Loading...
HomeMy WebLinkAboutWQ0012346_Residual Annual Report 2014_20150220tv oc) ! - 3 CLASS "A" WASTEWATER RESIDUALS ANNUAL APPLICATION REPORT YEAR 2014 UNITED STATES MARINE CORPS BASE ..... CAMP LEJEUNE, N.C. RECEIVEDIDEN N.C. PERMIT WQ0012346 FEb � v %'u15 wawr Quallt p��g S on I • UNITED.STATES MARINE CORPS MARINE CORPS INSTALLATIONS EAST -MARINE CORPS BASE PSC BOX 20005 CAMP LEJEUNE NC 28542-0005 5090.20.1 BEMD FEB 19 2015 Mr. Jon Risgaard North Carolina Department of Environment and Natural Resources Water Permitting Section, Wastewater Branch North Carolina Division of Water Resources 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Dear Mr. Risgaard: In accordance with requirements of 40 CFR Part 503, the enclosure forwards Marine Corps Installations East -Marine Corps Base Camp Lejeune's (MCIEAST-MCB CAMLEJ) Class "A" Wastewater Residuals Annual Application�Report for the Year 2014. If you have any questions please contact Mr. James Marshall- Zank, Environmental Quality Branch, Environmental Management Division, G-F, at (910) 451-9122. Sincerely, 11.. John R. Townson Director, Environmental Management By direction of the Commanding General Enclosure_: MCIEAST-MCB CAMLEJ's Class "A" Wastewater Residuals Annual Application Report Year 2014 (3 copies) RECEIVEDIDENEWR - FEB 0"?015 WaterQualdty Permfte SeMn 2011-4 A-----N--N-UAL _:_ OrN D�IS,T' UTI111-0,Nii, OF CLASS: �.A�. R ALS, MARINE CORPS BASE CAMP LEJEUNE PERMIT NO. WQ0012346 2014 ANNUAL REPORT ON DISTRIBUTION OF CLASS A WASTEWATER RESIDUALS MARINE CORPS BASE, CAMP LEJEUNE WQ0012346 • Cover Letter SECTION I • Class A Distribution & Marketing/ Surface SECTION 2 Disposal Certification & Summary Forms • Annual Residuals Sampling Summary Forms SECTION 3 • Residuals Analysis lab Sheets SECTION 4 • TLCP Lab Sheets SECTION 5 • Annual Pathogen & Vector Attraction Reduction Forms SECTION 6 • Pathogen & Vector Attraction Reduction Lab Sheets/Records SECTION 7 'Aw IMF' -_Is 2-4 Camp Lejeune Advanced Wastewater Treatment ATAD Facility Transferring Biosolids from Tanker to Applicator Reporting Period 2014 CLASS A ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: W00012346 FACILITY NAME: Camp Leieune AWWTP PHONE #: 910-451-7190 COUNTY: Onslow OPERATOR:,, _ _ Edwin Snider FACILITY TYPE (please check one): ® Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C):� ❑ Distribution and Marketing (complete Parts A, B, C) Was the facility in operation during the past calendar year? Yes ® No ❑ > If No skip parts A, B, C and certify form below Part A Part B Month Source(s) (include NPDES # if applicable) PP ) Volume dr tons Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) JaIlUary Camp Le'eune AWWTP NCO063029 26.7 February Camp Le"eune AWWTP NCO063029 47.5 March Camp Le'eune AWWTP NCO063029 50.4 April Camp Le"euneAWWTP NCO063029 62.7 May Camp Le'eune AWWTP NCO063029 112.9 June Camp Lejeune AWWTP NCO063029 64.9 July Camp Le"eune AWWTP NCO063029 53.6 August Camp Le"eune AWWTP NCO063029 32.0 September Camin Le'eune AWWTP NCO063029 36.8 October Camp Le"eune AWWTP NCO063029 140.9 November Camp Le"eune AWWTP NCO063029 15.5 December Total from FORM DMSDF(sup) 0.0 Totals Annual (dry tons): 643.8 _ Amendments used: ng Agent(s) used:,�� If more space is required, attach additional information sheets (FORM DMSDF (supp)): Part C: Total Number of Form DMSDF (Sapp) L0 Facility was compliant during the past calendar year with all conditions of land application permit ® Yes (Including but not limited to items 1-3 below) issued by the Division of Water Quality: []No —> If No, explain in Narrative 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laborator results are attached. 2. All operation and maintenance requirements were compiled with or, in the: case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention, of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the beset of my knowledge and belief, true, accurate and complete. I nm aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." � r Areparer t Permittee Date Signature ofPreparer** Date (if different from Permittee) is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) DENR FORM DMSDF (12/2006) BIODYNAMIC VOLATILITY ENHANCEMENT LOG WT-310CS SWEET CANE SYRUP (SUGAR WATER) • 10 January 2014, 275 gallons was added to Train 1 Reactor A And 275 gallons was added to Train 1 Reactor B. • 16 January 2014, 275 gallons was added to Train 1 Reactor A And 275 gallons was added to Train 1 Reactor B. • 18 January 2014, 275 gallons was added to Train 1 Reactor A And 275 gallons was added to Train 1 Reactor B. • 29 May 2014, 275 gallons was added to Train 3 Reactor A. • 30 May 2014, 275 gallons was added to. Train 3 Reactor A. • 31 May 2014, 275 gallons was added to Train 3 Reactor A and 275 -gallons was added to Train 3 Reactor B. • 18 June 2014, 275 gallons was added to Train 2 Reactor A and 275 gallons was added to Train 2 Reactor B. • 19 June 2014, 275 gallons was added to Train 2 Reactor A and 138 gallons was added to Train 3 Reactor A, and 138 gallons was added to Train 3 Reactor B. • 21 June 2014,138 gallons was added to Train 3 Reactor A and 138 gallons was added to Train 3 Reactor B. • 15 September 2014, 275 gallons was added to Train 1 Reactor A and 275 gallons was added to Train 1 Reactor B. • 23 September 2014,138 gallons was added to Train 1 Reactor A ' And -138 gallons was added to Train 1 Reactor B. • 24 September 2014,138 gallons was added to Train 1 Reactor A And 138 gallons was added to Train 1 Reactor B. BIODYNAMIC VOLATILITY ENHANCEMENT LOG WT-310CS SWEET CANE SYRUP j (SUGAR WATER) _l • 25 September 2014, 275 gallons was added to Train 1 Reactor A. • 17 November 2014, 275 gallons added to Train 3 Reactor A, and 275 gallons added to Train 3 reactor B. • 29 December 2014, 275 gallons added to Train 3 Reactor A, and 275 gallons added to Train 3 Reactor B. i 30 December 2014, 275 gallons added to Train 3 Reactor A, and L 275 gallons added to Train 3 Reactor B. ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF -13 WQ Permit Numner: WQ0012346 Laboratory 1) EQM.EMD _ Facility Name: Camp Leieune AWWTP 2) Environmental Chemists, I Residual Source WQ# or 3)�_ _ NPDES # .N00063029 4) WWTP Name: Camp Leieune AWWTP 5) Parameter m /k Ceiling Conc.Limit Sam le or Com osite Date 1 14/2014 4/82014 7 15/2014 10 28/20 4 _ Percent Solids NA - 2.700 2,85 2.720 1.6.40 Arsenic 75 3,330 12.300 4.690 5 E70 admium 85 .3.670 3.610 5.560 5: 70 _ C000er 4,300 415.00 358.00 494.000 26 .000 Chromium NA 35.90 23.900 31.300 19.400 Lead 840 9.1101 12.100 13.300 7.600 Mercury 7 0.889 0.596 0.801 1.270 _ Mol bdenum 75 3.890 3.370 7.700 5.570 Nickel 420 23.400 21.300 30.400 22.600 Selenium 1 3.330 3.470 5.360 ' 6.1.40 Zinc 7,500 1.280.0001 1.190.000 1.640.000 778.000 Total Phos horns NA 50 800.00 6.320.00 49 900.00 48 40 ).00 _ TKN NA 70 8 0.0 85,300.00 . 68 500.00 100,00).00 Ammonia -Nitro en NA 34 900.00 34 100.00 60100.00 64 0 ). 0 Nitate-Nitro en NA 64.8001 47.300 16.300 1.270 _ "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. _ I am aware that there are significant penalties for submitting false Information, including the possibility of fines and imprisonment fir knowing violations." Signature of Preparer* Date •Preperer Is de0ned In 40 CFR Part503.9(r) and 15A NCAC 2T.1102 (26) DEM'FORM SSF (12/2006) 6602 Windmill Way e Wilmington, NC 28405 _ _ (910) 392-0223 (Lab) a (910) 392-4424 (Fax) srn ! i 0 Bowsertown Road e Manteo, NC 27954 (252)473-5702 AN,:LYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 USMC Camp Lejeune Date of Report: Feb 17, 2014 12 Post Lane Customner PO r-: Camp Leleune NC 28547 Report J#% 2014-00601 Attention: Alberta Y. Okamoto Report to: Alberta Y. Okamoto Project ID: Lab ID Sample ID: Collect DatelTime Matrix Sampled by 14-01179 Site: CROM Tank 1/14/2014 8:15 AM Solid/Sludge Snider Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 43700 mg/kg 02/04/2014 Arsenic EPA200.7 <3.33 mg/kg 01/22/2014 Cadmium EPA200.7 3.67 mglkg 01/22/2014 . Calcium EPA200.7 64400 mg/kg 02/05/2014 chromium EPA200.7 35.9 mg/kg 01/22/2014 Copper EPA200.7 415 mg/kg 0112212014 Lead EPA200.7 9.11 mglkg 01/22/2014 Magnesium EPA200.7 5150mg/kg 02/05/2014 Molybdenum EPA200.7 3.89 mglkg 01122/2014 Nickel EPA200.7 23.4 mg/kg 01/22/2014 Potassium EPA200.7 7590mg1kg 02/05/2014 Selenium EPA200.7 <3.33 mg/kg 01/2212014 Sodium EPA200.7 5560 mg/kg 02/05/2014 Zinc EPA200.7 1280mg/kg 02/04/2014 Ammonia Nitrogen EPA350.1 34900 mg/kg 01/17/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 70800 mg/kg 0112312014. Nitrate+Nitrite-Nitrogen EPA353.2 64.8mg/kg 0211412014 Total Solids (%) SM 2540 B 2.70 % 01115/2014 pH SM 4500 H B 7.85 units 01/23/2014 Total Phosphorus SM 4500 P F 50800 mg/kg 01/24/2014 Mercury SW8467471B 0.8890mglkg 01/17/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. "eviewed by: _0OULT( '0 UaN& Report#:: 2014-00501 Pagel of 1 Analytical & Consulting Chemists CLIENT: Commanding-G 12 .Post-. Lane Camp L-eieur 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com (I0�0 PROJECT NAME: Camp Lejeune MCB REPORT NO: _ CONTACT NAME: IAlberta Y. Okamoto PO NO: REPORTTO: Patricia H. Ra er PH ONFJFAX: 910-451-0020 (fax) 910-451-7195 28547 COPYTO: ' email: patricia.raper@usmC.mil — G.�..9 Of c1..Ano rtttiar- ENVIRONMENTAL CHEMIST 3 INC NCDENM DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY '��rBl ledDY:2 s�I 1 SAMPLE TYPE: �� Collection p c Sample lclentuficatiora F�F 1' 9 ' yh Eo. U V� lute Time Temp I = Influent, E- PRESERVATION ANALYSIS REQUESTED luminum, Arsenic, Cadmiun r _ •Lead— F °' U� tu w d`0 Jx Z X ' I o 0 x w _ CROM TANK -I - L O L LUD E-C P �) G G C P 4agnesium, Molybdenum, TlcZeE, 7o assium, o a.utn, elenium, Zind, Mercury Sludge, Nitrite, G G - C P G -- -- --- C P G G C P FKN, Total Solids/Soils & - — -- G G - C P 3hosphorus G G - ---- C P G G P G G `- G G C P G j G r DatelTime Received By: Date rime Transfer Relinquished By: 2• 1= ..., ,t. Resamole Requested: 8 emperaTure w"nln neaet Deliverer M:� r✓ omments: - lq Time: i h :NA OUND: Date: Client: Date Collected: Date Received: Sample: . Analyte % Solids pH Marine Corps Base @&EE/El-IiD!/ECIS 12 Post Lane Camp Lejeuner NC 20547 FC Wastewater 1/14/2014 1/14/2014 Quarterly Sludge Date Results Units Analyzed 2.80 % 1/15/2014 7.83 SU 1/14/2014 Tech Method AYO AYO CERTIFIED BY: 2540B - 1997 4500H+ B - 2000 PATRICIA H. RAPER Chain of C�uty Record CLIENT: Commanding General ISLE/EIVID/ECB 12 Post Lane Camp Lejeune, NC 28547 Attn: Alberta Y. Okamoto (910) 451 - 0020 Collected by: Date 1Colht.cted: Time CoHected: - ---- - t._a CaViorB of S8.Pru nBG - truck Loading Station CouiUia'Grab: Grab Number of Containers: 2 --- -- %Solids, pH i®c'ciEa�nsted: _ _ Report all results as mg/kg drywt.__ W,vs sE mn!n dochiori.U'liate'd _��ti f-_vi'fi ��aGtiQ7 C11; g a� ,? _ IGe, e's ^T—� Y_ I lfield pN: W _ Comments: _ - relinquishred b>>T--,_— -� rate W �M Time _� Received by: r — Date -- I ir7re — r _ �fi D. 15 CAMP LEJEUNE VVWTP p PH Fm-' E A rL-' jR N G S C 3 F R QUART ERLY SLUDGE SAMPLING COLLECTED DATE COLLECTED: TiME: L) t � BY: DATE: 1.14.1 ANALYZED BY: 04 TIME: METHOD: 4500H+ B - 2000 6&2,� _ TIME VOLUME % SAMPLE TEMP pH (SD) COLLETIMECTED ANALYZED RECOVERY UALIbKA I IUN BUFFER 4.00 6 0 4.01 CALIbRA I IUN BUFFER 10.00 �-Lmwjg 60 10,0L W itM",4 il MR -,' a CHECK BUFFER 7.00 60 CROM TANK OV 100 -7 V. .... .sus..,.. . CROM TANK DUP 100 'om 4 211; CHECK BUFFER 7.00 60 FORM UPDATED: SEPTEMBER 2012 CHECKED BY: i i '4 '+"Lli x` ni. LL1:.. a-eT,._I 1.1a"11 IC J=L, e 660, Wbdmill Way o WilmiiLgton, NC 2S^_05 (910) 392-0223 (Lab) c, (910) 392-4 24 (Fax) s 710 Bona*sertoTn Li Road 6 Ia mteo,1\C 27954 - (252) 473-5702 ANALYTICAL L.GONSUI T!NG CHEMISTS NCDE1\TR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 UrSMO Cali p Lejeune Date of Report. May 02, 2014 12 Past Lane Custo:r e,r, F0 Camp Lejeune NC 28547 Report r�: 2014-04161 Attention: Alberta Y. Okamoto Report, 'Lc: Alberta Y. Okamoto Project ID: Camp Lejeune MCB Lab ID Sample ID: Collect DateMme Matrix Sampled by 14-10030 Site: CROM Tank 4/8/2014 7:45 AM Solid/Sludge Acosta Julius Test Method Results Date Analyzed Aluminum EPA200.7 32300mg/kg 04/21/2014 Arsenic EPA200.7 12.3 mg/kg 0411712014 Cadmium EPA200.7 3.61 mg/kg - 0411712014 Chromium EPA200.7 23.9 mg/kg 04117/2014 Copper EPA200.7 .358 mg/kg 04/14/2014 Lead EPA200.7 12.1 mg/kg 04/17/2014 Magnesium EPA200.7 4630 mg/kg 04/14/2014 Nlol-bdenum EPA200.7 c337mrt/4n 04,11TI2014 Nickel EPA200.7 21.3 mg/kg 0411712014 Potassium EPA200.7 6320 mg/kg 04/14/2014 Selenium - EPA200.7 3.47mg/kg 04/23/2014 Sodium EPA200.7 4420 mg/kg 0411412014 Zinc EPA200.7 1190 mg/kg 04/23/2014 Ammonia Nitrogen EPA350.1 34100 mg/kg. 04/22/2014 Total Kjeldahl Nitrogen (TKN) EPA 351.2 85300 mg/kg 04/30/2014 Total Solids (%) SM 2540 s 2.85 % 04/09/2014 Total Phosphorus SM 4500 P P 46200 mglkg 04/29/2014 Mercury SW8467471B 0.5960 mg/kg 04/21/2014 Nitrate Nitrogen (cafe) Nitrite Nitrogen EPA353.2 11.3 mglkg 04/10/2014 Nitrate+Nitrite-Nitrogen EPA353.2 47.3mglkg 04/21/2014 Nitrate Nitrogen Subtraction Method 36.0 mg/kg 04/23/2014 Comment: Results reported on a dry weight basis. Reviewed by: op(I*- Report#.-: 2014-04161 Page 1 of 1 i♦ • �(� r eu Analytical &. Consulting Chemists ENVIRONMENTAL oflEM1STS, -ANC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 r.e ■ n r1■ Ar nr �CTl1[-Irl 6602 Windmill Way Wilmington, 405 OFFICr: 9.10-092-0223 FAX 9.10-3:jc-4424 info@environmenlalch� emists.coi / CI_IENT�Cammanding General PROJECT NAME: Camp Lejeune MCB ILI�-4. REPORT No ADDRESS: I&E/EMDIELS CONTACT NAME: Alberta Y. Okamoto PO NO: _ 12 Post Lane REPORT TO: Patricia H. Raper PHONEIFAX: 910-451-0020 (fa)o 910-451-7195 Camp Leieune, NC 28547 COPY TO: I email: atricia.ra per usmc.mil -'---- _ em......a %nr_Mr-ty OT- qzf-- sn = !-;n�u tii - tininne- LJMer. Sample IdentificationE Collection >, v� ~ °o c A o U d _ (+ 0 `o V !~ m FLU o o E a m PRESERVATION lUSALYStS REGtU!_STL-:D ------ Date Time Temp z o $ oz o w CROM TANK - V MUD UM C P X luminum, Arsenic, Cadmiun gym, —Go Vagnesium, Molybdenum, is e , o assium;�o 1um, elenium, Zinc, Y 8v y o7YSr G G C P G C G P G. G C p 4ercury Sludge, Nitrite, qi J- ra .e,. Ni i-rai e-N-3 G G C P Vkaq, Total Solids/Soils & hosphor_us _ _G G G G C P G G C P G G- C P G G C P ---- G G Transfer Rei quished By: Date/Time Recrjved By: Date#Time � • 2. fl"CaS'To� `i ors 0 _ r•._-e._ ._-n. t emperawire w I fHccepieu:� Delivered By.v �-L=— _�_ Received By Date: Comments: TUR ARI UND: Client: Effete Collected: Date deceived: Semple: Ana@yte % Solids pH Camp Lejeunel NIC 2,13547 4 -- L4 _ "T--112 e I L FC Wastewater 4/00/20 4 4/Q/2014 Quarterly Sludge Date Results Unks Ana@yzed 2.80 % 4/8/2014 1.6 SU 4/8/2014 Tech Method DI% 2I-rVQU - 1997 DRS 4500H+ B - 2000 CERTIFIED BY: TIM BOC NGER� b _TENT: Commanding General I g,.E/EM D/ECB 12 Post Lane Camp Lejeune, NC 28547 Attn: Alberta Y. Okamoto (910) 451 - 0020 i Date Collected: d: s011-n-plot.. Truck Loading Station -----LOCE41.1un, _ --_ ccxaigl ,%Gvalr: Grab Muniiber 01 CoEitainers: 2 % Solids, pH t=Fc�Efi-W: _ —Report all resuli:s as mg/kg dry vnrt__— dF._a frfEan°iai::tE*c` n/a --�nfa_s,�,rrifRo _ -- - lw fi( Cr,CifcFiC,ln")i •'sr.d:EiIIICa': YESS ---- Relllif�UlSl"IC?d by: --- Date!f I-Iil—G��` Received by: __ - C�al:e_-__-- -- I irr.e CAMP LEJEUNE TFF PHU RILE- Ak, ED, 1, H G T`21 F 0 RR QUJA, R' T E R, L 8 L U 0) . G E 8 P -1 NA, F. L I Nli, 35 COLLECTED BY: DATE COLLECTED: T I Ml E: DST LE T i", fTb E: ANALYZED BY: METHOD: A500H.+B-2000 TIME TIME VOLUME % SAMPLE TEMP pH (SU) —COLLECTED ANALYZED mLs L;ALIbKA] ION -RECOVERY BUFFER 4.00 60 Ll if -Al MWATIMKI -3 BUFFER 10.00 3. N 60 0 CHECK BUFFER 7.00 60 gpg CROM TANK loo •1 7 -."U" lk-A W CROM TANK DUP e4L-y<-753 100 -2) "2s-,9 ..... ...... CHECK BUFFER 7.00 60 FORM UPDATED: SEPTEMBER 2012 CHECKED BY: Environmental Chell"Iy1sts, Inc. ® 6602 AFindmill Way e Wilmington, NC 28405 (910) 392-0223 (Lab) Y (910) 392-4424 (Pax) srr 710 Bowsertown Road m Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMIST NCDENR: uvdQ CERTFCAi EE #94. DLS C—EX iriCA'I E #'3r i29 USMC Camp Lejeune 112 Post Lane Camp Lejeune NC 28547 Attention: Alberta Y. Okamoto Cate of Report: Aug 20, 2014 Cc: tamer P C: Customer IC: 12060026 Report M. 2014-08683 Project ID: Camp Lejeune MCB Lab ID Sample Ilia: 14-21485 Site: CROM Tank Test Collect CatefTime 7/15/2014 7:40 AM Method Matrix Sampled by Solid/Sludge Acosta Julius Results ®ate Analyzed Aluminum EPA200.7 62200 mg/kg 07/28/2014 Arsenic EPA200.7 <4.69 mg/kg 07/26/2014 Cadmium EPA200.7 5.56 mg/kg 07/25/2014 Chromium EPA200.7 31.3mg/kg 07/26/2014 Copper EPA200.7 494 mg/kg 07/25/2014 ,ead EPA200.7 13.3 mg/kd 07/25/2014 Magnesium EPA200.7 7650 mg/kg 07/31/2014 Molybdenum EPA200.7 7.70 mg/kg 07/25/2014 Nickel EPA200.7 30.4 mg/kg 07/25/2014 Potassium- EPA200.7 9180 mg/kg 07/31/2014 Selenium EPA200.7 5.36 mg/kg 07/25/2014 Sodium EPA200.7 8420 mglkg 07/31/2014 Zinc EPA200.7 1640 mg/kg 07/28/2014 Ammonia Nitrogen EPA350.1 60100 mglkg 08/19/2014 Total Kjeldahl Nitrogen (TKN) EPA 351.2 68500 mg/kg 08/19/2014 Total Solids (%) SM 2540 B 1.96 % 07/23/2014 Total Phosphorus SM 4500 P F 49900 mg/kg 08/01/2014 Mercury Sw8467471B 0.8010 mg/kg 07/28/2014 Nitrate Nitrogen (calc) Nitrite Nitrogen EPA3532 375 mg/kg 08/12/2014 Matrix interference. Nitrate+Nitrite-Nitrogen EPA353.2 16.3 mg/kg 07/3012014 Nitrate Nitrogen subtraction Method <1.02 mglkg 08/13/2014 .omment: Results reported on a dry weight basis. Reviewed by: Report #:: 2014-08683 Page 1 of 1 . Aqlr er Analytical 8. Consulting Chemists CLIENT: Commandina G 12 Post Lane Camp Lejeune NC 2854 Sampled BY: c��Sta vL� <' S Collect Sample Identification Tim CROM TANK Date ENVIRONMENTAL CHEMISTS$ INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION. AND CHAIN OF CUSTODY 6602 Wiaidmill Way Wilmington, A05 � OFFICE: 910-392-043 PAX 9•10-392-4424 Info@environmentalchemists_c0m PROJECT NAME: Camp Lejeune MCB REPORT NO: CONTACT NATIVE: Alberta Y. Okamoto PO NO: - -- REPORT TO: Patricia H. Raper PHONEIFA)C: 910-451-0020 (fax) 910-451-7195 7 COPYTO: email: natricia raper(c�usmc.mil u SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stre iara d c d _ W PRESERVATION �y C A tN C p G, (Q(� J O p d�d W N F O C)V~ V E J x X z S 2 O e Temp SLUD13,19 C P X Li e-, r_ I LWti C P G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By: Datelrime 2. ' vw- l 5.1 y e'ected• Resample 1 Temperature when Received: • 0 Accepted: 1 y Delivered By: 1�i[•4A-&O WILD S' Received By: Date TU Comments- 1, So = Svil, SL a Sludge, Glher: ANALYSIS'REQUE-5TED lumiji m, Arsenic, Cadmiun , agnesium, Molybdenum, icReT,—Fo-Tassium, o Zum, elenium, Zinc, ercury Sludge, Nitrite, ICN, Total Solids/Soils & oateffime �;•14- 1 Marine Corps Base &E/EKAD/ECR 12 Post Lane Camp Lejeune, NC 29547 Date: 8/14/2014 Client: FC Wastewater Date Collected: 7/15/2014 Date Received: 7/15/ 2014 Sample: Quarterly Sludge Date Analyte Results Units Analyzed Tech Method Solids 2.72 % 7/15/2014 DRS _ 2540B - 1997 pH V 7.9 SU 7/15/2014 DES 4500H+ B - 2000 CERTIFIED BY: f TIM BOLLINGER Chain of Custody Record LIENT: Commanding General I&E/EMD/ECB 12 Post Lane Camp Lejeune, NC 28547 Attn: Alberta Y. Okamoto (910) 451 - 0020 Collected by: Signature• , j Date Collected: O ? 1- Time Collected: © 7 7' a Location of sample: Truck Loading Station Comp/Grab: Grab Number of Containers: 2 Analyses Requested: % Solids, pH *** Report all results as mg/kg dry wt. Was sample dechlorinated? n/a Preservation:. Ice Regulatory Sample: Yes Field pH: Comments: Relinquished by: Date Time Received by: saran Date Time 4� H READINGS FOR QI VdpffrP V SP M IDGE SA MaMUNP135 r ' _ C:VLLtC:ItU � LATE COLLECTED: T €hTi E: BY: DATE: -1 : t t�- . l$ TIME: ANALYZED BY: bes METHOD: 4500H+ D - 2000 01 I' SAMPLE TIME TIME VOLUME TEMP pH ��U' % COLLECTED ANALYZED mLs RECOVERY FFER4.00 BPSUI ' �5n,T~'�--w—T�yLt " ��ai `5.]C� ', 's' w�ri �-�,p_J"�x' af,:M„�e..,Zi.'+:. ,�,�: .-..•Z._r¢, xm, I .�i� ��71iW .'` .r.i. �.�i•r!��,t1..^^��z i,���pNy4`a9T°'s4.''�k.•��:66Ir,wY. !5p �r �c`a il, .S +'�Eti N�a:`vy,+ NlP"�a BUFFER 10.00 r�fyxie�fy.9i`��J :fE TvF!c1,:cya.KT.:° �e_'iey'�, Y.R�. F�-^5%tnwyth ��ay;.,.xai�%'ir OU 99 �1 i Y'1 •n �1 =raK< su7 CHECK BUFFER7.00le- ' Q (rs-T�i" ,y/i��NN f' @ c'n,,,�(r'''�°.. ..$, v xti yr fi 60 i'iT;�% dl,. CROM TANK' 0-14-0 O"1 100 33 CROM TANK DUP Eipm . b , ,,._ (3`1� 100 ✓3 ,7 y}... t .. v.e. CHECK BUFFER 7.00 ��_3:^Z,an� it `';�e�'�x:° •r35.a��w`sx"u^.'�.'.^`a�:.E4 FORM UPDATED: SEPTEMBER 2012 CHECKED BY: 6602 Windmill Way a Vdilmington, N`TC 28405 (910) 992-0223 (Lab) e (910) 392-4424 (Fa ) 710 Bowsertown Road 6 Manteo, NC 2.7954 (252) J:73-5702 ANALYTICAL CONSULTING CI- FAISTS 1JCD'r.NR: D14TQ CER=C ATE N-94. DL9 CERTIfCATE 437: 110 USWIC Camp Lejoune Cete of Rcport: Nov 20, 2014 12 Post Lane Pia f1 Camp i_ejaune i C 28847 Custouner CD: 112060026 Attention: Ai'certa Y. Okamoto Rep®rt 9: 2014- i 343 i Project ED: Camp Lejeune MCB, Lab ID. Sample ID: Collect Date/Time Matrix Sampled by 14-32946 Site: CROM Tank 10/28/2014 7:25 AM Solid/Sludge Acosta Julius Test Method Results Date Analyzed Aluminum EPA20o.7 46300mg/kg 11/06/2014 Arsenic EPA2oo•7 <5.57 mg/kg 11/ 1012014 Cadmium EPA200.7 <5.57mg/kg 11/05/2014 Chromium EPA200.7 19.4 mg/kg 11/05/2014 ^.opper EPA200.7 263 mg/kg 11/10/2014 :ad EPA2ao•7 7.60 mg/kg 11/05/2014 .Aagnesium EPA200.7 4420 mg/kg 11/04/2014 Molybdenum EPA200.7 <5,57 mg/kg 11/10/2014 Nickel EPA200.7 22.6 mg/kg 11110/2014 Potassium EPA2o0.7 8100 mg/kg 11/04/2014 Selenium EPA2001 6.14 mg/kg 11/05/2014 Sodium EPA200.7 7470 mg/kg 11/04/2014 Zinc EPA2001 778 mg/kg 11/05/2014 Ammonia.Nitrogen EPA350.1 64400mg/kg 11/03/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 100000mg/kg 11/04/2014 Total Solids M SM2540 B 1.58 % 11/03/2014- Total Phosphorus SM 4500 P F 48400 mg/kg 11/05/2014 Mercury Sw8467471s <1.27 mg/kg 11/11/2014 Nitrate Nitrogen (cafe) Nitrite Nitrogen EPA353.2 32.5 mg/kg 11/18/2014 Nitrate+Nihlte-Nitrogen EPA353.2 <1.27.mg/kg 11/07/2014 Nitrate -Nitrogen 5ubtracdon WOW <1.27 mg/kg 11/20/2014 Comment:- Results reported on drybasis. :viewed by:. 'weight �a Report#:: 2014-13431 Pagel of 1 ' • u Analytical & Consulling Chemists ENVIRONMENTAL C HEMISTS3 INC NCDENR: DWR CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 rnr r er•rtr�ul AAltl rRle1'Ae ['1C t^_I1�TC1ilY 66D2 Vifinrimill Way Wilmington, a._ /8405 OFFICE: 910-392-0223 FAX 910-392-4424 lnfo r&environmen4ilchemists.c(-�m CLIENT: Commanding Qa PROJECT NAME: Camp Lejeune MCB REPORT Nc1: ADDRESS: I&E/EMD/ELS CONTACT NAME: Alberta Y. Okamoto PO NO: 12 Post Lane REPORT TO: Patricia. H. Raper PHOFJFJFAX: 910-451-0020 (fax) 910-451-7195 Cam Lejeune NC 28547 COPY TO: email: atricia.l•aper(a�usmc.mil 1, . e- -- -. 1 _ a r — aFfl.. .,t w — Wn11 RT = !gfroam_ SC) = Anil. SL = Slud Ge. Mier. Sample Identification Collection n a o E S PRESERVATION ANALYSIS REQUESTED Date Time Temp z ^o ; o w CROM TANK -z SLUDGLEP, C P I X 11UMLIALM, Atisexa.:ic, Cadmiuii 4agilesium, Molybdenum, 1C ;-e_ � �tassaum, o ium, elenium, Zinc,�_� C P G C G P G G C P ercui-y Sludge, Nit7:i't:e, i t7y. - l�U�.s al�e.J�� tom' . G G C P 1 lit -1 -1 rKN, Total Solids/Soils & 3 udgu�:KtrmortT�,—"T a t hospho_cus G C G P G G C P _ G G C P G G_ C P G G C P Transfer 1. Relinquished By: C Ste' 1UC-cJ S Datefrime •2 Received By: Datefiime ,y :gyp �7i /! �cry9`Yr/s , f plQ �� I emperature wnen Kecelvea:_p . Z-a�Acceptew r�e�e�1. �. •• I.�.�Ia1.11,... �- ��.-- ._ - Delivered By: Received By:^! Date: L 1 Y Tune: Comments: TURNAROUND: 0 Date: Client: Date Collected Date Received: Sample: 11/3/2014 FC Wastewater 10/28/2014 10/28/2014 Quarterly Sludge rtga, `Ere Corps G��sc ProE/E- 50D/Er—F, 2- Post Lane Camp Lejeuner NT-C 285,47 Date Analyte Results 'Units Analyzed Tech Method Solids 1.64 1 % 10/30/2014 DRS 2540B - 1997 pH 7.8 SU 10/28/2014 AYO 4500H+ B - 2000 CERTIFIED BY: TIM BOLLINGER b ;LIEIVT: Commanding General I&E/EMD/ECB 12 Post Lane Camp Lejeune, NC 28547 Attn: Alberta Y. Okamoto (910) 451 - 0020 _—_—_ -- Collected by: Signature:. — Date Coilected: lC3 • 2 / `f Time Collected: OP Z Sr- --_— L €rcationr. of sE FrIple: Truck Loading Station CrN�un/� alp: _—_— ^N_ Grab %kuiki er of Conitt.ainers: 2 __— AE6a.iyse5 €1.equ steel: % Solids, pH Report all results as mg/kg dry wt. _ Woo. sarmpkc decrh-YIo' rfFlatod? fl n/a faro F36.vailion: _ .� — ----- ICG (tC''Eli�fiC�fi�(^f:k`FiXGf3: _ _ YCss Relinquishod by:----� _-�— -- — -Date Tinge ^ ��--Received by: CAMP LEJEUNE V TP pH RE I=,:,, Mf,-�GS FO R -QLJNlk. RTLEFFR LY SLUDGE S-AIMPL�, NG DATE COLLECTED: P L- ,-7 p - / V DATE: ANALYZED BY: u T I kh E: BY: TIME: METHOD: 4500H+ B - 2000 TIME TIME VOLUME % SAMPLE TEMP pH(SU) COLLECTED ANALYZED mLs EC- VERY L;ALIbKA I JUN T1 WK , 4-00 i-R4 ;O ma BUFFER 4.00 60 �'!m UALI bKA 1 !(-1- BUFFER 10.00 $01 60 W OWN ON INN 60 WEI MOORE CHECK BUFFER 7.00 WDOW 60' MINIM CROM TANK ol)� loo BOOM sAfto-11-10.1, -P" g1 mommo 1 R WIN ILI" CROM TANK DUP 100 I'loll-I CHECK BUFFER 7.( 0 FORM UPDATED: SEPTEMBER 2012 CHECKED BY: � F � � � C.Jl eirn ' s- g am ® e !! h 9 6602 Windmill Way o Wilmington, NC 28?05 (910) 392-0223 (Lab) . (910) 392 41224 (Fax) 710 Bowsertown Road o Manteo, NC 27954 (252)a73-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENP: DWQ CEP,=A'TE t 94. DLS CEPXLrJCAT . T3772° USMC Camp Lejeune Date of Report: Feb 19, 2014 l t'1 P'� F.-- �_ O h.a r'C,.4,t Lane ��� r�rE<�cE �'Lu �� Camp Lejeune NC 28547 Repof� �:. 2014-00502 Attention: Alberta Y. Okamoto Report to: Alberta Y. Okamoto Project ID:. Camp Lejeune MCB Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-01180 Site: CROM Tank 1/14/2014 8:20 AM Solid/Sludge Snider Test Method results Date Analyzed Chlordane SW 846 Method 80818/3510 <0.005 mg1L 01123/2014 Endrin SW 846 Method 8081 B/35i0 <0.00005 mg/L 01 /23/2014 Heptachlor SW 846 Method 8081 B1351 0 <0.00005 mg/L 01/23/2014 Heptachlor epoxide SW 846 Method 8081613510 <0.00005 mg/L 01/23/2014 Lindane SW 845 Method 8081813510 <0.00005 mg1L 01/23/2014 Vlethoxychlor SW846 Method 8081 B13510 <0.00005 mg/L 01/23/2014 Toxaphene ' SW 846 Method 808iB/3510.. <0.005 mg/L 01/23/2014 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/23/2014 2,4,5-Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 01/23/2014 2,4,6-Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 01/23/2014 2,4-Dinitrotcluene (TCLP) SW 846 method 8270/3610 <0.050 mg/L 01/23/2014 Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01123/2014 Hexachloro-1,3-butadiene (TCLP). SW 646 method B27013510 <0.050 mg/L 01/23/2014 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/23/2014 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/23/2014 m + p-Cresol (TCLP) SW B46 method 827013510. <0.050 mg/L 01/23/2014 Nitrobenzene (TCLP) SW 845 method 8270/3510 <0.050 mg/L 01/23/2014 o-Cresol (TCLP) SW 846 method, 827013510 <0.050 mg/L 01/23/2014 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 01/23/2014 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg1L 01/23/2014 2 4 5-TP SW846 Method 8151A <0.0003 mg/L 0,1/2812014 2,4-D SW846 Method 8151A <0.0003 mg/L 01/28/2014 1,1-Dichloroethylene SW846 Method826015030 <0.01mg/L 1/30/2014 1,2-Dichloroethane SW846 Method 826015030 < 0.01 mg/L 1130/2014 Benzene SW846 Method 826015030 < 0.01 mg/L 1 /301201 A Carbon Tetrachloride SW846 Method 8260/5030 < 0.01 mg/L 1 /30/2014 Report R : 2014-00502 Page 1 of 2 6602 Windmill Way 6 Wilmington, NC 28405 (910) 392-0223 (Lab) 0 (910) 392-4424 (Fax) sni 710 Bowsertown Road ® Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCD--E7,Ti : D Q CER1 � E CA i E j7k. D- S CEZ'i` C—A.TE #37. 729 USMG Capp Lejeune Cate of Report: Feb 19, 2014 12 Post Lane Camp Lejeune fqC 2854% 4,--,et Aiiention: Alberta Y. Okamoto Report*j: 2014-00502 Report to: Alberta Y. Okamoto Project ID-. Camp Lejeune MCB Chlorobenzene SW846 Method 8260/5030 < 0.01 mg/L 1/30l2014 Chloroform SW848 Method B260/5030 < 0.01 mg/L 1/30/2014 Methyl ethyl ketone SWU6 Method 8260/5030 < 0.05 mg/L 1/3012014 Tetrachloroethylene SW846 Method 826015030 < 0.01 mg/L 1/30/2014 Trichloroethylene, SW846 Method 8260/5030 < 0.01 mg/L 1/30/2014 Vinyl Chloride SW840 Method 8260/5030 < 0.01 mg/L 1/30l2014 RCl Cyanide EPA 335.4 <0.119 mg/kg 01 /31/2014 i sM 4500 x a 7.89 units 01 /23/2014 Ifide sM 4500 s a 13.1 mglkg 02/03/2014 lgnitability SW 846 method 1010 >212 OF 01128/2014 TCLP Metals Arsenic EPA200.7 <0.100mg/L 02/03/2014 Barium . EPA200.7 <0.100mg/L 02/01/2014 Cadmium EPA2o0.7 <0.100mg/L 02/03/2014 Chromium EPA200.7 <0.100mg1L 02/03/2014 Lead EPA 200.7 <0.100 mg1L 02/03/2014 Selenium EPA200.7 <0.100 rrig/L 02/04/2014 Silver EPA200.7 <0.100 mg/L 02/01/2014 Mercury swe467470A <0.002mg/L 02/14/2014 Comment: RCl reported. on an as received basis. Reviewed r i Report #:: 2014-00502 Page 2 of 2 ENVIRONMENTAL HEM[ STS, INC Anafylical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHIiS: DLS CERTIFICATION # 37729 is rlr r�+T��1w1 Awrn nd-IAird #'1C #_"Q_rn VM 6602 Windmill Way Wllrnington, r.. .j405 OFFICE: 910�92-0223 FAX 910-392-34211. info@environmentaiahemists.com CLIENT: Com n in it - PROJECT NAME: Camp Lejeune MCB REPORT NO: Z/_ — ADDRESS: I&E/E.MD ELS CONTACT NAME: Alberta Y. Okamoto PO NO: 12 Post Lane REPORT TO: Patricia H. Raper' PHONFJPAX.- 910-451-0020 (fax) 910-451-7195 Camp Lejeune NC 28547 COPYTO: email: atricia.ra er usmc.mil - SARR01 = TYPE' I = Influent, E = Effluent, W Well ST' Stream, SO =Soil, SL Sludge, Mier Sam led B - Sample Identification Crom Tank "— ` Collection rA gL E o � C 4_ o a V✓ P V lu S� Y „ l�� tj�V r PRESERVATION: - — . ANALYSIS REf�UESTGD --- rctP - volatile, Semi -volatile, est'icides, Herbicides, Date Time 2f7 Temp o x x N x o z x Q; x: p G G C P RCRA (8 metals G G Zeactivity, Corrosivity, Ignitiability C P G G C p _ G G C P _ - G G C P G G C P �— G G C P G G C P _ __-- GG C P G G Transfer Relinquished By: Daterrime Received By: Da.£efiirsle y--ly 2. - _Date: TUR 8 DLIND. __ Chain of Custody.Record CLIENT: Commanding General l8tE/ENID/ECB 12 Post Lane Camp Lejeune, NC 28547 Attn: Alberta Y. Okarnoto (910) 451 - 0020 � g— _ .`vif�. natICB'f'.: ---- ------ Date Collected: .l h-ne %oiled ed: L.Cecitio-Irn of 88i11bj2 2: ------•truck Loading Station --___-- ___grL bli )/Gvalb: Grab Number of Containers: 2 % Solids, pH —_....._— _6►C��tl�rsc�r, Rklkq ested: Report all results as mg/kg dry wt.__ _^ P,re 3wfrveliIfan: Ice; Rnc Eal��tcrrry:s�,a�ti�* Yes — I Field ift [Comments: r elinquished bar--�— _. Gate —� —_�_ Time -_— Received by: - — _— Date —_ — �.1 NTYJAL PAS F€Q CENT AND VECTOR ATTRACTION REDUCTION FORS T (503 Rules) Facility Name:. Camp Lejeune AWWTP WQ Perm t number: WQ0012346 ` -WTP Name: Camp Lejeune AWWTP NPDRS Number: NCO063029 ionitoring Period: From 1/1/2014 To 3/31/2014 Pathogen Deduction (40 CFR 503.32) - Please Indicate level Achieved and alternatve performed: Class A Alternative 10 1 Alternative 2 ❑ I Alternative 3 ❑ Alternative 4 ❑ I Alternative 5 ❑ I ' Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": I Compost ❑ I heat Drying F� I Heat Treatment F� Thenmophillic XI 1 Beta Ray ❑ Gamma Ray ❑ I Pasteurization Class B Alternative 1 ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ I Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level In Sludge Pathogen Density Number of Exceedences Frequency of Analysis Sample Type Analytical Technique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) 1.00 1.27 4.00 NTN/g 0 Weekly Grab SM9221E Sabnonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed Alt. 1 (VS Reduction) ❑ Alt. 2 (40-Day Bench) ❑ I Alt. 3 (30-Day Bench) ❑X Alf. 4 (Spec. 02 Uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization) ❑ I Alt. 7 (Drying -Stable) ❑ Alt. 8 (Drying -Unstable) U Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ I No vector attraction reduction alternatives were performed ❑ . CERTIFICATION STATEMENT (please check the appropriate statement) ❑X "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requrement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requrement in 40 CFR 503.33 have not been met." (Please note if you check this statement attached an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the infromation used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." 17 L J 1 k(- c5N 1 DJ:oD- 6-( V10 l5 Preparer Name and Title (type or print) Signature of Preparer* Date 5b f4 c51ViP671-1-'K.KV0) �51n Land Applier Name and Title(if applicable) (type or print) r 0 Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) DENR FORM PVRF 503 (12/2006) L-- ACTUAL PATIIOGENT AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Fae ity Name: Camp Leieune A`W\uTP WQ Permit number: ` Q0012346 Vv'VVTP Name: Camp Lei eune AWW P NPBE+ S Number: NC0063029 lUon1toring Period: From 4/1/2014 To 6/30/2014 Pathogen R.educdon (40 CFR 503.32) - Please ftidicate level achieved and- alterriative performedl: Class A Alternative 1 '�> Alternative 2 0 Alternative 3 0 Alternative 4 Alternative 5 E] I Alternative 6 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": r---� I I T I � I Compost' Ell treat Drying L7 I teat Treabnent'� The_rmophillic I I Beta Ray ❑ Gamma Ray ❑ Pasteurization Class 13 Alternative 1 Alternative 2 If applicable to alternative performed (Class lI only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying'Q I Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class R) complete the following monitoring data: Parameter Allowable Level In Sludge Pathogen Density Number of Exceedences Frequency of Analysis Sample Type Analytical Technique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) 1.00 1.00 1.00 MPN/g 0 Weekly Grab SM9221E Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed. Alt. 1 (VS Reduction) Ej I Alt. 2 (40-Day Bench) ❑ Alt. 3 (30-Day Bench) RX Alt. 4 (Spec. 02 Uptake) Alt. 5 (14-Day Aerobic) ❑ I Alt. 6 (Alk Stabilization) Alt. 7 (Drying -Stable) Alt. 8 (Drying -Unstable) El I Alt. 9 (Injection) 1:11 Alt. 10 (Incorporation) No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) QX "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requrement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 563.32 and the vector attraction reduction requrement in 40 CFR 503.33.have not been met." (Please note if you check this statement attached an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed. to ensure that qualified personnel properly gather and evaluate the infromation used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Ej-R (1-1 V D ) * -� L', P v )e�,�> L-� /--/ - 61 V Preparer Name and Title (type or print) Land Applier Name and Title (if.applicable) (type or print) �i Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) DENR FORM PVRF 503 (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORlif (503 Rules) Facility Name: Camp Lejeune AWWTP WQ Permit number: W00012346 dTP Frame: Camp Lejeune AVJWTP NPDES Number: NCO063029 Monitoring Period: From 7/1/2014 To 9/30/2014 Pathogen Reduction (40 CFR 503.32) - please indicate level achieved and alternative ttiert�xt rrtnri• Class A 'Alternative 1 FX-1 Alternative 2 Alternative 3 Alternative 4 Alternative 5 Alternative 6 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Fj j Heat Drying L7 I Heat Treatment L I 1 henhophillic r¢ B i Beta Ray E) I Gamma Ray Ej I Pasteurization Q li Class B Alternative 1 Alternative 2 a If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting p g ❑ Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level In Sludge Pathogen Density Number of Exceedences Frequency of Analysis Sample Type Analytical Technique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6lh power per gram of total solids MPN CFU . 