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WQ0001048_Renewal (Application)_20190903
State of North Carolina Department of Environmental Quality DWR Division of Water Resources WATER QUALITY REGIONAL OPERATIONS SECTION Division of Water Resources NON -DISCHARGE APPLICATION REVIEW REQUEST FORM n September 3, 2019 To: WaRO-WQROS: David May / Robert Tankard From: Ranveer Katyal, Water Quality Permitting Section - Non -Discharge Branch a ,o p 0? �sh'9r at;'ai,9 0I19 io �`ro"oar Permit Number: WQ0001048 Permit Type: Land Application of Residual'§@ds (503) gee Applicant: Contentnea Metropolitan Sewerage District Project Type: Renewal Owner Type: Organization Facility Name: Contentnea MSD RLAP Signature Authority: Charles Smithwick, Jr. Address: PO Box 477, Grifton, NC 28530 Fee Category: Non -Discharge Minor Comments/Other Information: Owner in BIMS? Yes Facility in BIMS? Yes Title: District Manager County: Pitt Fee Amount: $0 -Renewal Attached, you will find all information submitted in support of the above -referenced application for your review, comment, and/or action. Within 45 calendar days, please take the following actions: ® Return this form completed. ® Return a completed staff report. ❑ Attach an Attachment B for Certification. ❑ Issue an Attachment B Certification. When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and return it to the appropriate Central Office Water Quality Permitting Section contact person listed above. RO-WQROS Reviewer: Date: FORM: WQROSNDARR 09-15 Page 1 of 1 ROY COOPER Governor MICHAEL S. REGAN Secretary LINDA CULPEPPER Director NORTH CAROLINA Environmental Quality September 3, 2019 CHARLES SMITHWICK, JR. — DISTRICT MANAGER CONTENTNEA METROPOLITAN SEWERAGE DISTRICT PO BOX 477 GRIFTON, NORTH CAROLINA 28530 Subject: Acknowledgement of Application No. WQ0001048 Contentnea MSD RLAP Residuals Management System Pitt County Dear Mr. Smithwick: The Water Quality Permitting Section acknowledges receipt of your permit application and supporting documentation received on August 29, 2019. Your application package has been assigned the number listed above, and the primary reviewer is Ranveer Katyal. Central and Regional Office staff will perform a detailed review of the provided application, and may contact you with a request for additional information. To ensure maximum efficiency in processing permit applications, the Division of Water Resources requests your assistance in providing a timely and complete response to any additional information requests. Please note that processing standard review permit applications may take as long as 60 to 90 days after receipt of a complete application. If you have any questions, please contact Ranveer Katyal at (919) 707-3661 or ranveer.katyal@ncdenr.gov. Sincerely, aux�' Nathaniel D. Thornburg, Supervisor Division of Water Resources cc: Washington Regional Office, Water Quality Regional Operations Section Permit File WQ0001048 D E Q�Z i;ZA North Carolina Department of Environmental Quality I Division of Water Resources 512 North Salisbury Street 1 1617 Mail Service Center I Raleigh, North Carolina 27699-1617 919.707.9000 SF,o !y pat'i�a�O Application for Renewal of �70�,�d Permit No. WQ0001048 Non -Dedicated Residuals Land Application Program Contentnea Metropolitan Sewerage District Grifton, North Carolina August 2019 TV THE WOOTEN COMPANY License No. F-01 15 TWC: 2301 9�c�44:�_ ZXti August 27, 2019 `SF,o �Q14,9 41 �ash�aa� OGaiZOJ9 Mr. Nathaniel Thornburg, Branch Chief �9'o�9ass9�9,0 Division of Water Resources 9io�a�•o THE Non-Discharge Branch WO OT E N 1617 Mail Service Center LL!! V Raleigh, NC 27699-1617 Re: Residuals Land Application Program Permit Renewal Permit No. WQ0001048 RECt.!`��'A'�'�F�''Ul' Contentnea Metropolitan Sewerage District, Pitt County TWC No. 2301 AUG 2019 Dear Mr. Thornburg: Non-D,"charge Permitla'-1, Unil On behalf of the Contentnea Metropolitan Sewerage District (CMSD), enclosed please find one (1) original and two (2) copies of an application to request renewal of the above referenced permit. CMSD is requesting renewal of Sites B, C, and D which totals 68.55 acres and is permitted for the application of 291 dry tons per year. Each application section is divided into the following sections: 1. Form RLAP 06-16 a. Current Land Application Permit b. Operation and Maintenance Plan 2. Form RSC 06-16 for WWTP Residuals a. Vicinity map b. CMSD Schematic Flow Diagram c. Residuals Production Documentation d. Sampling and Monitoring Plan 3. Form LASC 06-16 with attachments a. Vicinity, Soils, and Setback Maps b. Updated Cumulative Pollutant Loadings 4. Form LOA 06-16 for: Site D (Gaskins owned site); Sites B and C (CMSD owned sites) If you have any questions about the application contents or require any additional information, please do not hesitate to contact our office at (919) 828-0531 or Charles Smithwick Jr. at (252) 524-5584. Sincerely, THE WOOTEN COMPANY 120 North Boylan Avenue Raleigh, NC 27603-1423 Casey Garland, PhD. 919.828.0531 Enclosures Fax 919.834.3589 cc: Charles Smithwick Jr., Contentnea Metropolitan Sewerage District www.thewcotencompany.com TWC files State of North Carolina DWR Department of Environmental Quality k a �-� 0 2010 Division of Water Resources Division of Water Resources 15A NCAC 42jb.1100 — RESIDUALS LAND APPLICATION PROGRAM INSTRUCTIONS FOR FARM: RLAP 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two conies of the application and supportinLy documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permittintr Unit General — This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under 15A NCAC 02T .1 100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages): in Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. The Applicant's Certification on Page 5 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). ® If this project is for a modification of an existing permit, submit one copy of the existing permit. ® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit Major Modification Major (land are permitted for > 300 acres) $1,310 $395 Minor (land are permitted for < 300 acres) $810 $245 ' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional land application areas not previously approved for that particular program [including transferring of field(s) from one program to another]; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor modifications to a permit. C. Cover Letter (All Application Packages) List all items included in the application package, as well as a brief description of the requested permitting action. D. Environmental Assessments (Maybe Required— See 15A NCAC 1C .0300) in Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: RLAP 06-16 Pagel of 3 E. Operation and Maintenance Plan (New and Renewal Application Packages) For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ® Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum: Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ® Maintenance schedules; may include equipment calibration, maintenance of signs, etc. ® Safety measures; may include safety training program, manuals, signs, etc. ® Spill response plan; including control, containment, remediation, emergency contact information, etc. ® Inspection plan including the following information; ® Names and titles of personnel responsible for conducting the inspections. ® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ®, Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. Z Sampling and monitoring plan including the following information; ® Names and titles of personnel responsible for conducting the sampling and monitoring. ® Detailed description of monitoring procedures including parameters to be monitored. Z Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY. F. Program Determination Dedicated residuals land application programs are ones in which land application sites meet the criteria in 15A NCAC 02T .110202). Specifically, a residuals land application program is designated as dedicated if any of the following are applicable: ❑ Any land application site certified for the residuals land application program that receives residuals at rates or frequencies greater than agronomic rates. ❑ Any land application site certified for the residuals land application program that is used primarily for residuals disposal, and agricultural crop production is of secondary importance. Any land application site certified for the residuals land application program that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system. Please contact the Non -Discharge Permitting Unit if you need any assistance in determining whether your residuals program falls under the dedicated program definitions. G. Program Information ❑ Provide an explanation of why a dedicated system is required instead of a conventional non -dedicated system. ❑ Provide an explanation of the dedicated system and its operation. II. Detailed Site Maps (All New or Modification Application Packages) ❑ Submit three (3) sets of standard size plans and two (2) sets of I by 17" plans (electronic format is acceptable - Adobe PDF only). For Modifications, submit plans specific to the modification(s) only. ❑ Plans must include the following minimum items: ❑ A general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 25% of the total site relief and showing all facility related structures and fences within the land application area. ❑ The location of all wells (including usage and construction details if available), streams (ephemeral, intermittent, and perennial), springs, lakes, ponds, and other surface drainage features within 500 feet of the land application site(s). ❑ Delineation of the review and compliance boundaries ❑ Setbacks as required by 15A NCAC 02T .1108 ❑ Site property boundaries within 500 feet of all waste treatment, storage, and disposal site(s). ❑ A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist's evaluation. The irrigation plans shall show each nozzle/emitter and wetted area (when applicable). Clearly label spray irrigation zones as they will be operated. Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans. However, the plans may be labeled with the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION INSTRUCTIONS FOR FORM: RLAP 06-16 Page 2 of 3 1. LM L. M. Project Evaluation and Receiver Site Management Plan (All New Application Packages or Modifications that include new sites) IM Submit a project evaluation and a receiver site management plan (if applicable) with recommendations concerning cover crops and their ability to accept the proposed application rates. Hydrogeologic Report (All New Application Packages or Modifications involving increasing the total design capacity) Submit a detailed hydrogeologic evaluation in accordance with 15A NCAC 02T .1104(d)(4) and current Division Policy available at: hn://www.ncwater.org,!&ules Policies and Regulations/. The document shall be signed, sealed and dated by a qualified professional. Engineering Design Documents (All New or Modification Application Packages with fixed irrigation facilities or irrigation facilities fed through fixed supply system) ❑ Submit engineering design documents that have been signed, sealed,. and dated by a NC licensed Professional Engineer and/or Professional Land Surveyor in accordance with 15A NCAC 02T .1104(d)(2). For Modifications, submit an updated site map specific to the modification(s) only. ❑ The design documents must include the following minimum items: ❑ Engineering plans for the facility and equipment except those previously permitted unless they are directly tied into the new units or are critical to the understanding of the complete process; ❑ Specifications describing materials to be used, method of construction, and means for ensuring quality and integrity of the finished product including leaking testing; and ❑ Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head curve analysis for each pump, and irrigation design. El Soil mapping units shown on all disposal sites. Water Balance (All New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities or irrigation facilities fed through fixed supply systems) IM Submit a completed and accurate water balance in accordance with 15A NCAC 02T .1104(d)(5) and current Division Policy available at: bttp://www.ncwater:org/Rules Policies and Regulations/. Property Ownership Documentation (All New or Modification Application Packages involving new and/or relocated treatment or irrigation components) Property ownership documentation shall consist of one of the following: ❑ Legal documentation of ownership (i.e., GIS, deed or article of incorporation), or ❑ Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or ❑� An easement running with the land specifically indicating the intended use of the property and meeting the requirements of 15A NCAC 02L .0107(f) or IN A written notarized lease agreement signed by both parties, indicating the intended use of the property, as well as a plat or survey map. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: RLAP 06-16 Page 3 of 3 State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM FORM: RLAP 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: Contentnea Metropolitan Sewerage District Applicant type: ❑ Individual E Corporation ❑ General Partnership Privately -Owned Public Utility ❑ Federal IS State Z Municipal County Signature authority's name per 15A NCAC 02T .0106: Charles Smithwick, Jr. Title: District Manager Applicant's mailing address: PO Box 477 City: Grifton State: NC Zip: 28530 Telephone number: (252) 524-5584 Email Address: crosd100(a,embargmail.com 2. Consultant's name: Charles Davis License Number (for P.E.): 22531 Affiliation: JAOn Staff E Retained (Firm: The Wooten Company) Consultant's mailing address: 120 N. Boylan Ave. City: Ralei State: NC Zip: 27603 Telephone number: (919) 828-0531 Email Address: cdavis@thewootencompany.com 3. Agronomist's name: = License Number: Affiliation: in N/A 0 On Staff ll Retained (Firm: En RECENFrINICDFOJUNR Agronomist's mailing address: = A U G :; 9 2 019 City: an State: Zip: Telephone number: (_)_- Email Address: _ Non-Di�Charge Permitting Unit 4. Soil Scientist's name: License Number: Affiliation: M N/A ❑ On Staff ❑ Retained (Firm: ) Soil Scientist's mailing address: City: State: Zip: - Telephone number:) _-A Email Address: 5. Fee submitted: $0 (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): 0 new, ❑ modified, N renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: WQ0001048 Date of most -recently issued permit: FebruM 1, 2015 to January 31, 2020 Date of most -recently certified Attachment A (if different than the permit): same as permit Date of most -recently certified Attachment B (if different than the permit): same as permit FORM: RLAP 06-16 Page 1 of III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility's physical address: 900 Wiley Gaskins Rd. City: Grifton State: NC Zip: 28530 Coordinates: Latitude: 35' 21' 36.7" Longitude: 77' 24' 57.6" Datum: NAD83 Level of accuracy: 1/100 Method of measurement: UTM 2. County where residuals land application program is headquartered: Pitt County 3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Renee B. Smith CMSD 14790 Back -Up ORC Charles Smithwick Jr. CMSD 991850 Additional Back -Up ORCs (if applicable) N/A N/A N/A If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitro -yen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 291 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 52.46 53.25 15,266 15,496 Five -Year Maximum Adjusted 76.62 77.41 22,297 22,526 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation 0 N/A Row Crops 0 N/A Hay 68.55 Coastal Bermuda Grass Pasture 0 N/A Total: 68.55 N/A Methods Surface 68.55 N/A Incorporation or Injection 0 N/A Total: 68.55 N/A FORM: RLAP 06-16 Page 2 of 5 c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Application Rate qbs PAN/ac yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 305.3 309.9 445.9 450.5 100 152.7 155.0 223.0 225.3 150 101.8 103.3 148.6 150.2 200 76.3 77.5 111.5 112.6 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): No 7. Specify type of residuals program (See Instruction F): M Non -dedicated IM Dedicated If Dedicated, specify the following (check all that apply): ❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; ❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; ❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals Source Certification and all associated documentation. EM Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. El Land Application Site Certification.doc FORM: RLAP 06-16 Page 3 of 5 Note: Item VI. Applicable to Dedicated Program with fixed irrigation system only. 1 DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM 1. The irrigation system is: IM Spray IM Drip 2. Disposal system is: In existing IM proposed. 3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet below ground surface. Rules 15A NCAC 02T .050M requires at least one -foot vertical separation between SHWT and ground surface. 4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area? ll Yes or IN No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if structures are to be maintained or modified: 5. Loading rates recommended by the Soil Scientist Evaluation: Recommended Recommended Soil Series Fields within Soil Area Loading Rate Loading Rate inr in/ r ME am 6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist? ❑ Yes or 0 No If No, explain why 15A NCAC 02T .0505(n) is not met: 7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system): Field / Zone Design Area (ft Z) Number of Nozzles Maximum Application Rate allons/hr Design Annual Loading Rate allons/ r s Total Spray Irrigation Design Element Plan Sheet Number Specification Page Number Wetted diameter of nozzles ft „ Wetted area of nozzles ft2 " Nozzle capacity gpm Nozzle manufacturer / model / Elevation of highest nozzle ft FORM: RLAP 06-16 Page 4 of 5 pplicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. Yes M No, Explain; I, L-)y\c Cke,g M �1YtC� c:V �A'\o.t�.� (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for Co,n v�ku� __ Kkkkf 0 W`: A-V- (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a.technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any Ise statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine >t to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: C wl CC Date: ' zZ - lq FORM: RLAP 06-16 Page 5 of 5 Contentnea Metropolitan Sewerage District 2019 Residuals Land Application Permit Renewal Supporting Information: Existing (Non -Dedicated) Residuals Land Application Permit Existing Operation and Maintenance Plan t hr , wy HCDENR North Carolina Department of Environment and Natural Resources Pat Ivl; :Crory Governor December 2, 2014 Charles Smithwick, District Manager Contentnea Metropolitan Sewerage District Post Office Box 477 Grifton, North Carolina 28530 Dear Mr. Smithwick: John E, Skvatla, III . Secretary/ Subject: Permit No. WQ0001048 Contentnea MSD WWTP Land Application of Class B Residuals (Non -Dedicated) Pitt County In accordance with your permit application minor modification and renewal request received September 2, 2014, we are forwarding herewith Permit No. WQ0001048 dated December 2, 2014, to Contentnea Metropolitan Sewerage District for the continued operation of the subject residuals management program. Please note that this renewed permit shall become effective on February 1, 2015 (i.e. the day after the expiration date of the existing permit), which differs from the date of this letter. Modifications to the subject permit are as follows: © The maximum dry tons have been decreased from 320 to 291. • Acreage changes to Sites B, C and D because of new homes around application sites which resulted in redefined field boundaries or updated GIS mapping techniques for fields. © Deleted Site CMSD2 Fields 1,3,4,5, and 9, and Site CMSD3 Fields 5, 6, 7, 9 and 11 totaling 89.96 acres. This permit shall be effective from February 1, 2015 until January 31, 2020, shall void Permit No. WQ0001048 issued February 18, 2008 and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring requirements listed in Attachments A and C for they may differ from the previous permit issuance. Failure to establish -an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. Please note the following permit conditions and attachments are new since the last permit issuance dated February 18, 2009: - 9 Condition 1.2. — This condition requires that the Permittee to be in compliance with the signage requirements established in Condition M.13. prior to land application. Non -Discharge Pernvtting Unit 1617 Mail Service Center, Ralelgh, North Carolina 27699-1617 Phone: 919-807-M41 Internet: htlp:/1oortal.ncdenr.orglweb/t4o An Equal Opporiuniy t Affirmative Action Employer - Made in part ivith recycled paper (C) a description of the system used to monitor the air for methane gas in the air in any structures within the surface disposal unit boundary and at the property line of the surface disposal unit, if applicable; (D) a discussion of how public access to the surface disposal unit will be restricted; and (E) proof that the deed for the surface disposal unit property has been amended to provide permanent written notification to subsequent owners of the property that the property was used for the purposes of operating a surface disposal unit. History Note: Authority G.S. 143-215.1; 143-215.3(a); Eff. September 1, 2006, 15A NCAC 02T.1110 OPERATION AND MAINTENANCE PLAN An Operation and Maintenance Plan shall be maintained for all residuals management programs. The plan shall: (1) describe the operation of the program and any associated facilities and equipment in suflicientdetailto show what operations are necessary for the program to function and by whom the functions aretobe conducted; (2) describe anticipated maintenance of facilities and equipment that are associated with the program. (3) include provisions for safety measures including restriction of access to the site and equipment, as appropriate; (4) include spill control provisions including: (a) response to upsets and bypasses including control, containment, and remediation; and (b) contact information for program personnel, emergency responders, and regulatory agencies; (5) detail procedures for sampling and monitoring to ensure that the program stays in compliancevviththis Section and any issued permit; and (6) for surface disposal units, detail procedures for post -closure care management. History Note: Authority G.S. 143-215.1; 143-215.3(a); Eff. September 1, 2006. 15A NCAC 02T .1 I I I MONITORING AND REPORTING (a) Representative samples of residuals that are prepared for application to the land or placed in a surface disposalunit shall be collected and analyzed. (b) The analytical methods listed in 40 CFR 503.8(b) as stated on January 1,1996 shall be incorporated into this Section by reference. (c) Residuals applied to the land orplaced in a surface disposal unit shall be monitored fo r pollutants as listed in Rule .1105(a) and Rule .1105(d) of this Section as well as Rule .1106 and Rule .1107 as applicable at the frequency as stipulated in the following: Metric Tons per 365 day period Monitoring Frequency (Dry Weight Basis) Greater than zero but less than 290 Once per year Equal to or greater than 290 but less than 1,500 Once per quarter (four times per year) Equal to or greater than 1,500 but less than 15,000 Once per 60 days (sixtimes per year) Equal to or greater than 15,000 Once per month (12 times per year) (d) A report of all monitoring and reporting requirements as specified in the permit shall be submitted to theDivisionby the permittee annually on or before March 1st of each calendar year. (e) All records shall be retained for a minimum o f five years. HistolyNote: Authority G.S.143-215.1; 143-215.3(a); Eff September 1, 2006. SECTION .1200 — COAL COMBUSTION PRODUCTS MANAGOVMT NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH LAND APPLICATION OF CLASS B RESIDUALS PERMIT (NON -DEDICATED) In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO C®ntentnea Metropolitan Sewerage District Pitt County FOR THE continued operation of a residuals management program for Contentnea Metropolitan Sewerage District and consisting of the land application of Class B residuals generated by the approved facilities listed in Attachment A to the approved sites listed in Attachment B with no discharge of wastes to surface waters, pursuant to the application received September 2, 2014, and in conformity with and other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 503. This permit does not exempt the Permittee from complying with the federal regulations. This permit shall be effective from February 1, 2015 until January 31, 2020 shall void Permit No. WQ0001048 issued February 18, 2008 and shall be subject to the following specified conditions and limitations: I. SCHEDULES No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A NCAC 02T .0105(d) requires an updated site map to bqi suJ mitted with the permit renewal application. 