WQ0010615_Residual Annual Report 2014_20150209

G\
_ a
r
m
1974
V
Facility Name
o-s
q"owBs of3Yaggie 4T%alley.
Phone [phone] • Fax [phone] Soco Rd., Maggie Valley, NQ� 28751
NPDES Permit. #
NC Water Quality #
Responsible Official
Operator
Engineer
Dry Tons Processed in 2014
Dry Tons Stockpiled in 2014
Plant Location
Town of Maggie Valley
Wastewater Treatment Plant
NCO056561
WQ0010615
Nathan Clark
Town Manager
Town of Maggie Valley
3789 Soco Road
Maggie Valley, NC 28751
828-926-0866 ext. 103
Michael Mehaffey
94 Indian Springs Road
Clyde, NC` 28721
828-926-0866 ext. 102
McGill Associates, RA.
Post Office Box 2259
Asheville, NC 28802 '
828-252-0575
280 Dry Tons
0 Dry Tons
5320 Jonathan Creek Road
Waynesville, NC 28785
RMYEDIDENPOR
FEB 7 9 2015
W�rQu�lii
,out

ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
PERMIT #: 146010 0_5'� FACILITY NAA
PHONE: 9 -c/,?� �j f COUNTY: Q way OPEAA TOR: �4 a • �
FACILITY TYPE (please check one): 0 Surface Disposal (complete Part A (Source(s) and "Residual In'(Volume only) and Part C)
lid Distributio and Marketing (complete Parts A, B, and C).
Was the facility in operation during the past calendar year? (wYes ❑No No If No skip parts A, B, C and certify form -below
Part A*:
Month
October
Sources(s) (include NPDES # if
applicable)
Volume
Residual In I Product Out
t( 77—
76/1S �+a2.
1 y funs im-e..
Bv�S
/y ,1, 5
#�jts
8 to«s
i
i T
c( t
q4( n S
I
4 *A3
r
36 fVA5
��- �1)s
c
1 t !
01 Y kfis `�n e
o� y Apr*
J/9 fowS
r �
I
Part B :
Recipient Information
Name(s) Volume (dry tons) Intended use(s)
I(
* If more space than given is required, please attach additional information sheet(s). ❑ Check box if additional sheet(s) are attached
Part C:
Facility was compliant during calen ar year Z/J-{ with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Resources. 19Yes ❑ No If No, please provide a written description why the facility was not compliant. ant.
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water
Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware
that there a i ' is t penalties for submitting false information, includi t e possibility o fi s and imprisonment for knowing violations."
Signatur of ermittee '41—
Date Signature of Prepazer** Date
(if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r)
DENR FORM DMSDF (11/2005)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized an +hic fnv-m
Permit Number:/� f AQ/Mv /-
Facility Name: 7e'c,/,t/ _o Wlf ; tj,
NPDES # or v ✓ f
WQ#: ".Irfr
WWTP Name:
Residual Analvsic Data
Laboratory: 1)„r�% r.F°tc�,✓,✓!� P�t�
4)ac�2/;S Cu �lc�v �fI!/U�✓Ldledp/
5)
a
Sample or
Composite Date
Percent Solids
/, �e
.541®
�0
�,D90
Arsenic
q 50
Cadmium
.e /, yq
Chromium
40, ps-
Copper
Lead
6,
Mercury
,gyp,/g
y
B
Molybdenum
at cf
Nickel
/a, g
Selenium
,� q �3
Zinc
LL7
Total Phosphorus
3 %0
TKN
9100
Ammonia -Nitro a
%0
Nitrate and Nitrite
�!L_
x eer«iy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer
Date
11CAIG Cr%mne moor- ir..,.......

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on, this form.
Permit Number: jtl(`� QO�Qj/,� Laboratory:
Facility Name: W.✓ /�1a 1i'
NPDES # or 3) �,,°✓v�r�1� / eS�vjtts,�s�
wQ#:
WWTP Name: �,�,/.r/ p 7,
Cic�Ci�C' l��1 le y 5) Aae, � OL e4r IleV7'1
Residual Analvsis Data
.. • le 's . -
'
----
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Prepay
Date
DENR FORM RSSF-R rr%19nna\

