WQ0010689_Residual Annual Report 2014_20150127

�0-o T
Baxter
January 26, 2014
NCDENR - DWQ-
Aquifer Protection Section
Land Application Unit
1636 Mail Service
Raleigh, NC 27699
RE:. 2014 Annual Ash Report
Permit No.- WQ001.0689
Wood Boiler - North Cove, NC .
Enclosed is the annual ash distribution report for the .calendar year 2014, using the forms
Provided. by NCDENR=DWQ.
If you have any questions or require additional information, please contact Amanda Richcreek at
828.756.6809.
I certify, under penalty of law that the above information is, to the best of my, knowledge and
belief, true, accurate and complete. I am aware that there are significant penalties for submitting
false. information, including the possibility of fines and imprisonment for knowing violations.
Sincerely,
J. Alan Weiler
Plant Manager .
Cc: NC Division of Water Quality (3 additional copies with enclosures)
Ricky Styles
RECEIVEDIDENDIDWR
JAN 2 7 2015
lWeterQueli
Pen gse an
Baxter Healthcare Corporation
PO Box 1390, Marion, NC 28752
T 828.756.4151

CLASS A ANNUAL DISTRIBUTION AND MARKETIN.G/ SURFACE DISPOSAL CERTIFICATION AND-SUlV MARY FORM
WQ PERMIT #:. WQ0010689 FACILITY NAME:. Baxter -Healthcare Corporation North Cove Steam Generation Plant Ash ..
PHONE: [phone] COUNTY: McDowell OPERATOR: Baxter Healthcare
FACILITY TYPE (please check one): ® Surface Disposal (complete.Part A (Source(s). and "Residual In" Volume only) and Part C)
E Distribution and Marketing (complete Parts -A; B. and C)
Was the facility in operation during the past calendar year? - Yes 21 No ® If No skip parts A; B, C and certify form below
Fart A*:
Part_B*:
( include NPDES # if Volume fdry tons)
Sources s .
Recipient' Information
Month
Amendment/
applicable) Bulking A Residual In Product Out
, gent
Name(s)
Volume (dry tons)
Intended use(s)
Tanuary
See DMSDF sheet
February
supplemental for
March
breakdown
April .
%lay .
Tune
Tuly
August
5eptemlier=
Dctober
November
December
Total from FORM DMSDF. (sup)
( . P)
150
1565:T
1`71`57
1715:7
•. •. •. .. .. .. •. •. •. .. •..
Totals:
Annual (dry tons):
- IL50
1`56;5:7
1715 7
...... ................
;::::::: ?..... «< ::•:•:....:::.:.:.«
171-5 .7
Amendments) used: Bulking Agent(s). used: Dry Wood Chi s.
k If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) .1
pia* n.
Facility was compliant during the past calendar year with all conditions of the land, application permit Yes
;including.but not limited to items 1-3 below) issued :by the Division of Water Quality: ® No:-♦ If No, Explain in Narritive ,
1. -All monitoring was done in accordance with the permit and reported for the.year as required and three (3) copies of certified laboratory results are attached.
!.,All operation. and maintenance requirements.were compiled with. or, in the case of.a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water- Quality Standards occurred at a monitoring well. .
'I certify; under penalty, of.law, that the above information is, to the best of my knowledge and belief,'true, accurate 'and complete. I.am aware that there are significant.
ienalties for submitting false information; including the possibility of fines and imprisonment forknowing nowing violations./° .
>ignature U Permittee Date
**Preparer is defined in 40 CFR Part503.9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer**
(if different from Permittee)
Date
DENR FORM DMSDF (12/2006)

'CLASS A ANNUAL. DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORNt
Supplemental Information
WQ'PERMIT #: WQ0010689 _ FACILITY NAME: F Baxter -Healthcare Corporation_ North Cove _Steam Generation Plant Ash
PIIONE: 828=75G=6`809 d COiJNTY: McDowell i OPERATOR:( Baxter Healthcare
FACILITY TYPE (please check one): ® :Surface Disposal (complete Part A -"Month" "Source(s)" and "Residuial In" columns only)
0 - nictrihminn and MavL-.+;nrr
Part A*:.
Part B*:
Month
- . March
March
April
June
June
October
Sources(s) (include NPDES # if
applicable)
WQ0010689
WQ001.0689
WQ0010689
WQ0010689
WQ0010689
WQ00.10689
Volume (dry. tons)
Recipient Information
Amendment/
Bulking Agent
19.79 , -
30.21
30.00 _
•19.1.4
5.86
45.00-
Residual In
200.71
306.39
205.80
385.11
11-7.89
349.80
Product Out
220.50
336.60
235.8.0
404.25.
123.75
394.80
Names
(s)
Bobby Boone ,
Brian McKinney
Chris Clark
Henry Brown
Terry English
Ray Watson. -
Volume (dry
tons)
220.50
336.60-
235.80
404.25
123.75
394.80
Intended use(s)
Land Application
Land Application .
Land Application
Land Application
Land Application
Land.Application
Cotals: Annual (dry tons): 150
Amendment(s) used:
...... ....................................
1565:7 . _ 17,15.7 _ 17 15.7
Bulking Agent(s) used: Dm Wood Chins
lI more space. is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 1
DENR FORM DMSDF (Supp) (12/2006)

ANNUAL. RESIDUAL SAMPLING SUMMARY FORM " ,
Please note that your. permit maycontain additional parameters to be analyzed. The parameters: can be. reported in FORMRSSF - B
WQ Permit Number: . WQ0010689 Laboratory: 1) Pace Analytical, Services . .
Baxter. Healthcare Corporation North Cove
Facility. Name:.. 2)
Steam Generation-Plant'Ash
Residual Source WQ # or WQ0010689 3)
NPDES #: .
4)
WWTP Name: NA 5)
Residual A"RIVRiS data
Parameter
(m g)
Percent Moisture (%)
Arsenic
Conc.
Limit
m a
NA
.75
Sample or Composite -Date
WBNP1.14.14A .
.51..9
5.9
' WBNP1.14.14B
27.9 '
4.2
WBSP41141
' 47.6
6:1.
WBSP41-142-
54:4 .
5.5
LAPSE -14A1.
44
6.2
NPSEP14B2
44.81
.4.8
Cadmium
85
1.7
1:2
.1.2
1.4
0.99
0.9
Copper
Chromium
4,300
NA
78.3.
23.4
52.4
15.4
78.2'
"26.6
80A-
25:8
1:17
25.7
93.9'
18.9 .
Lead
Mercury
840
57 "
38.8
ND-
14.5
0.004
20.5
ND
2.1.5
ND , .
95.5
ND
31.5
ND
Molybdenum
75
0.92.
ND
1.8.
2.5
0.99
1:2
Nickel
420
20.9
14.3
22A
.23
28.5
23.8
Selenium
100
ND"
ND
ND
ND
8.4
7.2
Zinc
7,500
184
:124
167
175 . -
348
293
Total Phosphorus
NA
2510
894:'
3300
3000
1510
915
Barium
NA.
1330
962
:1580
1590
1960
1560
Calcium
NA
79400
54900.
90200
90200
1:14000
91200
Iron
NA
_12900.
8540
15000,
15200'
10800
8630
�Vu�VuUaLIVH i,iu►u nsLeu in,uns roan are not applicable: Keterence the individual permit for metals;limlts:
"I certify; under: penalty of law, that -this document was prepared under my direction or supervision in accordance with -a system designed
toassure that qualified personnel properly, gathered- and: evaluated .the: information submitted: I. am aware that there. are significant
penalties for submitting false information, including the possibility, of fines and imprisonment for knowing violations.,"
N L
Signatur f Preparer 7
Date.
*Preparer is,defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 '(26)
DENR FORM RSSF (12/20,06)

ANNUAL RESIDUAL. SAMPLING SUMMARY FORM - B
Report all sampling analysis results. for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed. .
WQ Permit Number: WQ0010689
Baxter Healthcare Corporation North Cove .
Facility Name: Sieam.Generation Plant Ash
Residual Source WQ0010689
NPDES #,or.WQ#: .
WWTP Name: _ .. NA.
Residual Analvsis Data
Laboratory:.. 1) Pace Analytical Services
2)
3)
4)
5) "
Parameter.
(mg/kg)
Sample or -Composite Date
WBNP1.14.14A
WBNP1.14.14B
WBSP41141
WBSP41142
NPSEP14A1
NPSEP14B2
Magnesium
Manganese
pH.
Potassium
14700
2390
Not -Reported
19200
- 10100.
1690
Not -Reported
13300
1650.0
2900
10:9,
26200
16100
2960
11.1
27900
23600
3690
9.1
25300
19500
3000
9.1
21300
Silver.
ND
ND
ND
ND
0.86
0.68
Sodium
4990
3100
4010
4280
8860'
7510
"I certify, under. penalty of law, that this document was prepared under -my direction or supervision in accordance with a. system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for -submitting false information, including.the. possibility of fines and imprisonment for knowing violations."
a,
Signature of r parer * -Date
*Preparer is.defined in 40,CFR Part 503.9(r) and 15A NCAC 2T .1102 (26).
'DENR FORM RSSF - B (12/2006)