2. The perinittee shall be in full compliance with the regional office notification requhements established in Condition 111.3. by March 1, 2015, 3. The permittee shall be in full compliance with the signage requirements established in Condition 1II.13. by June 1, 2015. WQ0001048 Version 3.0 Shell Version 141027 Page I of 12 9. Setbacks for treatment and storage facilities shall be as follows: Setback Description Setback feet Habitable residence or place of public assembly under separate ownership or not to be maintained as art of the project site 100 Property lines 50 Private or public water supply 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and wetlands 50 Wells with exception to monitoring wells 100 10. Setbacks for Class B land application sites shall be as follows: Setback by application type (feet) Setback Description Vehicular Irrigation Surface Surface Injection / Application Application Incorporation Habitable residence or place of public assembly under separate ownership or not to be maintained as 400 400 200 art of the project site Habitable residence or places of public assembly owned by the Permittee, the owner of the land, or the lessee/operator of the land to be maintained as part 0 200 0 of the project site Property lines 50 150 50 Public right of way 50 50 50 Private or public water supply 100 100 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and wetlands 100 1 QO 50 Surface water diversions (ephemeral streams, waterways, ditches) 25 100 25 Groundwater lowering ditches (where the bottom of the ditch intersects the SHWT 25 100 25 Subsurface groundwater lowering system 0 100 0 Wells with exception to monitoring wells 10Q 100 100 Bedrock outcrops 25 25 25 Top of slope of embankments or cuts of two feet or more in vertical height 15 15 15 Building foundations or basements 0 15 0 Water lines 0 10 0 Swimming pools 100 100 100 Nitrification fields 0 20 0 11. Land application areas shall be clearly marked on each site prior to and during any residuals application event. WQ0001048 Version 3.0 Shell Version 141027 Page 3 of 12 17. In accordance with 15A NCAC 02L .0108, the review boundary shall be established midway between the compliance boundary and the residual land application area. Any exceedanee of groundwater standards at the review boundary shall require action in accordance with I SA NCAC 02L .0106. ffi. OPERATION AND MAINTENANCE REQUIREMENTS 1. The residuals management program shall be properly maintained and operated at all times. The program shall be effectively maintained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. 2. The Washington Regional Office, telephone number (252) 946-6481, and the appropriate local government official (i.e., county manager, city manager, or health director) shall be notified at least 48 hours prior to the initial residuals Iand application to any new land application site. Notification to the regional supervisor shall be made from 8:00 a.m. until 5:00 p.m. on Monday through Friday, excluding State Holidays. 3. The Washington Regional Office shall be notified via email or telephone, (252) 946-6481, at least 24 hours prior to conducting any land application activity. Such notification shall indicate, at a minimum, the anticipated application times, field IDs, and location of land application activities. If it becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be notified prior to commencing the application to those fields. 4. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) pursuant to 15A NCAC 02T . i 110. Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan, at the minimum, shall include: a) Operational functions; b) Maintenance schedules; c) Safety measures; d) Spill response plan; e) Inspection plan including the following information: i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f) Sampling and monitoring plan including the following information: L Names and/or titles of personnel responsible for conduetingthe sampling and monitoring; ii. Detailed description of monitoring procedures including: parameters to be monitored; iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most Iimiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). WQ0001048 Version 3.0 Shell Version 141027 Paua 5 nf 12 k. If the vertical separation of bedrock and the depth of residuals application is less than one foot; 12. The following public access restrictions apply to residual land application sites: a. Public access to public contact sites (e.g., golf courses, parks, ball fields, etc.) shall be restricted for 365 days after a residuals land application event; b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land application event. 13. Public access controls shall include the posting of signs with a minimum area of 3 square feet (e.g., 1.5' x 2'). Each sign shall indicate the activities conducted at each site, permit number, and name and contact information, including the Permittee or applicator's telephone number. Signs shall be posted in a clearly visible and conspicuous manner at the entrance to each land application site during a land application event, and for as long as the public access restrictions required under IU.12 apply. 14. The following harvesting and grazing restrictions apply to residual land application sites after each land application event: Harvesting and Grazing Description Restricted Duration Animals shall not be allowed to graze during land application activities and restricted period. Sites that are to be used for grazing shall have fencing to 30 days prevent access after each land application event. Food crops, feed crops and fiber crops shall not be harvested for: 30 days Turf grown on land where residuals have been applied shall not be harvested for: 12 months Food crops with harvested parts that touch the residual/soil mixture and are totally above the land surface (e.g., tobacco, melons, cucumbers, squash, etc.) 14 months shall not be harvested for: When the residuals remain on the land surface for four months or longer prior to incorporation into the soil, food crops with harvested parts below the land 20 months surface (e.g., root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for: When the residuals remain on the land surface for less than four months prior to incorporation into the soil, food crops with harvested parts below the land 3 8 months surface shall not be harvested for: 15. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume of other nutrient sources (i.e., manufactured fertilizers, manures,, or other animal waste products) that have been applied to the site, and a copy of the most recent Ntrient Management Plan (NMP) for those operations where a NMP is required by the US Department of Agriculture — National Resources Conservation Service (MRCS) or other State Agencies. The Permittee shall calculate allowable nutrient loading rates based on the provided information and use appropriate reductions. For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan (WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient Management Plan. 16. No residuals shall be land applied unless the submitted Land Owner Agreement Attachment (LOAA) between the Permittee and landowners or lessees/operators of the land application site is in full force and effect. These agreements shall be considered expired concurrent with the permit expiration date, and shall be renewed during the permit renewal process. WQ0001048 Version 3.0 Shell Version 141027 Page 7 of 12 Residuals shall be monitored for compliance with pathogen and vector attraction reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class B pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (c) and one vector attraction reduction requirement in 15A NCAC 02T .1107 (a) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. 5. An annual representative soils analysis (ire., Standard Soil Fertility Analysis) shall be conducted on each land application site listed in Attachment B on which a residuals land application event will occur in the respective calendar year. This analysis shall be in accordance with the "Guidance on Soil Sampling" located in the Sampling Instructions section of the NC Department of Agriculture & Consumer Services' website(littp://www•ncagr.gov/agi-otioiiii/pubs•litm). The Permittee shall maintain these results and a description of the sampling methodologies used to determine soil fertility for a period of no less than five years, and shall be made available to the Division upon request. At a minimum, the Standard Soil Fertility Analysis shall include the following parameters: Acidity Exchangeable Sodium Percentage Phosphorus Base Saturation (by calculation) Magnesium Potassium Calcium Manganese Sodium Cation Exchange Capacity Percent Humic Matter Zinc Copper pH 6. Laboratory parameter analyses shall be performed on the residuals as they are land applied, and shall be in accordance with the monitoring requirements in 15A NCAC 02B .0505. 7. Monitor wells shall be sampled after construction and within three months prior to initiating residual application operations. Monitoring wells shall be sampled thereafter at the frequencies and for the parameters specified in Attachment C. All mapping;, well construction forms, well abandonment forms and monitoring data shall refer to the permit number and the well nomenclature as provided in Attachment C. 8. For initial sampling of monitoring wells, the Permittee shall submit a Compliance Monitoring Form (GW-59) and a Well Construction Record Form (GW-1) listing this permit ,number and the appropriate monitoring well identification number. Initial Compliance Monitoring Forms (GW-59) without copies of the Well Construction Record Forms (GW-1) are deemed incomplete, and may be returned to the Permittee without being processed. 9. Two copies of the monitoring well sampling and analysis results shall be submitted on a Compliance Monitoring Form (GW-59), along with attached copies of labozatory analyses, on or before the last working day of the month following the sampling month. The Compliance Monitoring Form (GW- 59) shall include this permit number, the appropriate well identification number, and one GW-59a certification form shall be submitted with each set of sampling iregults. All information shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 WQ0001048 Version 3.0 Shell Version 141027 Nee 9 .of 12 d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment. e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to be taken to ensure that the problem does not recur. V. INSPECTIONS 1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan. 2. Prior to each bulk residuals land application event, the Permittee or his designee shall inspect the residuals storage, transport and application facilities to prevent malfunctions, facility deterioration and operator errors resulting in discharges, which may cause the release of wastes to the environment, a threat to human health or a public nuisance. The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. 3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the land application sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples. VI. GENERAL CONDITIONS 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143- 215.6A to 143-215.6C. 2. This permit shall become voidable if the residuals land application events are not carried out in accordance with the conditions of this permit. 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation. 4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes, rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCG010000; any requirements pertaining to wetlands under 15A NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. WQ0001048 Version 3.0 Shell Version 141027 Pam i l of 12 ATTAC MI . f A - Approved Residual Sources Contentnea Metropolitan Sewerage District Certification Date: December 2, 2014 Permit Number! WOOODIO41 VP11C11111D 11) Maximum Monitoring Monitoring Monitoring Frequency for Approved Owner Facility Name County Permit SioIogical Dry Tons (Frequency for Frequency for Pathogen & Mineralization Number Residuals Per Year r Non-hazardous Metals and Vector Attraction Rate Characteristics Nutrients Reduchonsa,s Co enmea Metropolitan Contentnea Metropolitan Sewera a District Sewera a District WWTP Pitt NCO032077 Yes 291 Annually Annually Annually 0.30 Total 291 1. Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility. 2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2. 3. Testing of metals and nutrients as stipulated under permit Condition IV.3. 4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IVA. 5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above. Dry Tons Generated short tons per ear(Established Monitoring Frequency in 40 CFR 503 and 15A NCAC 02T .1111 <319 I/Year =>319 - <1,650 1/ Quarter 4 times per year =>1 650 - <16,500 1160 Days 6 times per ear >16,500 1/month (12 times per year If no land application events occur during a required sampling period (e.g. no land application occur during an entire year when annual monitoring is required), then no sampling data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification. Page 1 of 1 ATTACM _ ,iT B - Approved Land Application Sites Contentnea Metropolitan Sewerage District Certification Date: December 2, 2014 Permit Number! WQ0001048 Version: 3.0 —field/ Site Owner Lessee County ]Latitude Y.ongitude Net Acreage_ Dominant Soil Series Footnotes B-1 Contentnea Metropolitan Sewerage District Mills Creston Pitt 350 21' 26" 7702415811 2.84 Portsmouth B-2 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 26" 770 24' 58" 2.62 Pactolus B-3 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 26" 770 24' 58" 2.72 Portsmouth B-4 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 26" 770 24' 58" 3.34 Pactolus B-5 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 26" 770 24' 58" 3.74 Pactolus B-6 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 35" 21' 26" 77" 24' 58" 2.48 Chipley B-7 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 26" 770 24' 58" 1.32 Chipley CI-10 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 22' 00" 770 25' 03" 8.55 Alaga CII-8 Contentnca Metropolitan Sewerage District Mills, Creston Pitt 350 22' 03" 770 25' 05" 7.73 Alaga CH-9 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 22' 03" 77' 25' 05" 5.15 Alaga CH-13 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 22' 03" 770 25' 05" 3.30 Ocilla CIU-12 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 48" 770 24' 57" 5.23 Osier CIV-11 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 50" 770 24' 52" 5.13 Osier D-14 Gaskins, Michael Mills, Creston Pitt 350 21' 40" 770 24' 42" 3.00 Portsmouth D-15 Gaskins, Michael Mills, Creston Pitt 350 21' 40" 770 24' 42" 2.38 Portsmouth D-16 Gaskins, Michael Mills, Creston Pitt 350 21' 40" 770 24' 42" 2.98 Alaga D-17 Gaskins, Michael Mills, Creston Pitt 350 21' 40" 770 24' 42" 3.62 Alaga D-18 Gaskins, Michael Mills, Creston Pitt 350 21' 40" 770 24' 42" 2.42 Pactolus Total 68.55 Page 1 of 1 ATTACffi.,,__ 4T C — Groundwater Monitoring and Limitations Contentnea Metropolitan Sewerage District Monitoring wells: MW-9, AM-10, MW-14, MW-15, MW-18 Permit Number: WQ0001048 Version: 3.0 GROUNDWATER CHARACTERISTICS GROUNDWATER STANDARDS MONITORING REQUIREMENTS PCS Code Parameter Description Daily Maximum Frequency Measurement Sample Type Footnotes 82546 Water level, distance from measuring point feet 3 x year Calculated 1,2,3,7 316*16 Coliform, Fecal MF, M-.FC Broth,44.5C #/100mi 3 x year Grab 1,7 70300 Solids, Total Dissolved- I80 Deg.0 500.00 mg/1 3 x year Grab 1,7 00403 Ph, lab s.u. 3 x year Grab 1,7 . 00680 Carbon, Tot Organic (TOC) mg/l 3 x year Grab 1,6,7 00610 Nitrogen, Ammonia Total (as N) 1,500.00 µg/1 3 x year Grab 1,7 00620 Nitrogen, Nitrate Total (as N) 10.00 mg/1 3 x year Grab 1,7 01034 Chromium, Total (as Cr) 10.40 µg/l 3 x year Grab 1,7 01042 Copper, Total (as Cu) 1.00 mg/1 3 x year Grab 1,7 78732 Volatile Compounds, (GC/MS) mg/l Annually Grab 1,4,5,7 . . m u.v,uu,'u.s Luau uc wuuuucu m rcoruwy June 6G Uctooer; AnnuaJ monitoring snau be conuuctea everyUetober. 2. The measurement of water levels shall be made prior to purging the wells. The depth to water in each weII shall be measured from the surveyed point on the top of the casing. The measurement of pH shall be made after purging and prior to sampling for the remaining parameters. 3. The measuring points (top of well casing) of all monitoring wells shall be surveyed to provide the relative elevation of the measuring point for each monitoring well. The measuring points (top of casing) of all monitoring wells shall be surveyed relative to a common datum. 4. Volatile Organic Compounds (VOC) --In November only, analyze by one of the following methods: a Standard Method 6230D, PQL at 0.5 µg/L or less b. Standard Method 6210D, PQL at 0.5 µg/L or less c. EPA Method 8021, Low Concentration, PQL at 0.5 µg/L or less d. EPA Method 8260, Low Concentration, PQL at 0.5 µgal, or less e. Another method with prior approval by the Water Quality Permitting Section Chief Any method used must meet the following qualifications: a. A laboratory must be DWQ certified to run any method used. b. The method used must, at a minimum, include all the constituents listed in Table VIII of Standard Method 6230D. c. The method used must provide a PQL of 0.5 µg/L or less that must be supported by laboratory proficiency studies as required by the DWQ Laboratory Certification Unit. Any constituents detected above the MDL but below the PQL of 0.5 µg/L must be qualified (estimated) and reported. 5. If any volatile organic compounds (VOC) are detected as a result of monitoring as provided in Attachment C, then the Washington Regional Office supervisor, telephone number (252) 946-6481, must be contacted immediately for further instructions regarding any additional follow-up analyses required. 6. If TOC concentrations greater than 10 mg/l are detected in any downgradient monitoring well, additional sampling and analysis must be conducted to identify the individual constituents comprising this TOC concentration. If the TOC concentration as measured in the background monitor well exceeds 10 mg/l, this concentration will betaken to represent the naturally occurring TOC concentration. Any exceedances of this naturally occurring TOC concentration in the downgradient wells shall be subject to the additional sampling and analysis as described above. 7. Monitoring wells shall be reported consistent with the nomenclature and location information provided in this attachment. Page 1 of I bf()N cONT __ T.—N A tiIEI RcrPpl J1tr 1-ORD - Sh14AC.t3 0s st7. y e *? Y �T�s i 9 87 Gr4ss`Ac ;� z PRMICINR r : r (OIIB - e t errs` GRAHMI FRANCINE r cofm 12 Wiley Gasla'ns 1t �3- tt t 3.17'Gross Ac. Y NOR�C4TT d r QN JR NHURS 3.03 Gross f�c. °SKEIVDA•GAHD_NEN 3 32kGross VC. ~ U rHARRIS t.. ON A METROI'C3LIJ: 5 ► SEWAGE Y 4 3 f 3.74 Net Ac. t5 ltirv�{i0 1 TON SRUCE ANIVOIV JR CONTENTNFA ETRDPOS l7'AIV h'- AISEWAGE 3634 Net Ac. 2.62 Net Pic. �' TOWN OF SITE S'' 2.72 Net AC. W , �;: ► Legend w GRIFFON - � $4 Net Aet =x 2�28 GrossrAc Y �� NORCOTT { HOtlSe jRH�E,IRSF �t� i�a+ 2.50 Gross Ac, r +K _ s,.. Monitor Weil j ` rr V Ditch 7� ��� 2.48 Net AA: --- .Stream Building Field Baundar� .MW9 Machine Net Area RGiNIN.h' PAYTOIV CONTENTINEA +r4ETftOPC+LlT a q r. y7. A'4 k i-Si.�i AGI: X r�k. Machine Buffer F �< Ak Pond v 0 150 300 600 Property Boundary sr b U M Feet ' 1Y /, .ate: I inch = 300 feet SITE B BUFFER MAP - FIELDS 1, 7 FIGURE I7ramm By: CSC r" - C\[SD CLASS B LAND APPLICATION Reviewed By: '�` _ Chiss B Ilct»ut 1�'(){?Q010aS Date: tlug'14 _ Soil Plus Project # 200710.A10 X ' .sU 3:30 Grass Ac7 � �T 6 13 P, 3.30 Net Ac. '- -. ra '.�--._J_..-.—Mrs. ''S -: � • . t `� • 1 DEMON ? CON7ENrIVGA�A{ETROPOLiTAN� •i�CliD � � „� SEWAGE „_- °�' x� _ �� - d %„ ,:.� �� � 3} �' _ - ��i , _.:ter-+•ai�us�"r"•3'�'c a 664 Gross Ac hIAR1AN NELSON nlciriuHoRni 3.00 5'ITE C` 14 t n r,� ♦' T a;-. ; y at LSON r� �ICLA O'RN 2.338 Net 1j 2 INE s r ` •' . 2.98 Net A REAVES d LAURA E3 GARI I-S Net Ac. TCE,�..� GLOSS AC. y f Legead r F )Y'EiGt1A O H USE =CONTENTl'JEA METROPOL-I-T g �`i�t c Monitor Well SEWAGE ad' — Ditch 3. x -----� Stream 1� Building a 4 Field Boundary 4 l K Machine Net Area 2:G2 NeAt Nc. Machine Buffer 2.84 Net ,Pond G��• *�� s r a 150 300 600 r property Bourd ary 2 30 GrossFeet 2le:1 inch = 300 feet SITE C III & IV BUFFER MAP FIGURE Drawn By: CSC � �J � 1,S CMSD CL.-kSS B LAND APPLIC.ITION Reviewed By: Class B Permit '4l Q0001048 Date: Aug `14 Soil Plus Project # 20071O.A10 A . :.v� � �, ': tt ' Machine Buffer n Pond s s b 0 150 300 600 Q r our Property B xiary x Feet z i :ale: l iriC1} 300 feet SITE D BUFFER MAP FIELD MELDS 14 -18 FIGURE Drawn By: CSC C\ISD CLASS B LANDAPPLICATION, Reviewed By:'sw Cliss B Pcrnut 1VQQOQIQ48 9 Date: Aug `l4 Soil Plus Pxoject # 200710,A10 SEWERAGE DISTRICT .1, , APPLICATION ;. BIOSOLIDS Effi- OPERATION AND MAINTENANCE PLAN January 2015 Land Application Notification Requirements Notification must be made to the Washington Area Regional Office (WARO) 24 Hours prior to any land application activity. Notification can be either email or by telephone. Contact information is as follows: Washington Area Regional Office 252-946-6481 Randy Sipe 252-948-3849 email: randy.sipe(@ncdenr.gov Notification is to include: 1) Anticipated application times 2) Field Identification 3) Location of land application activities If it becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be notified prior to commencing the application to those fields. Before each land application event signage must be posted at public access areas. Signs shall be posted in a clearly visible and conspicuous manner at the entrance to each land application site during a land application event, and for as long as the public access restrictions required under 111.12 of the permit apply. Each sign shall be a minimum of 3 square feet and shall include: 1) Activities conducted at each site 2) Permit number 3) Name and contact information -including Permittee's telephone number The CMSD has three (3) signs that meet this requirement and are stored in the Chemical Feed Building. An example of this sign is depicted on the following page (Fig. 1). Land Application of Biosolids in Progress Contact® Chuck Smithwick (Fig. 1) Overview The Contentnea Metropolitan Sewerage District (CMSD) is permitted to land apply biosolids to land 1) owned and 2) leased by CMSD under permit # WQ0001048. The purpose of the land application program is to dispose of the biosoloids generated by the operations of the Wastewater Treatment Plant (WWTP) which operates under NPDES Permit # NC0032077. Biosolids are land applied to our application sites via two (2) methods: 1) Spray Irrigation via "rain reel" 2) Land application via "terragator" (wheeled application vehicle) Spray Irrigation Application Biosolids are conveyed from aerobic digesters located on the WWTP site to the land application sites by pumps located in the "Intermediate Pump Station". The pump configuration consists of a 60 Hp Gorman Rupp centrifugal pump and a 25 Hp "grinder pump". There are two (2) of these pump configurations; however, only one (1) pump can be used at a time. These pumps are capable of pumping approximately 250 gallons per minute depending on the field location and the amount of "debris" on the impeller. Piping to the land application fields is via 6 inch PVC pipe that is buried underground in order to offer protection to the pipe. At each field, a riser is stubbed up at ground level to allow for the attachment of the "rain reef". The "rain reel" gun cart is extended out into the application field and is retrieved at a slow rate in order to evenly apply the biosolids to the desired location. This means of application is performed by CMSD personnel. Terragator Application This method of land application uses a "terragator" which is a wheeled vehicle with large "floatation" tires and a 4,000 gallon storage tank. Biosolids are pumped into the "terragator" by a pump located at the Northwest corner of digester #1. The vehicle is then driven to the desired location and the biosolids are applied to the site. This method is used for applying biosolids to fields 6, 7,13 and Gaskins 5 due to their small size and proximity to buffers, roads, power lines and ditches. This means of application is performed by contracted personnel (i.e. Granville Farms, Inc.). Maintenance Grinder pump/Centrifugal Pump Grease both pumps (grinder and centrifugal) daily before a land application event commences. Check For visible leaks at pump and fittings after the pump is primed. Centrifugal pump impeller may require cleaning after 20-30 hours of runtime. "Plastics/debris" tend to accumulate on the vanes of the impeller and the volume of biosolids pumped will decrease. Follow 3roper lock out/tag out procedures while performing this task. liser/Rain Reel Jisually inspect the caps located on the top of each riser. If the cap shows signs of deterioration/leaks, it Nill need to be replaced or tightened. Grease the rain reel weekly. Check gas and oil daily. Check for any deteriorated hoses, parts, etc. and replace accordingly. During land application events, monitor the rain reel and associated piping at least twice (2) per hour to assure that the system is operating properly. Safety -Working with heavy equipment and moving parts is inherently dangerous. Use extreme caution and common sense. Hl BE SAFE !!!! -Keep hands, feet and clothing clear of all moving parts associated with the pumps and/or rain reel. -Use PPE (Personal Protective Equipment-i.e. gloves and glasses) when working around equipment and biosolids -Proper lock out/ tag out procedures must be observed during maintenance events. -Access to land application sites is restricted to authorized personnel only. Gates are to be closed at all times in which a land application event is not being actively performed. -Property is registered with the Pitt County Sheriff's Department. In the event that trespassers are observed, call 911 and report the violation. is Spill Response Plan Contacts: CMSD Main Office 900 Wiley Gaskins Road, Grifton 252-524-5584 Chuck Smithwick District Manager/Backup ORC 252-413-8898 Renee Smith ORC 252-531-0368 NCDENR Washington Area Regional Office 252-946-6481 Randy Sipe WARO-Contact/Inspector 252-948-3849 NCDENR Division Emergency Response 800-662-7956 800-858-3068 919-733-3300 While land applying biosolids by means of spray irrigation, the operator shall monitor the entire system twice (2 times) every hour to check for leaks associated with the rain reel and irrigation pipe. In the event of a leak, the system should be shut down and the leak corrected. The land application sites have raised berms around their perimeters to contain any runoff that may occur if a spill does occur. In the event that biosolids do reach surface waters (i.e. ditches), measures should be taken to contain the spill. Topsoil is stockpiled on the Southeast side of the WWTP. This topsoil can be transported via frontend loader and placed in the ditch in order to "dam" the ditch and contain the spill. Portable trash pumps are available onsite at the WWTP to pump the water out of the ditch and onto the land application field. NCDENR (WARD) should be notified within 24 hours of a spill and a written report in letterform shall be filed within five (5) days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to be taken to ensure that the problem does not reoccur. 3 Inspection Plan Names and titles of persons authorized to operate, maintain and inspect land application facilities/equipment: Chuck Smithwick District Manager/Backup ORC 252-413-8898 Renee Smith Lab Manager/ORC 252-531-0368 James Woodard Operator 252-413-8285 Ricky Barrow Operator 252-413-8560 Stephen Berry Operator 252-413-7594 Jimmy Edwards Mechanic 252-531-9060 Frequency of Inspection Equipment (grinder/centrifugal pumps, and rain reel) and associated piping/risers shall be inspected daily before each land application event. Check the following: 1) Grinder/centrifugal pump -properly greased 2) Rain reel -properly greased, fuel, support arms in place, gun head properly adjusted for the field that is being applied to, leaks (at riser, associate piping, flexible hoses, joints, etc.). During a land application event the operator shall monitor the system twice (2 times) per hour to assure that the system is operating properly and that there are no leaks present. If there is a problem, the land application event shall be stopped and the problem corrected before land application of biosolids is to resume. An "Inspection Log" (Fig. 2) shall be kept for each day that a Land Application of Biosolids is performed. The ORC or Backup ORC shall inspect the entire system before initial land application activities occur for that calendar year. Land application normally commences in April of the calendar year. In the event of a "noncompliance" situation, the ORC/Backup ORC shall refer to Section IV, No. 12 (Noncompliance Notification) of the permit (page 10) and follow the outlined procedures as set forth by NCDENR. 4 INSPECTIONS LOG Inspections Prior to/During Land Application Event Date: 1) Grinder Pump greased Yes No 2) Centrifugal Pump greased Yes No 3) Rain Reel greased Yes No 4) Support arms down/locked Yes No 5) Gun Head extended and adjusted Yes No 6) Visual Inspection of risers/pipes/joints Yes No 7) Fuel Yes No Location/Field of Application Event Start Time of Application Event End Time of Application Event Approximate Gallons Applied Monitoring of Land Application Event (2 times per Hour) -write time and initialize for each inspection during event. Comments: (Fig. 2) Land Application Checklist 1) 24 hour prior notification to NCDENR Regional Office (WARD) 2) Signage placed at public access entrances 3) Proper inspection of equipment 4) Maintenance (if required) performed S) Startup and observation of land application event SAMPLING AND MONITORING PLAN FOR CONTENTNEA MSD Land Application of Class B Residuals Permit No. WQ0001048 The Sampling and Monitoring Plan for Contentnea MSD Land Application of Class B Residuals is developed pursuant to Permit No. WQ001048 Section III. Part f. The sampling techniques and subsequent analyses are collected and analyzed in accordance with Federal and State of North Carolina requirements. As a general rule, land application of sludge at the Contentnea MSD facility will occur only during the months of March through October of each year during the growing season of the Coastal Bermuda grass that is the cover crop for the CMSD designated land application fields. Any deviation from this procedure will be addressed through NCDENR Division of Water Resources prior to application and any additional sampling and/or monitoring will be done per their instructions. The Land Application Operator in Responsible Charge/Backup Operator in Responsible Charge will be responsible for the monitoring requirements set forth in the Sampling and Monitoring Plan, and the WWTP sampling personnel will be collecting the samples as directed by the ORC/Backup ORC. All sludge samples for meeting the ceiling concentrations for metals, nutrient loading, pathogen and vector attraction reduction will be conducted during the months of March through October to insure the sludge analyses are representative of the sludge being land applied. All sludge samples will be taken from Digesters #1 and #2, and all sludge is land applied from Digesters #1 & #2. Renee Smith Land Application Operator in Responsible Charge Charles Smithwick, Jr. Backup Land Application Operator in Responsible Charge Ricky Barrow Plant Operator/Sample Collector Stephen Berry Plant Operator/Sample Collector James Woodard Plant Operator/Sample Collector I.TCLP and Corrosivity, Ignitability, Reactivity The corrosivity, ignitability, reactivity and the toxicity characteristic leaching procedure (TCLP) shall be performed annually as specified in Attachment A of Permit No. WQ001048. The samples will be a grab taken from sufficiently stabilized sludge and will be representative of the sludge that is land applied. The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and Its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) 1 Mercury (0.2) Vinyl Chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) II. Metals and Nutrients The metals and nutrients analysis shall be performed annually as specified in Attachment A of Permit No. WQ0001048. The samples will be a grab taken from sufficiently stabilized sludge and will be representative of the sludge that is land applied. The metals and nutrients analysis shall include the following parameters (the ceiling concentrations in mg/kg are in parentheses where applicable): Aluminum Mercury (57) Potassium Ammonia -Nitrogen Molybdenum (75) Selenium (100) Arsenic (75) Nickel (420) Silver Cadmium (85) Nitrate -Nitrite Nitrogen Sodium Calcium Percent Total Solids Sodium Adsorption Ratio (SAR) Copper (4,300) pH TKN Lead (840) Phosphorus Zinc (7,500) Magnesium Plant Available Nitrogen (by calculation) III. Pathogen Reduction The Pathogen Reduction shall be performed annually as specified in Attachment A of Permit No. WQ0001048. The samples will be grabs taken from sufficiently stabilized sludge and will be representative of the sludge that is land applied. The analyses will be Fecal Coliform monitoring and will meet the requirements in 15A NCAC 02T .1106 (c) Alternative (1). Seven samples will be collected over a 3 week period and analyzed using the MPN dilution method. The geometric mean fecal coliform density of these samples will be less than 2 million MPN per gram of biosolids (dry weight basis) in order to be land applied. The Fecal Coliform monitoring procedures were taken from the EPA.gov website/ENVIRONMENTAL REGULATIONS AND TECHNOLOGY/Control of Pathogens and Vector Attraction in Sewage Sludge (5.2) on February 26, 2015. IV. Vector Attraction Reduction The Vector Attraction Reduction shall be performed annually as specified in Attachment A of Permit No. WQ0001048. The samples will be grabs taken from sufficiently stabilized sludge and will be representative of the sludge that is land applied. The analyses will be the Specific Oxygen Uptake Rate (SOUR) and will meet the requirements in 15A NCAC 02T .1107 (a)(4). Seven samples will be collected over a 3 week period and analyzed using the acceptable SOUR test requirements. The average of the seven samples will be less than or equal to 1.5 mg of Oxygen per hour per gram of total sewage sludge solids (dry weight basis) at 20°C in order to be land applied. The Specific Oxygen Uptake Rate procedures were taken from the EPA.gov website/ENVIRONMENTAL REGULATIONS AND TECHNOLOGY/Control of Pathogens and Vector Attraction in Sewage Sludge (8.5) and the NCDENR.org website/Division of Water Resources/Non-Discharge Unit/Reporting Forms/Specific Oxygen Uptake Rate (SOUR) Testing Compliance on February 26, 2015. V. Soils Analysis As per Section IV. (5) of Permit No. WQ0001048 an annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on each land application site listed in Attachment B on which a residuals land application event will occur in the respective calendar year. This analysis shall be in accordance with the "Guidance on Soil Sampling" located in the Sampling Instructions section of the NC Department of Agriculture & Consumer Services' website (http://www.ncagr.gov/agronomi/pubs.htm). At a minimum the Standard Soil Fertility Analysis shall include the following parameters: Acidity Exchangeable Sodium Percentage Phosphorus Base Saturation (by calculation) Magnesium Potassium Calcium Manganese Sodium Cation Exchange Capacity Percent Humic Matter Zinc Copper pH VI. Groundwater Monitoring Wells There are five Monitoring Wells located on the sludge land application property. They are MW-9, MW- 10, MW-14, MW-15, MW-18. The Monitoring Wells will be sampled three times per year in February, June, and October for the following parameters (Groundwater Standards are in brackets where applicable): Water level, distance from measuring point Nitrogen, Ammonia Total (as N) [1500.00 ug/L] Coliform, Fecal MF, M-FC Broth, 44.5C Nitrogen, Nitrate Total (as N) [10.00 mg/L] Solids, Total Dissolved-180C [500.00 mg/L] Chromium, Total (as Cr) [10.00 ug/L] pH, lab Copper, Total (as Cu) [1.00 mg/L] Carbon, Total Organic (TOC) Volatile Compounds, (GC/MS) (October only) All Monitoring Well samples and analyses will be conducted according to the directions listed in Attachment C of the Contentnea MSD WWTP Land Application of Class B Residuals ((Von -Dedicated) Permit No. WQ0001048. r , j HCDENR North Carolina Department of Environment and Natural Resources Pat It/,.Crory Governor December 2, 2014 Charles Smithwick, District Manager Contentnea Metropolitan Sewerage District Post Office Box 477 Grifton, North Carolina 28530 Dear Mr. Smithwick: John E. Skvarla, III . Secretary, Subject: Permit No. WQ0001048 Contentnea MSD WWTP Land Application of Class B Residuals (Non -Dedicated) Pitt County In accordance with your permit application minor modification and renewal request received September 2, 2014, we are forwarding herewith Permit No. WQ0001048 dated December 2, 2014, to Contentnea Metropolitan Sewerage District for the continued operation of the subject residuals management program. Please note that this renewed permit shall become effective on February 1, 2015 (i.e. the day after the expiration date of the existing permit), which differs from the date of this letter. Modifications to the subject permit are as follows: The maximum dry tons have been decreased from 320 to 291. Acreage changes to Sites B, C and D because of new homes around application sites which resulted in redefined field boundaries or updated GIS mapping techniques for fields. Deleted Site CMSD2 Fields 1,3,4,5, and 9, and Site CMSD3 Fields 5, 6, 7, 9 and 11 totaling 89.96 acres. This permit shall be effective from February 1, 2015 until January 31, 2020, shall void Permit No. WQ0001048 issued February 18, 2008 and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring requirements listed in Attachments A and C for they may differ from the previous permit issuance. Failure to establish.an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. Please note the following permit conditions and attachmei►ts' are new since the last permit issuance dated February 18, 2008: Condition 1.2. — This condition requires that the Permittee to be in compliance with the signage requirements established in Condition 1H.13. prior to land application. Non -Discharge PenTOing Unit 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Phone: 919-807-M41 Internet: htt01oortalmdenr.orghveb4o An Equal Opporlunily 1 Affirmative Aclion Employer - Made in part with recycled paper (C) a description of the system used to monitor the air for methane gas in the air in any structures within the surface disposal unit boundary and at the property line of the surface disposal unit, if applicable; (D) a discussion of how public access to the surface disposal unit will be restricted; and (E) proof that the deed for the surface disposal unit property has been amended to provide permanent written notification to subsequent owners of the property that the property was used for the purposes of operating a surface disposal unit. History Note: Authority G.S. 143-115,1; 143-215.3(a); E, ff. September 1, 2006. 15A NCAC 02T.1110 OPERATION AND MAINTENANCE PLAN An Operation and Maintenance Plan shall be maintained for all residuals management programs. The plan shall: (1) describe the operation of the program and any associated facilities and equipment in sufficientdetailto show what operations are necessary for the program to function and by whom the functions areto be conducted; (2) describe anticipated maintenance of facilities and equipment that are associated with the program. (3) include provisions for safety measures including restriction of access to the site and equipment, as appropriate; (4) include spill control provisions including: (a) response to upsets and bypasses including control, containment, and remediation; and (b) contact information for program personnel, emergency responders, and regulatory agencies; (5) detail procedures forsampling and monitoring to ensure that the programstays in corrpliancewiththis Section and any issued permit; and (6) for surface disposal units, detail procedures for post -closure care management. History Note: Authority G.S. 143-215.1; 143-215.3(a); E,ff. September 1, 2006. 15A NCAC 02T .1111 MONITORING AND REPORTING (a) Representative samples of residuals that are prepared for application to the land or placed in a surface disposalunit shall be collected and analyzed. (b) The analytical methods listed in 40 CFR 503.8(b) as stated on January 1,1996 shall be incorporated into this Section by reference. (c) Residuals applied to the land orplaced in a surface disposal unit shall be monitored forpollutants as listed in Rule .l 105(a) and Rule .1105(d) of this Section as well as Rule .1106 and Rule .1107 as applicable at the Fequency as stipulated in the following: Metric Tons per 365 day period Monitoring Frequency (Dry Weight Basis) Greater than zero but less than 290 Once per year Equal to or greater than 290 but less than 1,500 Once per quarter (four times per year) Equal to or greater than 1,500 but less than 15,000 Once per 60 days (sixtimes per year) Equal to or greater than 15,000 Once per month (12 times per year) (d) A report of all monitoring and reporting requirements as specified in the permit shall be submitted to thebivision by the permittee annually on or before March 1st of each calendar year. (e) All records shall be retained for a minimum o f five years. HistoiyNote: Authority G.S. 143-215.1; 143-215.3(a); E .ff September 1, 2006. SECTION .1200 — COAL COMBUSTION PRODUCTS MANAGEMENT NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH LAND APPLICATION OF CLASS B RESIDUALS PERMIT (NON -DEDICATED) In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO C®ntentnea Metropolitan Sewerage District Pitt County FOR THE continued operation of a.residuals management program for Contentnea Metropolitan Sewerage District and consisting of the land application of Class B residuals generated by the approved facilities listed in Attachment A to the approved sites listed in Attachment B with no discharge of wastes to surface waters, pursuant to the application received September 2, 2014, and in conformity with and other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 503. This permit does not exempt the Permittee from complying with the federal regulations. This permit shall be effective from February 1, 2015 until January 31, 2020 shall void Permit No. WQ0001048 issued February 18, 2008 and shall be subject to the following specified conditions and limitations: L SCHEDULES No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem; appropriate. Please note Rule 15A NCAC 02T .0105(d) requires an updated site map to be,. suhmitted with the permit renewal application. 2. The permittee shall be in full compliance with the regional office notification requirements established in Condition 111.3. by March 1, 2015. 3. The permittee shall be in full compliance with the signage requirements established in Condition 1I1.13. by June 1, 2015. WQ0001048 Version 3.0 Shell Version 141027 Page J of 12 9. Setbacks for treatment and storage facilities shall be as follows: Setback Description Setback feet Habitable residence or place of public assembly under separate ownership or not to be maintained as art of the project site 100 Property lines 50 Private or public water supply 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and wetlands 50 Wells with exception to monitoring wells 100 10. Setbacks for Class B land application sites shall be as follows: Setback by application type (feet) Setback Description Vehicular Irrigation Surface Surface Injection J Application Application corporation Habitable residence or place of public assembly under separate ownership or not to be maintained as 400 400 200 art of the project site Habitable residence or places of public assembly owned by the Permittee, the owner of the land, or the lessee/operator of the land to be maintained as part 0 200 0 of the project site Property lines 50 150 50 Public right of way 50 50 50 Private or public water supply 100 100 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and wetlands) 100 100 50 Surface water diversions (ephemeral streams, waterways, ditches) 25 100 25 Groundwater lowering ditches (where the bottom of the ditch intersects the SHWT) 25 100 25 Subsurface groundwater lowering system 0 100 0 Wells with exception to monitoring wells .1010 u. 100 100 Bedrock outcrops 25 25 25 Top of slope of embankments or cuts of two feet or " more in vertical height 15 15 15 Building foundations or basements 0 15 0 Water lines 0 10 0 Swimming pools 100 100 100 Nitrification fields 0 20 0 11. Land application areas shall be clearly marked on each site prior to and during any residuals application event. WQ0001048 Version 3.0 Shell Version 141027 Page 3 of 12 17. In accordance with 15A NCAC 02L .0108, the review boundary shall be established midway between the compliance boundary and the residual land application area. Any exceedance of groundwater standards at the review boundary shall require action in accordance with 15A NCAC 02L .0106. ffi. OPERATION AND MAINTENANCE REOUIREMENTS L The residuals management program shall be properly maintained and operated at all times. The program shall be effectively maintained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. 2. The Washington Regional Office, telephone number (252) 946-6481, and the appropriate local government official (i.e., county manager, city manager, or health director) shall be notified at least 48 hours prior to the initial residuals land application to any new land application site. Notification to the regional supervisor shall be made from 8:00 a.m. until 5:00 p.m. on Monday through Friday, excluding State Holidays. 3. The Washington Regional Office shall be notified via email or telephone, (252) 946-6481, at least 24 hours prior to conducting any land application activity. Such notification shall indicate, at a minimum, the anticipated application times, field IDs, and location of land application activities. If it becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be notified prior to commencing the application to those fields. 4. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) pursuant to 15A NCAC 02T .1 110. Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan, at the minimum, shall include: a) Operational functions; b) Maintenance schedules; c) Safety measures; d) Spill response plan; e) Inspection plan including the following information: L Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f) Sampling and monitoring plan including the following information: i. Names and/or titles of personnel responsible for conducting -the sampling and monitoring; ii. Detailed description of monitoring procedures including: parameters to be monitored; iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have. an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). WQ0001048 Version 3.0 Shell Version 141027 psva S of 1 k. If the vertical separation of bedrock and the depth of residuals application is less than one foot; 12. The following public access restrictions apply to residual land application sites: a. Public access to public contact sites (e.g., golf courses, parks, ball fields, etc.) shall be restricted for 365 days after a residuals land application event; b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land application event. 13. Public access controls shall include the posting of signs with a minimum area of 3 square feet (e.g., 1.5' x 2'). Each sign shall indicate the activities conducted at each site, permit number, and name and contact information, including the Permittee or applicator's telephone number. Signs shall be posted in a clearly visible and conspicuous manner at the entrance to each land application site during a land application event, and for as long as the public access restrictions required under III.12 apply. 14. The following harvesting and grazing restrictions apply to residual land application sites after each land application event: Harvesting and Grazing Description cted iDuration Duration Animals shall not be allowed to graze during land application activities and restricted period. Sites that are to be used for grazing shall have fencing to 30 days prevent access after each land application event. Food crops, feed crops and fiber crops shall not be harvested for: 30 days Turf grown on land where residuals have been applied shall not be harvested for: 12 months Food crops with harvested parts that touch the residual/soil mixture and are totally above the land surface (e.g., tobacco, melons, cucumbers, squash, etc.) 14 months shall not be harvested for: When the residuals remain on the land surface for four months or longer prior to incorporation into the soil, food crops with harvested parts below the land 20 months surface (e.g., root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for: When the residuals remain on the land surface for less than four months prior to incorporation into the soil, food crops with harvested parts below the land 3 $ months surface shall not be harvested for: 15. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume of other nutrient sources (i.e., manufactured fertilizers, manures,) or other animal waste products) that have been applied to the site, and a copy of the most recent Ntrient Management Plan (NMP) for those operations where a NMP is required by the US Department of Agriculture — National Resources Conservation Service (MRCS) or other State Agencies. The' Permittee shall calculate allowable nutrient loading rates based on the provided information and use appropriate reductions. For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan (WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient Management Plan. 16. No residuals shall be land applied unless the submitted Land Owner Agreement Attachment (LOAA) between the Permittee and landowners or lessees/operators of the land application site is in full force and effect. These agreements shall be considered expired concurrent with the permit expiration date, and shall be renewed during the permit renewal process. WQ0001048 Version 3.0 Shell Version 141027 Page 7 of 12 4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class B pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (c) and one vector attraction reduction requirement in 15A NCAC 02T .1107 (a) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. 5. An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on each land application site listed in Attachment B on which a residuals land application event will occur in the respective calendar year. This analysis shall be in accordance with the "Guidance on Soil Sampling" located in the Sampling Instiuctions section of the NC Department of Agriculture & Consumer Services' website(littp://w;vw.licagl'.gov/agrorionii/pubs.litm). The Permittee shall maintain these results and a description of the sampling methodologies used to determine soil fertility for a period of no less than five years, and shall be made available to the Division upon request. At a minimum, the Standard Soil Fertility Analysis shall include the following parameters: Acidity Exchangeable Sodium Percentage Phosphorus Base Saturation (by calculation) Magnesium Potassium Calcium Manganese Sodium Cation Exchange Capacity Percent Humic Matter Zinc Copper pH 6. Laboratory parameter analyses shall be performed on the residuals as they are land applied, and shall be in accordance with the monitoring requirements in 15A NCAC 02B .0505. 7. Monitor wells shall be sampled after construction and within three months prior to initiating residual application operations. Monitoring wells shall be sampled thereafter at the frequencies and for the parameters specified in Attachment C. All mapping, well construction forms, well abandonment forms and monitoring data shall refer to the permit number and the well nomenclature as vrovided_in Attachment C. 8. For initial sampling of monitoring wells, the Permittee shall submit a Compliance Monitoring Form (GW-59) and a Well Construction Record Form (GW-1) listing this permit , number and the appropriate monitoring well identification number. Initial Compliance Monitoring Forms (GW-59) without copies of the Well Construction Record Forms (GW-1) are deemed incomplete, and may be returned to the Permittee without being processed. 9. Two copies of the monitoring well sampling and analysis results shall be submitted on a Compliance Monitoring Form (GW-59), along with attached copies of laboratory analyses, on or before the last working day of the month following the sampling month. The Compliance Monitoring Form (GW- 59) shall include this permit number, the appropriate well identification number, and one GW-59a certification form shall be submitted with each set of samplingiresults. All information shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 WQ0001048 Version 3.0 Shell Version 141027 Paee 9 .of 12 d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment. e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to be taken to ensure that the problem does not recur. V. INSPECTIONS 1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan. 2. Prior to each bulk residuals land application event, the Permittee or his designee shall inspect the residuals storage, transport and application facilities to prevent malfunctions, facility deterioration and operator errors resulting in discharges, which may cause the release of wastes to the environment, a threat to human health or a public nuisance. The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. 3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the land application sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples. YI. GENERAL CONDITIONS 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143- 215.6A to 143-215.6C. 2. This permit shall become voidable if the residuals land application events are not carried out in accordance with the conditions of this permit. 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation. 4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes, rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCG010000; any requirements pertaining to wetlands under 15A NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. WQ0001048 Version 3.0 Shell Version 141027 Paae 11 of 12 ATTACEI , , f A -Approved Residual Sources Contentnea Metropolitan Sewerage District Certification Date: December 2, 2014 Permit Number! WQ0001041 Vevdaly 1-0 Maximum Monitoring Monitoring Monitoring Frequency for Approved Owner Facility Name County Permit Biological Dry Tons Frequency for Frequency for Pathogen & Mineralization Number Residuals Per Year r Non-hazardous Metals and Vector Attraction Rate Characteristics Nutrients Reductions°'S Co Metropolitan Co tentnea Sewer Sewera a District Sewerage Sewera a District WWTP Pitt NC0032077 Yes 291 Annually Annually Annually 0.30 r- Total 291 1. Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility. 2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2. 3. Testing of metals and nutrients as stipulated under permit Condition IV.3. 4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IVA. 5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above. Dry Tons Generated short tons per ear(Established Monitoring Frequency in 40 CFR 503 and 15A NCAC 02T .1111 <319 1/Year =>319 - <1,650 1/ Quarter 4 times per year =>1 650 - <16,500 1/60 Days 6 times per ear >16,500 1/month 12 times per year If no land application events occur during a required sampling period (e.g. no land application occur during an entire year when annual monitoring is required), then no sampling data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification. Page 1 of 1 ATTACHN. iT B - Approved Land Application Sites Contentnea Metropolitan Sewerage District Certification Date: December 2, 2014 Permit Number: WQ0001048 Version: 3.0 Field/ Site Owner Lessee County Latitude Longitude Net Acrea e Dominant Soil Series Footnotes B-1 Contentnea Metropolitan Sewerage District Mills Creston Pitt 350 21' 26" 770 24' 58" 2.84 Portsmouth B-2 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 26" 7702415811 2.62 Pactolus B-3 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 35' 21' 26" 770 24' 58" 2.72 Portsmouth B-4 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 26" 7702415811 3.34 Pactolus B-5 Cbntentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 26" 770 24' 58" 3.74 Pactolus B-6 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 26" 77" 24' 58" 2.48 Chipley B-7 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 26" 77" 24' 58" 1.32 Chipley CI-10 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 3502210011 770 25' 03" 8.55 Alaga CII-8 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 22' 03" 770 25' 05" 7.73 Alaga CII-9 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 22' 03" 77" 25' 05" 5.15 Alaga CII-13 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 22' 03" 770 25' 05" 3.30 Ocilla CIU-12 Contentnea Metropolitan Sewerage District Mills, Creston Pitt 350 21' 48" 770 24' 57" 5.23 Osier CIV-I I Contentnea Metropolitan Sewerage District Mills, Creston Pitt 35" 21' 50" 77' 24' 52" 5.13 Osier D-14 Gaskins, Michael Mills, Creston Pitt 350 21' 40" 770 24' 42" 3.00 Portsmouth D-15 Gasldns, Michael Mills, Creston Pitt 350 21' 40" 770 24' 42" 2.38 Portsmouth D-16 Gaskins, Michael Mills, Creston Pitt 350 21' 40" 7702414211 2.98 Alaga D-17 Gaskins, Michael Mills, Creston Pitt 350 21' 40" 770 24' 42" 3.62 Alaga D-18 Gaskins, Michael Mills, Creston Pitt 350 21' 40" 770 24' 42" 2.42 Pactolus 7Cota1 68.55 Page 1 of I ATTACMk -- T C — Groundwater Monitoring and Limitations Contentnea Metropolitan Sewerage District Monitoring wells: MW-9, MW-10, AM-14, MW-15, MW-18 Permit Number: WQ0001048 Version: 3.0 GROUNDWATER CHARACTERISTICS GROUNDWATER STANDARDS MONITORING REQUIREMENTS PCS Code Parameter Description Daily Maximum Frequency Measurement Sample Type Footnotes 82546 Water level, distance from measuring point feet 3 x year Calculated 1,2,3,7 31616 Coliform, Fecal MF, M-FC Broth,44.5C 41100m1 3 x year Grab 1,7 70300 Solids, Total Dissolved- 180 Deg.0 500.00 mg/l 3 x year Grab 1,7 00403 Ph, lab S.U. 3 x year Grab 1,7 . 00680 Carbon, Tot Organic (TOC) mg/l 3 x year Grab 1,6,7 00610 Nitrogen, Ammonia Total (as N) 1,500.00 µg/1 3 x year Grab 1,7 00620 Nitrogen, Nitrate Total (as N) 10.00 mg/l 3 x year Grab 1,7 01034 Chromium, Total (as Cr) 10.00 99/1 3 x year Grab 1,7 01042 Copper, Total (as Cu) 1.00 mg/l 3 x year Grab 1,7 78732 Volatile Compounds, (GC/MS) mg/1 Annually Grab 1,4,5,7 a,,.s auau uu wiauu%;Lcu uu rourutuy June ix ucwDcr; Annuai monitormg snail De connuctec eVeryUCtober. 