Earth Environmental Services
Michael Ladd
75 Bison Lane
Murphy, NC 28906
Robbinsville Lab [phone]
Weaverville Lab [phone]
Residence [phone]
Name and Address of Facility:
Date:
Town of Ma ie Valley
1/12/2015
3987 Soco Road
Sample Collector.
ML
Maggie Valley, NC 28751
Date and Time Sample Received:
8/26/2014 11:20 AM
Aft: Mike McHaffey
Date and Time Sample Collected:
8/26/2014 11:20 AM
Date Time Sample Analyzed:
Note: ALL Results In MG/KG Dry Basis Unless
< MHT
Otherwise Notedd
Influent Cl. A Biosolids
Report Lim" Method
Units
SPENDED RESIDUE
2.0
SM5210B
mg/L
LIFORM
1.0
SM2540D
mg/L
< 104
104
SM9221 E
MPN/Gra
NITROGEN
F02+NO3-N
11.9
0-14
SM90450
units
-N
170
6.9
SM400 NH3 D mg/Kg
ELDAHL NITROGEN
44.74
38.860 EPA 6010 C rn
OSPHOROUS
9700
324
EPA 351.2mg/Kg
(DRY WEIGHT)
3290OLIDS
189
EPA 6010 C
mg/Kg
NO3-N
58.0%
0.1 %
SM2510 G
%
TOTAL DISSOLVED RESIDUE 180 C
3.6
SCA
SETTLEABLE RESIDUE
1.0
SM2540C
mg/Kg
SAR
0.1
SM254OF
ml/L
•
0.342422
N /A
CALC
PAN - SURFACE
3941.74
PDM DRY
NIA
CALC
wr
PAN SUBSURFACE
4026.74
PDM DRY
MIXED LIQUOR SUPSPENDED SOLIDS
N/A
CALC
WT
CALCIUM
356,000
1.00
NIA
mg/L
ALUMINUM
11800
EPA 6010 C
mg/Kg
CADMIUM
6570
237
EPA 6010 C
mg/Kg
CHROMIUM
< 1.89
1.89
EPA 6 010 C
mg/Kg
COPPER
EPA 6010 C
rn Kg
'�D
1.22
1.89
EPA 6010 C
mg/Kg
JICKEL
6.25
4.73
EPA 601'0 C
mglKg
:INC
12.9
1.89
EPA 6010 C
mg/Kg
PODIUM
12.1
4.73
EPA 6010 C
mg/Kg
'OTASSIUM
743
473.0
EPA 6010 C
mg/Kg
IAGNESIUM
2740
9.74
EPA 6010 C
mg/Kg
RSENIC
< 4.73
4.73
EPA 6010 C
mg/Kg
�
ELENIUM
4.80
4.73
EPA 6010 C
mg/Kg
OLYBDENUM
< 4.73
4.73
EPA 6010 C
mg/Kg
ERCURY
12.9
1.89
EPA 6010 C
mg/K9
C. Laboratory ID# 352
< 0.18
0.18
EPA 7471 B
mg/Kg
Analyzed By. MB
b Supervisor: Michael J. Ladd; EES-Robbinsville
Certified By: /
o�-

PAN
Rate
0.4
Maggie Valley Class A Biosolids 8/26/14
9700 170 I 42.4 I 2.34
PAN Surface
3941.74 m /k
7.88348 Ibs/d ton
0
Ibs total PAN
#DIVIO!
Ibs PAN/acre
PAN In'ection
4026.74 mg/k
8.05348 Ibs/d ton
0
Ibs total PAN
#DIV/01 Ibs PAN/acre
D Tons/1000 al.
2.4186
1st year PAN
Ibs./acre
Surface Ibs.
0
Surface
#DIV/0!
1st year PAN
Ibs./acre
in" ected Ibs.
0
Injected
#DIV/0!
bouas I tons/ ear I ARO ed on
0.58
MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibs/dry ton
MR(TKN-NH3) + 1(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibs/dry ton
1000 X 8.34 X %solids X so aravi "=dry tons/1000gal."
2000

SAR & ESP Maggie Valley Class A Biosolids 8/26/14
Sodium Absorption Ratio
Na: Sodium (Mg/L) Equivalent weight: 23
Na M /L Ca(Mq/l I M M /L
Ca: Calcium (Mg/L) Equivalent weight: 20
1 743 1 ;560001 1
4.73
Mg : Magnesium (Mg/L) Equivalent weight: 12
Na ME
1
Ca ME Mom
Milli Equivalent = Mg/L / Equivalent weight
32.30435
17800
10.394167
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 0.342422 (From Mg/L entered above)
SAR= 0.342422 (From ME entered below)
Na ME Ca ME Mo I E�
32.30435 17800 0.394167
The amount of exchangeable sodium ions versus the
amount of exchangeable calcium & magnesium ions in a given
material.
Permitting guidance is if greater than 10. require ESP in permit.
ESP = � (Milli Equivalents) / CEC X 100
The percentage of sodium ions occupying the cation exchange complex of soils
A
ESP = 1. 4564 0
Na on NC soil test is expressed as meq. Should be less than 15% (15-20%)
N\�
.1Z

Earth Environmental Services
I
Michael Ladd
75'Bison Lane
Murphy, NC 28906
Robbinsville. Lab [phone]
Weaverville Lab [phone]
Residence [phone]
Name and Address of Facility:
Town of Maggie Valley WWTP
3987 Soco Road
Maggie Valley, NC 28751
Aft: Mike McHaffe
Class A Biosolids - TCLP
Date: 1/12/2014
Sample Collector:
ML
Date and Time Sample Received:
8/26/2014 11:20 AM
Date and Time Sample Collected:
8/26/2014 11:20 AM
Date and Time Sample Analyzed:
< MHT
t
Influent CI. A Biasolids Upstream Downstream Report Lim'
11.90-14
Method
Units
r
- 8151jBjj
EPA9045C
units
< 0.0003 0.0003
SCAm
- 8260
< 0.200
EPA 8270 D
0.200
SCA
mg/L
< 0.200 0.20n
ere
CPA 5031 B
I< 0.0050 1
0.0050
SCA
cORROSIVITY
NOT CORROSIVE
mg/I
IGNITABILITY
< 0.8
SCA
PAINT FILTER TEST
< 0.1
0.8
SW8461030
mm/sec
TOTAL REACTIVE CYANIDE
< 0.05 m /K �
0.1
SWI346 9095E
ml
CADMIUM
0.05
EPA335.4
mg/Kg
CHROMIUM
< 0.05
0.05
EPA6010C
mg/L
< 0.10
0.10
EPA6010C
mg/L
LEAD
< 0.25
0.25
EPA6010C
mg/L
SILVER
< 0.10
0.10
EPA6010C
mg/L
.REACTIVE SULFIDE
2.59
0.259
SM4500SD
mg/Kg
BARIUM
< 2.50
2.50
EPA6010C
mg/L
ARSENIC
< 0.25
0.25
EPA6010C
mg/L
SELENIUM
< 0.25
0.25
EPA6010C
mg/L
MERCURY
< 0.0020
0.0020
EPA7470A
mg/L
V.C. Laboratory ID# 352
Analyzed By:
MB
.ab Supervisor. Michael J. Ladd; EES-Robbinsville Certified By:

F TS
Environmental Testing Solutions, Inc.
Project name: Earth Environmen
96&ILA
Collection date: -64-
Date received: 26-Aug-14
Sample identification: #081423
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
of Analysis
ices I Project number: 140826.531
C(a SS A
Sample number: 119634
Par,>lfm�i'er Method I Result RL Units Date Analyst Footnotes
LL // Analyzed
Cyanide
Sulfide
--TCLP
z TCLP
m -TCLP
urn - TCLP
CCLP
n - TCLP
TCLP
F - TCLP
;LP Organics
Is
ite
To hosphorus
Total Kjeldahl Nitrogen
iia Nitrogen
Solids
Fecal
335.4
SM 4500 S
SW 84610.'
SW846 9095
9045 D
6010 C
6010 C
6010 C
6010 C
6010 C
6010 C
6010 C
6010 C
See a
SM 2540
7471B
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
6010C
351.2
SM 4500 NIP D
SM 2540
SM 9921
<0.05
0.05
rrig/kg
rl-Sep.14
ECHEM
2.59
mg/kg
4-Sep-14
ECHEM
<0.8
0.8
mm/sec
3Sep-14
ECHEM
<0.1
0.1
ml
27-Aug-14
KEK
11.9
S.U.
26-Aug-14
KW
<0.25
0.25
mg/L
29-Aug-14
MEC
<2.50
2.50
mg/L
29-Aug-14
MEC
<0.05
0.05
mg/L
29-Aug-14
MEC
<0.10
0.10
mg/L
29-Aug-14
NEC
<0.25
0.25
mg/L
29-Ai 14
MEC
<0.25
0.25
mg/L
29-Aug-14
MEC
<0.10
0.10
mg/L
29-Aug-14
MEC
<0.0020
0.0020
mg/L
2-Sep-14
DER
sheets
52.0
0.10
%
27-Aug-14
MLR
<0.18
0.18
mg/kg
2-Sep-14
DER
6570
237
mg/kg
"ep-14
MEC
4.80
4.7
mg/kg
4-Sep-14
MEC
<1.89
1.89
mg/kg
4-Sep-14
MEC
356000
11800
mg/kg
14-Sep-14.
MEC
122
1.89
mg/kg
4-sep-14
NEC
6.25
4.73
mg/kg
"op-14
MEC
2710
237
mg/kg
4-scp-14
MEC
<4.73
4.73
mg/kg
4-Sep-14
MEC
12.9
1.89
mg/kg
4-sep44
MEC
2740
9.74
mg/kg
4-Sep-14
MEC
<4.73
4.73
mg/kg
4-Sep-14
MEC
743
473
mg/kg
4-Sep-14
MEC
121
4.73
mg/kg
4-sep-14
MEC
44.74
38.86
mg/kg
29-Aug-14
3290
189
mg/kg
4-Sep-14
MEC
9700
324
mg/kg
4-Sep-14
LDP
9740
324
mg/kg
4-Sep-14
LDP
170
6.9
mg/kg
28-Aug-14
KEK
58
%
26-Aug-14
KW
<104
104
%
27-Aug-14
KEK
not be reproduced, exept in its a tirety, without the written consent of Environnrei
The results in this reporq relate only to the samples submitted for analysis.
2
2
2
3
1
1
1
l
1
1
1
1
1,2
1
1
1
1
1
1
I
1
1
1
1
1
1
1
1
1,4
1
1
I

r
Rogers & Callcott
Wh-F__
ENVIRONMENTAL
Environmental Testing Solutions Project: Earth Environmental Services
351 Depot St. Work Order: 4081001
Asheville, NC 288014310 Reported: 09/11/14 14:50
Sam le Data
Sample Number 4081001-01
Sample Description Earth Environmental Services #081423 collect d on 08/26/14 11:20
Reporting
Parameter Result Limit Units DF Analyzed Method Flag Analyst Bateb
TCLP Metals
Mercury
ND
0.0020
mg/L
10.0
00/02/14 10:59
EPA 7470A
DER
B410009
Arsenic
ND
0.25
mg/L
5.00
09/29/14 11:35
EPA 6010C
MEC
B41­10990
Barium
ND
2.50
mg/L
5.00
08/29/14 11:35
EPA 6010C
MEC
B4H0990
Cadmium
ND
0.05
mg/L
5.00
08/29/14 11:35
EPA 6010C
MEC
B4H0990
Chromium
ND
0.10
mg/L
5.00
09/29/14 11:35
EPA 6010C
MEC
B4H0990
Lead
ND
0.25
mg/L
5.00
08/29/14 11:35
EPA 6010C
MEC
B41­10990
Selenium
ND
0.25
mg/L
5.00
08/29/14 11:35
EPA 6010C
MEC
B4H0990
Silver
ND
0.10
mg/L
5.00
0829/14 11:35
EPA 6010C
MEC
B4H0990
TCLP Volatile Organics
Benzene
ND
0.100
mg/L
50.0
09/02/14 16:03
EPA 8260B
LBW
B410342
2-Butanone (MEK)
ND
0.200
mg/L
50.0
09/02/14 16:03
EPA 8260E
LBW
13410342
Carbon tetrachloride
ND
0.100
mg/L
50.0
09/02/14 16:03
EPA 8260B
S 1 LBW
B4I0342
Chlorobenzene
ND
0.100
_91L
50.0
09/02/14 16:03
EPA 8260B
LBW
B4I0342
Chloroform
ND
0.100
mg/L
50.0
09/02/14 16:03
EPA 9260E
LBW
B4I0342
1,2-Diebloroethane
ND
0.100
mg/L
50.0
09/02/14 16:03
EPA 8260E
LBW
B410342
IA-Dieblorobenzene
ND
0.100
mglL
50.0
09/02/14 16:03
EPA 8260B
LBW
B410342
1.1-Dichloroethene
ND
0.100
mg/L
50.0
09/02/14 16:03
EPA 8260B
LBW
B4I0342
Tetrachloroethene
ND
0.100
mg/L
50.0
091OV14 16:03
EPA 8260E
LBW
B410342
Trichloroethene
ND
0.100
mg/L
50.0
09/02/14 16:03
EPA 8260B
LBW
B410342
Vinyl chloride
ND
0.100
mg/L
50.0
09/02/14 16:03
EPA 8260B
LBW
B410342
Surrogates
%REC
%REC Limits
Flag
1,2-Dicbloroethane-D4
97
70-130
Toluene-D8
88
70-130
a-BrontnjGmmbeir-eae
98
70-130
TCLP Semi -Volatile Organics
2-Methylphenol (o-Cresol)
ND
0.100
mg/L
10.0
09/10/14 00:20
EPA 8270D
RJM
B410152
3/4-Methylphenol (m,p-Cresol)
ND
0.100
_WA
10.0
09/10/14 00:20
EPA 8270D
RJM
B410152
total Cresol
ND
0.200
mg/L
10.0
09/10/14 00:20
EPA 8270D
RIM
B410152
1.4-Dinitrotoluene
ND
0.100
mg/L
10.0
09/10/14 00:20
EPA 8270D
RIM
B4I0152
Hexachlorobenzene
ND
0.100
mg/L
10.0
09/10/14 00:20
EPA 8270D
RJM
B410152
Hexachlorobutadiene
ND
0.100
mg/L
10.0
09/10/14 00:20
EPA 8270D
RJM
B410152
Hexachloroethane
ND
0.100
mg/L
10.0
09/10/14 00:20
EPA 9270D
RJM
B4I0152
Nitrobenzene
ND
0.100
mg/L
10.0
09/10/14 00:20
EPA 8270D
RJM
B4I0152
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforesc Way
Green Ile, SC 29607 1
main 864-232-1556 i fax [phone] rogersandeallcott.eom
-- -
-
- - -
-
- - -- -�-
an employee -owned company
09.71,701,1 14:50
This report may not he reproduced, ecce r in fill, without written permission from Rogers X
Callcott, Inc.

Rogers & Callcott
"r-: - - ENVIRONMENTAL
Environmental Testing Solutions
351 Depot St.
Asheville. NC 28801-4310
Project: Earth Environmental Services
Work Order: 4081001
Reported: 09/11/14 14:50
Sample Number 4081001-01
Sample Description Earth Environmental Services #091423 collecte on 09/26/14 11:20
Parameter Reporting I
Result Limit Units DF Analyzed
TCLP Semi -Volatile Organics
Pentachlorophenol ND 0.100
Pyridine ND 0.100
2.4,5-Trichlorophenol ND 0.100
214.6-Trichlorophen.ol ND 0.100
Surrogates
2-Fhrorobiphei{vl
2-Fhmrophenol
phenol -US
Z4.6-Tribmmophenol
TerpheWry DI4
TCLP Pesticides
Gamma-BHC (Lindane)
Chlordane
Endrin
Heptachlor
Heptachlor epoxide
Toxaphene
Methoxychlor
Surrogates
--u-1 emacntorn-m xylene
Decachlomhipheiryl
ND 0.00050
ND 0.0050
ND 0.00050
ND 0.00050
ND 0.00050
ND 0.0050
ND 0.00050
mg/L 10.0
09/10/14 00:20
mg/L 10.0
09/10/14 00:20
_91 10.0
09/10/14 00:20
mg/L 10.0
09/10/14 00:20
%REC
% REC Limits
61
35-114
61
43-116
37
21-110
27
10-110
88
10-123
70
33-141
mg/L
10.0
09/10/14 04:34
m8/L
10.0
09/10/14 04:34
mg/L
10.0
09/10/14 04:34
mg/L
10.0
09/10/14 04:34
m81L
10.0
09/10/14 04:34
m9/L
10.0
09/10/14 04:34
m9/1.
10.0
09/10/14 04:34
%REC
%REC Limits
79
60-130
82
30-150
Method Flag Analyst Batch
EPA 8270D
RJM
B4I0152
EPA 8270D
P2 RJM
B4I0152
EPA 8270D
RJM
B4I0152
EPA 8270D
RJM
B410152
me..
EPA 8081B
EPA 8081B
EPA 8081B
EPA 8081E
EPA 8081B
EPA 6081E
EPA 809113
Flag
RKH B4I0133
RICH 134I0133
RICH B4I0133
RKH B410133
RKH 134I0133
RKH B410133
RICH B4I0133
PO Box 5655 1 Greenville, SC 29606 1 426 FairfOreSrWay : Greenville, C 29607 1 rmair. 864.232.1556 . fax 864.232,6140
Y rogersandcallcott.com
�"""""'�- --- an employee -owned company
09112014 14:50 This report may not be reprt/ducet{ except in dl, without written permission from Rageee & C'allcon, Inc.
Page 4 of 1

