 DM1007/14021108 6.4 % 0.1 0.33 SM(20) 254OG MMSD 10/08/14 DM1.008/14021160 7 % 0.1 0.33 SM(20) 254OG MMSD 10/09/14 DM1009/14021179 5.8 % 0.1 0.33 SM(20) 254OG MMSD 10/10/14 DM1010/14021194 7.7 % 0.1 0.33 SM(20) 2540G MMSD 10/11/14 DM1011/14021244 9.6 % 0.1 0.33 SM(20) 254OG MMSD' 10/12/14 DM1012/14021263 8.7 % 0.1 0.33 SM(20) 254OG MMSD 10/13/14 DM1013/14021276 6.5 % 0.1 0.33 - SM(20) 254OG MMSD 10/14/14 DM1014/14021304 6.9 % 0.1 0.33 SM(20) 254OG MMSD 10/15/14 DM1015/14021332 8.4 % 0.1 0.33 SM(20) 254OG MMSD 10/16/14 DM1016/14021351 5.6 % 0.1 0.33 SM(20) 2540G MMSD 10/17/14 DM1017/14021787 5.3 % 0.1 0.33 : SM(20) 254OG MMSD 10/18/14 DM1018/14021798 8.6 % 0.1 0.33 SM(20) 2540G MMSD 10/19/14 DM1019114021817 7.4 % 0.1 0.33 SM(20),254OG MMSD 10/20/14 DM1020/14021830 8.6 % 0.1 0.33 SM(20) 2540G MMSD 10/21/14 DM1021l14021857 11 % 0.1 0.33 SM(20) 2540G MMSD 10/22/14 DM1022/14021885 7.6 % 0.1 0.33 SM(20) 254OG MMSD 5Y5/rptIA1bMontl1y 1110113 tj Page 94 of 106 Printed:1/8/1510:48 � f � ,uf MSD POINf(dfb£A:CtWIRIVIR NNI Solids (% Moisture) Annual Milorganite Report January 1 to December 31, 2014. 10/23/14 DM1023/14022256 8.2 % 0.1 0.33' SM(20) 2540G MMSD 10/24/14 DM1024/14022273 6.5 % 0.1 0.33 SM(20) 254OG MMSD 10/25/14 DM1025/14022286 6.3 % 0.1 0.33 SM(20) 254OG MMSD 10/26/14 DM1026/14022305 5.2 % 0.1 0.33 SM(20) 254OG MMSD 10/27/14 DM1027/14022318 8.4 % 0.1 .0.33' SM(20) 2540G MMSD 10/28/14 DM1028/14022409 7.2 % 0.1 0.33 SM(20) 254OG MMSD 10/29/14 DM1029/14022439, 7.7 % 0.1 0.33 SM(20) 2540G MMSD 10/30/14 DM1030/14022510 7.3 % 0.1 0.33 SM(20) 2540G MMSD 10/31/14 DM1031/14022525 6 % 0.1 0.33 ' SM(20) 2540G MMSD 11/01/14 DM1101/14022536 6.3 % 0.1 6.33 SM(20) 254OG, MMSD 11/02/14 DM1102/14022555 6.6 % 0.1 0.33 SM(20) 254OG MMSD 11/03/14 DM1103/14022568 5.7 % 0.1 0.33 SM(20) 254OG MMSD 11/04/14 DM1104/14023111 7.1 % 0.1 0.33 SM(20) 254OG MMSD 11/65/14 DM1106114023139 9.5 % 0.1 0.33 S14(20) 2540G. MMSD 11/06/14 DM1106/14023158 7.9 % 0.1 0.33 SM(20) 2540G MMSD 11/07/14 DM1107/14023173 7.1 % 0.1 0.33 SM(20) 254OG MMSD 11/08/14 DM1108/14023184 5.9 % 0.1 0.33 SM(20) 254OG MMSD 11/09/14 DM1109/14023203 8 % 0.1 0.33 SM(20) 2540G MMSD 11/10/14 DM1110/14023767 6.7 % 0.1 0.33 SM(20) 2540G MMSD 11/11/14 DM1111/14023796 8.9 % 0.1 0.33 SM(20) 2540G MMSD .. 11/12/14 DM1112/14023876 7.6 % 0.1 0.33 SM(20) 254OG MMSD 11/13/14 DM1113/14023895 5.6 % 0.1 0.33 SM(20) 2540G MMSD 11/14/14 DM1114114023910 5.6 % 0.1 0.33 SM(20) 2540G MMSD 11/15/14 DM1115/14023929 5.6 % 0.1 0.33 SM(20) 254OG MMSD 11/16/14 DM1116/14023948 6 0/6 0.1 0.33 SM(20) 254OG MMSD 11/17/14 DM1117/14023961 8.6 % 0.1 0.33 SM(20) 254OG MMSD 11/18/14 DM1118/14024236 6.9 % 0.1 0.33 SM(20) 254OG MMSD 11/19/14 DM1119/14024264 8.2 % 0.1 0.33 SM(20) 2540G MMSD 11/20/14 DM1120/14024283 5.8 % 0.1 0.33 SM(20) 254OG MMSD 11/21/14 DM1121/14024302 5.1 % 0.1 0.33 SM(20) 2540G MMSD 11/22/14 DM1122/14024313 6.2 % 0.1 0.33 SM(20) 254OG MMSD 11/23/14 DM1123/14024393 8.3 % 0.1 0.33 SM(20) 254OG MMSD 11/24/14 DM1124/14024414 8.2 % 0.1 0.33 SM(20) 2540G MMSD 11/25/14 DM1125/14024441 7.2 % 0.1.. 0.33 SM(20) 2546G MMSD 11/26/14 DM1126114024469 6.1 % 0.1 0.33 SM(20) 2540G MMSD 11/27/14 DM1127114024529 8.4 % 0.1 0.33 SM(20) 2540G MMSD 11/28/14 DM1'128/14024544 4.8 % .:0.1 0.33 SM(20).2540G MMSD 11/29/14 DM1129/14024555 6.4 % 0.1 0.33 SM(20) 254OG MMSD 11/30/14 DM1130/14024574 8.1 % 0.1 0.33 SM(20) 254OG MMSD 12/01/14 DM1201/14024601 8 % 0.1 0.33 SM(20) 2540G MMSD 12/02/14 DM1202/14025299 6.5 % 0.1 0.33 SM(20) 2540G MMSD 12/03/14 DM1203/14025327 8.1 % 0.1 0.33 SM(20) 254OG MMSD 12/04/14 DM1204/14025346 7.1 % 0.1 0.33 SM(20) 254OG MMSD 12/05/14 DM1205/14025361 6.7 % 0.1 0.33 SM(20) 254OG MMSD 12/06/14 DM1206/14025372 7.3 % 0.1 0.33 SM(20) 2540G MMSD 12/07/14 DM1207/14025391 7.2 % 0.1 0.33 SM(20) 254OG MMSD 12/08/14 DM1208/14025404 7.5 % 0.1 0.33 SM(20) 254OG MMSD SYS/rptlMi/oMonth/y 1/10/13 tj Page 95 of 106 Printed: 1/8/1510:48 � e e L Annual Milorganite Report M S D January 1 to December 31, 2014 1 P.1IMlot ACII1.t1R11i114, RN1 Solids (% Moisture) Sample D, •e LOQ QA Flags Analytical Method Lab 12/09/14 DM1209/14026WO 6.1 % 0.1 0.33 SM(20) 254OG MMSD 12/10/14 DM1210/14026198 5.5 % 0.1 0.33 SM(20) 254OG MMSD 12/11/14 DM1211/14026217 7.5 % 0.1 0.33 SM(20) 2540G MMSD 12/12/14 DM1212/14026232 6.3 % 0.1 0.33 SM(20) 254OG MMSD 12/13/14 DM1213/14026243 6.3 % 0.1 0.33 SM(20) 2540G MMSD 12/14/14 DM1214/14026262 7.5 % 0.1 0.33 SM(20) 254OG MMSD 12/15/14 DM1215/14026277 9.5 % 0.1 0.33 SM(20) 2540G MMSD 12/16/14 DM1216/14026475 6.6 % 0.1 0.33 SM(20) 2540G MMSD 12/17/14 DM1217/14026503 8.8 % 0.1 0.33 SM(20) 254OG MMSD 12/18/14 DM1218/14026522 9.7 % 0.1 0.33 SM(20) 2540G, MMSD 12/19/14 DM1219/14026537 7.3 % 0.1 0.33 SM(20) 2540G MMSD 12/20/14 DM1220/14026653 9.5 % 0.1 0.33 . SM(20) 2540G MMSD 12/21/14 DM1221./14026672 9.3 % 0.1 0.33 SM(20) 254OG MMSD. 12/22/14 DM1222/14026685 7.4 % 0.1 0.33 SM(20) 2540G MMSD 12/23/14 DM1223/14026713 7.6 % 0.1 0.33 SM(20) 254OG MMSD 12/24/14 DM1224/1402674.1 7.2 % 0.1 0.33 SM(20) 254OG MMSD 12/25/14 DM1225/14026760 6.2 % 0.1 0.33 SM(20) 2540G MMSD 12/26/14 DM1226/14026777 4.8 % 0.1 0.33 SM(20) 254OG MMSD 12/27/14 DM1227/14026788 5.8 % 0.1 0.33 SM(20) 2540G MMSD 12/28/14 DM1228/14026807 7.5 % 0.1 0.33 SM(20) 2540G MMSD 12/29/14 DM1229/14027031 6.7 % 0.1 0.33 SM(26) 2540G MMSD 12/30/14 DM1230/14027058 4.5 % 0:1 0.33 SM(20) 2540G MMSD 12/31/14 DM1231/14027086 5.8 % 0.1 0.33 •. SM(20) 2540G MMSD Avg: 6.2 % Weekly Composite 01/04/14 WMC1/1.4000137 6.4 % Max: 0.1 0.33 110/0 SM(20) 254OG MMSD 01/11/14 WMC2/14000475 6.2 % 0.1 0.33 SM(20) 254OG MMSD 01/18/14 WMC3/14000605 5.6 % 0.1 0.33 SM(20) 2540G MMSD 01/25/14 WMC4/14001097 6.7 % " 0.1 0.33 SM(20) 254OG MMSD 02/01/14 WMC5/14001445 5.8 % 0.1 0.33 SM(20) 2540G MMSD 02/08/14 WMC6114001578 6 % 0.1 0.33 SM(20) 2540G MMSD 02/15/14 WMC7/14001916 6.8 % 0.1 0.33 SM(20) 254OG MMSD 02/22/14 WMC8/14002226 6.2 % 0.1 0.33 SM(20) 2540G MMSD 03/01/14 WMC9/1.4002955 5.5 % 0.1 0.33 SM(20) 254OG MMSD 03/08/14 WMC10/14003247 6.2 % 0.1 0.33 SM(20) 2540G MMSD 03/15/14 WMC11/14003938 5.6 % 0.1 0.33 SM(20) 2540G MMSD 03/22/14 WMC12/14.004463 5.5 % 0.1 0.33. SM(20) 2540G MMSD 03/29/14 WMC13/14004923 4.3 % 0.1 0.33 SM(20) 2540G MMSD 04/05/14 WMC14/14005242 4.9 % 0.1 0.33 SM(20) 2540G MMSD 04/12/14 WMC15/14005643 6.1 % 0.1 0.33 SM(20) 254OG MMSD 04/19/14 WMC16/14.006129 7.2 % 0.1 0.33 : SM(20) 2540G MMSD 04/26/14 WMC17/14006429 5.5 % 0.1 0.33 SM(20) 2540G MMSD 05/03/14 WMC18/14007184 5.1 % 0.1 0.33 SM(20) 2540G MMSD 05/10/14 WMC19/14007579 6 % 0.1 0.33 SM(20) 2540G MMSD 05/37/14 WMC20/14007770 5.5 % 0.1 0.33 . SM(20) 2540G MMSD 05/24/14 WMC21/14008326 5 % 0.1 0.33 SM(20) 2540G MMSD SYS/rptSMiloMonthly 1110113 tj Page 96 of 106 Printed:11811510:98 L(�' �'AMA M S D PAN VWLlE U MIUM I Solids (% Moisture) Sample 1/ gesult LOD 1 1 QA Flags f I Annual Milorganite Report January 1 to December 31, 2014 Analitical Method', Lab 05/31/14 WMC22/14009595 6 % 0.1 0.33 SM(20) 2540E MMSD 06/07/14 WMC23/14009882 6.4 % 0.1 0.33 SM(20) 254OG MMSD 06/14/14 WMC24/14010321 5.7 % 0.1 0.33 SM(20) 254OG MMSD 06/21/14 WMC25/14011515 6.6 % 0.1 0.33 SM(20) 254OG MMSD 06/28/14 WMC26/14011826 6 % 0.1 0.33 SM(20) 2540G MMSD 07/05/14 WMC27/14012198 7.1 % 0.1 0.33 SM(20) 254OG MMSD 07/12/14 WMC28/14013005 : 6.7 % 0.1 0.33 SM(20) 2540G MMSD 07/19/14 WMC29/14013339 6.1 % 0.1 0.33 SM(20) 254OG MMSD 07/26/14 WMC30/14014042 6.2 % 0.1 0.33 SM(20) 254OG MMSD 08/02/14 WMC31/14015002 7 % 0.1 0.33 SM(20) 2540G, MMSD 08/09/14 WMC32/14015986 7.6 % 0.1 0.33 SM(20) 254OG MMSD 08/16/14 WMC33114016294 6.1 % 0.1 0.33 SM(20) 2540E MMSD 08/23/14 WMC34/14016490 5.6 % 0.1 0.33 SM(20) 254OG MMSD 08/30/14 WMC35/14017716 5.3 % 0.1 0.33 SM(20) 254OG MMSD 09/05/14 WMC36/14018081 5.2 % 0.1 0.33 SM(20) 254OG MMSD 09/20/14 WMC 38/14020851 4.6 % 0.1 0.33. SM(20) 2540G MMSD 09/27/14 WMC39/14020976 6.3 % 0.1 0.33 SM(20) 254OG MMSD 10/04/14 WMC40/14021278 5.5 % 0.1 0.33 SM(20) 2540G MMSD 10/11/14 WMC41/14021279 6.7 % 0.1 0.33 SM(20) 2540G MMSD 10/18/14 WMC42/14021832 7.2 % 0.1 0.33 SM(20) 2540G MMSD 10/25/14.. WMC43114022322 7.9 % 0.1 0.33 SM(20) 2540E MMSD 11/01/14 WMC44/14022570 ; 6.5 % 0.1 0.33 SM(20) 254OG MMSD 11/08/14 WMC45/14023769 7 % 0.1 0.33 SM(20) 254OG MMSD 11/15/14 WMC46/14023963 6.8 % 0.1 0.33 SM(20) 2540G MMSD 11/22/14 WMC47/14024416 6.5 % 0.1 0.33 SM(20) 254OG MMSD 11/29/14 WMC48/14025406 6.9 % 0.1 0.33 SM(20) 254OG MMSD 12/06/14 WMC49/14025407 7.2 % 0.1 0.33 SM(20) 254OG MMSD 12/13/14 WMC50/14026219 6.5 % 0.1 0.33 SM(20) 254OG MMSD 12/20/14 WMC51/14026687 8.1 % 0.1 0.33 SM(20) 254OG MMSD 12/27/14 WMC52/14027033 7 % 0.1 0.33 SM(20) 254OG MMSD Grab Sample 01/05/14 MF/14000281 8.1 % 0.1 0.33 SM(20) 2540G MMSD 01/12/14 MF/14000893 4.9 o 0.1 0.33 SM(20) 2540G MMSD 01/20/14 MF/14001250 6.5 % 0.1' 0.33 . SM(20) 254OG MMSD 02/14/14 MF/14002911 8.6 % 0.1 0.33 SM(20) 254OG MMSD 02/17/14 'MF/14003047 6.3 % 0.1 0.33 SM(20) 254OG. MMSD 02/24/14 MF/14003138 7.8 % 0.1 0.33 SM(20) 2540G MMSD 03/07/14 MF/14004378 7.7 % 0.1 0.33 SM(20) 2540G MMSD 03/09/14 MF/14004426 8.2 % 0.1 0.33 SM(20) 254OG MMSD . 03/16/14 MF/14004744 7.7 % 0.1 0.33 SM(20) 2540G MMSD 04/07/14 MF/14006115 5.4 % 0.1 0.33 SM(20) 2540G MMSD 04/14/14 MF/14006564 9 % 0.1 0.33 SM(20) 254OG MMSD 04/21/14 MF/14007114 3.9 % 0.1 0.33 SM(20) 2540G, MMSD 05/04/14 MF/14008425 6.2 % 0.1 0.33 SM(20) 254OG MMSD 05/11/14 MF/14008787 5 % 0.1 0.33 SM(20) 2546G MMSD 05/18/14 MF/14009431 8.8 % 0.1 0.33 SM(20) 2540G MMSD 06/02/14 MF/14010891 9.1 % 0.1 0.33 SM(20) 254OG MMSD 5Y5/rptlMi/oMonth/y 1110113 tj Page 97 of 106 Printed.-11811510:48 Annual Milorganite Report January 1 to December 31, 2014 PAINIPS I(is A ULM [IN'itt KHM Solids (% Moisture) SamplePate Sample XD Result L.. .• Flags Aiialytical Method Lab 06/09/14 MF/14011493 5.4 % 0.1 0.33 SM(20) 2540G MMSD 06/16/14 MF/14012167 6.2 % 0.1 0.33 SM(20) 254OG MMSD 07/06/14 MF/14014180 8 % 0.1 0.33 SM(20) 2540G MMSD 07/14/14 MF/14014642 4.6 % 0.1 0.33., .SM(20) 254OG MMSD 07/26/14 MF/14015263 6.7 % 0.1 0.33 SM(20) 2540G MMSD 08/04/14 MF/14016731 9 % 0.1 0.33 SM(20) 2540G. MMSD 08/11/14 MF/14017429 4.3 % 0.1 0.33 SM(20) 254oG MMSD 08/18/14 MF/14018002 . 4.1 % 0.1 0.33, SM(20) 254OG MMSD 09/02/14 MF/140194423' 6.5 % 0.1 0.33 SM(20) 2540G MMSD 09/16/14 MF/14020820 3 % 0.1 0.33 SM(20) 254OG MMSD 09/24/14 MF/14021446 7.6 % 0.1 0.33 SM(20) 2540G MMSD 10/06/14 MF/14022464 3.6 % 0.1 0.33 _ _ SM(20) 2540G MMSD 10/13/14 MF/14023066 6.2 % 0.1 0.33 SM(20) 2540G MMSD 10/27/14 MF/14024179 9.8 % 0.1 0.33 SM(20) 2540G MMSD 11/03/14 MF/14024712 9.6 % 0.1 0.33 SM(20) 254OG MMSD 11/10/14 MF/14025198 6.8 % 0.1 0.33 SM(20) 254OG MMSD 11/17/14 MF/14025811 5.6 % 0.1 0.33 SM(20) 254OG MMSD 12/02/14 MF/14026563 6.4 % 0.1 0.33 SM(20) 2540G MMSD 12/08/14 MF/14026987 5.9 % 0.1 0.33 SM(20) 2540G MMSD 12/15/14 MF/14027309 8.9 % 0.1 0.33 SM(20) 2540G MMSD Page 98 of 106 SYS/rptlMiloMonthly 11-10113 t/ Printed: 1/8/1510:98 P,tlI1H(t6 IDt � ClL4MR [AIfd�NN[h1 ZINC ICP METHOD Sample Date Sample ID Result LOD LOQ QA Flags Annual Milorganite Report January 1 to December 31, 2014 Analytical MethGd Lab 01/01/14 DMO101/14000012 510 mg/kg D.W. 0.52 6: SW846: 6010C MMSD 01/02/14 DMO102/14000039 520 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/03/14 DMO103/14000088 550 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/04/14 DMO104/14000103 540 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/05/14 DMO105/14000122 540 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/06/14 DMO166114000136 560 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/07/14 DMO107/14000162 540 mg/kg D.W. 0.52 6 SW846:.6010C MMSD 01/08/14 DMO108/14000188 530 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/09/14 DMO109/14000207 490 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/10/14 DM0110/14000430 510 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/11/14 DM0111/14000441 540 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/12/14 DM0112/14000460 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/13/14 DM0113/14000473 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/14/14 DM0114/14000500 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/15/14 DM0115/14000526 530 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/16/14 DM0116/14000545 520 ing/kg D.W. 0.52 6 SW846: 6010C MMSD 01/17/14 DM0117/14000560 550 ing/kg D.W. 0.52 6 SW846: 6010C MMSD. 01/18/14 DM0118/14000571 . .620 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/19/14 DM0119/14000590 630 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/20/14 DMO120/14000603 640 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/21/14 DMO121/14000630 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/22/14 DM0122/14000656 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/23/14 DMO123/14000675 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/24/14 DMO124/14000690 550 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/25/14 DMO125/14000923 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/26/14 DM6126/14000942 590 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/27/14 DM0127/14001095 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/28/14 DMO128114001122 610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/29/14 DMO129/14001148 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/30/14 DM0130/14001167 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 01/31/14 DM0131/14001182 560 mg/kg D.W. 0.52 6. SW846: 6010C MMSD 02/01/14 DM0201/140011.93 590 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/02/14 DM0202/14001430 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/03/14 DM0203/14001443 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/04/14 DM0204/14001470 560 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/05/14 DM0205/14001498 620 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/06/14 DM0206/14001517. 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/07/14 DM0207/14001532 540 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/08/14 DM0208/14001543 560 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/09/14 DM0209/14001562 550 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/10/14 DM0210/14001576 550 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/11/14 DM0211/14001811 560 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/12/14 DM0212/14001837 530 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/13/14 DM0213/14001856 510 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/14/14 DM0214/14001871 530 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/15/14 DM0215/14001882 510 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/16/14 DM0216/14001893 480 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 5Y51rpt1N1/oMonth1y 1110113 tJ Page 99 of 106 Printed:1/8/1510:48 1. L + PAi(iXC�s (Gt A �LE/.53it lltltaNNEliT ZINC ICP METHOD. Sartiple Date Sample ID 02/17/14 DM0217/14001914 Reshlt 480 mg/kg D.W. 1,01) 0.52 1QQ 6 Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 02/18/14 DM0218/14002002 470 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/19/14 DM0219/14002028 500 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/20/14 DM0220/14002101 500 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/21/14 DM0221/14002181 540 mg/kg DN. 0.52 6 SW846: 6010C MMSD 02/22/14 DM0222/14002192 550 mgjkg D.W. 0.52 6 SW846: 6010C MMSD 02/23/14 DM0223/14002211 590 mg/kg D.W: 0.52 " 6 SW846: 6010C MMSD 02/24/14 DM0224/14002224 570 mg/kg D.W. 0.52 6 :::SW846: 6610C MMSD 02/25/14 DM0225/14002251 540 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 02/26/14 DM0226/14002310 510 mg/kg D.W. 0.52 6 SW846:.6010C MMSD 02/27/14 DM0227/14002329 540 mg/kg D.W. :0.52. 6 SW846:6010C MMSD 02/28/14 : _ DM0228/14002350 510 mgjkg D.W. 0.52 6 SW846: 6010C MMSD 03/01/14 . DM0301/14002921 550 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/02/14 W0302/14002940. 570 mg/kg D.W. 0.52 6 SW846:.6010C MMSD 03/03/14 DM0303/14002953 630 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/04/14 - DM0304/14002986 530 mg/kg D^ 0.52 6'" SW846: 6010C MMSD 03/OS/14 DM0305/14003012 520 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/06/14 DM0306/14003182 520 mg/kg D.W: . 0.52 6 SW846: 6010C MMSD 03/07/14 DM0307/14003197 520 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/08/14 DM0308/14003208 500 m6/k6 D.W. 0.52 6 SW846: 6010C MMSD 03/09/14 DM0309/14003232 540 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/10/14 DM0310/14003245 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/11/14 DM031.1/14003272 570 mg/kg D.W. 0.52 6 :SW846: 6010C MMSD 03/12/14 DM0312/14003360 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/13/14 QMQ313/14003871 630 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/14/14 DM0314/14003886 .590 mg/kg D.W. 0.52 6 SW846:'6610C MMSD 03/15/14 DM0315/14003899 540 mg/kg D.W. 0.52 6. SW846: 6010C MMSD 03/16/14 DM0316/140039i8 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/17/14 DM0317/14003936 540 mg/kg D.W., 0.52 6 SW846::6010C MMSD 03/18/14 DM0318/14003963 520 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/19/14 DM0319/144004217 560 mg/kg D.W. 0.52 6 SW846: 6010C MMSD -03/20/14 DM0320/14004315 520 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/21/14 DM0321/14004330. 530 mg/kg D.M. 0.52 6 SW846: 6010C MMSD 03/22/14 DM0322/14004341 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03%23/14 .: DM0323%14004360 516 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/24/14 DM0324/14004461 400 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/25/14 DM0325/14004638 380 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/26/14 DM0326/14004664 370 mg/kg D.W. 0.52 6. SW846: 6010C MMSD 03/27/14 DM032.7/14004683 380 mg/kg DM. 0.52 6 SW846: 6010C MMSD 03/28/14 DM0328/14004698 380 mg/kg D.W. 0..52 6 SW846: 6010C MMSD 03/29/14 DM0329/14004889 430 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/30/14 DM0330114004908 480 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 03/31/14 DM0331/14004921 470 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/01/14 DM0401/14004948, 460 mg/kg D.W. 0.52 6 SW846:.6010C MMSD 04/02/14 DM0402/14004974 470 mg/kg D.W. 0.52 6 SW846: 6010C MMSD : 04/03/14 DM0403M-4004993 500 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/04/14 DM0404/1'4005195 490 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 5Y5/rptimi/oMonth/y 1110113 tj Page 100 of 106 Printed. 11811510.48 MSU hsNt�t rua a 4tt�� t�r��utt� ZINC ICP METHOD saknplebat�to 04/05/14 DM0405/14005206 540 mg/kg D.W. 0.52 OQ u• Flag 6 Annual Milorganite Report January 1 to December 31, 2014 -Loib SW846: 6010C MMSD 04/06/14 DM0406/14005226 530 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/07/14 DM0407/14005240 .540 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/08/14 DM0408/14005267 510 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/06/14 DM0409/14005397 480 mg/kg D.W. 0.52 6" SW846: 6010C MMSD 04/10/14 DM0410/14005416 460 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/11/14 DM0411/14005434 .550 mg/kg D.W. 0.52 6 SW846:.6010C MMSD 04/12/14 DM0412/14005605 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/13/14 DM0413/14005627 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/14/14 DM0414/14005641 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/15/14 DM0415/14005668 .610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/16/14 DM0416/14005791 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/17/14 DM0417/14.005815 570' mg/kg D.W. 0.8 6 SW846: 6010C MMSD 04/18/14 DM0418/14006027 550 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/19/14 DM0419/14006038 520 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 04/20/14 DM0420/14006057 540 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 04/21/14 DM0421/14.006127 530 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 04/22/14 DM0.422/14006154 590 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/23/14 DM0423/14006180 590 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/24/14 DM0424/14006339 560 mg/kg D.W. 0.52 .6.': SW846: 6010C MMSD 04/25/14 DMO425/14006354 600 mg/kg D.W. 0.52 6 SW846: 6010C. MMSD 04/26/14 DM0426/14006365' 640 mg/kg D.W:. O.S2 6 SW846::6010C MMSD 04/27/14 DM0427/14006384 590 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/28/14 DM0428/14006397 620 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 04/29/14 DM0429/14006454 560 mg/kg D.W. 0.52 6" " SW846: 6010C MMSD 04/30/14 DM0430/14006482 570 mg/kg D.W: 0.52 6 SW846: 6010C MMSD 05/01/14 DM0501/14006976 620 mg/kg D.W. 0.52 6., SW846: 6010C MMSD 05/02/14 DM0502/14006991 540 mg/kg D.W. 0.52 '6 SW846: 6010C MMSD OS/03/14 DM0503/14007150 500 mg/kg D.W. 0.52 6 SW846:, 6010C MMSD 05/04/14 DMO504/14007169 480 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 05/0S/14 DM0505/14007182 470 mg/kg D:W. 0.52 6: SW846: 6010C MMSD 05/06/14 DM0506/14007209 500 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 05/07/14 DMO507/14007235 500 mg/kg D.W. 0.52 6 SW846:, 6010C MMSD 05/08/14 DM0508/14007254 440 mg/kg D.W. 0.52 6 SW846: 6010C MMSD OS/09/14 .: DM0509/14007269 460 mg/kg D.W. 0.52 6:: SW846: 6010C MMSD 05/10/14 DM0510/14007286 460 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 05/11/14 DM0511/14007456; 430 mg/kg D.W.: 0.8 6 SW846:;6010C MMSD 05/12/14 DMO512/14007469 430 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 05/13/14 DM0513/1400755.1 500 mg/kg D.W. 0.52 6 SW846: 6010C 'MMSD 05/14/14 DM0514/14007577 440 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 05/15/14 DMO515/14007665 480 mg/kg D.W.' '0.52 6 SW846: 6010C MMSD 05/16/14 DM0516114.007680 520 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 05/17/14 DMO517/14007691 440 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 05/18/14 DMO518/14007710 450 mg/kg D.W., 0.52 6 SW846: 6010C MMSD 05/19/14 DM0519/14007764 440 mg/kg D.W. 0.52 6 A0. SW846: 6010C MMSD 05/20/14 DM0520/14007997 490 mg/kg D.W. 0.52 6. SW846: 6010C MMSD 3/21/14 DM0521/14008023 470 mg/kg D.W. 0.52 6 SW846: 6010C MMSD SYS/rptlMilaMonth/y 1/10/13 of Page 101 O 106 Printed.•-1/8/1510.48 i Annual Milorganite Report ",M,Mso w- January 1 to December 31, 2014 RitINUS M XCLL4111 froMAN(Nt ZINC ICP METHOD sample Date sample v Result LOD LOQ QA Flags Analytical Lab 05/22/14 DM0522/14008042 480 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 05/23/14 DM0523/14008057 510 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 05/25/14 DM0525/14008310 480 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 05/26/14 DM0526/14008323 510 mg/kg D.W. 0.52 6' SW846: 6010C MMSD 05/27/14 DMO527/14008646 .. 510 mg/kg D.W. L 0.52 6 SW846: 6010C MMSD 05/28/14 DM0528/14008672 510 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 05/29/14 DM0529114008691 490 mg/kg D.W. 0.52 6.. SW846: 6010C MMSD 05/30/14 DM0530/14008845 510 mg/kg D:W. 0.8 6 SW846: 6010C MMSD 05/31/14 DM0531/14008856, 530 mg/kg D.W., 0.8 6 SW846:.6010C MMSD 06/01/14 DM0601114009580 510 mg/kg D.W.. 0.8 6 SW846: 6010C MMSD 06/02/14 DM0602/14009593 500 mg/kg DA 0.8 6 ::SW846: 6010C MMSD 06/03/14 DM0603/14009620 490 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/04/14 DMO604/14009635 500 mg/kg D.W. 0.52 6 SW846: 60110C MMSD 06/05/14 DM0605/14009654 550 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 06/06/14 DM0606/14009669 540 mg/kg D.W. 0.52 6; :-SW846: 6010C MMSD 06/07/14 DM0607/14009844 560 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 06/08/14 - DM0608/14009867. 570 mg/kg D.W. 0.52 6 SW846:'6010C MMSD 06/09/14 DM0609/14009880 560 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 06/10/14 DM0610/14009907 530 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 06/11/14 DM0611/14010237 560 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/12/14 DM0612/14010256- 550 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/13/14 DM0613/14010271 580 mg/kg D.W. 0.8 6. SW846: 6010C MMSD 06/14/14 DMO614/14010282 550 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/15/14 DM0615/14010301 530 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/16/14 DM0616/14010319 540 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/1-7/14 DM0617/14010346 570 mg/kg D:W. 0.8 6, SW846: 6010C MMSD 06/18/14 DMO618/14010687 550 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/19/14 DM0619/14010706 580 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/20/14 DM0620/14010721 560 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/21/14 DM0621/14010732 530 tng/kg D.W. 0.8 6: SW846: 6010C MMSD 06/22/14 DM0622/14010751 530 mg/kg D.W. 0.8 6 SW846: 6010C MMSD. 06/23/14 DM0623/14011513: 530 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/24/14 DM0624/14011540 540 mg/kg D.W. 0.8 6 SW846: 6016c MMSD 06/25/14 DM0625/14011566 560. mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/26/14 DM0626/14011766 600 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/27/14 DM0627/14011781 540 mg/kg D.W. 0.8 6 SW846: 60 10 C MMSD 06/28/14 DM0628/14011792 520 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 06/29/14 DM0629/14011811 530 mg/kg D-.W. 0.8 6 SW846: 6010C MMSD 06/30/14 DM0630/14011824 . .. 530 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 07/01/14 DM0701/14011851 520 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 07/02/14 DM0702/14011879 550 mg/kg D.W. 0.8 6 " SW846: 6010C MMSD 07/03/14 DM0703114011898 590 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 07/04/14 DM0704/14011911 550 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 07/05/14 DM0705/14011924 560 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 07/06/14 DM0706/14011943 550 mg/kg D.W. 0.8 6:. SW846: 6010C 'MMSD 07/07/14 DM0707/14012196 540 mg/kg.D.W. 0.8 6 SW846: 6010C MMSD 5YS/rpt1M11oMonth1y 1110113 tj Page 102 of 106 Printed. • 118/1510:96 , tMMSD Pdwigs IvIklEt,StR [YOUNN[w ZINC ICP METHOD Sample Date Sample ID Result LOQ QA Flags Annual Milorganite Report January 1 to December 31, 2014 Analytical Method Lab i 07/08/14 DM0708/14,012898 530 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 07/09/14 DM0709/14012926 540 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 07/10/14 DM0710/14012945 540 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 07/11/14 DM0711/14012961 610 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 07/12/14 DM0712/14012971 620 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/13/14 DM0713/14012991 640 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/14/14 DM0714/14013004 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/15/14 DM0715/14013031 620 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/16/14 DM0716/14013059 620 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/17/14 DM0717/14013078 640 mg/kg D.W. 0.S2 6 SW846: 6010C MMSD 07/18/14 DM0718/14013295 600 mg/kg D.W. 6.52 6 SW846: 6010C MMSD 07/19/14 DMO719/14013305 610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/20/14 DM0720/14013324 610 mg/kg D.W. 0.52 6. SW846: 6010C MMSD 07/21/14 DM0721/14013337 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/25/14 DM0725/14013997 630 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/26/14 DM0726/14014008 610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/27/14 DM0727/14014027 S70 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/28/14 DM0728/14014040 540 mg/kg D.W. '0.52 6 SW846: 6010C MMSD 07/29/14 DM0729114014895 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/30/14 DM0730/14014923 650 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 07/31/14 DM0731/14,014942 610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/01/14 DM0801/14014957 620 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/02/14 DM0802/14014968 620 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 08/03/14 DM0803/14014987 620 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 08/04/14 DM0804/14015000 600 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 08/05/14 DMO805/14015027 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/06/14 DMO806/14015405 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/07/14 DMO807/14015456 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/08/14 DM0808/14015471 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/09/14 DMO809/14015482 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/10/14 DMO810/14015966 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/11/14 DMO811/14015984 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/12/14 DMO812/14016011 560 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/13/14 DM0813/14016039 560 mg/kg D.W. 0.S2 6 SW846: 6616C MMSD 08/14/14 DMO814/14016058 610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/15/14 DM0815/14.016181 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/16/14 DMO816/14016192 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/17/14 DMO817/14016211 570 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/18/14 DM0818/14016290 540 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/19/14 DM0819/14016319 TDMO820/14016347 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/20/14 540 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/21/14 DM0821/14016366 490 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/22/14 DM0822/14016381 470 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/23/14 DM0823/14016392 560 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/24/14 DMO824114016411 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/25/14 DM0825/14016488 630 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 08/26/14 DMO826/14016515 620 mg/kg D.W. 0.52 6 SW846: 6010C MMSD SYS/rptlMi/oMonthiy 1110113 tj Page 103 of 106 Printed., 1/8/1510:48 ZINC ICP METHOD Sample Date Sample ID 08%28/14 .. DMO828/14016907 Result 540 mg/kg D.W. Lop 0.52 LOQ QA Flags 6 . Annual Milorganite Report January 1 to December 31, 2014 Analytical Method Lab ;:SW846: 6010C MMSD 08/29/14 DM0829/14017671 510 mg/kg D.W. 0.52 6 SW846: 6010C MMSD " 08/30/14 DM0830/14017682 530 mg/kg D.W. 0.52 6 SW846::6010C MMSD 08/31/14 DM0831114017701 610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 09/01/14 DMO901/14017714 650 mg/kg DA 0.52 6 SW846: 6010C MMSD 09/02/14 DMO902/14017871 630 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 09/03/14 DMO903/14017886 610 mg/kg D.W. 0.52 - 6 SW846::6010C MMSD .09/04/14 DM0904/14017920 640 mg/kg D.W. 0.52 6:. :.SW846: 6010C MMSD 09%OS/14 DM0905/1401790,1 590 mg/kg D.W. 0.52 6. SW846: 6010C MMSD 69/16/14 ' DM0916/14019167 680 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 09/17/14 DM0917/14019195 650 mg/kg D.W.. .:0.52 6 SW846: 6010C MMSD 09/18/14 DMO918/14019229 640 mg/kg D:W. 0.52 6.:. SW846: 6010C MMSD 09/19/14 DM091,9%14019244 680 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 09/20/14 DM0920/14019255 700 mg/kg D.W. 0.52 6 SW846:•6010C MMSD 09/21/14 DM0921/14019274 690 mg/kg D.W. 0.52. 6 SW846: 6010C MMSD 09/22/14 DMO922114019287 680 mg/kg D.W. 0.52 6:' ""SW846: 6010C MMSD 09%23/14 DM0923/14019778 640 mg/kg D.W. 0.52 '6 SW846: 6010C MMSD 09/24/14 DM0924/14019806 610 mg/kg D.W. 6.52 6 SW846::6010C MMSD 09/25/14 DM0925/14019825 610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 09/26/14 DM0926/14019840 650, mg/kg D.W. 0.52 6' "' SW846: 6010C MMSD 09/27/14 DM0927/14019851 690 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 09/28/14 DM0928/14019870. 690 mg/kg D.W. 6.52 6 SW846: 6010C MMSD 09/29/14 DM0929/14019883 740 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 09/30/14 DM0930/14019909 690 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/01/14 DM1001/14019927 710 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/02/14 DM1:002/14020572 770 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/03/14 DM1003/14020587 1200 mg/kg D.W. 0.52 6 Q3. SW846: 6010C MMSD 10/04/14 DM1004/14020598 720 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 10/05/14 DM1005114020617 700 mg/kg D.W. 0.8 6 SW846:.6010C MMSD 10/06/14 DM1006/14020630 750 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 10/07/14 DM1007114021108 750 mg/kg D:W. 0.8 6 SW846: 6010C MMSD 10/0,8/14 DM1008/140211.60 770 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 10/09/14 DM1.009/14021179 800 mg/kg D.W. 0.8 6 SW846:.6010C MMSD 10/10/14 DM1010/14021194 750 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 10/il/14 DM1011/14021244 730. mg/kg D.W. 0.52 6 "SW846: 6010C MMSD 10/12/14 DM1.012/14021263 740 mg/kg D.W. 0.52 6 SW846: 6010C.. MMSD 10/13/14 DM1013/14021276: 750 mg/kg D.W: '0.52 .: 6 SW846:6010C MMSD 10/14/14 DM1014/14021304 760 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/15/14 DM1015/14021332 770 mg/kg D.W. 0.52 6 SW846: 6010C 'MMSD 10/16/14 DM1016114021351 ... 820 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/17/14 DM1:017/14021787 .810 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/18/14 DM1018/14021798 780 mg/kg D.W. 0.52 6 . SW846: 6010C MMSD ' 10/19/14 DM1019114021817 780 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/20/14 DM1020/14021830 750 mg/kg D.W. 0.52 6 SW846:. 6010C MMSD 10/21/14 DM1.021/14021857 750 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/22/14 DM1022/14021885 770 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/23/14 DM1023/14022256 760 'mg/kg D.W. 0.52 6 SW846: 6010C MMSD. SYS/rptlMi/oMonth/y 1110113 tj -' - Page 104 of 106 Printed• 1/8/1510:48 1 MSD. PdA kis m d al." form ZINC ICP METHOD SarhPle Date, Sam 1 0 10/24/14 DM1024/14022273 7S0 mg/kg D.W. ®0 0.52 6 Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 10/25/14 DM1025/1:4022286 760 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/26/14 DM1026/14022305 770 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/27/14 DM11027/14022318 710 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/M/14 DM1028/14022409 740 :mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/29/14 DM1029/14022439 750 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 10/30/14 DM1030/14022510 640 mg/kg D.W. 0.52 6 SW846:; 6010C MMSD 10/31/14 DM1031/14022525 720 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/01/14 DM1101/14022536 700 mg'/kg D.W. 0.52 6' SW846: 6010C MMSD 11/02/14 DM1102/14022555 650 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/03/14 DM1103/14022568 650 mg/kg D.W: 0.52 6 SW846:6010C MMSD 11/04/14 DM110.4/14023111 580 mg/kg D.W. 0.52 6_ „SW846: 6010C MMSD 11/05/14 DM1105/14023139 620 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/06/14 DM1106/14023158 610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/07/14 DO 107/14023173 650 mg/kg D.W. 0.52 6 SW846:6010C MMSD 11/08/14 DM1108/14023184 680 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/09/14 DM1109/14023203 640 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/10/14 DM1110/14023767 660 mg/kg D.W. 0.52 6 SW846:, 6010C MMSD 11/11/14 DM1111/14023796 630 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/12/14 DM1112/14023876 650 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/13/14 DM1113/14023895 590 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/14/14 DM1:114/14023910 650 mg/kg D.W: 0.52 6 SW846:.6010C MMSD 11/15/14 DWI15/14023929 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/1'6/14 DM1116/14623948 560 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/17/14 DM1.117114023961 560 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/18/14 DM1:118/14024236 600 mg/kg D.W: 0.52 6 SW846: 6010C MMSD 11/19/14 DM1'119/14024264 620 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/20/14 DM1120/14024283 650 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/21/14 DM1121/14024302 680 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/22/14 DM1122/14024313 690 mg/kg D.W: 0.52 6 SW846: 6010C MMSD .11/23/14 DM1123/14024393 670 mg/kg D.W. 0.52 .6 SW846: 6010C MMSD 11/24/14 DM1124/14024414 730 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/25/14 DM1125/14024441 670 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/26/14 DM1126/14024469 590 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/217/14 DM1127/14024529 670 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 11/28/14 DM1128/14024544 690 mg/kg D.W. 0.52 6 . SW846: 6010C MMSD 11/29/14 DM1.129/14024555 680 mg/kg D.W: 0.52 6 SW846: 6016C MMSD 11/30/14 DM1:130/14024574 670 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/61/14 DM1201/14024601 650 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/02/14 DM1202/14025299 620 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/03/14 DM1203/14025327 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/04/14 DM1204/14025346 610 mg/kg D.W. 0.52 6. SW846: 6010C MMSD 12/65/14 DM1205/14025361 600 Mg/kg D:W. 0.52 6 SW846: 6010C 'MMSD 12/06/14 DM1206/14025372 610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/07/14 DM1207/14025391 600 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/08/14 DM1208/14025404 590 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/09/14 DM1209/14026170 610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD SYS/rptimloMonth/y 1110113 U Page 105 of 106 Printed.• 1/8/1510:48 G as»ages 144a'rt��t �/u�M�tat ZINC ICP METHOD: sapfple Date Sample ID 12/10/14 .. DM1210/14026198 630 mg/kg D.W. 0.52 aMethod 6 Annual Milorganite Report January 1 to December 31, 2014 SW846: 6010C MMSD 12/11/14 DM121'1/14026217 580 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/12/14 "' DM1212/14026232 600 mg/kg D.W.' 0'.52 6 SW846:'6010C MMSD 12/13/14 DM1213114026243 570 mg/kg D.W. 0.52 6. SW846: 6010C MMSD, 12/14/14 DM1214/14026262 520 mg/kg D.W. 0.52 6. SW846: 6010C MMSD 12/15/14 DM1215/14626277 526 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/16/14 DM1216/14026475 480 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/17/14 DM1217/14026503 530 mg/kg D.W. 0.52 6. SW846: 6010C MMSD 12/18/14 DM1218/14026522 520 mg/kg D.W. 0.52 6' SW846: 6010C MMSD 12/19/14 DM1219/14026537 S30 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/20/14 DM1220/14026653 500 mg/kg D.W. '0.52 6 SW846: 6010C MMSD : 12/21/14 DM1221/14026672 500 mg/kg' D.W. 0.52 6.'. 'SW846: 6010C MMSD 12%22/14 . DM1222/14026686 520 mg/kg D.W. 0.52 6 Q2. SW846: 6010C MMSD 12/23/14 DM1223/14026713 530 mg/kg D.W. 0'.52 6 SW846:6010C MMSD 12/24/14 DM1224/14026741 550 mg/kg D.W. 0.52 6 SW846: 6010C MMSD -.12/25/14 DM1225/14026760 590 rrig/kg D.W. 0.52 6, SW846: 6010C MMSD 12/26/14 DM1226/14026771 610 mg/kg D.W. 0.52 6 SW846: 6010C MMSD 12/27/14 DM1227/14026788 .610 mg/kg D.W. 0.8 6 SW846: 6010C MMSD 12/28/14 DM1228114026807 590 mg/kg, D.W. 0.8 6. SW846: 6010C MMSD 12/29/14 DM1229/14027031 600 mg/kg D.W. 0.8 6: SW846: 6010C MMSD 12/30/14 ' DM1230/14027058 600 mg/kg D.W. 0.8 6 SW846: 6010C: MMSD 12/31/14 DM1231/14027086' :590 mg/kg D.W. 0.52 6 SW846: 6010c MMSD Flan Descripti6ns Avg: S80 mg/kg D.W. Max: 1200 mg/kg D.W. AD Other Flag requires additional explanation IS Insufficient sample volume for analysis. AX.. Qualified data - see contract lab report 7 Estimated concentration above the adjusted method detection limit B3 : Target analyte detected in method blank > 10% of sample and:bel6W ;the adjusted reporting limit concentration. LA Not analyzed - lab accident. B7 LCS recovery was above control limits. MI Too numerous to count. B8 LCS recovery -was below control limits. Mi Sample incubation period exceeded method requirement. B9 Low Level CCV recovery was outside of method acceptance limits M3 Spreading_ colonies - unable to determine result. to' Data used for calculation of'result was qualified MS Incubato0w' ater.bath temperature was outside method DI Duplicate precision control limit was exceeded. requirements. D2 Matrix.spike:precision control limit was exceeded.. M7 Micro sample received without adequate headspace. D3 Sample is heterogeneous. Sample homogeneity could not be M9 ' Target organism detected in associated method blank. readily achieved using routine laboratory practices. NO Not usable Data. W Sample was received past holding time. Q2 Matrix spike recovery for this sample was above :control limits. H3 Analysis performed beyond holding time. Q3 Matrix spike recovery for this sample was below control limits. H4 Initial analysis within holding time. Reanalysis for the required RT Sample temperature upon receipt exceeded regulatory or project dilution was_past holding time. requirements. Ai :: Analysis performed beyond holding time. SS Reading was not confirmed by a constant.weight measurement T3 The dilution water D.O. depletion was > 0.2 mg/L. T4 GGA 80D was below method acceptance criteria. TS GGA BOD was above method acceptance criteria. T7 The dilution water D.O. increase was > 0.2 mg/L. Page 106 of 106 5Y5/rpt1ki1bMonth/y 1110113 tj Printed:1/8/1510:48 2014 IVlilorganite Daily Production Samples COLLECTION DATE PCB Aroclors. (ppb)1 PCB-10.16, PCB-1221 PCB=1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260 Total PCBs. 1/1/14 < 53 < 53 < 53 < 53 < 53 < 53 56 56 1/2/14 < 54 < 54 < 54. < 54 < 54 < 54 58 58 1/3/14 < 53 < 53 < 53 < 53 < 53 < 53 85 85 1/4/14 : < 54 < 54 < 54 < 54 < 54 < 54, 63 63 1/5/14 < 54 < 54 < 54 < 54 < 54 < 54 58 58 1/6/14 < 55 < 55 < 55 < 55 < 55 < 55 65 65 < 54 < 54 < 54 < 54 < 54 < 54 68 68 1/8/14 < 54 < 54 < 54 < 54 < 54 < 54 96 96 1/9/14 < 54 < 54 < 54 < 54 < 54 < 54 55, 55. 1/10/14 < 54 < 54 <'54 < 54 < 54 < 54 56: 56 1/11/14 < 53 < 53 < 53 < 53 < 53 < 53, 56 56 1/12/14 < 55 < 55 < 55 < 55 < 55 < 55 57 57 1/13/14 < 53 < 53 < 53 < 53 < 53 " < 53 61. 61 1/14/14P . < 53 < 53 < 53 < 53 < 53 < 53 85 85 1/15/14' < 27 < 27 < 27 31 < 27 < 27' 90 120 1/16/14 < 26 < 26 < 26 35 < 26 < 26 110 140 1/17/14 < 27 < 27 < 27 30 < 21 < 27 95 120 1/18/14 < 27 < 27 < 27 31 < 27 < 27 92 12.0 1/19/14 < 27 < 27 <.27 28 < 27 < 27 80 110. 1/20/14 . < 27 < 27 < 27 35 < 27 < 27 84 120 1/21/14 < 27 < 27 < 27 37 < 27 < 27 75 110 1/22/14 < 28, < 28 < 28 : 34 < 28 < 28 73 110 1/23/14 < 55 < 55 < 55 < 55 < 55 < 55 78 78 1/24/14 < 54 < 54 < 54 < 54 < 54 < 54 79 79 1/25/14 < 54 < 54 < 54 < 54 < 54 < 54 64 64 1/26/14 < 54 < 54 < 54 < 54 < 54 < 54 76 76 1/27/14. < 54 < 54 < 54 < 54 < 54 < 54 71 71 1/28/14' < 27 < 27 < 27 34 < 27 < 27 94 130 1/29/14 < 26 < 26 <16. 37 < 26 < 26 88 120 1/30/14:: < 52 < 52 < 52 < 52 < 52 < 52 91 91 1/31/141 < 52 < 52 < 52 < 52 < 52 < 52 92 92 2/1/14 < 54 < 54 < 54 < 54 < 54 < 54 78 , 78 2/2/14 < 54 < 54 < 54 < 54 '< 54 < 54 68 68 2/3/14 < 54 < 54 < 54 < 54 < 54 < 54 80 80 2/4/14 < 54 < 54 < 54 . < 54 < 54 < 54 71 71 2/5/14 < 26 < 26 <:26 < 26 < 26 < 26 82 82 2/6/14 . < 52 < 52 < 52 < 52 < 52 < 52 96 96 2/7/14 < 54 < 54 < 54 < 54 < 54 < 54 88 1 88 2/8/14 < 54 < 54 < 54. < 54 < 54 < 54 93 93 2/9/14 < 54 < 54 < 54 < 54 < 54 < 54 85 85 2/10/14 < 54 < 54 < 54 < 54 < 54 < 54 90 90 2/11/14 < 53 < 53 <:53 < 53 <. 53 < 53 95 95 2/12/14 . < 54 < 54 < 54 < 54 < 54 < 54 84 84 Page 1 of 9 2014 Milorganite Daily: Production Sam- pies COLLECTION DATE PCB Aroclors , b )l (pp PCB-1016 PCB-1221 PCB=1232 PCB-1242 PCB-1248 PCB-1254 PC9-1260 TotalPCBs 2/13/14 < 54 < 54 < 54 '54 < 54 < 54 78 78 .1. 2/14/14 < 27 < 27 < 27 -< 30 < 27 < 27 92 120 2/15/14 < 53 < 53 < 53 < 53 < 53 < 53 84 84 2/16/14 < 53 < 53 < 53 <:53 < 53 < 53 81 81 2/17/14 < 53 < 53 < 53 < 53 < 53 < 53 86 86 2/18/14 < 54 < 54 < 54 < 54 < 54 < 54 86 86 2/19/14 < 54 < 54 < 54 < 54 < 54 < 54 81 81 2/20/14 < 53 < 53 < 53 < 53 < 53 < 53 85 85 2/21/14 < 54: < 54 < 54 < 54 < 54 < 54 90 90 2/22/14 < 54 < 54 < 54 < 54 < 54 < 54 120 120 2/23/14 <52 < 52 < 52 < 52 < 52 < 52 92 92 2/24/14 < 54 < 54 < 54 < 54 < 54 < 54 97 97 2/25/14 < 54 < 54 < 54 < 54 < 54 < 54 67 67 2/26/14 < 53 < 53 < 53 < 53 < 53 < 53 63 63 2/27/14 < 54.. < 54 < 54 < 54 < 54 < 54 65 65 2/28/14 < 54 < 54 < 54 < 54 < 54 < 54 66 66 3/1/14 < 53 < 53 < 53 < 53: < 53 < 53 88 88 3/2/14 < 54 < 54 < 54 54 < 54 < 54 96 150 3/3/14 < 53 < 53 < 53 61 < 53 < 53 100 160 3/4/14 < 53 < 53 < 53 < 53 < 53 < 53 110 110 3/5/14 < 54 < 54 < 54 60 < 54 < 54 93 150 3/6/14 < 53 < 53 < 53 < 53 < 53 < 53 72 72 3/1/14 < 54 < 54 < 54 < 54 < 54 < 54 67 1 67 3/8/14 < 54 < 54 < 54 < 54 < 54 < 54 79 79 3/9/14 < 53 < 53 < 53 66 < 53 < 53 120 180 3/10/14 < 54 < 54 < 54 65 < 54 < 54 140 200 3/11/14 < 54 < 54 < 54 63 < 54 < 54 120 190 3/12/14 < 53 < 53 < 53 55 < 53 < 53 96 150 3/13/14 < 52 < 52 < 52 64 < 52 < 52 96 160 3/14/14 < 52 < 52 < 52 64 < 52 < 52 85 150 3/15/14 < 54 < 54 < 54 71 < 54 < 54 120 190 3/16/14 < 52 < 52 < 52 64 < 52 < 52 120 1 180 3/17/14 < 54 < 54 < 54 61 < 54 < 54 110 170 3/18/14 < 54 < 54 < 54 69 < 54 ¢ 54 120 190 3/19/14 < 52 < 52 < 52 < 52 < 52 < 52 120 120 3/20/14 < 53 < 53 < 53 < 53 < 53 < 53 92 92 3/21/14 < 53 < 53 < 53 < 53 < 53 < 53 87 87 3/22/14 < 52 < 52 < 52 < 52 < 52 < 52 130 130 3/23/14 < 52 < 52 < 52 < 52 < 52 < 52 100 100: 3/24/14 < 52 < 52 < 52 62 < 52 < 52 74 140 3/25/14 < 52 < 52 < 52 67 < 52 < 52 82 15'0 3/26/14 < 53:: < 53 < 53 < 53 < 53 < 53 54 54 3/27/14 < 52 <,52. < 52 <.52 < 52 < 52 < 52 < 52 Page 2 of 9 6 Jo E aged tiS > tiS > tis > tiS > bS > tiS > 1iS > tiS > tiT/6/S SS > ss.> SS > SS > Ss > SS > SS > SS > tit/9/S 69 69 tiS > tiS > tiS > tiS > tiS > tiS > tVI/S OL OL tiS > tiS > tiS > tiS > tiS > tiS > tiT/9/S 96 .96 ZS > zs >. ZS > ZS:> zs > zs > tiT/S/S 88 89 ZS > ZS > zs > ZS > zs > zs > tiT/ti/S tiL tiL tiS > tiS > tiS > tiS > t s > tiS > . tiT/E/S OOT DOT ES > ES > ES > Es > ES > ES > tiT/Z/S, 88 88 :. ZS > ZS > ZS > ZS > Zs > ZS > tiT/T/S 6L 6L £S >.. ES > ES > ES > £S > ES > tiT/OE/ti 99 .99 ES > ES > ES > ES,> ES > £S > tiT/6Z/ti OOT ooi zs > Zs :>: ZS > ZS > zs > zs > tiT/8Z/ti ooT OOT ES > ES > ES > ES > ES > ES > tiT/LZ/ti 96 96 ES >., ES > £S > ES > £S > ES > tiT%9Z/ti 68 68 ES > ES > ES > ES:> £S > ES > tiT/SZ/ti 9L 9L zs > zs > zs > zS > ZS > ZS > tit/tiZ/ti SL SL £S > ES > ES > ES > £S > ES > tiT/EZ/ti OLT OTT ZS > zs > 8s ZS > ZS > ZS > tiT/ZZ/ti 091 96 tiS > tiS > 99 17S > tiS > tiS > tiT/TZ/ti OLT OTT ES > £S > S9: ES > ES > ES > tiT/OZ/ti m tis ss > SS >: 6S ss > SS > SS > tiT/6T/ti Z9 Z9 SS > ss. > ss > ss:> Ss > SS > tiT/9t/:ti 99 99 SS > SS > SS > SS > SS > Ss > 'tit/LT/ti z8 Z8 ss > SS > SS > SS > SS > SS > tiT/9T/ti ss s8 tiS > tiS >. tiS > tFs > tiS > tiS > tiT/ST/ti LL LL VS > tiS > tiS >. tiS > tiS. > tiS > tiT/tiT/ti 6L 6L ZS >' ZS > Zs > ZS > zs > ZS > tiT/ET/ti tiL tiL tiS > tiS > tiS > tiS > tiS > tis > tiT/ZT/ti 69 69 ES > . ES > ES > Es > ES > £S > tiT/Zi/ti 9L 9L ES > ES > ES > ES > £s.