WQ0011244_Residual Annual Report 2014_20150302

CITY OF OXFORD, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit. No. WQ0011244
2014 ANNUAL REPORT

City of Oxford, NC
Residuals Land Application Program
2014 Annual Report
TABLE OF CONTENTS
1. Certification Form, Annual Operations Summary, Facility and
Land Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil, pH & Lime Application Records
7. Soil Analyses

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00011244 County Granville Year 2014
Facility Name (as shown on permit) City of Oxford WWTP NPDES No. NC0025054
Land Application Operator Synasro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A— Residuals Application Summary:
Total number of application fields in the permit: 27
Total number of fields utilized for land application during the year: 4
Total amount of dry tons applied during the year for all application sites: 524.56
Total number of acres utilized for land application during the year: 145.3
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. 1
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Randall Heman. City Manager
.P-o*tteeName and Title ( e or pr nt)
Signature of Prepar r* Date
(if different from P ' ittee)
9 n e i Date
DEB Fly20i �
ignature of Land Applier Date
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
OXFORD, NC
OXFORD, NC AEROB. DIGESTED LIQUID
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
July 2014
520,800.00 G
99.47
D
August 2014
2,225,800.00 G
425.09
D
YEARLY TOTAL
2,746,600.00 G
524.56
D
61
DRY METRIC
TONS
90.22
385.55
475.77
1 /30/2015

2014 ANNUAL REPORT
PROJECT: Oxford WWTP
FACILITY: Oxford WWTP
1649 New Commerce Drive
Oxford, NC 27565
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
NCO025054
Amy Ratliff, City Engineer
City of Oxford
P.O. Box 1307
Oxford, NC 27565
919-603-1104
Dennis Wilson
WWTP Supervisor
1649 New Commerce Drive
Oxford, NC 27565
919-693-8783
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0011244
Facility Name: OXFORD, NC'
NPDES# : NCO025054
or_WQ# (residual only)
WWTP Name: OXFORD
Residuals Analysis Data
Laboratory
A&L Eastern Laboratories Inc.
Product Type
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
Date Sampled (grab) or 06./02/14
10/22/14
11/10/14
12/02/14
Date Composited
Percent Solids
4.58
3.76
4.09
5.01
PARAMETERS (mg/kg dry weight)
Arsenic
4
4
4
4
Cadmium
<2
<2
<2
<2
Mercury
0.4
0.6
0.7
<0.4
Chromium
89
55
71
98
Copper
378
328
380
314
Lead
19
18
22
16
Molybdenum
6
<5,
6
5
Nickel
30
12
19
33
Selenium
6
<5
5
<5
Zinc
1500
1420
1600
1370
Total Phosphorus
19400
15900
17700
15400
7KN
33200
51900
43800
35500
Ammonia -Nitrogen
7420
16000
14200
7390
Nitrate and Nitrite
30.6
205
41.6
<2
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date
(SIGNATURE OF PREPP,rRER)
DENR FORM RSSF (5/2003) Printed: Friday - January 30, 2015 at 16:25:21 for: 2049 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0011244
Facility Name: OXFORD, NC
NPD,ES# : NCO025054
or WQ# (residual only)
WWTP Name: OXFORD
Residuals Analysis Data
Laboratory
A&L Eastern Laboratories Inc.
Product Type
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
Date Sampled (grab) or 06/02/14
10/22/14
11/10/14
12/02/14
Date Composited
Percent Solids
4.58
3.76
4.09
5.01
PARAMETERS (mg/kg dry weight)
Aluminum
59000
65200
68800
57500
Calcium
14200
11600
12900
10500
Magnesium
4580
2630
3130
3400
pH
7.31
7.74
7.51
7.77
Potassium
2470
1880
2090
2150
Sodium
2330
406
2220
1930
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
L
�d
GNATURE OF PRE
NR - Data Not Reported or Data Not Required
Date ;�17
DENR FORM RSSF-B (7/2002) Printed: Friday - January 30, 2015 at 16:25:43 for: 2049 01

Page: 1 of 2
Report Number: 14-157-0204
Account Number: 46478
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL/OXFORD
MARY BREWER
284 BOGER' RD
MOCKSVILLE , NC 27028
Lab Number : 55810
Sample Id : OXFORD WWTP
@-P,A&L Eastern Laboratories, Inc..
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern.conn
Project: OXFORD WWTP
NC CERT # 257
REPORT OF ANALYSIS Date Sampled: 6/2/2014 08:00:00
Date Received: 06/06/2014 00:00
Date Reported: 06/12/2014
Total Solids *
4.58
45800
100.0
JM
06/06/2014 14:30
SM-254OG
Moisture *
95.42
100.0
JM
06/06/2014 14:30
SM-2540G
Total Kjeldahl Nitrogen
3.32
33200
10.0
JM
06/09/2014 08:19
SM-4500-NH3C-TKN
Total Phosphorus
1.94
19400
100
KM
06/11/2014 10:06
SW 6010C
Total Potassium
0.25
2470
100
KM
06/11/2014 10:06
SW 6010C
Total Sulfur
0.74
7410
100
KM
06/11/2014 10:06
SW 6010C
Total Calcium
1.42
14200
100
KM
06/11/2014 10:06
SW 6010C
Total Magnesium
0.46
4580
100
KM
06/11/2014 10:06
SW 6010C
Total Sodium
0.23
2330
100
KM
06/11/2014 10:06
SW 6010C
Total Iron
25700
100
KM
06/11/2014 10:06
SW 6010C
Total Aluminum
59000
100
KM
06/11/2014 10:06
SW 6010C
Total Manganese
621
5
KM
06/11/2014 10:06
SW 6010C
Total Copper
378
5
KM
06/11/2014 10:06
SW 6010C
Total Zinc
1500
5
KM
06/11/2014 10:06
SW 6010C
Ammonia Nitrogen
0.74
7420
10.0
JM
06/09/2014 08:19
SM-4500-NH3C
Organic N
2.58
25780
10.0
06/09/2014 08:19
CALCULATION
Nitrate+Nitrite-N
30.6
2.00
JM
06/09/2014 08:20
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
06/11/2014 10:06
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of,2
Report Number: 14-157-0204
Account Number: 46478
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL/OXFORD
MARY BREWER
284 BOGER RD
MOCKSVILLE , NC,27028
Lab Number: 55810
Sample Id : OXFORD WWTP
@L A&L Eastern Laboratories, Inc._
7621.Whitepine Road Richmond, Virginia 2323T (804) 743.9,401 Fax [phone],946
wwwaleastera.;
Project: OXFORD WWTP
NC CERT # 257
REPORT OF ANALYSIS Date Sampled: 6/2/2014 08:00:00
Date Received: 06/06/2014 00:00
Date Reported: 06/12/2014
Total Chromium
89
5
KM
06/11/2014 10:06
SW 6010C
Total Nickel
30
5
KM
06/11/2014 10:06
SW 6010C
Total Lead
19
5
KM
06/11/2014 10:06
SW 6010C
Total Arsenic
4.0
3.0
KM
06/11/2014 10:06
SW 6010C
Total Mercury
0.4
0.4
JM
06/09/2014 10:30
SW-7471 B
Total Selenium
6.0
5.0
KM
06/11/2014 10:06
SW 6010C
pH (Standard Units) *
7.31
2.00
JM
06/09/2014 08:19
SW-9045D
Total Molybdenum
6
5
KM
06/11/2014 10:06
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca" AND "Se". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in,any advertising, news release, or other public announcements without obtaining our prior written authorization.
4
Debbie Holt

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Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2049-01-AEDLIQ-NC OXFORD, NC AEROB. DIGESTED LIQUID 6/2/2014 7/1/2014-9/30/2014 0.9280
Na mg/I = (Na mg/kg x % Solids) = 100 = (2330 x 4.5800) = 100 = 106.714
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (14200 x 4.5800) _ 100 = 650.36
Mg mg/I = (mg mg/kg x % Solids) = 100 = (4580 x 4.5800) _ 100 = 209.764
Na meq = Na mg/I _ Molec.Wgt.Na = 106.714 _ 23 = 4.63974
Ca meq = Ca mg/I = Molec.Wgt.Ca = 650.36 = 20 = 32.518
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 209.764 _ 12 = 17.4803
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.63974 + SgrRoot[0.5(32.518+17.4803)] = 0.927963
Printed: 1/30/2015
Page 1 16:29

Page: 1 of 2
Report Number: 14-296-0213
Account Number: 46478
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL/OXFORD
MARY BREWER
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58322
Sample Id: OXFORD WWTP
A� A&L Eastern Laboratories, Inc.
v
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271-W6
www.aleastern.com
Project: OXFORD WWTP
NC CERT#257 .
REPORT OPANALYSIS Date Sampled: 10/22/2014 11:30:00
Date Received: 10/23/2014 00:00
Date Reported: 10/29/2014
Total Solids
3.76
37600
100.0
JM
10/23/2014 14:44
SM-254OG
Moisture *
96.24
100.0
JM
10/23/2014 14:44
SM-2540G
Total Kjeldahl Nitrogen
5.19
51900
10.0
JM
10/27/2014 08:55
SM-4500-NH3C-TKN
Total Phosphorus
1.59
15900
100
KM
10/24/2014 13:19
SW 6010C
Total Potassium
0.19
1880
100
KM
10/24/2014 13:19
SW 6010C
Total Sulfur
0.79
7900
100
KM
10/24/2014 13:19
SW 6010C
Total Calcium
1.16
11600
100
KM
10/24/2014 13:19
SW 6010C
Total Magnesium
0.26
2630
100
KM
10/24/2014 13:19
SW 6010C
Total Sodium
0.04
406
100
KM
10/24/2014 13:19
SW 6010C
Total Iron
13600
100
KM
10/24/2014 13:19
SW 6010C
Total Aluminum
65200
100
KM
10/24/2014 13:19
SW 6010C
Total Manganese
470
5
KM
10/24/2014 13:19
SW 6010C
Total Copper
328
5
KM
10/24/2014 13:19
SW 6010C
Total Zinc
1420
5
KM
10/24/2014 13:19
SW 6010C
Ammonia Nitrogen
1.60
16000
10.0
JM
10/24/2014 09:00
SM-4500-NH3C
Organic N
3.59
35900
10.0
10/24/2014 09:00
CALCULATION
Nitrate+Nitrite-N
205
2.00
JM
10/27/2014 08:30
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
10/24/2014 13:19
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
9
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-296-0213
Account Number: 46478
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL/OXFORD
MARY BREWER
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58322
Sample Id : OXFORD WWTP
A&L Eastern Laboratories, Inc.
99. 7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwalegstern.com
Project: OXFORD WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 10/22/2014 11:30:00
Date Received: 10/23/2014 00:00
Date Reported: 10/29/2014
Total Chromium
55
5
KM
10/24/2014 13:19
SW 6010C
Total Nickel
12
5
KM
10/24/2014 13:19
SW 6010C
Total Lead
18
5
KM
10/24/2014 13:19
SW 6010C
Total Arsenic
4.0
3.0
KM
10/24/2014 13:19
SW 6010C
Total Mercury
0.6
0.4
KM
10/24/2014 11:15
SW-7471 B
Total Selenium
<5.0
5.0
KM
10/24/2014 13:19
SW 6010C
pH (Standard Units) "
7.74
2.00
JM
10/24/2014 09:00
SW-9045D
Total Molybdenum
<5
5
KM
10/24/2014 13:19
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2049-01-AEDLIQ-NC OXFORD, NC AEROB. DIGESTED LIQUID 10/22/2014 / / - / / 0.1712
Na mg/I = (Na mg/kg x % Solids) = 100 = (406 x 3.7600) = 100 = 15.2656
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (11600 x 3.7600) =100 = 436.16
Mg mg/I = (mg mg/kg x % Solids) + 100 = (2630 x 3.7600) + 100 = 98.888
Na meq = Na mg/I + Molec.Wgt.Na = 15.2656 = 23 = 0.663722
Ca meq = Ca mg/I = Molec.Wgt.Ca = 436.16 = 20 = 21.808
Mg meq = Mg mg/I + Molec.Wgt.Mg = 98.888 = 12 = 8.24067
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.663722 + SgrRoot[0.5(21.808+8.24067)] = 0.171233
Printed: 1 /30/2015
Page-1 16:29

Page: 1 of 2
Report Number: 14-315-0201 A&L Eastern Laboratories Inc.
Account Number: 46478 @D 7621 WhitepineRoad Richmond, Virginia-23237 (804)'743-9401, Fax(804)271-W6
Submitted By: NATE ROTH wwwaleasternxom
Send To: SYNAGRO CENTRAL/OXFORD Project: OXFORD WWTP
MARY BREWER NC CERT#257
284 BOGER RD
MOCKSVILLE , NC 27028
` REPORT OFANALYSM Date Sampled: 11/10/2014 10:30:00
Lab Number: 58589 Date Received: 11/11/2014 00:00
Sample Id: OXFORD WWTP Date Reported: 11/14/2014
Total Solids *
4.09
40900
100.0
JM
11/11/2014 15:15
5M-1b4uU
Moisture
95.91
100.0
JM
11/11/201415:15
SM-2540G
Total Kjeldahl Nitrogen
4.38
43800
10.0
JM
11/12/2014 08:55
SM-4500-NH3C-TKN
Total Phosphorus
1.77
17700
100
KM
11/12/2014 12:22
SW 6010C
Total Potassium
0.21
2090
100
KM
11/12/2014 12:22
SW 6010C
Total Sulfur
0.82
8240
100
KM
11/12/2014 12:22
SW 6010C
Total Calcium
1.29
12900
100
KM
11/12/2014 12:22
SW 6010C
Total Magnesium
0.31
3130
100
KM
11/12/2014 12:22
SW 6010C
Total Sodium
0.22
2220
100
KM
11/12/2014 12:22
SW 6010C
Total Iron
18200
100
KM
11/12/2014 12:22
SW 6010C
Total Aluminum
68800
100
KM
11/12/2014 12:22
SW 6010C
Total Manganese
572
5
KM
11/12/2014 12:22
SW 6010C
Total Copper
380
5
KM
11/12/2014 12:22
SW 6010C
Total Zinc
1600
5
KM
11/12/2014 12:22
SW 6010C
Ammonia Nitrogen
1.42
14200
10.0
JM
11/12/2014 09:35
SM-4500-NH3C
Organic N
2.96
29600
10.0
11/12/2014 08:55
CALCULATION
Nitrate+Nitrite-N
41.6
2.00
JM
11/12/2014 09:05
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
11/12/2014 12:22
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. lm�dg
Our re Ports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-315-0201
Account Number: 46478
Submitted By: NATE ROTH
Send To: SYNAGRO CENTRAL/OXFORD
MARY BREWER
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58589
Sample Id: OXFORD WWTP
A&L Eastern Laboratories, Inc.
99. 7621 Whitepine Road Richmond, Virginia 23237 (804)'743.9401 Fax [phone]
www.aleastern.com
Project: OXFORD WWTP
NC CERT#257
REPORT OFANALYSIS Date Sampled: 11/10/2014 10:30:00
Date Received: 11/11/2014 00:00
Date Reported: 11/14/2014
Total Chromium
71
5
KM
11/12/2014 12:22
SW 6010C
Total Nickel
19
5
KM
11/12/2014 12:22
SW 6010C
Total Lead
22
5
KM
11/12/2014 12:22
SW 6010C
Total Arsenic
4.0
3.0
KM
11/12/2014 12:22
SW 6010C
Total Mercury
0.7
0.4
KM
11/13/2014 09:00
SW-7471 B
Total Selenium
5.0
5.0
KM
11/12/2014 12:22
SW 6010C
pH (Standard Units) *
7.51
2.00
JM
11/12/2014 09:04
SW-9045D
Total Volatile Solids
55.08 550800
100.0
JM
11/11/2014 15:15
SM-2540G
Total Molybdenum
6
5
KM
11/12/2014 12:22
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
ReportRange
Ratio
2049-01-AEDLIQ-NC
OXFORD, NC AEROB. DIGESTED LIQUID
11/10/2014
/ I - I l
0.9172
Na mg/1= (Na mg/kg x % Solids) = 100 = (2220 x 4.0900) _ 100 = 90.798
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (12900 x 4.0900) =100 = 527.61
Mg mg/1= (mg mg/kg x % Solids) = 100 = (3130 x 4.0900) =100 = 128.017
Na meq = Na mg/l - Molec.Wgt.Na = 90.798 = 23 = 3.94774
Ca meq = Ca mg/1= Molec.Wgt.Ca = 527.61 = 20 = 26.3805
Mg meq = Mg mg/1= Molec.Wgt.Mg = 128.017 = 12 = 10.6681
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.94774 = SgrRoot[0.5(26.3805+10.6681)] = 0.917229
Printed: 1 /30/2015
Page 1 16:29