Rogers & Callcott
n7t,- ENVIRONMENTAL
Environmental Testing Solutions Project: Earth Environmental Services
351 Depot St. Work Order: 4081001
Asheville, NC 28801-4310 Reported: 09/11/14 14:50
Sample Number 4081001-02
Sample Description Earth Environmental Services #081423 collect d on 08/26/14 11:20
Reporting
Parameter Result Limit Units DF
General Chemistry Parameters
Nitrate as N, extractable
Nitrite as N, extractable
Total Kjeldahl Nitrogen
Total Nitrogen (TKN+Nitrate+Nitrite)
Total Solids
Total Metals
Mercury
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Total Phosphorus as P
Zinc
42.4 38.1
2.34 0.76
9700 324
9740 324
52.0 0.10
ND 0.18
6570 237
4.80 4.73
ND 1.89
356000 11800
122 1.89
6.25 4.73
2710 237
ND 4.73
12.9 1.89
2740 9.47
ND 4.73
743 473
3290 189
121 4.73
Analyzed Method
Flag Analyst Batch
mg/kg dry
5.00
08/29/14 10:20
EPA 9210A
X LDP
B41-10979
mg/kg drY
10.0
08/29/14 14:35
SM 4500NO2B-2011
REH
B4I0013
mg/kg dry
10.0
09/04/14 14:09
EPA 351.2
LDP
B410006
mg/kg dry
10.0
09/04/14 14:09
-
LDP
B410004
%
1.00
08/27/14 14:16
SM2540G
MLR
B4H0986
mg/kg dy
5.00
09/02/14 14:54
mg/kg dry
50.0
09/04/14 12:03
mg/kg dry
1.00
09/04/14 12:06
mg/kg dry
1.00
09/04/14 12:06
mg/kg dry
2,500
09/04/14 14:31
mg/kg dry
1.00
09/04/14 12:06
mg/kgdry
1.00
09/04/14 12:06
mgtkg dry
50.0
09/04114 12:03
mg/kgdry
1.00
09/04/14 12:06
mg/kg drY
1.00
09/04/14 12:06
mg/kg dry
1.00
09/04/14 12:06
mg/kg dry
1.00
09/04/14 12:06
mg/kg dry
50.0
09/04/14 12:03
mg/lrk- dry
50.0
09/04/14 12:03
mg/kgdry
1.00
09/04/14 12:06
EPA 7471B
EPA 6010C
EPA 6010C
EPA 6010C
EPA 6010C
EPA 6010C
EPA 6010C
EPA 6010E
EPA 6010C
EPA 6010C
EPA 6010C
EPA 6010C
EPA 6010C
EPA 6010C
EPA 6010C
DER B410007
MEC B4I0032
MEC B4I0032
MEC B410032
MEC B410032
MEC B410032
MEC B410032
MEC B410032
MEC B410032
MEC B410032
MEC B410032
NEC B410032
MEC B410032
MEC B410032
MEC B4I0032
PO Box 5655! Greenville, SC 29606 E 426 Fairforesc Way 1 Green Ile, SC 29607 i rrnin 864.232.1556 fax [phone] rogersandcallcott.eom
09112014 14.50
an employee -owned company
This report may not he reproduced, ecce t in fill, without written permission from Ragem R C.'allcon, Inc. p.��... - .1

Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wilmington, NC 28405
® [phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Mantel, NC 27954
ANALYTICAL & CONSULTING [phone]
CHEMISTS NCDENR. DWQ CERTIFICATE #94 -DLS CERTIFICATE #37729
Environmental Testing Solutions, Inc.
Post Office Box 7565 _ Date of Report: Sep 11, 2014
Asheville NC 28802 Customer PO
Attention: Kelley Keenan (ETS) `ASS a' �� oSz `�-S Customer ID: 08100055
Report #: 2014-10516
Project ID: EES
Lab ID Sample ID: 081423
14-25894
Collect Date/Time Matrix Sampled by
Site:
- 8/27/2014
11:20 AM Solid/Sludge Client
Test
Method
Results
Date Analyzed
Sulfide
SM 4500 S D
2,4,5-TP
SW846 Method 8i51A
2.59 mg/kg
09/04/2014
2,4-D
sws46 method 8151A
<0.0003 mg/L
09/03/2014
RCI
<0.0003 mg/L
09103/2014
Ignitability
EPA 1030
Cyanide
EPA 335.4
<0.8 mm/sec
09/03/2014
Comment:
<0.05 mg/kg
09/11/2014
Reviewed by:
Report#:: 2019-1o51e
Page 1 of 1

-AI IlrUALrFkIX1Vhi4lr A1r10 VJ&UIVKAl IMAU-IIUN KUDUU'IIUN FORM
Facility Name: o � e G/a 1AV Permit Number:ya 00 106 /S--
WWTP Name: r,,,,/ o NPDES Number:
Monitoring Period: From /— / — 014( To
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 89
Alternativex
3
s`"
Alternative 413
Alternative 5 ❑
T Alternative 6 ❑'
If applicable to alternative performed (Class A only) indicate "Process
to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑.,x
Beta Ray ❑
Gamma Ray❑
Pasteurization ❑
Class B:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑rT?
If applicable to alternative performed (Class B only) indicate "Process
to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Di estion❑
ig
NEW— IMF
.. -x Y
If applicable to
alternative performed (Class A or Class B) complete the following monitoring data: .
Parameter
Allowable Level
in Sludge
Pathogen Densi
g �'
Number o
Excee-
ences
Frequency
of Analysis
Sample
T' a
YP
Analytical
Tech niqu
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the 6th
power NTN per
gram of total
solids or 2 x 10 to
the 6th power
CFU peraram of
1000 mpn per
gram of total solid
(dry weight)
L,D q
L/ 1�/
L /3
60
/ �'Y
Salmonella bacteria
(in lieu of fecal
coliform)
3 N?N per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ❑
Option 2 ❑Option
3 ❑
Option 4
❑ Option 5 ❑
❑ lion 1 ❑ ` ..
Op 0
Option 6 ❑
Option 7 ❑ Option 8
No vector attraction reduction performed were
o tions
P
Option 9
❑
1:�tt i it IUA 11 N N'1'A7'1GMLN1' (please check the appropriate statement)
I••J1 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ " I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment"
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Prep arer Date Signature of Land Applier (if applicable)
Date
DENR FORM RF (5/2003)

Earth Environmental Services
Michael Ladd
75 Bison Lane
Murphy, NC 28906
Robbinsville Lab [phone]
Weaverville Lab [phone]
Residence [phone]
Name and Address of Facility: Date: 1/22/2014
Town of Ma gie Valley Sample Collector. ML
3987 Soco Road Date and Time Sample Received: 1/16/2014 11:10 AM
Maggie Valley, NC 28751 Date and Time Sample Collected: 1/16/2014 11:10 AM
At Mike McHaffey Date and Time Sample Analyzed: < MHT
Note: ALL Results in MG/KG Dry Basis Unless nthermeme Nntad
Test
Influent
Cl. A Biosolids
Report Lim"
Method
Units
BOD
2.0
SM5210B
mg/L
TOTAL SUSPENDED RESIDUE
1.0
SM2540D
mg/L
FECAL COL• IFORM
< 110
110
SCA
MPN/Gram
pH
12.1
0-14
SCA
NITROGEN5.9
SCA
AunitsAMMONIA
NO2 + NO3 - N
7.4
SCA
TOTAL KJELDAHL NITROGEN
740
SCA
mg/Kg
TOTAL PHOSPHOROUS
37
SCA
mglKg
% TOTAL SOLIDS (DRY WEIGHT)
61 %
1 %
SCA
NO3-N
3.6
SCA
TOTAL DISSOLVED RESIDUE 180 C
1.0
SM2540C
mg/Kg
SETTLEABLE RESIDUE
0.1
SM254OF
mi/L
SPECIFIC CONDUCTANCE
10
SM25106
umhos/cm
PAN -SURFACE
NIA
CALC
rum DRY
WT
PAN SUBSURFACE
N/A
CALC
WT
MIXED LIQUOR SUPSPENDED SOLIDS
1.00
WA
rng/L
CALCIUM
2900
SCA
mg/Kg
ALUMINUM
37
SCA
mg/Kg
CADMIUM
3.7
SCA
mg/Kg
CHROMIUM
SCA
mg/Kg
COPPER
7.3
SCA
mg/Kg
LEAD
3.7
SCA
mg/Kg
NICKEL
15
SCA
mg/Kg
ZINC
37
SCA
mg/Kg
SODIUM
180
SCA
mg/Kg
POTASSIUM
180
SCA
mg/Kg
MAGNESIUM
37
SCA
mg/Kg
ARSENIC
7.3
SCA
mg/Kg
SELENIUM
37
SCA
mg/Kg
MOLYBDENUM
7.3
SCA
mg/Kg
MERCURY
0.030
SCA
mg/Kg
V.C. Laboratory ID# 352
-ab Supervisor: Michael J. Ladd; EES-Robbinsville
Analyzed By: MB
Certified By:

torch tovironmental Services
Michael Ladd
75 Bison Lane
Murphy, NC 28906
Robbinsville Lab [phone]
Weaverville Lab (828) 64"196
Residence [phone]
Name and Address of Facility: Date: 1/12/2015
Town Of Maggie Valley Sample Collector.
3987 Soco Road ML
Date and Time Sample Received: 8/26/2014 11:20 AM
Maggie Valley. NC 28751 Date and Time Sample Collected:
Aft: Mike MCHaffey 8/26/2014 11:20 AM
Note: ALL Results In MG/KG Dry Basis Unless Otherwise Ntoted d Time Sample Analyzed: < MHT
Test IInfluent I CL A Biosolids I Io
OTAL SUSPENDED RESIDUE
ECAL COLIFORM
[AMMONIA
< 104
11.9
NITROGEN
170
NO2 + NO3 - N
44.74
TOTAL KJELDAHL NITROGEN
9700
TOTAL PHOSPHOROUS
3290
TOTAL SOLIDS (DRY WEIGHT)
58.0°Io
NO3-N
TOTAL DISSOLVED RESIDUE 0180 C
SETTLEABLE RESIDUE
SAR
PAN -SURFACE
PAN SUBSURFACE
MIXED LIQUOR SUPSPENDED SOLIDS
".ALCIUM
4LUMINUM
:ADMIUM
:HROMIUM
TOPPER
.EAD
IICKEL
3NC
;ODIUM
OTASSIUM
IAGNESIUM
RSENIC
ELENIUM
OLYBDENUM
ERCURY
C. Laboratory ID# 352
b Supervisor: Michael J. Ladd; EES-Robbinsville
0.342422
3941.74
4026.74
i
356,000
6570
< 1.89
1.22
6.25
12.9
12.1
2.0
1.0
104
044
6.9
38.860
324
189
0.1%
3.6
1.0
0.1
N/A
Method
SM5210B
SM2540D
SM9221 E
SM400 NH3 D
EPA 6010 C
EPA 351.2
EPA $010 C
SM2510 G
Units
units
Z2540C mg/Ki
2540F mill.
CALC
NIA CALL WT
N/A
1.00
11800
237
1.89
1.89
4.73
1.89
4.73
473.0
2740
9.74
< 4.73
4.73
4.80
4.73
< 4.73
4.73
12.9
1.89
#0.18
< 0.18
Analyzed By: MB
41
Certified By:
CALC
NIA
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 6010 C
EPA 7471 B
WT