> ES > tiT/OT/ti ZL ZL ES > ES > ES > £S > ES > ES > tit/6/ti 08 08 ES > ES. >: ES > ES > £S > ES > tit/8/ti 68 68 ES > ES > £S > ES > ES > ES > tiZ/L/ti 08 08 tiS > tiS > tiS > tiS > tiS > tiS > tiT/9/ti OOT 60Z .: zs > Z:s > zs > ZS > zs > Zs > tiT/S/ti 08 ZS 9Z > 9z > 6? 9Z > 9Z > 9z > 1 tIft, LL Lti LZ > LZ > O£ LZ > LZ > LZ > tit/£/V 08 T ti LZ > LZ > 6E LZ > LZ > LZ > tit/Z/ti S6 LS 9Z > 9Z > 8£ 9z > 9z > 9Z > tiT/T/ti tiL tiL Zs >, zs > Zs > zs > zs > zs > :tiT/TE/E tis tis ZS > ZS > ZS > ZS > zs > zs > tit/OE/E L9 L9 ES > Es > ES > ES > £S > tS > tiT/6Z/t ZS > ZS > ZS > zs > ZS ? . zs > Zs > . zs > ...t?.T/8Z/E s.83d IBIOI 09ZT`83d tlSZT-83d 8bZT-83d ZbZT-83d ZEZT-83d TZZT-83d 9TOT-83d Uva NO113311O3 T(gdd.) sjol3ojV Md saldwes uoil:)npoad Alm amuesaoM vToz 2014 Milorganite Daily Production Samples COLLECTION DATE PCB koclors _(ppb)1 PC97-1016 PCB-1221 PC9-1232 PCB-1242 PCB-1248 PCB-1254 PCEi-12601 Total PCBs 5/10/14 < 53 < 53 < 53 < 53 < 53 < 53 70 70 5/11/14 < 54. < 54 < 54 < 54 < 54 < 54 < 54 < 54 5/12/14 < 54 < 54 < 54 < 54 < 54 < 54 < 54 < 54 5/13/14 < 53 < 53 < 53 <S3 < 53 < 53 . 76 76 5/14/14 < 53 < 53 < 53 < 53 < 53 < 53 98 98 5/15/14 < 53 < 53 < 53 < 53 < 53 < 53 82 82 5/16/14 < 52 < 52 < 52 < 52 < 52 < 52 97 97 5/17/14 < 53 < 53 < 53 < 53 < 53 < 53 100 100 5/18/14 < 53 : < 53 < 53 < 53 < 53 < 53 94 94 5/19/14 < 54 < 54 < 54 .554 < 54 < 54 89 89 5/20/14 < 54 < 54 < 54 < 54 < 54 < 54 : 90 90 5/21/14 < 53, < 53 < 53 < 53 < 53 < 53 75 75 5/22/14 < 52 < 52 < 52 < 52 < 52 < 52 87 87 5/23/14 < 52 < 52 < 52 < 52 < 52 < 52 94 94 5/24/14 < 54 < 54 < 54 < 54 < 54 < 54 70 70 5/25/14 < 5.4 < 54 < 54 < 54 < 54 < 54 67 67 5/26/14 < 54 < 54 < 54 <.54 < 54 < 54 69 69 5/27/14 < 53 < 53 < 53 < 53 < 53 < 53 80 80 5/28/14 < 53- < 53 < 53 < 53 < 53 < 53 75 75 5/29/14 < 53 < 53 < 53 < 53 < 53 < 53 76 76 5/30/14 < 54 < 54 < 54 < 54 < 54 < 54 78 78 5/31/14 < 53 < 53 < 53 < 53 < 53 < 53 78 78 6/1/14 < 54 < 54 < 54 < 54 < 54 < 54 63 63 6/2/14 < 54 < 54 < 54 < 54 < 54 < 54 65 65 6/3/14 < 54 < 54 < 54 < 54 < 54 < 54 74 74 6/4/14 < 54 < 54 < 54 < 54 < 54 < 54 72 72 6/5/14 < 53 < 53 < 53 < 53 < 53 < 53 76 76 6/6/14 < 54 < 54 < 54 < 54 < 54 < 54 75 75 6/7/14 < 53 < 53 < 53 < 53 < 53 < 53 73 73 6/8/14 < 53 < 53 < 53 < 53 < 53 < 53 83 83 6/9/14 < 53 < 53 < 53 < 53 < 53 < 53 . 81 81 6/10/14 < 53 < 53 < 53 < 53 < 53 < 53 75 75 6/11/14 < 53 < 53 < 53 < 53 < 53 < 53 91 91 6/12/14 < 54 < 54 < 54 < 54 < 54 < 54.90 90 6/13/14 < 53 < 53 < 53 < 53 < 53 < 53 78 78 6/14/14 < 53 < 53 < 53 < 53 < 53 < 53 73 73 6/15/14 < 54 < 54 < 54 < 54 < 54 < 54 62 62 6/16/14 < 54 < 54 < 54 < 54 < 54 < 54 62 62 6/17/14 < 54 < 54 < 54 < 54 < 54 < 54 67 67 6/18/14 < 54 < 54 < 54 < 54 < 54 < 54 92 92 6/19/14 < 53 < 53 < 53 < 53 < 53 < 53 81 81 6/20/14 < 53 < 53 < 53 < 53 < 53 < 53 95 95 6/21/14 < 53 < 53 < 53 < 53 < 53 < 53 77 77 Page 4 of 9 6 10 S 08ed 176 t,6 t,S > t,S > tiS > tiS > tiS > tt5 > tit/9/8 ON 68 8Z > 8Z > 6Z 8.Z.> 8Z > 8Z > tiT/S/8 58 S8 tiS > t,S > t,S > tiS > t7S > VS > t,T/t,/8 OOT OOT £S > ES > ES > ES > ES > ES > t T/£/8 E6 £6 £S > ES >: ES > ES > ES > ES > t,T/Z/8 88 88 t,S > t,5 > t,S > tiS > t,S > t,S > KAM OET L6 LZ > LZ > t,E LZ > LZ >' LZ > KA£/L OTT OTT LZ > LZ > LZ > LZ.> LZ > LZ > tit/OE/L OZT Z6 LZ > LZ > 8Z LZ > LZ > LZ > tT/6Z/L OET OOT 8Z > 8Z > T£ 8Z > 8Z > 8Z > tT/8Z/L 09T OZT LZ > LZ > 9E LZ > LZ > LZ > tiTUM 09T ON 9Z > 9Z >. 9E 9Z > 9Z > 9Z > t,T/9Z/L 06T Ot,T 9Z > 9Z > Et, 9Z > 9Z > 9Z > t T/SZ/L OZT OZT t,S > t,S > t,S > t,S > tiS > t,S > tT/TZ/L OZT OZT tiS > t7S > t,5 > is > tiS > tiS > tT/OZ/L OZT OZT SS > SS > SS > SS > SS > SS > t T/6T/L T L T L t7S > t7S > t,5 > tiS > t,S > tiS > ST/L 08T OVT LZ > LZ > 9t, LZ > LZ > LZ > tT/LT/L OTZ 09T 9Z > 9Z > ZS 9Z > 9Z > 9Z > t T/9T/L OZZ OLT 9Z > 9Z > SS 9Z > 9Z > 9Z > tiT/ST/L OZZ OLT 9Z > 9Z > ZS 9Z.> 9Z > 9Z > t7T/t,T/L OTZ 69T LZ > LZ > t,5 LZ.> LZ > LZ > VVET/L OOZ OST LZ > LZ > ZS LZ > LZ >. LZ > t,T/ZT/L 08T OET LZ > LZ > St, LZ > LZ > LZ > -WTT/L OLT OZT LZ > LZ > St, LZ > LZ > LZ > t T/OT/L 091 OTT LZ > LZ > 81i LZ > LZ >. LZ > V116/L 09T OZT LZ > LZ > 6ti LZ > L'Z > LZ > tT/8/4 OLT OZT LZ > LZ >: ZS LZ.> LZ > LZ > t,T/L/L OLT OZT LZ > LZ > ZS LZ > LZ > LZ > tiT/9/L OLT OZT 9Z > 9Z > TS 9Z > 9Z > 9Z > tT/S/L 09T OTT 9Z > 9Z >: Lt, 9Z > 9Z > 9Z > tT/t,/L 09T ON LZ > LZ > St, LZ > LZ > LZ > VVE/L 091 OZT 8Z > 8Z > 6E 8Z > 8Z > - 8Z > t T/Z/L Z6 Z6 SS > SS > SS > SS > SS > SS > tiT/T/L 96 96 tiS > t,.5 > t,S > tiS > t,S > tiS > t T/0£/9 OTT OTT tiS > t,S > t,5 > t,S > t,5 > t,S > t T/6Z/9 L6 L6 t,5 > t,S > t,S > tiS > tiS > t,S > t,T/8Z/9 OET L6 LZ > LZ >. t,E LZ > LZ > LZ > t7T/LZ/9 86 86 ES > ES > ES > £S > ES > ES > t T/9Z/9 08T . OET LZ > LZ > SS LZ > LZ > LZ > -t T/SZ/9 E8 E8 ES > ES > ES > ES > £S > ES > tit/tiZ/9 Z8 Z8 ZS > ZS > ZS > ZS > ZS > ZS > t,T/EZ/9 8L 8L ES > £S > ES > I £S > ES > . ES > t T/ZZ/9 S93d IBTol 09ZT-83d I t7SZT-8:)d I 8VZT-83d I ZtZT-8Jd I ZEZT-133d TZZT-83d. 9ZOT-8Jd 31V(3 N011331103 T(gdd) saol3oad 83d saldweS uoil�npoad Allen alluegaol,lw titOZ 2014 Milorganite Daily Production Samples COLLECTION DATE PCB Aroclors (ppb) PCB-1016 PCB-1221 00-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260 Total PCBs 8/7/14 < 54 < 54 < 54 < 54 < 54 < 54 79 79 8/8/14 < 28 < 28 < 28 < 28 < 28 < 28 61 61 8/9/14 < 54 < 54 < 54 < 54 < 54 < 54 90 90 8/10/14 < 53 < 53 < 53 < 53 < 53 < 53 150 150 8/11/14 < 53 < 53 < 53 < 53 < 53 < 53 210 210 8/12/14 < 54 < 54 < 54 < 54 < 54 < 54 310 310 8/13/14 < 55 < 55 < 55 < 55 < 55 < 55 380 380 8/14/14 < 52 < 52 < 52 < 52 < 52 < 52' 630 630 8/15/14 < 53 < 53 < 53 < 53 < 53 < 53 540 540 8/16/14 < 53 < 53. < 53 < 53. < 53 < 53 490 490 8/17/14 < 52 < 52 < 52 < 52 < 52 < 52 : 510 510 8/18/14 < 54 < 54 < 54 < 54 < 54 < 54 490 490 8/19/14 < 52 < 52 < 52 < 52 < 52 < 52 580 580 8/20/14 < 52 < 52 < 52 < 52 < 52 < 52 310 1 310 8/21/14 < 53 < 53 < 53 < 53 < 53 < 53 180 180 8/22/14 < 54 < 54 < 54 < 54 < 54 < 54 160, 160 8/23/14 < 53 < 53 < 53 < 53 < 53 < 53 220 220 8/24/14 < 53 < 53 < 53 < 53 < 53 < 53 400 400 8/25/14 < 53 < 53 < 53 < 53 < 53 < 53 280 280 8/26/14 < 52 < 52 < 52 < 52 < 52 < 52 580 580 8/28/14 < 52 < 52 < 52 < 52 < 52 < 52 410 410 8/29/14 < 52 < 52 < 52 < 52 < 52 < 52 270 270 9/30/14 < 54 < 54 < 54 220 < 54 < 54 310 520 8/31/14 < 53 < 53 < 53 < 53 < 53 < 53 420 420 9/1/14 < 52 < 52 < 52 < 52 < 52 < 52 440 440 9/2/14 < 54 < 54 < 54 < 54 < 54 < 54 640 640 9/3/14 < 54 < 54 < 54 < 54 < 54 < 54 520 520 9/4/14 < 52 < 52 < 52 < 52 < 52 < 52 560 560 9/5/14 < 52 < 52 < 52 < 52 < 52 < 52 520 520 9/16/14 < 52 < 52 < 52 < 52 < 52 < 52 440 440 9/17/14 < 52 < 52 < 52 < 52 < 52 < 52 500 1 500 9/18/14 < 52.. < 52 < 52 < 52 < 52 < 52 340 340 9/19/14 < 52 < 52 < 52 < 52 < 52 < 52, 200 200 9/20/14 < 52 < 52 < 52 < 52 < 52 < 52 380 380 9/21/14 < 52 < 52 < 52 < 52 < 52 < 52 400 400 9/22/14 < 52 < 52 < 52 < 52 < 52 < 52 380 1 380 9/23/14 < 54 < 54 < 54 < 54 < 54 < 54 320 320 9/24/14 < 54 < 54 < 54 < 54 < 54 < 54 310 310 9/25/14 < 5.3 < 53 < 53 < 53 < 53 < 53 340 340 9/26/14 < 52 < 52 < 52 < 52, < 52 < 52 340 340 9/27/14 < 54 < 54 < 54 < 54 < 54 < 54 320 320 9/28/14 < 5.4 < 54 < 54 < 54 < 54 < 54 340 340 9/29/14 . < 53 < 53 < 53 < 53. < 53 < 53 390 390 Page 6 of 9 6 10 L 09ed ON OOZ SS >' SS > SS > SS > SS > SS > tiT/TT/TT OZZ ON VS > tiS >: t'S > t'S > t'5 > tiS > tbT/OT/TT. ON ON tiS > t'S > tiS > tiS > tiS > tiS > tFT/6/TT OZ£ 09Z ES > ES > 95 ES > ES > ES > t T/8/TT 06Z ObZ tiS > tiS > SS bS > tiS > tiS > t7T/L/TT OOE OSZ SS > SS > 95 SS > SS > SS > t�T/9/TT OST OST 9S > 95 > 95 > 9S > 9S > 95 > t?T/S/TT OZ£ 09Z t'S > t'S >. 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SS > VT/OZ/OT OZZ OZZ t?5 > t'S > tiS > tiS > ii5 > t'S > t�T/6T/OT OZZ OZZ :: SS > SS > SS > SS > SS > SS > tT/8T/OT OLti OTb £S > ES > 09 ES > £S > ES > tiT/LT/OT Obt, 08E £S > ES > LS ES > £S > ES > i7T/9Z/OT OR ON SS > SS >, SS > SS .> SS > SS > t T/SI/OT OLT OLT t'S > tiS > t'S > tiS > t'S >. tiS > t T/t T/OT 0ST 08T t7S > t'S > 17S ?. b5 > t'S > tiS > tiT/ET/OT 09T 09T SS > SS > SS > SS > SS > SS > t T/ZT/OT OLT OLT SS > SS > SS > SS > SS > SS > t T/Tt/OT OOti OVE t'S > t'S > L9 t'S > t'S > tFS > WOT/OT OOt, OEE ES > ES > 69 ES_> £S > ES > KNOT OEE OLZ tiS > t'S > 6S tiS-> tiS > ti5 > t T/8/OT 0£ti 09E t'S > t'S > SL t'S > tiS > t'5 > VT/L/OT OSti .08E ZS > ZS > 89 ZS > ZS > ZS > tiT/9/OT 06E OEE tiS > VS > SS t s > tiS > t'5 > t T/S/OT OEE OEE ES > ES > ES > £S > ES > ES > -tT/tr/OT 08t, OZt, ZS > ZS > S9 ZS > ZS > ZS > aI/E/OT 0£ti OLE t'5 > t'S > 85 tiS > t'S > is > t T/Z/OT OEZ OEZ ES > ES > ES > ES > ES > ES > t T/T/OT OSZ OSZ ZS > ZS > ZS > ZS > ZS > ZS > iiT/0£/6 St3:)d P101 09ZZ-135d t7SZT-B:)d BbZT-O:)d ZbZT-8Jd ZEZT-93d TZZT-8:)8 9tOT-83d 31Va N011331103 ,(qdd) SA0130JV 80d saidwes uoipnpWd Alien ajaueSaojiw mtFTOZ 2014 Milorganite Daily Production Samples COLLECTION DATE PCB Aroclors (ppb)1 PCB-1016 PCB-1221 PCB=1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260 Total PCBs 11/12/14 < 54 < 54 < 54 < 54 < 54 < 54 _ 210 210 11/13/14 < 53 < 53 < 53 < 53 < 53 < 53 190 190 11/14/14 < 53 < 53 < 53 < 53 < 53 < 53 180 180 11/15/14 < 54 < 54 < 54 < 54 < 54 < 54 200 200 11/16/14 < 54 < 54 < 54 < 54 < 54 < 5.4 160 160 11/17/14 < 55 < 55 < 55 < 55 < 55 < 55 160 160 11/18/14 < 54 < 54 < 54 < 54 < 54 < 54 160 160 11/19/14 < 55 < 55 < 55 < 55 < 55 < 55 200 200 11/20/14 < 53 < 53 <.53 < 53 < 53 < 53 190 190 11/21/14 < 53 < 53 < 53 < 53 < 53 < 53 180 180 11/22/14 < 54 < 54 < 54 < 54 < 54 < 54 180 180 11/23/14 < 55 < 55 <:55 < 55 .< 55 < 55 180 180 11/24/14 < 55 < 55 < 55 < 55 < 55 < 55 200, 200 11/25/14 < 54 < 54 < 54 < 54 < 54 < 54 180 180 11/26/14 < 54 < 54 < 54 < 54 < 54 < 54 210 210 11/27/14 < 55 < 55 < 55 < 55 < 55 < 55 220. 220 11/28/14 < 53 < 53 < 53 < 53 < 53 < 53 210 210 11/29/14 < 54 < 54 < 54 < 54 < 54 < 54 190 190 11/30/14 < 58 < 55 < 55 < 55 < 55 < 55 190 190. 12/1/14 < 54 < 54 < 54 < 54 < 54 < 54 180 180 12/2/14 < 54 < 54 < 54 < 54 < 54 < 54 180 180 12/3/14 < 55 < 55 < 55 < 55 < 55 < 55 150 150 12/4/14 < 544 < 54 < 54 < 54 < 54 < 54 160 160 12/5/14 < 54 < 54 < 54 < 54 < 54 < 54. 150 150 12/6/14 < 54 < 54 < 5.4 < 54 < 54 < 54 150 150 12/7/14 < 54 < 54 < 54 < 54 < 54 < 54 150 150 12/8/14 < 54 < 54 < 54 < 54 < 54 < 54 160 160 12/9/14 < 53 < 53 < 53 < 53 < 53 < 53 150 150 12/10/14 < 53 < 53 < 53 < 53 < 53 < 53 140 140 12/11/14 < 54 < 54 < 54 < 54 < 54 < 54 150 150 12/12/14 < 54 < 54 < 54 < 54 < 54 < 54 130 130 12/13/14 < 54 < 54 < 54 < 54 < 54 < 54 120 120 12/14/14 < 54 < 54 < 54 < 54 < 54 < 54 98 98 12/15/14 < 55 < 55 < 55 < 55 < 55 < 55 86 86 12/16/14 < 54 < 54 < 54 < 54 < 54 < 54 100 100 12/17/14 < 55 < 55 < 55 < 55 < 55 < 55 110 110 12/18/14 < 56 < 56 < 56 < 56 < 56 < 56 140 140 12/19/14 < 54 < 54 < 54 < 54 < 54 < 54 130 130 12/20/14 < 56 < 56 < 56 < 56 < 56 < 56 130 130 12/21/14 < 56 < 56 < 56 < 56 < 56 < 56 140 140 12/22/14 < 54 < 54 < 54 < 54 < 54 < 54 150 150 12/23/14 < 55 < 55 < 55 < 55 < 55 < 55 110 110 . 12/24/14 < 54 < 54 < 54 < 54 < 54 < 54 130 130 Page 8 of 9 4 2014:Milorganite Daily'Production, Sam Aes COLLECTION DATE PCB Aroclors:(ppb) PCB-1016 PCB-1221 PCB=1232 PCB-1242 PCB-1248 PCB-1254 PC9-1260 Total PCBs. 12/25/14 ' < 54 < 54 < 54 < 54 < 54 < 54:: 150 :. ' 150 12/26/14 < 53 < 53 < 53, < 53 :< 53 < 53 .: 190 190 12/27/14 < 54 < 54 < 54 < 54 < 54 < 54 190: 190 12/28/14: < 55 < 5:5 < 55 <: 55 < 55 < 55 160 160 12/29/14 < 54 < 54 < 54 < 54 < 54 < 54 170 170 12/30/14 < 53 < 53 < 53 < 53 < 53 < 53 -200 200 12/31/14.: < 53 <.53 < 53 <.53 < 53 < 53: 160 :160 'Samples analyzed by Pace Analytical Services, Green Bay, Wisconsin (WI Certification #405132750) by EPA 8082. All results reported on a dry weight basis. Milor anite Toxic Equivalent Concentrations 2014 Measured Concentration i pg/gor t Factor CAS Congener 1/11/2014 2/8/2014 3/8/2014 4/12/2014 5/10/2014 6/7/2014 7/12/20141 8/9/2014 9/27/2014 10/11/2014 11/8/2014 12/13/2014 EPA Maine 1746-01-6 2,3,7,8- Tetrachlorodibenzo-p-dioxin 0 0 0 0 0 0 0 0 0 0 0 0 1.0 1.0 40321-76-4 1,2,3,7,8- Pentachlorodibenzo-p-dioxin 0 0 0 0 0 0 6.2 0 0 5.5 0 0 1.0 0.5 39227-28-6 1,2,3,4,7,8- Hexachlorodibenzo-p-dioxin 0 0 0 0 0 6.4 7.1 0 5.2 5.2 0 0 0.1 0.1 57653-85-7 1,2,3,6,7,8- Hexachlorodibenzo-p-dioxin 0 6.4 8.4 7.6 9 16 16 12 14 15 9.3 7.6 0.1 0.1 19408-74-3 1,2,3,7,8,9- Hexachlorodibenzo-p-dioxin 0 0 5.2 5.6 0 13 14 0 10 11 9.3 5.4 0.1 0.1 35822-46-9 1,2,3,4,6,7,8- Heptachlorodibenzo-p-dioxin 79 100 110 120 280 270 330 180 180 320 190 140 0.01 0.01 3268-87-9 1,2,3,4,6,7,8,9- Octachlorodibenzo-p-dioxin 700 1100 1100 1100 3100 2400 2500 1500 1600 3200 1900 1400 0.0001 0.001 51207-31-9 2,3,7,8-Tetrachlorodibenzofuran 2.0 2.1 2.9 3.3 2.3 2.2 3.4 2.6 3.5 3.3 3.4 2.4 0.1 0.1 57117-41-6 1,2,3,7,8- Pentachlorodibenzofuran 0 0 0 0 0 0 0 0 0 7.8 0 0 0.05 0.05 57117-31-4 2,3,4,7,8- Pentachlorodibenzofuran 0 0 0 0 0 0 5.1 0 0 5.6 0 0 0.5 0.5 70648-26-9 1,2,3,4,7,8- Hexachlorodibenzofuran 0 0 10 0 0 10 9.4 10 7.2 11 0 0 0.1 0.1 57117-44-9 1,2,3,6,7,8- Hexachlorodi benzofu ran 0 0 0 5.7 8.9 9.0 9.2 6.7 7.4 8.4 6.1 0 0.1 0.1 72918-21-9 1,2,3,7,8,9-Hexachlorodibenzofuran 0 0 0 0 0 0 0 0 8.2 0 0 0 0.1 0.1 60851-34-5 2,3,4,6,7,8- Hexachlorodibenzofuran 0 0 5.1 5.2 0 0 11 7.9 11 5.9 6.5 0 0.1 0.1 67562-39-4 1,2,3,4,6,7,8- Heptachlorodibenzofuran 31 44 48 61 120 140 160 93 110 130 92 66 0.01 0.01 55673-89-7 1,2,3,4,7,8,9-Heptachlorodibenzofuran 0 0 0.0 0 6.1 9.0 8.6 9.5 0 7.3 6.9 0 0.01 0.01 39001-02-0 1,2,3,4,6,7,8,9- Octachlorodibenzofuran 76 100 140 1 150 290 1 310 350 220 210 360 200 150 0.0001 0.001 32598-13-3 3,3',4,4'-Tetrachlorobiphenyl 402 344 339 231 343 384 440 398 413 870 526 313 0.0001 0.0005 70362-50-4 3,4,4',5- Tetrachlorobiphenyl 0 0 0 0 0 0 0 0 0 0 0 0 0.0001 57465-28-8 3,3',4,4',5- Pentachlorobiphenyl 0 0 0 0 0 0 0 0 0 0 0 0 0.1 0.1 32598-14-4 2,3,3',4,4'- Pentachlorobiphenyl 2150 1770 1860 1580 2050 1980 2300 2090 2780 4420 2920 2300 0.0001 0.0001 31508-00-6 2,3',4,4',5- Pentachlorobiphenyl 5060 4140 4440 3450 4200 4300 4590 4460 6150 7960 5840 3820 0.0001 0.0001 65510-44-3 2',3,4,4',5- Pentachlorobiphenyl 115 0 0 0 0 105 107 172 138 182 207 0 0,0001 0.0001 74472-37-0 2,3,4,4',5- Pentachlorobiphenyl 149 104 101 106 135 119 138 134 192 330 189 132 0.0005 0.0005 32774-16-6 3,3',4,4',5,5'- Hexachlorobiphenyl 0 0 0 0 0 0 0 0 0 0 0 0 0.01 0.01 38380-08-4 2,3,3',4,4',5-Hexachlorobiphenyl 1110 1030 1200 765 1090 1110 1340 1070 2590 3550 2190 1430 0.0005 0.0005 69782-90-7 2,3,3',4,4',5'- Hexachlorobiphenyl 0 0 0 0 0 0 0 0 0 0 0 0 0.0005 0.0005 52663-72-6 2,3',4,4',5,5'-Hexachlorobiphenyl 355 329 382 265 344 351 488 377 948 1320 747 454 0.00001 0.00001 39635-31-9 2,3,3',4,4',5,5'- Heptachlorobiphenyl 190 151 0 121 147 149 220 175 579 674 486 340 0.0001 0.0001 35065-30-6 2,2',3,3',4,4',5-Heptachlorobiphenyl 3920 3930 5390 2820 3180 3580 4750 4370 14900 18500 12100 0 0.0001 69782-91-8 2,2',3,4,4',5,5'-Heptachlorobiphenyl 8990 9040 12700 6910 8310 7860 12100 9680 39800 48400 32700 0 0.0001 Total EPA Toxic Equivalent (TEQ) 2.8 3.6 6.1 5.7 7.7 11.4 22.5 8.2 12.1 23.0 8.8 5.2 Total Maine Toxic Equivalent (TEQ) 5.0 6.1 9.2 7.8 12.0 15.2 23.9 11.4 19.4 30.5 1 15.3 6.7 "0" means that the concentration was less than the level of detection r 4, �SAMSD MATKM KI h MAKI fXllM. W1111 964 4/13/14 Su Sample Date Site Code Customer ID Milorganite Priority Pollutant and VOC Analysis Apri12014 Milo. Priority Pollutant Sample 14006667 LIMS Number 1253 1,2,4-Trichlorobenzene Dry wt < 120 ug/kg D.W. 120 8400 4/25/14 8270D Test America 3 1315 1,2-Diphenylhydrazine Dry wt. < 1000 ug/kg D.W. 1000 8400 4/25/14 8270D Test America 3 1234 2,4,6-Trichlorophenol Dry wt. < 280 ug/kg D.W. 280 4300 4/25/14 8270D Test America 3 1226 2,4-Dichlor6phenol Dry wt < 230 ug/kg D.W. 230 4300 4/25/14 8270D Test America 3 1227 2,4-Dimethylphenol Dry wt < 1200 ug/kg D.W. 1200 4300 4/25/14 8270D Test America 3 1229 2,4-Dinitrophenol Dry wt < IS00 ug/kg D.W. 1500 8400 4/25/14 8270D Test America 3 1252 2,4-Dinitrotoluene Dry wt. < 670 ug/kg D.W. 670 4300 4/25/14 8270D TestAmerica 3 1317 2,6-Dinitrotoluene Dry wt. < 1100 ug/kg D.W. 1100 4300 4/25/14 8270D TestAmerica 3 1249• 2-Chloronaphthalene Dry wt. < 290 ug/kg D.W. 290 4300 4/25/14 8270D Test America 3 ' 1225 2-Chlorophenol Dry wt. < 220 ug/kg D.W. 220 4300 4/25/14 8270D Test America 3 1230 2-Nitrophenol Dry wt. < 200 ug/kg D.W. 200 4300 4/25/14 8270D Test America 3 1324 3,3'-Dichloiobenzidine Dry wt. < 3800 ug/kg D.W. 3800 4300 AX. 4/25/14 8270D Test America 3 1260 4,4DDD Dry wt. < 16 ug/kg D.W. 16 85 4/23/14 8081B Test America 3 1259 4,4-DDE Dry wt. 18 ug/kg D.W. 18 85 1 4/23/14 8081E Test America 3 1258 4,4-DDT Dry wt 37 ug/kg D.W. 20 85 J 4/23/14 8081E Test America 3 1228 4,6-Dinitro-o-Cresol Dry wt < 1500 ug/kg D.W. 1500 8400 4/25/14 8270D Test America 3 1247 4-Bromophenyl Phenyl Ether Dry wt. < 1400 ug/kg D.W:. 1400 4300 4/25/14 8270D Test America 3 1250 4-Chloro-phenyl-phenyl ether Dry wt. < 92 ug/kg D.W. 92 4300 4/25/14 8.270D Test America 3 1231 4-Nitrophenol Drywt < 1000 ug/kg D.W. 1000 8400 4/25/14 8270D Test America 3 1254 A-BHC-Alpha Drywt. 19 ug/kg D.W. 15 85 1 4/23/14 8081E Test America 3 1235 Acenaphthene Dry wt < 51 ug/kg D.W. 51 4300 4/25/14 8270D Test America 3 1318 Acenaphthylene Dry wt. < 35 ug/kg D.W. 35 4300 4/25/14 8270D TestAmerica 3 1304 Aldrin Drywt. 30 ug/kg D.W. 21 85 J 4/23/14 8081B Test America 3 524 ALUMINUM ICP Dry wt 5100 mg/kg D.W. 4.6 10 4/21/14 6010C Test America 3 1236 Anthracene Dry wt. < 110 ug/kg D.W. 110 4300 4/25/14 8270D TestAmerica 3 545 ANTIMONY ICP Dry wt. 1.7 mg/kg D.W. 0.42 16 J 4/21/14 6010C Test America 3 525 ARSENIC ICP Dry wt. 4.7 mg/kg D.W. 0.42 2.1 4/21/14 6010C Test America 3 1255 B-BHC-Beta Dry wt 26 ug/kg D.W. 15 85 1 4/23/14 8081B Test America 3 1237 Benzidine Dry wt < 54000 ug/kg D.W. 54000 130000 AX. 4/25/14 8270D TestAmerica 3 1238 Benzo(a)Anthracene Dry wt. < 74. ug/kg D.W. 74 4300 AX. . 4/25/14 8270D Test America 3 1239 Benzo(a)Pyrene Dry wt < 100 ug/kg D.W. 100 4300 4/25/14 8270D Test America 3 1240 Benzo(b)Fluoranthene Dry wt. 950 ug/kg D.W. 84 4300 1 4/25/14 .8270D Test America 3 1241 Benio(g,h,i)Perylene Drywt. 840 ug/kg D.W. 52 4300 J 4/25/14 8270D Test America 3 1242 Benzo(k)F16oranthene Dry wt < 47 ug/kg D.W. 47 4300 4/25/14 8270D Test America 3 1256 BHC-Delta Dry wt. 21 ug/kg D.W. 16 85 J AX 4/23/14 8081B Test America 3 1243 Bis(2-Chloroethoxy)Methane Dry wt. < 230 ug/kg D.W. 230 4300 4/25/14 8270D TestAmerica 3 1244 Bis(2-Chloroethyl)Ether Dry wt. < 370 ug/kg D.W. 370 4300 4/25/14 $270D Test America 3 1245 Bis(2-Chloroisopropyl)Ether Dry wt < 450 ug/kg D.W. 450 4300 4/25/14 8270D Test America 3 1246 Bis(2-Ethylhexyl)Phthalate Dry wt. 17000 ug/kg D.W. 1400 4300 AX. 4/25/14 8270D Test America 3 1205 BN's SW846: 8270 (Milo) M User Defined' N.A. N.A. 4/25/14 SW846: 8270 TestAmerica 3 1206 BNA's SW846: 8270 (Milo) M User Defined N.A. N.A. 4/25/14 SW846: 8270 Test America 3 526 BORON ICF Dry wt. 13 mg/kg D.W. 0.2 2.1 4/21/14 6010C Test America 3 1248 Butyl Benzyl Phthalate Dry wt < 1200 ug/kg D.W. • 1200 4300 AX. 4/25/14 8270D TestAmerica 3 530 CADMIUM ICP Drywt. 0.9 mg/kg D.W: 0.031 0.21 4/21/14 6010C Test America 3 SYS1rpt5Genedc3 4111114 tj Page 1 of 4 Printed: 5,1911412:25 I, MSD RIRINfisla it LI[A111RAPP.�f}i !INI 529 CALCIUM ICP Dry wt • r Milorganite Priority Pollutant and VOC Analysis April 2014 20000 mg/kg D.W. 3.4 52 4/21/14 6010C TestAmerica 3 1305 Chlordane Dry wt. 680 ug/kg D.W. 190 850 J 4/23/14 8081E Test America 3 532 CHROMIUM ICP Dry wt. 160 mg/kg D.W. 0.21 0.52 4/21/14 6010C Test America 3 1251 Chrysene Dry wt. 840 ug/kg D.W, 43 4300 J AX 4/25/14 8270D Test America 3 531 COBALT ICP Dry wt. 56 mg/kg D.W. 0.052 0.52 4/21/14 6010C Test America 3 533 COPPER ICP Dry wt. 230 mg/kg D.W. 0.22 1 4/21/14 6010C Test America 3 263 Cyanide - Total 4.6 mg/kg D.W. 0.48 0.98 4/23/14 9012B Test America 3 1325 Dibenzo(a,h)Anthracene Dry wt. < 51 ug/kg D.W. 51 4300 4/25/14 8270D Test America 3 1306 Dieldrin Dry wt < 20 ug/kg D.W. 20 85 4/23/14 8081E Test America 3 1314 Diethyl Phthalate Dry wt. < 130 ug/kg D.W. 130 4300 4/25/14 8270D Test America 3 1328 Dimethyl Phthalate Dry wt. < 110 ug/kg D.W. 110 4300 4/25/14 8270D Test America 3 1320 Di-n-Buty]phthalate Dry wt: < 1500 ug/kg D.W. 1500 4300 4/25/14 8270D Test America 3 1323 Di-n-octyl phthalate Dry wt 1100 ug/kg D.W. 100 4300 J AX 4/25/14 8270D Test America 3 1261 Endosulfan alpha Dry wt. < 16 ug/kg D.W. 16 85 4/23/14 8081E Test America 3 1262 Endosulfan beta Dry wt. < 15 ug/kg D.W. 15 85 4/23/14 8081E Test America 3 1263 Endosulfan Sulfate Dry wt < 16 ug/kg D.W. 16 85 4/23/14 8081B Test America 3 1265 Endrin Aldehyde Dry wt. < 22 ug/kg D.W. 22 85 4/23/14 8081E Test America 3 1264 Endrin Dry wt < 17 ug/kg D.W. 17 85 4/23/14 8081B Test America 3 1321 Fluoranthene Drywt 710 ug/kg D.W. 62 4300 J 4/25/14 8270D Test America 3 1316 Fluorene Dry wt. < 99 ug/kg D.W. 99 4300 4/25/14 8270D Test America 3 1266 Heptachlor Dry wt. < 18 ug/kg D.W. 18 85 4/23/14 8081B Test America 3 1267 Heptachlorepoxide Dry wt < 22 ug/kg D.W. 22 85 4/23/14 8081B Test America 3 1330 Hexachlorobenzene Dry Wt. < 210 ug/kg D.W. 210 4300 4/25/14 8270D Test America 3 1327 Hexachlorobutadiene Dry wt < 220 ug/kg D.W. 220 4300 4/25/14 8270D Test America 3 1308 Hexachlorocyclopentadiene Drywt. < 1300 ug/kg D.W. 1300 4300 4/25/14 8270D Test America 3 1329 Hexachlorcethane Dry wt . < 330 ug/kg D.W. 330 4300 4/25/14 8270D Test America 3 1326 Indeno(1,2,3-cd)Pyrene Dry Wt 840 ug/kg D.W. 120 4300 J 4/25/14 8270D Test America 3 534 IRON ICP Drywt. 31000 mg/kg D.W. 1.1 10 . 4/21/14 6010C Test America 3 1311 Isophorone Dry wt. < 220 ug/kg D.W. 220 4300 4/25/14 8270D Test America 3 544 LEAD ICP Dry wt. 27 mg/kg D.W. 0.25 1 4/21/14 6010C Test America 3 538 MAGNESIUM ICP Dry wt. 5400 mg/kg D.W. 0.96 21 4/21/14 6010C Test America 3 539 MANGANESE ICP Dry wt. 1400 mg/kg D.W. 0.033 0.21 4/21/14 6010C Test America 3 428 MERCURY by M. 7471 (sludge) 0.37 mg/kg D.W. 0.0078 0.019 4119/14 7471B Test America 3 540 MOLYBDENUM ICP Dry wt. 7.8 mg/kg D.W. 0.14 1 4/21/14 6010C Test America 3 1312 Naphthalene Dry wt. < 72 ug/kg D.W. 72 4300 4/25/14 8270D Test America 3 542 NICKEL ICP Dry wt. 37 mg/kg D.W. 0.24 5.2 4/21/14 6010C Test America 3 1310 Nitrobenzene Dry wt. < 190 ug/kg D.W. 190 4300 4/25/14 8270D Test America 3 1307 N-Nitrosodimethylamine Dry wt. < 810 ug/kg D.W. 810 8400 4/25/14 8270D Test America 3 1309 N-Nitrosodi-n-propylamine Dry wt. < 340 ug/kg D.W. 340 4300 4/25/14 8270D Test America 3 1313 N-Nitrosodiphenylamine Dry wt. < 240 ug/kg D.W. 240 4300 4/25/14 8270D Test America 3 1094 PCB by m. 8082 (Aroclors) < 0.11 User Defined 0.11 N.A. 4/19/14 SW846: 8082 Test America 7 678 PCB-1016 <0.046 mg/kg D.W. 01046 0.24 4/19/14 8082A Test America 3 674 PCB-1221 < 0.046 mg/kg D.W. 0.046 0.24 4/19/14 8082A Test America 3 675 PCB-1232 < 0.046 mg/kg D.W. 0.046 0.24 4/19/14 8082A Test America 3 672 PCB-1242 <0.046 mg/kg D.W. 0.046 0.24 4/19/14 8082A Test America 3 676 PCB-1248 < 0.046 mg/kg D.W. 0.046 0.24 4/19/14 8082A Test America 3 673 PCB-1254 <0.11 mg/kg D.W. 0.11 0.24 4/19/14 8082A Test America 3 677 PCB-1260 < 0.11 mg/kg D.W. 0.11 0.24 4/19/14 8082A Test America 3 1224 p-Chloro-m-Cresol Dry wt. < 180 ug/kg D.W. 180 4300 4/25/14 8270D Test America 3 1232 Pentachlorophenol Dry wt. < 1500 ug/kg D.W. 1500 8400 4/25/14 8270D Test America 3 SYS/rpt5Generio3 4111114 tj Page 2 of 4 Printed: 51911412:25 . 1 .: . MMSD pl$l" Re A wAki ammalwi 1207 Pesticides by m. 8081 (Milo) M User Defined Milorganite Priority Pollutant and VOC Analysis April 2014 N.A. N.A. 4/23/14 SW846: 8081 TestAmerica 3 1319 Phenanthrene Dry wt. < 90 ug/kg D.W. 90 4300 4/25/14 8270D Test America 3 1233 Phenol Dry wt. < 450 ug/kg D.W. 450 4300 4/25/14 8270D Test America 3 543 PHOSPHORUS ICP Dry wt 11000 mg/kg D.W. 72 180 4/24/14 SM 4500 P E Test America 3 536 POTASSIUM 3CP Dry wt. 3900 mg/kg D.W. 21 31 4/21/14 6010C Test America 3 1322 Pyrene Dry wt < 28 ug/kg D.W. 28 4306 AX. 4/25/14 8270D Test America 3 546 SELENIUM ICP Dry wt. 4.2 mg/kg D.W. 0.42 4.2 4/21/14 6010C Test America 3 1187 Solids for dry weight determination (T 96 % ** *** 4/17/14 Moisture Test America 3 550 THALLIUM ICP Dry wt < 0.31 mg/kg D.W. 0.31 6.2 4/21/14 6010C Test America 3 1268 Toxaphene Dry wt. < 490 ug/kg D.W. 490 850 4/23/14 8081E Test America 3 1257 Y-BHC-Gamma(Lindane) Dry wt. < 16 ug/kg D.W. 16 85 4/23/14 8081B TestAmerica 3 552 ZINC ICP Dry wt. 430 mg/kg D.W: 0:16 2.1 4/21/14 6010C TestAmerica 3 4/14/14 su Sample Date Site Code 1341 1,1,1-Trichloroethane Dry wt. Customer ID < 2.9 ug/kg D.W. 2.9 41 4/17/14 8260C 14006565 LIMS Number Test America 3 1350 1,1,2,2-Tetrachloroethane Dry wt < 6.6 ug/kg D.W. 6.6 41 4/17/14 8260C TestAmerica 3 1348 1,1,2-Trichloroethane Dry wt. < 5.3 ug/kg D.W. 5.3 41 4/17/14 8260C Test America 3 1338 1,1-Dichloroethane Drywt. <4.9 ug/kg D.W. 4.9 41 4/17/14 8260C TestAmerica 3 1336 1,1-Dichloroethylene Dry wt. < 5 ug/kg D.W. 5 41 . . . 4/17/14 8260C Test America 3 1355 1,2-Dichlorobenzene Dry Wt < 3.2 ug/kg D.W. 3.2 41 4/17/14 8260C Test America 3 1340 1,2-Dichloroethane Dry wt. < 2 Qg/kg D.W. 2 41 4/17/14 8260C Test America 3 1222 1,2-Dichloropropane Dry wt < 20 ug/kg D.W. 20 41 4/17/14 8260C TestAmerica 3 1356 1,3-Dichlorobenzene Dry Wt < 2.1 ug/kg D.W. 2.1 41 4/17/14 8260C Test America 3 1357 1,4-Dichlorobenzene Dry Wt < 5.7 ug/kg D.W. 5.7 41 4/17/14 8260C. Test America 3 1337 2-Chloroethylvinyl Ether Dry wt. < 20 dg/kg D.W. 20 81 4/17/14 8260C TestAmerica 3 1334 Acrolein Dry wt. < 64 ug/kg D.W. 64 200 4/17/14 8260C Test America 3 1335 Acrylonitrile Dry wt < 17 ug/kg D.W. 17 200 4/17/14 8260C Test America 3 1346 Benzene Dry wt. < 2 ug/kg D.W. 2 41 4/17/14 8260C TestAmerica 3 1343 Bromodichloromethane Dry wt < 5.4 ug/kg D.W. 5.4 41. 4/17/14 8260C Test America 3 1219 Bromoform Dry wt. < 20 ug/kg D.W. 20 41 4/17/14 8260C Test America 3 1342 Carbon Tetrachloride Dry wt. < 3.9 ug/kg D.W. 3.9 41 4/17/14 8266C Test America 3 1352 Chlorobenzene Dry wt. < S. 3 ug/kg D.W. 5.3 41 4/17/14 8260C Test America 3 1220 Chloroethane Dry wt. < 9.2 ug/kg D.W. 9.2 41 4/17/14 8260C Test America 3 1339 Chloroform Dry wt. < 2.5 ug/kg D.W. 2.5 41 4/17/14 8260C Test America 3 1344 cis-1,3-Dichloropropene Drywt. < 5.8 ug/kg D.W. 5.8 41 4/17/14 8260C TestAmerica 3 1347 Dibromochloromethane Dry wt < 5.2 ug/kg D.W. 5.2 41. 4/17/14 8260C TestAmerica 3 1353 Ethylbenzene Dry wt. < 2.8 ug/kg D.W. 2.8 41 4/17/14 8260C Test America 3 1331 Methyl Bromide Dry wt. < 3.6 ug/kg D.W. 3.6 41 4/17/14 8260C Test America 3 1354 Methyl Chloride dry wt. < 2.4 ug/kg D.W. 2.4 41 4/17/14 8260C TestAmeka 3 1333 Methylene Chloride Dry wt. < 19 ug/kg D.W. 19 41 4/17/14 8260C Test America 3 1187 Solids for dry weight determination (T 78 % ** *** 4/23/14 Moisture Test America 3 1349 Tetrachloroethylene Dry wt < 5.4 ug/kg D.W. 5.4 41 4/17/14 8260C TestAmerica 3 1351 Toluene Dry wt., 4.3 ug/kg D.W. 3.1 41 ] 4/17/14 8260C TestAmerica 3 1221 Trans-1,2-Dichl6roethylene Dry wt. < 4.2 ug/kg D.W. 4.2 41 4/17/14 8260C Test America 3 1223 Trans-1,3-Dichloropropene Dry wt. < 18 ug/kg D.W. 18 41 4/17/14 8260C TestAmerica 3 1345 Trichloroethylene Dry wt. < 8.9 ug/kg D.W. 8.9 41 4/17/14 8260C TestAmerica 3 1332 Vinyl Chloride Dry wt < 4.9 ug/kg D.W. 4.9 41 4/17/14 8260C Test America 3 SYS1rpt5Genenc3 401114 tj Page 3 of 4 Printed: W11412:25 '.. _ MSD P.}mal leg d G.LiWa flitif! ylvi 1204 VOCs by m.8260 (Milo) Milorganite Priority Pollutant and VOC Analysis April 2014 M mg/kg D.W. N.A. N.A. 4/17/14 SW846: 8260 Test America 3 ** The MDL for this test is the lowest level of precision shown, example: 4.1 would be "0.1". *** The LOQ for this testis the lowest level of precision shown, example: 4.1 would be "0.1". N.A. The MDL/LOQ is Not Available or Not Applicable for this test. . Column S: Test Status. Not Started=8, Intermediate=7, Final=3, Analyst Approved=12, Not Reportable=15. 140 Fla Descri tions AO Other -- Flag requires additional explanation IS Insufficient sample volume for analysis. AX Qualified data - see contract lab report J Estimated concentration above the adjusted method detection limit B3 Target analyte detected in method blank > 10% of sample and below the adjusted reporting limit concentration. LA Not analyzed - lab accident. B7 LCS recovery was above control limits. M1 Too numerous to count. BB LCS recovery was below control limits. M2 Sample incubation period exceeded method requirement. B9 Low Level CCV recovery was outside of method acceptance limits M3 Spreading colonies - unable to determine result. CQ Data used for calculation of result was qualified MS Incubator/water bath temperature was outside method D1 Duplicate precision control limit was exceeded. requirements. D2 Matrix spike precision control limit was exceeded. M7 Micro sample received without adequate headspace. D3 Sample is heterogeneous. Sample homogeneity could not be M9 Target organism detected in associated method blank. readily achieved using routine laboratory practices. MU Not usable Data. Hi Sample was received past holding time. Q2 Matrix spike recovery for this sample was above control limits. H3 Analysis performed beyond holding time. Q3 Matrix spike recovery for this sample was below control limits. H4 Initial analysis within holding time. Reanalysis for the required RT Sample temperature upon receipt exceeded regulatory or.project dilution was past holding time. requirements. HS Analysis performed beyond holding time. S5 Reading was not confirmed by a constant weight measurement T3 The dilution water D.O. depletion was > 0.2 mg/L. T4 GGA BOD was below method acceptance criteria. TS GGA BOD was above method acceptance criteria. T7 The dilution water D.O. increase was > 0.2 mq/L. Page 4 of 4 SYS/rpt5Generic3 4111114 tj Printed: W11412:25 rt rhRINit3lot A ClU." GWlt"WINI September: Milorganite. Priority Pollutant and VOC Analysis September 2014 9/21,/14 Milo., Priority Pollutant Sample 1:4021363 1,2,4-Trichlorobehiene Dry wt. 10/9/14 < 5 ug/kg D.W. 5 8270D Test America Buffalo 1,2-Diphenylhydrazine Dry wt. 10/9/14 48 ug/kg D.W: 42 ] 8270D Test America Buffalo 2,4,6-Trichlorophenol Dry wt. 10/9/14 < 12 ug/kg D.W. 12 8270D Test America Buffalo 2,4-Dichlorophenol.Dry wt.. 10/9/14 < 9.2 : Ug/kg D.W. 9.2 8270D Test America Buffalo 2,4-Dimethylphe.nol Dry wt. 10/9/14 < 48 ug/kg.D.W. 48 8270D Test America Buffalo 2,4-Dinitfophenol Dry wt 10/9/14 < 62 ug/kg D.W. 62 8270D., Test America Buffalo 2,4-Dinitrotoluene Dry wt. 10/9/14 < 27 ug/kg D.W. 27 8270D Test America Buffalo 2,6-Dinitrotoluene Dry wt. 16/9/14 < 43 ug/kg D.W. 43 8270D Test America Buffalo 2-Chloronaphthalene Dry wt. 10/9/14 < 12 ug/kg D.W. 12 8270D Test America Buffalo 2-Chlorophenol Dry wt. 10/9/14 < 9 ug/kg D.W. 9 8270D Test America Buffalo 2-Nitrophenol Dry wt. 10/9/14 < 8.1 ug/kg D.W. 8.1 8270D Test America Buffalo 3,3'-Dichlorobenzidine Dry wt. 10/9/14 < 150 . ug/kg D.W. 150 8270D Test America Buffalo 4,6-DiniOro-o-Cresol Dry wt. 10/9/14 < 61 ug/kg D.W. 61 8270D Test America Buffalo 4-Bromophenyl Phenyl Ether Dry wf. 10/9/14 < 56 ug/kg D.W. 56 8270D Test America Buffalo 4-Chloro-phenyl-phenyl ether Dry wt. 10/9/14 < 3.8 ug/kg D.W. 3.8 8270D Test America Buffalo 4-Nitrophenol Dry wt. 10/9/14 < 43 ug/kg D.W. 43 8270D Test America Buffalo Acenaphthene Dry wt. 10/9/14 < 2.1 ug/kg D.W. 2.1 8270D . Test America Buffalo Acenaphthylene Dry wt. 10/9/14 < 1.4 ug/kg D.W. 1.4 8270D Test America Buffalo ALUMINUM ICP Dry wt. - 10/8/14 3200 : mg/kg D.W. 5.1 6010C Test America Buffalo Anthracene Dry wt. 10/9/14 < 4,5 ug/kg.D.W. 4.5 8270D Test America Buffalo ANTIMONY.ICP Dry wt. 10/8/14 1.3 mg/kg D.W. 0.46 ] 60fOC Test America Buffalo ARSENIC ICP Dry wt. 10/8/14 3.5 mg/kg D.W. 0.46 6010C Test America Buffalo Benzidine Dry wt: 10/9/14 < 2200 ug/kg D.W. 2200 AX. 8270D Test America Buffalo Benzq(a)Anthracene Dry wt: 10/9/14 < 3 ug/kg D.W. 3 8270D Test America Buffalo Benio(a)Pyrene Dry wt 10/9/14 340 ug/kg D.W. 4.2 8270D Test America Buffalo Benzo(b)Fluoranthene Dry wt. 10/9/14 < 3.4 ug/kg D.W. 3.4 8270D Test America Buffaio Benzo(g,h,i)Perylene Dry wt. 10/9/14 300 ug/kg D.W. 2.1 8270D Test America Buffalo Benzq(k)Fluoranthene Dry Wt. 10/9/14, < 1.9 ug/kg D.W. 1.9 827OD, Test America Buffalo BERYLLIUM ICP Dry wt. 10/8/14.. < 0.032 mg/kg D.W. 0.032 6010C Test America Buffalo Bis(2-Chloroethoxy)Methane Dry wt. 10/9/14 < 9.6 ug/kg D.W. 9.6 8270D :Test America Buffalo Bis(2-Chloroethyl)Ether Dry wt. 10/9/14 < 15 ug/kg D.W. 15 8270D Test America Buffalo Bis(2-Chlor6isopropyl)Ether Dry wt. 10/9/14 < 18 ug/kg D.W. 18 8270D' Test America Buffalo Bis(2-Ethylhexyl)Phthalate Dry wt. 10/10/14 13000 ug/kg D.W. 1100 8270D Test America Buffalo BORON ICP Dry wt..: 10/8/14 13 mg/kg D.W. 0.22 AX. 6010C Test America Buffalo Butyl Benzyl Phthalate Dry wt 10/9/14 < 47 ug/kg D.W. 47 8270D Test America Buffalo CADMIUM ICP Dry wt. 10/8/14 0.55 mg/kg D.W. 0.035 :60fOC.. Test America Buffalo CHROMIUM ICP Dry wt. 10/8/14 200 mg/kg D.W. 0.23 .6010C Test America Buffalo Chrysene Dry wt..: 10/9/14 < 1.8 ug/kg D.W. 1.8 8270D Test America Buffalo COBALT ICP Dry wt. 10/8/14 4.2 mg/kg D.W. 0.058 6010C Test America Buffalo COPPER ICP Dry wt. 10/8/14 160 mg/kg D.W. 0.74 6010C : Test America Buffalo Cyanide - Total 10/6/14 2.9 mg/kg D.W. 0.49 9012E Test America Buffalo Dibenzo(a,h)Anthracene Dry. wt. 10/9/14 < 2.1 . ug/kg D.W. 2.1 8270D Test America Buffalo Diethyl Phthalate Dry wt. 10/9/14 - 41 ug/kg D.W. 5.3 J 8270D Test America Buffalo Dimethyl Phthalate Dry wt. 10/9/14 < 4.6 ug/kg D.W. 4.6 8270D Test America Buffalo SYS4pt1 M#oPP 1/10/13 tj Page 1 of 4 Printed: 11118/14 07:57 , MM, D, PrtkiR£iS lD4,� C££4s£R a`i1�9ild£NI September. Milorganite Priority Pollutant and VOC Analysis September 2014 9/21/14 Milo. Priority Pollutant Sample 14021353 u4-Cl..j=t-w ®.. -. a t �h _ . .. ' L :C•.R.11 /,,.lA1A11145 0 �W. Di-n-Butylphthalate Dry wt 10/9/14 < 61 ug/kg D.W. 61 8270D Test. America Buffalo Di-n-octyl phthalate Dry wt. 10/9/14 560 ug/kg D.W. 4A 8270D Test America: Buffalo Fluoranthene Dry wt. 10/9/14 710 ug/kg D.W.. 2.6 8270D Test America Buffalo Fluorene Dry wt. 10/9/14 < 4.1 ug/kg D.W. 4.1 8270D Test America Buffalo Hexachlorobenzene Dry wt. 10/9/14 < 8.8 ug/kg D.W. 8.8 8270D Test America Buffalo Hexachloirobutadiene Dry wt. 10/9/14 < 9 ug/kg D.W. 9 8270D Test America. Buffalo Hexachlorocyclopentadiene Dry 4.' 