Page: 1 of 2
Report Number: •14-337-0201
Account Number: ' 46478
Submitted By: NATE ROTH
Send To: SYNAGRO CENTRAL/OXFORD
MARY BREWER
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 59016
Sample Id: OXFORD WWTP
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804), 743 9401 Fax [phone]
Wwwaleastern.com
Project: OXFORD WWTP
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 12/2/2014 10:30:00
Date Received: 12/03/2014 00:00
Date Reported: 12/09/2014
Total Solids *
5.01
50100
1.00.0
JM
12/03/2014 13:45
SM-254OG
Moisture *
94.99
100.0
JM
12/03/2014 13:45
SM-2540G
Total Kjeldahl Nitrogen
3.55
35500
10.0
JM
12/04/2014 08:30
SM-4500-NH3C-TKN
Total Phosphorus
1.54
15400
100
KM
12/04/2014 12:03
SW 6010C
Total Potassium
0.22
2150
100
KM
12/04/2014 12:03
SW 6010C
Total Sulfur
0.67
6710
100
KM
12/04/2014 12:03
SW 6010C
Total Calcium
1.05
10500
100
KM
12/04/2014 12:03
SW 6010C
Total Magnesium
0.34
3400
100
KM
12/04/2014 12:03
SW 6010C
Total Sodium
0.19
1930
100
KM
12/04/2014 12:03
SW 6010C
Total Iron
19200
100
KM
12/04/2014 12:03
SW 6010C
Total Aluminum
57500
100
KM
12/04/2014 12:03
SW 6010C
Total Manganese
527
5
KM
12/04/2014 12:03
SW 6010C
Total Copper
314
5
KM
12/04/2014 12:03
SW 6010C
Total Zinc
1370
5
KM
12/04/2014 12:03
SW 6010C
Ammonia Nitrogen
0.74
7390
10.0
JM
12/04/2014 08:30
SM-4500-NH3C
Organic N
2.81
28110
10.0
12/04/2014 08:30
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
12/04/2014 08:30
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
12/04/2014 12:03
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-337-0201
Account Number: 46478
Submitted By: NATE ROTH
Send To: SYNAGRO CENTRAL/OXFORD
MARY BREWER
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 59016
Sample Id: OXFORD WWTP
V
A&L Eastern Laboratories Inc.
7621 Whitepine Road, Richmond, Virginia 23237 [phone] Fax [phone]
www,aleastern.com
Project: OXFORD WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 12/2/2014 10:30:00
Date Received: 12/03/2014 00:00
Date Reported: 12/09/2014
Total Chromium
98
5
KM
12/04/2014 12:03
SW 6010C
Total Nickel
33
5
KM
12/04/2014 12:03
SW 6010C
Total Lead
16
5
KM
12/04/2014 12:03
SW 6010C
Total Arsenic
4.0
3.0
KM
12/04/2014 12:03
SW 6010C
Total Mercury
<0.4
0.4
KM
12/05/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
12/04/2014 12:03
SW 6010C
pH (Standard Units) *
7.77
2.00
JM
12/04/2014 08:30
SW-9045D
Total Molybdenum
5
5
KM
12/04/2014 12:03
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2049-01-AEDLIQ-NC OXFORD, NC AEROB. DIGESTED LIQUID 12/2/2014 10/112014-12/31/2014 0.9343
Na mg/I = (Na mg/kg x % Solids) + 100 = (1930 x 5.0100) .= 100 = 96.693
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (10500 x 5.0100) = 100 = 526.05
Mg mg/1 = (mg mg/kg x % Solids) _ 100 = (3400 x 5.0100) _ 100 = 170.34
Na meq = Na mg/I = Molec.Wgt.Na = 96.693 = 23 = 4.20404
Ca meq = Ca mg/1 = Molec.Wgt.Ca = 526.05 _ 20 = 26.3025
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 170.34 _ 12 = 14.195
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.20404 _ SgrRoot[0.5(26.3025+14.195)] = 0.934261
Printed: 1/30/2015
Page 1 16:30

FACILITY NAME: OXFORD, NC
OWNER: HENRY THORPE
SITE #: NC GR 00001 FIELD# : GR 00001 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00011244 ANNUAL DRY TONS APPLIED: 197.75
OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 46.10 ACRES PERMITTED: 46.10
Page
Liue Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
7/24/14
31,000.00 (G)
672.451
4.58
0.128
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
7/29/14
148,800.00 (G)
3227.766
4.58
0.616
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
7/30114
179,800.00 (G)
3900.217
4.58
0.745
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
7/31/14
161,200.00 (G)
3496.746
4.58
0.668
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
Jul-14
1 520,800.00 (G)
11,297.180
8/4/14
155,000.00 (G)
3362.256
4.58
0.642
OXAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
I FESCUE
8/5/14
148,800.00 (G)
3227.766
4.58
0.616
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
I FESCUE
8/6/14
124,000.00 (G)
2689.805
4.58
0.514
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
8/7/14
68,200.00 (G)
1479.393
4.58
0.283
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
I FESCUE
8/8/14
18,600.00 (G)
403.471
4.58
0.077
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
Aug-14
514,600.00 (G)
11,162.691
1

FACILITY NAME: OXFORD, NC
OWNER: HENRY THORPE
SITE #: NC GR 00001 FIELD# : GR 00001 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00011244 ANNUAL DRY TONS APPLIED: 197.75
OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 46.10 ACRES PERMITTED: 46.10
Page : 2
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method ,
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Total Gallons/Ac: 22,459.87
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.034
0.017
0.764
3.243
0.163
0.003
0.051
0.257
0.051
12.869
166.43
98
Cumulative lbs/acre
0.089
0.056
2.114
12.056
1.210
0.019
0.388
0.634
0.522
80.716
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
. w
S�' o�.
}, pa„�'..
��
vA3'�^`�: r3
t x �
vl;.�✓'+,. '"„&;.".:`:'.+.
,'7,.
�i>
`rfPo.n,i
158
FD Cumulative Pollutant LoadingRate Limit (lbs/acre)
( )
36.6
34.8
1339.0
267.9
15.0 375.0
'
89.0
j =
2500 0
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: OXFORD, NC PREDOMINANT SOIL SERIES: LIGNUM
OWNER: JOHN WILLIFORD PERMIT #: W00011244 ANNUAL DRY TONS APPLIED: 81.70
SITE #: NC GR 00003 FIELD# : GR 00003 0001 OPERATOR: JOHN WILLIFORD CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 38.20 ACRES PERMITTED: 38.20
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip,
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
8/25/14
136,400.00 (G) .
3570.681
4.58
0.682
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
F 11475
I FESCUE
8/26/14
161,200.00 (G)
4219.895
4.58
0.806
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
I FESCUE
8/27/14
130,200.00 (G)
3408.377
4.58
0.651
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 ' p
30.60 p
11475
FESCUE
Aug-14
427,800.00 (G)'
11,198.953
Total Gallons/Ac: 11,198.95
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.017
0.009
0.381
1.617
0.081
0.002
0.026
0.128
0.026
6.417
82.99
49
Cumulative lbs/acre
0.058
1 0.045
1 1.605
7.826
1 0.985
1 0.010
0.341 1
0.478
0.316
19.160
190
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
t
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
q.
1339.0
267.9
15.0 375.0
89.0
2500.0
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
X D 7— l / S�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.6
* Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: OXFORD, NC
OWNER: EDWARD DENNY
SITE #: NC GR 00004 FIELD# : GR 00004 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00011244 ANNUAL DRY TONS APPLIED: 45.00
OPERATOR: EDWARD DENNY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 8.50 ACRES PERMITTED: 8.50
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pptn)
Crop
MONTH
Total
Per Acre
Solids
8/21/14
124,000.00 (G)
14588.235
4.58
2.786
OXAEDL
DRY
0-<I/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
I FESCUE
8/22/14
111,600.00 (G)
13129.412
4.58
2.508
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11415
1 FESCUE
Aug-14
235,600.00 (G)
27,717.647
Total Gallons/Ac: 27,717.65
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
121
Annuallbs/acre
0.042
0.021
0.942
4.002
0.201
0.004
0.064
0.318
0.064
15.881 205.39
7c.,
i)
Cumulative Ibs/acre
0.062
0.034
1.382
6.047
0.301
0.007
0.097
0.451
0.097
24.339
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
158
n
F e
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: OXFORD, NC
OWNER: EDWARD DENNY
SITE #: NC GR 00004 FIELD# : GR 00004 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: ' W00011244 ANNUAL DRY TONS APPLIED: 200.12.
OPERATOR: EDWARD DENNY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 52.50 ACRES PERMITTED: 52.50
Page
Lime Applied
***
Date
Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
8/6/14
49,600.00 (G)
944.762
4.58
0.180
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
8/7/14
204,600.00 (G)
3897.143
4.58
0.744
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
8/8/14
210,800.00 (G)
4015.238
4.58
0.767
OXAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
8/14/14
130,200.00 (G)
2480.000
4.58
0.474
OXAEDL
DRY
0-<1/2"
SUR .
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
8/15/14
111,600.00 (G)
2125.714
4.58
0.406
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
I FESCUE
8/16/14
55,800.00 (G)
1062,857
4.58
0.203
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
I FESCUE
8/18/14
86,800.00 (G)
1653.333
4.58
0.316
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
8/20/14
142,600.00 (G)
2716.190
4.58
0.519
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
8/21/14
37,200.00 (G)
708.571
4.58
0.135
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
8/22/14
18,600.00 (G)
354.286
4.58
0.068
OXAEDL
DRY
0-<1/2"
SUR
0.5
0.30
33,200. p
7,420.00 p
30.60 p
11475
FESCUE
Aug-14
1,047,800.00 (G)
19,958.094

FACILITY NAME: OXFORD, NC
OWNER: EDWARD DENNY
SITE #: NC GR 00004 FIELD# : GR 00004 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00011244 ANNUAL DRY TONS APPLIED: 200.12
OPERATOR: EDWARD DENNY CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 52.50 ACRES PERMITTED: 52.50
Page: 2
Lime Applied'**
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
ova
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Total Gallons/Ac: 19,958.10
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.030
0.015
0.678
2.882
0.145
0.003
0.046
0.229
0.046
11.435
147.89
87
Cumulative lbs/acre
0.060
0.029
1.213
6.039
0.279
0.008
0.088
0.373
0.139
24.049
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
211
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
OXAEDL = OXFORD, NC AEROB. DIGESTED LIQUID
X5-
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

�td'tPlHtjllfetEk,}T,GL`'s`f�:i4,lU��^-.lE�, 9Pdt�
.�re�l�[rt'a�l ii17Qr�ic?F'1�5�
June 17, 2014
Marshall Puryear
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Oxford WWTP
Dear Marshall Puryear:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: hup.-Ilwww.settekcom
Order No.: 14060462
Summit Environmental Technologies, hic. received 1 sample(s) on 6/5/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Fo�
Dr. Mo Osman
Proj ect Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabaina 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia
E87688 and 943, Idaho 01100923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky
90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
0112O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-
L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Page 1 of 6
Page 1 of 8

Summit Environmental Technologies, Ina
1 3310 Win St.
Workorder
M,
Sample Summary
��VI13dfl1aiEPJ`ItiL ➢E�t$CiQLt7,lrS;
3idG, Cuyahoga Falls, Ohio 44223
t#teil�+.�'t:a1'Ltih'r�pt'ts
TEL: [phone] FAX. • [phone]
WO#: 14060462
_
Website: http:/hvww.settek.com
17-Jun-14
CLIENT:
Synagro
Project:
Oxford WWTP
Lab SampleID Client Sample ID
Tag No Date Collected
Date Received Matrix
14060462-001
Oxford WWTP
6/2/2014 8:15:00 AM
6/5/2014 9:45:00 AM Sludge
Page 2 of 6
Page 2 of 8

SuMMIFF
Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
PHVIftOUMEb1'fAL'tfL4NQLC6r:SrVIC CiryahogaFalls, Ohio 44223 WO#: 14060462
r1na.P}ef r.'a11 �kiaxYrt�YTE TEL: [phone] FAX.- [phone]
Website: h�://www.settek.com Date: 6/17/2014
CLIENT: Synagro
Project: Oxford WWTP
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
Original
Page 3 of 6
Page 3 of 8

Summit Environmental Technologies, Inc.
3310 Win St.
WO#: 14060462
a
a S1il#iCkhlfriEPJ'i'x�L �l l;f a rwkiv Cuyahoga Falls, Ohio 44223 Date Reported: 6/17/2014
fora%trsaf Laraiarae TEL: [phone] FAX. • [phone]
Company: Synagro
Website: http://wwlv.settek.com
Address: 284 Boger Rd.
Mocksville
NC 27028
Received: 6/5/2014
Project#: Oxford WWTP
TCLP Metals Analysis (6010)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units
Matrix Method
DF
RegLvl
Run Analyst
Oxford WWTP 001 6/2/2014 TCLP Arsenic(As) 0.50 ND mg/L
Sludge EPA 6010 C
1
5.0
6/9/2014 WK
Oxford WWTP 001 6/2/2014 TCLP Barium(Ba) 5.0 ND mg/L
Sludge EPA 6010 C
1
100
6/9/2014 WK
Oxford WWTP 001 6/2/2014 TCLP Cadmium(Cd) 0.10 ND mg/L
Sludge EPA 6010 C
1
1.0
6/9/2014 WK
Oxford WWTP 001 6/2/2014 TCLP Chromium(Cr) 0.20 ND mg/L
Sludge EPA 6010 C
1
5.0
6/9/2014 WK
Oxford WWTP 001 6/2/2014 TCLP Lead(Pb) 0.50 ND mg/L
Sludge EPA 6010 C
1
5.0
6/9/2014 WK
Oxford WWTP 001 6/2/2014 TCLP Selenium(Se) 0.50 ND mg/L
Sludge EPA 6010 C
1
1.0
6/9/2014 WK
Oxford WWTP 001 6/2/2014 TCLP Silver(Ag) 0.50 ND mg/L
Sludge EPA 6010 C
1
5.0
6/9/2014 WK
TCLP Mercury Analysis (1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units
Matrix Method
DF
RegLvl
Run Analyst
Oxford WWTP 001 6/2/2014 TCLP Mercury 0.0020 ND mg/L
Sludge EPA 7470 A
1
0.20
6/9/2014 ALJ
SVOC SW-846: 8081 Pesticides-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Oxford WWTP
001
6/2/2014
Chlordane, total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030
6/10/2014
JBN
Oxford WWTP
001
6/2/2014
Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1
0.50
6/10/2014
JBN
Oxford WWTP
001
6/2/2014
Endrin
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
6/10/2014
JBN
Oxford WWTP
001
6/2/2014
gamma-BHC
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.40
6/10/2014
JBN
Oxford WWTP
001
6/2/2014
Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
6/10/2014
JBN
Oxford WWTP
001
6/2/2014
Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
6/10/2014
JBN
Oxford WWTP
001
6/2/2014
Methoxychlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
10
6/10/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Oxford WWTP
001
6/2/2014
1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
6/9/2014
MES
Oxford WWTP
001
6/2/2014
1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
6/9/2014
MES
Oxford WWTP
001
6/2/2014
Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
6/9/2014
MES
Oxford WWTP
001
6/2/2014
Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
6/9/2014
MES
Oxford WWTP
001
6/2/2014
Chlorobenzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
100
6/9/2014
MES
Oxford WWTP
001
6/2/2014
Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
6/9/2014
MES
Oxford WWTP
001
6/2/2014
Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
6/9/2014
MES
Oxford WWTP
001
6/2/2014
Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
6/9/2014
MES
Oxford WWTP
001
6/2/2014
Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
6/9/2014
MES
Oxford WWTP
001
6/2/2014
MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
6/9/2014
MES

!`
#/
ma—
Sumn:itEnvironmental Technologies, Inc.
3310 t. Win S
in St.
GSVIRCItJP+1Eh1ILTC�9ddl43s5��
C aho a Falls, Ohio
g
Date Reported:
6/17/2014
Anaiyffd-al C
TEL: [phone] FAX.- [phone]
Company:
Synagro .
Websile: http:/hvww.settek.coni
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
6/5/2014
Project#:
Oxford WWTP
SVOC 8270 TCLP BNA List
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Oxford WWTP
001
6/2/2014
1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
6/10/2014
JRT
Oxford WWTP
001
6/2/2014
2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
6/10/2014
JRT
Oxford WWTP
001
6/2/2014
2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
6/10/2014
JRT
Oxford WWTP
001
6/2/2014
2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
6/10/2014
JRT
Oxford WWTP
001
6/2/2014
Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
6/10/2014
JRT
Oxford WWTP
001
6/2/2014
Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
6/10/2014
JRT
butadiene
Oxford WWTP
001
6/2/2014
Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
6/10/2014
JRT
Oxford WWTP
001
6/2/2014
Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
6/10/2014
JRT
Oxford WWTP
001
6/2/2014
Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
6/10/2014
JRT
Oxford WWTP
001
6/2/2014
Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
6/10/2014
JRT
Oxford WWTP
001
6/2/2014
Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
6/10/2014
JRT
SVOC SW-846: 8321 Herbicides-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Oxford WWTP
001 6/2/2014 2,4-D
5.0 ND mg/L
Sludge
EPA 8321 A
1
10
6/11/2014
AMZ
Oxford WWTP
001 6/2/2014 2,4,5-TP
0.50 ND mg/L
Sludge
EPA 8321 A
1
1.0
6/11/2014
AMZ

Summit Em,ironniental Technologies, Inc•
WO#:
14060462
{P 111 iG3tIPelEtJieh.L & _CY�ud� L[}i3Sc INC
3310 Win St.
Cuyahoga Falls, Ohio 44223
Date Reported:
6/17/2014
tr�!rr.21 Ltiar �Tiatlex TEL: [phone] FAX.- [phone]
Company:
Synagro
Website: htto://wwiv.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received: 6/5/2014
Project#: Oxford WWTP
Client ID#
Lab ID#
Collected Analyte
Result Units
Matrix
Method
DF
RL Run
Analyst
Oxford WWTP
001
6/2/2014
Flashpoint (140T)
>140 T
Sludge
EPA 1010
1
6/13/2014
TAH
Oxford WWTP
001
6/2/2014
Cyanide, Reactive
ND ppm
Sludge
EPA 9014
1
0.50 6/6/2014
TIR
Oxford WWTP
001
6/2/2014
pH
6.3 s.u.
Sludge
EPA 9045 D
1
6/9/2014
AYS
Oxford WWTP
001
6/2/2014
Sulfide, Reactive
ND ppm
Sludge
EPA 9034
1
25 6/6/2014
TIR

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CD
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Retched III bb"fiy:, 6ppRnvcl
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Oxford WWTP WQ Permit Number: WQ 0011244
WWTP Name: Oxford WWTP NPDES Number: NC 0025054
Monitoring Period: From 01/01/14 To 03/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Cl No Land Application this Period
Al
If
Ad
Iry ......t, hi. —f .d Wince A nr Clacc Rl rmmWe the fnllnwing monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Excee-
Frequency
of
Sample
Type
Analytical
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 1h
MPN
MPN/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
(VS reduction)
Option/Alt.2
(40-day bench)
Option/Alt.3
(30-day bench)
Option/Alt.4
(Spec. 02 uptake)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7
(Drying — Stable)
Option/Alt. 8
(Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Dennis Wilson, Plant Superintendent
(7p)reaareNaml? and Title ( t �eq print) �/� �!� Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* / Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 FR Part 503.9(r) and 15A NCAC 2T.1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Oxford WWTP WQ Permit Number:
WWTP Name: Oxford WWTP NPDES Number: _
Monitoring Period: From 4/01/14 To 06/30/14
WQ 0011244
NC 0025054
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
'as
NO Land Ap
Alt. plication this Period
If ap
•c _ _r __. l.l.. a.... u..-_..a:-..... ..C.........d 10,1 A - I'l— W1 .. ..l040 +h. fnlln—it—in" data.
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Excee-
Frequency
of
Sample
Type
Analytical
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 th
CFU
CFU/g
0
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
(VS reduction)
Option/Alt.2
(40-day bench)
Option/Alt. 3 Option/Alt.4
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Dennis Wilson, Plant Superintendent
�reparo Name And Title (typ o
Signature ofPreparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Oxford WWTP WQ Permit Number: WQ 0011244
WWTP Name: Oxford WWTP NPDES Number: NC 0025054
Monitoring Period: From 07/01/14 To 09/30/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
it applicame to alternative periormea Class
A or l lass is com fete the ionowing monitoring
oata:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6 th
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
17500
43251
140000
CFU/g
0
4/yr
Grab
9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Dennis Wilson, Plant Superintendent
arer name And Title ri t or type) Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer ` Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

Cameron Testing, Services, Inc., Laboratory Report
NO PENR W654
NC PHHS #37790
US F-PA *NCO I gi8
n,,-:
Synagro PTO_ Pr
140576-
Oxford June 2014, keg',tilatory.
Yes
Sample Information
i
M. Puplear
DEW 06102/14 1"R'euefv6d
C. Cameron
-Date
06/02/14
Analyses and Results
Lab'16
P
'Sam ,
140576 01
SWG.- Or Fec. Coliforni-S <140000
rNY9
140000
06102114
BG
9222D - MF
b
<67600
GFUrEl
07000
<51600
C-Mg
5150D
d
<47300
CFUfQ
47300
e
<27200
UPlo
27200
f
<25800
L;Fufq
25800
<17500
Uufo
1756b
GE-omean <43300
140576-- 01
c3
;uCIN Gt TS 4.36
%
G.01
W02-1-14
BC�
2540 G -TS
b
4.25
%
G.0 I
C
3,92
0.01
d
4.30
0
G01
C-
3.99
001
f
4.28-
G.M.
9
3.69
0,01
Data
Revlaw
Lab Technician,
Date
Report
Ravlaw
Lab Virectur
Dato
219 S. Stcelc Str, 919-2084240
ti�omrbrd N'C 273-JO

30D Report Sheet
Project O-xford.Juno-2014
30 Day Ben- chtop Test
CTS Prbj.
Client synagro
(EPA 6251IRm92101 3, Appendix b)
Regulatory
Sarrigaled
Received
Reif.. DAelt,hbds
Std- Moth. -22rId ad.
By, kpuryear
By C. CaTnOron
Reques.ted
2540 G - TS
DdLe OSMi14
Date 0,6102114
Analysis
25AO G - VS
Type Grab
Matrix
Slracige.
S.
L -ID---
-TS. %
v
-All a YA19
t na
A 9 2'O/b
FVSRIrn.b.) 82011/o
'Pass, I'Vo'
Lab Director' Date,
litotes: Sample. started at TS 2%.-
Page 1

219S.SieeleS*r. Cameron Testing Services, Inc. Chain of Custody
Sonford, NC 2'a30
Phone: 9`9-208-42r0 NC tifPA',-GVV Cer #854 NC PHHS Cert #t 37799 US EPA NCO19in �c� c t Of
Company: Synagro
Email:
CTS lab use only
Contact: Marshall Puryear
Ph°'r'
_ -33�r46?i"�"ht
Sample
Temp {Cj
*7.It Pro}. ; k � {
Address 2$4 go Rd.
Boger
9
Fax:
J p&;Ay e4l%- -SXU•r�Ao. cc
T Blank
(Y1N#NA)
Arrive:
{City, State,
Zip) Mocksville, NC 27028
Notes-
'i% — gDG'� �
Due_
Project: l� V
Regulatory
I (YIN)
Mush
(YIN)
Collected: Name: L
PVVW
Signature. -
t 1 Ass CL
e CV
Sample InformaticiA
N umber of bottles
Sample ID
n E
r,
Mu
R
n
x
z
w w
p N "
�? A h
tG
Requested Analysis
CTS Lab
ID
[j i—
E
us
a
O
C)
a�
7
a
Si juge Fecal/ Io.Solids
I
30 Day
0
y-
Relinquished:
Received:
DatelTimc
Rush work will require prior approval. Additional charges will apply

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Oxford WWTP WQ Permit Number: WQ 0011244
t
WWTP Name: Oxford WWTP NPDES Number: NC 0025054
Monitoring Period: From 10/01/14 To 12/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B: NO Land Application this Period
Alt. (1)
If applic
Lime
u applicame to aiternanve periormea %-
ass .v or t,iass n com fete ine ionowing momrorm
data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 61
CFU
CFU/g
Coliform
power per gram
of total solids
CFU
CFU/g
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Dennis Wilson Plant Superintendent
rep Namy and Title -A0 , A —Land Applier Name and Title (if applicable) (type or print)
0
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