Each. Environmental Services
Michael Ladd
75 Bison Lane
Murphy, NC 28906
Robbinsville Lab [phone]
Weavervilie Lab [phone]
Residence [phone]
Name and Address of Facility:
Date: 4/21/2014
Town of Maggie Valley
Sample Collector: CL
3987 Soto Road
Date and Time Sample Received: 4/16/2014 9:35 AM
Maggie Valley, NC 28751
Date and Time Sample Collected: 4/16/2014 9:35 AM
Aft: Mike McH^y
Date and Time Sample Analyzed: MHT
Note: ALL Resuita In MC/KG nru Raare
r irrace rhhn ..A— u..&-.a
Test
Influent
Cl. A Biosolids
Report Limil
Method
Un"ds
BOD
2.0
SM5210B
mg/L
TOTAL SUSPENDED RESIDUE
1.0
SM2540D
mg1L
FECALCOUFORM.
< 117
117
SM9221E.
PN/Gram
pH
12.1
0-14
SM9045D
units
AMMONIA NITROGEN
6.9
EPA 350.3
mg/Kg
NO2 + NO3 - N
5.6
SM4500 NO3 F
mg/Kg
TOTAL KJELDAHL NITROGEN
276
EPA 351.2
mg/Kg
TOTAL PHOSPHOROUS
141
SM4500 P F
m K
% TOTAL SOLIDS (DRY WEIGHT)
65%
0.1 %
SM2510 G
%
NO3-N
3.6
SCA
TOTAL DISSOLVED RESIDUE @180 C
1.0
SM2540C
mg/Kg
SETTLEABLE RESIDUE
0.1
SM254OF
ml/L
SPECIFIC CONDUCTANCE
10
SM25108
umhosh:m
PAN -SURFACE
NIA
CALC
PDM DRY
WT
PAN SUBSURFACE
N/A
CALC
PDM DRY
WT
MIXED LIQUOR SUPSPENDED SOLIDS
1.00
N/A
mg/L
CALCIUM
17500
EPA 6010 C
mg/Kg
ALUMINUM
175
EPA 6010 C
mgiKg
CADMIUM
1.40
EPA 6010 C
mg/Kg
CHROMIUM
EPA 6010 'C
mglKg
COPPER
1.40
EPA 6010 C
mg/Kg
LEAD
3.50
EPA 6010 C
mglKg
MIC ­116
1.40
EPA 6010 C
mg/Kg
INC.1
ZINC
7.00
EPA 6010 C
mgFKg
SODIUM
14.0
EPA 6010 C
mg/Kg
POTASSIUM
350
EPA 6010 C
mg/Kg
MAGNESIUM
175
EPA 6010 C
mg/Kg
ARSENIC
3.50
EPA 6010 C
SELENIUM
3.50
EPA 6010 C
MOLYBDENUM
3.50
EPA 6010 C
lmgWlKg
MERCURY
0.14
EPA 7471 B
r.L.. L.UuUm my ix w a0z Analyzed By: MB
e
Ab Supervisor. Michael J. Ladd, EES-Robbinsville Certified By: '

Each Eoriromeotol Services
Michael Ladd
75 Bison Lane
Murphy, NC 28906
Robbinsville Lab [phone]
Weaverville Lab [phone]
Residence [phone]
Name and Address of Facility:
Date: 1/13/2015
Town of Maggie Valley
Sample Collector.
3987 Road
ML
Maggie Valley,
Valley, 28751
Date and Time Sample Received: 10/14/2014 12:00 PM
Aft: Mike
Att: Mike McHaffey
a
Date and Time Sample Collected: 10/14/2014 12:00 PM
Note: ALL Results In MG/KG Dry Basis Unless
Date and Time Sample Analyzed: < MHT
Otherwise
Noted
Test
IInfluent
CI. A Biosolids
Re ort L'
M
OTAL SUSPENDED RESIDUE
ECAL COLIFORM
H
MMONIA NITROGEN
D2+NO3-N
)TAL KJELDAHL NITROGEN
)TAL PHOSPHOROUS
TOTAL SOLIDS (DRY WEIGHT)
)3-N
ITAL DISSOLVED RESIDUE @180 C
TTLEABLE RESIDUE
ECIFIC CONDUCTANCE
N-SURFACE
N SUBSURFACE
(ED LIQUOR SUPSPENDED SOLIDS
POTASSIUM
MAGNESIUM
ARSENIC
SELENIUM
MOLYBDENUM
MERCURY
4.C. Laboratory ID# 352
.ab Supervisor. Michael J. Ladd; EES-Robbinsville
< 131
12.1
73%
Analyzed By. MB D
Certified By:
p imr
ethod
2.0
SM5210B
1.0
SM2540D
131
SM9221 E
0-14
SM9045D
6.9
EPA 350.3
5.6
SM4500 NO3
276
EPA 351.2
141
0.1 %
SM4500 P F
SM2510 G
3.6
SCA
1.0
0.1
SM2540C
SM25OF
10
SM2510B
NIA I CALL
N/A
1.00
CALC
NIA
17500
EPA 6010 C
175
EPA 6010 C
1.40
EPA 6010 C
EPA 6010 C
1.40
EPA 6010 C
3.50
EPA 6010 C
1.40
EPA 6010 C
7.00
EPA 6010 C
14.0
EPA 6010 C
350
EPA 6010 C
175
EPA 6010 C
3.50
EPA 6010 C
3.50
EPA 6010 C
3.50
EPA 6010 C
0.14
EPA 7471 B
Units
mUL
PDM D
WT
PDM D
WT

Town of Maggie Valley
Daily Field Parameter Worksheet
Dewatered Sludge/Mixed Sludge pulTemp.
Analyst:
Gallons Cal bration Ca ibration Check Time Time
Date Dewatered Bu er 7.0 Buffer 12.45 Buffer 10.0 Sam led ♦ Analyzed
�-ii �sya5
U,y5 10.v7
prn pry,
1-15 -- of 6a.�5 1C�• o5 3 '310
ern
1-17 7ol I R,q5 10.0 5 3 pro 3' m
3- ,oI 12•g5 1o.d6 3.30 3V
PM 3- 6 -- .ol E�. S 10.0� 305 3:z5
YWV PM
3 :Z7 -- 701 19 qJ 10•©3 )2 3PPM
PAX-
7 1 12.95 lo.0g 3 L-0 AO
pn
3 s /a425G
3 =�7 7 1 1?. y5 lo.0 9
.3° 3.40
J� prn.
3' 7. 1 g.q.5 to-oC 3130 Prn 3:qQ
3( - 7 / p,q5 10.0e 3:00 3:19
Pfn p rr L
' The n check buffe must be within t .1 units of the buffer's true value.
♦ If sample is measu led directly at the source only time analyzed would be recorded
n
Deb Month vna� 20ly' .
ir10�i}1.
;PHsu
Sludge
Tern'C
Air Temp
°C
Correction
Factor su
Corrected
PH su
Comment
42• �!
Q7.1c
C-
o
1-2- 26a
1Z53
93 ,
20 G
p. 15
l.Z.
o,
/a.yy
7?C.
a,�°�
'o.��
12.E
13.V 1
770
22°c
0.041
13,32
1,2.51
7y�c,
2a °E
p.t7 y
USo
7o ,
Svc.
at 5
M. 35
l2.�52
�51 Oc_
21
012
la. (10
`2 6-2-
We
Z2 G
o.©r�
1.2 33
0. y7
`17G
20 c
o 15
11.32
12- 50
151;c
21 F,
0.12
1.2.3

q-rq
-r5 34'
�-13
-13 138,
7-�Z
73
jjq
Town of Maggie Valley
Daily Field Parameter Worksheet
Dewatered Sludge/Mixed Sludge P UIf I
���%:
g PH/Temp.
ion (Check
2.45 Buffer 1
Time
• IAnalvzed
Temp Correction Corrected
`C Factor su PH su
7.0 l
!a, 15
lo.o6
/2,
q7c
�! c
~
a
1042q
7ol
la,� 5
/0,o
�.��p
.
3'F5
l�,s�
�P°G
aa9L
-,oq
116-0
70I
Zo t
Q,15
102,gS
10p.5
la. o6
3:1oP�n
El©ry
3;z m
�s
1a.75
/Zap
77C
65 c
�2-I c
- 2
Ot—
U,61
p
v.o(4
1,2, 5 l
701
701
-701
Vo?-,�5
/c2,L/5
1),y5
/.o,oe-
lo,r.,6
l4,95
3� Art,
:1
3' S
Pry t
3Pan
3' �,°n
3`as
,err.
a.5/
l Z1,5
?7G
&S
Z2 C-
o. c(
�.�
I c.
al G
o 1�.
C�Z.33
o09
la.34f
7o 1 U, 61lo.o�1/0
7-1s — To l 1 ,�f5 /o_ P5 3:0
7Pl
O
3 :o0 3 � o�
717 — �'o I 1�.y5 10.oC Fn per,
The pH check buffer must be within t .1 units of the buffer's true value.
*If sample is measured directly at the source only time analyzed would be recorded
qw
o.o`I
o.o6
-
1a2e5`J
PJ6
IR. 63
�a.V;.
7e
�c
1 G
o 0&
1.211tO
A R I
r 0 /i�-
Month c� AV Yearc&f 1

U
Date
97
Gallons
Dewatered
5,351
Calibration
Buffer 7.0
Calibration
Buffer 12.45
Check
Buffer 10.0
Time
Sam led ♦
Time
Anal zed ♦
PH su
'o
to
a. V
fr-—'
7 o I
la. y5
10.0 5
3' 00
3' ern°,
7.o !
1,2.15
1006
3 0o
3:10
50
8-I
33,7q3
a-«
—
7o l
1.2.Y5
10.05
3:0a
3Pm
ra 5z
7.o 1
1a.g5
w.06
7110
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Town of Maggie Valley
Daily Field Parameter Worksheet
Dewatered Sludge/Mixed Sludge PH/Temp.
Analyst: JL&I r.P
�ruy
Month _ CA wJ
Sludge Air Temp
Temp "C 'C
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c
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PH
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4 If sample is measured directly at the source only time analyzed would be recorded

Town of Maggie Valley
Daily Field Parameter Worksheet
Dewatered Sludge/Mixed Sludge PH/Temp.
Anal st• ,�&L(/
Date
•
Gallons
Dewatered
��,T53
Calibration
Buffer 7.0
Calibration
Buffer 12.45
Check
Buffer 10.0
Time
Sam led ♦
Time
Analyzed ♦
PH su
Sludge
Tem °C
mun[n Tear O&W
Air Temp
°C
Correction
Factor su
Corrected
PH su
Comment
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9 it sample is measured directly at the source only time analyzed would be recorded