1000 mpn per gram of total solid (dry weight) 1.00 1.64 10.00 MPN/g 0 Weekly Grab SM9221E Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed Alt. 1 (VS Reduction) Alt. 2 (40-Day Bench) Alt. 3 (30-Day Bench) QX Alt. 4 (Spec. 02 Uptake) Alt. 5 (14-Day Aerobic) U Alt. 6 (Allc. Stabilization) U I Alt. 7 (Drying -Stable) Alt. 8 (Drying -Unstable) Alt. 9 (Injection) Alt. 10 (Incorporation) 0 1 No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) QX "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requrement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requrement in 40 CFR 503.33 have not been met." (Please note if you check this statement attached, an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the infromation used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." 'rJw%Zt/�illt�/:Q (M 5=rAe�jG�Sinf.ill1��,2 L Preparer Name and Title (type or print) Land Applier Name and Title (if applicable) (type or print) 01 Signature of Preparer* r Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) DENR FORM PVRF 503 (12/2006) ANTNUAL PATHOGEN AND VECTOR ATTP A-CTION REDUCTEON FORM (503 Rules) Faeility Name: Camp L ejeune A1A7VdTP WQ Perrnit number: W00012346 VY'WTP Name: Camp Lei eune AVJWJiP NPDES Dumber: NCO063029 Tvhonitoring Period: From 10/1/2014 To 12/31/2014 Pathogen Reduction (40 CFR 543.32) - Please indlcate level achieved and alternative netfor mied: Class A Alternative 1 X Alternative 2❑ Alternative 3❑ Alternative 4 ❑ I Alternative 5 ❑ ( Alternative 6 ❑ Ef applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": f Compost ❑ f Heat Drying L l Neat Treatment l7.l p T helnnop' hillic 5, , f Beta Ray ❑ I Gamma Ray ❑ I Pasteurization ❑ Class Ii'I Alternative 1 ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ I Composting ❑ r Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class P) complete the following monitoring data: Parameter Allowable Level In Sludge Pathogen Density Number of Exceedences Frequency of Analysis Sample Type Analytical Technique Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MTN CFU 1000 mpn per gram of total solid (dry weight) 1.00 4.54 24.00 MPN/g p Weekly Grab M9221E Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed Alt 1 (VS Reduction) ❑ Alt 2 (40-Day Bench) ❑ Alt 3 (30-Day Bench) ❑X Alt. 4 (Spec. 02 Uptake) ❑ Alt 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization) ❑ Alt 7 (Drying -Stable) ' ❑ I Alt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) ❑ Alt 10 (Incorporation) No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) QX "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requrement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requrement in 40 CFR 503.33 have not been met." (Please note if you check this statement attached an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the infromation used to .determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Preparer Name and Title (type or print) &.�,.. 1-7 C,i5 Signature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) DENR FORM PVRF 503 (12/2006) DATE COLLECTED: JLf TIME COLLECTED:t j %—. RECEIVED BY: ``• DATE: i • •� �� TIB�iE• c cr2- 1 _I DATE ANALYZED: - "� ��-' [TIME: METHOD: 3 HOURS at 35 * 0.5'C In INCUBATOR 21 z 2 HOURS -at 44.5 t 0.2"C In WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0,010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF POSITIVES MPRV10+0 mL _ MPOVVGRAliM 1 . / S mL C) Is mL / 5 mL / 5 mL / 5 mL / 5 mL 15 mL / 5 mL OUPY /5 mL /5 mL l - ------ 3 HOURS at 35 t 0.5°C- in INCUBATOR DATE IN INCUBATOR: r , DATE OUT INCUBATOR: 21 t 2 HOURS at 44.5 :L- 0.2°C in WATERBATH DATE IN WATERBATH: DATE OUT WATERBATH: ( � TNEdN INCUBATOR: ! NNCUBA70fl• �� (,,�� T IN WA WATERBATH: r 1` fWAT,RBATH: t POSITIVE CONTROL NEGATIVE CONTROL BLANK SS A 1 BROTH�� DS A-1 BROTH i �' �� N'( FORM UPDATED: APRIL 2007 iFL�FnnTUNCOF 3J 0 TtlIPET 1NpGQF !''-.J' V4119A'UR ✓- WAIFM^TM �lll C = ATt Arr.+m T-m- • S W�tt j CALCULATIOI'J: % TOTAL SOLIDS MPN Fecal Coliiorm/gram sludge l (ATAD SOLIDS ANALYSIS) . _ 10 x. NIPN In L Largest volume x % dry solids CHECKED BY: COPY MADE: CA1V1 LE - AT'AD SLUPGE rECAL ANALYSIS DATE COLLECTED': .�.,�u / TIME COLLECTED: p� 1 COLLECT"Elf BAP: RECEIVED BY: �� �IDATE: j, Icy. f TIG�II�'�(•� -� DATE ANALYZED: CTIME- 1AL.YST: METHOD: . V 3 HOURS at 35 * 0.5'C in INCUBATOR 21 * 2 HOURS at 44.5 :6 0.2'C In WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0,010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF Mp il-VIOD MIL NI1119GARPAI POSITIVES 0 (J 0 v L ti- / 5mL / 5mL / 5mL / 5mL / 5mL / 5 mL / 5mL / 5 mL FDUP l v /5mL /5mL ...... .. 3 HOURS at 35 t 0.5°C in INCUBATOR DATE IN INCUBATOR: (• I C� r DATE OUT INCUBATOR: '. q, f `1- } 21 fi 2 HOURS at 44.5 t 0.2°C in WATERBATH DATE IN WATERBATH: DATE OUTWATERBATH: POSITIVE CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH DS A-1 BROTH S r FORM UPDATED: APRIL 2007 v v TIME IN �� INCUOATOR: TIME OUi ' �� j INCUOATCR• � 1 TIME 1N ^� WATEROATH: '✓'-t V TIME OUT WATERBATH: TFLPEMTUt20F eyj �-r: i ueCueATOPo / � VI TeuPmAT - O2LlAlOR �.� -�• TrurF Tuftdw WATE a TIL TELPFAA7UIrtoF `� f/ ! WAttrGa111: ^(� (7S� % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) CALCULATION: MPN Fecal Coliforrn/41ram sludge — _ 10 x MPN Index Largest volume x % dry solids CHECKED BY: °" ie COPY MADE: ATAD LU -rE AL ANALYSIS DATE COLLECTED: 12L I TIME COLLECTED:. I�ECEWED BY: � DATE: �. DATE ANALYZED: TIME: MEY•H01:1; COLLECTED BY: TIME: 1000 ANALYST: 3 HOURS at 35 * 0.5'C In INCUBATOR 21 x 2 HOURS at 44.5 .*0.2'C In WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10.mL 1 mL 0.10 mL 0.010 mL COMB, OF POSITIVES MP9,1/100 mL MPIVIAGRA M 0-/5mL 0 /5mL O/5mL � /5mL Ci% /5mL n v /5mL %} v /5mL 0•9--c-) 1 r � _ mL ...�. 3 HOURS at: 5 t: 0.5AC- in ONCUBATOR DATE IN INCUBATOR: � • � a, ��- DATE OUT INCUBATOR: (. t 21 :t :2 HOURS at 44,5-:t 0.2-C in WATERBATH DATE IN WATERBATH: �. • .( DATE OUT WAI-ERBATH: j, r If POSITIVE CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH r DS A-1 BROTH ro'S jf � � - U FORM UPDATED: APRIL 2007 L/ U TIME IN _ ,� ^ INCu9A70R: (vyl�(v) TIME OUT Mcu9ATOH: TIME IN / WATERSATN: f v L� TIME OUT WATERBATH: I V TFLPFAArI11K OF �� wweAlvlr. ,(� rwPouTure aF ' � �� Uii19AYOR TFLPPAATIIAe OF j j /% walnleAln: /-�I .-�T/ TdPEBAYUR90F WA1YrrATw ✓ CALCULATION: % TIDTAL SOLIDS MPN Fecal Coliforrn/gram sludge = (ATAD SOLIDS ANALYSIS) . 10 x MPN Index Largest volume x % dry solids CHECKED BY: COPY MADE: -iN- l�- CAMP LJ INE*WWTP DATE COLLECTED: ;l_ _ j FTIWE COLLECTED: 0 36, COLLECTED BY. RECEIVED BY: OL.�,.1�. DATE: , �<. L�- TI IIlI E• �-Pi .i (J (, ry Gl: DATE ANALYZED; r 1 TIME:C _._.. _ _...p METHOD: 3 HOURS at 35 * 0.5'C In INCUBATOR 21 :t 2 HOURS at 44.5 * 0.2"C In WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL '10 mL i mL 0.10 mL 0.010 mL COMI®' OF RRPIW100 sink. POSITIVES RNI!IBdI GRAMA , / 5mL / 5mL / 5mL 0 / 5mL 15 mL / 5mL / 5mL / 5mL [DILIP V 15mL /5mL 3 HOURS at 35 e: 0.5°C in INCUBATOR DATE IN INCUBATOR: r7 4 DATE OUT INCUBATOR: TIME IN INCUBATOR: TIME OUT INCUBATOR: rUVAT 11. J C vXetuerTom // J T@�Pfl1ATUNLOF 2 � •� uCUMTOR .J 21 -t 2 HOURS at 44.5 :t 0.2°C in WATERBATH _ DATE IN WATERBATH: � , f�• I TIME IN r`� WATT AAM - 44-T1 WATERBATN: waTmearn: DATE OUT WATERBATH: ,yam, ij^ L� TIME WATERS i. v �O TE7lFFAANIeEOF 4d WATERBATH: l warrrr.+m POSITIVE. - CONTROL CONTROL BLANK SS A-1 BROTH DS A-1 BROTH OS 1- FORM UPDATED: APRIL 2007 C: J (� % TOTAL SOLIDS (ATAD SOLID'S ANALYSIS) 5 CALCULATION: MPN Fecal ColifOrm/Aram sludge = _,10 x RIIPN in le?, Largest vole ne x % dry solids CHECKED BY: COPY MADE: " li CAMP LEJ")NE WWTP A TAD SLUDGE FECAL A LYIS DATE COLLECTED: LiE= aFME'COLLECTED: 0 ,§ SCOLLCCTE,ID RECEIVED BY; DATE: TIME; O57�L' DATE ANALYZED; TIME: EN=AL:Y�T. , 3 HOURS at 35 0,51C In INCUBATOR 21 z 2 HOURS at 44.5 t 0.2:'6 In WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF POSI'nVE S [WPI d/100 mraP.. MItw1unc!m / 5 mL 0 / 5 mL 0 / 5 mL D / 5 mL 0 / 5 mL 15 mL O / 5 mL 0 / 5 mL C,—) N Imp v /5 mL �•-� /5 mL 3 HOURS at 35 t 0.5°C• in INCUBATOR DATE IN INCUBATOR: jJ (, �/[� �� NCM I�� 1 �.7� NCUOATOR: 'lri -{1- 7EIePmATUnE OF �� �1 vicueAtOR � 7 : V DATE OUT INCUBATOR: �\ I I 1 INCUBATOfl: � I l_�/ — vsueA7ox 3� �V 21 t 2 HOURS at 44.5 t 0XQ in WATERBATH DATE IN WATERBATH: I I I ' THaEIN WATER9ATH: I wwr�newtn; . DATE OUT WATERBATH: —. _ �- ' TIME OUT 2 t� WATERSATH:wwnfin�rn reuPMAULEOF ji � 4 —I POSITIVE CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH DS A-1 BROTH :70,51 . E .� %TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) CALCULATION: MPN Fecal Goliforrri/ilram sludge 10 Vic. NeWN Index Largest volume r, % dry solids FORM UPDATED: APRIL 2007 f_•111ECKED BY:UV COPY MADE: 4 CAMP. I.EJ"-"JNE WWTP ATAD SLUDGE �-EQAL ANALYSIS DATE COLLECTED: ET,ME COLLECTED: p�0� COLLECTEIlT I; �': ^ Grl /mot ��il� RECEIVED BY:. 2 FATE: '�,. ��J-(�- =TWE-z(�T DATE ANALYZED: �• TIME: 0b7I0 " �A�eImALYtiRI:�.a�n_}__ _.....n METHOD: GJ1'wy 3 HOURS at 35 0.51C In INCUBATOR 2.1 x 2 HOURS at 44.5 t 0.2" C: in WATERBATH COMB. OF nnr aA/1Q� mrt0.: MI6T�W rGdfMIII n15mL SAMPLE LOCATION 10 mL 1 ML 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mlic- �, aPOSITIVE clewl DVP /5mL V /5mL ® / 5mL15mL/5— 3 HOURS at 35 0.5°C• in INCUBATOR DATE 1N INCUBATOR: �'7 • ��J • f DATE OUT INCUBATOR: "d-, to-), 21 -t 2 HOURS at 44.5 :t 0.2'C in WATERBATH DATE IN WATERBATH: 7 l I)l DATE OUT WATERBATH: G_ POS BLANK SS A-1 BROTH S DS A-1 BROTH FORM UPDATED: APRIL 2007 TIME IN INCU9ATOR: TIME OUT ' I INCU9ATOFI: rdro�AruneoF awenron: �'�i� TEYPOUTUnr OF i 0 TINE IN '1'''�''`�''7� WATERBATH: I �'� I tEvrFnATuneaF waivlmrn: 44. 5 RBATN: �� �.—�•^^•�/��l TIME OUT wA�rtrrntem � � � �' . CALCULATION: %TOTAL SOLIDS MPN Fecal Coliform/grAm s-ludge (ATAD SOLIDS ANALYSI S) . 10 xf19PN Inclex Largest volume x % dry solids GI-II-tCKI=D 8Y: v- COPY MADE: ,A,TAD SLUDGE i-ECAL. ANALYSIS DATE COLLECTED: � ITIME COLLECTED: COLLECTED I:BaI": RECEIVED BY:-r CL [DATE: IL DATE ANALYZED; jT—�----••------- METHOD: S at 35 0.5'C In INCUBATOR 21, 2 HOURS at 44.5 t 0.2"C In WATERBATH COltld®' OD �nl�ira�aa� mrop. I1NrT0VllG-nG3i�i�llB}` SAMPLE LOCATION _ 1 mL 0,10 mL 0,010 mL 10 mL " /5mL 1 mL 0.'10 mL 4],010 mL 1POSITIVES T1 1 'y r3HO.UL D/5mL v /5mL /5mL /5mL Q /5mL / 5 mL 0' u' 3 HOURS at 35 :t 0.5°C- in INCUBATOR DATE IN fNCUBATOR: �. �5 .I (� DATE OUT INCUBATOR: 9-a 21 :t 2 HOURS at 44.5 :t 0.2°C in WATERBATH DATE IN WATERBATH: LC DATE QUT WATERBATH: POSITIVE CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH OS ,^ ^l Pvw DS A-1 BROTH p v U FORM UPDATED: APRIL 2007 INCU IN I I / flATOR: ` L TIME OUT INCUBATOR: `"t1 TIME IN WATERBATH: I l TIME OUT WATERBATH: it,e�b1ATVAE VF %J _ WcueAT011: 7��y� TEU ERATOIIt OF 0=8ATVR T6iPF11ATunEOF LI.� WATEIIpgTIL• TEYPFAATUrtEOF i W47TTE4/iL• /`' ry�, % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Coliforrn/gram ,sludge = 10 x fv1PN Index L•srgesl volume x % dry solids 1 C H ECKED BY: COPY MADE: U1e CAM LF"PRINE WWTP ATA L ID G L FECAL ANALYST co�� DATE QOLLECTED: ��q� It( TIME COLLECTED: 6 Z z0 FIECEIIIED BY: DATE ANALYZED: TIME: C50, METHOD: COLLECTED BY: �/�c-�� FIN�AL 3 HOURS at 35 * 0.5"C In INCUBATOR 21 m 2 HOURS at 44.5.*0.2"C In WATERBATH COMB, OF MPIWIG1+0 mnlL ml."OJilGRAMB POSITIVES SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL .0.10 mL 0.010 mL \- �` L , l.� /5mL 0/5mL Q () ' o" /5mL /5ml_ /5mL /5mL 1�� /5mL /5mL ®Uh /5 mL 3 HOURS at 35 zi: 0.5°C• in INCUBATOR DATE IN INCUBATOR: L nNE w �aC � � ` INCUBATCfl: � vE' DATE OUT INCUBATOR: .y7 TIFAE OUT INCURATO NCUBR: 21 t 2 HOURS a9: 44.5 t 0.2'C in WATERBATH DATE IN 1ATERBATH: TIME IN WATERBATH: L7 lJ lJ DATE OUT WATERBATH: TIME WATERBRS ATH: (f PO§I—WE CONTROL. NEGATIVE CONTROL BLANK SS A-1 BROTH DS A-1 BROTH JL� l/ v FORM UPDA-rED: APRIL 2007 TFLPE11A1U,1L 6F ��-� ecueATaR Wf]19ATOR � 5 E.=:: NgCOF 074q. wnttrrnTro j 17 % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . . CALCULATION: MPIN Fecal Coliform/Ilram sludge . = __I O r. PvIPN Inclex Largess volurne x % dry solids CHECKED BY: COPY MADE: _ �� TP TAD SLUIDGL FECAL ANALYSI, DATE COLLECTED: 3 -/ 1 - 2� / L� FTIECOLLECTED:8.7 COLLECTi'ED BY: RECEIVED BY: (,�•r. DATE: (�. I TIIMIE• �S�C:10 DATE ANALYZED; rI1V1E: AI4IAIl.Y,nT: • �._......MF ......y- 3 HOURS. at 35 * 0.5"C In INCUBATOR 21 x 2 HOURS at 44.5 0.2" C: In WATERBATH SAMPLE LOCA-nON 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.•10 mL 0.010 mL COMB. OF POSITIVES IVIP11, 100 mIL IIIOVNIG RAI110 r V / 5mL 15 mL / 5mL V / 5 ml_ O / 5mL / 5mL / 5 mL O / 5mL 0 • p 0 .�-� / 5mL 3 HOURS at 35 :j: 0.5°C- in INCUBATOR DATE IN 6NCUBATOR: 3- l I , ? I I DATE OUT INCUBATOR:. 21 :t 2 HOURS all: 44.5 :t 0.2°C-In WATERBATH DATE IN WATERBATH: I II _ DATE OUT WATERBATH: i•1„�:�D(� POSITIVE CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH DS A-1 BROTH Y1 C Yt_e& U FORM UPDATED: APRIL 2007 TIwME IN i Irk cueATafl: l2l x ^� INIGlE18ATOfl: I ! /,/ TIME IN � rJ WATERBATH: i TIME OUT WATERBATH: � 1 d TEYPFAA7'Wul OF '/`/•O ucuOATOR TdPEAATUACOf -3 -'s ULl16Al'OR' rFaesanTuneaF //// r r TdPFAATUpl OF L,• l�• �✓ wwnrwm: LI� CALCULATION: � J % TOTAL SOLIDS MION Fecal C(Aiforrn/4lram sludge — (ATAD SOLIDS ANALYSIS) 10 x NIPN Inclex Largest volume x % dry solids CHECKED BY: COPY MADE: i CAM P'LF-1 ATAD SLUIDGL FECAL ANALYSED DATE COLLECTED: l c / % TIME COLLECTED: r % _/ o COLLECTED BY: RECEIVED BY: � DATE: =TIME: ANALYZED: 'r• t J l TIME: ; I ENALYST- DATE 3 HOURS at 35 * 0.5'C In INCUBATOR 21 s 2 HOURS at 44.5 * 0.2"C In WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF POSITIVES I1 POW10+0 mL MPOWURAM9 f') /5mL V /5mL 0 /5mL /5ml_ - /5mL V /5mL U /5mL /5mL ®UP 3 HOURS at 35 a: 0.56C• in INCUBATOR (DATE IN INCUBATOR: I t✓ \ '• I � TIME IN 1� INCl10ATOfl: � v' l DATE OUT INCUBATOR: �. (�S' . �`� nMEovr f INC(IeATOfl: I 21 :t 2 HOURS at 44.5 s 0.2"C in WATERBATH DATE IN WATERBATH: �' & ( TIME IN r� _ - I � � WATEFlBATH; I DATE OUT WATERBATH: WATE(iOATH: I lJ POSITIVE CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH -D7 DS A-1 BROTH FORM UPDATED: APRIL 2007 TFLP61AlU/ll OF '�./ .� WGl0Al9R J l/ TAIPPAAT11ne Of 7:� �� VeLt19A7pR WATEAAATIt: 7 TELPEIIATUAE OF wAUrmTL• �•• % TOTAL SOLIDS (ATAD SOLIDS ANALYSVS) CALCULATION: MPN Fecal Coliform/gram sludge — 1 D r. NIPN Index i Largest vOlUrne x % dry solids CHICCKED BY: COPY MADE' DATE COLLECTED: —2 �- Zv/ �f TIME COLLECTED: p ? �,� COLILI=C111CIt�i I31Ir: I� _. RECEIVED E7��`� � ®ATE ANIALYZED: '?j.2-5, 7l FATE- TIME: Q 2 METHOD: TIME: 05 co_____.� FIYA1L''P$T:: 3 HOURS at 35 t 0.5-C In INCUBATOR .21 t 2 HOURS at 44.5 t 0.2'C In WATERBATH SAMPLE LOCATION — 10 mL 1 mL 0.10 mL 0.010 n1L 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF POSMVE o MPIh9/100 a1nIL IU9r"OWGRAI'd Dup. _" /5mL `-+ /5mL 0 /5mL 0 /5mL /5mL 0' /5mL O /5mL l. 0 /5mL v /5mL 0 /5mL 0.0.. 3 HOURS at 35; tt 0.5°C- hii ONCU.UBATOR DATE IN INCUBATOR: DATE OUT INCUBATOR: 21 s 2 HOURS at 44.5 i 0.2"C in WATERIC ATH [DXU�E Ifd VVa1TIERF3,Al"N: '� t �i. DATE OUT WATEFIIBATN: k'IOSIIIVE CONTROL NEGAME CONTROL BLANK SSA-1 BIFiOTI-I DS A-1 MOTH o� Vim' FORM UPDATED: APAIL 2007 TIME IN OG' � INGN9ATOR: TIME OUT iy INcuaaTOR: (�' j TIME IN WATERBATN: TIME OUT (I l U WATERBATN: IT-1---., ~' u1CLUAT011: � 5+�/ TFLPt]L1TUl�l OF �///s7 U iHWOAIOR TEvtEnANAG OF J 44- wAT TR: TOlPFAATUMOF watt : rtATI Z % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Cc:,lifarrn/grarn sludge = _ 10 x MPN Index Largest VOILime x % dry solids CHECKED BA — COPY MADE: iqs_ Camp Lejeune, IIC 2014 ATAD Performance Data Date AT AD Train 1 A �, Train 1 B Coliform Feed (Gallon) Temp (oC) Temp (CC) Fecal (!1flPN) 1/ 1/2014� I I I l 1 /212014 1 /3/2014 1/4/2014 -1 /5/2014 1 I6/20141 120,000 1 /7/2014 .19.8 20.3 1.0 1 /8/2014 19.6 20.8 1 /9/2014 20.2 22.0 1 /10/2014 22.3 24.4 1 /11 /2014 25.3 27.9 1 /12/2014 27.2 30.7 1 /13/2014 28.5 33.4 1 /14/2014 30.3 37.4 1.0 1 /15/2014 32.2 41.7 1 /16/2014 35.0 46.1 1/17/2014 38.3 51.2 1/18120 14 42.7 U4. 1 1 /19/2014 18,000 42.2 56.7 1 /20/2014 18,000 41.8 56.0 1 /21 /2014 18,000 43.2 55.9 1 /22/2014 50.8 57.1 1.0 1 /23/2014 58.9 57.4 1 /24/2014 18,000 56.5 57.1 1/25/2014 59.6 56.7 1 /26/2014 60.0 55.2 1 /27/2014 58.8 54.1 1 /28/2014 57.2 52.3 1 /29/2014 55.6 49.8. 1/30/2014 52.8 47.4 1 /31 /2014 50.3 TOTAL = 192,000 1,029 1,066 3 Ave = 38,400 41 44 1 Max = 120,000 60 57 1 Min = 18,000 20 20 1 Camp Lejeune, NC 2014 A T AD Performance Data Date ATAD Train 3 A Train 3 B Coliform Feed (Gallons) Temp (oC) I Temp (oC) I Fecal (m"PI") 1 /1 /2014 57.5 52.7 1 /2/2014I 18,000 1 54.5 51.5 113120141 1 52.9 49.5 1 /4/20'l41 51.0 j 48.1 ( I 1 /5/2014 49.4 i 45.7 1 /6/2014 48.0 44.8 1 /7/2014 46.2 43.2 1.0 , 1 /812014 43.8 41.7 1 /9/2014 41.7 40.5 1/10/2014 1/11/2014 1/12/2014 1/13/2014 63,000 21.5 1/14/2014 23.7 1.0 1/15/2014 27.1 1/16/2014 63,000 26.1 25.3. 1/17/2014 27.0 30.4 1/18/2014 30.7 35.2 1 /19/2014 35.1 44.1 1 /20/2014 42.3 53.3 1/21/2014 -52.6 62.9 1 /22/2014 18,000 58.7 65.3 1.0 1/23/2014 18,000 60.5 65.3 1/2-At /2014 0 65.4 63.6 1/25/2014 18,000 62.4 61.5 1/26/2014 18,000 60.6 60.7 1/27/2014 18,000 59.3 60.0 1/28/2014 18,000 61.2 59.5 1/29/2014 18,000 59.9 59.1 1/30/2014 18,000 59.0 58.5 1/31/2014 18,000 59.2 58.8 TOTAL = 306,000 1,337 1,281 3 Ave = 23,538 48 51 1 Max = 63,000 65 65 1 Min = 0 21 25 1 Camp Lejeun �e, NC 2014 ATAD Performance Data . Date ATAD Train 1 A Train 1 B ColifonYi Feed' I Gallons) Temp (oC) ► emp (oC) I Fecal (MPN) 2/1 /2014 48.4 44.6 ' 2/2/2014 41.3 43.6 F 2/3/2014 46.5 42.9 2/4/2014 44.8 41.9 1.0. 2/5/2014 43.1 40.9 2/6/2014 2/7/2014 2/8/2014 2/9/2014 2/10/2014 2/11/2014 2/12/2014 2/13/2014 2/'14/2014 2/15/2014 2/16/2014 2/17/2014 2/18/2014 2/19/2014 2/20/2014 2/21/2014 2/22/2014 2/23/2014 . 2/24/2014 2/25/2014 2/26/2014 2/27/2014 2/28/2014 TOTAL = 0 .230 214 1 Ave = #DIV/01 46 43 1 Max = 0 48 45 1 Min = 0 43 41 1 Camp Lejeune, IBC 2014 ATAD Perormance Daia Date ATAD Train 3 A i Train 3 B I Coliform Feed (Gallons) Temp (oC) Temp (oC) Fecal 2/1/2014 18,000 58.5 59.2 2/2/2014 18,000, 58.6 59.4 2/3/2014 59.8 60A 2/4/201 A ^18,000 i 8,000 60. 1 50.4 1.0 2/5/2014 18,000 60.0 60.5 2/6/2014 18,000 57.8 61.0 2/7/2014 18,000 60.7 61.5 2/8/2014 18,000 61.7 61.5 2/9/2014 18,000 62.7 61.8 2/10/2014 18,000 62.5 62.8 2/11/2014 18,000 61.4 62.5 1.0 2/12/2014 18,000 61.0 62.2 2/13/2014 18,000 61.0 62.3 2/14/2014 18,000 60.1 62.4 2/15/2014 18,000 60.8 62.7 2/16/2014 18,000 62.5 63.1 2/17/2014 18,000 62.5 62.8 2/18/2014 18,000 62.9 63.4 4.0 2/19/2014 18,000 63.2 63.5 2/20/2014 18,000 63.4 63.7 2/21/2014 18,000 62.0 63.4 2/22/2014 18,000 61.9 63.1 2/23/2014 18,000 62.2 62.5 2/24/2014 18, 000 .62.0 62.6 2/25/2014 18,000 61.4 62.4 11.0 2/26/2014 18,000 60.2 61.5 . 2/27/2014 18,000 60.3 61.2 2/28/2014 18,000 60.6 60.8 TOTAL = 504,000 1,712 1,734 7 Ave = 18;000 61 62 2 Max = 18,000 63 64 4 Min = 18,060 58 59 1 Camp Lejeune, NC 2014 ATAD Perormance Data I Date ATAD Train 2 A Train 2 B Coliform Feed (Gallons) - I Temp (oC) 1 Temp ` (oC) 1 Fecal (,m,Piq) 3/1 /2014! 3/2/2014 3/3/2014 60,G00 17.4 3/4/2014I ( 21.1 j j 1.0 3/5/2014 24.0 I 3/6/2014 28.1 3/7/2014 33.7 3/8/2014 39.6 3/9/2014 46.7 , 3/10/2014 54.0 3/11 /2014 58.6 1.0 3/12/2014 60,000 40.6 41.1 3/13/2014 37.4 56.6 3/14/2014 43.7 58.7 3/15/2014 53.2 58.4 3/16/2014 62.9 58.6 3/17/2014 63.9 56.8 3/18/2014 61.5 55.1 1.0 3/19/2014 59.1 53.4 3/20/2014 56.5 51.7 3/21 /2014 53.9 50.1 3/22/2014 51.6 48.5 3/23/2014 49.9 47.3 3/24/2014 48.1 45.8 3/25/2014 46.6 44.2 1.0 3/26/2014 45.1 42.7 3/27/2014 43.3 41.3 3/28/2014 42.2 40.6 3/29/2014 41.4 40.2 3/30/2014 40.3 39.3 3/31/2014 TOTAL = 120,000 1,264 930 4 Ave = 60,000 45.1 49 1 Flax = 60,000 63.9 59 1 Min = 60,000 17.4 39 1 Camp Lejeune, NC 2014 AT AD Perormance Data Date ATAD Train 3 A Train 3 B Coliform Feed (Gallons) Temp (oC) , Temp (oC) Fecal 3/ i/20i41 18,000 1 59.9 61.2 3/2/2014 18,000 59.7 G 1.6 3/3/2014 18,000 60.4 61.9 3/4/20141 18,000 j 58.7 61.5 1.0 i 3/5/2014 18,000 59.2 61.8 3/6/2014 18,000 59.8 62.5 3/7/2014 18,000 ' 59.2 63.1 3/8/2014 18,000 61.0 64.0 3/9/2014 18,000 60.8 66.2 3/10/2014 9,000 66.6 65.7 3/11/2014 9,000 66.6 64.4 1.0 3/12/2014 9,000 67.5 62.9 3/13/2014 13,500 62.8 61.3 3/14/2014 13,500 63.9 60.5 3/15/2014 13,500 64.7 60.9 3/16/2014 13,500 65.2 61.3 3/17/2014 18,000 62.0 62.2 3/18/2014 18,000 60.6 62.9 1.0 3/19/2014 18,000 59.5 64.5 3/20/2014 18,000 58.6 66.1 3/21/2014 18,000 58.6 67.0 3/22/2014 18,000 59.3 67.2 3/23/2014 18,000 60.4 .67.5 3/24/2014 18,000 59.7 67.4 8/25/2014 18,000 60.1 66.7 1.0 3/26/2014 18,000 59.1 65.9 3/27/2014 18,000 58.9 65.6 3/28/2014 18,000 61.5 65.1 3/29/2014 18,000 59.2 65.3 3/30/2014 18,000 59.5 65.5 3/31/2014 18,000 57.5 65.5 TOTAL = 513,000 1,890 1,985 4 Ave = 16,548 61.0 64 1 Max = 18,000 67.5 67 1 Min = 9,000 57.5 61 1 CP LEJEUNE BENCH SCALE ATAD V ATILE SOLIDS RE UCTM ,ANA, • SIS DATE 2/7/2014 A B G D E F G H I SAMPLE SOLIDS ASH SOLIDS INHOUSE WT OF WEIGHT WT OF WEIGHT % TOTAL WT OF WEIGHT WEIGHT % VOLATILE % VOLATILE SAMPLE ATAD WT OF DISH DISH+WET (g) [B DISH+DRY (g) SOLIDS DISH+ASH (g) (g) SOLIDS WEEKLY SOLIDS TEMP DATE DIGESTION (g) SOLIDS (g) A] SOLIDS (g) [D-A] ' [(E/C)X100] (g) [G-A] [E-H] [(I/E)X700] AVERAGE REDUCTION 0°C r; 2/10/2014 I.H. ATAD 74.0518 79.07 5.02 74.1246 0.0728 1.45 74.0855 0.0337 0.0391 53_71 53.21 20 DUP 87.8141 92.82 5.01 87.8860 0.07'19 1.44 87.8481 0.034 0.0379 52.71 ,.., 't a :�,.> ,. ,,..:...._.,,<k.ra.. '. Kim sY , p "'2i'3asw'r, .,H . t cM k .. x, e.. <,. . •»..- „'� a z •.. ..... ... ....ti ... .. .. ,. .,, ...x> E. ,.. z..•,. .;,., r, .,Yi r.s < ..._. _. ,_., ,x.e x, .. ,. .a••. #.r. -i. S r,a .+ ., .,:a`X .x .� <r >„n ..x, <x •,.i,. � > V„y0.0723wX'N Y�,M 4+vt ^ ;- fY Y r„ < ?' x`�rw;0.0337 _ a, ^0.0386`x 2/14/2014 I.H. ATAD 84.2163 89.23 5.01 84.2886 1.44 84.2500 53.�39 53.95 95 -1.39 20 f DUP 86.4453 91.45 5.00 86.5196 0.0743 1.48 86.4791 0.0338 0.0405 54.�1 „ ...,, .„ ....,..., a a . , {a� �.. 11 v.. .. .. .. .. .. ... .. r. < .. < .. <. , ..... , .w•.. e .1r „ ..x, .,;• ...,,<..,., , •e >y a .`ai' 'Pi. { , ,.. .>, .. ... rx.. ,,, L .. x x :?' n,, i," .. .a .,, 3 .<., } d .., x,x_ ..4 �< �,.r#„,,;,.x : ;q..• b - w. <� �E,. r«.,.,r ,.%v x a € ., .. , . .. ... _ ,. .. •< , s s .,,<,, st .:< a,.<„.,,,-. .rr... '�',y.< „Tx, .<.. tr.. 2/21 /2014 I.H. 'ATAD ' 85.1032 90.10 5.00 85.1633 0.0601 1.20 85.1309 0.027 7 . 0.0324 53. 2 0.99 20 DUP 91.8007 96.81 5.01 91.8606 0.0599 1.20 01.8289 0.0282 0.0317 52.92 .fi.,,.:ra ,','•P�� . „r .. .. ,. s .> ..<.,, ... < � . , n . ., ., e ':y ._ z , .. .< , �; :,+:✓><,,.e=.r' f5 <,_ r,.-x2i.Lx• fxxix Y.<i, . �>, '`a�a Wa-:>�;a.,._e':;6' x< }} `;'}r, '. s ai ri. <tti�Y x✓Yis'�i 2/28/2014 I.H. ATAD 85.103 90.10 5.00 85.1578 0.0548 1.10 85.1285 0.0255 0.0293 53_47 F53A4 0.53 1 20 DUP 71.9172 76. 433 0.0261 0.0292 52.80 .�3 .. ......._ _ .._ .,•... .,. _„ ...... _ ..... .. .<.. ..r:..t yKi ., .. .. v sF .<...... x .<. � , w .„ x. �. .. - 4�, ss,,, Sr �< � % ... -.. .. .. .t , ,,.. ,. . r ,<nax . r r ✓ W ,. .<.a .>.. ..,�r-»4, ,, ,, .x-a <,.r ,#{„ S..t✓ .. , ♦. '� �, T. r ✓ sre_ r, ,>xo- Y.'E'.. .t�, 3/7/2014 I.H. ATAD 75.4557 80.46 5.00 75.5165 0.0608 1.21 75.4843 0.0286 0.0322 52.96 52.83 0.57 20 DUP 75.2258 80.23 5.00 75.2869 0.06'11 1.22 75.2547 0.0289 0.0322 52.70 :. t' t . ,... , ., ,.. < .... .. .. .. ,..< x .., hb,. .,:, ,sin. . >, -i, yi, ;. :e ..,.: .. , ,rs 3<.. x, •4c 3 r,x h> m , �3 T �. K r� '.3.'.. t ,. 'N a i:ui:,n-.,.3"•��S"d: ., ... .e. ., ,. x. >F ......r,•. =n,. , . h x„ .,'u. .,i ., ., � , � .... Y his , €w• .. ., - v.:. ,.:.:.:,., 3/13/2014 I.H. ATAD 75.2260 80.23 5.00 75.2753 0.0493 0.99 75.2491 0.0231 0.0262 53.14 52.39 0.84 20 DUP 87.8149 92.81 5.00 87.8639 0.04.9 0.98 87.8386 0.0237 0.0253 51.6 a.r. � €-: •tr: , .a < ,. , . .x t <R .-,.. .. ,x ,x.:.< ,.a [^ < r:•�: xr;•,x < . ., . . r,. .., . .. .. ,,... .< 1. .£, .. . xP .., > a Yii E., ,. ✓ d _ 3a E_ .:«s i�' ry at , VOLATILE SOLIDS REDUCTION = INITIAL VS - FINAL.VS X 100 INITIAL VS (VSR <15%) CAMP LE -ILINE WWIFP ATAD SLUDGE FECAL LY1'%Q DATE COLLECTED: N I ► 1 N TIME COLLECTED: 72 FEOLLE�TE� fig P: - /c,C RECEIVED BY: �, � , (� �EFJ ®ATI: ANALYZED: 4.1 .1 Ir, IME: oqg�5— M �TFIO®: 3 HOURS at 35 t 0.5'C In INCUBATOR .21 s 2 HOURS at 44.5 t 0.2'C ITT WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL` 0.•10 mL 0.010 mL COMB. OFM6�lhdll®� POSITIVES raalL Ili9E°IVI/ RAM G�DI 0 /5mL O /5mL 0 /5mL O /5mL O /5mL (9 /5mL /5mL C) /5mL0'0'©Dur-, ^ _ 0 /5mLl IS mL 3 HOURS at 35 :t 0-5'C• ftt INCUBATOR IRATE IN INCUBATOR: q-, l . l`T DATE OUT INCUBATOR: l +, l+ ((� 21 :t 2 HOURS at 44.5 -t 0.2'C in WATERBATH DA%"E IN WATERBATH: L� _ f DATE OUT WATERBATH: POSII1IVE CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH �s DS A-1 BROTH aS U U FORM UPDATED: APRIL 2007 TIME W DC�/� INGUBgTOfl: •h/ TIME OUT INGOBgTOfl• ` } TIME IN .•y ��., ''� WATEfl9ATH: (�v TIME OUT WATEflBATH: 0G�30 TW P61a111IfG OF o vtWEATOR: ,f V�-�_ TWPEILlTOIIL OF =_5 VGL6A1UIt T -- ' 4-4- T W—Avuarn, S ,_�f TWPFJI..OF 414 waTTTGCm . F;-!• % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS). CALCULATION: MPN Fecal Coliforrn/4lrarn sludge — _ 10 tt MPN Index Largest valu ne x % dry solids CI-IIECKED BY: �P COPY MADE: 1: e 4.9 ATAD SLUDGEFECAL ALY1,E- [®A:r E 1COLLEICTED: CIME COLLECTED: � Cl'? 1 c. OOLLEC�'IwICt"(I3;�P': :•:!. c.0 `^'ITV:_ I I�EOEI!!E® BY: FIATE: L�. . I TIME. Ot . ®ATE ANALYZED: TIME: 61lU ETI� O I7: _ 3 HOURS at 35 * 0.5'0 In INCUBATOR . 21 :t 2 HOURS at 44.5 t 0.Z'C In WATERBATH SAMPLE LOCATION 10 mL R 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.•10 mL 0.010 mL COMPS. OF POSITIVES M rPIWIUG grill RM PHI RAN 0 /5mL /5mL /5mL /5mL `' (`�% /5m (�jL /5mL /5mL G, /5mL{— �': up 0, /5mL 3 "OURS at 35 :k 0.5'C• Iall INCUBATOR FA=TEININCUBATOR: L�. _ �, DA"II'E OUT INCUHEaTOR: , - � r,_,J_ 21 t 2 HOURS at 4.4.5 t 0.2°C in WATERBATH DATE IN WATERBATH: /�. . I+ DA-E'E OUT WATERBATH: �l Vr° I�'OSI111VE CONTROL NEGATIVE CONTROL BLANK SS-A-1 BROTH DS A--1BROTH1 Lul�— U O FORM UPDATED: APRIL 2007 TIME IN [•II ,.7 INCUEATOR: INI CURATOR: TIME IN y i' WATERBATH: l i�%� TIME OUT WATERBATH: lJ TELPFSU1TIl1¢' OF • V6LeAT0? TENPE141T1�'OP �•� :� Vbl1VATOR TFLPFAATUHGOF � waTFMnTM: �^�• TELPFA �•!p� w4.AT11.M �/ % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Cedifurm/gram sludge _ 10 x NlPN Inclax Largest Volume x % dry solids £=" CHIECKED BY: �f 1i,l COPY NIADE:^lP I'. lk Fmit= COLLECTED: FRECEOVED BY: EKT:E::A:N�ALYMD: CAMP LE AINE WWIFP 1EI11E COLLECTED: 7� s [DATE: 4 CFINI IE: METHOD: COLLECTED BY: 14 C TIME 3 HOURS at 35 t 0.5"C In INCUBATOR 21 x 2 HOURS st 44.5 � 03'C In WATCRBATH SAMPLjLOCAj-n 10 enL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.'10 mL 0.010 mL COMB. OEMP11, /10Gou L fiff" IG RAAhl /5mL 0 /5mL 0 /5mL D /5mL n/ /5mL ®/5mL 0 /5mL /POSITIVEc 0 /5mL 010-0 111°`21 ^-� _.._ �- � _ 1• D� r!� V / 5mL 3 HOURS at 35 zt 0.5'C- in INCUBATOR DATE ON INCUBATOR: DATE OUT INCUBATOR:� 21 :t 2 HOURS at 44.5 :1: 0.2°C 8n WATERBATH DAT=1N WATERBATH: E I"E OUT WATERBATI* . I6`,�(� 1=I5SI11VE CONTROL NEGAnVE CONTROL BLANK SS AO-1 BROTH �0 DS A-1 BROTH OC v u FORM UPDATED: APRIL 2007 TIME IN ,�"(� INCUBATOR: 0 �..i TIME OUT I •"J INCUBATOR: TIMEIN _ WATERBATH: TIME OUT WATERBATH: TEVPEAATUhC OF (�{{ � �^ TEUPEN 1TUrtGOF �L VAa19AiD1G �` TFJdPEMTUHL OF / WATERWH: ��, TELPFAAM OFWATErrA T f % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Coliforrn/gram sludge = _ 10 x MPN Index Largest volurne x % dly solids CHECKED BY: COPY MADE: la C"'AMP IL a61" ' I E W,IF P ATAD SLUDGE I-ECAL ANALYSMS P-yrE C�DLLECTEIO: Y Z Z r'11111E COLLECTED: (�7ZS COLLECTE�1�7, U3�Y: I� ��� REQ:E01/1CD BY: [IATE: =E.�" 7 ®ATE ANALYZED:� �h-, i IT'IWIE: Q� V�� METHOD: 3 HOURS at 35 zt 0.5"C In INCUBATOR .21 :m 2 HOURS at 44.5 * 0.2"C In WATERBATN _ SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OIL MI'lld/IGI� full NII°IVV �RASu9'' POSITIVEko C_ �1 �/ /SmL O /5mL V /5mL G/5mL / f v r✓ /5mL I /5mL O /5mL /5mL 0 "0 ®U P V / 5mL � 3 HOURS at 35 a: 0.5'C• in INCUBATOR DATE IN (NCUBATOR: DATE OUT INCUBATOR: ��• L� 21 :t 2 HOURS at ".5 :t U'.2°C lug WATERBATI-I 1. DATIE IN WATERBATN: � _• 1 S TE OUT WATERBAT1-I: POSI-11VE CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH Y DS A-1 BROTH us � y,szr FORM UPDATED. APRIL 2007 TIME IN { INCUBATOR: 06 1 TIME OUT INCUBATOR: GPI TIME IN WATERBATN: TIME OUT�'- WATERBATH: r r5 uweArom _ lJ TIMPF Im or � �� u¢venrols Tme�nAnlnaoF / waTale4Tn: F�—� ;'� T.11ATUI.OF '- wnnrMM % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Coliforrn/4lrarn sludge _ 10 x MPN lncict Largest volt.u-ne x % dry solids CHECKED BY:'_J COPY MADE: 1 .: dl 1'Y IL . ^ ' .1 E W lV Wm P ATAD SLUDGE FECAL ANJ%LYS1'%Q3' ®ATIE CQ➢L-ECTEID: ITIME COLLECTED:07/p �COLIL.ECTEIf�` BY: RECEWEDD BY: Fo,ATE: -�.. � `� � - TIME:: DATE ANALYZED: � 2 �� � '-- . FTIM' E: (�`Z�EN::ALYST:_..�"1�?� __._...� 6UV rT0-DOI�: 3 HOURS at 35 :t 0.5"C In INCUBATOR, .2 1 m 2 HOURS at 44.5 :t 0.2'C: In WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. O6� POSMVES:o IUl6TIId/141�b mralL 11106�OIN �ffBJakV9 /5mL /5mL 0/5mL /5mL �"� /5mL /5mL C�/5mL /5mL Dup 11 /5mL /5mL 3 HOURS a8 35 2i: 0.5°C- irn INCUBATOR (DATE IN INCUBATOR: DATE OUT INCUBATOR: 21 :t 2 HOURS at 44.5 :t 0.2°C to WATERBATH t DATE IN WATERBATH. DATE OUT WATERBATH:��J (` POSIIIVE CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH (N� DS A-1 BROTH FORM UPDATED: APRIL 2007 TIME IN %�Ct � Ufl' INCATOfl; V Lz INCUHATOfl: l mil-' L1i.i TIME IN t.�y WATEFISATN: TIME DUr y 2.` WATEflBATN: L J �' S C•• uwoArom WLVMroR +..a IT... WATE I TJJ: TEIJPMFJ1ATIlfdE l WATTrtATlii 1% TOTAL SOLIDS (ATAID SOLIDS ANALYSIS) CALCULP,TI ON: MPN Fecal Cc:difrarrn/4lram sludge _ 10 x N1PN Index Largest volurae x % dry solids r.l,lJl. 01-IIECKED BY: jtAi-- rCOPY MADE: (_ ATAD SLUDGE FECAL AN, LY S I "'ED DATE GOLLECTED: (v ! r ( TIME COLLECTED: 07 Z �' FLOLLEfE-I'DCI:;'P: 1 j (�r_l7� RECEWED BY: ��'t��'� [DATE:�. C<% � �� �`I(MIE: D ATE ANALYZED: rj`, C;, . j �- CluulE: J C� �� :% :N:A6...'J T METHOD: 3 HOURS at 35 zh 0.5`C In INCUBATOR .21 m 2 HOURS at 44.5 * 0.2'C: In WATERSATH SAWPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 'I mL 0.10 mL 0.010 mL COMB. OF POSITIVES IVIP11-411010 oink. _ Illll° WGRlh.M 7 % ;� l i 1�o /'M IS mL 15 mL / 5 mL / 5 mL / 5 mL (r�J v / 5 mL 0 / 5 mL /��.) V / 5 mL DU(rr} 3 HOURS at 35 :t 0.5'G Wi ItNC:UBA'1"COR DATE IN INCUBATOR: DATE OUT INCUBATOR: 21 dt 2 HOURS at 44.5 :t 0.2°rC un WATERBATH DATE IN WATERBATH: _j_(0 , I DA'O"E OUT VVATERBATH: L -7 ��- `4 TIME IN INCUOATOFI: G TIME OUT _ _ INCUOATOR: � ,�� TINE IN WATE110A714: FTINE OUT 1 L l V WATEROATN: 9:I0SI11VE CONTROL NEGATIVE CONTROL BLANK SS AA BROTH -D5_�- D)S A-1 BROTH T6LFEAnT -' U:cutlATT1R (' C, 5 „ . T-I r,v ' , ) U6JJIfATOR ! TEUPE TURL VF rwrFnnTurtEOF ��� wnttrwTw % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Coliform/grarn sludge = _ 10(NjPN IncLex Largest uolurne x % dry solids CHECKED BY: ---f FORM UPDATED: APRIL 2007 C()PY MADE: _ DATE COLLECTED: DATE ANALYZED: �� . i � • 1�' C"AMP LEJ ".)NE WWTP ATAD SLUDGEFECAL ANALMS S [T- INIE COLLECTED: C7 ZS [)A )ATE: TIME: METHOD: COLLEc-rEID,, R o'Y: P 3 HOURS at 35 zE 0.5"C. In INCUBATOR ..21 :t 2 HOURS at 44.5 :k 0.2"C; In VVATr=RBATH SAMPLE LOCATION 10 bnL ^0 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF n A1011-alloG Hnk. �lNS'tOJIfG�1L��dll9 /5mL O /5mL 0 /5mL /5mL /5mL 0 /5mL /j� 's1' /5mL C\y /5mL1•f t�POaMVE 3 HOURS a4 35 ± 0.500 in INCUBATOR DATE IN INCUBATOR: -- [DATE OUT INCUBATOR: 21 -t 2 HOURS at 44.5 :rc C1.2'C 1E B H [EA71=1NWATERBATH: DATE OUT 11VATERBATH: 1.10SI UVE CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH o _ 066 DS A-1 BROTH % jjj f/fi 1-1-1 14 FORM UPDATED: APRIL 2007 INCUflgTOR• i TIME OUT + 1 2-el 1 TIME IN WATERBATH: TIME i WATERB0ATERBATH: . TE7I1ET--- - TEltPOUTUt2OF j'`, ^; �� UtW9ATOR �/ V TODPEMTUhE OF � � WATEIIIlCM:� i TEYPFAATUItEOF ! 4lIL % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Ccslifcorrgl/41r-arir sludge _ 10 r NIFIN Index Largest velurne x % r11y solids CI-IIECKI=D BY: COPY MADE:p°'� '�\ GmMr LLt,-,,F=LemAE 4W m P MAD SLUDGL.,,0ECAL ANALYSES D.,'kTIE COLLECTED: E :� ��•I °/ EM:ECOLLECTED: �J7 � r-.• F—LLCC:�'I�D BY: LRV CEVVIED BY: -�:�'_ D09TIr: =MF-- EW,=1EAHALYZED. 2 =TIME-_��� ANALYST, 3 HOURS at 35 .-,: 0.5-C In INCUBATOR - _ .21 w 2 HOURS at 44.5 & 0.2" C; In WATERBATH SAMPLE LOCH;YION _ J 6)u 10 mL 0 / 5 mL 1 mL 15 mL 0.10 mL JJJ''' 0/ 5 mL 0.010 mL r \J �✓ / 5 mL 10 mL D / 5 mL 1 mL �/ 5 mL 0.10 mL / 5 mL 0.010 mL `� / 5 mL COM®. OE MP9,Y1(1G mnL 'MPIW068M POSITIVE_ j 1-30U 'S a4 35 j_ 0.5" C' hii IR9CUBATOR IIDAYE IN INCUBATOR: EID,ATE OUT INCUBATOR: 21 :t 2 HOURS all: 44-6 z Q1.2'C h WATERBATIH IDA u E 11�1 VN,4TEhlBATH: DNFE OUT WATEMATo-1 Y� ` POSIIIVE CONTROL NEGATIVE CONTROL BLANK SS A- J BROTH I �JL�`� I `}� v Yv� DG.A-1 BROTH --E] TINE IN� INCUflA70A• IJ TINE OUT `•� INCUOATOft• ! TINE IN WATEABATH: TIME OU7 + O �sra� WATER9ATH: l ��/ TEY wwUATUMenrolr.rtCOF 1 EUPmAiur2 of u¢al mm TF]1PEM7Lfl£OFl wommnm: 7flfPFAANIIE OF � L l� wattrrAix i � % TOTAL SOLIDS (ATAD SOLIDIS ANALYSIS) . CALCULATION: MPN Fecal Ccdiforrn/gram sludge = _ 10 x NIPN Inclex Largest VOlUrne x % dry solids CI-IIECKED BY: FORM UPDATED: APAIL 2007 � COPY MADE: .� ) CAMPLE-11ELINE WWTP MAVCE COLLEtGIFE10�_ 5-.2 8 • / 5/ TI�11� COLLlEC7ECD: p��s ®LLE�TfEII? 1�`r"�J��(.cv5?`�? Uhl= �GIEO�VV�6� V��f': DATE: "�1fIE AVVALIf IE:Ia: _ _?.�;.-��G. TIME: Dot 9sE...... °s�:.- 3 HOURS at 35 z 0.5°C In INCUBATOR .21 x 2 HOURS at 44.5 t 0.2'C In WATERBATH vNlloNVGRAM SAMPLE LOCA>;1fION ��U� 10 vnl- / 5 rnL �•� /5mL 1 mL / 5 mL 0.10 mL / 5 mL 0,010 mL / 5 ml_ 10 mt- 15 mL �l5mL 1 mL / 5 mL 0.10 mL J / 5 mL 0.010 mL COMB. OF Mp1W10-0 o1nL POSITIVES DAME IN INCUIBAYOR: ID'XCE OUT INCUBAT0N: 21 :t 2 HOURS at44.5 _ 0.2'G fin UWATERSATIH IDTr IE IN WATEFIBM'H c ,7 'y 2`-- 1Lf IDNVE OUT IATERBATI-1: INCNflATOR: ��'3 � V IfME OUT .,CueATOR: POS111VE CONTROL NEGATIVE CONTROL BLANK SS A-1 MOTH DS IA-1 BROTH ��L)5 FORM UPDATED: APRIL 2007 TIME IN WA7ERRA7N; � I ?� TIME OUT F WATERBA7N:��� u�G11EAT0R. S V idPma7ugG OF TFLfFAANMEOF `— WAiE31n.1TH: L I qTEMPFMATUng „. J WwTrrWTlt• :�� % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Ccdiform/p am sludge / _ 10 x NIPN Inclex Largest Volurne x % dry solids CHECKED BY: (;OPY MADE: � � CAMP LE, -I U114 E W W I P DATE �C:OLLIEC"GED TIMECOLLECTED: 0'� 30 �'iDLLEllti' 9�aP'�� RE'C 11VED BY: `��r� ; DATE: .2, . IL{- WATE ANALYZED:— (�; . � . 'dam_ TIIUIE�� SAMPLE LOCATION D Ul II,J I 3 HOURS at 35 :E: 0.5' C In INCUBATOR .21 x 2 1-10URS at 44.5 :k 0.2'C; In WATERBATH _-1!0 6nL ^ 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.'10 mL 0.010 mL C /5rrIL V /5mL /5mL 0 /5mL `✓ /5mL `-' /5mL v /5mL (D /5mL �J /5mL IDA Y E IN INCUBATOR: II X(E OUT INCUBATOR:_ 2-I :1- 2 HOURS at: 4JU15 'i 0.2°C in vViVrER BATH EDIV.-E IN WATIERBATI-1: DAYE OIUT WATERI3ATI-I: POS111VE CONTROL NEGATIVE CONTROL BANK _ SS A-1 BROTH DS A-1 BROTH FORM UPDATED: APRIL 2007 INCl1ElATOfl: l.��J J� TIM17E oY� I l � � ING49ATOp: TIME IN � WATENBATH: n a WATERBC7C; i fl7 ATN: wcuenroRrmpoukTu U=uAyuf. F ?� V+LueA7UR mI°`EiuNnG OF r � 1_ WaiF]16aTM: 1 . TeurFanturtEOF -1 L:r. Wartream: .✓ sl % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS). COMB. OF M6'lld/1m®mroIL�NIf°IdUQn68d!�4llI POSITIVES CALCULATION: MPN Fecal Coliform/4lram sludge NIPN Inclex Largest VOILIMe x W. dry solids X CI-IIECKL=D BY:. COPY MADE: ,) ,AMP LE,, ---.LINE VVT DATE COLLECTED,-����1 + I �(� TIMECOLLECTED:�, ®LLCCti_EICB„I�`P�^_^c-�'!!, �:r ^`t�+_►m�> _ ._ _ .,M.. �9 CDED v: �FgEDATE: a _0 DATE ANALYZED: _ ('. � b , l �f V _ TIME: I ! D FIo44JALY-13 i_ 3 HOURS at 35 ze 0.5'C In INCUBATOR 21 � 2 HOURS at 44.5 a. 0.2'C; In W,ATERBATH �M SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.'10 mL 0.010 mL COMB. Of MP'IQ1100 Um L POW GRAM POSITIVES 1 ;^I�,I�I�1% .Jva Y\II _ / 5 mL} / 5 mL�/ 5 mL �' / 5 mL �-% / 5 mL / 5 mL / 5 mL / 5 mL CJ / 5 mL 3 HOURS at 35 j- 0.5'C.6eu INCUBATOR E E IN INCUBATOR: i _ y LP i DATE OUTINCUBATOR: 1/ [DATE 21 � 2 HOURSat 44.5:t 0.2'C in IdWRATEI•I RbAT IN WATERBATH: � � t A: =DATEOUT WdATERIBATH: POSITIVE NEGATIVE CONTROL CONTROL BLANK SS DS A-1 BROTHU:r -- � 1" FORM UPDATED: APRIL 2007 TIPJE IN I j �� INCUBATOfl: 1 TIME OUT (F / INCUBATOfl: ,�E �(�� TIME IN WATEflBATH; �'�L� TIME OUT l 3 �U WME UT7H: TEYPFA '-- J S • 0 w=OATVM .•'J1 T61PF]wTUI1C OI' �� V6LOATOR T6�PEAAT4FlG OF '�_ WATEACnTH: )l J� WATT AATVPi£ OF d-lam (f —' wanrrnnu I%TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) CALCULATION: MPN Fecal Colif,lrrvi/gram sludge - _.10 x MPN Index Larges-i volume x % dry solids CHIECKED BY: COPY MADE: � I L -" =. LEI E lVVVV_TP ATA LU D L roCAS® AEI A LY MS, DATE GO,OILLECu ED: �.:��. �.� / �( TIME COLLECTED: C IE D BY: ,� 1 �� f..�-••7.�-I f' RE'CEWED BY: DATE: [t]IATE ;�AMAL.V ✓IED: ��1� _ �,: 1ru .. ��- TIDE: [1I E: ( 7 23 S_ lKNKy:i_s_:-_p es _-.R 3 HOURS at 35 r 0.5"C In INCUBATOR .21 :t 2 HOURS at 44.5 t 0.2"C In WATI=RBATH SAMPLE LOCA'!- 011 L`10 mL }} (✓/SmL /5mL 1 mL ice+ �'/5mL 0.10 mL /5mL 0.010 mL /5ml_ 10 mL /5mL ! /5mL 1 mL 0/5mL 0.10 mL /5mL 0.010 mL II V'/5mL COMB. OF MPIN/1010 onlL Nq PuvVGRAAdv9 PO�59T VE n _ �21—~ jj3 HQU. FBS at 35 a: 0.5`0 hii IaWQ l SATOR IDAYIEINONCUB1ATOR: _ ��.^� � � 1� DADXH't OUT INCtJfdl,G'rb6'i:__ 1 3_2 I;14sURS at 44.5 i- 0.2' ,` In WATERB ATH DAME IN VI/AYEABATH: S L:, . ++ �J ll E OUT 11VATEnB1l•,TH: —�— -- - I:I0SI97VE CONTROL NEGATIVE CONTROL BLANK SSA-1 BROTH 7 r 1 �(b , DS .,A-1 BROTH FORM UPDATED: APRIL 2007 TINE IN /,e��`M INCUAA7Nfl: V �Y.�� TIME OUT � j ,� INCUBATNfl: Il TIME IN 1 ! .� WATEABATN: TIME NUT fj 11 WATEABATN: TELPFA0.TV11COF /� ./"� TEl1POL1TUP:l OF �If'. �� u:weATox ./' rEveEnwiu F[oF � '� wnreannnr. .� ;� TE/1- AnIfPE OF wnnrwTw % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Conform/41r'am sludge — _ 10 x NIPN Index Largest VOILIMe x % dry solids CHIECKED BY: COPY MADE: A�I11�AD SLUDGE DECAL NLYS H.3' DATE COLLECTED:S` �i ] TIME COLLECTED: U9 a 2 EKLECTE10 BY: � En. �G IEU@7L-D BY:_�_ IG•,��a IDATE:/r`_ ?� .. I TlIIl191r E7 !%' C'�� DATE ANALYZED: �[ �� - I TIME: � ANALYST. 6VD E- TH 0LU: — -- _ 3 HOURS at 35 d: 0.5'0 In INCUBATOR .21 s 2 HOURS at 44.5 * 0.21 C In WATLRBATH SAMPLE LOCATION 10, uvtL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF � MIP6-U100 mralL �NOPOVI/ RAAM • POSITIVES b! /5mL pp� 0 t r�/ / 0/5mL L) L� meµ` --_� /5mL /5mL /5mL `-'' /5mL `-' /5mL /5mL DILpP 3 HOURS at 35 1: hii INu:;UB AT OR ID:�CIE ON UNCUIBA><TOR: - OZA4'li E OUT INCUBATOR: & � �� � ILk 21 :t 2 C,9OU FBS Ed. -tPLG 0- 2'°C on @1WATERB ATH FDA`j OiV VNA4TIEFIBI�TI�i - -- (,, y FD(V' •IE OUT WATE11SATOI INC08A70R: (� TIME OUT �••yp, i INCu6ATOfl: V'�C TIME IN ..��qq ' nME our I I WATERBATH: —�—�— POSIME CONTROL NEGATIVE CONTROL BLANK SS ,AA (BROTH IDS :a-1 BROTH �- i, - U (.y TELPOIAT __ W aATOR rv�rETurwn ear J '�'+) V+LLeAT°R 5 ..�/ TFJ1PErNTUPE pF �'� warennnrn: - 4- _5 TOIPFAATUIIE °F % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS). CALCUI.J4TION: MPN Fecal CUliform/flram sludge = 10 x MPN Inclex Largest volurne x % dry solids CI-IIECKED BY: FORM UPDATED: APAIL 2007 � l COPY MADE: Camp Lejeune, NC 2014 ATAD Performance Data Date AT AD Train i A Train 1 S Coliform, Feed (Gallons) Temp (oC) Temp (oC) Fecal (N4PN) 4/1 /2014 i 4/2/2014 63,000 18.7 I 4/3/2014 22.9 4/4./2014 26.7 4/5/2014 30.8 4/6/2014 35.2 4/7/2014 42.1 4/8/2014 51.2 1.0 4/9/2014 62.2 4/10/2014 67.2 4111 /2014 66.1 4/12/2014 64.6 4/13/2014 63.4 4/14/2014 62.1 4/15/2014 60.2 1.0 4/16/2014 57.7 4/17/2014 55.4 4/1812014 52.9 4/19/2014 51.1 4/20/2014 49.0 4/21 /2014 47.9 4/22/2014 47.6 1.0 4/23/2014 47.4 4/24/2014 47.0 4/25/2014 46.8 4/26/2014 46.5 4/27/2014 46.3 4/28%2014 46.1 4/29/2014 46.0 1.0 4/30/2014 45.9 TOTAL = 63,000 1,407 0 4 Ave = 63,000 48.5 #DIV/01 1.0 Max = 63,000 67.2 0.0 1.0 Min = 63,000 18.7 0.0 1.0 Camp Lejeune, NC 2014 ATAD Perriormance Data l ` I Dare i 4TAn Train 2 4 irani.r-� l Twin '3 R tianu C` liFnrrrl Colifor Feed Temp (Gallons} I (00) Temp (oC) Fecalm" (PI\') 4/1/20141 18,000 1 58.6 64.7 1.0 4/2/20141 18,000 I 58.9 64.5 4/3/20141 18,000 58.3 64.0 4/4/20141 18,000 58.7 64.2 I i I l 4/5/2014I 181000 1 60.4 64.9 i 4/6%2014 18,000 60.8 65.2 4/7/2014 18,000- 60.3 65.7 4/8/2014 18,000 60.9 65.9 1.0 4/9/2014 18,000 61.0 65.9 4/10/2014 18,000 61.2 65.8 4/11/2014 0 66.6 64.8 4/12/2014 18,000 63.0 63.4 4/13/2014 18,000 62.4 63.3 4/14/2014 18,000 63.4 63.8 4/15/2014 18,000 63.4 63.7 1.0 4/16/2014 18,000 62.3 62.4 4/17/2014 18,000 60.3 61.5 4/18/20141 18,000 60.6 61.4 4/19/2014 18,000 58.1 60.5 4/20/2014 18,000 60.2 60.4 4/21/2014. 18,000 61.2 61.2 4/22/2014 18,000 62.7 62.5 1.0 4/23/2014 18,000 63.1 63.4 4/24/2014 18,000 62.1 63.2 4/25/2014 18,000 61.8 62.5 4/26/2014 18,000 60.8 61.9 4/27/2014 18,000 60.3 61.3 4/28/2014 18,000 59.1 60.9 4/29/2014 18,000 57.1 60.3 1.0 4/30/2014 18,000 59.8 60.5 TOTAL = 622,000 1,827 1,893 5 Ave = 17,400 60.9 63.1 1.0 Max = .18,000 66.6 65.9 1.0 PAin = 0 57.1 60.3 1.0 Camp Lejeune, ILC 2014 AT AD Perormance Data Dare ATAD Train 4 A Train 4 B Coliiorm Feed (Gallons) Temp (oC) Temp (oC) Fecal (A�PI�!) . /'I /2014 E ` 4/2/2014 4/3/2014 4/5/20141 4/6/2014 4/7/2014 4/8/2014 4/9/2014 4/10/2014 4/11/2014 4/12/2014 4/13/2014 4/14/2014 . 4/15/2014 4/16/2014 4/17/2014 4/18/2014 63,000 24.7 4/19/2014 27.4 44/2WOU 31.1 4/21 /2014 35.3 4/22/2014 40.9 1.0 4/23/2014 47.1 4/24/2014 53.4 4/25/2014 61.3 4/26/2014 63.5 4/27/2014 61.7 4/28/2014 63,000 47.6 36.0 4/29/2014 44.6 50.6 1.0 4/30/2014 52.7 53.8 TOTAL = 126,000 591 140 2 Ave = 63,000 45.5 46.8 1.0 Max = 63,000 63.5 53.8 1.0 rEFln = 63,000 24.7 36.0 1.0 Camp Lejeune, NC 2014 ATAD Performance Data Date ATAD Train 1 A j Train 1 L i Colitorm Feed (Gallons) Temp (oC) Temp (oC) Feca! (MPN) ` 5/1/2014 45.7 5/2/20141 45.5 I 5/3/2014 5/4/2014 5/5/2014 EE 5/6/2014 1.0 5/7/2014 5/8/2014 5/9/2014 511012014 5/11/2014 5/12/2014 5/13/2014 5/14/2014 5/15/2014 5/16/2014 5/17/2014 5/18/2014 iJ! 1�/GV I'4 6/20/2014 5/21 /2014 5/22/2014 5/23/2014 5/24/2014 5/25/2014 5/26/2014 5/27/2014 5/28/2014 5/29/2014 5/30/2014 5/31 /2014 TOTAL = 0 317 0 1 Ave = #DIV/O! 45.3 #DIV/O! 1.0 Max = 0 45.7 0.0 1.0 Min = 0 45.2 0.0 1.0 Camp Lejeune, NC 2014 AT AD Performance Data DG.te ATAD Train 3 A Train 3 B Coliform Feed (Gallons) I Temp I (oC) Temp f (oC) f Fecal (m,P("') 5/1/2014 18,000 62.6 61.6 5/2/2014I 18,000 I 53.6 62.8 5/3/2014, 18,000 63.6 63.0 5/4/20'i4l 'i8,000. j G4.8 j 0-3.9 I I 5/5/2014 18,000 65.1 64.5 I 5/6/2014 18,000 65.3 64.8 1.0 5/7/2014 18,000 64.9 64.9 5/8/2014 18,000 64.7 64.8 5/9/2014 18,000 64.7 64.5 5/ 10/2014 18,000 65.5 64.5 5/11/2014 18,000 65.6 64.5 5/12/2014 18,000 65.3 65.0 5/13/2014 18,000 65.1 65.4 1.0 5/14/2014 13,500 67.1 65.7 5/15/2014 13,500 67.5 65.4 5/16/2014 13,500 66.1 64.5 5/17/2014 18,000 64.3 63.6 5/18/2014 18,000 63.4 63.3 5/19/2014 18,000 62.6 63.2 5/20/2014 18,000 61.2 63.0 1.0 5/21/2014 18,000 59.8 62.3 5/22/201.4 18,000 59.9 62.0 5123/2014 18,000 60.0 61.9 5/24/2014 11,250 60.8 61.6 5/25/2014 18,000 58.7 '61.3 5/26/2014 11,250 58.2 60.8 5/27/2014 18,000 56.6 59.8 5/28/2014 18,000 54.6 58.8 1.0 5/29/2014 18,000 54.5 57.8 5/30/2014 18,000 56.2 57.1 5/31/2014 18,000- 56.6 58.0 TOTAL = 531,000 1,929 1,944 4 Ave = 17,129 62.2 62.7 1.0 Max = 18,000 67.5 65.7 1.0 Min = 11,250 54.5 57.1 1.0 I Camp Lejeune, NC 2014 ATAD Performance Data Daie ' ATAC Train 4 A Train 4 B Coliiori"fi Feed I (Gallons) Temp (oC) { Temp (oC) Fecal (!\riPf�) 5/1/2014 59.8 54.2 5/2/2014 ! 61.9 53.7 5/3/2014 61.7 52.7 5/4/2014 61.0 51.8 _ 5/5/2014' 59.8 50.6 5/6/20141 58.4 49.4 I 1.0 5/7/2014 57.2 48.2 5/8/2014 55.8 47.2 . 5/9/2014 54.3 46.2 5/10/2014 53.0 45.4 5111 /2014 51.8 44.6 5/12/2014 50.7 44.0 5/13/2014 49.6 43.3 1.0 5/14/2014 48.6 42.6 5/15/2014 47.5 42.1 5/16/2014 46.5 41.7 5/17/2014 45.4 40.9 5/18/2014 44.6 40.0 6/19/2014 44.0 39.5 5%2U%2U14 5/21/2014 5/22/2014 5/23/2014 5/24/2014 5/25/2014 5/26/2014 5/27/2014 5/28/2014 5/29/2014 5/30/2014 5/31/2014 TOTAL = 0' 1,011 878 2 Ave = # DIV/0! 53.2 46.2 1.0 Ibex = 0 61.9 54.2 1.0 Min = 0 44.0 39.5 1.0 Camp Lejeune, NC 2014 ATAD Performance Data Date ATAD Train 1 A Train 1 B Coliform Feed (Gallons) Temp (oC) I Temp (oC) Fecal (MPN) 6/i/20i4� 6/2/2014 6/3/2014 6/4/2014 6/5/2014 6/6/2014 6/7/2014 6/8/2014 6/9/2014 6/10/2014 6/11 /2014 6/12/2014 6/13/2014 6/14/2014 6/15/2014 6/16/2014 6/17/2014 6/18/2014 6/19/2014 6/20/2014 6/21 /2014 6/22/2014 6/23/2014 6/24/2014 6/25/2014 6/26/2-014 6/27/2014 63,000 29.6 6/28/2014 31.3 6/29/2014 33.5 6/30/2014 35.6 TOTAL = 63,000 130 0 0 Ave = 63,000 32.5 #DIV/O! #DIV/0! Max = 63,000 35.6 0.0 0.0 Min = 63,000 29.6 0.0 0.0 1 Camp Lejeune, NC 2014 ATAD Performance Data Date ATAD Train 2A Train 2 B Coliform Feed (Gallons) I Temp (QC) Temp (oC) Fecal (MPI\) 6/1 /20141 612/20141 6/3/2014 1 6/5/2014 6/6/2014 6/7/2014 6/8/2014 6/9/2014 63,000 27.4 6/10/2014 63,000 28.4 29.0 1.0 6/11 /2014 30.7 31.7 6/12/2014 33.3 35.0 6/13/20141 35.5 38.1 6/14/2014 37.1 41.7 6/15/2014 38.7 45.2 6/16/2014 40.6 49.9 6/17/2014 43..0 52.6 1.0 6/18/2014 46.9 53.8 6/ 19/2014 53.9 57.2 6/20/2014 64.1 57.8 6/21 /2014 66.7 58.0 6/22/2014 65.9 57.2 6/23/2014 63.5 56.1 6/24/2014 60.0 54.6 6/25/2014 18,000 53.0 54.1 1.0 6/26/2014 54.7 54.7 6/27/2014 59.4 53.9 6/28/2014 58.7 52.4 6/29/2014 56.7 50.8 6/30/2014 55.7 49.4 TOTAL = 144,000 1,074 1,033 3 Ave = 489000 48.8 49.2 1.0 Max = 63,000 1 66.7 58.0 1.0 fin = 18,000 1 27.4 29.0 1.0 Camp Lejeune, IBC 2014 ATAD Performance Data Date ATAD Train 3 A I Train 3 B Coliform Feed (Gallons) Temp (oC) Temp i ' (oC) Fecal PI.) 6/ 1/2014, 18,000 58.1 60.2 6/2/2014 18,000 58.5 60.2 6/3/2014, 18,000 58.4 60.1 1.0 6/4/2014 15,000 57.5 60.0 j 6/5/2014 18,000 57.5 59.7 6/6/2014 18,000 57.2 59.3 6/7/2014 18,000 55.9 58.8 6/8/2014 18,000 55.1 58.4 6/9/2014 18,000 55.6 57.9 6/ 10/2014 18,000 58.3 57.8 1.0 6/11/2014 9,000 58.6 57.5 6/12/2014 18,000 58.2 57.5 6/13/2014 18,000 59.0 57.7 6/14/2014 18,000 59.7 58.2 6/15/2014 18,000 58.7 58.6 6/16/2014 18,000 57.6, 58.4 6/17/2014 18,000 56.8 58.1 1.0 6/18/2014 18,000 56.0 57.5 6/19/2014 18,000 54.3 57.1 6/20/2014 18,000 54.0 57.2 6/21/2014 18,000 53.3 56.6 6/22/2014 18,000 55.2 57.0 6/23/2014 18,000 56.7 57.0 6/24/2014 18,000 57.2 57.3 6/25/2014 18,000 58.2 57.9 1.0 6/26/2014 18,000 58.6 58.5 6/27/2014 18,000 57.9 58.9 6/28/20141 0 63.8 58.4 6/29/2014 0 65.1 57.0 6/30/2014 11,250 62.6 56.6 TOTAL = 488,250 1,733 1,746 4 Ave = 16,275 57.8 58.2 1.0 Miiax = 18,000 65.1 60.2 1.0 - i'iffln = 0 53.3 56.6 1.0 m Ci4R EJEUNE BENCH SCALE ATAD V®IL•. • ,1LE SOLIDS RE®UCT i��i ANAL' . START-UP DATE 4/10/2014 A B C D E F G H I J TOTAL VOLATILE SAMPLE SOLIDS ASH SOLIDS INHOUSE WT OF WEIGHT WT OF WEIGHT % TOTAL WT OF WEIGHT WEIGHT % VOLATILE % VOLATILE SAMPLE ATAD WT OF DISH DISH+WET (g) [B DISH+DRY (g) SOLIDS DISH+ASH (g) (g) SOLIDS WEEKLY SOLIDS TEMP DATE DIGESTION (g) SOLIDS (g) A] SOLIDS (g) JD -A] [(E/C)X100] (g) [G-A] [E-H] [(I/E)X100] AVERAGE REDUCTION I 0°C 4/15/2014 1.H. ATAD 71.9176 76.92 5.00 72.0068 0.0892 1.78 7149607 0.0431 0.0461 51.68 51.94 '`'.1 20 DUP 87.8155 92.82 5.00 87.9040 0.0885 1.77 87.8578 0.0423 0.0462 52.20 - - a. r.xn.,! ..r." .�x„a, a; •3 A.rv.. .,Y.t. ,B.. ., .,..., _..:... rd. .r ._... . . .:.. < <,j a .<k.. w <::•.: i':.:t-s:... ,4 .... .a z, :. vx._.z. .....«......: _ ,".. m.rr^.:.,t,•sv.x>•" >'..!.rWcr . xJxa:....:%. :'xv',.,+.x».: .ii.�x: pr«.,'�a.r:.i...iiAv.....3..:_.x, r k .x.,,,.. 4/18/2014 1.H. ATAD 74.052 79.06 5.01 74.1275 0.0755 1.51. 74.0914 0.0394e" 0.0361 47.81 47.11 9.30 20 UP 85.1034 90.11 5.01 85.1730 0.0696 -1.39 8.9 1407 0.0373 0.0323 46.41 . �•,r� v.., E•:s •xr . .. r. ,!: „,,. .. ,,.r t .. , c ., ,.. ,.. >. v .•, ,... . . q -L" v..,, 4/25/2014 1.H. ATAD 75.2281 80.18 4.95 1 75.3088 0.0807 1.63 75.2704 0.0423 0.0384 47.58 48.38 -2.70 20 DUP 84.2184 89.12 1 4.90 1 84.2981 0.0797 .63 84.2 5v., 0:rer.0::4.iY0v..5.ac 39!2're 0.�:.0f-.. 49.18 .._ : .a_e. . ."...... '-x8.xr.X9x.,•, •:`.EiY-x ' . .s. ..... .< ,.., ._, :..x^".. .x. _.,...+ ..,.:<� •L€L._, < , ..ra, r -, r - ,..vx, -,r •s ax .4„ .n N, r< .:.. x F v ., < v, _."":.i:..........:..,...a,..: <'..,..� :":"':�'�:.: ::,':i: •,. ...:'� ::., 48.27 ::: �':•:.... �':.::::..:: '?,.. ,; :.:£... LL ... :. ..::.:.::._.":.+:;. •,;::.. 5/1/2014 I.H. ATAD 81.8180 92.82 5.00 87.8787 0.0607 1.21 87.8494 0.0314 0.0293 45.48 6.00 20 DUP 84.2188 8 9.22 5.00 84 2722 0.0534 1.07 84.2494 0.0306 0.0228 42.70 ., f� .... .. . . , . ,r..♦.. .F .... .... x .... a <. .,r3„i.. <..,.... ... , . � 3 .. .. r. _,. r.!- ..... , .. .. .. .... .. : z ..., .. _ ., ..^.... r r .. ..... ,av, ,. ,?.. d. .. ,.. , % ..-.. .,......... x .. .. .. .. .. .," .... r Ni 5/8/2014 1.H. ATAD 85.1042 90.11 5.01 85.1686 0.0644 1.29 85.1343 0.0301 0.0343 53.26 53.03 F -16.60 20 DUP 72.8987 77.90 5.00 72.9646 0.0659 32 72 929152 1. 8 0.0311 0.0348 81 .,.r ... a. r . ...,. ,., ra....., ;«, •..:., .�: :aat4=,::•., i•%ki:E:: ::, -::St:- . .. .. , fr. .... ........ .... .. s .. ,. s .. n..x. ..,....... ...., r.. .i ... ... _ .... "..., ....,_ < . r .>.i r >.,: x"_,..4.,.i x...a: a ..: k..,•::::.::.. .... .. .a.x . , ' s <4. ., it .r ...... _. 4, , ♦., � . , ,.. , , s. ,. r....... . .... ..r. .. .... ._rv. ... i.v......r ,-. v :. ...,, .....-..,.....v>. rr=.. " ... ... .. : .. .<.._.. .... 3.. ,f ♦........r,.. 5/15/2014 I.H. ATAD 84.2196 89.23 5.01 84.2784 0.0588 1.17 84.2464 0.0268 0.032 1 54.42 54.54 -2.83 20 :1. DUP 89 1854 94.19 89.2445 0.0591 1.18 89.2122 0.0268 0.0323 1 54.65 ,.. . , � , .. ,rx:.... .,.. r... ,....... .-F�:xY:,_.,r>•:,.,;xa:.:,.x,;x .;::,».�:r.r.,.,-. , „ .. ... .... as .... ,. .,, .... , _.. ._., .. .x .._.. �" .. .. t.. , ... .,. 1. ..� ri:'il fed VOLATILE SOLIDS REDUCTION = INITIAL VS - FINAL VS X 100 INITIAL VS (VSR <15%) U vv i Ir" ATAD SLUDGE. ECAL ANALYSIS DATE (COLLECTED: TIME COLLECTED: 7Tv ELLECLEDIW",4c:,,�&,'�.��j � r RECEIVED BY: (DATE: L =ME DATE ANALYZED:. 7 • t j [TIME: 084 AnaALY�T: TES �_l METHOD: 3 HOURS at 35 :t 0.5'C In INCUBATOR .21 * 2.HOURS at 44.5 t 0.2'C In WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF POSITIVES WIPW100 r1nL 141"RUGRAdUB r) c!-lLo/ /5mL /� 0 /5mL `, V /5mL /5mL 0 /5mL C) /5mL 0 /5mL © /5mL UP 10... /5mL 3 HOURS at 35 zt 0.5'G in INCUBATOR [DATE IN INCUBATOR:�— DATE OUT INCUBATOR: 't , 1 t 21 fi 2 HOURS at 44.5 :t 0.2'C in WATERBATH DATE IN WATERBATH: T I [ DA17E OUT WATERBATH: `7 _ POSITIVE CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH PCs DS A-1 BROTH PC, 0 r-� Gv FORM UPDATED: APRIL 2007 TINE IN INCUBATOfl: � �'�^S TIME OUT ry j INCUBATOR: 4 TIME IN r J �� WATERBATH: l ` TIME OUT WATERBA714: �1(� TELPAWIr. 1CUF' WCIIeATOR \ O 3 J TeLPFA. ft- V"myOR 3 WnrF7WATEMwM OP TM: oo� TELPFAATUIIG OF wArcrGlm l�%TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) CALCULATION: MPN Fecal Coliform/grarn sludge = _ 10 x MPIV Index i Largest volume x % dry solids/r CHECKED BY: {"[ COPY MADE: DATE COLLECTED: y �CAL ANALYSIS ATAD SLUDGE 1. (TIME COLLECTED: 7� S FECEIVED BY: [DATE: [DATE ANALYZED: [TIME: METHOD: ; =COLLECTED931r: TIME. JANALYST' 3 HOURS at 35 * 0.5"C In INCUBATOR 21 m 2 HOURS at 44.5 t 0.2" C: In WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF HPW10�0 mL MPOWGRAM POSITIVES O/5mL (0/5mL C--)/5mL 6-0-ram /5mL /5mL /5mL /5mL /5mL D U P O 15 mL / 5mL 3 HOURS at 35 ttz- 0.5°C• In INCUBATOR . DATE IN INCUBATOR: DATE OUT INCUBATOR: 21 :t 2 HOURS at 44.5 :t 0.2°C in WATERBATH DATE IN WATERBATH: O , DATE OUT WATERBATH: -2 POSITIVE. CONTROL NEGATIVE CONTROL BLANK SS A-1 BROTH DS A-1 BROTH O S t�G FORM UPDATED: APRIL 2007 TIME IN ql � } INCUOATOR: t� �j4V I/�-� FTINE our IHCUBATOR• TINE IN �I��( WATERBATH: T1 TIME OUT G �� warERaarH: TEY�6uTUk-OF WGIOATOR J TFLPE31AiVt:GOF �S� O TEY'EMTING OF ' 'J^ WaTF]ICnTl1: .\J WATCil� TlTR: Ur TII- / f 7 �S I.7 % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) CALCULATION: MPN Fecal Coliforrn/gram sludge = 10 x NIPN Index Largest volume x % dry solids i CHECKED BY: G COPY MADE: ` ATAD SLUDGEFECAL ANALYSES DATE COLLECTED- 47 .. fs , TIME COLLECTED: 0, [COLLECTED 131f- RECEIVED BY: 7 �r 7 Y [)ATE: 7— /,F / y DATE ANALYZED 7— [TIME. 1030 METHOD: TIIlIIE- C� P6 O KN:AL:Y:S1F� 3 HOURS at 35 * 0.5'C In INCUBATOR .21 s 2 HOURS at 44-5 :t 0.2" C: In WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL mo10 mL COMB, OF POSITIVES NIIPIId/1tl� RnIL IMPOWGRA1M /7 C JZ G �% 0 / 5mL r� v 15 mL / 5 mL / 5 mL 0 15 mL / 5mL L� ®UP V /5mL/5mL 3 HOURS at 35 � 0.5'C. in INCUBATOR (DATE IN INCUBATOR: DATE OUT INCUBATOR: 21 :t 2 HOURS at 44.5 :t 0.2'C in WATERBATH DAlEINWATERBATH: `I L DAI'E OUT WATERBATH: 7 POSITIVE CONTROL_ NEGATIVE CONTROL BLANK SS A-i BROTH !n DS A -•I BROTH. ^�1 �C�� ,`o+ s FORM UPDATED: APRIL 2007 TIME IN INCUBATOR: TIME OUT INCUBATOR: l TIME IN � �r I WATEROATN: ��1�1,�9 TIME OUT ,:S j rf WATEROATH• TdPPnwTuneoa< uweATvm TEUPENATUaP or -' 0 U¢ EWIWR WATETUIIGOF WAtt]IEaitL• J wATtr WattrmTx l• _\.7 % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Csliiorrrl/gram sludge = 10 x MPN Index Largest Trolurne x % dry solids' -v? CHECKED BY:�. COPY MADE:�/V ]�,,._ CAMP L' ILINE WWTP ATAD SLUDGEFECAL, ANALYSIS DATE COLLECTED: ?. 22 - / y TIME COLLECTED: 7 'rJ COLLECTED IRY: A.`e.,; RECEIVED BY: [)ATE: DATE ANALYZED: `z `Z - t_ f F1- IME: l l l METHOD: 3 HOURS at 35 ze 0.51C In INCUBATOR ..21 x 2 HOURS at 44.5 :k 0.2"C In WATERBATH SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 ml- 10 mL 1 mL 0.'10 mL 0.010 mL COMB. OF POSITIVES Nlhq-UI00 nnlL _ MPOWGR AM C'.-20-/�-7 J /5mL /5mL /5mL l5mL /5mL /5mL /5mL /5mL j_DQP/ 5mL J / 5mL 3 HOURS at 35 zt: 0.5°C ini INCUBATOR DATE IN INCUBATOR: DATE OUT INCUBATOR: '7 21 :t 2 HOURS at 44.5 :t 0.2'C in WATERBATH DAi"E IN WATERBATH: -7 - 22 - I L4 DATE OUT WATERBATH: ''l , 2�j 14 POSI111VE CONTROL NEGATIVE CONTROL BLANIC SS A-1 BROTH N)S N e II``�� �L- N; DS A-1 BROTH ?S.M rJ,1-61 1� V FORM UPDATED: APRIL 2007 TIME IN ` INCUBATOR: I �� IIIn-0 T.. I WATERBATH• J WATERBATH: TFL16AAT -- MCUVATUM r O -3 . TELPFnATIIaY OF � �� VQ,119A1'UR \.l d waTtneaTro TFLPKAA1LaEOF waiCi'!aM E% TOTAL SOLIDS (ATAD SOLIDS ANALYSIS). CALCULATION: MPN Fecal Coliforrn/gram sludge _ 10 x MPN Index Largest vdlurne x % dry solids CHECKED BY: COPY MADE: ��� _ •T SLUDGEFECAL ANAL SHra I[�A1fE COLLECTED: EThIflE COLLECTED: O %�`� COLLECTED,B'y- FATE- `7. TIME. TIME: dANALYST ��`�="� a — vvIL (� 3 HOURS at 35 t 0.5'C In INCUBATOR x 2 HOURS at 44.5 t 0,2"C In WATER BATH .21 SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.'10 mL 0.010 mL COMB. OFF MPII-000 mnlL N11"DWGRAAM POSITIVES `r_— �, `� /5mL /5mL !� V O 0 0 0 —_ /5mL /5mL. /5mL /5mL /5mL /5mL IIJLBIro /5mL �I3 0-30UFIS at 35 d: 0-;_i_*0 hh 1bq(-,'[Jh3A1"0R _ L—aIE IN INCUBATOR: — 2� I+ I s7�/A:tlE09JrINCui3.krV]6t:�_2G, _ 91 x 2 C-UOURS,at 44.5� :r 0.2°r- urra UVAATEB�U3dATUI IDih"u'IE Ilv w,nTIEFICi.ATH: 4J,�AlI-E OUT WdATERBATI-1 CONTROL NEGATIVIE CONTROL BLANK SS ,A-1 BROTH Po's o a A � FORM UPDATED: /-APRII_ 2007 WC1E19ATUH: t? L � D TIME OUT l �G-C� INCN9ATOfl- TIME IN WATERAATH: TIME 0trr WATEPBATH: -` O TEP16tATW .S u�vATOR 35 t...% TFLPEAATunt of ��� uuaieATwe a•�• 7Ewr Tunalw 1. ' C WAr 7"; —t .`�. WATCTAArnre CF Wanr [a-R� % TOTAL SOLIDS (ATdAD SOLIDS ANALYSIS). CALCULATION: MPN Fecal Ccsliforrn/grarn sludge = _ 10 x MPN Inclex Largest volurne x % dry solids CHIECKED BY: COPY MADE- CAMP Lr, "7—.-LINE WMITP ikTAD SLUDGE FECAL ANALYS11cu, 1ftDTE --.c —),L —L! ETE �o �El iv T D B COLLECTED: Cd (L DAT —E: .21 :t2 HOURS at44X:i:0.2"C In WATERBATH SAMPLE I-Oefl,Tfoblj 10 bulL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL .,EIRBATH] 0010 L 0.010 mL CO OF 0 COMB. POSIMES WINVIG-0 u1nL N11�10'\R/GRWI'a ILLk—.— — /5 mL - -0-.— V/smL - D/5mL /SrnL .0 f S,rnL /5 mL /5ML -C 5 mL 0. C-) 0 --------- 3 HOURS a1t:35 ZL- ho INCUBAT orl FA�(:E IN I N G U BAI 0 R E—No =EO UT—IN--Cu —,3,%=Tovk--- S-14- ,m=-T--- I PT-' ---u- --T-- -- TE PMAWMUF =UDAMM. 2-d :t 2 GIOURS at 44.5:t 0.2'C un VVATERBATA Fk--V�IN WATERBA17H: 2-d :t 2 GIOURS at 44.5:t 0.2'C un VVATERBATA Fk--V�IN WATERBA17H: T- AT .AI. =. TFYrFnATu°EOF 44L, 'E GUT WATERBATI-11: 'T 0- T .. =AT.- wm%r4m 505§1—TIVE NEGATIVE SGA-1 BROTH -.1.OWTROLCONTROL BLANK y—` b-� CALCULATION: % TOTAL SOLIDS fv]PN Fecal COlifOrrn/gram sludge IDS 4-1 FiFIOTH (ATAD SOLIDS ANALYSIS). FORM UPDATED. APRIL 2007 10 x fv1PN Index Largest VOILime x 1% dry slids CHECKED 8 COPY MADA-l"'-p 71 ICyiUE iCOLLECIflElfo�' _ 13 j y ] TIME COLLECTED: HIIECDVED BY- DATE: tCOLLE( 1i; 13'(: 6tl (_L(,An7 l" I 00 3 HOURS at 35 2e 0.5'C In INCUBATOR 21 :t 2 HOURS at 44.5 * 0.2"C In WATE_RBATH SAMPLELOCATION �a0 serL 1 mL 0.10 mL 0.010 mL 10 mL 1 niL 0.10 mL 0.010.mL __ COMB. PPOSITIVESPOSITIVESE MPIW10,0 RNIL NOPOWGRA M _ GUw ' •� V� � � 0 C� � f 0 � Gp ei ` v / 5mL ! 5mL / 5mL / 5mL _ / 5mL / 5mL / 5mL / 5mL -- DL��.� ------ --_.,-.-._... ., " /5mL - ---------- /5mL -� m. 3 I-30UHS gut T; �L 0.5'0 in [11M Cr9B ATon DA o f IN INCUBATOR: ItDXti E OUT INCUBATOR- 2-1 :1: 2 HOURS at 0.2'C rin UIVXrERB ATH DATE IN WATIEFIBJkll•W: EDI�._u,E OUT WAATEMM'1: ----------- cIasIuivy CONYIIOL NEGATIVE CONTROL BLANK SSA-1 ISROTH — OVL DS A-1 DRO VTH FORM UPDATED, AM-111_ 2007 TIME INC4flA7CR: TIME OITT - INCIIHATOfl: TIME IN 1 �� WATERBA7H: WATERBA7H: TELP6W W, OF .V V ATvm )) _yy TlS/PE)UTu�•OF !� •.� p u�WOAI'OR /// V TrvrenA'runtvP Pi'� �' waTtnmTn: Jr� T-MAMMOF / wnTTruTw ��' % TOTAL SOLIDS (ATdAD SOLIDS ANALYSIS). CALCULATION: MPN Fecal Coliform/gram kludge - _ 10 x NIPN Index Largest volurne x % dry solids GFIIECKED BY:L COPY MADE CAMP LF--' LINE `tVWI-P DATE COLLIECTIEC . (q. j RIECEOV ED DIY: TIME COLLECTED: O 7 3 v DATE:. TIWI E: d0 COLLECTIE10-BY: �'IB11IE: b � AT� - 3 HOURS at 35 te 0.5'0 In INCUBATOR .21 s 2 HOURS at 44.5 :t 0.2"C In WATEFIBATH pfllll'IVIlGRAhl � `10 - COMB. OF SAMPLE LOCATION mL 1 mL 0.10 mL 0.010 mL 10 mL. i mL 0.10 mL 0.010 mL POSITIVES MP1W10,0 mnlL —`'" /5mL G /5mL /5mL 0 /5mL V /5mL ( /5mL 0/5mL O /5mL 3 HOURS at :35 1- 0.5'0 IPII INCUBATOR _I �'rIE IN INCUBATOR; ____ __ � :��• (4 _ DP RE OUT INCUBAT161=ti__—__ � `C/ I J�J 21 :L 2 HOURS at 44.5 -t 0.2°C un WATERBATH LDrYE IN WATEo-iD.aT_o-1 p 1,141"E OUT WATENDAT0 U ------- -- P OS111VE CONTROL NEGATIVE CONTROL (BLANK :>.S :v '1 IE11FlOTl-I - 7 DS :A-1 WiO TH FORM UPDATED. /APF111- 2007 INGUOATOfl• U TIME OUT II J' V V INGUHATOp: WATEpOATH: liC/ nluE our �^ � O WATEfl8A7H: �I TtIIPEiIAiURL OF u:G1eATVR �� •O TFLPEwATurt[oF , uuyBATOR 5-� ,F]IPEJUITUNE OF s WATERUATM: TO'PFAAN�E OP � wattrwnc � �-, I % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS). CALCULATION: MPN Fecal Cc:.lifarrn/gram sludge _ 10 x MPN Inciec Largest Volurne x % dry solids CHECKED BY: COPY MADE: CAMP LrER1I N 'OI(T P �� TAD SLUDGL FECAL ANALYSiS IU[��lfl rt�lU ILLII��If ILf[ I: TIME COLLECTED: 0 I SC7 a' COI-L� CTE Ica BY. —_----- rsl_:CEWED OV: D.'aTE A N' AL'IYZE f l [DATE: Kl,. _yflq. TIIlNE CJc, ?',7 �? --- [TIME: — 3 HOURS at 35 t 0.5'G In INCUBATOR .21 t 2 HOURS at 44.5 t 0.2'C in WAATERBATH oNIVUWGRA SAMPLE LOCATION 30 ivtL 1 mL y 0.10 mL 0.010 mL 10 mL 1 mL 0.•10 mL 0.010 mL COMB. OF IIrIP1W10,0 ffn L M 1705ITIVIE S O/SmL 015mL 0/5mL 0/5mL � D Q 0 / /5mL /5mL /5mL /5mL C) 15mL 1_Xn E IN INCUBATOR: BAIEOUT INGUBATOII__i 21 3 2 HOUR'S at 4- 4.51 _ (J.2'C M UlYATEIF BATH (r X E IN WfiXEfIC-rATH: I'E Our vv,,hTErsDA-rI-Y-` •?j'�� -- ---��- CaOSIIIVE CONr11OL NEGATIVE CONTROL BLANK SS 4-1 BROTH JS '' ' IDS.-'A-1 BROTH --- YV4 FORM UPDATED: APFIII_ 2007 TIME IN INCUBATOR: �. ,i_;570 TIME OUT 1 iL� INGUBATOfl: 1 ., WATERBATN• WATERBATN: u�cueATvn: 1,j lJ PFLPEAArv120F :� J viwwenTorc TF�PFJN1 OF ,r �.� wniramnl:l: TELPFJIAN�E OF wATTr"ne - '' % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Cc:-liforrn/gram sludge = _ lox fv1PN Inclex Largest volums x % dry solids CHIECKED BY: ') COPY NIADE: ATAD D SLUDGEFECAL. NALY U'603) �D�i�TE 1i; )LUEtCTE-Do_ _ 13 TI611fE COLLECTED: ©7 z5 CCLLV_CTEIG, BY: I fC:EVl/IEVy I�igY:�_� DATE: 1Nk3T E= �1M AIL'IYZIE f�: C' — TIME, �' ° r^ dA1�9AL1Y 's I'; - — �� 6UdE-U-CaOV:. - --� 2. 3 I_IOURS at 35 �t 0.5"C In INCUBATOR .21 :t 2 HOURS at 44.5 t 0.2"C: In WATERBATH —__----�- , SAIM31LIE LOCATION --- _. ` 'a0 vVIL _— 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF: POSITIVES MPP,I/10,0 nnlL PoUr°IVl/GffdAM ---�------ 6 /5mL --•—'-- 0/5mL O/SmL 0/5mL lJ /5mL 0 /5mL 0/5mL /5ml aA,dacai. V,®eood.®m,i„ -.�s.m.,��.mh� DUP------- -".� / 5mL -- V /'� / 5mL L_ilE IN INCUBATOR: OAIE OUTINClIY3,�TLSIt:--�l 21 �L 2 CJOUF6:S at 4ILL; s 0.2-C un WAATERBATV-V EVVE IN �ATEABIATH- O,1v -u. OUT UV:OTERIt3d4TI I_ --__---__ _-- --- _ POSi`Ii1lE NEGAME CONTROL CONTROL BLANK SS AA IBAOTOI 1�(.1s fl35 :9-'i EiIFiO T6-1 FORM UPDATED: fAPRIL. 2007 TIME IN ffy,l INCUHATOFl• 1 CAJ TIME IN � 1 WATEflOATH: Il TIME ❑ur /��a��� WATEFlBATH• (. �J TE1+Pfl1ATU++t OP TELPEA..1 V,P19.ATDR TEYPFAAwmw WATFAeATH: IT.....1 WATTr"TL• I% TOTAL SOLIDS (ATAAD SOLIDS ANALYSIS). CALCULATION: MPN Fecal Coliform/gram sludge - 10 x N1PN Index Largest VOlUrne x % dry solids C•I-IIECKED BY: COPY n/I,aDE: ��' ATA D SLUDGE FECAL ANALYSISSi 19 ATE COLLECT E� : G L TIME COLLECTED: d COLLECTED BY: Emi.:IGIEU!/IEIi�3gY: DATE: ��(, TIME. - � TIME: Dl aT E ANALYZED: l 3 HOURS at 35 z 0.5'C In INCUBATOR .21 :t 2 HOURS at 44.5 :k 0.2"C In WiATERBATH _ SAMPLELOCA,Ti011l 60 svaL 1 mL _ 0.10 mL 0.010 mL 10 mL 1 mL 0.'10 mL 0,010 mL COMB. OG POSITIVES MP114110-0 mrIIL NIG'0I/GR,�11llI 1 1 GZo` 0 ram, �/ 0/ ' O v 1 �1 / 5mL `� / 5mL 5mL 5 mL / 5 mL / 5 mL / 5 mL / 5mL DULD 0/5 mL /5mL HOURS at 35 :L- 0.!S'C- hu INCUBATOR j3 IU11AilE IN INCUIB ATOR: _I DXr E OUT INCUBATOR: 21 :t 2 HOURS at 44.5 s 0.2'IC iin WATERBATH DA u:IE IN W,IAYEAB A-ITH:` F,w'u-E OQIT W/ATERir "l-1: `B --_--�__ PO51111VE l�OWTnOL NEGATIVE CONTROL BLANKSS A-1 BROTH i,; @S rA-1 IF RO TH FORM UPDATED: APRIL 2007 TIMEIN �p�`�� INCUBATOR• ` J TIME OtIrr 1 •�D INCUBATATOR• l TIMEIN^ WATERBATH: Y!S TIME DUT WATERBATH: iEUPEilAT1f2 VF ['�•(�- �i�i WcueAivR fl J �/ irvPFruim2aF ✓=-0 u�e✓ Yt]LP£JIM1M OF .�1 wn*vuu�y , TEUPFAAYI➢1 M l wartrewitc J % TOTAL SOLIDS _ (ATAD SOLIDS ANALYSIS). CALCULATION: MPN Fecal Coliform/flram sludge _ Lo x MPN IncLex Largest VOILime u % dry solids Cl-IIECKED BY-, Q/ L I COPY MADE:.f�L `I� CAMP U ELINE "' V P ATAD SLUDGEFECAL. NALYSI'D DATES; 9LLIE�GICU fib; �( ! (� 1 `� TIME COLLI✓CTED: p �� OOLLO=�;TL_D UST : BATE: I lC =T11ME-4,`_n (�) C:�_—_V..� .�T E ANALYZED: � Left -� TI F1 aq 6U1 L:lf � �➢UJi_� __ �._ I� 3 C•IOURS at 35 tk0.5'C In INCUBATOR SAMPLE LOCATION 'c0 mL 1 mL 0.10 mL 0.010 mL G t20N� /5mL a /5mL 0 /5m1- /5mL IJ7M, /5 mL 3 HOURS ai4 ;35 �t 0_5'0 in 11MCUBATOR _I ID1A-dIE IN INCUBATOR: DJIXE OUT INCL1B AT01'1:_ , /`�ja�l6/' I 21 :1- 2 HOURS at 44-5 s 0.2°C tiro WATER13--,BATH IDXu E IN WATEFIB AI H: Etv F OUT W>'ATEKi(F MI--1 -- — t OSI u7VE l• ONTFlOL NEGATIVE BLANK SSAA BROTH [CONTROL rUS 9-1 BROTI.1lv�J`J_ FORM UPDATED. APRII_ 2007 ,21 :t 2 HOURS at 44.5 a- 0.2"C In WATT-RBATH 10 mL `0 /5 V /5 TIME IN j ^ INCUOATop: / •CI�U TIME OUT INCUBATOR: ✓ TIPAE IN � �� WATEpBATN: WATERBATN: li COMB. OF: 1 mL 0.10 mL (0.010 mL lPOSITIVE S 0 / 5 mL / 5 mL °� 15 ML WWe iw�bCmntvr2vF Sy r'� � A7T/R: I/ J L E== TUf2OFR 7S U TEL1•EMTURGOF /% ji y�� Wa�1T1: wanrrnnc P 6am Iv� v % TOTAL SOLIDS (ATAD SOLIIyS ANALYSIS). CALCULATION: Mp11-u1*D nnlL j NgrIC,NGRpdv1 MPN Fecal Cc4iforrn/4 f-an, sludge _ -10 x ,IPN IncLex Largess VOILime x % dry solids C•HIECKED BY: 0 COPY MADE: i` 1 CAMP' L"EUNE W'WTP ATAD SLUDGE FECAL, NALYS '' �iD�av ir+DLL��:T� �u: _ TIMECOLLECTED: m7 o coLLEcrlir� - - _-__- 3 �M___.___._.._� MILD K-W: DATE- • _.g . j TlME.' 10PffE ANALYZED: _ 91. TIME: 10 1 5 3 HOURS at 35 �k 0_5"C In INCUBATOR .21 :t 2 HOURS at 44.5 * 0.2"C In WATERBATH 9fv1P0 — COMB. OF SAMPLE LOCATION *W PuL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL POSITIVES MPII-1/100 nrkL l/G.n6dfiQl G'\O _ 1/ 0/5mL O � 0 0 4� ' /5mL /SmL /5ml_ /5mL /5mL /5mL l5mL I��JIr�e O /5mL � /5mL E ��'���''''C-J�'DURS aQ ;35 t 0. '(;- hu IhV' �L:f9B ATOn D_ -oE 1N INGLISATOL9: 67X E OUT INCUBATOR:— 1 2-d :t 2 HOURS at 44.5 s 0.2°C On WATERBATH IC9:y u IE 11V WATERBATH: E+,td'u E OUT WATERBATD 1 _ GF♦ '� - �--- ---- 0GSITIVE CONTROL NEGATIVE CONTROL BLANK SSA-1 BROTH IDS :a-1 BROTH ��� N� � fe&r FORM UPDATED: APRII_ 2007 TIME IN � I• INGUUATOfl: 1 TIME UIfT i �J- �� INGU9ATOfl: �J TIME IN h � 7, n WATEflOATN: I ;7 � l.� TIME UUr II I'� � C WATEFiaATN: `li J TE„PETIANA[OF ^5�- '1 TOIPElL1Nrtt OF '%.� V,AI9ATOR �j TEIdPEMTUFlE OF WATEn nr TEYPFA0.TUI,Z OF ��. '� wanrram TOTAL SOLIDS (AT,AD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Colifarrn/gram sludge = __IQ),N1PN Inclec Largest volume x % dry solids ci-e-CKED BY �a COPY MADE: ATAD SLUDGE FECAL ANALYSVI. �DATE (COLLECTED: r �j 3b � `� FEECLLECTED: G7aO Ent,:�G:lEUI91L=Vy lV: l�>` �j FDATE• �`i_ `j0. l�' TIME �LV�IXE ANALYZED: _ I,�c� • (�� TIME: ©3 — 3 HOURS at 35 :L 0.5"C In INCUBATOR .21 x 2 HOURS at 44.5 :t 0.2"C: In WATERBATH _ SAMPLE LOCATION §0 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.'10 mL 0,010 mL CO P05IPOSITIVES-MPIb1110,0 mnll NOQIOVI/GRA CV9 !� TI _ 0 /SInL /5mL (D /5mL 0/5ml_ /5mL 0 /5mL 0/5mL (D /5mL `� moo' n®v _ CCOV✓�� r /5mL 3 HOUR,'; att ;35 �L- O.S'C- Dull OhV'v::U BATOSI _ EDAYE IN INCUBATOR: -30.N1 DX E OUT INCUBATOR:Lt- 2-u 2 CiIGJIURS at 44.5 s QJ.2°C iin WATER BdATH N XG'E IN WATEftBATH:— Eiv o'E OUT W:AYIEKa�3:4'rB B+ _ I G1 • _ `A. J 1:ItlS!`IIVE CONTROL NEGATIVE CONTROL BLANK SSA-1 It1ROTo-1 — Dom Pc—& D5 :A-1 BROTH FORM UPDATED. fAPF111_ 2007 71ME IN / r INCUflATOfl: (� ��!-� TIME 0Ur 1 23 INCUBATOR: TIpeE IN �I j WATERBATN: " TIME OUT n WATERBA7H: TELPFAATIIII[OF /�� u1WtlATOR. 3 �J - Q rourEnaTw¢vF ��. G-� wW6A1pR TWY TUI GF C WATENlgt TOlPFl1ATVTiE OF V�-�` ��,^• WATL'Tfi1M % TOTAL SOLIDS (ATAD SOLIDS ANAL' SOS) . CALCULATION: MPN recal Coliform/ilram sludge 10 x NIPfV Index Largest volume x %, dry solids CHIECKED BY: COPY MADE: Camp Lejeune, i IC 2014 ATAD Performance Data Date A T AD Train i A j Train i o Coli ror Feet; (Gallons) Tamp (oC) I Temp Fecal , (oC) (MPf�) 7/1 /201 ^. 3 7. 0 { �� 1.0 7/2/2014 63"300 36.0 i J6.1. -7/3/2014 j 35.5 40.3 7/4/2014 38.0 43.8 7/5/2014 41.0 47.6 7/6/2014 44.7 51.7 7/7/2014 48.7 56.3 7/8/2014 -53.3 60.4 1.0 7/9/2014 13,500 54.4 61.3 7/10/2014 . 18,000 53.3 ' 61.1 7/11/2014 13,500 52.5. 60.5 7/12/2014 13,500 52.8 60.0 - 7/13/2014 13,500 53.9 59.6 7/14/2014 18,000 52.3 59.9 7/15/2014 18,000 53.1 60.5 1.0 7/16/2014 18,000 56.3 60.7 7/17/2014 18,000 56.7 60.9 7/18/2014 18,000 56.7 60.6 �.. ... r. A !l 1 `9120 IMF An nnn I o,000 CC ;,o a(*, 4 vv. , 7/20/2014 18,000 55.6 59.5 7/21 /2014 18,000 53.3 59.1 7/22/2014 18,000 51.1 60.0 1.0 7/23/2014 18,000 52.3 59.9 7/24/2014 18;000 52.8 59.9 7/25/2014 18,000 54.0 59.8 7/26/2014 18,000 53.1 60.1 7/27/2014 18,000 55.4 59.9 7/28/2014 18,000 56.1 61.0---- 7/29/2014 . 13,500, 58.1 .62.2 1.0 7/30/2014 13,500 60.5 62.9 7/31 /2014 13,500- 62.1 62.6 TOTAL = 445,500 1,595 1,728 5 Ave = 18,563 51.5 57.6 1.0 max = 63,000 62.1 62.9 11.0 iirlin = 13,500 35.5 36.1 1 1.0 Camp Lejeune, NC 2014 ATAD Performance Data {Dare ATAD Train 2 A Train 2 E i Coliform Feed (Gallons) Temp (oC) Temp (or) Fecal 7/1 /2014 I 55.1 48.4 I 1.0 7/2/2014 I 54.2 47.4 7/3/201A 52.8 46.5 j 7/4/2014I j 51.2 I 45.4 I -i I 7/5/2014 i 49.5 I 44.3 7/6/2014 47.8 43.3 7/7/2014 46.6 42.7 7/8/2014 45.6 42.5 1.0 7/9/2014 44.8 42.3 7/10/2014 44.3 42.1 7/11/2014 43.5 41.9 7/12/2014 42.7 41.9 7/13/2014 42.2 42.1 7/14/2014 7/15/2014 7/16/2014 7/17/2014 7/18/2014 7/19/2014 7/20/2014 7/21 /2014 7/22/2014 7/23/2014 7/24/2014 7/25/2014 7/26/2014 7/27/2014 7/28/2014 7/29/2014 7/30/2014 7/31/2014 TOTAL = 0 620 571 2 Ave = #DIV/0! 47.7 43.9 1.0 Max = 0 65.1 48.4 1.0 Min= 0 42.2 41.9 1.0 Camp Lejeune, NC 2014 AT AD Performance Data Cate { II ATAD Train 3 A Train 3 B Coli`orm Feed (Gallons) i Temp ' (oC) Temp (oC) Feca! (tlfPN) 7/1 /2014I 11,250 I 61.5 56.7 1.0 7/2/2014 11,250 I 61.2 I 56.9 7/3/2014 11,250 ( 60.6 56.8 7/4/20141 11,250 1 60.4 56.4 I 7/5/2014 11,250 61.1 56.4 7/6/2014 11,250 60.7 56.5 7/7/2014 9,000 60.8 56.6 7/8/2014 9,000 60.7 56.5 1.0 7/9/2014 61.3 55.7 7/10/2014 60.8 54.3 7111 /2014 59.7 52.7 7/12/2014 58.5 51.9 7/13/2014 57.3 50.5 7/14/2014 56.1 49.8 7/15/2014 54.5 49.0 1.0 7/16/2014 52.7 48.0 7/17/2014 51.1 46.9 7/18/2014 49.8 46.1 7/19/2014 48.8 45.4 7/20/2014 47.1 45:0 7/21 /2014 47.4 .44.8 7/22/2014 46.7 44.4 1.0 7/23/2014 46.2 44.2 7/24/2014 45.7 44.1 7/25/2014 44.8 43.6 7/26/201.4 44.1 43.4 7/27/2014 43.7 43.4 7/28/2014 43.4 43.4 7/20/2014 43.0 43.3 1.0 7/30/2014 7/31 /2014 TOTAL = 85,500 1,550 1,442 5 Ave = 10,688 53.4 49.7 1.0 «iax = 11,250 61.5 56.9 1.0 Min = 9,000 43.0 43.3 1.0 Camp Lejeune, NI!C 2014 A T AD Performance Data L Date AT AD Train 1 A j Train 1 B j Coliform Feed Temp (Gallons) I (oC) I Temp (oC) I P cal (IkAPN) 8/ 1/20141 9,000 1 62.4 62.2 8/2/2014 9,000 j 60.7 j 61.2 j I 8/3/2014 9,000 58.7 60.0 8/4/2014 13,500 55.9 59.0 8/5/2014 18,000 54.8 58.9 1.0 8/6/2014 18,000 54.0 59.0 8/7/2014 18,000 54.5 58.9 8/8/2014 18,000 56.5 58.9 8/9/2014 18,000 57.9 59.3 8/10/2014 18,000 59.2 59.8 8/11 /2014 13,500 61.0 60.5 8/12/2014 13,500 61.6 60.5 8/1312014 13,500 61.0 61.2 10.0 8/14/2014 18,000 58.8 61.1 8/15/2014 18,000 57.7 60.7 8/16/2014 18,000 58.0 60.5 8/17/2014 18,000 59.4 60.4 8/18/2014 0 60.2 60.6 8/1912014 9,000 1 62.2 61.4 Lu 8/20/2014 9,000 61.5 60.8 8/21/2014 13,500 60.6 60.1 8/22/2014 18,000 57.4 59.5 8/23/2014 18,000 57.3 59.6 W24/2014 18, 000 56'. 1 59.3 8/25/2014 18,000 54.2 58.9 8/26/2014 18,000 52.7 58.8 1.0 8/27/2014 18,000 51.7 58.3 8/28/2014 1.8,000 50.8 57.7- 8/29/2014 18,000 51.2 57.3 8/30/2014 18,000 51.3 56.9 8/31 /2014 18,000 51.0 56.8 TOTAL = 472,500 1,770 1,848 13 Ave = 151242 57.1 59.6 3.3 Max = .18,000 62.4 62.2 10.0 Min = 0 E50.8 56.8 1.0 Carnp Lejeune, NC 2014 P.TAD Performance Data Date ATAD Train 1 n i Train 1 E" { Cottfar Feed (Gallons) Temp-� Temp (oC) (& Fecal 9/1/20141 18,000 51.8 57.0 _ ' 9/2/2O14� C 55.0 5-.5 i f 9/3/2014 9,000 55.7 ' S7.8 1.0 9/4/2014 18,000 53.5 57.7 9/5/2014 18,000 52.1 57.4 9/6/2014 18,000 51.1 57.2 9/7/2014 18,000 50.8 56.5 9/8/2014 9,000 52.4 56.6 9/9/2014 18,000 51.7 56.6 _ 1.0 9/10/2014 18,000 49.9 56.1 9/11 /2014 18,000 49.7 55.5 9/12/2014 18,000 50.0 55.3 9/13/2014 18,000 50.1 55.0 9/14/2014 18,000 50.5 55.1 9/15/2014 18,000 51.8 56.0 9/16/2014 9,000 56.0 59.8 1.0 9/17/2014 9,000 57.2 60.4 9/18/2014 18,000 55.2 60.2 • QMn17n-1A Ol i ocv i-r nn nn Q a,C �rv. v� 50 7 9/20/2014 9,000 54.7 59.2 9/21/2014 0 54.6 58.2 9/22/2014 18,000 51.1 56.6 9/23/2014 18,000 49.5 55.5 1.0 9/24/2014 18,000 48.5 55.9 9/25/2014 0 50.9 57.1 9/26/2014 0 52.9 56.6 9/27/2014 0 53.1 55.7 9/28/2014 0 52.9 54.7 9/29/2014 0 52.6 53.6 9/30/2014 0 52.6 52.4 1.0 TOTAL =' 342,000 1,573 1,703 5 Ave = 11,400 52.4 56.8 1.0 Max = 18,000 57.2 60.4 1.0 Min = 0 48.5 52.4 1.0 Camp Lejeune, NC 2014 ATAD Performance Data Date ' ATAD Train 3 A Train 3 B I Coliiorm Feed (Gallons) Temp j (oG) `, Temp (oC) FecGl (��`iPh!) 9/1/20141 9/2/2014 9/3/2014 j 9/412014 j 9/5/2014 1 f i WD/LU 1141I j 9/7/2014 9/8/2014 9/9/2014 9/ 10/2014 9/11/2014 9/12/2014 M 9/13/2014 . 9/14/2014 9/15/2014 9/16/2014 9/17/2014 9/18/2014 9/19/2014 9/20/2014 9/21/2014 9/22/2014 9/23/2014 9/24/2014 9/25/2014. 63,000 28.3 9/26/2014 32.5 9/27/2014 36.0 9/28/2014 40.3 9/29/2014 45.2 9/30/2014 63,000 41.5 -37.5 1.0 TOTAL = 126,000 224 37 1 Ave = 63,000 37.3 37.5 1.0 Max = 63,000 45.2 37.5 1.0 fi in = 63,000 28.3 37.5 1.0 CAN -' EJEUNE BENCH SCALE ATAID V ATILE SOLIDS REDU(�fP ION ANf SI START-UP DATE 7/18/2014 A B C D E F G H I J_ _ iI TOTAL VOLATILE { SOLIDS ASH SOLIDS INHOUSE WT OF SAMPLE WT OF WEIGHT % TOTAL WT OF WEIGHT WEIGHT % VOLATILE % VOLATILE SAMPLE ATAD WT OF DISH DISH+WET WEIGHT (g) DISH+DRY (g) SOLIDS DISH+ASH (g) (g) SOLIDS WEEKLY SOLIDS TEMP DATE DIGESTION (g) SOLIDS (g) [B-A] SOLIDS (g) [D-A] [(E/C)X100] (g) I [G-A] [E-H] [(I/E)Xl00] AVERAGE REDUCTION 0°C 7/22/2014 I.H. ATAD 86.4491 91.45 5.00 86.5393 0.0902 1.80 86.4949 0.0458 0.0444 49.22 49.64 s;`,;-:k-,`, ^ 20 DUP 73.2500 78.25 5.00 73.3419 0.0919 1.84 73.2959 .,f.;.. ^aa: _t '� ' z�&.. ,."t,-s.: •�i�.t.`3£":` b".i 0.0459 0.046 5 i4�., 3xt �fr.::3`-"`''"=`= ��'J>'• <wf, .. ; ...=; (. , ,. ., .r ., t x ." . " <, >, .k „<.. - ._ ,".. ,." ,r a a ,z. ,<- ...7�vx-3,$-a _,..a, ,_ n .: .,.,.>., ,....,,<,.,-c» ,. .at,,,e- ✓'>i�: xd:. �4hrt �t x 7/28/2014 L H. ATAD 72.9008 78.90 6.00 73.011 0.1102 4 1.8 72.9550 0.0542 0.056 50.82 54.47 -9.74 ' 20 DUP 73.3132 78.31 5.00 73.3987 0.0855 1.71 73.349 0.0358 0.0497 58.13 �Y- :' xi` � ��>v ..< ._..,s,- ..:.. -x .,.x, . -. .. ... .s .< , . 3u. ,. � , x ,.,xs, _ _ ,. ._..r __. a S ,x �k 'Sr .S > , r x, r•, ». r.r., a -< .. .. ... x ., .ra ,. ..xY...0 s.. .. xv ,?'xv, ;>-.... ..... ." - • v� ", ,. Yv x .•t r�_r , .., o aa.... .,, x. fix.:_, .. ��• 5^ ,i ,,. _ >.. .. .,.r x - ..,.,a., 50.54` 50.65 7.02 2U 8/5/2014 I.H. ATAD 73.2509 78.26 5.01 73.3433 0.0924 1.84 73.2966 0.04.57 0.0467 DUP 86.4509 91.45 5.00 86.5437 0.09.28 1.86 86.4966 0.0457 0.0471 50.7� _ t..,.x.�. .� . x,e ..... i. r<, .x , -.x 4f•.. ,E , .. ,::,,,..<.:.t..:,x.,:"r.x<...�r,,..�:�x,.:a,x ..., ..,. _ <. ,i .<. t. , x <. .r .> .-a .. .. x x ...r. Y.e. ........... ..raar ,+.a•C<,...... a�.a:xr,�<xax3tt:,w;r.}„,. ,firx.ar ".v 1. .,'r '•<�,. -Ga:%�`�.t„a:#a, t': .. ..x, ,x ,. .. .., .< ., ... 4 axzx.... ,F 3x , ,:,,,,., x r.. " Jm sr,. z .. ..-<,...t.. a .x s a x aJ ».., .x x..<... _ f,.. ,." .-x ...,,.x _._ ._, . , ,>x.a ., ><., e. .. .x, .< . , a.. L, 3 , , <._.-t . _ rr , ... ..£ € x- s. '}-". .. ..... ... .r.,._tr .. _.. ,. .. ..,,4., , ., x.... . , , f ., a. _,„.-..^-<s,r ,.,: ra.Y;,,..,..,..x ..:, ,..v....,xx....,.,. .>" .u.x. ..v,-.-w ...><3�.3~e:x. .rr ... .. .. .. C . ._ ... .rr-3 .2 Six a_ a.._, t,.M .. .. : ....s.aa-. x.Y, .x �x , x "'tr r s,.wS "aaxz .m s,. ,,r a»x. ,.,x ,x r , '._< ,."<,.,:c,.� ... r" +`r .,rx"rr•y;- ,.xT�,. .-a.,.. ._.n_ 8/12/2014 I.H. ATAD 73.5586 78.56 5.00 73.6527 0.09.41 1.88 1 73.6063 1 0.0477 0.0464 49.31 49..18 2.91 20 �•-�ri � -., ""r ' ; F' �'.�:44-�'+� a`. ;y �."'i'=��' : ` „f .: .^ t; .':<.:• ;.- .".� ..K. DUP 72.9037 77.90 5.00 72.9977 0.0940 1.88 72.9516 0.0479 0.0461 49.04 . c _ x_ r , h ,,.x , x.v ,. •x ,, a o^:,.,>,r�<, stx ::::a. < i j n t _ .r, , » , x .x _ ,". „ si x ,.... ,...,,, . .. n a ,.., .. , _ -x-,: 'r::-<-; <.; • .,: *.:;' „ .. ....nx . , x .. , .: v<..... .x ,r „a ,_ .. Y . ",.. { h e x .,..exx ... <. _ ., ax>•.3 < ,. # "�:""; i;:':;.:`•`;'i, h�'f;`n3:": .: _,'` ; . ,. ,:, N_..,:.,>:.., <,. ., _ .,..;,..:..a";: .>..ax, „ a.r`a,> x.rr. ,: .. .:. ,; -.%.. .:, :,t. `•;,., ,_ ,,.,,xrt. .�:.,<::':;;., ...�,x. _.. .-.:x:,,ax.,�.:V ;: ... .. ..... .:. 8/19/2014 I.H. ATAD 72.3633 77.36 5.00 72.4362 0.0729 1.46 72.3995 0.0362 0:0367 50.34' 50.79 -3.27 20 .037,w5 51.23 0.12 5."<01 810.0375 90.1246ox D.U,P...85.r..ar>..,, 1.n.u.rt8.1.....,._,,2 0x.,< 0aFA`. 7..o 3„ 2Kr'x'F 0.,80.., n Kx t^.h''•,:° .. x .1.r .,_}. ..v Y , i.,r .n-s5< x_ ..5.. .v .. ...n # ..r „ • '�' x. a ,. ,. ,,.< �, x „> <. ,x .,r..#:.., > t a p .x x,. ..:...,. xr. .. . ,..._. ...Y.-P >x, ..5 .., ., . x : r #r f" k. .. .. ,.. #.. > , m <.. .» xcR .,. a.•:>.:.R £. :'r'v.Y Ir, ., . ,- _ v,.> U ... x ,f c. x , „ k v v 3. va <-x...... .-^-^, x-srcx.:-c --.. _. 1^.>.•. .A, ?xxxxc, ... x, xx, x""",x ,f_ ,.. r.:f .. „t .a, .. x•:na :._.. x. _> F--9,a,x _ ,r. <._" . 8/26/2014 I.H. ATAD 87.8201 92.82 5.00 87.8944 0.0743 1.49 87.8559 0.0358 0.0385 51.82 52.05 -2.50 20 -- 86.4510 91.45 5.00 86.5252 6.4864 k0.,'0.£388 . .29 <.- 86.4864 .074..x.�. .,. ..2.•..f.... .i0�Fo3'rrx54 52;. .0'<a. e.0 ,:..:«x_,<P.,xc,.d..Y 1w_x;Y.- `t.4.8 : f"r >`L... a"=7.aaT.•.•a .w .x >x>VD x.: S;rv` .,.:=T <t,,.:x, .r»xc•.9>a.x.x.• x, .xxnr � - .. > VOLATILE SOLIDS REDUCTION = INITIAL VS - FINAL VS X 100 INITIAL VS (V SR <15%) ;,AMP Lr LINE 1VVTP ATAD SLUDGE FECAL fikNALYSK,.1D ID AYE GOLLECTEH'in %4 - % . TIME COLLECTED: 021s-- COLLC:CTiIED BSI'': �I:CEUlPIL`-fLU C-iY:` _ DATE: TIIIJdE: �.•^� v ` __'.� j?',�E : V 1,WL'VZED' -_(' 0 —'7r-t TIME: SAMPLE LOCATION 3 HOURS at 35 zL 0.5"0 In INCUBATOR � 10 mL 1 mL 0.10 mL 0.010 mL .21 :t 2 HOURS at 44.5 .L0:2" C In WdATERBATH 10 mL 1 mL 0.10 mL 0.010 mL -�, COMB. OF MPIh11100 unalL 'NIPRWGff3/! M POSMVEfo C/Zo IL71ll )Grp --- —_ I5mL t/ /5mL C:- 5mL b /5ml- _ ___ �✓ / 5 mL 0/5mL O/5mL o /5mL C. )/5mL � D.!4'dE I1\9 INCUBATOR: D rE OUT INCUBATOR: 2-d t 2 HOURS at dW.b; s 0-VC BSI UIYATERB ATH lrs,V-o:E IN 1N,R�fIEr�iB�all-H: — -G�a_/ �G� p3,4'B-IE OUT WATENf3M11 -' — ------ P13SIuIVE CONTROL NEGATIVE BLANK SS :i-d BROTH — CONTROL PC,& 0 DS :V1 BROTH _Pa_s FORM UPDATED: APRII_ 2007 wcueArGR: � ?, 2 T!ME OUT - z 5 INGU9ATOP: �� S WATEHBATH: �/�zs TIME OU7 � f'1 WATERBATH: �'� TEI1PTl1ATUHG OF C wcueATOR �,` _ TELPF3UNrtt OF `v rrvrennTunt OF /(J� �- WATFReAT,l: TFJIPFAATUrt£OF 11 / �` % TOTAL SOLIDS (r4TAD SOLIDS ANALYSIS) . CALCULATION: MPN Fecal Coliforrrl/41ram sludge _10 r MPN L-L(. Largest Volume x % dry solids C•I-IIECKED BY: " I ,., COPY 5MDE: IU�dATE r,OLLIEG`V-E.D: / o - / /• / IiTIME COLLECTED: H11:'G'EOlIIL`D BY: S__�L�— ``10.4TE ANALYZED: l 1) l$ t 9— TIME: METHOD: -- — -- CAMP L f '--- LI E 1YVT AVD SLUDGE FECAL ANALYHS' COLLE4:�f� Ifs her: -:y:--, 3 HOURS st 35 zk0.5"C In INCUBATOR 0.010 mL .21 x 2 HOURS 10 mL at 44.5.+0.2:'C 1 mL In WATERBATH 0.'10 mL 0.01� 0 mL SAMPLE LC)C�,YI2hN I 10 ertL 1 mL 0.10 mL C�2 U /11 / ^` _ / 5 mL 0 / 5 mL '�, 0/ 5 mL O / 5 mL 0 / 5 mL V / 5 mL l./ / 5 mL D / 5 mL 117 JIL9L� o � IsmL v 15 mL ,®•�,e 3 O-OOUAS at 35 zt 0.5'0 ho OhV' C19By'AT'OR _ BA p E ON INl .t�SA OIR: l O .^, 1 r� J TIMEIN ,(} � (� TD1PE31AN�OF INCNflATOfl: v C�•i ' u cueArorr f�, l/ — ID�i (E OUT I NGLIB ATOM'— � l% ^`� c � OUT r� TrvPes,aTwROF � � �'1 weuearon: � � ✓ � vua aAre e — , l J 21 :t 2 OJGUFI:E; at 410.�. :k 0.2°C in WATERBATH IL3=y 0 E IN UI ATIERB.I TH: [ V �� � L WATEfiBATN: l � 3 � WarEnnnT": —'I TIME OUT *�, C .--- TEVPcnnTvnE nF p D,(I E OUT WATERDATH: 1 %'1�—I C ' �' I WATEPEATM O ( o- WAnrum: �"� `I —J_ -- F-10SI` IVE CONTROL NEGATIVE CONTROL BLANK BROTH ? � N uS A-1 FROTH FORM UPDATED: APF-111_ 2007 I � J % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS). ,�,a�„ , o„mw�m� .•m,aee�m COMB. OF Illlf?Od1100 mralL N➢��IVUG➢�A9 POSITIVES CALCULATION: MPN Fecal Coliiorm/41ram sludge = 10 n NIPN Inclec 1_argesi volume x % dry solids Cl-IIECKED BY��„_ COPY MADE: �_ CAMP LIB LEI N E WWTP MAW W LUD FECAL ANALYSH�.,'D IDATf r (COLLEIL;11'E- 1): _ _.� . TI61flE COLL(ECTDD: IL:OLLEQ�'TI'lr ICh BY: =ME. DATE: � il- -x l - � �. A :tG4E V ED BY: __-- � li :� 1,• � (� TIME: I =kms W'&TIE A N A LY ZED.- 6U1Llfo-ilLr'VV7�^— �� SAMPLE LOCATION Coo 3 HOURS at 35 zk 0.5"0 In INCUBATOR .21 :t 2 HOURS at 44.5 * 0.2'C In WATI_RBATH `10 buL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL ^� /5mL U /5mL 0 /5mL (J /5mL /5mL /5mL /5mL 5mL L� / J cam/ 5 mL 3 HOURS mil 35 :: 0.5'0 ho [141 C:UBATOR IfDA'S lE IN INCUBATOR. DXm'E OUT INCUBATOR: 2-1 ::L- 2 HOURS at 411.5 s 0.2'C`j nn VIVATERBATIH .1%70E IIV WATIEABAI"H: WVE OUT WATIERIE3,,YI-1: — --- SS �,14-1 BROTH POSITIVE {;i+��NYdIQL NEGATIVE CONTROL BLANK DJS -k-•d BROW FORM UPDATED: APF(Il- 2007 INCNBATOR: TIME OITT I � �.'�I INWfiATOR• Vv TIME IN WATERBATH• 1ffvJ -J TIME DUT I � Z� WATERBATH• 1 r �J TdPFAANIROF (,T TdPEAATnnt OF WW6 =, V TdPFl1ATUnGOF / WAn7wanl: TdPFAA1Lf1E OF �(,��� waTl'itAM % TOTAL SOLIDS (A.TAD SOLIDS ANALYSIS) . COMB. OFIUIt'lll/iO4b mnlL �1llII�I1NQnRd!�II CALCULATION: MPN Fecal Coliform/gram _,lUdge = 10 x NIPN Index Largest v0lL1rne x % dry solids CHECKED 4YJ. 4_;_ COPY MADEy i,� m ATAD SLUDGEFECAL. ANALYSH-,'� DATE rC OLLIElC TE .O: 0 � �/ TI6VIE COLLECTED• C®O_LEd�'�I[_I[F b",If - J R[II.,C-E-11VEliy I�ilf: -/ , DATE: TIME: �PaTE AN1jf4LYZEu: TIME: � � v LLY;�T� 3 HOURS at 35 zt 0.5`C In INCUBATOR 21 x 2 HOURS at.44.5,d: 0Z'C In WATI:RBATH SAMPLE LOCA,T60111 10 brtL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL �2 4 /Y1 ---- — - — ll / 5 mLl.' - -- / 5mL v / 5mL IS mL L) / 5mL / 5mL 2- / 5mL L� / 5mL MHz' j-} v / 5 mL � / 5mL 3 HOURS a4 ;.35 � 0.5'C- OuI ON CUBATOR Imk'u IN INGUBATOR: _ k7�Ali � OUT IIVCIIB ATO6"I' 21 :L 2 HOURS at :R: 0.2°C un WA4TERBATH LA-_f E IN W/.TIEAB ATH: _ (� �� • I Sm' -IF OUTUVATERDA+IH: TIME IN wcuaATon: F.ATEIAM •I f7 tJ TIME our WATEPBATN: � /s 5 C=G I11VE NEGATIVE ---�— —_ ONTROL CONTROL BLANK SSA-1 BROTH t BROTH FORM UPDATED; APFIII- 2007. �J TELPFAANIft OF -7 �� • VIG40ATOR J rrvrouru� of uw�oatvie •��.�L nyrFJatuneoF fl z / WAnmw nf: reuronarwrzoF (� wnnr�+.m � / • � .� COMB. OF 1M6�Ihd/700oINIL �fvll'IJUCIRRJ;vI PGSMVEFrr. G- CALCULATION: % TOTAL SOLIDS WN Fecal Cc:di(arrri/dram sludge = (ATdAD SDLIEG ANALYSIS). i o �� r�1Pry Index Largest volume x % dry solids GI-IIECKED BY: ;— COPY P/IAOE:hr ' 1, L r '"RINE WWTP ATAD SLUDGE FECAL, ANALYSIS DATE COLLIECTED. —.._._ TIME COLLECTED: 0gr is �;OILLE�:T�;�ifl fu✓vy BY: --_-� [DATE: Do�TE s�eV�9�WL I� ILI<y:TIME: 12 I �� �ANA1L'V'rynT:�.- 3 HOURS at 35 -t 0.5"0 In INCUBATOR .21 x 2 HOURS at 44.5 :t 0.2" C: In WATERBATH SAMPLE LOCA,YIOkkl FnL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL l� R 011A -�10 /5 mL Ir?/5mL 0 /5mL 0/5ml- /5mL O /5mL /5mL /5 mL _- - j_._0/5mLj /5 mL jj3 HOURS a4 :35 :f- 0.6'C. uuu OhVCUBATOR _II IIDk=dbr IN INCUBATOR; DME OUT INCUBATOR- 2-0 3 2 HOURS at 41U", :t 0.2°C On UIYd4`FERBATH DDAYEINWATERBATH:OUT WATERS"H: ---------- POSI VIVE CONTROL NEGATIVE CONTROL BLANK 16S ,-9 FSRt7"PFI FORM UPDATED: APRiI_ 2007 TINE IN ��^ INGUBATOfl: Jf� TINE LA T INCUBATOfl- �J TINE IN WATEflBATH: I � �� TIME ❑UT I •��O WATEfaBATH: TEIIPEFIATIAY OF } , ViWOAiOR 'f� � `V rrvPouni�oF � j : � V V�IMIOR rF]°PFAAT1At OF r WATFA➢ ft L -. TEYPFAATVAE Of WAnrum �`�'• I% TOTAL SOLIDS (ATAD SOLIDS ANALYSIS) . ICOM43. OIL 'Iplitr�lh�/10�0 mall �NOI�OIIlUGIr�/!Illla POSITIVES (_ /,� 7o�m CALCULATION(: MPN Fecal ( offorrn/41ram sludge 10 n NWN Index Largest vole-n•ne x % dry solids �f�/fir• C•I-IIECKED 0 I \_ COPY MADE A,rAD SLUDGr*FECAL NALYSI', IDr.1 TE iGOLLEC V r--D: i I �, i t KIME COLLECTED: G)—� C Ll COLLIEC'� EID I�0P': .C:EWED Er,Yf': / �, �_, DATE: ; %}, [T:IPIII�E- 0(`'pU l TIME. Q�S C�fl9l�1. i^ �,�• (� _ ..� 6UJL':= 3 HOURS at 35 trc 0.5"C In INCUBATOR .21 m 2 HOURS at 44.5 * 0.2"C in WAaTERBATH. GASMPLIE LOCH-HOM -E0 6S L I 1 mL 0.10 mL 0.010 ML. 10 mL 1 mL 0.10 mL. 0.010 mL COMB. OI=—� POSITIVES MPg,d110-0 gjnL —NIPOWGRA M C 0 /5mL /5mL /5mL IS mL /5mL /5mL /5mL /5mL , 1— j J L) I I . . `....-/ 5mL ----------•— — / 5mL 3 HOURS a 35 a: Il➢.5'C- hii IhIIC UBA`I'ICDrI _I FV.-E 911S 4� J IL�s i rE OUT INCUBATOR.. _— — —� �_ ` � • �{ 2-9 -t 2 HOURS ae 02'Ii; un WATERBAT I -I IC�.yI(IE lIV VN,IllfEsciB.Cll iri: �` "f 1 1E OUT W>6TEr-.iB f0 J— INCUf3ATOfl: �7� /�,J INCU[ul7Ofl: V WATEfiBA7H: � 1 � �% 1TWE OUT WATEflflATH: v �� —_ --_—_------- - POSITIVE t;ON AOL NEGATIVE CONTROL_ BLANK SS ;+ 1 BROTH Ds;.-1 E,IFIl9 ��r------•-----���� S `I(L.� 1(� v (J FC FIM UPDATED: AP'Vill- 2007 wcueATolr ��JJ rO,rFsun,rtt of u:cveA,ox 7tlIlEnnTUflf OF �' WnTF]Uwni:•� WaTOJPFAATnru+Tm -- 4 4 % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS). . CALCULATION: MPN Fecal Csiiform/gram sludge 10 x NIPIV Inclec Largess VDIr.Wrne x % dry solids C•I-IIECKED BY.b, . COPY MADE: � � �AIP I "JELINE WMITP AT11:: D SLUDGE FECAL. ANALY M TIME COLLIECTED:©1.7? COLLECTED 930f: IRiC::�C:�=UA/ED EB Y: � DATE: � � --- - YST:—. �� 6UJ1:� U U,IuU .: _ SAIVIVIL1E LbCAY16,N -----------�__ 3 C9OUR5 at 315 zk 0.5"0 In INCUBATOR ` 0 artL 1 MI_ —0.10 mL 0.010 mL .21 * 2 HOURS at 44.5 :t 0.2" C In WATERBATH 10 mL 1 mL 010 mL 0.010 mL _ COMB. OF MPI1W10G nnlL MPOdVGRAAM POsmVIE u / 5 mL O / 5 mL 0 15 ML 0 / 5 mL 0/ 5 mL 0 / 5 mL 0 / 5 ml- / 5 rnL L.) /5 mL 3 010URS bait 3_5 --L- 0.5, h1i 11AC:UISARTOR _ If1,�"i IE OPJ INU'49 [3;AT--- -- �q I+- ' 21 :L y HIGUF1 S J311[ 4,111LE; :_ 0... 'C u,up VV rERB ATH 13.E n'IE CIV UU,IEII"fib 1R.11"Pri: �� A hJ,4"'IF OUT jjj L•'f3'31111VE NEr�.ATCVIE t;a7rdYtlOL CONTROL BLANK SS eh-1 BROTH COG C\J h}�S :A-1 IEllf-10"9'C•I 1� C I � J /. FORM UPDATED; fAPVilI_ 2007 TINE IN ' S INCH9ATOR: IIJI TIIUE IN ` WATER9ATH: L�� TInrE our I/AJ��J�{ !�/y WATER9ATH: ---Il• l l ' L l TEV P61ANr2 of 35- (D- C TfLPEAaT111C Of rf'� �� eiaearoer ;� � •y G TEYPEMTUgG Of1 �.��. s".��� rt'V wnTvwnni: l rviPf�aTurrgof ` WATCrG m % TOTAL SOLIDS (ATaAD SOLIDS ANALYSIS). CALCULATION: MPN Fecal Goliforrn/gram sludge = _ 10 ;c MPN Index Largest Volurne :c % dry solids r CHECKED BY: COPY MADE: CAMP I 'J LINE W'UVTP KrAfiD SLUDGE FECAL PNALYH' Ejff'E IC0LL_IcC U l� D: 7 I TIME COLLECTED: D � S- COLLECTED EilI.:IC:IcuerlL.D IEW: �,� 1 - 2� . '1 TIME:: -----_y-I BATE: �— 0.7 DA,ti EahV�riaL IYILL�- ._ �._— 4 TIME: j� ANALYST: VVI1:`I HCV E�-- -- - 3 HOURS at 35 :�- 0.5'C In INCUBATOR 21 :t 2 HOURS at 44.5 :e 0.2'C; In WAAT5RBATH SAMPLELOCATION -50 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL CA mL 0.010 mL d:G(lfl®. OP POS`I�FII/ES MPU,V10r0 mra!L MPad! GRA M � — 0 /5mL /5mL /5mL /5mL /� v /5mL ( L//5mL /fly /5mL ^�J' /� Z— IS mL maQ�m®err., �arme�n uE alas INCUBATOR; k7�i � �' OtJT lIVCLIEI�TiCsI�6: .- � — 2-I :: 2 CiIOIl.DRS 81ii *d_.;;r__ 0..2-C, tin W dATERD ATH ilE IN WATkFlBATH: u•E OUT 11U:4 d EFS1;1 Vfa Y: Z ——__-.---__—_-- - t:IT3Sll7VE REGIATIVIE —.---------- — — :OiVYn0L CONTROL BLANK SS e!"j IElIFIOT&-a LIDS A--i OFIG-R-1 / FORM UPDATED, AMR[!- 2007 TIME IN ©� INCU9gTOR; ) INCUHA70fl: l ` v TIME IN 1141 WATEflBATH: TINE OUT =crb LPrnwNI -"F 0ATO1F.� TELPmATurtl OF V;LLpATOR TEIIPENATUK OF 11 - j WnTT]W4nl: J TQIPFAAIUIIE OF WsiCTL4T1� /—j-c� `.f4 % TOTAL SOLIDS (ATAD SOLIIIS ANALYSIS). CALCULATION!: MPN Fecal Colifarrn/grarn sludge = 10 x fvlPN Index Largest Volurne x % dry solids CHECKED BY: COPY P/IADE: CAP L LINE WYVTP ATAD SLUDGE FECAL ANALYSU.�,�,') COLLE IU�i��TE Ii; LLlcl(; V`U LU: 1IBUIE COLLECTED: c ti,;'11 L:?IC', 13�('—___L_t l'r -` _ •--------:.. _.. -..1! c•7 IS �_ Ul91LD BY: DX�'XE AN ALYZ ED.- SAMPLE LOCATION —� -o N _ IDAATE: ITIME- 3 HOURS at 35 t 0.5'C In INCUBATOR _ - .21 w 2 HOURS at 44.5 t 0.2"C In WATERBATH '10 mL 1 mL 0.10 mL 0.010 mL '10 mL 1 mL 0.10 mL 0.010 mL O /5mL+ �/ /5mL 0 /5mL /5mL /5mL 0/5mL 0 /5mL 015mL /5mL 0 /5mL j3 C-IOURS. at ;35 --L 0.5'0 ho 111A CCUBATOR _I I DA a C_ I1\9 INCUBATOR: IDXi E OUT INCUBATOR: . -D- . 4 I 21 �L 2 CAG.DQ.➢FgS at 4-4-5 s 0.2'C iin W'NFERB ATU-U IiS.IA-u'E IN W,ATEfiD ATH. StD,4'•u'IE OUT W>ATIERBATH: —la_ �_{ �- - --- - - — POSITIVE C;ONT190L NEGATIVE CONTROL IBLAN/K ---� --� - SS,A-1 BROTH IDS A-1 BROTH TF9 FORM UPDATED: APR11- 2007 TIME IN INCVBATOfl: _ TIME DUT ,Ir��� INCV9ATOR• ,I TIME IN 2i WATERSAT14; O l WATERBATN: 1 TELPPAnN�cG OF `' r\ u�CLVATvic u1GL9ATOR V V TEL�EJ,nNf1G OF / p wnTmlwrn: ��- TPLPFIIANIIE OP ��-a wattrranu % TOTAL SOLIDS (ATAAD SOLIDS AANAAL'1Ys11S) . COMB. Of MfIPa/700 mrof_ IU06� dVQnIf�.A AUB POSIT V ES• CALCULATION: WN Fecal Coliforrvi/gram-=•I1adge to >: Iv1PN Index Largest volui ne a %, dty solids COPY IVIADE:rk—, xY CAMP, LE -LINE WIWTP 11D.,11 U ILA CC' LLIEC Y LL.D- _.1 � � TIME COLLECTED: �®ILL9��, l��E] "; 6111. �. � �l /-.- �ur�v �:]�'-s I DATE: a 4i . l �- I o o�= rffil�'a E d�NjtL` ILLS: 1 L ITtoutr: 3 HOURS at 35 ze 0.5"C In INCUBATOR .21 -t 2 HOURS at 44.5 d: 0.2'C' In WATERBATH SAMPLE LOCJliTdGb\l- ml- 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL --JO D /SmLI 0/5mL 0/5ml- 0/5mL v /5mL 0/5m'L c—') /5mL �/5mL �4�1�fG-a lJ /5 mL /5 mL 3 HOURS at 35 :1- 0.5°0 hu INCUBATOR LWk)�EdN YN-UIEE:ATO- R: - l �1- 01 Sp RE OUTINCLIG3�NTO6t �- -� ✓-II -t 2 HGfl..DF'd:S at {44J.:;; :k Q1.2°rG Bn UIVATERBATH B ti E OU'>r WAYERBAYI-1 --- --- IGIO.51 11VE CONTROL NEGATWE CONTROL_ BLANK SS,.',-1 BROTH PC) 5 IDS 4-1 BROTH TIMEIN � INCN9ATOR: ©� YaD nMe our , 11 (}'ti iNcuearoR• TIME IN � j O WATERBATH: ` IMeouT 0`62-0 WATEfiRATH: revemnnn¢oF u�WOAroM. ✓ revrmnrurteaa: _3�- �� - wcue,�roie — rtvrenn7unevF ! i \ . wnrF3uwna t '.a _ rr�urcnntu�rt of �,��. r wnnrrxm — `}, I� . TOTAL. SOLIDS (ATAD SOLIDS ANALYSIS) . CC3MB' OFPOSMVIE r ME�II'N1U1 mNl_1 'fUdd"dNQnFdd!Jdl9 CALCULATION: ' fVIPN Fecal Cc,li(arm/gram sludge = _ io x nn�r�l index. Largess /olume x %� dry solids FORM UPDATED. APRII- 2007 CHECKED r�Yr,�; ATAD SLUDGE FECAL ANALYS E' �DhTE (COLLIL�:-u`ED:Cl"➢ME COLLECTED EOLL�C o IF;iI_.GEuIYED BY: / [DATE: l C.A. TOOiIBE �D.k'iTEAVV'ALVZEID' � l� .l (a,l� [I'ImE: 3 HOURS at 35 s 0.5'0 In INCUBATOR .21 :t- 2 HOURS at 44.5 t 0.2"C; In W{ATI=RBATH _ _ �„m��s� �m•o�nYn, _ � SAMPLE LOCATION — „110 mil- 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 m COMB, OEL 1111fr�IId/10IA nllalL QIYI''u�uinlllallala POSITIVES —_ --Q�✓L _—_-0/5mL 0/5mL 0/5mL /5mL /5mL /5mL /5mL- (� 15 mL 5mL �3 HORS all ;-35� 0.�`; '0 hn OOW�:UBATOR I_I Im,1 (E IN INI:,Il91E3:rATOR: - -_.l � 14 I D I E OUT INCLIB ATGn: 21 * 2 HOURS at 44.5 :r 0.2'C M W ATERBATH DAME nN VII,IATEFiBATH: GtL D.ri-B'E OUT <fUAY1cK,tF3ATI-1: _ a^ �•� • i ------ POSIME UONYAOL NEGATIVE CONTROL BLANK ;h-1 BROTH ro-a ?0S- M � -b- (0 L6- DGa rA- i ESIFlOYF9 �0� s 1 �/ FORM UPDATED, APF111- 2007 TIME IN 1 I 1 INCU9ATOfl• ` A E IN WATEflBATN: J TIME OUi L i �� WATEflBATH: ` iwemn7r1:e u+wearolr. revrouTurteoF uvaiearo e TFLfFJWT4f1EOF � v�arenunrn: l I�•' �) TELPFJ1arVrtE OF 6<;-�• wsttrwm � ! L 14 % TOTAL SOLIDS (ATAD SOLIDS ANALYSIS). CALCULATION: MPN Fecal Ci:di(Orrn/Ilrarn sludge ___U )x IvlPl�l Index LalgeBl VOILIMe n % dry solids C•1-I0_C;4ED BY:J"" - '' ; ll rC:IPY MADE:'L`�� % AMPLE- ''LINE WVVTP ��``� �� SLUDGEFECAL ANALYS1%,'t'1, MhTE GOLLIEC V`li✓.ICu: - I Z z-:;, TIME COLLECTS®: b 7' Q;OLLI=4�^Tti `IC, fl3'P___y. ;_'.- _J :.I EovIED BY: DATE- l3 - • I ll IWBE. �_ . • >_ �0.1�'XE D"AVVALYZED.- _ 1 �_ a-3 • ��` ; TIME: _ 3 HOURS at 35 tt 0.5'C In INCUBATOR SAMPLE LOCA,TIC6M -50 ml- 1 mL 0.10 mL 0.010 mL .21 :v 2 HOURS at 44.5 t 0.2PC In WdATE-RBATH 10 mL 1 mL 0.10 mL 0:010 mL - COMB. Of lVIG�IId/1tJ0 HroP_ NUIIOVI/Qaff1+t!IAua POSIY V&dI , /S,mL V � /5mL /5mL /5mL V 11 �f / 5mL J5mL /5mL /5mL !(..,,t -•._.... � II II��L1G�' V /5mL /5 mL r_! 3 HOURS at 35 zL, 0_5'C• 6uo INCF9BATOIR IDAa'u E IN INCUBATOR: OdJrINCllg3t�kTC1R:`� 2-II �L 2 HOURS at 44_5 :t 0.2'C un 11VATEIF8BATH D.(VdIE IN WATIERBATIo-I: �r� • 2 3 S—A.'r E OUT VII ATER1BA,'TI I_ —) )L INCUBATCfl• TIME OUr INcumnroH: � I • j 5 f,ATE HBATN: TIME OUT WATEHBATN: ���� j -- POSl01VE (;OtgTnOL NEGATIVE CONTROL BLANK _ SS AA BROTH N7St :a-1 EtROYFI K6 FORM UPDATED: APF ih- 2007 TdP61ATIfK OF mcuearom �� �'�JII idPFnAIUAL I>F UIL118aTOR �,•� (; ..RG l7F WATE WATM TfLPFJNTLA£OF �1 ` WATCrt4Tl• .\!T % TOTAL. SOLIDS (ATAD SOLIDS ANALYSIS). CALCULATION: WN Fecal zJudge 70 x Id1PIV IIICIE)( Largest vniurne )(, dry solids CHECKED LAY:__ COPY I(/IADD— __ CAMP LEI" LINE M('T ° ATAD SLUDGEFECAL A N, LY 0 Via;) DATE GOILLIEfC:II`Il:D: --� �a.�� I TIME COLLECTED: g .7r0 :CDlIIL---`D BY: �_--� _ IDATE:, 14 ITllOUII=: D1,;'aTIE ANALYZED: — � )20 TIME: (),,j'7� pp , i � I- 3 U-IOURS at 35 Y 0.5'G In INCUBATOR — .21 x 2 HOURS at 44.5 * 0.21'C In WAT15RBATH SAMPLE LOCATION M mL 1 mL 0.10 mL 0,010 mL 10 mL 1 mL 0.'10 mL 0,010 mL M1imPIM/100 gin POSATEidEc°. ----- — (i 0 � 0 („� l`�'�-/. �• �— Q /1i � /5mL l / 5mL " /5mL /5mL / 5 mL / 5 mL / 5 mL / 5 mL �oV=mac �u — _ _ —_ /5 mL U /5 mL '�� •, o 3 U-JrGUIRS riff :35 :5-- 0_5°C. uafl M1C:UBATOR IDk a IE 91v INCiUB ATOR: — °} .�JC7.1 ! J D'vi n E OUT INCUBATOR: _—_ � � _97 V - 21 .2L 2 HIG),URc,) at.t1J.G s 0.2°C uw UIWNFEDIBATH DXii"IE YID W XEFIBATH: E OUT WATERfA: TH, TIME IN INCUBATOR: t IV -) ��_g fTIME OUT II ` ,2A INcueATOfl: ` TIME IN fifi WATHflBATH: ME Otrr TERSATI F. -------- -- POST u7VtE GONT110L NEGATOVfE CONTROL BLANK SS J '1 BROTH IDS A B F10TFI ti FORIVI UPDATED: APG-1IL 2007 Tfy PTAa711AL OF /,� �1f TFVPauN�l OF '••Z� � , �� u,aaATOIc J TI]/PEMTUI:C OF �" warETWarn: { I� TfLPFAAnIAE OF �� wanrwnc sue^ -, J" % TOTAL SOLIDS (ATAD SOLILS ANALYSIS). CALCULATION: MPN Fecal Coli(nrm/gmmn sludge — _ - Io r fulPl,1 Inclex Largess Volume x %6 dry solids C•1-IIECKEOCOPY MADE. �f Camp Lejeune, NC 2014 P,T�D Performance Data Date AT AD Train 1 A j T rain 1 u Colifon c, Feed Temp (Gallons) (oC) Temp (oC) Fecal (Mplq) , 10/1 /2014 1_ - 0 - 52.3 I 51.2 i 0/2/2014 0 50.9 i S. 10/3/2014 0 49.8 48.6 10/4/2014 0 48.6 47.5 10/5/2014 0 47.1 45.7 10/6/2014 0-- 45.8 44.7 1017/20141 0 44.8 43.7 1.0 10/8/2014 0 43.8 42.9 10/9/2014 0 43.0 42.1 10/10/2014 0 ..42.3 41.3 10/11/2014 0 42.1 40.8 10/12/2014 0 41.8 40.5 10/13/2014 0 41.2 40.2 10/14/2014 0 41.0 40.5 1.0 10/15/2014 0 40.6 40.7 10/16/2014 0 39.6 40.5 10/17/2014 0 38.6 40.4 10/18/2014 0 38.0 40.4 10/1 0/2014 0 37.1 40.4 10/20/2014 0 36.1 40.3 10/21 /2014 0 35.5 40.4 1.0 10/22/2014 0 34.9 40.4 10/23/2014 0 '33.6 39.5 10/24/2014 10125/2014 10/26/2014 10/27/2014 10/28/2014 10/29/2014 10/30/2014 10/31/2014 TOTAL = 0 969 983 3 Ave = 0 42.1 42.7 1.0 Max = 0 52.3 51.2 1.0 Min = 0 33.6 39.5 1.0 Camp Lejeune, IBC 2014 ATAD Perormance Data Da Date ATAD Train 3 A Train 3 B I Coliform Feed (Gallons) Temp P (oC) Temp P (oC) ! Fecal (MPf�) 10/1 /2014I 0 - I 40.2 I 48.2 10/2/2014 0 45.1 54.3 10/3/2014 13500 49.8 57.6 10/4/20141 18,000 53.7 59.2 I I 10/5/2014I 18,000 57.0 61.8 10/6/2014 11,250 59.9 62.0 10/7/2014 13,500 61.5 62.0 1.0 10/8/2014 13,500 63.1 61.7 10/9/2014 18,000 60.8 61.8 10/10/2014 18,000 50.7 61.5 10/11/2014 18,000 59.0 61.6 10/12/2014 0 64.3 61.2 10/13/2014 0 64.4 59.6 10/14/2014 11,250 60.8 58.6 1.0 10/15/2014 11,250 59.0 58.2 10/16/2014 18,000 56.4 .58.0 10/17/2014 18,000 56.1 57.9 10/18/2014 18,000 57.3 58.0 10/19/2014 11,250 60.3 57.9 10/20/2014 11,250 61.8 57.6 10/21 /2014 11,250 61.7 57.8 1.0 10/22/2014 11,250 60.7 57.5 10/23/2014 11,250 60.5 56.9 10/24/2014 11,250 61.1 56.7 10/25/2014 18,000 57.7 56.8 10/26/2014 18,000 55.9 57.1 10/27/2014 11,250 58.8 57.2 10/28/2014 11,250 60.0 57.7 24.0 10/29/2014 11,250 62.4 58.5 10/30/2014 13,500 60.1 58.9 10/31 /2014 11,250' 60.6 58.9 TOTAL = 380,250 1,811 1,812 27 Ave = 12,266 58.4 58.5 6.8 Max = 18,000 64.4 62.0 24.0 Min = 0 40.2 48.2 1.0 1 Camp Lejeune, NC 2014 AT AD Perforn lance Data ' Date ATAD Train 3 A ( Train 3 E Coliform Feed (Gallons) Temp (oC) Temp (oC) FeCa.I (fkfiPi�} 11/1/201A 13,500 I 60.3 ` 58.9 11/2/2014 13,500 64.3 . 58.1 1 1 /3/2014 1 18,000 I 58.8 58.1 � 11i4/2u 14' l 11,250 I uu. 7 I 59.11 I l i .0 l 11 /5/2014 11,250 62.2 I 59.2 11/6/2014 9,000 60.9 58.8 11/7/2014 9,000 I 62.2 I 58.0 11/8/2014 9,000 62.2 57.0 11./9/2014 9,000 61.4 56.2 11/10/2014 9,000 59.8 55.5 11/11/2014 9,000 59.5 54.9 11/12/2014 9,000 59.5 54.6 24.0 11/13/2014 9,000 57.2 54.4 11/14/2014 9,000 58.1 53.6 11/15/2014 9,000 56.2 52.5 11/16/2014 18,000 51.9 52.8 11/17/2014 0 57.2 53.7 11/18/2014 18,000 56.8 56.8 1.0 11/19/2014 18,000 55.8 56.5 11/20/2014 18,000 53.7 56.2 11 /21 /2014 18, 00Q 55.4 56.1 11/22/2014 18,000 55.6 55.6 11/23/2014 18,000 56.4 56.0 11/24/2014 18,000 56.2 56.8 11/25/2014 18,000 57.4 57.9 1.0 11/26/2014 18,000 57.4 58.3 11/27/2014 13,500 58.1 58.4 11/28/2014 18,000 55.8 58.4_ 11/29/2014 18,000 54.5 58.5 11/30/2014 13,500 57.7 59.2 TOTAL = ' 400,600 1,743 1,700 27 Ave = 13,356 58.1 56.7 6.8 Max = 18,000 64.3 59.2 24.0 P0lin = 0 51.9 52.5 1.0 Camp Lejeune, NIC 2014 ATAD Performance Data Dame ATAD Train 3 A Train 3 B j Coliform reed (Gallons) Temp (OC) Temp (oC) Fecal (N11PNI) 12/1 /2014I 0 I 63.3 59.1 12/2/2014 0 64.7 57.6 1.0 12/3/20141 181000 58.8 57.2 12/4/20i4 13,500 i 57.7 57.8 ` 12/5/2014 18,000 56.7 58.1 12/6/2014 18,000 I 55.9 58.9 12/7/2014 18,000 57.6 59.1 12/8/2014 18,000 I 56.2 58.6 12/9/2014 18,000 55.8 58.4 1.0 12/10/2014 18,000 56.1 58.5 12/11/2014 18,000 56.2 58.6 12/12/2014 18,000 56.7 58.7 12/13/2014 13,500 58.1 58.9 12/14/2014 13,500 58.8 59.6 12/15/2014 13,500 61.9 59.6 12/16/2014 18,000 60.3 60.4 1.0 12/17/2014 18,000 57.4 60.7 12/18/2014 18,000 59.8 63.0 12/19/2014 11,250 63.7 62.6 12/20/2014 .11,250 64.0 61.2 12/21/2014 11,250 63.2 59.6 12/22/2014 18,000 60.4 58.4 12/23/2014 18,000 58.1 58.2 1.0 12/24/2014 18,000 55.2 58.1 12/25/2014 0 57.7 57.4 12/26/2014 18,000 55.8 56.1 12/27/2014 0 55.7 54.5 12/28/2014 18,000 52.9 53.4 12/29/2014 18,000 50.2 52.9 12/30/2014 0 54.4 56.1 1.0 12/31/2014 0 56.3 56.7 TOTAL = 411,750 1,799 1,808 5 Ave = 13,282 58.0 58.3 1.0 Max = 18,000 64.7 63.0 1.0 [Vain = 0 50.2 52.9 1.0 RP LEJEUNE BENCH SCALE ATAD V( TILE'SOLIDS REDUCTMI ANALYSU. START-UP )ATE 10/31 /2014 A B C D E F G H I TOTAL VOLATILE SOLIDS ASH SOLIDS INHOUSE WT OF SAMPLE WT OF WEIGHT % TOTAL WT OF WEIGHT WEIGHT % VOLATILE % VOLATILE SAMPLE ATAD WT OF DISH DISH+WET WEIGHT (g) DISH+DRY (g) SOLIDS DISH+ASH (g) (g) SOLID: WEEKLY SOLIDS TEMP DATE DIGESTION (g) SOLIDS (g) [B-A] SOLIDS (g) [D-A] [(E/C)X100] (g) [G-A] [E-H] [(I/E))C900] AVERAGE REDUCTION 0°C 11/3/2014 I.H. ATAD 73.5577 78.57 5.01 73.6552 0.0975 1.95 73.6059. 0.0482 0.0493 50.56 50.18 20 0.0966 1.93 DUP 75.2333 80.23 5.00 75.3299 75.2818 2818 0.0485 0.0481 4.9.79 {a.. >i - , .v, .. .� .., :.. > ,. r r ,« d .,Y,.«rx, .r „x,r .. ... ,, R .i .. i.i. .r _ .. .. ..R L.2<t�, ., v'.. ✓. _... .,_ .. .. ,,. ✓� d < <� r ., .. ✓.< ... <. ne, ..,..- x .re-:x. -F,; v v r,: r x .. :.r , ..4 a x.... .. r . ., ...x.,tr.., rv.,...x.x. _, .✓ «. « .. � ,s .x.. k'' s _ .. .,.a:Y>.xxtfm 3, r .v"x,..:"�ie.... ..>. ... 4 ... an k`.,-..., .,.3 5 uF < : ¢ < v > n ., x ,. ,.. .. .. .. .x x _,. .,. S> .>, x_t Y.,,,fr br . `i✓s°" � 3 S ,a<r £e to x« ,. . a .. *+ , .. , x- � k .aw.... 'S .., .. .. .3....»v, r.R S .. ....1.t... _. �,�-. ..... «. w-a<« r,- ✓_.<r x„3:'. £,: •x .,5s,_a. rvo $,. k, ys z, rt .<.x".�...x,:x.x- .,. I , . xa _ "hta'- >`Axr, <3 .-- . Y•" , .k t x ,5 .,}<.. - v.. ,,. ,• .-a., r?„ v x a. x., r «,,,.^> < .-. .< _»r..x.....<x. ex.x .> x_, .... .. .a s ., r.x „, x- rx. .,. ..a t,. :: .. FC .. ,✓. -, :" a .. .,,. s.._,.,«. x x. .. S,. ,. � _Y,'.x.k _.,.xxa . r a , x r. .t.t, > .,,✓ x .. `e xx ..x ..�f _a v <. x,..za .. .. .. .... .. ., r .. '•::'•" "":' .a:_ . .... .. ..... .4. 11/7/2014 I.H. ATAD 73.3061 78.31 5.00 73.3985 ' 0.0924 1.85 73.3521 0.046 0.0464 50.22 49.86 0.63 20 DUP 73.8906 78.89 5.00 73.9827 .� 0.09._1 1 84 73.9371 0 0465 0.0456 r• 4 9.� d3 k„ ...,..+. , _ . ... ..: .. ... .... r ..>.... .<x .,. r,et r..e r , r v, , ,, _... a c«, -., s "1 a< ,_. , x, x .. . , o- .>:: m....« . « wt , :.l -n, ... ,-<><> �.:� ,3,:.¢ -<:r. >t ,fin .. .u..a t. �. .rx'a .. a` < ,.° .. ,- - _>< « ,..:.x._r. xx ..... x..$.,<. x, x .>,_.. - r v ... >rt v,xS.x, s . � .., «.fi..< >Et v xw ,, e+. ., .. a k.. ... r . ,«a.>.v.+�,..« to .,.e ... v.axs e, -. x.. ., x;-., ,.rh .o.. e:<„ L _... « t. c.x .r a,,, .. ' r,-„„aI, %r r #£-'v .b: .7--, " « __.. v,:-i;i: �✓k�r<'�•`�,i:�.-`'„ .>r_.., a , s.}'' .1, t-ex_•.v .xw«.: .-.. ..,_.. .x_r.x :°r.,,.t,.L r.> ,.x ., x.ev<.�. ,> . , r sr,t, x,.v,.r_...:...-u. ».r<x :•r.-r�r.x,.x <-,..ex-..,,yw,, xa.:. •, .. .... _. .. .. ,..... `{rr ... .. �`. . x« kmr - �.':tu. ._< r ,. Y a < x • ,r .. t 1 xr.x x .. a*-x .. v� xt':.r . , ., ,..._. «.. r. > vu < x .. ..+✓ , nr .. Fw>x. s,-t, ,v< xx .. 4 u ., x , v ,wr_._ . r rxxi?v - r .. s: 11/14/2014 I.H. ATAD 73.3049 78.30 5.00 73.4008 0.09'59 1.92 73.3534 0.0485 0.0474 49.43 49.56 0.62 20 DUP 74.584 79.58 5.00 74.679 0.09,�0 1.90 74.6318 0.0478 0.0472 xx rt w x x, < ,. r ..... x r .. u.. ,. .. . ..r ..< ..,. ;-i.x..., x xr x.sx ..x .. x v _ �. ..+ .., <_.. s � } •, «„ xYx a, <,r,xks ••.• . i> ... .., r ., ... ..,k .w , r<, ,.r .Y« ,xr x>+v ., et .., . r ., t ,r< ><x -, ,....,., .�-. .,.._ r .. _ <-.x - ,.xY,�,.-.....-, .,.... ,,x.,x.....ro, t>t n., i ,� x,r rx r,•.`•"E+✓e<.<,r_,r..s<.,.«..1"e....:..<t..<«.r,.+..,xzn,,..,a..<i,....,Yx.<rz-..Y.,..axn<..r-<<.,_c_<.,x.e=.z..._»'uiv.`1'»$._..,_.xw,.. sv..._.a.r. _....J>v._.. v,. ,.x ., . ;3•r ;.-••r'_< ri_f ..�vC. .,..... .c ,-rC--... vew...-_,kn_ ,;.: _ _ 11 /21 /2014 I.H. ATAD 73.3615 78.36 - 5.00 73.4815 0.1200 2.40 73.4213 0.0598 0.0602 50.17 52A 5 -5.24 20 DUP 73.5585 78.56 5.00 73.6686 0.1101 2.20 73.609 r 0.0505 0.0596 54.13 F , < ., .n ,.. <........r. t . .. #.i 3 s. Yx ..., i x , ... x <e. ."x, i Y Y i _, ,. z ._. .,.. �' .. « C„ rxv, .. .xx -z,x, ><x., >� .. , , ., xxx� ...__.w. x .. � .wa gg �z..x * Y _.. .._ « x .f i YIi`c RY ...... {^" _ . ,,., . xx.,-•2.n, _ 7 .r n ., x .r r..«..,...x u .... ,. .,_ r . 3; _,... ,. .,- ,. > , < f x e ,,.av r u. "r,< .._a.x > d is r.< x #.° _v,.,.... x 1 ,, m - .,^, «S xJri, v <•,„ - .r< x> t 3 >„v_xw: s,`Jx z>v�t v -n �. •:.:,t xr's>,rt::i='% .. : A . F'a .,x: -., . . 11/29/2014 I.H. ATAD 72.3622 77.36 5.00 72.4707 0.1085 2.17 72.4156 0.0534 0.0551 . 50.78 50.60 2.97 20 DUP 73.8895 78.89 5.00 73.9976 0.10£31 2.16 73.9431 0.0536 0.0545 50.42� .,, a a r r .,. < ✓<x, r rx««„ > .>~. k «xr.> .,, <. ,. . ,.....x.x.✓. .c r .:. _., _a,.wr >. .. . « .,, ✓ ,. 'rc .xr, a . t v.r <+ x., e„} x ..._., z< xr., ...> 3� .. x t. .... J 9 S_ i. 3 3 _h'Y% _ « ,.., ,,. fix. ✓,.,,,�rx za..'i,.c .a v.. ,v ,r.. �,_..,. « .«,, ...<.,s ,. <.,. < x w #✓ , . -, .: x r. ..., .. < ,x. r , ,x. ,, .x< ..x . s, x., t r.. <x -.>rx .rr ...-x. .> - -_ 12/5/2014 I.H. ATAD 74.5830 79.58 5.00 74.6696 0.0866 1.73 74.6261 0.0431 0.0435 50.23 50.14 0.90 20 DUP 86.4499 9.1.45 5.00 86.5366 0.08Ei7 7 1.73 86.4932 0.0433 0.0434 50. OG _ . . > ^s t.. x .. . _ .. �- ..%a<�.-<x.,.,.-.zx.,,_ x_> ... r .. _...., f. _ ., . „w> o ,3 ,.,: >1, .Ic. x_>✓ .<ay. ,> s� v. .. .._ ,rr,., .,, r, . „ , <. x,. _.t .�:z:...><ka�`"•:, _ .,. F. .. .. .3.,,, VOLATILE SOLIDS REDUCTION = INITIAL VS - FINAL VS X 100 INITIAL VS (VSR <15%)