205 Eas', Meadow Road - Suite A 2225 Riverside Dr. 9830 Kinse-YAve; Suite 100
Eden.. NC 27288 Asheville, NO 26804 Hunters--,ifle; NIC 28P78
[phone]
ANALYTICAL RESULTS
Project: WOOD BOILER POND ASH
Pate Project No.: 92196896
Sample, WBNP1.14.14A Lab ID: 92186096001 Collected: 01114114 15:00 Received: 01117/14 14.15 Matrix-. Solid
Results repoffod on a -dry-weight- basis
Parameters Results units Report Limit DF Prepared Analyzed GAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
6.9 mg/kg
1.8
1
01121114 13*45
0112S/1415--02
7440-38-2
Barium
1330 mg1k �g
0.89
1
01i21j-1413-45
0T123A 4 15-02
7440-39-3
Cadmium
ll.t mg/kg
018
1
01121114 ISAS
Oij29114 15,02
7440-43-9
Calcium
79400 mg/kg
177
10
01/21114 13:45
01124/114 12:01-
7440-70-2
Chrorr,flum
23.4 mg/kg
0.89
1
0119411413:45
01,0114115',0
-74,40-47-3
Dapper
Mt m -g/kg
0.69
1
01/21114 13A5
01/231141-8.02
7440-60-8
Iron
129GO mq/kg
17.7
1
01/2111413:45
0112311415.02
7439-89-6
Lead
38.6 mg/kg
0.69
1
01/21/1413:4-5
01,/23114 15:02
7439-92- . I
Magnesium
14700 mg/kg
17.7
1
01j21/14 113,45
011031114 15-J02
7439-9,5-4
Manganese
2390 mglkg
8.9
10
01121114 113� -:4 5
-
OIJ2411412.01
7439-96.5
Molybdenum
042 mg/k9
0Z9
1
01121114 13-45
OV231114 15.02
743998-7
Nickel
20.9 mg/kg
0,69
1
0112111413,45
011"2311415-62
7440-02O
Potassium
19200 mglkg
8850
10
0112111413.45
0112411412-01
74,40709-7
S , elenium
ND rngjkq
13
1
01/21/14 13-45
01i23/14 i5�02-
7782-49 -2
,Silver
ND mglkg
0;89
1
011P21M4 113:45
01123/1415.02
7440-22-4
Sodium
4990 mg/kg
.885
1
01/21114 13.45
01i23?11 4 15:02
7440-23-5
Zinc
184 mglkg
1.18
1
01121/14 13.45
OV23/1415:02
7440-666
5010 MET lCP, TCLP
Analytical Method: EPA6010
Preparation Method:EPA3010
Leachate MathodlDate: EPA 1311, 01121/14 22-30
Arsenic
ND mg1L
01050
1
0112:3114 17-00
01/241141:6.-10
7440-38-2
Barium
7.0. mg/L
0.25
1
01123i,14 17:00
01124/141613
7440-39-3
Cadmium
0.020 mg/L
0-0050 1
1
01/23/14-17*00
011241.1416-1.$
7440-43-9
Chrdmium
0.040 mg/L
0.025
.1
01123114 17-Od
01124/1416:13
7440-47-3
Lead
0.034 mg/L
0,025
1
011/23,14 17:00
0112411416-13
743�-9:7>-1
Selenium
ND mg/L
0.10
1
01 . /23/1417.00
01/241141613.
7782-49-2
Silver
ND mg/L
0.025
1
01/23114 17fOO
0 1 jP-41 14 16 : 1.3
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470
Preparation Method: EPA 7470
Leachate wllethod/Date: EPA 1311; 01121114 22,30
Mmury
ND u g,/L
0.20
1
01/22114 18:15
01/23114 18:3.2
7439-97-6
N71 Mercury
Analytical Method: EPA747 I I
Preparation Method: EPA 7471
Mercury
ND mg/kg
0.0073
1
01121/1421.30
01122/1415:53
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
5113%
OAQ
1
01121/14 14-.07
9045 OH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
10 Std. Units
1
011;.3011415:00
265:1 Phosphorus, Total
Analytical Method. EPA $65.1
Phosphorus
2O mg/kg
64,2
.20
0112411416,13
772$-14-0

Lab

205 East P-lea.dow Road - Suite A 2225 Ptierside Dr. 980QKlrreYAv.e. S)j4e-100
�-WeAnafjdicaf Eden. NC 27288 Asheville. NC 2$B04 pto78
(M)623-8921 (828)2-54-7176 (704)87644392
Project WOOD BOILER POND ASH
Pace Project No.: 921868915
Sample: WSNP114.14S Lab 111; 9,2186,996002 Colltoted: 011141/14 15:00 Received: 01117114 14:15 Matrix: Solid
Resufte reported on a dry -weight- basis
Parameters . Results - Units Report Limit DIF Prepared Analyzed CAS No. Qua]
6010 MFET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
4.2 nI
1.1
1
01/21114 13:45
01123/14 15:08
7440.39-2
Barium
962 nI
0.56
1
01/21/14 13:45
01123,114 15:08
7440-39-3
Cadmium
1.2 nI
vi
1
01/21/1413:45
01123/14 15:08
7440-43-9
Calcium
64900 M,9/kg
112 .
1.0
0
61121/14 13:45
011j241412,04
74.40�70-2
Chromium
15.4 m4tkg
0.56
1
01121/14 13:45
01123/1415 08
7440-47-3
copper
52.4 nI
0.56
1
01/21/14 13:45
01/23114 15:08
7440-5078
Iron
8640 mg/kg
11,2
1
01121/14 13:45
01123/1415:08
7439-89-6
Lead
14.6 mgJkq
0.56
1
01/21/14 13:45
01/23/14 i5:08
7439-92-1
Magnesium
10100 mg/kg
11.2
1
01,121/14 13:45
01/23/14 15:08
7439- -65-4
Manganese
1690 mg1kg
5.6
10
01121114 13:45
01124J14 12.04
7439796.5
Molybdenum
ND mg/kg
OZ6
1
01/21/14 13:45
01/22/14 15:08
74.39-98-7
Nickel
14.3 mI
0.56
1
0112-1/14 13:45
011231.14 15:08
7440-62-0
Potassium
1330o mg/kg
5590
10
01121/14 13'45
01124114 12:04
7440-09.7
Selenium
IND mg/kg
1.1
1
W21/14 13.45
0 1 fV114 16:06
7782-49�2
Silver
ND mgi.kg
0.55
1
011211-14 13:45
011,23/14 15:08
7440m22-4
Sodium
3190 mgtrkg
559
1
01/21/14 13:45
01/23/1415:08
7440-23-5
Zinc
124 mglkg
1A
1
01/21,114 13.45
D1123/14 15:08
7440-66-6
6010 MET ICP, TCLP
Analytical Method. EPA 6010
Preparation Method: EPA 801.0
L94chem Method/Date: EPA 1311; 01122/14 21'-190
Arsenic
ND rng1l-
0.056
1
01/23114117.-25
01/24114 i4,40
7440-38-2
11.1 mg/L
0.25
1
0 1123/ 14 17:25
01124/14 14:40'7440-39-2
Cadmium
0.023 mg/L
0.0050
1
01123/1417:25
01124/1414:4)
744043-9
chromium
ND mg/L
0.t125
1
0.1123/14 17:25
01i2.4/14 14:40
7440-47-3
Lead
ND mail.
O.625
1
01123/14 17:25
OV24/14 14:40
7439-92-1
Selenium
ND mg1L
0.10
1
01123114 17:25
011'24!14 14:40
7782-49-2
Silver
ND mg/L
0.025
1
01/23,114 17:25
01/24/14 14:40
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470
Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 01122114 21:00
Mercury
ND ug1L
0.20
1
01123/1418:30
01124/14 16:26
7439-97.6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
0.0040 mgikg
0,0038
1
0112111, 21:30
01122/14 15:55
74S9.97-6
Percent MoWure
Analocal Method: ASTM 02974-87
Percent moisture
21.9%
0.10
1
01/21114 14:07
9045 pH Soil
Analytical Method. EPA 9045
pH at 25 Degrees C
9.8 Std. Units
0.10
1
01/30;14 15.00
365.1 Phosphorus, Total
Analytical Method: EPA 365A
Phosphorus
894 m9*9
18.3
10
011241141&G6
7723-14-0

La—b-
.-Sectaion 3
...J.anuary 1-4-, 2014

Pace Analytical
Services; Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc..
® 205 East Meadow Road - Suite A 2225 Riverside Dr..
�eAnaljdicat
9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804
Huntersville, NC 28078
wrnvpacelebscnrrr
[phone] (828)254-7.176
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896
QC Batch: MERP/6083
Analysis Method: EPA 7470.
QC Batch Method: EPA 7470
Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92186896001
METHOD BLANK: 112,5986
Matrix: Water
Associated Lab Samples:. 92186896001
Blank Reporting.
Parameter Units
Result Limit Analyzed Qualifiers
Mercury ug/L
ND 6.20 .01/23/14.17:50
LABORATORY CONTROL SAMPLE: 1125987
Spike -LCS LCS . % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Mercury ug/L
2.5 , .. 2.6 102, 80-120
MATRIX SPIKE &MATRIX SPIKEDUPLICATE: 1125688' 1125989 '
MS MSD
92186822001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units : - Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD Qual
Mercury ug/L ND
2.5 2.5 2.6 2.5 102 100
75-125 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /27/2014 02:11 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 18

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
�
i��ieiAna6d caj
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC,28804
9800 KinceyAye. Suite 100
Huntersville, NC.28078
Pew•
[phone] [phone]
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILER POND
ASH
Pace Project No.: 92186896
QC Batch: MERP/6091
Analysis Method:" EPA7470
QC Batch Method: EPA 7470
Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92186896002
METHOD BLANK: 1126927
Matrix: Water
Associated Lab Samples: 921868.96002
Blank Reporting
Parameter
Units. Result Limit" Analyzed Qualifiers
Mercury' ug/L
ND 0.20 01/24/14 15:54
LABORATORY CONTROL SAMPLE: 1126928
Spike LCS LCS % Rec
Parameter
Units Conc. Result ._ % Rec Limits Qualifiers
Mercury ug/L.
2.5 2.2. 88. 807120 .
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1126929 1126930
MS MSD
92185790001 Spike .. Spike Ms. MSD MS MSD
% Rec
Parameter Units
Result Conc. Conc. Result Result %Rec % Rec
Limits ROD Qual
Mercury ug/L
ND 2.5 2.5 -2.2. 2.2 90 88
75125. '3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date:-01 /27/2014 02:11,' PM - _
without the written consent of Pace Analytical Services, Inc..
Page 7 of 18

Pace Analytical Services; Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
e 205 East Meadow Road -,Suite A 2225 Riverside Dr. 9800 I(incey Ave. Suite 100
aceAng1j trca1 Eden, NC 27288 Asheville, NC 28804 Huntersvilie; NC 28078
www.peceleb&cvm [phone] [phone] [phone]
QUALITY CONTROL VATA
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896
QC. Batch: MERP/6080
Analysis Method: EPA7471
QC Batch'Method: EPA7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 92-186896001, 92186896002
METHOD BLANK: 1125341.
Matrix: Solid
Associated Lab Samples: 92186896001; 92186896002
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Mercury mg/kg
ND 0.0050 01/22/1415:13
LABORATORY CONTROL SAMPLE: 1125342
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Mercury mg/kg
.067 0.063 95 80-120
MATRIX "SPIKE & MATRIX SPIKE DUPLICATE: 1125343 1126344
MS MSD
92186843002
Spike ; Spike MS: MSD MS. MSD %Rec
Parameter Units Result
Conc. Conc. Result Result %Rec. %Rec Limits RPD Qual
Mercury mg/kg 6.055
.066 M .0.10. 0.11 75 70. 75-125 3 M1
Date: 01/27/2014 02:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 18

CgC1 lytocal
wwnscpacelebscom
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/15085 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92186896601, 92.186896002
METHOD BLANK: 1124474 Matrix: Solid
Associated Lab Samples: 92186896001, 92186896002
Parameter
Units
Blank
Result
Arsenic
mg/kg
ND
Barium
mg/kg
ND
Cadmium
mg/kg
ND
Calcium
mg/kg
ND
Chromium
mg/kg
ND
Copper
mg/kg
ND
Iron
mg/kg
ND
Lead
rrg/kg
ND
Magnesium
mg/kg
ND
Manganese
mg/kg
ND
Molybdenum
mg/kg
ND
Nickel
mg/kg
ND
Potassium
mg/kg
ND
Selenium
mg/kg
ND
Silver
mg/kg
ND
Sodium
mg/kg
ND
Zinc
mg/kg
ND
'LABORATORY CONTROL SAMPLE: 1124475
Parameter Units
Arsenic
mg/kg
Barium
mg/kg •
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Date: 01/27/2014 02:11 PM
Reporting
Limit
Analyzed
1.0
01/23/1414:12
0.50
01/23/1414:12
0.10
01/23/1414:12
10.0
01/23/1414:12
0.50
01/23/1414:12
0.50
01 /23/14 14:12
10.0
01/23/1414:12
0.50
01/23/1414:12
10.0
01/23/1414:12
0.50
01/23/1414:12
0.50
01/23/1414:12
0.50
01/23/1414:12
500
01/23/1414:12
1.0
01/23/1414:12
0.50
0.1/23/14 14:12
500
01/23/1414:12
1.0
0.1/23/1414:12
Qualifiers
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
50
50.7
101'
80-120
50
51.8
104
80-120
50
51.3
103
80-120
500
509
102
80-120
50
50.8
102
80-120
50
51.6
103
80-120
500
518
104
80-120
50
51.0
102
80-120
500
533
107
80-120
50
51.4
103
80-120
50
53.4
107
80-120
50
51.7
103
80-120
500
522
104
80-120
50
51.2
102
80-120
25
25.4
102
80-120
500
540
108
80-120
50
50.3
101
80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 9 of 18

Pace Analytical Services,
Inc.
Pace Analytical Services, Inc.
Pace Analytical Services; Inc.
G �7�/ ®
�CGA�-PAPICaI
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. ,Suite 100
Eden, NC 27288
Asheville,
NC 28804
Huntersville, NC 28078
wmpacelabs com
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1124476
1124477"
MS
MSD
92186851015
Spike
Spike
MS
MSD
MS
MSD.
% Rec
Parameter
Units
Result
Cond.
Conc.
Result
'Result.
%Rec
% Rec
Limits
RPD Qual
Arsenic .
mg/kg
ND
58
43.9
55.6
42.1
95
95
75-125
28. R1
Barium
mg/kg
20.4
58
43.9
79.5
61.9
102
95
.75-125
25 RI
Cadmium
mg/kg
ND
58
43.9.
56.0
42.4.
97
-97
75-125
28_ R1
Calcium
mg/kg
629
580
439
1190
1010.
97
86
75425
17
Chromium
mg/kg
3.5
58
43.9
60.5
46:7
98
99
75-125
26 R1
Copper
mg/kg
1.9
58
43.9
.61.2
47.2
102
103
75-126
26 R1
Iron
mg%kg •
2450
580
439
3340-
2980
153
121
75-125
11 M1.
Lead
mg/kg
8.5
58'
43.9
64.0
49.0
- 96
92
75-125
. 26 R1
Magnesium
mg/kg
123
580
439
739
589'
106
106
75-125
22 R1 .
Manganese
mg/kg
12.A
58
43.9
67.4
54.0
95
95
75-125
22 R1
Molybdenum
mg/kg
ND.
58
43.9
56.2
42.6
97
97
.75A25
27 R1
Nickel
mg/kg
0.83
58
43.9.
57.8
44.6
98
99
75.-125
27 R1
Potassium
mg/kg
ND.
580.
439
893
739
.120
123
75-125
19
Selenium
mg/kg
ND
58
43.9
55.2
40.4.
95
92
75-125
31 R1
Silver
mg/kg
ND
29
22
28.3
21:5
97
98
75-125 '
27 R1
Sodium
mg/kg
ND
580
439
685
533
117
119
75-125
25 R1
Zinc
mg/kg:
9.2 _
. _. 58,
_ 43.9
65.5
51.9
_ . 97
-97
75-125--
23 R1-
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2014 02:11 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 18

Pace Analytical Services, Inc. Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
�acekvlicalyi
205 East Meadow Road - Suite A
2225 Riverside Dr.
9806 Kincey Ave. Suite 100
Eden, NC.27288
Asheville, NC28804
Huntersville, NC 28078
•web•-
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896
QC Batch:. MPRP/15117
Analysis Method: EPA 6010 .
QC Batch Method: EPA 3010
Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92186896002
METHOD BLANK: 1126926
Matrix: Water
Associated Lab Samples: 92186896002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
.
Arsenic
mg/L
ND 0.650
01/24/1414:11
Barium
mg/L
ND . 0.25
01/24/14 14:11
Cadmium
mg/L
ND 0.0050
- 01/24/14 14:11
Chromium
mg/L
ND 0.025
01/24/1414:11
Lead
mg/L
ND 0.025
01/24/1414:11
Selenium
mg/L
ND 0.10
01/24/1414AI
Silver
mg/L
ND- 0.025
01/24/1414:11
LABORATORY CONTROL SAMPLE: 1126921
Spike LCS
LCS % Rec
Parameter .
Units
Conc. Result % Rec Limits Qualifiers
Arsenic
mg/L
2.5 2.6
104 80-120
Barium
mg/L
2.5 2A
95 80-120
Cadmium
mg/L
2.5 " 2.3
94 80-120
Chromium
mg/L
2.5 2A
94 80-120
Lead
mg/L
2.5 2.2
89 80-120
Selenium
mg%L
2.5 2.7
10.7 60-120
Silver
mg/L ..
1:.2 1.2
99 80-120
MATRIX SPIKE 8< MATRIX SPIKE DUPLICATE: 1126922 " 1126923
MS MSD
92185790001
Spike Spike MS
MSD MS "MSD
% Rec
Parameter
Units " Result
Conc. Conc. Result
Result, % Rec _ % Rec
Limits
RPD . Qual
Arsenic
mg/L ND
2.5 2.5 2.7 '
2.7 106 110
. 75-125"
3
Barium
mg/L PAR
.2.5 2.5 2.9
3.0 98 101
75-125
3
Cadmium
mg/L ND
2.5 2:5 2A
2.5 98 100
75-125
3
Chromium
mg/L ND
2.5 2.5 2.4
2.5 98 100
75-125
3
Lead
mg/L ND
2.5 2.5 2.3
2.4 94 96.
75-125.
3
Selenium
mg/L ND.
2.5 2.5 2.8
2.9 112 115
75-125
3
Silver
mg/L ND
1.2 .. 1.2 1.3
.1.3 102 104
.. 75-125
2 "
Date: 0 1 /27/2014 02:11-PM
REPORT OF LABORATORY ANALYSIS"
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 19

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acea 205 East Meadow Road - Suite A 2225 RlveYside Dr. 9800 Kincey Ave. Suite 100
jical _ Eden, NG 27288 Asheville; NC 28804 Huntersville, NC 28078
wwapecelaba"eom [phone]
[phone] [phone]
QUALITY CONTROL DATA
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896
QC Batch: MPRP/15118 Analysis Method: EPA 6010
QC Batch'Method: EPA 3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92186896001
METHOD BLANK: 1126932 Matrix: Water
Associated Lab Samples: 9216M6001
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
01/24/1415:12
Barium
mg/L'
ND
6.25
61/24/1415:12
Cadmium
mg/L
ND,
0.0050
01,/24/1415:1'2
Chromium
mg/L
ND
.0.025
01/24/1415:12
Lead
mg/L
ND
0.025
01/24/1415:12
Selenium
mg/L
ND
0.10
01/24/1415:12
Silver
mg/L
ND
0.025
01/24/1415:12
LABORATORY CONTROL SAMPLE:
.1126933
.
Spike
LCS
LCS
% Rec
'Parameter
. Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
2.5
2.6-
104
80-120
Barium
mg/L
2.5
2A
97
:. 80-120
Cadmium
mg/L
2.5
2.4
95
80-120
Chromium
mg/L
2.5
2.4
95
80-120
Lead
mg/L.
2.5
2.3
91
80-120
Selenium
mg/L_
2.5
2.7
107
80=120 ,
Silver
mg/L
1.2
1.2
99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1126934
1126935
MS
MSD
92186822001
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5.
2.5
2.9
2.9
115 116
75A25
1
Barium
mg/L
97.0J.
.2.5,
2.5
2.8
2.8
108 107
75425
1
ug/L ,
Cadmium
mg/,L
12.9
2.5
2.5
2.6
2.6
105 105
75-125
1
ug/L
Chromium
mg/L
.
96.5.
2.5
2.5
2.7
2.7
106 105
- 75-125
1
uglL-
Lead
mg/L
- 65.0
2.5
2.5
2.6
2.6'
102' 101
75-125
1
ug/L
Selenium
mg/L
33.8)
2.5
2-.5
3.0
3.0.
121 119
75.425
1
ug/L
Silver
mg/L
ND
-1.2
1.2
1.2
1.2
93 92
75-125
0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/27/2014 02:11 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 18

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
/�7/80
r205 East Meadow Road - Suite A 2225 Riverside Dr.
eAna6 «I Eden, NC 27288 Asheville, NC 28804
ovmpsceMba.com [phone] [phone]
QUALITY CONTROL DATA
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896
QC Batch: PMST/6171 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92186896001, 92186896002
SAMPLE DUPLICATE: 1124088
92186929001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 22.9 22.4 2
SAMPLE DUPLICATE: 1124089
Parameter
Percent Moisture
Date: 01/27/2014 02:11 PM
92186896002 Dup
Units Result Result
% 27.9 46.2
RPD Qualifiers
49 R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 18

1
Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytieal ® 205 East Meadow Road - Suite A 2226 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 272t38 Asheville, NC 28804 Huntersville, NC.28078
1�& [phone] [phone] [phone]
QUALITY CONTROL DATA
Project: WOOD BOILER POND ASH
Pace Project No.: 92186896 "
QC Batch: WETA/17841- Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92186896601, 92186896002
METHOD BLANK: 1126549
Matrix: Solid
Associated. Lab Samples: 92186896001; 92186896002
Blank"
Reporting
Parameter Units
"Result
Limit
Analyzed Qualifiers
Phosphorus. mg/kg,
ND 2.0
01/24/1415:44
LABORATORY CONTROL SAMPLE: ' ' 1126550
-
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
Phosphorus mg/kg
50
50.6
101 '907110
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 1126551
1126552
MS
MSD
92185776001
- Spike
Spike Ms.
MSD MS_ MSD % Rec .
Parameter Units Result
Conc.
Coric. Result
Result % Rec % Rec 'Limits RPD Qual
Phosphorus mg/kg 123.
10.8
11.6 146
90.2 219 -280 90-110 47 M1,R1
Date: 01/27/2014 02:11'PM
REPORT OF LABORATORY ANALYSIS
This report shall"not be reproduced, except in full,
Without the written consent of Pace Analytical Services, Inc..
Page 14 of 18

Section" 3 Lai

Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 10.0
ac,eAnalXical
Huntersville, NC 28078
www.pwWabs.com
(704)875-909.2
ANALYTICAL RESULTS
Project: - ' .:Wood Boiler Pond Ash 4/1
Pape Proj6ct No.: 62.1954 . 61
Sample:, WBSP41141
Lab ID' 921.95461001-
Collected: 04/01/1410:10 Received: 04/01114 11:50 Matrix: Solid
Results reported on a Vry=weight'. basis
Parameters
Results. Units
Report Limit QF
Prepared
Analyzed CAS No; Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
6.1 mg/kg
1.7 1
04/02/14 11:40
04/03/14 21:55 7440-38-2
Barium
15.80 mg/kg
0.87 1
04102/14 11:40
04/03/14 21;55 744 1 0=39-3
Ca.dmium
1'..2 mg/kg
0.17 1
04102/14 11:40
0.4/031/14 21:55 7440-43-9 .
Calcium
90200 Mg/kg
.173 10
04/02/14 11:40
04/04/14 13:16 7440-70-2
Chromium
26.6 mg/kg
0.87 1
, 04/02/14 11:40
04/03/114 21:55 7440-47-3
Ccipper,
78.2 mg/kg
0.87: 1
04/02/1411:40.
04/0/114 21:55 7440-50-8
Iron
15000 mg/kg
.17.3 1
04/02/14 11;40.
04/03/14 21;55 7439-89-6
Lead
20.5 mg/Kg
0.87 1
04/02/1411:40
04/03/14 21:55 7439-92-1
Magnesium
16500 mg/kg
17.3 1
'04/02/14 11:40
- 04/03/14 21:55 7439-964
Manganese
2900 mg/kg
.8.7 10
04/02/14 11:40
04/04/14 13:16 7439-96-5
Molybdenum
1.8 mg/kg
0.87 1
04/02/14 11:40,
04/03/14.21:5 . 5 7439-98-7
Nickel
22.4:.mg/kg
0.87 1
04/02/141 . 1:40
04/03/14 21:55 7440-02-0
Potassium
26200 mg/kg
8670 10
04/02/14 11:40
04/64/14 13:16 .7440-09-7
Selenium
ND-mg/kg
1.7 1
04/02/14 11:40
04/03/14 21:55 7782-49-2:
Silver
ND mg/kg
0.87 1
04/02/14 11:40
04/03/14 21:55 7440-224
Sodium
4010 mg/kg
-867 1
04/02/14 11,40
04/03/14 21:55 7440-2375
Zind
167 mg/kg'
1.7, 1
04/02/14
2/14 11.40
04103/14 21;55 7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 60.10 Preparation Method: EPA 3010
Leachat.e Method/Date: EPA
1311; W01/14.19:110
Arsenic
ND mg/L
0.050 1-'
04/02114 17:20
04/63/14 16:13 7440-38-2
Barium
3.0 mg/L'
0.25 1.
04/02/14 17:.20
04/03/14 16:13 7440-34-3
Cadmium
ND mg/L
0.0050 1
04/02/14 17:20
04/03/14 16:13 7440-43-9
Chromium
ND mg/L
0.025 .1
04/02/14 17:20
04/03/14 16:13 744047-3
Lead
ND mg/L
0.025 1
04/02114 17:20
04/03114 16:121 7439-92-1
Selenium
ND mg/L
0.10 1
04/02/14 17:.20'
04/03/14 16:13 778249-2
Silver/0
ND mg/L
0.025 1
04/02/14 17:20
04/03/14 16:13 7440-224
7470 Mercury, TCLP
Analytical Method: EPA 7470
Preparation Method: EPA 7470
Leachate Method/Date: EPA
131.1; 04/01/14 19:10
M,iircyry
ND ug/L
0.20 1
04/02/14 18:00
04/021/14 15:50 7439-9776
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
ND mg/kg
0.0095 1
04/01/14 18:30
04/01/14 21:33 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
47.6 %
0.10 1
04/08/114 15:43
9046, pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
10.9 Std. Units
0.10 1
-04/03/14
15:24
365.1 Phosphoftis, Total. Analytical Method: EPA 365.1
Phosphorus 3300,mg/kg 112 20 -04/15/14 16:bl 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: .04/16/2014 01:00 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 17.

aceAnalOcal0
wn�w.pece!®bs.com
ANALYTICAL RESULTS
Project: Wood Boiler,Pond Ash 4/1
Pace Project No.:. 92195461
Pace Analytical Services; Inc.
9800 Kincey Ave. Suite 100
Huntersville; NC 28078
[phone]
Sample:. WBSP41142
Lab ID: 92195461002
Collected: 04/01/14.16.15 ; Received: 04/01/14 11:50 Matrix: Solid
Results reported on a dry=weight"basis
Parameters
Results Units
Report Limit DF
Prepared
Analyzed CAS No: Qual
6010 MET ICP
'Analytical Method: EPA 6010 Preparation Method: EPA3050
Arsenic
5.5 mg/kg
1.8 1
04/02/14 11:40
04/03/14 21:58 7440-38-2
Barium
1590 mg/kg
0.91 t
04/02/14 11:40
04/03/14 21:58 7440-39-3
Cadmium
1:4 mg/kg
0.18 1 .
04/02/14 11:40
04/63/1421:58 7440-43-9
Calcium
90200 mg/kg
183 10
04/02/14 11:40
04/04/14 13:19 7440-70-2
Chromium
25.8.mg/kg
0.91 1
04/02/1411:40
04/03/1421:58 7440-47-3
Copper
80.4 'mg/kg
0.91: 1
04/02/14 11:40
04/03/14 21:58. 7440-50-8
Iron
15200 mg/kg
18.3 1
04/02/14 11:40
04/03/14 21:58 7439-89-6
Lead
21.5 mg/kg
0.91- 1
04/02/14 11:40
04/03/14 21:58 7439-92-1
Magnesium
16100 mg/kg
18.3- 1
04/02/14.11:40
04/03/1421:58 7439-95-4
Manganese
2960 mg/kg
9.1 10
04/02/1.4 11:40
04/04/14 13019 7439-96-5
Molybdenum
2.5 mg/kg
0.9.1 .1
04/02/14 11:40.
04/03/14 21:58 7439-98-7
Nickel
23.0 mg/kg
0.91 1
04/02/14 11:40.
04/03/14 21:58 7440-02-0
Potassium
27800 mgkg
9130 10
04/02/14 11:40
04/04/1413:19 7440-09-7
Selenium
ND mg/kg
1.8 1
64/02/14 11:40
04/03/14 21:58 7782.49-2
Silver
ND mg/kg
0.91 - 1
04/02/14 1,1:40
04/03/14 21:58 7440-22-4
Sodium
4280 mg/kg
913 1
04/02/14.11:40
04/03/14 21:58 7440-23-5
Zino .
175 6ng/kg
1.8 1
04/02/14 11.40
04/03/14 21:58 7440-66-6 .
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA
1311; 04/01/14 19:10
Arsenic
ND mg/L
01.050 1 .
04/02/14 17:20
04/03/14 16:19 7440-38-2
Barium
2.8 mg/L
0.25 1
04/02/14 17:20
04/03/14 16:19 7440-39-3
Cadmium
ND mg/L
0.0050 1
04/02/1417:20
.
04/03/14 16:19 7440 43-9
Chromium
ND. mg/L
0.025 1.
04/02/14 17:20
04/03/14 16:19 7440-47-3
Lead
ND mg/L
0.025 1
04/02/14.17:20
04'/03/14 1619 7439-92-1
Selenium
ND mg/L
0:10 1
.04/02/14 17:20
04/03/14 16:19 7782-49-2
Silver
ND mg/L
0.025 1
04/02/14 17:20
04/03/14 16:19 7440-22 4 '
7470 Mercury, TCLP
Analytical Method: EPA 7470
Preparation Method: EPA 7470
Leachate Method/Date: EPA
1311; 04/01/14 19:10
Mercury
ND ug/L _
0.20 .1
0.4/02/1418:00
04/63/1415:53 7439-9776
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
ND mg/kg
0.0097 1
04/01/14'18:30
04/01/14 21:36 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture - .
54.4 %
0.10 1
04/68/14 15:43 .
904.5 pH Soil
Analytical Method:, EPA 904.5
pH at 25 Degrees C
11.1 Std. Units.
0.10 1
04/03/14 15:24
365.1 Phosphorus, Total, Analytical Method: EPA 365.1
1
Phosphorus 3000 mg/kg 91,.3 10 04/15/14 16:02 7723-14-0
Date: 04/16/2014 01:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, .
without the written consent of Pace Analytical Services, Inc..
Page 5 of 17.

aceAnglXical
www.pacelabs cbm
QUALITY CONTROL DATA
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MERP/6415 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92195461001; 92195461002
METHOD BLANK: 11.76110 Matrix: Water
Associated.Lab Samples: 92195461001, 92195461002
Blank Reporting
Parameter Units, Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 04/03/14.15:37
LABORATORY CONTROL SAMPLE: 1170111
Spike LCS LCS . % Rec
Parameter Units Conc: Result % Rec Limits Qualifiers
Mercury ug/L 2,5 2:7, 107 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1170112: 1170113
- MS. MSD
92193601001 Spike . Spike Ms. MSD MS MSD % Rec
Parameter Units Result .'Conc. Conc. Result Result % Red % Rec Limits RPDQual
Mercury. ug/L ND 2.5 2.5 3.1 2.8 121 109 75-125 10
Date: 04/1.6/2014 01:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
.without the written consent of Pace Analytical Services, Inc..
Page 6 of 17

aceArtaIXica!®
www.psWsbs.c=
QUALITY CONTROL DATA
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461
QC Batch: MERP/6410 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92195461001, 92195461002
METHOD BLANK: 1169339 Matrix: Solid
Associated Lab -Samples: 92195461001, 92195461002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0050 04/01/14 21:01
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1169340
Spike
LCS
LCS
% Rec
Parameter Units
Conc.
Result
% Rec
Limits Qualifiers
Mercury mg/kg
.067
6.067
100
80-120
MATRIX SPIKE &-MATRIX SPIKE DUPLICATE: 1169341
1169342
MS
MSD
92195408001
Spike
Spike MS
MSD
MS MSD % Rec
Parameter Units Result
Conc.
Conic. Result
Result
% Rec % Rec Limits RPD Qual
Mercury mg/kg ND
.056
.056 0.043
0.042
77 76 75-125 2
Date: 04/16/2014 01:00 PM
REPORT OF LABORATORY ANALYSIS
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aceAnalg cal
www.pa wabs.com .
QUALITY CONTROL DATA
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461
QC Batch: MPRP/15581 Analysis Method:EPA 6010
QC.Batch Method: EPA 3050 Analysis Description:_ .6010 MET
Associated Lab Samples: 92195461001, 92195461002
METHOD BLANK: 1169506 Matrix: Solid
Associated Lab Samples: 92195461001, 92195461002
Parameter
Units.
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
:Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
LABORATORY CONTROL SAMPLE: 1169561
Blank
Reporting
Result
Limit
Analyzed Qualifiers .
ND
1.0
04/03/14 21:08
ND
0.50-
04/03/14 21:08
ND
0.10
04/03/14 21:08 .
ND
10.0
04/03/14 21:08
ND
0.50
04/03/14 21:08
ND
0,50
04/03/14 21:68
ND
10.0
04/03/14 21:08
ND
0.50
04/03/14 21:0.8
ND
10.0
04/03/14 21:08
ND
0.50.
04/03/14 21:08
ND
0.50
04/03/14 21:08
ND
0.50
04/03/14 21:08
ND,
506
04/03/14 21:08
ND
1.0
04/03/14 21:08
ND
0.50.
04/03/14 21:08
ND
500
04/03/14 21:08
ND
1.0
04/03/14 21:08 .
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter
Units
Spike
Conc.
- LCS
Result.
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
50.
47.5
95
80-120
Barium-
mg/kg
50
47:7
95
80-120.
Cadmium
mg/kg
50
48.8
98
80-120
calcium
mg/kg
560
471
94
80-120
Chromium
mg/kg
50
47.3
95
80-120
Copper.
mg/kg
50.
49.0
98
80-120
Iron
mg/kg
500
486
97
80-120
Lead
mg/kg
50 '
47.3
95
80-120
Magnesium
mg/kg
500
485
97
80-120
Manganese
mg/kg
50
47.8
96
80-120
Molybdenum
mg/kg
50
48.7
97
80-120.
Nickel
mg/kg
50
48.6
97
80-120
Potassium
mg/kg
500
501
100
80A20
Selenium
mg/kg
50
48.0
96
807120
Silver
mg/kg
25
24.2
97
80-120
Sodium
mg/kg
500
508
102
80120
Zinc
mg/kg
50
47.2
94
80-120'
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/1.6/2014 01:00 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 17

Pace Analytical Services, Inc. .
®
amAnaljftal
9806 KinceyAve. Suite 10.0
Huntersville, NC 28078
.. wwwpacWsb&corn
[phone]
.QUALITY
CONTROL DATA.
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461
. .
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1169502
1169503
MS
MSD
92195233001
Spike
'Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result.
Conc.
Conc.
Result
Result
% Red
% Rec
Limits
RPD Qual
Arsenic
mg/kg
ND
43.1
49
40.3
45.4
93
92
75-125
12
Barium
mg/kg
ND
43.1.
49
40.4
45.9
93
91
75-125
11
Cadmium
mg/kg
ND
43.1
49
39.1
45.6
91
93
75-125
15
Calcium.
mg/kg
280
431
490
650
737
86
93
75-125
12
Chromium
mg/kg
10.7
43A
49
50.8
56:2
93
93
75-125
10
Copper,
a mg)kg
1.4
43.1
49
. 43.0
48.5
97
96
75-125
.12
Iron
mg/kg
78.8
431
490,
378
492
70
84
757125
26 M1,R1 .
Lead.
mg/kg
ND
43.1
•• .49
3.9.4
44.3
91
90
75-125
12
Magnesium
mg/kg
46.7
431
490
448
504
93
93
75-125
12
Manganese
mg/kg •
2,8
43.1
49
42.5
47.8
92
92
75-125
12
Molybdenum
mg/kg
ND
43.1
49
35.8
43.5
82
88
75-125
19,
Nickel
mg/kg
4.8
43.1
49
451
, , 51.1
95
95
75-125
11
Potassium
mg/kg
ND
431
490
423J
478J
93
93.
75-125
Selenium
rng/kg
ND
43.1
49
40:9
45.9
95
9.4
75-125
12
Silver
mg/kg
ND.'
:.21.6
24.5
19.1
22.0
88
89
75-125
14
Sodium -
mg/kg
550 ..
431
490
.948
1020
92
96
75-125
7
Zinc
mg/kg
1.7
43.1
.49
39.8
45.6
88
90
75-125
14
REPORT OF LABORATORY ANALYSIS
'This report shall
not be reproduced, except in full,
Date: 04/1.6/2014 01:00 PM
without the written consent of Pace Analytical Services, Inc..
Page 9 of 17

aceAnalj cal
ewvw.pacelabs.com
QUALITY CONTROL DATA
Project: . Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461 1
.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MPRP/15583
Analysis Method: EPA6010
QC Batch Method: EPA 3010
Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92195461001,
921.95461002
METHOD BLANK: 1170118
Matrix: Water
Associated Lab Samples: 92195461001,
92195461002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Arsenic
mg/L
ND 0.050
.04/03/1415:54
Barium
mg/L
ND 0.25
04/03/1415:54
Cadmium
mg/L
ND 0.0056
04/03/1415:54
Chromium
mg/L
ND 0.025
04103/1415:54
Lead
mglL
ND 0.025
04/03/1415:54
Selenium
mg/L
ND 0.10
04/03/1415:84
Silver
mg/L
ND 0.025
04/03/1415:54
LABORATORY CONTROL SAMPLE:
1170119,
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Arsenic
mg/L
2.5
2.6
104
80-120
Barium
mg/L
2.5
2.2
90
80-120
Cadmium
mg/L
2.5
2.4
96
80-120
Chromium
mg/L
2.5
2.4
96
80-120
Lead
mg/L
2.5
2.4
94
80-120
Selenium
mg/L
2.5
2.7
108
80-120
.Silver
mg/L
1.2
1.3
102
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1170120
1170121
MS
MSD
92193601001
Spike
Spike.
MS
MSD
Ms.
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
% Rec
Limits
RPD • Qual
Arsenic
mg/L.
ND
2.5
2.5
2.8
2.9
112
114
75-125
2
Barium
mg/L
ND
2.5
2.5
2.7
2.7
100
101
75-125
1
Cadmium
mg/L
ND
2.6
2.5
2.6
2-.6
103
103
75-125
1
Chromium
mg/L
ND.
2.5
' 2.5
2.6.
2.6
104
104
75-125
0
Lead
mg/L
ND
2.5
2.5
2.6
2.6
102
102
75-125
0
Selenium
mg/L
ND
2.5
2.5
2.9
3.0
116
117
757125
1
Silver
mg/L
ND
1.2
- 1.2
1.4.
1.4
112
112
75-125
'0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced; except in full,
Date: 04/16/2014 01:00 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 17

1a(c#.qenAna1j4ica1
www.pa&Wabs.com
QUALITY CONTROL DATA
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461
QC Batch: PMST/6442 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92195461001, 92195461002
SAMPLE DUPLICATE: 1173376
92195648001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 21.2 21.1 0
SAMPLE DUPLICATE: 1173377
92196300003 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 13.8 13.4 3
Date: 04/16/2014 01:00 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 17

aceAna1j cal
wnrm�pacelabs.com
QUALITY CONTROL DATA
Project: Wood Boiler Pond Ash 4/1
Pace Project No.: 92195461
QC Batch: WET/30336 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH.
Associated Lab Samples: 92195461601, 92195461002
SAMPLE DUPLICATE: 1170868
Parameter
pH at 25 Degrees C
Date: 04/16/2014 01:00 PM
92195093001 Dup
Units Result Result
Std. Units 7.8 7.7
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
0
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 17

Pace Analytical Services, Inc.
aceAna! ica�® 9800 Kincey Ave. Suite 100
•.. Huntersville; NC 28078
www.pa dabs com
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Pnnrl Ach All
Pace Project No.: 92195461
QC Batch: WETA/18684 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total .
Associated Lab Samples: 92195461001, 92195461002
METHOD BLANK: 1177434 Matrix: Solid
Associated Lab Samples: 92195461001, 92195461002,
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 2.0 04/15114.15:30
LABORATORY CONTROL'SAMPLE: 1177435
Spike LCS LCS - % Rec
Parameter Units Conc. Result % Rec . Limits Qualifiers
Phosphorus mg/kg 50 47.2 94 1. 90-110
MATRIX SPIKE &' MATRIX SPIKE DUPLICATE: 1177436 1177437 -
MS MSD
92195456001 Spike Spike MS • MSD MS MSD % Rec
Parameter, Units Result Conp. Conic. Result Result. % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 198 284 284 427 '323 8.1 44 90-110 28 M1,R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/16/2014 01:00 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 17

\
OEM

ac"AnaVica! ®
WW..pXd&b&C=
ANALYTICAL RESULTS
Project:- - Wood Boiler Ash 9/12
Pace Project No.: 92217262
Pace Analytical Services, Inc.
9800 Kiricey Ave.' Suite 100
Huntersville, NC 28078
[phone]
Sample: NPSEP14A1
Lab ID: '92297262001
Collected: 09/12/14 12:45 Received: .09/12/14 13:50 Matrix: Solid
Results repoded on a Vry:weight"basis
Parameters
Results Units
Report Limit DF
Prepared
Analyzed' . CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050'
Arsenic
6:2 mg/kg
1.5 1
09/16/1415:30
09/17/14 01:42 7440-38-2
Barium
1960 mg/kg
15.4 20,
09/16/14 15:30.
09/17/14 14:40 7440-39-3
Cadmium
0.99 mg/kg
0.15 1
09/1611415-30
09/17/14 03:42 7440-43-9
Calcium
114000 mg/kg
30.8 20
09/16/14,15:30
09/17/14 14:40 7440-70-2
Chromium
25.7 mg/kg
0.77' 1
09/16/14 15:30
09/1.7/14 03:42 7440-47-3
Copper
117 mg/kg
0.77: 1
09/16/14 15:30
09/17/14 03:42 7440-50-8
Iron
10800 mg/kg
15.4 1
09/16/14 15:30
09/17/14 03:42 7439-89-6
Lead
95.5 ,mg/kg
0.77 1
09/16/14 15:30
09/17/14 03:42. 7439-92-1
Magnesium
23600 mg/kg.
308 -20.
09/16/14.15:30
007/1.4 14:40 7439-95-4
Manganese
3690 mg/kg.
15.4 20
09/16/14 15:30
09/17/14 14:40 7439-96-5
Molybdenum
0.99 mg/kg
0.77 1
09/16/14 15:30
09/17/14 03:42 7439-98-7
Nickel
28.5 mg/kg
0.77 1
09/16/14 15:30
05/17/14 03:42 7440-02-0 .
Potassium
25300 mg/kg
15400 20
09/16/14 15:30
09/17/14 14:40 7440-09-7 .
Selenium
8.4 mg/kg
1.5 1
09/16/14 100
09/17/14 03:42 778249-2
Silver
0.86 mg/kg
0.77 1 :
09/16/1415:30
09/17/14 03:42 7440-224
Sodium
8860 mg/kg
770 1
09/16/14 15:30
09/17/14 03:42 7440-23-5
Ziric
348 mg/kg .
1.5 1
09/16/14' 15:30.
09/17/14 03:42 7440-66-6 .. ,
6010 MET ICP, TCLP
Analytical Method: EPA6010 Preparation Method: EPA3010
Leachate Method/Date: EPA 1311; 09/17/14 19:00
Arsenic
ND mg/L
0.050 1
09/18/1.4 15:50
09/19/14 02:32 7440=38-2
Barium
4.5 mg1L
0.25 1
09/18/14 15:50
09/19/14 02:32 7440-39-3�
Cadmium
ND- mg/L -
. 0.0050 1
09/18/14 15:60
09/19/14 02:32 ' 7440-43-9
Chromium
ND mg/L
0.025 1
09/18/14 1550
09/19/14 02:32 7440-47-3
Lead
ND mg%L
0.025 1
09/18/14 15:50
09/19/14 02:32. 7439-92-1
Selenium.
ND, mg/L
0.10 - 1
.09/18/14 15:50
09/19/14 02:32 7782-49-2
Silver
ND mg/L
0.025 ' 1
09/18/14 15:50
09/19/14 02:32 7440-22-4
7470 Mercury, TCLP
Analytical Method, EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA1311; 09/17/14 19:00
Mercury
ND ug/L
0.20 1
09/18/1416:50
09/19/1413:44 7439-97-6
7471. Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND mg/kg
0.0061 1
09/16/14 14:30
09/18/14 13:19 7439-97-6
Percent Moisture
Analytical, Method: ASTM D2974-87
Percent Moisture
44.0 %
0.10 1
09/15/14 13:17'
9045 pH Soil Analytical Method: EPA9045
pH at 25 Degrees C 9.1 Std. Units 0.10 1 09/15/14 14:10 H1
365.1 Phosphorus, Total. Analytical Method: EPA 365.1
Phosphorus 1510 mg/kg 42.6 10 09/21/1411:44 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09'AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 17

J

aceAnalykal
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ANALYTICAL RESULTS
Project: Wood Boiler Ash 9/12
Pace Project No.: 92217262
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NPSEP14B2
Lab ID: 92217262002
Collected: 09/12/14 12:45
Received: 09/12/14 13:50 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters
Results Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010
Preparation Method: EPA 3050
Arsenic
4.8 mg/kg
1.3
1
09/16/14 15:30
09/17/14 03:48
7440-38-2
Barium
1560 mg/kg
13.1
20
09/16/14 15:30
09/17/14 14:44
7440-39-3
Cadmium
0.90 mg/kg
0.13
1 .
09/16/14 15:30
09/17/14 03:48'
7440-43-9
Calcium
91200 mg/kg
263
20
09/16/14 15:30
09/17/14 14:44
7440-70-2
Chromium
18.9 mg/kg
0.66
1
09/16/14 15:30
09/17/14 03:48
7440-47-3
Copper
93.9 mg/kg
0.66
1
09/16/14 15:30
09/17/14 03:48
7440-50-8
Iron
8630 mg/kg
13.1
1
09/16/14 15:30
09/17/14 03:48
7439-89-6
Lead
31.5 mg/kg
0.66
1
09/16/14 15:30
09/17/14 03:48
7439-92-1
Magnesium
19500 mg/kg
263
20
09/16/14 15:30
09/17/14 14:44
7439-95-4
Manganese
3000 mg/kg
13.1
20
09/16/14 15:30
09/17/14 14:44
7439-96-5
Molybdenum
1.2 mg/kg
0.66
1
09/16/14 15:30
09/17/14 03:48
7439-98-7
Nickel
23.8 mg/kg
0.66
1
09/16/14 15:30
09/17/14 03:48
7446-02-0
Potassium
21300 mg/kg
13100
20
09/16/14 15:30
09/17/14 14:44
7440-09-7
Selenium
7.2 mg/kg
1.3
1
09/16/14 15:30
09/17/14 03:48
7782-49-2
Silver
0.68 mg/kg
0.66
1
09/16/14 15:30
09/17/14 03:48
7440-224
Sodium
7510 mg/kg
657
1
09/16/14 15:30
09/17/14 03:48
7440-23-5
Zinc
293 mg/kg
13
1
09/16/14 15.30
09/17/14 03.48
7440 66 6
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
7471 Mercury
Mercury
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
365.1 Phosphorus, Total
.Phosphorus
Date: 09/22/2014 11:09 AM
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 09/17/14 19:00
ND mg/L 0.050 1
09/18/14 15:50
09/19/14 02:36 7440-38-2
4.4 mg/L 0.25 1
09/18/14 15:50
09/19/14 02:36 7440-39-3
ND mg/L 0.0050 1
09/18/14 15:50
09/19/14 02:36 7440-43-9
ND mg/L 0.025 1
09/18/14 15:50
09/19/14 02:36 7440-47-3
ND mg/L 0.025 1
09/18/14 15:50
09/19/14 02:36 7439-92-1
ND mg/L 0.10 1
09/18/14 15:50
09/19/14 02:36 7782-49-2
ND mg/L 0.025 1
09/18/14 15:50
09/19/14 02:36 7440-22-4
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 09/17/14 19:00
ND ug/L 0.20 1
09/18/14 16:50
09/19/14 13:47 7439-97-6
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg 0.0060 1
09/16/14 14:30
09/18/14 13:22 7439-97-6
Analytical Method: ASTM D2974-87
44.8 % 0.10 1
09/15/14 13:17
Analytical Method: EPA 9045
9.1 Std.-Units 0.10 1
09/15/14 14:10 H1
Analytical Method: EPA 365.1
915 mg/kg 19.3 5
09/21/14 11:41 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 17

Pace Analytical Services, Inc..
,�a'neAnalyiical ® 9800 KinceyAve..Suite 10.0
Huntersville, NC 28078
www..pacelabs.com
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9/12
Pace Project No.: 92217262
QC Batch: MERP/7094 • Analysis Method: EPA7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCILP
Associated Lab Samples: 92217262001, 92217262002
METHOD BLANK: 1288318 Matrix: Water
Associated Lab Samples: 922172.62001, 92217262002
Blank- Reporting
Parameter Units . Result Limit Analyzed Qualifiers
Mercury . ug/L ND 0.20 .09/19/14.13:02
LABORATORY CONTROL SAMPLE: 1288319
Spike ' LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.4 94. 80-120
MATRIX -SPIKE &MATRIX SPIKE DUPLICATE: 1288320 1288321'
MS MSD
92216155001 Spike Spike MS . MSD MS MSD %-Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.5 2.4 95 92 75-125 : ' 3
Results presented on this page are in the units indicated. by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 17

aMAnapcal
www.pacefaftcom
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9112
Pace Project No.: 62217262
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
"Huntersville, NC 28078
[phone]
QC Batch: MERP/7090 Analysis Method: EPA 7471
QC Batch Method: EPA 747.1 Analysis Description: 7471 Mercury
Associated Lab.Samples: 92217262001, 92217262002
METHOD BLANK: 1285880 Matrix: Solid
Associated Lab Samples: 92217262001; 92217262002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0050 .09/18/141258
LABORATORY CONTROL SAMPLE:-1285890
Spike LCS LCS % Rec :
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg .067 0.056 84 80-120
MATRIX SPIKE & MATRIX SPIKE, DUPLICATE: 1285891: 1285892
MS MSD
92216652001 Spike Spike MS ; MSD MS MSD %:Rec
Parameter Units Result Conc.. Conc. Result Result "/°, Rec- %Rec Limits RPD Qual
Mercury mg/kg ND .05 .049 0:034 0.031 62 58 75-125 -8 M1 -
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is'presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be -reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of,17

aceAnalytical
www.pwdabs.com
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9/12
Pace Project No.:. 92217262
Pace Analytical Services, Inc.
9800 Kincey Ave. ,Suite 100
Huntersville; NC 28078
[phone]
QC Batch: MPRP/16906
Analysis Method:
EPA 6010,
QC Batch Method: EPA 3050 .
Analysis Description:
6010 MET
Associated Lab Samples: 92217262001, 92217262002
METHOD BLANK: 1286250
Matrix: Solid
Associated Lab Samples: 92217262001, 92217262002
Blank
Reporting
Parameter
Units.
Result
Limit
Analyzed
Qualifiers
Arsenic
mg/kg
ND
_
1.0
09/17/14 02:35
Barium
mg/kg
ND
'0.50
09/17/14.02:35
Cadmium
mg/kg
ND
0.10
09/17/14.'02:35
Calcium
mg/kg
ND
.•
10.0
09/17/14 02:35
Chromium
mg/kg
ND
_
0.50.
09/17/14 02:35
Copper
mg/kg
ND
0.50
09/17/14 02:35
Iron
mg/kg.
ND'
.
10:0
69/17/14 02:35
Lead
mg/kg
ND
0.56
09/1.7/14 02:35
Magnesium
mg/kg
ND
10.0
09/1.7/14 02:35
Manganese
mg%kg
ND
0.50
09/17/14 02:35
Molybdenum
mg/kg
ND
0.50
09/17/1414:00
Nickel
mg/kg
ND
0.50
09/17/14 02:35
.Potassium
mg/kg
ND
500
• 09/17/14 02:35
Selenium
mg/kg
ND
1.0
. 09/17/14 02:35
Silver v
mg/kg
ND
0.50.
'09/17,/14 02:35
Sodium
mg/kg
ND
500
09/17/14 02:35
Zinc .
mg/kg"
ND
-1.0
09/17/14 02:35
LABORATORY CONTROL SAMPLE:
1286251
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits '' Qualifier,
Arsenic ,.
mg/kg
50
48:7
97
80-120
Barium
mg/kg
50
50.5
101
80-120.
Cadmium
mg/kg
50
48.8
98
80-120
Calcium
mg/kg
500
485
97
80-120
Chromium
mg/kg
50
48.8
98
80-120
Copper
mg/kg
50
50.6
101
80120. "
Iron
mg(kg
500
50.0
100
80-120-
Lead
mg/kg
50
49.5.
99
80-120
Magnesium
mg/kg
500
512.
102
80.120
Manganese
mg/kg
50
49.1
98
80-120
Molybdenum
mg%kg
50
52.0
106
80-120
Nickel
mg/kg
50
49.7
99
80-120
Potassium
mg/kg
560
496J ..
99
80-120
Selenium
mg/kg
50
49.8
100
80-120
Silver
mg/kg
25
24.4
98
80-120
Sodium
mg/kg
500
486J
97
80-120
Zinc
mg/kg .
50
47.8
96
80-120
Results presented on this page.are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc..
Page 8 of 17

aUuAnaiXical
www.paWabs.com
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9/12
Pace Project No.: 92217262 .
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX
Parameter
SPIKE DUPLICATE: 1286252
MS
92217197001 Spike
Units Result Conc:
MSD
Spike
Conc.
1286253
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
ND
239
239
237
239
99
100
75-125
1
Barium
mg/kg
284
239
239
540
512
107
95
75-125
5
Cadmium
mg/kg
ND
239
239
222
222
93
93
75-125
0
Calcium
mg/kg
21600
2390
2390
25200
22900
151
55
75-125
10 M1
Chromium
mg/kg
11.6
239
239
241
237
96
95
75-125
2
Copper
mg/kg
378
239
239
653
615
115
99
75-125
6
Iron
mg/kg
3470
2390
2390
5820
5510
98
86
75-125
5
Lead
mg/kg
5.9
239
239
228
228
93
93
75-125
0
Magnesium
mg/kg
2730
2390
2390
5280
5010
107
96
75-125
5
Manganese
mg/kg
140
239
239
374
361
98
92
75-125
4
Molybdenum
mg%kg
9.9
239
239
237
240
95
96
75-125
1
Nickel
mg/kg
8.4
239
239
236
236
95
95
75-125
0
Potassium
mg/kg
ND
2390
2390
4880
4620
139
128
75-125
5 M1
Selenium
mg/kg
4.8
239
239
252
247
103
101
75-125
2
Silver
mg/kg
2.6
119
119
119
119
98
98
75-125
0
Sodium
mg/kg
ND
2390
2390
3800
3590
123
114
75-125
6
Zinc
mg/kg
629
239
239
906
844
116
90
75-125
7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall 'not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc..
Page 9 of 17

a
Pace Analytical Servicesi Inc.
9/n/1e
G �/le' 9800 Kincey Ave. Suite 100
GiVr
snanvpeceleDs.com Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9/12
Pace Project No.: 92217262
QC Batch: MPRP/16923
Analysis Method: EPA 6010
QC Batch Method: EPA 3010
Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92217262061; 92217262002
METHOD BLANK: 1288252
Matrix: Water
Associated Lab Samples: 92217262001, 92217262002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Arsenic
mg/L
ND 0.050 .09/19/14'01:04
Barium
mg/L
ND 0.25
09/19/14 01:04.
Cadmium
mg/L
ND 0.0056
09/19/14.01:04 .. .
Chromium
mg/L
ND .0.025'
09/19/14 01:04
Lead
mg/L
ND 0.025,
09/19/14 61:64
Selenium .
mg/L
ND 0.10
.09119/14 01:04
Silver
mg/L
ND 0.025
09/19/14 01:04 .
LABORATORY CONTROL SAMPLE: 1298253
Spike
LCS
LCS
% Rec
Parameter
Units.
Conc.
Result
% Rec
Limits
Qualifiers
Arsenic
mg/L
2.5
2.6
106
80A20
Barium
mg/L
2.5
2.5
100
80-120
Cadmium
mg/L .
2.5
2.6
104
80-120
Chromium
mg/L
2.5
2:5
100
80-120
Lead
mg/L
2.5
2.A
97
80-120
Selenium
rng/L
2.5
27
107
.. 80-120
Silver
mg/L
1:.2
1.3
102
80-120
MATRIX SPIKE B,MATRIXSPIKE DUPLICATE:
1288254 _
1288255
MS
MSD;
92216155001
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units Result
. Conc.
Conc.
Result
Result
% Rec .. %Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.7
2.7.
101
107
- 75-125
0
Barium
mg/L
3.8,
2.5
2.5
6.3
6.5
101
110
75-125
3
Cadmium
mg/L
0.21
2.5
2.5
2.8
2.9
10.5
106
.75-125
1
Chromium
mg/L
ND
2.5
2.5
2.5
2.5
99
100
75-125.
1
Lead
mg/L
3.9
2.5
2.5
6.2
6.4
92
99
75-125
3
'Selenium
mg/L
ND
2.5
2.5
2.7
2.7
108
108
75-125
0
Silver
rrig/,L
ND
1.2
12
1.3
1.3
103
104
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is'presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 17

acMnalyiical
wlnp wacelabs.com
Project: Wood Boiler Ash 9/12
Pace Project No.: 92217262
QC Batch: PMST/7035
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92217262001, 92217262002
SAMPLE DUPLICATE: 1285024
Parameter Units
Percent Moisture %
SAMPLE DUPLICATE: 1285025
Parameter
Percent Moisture
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92215495001 Dup
Result Result RPD Qualifiers
39.6 29.4 29 R7
922172620.02 Dup
Units Result Result
% 44.8 45.6
RPD
Qualifiers
2
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc..
Page 11 of 17

PaceAnalytiaal Services; Inc.
acewwwpscelab cornAnafyt�cal 980.0 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9/12
Pace Project No.: 62217262
QC Batch WET/33166 Analysis Method- EPA 9045
QC. Batch Method: EPA 9045 Analysis Description: .9045 pH
Associated Lab Samples: 92217262001, 92217262002
SAMPLE DUPLICATE: 1285152
92217262001 -DUp
Parameter Units Result Result RPD Qualifiers.
pH at 25 Degrees C Std. Units 9.1 9.1 0-HI
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report, shall not be reproduced, except in full,
Date: 09/22/2014 11:09 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 17

aceAnalytical
www.pace/abscom
QUALITY CONTROL DATA
Project: Wood Boiler Ash 9/12
Pace Project No.: 92217262
QC Batch: WETA/20300 Analysis Method: EPA365.1'
QC. Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92217262001, 92217262002
Pace Analytical Services, Inc.
98,00I(inceyAve. Suite 100
Huntersdilla, NC 28078
[phone]
METHOD BLANK: 1289341
Matrix: Solid
Associated Lab Samples: 92217262001i'M17262002
Blank
Reporting
Parameter Units.
Result
Limit
Analy2ed Qualifiers
Phosphorus mg/kg
ND 2.0
09/21/1411:13
LABORATORY CONTROL'SAMPLE: 1289342
Spike
LCS
LCS %Rec
Parameter Units
Conc.
Result
% Rec Limits Quaimers
Phosphorus Trig/kg
'50
51.9
104. 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:. 1289343
1289344
MS
MSD
92216551001
Spike
Spike MS
MSD' MS, MSD %•Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec %Rec Limits RPD Qual
Phosphorus mg/kg 178
229
215 333
381 68 95' 90-110 .14 M1,R1
Results presented on this page, are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014' 11:09 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 17

i
Baxter Healthcare, Corp.
2859-Old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet — Return this sheet to Ricky Styles.
Baxter Healthcare, Corp.,; is the generator of the ash provided to `(/ :
(Recipient). Application of the aforementioned ash is prohibited e e Pt in accordance
instructions on this sheet.
Transport.- Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash. in. leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessaryunder windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited. to..
that needed ,to meet the liming requirements of the crops being grown on the land). .
Ash shall not be placed within 50 feet of any surface water. .
• Ash shall not be placed within one foot of the seasonal high water table:
•. Ash shall not be placed within- 100 feet of any water supply well, or spring unless underlain and
overlain by a liner with a maximum hydraulic. conductivity of 10"6 centimeters per second. 'If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or. spring.
• The ash shall, not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon _delivery. thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify; save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys'- fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party,, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
'Signed (Ash-R.ecipient): / Date:
Ash Recipient's Address:
t �r
Intended Use of Ash:
Expected. Qty/Yr: ��® '� Acres of Land:
Page 1 of 3
Updated: 3/5/12

ro
Baxter
Marien,,Nar i Carolina 28 75,
Ash Distribution Program Information Sheet
Baxter Healthcare, Corp., is the generator of the ash provided to
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and. hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
Wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, _berins, barriers, or tarps, may be necessary under windy or :rainy conditions or if
erosion or runoff cannot be controlled. -
Application: When using ash, the following shall apply:
The ash application rates shall be limited. to those that can -be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
- • Ash shall not be -placed within 50. feet of any surface water:
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 , of the information sheet. Detailed,
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shallnot be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered: by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Banter Healthcare, .Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter. Healthcare, Corp. by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): J e r,� 6�! ; /� w �� f2L y Date: _ . ��17
Ash Recipient's Address:
Intended Use of Ash:
Expected Qty/Yr:5 Acres'of Land:
Page 1 of 3
Updated: 3/5/10

axter Healthcare, Corp®
2559 Old Linville Road
Marion, forth Carolina 25752
Ash Distribution Program Information Sheet, Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to 6' i A �
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
e The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to
that needed, to meet the liming requirements of the crops being grown on the land).
• Ash, shall not be placed within 50 feet of any surface water.
® Ash shall not be placed within one foot of the seasonal high water table.
® Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
® The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim; demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient):Date: '7®21— 04_
Ash Recipient's Address: 7.%�i1v0 , le 12(),9 d
Intended Use of Ash: �® `�! ��a� 1�e ✓�
/YYr: Expected Qt �J p y � ��� ZPA/ Acres of Land: /Ede -
Page 2 of 3
Updated: 9-12-13

axter Healthcare, Corp.
2559 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Program Information Sheet — Return this sheet to Ricky Styles
Baxter Healthcare, Corp., is the generator of the ash provided to
(Recipient). Application of the aforementioned ash is prohibited exce t in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e,g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10"6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the, information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
.Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all, liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): COW Aoe.
Date: L' 30
Ash Recipient's Address: /V '; z�"
Intended Use of Ash: .,.,C ta-``
Expected Qty/Yr: Acres. of Land: //
Page 1 of 3
Updated: 3/5/12

Baxter Healthcare, Corp®.
2859 Old Linville Road -
Marion, North Carolina 28752
Ash Distribution Program Information Sheet
Baxter, Healthcare, Corp., is the generator of the ash, provided to )�N G t ZS A A�Z 2 Y A�
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport. Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ashin leak -proof trucks or cover dry ash).
Storage: The ash shall'be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under 1'Iormal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
-;4
Application: When using ash, the following shall apply:
The ash application rates skull be limited to those that can be.agronom'ically justified (i.e.; lilt jted: to i }
that needed to. meet the liming requirements of the crops being grown -on the'land).
e Ash shall not be placed within 50 feet of any surface water.
Ash shall not be placed within one foot of the seasonal high water table. ,
• Ash shall not be placed within 100. feet of any water supply_ well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10"6 centimeters per second. If such a
liner/cover is provided, ash shall not beplaced within 25 feet of any water supply well or spring.
e The ash shall not be applied to any site that is flooded, frozen, or snow-cover9d.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available .upon request..
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill,, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is -being delivered by Baxter Healthcare, Corp to Recipient a an accommodation to
Recipient. In exchange therefore. Recipient agrees to indemnify, save and hold Baxter Iealthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (includint,attomeys' fees),
claim; demand,, suit, action, judgment .or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
A
Signed. (Ash Recipient): Date: Z Z S "!, .3
Ash Recipient's :address: U A1a {
7.S z
Intended Use of Ash::
Expected Qty/Yr: Acres'of Land: 3 561
Page 1 of 3
Updated: 3/5/10

Baxter kllealthcare, Corp,
Ash Distribution Program Information Sheet
Baxter Healthcare, Corp., is the generator of the ash provided to
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash
into any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
® The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming requirements of the crops being grown on! the land).
® Ash shall not be placed within 50 feet of any surface water.
® Ash shall not be placed within one foot of the seasonal high water table.
® Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and
overlain by a liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a
liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring.
® The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): Date:
Ash Recipient's Address:
Intended Use of Ash:
Expected Qty/Yr: l2 j l �Z: 06 ,,-.t
IJ Page l of 3
Acres of Land: 66
�4 i71�
Updated: 3/5/ 10