Meritech., Inca
Environmental Laboratory
Laboratory Certification No.165
Pale 1
Contact: Marshall Puryear Report Date 10/28/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 10/22/2014
Meritech Work Order # 10221436 Sample: Oxford WWTP 1 Grab 10/22/14
Parameters Results Analysis Date Reporting Limit M—et IM
% Total Solids
4.10 %
10/22/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 244 col/g dry wt
10/22/14
244 col/g dry wt
SM 9222D
Meritech Work Order # 10221437 Sample: Oxford WWTP 2 Grab
10/22/14
Parameters
Results
Analysis Date
Repotting Limit
Method
% Total Solids
4.14 %
10/22/14
0-100 %
SM 2540B
l Fecal Coliform (Sludge)
< 242 col/g dry wt
10/22/14
242 cal/g dry wt
SM 9222D
Meritech Work Order #
10221438 Sample:
Oxford WWTP 3 Grab
10/22/14
Parameters
Results
Analysis Date
Reporting Limit
Method
%Total Solids.:::.........:.....::::.4..07.%
.....:::.......:......._...10/22/14
.0-100 %
SIaI2540B
I?c�el,Colifox'iti.(S..1.ttclge).........................<146.:
c41/g.41ry. wl....
..... .10/22/1�1....................:...2G.col/g
cit'Y1��t.,........:SM,222D...:::........................:......
Meritech Work Order #
10221439 Sample: Oxford WWTP 4 Grab
10/22/14
Parameters
Results
Analysis Date
Reporting Limit
Metho
%Total Solids
4.02 %
10/22/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 249 col/g dry wt
10/22/14
249 col/g dry wt
SM 9222D
Meritech Work Order #
10221440 Sample:
Oxford WWTP 5 Grab
10/22/14
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
4.10 %
10/22/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 244 col/g dry wt
10/22/14
244 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 2732.0
tel.[phone] fax.[phone]

Meritec , Inc.
'�� .sue
Environmental Laboratory
Laboratory Certification No.165
Page 2
Contact: Marshall Puryear Report Date 10/28/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 10/22/2614
Meritech Work Older It 10221441 Sample: Oxford WWTP 6 Grab 10/22/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 4.82 % 10/22/14 0-100 % SM.2540B
Fecal Coliform (Sludge) < 207 col/g dry wt 10J22/14 207 col/g dry wt SM 9222D
Meritech Work Order # 10221442 Sample: Oxford WWTP 7 Grab 10/22/14
Parameters Results Analysis Date Reporting Limit Method
%Total Solids
3.61 %
10/22/14
0-100 %
SM 2540B
Fecal Coliforin (Sludge)
< 277 col/g dry wt
10/22/14
277 col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. ,
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
teI.[phone] fax.[phone]

3-20-2023
Chain of Custody Record (COC)
NPDES#:
Client:SVo&'A 4Y'42 Phone:
INICOa
I
Address: Fax:
ENVIRONMENTAL LABORATORIES
Email:
642 Tamco.Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:—
Email: [e-mail]
Attention:
Turn Aroundrime*
How would you like your report sent?
*RUSH work needs prior . approval.
www.mer!tE)ch-icil.---,.s.com
Circle all that apply:: imall (preferred), Fax, Mail
3-5 Days 24 - 48 Hrs
L—D]
.Sampling Dates & Times
Person Taking Sample (Sign/Priht):
Lab Use Only
Sample Location and/or ID #
Start
End
Comp?
of
Tests) IR"ecluired ....
PH OK?
Date
6e
Time
Date
I Time
Grab?
Cont.
Mice?
No
C1 OK?
Lkt)
Lxv
Temperature Upon
Receipt:
Method of
Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol
and TKN samples
must be done in the field prior to preservation.'
Comments:
Compositor#*
1JUg#
Shipment:
UPS
Fed Ex.
Are these results for regulatory purposes? Yes
No
Report results in: mg/L
mg/kg ug/L
Qlt� en/ ..-Hand delivery
Hell squished by Date Date Time:
Received by:
Date.
Time:,
Other
Relinquished Date.,
hd bTime:
Received by:
Date:
Time:
Relinquished by: Date: Time:
Rece,iyed-bY4abl'X;
Date:
Time
I L

Meritech, Inc.
Environmental Laboratory
:, _.
Laboratory Certification No.1fi5
......_..ti........................................................................................................................................
Contact: Marshall Puryear
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Report Dale: 11/25/2014
Date Sample Rcvd: 10/22/2014
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test
Meritech Worlc Order # 10221443 Sample: Oxford WWTP 1022/14
'total Solids Volatile Solids %Volatile Solids
Week 1
1.740 0.937 0.537
Week 2
1.820 0.930 0.512
Week 3
2,030
Week 4
0.441
I hereby certify that I have reviewed and approve these data, 4�.' 'f e a
ahoratofy Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

NPDES#-.
Chain of Custody Record (COC)
tom
Client:S,P'�s�Phone:
--
Fax:
m
Address:
Aj
ENVIRONMENTAL LABORATORIES
Email:
642 Tamco.Rd. Phone- 336-342-4748
Project:
P 0 #-
Reidsville NC 27320 Fax: [phone]
Turn Around Time*
Email: [e-mail]
Attention:
*RUSH work needs prior approval.
How would'yqU like your report sent?
ww-vv.mer! tech-labs.com
Mail
Circle all that apply: Email (preferred), Fax, M
Std. (20 da S)
3-5 Da 1
24-48 Firs
Person Takingsamole. (Sign/Print);
Lab Use 01111Y
.Sampling Dates & Times
'T
sample Location and/or ID # Start
St
End
Test (s)
l0enuired
r%
on lce�?
::Yes No
PH. OK?
CJ'OK?
Date
Time
34
Method of *** Dechlorination (<o.5 ppm) of Ammonia, Cyanide, Phenol and TKN
lCommients:
Shipment:
UPS
Fed Ex Are these results for regulatory purposes? Yes No
e:
f Relinquished by:, Tim
�':Hand Deliven,( 'I
Hand
by: Date: Time:
Other 'e
I FRevinquished by; Date: Time:
Temperature.,Upon
t R t
must be done in the field prior to preservation. r,
Compositor.#::
Jug# -
Report results inmg/L : mg/kg ug/LDate. Time:
ceived by:
�e;ved by: Date: Time:
!
Date:
Time:

Meritech, Inc.
¢' Environmental Laboratory
Laboratory Certification No.165
Contact: Marshall Puryear
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 1
Report Date 11/17/2014
Date Sample Rcvd: 11/10/2014
Meritech Work Order # 11101432 - Sample: Oxford WWTP 1 Grab 11/10/14
Parameters RgNults Analysi� Date Rem L,g unit Method
% Total Solids
3.69 %
11/12/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 272 col/g dry wt
11/10/14
272 col/g dry wt
SM 9222D
Meritech Work Order # 11101433 Sample: Oxford WWTP 2 Grab
11/10/14
Parameters Results Analysis Date Reporting Limit. Method
% Total Solids 3.74 % 11/12/14 0-100 % SM 2540E
Fecal Coliform (Sludge) < 267 col/g dry wt 11/10/14 267 col/g dry wt SM 9222D
Meritech Work Order # 11101434 Sample: Oxford WWTP 3 Grab 11/10/14
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
3.76 %
11/12/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 266 col/g drywt
11/10/14
266 col/g dry wt
SM 9222D
Meritech Work Order # 11101435 Sample: Oxford WWTP 4 Grab 11/10/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 4.00 % 11/12/14 0-100 % ' SM 2540B
Fecal Coliform (Sludge) < 250 col/g dry wt 11/10/14 250 col/g dry wt SM 9222D
Meritech Work Order # 11101436 Sample: Oxford WWTP 5 Grab 11/10/14
Parameters ResuM Analysis Date Reg Limit Method
% Total Solids
3.95 %
11/12/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 253 col/g dry wt
. 11/10/14
253 col/g dry wt
SM 92221)
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
. Laboratory Certification No.165
Page 2
Contact: Marshall Puryear Report Date 1/17/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 11/10/2014
Meritech Work Order # 11101437 Sample: Oxford WWTP 6 Grab 11/10/14
Parameters Results Analysis Date R��Qrting Limit Method
% Total Solids 3.55 % 11/12/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 282 col/g dry wt 11/10/14 282 col/g dry wt SM 9222D
Meritech Work Order # 11101438 Sample: Oxford WWTP 7 Grab 11/10/14
Parameters Resulpq Analysis Date Reporting Limit Method
% Total Solids 3.64 % 11/12/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 3,218 col/g dry wt 11/10/14 244 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.
- Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3402013
Chain, of Custody Record (COC)
NPDES#:
Client: �y Yt�� Y' c.� Phone:_
Address: Fax:
Email:
Project:
P.O:#:
Attention: Turn Around Time*
How would you like your report sent?. *RUSH work needs prior approval.
Circle all that apply: Email (preferred) , Fax, Mail 5trd (10 days) 3- 5 Da s Za - as Hrs
fl
!l �l �.a
2
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone; 336-342-4748
Reidsville NC 27320 Fax: [phone]
Email: info@ineritech-labs•com
n �� n t� �+h �y1
W V V v V. m e I i to c 1 I— I a b5 . C o I 1 1
Sample Location and/or ID #
Sampling ®at�s i�t Times
Person S Ta
king aking ample (Sign/Print)'
Use ®nly
Start
End
Comp?
(Grab?
# of
Cont.
Test
(s) Required
onlce?
e Na
pH OK?
Cl OK. -
Date
Time
Date
Time
U-
<
-
IY
Temperature Upon,
Receipt:
C—
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide; Phenol
and TKN
samples
must be,done in the field prior to preservation.
Comments:
Compositor #
Jug It
❑ UPS
=. Fed Ex
Are these results for regulatory purposeq?I Yes
No 0;:
Report results in: mg/t U'
mg/kg ❑: ' ug/L ❑
0
—. Hand Delivery
Relinquished by:. Date Time:
y
�;
Received by:
Date: Time:
�_ Other
1
by: Date: Time:
Received by:
Date: Time:
Relinquished by: Date: Time:
ved by LRIF l G
Df Titn
r V
M

Meritech, Inc.
_ Environmental Laboratory
Laboratory Certification No.165
Contact: Marshall Ptuyear Report Date: 12/17/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 11/10/2014
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test)
Meritech Work Order## 11101431 Sample: Oxford WWTP 11/10/14
Total Solids Volatile Solids % Volatile Solids
Week 1
1.770 0.960 0.543
Week 2
Week 3
Week 4
Week 5
1.730 0.570 0.330
2.690 1.680 0.597
1.640 0.750 0.458
1.790 0.920 0.512
J
I hereby certify that I have reviewed and approve these data. ., &Z �t
Laboratory Represen ative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES#:
C®
Client: S�� 4�4
Phone:
Fax:
_
_
Address:
ENVIRONMENTAL LABORATORIES
Email:
642 Tamco Rd. Phone: [phone]
Project:
w
r
Reidsville NC 27320 Fax: [phone]
Email [e-mail] Attention:
How would you like your report sent?
` � /� � /� � � S
VV VV yV .meritechdabs�com Circle all that apply: Email(preferred), Fax, Mail
.Sampling Dates & Times Person Taking Sample (Sign/Print):
Sample Location and/or ID # Start End comp? #of Test(s) Required
Date Time /Date Time Grab? Cont.
3V �t
Method of "** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservatic
Comments:
Shipment:
UPS
Are these results for regulatory purposes? Yes No Report results in: mg/L
Fed Ex
Relinquished by: Da Time: Received by:
Hand Delivery f lJ/14
Z
Relinquished by: Date: rme: Received b
other
Relinquished by: Date: Time: eceived by
Compositor
Jug #°
mg/kg ug/L•
Date: Time:
t ,Date: Time:
pj
r t✓ a e f Tir1e�J �1

Meritech, Inc,
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: date Roth Report Date 12/9/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 12/2/2014
Meritech Work Order # 12021412 Sample: Oxford WWTP 1 Grab 12/2/14
Parameters
Results
Analysis Date Reporting Limit
Method
Qualifier
% Total Solids
3.86 %
12/3/14 0-100 %
SM 2540B
B2
Fecal Coliform (Sludge)
< 2'59 col/g dry wt
12/2/14 259 col/g dry wt
SM 9222D
Meritech Work Order # 12021413 Sample:
Oxford WWTP 2 Grab
12/2/14
Parameters
Results
Analysis Date Reporting Limit
Method
Qualifier
% Total Solids
4.03 %
12/3/14 0-100 %
SM 2540B
B2
Fecal Coliform (Sludge)
< 248 col/g dry wt
12/2/14 248 cal/g drywt
SM 9222D
Meritech Work Order # 12021414 Sample: Oxford WWTP 3 Grab
12/2/14
Parameters
Results
Analysis Date Reporting Limit
Method
Qualifler
% Total Solids
8.01 %
12/3/14 0-100 %
SM 2540B
B2
Fecal Coliform (Sludge)
< 125 col/g dry wt
12/2/14 125 col/g dry wt
SM 9222D
Meritech Work Order # 12021415 Sample:
Oxford WWTP 4 Grab
12/2/14
Parameters
Results
Analysis Date Reporting Limit
Method
Qualifier
% Total Solids
4.01 %
12/3/14 0-100 %
SM 2540B
B2
Fecal Coliform (Sludge)
< 249 col/g dry wt
12/2/14 249 col/g dry wt
SM 9222D
Meritech Work Order # 12021416 Sample:
Oxford WWTP 5 Grab
12/2/14
1
Parameters
Results
Analysis Date Reporting Limit
Method
Qualifler
% Total Solids
3.70 %
12/3/14- 0-100 %
SM 2540B
B2,
Fecal Coliform (Sludge)
< 270 col/g dry wt
12/2/14 270 col/g dry wt
SM 9222D
132 Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that
would have been reported if there had been one colony on the filter representing the largest filtration volume
(reported as a less than "<" value).
642 Tamco Road, Reidsville, Nortlr Carolina 27320
tel.[phone] fax.[phone]

Contact: Nate Roth
Client; Synagro
284 Boger Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Report Date 12/9/2014
Date Sample Rcvd: 12/2/2014
Meritech Work Order # 12021417 Sample: Oxford WWTP 6 Grab 12/2/14
Parameters Results Analysis Date Reporting Limit Method Quallfier
Vi Total Solids 3.64 % 12/3/14 0-100 % SM 2540B B2
Fecal Coliform (Sludge) < 275 col/g dry wt 12/2/14 275 col/g dry wt SM 9222D
Meritech Work Order # 12021418 Sample: Oxford WWTP 7 Grab 12/2/14
Parameters
Results
Analysis Date
Reporting Limit
Me had Quallfler
% Total Solids
3.51 %
12/3/14
0-100 %
SM 2540B B2
Fecal Coliform (Sludge)
< 285 col/g dry wt
12/2/14
285 col/g dzywt
SM 9222D
132 Counts from all filters were zero. The vahie reported is based on the number of colonies per 100 nil that
would have been reported if there had been one colony on the filter representing the largest filtration volume
(reported as a less than "<" value).
t
I hereby certify that I have reviewed and approve these data.,.
Laboratory Represen tative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

�xo-m>3 Chain of Custody Record (COC)
NPDESt#:
Client:���� Phone:
Address: Fax:
Email: Yro�4r� Sync ice. ��r _
Project:
P.O.#:
/��,� Turn Around Time*
�
Attention: /� ��oA *RUSH work needs prior approval.
How would you like your report sent?
Circle all that apply:�eferred), Fax, Mail Std(10da s) 3-5 Days 24 - 48 Kr5
E ��� H"p � �a
ENVIRONMENTAL LABORATORIES
642TamcoRd. Phone: [phone]
L;
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com
Sample Location and/or ID #
Sampling Dates &-Times
Person Taking Sample (Sign/Print):
Lab Use; Only'
Start
Endcomp?
Grab?
Cont
Test(s)
Required
Ice? :
Yes /; No'
pH:OK?:
° CI -OK.?':.
Date
Time
Date
Time
o �!� W wTP
J
ld:3o
�GGd! SAC e
:°
Z
/
V3
Temperature.Upon
Re7:
Method of
shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TO
samples
must be done in the field prior to preservation.
Comments
Jug# :....::
UPS
t: Fed Ex
Are these results for regulatory purposes? YesNo
Report results in: mg/L?'• mg/kg;j' ug/L!
WiHand Delivery
Relinquished by: DaTime:
te:. � %�Z.5
Received by: Date: Time:
Q; Other
Relinquished by: Date: Time:
Received by: Date: Time:
Relinquished by: Date: Time:
Rec ed by 7i e t
,�`

Meritech, Inc.
Environmental Laboratory
- - - Laboratory Certification No.165
Contact: Nate Roth Report Date: 1/5/2015
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 12/2/2014
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test)
Meritech Work Order # 12021419 Sample: Oxford WWTP 12/2/14
Total Solids Volatile Solids % Volatile Solids
Week 1
1.840 0.910 0.494
Week 2
1.780 0.850 0.477
Week 3
1.610 0.750 0.465
Week 4
1.800 0.740 0.413
Week 5
1.990 0.980 0.490
I hereby certify thatl have reviewed and approve these data.
Laboratory Representative
642 Tainco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-zaza�3 Chain of Custody Record (COC)
NPDES#:
Client:ym�o o Phone:
Address:, Fax:
Email: KV^o r47,Co"
Project:
P.O.#:
A a!& �C Turn Around Time*
Attention: h
*RUSH work needs prior approval.
How would you like your report sent?
Circle all that a I mai preferred Fax, Mail std i0da s) 3�s Dates za.ast{rs
apply: � ? �
MERI C INC.
ENVIRONMENTAL LABORATORIES
642TarncoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
� � n � � j �y
wVV VY.meritech—labs.com
Sample Location and/or ID #
.Sampling Dates &Times
l Person Taking Sample (Sign/Print):
La6,:Use. Orly::
Start
End
comp?
crab?
#of
cons.
1 est(s) Required u i red
:!on Ice'?`:.:.pH!OK?:
/ No;'
��;O.K?
Date
Time
Date
Time
4� wLJ' !>
/ z
M 3®
�_
D- I enc,41
7emperature:Upon:: .
'
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field priorto preservation.
Comments:
Comppsitor #
Jug:#
UPS
Fed Ex
Are these results for regulatory purposes? Yes No
Report results in: mg/L mg/kg ug/L6
1<
Hand Delivery
Relinquished by: Date: Time: / r Z�
Received by: Date: Time:
Other
Relinquished by: Date: Time:
Received by Date: Time:
Relinquished by: Date: Time:
iv a iMI.
1J775_1rf

Agricultural Lime Application Log
Year: 2014
Project:
Oxford
Field
(state -county -site -field)
NC-GR-01-01 HenryThorpe
soil
pH 11
6.1
Lime Requirement
(from soil analysis)
O.OT/Ac.
Tons/Acre 1[Date
Applied
Applied
NC-GR-03-01 John Williford
6.1
O.OT/Ac.
NC-GR-04-02 Edward Denny
6.1
0.0T/Ac.
NC-GR-04-03 Edward Denny
6.2
O.OT/Ac.

NCDA&CS r __ comic Division Phone: [phone] Website: www.i t,,.-._t,'�',gov/agronorhil
Client: Henry Thorpe
Predictive 5676 Old Roxboro Rd.
F,' a Oxford, NC 27565
' l} Soil Re port Mehlich-3 Extraction
.° p Sampled County: Granville
4?
Report No. FY' ,.-L'001831
Advisor: Creighton Brown
Synagro Central
284 Boger Rd
Mocksville, NC 27028
Sampled: 07/01/2014 Received: 07/30/2014
completed: 08/07/2014
Farm: Oxford
Links to Helpful Information
Sample ID: GR1-1
Recommendations: Lime
Nutrients (Ib/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg S
Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
40
0 0
0 0
0 0
Note: 12
2 -
$pH
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2
Zn-I Zn-AI
Cu-1 Na ESP SS-1 NO3-N
0.46 1.05 10.4 86 1:5 6.1 163 53
52 31
42 116
84
455 455
142 0.1 1
:North -=Carolina
F''
'Tfu3t'fursiJ,Ca�umi8ssl�sre.
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

Page 1 of 2
Report Number: 15-007-0676
Account Number: 46478
wwwaleastem.com
Send To: SYNAGRO CENTRAL/OXFORD
MARY BREWER
284 BOGER RD
MOCKSVILLE NC 27028
nnfp RpcpivPd. n1/n7/21`116 Date OfAnalvsis: 01/08/2015
.A.&L Easte_m L_aboratories_.
21
7621 Whitepine Road Richmond, Virginia 23237 (804)_743-9401 Fax [phone]
Grower:
JOHN WILLIFORD
OXFORD PROJECT
SOIL ANALYSIS REPORT
Date Of Report: 01/09/2015
Submitted By: NATE ROTH
Farm ID: GR-03
Analytical Method(s):
Mehlich 3
Organic Matter'
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity,C.E.C`
Sample ID _
Lab
. - ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
'H
Field ID
Number
°
/° Rate Ibs/A'
ppm Rate'
ppm.. Rate
- ppm Rate-
ppm Rate-
ppm Rate
ppm Rate
P H
Index
meg1100g
' megl100g
03-01
01135
4.8 M 135
123 VH
37 VL
238 VH
911 M
35 VL
6.1
6.82
1.1
7.9
NC=102
NC=19
Percent Base Saturation_
Nitrate
;Sulfur "
Zinc
Manganese
Iron
Copper
Boron
-Solu&le Salts
- Chloride-
Aluminum
Sample ID _
K
Mg
Ca
Na
H
NON
S
Zd
M'n
Fe
Cu
B
B.
SS
CI
Al
Field ID
_
_
°/d"
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
`ppm Rate
mslcm Rate
ppm . Rate
ppm
03-01
12 L
18.6 VH
121 VH
213 VH
7.6 VH
0.5 L
0.08 VL
1.2
25.1
57.7
1.9
13.7
NC = 25
NC = 465.0
NC = 756
NC = 380.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
by: prc me G�
Pauric McGroary

Page 2 of 2 '
Report Number: 15-007-0676
Account Number: 46478
Send To: SYNAGRO CENTRAL/OXFORD
MARY BREWER
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 01/07/2015
Date Of Renort: 01/09/2015
a
A&L Eastern :L_aborato_res
7,621 Whitepine Road Richmond, Virginia 23237 (804),743.9401 Fax [phone]^
wwwaleastern:com
Grower: Submitted By: NATE ROTH
JOHN WILLIFORD Farm ID: GR-03
OXFORD PROJECT
SOIL FERTILITY RECOMMENDATIONS
Nitrogen
Phosphate
Potash `"
Magnesium
Sulfur ,
Zinc
Manganese
"' Iron
Copper
Boron -
,,.
Sample ID
Intended Crop
Yield Goal.
Lime
Tons -_
_ N
p205
Kz0
Mg
S "
Zn
Mn
Fe
Cu
B
Field ID
Tons
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
115/A
Ib/A
lb/Al
03-01
Fescue Hay
4
0.8
50
0
250
0
17
0
0
0
01
0-
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." o�1t
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the +"c
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

NCDA&CS':::, _nomic Division, Phone: '[phone]
Website: www.----.--.gov/agronomi/
Report No. WS,-,—a_'.016369
A— 90
Client:
Edward Denny
Advisor:
te ate RothY
Na
>
„ Predictive
6633 Old Roxboro Rd
Oxford, NC 27565
S na ro
g
284 Boger Rd
S Mehlich-3 Extraction
` Soil ReportCounty:
Mocksville, NC
Sampled County : Granville
Sampled: Received: 11/14/2014
Completed: 12/09/2014
Farm: NC-GR-04
Links to Helpful Information
Sample ID: 04-02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.0
120-200 0
100
0 0
0
0
0
0
Note: 12
2-
Test Results [units - WN in glcd; CEC and Na in meq/100 crrr�; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM%' WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.60 1.03 9.6 87 1.3 6.1 168 19
58 28
42 179
123
458
458
303
0.1 1
Sample ID: 04-03
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
110
0 0
0
0
0
0
Note: 12
2-
Test Results [units - WN in g/crrP; CEC and Na in meg1100 crrr3; NO3-N in mg/dr&]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.27 1.00 9.2 87 1.2 6.2 140 17
57 29
56 176
120
368
368
265
0.1 1
I .orth Carolina:
1�irac€�:T�zisr,F wrd :Ca3ust3ssron
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture