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WQ0011448_Residual Annual Report 2014_20150302
hl-p 6-r-> I / (� �� TOWN OF SNOW HILL 2014 ANNUAL LAND APPLICATION OF RESIDUAL BIO-SOLIDS REPORT CLASS B PROGRAM WQ0011448 Submitted by: Soil Plus 208 Williams Street Greenville, North Carolina 27858 February 2, 2015 r- RECEAVE®1®ENROWR MAR - 2 -2015 wateTauality p®n"fig Section February 2, 2015 NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: 2014 LAND APPLICATION ANNUAL REPORT Town of Snow Hill"Class B" Program NC Permit No.: WQ0011448 Soil Plus Project No. 200804.A10 Information Processing Unit: Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as specified in the above referenced permit for the Town of Snow Hill on behalf of Granville Farms, Inc. Soil Plus compiled this report using data gathered during the compliance year. This data includes (1) certification form, (2) residual sampling, (3) field loading calculations, (4) pathogen and vector attraction reduction documentation, (5) standard soil fertility nutrient analysis. The Town of Snow Hill conducted application events on permitted fields in Greene County during 2014. A total of 19.35 Dry Tons or 195,800 gallons of permitted residual bio-solids were land applied to permitted fields. If there is any further information required or questions regarding this annual report please do not hesitate to contact me or the Town of Snow Hill. (252-935-5994) for further assistance. Respectfully, C. Scott Carpenter, L. . . North Carolina Nutrient Management Planner Joe Roberts, Town of Snow Hill Bryan Smith, Granville Farms 208 Williams Street Greenville, NC 27858 t (252) 917-4288 f (800) 755-7153 www.soilplus.net Town of Snow Hill 2014 Annual Land Application' of Residual Bio-Solids Report WQ0011448 Snow Hill, NC ANNUAL LAND APPLICATION CERTIFICATION FORM Source Summary Field Loading Summary ANNUAL RESIDUAL SAMPLING SUMMARY FORM - Analytical Data TCLP FIELD LOADING SUMMARY FORM Town of Snow HillFarm ANNUAL PATHOGEN & VECTOR ATTRACTION REDUCTION FORM SOIL SAMPLES Town of Snow Hill Farm APPENDIX I CERTIFICATION FORM SUMMARY FORM PermitNumber ANNUAL LAND APPLICATION CERTIFICATION FORM FacilityName Land Application Operator County Phone Number WQ0011448 Year: 2014 Town of Snow Hill Granville Farms, Inc. Greene (252) 939-5051 `Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the V ❑o residuals were handled. Part A - Residuals Application Summary: Total number of application fields in the permit: 3 Total number of fields utilized for land application during the year: 1 -= Total amount of dry tons applied during the year for all application sites: 19.35 Total number of acres utilizes for land application during the year: 12.5 Part B - Annual Compiance Statement: Facility was compliant during calendar year with all conditions of the land application permit? Yes No Including but not limited to items 1-13 below) issued by the Division of Water Quality d❑ ❑© tf no please, provide a written description why'the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites ,?. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory' .results are attached 1. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached i. All other monitoring was`performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached i.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T 17. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilit 3. Allmonitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilitie I. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was . •eceived from the Division of Water Quality 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to Include appropriate actions and remediations. 1. Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. '13. All buffer requirements as specified on the permit were maintained during each application of residuals. ?art C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and :omplete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and mprisonment for knowing violations." / )ennis Liles, Mayor L. 'ermittee Name and Title (type or print): signature of Preparer* if different from Permittee) Signature of Permittee 02/02/2015 Date Signature of Land Applier Date (if different from Permittee) - ' Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)' Monday, February 2, 2015 Source Summary Report WWTPI . Vohirni4plied, Total Dry Tons Town of Snow Hill WVV P 195,800 19.35 �- Total 195,800 19.35 i a 'Monday, February 2, 2015 Page 1 of 1 YEAR TO DATE FIELD LOADING SUMMARY CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2 Field Used Avvlied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used Site# SH 3 Total 12.5 195,800 195,800 19.35 29.87 35.84 Common, 220 13.6% Annual Ryegrass - 50 71.7% Bermudagrass Hay Hay Monday, February 2, 2015 Page 1 of 1 APPENDIX II * RESIDUAL SAMPLING SUMMARY FORM FIELD LOADING CALCULATIONS ANALYTICAL ANNUAL RESIDUAL SAMPLING SUMMARY FORM WQ Permit No. WQ0011448 Facility Name Town of Snow Hill Source Permit No. NC0020842 Laboratory 1 A&L Easter Labs, Inc. Laboratory 2 Sample or CompositeDate 5/27/2014 Parameter (mg/Kg) Class A Clas B Aluminum N/A N/A 12,000 Ammonia Nitrogen N/A N/A 13,900 Arsenic 41 75 4 Cadmium 39 85 2 Calcium N/A N/A 17,800 Copper 1,500 4,300 619 Lead 300 840 44 Magnesium N/A N/A 4,960 Mercury 17 57 3.8 Molybdenum N/A 75 6 Nickel 420 420 34 Nitrate -Nitrite Nitrogen N/A N/A 84 Percent Solids N/A N/A 2.37 pH (no units) N/A N/A 7.74 Phosphorus N/A N/A - 32,300 Potassium N/A N/A 5,460 PAN (Inj./Inc.) N/A N/A 28,174 PAN (Surface) N/A N/A 21,224 Selenium 100 100 5 Sodium N/A N/A 5,490 SAR N/A N/A 1.44 TKN N/A N/A 61,200 Zinc 2,800 7,500 874 Source Name Town of Snow Hill WWTP "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) �� �& AOJN , Facility Town of Snow Hill WWTP Sampling Date 5/27/2014 % Solids 2.37' _ Mineralization Rate 0.3 Gallons per DT 10,118.49 pH 7.74 FIELD LOADING ESTIMATES Sodium Absorpotion 1.44 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply Ratio NITROGEN APPLICATION NUTRIENT APPLICATION TKN (mg/Kg) 61,200 lbs./1,000 gal 12.10 Potassium lbs./1,000 gal 1.08 Ammonia Nitrogen (mg/Kg) 13,900.00 lbs./1,000 gal 2.75 Phosphorus lbs./1,000 gal 6.38 1 Nitrate -Nitrite (mg/Kg) 84.39 lbs./1,000 gal 0.02 Calcium lbs./1,000 gal 3.52 PLANT AVAILABLE NITROGEN SURFACE APPLIED Calcium lbs./1,000 gal 0.98 PAN (mg/Kg) 21,224 lbs./1,000 gal 4.20 Manganese lbs./1,000 gal 0.08 PLANT. AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./1,000 gal 1.79 PAN (mg/Kg) 28;174 lbs./1,000 gal 5.57 Molybdenum lbs./1,000 gal 0.00, Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Limits (mg/Kg) 41 1st Year 2nd Year 3rd Year 4th Year 5th Year Class B Ceiling Limits (mg/Kg) 75 HEAVY METAL CONCENTRATION HEAVY METAL LOADING Arsenic (mg/Kg) 4.00 Arsenic lbs./1,0.00 gal 0.00 Cadmium (mg/Kg) 2.00 Cadmium lbs./1,000 gal 0.00 Copper (mg/Kg) 619.00 Copper lbs./1,000 gal 0.12 Lead (mg/Kg) 44.00 . Lead lbs./1,000 gal 0.01 Mercury (mg/Kg) 3.80 Mercury lbs./1,000 gal 0.00 Nickel (mg/Kg) 34.00 Nickel lbs./1,000 gal 0.01 Selenium (mg/Kg) 5.00 Selenium lbs./1,000 gal 0.00 Zinc (mg/Kg) 874.00 Zinc lbs./1,000 gal 0.17 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen 133,026 PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Y-g) 61,200 21,224 42.45 39,976 61,200 28,174 56.35 33,026 39,976 5,996 11.99 33,979 4,954 9.91 28,072 33,979 2,548 5.10 31,431 28,072 2,105 4.21 25,966 31,431 1,179 2.36 30,252 25,966 974 1.95 24,993 30,252 567 1.13 29,685 24,993 469 0.94 24,524 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Total 31,515 63.03 Total 36,676 73.35 Page: 1 of 2 Report Number: 14-148-0204 Account Number: 04596 - Submitted By: SCOTT CARPENTER Send To: SOIL PLUS, LLC SCOTT CARPENTER P.O. BOX 1396 OXFORD, NC 27565 Lab Number: 55597 Sample Id : SH 052714 A� A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 www aleastemxom Project: 200804.A10-TOWN OF SNOW HILL WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 5/27/2014 11:30:00 Date Received: 05/28/2014 00:00 Date Reported: 06/04/2014 Total Solids " 2.37 23700 100.0 JM 05/28/2014 13:34 SM-2540G Moisture " 97.63 100.0 JM 05/28/2014 13:34 SM-2540G Total Kjeldahl Nitrogen 6.12 61200 10.0 JM 05/29/2014 08:30 SM-4500-NH3C-TKN Total Phosphorus 3.23 32300 100 KM 06/03/2014 13:46 SW 6010C Total Potassium 0.55 5460 100 KM 06/03/2014 13:46 SW 6010C Total Sulfur 0.91 9060 100 KM 06/03/2014 13:46 SW 6010C Total Calcium 1.78 17800 100 KM 06/03/2014 13:46 SW 6010C Total Magnesium 0.50 4960 100 KM 06/03/2014 13:46 SW 6010C Total Sodium 0.55 5490 100 KM 06/03/2014 13:46 SW 6010C Total Iron 44000 100 KM 06/03/2014 13:46 SW 6010C Total Aluminum 12000 100 KM 06/03/2014 13:46 SW 6010C Total Manganese 389 5 KM 06/03/2014 13:46 SW 6010C Total Copper 619 5 KM 06/03/2014 13:46 SW 6010C Total Zinc 874 5 KM 06/03/2014 13:46 SW 6010C Ammonia Nitrogen 1.39 13900 10.0 JM 05/29/2014 08:30 SM-4500-NH3C Organic N 4.73. 47300 10.0 05/29/2014 08:30 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 05/29/2014 08:30 SM-450ONO3F Total Cadmium 2.0 2.0 KM 06/03/2014 13:46 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-148-0204 Account Number: 04596 Submitted By: SCOTT CARPENTER Send To: SOIL PLUS, LLC SCOTT CARPENTER P.O. BOX 1396 OXFORD, NC 27565 Lab Number: 55597 Sample Id : SH 052714 DA&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastern.com Project: 200804.A10-TOWN OF SNOW HILL WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 5/27/2014 11:30:00 Date Received: 05/28/2014 00:00 Date Reported: 06/04/2014 Total Chromium 82 5 KM 06/03/2014 13:46 SW 6010C Total Nickel 34 5 KM 06/03/2014 13:46 SW 6010C Total Lead 44 5 KM 06/03/2014 13:46 SW 6010C Total Arsenic 4.0 3.0 KM 06/03/2014 13:46 SW 6010C Total Mercury 3.8 0.4 KM 05/29/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 06/03/2014 13:46 SW 6010C pH (Standard Units) " 7.74 2.00 JM 05/29/2014 08:30 SW-9045D Total Molybdenum 6 5 KM 06/03/2014 13:46 SW 6010C Soluble Phosphorus 0.34 3400 100 JM 05/29/2014 11:10 SOLUBLE PIN MANURE Comments: WATER SOLUBLE P, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mo". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "AL" AND "As". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Analytical Results Date: Tuesday, June 24, 2014 Client: Microbac Southern Testing Division Client Project: AA50017 & AA50018 Client Sample ID: AA50017 Snow Hill WWTP Work Order/ID: 14E1534-01 Sample Description: Sampled: 05/27/2014 12:00 Matrix: Aqueous Received: 05/30/2014 9:15 Analyses Certs AT Result RL Qua[ Units DF Analyzed Ignitability (Closed Cup) Method: SW-846 1010 Analyst:EB Prep Date/Time:06/06/2014 09:45 Ignitability cgk A i> 170 30 °F 1 1 06/06/2014 9:45 1 pH Method: SW-846 9045C Analyst:EB Prep Date/Time:06/03/2014 14:45 pH cgk I A 117.55 2.00 pH Units 1 1 06/03/2014 14:45 Reactive Cyanide Method: Chapter 7/9014 Prep Method: Aqueous Reactive CN Distillation Analyst:AGRIE Prep Date/Time:06/03/2014 08:30 Reactive Cyanide I cg A_ Ji -.u- ___ND i 2,01 Jrng/L 1 1 06/04/2014 11:45 Reactive Sulfide Method: Chapter 7/9034 Prep Method: Aqueous Reactive Sulfide Distillation Analyst:EB Prep Date/Time:06/03/2014 08:30 Reactive Sulfide cg A 8.5 2.0 mg/L 1 06/03/2014 8:30 Microbac Laboratories, Inc. 250 West 84th Drive I Merrillville, IN 46410 1800.536.8379 p 1219.769.8378 p 1219.769.1664 f I www.microbac.com Page 4 of 10 Lab Report #: L14070156 Lab Project #: 2941.016 Project Name: Wilson NC Lab Contact: Emily Yoak * _ _ Certificate of Analysis f : Sample #: 1-14070156=61- PrePrep Method: Instrument:. HPMS8 • Client ID: AA52511 , Prep Method: 50306/5030C/5035A.. Prep Date:' N/A . Matriz:: TCLP Leach • , Analytical Method:. 82606 Cal Date: 06/24/2014 17:18 Wofkgroup #: WG483538, .: '• "Analyst: TMB . ` RuneDate: 07/10/2014 12:53,:',.. Collect Date: 06/26/2014:00:01 Dilution: 10 File ID: ' 8M398586 Sample:Tag:, DL01 Units: ug/L Analyte Result Qual RL MDL EPA HW# Reg. Limit Benzene U 50.0 1.25 D018 500 Carbon tetrachloride U 50.0 2.50 D019 500 Chlorobenzene U 50.0 1.25 D021 100000 Chloroform U 50.0 1.25 D022 6000 1,2-Dichloroethane U 50.0 2.50 D028 500 1,1-Dichloroethene U 50.0 5.00 D029 700 Methyl Ethyl Ketone U 100 25.0 D035 200000 Tetrachloroethene U 50.0 2.50 D039 700 Trichloroethene U 50.0 2.50 D040 500 Vinyl chloride U 100 2.50 D043 200 Surrogate Recovery Lower Limit Upper Limit Q Dibromofluoromethane 115 86 118 1,2-Dichloroethane-d4 121 80 120 Toluene-d8 106 88 110 4-Bromofluorobenzene 103 86 115 * Surrogate or spike compound out of range U Not detected at or above adjusted sample detection limit ( .' •Sample#: 1-14070156-01 PrePrep Method: Instrument: HPMS12 . , Client ID: AA52511 , _Prep Method: 3510C . Prep Date: 07/09/2014 13:45 - Matrix:, .TCLP Leach Analytical Method: 8276C Cal Date: 06/19/201412:39 Workgroup #: WG483545 , . • . Analyst: - CAA Run Date:. I 07/10/2014 15:28 Collect Date: 06/26/2014 00:01 ::Dilution: 1 File_ ID: 12M49662 j Sample Tag: 01• Uriits:. ug/L Analyte Result Qual RL MDL EPA HW# Reg. Limit o-Cresol U 50.0 25.0 D023 200000 m-,p-Cresol U 50.0 25.0 D025 200000 1,4-Dichlorobenzene U 50.0 25.0 D027 7500 2,4-Dinitrotoluene U 50.0 25.0 D030 130 .Hexachlorobenzene U 50.0 25.0 D032 130 Hexachlorobutadiene U 50.0 25.0 D033 500 Page 1 of 2 Generated at Jul 14, 2014 14:33 Page 9 14070156 / Revision: 0 / 17 total pages Generated: 07/14/2014 14:34 Lab Report #: L14070156 Lab Project #: 2941.016 Project Name: Wilson NC Lab Contact: Emily Yoak Certificate of Analysis Analyte Result Qual RL MDL EPA.HW# Reg. Limit Hexachloroethane U 50.0 25.0 D034 3000 Nitrobenzene U 50.0 25.0 D036 2000 Pentachlorophenol U 250 125 D037 100000 Pyridine U 250 125 D038 5000 2,4,5-Trichlorophenol U 50.0 25.0 D041 400000 2,4,6 Trichlorophenol U 50.0 25.0 D042 2000 Surrogate Recovery Lower Limit Upper Limit Q 2-Fluorophenol 65.3 21 100 i ' Phenol-d5 41.5 10 94 Nitrobenzene-d5 102 35 114 i 2-Fluorobiphenyl 96.5 43 116 2,4,6-Tribromophenol 121 10 123 p-Terpheny1-d14 110 33 141 U Not detected at or above adjusted sample detection limit Sample #: L14070156r01 PrePrep Method: Instrument:. HP17 ' Client ID: AA52511 I' Prep Method: METHOD-:' '; Prep'Date: ; 07/08/201415:45 Matrix: TCLP Leach Analytical, Method 8151A Cal Date: 07/11/201417:34 Workgroup #: WG483601 Analyst: ECL Run Date: 07/11/2014 21:04 -:Collect Date: 06/26/2014 00:01 Dilution: 1 : 011013: 17G17462.F Sample Tag:.01 Units- ug/L Analyte Result Qual RL MDL EPA HW# Reg. Limit 2,4-D U 20.0 5.00 D016 10000 1 2,4,5-TP (Silvex) U 2.00 0.500 D017 1000 Surrogate Recovery Lower Limit Upper Limit Q 2,4-Dichlorophenylacetic acid 46.3 20 144 U Not detected at or above adjusted sample detection limit Page 2of2 Generated at Jul 14, 2014 14:33 Page 10 .4070156 / Revision: 0 / 17 total pages Generated: 07/14/2014 14:34 APPENDIX III t FIELD LOADING SUMMARY FORM r i PermitNumber WQ0011448 Facility Name Town of Snow Hill LandOwner Town of Snow Hill Operator ANNUAL LAND APPLICATION FIELD SUMMARY FORM Site# SH County Greene Crop 1 Common Bermudagrass Hay Field Name 3 SoilSeries N/A Crop 1 Pan 220 Acres Permited 12.50 Soil Abbrevation: Crop 2 Annual Ryegrass - Hay Crop 2 Pan 50 Volume Acres Dry Soil Application Total Nitrate- Crop 1 Crop 2 Date Measurement Applied % Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop 04/02/2014 Gallons . 89,000 2.37 12.50 0.70 8.80 Town of Snow Hill WWTP Moist 0 Surface 45.46 0.50 0.3 61,200 13,900.00 84.39 29.87 Crop 1 12/04/2014 Gallons 106,800 2.37 12.50 0.84 10.55 Town of Snow Hill WWTP Moist 0 Surface 54.55 0.50 0.3 61,200 13,900.00 84.39 35.84 Crop 2 Total Volume Applied 195,800 Total Dry Tons 19.35 Sum Total P 100.00 Total 29.87 35.84 Total Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2 PAN PAN Current Year 0.012 0.006 1.916 0.254 0.136 0.012 0.019, 0.105 0.015 2.706 (lbs./Ac.) (lbs./Ac.) (T/Date Prior Year 0.132 0.050 17.577 1.765 1.235 0.116 0.184 0.744 0.176 24.659 Lime Ac.) Cumulative Total 0.144 0.056 19.494 2.019 1.371 0.128 0.203 0.849 0.191 27.365 Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 094--c=- 02/02/2015 *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4 Signature of Land Applier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate 5 APPENDIX IV PATHOGEN AND VECTOR VERIFICATION ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Town of Snow Hill WQ Permit Number: WQ0011448 WWTP Name: Town of Snow Hill WWI'P NPEDS Number: NCO020842 " Monitoring Period: 01/01/2014 to 12/31/2014 Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed: "Class A" Alternative: Not Applicable If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": ]"Class B" Alternative: Alternative 1 If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Fecal Coliform Minimum Colonies Per Gram of Total Solids(Dry 29,353 Weight) Analytical Technique SM 9221 E Geo. Mean 51,571 Not Applicable Not Applicable Maximum # of Exceedences Frequency 74,300 0 Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 3 (30-day bench) 1 Sample Type Grab Samples "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32,and the vector attraction reduction requirement in 40 CFR 503.33 have been met." 4 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) , "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Joe Roberts, ORC J. Bryan Smith Operator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) " 02/02/2015 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) f Monday, February 2, 2015 PROMPT- A CC U RATE -RE LIABLE LABORATORIES., INC 1 WWIV.PARLABS.00Nl REPORT OF ANALYSES Attn: SCOTT CARPENTER ,SOIL PLUS 208 WILLIAMS STREET GREENVILLE, NC 27858- SAMPLE NUMBER- 114098 SAMPLE ID- SH052714 DATE SAMPLED- 05/27/14 DATE RECEIVED- 05/28/14 SAMPLER- SC TIME RECEIVED- 1000 DELIVERED BY -'UPS Page 1 of 1 PROJECT NAME: MAY 14 DATE: 07/07/14 SAMPLE MATRIX- SO TIME SAMPLED- 1130 RECEIVED BY- DJ TYPE SAMPLE- Grab ANALYSIS ANALYSIS METHOD DATE TINE BY RESULT UNITS 30 DAY BENCH SCALE TEST VAR 05/29/14 RE ATTACHED FECAL COLIFORM (GEOM. MEAN) SM 9221 E 05/29/14 RE ATTACHED MPN/g LABORATORY DIRECTOR A.O. Box 411483 • Charlotte, NC 28241-1483 Alione: (704) 588-8333 • Fax: (704) 588-8335 RA } PROMPT -ACCURATE- R ELIAS LE LABORATORIES, INC WWW.PA,RLABS.CnM 30 ®ay Bench Scale Extended Aeration Test Percent Volatile Solids Reduction SOIL PLUS SH052714 W® 114098 05/29/14 e a 06/26/14 Start: End: TS 0.2336 0.2199 TS% 1.80% 1.80% VS 0.1518 0.1426 VS% 64.98% 64.85% yIN 0.004577 OUT 0.00440045 FSVR (Mass Balance) 3.85% FSVR (Van Kleeck) 0.59% FSVR Mass Balance) <15% YES FSVR (Van Kleeck) <15% YES I :O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Pax: (704) 588-8335 a AM P/A FZ PROMPT- ACOUP.A-rE:-RELIAC3LE 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 ® SOIL PLUS SHOS2714 05/27/14 FECAL COLIFORM, GEOMETRIC MEAN SM 9221 E 114098 1 1,827 2.46% 74,299.91 2 711 2.42% 29,352.99 3 1,442 2.50% 57,678.44 4 1,162 2.44% 47,643.05 5 1,326 2.43% 54,557.92 6 1,217 2.47% 49,267.82 7 1,481 2.46% 60,222.82 Fee -all 0011fom Gen.�mel�a'� I APPENDIX V SOIL SAMPLES I- NGuA&La Agronomic Division - - - - - - - - Pnone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ - J Report No. FY15-SL019198 Client: Granville Farms Advisor: Scott Carpenter Predictive PO Box 1396 Soil Plus LLC 8220 NC Hwy 96 208 Williams St. Soil Report Mehlich-3 Extraction Oxford, NC 27565 Greenville, NC 27858 Sampled County: Greene Sampled: 12/11/2008 Received: 11/21/2014 completed: 01/09/2015 Farm: SH Links to Helpful Information Sample ID: 3 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Bermuda hay/past., M 0.4 180-220 0 200 0 20 0 0 0 0 Note: 12 2- Small Grain (SG) 0.0 80-100 0 110 0 20 0 0 0 0 Note: 3 Test Results [units - W/V in g/ 0; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-I Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.32 1.25 3.1 64 1.1 5.6 193 17 46 16 25 34 37 30 213 213 231 0.1 3 North Carol ina r.P - Tobacco Ti u%t Fuad Cirmitiissluro Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture