WQ0010528_Residual Annual Report 2014_20150126

ANNUAL SLUDGE DISPOSAL REPORT
RECEIVED/DENR/DWR
JAN 2 3 2015
Water Quality
Permitting Section
SUMMARY OF THE
LAND APPLICATION PROGRAM
FOR THE
TOWN OF RAMSEUR
prepared by
United Water
Clemmons, North Carolina
[phone] RECEIVEDIDEMDWR
JAN 2 6 2015
WaterQuality
-t
Perrmog Section

1
Town of Ramseur
P. O. Box 545
Ramseur, NC 27316
336-824-4111
January 30, 2015 RECEIVED/DENROM
JAN � .S 2oI5,
N'CDENR/DWR/Water Quality Permitting Section
1617 Mail Service Center Water Permitting Section
y
Raleigh, NC 27699-1617 - .
Dear Sirs,
I am enclosing three copies of the 2014 Annual Surface Disposal of Residuals
(Sludge) Monitoring Report for the Town of Ramseur, Permit No. WQ0010528. We
believe the report to be accurate and complete however, if you have any questions or
require additional information, please advise.
Sincerely,
Town of Ramseur
Danny Shaw, Mayor
cc: Nadine Blackwell
Terry LeWallen
ENCLOSURES (three copies of report)
Sent Certified Mail Return Receipt Requested

NNUAL DISTRIBUTION AND MARKETING/ SURF ; DISPOSAL CERTIFICATION AND SUMMARY FO
PERMIT #: WQ00010528 FACILITY NAME: Town of Ramseur
PHONE: [phone] COUNTY: Randolph OPERATOR: Terry LeWallen
FACILITY TYPE (please check one): 0 Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? L7 Yes ❑% No If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) s) (include NPDES # if
applicable)
Volume (d tons
Recipient Information
Admendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
January
February
WWTP
0.03
0.33
0.36
March
April
WWTP & WTP
0.03
7.65
7.68
May
WWTP
0.03
0.33
0.36
June
WWTP
0.03
0.33
0.36
July
August
WTP
7.43
7.43
September
WWTP & WTP
0.03
7.09
7.12
October
WWTP
0.03
0.33
0.36
November
December
Totals:
Annual (dry tons)-T.-O.
18
23.49
23.67 10
Admendment s used:I
Lime
Bulking Agent(s)
used:
* If more space than given is required, please attach additional information sheet(s). ❑ Check box if additional sheet(s) are attached
Part C:
Facility was compliant during calendar year 2014 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality. p Yes ❑ No If No, please provide a written description why the facility was not compliant.
1. All monitoring wasdone in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory'results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water
Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law„ that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware
th there are si ifi/(` ntpenalties for submitting false informaiton, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee Date Signature of Preparer** Date
(if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r)
DENR FORM DMSDF (5/2003)

ANNUAL RESIDUAL SAl _ ING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ00010528 Laboratory:
Facility Name: Town of Ramseur
NPDES # or NCO026565
WQ#:
WWTP Name:
Residual Analysis Data
Ramseur WWTP
1) Pace Analytical
2)
9
4)
5)
Sample or
Composite
I
-.-
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of reparer Date
DENR FORM RSSF (5/2003)

aceAnalj 6cal
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September 22, 2014
Lisa Morris
United Water - Ramseur WWTP
PO Box 1279
Clemmons, NC 27012
RE: Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)6344964
Dear Lisa Morris:
Enclosed are the analytical results for sample(s) received by the laboratory on August 07, 2014. The
results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
\-3pv--
Terri Page
[e-mail]
Project Manager
Enclosures
cc: Mr. Terry Lewallen, HMS Ramseur WWTP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 1 of 25

lacieAnalj&cal
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Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320-
Arizona Certification #: AZ0735
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
heville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
CERTIFICATIONS
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification #: FL765
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Washington Certification #: C955
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 25

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SAMPLE SUMMARY
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92212484001
92212484002
SLUDGE
SLUDGE
Other
Solid
08/07/14 09:00
08/07/14 09:00
08/07/14 13:50
08/07/14 13:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 25

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SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project:
Pace Project No.:
SLUDGE 8/7/2014
92212484
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92212484001
SLUDGE
EPA 8081
RES
8
PASI-C
EPA 8151
LJM
11
PASI-O
EPA6010
SH1
7
PASI-A
EPA 7470
HVK
1
PASI-A
EPA 8270
BPJ
18
PASI-C
EPA8260
GAW
14
PASI-C
-
ASTM D2974-87
ACS
1
PASI-C
EPA 1010
TEP
1
PASI-A
EPA 9045
MDW
1
PASI-A
92212484002
SLUDGE
EPA200.8
HEA
3
PASI-O
REPORT OF LABORATORY ANALYSIS
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Page 4 of 25

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1
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: SLUDGE Lab ID: 92212484001 Collected: 08/07/14 09:00 Received: 08/07/14 13:50 Matrix: Other
Results reported on a "dry -weight' basis
Parameters
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinated Herbicides
Bentazon
2,4-D
Dalapon
2,4-DB
^'camba
'noseb
- mtachlorophenol
Picloram
2,4,5-T
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Date: 09/22/2014 03:48 PM
Report
Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA8081 Preparation Method: EPA3510
Leachate Method/Date: EPA 1311; 08/18/14 15:15
ND ug/L
0.50
0.50
1 08/1,9/14 10:01
08/20/14 10:42
58-89-9
ND ug/L
3.0
3.0
1 08/19/14 10:01
08/20/14 10:42
57-74-9
ND ug/L
0.50
0.50
1 08/19/14 10:01
08/20/14 10:42
72-20-8
ND ug/L
0.50
0.50
1, 08/19/14 10:01
08/20/14 10:42
1024-57-3
ND ug/L
1000
1000
1 08/19/14 10:01
08/20/14 10:42
72-43-5
ND ug/L
3.0
3.0
1 08/19/14 10:01
08/20/14 10:42
8001-35-2
60 %
10-138
1 08/19/14 10:01
08/20/14 10:42
2051-24-3
35 %
10-110
1 08/19/14 10:01
08/20/14 10:42
877-09-8
Analytical Method: EPA8151 Preparation
Method:
EPA8151
ND ug/L
0.094
0.016
1 08/14/14 08:00
08/15/14 15:23
25057-89-0
ND ug/L
0.94
0.22
1 08/14/14 08:00
08/15/14 15:23
94-75-7
ND ug/L
0.91
0.43
1 08/14/14 08:00
08/15/14 95:23
75-99-0
ND ug/L
1.9
0.51
1 08/14/14 08:00
08/15/14 15:23
94-82-6
ND ug/L
0.094
0.030
1 " 08/14/14 08:00
08/15/14 15:23
1918-00-9
ND ug/L
0.19
0.057
1 08/14/14 08:00
08/15/14 15:23
88-85-7
0.040 ug/L
0.028
0.017
1 08/14/14 08:00
08/15/14 15:23
87-86-5
ND ug/L
0.094
0.019
1 08/14/14 08:00
08/15/14 15:23
1918-02-1
ND ug/L
0.19
0.042
1 08/14/14 08:00
08/15/14 15:23
93-76-5
ND ug/L
0.19
0.049
1 08/14/14 08:00
08/15/14 15:23
93-72-1
115 %
66-130
1 08/14/14 08:00
08/15/14 15:23
19719-28-9
Analytical Method: EPA
6010 Preparation
Method:
EPA 3010
Leachate Method/Date: EPA 1311; 08/11/14 21:00
ND mg/L
0.050
0.014
1 08/12/14 14:45
08/14/14 14:39
7440-38-2
0.32 mg/L
0.25
0.0050
1 08/12/14 14:45
08/14/14 14:39
7440-39-3
ND mg/L
0.0050
0.0025
1 08/12/14 14:45
08/14/14 14:39
7440-43-9
ND mg/L
0.025
0.0020
1 08/12/14 14:45
08/14/14 14:39
7440-47-3
ND mg/L
0.025
0.020
1 08112/1414:45
08/14/14 14:39
7439-92-1
ND mg/L
0.10
0.019
1 08/12/14 14:45
08/14/14 14:39
7782-49-2
ND mg/L
0.025
0.00050
1 08/12/14 14:45
08/14/14 14:39
7440-22-4
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 08/11/14 21:00
ND ug/L
0.20 0.090
1 08/12/14 15:10
08/13/14 15:54
7439-97-6
Analytical Method: EPA8270 Preparation Method:
EPA3510
Leachate Method/Date: EPA 1311; 08/18/14 15:15
ND ug/L
50.0 4.8
1 08/19/14 10:01
08/20/14 12:25
106-46-7
ND ug/L
50.0 4.7
1 08/19/14 10:01
08/20/14 12:25
121-14-2
ND ug/L
50.0 4.8
1 08/19/14 10:01
08/20/14 12:25
87-68-3
ND ug/L
50.0 3.6
1 08/19/14 10:01
08/20/14 12:25
118-74-1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 25

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ANALYTICAL RESULTS
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: SLUDGE Lab ID: 92212484001 Collected: 08/07/14 09:00 Received: 08/07/14 13:50 Matrix: Other
Results reported on a "dry -weight' basis
Parameters
8270 MSSV TCLP Sep Funnel
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S) ,
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
-60 MSV TCLP
.=nzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene.
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percen Moisture
�1y �br, �S
010 Flash point, Closed Cup
Flashpoint
9045 pH Soil
pH at 25 Degrees C
Date: 09/22/2014 03:48 PM
Report
Results Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qua]
Analytical Method: EPA 8270 Preparation Method:
EPA 3510
Leachate Method/Date: EPA 1311; 08/18/14 15:15
ND ug/L
50.0
50.0
1
08/19/14 10:01
08/20/14 12:25
67-72-1
ND ug/L
50.0
8.0
1
08/19/14 10:01
08/20/14 12:25
95-48-7
ND ug/L
50.0
10.0
1
08/19/14 10:01
08120/1412:25
ND ug/L
50.0
5.5'
1
08/19/14 10:01
08/20/14 12:25
98-95-3
ND ug/L
100
23.0
1
08/19/14 10:01
08/20/14 12:25
87-86-5
ND ug/L
50.0
8.0
1
08/19/14 10:01
08/20/14 12:25
110-86-1
ND ug/L
50.0
4.6
1
08/19/14 10:01
08120/1412:25
95-95-4
ND ug/L
50.0
6.5
1
08/19/14 10:01
08/20/14 12:25
88-06-2
62 %
12-102
1
08/19/14 10:01
08/20/14 12:25
4165-60-0
66 %
13-107
1
08/19/14 10:01
08/20/14 12:25
321-60-8
78 %
21-132
1
08/19/14 10:01
08/20/14 12:25
1718-51-0
23 %
10-110
1
08/19/14 10:01
08/20/14 12:25
13127-88-3
34 %
10-110
1
08/19/14 10:01
08/20/14 12:25
367-12-4
77 %
27-108
1
08/19/14 10:01
08/20/14 12:25
118-79-6
Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 08/14/14 15:44
ND ug/L
5.0
1.2
1
08/18/14 14:46
71-43-2
14.3 ug/L
10.0
2.8
1
08/18/14 14:46
78-93-3
ND ug/L
5.0
2.7
1
08/18/14 14:46
56-23-5
ND ug/L
5.0.
1.0
1
08/18/14 14:46
108-90-7
ND ug/L
5.0
2.0
1
08/18/14 14:46
67-66-3
ND ug/L
5.0
1.2
1
08/18/14 14:46
106-46-7
ND ug/L
5.0
1.3
1
08/18/14 14:46
107-06-2
ND ug/L
5.0
3.4
1
08/18/14 14:46
75-35-4
ND ug/L
5.0
1.9
1
08/18/14 14:46
127-18-4
ND ug/L
5.0
1.0
1
08/18/14 14:46
79-01-6
ND ug/L
5.0
1.9
1
08/18/14 14:46
75-01-4
102 %
70-130
1
08/18/14 14:46
17060-07-0
100 0%
67-135
1
08/18/14 14:46
2037-26-5
106 %
70-130
1
08/18/14 14:46
460-00-4
Analytical Method: ASTM D2974-87
97.4 %
0.10
0.10
1
08/21/1414:31
d•(.o%
Analytical Method: EPA 1010
>200 deg F
70.0
70.0
1
08/20/14 01:50
Analytical Method: EPA 9045
12.1 Std. Units
0.10
0.10
1
08/13/14 12:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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Page 6 of 25

%Solids 2.6
Arsenic 0.0125 mg/I 0.480769 mg/kg
Chromium 0.0765 mg/I 2.942308 mg/kg
Nickel 0.0649 mg/I 2.496154 mg/kg
Formula: mg/I _ %Solids in decimal form

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ANALYTICAL RESULTS
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: SLUDGE
Lab lD: 92212484002
Collected:
08/07/14 09:00
Received: 08/07/14 13:50 Matrix: Solid
Results reported on a "dry -weight" basis
Report
Parameters
Results Units
Limit
MDL DF
Prepared
Analyzed
CAS No. Qua[
200.8 MET ICPMS
Analytical Method: EPA200.8
Preparation Method: EPA200.8
Arsenic
12.5 ug/L
5.0
2.5 1
08/14/14 19:58
08/19/14 03:39
7440-38-2 D3
Chromium
76.5 ug/L
5.0
2.5 1
08/14/14 19:58
08/19/14 03:39
7440-47-3 D3
Nickel
64.9 ug/L
5.0
3.1 1
08/14/14 19:58
08/19/14 03:39
7440-02-0 D3
Date: 09/22/2014 03:48 PM
REPORT OF LABORATORY ANALYSIS
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9
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QUALITY CONTROL DATA
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
QC Batch: MERP/6963 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: - 7470 Mercury TCLP
Associated Lab Samples: 92212484001
METHOD BLANK: 1262097
Associated Lab Samples-, 92212484001
Parameter Units
ug/L
Mercury
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.20 08/13/1415:09
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1262098
Spike - LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.5 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1262099 1262100
MS MSD
92212176001 Spike Spike NIS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
�rcury ug/L ND 2.5 2.5 2.4 2.4 98 95 75-125 3 20
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace, Analytical Services, Inc.. Page 8 of 25

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QUALITY CONTROL DATA
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
QC Batch: MPRP/20086 Analysis Method: EPA200.8
QC Batch Method: EPA200.8 Analysis Description: 200.8 MET
Associated Lab Samples: 92212484002
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
METHOD BLANK: 979974
Matrix: Water
Associated Lab Samples: 92212484002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
ug/L
ND 1.0
08/19/14 00:02
Chromium
ug/L
ND 1.0
08/19/14 00:02
Nickel
ug/L
ND 1.0
08/19/14 00:02
LABORATORY CONTROL SAMPLE:
979975
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Arsenic
ug/L
50
48.2
96 85-115
Chromium
ug/L
50
47.3
95 85-115
Nickel
ug/L
50
48.2
96 85-115
ATRIX SPIKE & MATRIX SPIKE DUPLICATE: 979976
979977
MS
MSD
35150294003 Spike
Spike MS
MSD
MS
MSD
% Rec
Max
Parameter Units Result Conc.
Conc. Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Arsenic ug/L 0.54J 50
50 48.9
48.9
97
97
70-130
.06 20
Chromium ug/L 0.50U 50
50 47.8
48.9
95
97
70-130
2 20
Nickel ug/L 1.7 50
50 48.8
50.0
94
97
70-130
3 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 979978
979979
MS
MSD
35150294006 Spike
Spike MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result Conc.
Conc. Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Arsenic ug/L
3.3 50
50 47.3
50.7
88
95
70-130
7 20
Chromium ug/L
0.50U 50
50 43.9
47.5
87
95
70-130
8 20
Nickel ug/L
1.1 50
50 43.3
47.8
84
93
70-130
10 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 25

(�IacieAnalXical
www.pacelabs.com
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
QC Batch: MPRP/16653
QC Batch Method: EPA 3010
Associated Lab Samples: 92212484001
METHOD BLANK: 1262087
Associated Lab Samples: 92212484001
Parameter Units
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 6010
Analysis Description: 6010 MET TCLP
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed
ND
0.050
08/14/1413:56
ND
0.25
08/14/1413:56
ND
0.0050
08/14/1413:56
ND
0.025
08/14/1413:56
ND
0.025
08/14/1413:56
ND
0.10
08/14/1413:56
ND
0.025
08/14/1413:56
Qualifiers
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE:
1262088
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
2.5
2.6
102
80-120
arium
mg/L
2.5
2.4
98
80-120
admium
mg/L
2.5
2.5
100
80-120
-iromium
mg/L
2.5
2.5
101
80-120
Lead
mg/L
2.5
2.4
97
80-120
Selenium
mg/L
2.5
2.6
102
80-120
Silver
mg/L
1.2
1.2
97
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1262089
1262090
MS
MSD
92212176001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.5
2.5
100
98
75-125
2
20
Barium
mg/L
ND
2.5
2.5
2.5
2.5
100
100
75-125
0
20
Cadmium
mg/L
1.1
2.5
2.5
3.8
3.8
108
106
75-125
1
20
Chromium
mg/L
ND
2.5
2.5
2.6
2.5
102
102
75-125
1
20
Lead
mg/L
ND
2.5
2.5
2.5
2.5
100
101
75-125
1
20
Selenium
mg/L
ND
2.5
2.5
2.5
2.5
100
100
75-125
0
20
Silver
mg/L
ND
1.2
1.2
1.2
1.2
97
97
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 25

(�IaneAnalyfical
www..pacelabs.com
QUALITY CONTROL DATA
Project: SLUDGE 8/7/2014
Pace'Project No.: 92212484
QC Batch: MSV/27986 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV TCLP
Associated Lab Samples: 92212484001
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
METHOD BLANK: 1266086
Associated Lab Samples: 92212484001
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed Qualifiers
1,1-Dichloroethene
ug/L
ND
5.0
08/18/14 12:20
1,2-Dichloroethane
ug/L
ND
5.0
08/18/14 12:20
1,4-Dichlorobenzene
ug/L
ND
5.0
08/1811412:20
2-Butanone (MEK)
ug/L
ND
10.0
08/18/14 12:20
Benzene
ug/L
ND
5.0
08118/1412:20
Carbon tetrachloride
ug/L
ND
6.0
08/18/14 12:20
Chlorobenzene
ug/L
ND
'5.0
08/18/14 12:20
Chloroform
ug/L
ND
5.0
08/18/14 12:20
Tetrachloroethene
ug/L
ND
5.0
08/18/14 12:20
Trichloroethene
ug/L
ND
5.0
08/18/14 12:20
Vinyl chloride
ug/L
ND
5.0
08/18/14 12:20
1,2-Dichloroethane-d4 (S)
%
105
70-130
08/18/14 12:20
4-Bromofluorobenzene (S)
%
107
70-130
08/18/14 12:20
Toluene-d8 (S)
%
100
67-135
08/18/14 12:20
LABORATORY CONTROL SAMPLE:
Parameter
1266087
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1-Dichloroethene
ug/L
50
48.4
97
66-135
1,2-Dichloroethane
ug/L
50
46.3
93
67-128
1,4-Dichlorobenzene
ug/L
50
49.6
99
78-130
2-Butanone (MEK)
ug/L
100
98.9
99
61-144
Benzene -
ug/L
50
48.7
97
80-125
Carbon tetrachloride
ug/L
50
45.9
92
69-131
Chlorobenzene
ug/L
50
48.9
98
81-122
Chloroform
ug/L
50
52.2
104
73-127
Tetrachloroethene
ug/L
50
52.5
105
78-122
Trichloroethene
ug/L
50
48.7
97
78-122
Vinyl chloride
ug/L
50
45.7
91
58-137
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
107
70-130
Toluene-d8 (S)
%
100
67-135
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1266088 1266089
MS MSD
92212757001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
1,1-Dichloroethene ug/L ND 50 50 63.0 66.0 126 132 70-150 5 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 25

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1266088
1266089
MS
MSD
92212757001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
1,2-Dichloroethahe
ug/L
ND
50
50
52.9
55.1
106
110
70-150
4
30
1,4-Dichlorobenzene
ug/L
ND
50
50
53.9
56.7
108
113
70-150
5
30
2-Butanone(MEK)
ug/L
ND
100
100
117
122
117
122
70-150
4
30
Benzene
ug/L
ND
50
50
57.5
57.7
115
115
70-150
0
30
Carbon tetrachloride
ug/L
ND
50
50
55.7
56.6
111
113
70-150
2
30
Chlorobenzene
ug/L
ND
50
50
56.0
56.3
112
113
70-150
1
30
Chloroform
ug/L
ND
50
50
62.9
64.0
126
128
70-150
2
30
Tetrachloroethene
ug/L
ND
50
50
60.7
62.0
121
124
70-150
2
30
Trichloroethene
ug/L
ND
50
50
5&6
56:9
113
114
70-150
1
30
Vinyl chloride
ug/L
ND
50
50
57.8
59.5
116
119
70-150
3
30
1,2-Dichloroethane-d4 (S)
%
101
105
70-130
4-Bromofluorobenzene (S)
%
105
105
70-130
Toluene-d8 (S)
%
102
101
67-135
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 25

acmnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
QC Batch: OEXT/29481 Analysis Method: EPA 8081
QC Batch Method: EPA 3510 Analysis Description: 8081 GCS TCLP Pesticides
Associated Lab Samples: 92212484001
METHOD BLANK: 1266635
Associated Lab Samples:
92212484001
Parameter
Units
Chlordane (Technical)
ug/L
Endrin
ug/L
gamma-BHC (Lindane)
ug/L
Heptachlor epoxide
ug/L
Methoxychlor
ug/L
Toxaphene
ug/L
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
3.0
08/20/14 09:32
ND
0.50
08/20/14 09:32
ND
0.50
08/20/14 09:32
ND
0.50
08/20/14 09:32
ND
1000
08/20/14 09:32
ND
3.0
08/20/14 09:32
76
10-138
68/20/14 09:32
73
10-110
08/20/14 09:32
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
(919)8344984
LABORATORY CONTROL SAMPLE & LCSD: 1266636
1266637
Spike
LCS
LCSD
LCS
. LCSD
% Rec
Max
Parameter
Units
Cone.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qualifiers
�Eodrin
ug/L
1.2
1.1
1.0
87
81
20-134
7 30
imma-BHC (Lindane)
ug/L
1.2
0.99.
0.94
80
76
20-118
5 30
::aptachlor epoxide
ug/L
1.2
0.99
0.90
80
73
22-133
9 30
Methoxychlor
ug/L
3.7
ND
ND
81
79
44-150
30
Decachlorobiphenyl (S)
%
81
75
10-138
Tetrachloro-m-xylene (S)
%
78
70
10-110
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 25

acmnalytical
www.pacelabs.com
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
QC Batch: OEXT/18498
QC Batch Method: EPA 8151
Associated Lab Samples: 92212484001
METHOD BLANK: 978724
Associated Lab Samples: 92212484001
Parameter Units
2,4,5-T
ug/L
2,4,5-TP (Silvex)
ug/L
2,4-D
ug/L
2,4-DB
ug/L
Bentazon
Og/L
Dalapon
ug/L
Dicamba
ug/L
Dinoseb
ug/L
Pentachlorophenol
ug/L
Picloram
ug/L
2,4-DCAA (S)
%
!.IXBORATORY CONTROL SAMPLE:
Parameter
978725
Units
2,4,5-T
ug/L
2,4,5-TP (Silvex)
ug/L
2,4-D
ug/L
2,4-DB
ug/L
Bentazon
ug/L
Dalapon
ug/L
Dicamba
ug/L
Dinoseb
ug/L
Pentachlorophenol
ug/L
Picloram
vg/L
2,4-DCAA (S)
%
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 8151
Analysis Description: 8151AGCS Herbicides
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed
Qualifiers
ND
0.19
08/15/14 03:15
ND
0.19
08/15/14 03:15
ND
0.94
08/15/14 03:15
ND
1.9
08/15/14 03:15
ND
0.094
08/15/14 03:15
ND
0.91
08/15/14 03:15
ND
0.094
08/15/14 03:15
ND
0.19
08/15/14 03:15
,ND
0.028
08/15/14 03:15
ND
0.094
08/15/14 03:15
76
66-130
08/15/14 03:15
Spike
LCS
LCS % Rec
Conc.
Result % Rec Limits
Qualifiers
1.2
0.91
76
46-137
1.2
1.1
91
63-133
6
4.8
79
40-137
12
10.6
89
70-130
.6
0.49
81
58-130
6
3.8
64
17-137
.6
0.66
109
43-130
1.2
0.83
69
10-177
.18
0.18
102
70-144
.6
0.43
72
10-147
84
66-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 978726
10277252001
Parameter Units Result
MS
Spike
Conc.
MSD
Spike
Conc.
978727
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec Max
Limits RPD RPD Qua]
2,4,5-T
ug/L
ND
1.3
1.5
0.83
0.93
63
64
46-137
11
40
2,4,5-TP (Silvex)
ug/L
ND
1.3
1.5
1.4
1.5
103
104
63-133
10
40
2,4-D
ug/L
2.3
6.6
7:3
9.1
9.2
102
94
40-137
1
40
2,4-DB
ug/L
ND
13.3
14.6
13.0
14.2
91
92
70-130
9
40
Bentazon
ug/L
ND
.66
.73
0.47
1.3
70
177
58-130
94
40 M1,R1
Dalapon
ug/L
ND
6.6
7.3
6.1
6.9
92
95
17-137
12
40
Dicamba
ug/L
1.0
.66
.73
1.7
1.7
107
100
43-130
1
40
Results presented on this page are In the units indicated by the
"Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc.. `
Page 14 of 25

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 978726
978727
MS
MSD
10277252001 Spike
Spike MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result Conc.
Conc. Result
Result
% Rec
% Rec
Limits
RPD RPD Qua[
Dinoseb
ug/L
ND 1.3
1.5 0.98
1.1
73
78
10-177
15 40
Pentachlorophenol
ug/L
ND .2
.22 0.24
0.26
99
101
70-144
9 40
Pic[oram
ug/L
1.9 .66
.73 2.5
2.7
89
109
10-147
8 40
2,4-DCAA (S)
%
118
94
66-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc..
Page 15 of 25

acmnalytical
wvnvpacelabs.com
QUALITY CONTROL DATA
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
QC Batch: OEXT/29480
QC Batch Method: EPA 3510
Associated Lab Samples: 92212484001
Analysis Method: EPA 8270
Analysis Description: 8270 TCLP MSSV
METHOD BLANK: 1266632
Matrix:
Water
Associated Lab Samples: 92212484001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dichlorobenzene
ug/L
ND
50.0
08/20/14 10:28
2,4,5-Trichlorophenol
ug/L
ND
50.0
08/20/14 10:28
2,4,6-Trichlorophenol
ug/L
ND
50.0
08/20/14 10:28
2,4-Dinitrotoluene
ug/L
ND
50.0
08/20/14 10:28
2-Methylphenol(o-Cresol)
ug/L
ND
50.0
08120/1410:28
3&4-Methylphenol(m&p Cresol)
ug/L
ND
50.0
08/20/14 10:28
Hexachloro-1,3-butadiene
ug/L
ND
50.0
08/20/14 10:28
Hexachlorobenzene
ug/L
ND
50.0
08/20/14 10:28
Hexachloroethane
ug/L
ND
50.0
08/20/14 10:28
Nitrobenzene
ug/L
ND
50.0
08/20/14 10:28
Pentachlorophenol
ug/L
ND
100
08/20/14 10:28
Pyridine
ug/L
ND
50.0
08/20/14 10:28
2,4,6-Tribromophenol (S)
%
73
27-108
08/20/14 10:28
2-Fluorobiphenyl (S)
%
70
13-107
08/20/14 10:28
Fluorophenol (S)
%
40
10-110
08/20/14 10:28
itrobenzene-d5 (S)
%
70
12-102
08/20/14 10:28
Fnenol-d6 (S)
%
26
10-110
08/20/14 10:28
Terphenyl-d14 (S)
%
91
21-132
08/20/14 10:28
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 1266633
Parameter Units
Spike
Conc.
1266634
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
1
% Rec
Limits
RPD
Max
RPD Qualifiers
1,4-Dichlorobenzene
ug/L
500
325
331
65
66
10-110
2
30
2,4,5-Trichlorophenol
ug/L
500
444
441
89
88
39-108
1
30
2,4,6-Trichlorophenol
ug/L
500
419
417
84
83
40-104
0
30
2,4-Dinitrotoluene
ug/L
500
472
451
94
90
42-109
5
30
2-Methylphenol(o-Cresol)
ug/L
500
339
340
68
68
31-110
0
30
3&4-Methylphenol(m&p Cresol)
ug/L
500
314
318
63
64
30-110
1
30
Hexachloro-1,3-butadiene
ug/L
500
316
321
63
64
10-110
2
30
Hexachlorobenzene
ug/L
500
417
423
83
85
39-121
1
30
Hexachloroethane
ug/L
500
301
304
60
61
10-110
1
30
Nitrobenzene
ug/L
500
389
396
78
79
32-101
2
30
Pentachlorophenol
ug/L
1000
710
764
71
76
18-108
7
30
Pyridine
ug/L
500
165
192
33
38
10-110
15
30
2,4,6-Tribromophenol (S)
%
90
92
27-108
2-Fluorobiphenyl (S)
%
82
82
13-107
2-Fluorophenol (S)
%
45
45
10-110
Nitrobenzene-d5 (S)
%
77
78
12-102
Phenol-d6 (S)
%
33
33
10-110
Terphenyl-d14 (S)
%
92
85
21-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 25