10/9/14 < 53 ug/kg D.W. 53 8270D Test America, Buffalo Hexachloroethane Dry wt. 10/9/14 < 14 ug/kg D.W. 14 - 8270D Test America Buffalo Indeno(1,2,3-cd)Pyrene Dry Wt. 10/9/14 < 4.9 ug/kg D.W. 4,9 8270D Test America. Buffalo IRON ICP Dry wt. 10/8/14 19000 mg/kg D.W. 1.3 AX. 6010C Test America Buffalo Isophorone Dry wt. 10/9/14 < 8.8 ug/kg D.W. 8.8 8270D Test America Buffalo LEAD ICP Dry wt. 10/8/14 28 mg/kg D:W. 0.28 6010C Test America Buffalo MAGNESIUM ICP Dry wt. 10/8/14 4800 mg/kg D.W. i j 6010C _ Test America Buffalo MANGANESE ICP Dry wt. 10/8/14 1100 mg/kg D.W. 0.037 6010C Test America Buffalo MERCURY by M. 7471 (sludge) 10/2/14 0.55 mg/kg D.W. 0.0084 7471B Test America Buffalo MOLYBDENUM ICP Dry wt. 10/8/14 6.8 mg/kg D.W. 0.15 6010C Test.America Buffalo Naphthalene Dry wt. 10/9/14 < 2.9 ug/kg D.W. 2.9 8270D Test America Buffalo NICKEL ICP Dry wt. 10/8/14 17 mg/kg D.W. 0.26 6010C Test America Buffalo Nitrobenzene Dry wt. 10/9/14 < 7.8 ug/kg D.W. 7.8 8270D test America Buffalo N-Nitrosodimethylamine Dry wt. 10/9/14 < 13 ug/kg D.W. 13 8270D Test America Buffalo N-Nitrosodi-n-propylamine Dry wt.. 10/9/14 < 14 ug/kg D.W. 14 8270D Test AmericaBuffalo N-Nitrosodiphenylamine Dry wt. 10/9/14 < 9.6 ug/kg D.W. 9.6 8270D Test America Buffalo PCB-1016 10/1/14 < 0.47 mg/kg D.W. 0.47 8082A Test America Buffalo . PCB-1221 10/1/14 < 0.47 mg/kg D.W. 0.47 8082A Test America Buffalo PCB-1232 10/1/14 < 0.47 mg/kg D.W. 0.47 8082A Test America Buffalo PCB-1242 10/1/14 < 0.47 mg/kg D.W. 0.47 8082A Test America Buffalo PCB-1248 10/1/14 < 0.47 mg/kg D.W. 0.47 8082A Test America Buffalo ' PCB-1254 10/1/14 < 1.1 mg/kg D.W. 1.1 8082A Test America Buffalo PCB-1260 10/1/14 < 1.1 mg/kg D.W. 1.1 8082A Test America Buffalo p-Chloro-m-Cresol Dry wt. 10/9/14 < 7.3 ug/kg D.W. 7.3 8270D Test America Buffalo Pentachlorophenol Dry wt. 10/9/14 < 60 ug/kg D.W. 60 8270D Test America Buffalo Phenanthrene Dry wt. SO/9/14 < 3.7 ug/kg D.W. 3.7 8270D Test America, Buffalo Phenol Dry wt. 10/9/14 < 19 ug/kg D.W. 19 8270D Test America Buffalo POTASSIUM ICP Dry•wt. ' 10/8/14 2000 mg/kg D.W. 23 6010C Test America Buffalo Pyrene Dry wt. 10/9/14 1200 ug/kg D.W. 1.1 8270D Test America Buffalo SELENIUM ICP Dry wt. 10/8/14 1.5 mg/kg D.W: 0.46 J 6016C Test America Buffalo SILVER ICP Dry wt. 10/8/14 1.4 mg/kg D.W: 0.23 6010C Test America, Buffalo Solids for dry weight determination (Test America) 9/30/14 95 % 0.1 Moisture Test America Buffalo Solids for dry weight determination (Test America) 9/30/14 95 % 0.1 Moisture Test America Buffalo THALLIUM ICP Dry wt. 10/8/14 < 0.35 mg/kg D.W. 0.35 6010C Test America' Buffalo Total PCB Aroclors 10/1/14 < 1.1 mg/kg D.W. 1A 8082A Test America Buffalo ZINC ICP Dry wt. 10/8/14 340 mg/kg D.W. 0.18 AX. 6010C Test America Buffalo Page 2 of 4 SYS/rptiMiloPP 1110113 t% Panted: 1111W14 07:57 IS-MOISD 1"WHIZ lot A CEEMR LINNNfIll September . Milorganite Priority Pollutant and VOC Analysis September 2014 9129/14 Milo. Priority Pollutant Sample /4021354 u ^UL. A-"CsAl.9'o`L ftgI g 1J�7.-�aAS .. p P�,u u-1_1 _ J `-„��." ^ • ^i :4�Ys4J 1,1,1-Trichloroethane Dry wt. 10/3/14 < 3.8 ug/kg DM. 3.8 8260C Test America Buffalo 1,1,2,2-Tetrachloroethane Dry wt. 10/3/14 < 8.4 ug/kg D.W. 8.4 .8260C Test America Buffalo 1,1,2-Trichloroethane Dry wt. 1013/14 < 6.8 ug/kg D.W. 6.8 8260C Test America Buffalo 1,1-Dichloroethane:Dry wt 10/3/14 < 6.3 ug/kg D.W. 6.3 8260C Test America Buffalo 1,1-Dichloroethylene Dry wt. 10/3/14 < 6.4 ug/kg D:W. 6.4 8260C Test America Buffalo 1,2-bichlorobenzene Dry Wt. 10/3/14 < 4.1 ug/kg D.W. 4.1 8260C Test America Buffalo 1,2-Dichloroethane Dry wt. 10/3/14 < 2.6 ug/kg D.W. 2,6 8260C Test America Buffalo 1,2-Dichloropropane Dry wt,, 10/3/14 < 26 ug/kg D.W. 26 8260C Test America Buffalo 1,3-Dichlorobenzene, Dry Wt. 10/3/14 < 2.7 ug/kg D:W. 2.7 8260C Test America Buffalo 1,4-Dichlorobenzene Dry Wt. 10/3/14 < 7.3 ug/kg D.W. 7.3 .8260C Test America Buffalo 2-Chloroethylvinyl Ether Dry wt. 10/3/14 < 26 ug/kg D.W. 26 8260C Test America Buffalo Acrolein Dry wt._ 10/3/14 < 82 ug/kg D.W. 82 8260C Test America Buffalo Acrylonitrile Dry wt. 10/3/14 < 47 ug/kg D.W. 47 8260C Test America Buffalo Benzene Dry wt. 10/3/14 < 2.5 ug/kg D.W. 2.5 8260C Test America Buffalo Bromodichloromethane Dry wt. 10/3/14 < 7 ug/kg D.W. 7 8260C Test America Buffalo Bromoform Dry wt.. - 10/3/14 < 26 ug/kg D.W. 26 8260C Test America Buffalo Carbon Tetrachloride Dry wt. lO/3/14 < 5 ug/kg D.W. 5 8260C Test America Buffalo Chlorobenzene Dry wt. 10/3/14 < 6.9 ug/kg D.W. 6:9 8260C Test America Buffalo Chloroethane Dry wt. 10/3/14 < 12 ug/kg D.W. 12 8260C Test America Buffalo Chloroform Drywt 10/3/14 < 3.2 ug/kg D.W. 3.2 8260C Test America Buffalo cis-1,3-Dichloropropene Dry wt. 10/3/14 < 7.5 ug/kg D.W. 7.5 8260C Test America Buffalo Dibromochloromethane Dry wt. 10/3/14 < 6.6 ug/kg D.W. 6.6 8260C Test America Buffalo Ethylbenzene Dry wt. 10/3/14 < 3.6 ug/kg D.W. 3.6 8260C Test America Buffalo Methyl Bromide Dry wt. 10/3/14 < 4.7 ug/kg D.W. 4.7 8260C Test America Buffalo Methyl Chloride dry wt. 10/3/14. < 3.1 ug/kg D.W. 3.1 8260C Test America Buffalo Methylene Chloride Dry wt. 10/3/14 < 24 ug/kg D.W. 24 8260C Test America Buffalo Solids for dry Weight determination (Test America) 10/3/14 96 % 0.1 Moisture Test America Buffalo Tetrachloroethylene Dry wt: 10/3/14 < 7 ug/kg D.W. .7 8260C Test America Buffalo Toluene Dry wt. 10/3/14 < 3.9 ug/kg D.W. 3.9 8260C Test America Buffalo Trans-1,2-Dichloroethylene Dry wt 1013/14 < 5.4 ug/kg D.W. 5.4 8260C Test America Buffalo Trans-1,3-Dichloropropene Dry wt. 10/3/14 < 23 ug/kg D.W. 23 8260C Test America Buffalo Trichloroethylene Dry wt. ' 10/3/14 < 11 ug/kg D.W. 11 8260C Test America Buffalo Vinyl Chloride Dry wt. 10/3/14 < 6.3 ug/kg D.W. 6:3 8260C Test America Buffalo Page 3 of 4 SYSrrpt I NIOPP 1110113 tj Printed., 11118114 07:57 Milorganite Priority Pollutant and VOC Analysis September 2014 '�, P,t MIPS 1M A CM E0114AWEAl 119 Flag' besdiptions AO Other -- Flag requires additional explanation IS Insufficient sample volume for analysis. AX Qualified data - see contract lab report ] Estimated concentration above the adjusted method detection limit B3 Target analyte detected in method blank > 10% of sample and below.the adjusted reporting limit concentration. LA Not analyzed - lab accident. B7 LCS recovery was above control limits. M1 Too numerous to count. B8 LCS recovery was below control limits. M2 Sample incubation period exceeded method requirement. B9 Low Level CCV recovery was outside of method acceptance limits M3 Spreading colonies - unable to determine result. CQ . Data used for calculation of result was qualified MS Incubator/water bath temperature was outside method Di Duplicate precision control limit was exceeded. D2 Matrix spike precision control limit was exceeded. D3 Sample is heterogeneous. Sample homogeneity could not be readily achieved using routine laboratory practices. H3 Sample was received past holding time. H3 Analysis performed beyond holding time. H4 Initial analysis within holding time. Reanalysis for the required dilution was past holding time. HS Analysis performed beyond holding time. M7 Micro sample received without adequate headspace. M9 Target organism detected in associated method blank. NU Not usable Data. Q2 Matrix spike recovery for this sample was above control limits. Q3 Matrix spike recovery for this sample was below control limits. RT Sample temperature upon receipt exceeded regulatory or project requirements. SS Reading was not confirmed by a constant weight measurement T3 The dilution water D.O. depletion was > 0.2 mg/L. T4 GGA BOD was below method acceptance criteria. TS GGA BOD was above method acceptance criteria. T7 The dilution water D.O. increase was > 0.2 mq/L. Page 4 of 4 SYS/rpt1M11oPP 1110113 tj Punted: 11118114 07:57 V 4 p t M S D, P�81�{P3 (I6i A f ti�sis tltli4�aNfdO October Milorganite Priority Pollutant and VOC Analysis October 26, 2014 10/26/14 Milo. Priority Pollutant Sample i 4024367 ®a • e o .. ,te l S 1 4wua840J8u1laBLll 4,4-DDD Dry wt. 11/8/14 < 17 ug/kg D;W. 17 Test America Buffalo 4,4-DDE Dry wt. 11/8/14 < 18 ug/kg D.W. 18 -8081B Test America Buffalo 4,4-DDT Dry wt. 11/8/14 -< 20 ug/kg D.W. 20 8081B Test America Buffalo A-BHC-Alpha Dry wt.. 11/8/14 < 16 ug/kg D.W. 16 8081B Test America Buffalo Aldrin Dry wt. 11/8/14 < 21 ug/kg D.W. 21 8081B Test America Buffalo B-BHC-Beta Dry wt. 11/8/14 < 16 ug/kg D.W. 16 8081B Test America Buffalo BHC-Delta Dry wt. 11/8/14 46 ug/kg D.W. 16 ] 8081E Test America, Buffalo Chlordane Dry wt. 11/8/14 < 190 ug/kg D;W. 190 8081B Test America Buffalo . Dieldrin Dry wt.. 11/8/14 < 21 ug/kg D.W. 21 8081B Test America Buffalo Endosulfan alpha Dry wt. 11/8/14 < 17 ug/kg D.W. 17 .8081B Test America Buffalo Endosulfan beta Drywt. 11/8/14 < 16 _ug/kg D.W. 16 8081B Test America Buffalo Endosulfan Sulfate D}yWt. 11/S/14 < 16 ug/kg D;W. 16 : 8081B Test America Buffalo Endrin Aldehyde Dry wt. 11/8/14 < 22 ug/kg D.W. 22 8081B Test America Buffalo En drin Drywt. 11/8/14 .:< 17 ug/kg D.W. " 17 8081E Test America Buffalo Heptachlor Dry wt. 11/8/14 < 19 ug/kg D.W. 19 8081E Test America Buffalo Heptachlorepoxide;Dry wt. 11/8/14 <22 ;ug/kgD:W. 22 8081B Test America Buffalo Solids for. dry weight determination. Crest America) 11/4/14 .... 95 % 0.1 Moisture Test America Buffalo 'Toxaphene Drywt. 11/8%14 < 500 ug/kg D.W. sob 8081E Test America Buffalo Y-BHC-Gamma(Lindane) Drywt. 11/8/14 < 16 ug/kg D.W. 16 8081B Test America Buffalo 19 AO . Other -- Flag requires additional:explanation IS Insufficient sample volume for analysis. AX Qualified data - see contract lab report ] Estimated concentration above the adjusted method detection limit B3 Target analyte detected in method blank > 10% of sample and below the adjusted reporting limit concentration, LA Not analyzed - lab accident. B7 LCS recovery was above control limits. M1 Too numerous to count. 1138 LCS recovery was below control limits. M2 Sample incubation period exceeded method requirement. 1139 Low Level CCV recovery was outside of method acceptance limits M3 Spreading colonies - unable to determine result. . CQ Data used for calculation of result was qualified MS Incubator/water bath temperature was outside method ; DS Duplicate precision control limit was exceeded. requirements. D2 Matrix spike precision control limit was exceeded. M7 Micro sample received without adequate. headspace. 63 Sample is heterogeneous. Sample homogeneity could not be M9 Target organism detected in associated method blank. . readily achieved using routine laboratory practices. NU Not usable Data. H1 Sample was.received past holding time. Q2 : Matrix spike recovery for:this sample was above control limits. H3 Analysis performed beyond holding time. Q3 Matrix spike recovery, for this sample was below control limits. .H4. :'Initial analysis within holding time. Reanalysis for the required RT Sampletemperature upon receipt exceeded regulatory or project dilution was past holding time. requirements. HS Analysis performed beyond holding time. SS Reading was not confirmed by a constant weight measurement T3 The dilution water DA: depletion was > 0.2 mg/L. T4 GGA BOD was below method acceptance criteria. TS GGA.BOD was above method acceptance.criteria. T7 The dilution water-D.O. increase was > 0.2 mg/L. Page i of 1 SYS/rpt1MitoPP 1110113 tj Printed: IIII a114 07:40