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WQ0010059_2014 Annuual Report_20150220
0 � - February 17; 2015 City of Lenoir PO Box 958 Lenoir, NC 28645-0958 North Carolina Department of Natural Resources Division of Water Resources Water Quality Permitting Section Non -Discharge Permitting Unit 1636 Mail Service Center Raleigh, NC 27699-1636 Subject: Annual Residuals Report for CY 2014 To Whom It May Concern: Enclosed are three (3) copies of the annual residuals report for the 2014 calendar year for the City of Lenoir's Lower Creek WWTP Residuals Facility; permit number WQ0010059). Included are the following: • Annual Distribution and Marketing / Surface Disposal Certification and Summary Form (for Class A residuals) • Annual Distribution and Marketing / Surface Disposal Certification and Summary Form (for unpasteurized belt pressed sludge, which was disposed in the landfill) • Annual Residual Sampling Summary Form • Annual Pathogen and Vector Attraction Reduction Form • Plant Available Nitrogen calculations • All lab sheets received for 2014 for residuals analyses • Biosolids logs, which includes tonnage processed, pH, temperature Due to the "Class A" treatment being down performed two (2) times during the year. A end of the calendar year, was not performed. limits. for the latter half of the year, sampling was TCLP, which is normally performed near the All monitored parameters were below permit If there are any questions or if any further information needed, please call me at 828-757- 2198 or email me at mlwall-ci.lenoir.nc.us. Sincerely, RECEIVEDIDENROWR FEB 2 ® 2015 Monte L. Wall Superintendent UWVT wabrQnrl itiit�g Perm ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM , PERMIT #: WQ0010059 FACILITY NAME: of Lenoir - Lower Creek WWTP PHONE: 828-757-2198 COUNTY: Caldwell OPERATOR: Mr. Calvin Dula FACILITY TYPE (please check one): ® Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) 0 Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? CI Yes ❑vo No If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) s) (include NPDES # if applicable) Volume (d tons) Reci Tent Information Admendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January WWTP sludge from the 24.59 54.56 79.15 See attached 82.49 Pasture land: February following sources: 24.36 54.56- 78.92 list of biosolids 10.25 Crops and ha March Lower Creek WWTP 47.71 72.79 120.5 recipients 53.93 Lawns April Gunpowder Creek WWTP 0 55.96 55.96 145.94 "- May Lenoir Water Plant 25.04 60.76 85.8 123.73 see attached June Blowing Rock WWTP 24.48 67.2 91.68 51.33 sheet for Jul (Blowing Rock WWTP sludge 0 54.64 54.64 if 26.89 amounts read August is introduced at the 0 18.77 18.77 it19.56 by City of September headworks of theplant) 0 it0 Lenoir; also, October 0 it0 product that was November 0 it0 hauled awa December 0 0 by individuals Totals: Annual (dry tons): 146.18 439.24 585.42 514.12 Admendment s used: I Quicklime Bulking Agent(s) used: I None * If more space than given is required, please attach additional information sheet(s). Lff Check box if additional sheet(s) are attached Part C: Facility was compliant during calendar year 2014 with all conditions of the permit (including but not limited to items 1-3 below) issued by the Division of Water Quality. 0 Yes ® No If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that ere are significant penalties for submitting false informaiton, includin t e possibility f fines and imprisonment for knowing violations." Sign re of Permittee Date Signature of Preparer** Date (if different from Penmittee) **Preparer is defined in 40 CFR Part 503.9(r) DENR FORM DMSDF (5/2003) ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM • '* PERMIT #: WQ0010059 FACILITY NAME: City of Lenoir - Lower Creek WWTP (sludge pressed and taken to landfill) PHONE: 828-757-2198 COUNTY: Caldwell OPERATOR: Mr. Calvin Dula FACILITY TYPE (please check one): C] Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar ear? 0 Yes ❑vo No If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) s) ( include NPDES # if applicable) Volume (d tons) Reci lent Information Admendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January WWTP sludge from the February following sources: March Lower Creek WWTP April Gun owder Creek WWTP May Lenoir Water Plant June Blowing Rock WWTP Jul (Blowing Rock WWTP sludge August is introduced at the 33.05 33.05 33.05 All sludge September headworks of theplant) 70.5 70.5 70.5 listed on this October 68.65 68.65 68.65 spreadsheet November 55.1 1 55.1 55.1 was taken to December 60.4 1 60.4 60.4 landfill. Totals: Annual (dry tons : 1 0 287.7 1 287.7 287.7 Admendment s used:Quicklime Bulking Agent(s) used: I None * If more space than given is required, please attach additional information sheet(s). 0 Check box if additional sheet(s) are attached Part C: Facility was compliant during calendar year 2014 with all conditions of the permit (including but not limited to items 1-3 below) issued by the Division of Water Quality. R1 Yes ❑ No If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that tbjere are significant penalties for submitting false informaiton, includin he possibility o fines and imprisonment for knowing violations." Signaf6re of Permittee Date Signature of Preparer* Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) DENR FORM DMSDF (5/2003) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: NCO023981 Facility Name: City of Lenoir - Lower Creek WWTP NPDES # or WQ0010059 WQ#: WWTP Name: Residual Analysis Data Lower Creek WWTP Laboratory: 1) Blue Ridge Labs (#275) 2) Pace Analytical (# 12710) 3) 4) 5) Sample or Composite Date 4/16/14 6/24/14 Percent Solids 42.7 32.9 Arsenic 2.2 <1.0 Cadmium 0.8853 <0.1172 Chromium 14.7 19.4 ,b Copper 104 266 Lead 7.8 5.7 Mercury 0.0641 0.0613 Molybdenum <0.457 <0.586 Nickel 14.6 47.7 Selenium <1.5 <1.6 Zinc -167 382 Total Phosphorus 14,005 18,377 TKN - 19,995 28,495 nia-Nitrogen 1,083 1,155omand Nitrite 32.9 1 32.9 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware. that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer Date DENR FORM RSSF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM .Facility Name: City of Lenoir Permit Number: WWTP Name: Lower Creek WWTP NPDES Number: Monitoring Period: From 1/1/2014 To 12/31/2014 WQ0010059 NCO023981 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ s Alternative 4E—]--T Alternative 5 0 Alternative 6 ❑ If applicable to alternative erformed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ F Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ e a Beta R ❑ Y a GammRa ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 L-3--"T Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens Lime Stabilization ❑ 1 Air Drying ❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Die sdo n ............................................................................................ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- dences Frequency of Analysis Sample Type Analytical Tech - e Minimuni Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power WN per gram of total solids or 2 x 10 to the 6th power CFU per gram of 1000 mpn per gram of total solid (dry weight) <0.004 0 (<0.005) <0.006 MPN/G 0 7 / smpl grab mult.tub Salmonella bacteria (in lieu of fecal coliform) 3 NTN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 ❑ Option 2 ❑Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 R1 Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ 571 ' µ No vector attraction reduction options were ,performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been'made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Monte L. Wall / Superintendent WWTP Calvin Dula, ORC Biosolids / Land Application Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 91 2-4- -lam C— . L�, 4 1, — Sign46eofPrcparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) Plant Available Nitrogen: Lower Creek WWTP Biosolids For 2014 Calendar Year Residuals Facility Permit # WQ0010059 NPDES # NCO023981 :E ca rn o z .� m� �_ 0 2 L- is 0 N5 ca a M`- .-. `"' 0 O O Z 0a? Quarter / Sample Y o =rn 0 o z Z > Qa) c� a oz _. E 0m �u> �o CD 0 c($ :3 U w v)0 00 �' _Cc a 0- z + z (mg/kg) (mg/kg) (mg/kg) (mg/kg) % % 1 st Sample 2014 19,995 1,083 32.9 0.36 7,194 136.57% 1.40% 2nd Sample 2014 28,495 1,165 32.9 0.35 10,179 7.42% 1.84% CY 2014 Average: 1 24,245 1,119 32.9 0.35 8,687 1 72.00% 0.87% Note: The mineralization rate used (0.35) is based on the numbers given at the annual land application school. Composted sludge has a mineralization rate of 0.1; anaerobically digested, 0.2; aerobically digested, 0.3; unstabilized primary and waste activated, 0.4. Since our sludge is a mix from several sources and since there is some aerobic digestion (not complete) at the Gunpowder Creek WWTP and no digestion at the Lower Creek WWTP (these two are the major sources), a mineralization rate of 0.35 was chosen. City of Lenoir Siosolids.Lon e 77. ` F °' : -Gl PERCENT SOLIDS " VOLUME 'OF' FEED` SLUDGE - N Ow --COMMENTS--- W - . a Feed Belt Final ;Start :;, End Total y,Q _- i" o, Sludge Preis'. Product..'.-Reading Reading-.. Gallons -L - •i .i°.19, 1 S -YI,' I , WJ" - 7' ••y - ;'.{' _ ' 'i f .mot' �'f �' G i 4 ? G�jl`^ J � • � 'r•�/T•^��j � "�/ 'Y+ j- Sr ��1 i� J P. ? AVg 2- !'.�%r �~�' �•_j�:. :)�A _'�-.. yy �:: ` f7 !o.� e'✓ f'J t¢� !a ; ire `r,", {' i Av ' -. - ;�✓y�G�r� • 2 Avg Avg 2— Avg Avg - DRY -TONS -PROCESSED.°/6-SOLIDS FEED -SLUDGE X 8:34 X TOTAL GALLONS FEED SLUDGE /-200,000 Biosolids Forms 12/2/2014 City--4-Lenoir Biosolids Log _ w ti pH: / ;CORRECTED -pH of Final Product:, Initial pH . ` 2 Hour pH 24 Hour H w�o- o c - �a U McDv D. �Q U Oc HCcD E a . o m� - o, lit �m� o ;. a a� 1 :oEU c. m m��'o ;•Q,,`oO o-a; t - I u 3 Additional Comments Biosolids Forms 12/2/2014 I r-l"fis of-1 dino%'ir. MirtaMMa I two ,77.7 ''OEEID'SLUDGE 'Z - PERCENT SOLIDS'-- VOLUME 0 u F CO 0 w w .--COMMENTS.--- -0. W, a. Feed Belt Final `StartEnd Total -----Sludge.-,* Press:, Product., Retidihg irReaclind!- Gallons 2' 271 J6 3, /V ��I _4 2 AVc-f'/ Avdf z -1 —A-Yee 7� 2 Avd^/. '71) 2 ly Avg'- 2 V. A61 617 Ay ,/6. 2 IV7 7 t i '2 - ',4, _� �17 Avc_Y t --- DRY.TONS. PROCESSED = -9/o-SOLl08'FEEU SLUDGE--X8.5-4-XT 0 TALAGALLONS-FEED-SLUDGE/ 200,,000- Biosotids Forms 7/2/2014 • City .of i*of Lenoie'81,66011ft tog. PW/ "CORRECTEP, PH.of Final Prd'duct. Initial PH 2 Hour PH z 12.0) 24 Hour PH z 11.5) w o T O.S E 3f CL -0 'a) a CL de 12 0 L ') %, "' (D A �1-1 CL.Ld 0 a 1 0 . 1.0 (D O. 0 V W: 4) 2 t5 a t 0-0 aCL -0 jao), :D 0 0 C, it 4) -a' CL 8; 0-1 C. E C to D -0 r 0) t., 'M. 0 0 '3f aIM U js� S 4) I 0' U Additional Comments .-77777— ,NOTE. Be.sure to check 2,hourpH and 24 hour pWoreve r is ces y day that bibsolids.. re p o sod. Bios , ofids Forms m s " 7/2-'/'2014 P f%a%• &,kf 1 enO%iw Q®f1QA1;AC% 1 ~n �c 7777,777, , ` 1 PERCENT SOLIDS,": -VOLUME-OF'FEED-SLUDGE - z a cc - - -- - `CL t , -C „a Feed Belt Final Start E End,;! Total o Sludge, Press' Product Readin i =Readin Gallons --- IQ 7—�'r •�..LL .i_�_t, ('`_ _ _ `i `- --•' '-• � - �` a ::%i .-ts : �',;, � — 4 `''d' � La• ^i.; p.w - '�.,�•i _ ;'1•-_ , 4 -� � - Av ;-•,-. - j/ .Sr - r 7 yJ�,7 i tom.-.J _ fl„� h-�.r•- ::;��_�_:_ � - -_r_ 70 Ir 7i 2 /I.L.1a10 *.5 47p tti --- j %ram+ (0 � 20.`� r j,� �/ -5,l l AV / Avg 2,Ll ,;�J,'j , _� .: ;J���, I' : - y DRY TONS PROCESSED_ %SOLIDS`"FEED SLUDGE X-8 3*,L X TOTAL'GALONS FEED=SLUDGE % 200OC10 _ Biosolids Forms 7/2/2014 =City f L - - B 1 d ' L- o enoir ioso i s og 4 pH I. -CORRECTED :pH of. Final Product' Initial PH 2 Hour pH a: 12.0 24 Hour pH a 11.5 o am•-w -' CL as - CL ,< - UvN o u =` a Oc a. m Q, c UOcO5 FM- ; CL Ho. =-c �Q(D o .c.:.Icr co ..Q-U ��cw o0,.,0 0,20 Additional -Comments.. , - ..... ...,.....,...e.....�.,v.,..�.i..�..+,+�.�.�—..��.,................r,......,..,.+.,..+,+�.�..�.�...,,.,,.. mrwn�„—,w�ww�wr.,.,,e,�„erw•,.•�wn..�a.n+..�,�w,• uw.�.w,�,. .., f � j :.'4 4 NOTE: Be sure to check 2.hour, pH and 24: hour pH for emety da that biosolids are processed. Biosolids Forms 7/2/2014 It x f4f%& of 1 nnnir RiewmMirlc 1 nn 7 7„ PERCENT SOLIDS' VOLUME OF FEED SLUDGE' " Cc p I' w ce 1-K 1 Feed" Belt Final Start End Y Total Slud a Press ; Product - Readin Aeadin R Gallons i, F i- r 1 `; �. 1(r..'Z__--•' 6tl g;,•e j nr i'a' �+��I� ,}v��m�i(�1"'k ✓, — Avyr._..>�O���V� 2. ter . 7 . 15 s� Avd .: -� r Av 7r,) 9,0 It, Yg� 4v' � r•..�.�4.fi,,^.f. .y a'..ti� _ DRY_TONS.P.ROCESSED =-•'%-SOLIDS, FEED -SLUDGE X-8;' 4C TOTAL'GALLONS FEED SL- UDGE / 200;000 Biosolids Forms 7/2/2014 ------ -Ctitk of L4666 r Mosolids Log pKI LCORRECTED- pHof, Final Prod t Uc Initial PH 2 Hour PH 12.0) 24 Hour PH (2- 115) HoCL M ft Os -E '040 o A) C 16_ 6 0 < 3f t5 L -.0 0 E M, CL 0 D, 4) CL CL 0 < CL. 0 kd 0 co (D M! CL 0 C CL E D to 0 0 CL C 0,101. U. CO Additional .Comments ,NOTE., Be,surelo, check.2 hour pH and 24 hour pH for evety day, that blosolids are propessedi, bio-so'lidi Forms 7/2/2014 I i`_ifii of 1' ®nnir Rin�nliA� .1_nn , f t u4 ° PERCENT SOLIDS! Feed. Belt Final '''Stud a Press } Product,.. VOLUME OF -FEED SLUDGE - Start �'. End Total Readin , Reading.L Gallons- Z N o. .CO ENT MM S_ '� .. FL _ - �., { � 1� �� L'l.� Pt - { �1 �, Ca:;f./ a �:illJ. �1 •E' - - -_ ��,.. l .T} 1 g: Q f 5:»' 1 Ev 'i`'+/. yt.�, % /�/Y,�J � r%`/ V� �•"t _ 0.., '�.••F�-',r: (Ly �e!�. � �.. 1: - a ?.a ,�//�` 1 �� � / �' f' � ,��... 1 r•'�. _ �� •.� i�•R,R•� /" t •,1 _ - - ! _ . 1 _J — — ,,..._. .,—,g.__. ay'3 _cr�j .U/'r✓ ��. . _•J.,�. J _ /�I jj j ({•'f�, 1 p7 � )�^/5 2 f 4, (s' a • � �' y � �t � - - — _ [ . e Yam• — -.. . _ -, ._ .— �f' ..! � f � � �,✓1 J•, � �"-7�J_�n /y>,�t' /ly r/ 1j, "/ •� �1 .,� ,y�7n'' — G✓` j ,� � •f _ + . /. . �_ _ ,1'I U'' S..� ,a� -. i�+L- `G+.,_'__� - . . t� - 2. a-%�%' - 3 _._ - --. - - - -._--_._._- '; - --- - 1�y. �q�, ��i'..� -�,:._'•.ham �-�'��-t.�'; ,; ,� -GJ 4, ` • �/ `;,,1 !"�' �Pf 2. _,�'S � �� '"�""� AV ) 1.w M�.,�pY l �� . '�•.w� :. .L - J � �it t�'�' lri � �,� � r'e' : fir_. ^).`� � � -� � s �:%'6''�' _ C - 7 .;,�' � .'•i' -'"' y/' / - � - - � ! ..a a;'v t� - ,c'� ' i ..` �` - .. _ 2 `1...'l.- i n r r Y- -^ --DRY TONS -PROCESSED =-WSOLIDS-FEED`SLUDGE-X$.34-XTOTAL GALLONS FEED'SLUDGE--% 200;000- Blosolids Forms •7/2/2014_ -of Lenoiir=Biosolids Lo p, H / CORRECTED , .a - pH._of-Final Product,, Initial pH _ 2 Hour pH a 12.0 i 24.Hour pH z 11.5 o : CL Cts aD CL a �c° �t.c CL -.v in.• co OQUowO v..N-; m �W U = v UcO/) l Additional Comments - NOTE. Be sure to check 2 hour pH and 24 hour H for every -day that blosolids.are pr9cessed . . Biosoliiis Forms 7%2%2014 I f+:ir. wi 1 wr�wi.. Qiwc�wli�c 0 wp k U) u ui •0 PERCENT SOLIDS VOLUME OF FEED SLUDGE cc I- w COMMENTS_.._ ._. _. -_ • o. Feed : Belt Final Start End • Total o . _ Sludge, Press Product -Readihcj Readin ° Gallons, Avd Itl �3o�cy j,7z 2 �� • p 5 /Y/ - 7 _; 1 � $ 2 Avg Av f7lJ41g r7 DRY TONS PROCESSED = /. SOLIDS FEED SLUDGE-X'-8.34 X-TOTAL-- GALL-ONS- FEED SLUDGE / 200;000- = Biosolids Forms 7/2/2014 City of Lenoir-BiosolIds Log . _. _..-- • --- - - - " --�.-_ _. _. __ - ..._ - -- - --� -- - -_.___ - .. ? pH../ CORRECTED pH of Final Product. Initial PH 2 Hour PH >_ 12.0 24 Hour. PH >_ 11.5 o ` O .•_ - (n �° 0CL.Cs, •I/�(/ - }Y E •a IA .. �S C �_ �W i— '/� _C i/ sir 5 •a� QU /��� III , _ W. �V�, .. •F� U C m� •U� ': `_ 0 ..- '''� O •FJ if xP� /]may _ -L a �U 0. .. /��� /A. W' .Y�' �� �-�a� W.-l..-' �'a•O -' /� V m a.`o. '� V/" /�� .�- W V C �� o`� ,�`'� L� �� °'c, r 1 a� �U �� -/A'l� /�� N�� �i W C ;N� ;�� -�� r /� O .0 N ..'-� � sQ�.'° :_� �. 15 - c. L ff `oco Additional Comments ------�---�---•-� _ � - r - �-- _ `' _.�.� >,�...'�-t, , Wiz, .....�.-.._.....,.._A..,�..� "� - � ,.._� -- ... m��—��—ru�www�win.u.r—r��w•wr.�see�w��—.��w — _ ( � NOTE. Be sure to check 2 hourpH and 24 hour pH for me , da that biosoiids are processed.. Biosolids Forms 762014 If Piks of 1 enoiw 1 ors PERCENT SOLIDS' 'VOLUME OF FEED SLUDGE co _ x COMMENTS _ Ui �- °' Feed :- Belt Final -, Start End • ; Total o Sludge. Press, Product Rea_din --Readinf -Gallons 3' .1 Av' oZOsY t ,I Ci 1] c �AS7 afi'.t..�;_ ^ ��..�.+3 f�' "jjl /Y� �'� -•'�`� l��y` � Av /� Jr�• P � ' _._ , e _ . . • .' ! d S,i;: ' (�� ,�..�' _t. J YY � _ter • - , ..-. ..1 � ` lYp� ��' ` (,,.. s ii �. J ••i• - i . " 1�/` `u�i�e ' ta 41- /r-� •' .-R' /•i�j/� Y,� ,._. •'.,.�^ �• __ .. .._ _.-a-'`-- _. __. _ -. ..- ,_ -, - Av 4 � 9 5 -f •- , —:mod z-- ��^-� C__ 7: 16 e. 1...� -v . 2 L=• "yam . ��' . . _.- .- .P"� �- �-/ •%. (.. _ � f� 04 g.do i e Q ref n - t 'I _-� .� Al .2 4f� ��. �qp .5 i Z, TONS.PRO.CESSED = %-SOLIDS-FEED-SLUDGE X 8:34 X=TOTAL GALLONS FEED" SLUDGE /;200;000 Biosolids Forms 7/2/2014 - City ofLdnoir Biosolids Log ply}.:/ -,CORRECTED pH -of. Final Product. Initial PH ; _ 2 Hour PH z 12.0 24 Hour PH z 111.5 o y `m ca �c O, E oS� I—e CL �= o� �� Ci s'Q.t ao ¢U o� 'Uv1 v� ; m �' Q. O E y HU m= o ° �cn .Q� ao, QU c C o� U..� a O Coil a E HU ;�D 'a- �� .�. _ aci a t QU CL .r = aci c C Additional Comments 4 4 - - - NOTE: Be sure to check 2 hour pH and 24,hour pff for evety day, that biosolids are pwcessed.,�� Bi6toIIds' Form§ 7/2/2014 w T 0 r-ifts Af. I Amne%ir Minanlirla I nn LV PERCENT SOLIDS" 7777771777 :7 7.7 'VOLUME OFFEED, SLUDGE ij 0 cc �7 to_0 CL Feed"," Sludge Belt Press Final Product.. Start Readi -'h al End eadinb, i Total Gallons 71 2 -LV—V-- Avd/ i7 ly 13 5 1. 4 2� I Ave j �Iv 'Os/ 14' tea.IQ `74 2-/ Ir 2 Avgf/. 5, 4r 7 Y(I 31 �4 `:y� ,lam 2_ . _ - Avg ; ... -^ > L 'j - .� '' �' - ,� - = r f t; L� _ 0 r . C'• C�--��;�----- -.. _. _ . __,_ .._.. - - —_ 7- ,Avg 2 -c,� 5: Yl� Jr 7 -FEED ZLU -SLUDGE`f'200,000,- DRY-TONS- PROCESSED SOLIM X. r L GALLONS FEED' Biosolids Forms 7/2/2014 - pH / `CORRECTED- pH of, Final Product ::. 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[ CD J -6 A2I V, 35' I Y? ,2Li,. 2 y o 7V-Z 12.. Z37 T-7 3 e- 6 GC. 2 Additional Comments Bipsiofids'Forms 9/2 4-/20'13-- V c fNihi of I annir Rinanlitic I nn ui PERCENT SOLIDS VOLUME OF FEED SLUDGE '_Z'u) 00) (L COMMENTS Feed.--- Sludge Belt Press Final Produ'ct Start Reading End R6aclin' 1 9 Total Gallons i6 2 Avd S tl'� Z_ -4v 8' " Av9 , --Y S--7 35 2U, 5-)4 J '76 2 v 8v A 2 Lviij 17. 2 6 Avd�, f/I 2 2 Ayd 7 7) V, ls� vt Avc-y J, 2). Cr _DRYTONS PROCESSED-= % SOLIDS FEED SLUDGE 8.34 X TOTAL GALLONS FEED SLUDGE 200,000 Biosolids Forms 9/24/2013 } City of Lenoir Biosolids Log pH.I-PO RRECTED pH ;.of Final Product.. =-3 Initial PH . 2 Hour PH 24 Hour PH CL CL C �U C :; «.. , .-o ea :e -a , N _ .:: _ •G to N ~' y 0.N 7 = ij V C ++ N C' : l0 ''' R. �Qo o Q.2 O �U tea. 1QU �U� O = �U °�� �O 'U o:v ,8 :ate U a�i� oa _ I— o co _ I-- a Q U O c� iT c� K' -� �'! Y. saw/l�i - / dryC -- - %f7`-.( "'.S✓ ° O�t.J a,f^ F )q L I G �� `o All �r1 J L -, 6 3. J � /-• /� (�• ,[ �•J i� L, 2-3 ?i . 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Additional Comments - - --- -- -- - � N. .xurwwn—vv.x w.e.wunw..ww. vwwwwx.x+w.onxnn.xnwx .'rwxoi .wrxnn.xww�x.x.. w.... l.�.w.xxwnn r��x.w..sxw��w.nxv+.�xxw.w.xs.raxx+xxswwwirwr�xx..v�vr�..x�m�m.r .v.r..srn vn�vnvvw. v xxrwnwm� rwvxwr.� ! x...wwrn�wrvn� wxv.xx..xxw�xwv.wv..rwin vvwxx...vn k ..w. ) .. i, w.v'v"vx""° "'."'x'"'w`.^n _ � ^• _ � � F, . .�nx. -. .v..r..�.x,.x.�,n.�rxv�nx�...ow.wwvw...�xvx�.�v.xwnwr..w.�.uwax�.wwn _ www .y.. vvx..wxv • .xun i �vxoxi ew.x�r.. x�vw ; nv.vnr..w.uv. i _ _ .xxwnwxvww..wwvx.w�ww. _ _ _ _. _ _. v..x.r.rx�uxwur�.x�.ry - - _-�.�+rnvn.` xw.rw.�swvm.n`na.vxw.vvxxxrxx.vwvr.xxaw xwvx , h� w ieexu.vnvrv�r�vnr+.vwx.v�+w.xr.wv�nx®v�nnwrnru i ; �wxr.r.rn nuvwx�nw � vrwnwv. - - vu� - • • x � mv� S ^ s _ rn+wv�.rxv.x� _ w. � nv�aw.xxwrwxww�w nwrwxw..w ..w..n..wu.wnwvx. ( ' b ` - Biosdids Forms 9/24/2013 Ln f,62,4," 0%f I g%w%0%I"r 1 ~4 w W 7 PERCENT SOLOS t y Feed�,-, Belt 'Final Sludge. -J, Presw Product. 'A 7 ,7 7 VOLUME OF FEED SLUDGE 4 Start = End Total Otis Reading R4adihd: Gall' AU 0 CO) D 0ix .-COMMENTS - L'--V M6 2°z 2 Av6-- 1 •- �'��' �'_.�r.� ��'� � �^fir � � � ��1': �1 J. : 777 � � - - -- IdA; Av r. Avg 23 z 15�� �2 A�d 1, 9 Irj i R�15_aa:4; 2 77 t voc> - DRY TONS -PROCESSED -= P/b- SOLIDS- FEED-SLUDGEX 834, X-TOTAL-GALCONS FEED -SLUDGE-1-200,000- 7 i piosolids Forms 9/24/2013 City of Lenoir Biosolids Lg PWI'CORRECTED. PH of final Product, Initial PH 2 Hour pH 24 Hour PH o _ O NC Q Hv CO D �� N ¢U..VN`s�v.. V N D y Qv. 0.2 U.� I 0 �. 6M. L2 H,.v C N = �� � y ,;QU O C 0' � Ucn A. -'3v! �� ..�..G_,_3 �6= - `` �, y .: �f ` ' ! - f A- 3i-A 03 i z.z 1 L G= A ,:z / -ems p,'i 7 e- �'i 9,L ^'C` CID LIU47 -c,Y' c p A 3,, cV. Jb `� 6 i "1 'l T.�a pZ "{,�� �*Y • •: r.T'+n 1 ('j -i V3 Cis iG7 4 © s A✓ •i a1 Additional Comments .e.,....w....�.,.�.......wn.,w�........,�............,.�......,... ; .r_� �..n i �.�.—......�2.�.,. .�..�...�.�.n.�..�.�.�...r.....�.r...e...w.�...�..� t ` �„�....—...vo �; .�.w..k, , Biosdidsf F&ms'9124/2013 t; ,City -::of ,Lenoir. B osol ids- TTem peratu r-e .Log FOR,CALENDAR YEAR •_LP-NDEk:- PASTEURIZATION r= ,_ NOW MIM FM MINIM. M- 0111110IME 01110 0111 � J _ 6s+ .. r - — _ -- -- - --•- r•...,.....,- �.0wu1Un11111= aIIu IIW2L III ulermoolenaer ano tnen.are mcnarged .into the pasteurization vessel: the pasteurization vessel belt'travels at a slow -speed, taking greater than 30 minutes for the product to travel the length. of the belt,.where the temperature of the product is maintained at or above 1613* F. '' ` ' -, ' -" - ' Temperature Log City of---,Lelnoir I DISCHARGE TEMPERATURE (00) TEMPERATURE (OF) WRIT MJ� - , , ■r . _ 4 �AW I ♦ � A0 s�:Li�..• r � MW I rm.. ougas-,rum oea press are mmea wan gwcKume anal.heat in thermoblender and then are discharged into the pasteurization vessel: Thepasteurization vessel belt travels at a slow speed, taking greater than 36 `minutes for_ the. product to travel the length of the belt, where the temperature of the.product is maintained at or above 158* F. Temperature Log " - CiV pf Lonoir,,,. Biosolids, TemperatureLog FOR. -CALENDAR YEAR D, I DATE JIME THERMOBLENDER DISCHARGE' TEMPERATURE (OF) PASTEURIZATION VESSEL -TEMPERATURE (OF) T 1NLE 'DASCHARGE 3_1 q -2 rN 4 St, 7 C1 AIN3 73 PM - t 7 a—fo;i5 7 I v 20- -3 Apio s'- 5 3 `17 6 A V 1 71m: 6j '0 zy, Q—.-, 7 g- I -. 7 e, -2- 3-o f6 1R.& I J, 'G t 3pot 7777777X7# J. 1MV 1 ''00105 xrom, oell press are mmea with qu!cktime and heat in thermoblender and, then are discharged • into the Past6urikation vessel. -'-The pasteurization vessel belt travels a t,a.s low speed, taking greater than 30 minutes for the product to travel the fen th g,__ofthe belt, where the temperature of the product is maintained at or above 168* F. Temperature Log r City,of Lenoir , Siosolids Temperature Log FOR CALENDAR YEAR'. -- -- - -- • ►-•, - slo-vu mu, yumcrtumu dnu neat in inermoblender and then are discharged into the pasteurization. vessel. The _pasteurization vessel belt travels at a slow taking greater than 30 minutes for the product to travel the length ,of.the belt where the,temperature, of the product is. maintained at or above 1 SO- F. Temperature Log. ' City &Lenoir iosolids Temperature Log _ :..... - .FOR CALENDAR YEAR-.. J DATE' :.. THERMOBLENDE_R PASTEURIZATION VESSEL TIME ' . . DISCHARGE : . _ _- -' TEMPERATURE (°F) TEMPERATURE (OF) INLET . : DISCHARGE f �� �L5-� `1( pp CIO 91 HATE: Solids from. belt press are'moced wifti quickliriie and heat in.,fhermoblender-and-t ` "- into-the-pasteurization=vessel. than en are dis� ed "The'pasteurization vessel belt travels at a slow speed; taking gaeater 30 minutes for the product to travel the length of the belt, where the temperature of th is maintained at or above 168- F. e product Temperature Log . City of Lenoir:. , Biosolids Temperature- Log FOR CALENDAR YEAR C' DATE .TIME THERMOBLENDER '. DISCHARGE- ' TEMPERATURE (°F) - PASTEURIZATION VESSEL ' • - 'TEMPERATURE (°F) - INLET DISCHARGE Pa rnvc _ SL n a 3 0. S / _ =7 Ph _ -� .: , - .5 . , - 2 �o.._ Si ��� �' 6..- :- - t - L .. -.6.6 _ L NOTE:.- Solids from belt press are mixed with quicklime and heat in thermoblender and then are discharged = .,into the pasteurization vessel. The pasteurization vessel belt-travels.at.a•slow.speed, taking greater than. 30 minutes for the product to travel the length of the belt, where the -temperature. of the product is maintained at or above 158 F. Temperature Log City: of,Lehoir.-.L",j. Biosol-ids, Temperature Log FOR CALENDAR -YEAR DATE THERMOBLENDER" .DISCHARGE , TEMPERATURE (OF) `PAST EURIZATION VESSEL .'-TEMPERATURE(* INLET DISCHARGE _Z 911 2r .37 3 Pin �:2- -3 ; 5 T77 41Z' Oj _TZ'r 16C 7-9, L/ -A Zia:= Cf-cf /jq lz- .2 // 31PA L, tv '47 6_3 YP )I 7:!4 IJ -1 T- J k_1A 3- WiLl :3Q. Ail I Sri 7 12 I T:Z_ I Lan t t4—� -7 91 --- 14 L G CI - I, T I - 7 T-7 -7 -17 3 P/ 4 ------ -�LZ r4Vi1C:",5o11as.TrOm Deitpress; are mixed -with quicklime and h6at,inthem ioblend6earid'th'e'nare discharged Into the,pasteuiizatioh,ve%g-46sse a'slow speed, 'tal'dng greater igl.l'Thepasteti6iition I belt trav6l,,at than 30 minutes for the product to travel the length of the.bell; where the t6mperaiture'of the product is maintained at or above 168* F. 1. '. . - -1 ' I - Temperature Log GPI \'k City. of Lenoir , ?P Biosolids Temperature -Log- •� �t FOR CALENDAR YEAR 20J ° -ad � THERMOBLENDER = PASTEURIZATION VESSEL DATE TIME -DISCHARGE TEMPERATURE (OF) TEMPERATURE (OF) INLET DISCHARGE 9PL�' pIn 1. u17 - . .3. PUY 3 -D /9 PM.. �° 0- m 5 7 E - O •- , -�;7 , -► • e. 2. 3 ply III 4C •.� 1 " p _ 1 ="6— jV 141i. � , 7 1►IATC. pi� c.rr_ r__:Y _.a _ - .. •-- • - ��,. V11;,00 01=1111,AcU wnn yuiurcume anagneat.in tnermoblender and'then are discharged into the pasteurization vessel., The pasteurization vessel belt travels at a slow speed, -taking greater than 30 minutes for the- product .to travel the length of -the belt, where ,the temperatureof the product is maintained at or above I680' F. Temperature Log 41 t-'BIOSOLIDS RECIPIENTS 2014 ANNUAL "WET" # "DRY" TOTAL • 5 e , TONS TONS DRY, DATE NAME, FIELD OR PROPERTY ID # LOADS APPLIED. APPLIED TONS 1/1/14 Munday, Jim Pasture 1 7.43 3.17261 1 /1 /14 - V1/ilson Dykes Pasture ' 4 ....: " - ". ' 29.72 12.69044 - 1/8/14 ' Wilson ....Dykes Pasture :. _.. __ :._.:`._ . ' = 2' ...._ ..: _..:.14-.86 ---- - 6.34522 ' 1/15/14 Spears- Roger Hayfield 22.29 : „ 9.51,783 1/15/14 Fish House Com field ;.- - - „ _ :;.. _2- 14.86 6.34522 1/16/14 Miller. Boyd` Pasture 4 29.72 12.69044 1/16/14 Fish House Corn field _'I 7.43 3.17261' 1/20/14 Wilson Dykes Pasture 2 14.86 �6.34522 1 /20/14 ' ' Tower Drive 1 _ 7.43_ 3.17261, 1/21/14 Fish'H.ouse Corn field 2 14:8.6 6,34522 1/27/14 Griffin ;' Ben 3 22.29 9.51.,7.83 1/28/15 Fish House Com field 1 , 7.43'; 3.17261' JANUARY TOTALS =_> 26 193.18 82.48786 82:487.9 Scoops or. a o Loads (Wet) (Dry) y 2/6/14 Land.. Joel ,,' Hauled by recipient * 2 2.0000 .,._0.854. 2/8/14 Kent! Daniel Hauled by recipient * ? 2 4.0000 1.708 & E, 2/10/14 Lovins David Hauled by recipient * 8 16.0000 6.832.. -0.854 m o'E;3 6/10/14 Estes Gary ' Hauled by recipient * 1 2.0000 _' FEBRUARY TOTALS =_> NIA 24 10.2480 92.7359 3/4/14 Wagner `' ` Hayfield ; 3 22.29 "9:51783 3/5/14 Spears- -Floyd Hayfield - - ..3.. ' `22.29 9.51783 3/5/14 Ford Hayfield 1 7.43 3.17261 3/5/14 Brown D.A..(.:, Hayfield :. ;--2---. 14:86.. 6:34522 3/6/14 Brown D.A.. ;, Hayfield 4 29.72 12.69044 3/10/14 Bean Nathan Hayfield 2'; 14.86 6.34522 "• A 3/27/14 Spears Floyd ' - Hayfield -. -' <- 2 7. u- 14.86 " 6.34522 MARCH TOTALS =_> 17 126.31 53.93437 146.6702 4/1/14 Bean::. Nathan Pasture .3 22.29` 9251783 4/1114 Watson Joe Tree Farm = ' :1, 7.4-3 3 1-7261 ' 4/2/14 Mann , . Tommy. _ .Hayfield , _ , _ ... _ .-, _ . . ' 4 _ ... _. - .29.72' '-_ : 12._69044-. - . 4/2/14 . Alred Brett, Hayfield . 2' 14.86 .._ 6.34522_ `4/4114 Ford C Hayfield 2 14.86 " 6.34522 4/10/14 Barnhardt Harold Pasture 2 14.86 6.34522 4/11/14 Clark Brian Pasture T, 7.43 3.17261 4/11/14 Cloer Barry Pasture 2 14.86 6.34522 4/14/14 Cloer Barry Pasture 3 22.29 9.51783 4/14/14 Alred Brett Pasture - Smokey Creek Road 1 7.43 3.17261 4/14/14 Munda_ y Jim Pasture - JM Gray Road 1 7.43 3.17261 4/18/14 Cloer Barry Pasture 3 22.29 9.51783 4/21/14 Cloer Barry Hayfield 9 7.43 3.17261 4/22/14 Cloer Barry Hayfield 5 37.15 15.86305 = ANNUAL i #.'WET' # "DRY" TOTAL TONS TONS DRY - DATE` NAME FIELD OR PROPERTY ID # LOADS APPLIED APPLIED TONS 4/23/14 Bean Nathan Pasture 1 7.43 3.17261 4/24/14 Taylor-, Charles cornfield 4 29.72 12.69044 4/25114 Fish House '"cornfield 5 37.15" 15.86305 4/28/14 Greene Cornfield 3 22.29, 9.51783 4/28/14 Fish House Cornfield '`' 2 14.86 6.34522 APRIL TOTALS =_> 46 341.78 146.9401 292.6103 5/2/14 Fish' House Cornfield .3 22.29 9.51783 5/5/14 Pasture - Pine Mountain Road '' .6 44.58 �I 9.03566 5/6/14 ,Griffin •• Ben,'4. New ground '4 29.72 12.69044 5/8/14 Griffin Ben New ground 1 7.43 3.17261 5/8114 Cardwell Ronnie Pasture 3, 22.29,- 9.5,1783 5/9114 -Cannon; Kenny Field 3 22.29 9.51783 5127/14 Chuck ' Cail'oway Pasture 3 22.29 9.5.1783 5/27/14 Hendrix Jack 3 22.29 9.61783 5/28/14 Cannon Kenny 2 14.86 6.34522, ' 5/28/14 Chuck, Calloway Pasture :14 29.72 :12.,69044 5/28/14 ' Prestwood Kim 2", .. 14.86 6.34522 :Cardwell Ronnie --"5 37-.15 - 15.86305 - MAY: TOTALS =_> 39 289.77 123.7318 416.3421 6/5%14 Prestwood Kim ::. :�' 2' 14:86' 4.88894 6/5/14 Nursary Field - Little John's Church, Road.,:. 1 . 7:43 '° 2.44447 6/9/14 Wilson Dykes; _ 1:, 7.43'-. 2.44447 6/9114 Calloway Chuck 6 44.58 , 14.66682 6/9114 -- Cardwell Ronnie- - Hayfield _.....: _ . _ 1 -- .- - - 7:43 ' 2.4,W7 6/23/14 Bean, Nathan Hayfield 4 ' ,' . ! ,, '.- ;29:72 9.77788 6/24/14 Bean "" Nathan-_ Hayfield __ ' 4 29.72 9.77788 6/28/14 Cannon Kenny 14.86 4.88894 = JUNE TOTALS ==> 21, 156.03_, 51* 3387 467.6760 7/29/14 Cardwell Ronnie Pasture -" 2.; 14.86 4.88894"' " s 7/30/14 Cardwell Ronnie Pasture 5 37.15 12.22235 7131 /14 Parker ,: Junior Pasture - Clarks Chapel Road 4'' 29.72 `' 9.77788 5 . ': JULY TOTALS =_> 11 81.73 26,88917 494.5651 .. 8/8/14 Dennie . Jerry ,, Hayfield - Cajah Mountain Road 3:= 22.29, ' 7.33341'. 8/23/14 Hendrick Jack Hayfield 2 r 14.86:. 4.88894, 8/27/14 Hennissee Alan Hayfield ,,3, ; 22.29-: 7.33341:; AUGUST TOTALS ==> :. - -8:; 59M -, 19.56576 514.1209 ANNUAL TOTALS ==> 168 930.46' 514.1906 r , (dry tons)' ' 466.4002 „ (dmt)'4,.. BIOSOLIDS HAULED BY RECIPIENT NAME DATE NUMBER OF LOADER SCOOPS TONS OF PRODUCT CHECK IF INTENDED USE ANALYSIS RECEIVED INSTRUCTIONS RECEIVED example - John.Firmer:. -:.. 1/1:.1r1091.:. - . l0:. tons/scoop)=_ :� pastar�s land y . � '�' - y'' ice- �'�e '-::1.,• till .Y, � C, M4 1 JU I Acid, NOTE: PLEASE SIGN IN ABOVE WHEN HAULING BIOSOLIDS TONS ! SCOOP (Johq Denoc) f T ea vI sca"o C2aWeoieje.,,, /vim ) Blue Ridge Labs A® Box 2940 .Lenoir, NC 28645 828-728-0149 blueridgelabsienoir ftmail:G ti o ClieRit : City of Lenoir P. O. Box 958 Lcnoir, NC 28645 Attention: Mr. M. Wall Oate Received: 24-Jun-14 Report Date: 29-Jul-14 Sample bate: 24-Jun-14 811E #: l3KL-2014.-0409 ^ L5b Sample ID: LSID-2014-01873 Client Sample IIU: 062414-8ioSolids 1 Parameter Result MQL Analysis Az.L ! s Unit Method '' Time Da c Ana Fecal Coliform # 5 MPN/KG Fecal by Multi 6/25/ :, 14 Wh{ q. Reported By: 5. J. Johnson, D.R. Wessinger * Concentrations are below Minimuin Quantification Limit except where muted. NC.Laboratory'Certificate No. 276 Page 1' of I I Blue ,Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmaii.C. I ,� Client: City of Lenoir P. 0.8ox 958 Lenoir. NC 28645 Attention: Mr. M. Wall Date Received: 24-Jun-14 lieport Date; 29-Jul-14 Sample Date: 24-Jun-14 tZL BRL-2014-0409 Lab Sample'ID; LSID-20.14-01874 Client Sample ID: 062414-SioSolids 2 Parameter Result Result MQL Unit Method Time Ax <, �9is IDS :i Ana Fecal Colifonn - 5 MPNIKG Fecal by Multi 6/251 '- 14 w+ri Reported 1By- S ti S. ,l. Coneentrations arc below MI NC Labs on, P.R. Wessinger m Quantification UkAxit rxcept where noted. ^y Certificate No. 27.5 ,2of 11 I Blue Ridge .Labs PO ,box 2940 Lenoir, NC 28645 828-728-0149 blueridgelab$Ienoir@gmaii.cc,i'i - -- - - City --of Lenoir --- Client; ---City-of P. 0. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 24-Jun-14 Report pate: 29-J u I-14 Sample Date: 24-Jun-14 ORL #: 13RL-2014-0409 Lab Sample alb: LSID-2014-01875 Client Sample ID: 062414-Bio5olids 3 ' • - ,A,,ualysis. An .i. �-�;is Parameter Result MQL Unit Metb®d Time-- ' Do it Anal V Fecal Coliform 6 MPN/KG Fecal by Multi _ 6/25/ ! .4 Wt tJ -,. ;1V I� Reported By: S. J. ason, O.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Cer-tifteate No. 275 , Page 3 of I 1 Blue. Ridge. Labs. --PO Box 2940 Lenoir, NC 28645 828-72"149 blueridgelabslenoir®gmail.cc i- Client : City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 24-Jun-14 14port Date: 29-Jul-14 Sample pale: 24-Jun-14 BRL #: BRL-2014-0409 )I'ab Sample ID:, LSTD-2014-01876 Client Sample ID: 062414-Bio$olids 41, Analysis An 1 1 iis- Parameter Result MQL Unit Method Time Da ii Anai sl Fecal Coliform 5 MPN/K(.i Fecal by Multi 6/25/ 1 94 WtAt, Reported By: s . S. hnson,l�.1Z. Wessinger Concentrations arc below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 4 of 11 Blue Ridge Labs PO ,fox 2940 Lenoir, XC 28645 828-728-0149 b� " •d b " : . uer► �e a s enalr@gmail.cc � Client: - --- City of Lenoir _ - P. 0. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall - Date Received: 24-Jun-14 Report Date: 29-Jul-14 Sample Date: 24-Jun-14 BRL BRL-2014-0409 Lab Sample Ids: LSID-2014-01877 Client Sample IU: 062414-BioSolids 5 " Analysis An, d Y;•ls Parameter Result MQL Unit Method Time Da -r "'',Anal si Fecal Coliform 6 MPN/KG Fecal by Multi 6/25t '-8 WK t7 Reported By: � .....r S. I mson,' D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certifie$te No. 275 Pogo 5 of I I Blue ,ridge Labs PO.Rox 2940 Zenoir, ArC 28645 828-728-0149 blueridge,labslenoir@gmail.cc r 1 Client : City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention; Mr. M. Wall Date Received: 24-Jun-14 Report Date; 29-Jul-14 Sample Date: 24-Jun-14 IBRL 4. BRL-2014-0409 Lab Sample ID: LS1D-2014-01878 Client Sample lib: 062414-13ioSolids 6 Parameter Result MQL Unit Method Fecal Coliform 6 MPN/KG Fecal by Multi Reported By: . S. ohnson, D-R. Wessinger * Concentrations are below minimum Qualitification Limit except where noted. NC (Laboratory Certificate No. 275 Page 6 of I 1 Analysis A,n 1 pis Time Da a 612511 14 Blue Ridge Labs PO Box 2940 Lenoir, IVC 28645 828-728-0149 Client : City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention; Mr. M. Wall Date Received: 24-Jun-14 Report )date: 29-Jul-14 Sample Date: 24-Jun-14 SRI, a: BRL-2014-0409 Lab Sample ID. LSID-2014-01879 Client Sample ID: 062414-BioSolids 7 Parameter Result )SQL Fecal Coliform 5 Deported By- blueridgelabsienoirftmail.m r- Analysis An t v Os Unit McMod Time Da -I MPNIKQ Fecal by Multi 6/251 '+ • 14 .S. ohnson, D.R. Wessinger W Concentrations are below Minimum Quantiiacation Limit except where noted. NC Laboratory Ceirtificate No. 275 Page 7 of ' l 1 F .flue Ridge Lab, PO .Box 2940 ,Lenoir, NC 28645 828-728-0149 Client : City of Lenoir P. O. Box 958 Lenoir, NC 28645 Atten iva: Mr. M. Wall Date Deceived: 24-Jun-14 Report Date: 29-Jul-14 Sample Date: 24-Jun-14 ISRL M BRL-2014-0409 ;I,ab Sample )()lD: LSID-2014-01880 Client Sample AD-- 062414-BioSolids blueridgelabslenoirOgmaiLe, --i:l Parameter Result MQL Unit Method Analysis Time An i I, -As Do -; Anal Total Phosphorus 18377 188 dry mg/kg EP,A. 200.7 11:21 7/29/ .1 .4 KCJ Ag by ICP-AES 26.6 2.9 dry mg/kg SW-846-6010 11:21 7/29/ 1 .4 KCJ Al by ICP-ABS 19645 46.8 dry mg/kg SW-846-6010 11:21 7/29/ 1 .4 KCJ Ca by ICP-ABS 29678 234 dry mg/kg SW-846-6010 11:21 7/r9/ 1 .4 KCJ Cd by ICP-AES + 0.1172 dry mg/kg SW-846-6010 11:21 7/29/ (' 4 KCJ Cr by 1CP-AES 19.4 0.586 dry mg/kg SW-846-6010 11:21 7/29/ ('4 KCJ Cu by ICP-AES 266 0.586 dry mglkg SW-846-6010 11:21 7/29/ t : 4 KCJ K by IC.P-AE.S 1729 46.8 dry mg/kg SW-846-6010 11:21 7/29/ (' 4 KCJ Mg by ICP-AES 9041 46.8 dry mg/kg SW-846-6010 11:21 7/29t ' ' I KCJ Mo by ICP-AES * 0.586 dry mg/kg SW-846-6010 11:21 7/294 ; ' I KCJ Na by ICP-AES 72)4 14.7 dry mg/kg SW-846-6010 11:21 7/294 r : 4 KCJ Ni by ICP-AES 47.7 0.586 dry mg/kg SW-846-6010 11:21 7/29t.. r : I KCJ ,7,o by ICP-AES 382 0.586 dry mg/kg SW-846-6010 11:21 7/29t C•I KCJ l•1g by Cold Vapor AAS 0.0613 0.0297 dry mg/kg SW-846-7471 )5:12 7/21/: ( '-I KCJ Reported By: -' 5. ohnson�, D.R. Wessinger Concentrations are beluw Minimum Quantification Llndt. except where noted. NC Laboratory Certificatia No. 275 Pagc 8 of I 1 Blue Ridge Labs PO .Box 2940 Lenoir, .NC 28645 828-728-0149 blueridgelabslenoir�gmail.c< i `' Gi?ient City of Lenoir-- F. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall - Date Received; 24-Jun-14 Report Date: 29-Jul-14 Sample Date: 24-Jun-14 1BRfL �i: BRL-2014-0409 Liib Sample ID: L.SID-2014-01881 Client Sample ID; 062414-BioSolids Analysis : An L. Parameter Result MQL Unit Melhod Times pa ,E Ana Nitrate + Nitrite Nitrogen (N2+ 32.9 18.3 dryrng/kg • SM19 45U0-N 16:12 7/22l :1 !4 KCJ Total Kjelda111 Nitrogen (TKN), , 28495 272 dry mg/kg SM19 41.UU-N 9:03 7/231 J .4 , ; KCJ Reported By: S. oltnson, D.R;- Wessinger * Concentrations are below Minimum -Quantification Limit except where noted. NC"1Laboratory Certificate No. 275 ' Page 9 of fi Blue .Ridge .Labs PO Box 2040 Lenoir, NC 28545 828-728-0149 Client - City of Lenoir P. 0. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 24-.Iun-14 Report Date; 29-Jul-14 Sample Date; 24-Jun-14 OR BRL-2014-0409 Lab Sample ID; LSID-2014-01882 Client Sample 111): 062414-SioSolids blueridgeiabslenoir@gmail.ci ,1: Pg,rameter Analysis Ay. it IMS Result MQt, Unit Melbod 'Lime Da :1 Ana Solids 32.9 0.1 % %Solid.F 12:15 61261 ",14 KCJ PH 11.9 0.1 SIJ SW-846.904U 12:32 61261-. 14 ICJ Reported By: S. J. ohnsoa, U.R. Wessinger K Concentrations are below Minimum Quantification ,Limit except wiaea-e noted. NC Laboratory Certificate No. 275 Page 10 of I I 1 I Blue Ridge Labs ,PO Box 2940 .Lenoir, NC 28645 828-728-0149 _.blueridgelabslenoir@grnalLa r, Client: Giry ;of Lenoir P. O_' lox 958. I 'Lenoir, NC 28645 A.ttetition: Mr-M.-Wall ' Y,Date Received: 24-Jun-'14 -Report Date; '29-Jui-14 Sample Date: 24-Jun-14 BRI, 13RI.-2014-0409 _. a..ab S$ mple JD: LSID-2U14-01883 Client Sample J76: 662414-BioSolids ,' Analysis .`An i -rnis aPameter• Result MQL Unit Method- liAne .Yea a Anal st Aninian;a Nitrogem 1155 -295 dry mg%lcg Ammonia 13.-06 9i22! t 3 ICJ Reported -By- _.. S. J. nson; D.R. Wessinger *,'C®ncchtratioos are Mew Minimums Qttantificatioa JL(iojt except where noted. NC'Laboretory Certificate No. 275, ; Page 1•l of 11, NP DS Reporting _.. Z tbundvwater Rep�,rt` B-1ue Ridge Labs, Inc. P.O. Box 2040 - Lenoir, NC 28643 Telepkme (829) 728.0149 Fax (328) ?Z8-®131 Chain of Custody - Sanitary Landfill }Maaardous Waste -Industrial or QC *fort State Reporting_ USTMust Fund Reporting Bill •!b: Pr*ct Marne: IceI'Ment: Y N -- ;ime& ricia Pseld Resid Preservatives lab Check Sample 1D Sample Dale 'rune 'Temp HR:CAM Field sulfate ChlorE14611d Sulfide heSMf I Fieldina00A pH Redd Tent SType P ampler Analyse Regttestestcc Check Removed Y N Y N Y [YN Chlor eC Initials 062 Y14')N- r 1� (-24 102,q 1 P or A do�9A, It 17 —1 �• r' telinquis BW Date• Tune: pan sebmlatuograampler,stiad sweep lhe(iuvrnoes me duc ar Ncrirwcs�osfc ea v I� relin rskln rj �n ggys; sils ate due 20 days lirltpworra itrv�ice dYc. A finetrce eiar�e of 1.5"�Lper raorWr wilt be ieap4utd olr all u�xccaarfs• R� >! seraple5 to 8iue t2id�r t.ais {�til.1, htyerrrut$arite4 Aitt.eo pafenatiax6y tt� uanlyxfs ifldrutad abo+t Baertd 1 unsWe eppodec! R't to faro r r , t rc re � is Qiedtea9� emgpmesi5n•Yfy Go rcquwt on aria form � fa r3' prlrPo�s @1t1. taancri pu�an1Qltlgt arty r¢galeroiy authority will ama� any wotdr eppromristtttsis. �K:i1fE"t�tC:aniGcdt.a6H27i r ,; �° � �aceArialytical )` w 1w.pacdabs.com ANALYTICAL RESULTS Project Lenoir 6116 Pace Project No.: 92206836 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: 062414BIOSOLIDS Lab ID: 92206836001 Collected: 06124/1415:00 Received: 06/2511416:20 Matrix: Water 'Parameters Results Units' Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA3050. Arsenic , ND mglkg 1.0 1 0710311411:25 07/08/14 09:29 7440-38-2 Lead 5.7 mglkg 1.0 1 0710311411:25 07/08/14 09:29 7439-92-1 Selenium ND mg/kg 1.6 1 07/03/141125 07/08/14 09:29 7782-49-2 Date: 07/11/2014 07:07 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc - Page 4 of 13 Pace Analytical Services, Inc. x °acmnalytical o www.pacelabs.com SAMPLE ANALYTE COUNT Project: Lenoir 6116 Pace Project No.: 92206836 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 i Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92206836001 062414BIOSOUDS EPA6010 TAP 3 PASI-0 92206836002 061614M-GINF EPA 200.8 DRS 3 PASI-0 92206836003 061714M-GEFF EPA 200.8 DRS 3 PASI-0 92206836004 061714M-LEFF EPA 200.8 DRS 1 PASI-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 13 CHAIN-OF-COSTODY / Analytical Request Document The Chalh•oFCustody is a LEGAL DOCUMENT. All relevant fields must be comploted accurately' VaceAnalyteal* weAa.peoelaGs,aelo Soctlon C Section A Section B Invoice Information: t Infoation Required Prolect Information' Attention Required Orienrm tEGULATORY AGEtdCY r- ' NPDES I— GROUND Wi UST rt RCRA Site Location 1nalvS1S Filtered (YIN) sectionD Matrixcodoa C(SLLECTED RCtldlredGhrtlnfarmation Fyt17R14 r CAPE, 9 O. Ddnkino Water DW' Water vJT COHPWYE m-1poSITE ' Wealewotor WW START END'GRAB J, Product Solysolid SL $i _ v SAMPLE ID vnpe WP a (A•Z 0•9 1:) Air AR O � H Sample IDs MUST BE UNIQUE Ts Tlsaua Ot o Other a u w 2 a ) DATE S(ME DATE TIME � O N Il co • r 0 N r d) tm o: 1 of f 1564563 -J j" OTHER � C o r � to U' m O `m :ko m i SAMPLE CONPITIONS DATE TIME ACCEPTED By AFFILIATION DATE TIME AODITIONALCOMMENTS RELINOUISNEO Y I AFFILIATION C c4j, ALL eV d �-- SAMPLER NAME AND SIGNATIWRE t. � n 'bi �t '� �'. fl �• PRINT Name of SAMPLER: CIFOO f Clf�9�a4h.r�L , DATEsignaa/�F� SIGNATURE of SAMPLER *•. (MMIDDlYY): C o " i` r F•Al) .Q 020rev.07, 15•May 2007 . .......... a,rveairio Paeo's NET 20 day payment isrms and'n9rz=hl9lo Into chargoF bl 7.fiYn Der month lot'Bny fnVolrss not'Said within 30 daya. . Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 16-Apr-14 Report Date: 13-May-14 Sample Date: 16-Apr-14 BRL #: BRL-2014-0224 Lab Sample ID: LSID-2014-01155 Client Sample ID: 041614-Biosolids 1 Parameter Result MQL� Fecal Coliforrn * 5 blueridgelabslenoir@gmaii.com : Analysis Analysis Unit Method Time Date , :Anal ' yst MPN/KG Fecal by Multi 4/17/2014 . WtrQlty Reported By: S., ohnson, D.R. Wessinger Concentrations. are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 2 of 13 ;�i Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-'0149' blueridgelabsienoir@gmaii.com. Client: City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 16-Apr-14 Report Date: 13-May-14 Sample Date: 16-Apr-14 BRL #: BRL-2014-0224 Lab Sample ID: LSID-2014-01156 Client Sample ID: 041614-Biosolids 2 Analysis Analysis Parameter Result MQL. Unit Method Time Date Analyst Fecal Coliforni * 5 MPN/KG Fecal by Multi 4/17/2014 WtrQlty Reported By: _ C,20r— ohnson, D.R. Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 3 of 13 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149- blueridgelabslenoir@gmail.com , Client : City of Lenoir P. O. Box 958 :. . Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 16-Apr-14 Report Date: 13-May-14 Sample Date: 16-Apr-14 BRL #: BRL-2014-0224 Lab Sample ID: LSID-2014-01157 Client Sample ID: 041614-Biosolids 3 Analysis Analysis Parameter Result- MQL., . Unit Method Time Date Analyst Fecal Colifonn * 5' MPN/KG Fecal by Multi 4/17/20141 ,. WtrQlty Reported By:— S. ohnson, D.R. Wessinger x Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 4 of 13 � , Y Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 ' ' Client: City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 16-Apr-14 Report Date: 13-May-14 Sample Date: 16-Apr-14 BRL #• BRL 2014 0224 blueridgelabslenoir@gmail.com Lab Sample ID: LSID-2014-01158 Client Sample ID: 041614-Biosolids 4 Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Fecal Coliform -4 MPN/KG Fecal by Multi 4/17/2014 WtrQlty Reported By: S ohnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limitexcept where noted. NC Laboratory Certificate No. 275 Page 5. of 13 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-,728-0149 , ..;. blueridgelabslenoir@gmail.com Client: City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall ; Date Received: 16-Apr-14 Report Date: 13-May-14 Sample Date: 16-Apr-14 BRL #: BRL-2014-0224 Lab Sample ID: LSID-2014-01159 Client Sample ID: 041614-Biosolids 5 Analysis Analysis Parameter Result MQL: Unit Method Time Date _ Analyst _ Fecal Colifonn _ _ 5 MPN/KG Fecal by Multi 4/17/2014 WtrQlty Reported By: S. I non, D.R. Wessinger x Concentrations are below, Minimum Quantification Limit except where noted. NC Laboratory. Certificate.No. 275 Page 6 of 13 Blue Midge Labs PO Box 2940 Lenoir, NC 28645 828-728=0.149- - ' Client : City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 16-Apr-14 Report Date: 13-May-14 Sample Date: 16-Apr-14 BRL #: BRL-2014-0224 Lab Sample ID: LSID-2014-01160 Client Sample ID: 041614-Biosolids 6 Parameter Result MQL Fecal Colifonn * 5 blueridgelabslenoir@gmail.com Unit _ Method MPN/KG Fecal by Multi Analysis Analysis Time Date Analyst 4/17/2014 WtrQlty Reported By:`�" S. I nson, D.R. Wessinger *Concentration s'a're below Minimum Quantification Limit'except where noted. NC Laboratory Certificate No. 275 Page 7 of 13 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149- " blueridgelabslenoir@gmail.com Client : City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 16-Apr-14 Report Date: 13-May-14 Sample Date: 16-Apr-14 BRL #: BRL-2014-0224 Lab Sample ID: LSIO-2014-61161 Client Sample ID: 041614-Biosolids 7 Analysis Analysis Parameter,,.,, . Result MQL Unit Method Time Date Analyst Fecal Coliform MPN/KG Fecal by Multi 4/17/2014 WteQl y Reported By: S. J. y� son, D.R. Wessinger Concentrations are below Minimum. Quantification Limit, except where noted. NC Laboratory Certificate No. 275 Page 8 of 13 ti Blue Ridge Labs PO Pox 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com- . Client : City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 16-Apr-14 Report Date: 14-May-14 Sample Date: 16-Apr-14 BRL#: BRL-2014-0224 Reissued to.add parameter. Lab Sample ID: LSID-2014-01162 Client Sample ID: 041614-Biosolids Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Cr by ICP-AES 14.7 0.457 dry mg/lcg 6010C 15:59 4/24/2014 KCJ Total Phosphorus 14005 597 dry mg/kg EPA 200.7 15:59 4/24/2014 KCJ Ag by ICP-AES * 0.457 dry mg/kg SW-846-6010 15:59 4/24/2014 KCJ Al by ICP-AES 25948 149 dry mg/kg SW-846-6010 15:59 4/24/2014 KCJ Ca by ICP-AES 546289 747 dry ing/kg SW-846-6010 15:59 4/24/2014 KCJ Cd by ICP-AES 0.8853 0.0914 dry mg/kg SW-846-6010 15:59 4/24/2014 KCJ Cu by ICP-AES 104 0.457 dry mg/kg SW-846-6010 15:59 4/24/2014 KCJ K by ICP-AES 26387 149 dry mg/kg SW-846-6010 15:59 4/24/2014 KCJ Mg by ICP-AES 10584 149 dry mg/kg SW-846-6010 15:59 4/24/2014 KCJ Mo by ICP-AES * 0.457 dry mg/kg SW-846-6010 15:59 4/�4/2014 KCJ Na by ICP-AES 3311 747 dry mg/kg SW-846-6010 15:59 4/24/2014 KCJ Ni by ICP-AES 14.6 0.457 dry mg/kg SW-846-6010 15:59 4/24/2014 KCJ Zn by ICP-AES 167 0.457 dry mg/kg SW-846-6010 15:59 4/24/2014 KCJ Hg by Cold Vapor AAS 0.0641 0.0431 dry mg/kg SW-846-7471 15:12 5/6/2014 KCJ Reported By:`'�#�`' STianson, D.R. Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 1 of 1 Blue Ridge Labs PO Box 2940 Lenoir-, NC 28645 828-728-0149:' blueridgelabslenoir@gmail.com. Client : City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 16-Apr-14 Report Date: 13-May-14 Sample Date: 16-Apr-14 BRL #: BRL-2014-0224 Lab Sample ID: LSID-2014-01163 Client Sample ID: 041614-Biosolids Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Total Kjeldahl Nitrogen (TKN) 19995. 232 drymg/kg SM19 4500-N 16:25 5/12/2014 KCJ �,7inimum Reported By: �S.R. Wessinger Concentrations are belowantification Limit except where noted. NC Laboratory. Certificate No. 275 Page 10 of 13 ♦ 0 C; Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client: City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 16-Apr-14 Report Date: 13-May-14 Sample Date: 16-Apr-14 BRL #: BRL-2014-0224 Lab Sample ID: LSID-2014-01164 Client Sample ID: 041614-Biosolids Parameter Result MQL Nitrate + Nitrite Nitrogen (N2+ 32.9 18.2 blueridgelabsienoir@gmail.com Analysis Analysis Unit Method Time Date Analyst dry mg/kg SM19 4500-N 17:06 5/12/2014 . KCJ Reported By: P Soh son, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Pace 11 of 13 E Blue Ridge Labs PO Box 2940 Lenoir•, NC 28645 828-728-0149, - blueridgelabsienoir@gmail,.com-- Client City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 16-Apr- 14 Report Date: 13-May-14 Sample Date: 16-Apr- 14 BRL #: BRL-2014-0224 Lab Sample ID: LSID-2014-01166 Client Sample ID: 041614-Biosolids Analysis Analysis Parameter Result MQL, Unit Method Time Date Analyst Ammonia Nitrogen 1083 215 dry mg/kg Ammonia 14:08 4/23/2014 KCJ Reported By: S. J. nson, D.R. Wessinger Concentrations are below Minimum Quantification Limit. except where noted. NC Laboratory Certificate Np. 275 .Page 12-of 13 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0,149- blueridgelabslenoir@gmaii.com Client : City of Lenoir P. O. Box 958 Lenoir, NC 28645 Attention: Mr. M. Wall Date Received: 16-Apr-14 Report Date: 13-May-14 Sample Date: 16-Apr-14 BRL #: BRL-2014-0224 Lab Sample ID: LSID-2014-01167 Client Sample ID: 041614-Biosolids Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst % Solids 42:7 0.1 '% % Solids 12:35 4/23/2014 KCJ Plt Available Nitrogen 1 116 233 drying/kg Plant Availabl .17:15 5/12/2014 KCJ pH 11.4 0.1 su SW-846-9040 12:40 4/23/2014 KCJ Reported By: S. ..�oh.son' D.R. Wessinger 6 r Concentrations are b0ow Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 13 of 13 J Suminil Emdronmental Technologies, Inc A V Y, WO#: 14042301 Lk' N, � Y VU, LTIII 3310 Tin, S1. bate Reported: 4/28/2014 Cuyahoga Falls, Ohio 44223 TEL 330) 253-8211 FAX: (330) 2534489 Company: Blue Ridge Labs, Inc. Website: hp.11mmiefteLom Address: P 0 Box 2940 Lenoir NC 28645 Received- 4/24/2014 Project#: 1154,1188, 117 Client WN Lab ID# Collected Analyte Result Units Matrix Method DY RIL Run Analyst 1154 001 4/16/2014 Acetone 0.14 mg/L Non- EPA 624 1 0.050 4/25/2014 MES Potable Water Client ID# Lab lD# Collected Analyte' Result... Units Matrix Method DF' RL Run Analyst 1188 002 4122/2014 Acetone ..0.25 mg/L Non- EPA 624 1 0.050 MES Potable Water Client lD# Lab ID# 'Collected Analyte Result Units Matrix -Method DF Run Analyst 1178 003 4/1612014 Acetone 4.8 mg/L Non- EPA 624 10 0.50 4125/2014 MES Potable Water 0 P ajee4 Of 47 J. WATER QUALITY LAS & OPERATIONS, INC. -P.O. BOX 1167 BANNER ELK, NC 28604 (828)898-6277 CLIENT: BLUE RIDGE LABS ADDRESS: P.O. BOX 2940 CITY: "LENOIR RECEIVED DATE: 17-A)r-14 STATE: NC-.l, 1113 28645 REPORTED DATE: 25-Adr-14 !D#. MEMe" N T V 741 TOTAL SOUDS:,--.-, 39.5 SLUDGE FECAL-- 1155 <s 5.00 MPN/KG LENOIR 17-A1-r-14 • P.YV 1ps TOTAL SOLIDS, 42.8 % SLUDGE FECAL',- '11166 <5 600 MPN/KG LENOIR r-14 PIMPS TOTAL SOLIDS 40.1 % SLUDGE FECAL 1157 <5 5.00 MPN/KG LENOIR 17& M 4 PIAA,*PS TOTAL SOLIDS 44.7 % SLUDGE FECAL' i158'- 44 4.00 MPN/KG LENOIR 17 Ar r-14 PIM PS TOTAL SOLIDS -:. 39.7 % SLUDGE FECAL': 1159 <5 6.00 MPN/KG LENOIR Y:A PIM PS TOTAL SOLIDS",- '44.1 % SLUDGE-FECAL� d160 <5 5.00 MPN/KG L ENOI�l :A 1-14 PIMPS TOTAL SOLIDS 41.7 % I SLUDGE FECAL '. 1161' 1 <5 1 5.00 - I MPN/KG *l LENOIJ 7-Ap A4 t PIM I -IS REPORTED BY, NC CERTIFIED LAB 0 544 PAUL ISENHOUR, SUPERVISOR NPDS Reporting ✓ Groundwater Rep To. (' , Blue Ridge Labs, Inc. P.O. Box 2940 Lenoir, NC 28645 Telephone (829) 728-0149 Fax (829) 728-0131 Chain of Custody Sanitary Landfill Hazardous Waste Industrial or QC _.Non State Reporting USTITTust Fund Reporting Bill To: Project Name: PO Number: Ice Present: V N Field Preceruntisrec l.afn C hpric Sample ID Sample Type Date Tome Time& Temp BR:MM °C Field Sulfide Check Y N Field Sulfide Peesen[ I Removed Y N Resid Chlor Field Check Y N Field Dechlarination Y N pH Resid Chlor P mr A Temp °C Sampler Initials Analysis !Requested • C�( Ct:� Crv! r N AfrTT— q%ush be: ime: Date: Thne: , ` 6 ce' ed By: D10 Upon sobmissiun of samples, client agrees that invoices are due at the time work is comocced. Open accounts aic due 20 days following invoice date. A finance charge of 1.5%per month will be impnsed on all paalue accounts. When mrinquishing samples to Blur, Ridge Labs (BRL.), huycrarrthori= M to perform only the analysis indicated above and also agrees to pay collection and attorney ferf'ihe account becomes delinquent. Blue Ridge Lobs reserves the right to deny doeurnmiation fbr any svorlt where payment. has not been made, in effect rendering that data unsupported for tegulatnry pufypuses. BRL, cannot guaratnce rhos any regulatory authc nity will acctvt any WMI submitted, therefole it is the client's responsibility to request on this Form apprope;ore tests. NC DEER Cenifted Lab 4275 aceAnalytical www.pacelabs.com t ANALYTICAL RESULTS Project City of Lenoir 418 Pace Project No.: 92199422 Pace Analytical Services,.Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: 041614-BIOSOILDS Lab ID: 92199422002 Collected: 04/16/1415.45 Received: 04/30/1416:40 Matrix: Water . . Parameters. .. Results., _ Units ReportLimit - DF . Prepared . Analyzed' CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 2.2 mg/kg 1.0 1 05/09/14 06:30 05109/1416:43 7440-38-2 Lead 7.8 mg/kg 1.0 1 . 05/09/14 06:30 05/09/1416:43 7439-92-1 Selenium ND mglkg 1.5 1 05/09/14 06:30 05/09/1416:43 7782-49-2 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 49.8 % 0.10 1 05109/1411:33 D6 Date:.05/09/2014 06:27 PM REPORT OF LABORATORY ANALYSIS This report shall not tie reproduced, except in full, without the written consent of Pace Analytical Services, Ina. Page 5 of 12 ..aceAnalydcal wwwpacerabs.com Pace Analytical Services, Inc. 6701 Conferenps Drive Raleigh, NC 27607, (919)8344984 SAMPLE ANALYTE COUNT Project City of Lenoir 418 Pace Project No.: 92199422 ' Analyses Lab ID Sample ID., Method Analysts Reported Laboratory 92199422001 040814M-LEFF EPA200.8 DRS 1 PASI-O 92199422002 041614-BIOSOILDS EPA 6010 CRT 3 . PAS10 ASTM D297487` ` ' " ` GPVV 1 PASI-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. .. i ; • Page 3 of 12 CHAIN-®17-CUSTODY. 1 Analytical Request Document . i ;aneAna1j4ica1 The Chain•of-CUstgdy Is a LEGAL DOCUMENT: All relevant feids must be' completed accurately. c mmilecetabs.com Section'A Section B Section C. Page: �oi Required Client Information: Required Project Information: Involco Informallon: cc m �Z1 t ('- Report To: Attenlionf ` 15 E°� �j Address: Copy To; Company Name: REC$UE.ATORY AC�ENGY yst j j j W Address: r NPDE'S f GROUND WATER j DRINKING WATER I" UST r RCRA lOTHER E nail To: Purchase Order No.: Pau? Duck 116fafence: Fsx: Project Narn6: Pita Projcet Site Location Marmagar, STATE: r �.. `,n�`"I (.= • Requested Due QateITAT: Project Number. PacerPfonlofF. Requested Analysis Filtered (YM) Section D Matrix Codos a RaquimdeAlent lnformailon MRialX./ QDE n < COLLECTED Preservallves P Drinking Water DIN °u z Water Wr a wastctCBMPOaftr• PProdu Water WW '$ WY aiAr.T Comdposils GNnrtiRhe ram] SciVScad 5L �" SAMPLE ID °Nape i; $ w y WP IA•Z, 0-91 ri Air ¢R e[ a 2 d c 0 SomplD We MUST BE UNIQUE Tissue TS Other O U M ¢ m Z N V OT a a p� O m cabATE l=02b h Y = 2 TIME DATE TIME 0' Pace Pro ect No./ I,ab I.D. 1 �ti0 IYV C• z/—% d5, - op s 3 • a s 6 7 _ ' 8 8 • 10 11 12 ADDITIONAL COMMENTS REURQUISHED BY l AFFILIATION DATE_ 'TIME ACCEP BY I AFFILIATION DATE TIME SAMPLE CONDITIONS / te Pf SAMPLER NAME AND SIGNATURE u a ^ m PRINT No?fle of SAMPLER,. �;PICaif�Ar.DATE SJ ° SIGNATURE of SAMPLER (MM/DDlWjd_2 Impadanl Notd: By eigning ads form you are acrrptbig Patio's NET 3b day paynmeat terms and agreeing to late charges of 1.5% per month for airy Immlrns pot paid v ithln Soda yl & F-ALL-Q-020rev.07, 15-May-2007 a P!'Q� � ��"t �) ` � d — �. �- _ - - � � �..-. { � _ :. �� �2 7 �-� � __ - �yf.: - r t� f � �t�%�'C�'� � ��-�' '��j<i ice+ t ``,e �"�i �LL-�-p v�} h�'�+�( 1 . f. �. _.._ ,� / s � ' ', -_- �- -- _ _-- 5 ��4 n IAft - cioic l�LAI L Lr 1_ "A f\-, YI r n I .1 ,- 9 t , d t_ n e . Y