aceAnalj&al
www.pacelabs.com
QUALITY CONTROL DATA
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
QC Batch: PMST/6953 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92212484001
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
SAMPLE DUPLICATE: 1268884
92212484001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 97.4 97.3 0 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 25

aceAnalyiical
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QUALITY CONTROL DATA
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
QC Batch: WET/32738 Analysis Method: EPA 1010
QC Batch Method: EPA 1010 Analysis Description: 1010 Flash Point, Closed Cup
Associated Lab Samples: 92212484001
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
SAMPLE DUPLICATE: 1267530
92213302002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Flashpoint deg F >200 >200
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc.. Page IS of 25

aceAnalj&al
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Project: SLUDGE 8/7/2014
Pace Project.No.: 92212484
QC Batch: WET/32620
QC Batch Method: EPA 9045
Associated Lab Samples: 92212484001
SAMPLE DUPLICATE: 1262659
Parameter Units
pH at 25 Degrees C Std. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9045
Analysis Description: 9045 pH
92212484001 Dup
Result Result RPD
• 12.1 12.2 0
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Max
RPD Qualifiers
10
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 25

acmnalytical
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QUALIFIERS
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
DEFINITIONS
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted, reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
—ABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2014 03:48 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 25

(�15'cmnalj&alo
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SLUDGE 8/7/2014
Pace Project No.: 92212484
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92212484001
SLUDGE
EPA 3510
OEXT/29481
EPA 8081
GCSV/18613
92212484001
SLUDGE
EPA 8151
OEXT/18498
EPA 8151
GCSV/12138
92212484001
SLUDGE
EPA 3010
MPRP/16653
EPA 6010
ICP/15039
92212484002
SLUDGE
EPA200.8
MPRP/20086
EPA200.8
ICPM/8185
92212484001
SLUDGE
EPA7470
MERP/6963
EPA7470
MERC/6706
92212484001
SLUDGE
EPA 3510
OEXT/29480
EPA 8270
MSSV/9553
92212484001
SLUDGE
EPA 8260
MSV/27986
92212484001
SLUDGE
ASTM D2974-87
PMST/6953
92212484001
SLUDGE
EPA 1010
WET/32738
92212484001
SLUDGE
EPA,9045
WET/32620
Date: 09/22/2014 03:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 21 of 25

Report Results to:
RAMSEUR WWTP
ATT*N- TERRY LEWALLEN
Phone: [phone]
Chain of Cust
Bill Results to:
ATFN:
[3Standard Report Delivery
❑ Rush Report Delivery (w/ surcharge)
Requested Due Date:
Project Reference: SLUDGE
Purchase Order #:
Sampled By.
10,
1
1w-.m
......... .
O_M`
•Ng0
K
�7-��
(J�/���Z�� 4 -D, J
oeloo
I
5 ISLUDGE
FULL TCLP, REACTIVITY, CORROSIVITY, FLASHPOINT
6-7-lq
2
SLUDGE
TOTAL % SOLIDS, TOTAL METALS (ARSENIC-16020, CR & NI-6010)')
9 Leve+ -a 11P
U&J teael
Ltrw I- -e
C
ie V%A
L
9� 5V
e 6
Time
;Zk:0
da
w
�-
For Lab Use Only
ITemperature
Rgetwed
by
at —
NJ
_kJ7
411
• 50
at receipt:
ITemp: 42
Relinquished by (08nature)
Received by (s-kn-ature) I
Da tk I
Time
--
c.

Document Name: Sample Condition Upon
Document Revised: April 04, 2013
Receipt (SCUR)
Page 1 of 2
Document No.:
issuing Authorities:
i
F-RAL-CS-0171-rev.02
Pace Asheville Quality Office
Client Name:'Vf(j(1S'AN tl1�t�'1 T r .
Where Received: [] Huntersvilie C Asheville Eden Raleigh
Courier (Circle): • Fed Ex UPS LISPS Client Commercial Pace Other
Custody Seat on Cooler/Box Present: [ yes no Seals intact: yes !] no
Packing Material: Bubble Wrap Sags)6 Nog
Other
Circle Thermometer Used: (R Gun S •122065387T 0 of [Co. Blue None F1 Samples on ice, cooling process has begun
Temp Correction Factor: Add ubtract
Corrpcted Cooler Temp.: C
Biological Tissue Is Frozen: Yes No A
9
Date and Initials of person examining
cD l v 0 q
check: 1
Temp. should be above freezing to W-0
Comments".
Chain of Custody Present
U4. ON. - ❑NIA
f:
Chain of Custodx Filled Out:
Wyes C)N,
❑NIA
2. '
Chain of Custody Relinquished.
es ❑No
_ ❑NIA
3.
Sampler Name & Signature on COC:
Yes [IN.
❑NiA
4.
Samples Arrived within Hold Time:
ON.
ONIA
S.
Short Hold Time Anat is'(<72hr):
.❑yes GKo
©wA
6.
Rush Turn Around Time Re nested:
❑Yes ' ¢�o
❑NIA
7.
Sufficient Volume:
es ONo
OWA
S.
Correct Containers Used:
es ❑No
OwA
9.
-pace'Containers Used:
Yes ❑No
❑wA
Containers intact:
Yes ON.
DIVA
10.
Filtered volume -received for Dissolved tests
❑Yea EINo
NIA
11,
Sample Labels match COC:
C]No
❑NIA
12,
-includes dateltime/IDlAnalysls Matrix:
All wntalners needing preservation have been checked,
r7�ves ❑No
ON/A
13.
All containers needing preservation are found to be in
compliance with EPA recommendation.
yes ONO
❑NIA
exceptioea: VOA, coliform, TOO, D$G, W4DRO (water)
Yes 13No
Sam ' les checked for deohlorinatlon:
ea ONo
OWA
14.
Heads ace in VOA Vials >6mm :
C3Yos ❑No
ffWA
15.
Trip Blank Present:
Trip Blank Custody Seals Present
❑Yes C1No
❑Yes . ❑No
iWA
WA
16,
Pace Trip Blank Lot # it urchased :
Client Notification/ Resolution: Field Data Required?. Y l N
Person Contacted DateMme:
Commehsl Resolution:
SCURF iSRF
Review::
Date:
Place label here
Q[3
Note: Whenever there Is a discrepancy. affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR Handwrite project number
Codification-Offlea ( Le out of hold, incorrect preservative, out of temp, (if no label available)
incorrect containers)

Document No.:
e2of2
Authorities:
2013
-
.■
a
.e
.■
.■
.■
.■
..
r
w
•
a
•
■O■■�■■■■■■
ors
M____w
ammmm■■■
MEMO■■n■■U■■■■■■■■■■■■■■■®
■■■■■■■■■■■■■■■■■■■■■■■■■MM
=MNMMMMMMMNMMMMMNMMMMNMMNM
■■■■■■
MEMMM■■■■■■■■■■■■■■EE
�■■■■■■■■■■■■■■■■■■■■■■■sue
■■■■■■■■■■■■■■■■■■■■■■■■■
=MWMMMMNMMMMMMMMMMwMMMMMMM
Client Sam le ID s
Sam le Discrepancy
N Adjustment Log for Preserved Samples
Sample ID
Type of
Preservative
pH upon
receipt
Date preservation
Adjusted
Time Preservation
Adjusted
Am cunt of
Preservative added
Lot# of
Preservative
Bottle Code Key
125 ml Plastic Unp: BP4U
250 ml Plastic Unp: 13P3U
500 ml Plastic Unp: BP2U
1 Liter Plastic Unp: BP1U
250 ml Plastic H2SO4: BP33
250 ml Plastic HNO3: BP3N
250 ml Plastic ZN Acetate: BP3Z
250 mi Plastic NaOH: SPSO
Wide mouthed glass jar unp: WGFU
1 Liter Amber Unp: AG1U
1 Liter Amber HCI: AGIH
500 ml Amber Unp: AG2U
1 Liter Amber H2SO4: AG1 S
250 ml Amber H2804: AG3S
250 ml Amber NH4CLrAG3A
40 ml VOA HCl, D.G9H
40 ml VOA Na282O3: VG9T
40 ml VOA Unp: VG9U
40 ml VOA H2SO4: DG9S
55035 Kit: VOAK
VPH ! Gas Kit: VIGK
125 ml Sterile Plastic: SPST .
250 ml Sterile Plastic: SP2T

ANNUAL RESIDUAL SAP 1NG SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ00010528 Laboratory:
Facility Name:
NPDES # or
WQ#:
Town of Ramseur
NCO074454
WWTP Name: Ramseur Water Treatment Plant
Residual Analysis Data
1) Pace Analytical & Environment 1
2)
3)
4)
5)
Sample•
Composite Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature ohieparer Date
DENR FORM RSSF (5/2003)

0
E�1d000Emid Flo hcwpo
S.
BOX 7085, 114 OAKMONT DRIVE
ENVILLE, N.C. 27835-7085
UNITED WATER (RAMSEUR WTP-SLUDGE)
NADINE BLACKWELL
P.O. BOX 1279
CLEMMONS ,NC 27012
PARAMETERS
Arsenic (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Nickel (dry wt. basis), mg/kg
Total Solids,
Sludge Analysis Method
Sample Date Analyst Code
2
12/18/14
MTM
311313-04
5
12/18/14
LFJ
EPA200.7
26
12/18/14
LFJ
EPA200.7
0.96
12/11/14
LW
2540G-97
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 950
DATE COLLECTED: 12/09/14
DATE REPORTED : 12/22/14
REVIEWED BY:
`AW

01/11/zo1a IV:zr J;3b8241004 , RAM'SEURWTP #2456 P.002/002
CHAIN OF CUSTODY
Sample Location: 5-471Se V l W
Sample Collection Date:_ U - o ?,-I
Sample Collection Time: L3
Person Collecting Sample Na
Samples Sent to Laboratory for additional analyses? G
Comments:
NO
Attach copy of commerclal iabaratory Chain of Custody to this farm

aceAnalytical
www.pacelabs.com
i
Mr. Mark Grose
Ramseur WTP
P.O. Box 217
Ramseur, NC 27316
Project: 08/07/2014
Pace Project No.: 92212453
Sample: EFFLUENT
Laboratory Report
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 1 of 1
Report Date: 08/11/2014
Date Received: 08/07/2014
Lab ID: 92212453001 Collected: 08/06/14 16:20 'Matrix: Water
Parameters Results Units Report Limit Analyzed Qualifiers
Turbidity 4.2 NTU 1.0 08/07/14 17:20
Total Suspended Solids 9.7 mg/L 8.3 08/07/14 16:13
Sample: 51i` Lab ID: 92212453002 Collected: 08/06/14 14:30 Matrix: Solid
Results reported on a "dry -weight' basis
Parameters Results Units Report Limit Analyzed Qualifiers
Percent Moisture 94.6 % 0.10 08/11/14 15:20
o'viewed by: &X6 � -
TerriPage
[e-mail]
Raleigh Certification IDS
6701 Conference Drive Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
Page 1 of 5

aceAnalytical
vnnxpa�/aGs.com
Laboratory Report
Mr. Mark Grose
Ramseur WTP
P.O. Box 217
Ramseur, NC 27316
Project: Percent Solids
Pace Project No.: 92210368
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 1 of 1
Report Date: 08/13/2014
Date Received: 07/23/2014
Sample: Eff Lab ID: 92210368001 Collected: 07/22/14 12:40 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit Analyzed Qualifiers
Percent Moisture 98.2 % 0.10 08/13/14 14:49
Total Solids 1.8 % 0.000010 08/13/1410:45
Reviewed by: -YPW
Terri Page
[e-mail]
iarlotte Certification IDs
-,a800 KinceyAve. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
Pagel of 3

7aceAnalj4ical'
www.pacelabs.com
Mr. Mark Grose
Ramseur WTP
P.O. Box 217
Ramseur, NC 27316
Project: SLUDGE-TCLP
Pam Project No.: 92215797
Sample; SLUDGE
Laboratory Report
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 1 of 3
Report Date: 09/16/2014
Date Received: 09/03/2014
Lab ID: 92215797001 Collected: 08/28/14 09:25 Matrix: Water
Parameters
Results Units
garp'nia-BHC (Lindane)
ND ug/L
Chlordane (Technical)
ND ug/L
En€lrin
ND ug/L
Heptachlor epoxide
ND ug/L
Meti-noxychlor
ND ug/L
Toxap°hene
ND ug/L
Decachlorobiphenyl (S)
54 %
Tetrachloro-m-xylene (S)
79
Arsenic
ND mg/L
rium
ND mg/L
,dMium
ND mg/L
unr®innium
ND mg/L
Lead
ND mg/L
Selenium
ND mg/L
Silver
ND mg/L
MercDrY
ND ug/L
1 4-pichlorobenzene
ND ug/L
2 4-Dinitrotoluene
ND ug/L
Hexachloro-1,3-butadiene
ND ug/L
Hexachlorobenzene
ND ug/L
Hexachloroethane
ND ug/L
2-Methylphenol(o-Cresol)
ND ug/L
3&4- Methyl phenol (m&p Cresol)
ND ug/L
Nitrobenzene
ND ug/L
Pentachloro phenol
ND ug/L
Pyridine
ND ug/L
2,4,5-Trichlorophenol
ND ug/L
2,4,6-Trichlorophenol
ND ug/L
Nitrobenzene-d5 (S)
77 %
2-Fluorobiphenyl (S)
74 %
Terphenyl-d14 (S)
84 %
Phenol-d6 (S)
23
2-Fluorophenol (S)
38 %
2,4,6-Tribromophenol (S)
74 %
Benzene
ND ug/L
2-Butanone (MEK)
ND ug/L
Carbon tetrachloride
ND ug/L
Chlorobenzene
ND ug/L
oform
ND ug/L
lichlorobenzene
ND ug/L
_ Jichloroethane
ND ug/L
1,1-Dichloroethene
ND ug/L
Tetrachloroethene
ND ug/L
Trichloroethene
ND ug/L
Report Limit
Analyzed Qualifiers
0.50
09/15/1412:48
3.0
09/15/1412:48
0.50
09/15/1412:48
0.50
09/15/1412:48
1000
09/15/1412:48
3.0
09/15/1412:48
10-138
09115/1412:48
10-110
09/1511412:48
0.050
09/10/14 04:10
0.25
09/10/14 04:10
0.0050
09/10/14 04:10
0.025
09/10/14 04:10
0.025
09/10/14 04:10
0.10
09/10/14 04:10
0.025
09/10/14 04:10
0.20
09/10/1414:45
50.0
09/11/1416:52
50.0
09/11/1416:52
50.0
09/11/1416:52
50.0
09/11/1416:52
50.0
09/11/1416:52
50.0
09/11/1416:52
50.0
09/1111416:52
50.0
09/1111416:52
100
09/11/1416:52
50.0
09/11/1416:52
50.0
09/11/1416:52
50.0
09/11/1416:52
12-102
09/11/1416:52
13-107
09111/1416:52
21-132
09/11/1416:52
10-110
09/11/1416:52
10-110
09/11/1416:52
27-108
09/11/1416:52
5.0
09/10/14 09:05
10.0
09/10/14 09:05
5.0
09/10/14 09:05
5.0
09/10/14 09:05
5.0
09/10/14 09:05
5.0
09/10/14 09:05
5.0
09/10/14 09:05
5.0
09/10/14 09:05
5.0
09/10/14 09:05
5.0
09/10/14 09:05
Page 1 of 7

laneAnallj6cal
www.pacelabs.com
Sample: SLUDGE
Parameters
Vinyl chloride
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Flashpoint
pH at 25 Degrees C
Cyanide, Reactive
.Sulfide, Reactive
Lab ID: 92215797001 Collected: 08/28/14 09:25 Matrix: Water
Results Units
ND ug/L
100 %
100 %
99 %
>200 deg F
7.0 Std. Units
ND mg/L
ND mg/L
Report Limit
Analyzed Qualifiers
5:0
09/10/14 09:05
70-130
09/10/14 09:05
67-135
09/10/14 09:05
70-130
09/10/14 09:05
70.0
09/12/14 03:15
0.10
09/08/1415:21 H6
0.010
09/10/14 22:52
1.0
09/1011414:00
Sample: SLUDGE Lab ID: 92215797002 Collected: 08/28/14 09:25 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters
Results Units
Report Limit
Analyzed Qualifiers
Percent Moisture
96.7 %
0.10
09/05/14 08:44
Total Solids
3.3 %
0.000010
09/04/14 15:31
Sample: EFF
Lab ID: 92215797003 Collected:
09/03/14 10:10 Matrix: Water
Parameters
Results Units
Report Limit
Analyzed Qualifiers
Turbidity
12.4 NTU
1.0
.09/03/1417:40
Total Suspended Solids
28.0 mg/L
16.7
09/06/14 12:00
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
Reviewed by: & cf' -
Brittany Gibson for
Terri Page
[e-mail]
Pennsylvania Certification IDs
1638 Roseytown Rd Suites 2,3&4 Greensburg, PA 15601
ACLASS DOD-ELAP Accreditation #: ADE-1544
Alabama Certification M 41590
Arizona Certification #: AZ0734
Arkansas Certification
California/TNI Certification #: 04222CA
Colorado Certification
Connecticut Certification #: PH-0694
Delaware Certification
Florida/TNI Certification #: E87683
Guam/PADEP, Certification
Hawaii/PADEP Certification
Idaho Certification
Illinois/PADEP Certification
Indiana/PADEP Certification
Iowa Certification #: 391
Kansas/TNI Certification #° E-10358
Kentucky Certification #: 90133
Louisiana DHH/TNI Certification #: LA140008
Louisiana DEQ/TNI Certification #: 4086
Maine Certification #: PA00091
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
Michigan/PADEP Certification
Missouri Certification #: 235
Raleigh Certification IDs
6701 Conference Drive Raleigh, NC 27607
North Carolina Wastewater Certification #: 67
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
i th Carolina Drinking Water Certification #: 37706
th Carolina Field Services Certification #: 5342
rth Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Montana Certification #: Cert 0082
Nebraska Certification* NE-05-29-14
Nevada Certification
New Hampshire/TNI Certification #: 2976
New Jersey/TNI Certification #: PA 051
New Mexico Certification
New York/TNI Certification* 10888
North Carolina Certification #: 42706
North Dakota Certification #: R-190
Oregon/TNI Certification #: PA200002
Pennsylvania/TNI Certification #: 65-00282
Puerto Rico Certification #: PA01457
South Dakota Certification
Tennessee Certification #: TN2867
Texas/TNI Certification #: T104704188
Utah/TNI Certification #: PA014572014-4
Vermont Dept. of Health: ID# VT-0282
Virgin Island/PADEP Certification
Virginia/VELAP Certification #: 460198
Washington Certification #: C868
West Virginia DEP Certification #: 143
West Virginia DHHR Certification #: 9964C
Wisconsin/PADEP Certification
Wyoming Certification #: 8TMS-Q
North Carolina Bioassay Certification #: 16
North Carolina Drinking Water Certification #: 37731
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginiaNELAP Certification #: 460221
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 2 of 3
Page 2 of 7

aceAnalj&al
www.pacelabs.com
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaIVELAP Certification #: 460222
Pace Analytical Services, Inc.
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 3
Page 3 of 7

2ceAnaocalg Chain of Custody
Report Results to: Bill Results to: ❑ Standard Report Delivery
RAMSEUR WTP. ❑ Rush Report Delivery (w/ surcharge)
Requested Due Date:(
Project Reference: SLUDGE-TCLP �� 1
ATrN: MARK GROSE ATTN: Purchase Order #:
Phone: [phone] -Sampled By:III
i A.I.MR-
12
gc
Hpq
I IN all
d zS" SLUDGE FULL TCLP, REACTIVITY, CORROSIVITY, FLASHPOINT
2f
1 ud 5c
bV W s�
Reti fished (sign e) Received si ature}f Time
�✓�` /1 '_, For Lab Use Only
Retingv (signatu ) R re) i lht �- /! 09
71ma. .
/ l 1
"f �''�Z` „ -� Temperature at receipt:} '

Document Name., Sample Condition Upon
Document Revised: April 04, 2013
ace�lnalyiical�
Recel t (SCU.R)
Page i of 2
'"'�"'•A"°°'*°' °�'^
(r -r
Document No.:
issuing Authorities:
9
F-RAL-CS-001-rev.02
race Asheville Quality Office
Client Name:- RA=CP. W Y jNTY
Where Received: [] Huntersvllie Q Asheville EdenRaleigh
Courier (Circle): Fed l=x UPS USPS Client Commercial Pace Other .
Custody Seal on Cooler/Box Present: o yes Z no Seals intact: /6 yes E] no
Packing Material: Bubblb Wrap Bub cgs None El Other
Circle Thermometer Used: iR Gun :1 f)65387Type tee: et Blue None [] Samples on ice, cooling process has begun
Temp Correction Factor; Add Subtract � to
Corrected Cooler Temp.: C Biological Tissue is Frozen: Yes rf NIA
Data and Initials of person examining
co f ! ►es [v tl0 �f
check• �+
Temp should be above freezing to 6°4
Comments:
Chaln.of CustodyPresent:
es• ON.
OWA
1•. _ .. .
Chain of Custod •Filled Out
es ON.
ONlA
2. '
Chain of CustodyRelinquished"
Yes ONO
13NIA
3.
Sampler Name & Signature on COO:
Yes ONo
OWA
4.
Samples Arrived within Hold Time:
Yes ONO
CIWA
S.
Short Hold Time Mat is' g2hr :
Yes ONo
OWA
6.
Rush Turn Around Time Requested:
OYes o
❑NIA
7.
SufficlentVolume:
Yes ONa
ON/A
8.
Correct Containers Used:
Yes ONo
E3N1A
9.
-Pace Containers Used:
Yes Onto
ONIA
Containers Intact:
Yes ONO
ONlA
10.
Filtered volume -received for Dissolved tests
Oyes ONO
06.
11.
Sample Labels match WC:
Ye O , o� � 1N/A
12,
-Includes dateltimellD/Anal is Matrix:
[�
All containers needing preservation have been checked.
yes ONo
ONIA
13.
All containers needing preservation are found to be in
yYes ONO
ONIA
compliance with EPA recommendation,
l
exceptions: VOA, coriform, TOC, 0&G, WI-DRO (water)
Yes ONO
Samples checked for deohtorination:
es ONo
OWA
14.
Headspace In VOA Vials >6mm).
[]Yee ONO
VVrWA
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Oyes ONO
Oyes ONO
NIA
C1fA
16.
Pace Trip Blank Lot# if purchased):
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted:• DatelTime:
Comments/ Resolution:
SCURF ISRF
Review::
Note: Whenever there Is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( Le out of hold, incorrect preservative, out of temp,
Incorrect containers)
Place label here
OR
Handwrite project number
(If no label available)
Page 6 of 7

�
%t°2CEAi1r21ytlCd(;
Document Name: Sample Condition Upon
Recel t SCUR
Document Revised: Apri104, 2013
—Page 2 of 2
Document No.:
F-RAL-CS-001-rev.02
Issuing Authorities:
Pace Asheville Quality -Office
�
e
a
•
�
e
e
�
MEN
•
e
e
■■■■■■■■■■■■■■■
Client Sample ID s
Sam fe Discre anc
H Adjustment Log for Preserved Samples
Sample ID
Type of
Preservative
pH upon
receipt
Date preservation
Adjusted
Time Preservation
rousted
Amount of
Preasrvative added
Lot# of
Preservative
Bottle Code Key
125 ml Plastic Unp: BP4U
250 ml Plastic Unp: BP3U
500 ml Plastic Unp: BP21J
1 Liter Plastic Unp: BP1 U
250 ml Plastic: H2SO4. BP3S
250 ml Plastic HNO3: BP3N
250 ml Plastic ZN Acetate. BP3Z
250 ml Plastic NaOH: BP3C
Wide mouthed glass jar unp: WGFU
1 Liter Amber Unp: AG1U
1 LiterAmber NCI: AG1H
500 ml Amber Unp: AG2U
1 Liter Amber 1­128 4: AG1 S
250 ml Amber H2SO4: AG3S
250 ml Amber NH4CL: AG3A
40 ml VOA HCI: DG9H
40 ml VOA Na2S203: VG9T
40 ml VOA Unp: VG9U
Q ml VOA H2SO4: DG9S
5035 Kit: VOAK
VPH 1 Gas Kit: VIGK
125 ml Sterile Plastic: SP5T
250 mi Sterile Plasiio: SP2T
Page 7 of 7

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: Town of Ramseur Permit Number: WQ00010528
WWTP Name: Ramseur WWTP NPDES Number: NCO026565
Monitoring Period: From 1/1/2014 To 12/31/2014
AMWathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
1
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 40
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ra
Gmma Ray
Pasteurization ❑
Class B:
Alternative 1 ❑
Alternative 2 ®
Alternative 3 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization p
Air Drying ❑
Com ostin ❑
jAerobic Digestion ❑
Anaerobic Di estion
...........::. :: :: ::: ::._._.
.........................................
If applicable to alternative performed
(Class A or Class B) complete the
following monifto
Ing data:
Parameter
MIUMIUM
Level in
1Qj-A--
Pathogen Density �
Number o
Excee-
gucesysisType
requency
of
Sample
a ytica
Tech-
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the 6th
power MPN per
gram of total
solids or 2 x 10 to
the 6th power
CF[J per gram of
1000 mpn per
gram of total solid
(dry weight)
lmonella bacteria
in lieu of fecal
coliform
3 MPN per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ® Option 2 ❑ Option 3 ❑ Option 4 , ❑ Option 5 ❑
Option 6 R1 Option 7 ❑ I Option 8 ❑ Option 9 ❑ Option 10 ❑
No vector attraction reduction options were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Z, r A
arer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer Date Signature of Land Applier (if applicable) Date
DENR FORM RF (5/2003)

11/16/2014 22:05
Month
13363491008
)_aysuave %
REIDSVILLE WWTP
LiME LOG SHEET
Year .20 )N-
DATE
GAL. WASTED
initial TEMP "C
Initial pH, SU
LBS OF LIME
TIME
PH, SU
TEMP'C
Temp Corrected pH, 5U
pH after 2 HRS
TEMPT after 2 HIS
Temp Corrected pH, SU
PH after 24 HRS
TEMP "C after 24 HR5
P Corrected pH, SU
PAGE 01
fi Correction
Tem °C
Correction
40
Plus 0.45
39
Plus 0.42
38
Plus 0.39
37
Plus 0.36
36 -
Plus 0,33
35
Plus 0.30
34
Plus 0.27
33
Plus 0.24
32
Plus 0.21
31
Pius 0.18
30
Plus 0.15
29
Plus 0.12
28
Plus 0.09
27
Plus 0.06
26
Plus 0.03
25
0
24
Minus 0.03
23
Minus 0.06
22
Minus 0.09
21
Minus 0.17
20
Minus D.15
19
Minus 0.18
18
Minus 0.21
17
Minus o.24
16
Minus 0.27
15
Minus 0.30
14
Minus 0.33
13
Minus 0.36
17. I
Minus 0.39
11
Minus 0.42
10
MinusQ.45
"I certify, under penalty of law, that the Class 0 pathogen requlroments In 40 CFR, Part 503.32(b) have been met and the vector attraction reduction requirement in 40
CFR, Part 503.33(b)(4) and (6) have been met. This determination has been made under my direction and supervision in accordance with the system designed to ensure
that qualified Personnel properly gather and evaluate the Information used to determine that the pathogen and vector attraction reduction raquiremants have been met. I
am aware that there are significant penattles for false, certlflG7tion Including flne and imprisonment." 1�1 /�
Printed Name & Title 1-P v-' - -, �,_ w Ct i 1 e h -� U �
Signature i -A. A V` - ' , P 3 1 ~ ?

11/16/2014 22:05
13363491008
REIDSVILLE WWTP
PAGE 02
Month
1 LIME LOG SHEET
:e ID Ir 4x �r li Year . B
,DATE
!/ L F t
GAL, WASTED
3 oa4
initial TEMP °C
Initial pH, SO
1.85 OF LIME
�p
TIME
0 00
PH, SUJZ.
TF,MP °C
t
Temp Corrected pH, SU
pH after 2 HRS
TEMP °C after 2 HRS
7 t
Temp Corrected pH, SU
PH after 241-1RS
IS•✓
TEMP°Cafter24HR5
Z•s�
P Corrected PH, SU
PH Correction
Tem °C
Correction
40
Plus 0.45
39
Plus 0.42
38
Plus1339
37
Plus 0.36
36
Plus 033
35
Plus 0.30
34
Plus 0,27
33
Plus 0.24
32
Plus 0.21
31
Plus 0.18
30
Plus 0.15
29
Plus 0.12
28
Plus 0.09
27
Plus 0,06
26
Plus 0,03
25
0
24
Minus 0.03
23
Minus 0.06
22
Minus 0.09
21
Minus0.12
20
Minus 0.15
19
Minus 0.18
18
Minus 0,21
17
Minus 0.24
16
Minus 0.z7
15
Minus 0.80
14
Minus U33
13
Mlnus 0.36
12
Minus 0.39
11
Minus 0.42
10
Minus 0.45
"I certify, under penalty of law, that the Clnss 13 pathogen requlrements in 40 CFR, Part 503.32(b) have been met and tho vrCtor attrastlon reduction requirement in 40
CFR, Part 503-33(b)(4) and (6) have been met, This determination has been made under my direction and supervision In accordance with the systemdesigned to ensure
that, qualified personnel properly gather and evaluate the information used to determine that tha pathogen and vector attraction reduction requirements have been met.
am aware that there are signIRcitnt panaluna for false cerdficatlon Including finr, and imprisonment,''
Printed Name & Title a rb' V' 1►3 F .Q 1�0,
Signature

11/'16/2O14 22:05
Month
13363491008
Mcx V-G1 N .
REIDSVILLE WWTP
LIME LOG SHEET Year t ` l
DATE
GAL, WASTED
loe
Initial TEMP °C
Initial pH, 5U
LB5 OF I.IM@
TIM[
pH, su
TEMP °C
Temp Corrected pH, sU
pl,l after 2 HR5
TEMP "C After 214RS
Temp Corrected pH, 5U
pH after24 HR5
TEMP "C after 24 HR5
-p Corrected pH, 5U
PAGE 03
H Correction
Tem "C
Correction
40
Plus 0.45
39
Plus 0.41
38
Plus 0.39
37
Plus 0,36
= 36
Plus 0.33
35
Plus 0.30
34
33
Plus 0.27
Plus 0.7.4
32
Plus 0.21
31
Plus O.18
30
Plus 0.15
29
Plus O.12
28
Plus 0.09
27
Plus 0.06
26
plus 0,03
25
0
24.
Minus0.03
23
Mlnus0.06
22
MInLis 0.09
21
Minus 0.12
20
Minus 0.15
19
Minus 0.19
18
Minus 0.21
17
Minus 0.24
16
Minus 0.27
15
Minus 0.30
14
Minus 0.33
13
Minus 0.86
17
Minus 0.39
11
Minus 0.42
10
Minus 0.45
"I certify, under penalty of law, that the Class B pathogen requirements In 40 CFR, Part 503.32(b) have been met and the vector attraction reduction requirement In 40
CFR, Park 503.33(b)(4) and (6) have been met. This determination has been made under my direction and supervision In accordance with the system designed to ensure
that qualified personnel properly gathe.rand evaluate the Information used to datermine Lhat the pathogen and vector attracti0n reduction requirements have•, been met.
am aware tht there are significant penalties for false certification including floe and Imprisonment_"
Printed Name &Title -R r" -Li te w ( k-N
Signature � ;5 1 - I q

11/16/2014 22:05 13363491008 REIDSVILLE WWTP PAGE 04
Month
LIME LOG SHEET
Year
DATE
GAL.WASTED
3c�oa
Initial TEMP °C
01
6.
Initial pH, SU
LBS OF LIME
16
TIME
PH, su
TEMP'C
bs
Temp Corrected pH, SU
PH after 7. HRS
TEMP'C after 2 HRS
! �"
Temp Corrected pH, 5U
i2•Z
PH after 24 HRS
TEMP "C after 24 HRS
/ r
lip Corrected pH, SU
W Correction
Tem °C
Correction
40
Plus 0.45
39
Plus 0.42
38
Plus 0.39
37
Plus 0,36
=-°36 =
Plus-0.33--
35
Plus 0.30
34
Plus OX
33
Plus 0.24
32
Plus 0.21
31
Plus 0.13
30
Plus 0.15
79
Plus 0.17
U
PIUS 0.09
77
Plus 0.05
26
Plus 0.03
25
0
24
Minus 0.03
23
1 Minus 0.06
22
Minus 0.09
21
Minus 0.12
20
Minus 0.15
19
Minus 0,18
1s
Minus 0.21
17
Minus 0.24
16
Minus 0.27
15
Minus 0.30
14
Minus 0.33
13
Minus 0.36
12
Minus 0.39
11
Minus 0.42
10
Minus 0.45
"I certify, under penalty of law, that the Class B pathogen requirements In 40 Cr-R, Part 503.32(b) have been met and the vector attraction reduction requirement In 40
Cr•R, Part 503.33(b)(4) and (6) have been met. This daterntin-Ition has been made under my direction and supervision In accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the Inrormation used to determine that the pathogen and vector attraction reduction requirements have been met. I
AM aware that there are significant penalties for false certification including fine and Imprl onment."
Printed Name &Title A el ('
Signature

11/16/2014 22:05
Month
133634.91008
REIDSVILLE WWTP
LIME LOG SHEET �a
Year Zo
DATE
GAL. WASTED
200
Initial TEMP `C
Initial pH, SU
-
-
WS OF LIME
�OQ 1
TIME
Oct bO
PH, SU
TEMP 'C
Temp Corrected pH, SU
PH after 2 HRS
TEMP'C after 2 HRS
•
Temp Corrected pH, SU
PH after 24 HRS
b
TEMP "C after 24 HRS
yip Corrected pH, SU
QQ
�.0
PAGE 05
H Correction
Temp'C
Correction
40
Plus 0.45
39
Plus 0.42
38
Plus 0.39
37
Plus 0.36
- - 36
plus 0.33
35
Plus 0.20
34
Plus 0.27
33
Plus 0,74
32
Plus 0.21
31
Pius 0.18
. 30
Plus 0.13
29
Plus 0.12
28
Plus 0.09
27
Plus 0.05
26
Plus 0.03
25
0
7.4
Minus 0.03
23
Minus 0.06
22
Minus 0.09
21
Minus 0.12
20
Minus 0.15
19
Minus 0.18
18
Minus 0.71
17
Minus 0.24
R6
Minus0.27
15
Minus 0.30
14
Minus 0.33
13
Minus 0.36
12
Minus 0.39
11
Minus 0.42
10
Minus0.45
"I certify, Under penaTty of low, that the [lass 13 pathogen requirements In 40 CFR, Part 503.32(b) have been met and the vector attraction reduction requirement In 40
CPR, part 503.33(b)(4) and (6) have been met. This determination has been made under my direction and supervlsion In accorlllance with the, system designed to ensure
that qualified personnel property gather and evaluate the Information usod to determine that the pathogen and veetor attraction reduction requirements hive been met.
om'aware that there are significant penalties for false certification Including fine and imprisonment."
Printed Name &Title, _ R(rtiry ,o��,�,�f,_,
Signature
-&M

11/16/2014 22:05 13363491008 REIDSVILLE WWTP PAGE 06
Month
%A
LIME LOG SHEET
Year
DATE
GAL. WASTED
3 oac�
Initial TEMPT
©
InitlaI pH, Su
j
LB50FLIME
TIME
o
PH, SU
,z, b
TEMP °C
L
Temp Corrected PH, SU
PH after 2 HRS
`
TEMP °C after 7. HR5
Temp Corrected pH, SU
PH after 24 HRS
f
TEMP °C after 24 HRS
ip Corrected pH, SU
H Carrection
Tem °C
Correction
40
Plus 0.45
39
Plus 0.42
38
Plus 0,39
37
plus 0.36
- 36 - :—
Plus
35
Plus 0.30
34
Plus 0,27
33
Plus 0.24
32
Plus 0.21
31
Plus OAS
30
Plus 0.15
29
Plus0,12
28
Plus 0.09
27
Plus 0.06
26
Plus 0.03
25
0
24
Minus 0.02
23
Minus 0.06
22
Minus 0.09
21
Minus 0.12
20
Minus 0.15
19
Minus 0.18
18
Mlnus 0.21
17
Minus 0.24
16
Minus 0.27
15
Minus 0.30
14
Minus 0.33
13
Minus 0.36
12
Minus 0.39
11
Minus 0.42
10
Minus0.45
"I certify, under penalty of low, that the Class B pathogen requirements In 40 CFR, Part 503.32(b) have, been met and the vector attraction reduction requirement to 40
CFR, Part 503.33(b)(4) and (G) have been met. This determination has been made under my direction and supervision In accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the Information used to determine thatthe pathogen and vector attraction reductlon requirements have been met, I
am aware that there are significant penalties for false, certlFicmlon Includingflne and Imprisonment." �k
Printed Name&Title ��.�e"SA
5ignature 1 vtics �'

4
11/16/2014 22:05
onth
13363491008
REIDSVILLE WWTP
LIME LOG SHEET
Year
DATE
L
GAL. WASTED
Initial TEMP "C
Initial pH, SU
LB5 OF LIME
TIME
PH, SU
TEMP "C
Temp Corrected pli, SU
PH after 2 HRS
TEMP °C after 2 HRS
Temp Corrected pH, SU
pl•I after 24 HRS
TEMP "C after 2414PS
p Corrected pH, SU
'
PAGE 07
H Correction
Tem "C
Correction
40
Plus 0.45
39
Plus 0.42
38
Plus 0.39
37
Plus 0.36
36
Plus 0.33
35
Plus 0.30
34
Plus 0.27
33
Plus 0.24
32
Plus 0.21
31
Plus 0.18
30
Plus 0.15
29
Plus 0.12
28
Plus 0.09
27
Plus 0.06
26
Plus 0.03
25
0
24
Minus 0.03
23
Minus 0.06
22
Minus 0.09
21
Minus 0,12
20
Minus 0.15
19
Minus 0.18
19
Minus 0.21
17
Minus 0.24
IS
Minus 0.27
15
Minus0.30
14
Minus 0.33
13
Mlnus0.36
12
Minus0.39
11
Minus 0.42
10
jMlnus0,45
"I rortify, under penalty of law, that the Claw 9 pathogen requirements In 40 CPR, Part 503.32(b) have been met and the vector attraction reduction requirement in 40
CrR, Part 503.33(b)(4) and (6) have been met, This determination has been made under my direction and supervlslon In accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the Information used to determine that the pathogen and vector attraction reduction requirements have been met.
am aware that there are significant penalties for false certification iociuding Fine and imprisonme
Printed (dame & Title Y'
5ignature
0

11/16/2014 22:05 13363491008 REIDSVILLE WWTP PAGE 08
r
Month
LIME LOG SHEET A
Year
DATE
GAL, WASTED
Initial TEMP"C
KI
initial phl, SU
CBS OF LIME
TIMC
pH, SU
TEMP "C
Temp Corrected pH, SU
PH after 7, HRS
TEMP "C after 2 HRS
Temp Corrected pH, SU
pH after 24 Has
TEMP `C after 74 HRS
t
np Corrected pH, SU
I.1 Correction
Tempt
Correction
40
Plus 0.45
39
Plus 0.47
38
Plus 0.39
37
Plus 0.36
=_-36=PIos:0.33-
35
Plus 0.30
34
Plus 0,27
33
Plus o.74
32
Plus 0.21
31
Plus 0.18
30
Plus 0.15
29
Plus 0.12
28
Plus 0.09
7.7
Plus 0,06
26
Plus 0.03
25
0
24
Minus 0,03
23
Minus 0.06
22
Minus 0.09
21
Minus 0.12
20
Minus 0.15
19
Minus 0.18
18
Mlnus 0.21
17
Minus 0.24
15
Minus 0.27
15
Minus 0.30
14
Minus 0.33
13
Minus 0,36
12
Minus 0,39
11
Minus 0.42
10 1
Minus 0.45
'I certlfy, under penalty of law, that the Class > pathogen requirements in 40 CFR, Part $03.32(b) have been mat and the vector attraction reduction requirement In 40
CrR, Part 503,33(b)(4) and (6) have been met. This determination has been made under my direction andsupervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the information used to determine that the pathogen and Vector attraction reduction requirements have been met.
am aware that there are signlFlcant penalties for false certlfIcation including fine and ImprLson a t."
Printed Name & Title _ t v- �
Signature V '[o-- Vt' 'A 'Z 9.— 1

11/16/2O14 22:06
13363491008
REIDSVILLE WWTP
PAGE 09
onth
Gelp1,ems
LIME LOG SHEET LA
Year �� 1
DATE
GAL. WASTED
Initial TEMP °C
Initial pH, SU
LBSOFUME
tot) i
TIME
PH, SU
TEMP °C
Temp Corrected pH, SU
' r
PH after 214RS
.5
TEMP "C after 2 HRS
q Q
1• V
Temp Corrected pH, Su
,
PH after 24 HR5
TAMP °C after 24 HR5
1p Corrected pH, SU
H Correction
Temp"C
Correction
40
Plus 0.45
39
Pius 0.42
38
Pius 0,39
37
Plus 0.36
-36-
Plus0.33
35
Pius 0.30
34
Plus 0.27
33
Plus 0.24
32
Plus 0.21
31
Plus 0.18
30
Plus 0.15
29
Plus 0.12
28
Pitts 0.09
27
Plus 0.06
26
Plus 0.03
25
0
2A
Minus 0.03
23
Minus 0.06
22
Minus 0,09
21
Minus 0.12
20
Minus 0.15
19
Minus 0.18
18
Minus 0.21
17
Minus 0.24
16
Minus 0.27
15
Minus 0.30
14
Minus0.33
13
Minus 0.36
12
Minus 0.39
11
Minus 0.42
10
IMInus0.45
"I certify, under penalty of faw, thatthe Class 13 pathogen requirements In 40 CFR, Part 503,37(b) have been met and the vector attraction reduction requirement In 40
011, Port 503.331b)(4) 8nd (6) have been met. Tills determination has been made under my direction and supervision In accordance with the system deslitned to ensure
that; quilifled personnel properiygather and evaluate the Information used to determine thatthe pathogen and vector attraction reduction requirements helve been met. I
am aware that there are significant penalties for false certificatlon InrludlnR fine and Imprisonment."
�
Printed Name & Title
Signature 30 1 "6

11/16/2014 22:05 13363491008 REIDSVILLE WWTP PAGE 10
r
r
lonth 'D
LIME LOG SHEET
Year SO 1
DATE
GAL. WASTED
�D �
Initial TEMP •C
Initial pH, su
LB5 OF LIME
TIME
PH, su
TEMP •C
Z�
Temp Corrected pH, 5U
pl•I after 214RS
T[MP •C after 2 HRS
Temp Corrected pH, SU
pH after 24 HRS
TEMP •C after 24 WRS
ZZ•
np Corrected pH, SU
H Correction
Tempi
Correction
40
Plus 0-45
39
Plus 0.4.2
38
Plus 0.39
37
Plus 0.36
=----36
Plas'0.33
35
Plus 0.30
34
Plus 0.27
33
Plus 0.24
32
Plus 0.21
31
Plus OAS
30
Plus 0.15
29
Plus 0.12
28
Plus 0.09
27
Plus 0.06
26
Plus 0.01
25
0
24
Minus 0.03
23
Mlnus0.06
22
Minus 0.09
21
20
Minus0.12
Minus 0.15
19
Minus 0.18
18
Minus 0.21
17
Minus 0.24
16
Minus 0.27
15
Minus 030
14
Minus 033
13
Minus 0.36
12
Minus 0.39
11
lmjnusO.42
10
Minus 0.45
"I certify, under penalty of law, that the Class 1 pathogen requirements In 40 CFR, Part 503.32(b) have been met and the vector attraction reduction requirement In 40
CPR, Part 503.33(b)(4) and (6) have, been met. This determination has been made under my direction and supervlslon In accordance with the system designed to ensure
that qualif nd personnel properly gather and evaluate the Information used to doff rminethat the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine andq Impprisonme "
Printed Name & Title �V'!'—U L�(.) f,> c
Signature

11/16/2014 22:05
13363491008
REIDSVILLE WWTP
PAGE 11
RI-inth
���-cv►n�2v--
LIME LOG SHEET
Year
DATE
GAL WASTED
^
Initial TEMP °C
Initial pH, SU
LDS OF LIME
TIME
PH, SU
01
TEMP °C
Temp Corrected pH, SU
PH after 2 HRS
TEMP'C after 7. HRS
Temp Corrected pH, SU
PH after 24 HR5
TEMP "C after 24 HRS
p Corrected pH, SU
pH Correction
Tem 'C
Correction
40
Plus 0.45
39
Plus 0.42
38
Plus 0.39
37
Plus 0.36
35
Plus 0.33,
35
Plus 0.30
34
Plus 0.27
33
32
Plus 0.24
Plus 0.21
31
Plus 0.18
30
Pius 0.15
29
28
Plus 0.12
Plus 0.09
27
Plus 0.06
26
Plus 0,03
25
0
24
Minus 0.03
23
Minus 0.06
22
Minus 0.09
21
JMinusO.17
20
Minus 0.15
19
Minus 0.18
18
Minus 0.21
17
Minus 0.24
16
Minus 0.27
15
Minus 0.30
14
Minus 0.33
13
Minus 0.36
12
Minus 0.39
11
Minus 0.42
10
jMInus0.45
"I certify, under penalty of law, that the Class 8 pathogen requirements In 40 CFR, Part 503.37(b) have been met and the vector attraction reduction requirement In 40
CFR, Part 503.33(b)(4) and (6) have been met. This determinatlan has been made under my direction and supervision In accordance with the system designed to ensure
that qualifind personnel properly gatherand evaluate the Information used to dptermine that the pathogen and voCtorattraction reduction requirements have been met. I
am aware that there are significant penattles for false certification Including fine and imprlsonm t1"
Printed Name & Title C V`y `l Q 1�^�� C) l�
Signature
It--47,B--)

11/16/2014 22:05 13363491008 REIDSVILLE WWTP PAGE 12
I.IMr. 1,06 SHEET
,k
�� Year �. i�
"I Certify, vndnr ponalty of Iwk, that the CIn,;S g pathoSpn In Ap CPR, Part 50.3,32(b) have been met and t(ie vector AWIrtlon rRduction requirement In 40
CPR, Part S09.33tb)(4) Nnd (6) hstve been mtri, Thie detarminatlan Ills ho p alatic under my directlon and supervlslan In a=nrdance with the ryrtnm designed to ensure
that qunliflerl persr nnfl praperly gathRr and rvalunte t11+! Infnrmatlnn uE;Rd th1 rleti.trntine that the pathogen and vpctorattractlart reductlon requirement, hswe been mo..
7m aware that tt1P.ro am rIgniflcnnt penalritts fnr false COMIFICaatIown Inc10011+9 fine and inlpr1, Om" t "
Printed 1 BM(-- & 1140
71
Signaturp