2. The measurement of water levels shall be made prior to purging the wells. The depth to water in each weII shall be measured from the surveyed point on the top of the casing. The measurement of pIi shall be made after purging and prior to sampling for the remaining parameters. 3. The measuring points (top of well casing) of all monitoring wells shall be surveyed to provide the relative elevation of the measuring point for each monitoring well. The measuring points (top of casing) of all monitoring wells shall be surveyed relative to a common datum. 4. Volatile Organic Compounds (VOC) - In November only, analyze by one of the following methods: a. Standard Method 62301), PQL at 0.5 µg/L or less b. Standard Method 6210D, PQL at 0.5 µg/L or less c. EPA Method 8021, Low Concentration, PQL at 0.5 µg/L or less d. EPA Method 8260, Low Concentration, PQL at 0.5 µg/L or less e. Another method with prior approval by the Water Quality Permitting Section Chief Any method used must meet the following qualifications: a. A laboratory must be DWQ certified to run any method used. b. The method used must, at a minimum, include all the constituents listed in Table VHI of Standard Method 6230D. c. The method used must provide a PQL of 0.5 µg/L or less that must be supported by laboratory proficiency studies as required by the DWQ Laboratory Certification Unit. Any constituents detected above the MDL but below the PQL of 0.5 µg/L must be qualified (estimated) and reported. 5. If any volatile organic compounds (VOC) are detected as a result of monitoring as provided in Attachment C, then the Washington Regional Office supervisor, telephone number (252) 946-6481, must be contacted immediately for further instructions regarding any additional follow-up analyses required. 6. If TOC concentrations greater than 10 mg/1 are detected in any downgradient monitoring well, additional sampling and analysis must be conducted to identify the individual constituents comprising this TOC concentration. If the TOC concentration as measured in the background monitor well exceeds 10 mg/l, this concentration will be taken to represent the naturally occurring TOC concentration. Any exceedances of this naturally occurring TOC concentration in the downgradient wells shall be subject to the additional sampling and analysis as described above. 7. Monitoring wells shall be reported consistent with the nomenclature and location information provided in this attachment. Page 1 of 1 V ,4 DE}.h1DN COfy7'ThTNL�IC'hiB1ROi'O `V-*1 .. ��4 ... ' � � �w:: t - ��'�'� • � �> i,� �'� '� ' •sty , 19 8 Gress Ac"� ��- �,.. PRANC_IN COIBrb ( HrYYbTANe CRAIG u. RAHAAI F _AN CpINE? i � 513 NWAC W' CHt1•Rt,SRAI,''573 et, .c ;z.4 Road r 6: 0 Yros Ac. 3.17'Gross ORCOT"r 8 rs QN JR }fEhRS a 3. 3 Gross C. 4. A 1tsNDA GABDNE I 3:32�Gr�o's HARRIS =.QNTENTNEA METRO 5 d SEWAGE r 4 3 }. , ' ► 2 MW�10 3.74 Net Ac. i0lV BRUCE ANNON JR- CO N1 ENTNEA DIETROPO -1TAN SEWAGE 3934 Net Ac. 2.62 NeAll t l,c. N '8 fTOs SI�T'Ej,Ba 2.72NetAc. WNOF.:.. Legend �GRIFPON 2.84 Net _x 2S2$ G os _ c ® HOUSe vtlRi.t31"r — i 250 Gross Ac. Monitor Well d r ,� r_•,. _..._ pitch e3 7 '. v 2.48 Net Arc. Stream v Building Field Boundar �' `PAS'IONM "A'6"` MVV--9 Machine Net Area C' NTENTrti►M§TROFOL�� ` Machine Buffer SfiWAGf+ f T� s 1 F Pond a 150 y300 600 L s. Property Boundary � - Feet - �.�.�:�e t , - � ;n" :-<�"•; � i � ;. �•h ' ;, •"?`�i � � �` � - `�` is t ': ' " i ' �t :ale: 1 inch = 300 feet SITE B BUFFER MAP. FIELDS 1. 7 FIGURE Drawn By: CSC c Y . ^us CW10 CLASS B LAND APPLIC:1TION Reviewed By: Cliss B Permit W rQ0001043 6 Date: Aug'14 Soil Plus Proiect # 200710.A 10 v � 4 �' .�d� T tij'• �.Vf � �� „ `�' .R" 3''�� �::�.� t�if �"kx. �' . 2 w ' 1 ^. '�F Al 3c3D Gross C. ` ` r ib y, Y f: �•% 4 k i I t 3.30 Net Ac. ITEAA �C II 1# DEMON 3COfVTEN�r GAt1>\iETROPQLiTAN`',,' :�, ,� 'P�, " . �_. q•� 6�`64,�G oss Ac },bIAR1AN NELSON,• ;t -x 3SIT� 14 lit a s r `{'rGfLSON' 74 A3 C .1r 298 Net A iin CHRLES RAN_g 13 NetAc23rNet�Ac s. F RFl►VES '�,� . � '" � r �s. A3,62 Net Ac. z5r LAUFiA a GARIt.: s , k vas tsuhi TRuS'CCE- : 17 AC. Gros A i Legend i.ALI�i E,cup House sCNTENTNEA METRQPOLIT' rr I Wues G a Monitor Well V y: SEWAGE Ditch Stream Building CIE E, r Field Boundary t xS Mi, r - 2#� Machine Net Area 72Ne Ac: %7 �r Machine Buffer L84 Net c. :....�+, mot. Fond T X i t 0 150 300 600 a Properly Bourd ary 30 GrossTwFul .;'.ale: 1 inch = 300 feet SITE C III & IV BUFFER MAP FIGURE Drawn By: CSC _ ? k� CdISD C-A S B LAND APPLIC,k1`IO: Reviewed By: SW ME. / Class B Permit WQ0001048 Date:.Aug'14 jSoil Plus Project # 200710.A10 w 1. NT �+ l E MARIAN NELSON h1ICHAFL E AiC1,Al4IIORIV GASK .191 r 3 lr �a -11 t sq NIELS ON i. WHORN 3.00 Nei C. " r a 0-1 Alr 1q 4.21 cross C u TIANtNELSON ¢ A•ICwwFiORIV , � ' . "'� 2.38 Net Ac: L 15 2.78 Gross C. 2.98 Net Ac, I� 1G 3.37 Gross Ac, 4 MICH AFL E 3.62 Net Ac. GASKJN5 0 ?` a 6.69 Gross Ac, x SUll. D 17 _.. LA 1JRA�BmGARRIS ,�'IG 1-RUSTIM 2?42Net c. MICHAELE P G�ASK•INS - GASKINS _ ..m 18 " BF AAJ1N bIIGHAEL f' L r 7:18'Gross Ac. i , Legend i �'CLYDE L,.. INW-IS i_ IArRBROUGH III 7 House i� - Jrt *�- AI >~RB nY:G.rs BMonitor Well IJG5TON Ditch I i BERTRAY 4 e ; LANGS7ON Stream s° Building , 1"t = r . , J9 id e Boundary ' Field :a Machine Net Area I Machine Buffer Pond +I �0 150 300 600 j a Property Boundarymoml Fe J :ale: I melt T 300 feet SITE D BUFFER MAP FIELD FIELDS u -18 FIGURE Drawn By: CSC SOTC:IISD CLASS B LAND APPLICATION Reviewed By., U, S Class B Pernut NVQ0001048 Date:.Aug `1 4 Soil. Plus Project # 200710.A10 j DWR Division of %Vater Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted. the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Contentnea Metropolitan Sewerage District Status Code.Current Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year n Proposed R Contentnea Metropolitan Sewerage District Contentnea Metropolitan Sewerage District Wastewater Treatment Plant Pitt NCO032077 291 291 Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (Le, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 [P I_jL , j Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Contentnea Metropolitan Sewerage District Wastewater Treatment Plant 2. Facility permit holder is: Federal, 13 State, Is Local Government, or 0 Private. Facility permit issued by: Div. of Water Resources, 13 Div. of Environmental Health, or Other (explain: 3. Facility contact person and title: Charles Smithwick, Jr., District Manager Complete mailing address: PO Box 477 City: Grifton State: NC Zip: 28530 Telephone number: (252) 524-5584 E-mail address: crosd100na,embaMmail.com 4. Facility physical address: 900 Wiley Gaskins Rd. City: Grifton State: NC Zip: 28530 Coordinates: Latitude: 35' 21' 36.7" Longitude: 77° 24' 57.6" Datum: NAD83 Level of accuracy: 1/100 Method of measurement: UTM 5. Purpose of the facility: ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, ® treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: 1_1 % industrial and 98.9 % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: IS Yes IN No 7. Facility permitted/design flow: 3_5 MGD and facility average daily flow: 2.25 MGD 8. Average amount of residuals being generated at this facility 69.061 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Aerobic Stabilization/Storage Facilities (total volume: 2,655,600 gallons) Type and volume of residuals storage (i.e., outside of residuals treatment units): Sludge Drying Beds II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or ❑ 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ll Biological ❑ Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that tr 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: SGS North America Inc. and Date of analysis: 04/04/2019 - 04/11/2019 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: >200 °F (> 140°F) Passed reactivity test: ® yes ❑ no. HCN: <87 mg/kg (<250) & HZS: <2900 mg/kg (MCL 2900 mg/ke) (<500) TCLP Parameter Limit (mg/1) Result (mg/1) TCLP Parameter Limit (mg/1) Result (mg/1) Arsenic 5.0 <0.10 Hexachlorobenzene 0.13 ND Barium 100.0 <2.0 Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 <0.050 Lead 5.0 <0.050 Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 <0.0050 Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 <0.10 Nitrobenzene 2.0 ND m-Cresol 200.0 Pentachlorophenol 100.0 ND o-Cresol 200.0 Pyridine 5.0 ND p-Cresol 200.0 Selenium 1.0 <0.10 Cresol 200.0 Silver 5.0 <0.10 2,4-D 10.0 ND Tetrachloroethylene 0.7 0.0235 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1,1-Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Environment 1, Inc. and Date of analysis: 04/16/2018 — 04/23/2018 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 <2.5 Cadmium 85 39 1.1 Copper 4,300 1,500 247 Lead 840 300 18 Mercury 57 17 0.49 Molybdenum 75 n/a <5.0 Nickel 420 420 13 Selenium 100 100 <5.0 Zinc 7,500 2,800 651 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: IM and Date of analysis: ={.'fir Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 1.73 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient ai,u micronutrient parameters: Laboratory: Environment 1, Inc. and Date of analysis: 4/10/2018 to 5/31/2019 Parameter Result (mg1w Aluminum 17,916 Ammonia -Nitrogen 788 Calcium 16,099 Magnesium 4,632 Nitrate -Nitrite Nitrogen 12,950.98 pH (Standard Unit) 3.9 Phosphorus 27,260 Potassium 7,225 Sodium 3,163 Total Kjeldahl Nitrogen 39,930 c. Using the results listed in Item Il. 5b. above, calculate the sodium adsorption ration (SAR): 0.' [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (0) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 26,231 38,311 Injection/Incorporation 26,625 38,705 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, M heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: ® Alternative l [l5A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. ® Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: Z aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, or N lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item I1. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item Il. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ® Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ® Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. ® Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. ® Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. ® Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of Contentnea Metropolitan Sewerage District 2019 Residuals Land Application Permit Renewal Items for B. Residuals S ource- GeneratingFacility Information Vicinity Map CMSD WWTP Process Diagram Residuals Production Documentation Sampling and Monitoring Plan Legend � , Vicinity Map Stream CMSD Class B Land Application — NC Route _WOOTENCOMPANY Permit WQ0001048 Renewal 0 Field Boundary anc Qi1 UfBfi 9f VBrtd]ii'i-"ie:v�l11FJ PY..»i1C.'H.,.r.�AtlPY[iC L�TMy Pitt County, NC Municipal Boundary �:o�aJcc�v+mmaumeeaiac�ma�n`>rKfro�»mo,wwr.ao,eremm.� n�, �UV n agl�l un0 ,.rJ by Wu-__J Ni�M1s;W�ul Lyc JwwY - 'k.ffi: WR,tl Ve County Boundary Sodium Hydroxide Feed DISTRIB BOX gg gg ttoo tas Mc01 Spray�ield Chlo ne caustic LONTRO NITS 9UILgNG IARMERSYOLL BE LEGEND O — STRUCTURE EXIsxNG s1RUCiuRE E`E=E PIPE MOgFIED smUCTURE OMOOKIED SmUCNRE IRRIGRTpx uxE U. MODI AYERAOE I N', FLaysln FLOW SPILITER BOX Decant Return � NEW NEW CLARR'IE= CLA-l'N 100 ��l D. F55 4 SLUDGE OADON N STA ON I j AEROBIL SLUDGE Anoxic Tanks Anoxic Tanks STABILIUTION/ HOLDING TANKS Sludge Recirculatlon v IN. SI►\ M. ND I �IA#STAG 10 FIRST BTAGE CLARIFIER SDGE NO.IRECIRC. IPUMP k��AE.RAnOl Not¢ � I w S UDGE r� RELIRCUlAT1ONI WASTE PUMP DRAIN STATNON PUMP STATION O DENTIRIFICATION FILTER SYSTEM ULTRAVIOLET DISINFECTION BELT FILTER PRESS METHANOL BUILDING STORAGE& FEED FACILITY FILTER LIFT STATI Drain � SS `"" 5L100E ft ulatlon To Sprayfiald t —7 Chlorine 1 — Drain AEROBIC DIGESTER 1 Y Y L NO, tER AECOND RATION ASI AERATION BASIN NR t � F" SECOND STAGE '. AERATON BASIN No 2 1 slt- o SCHEMATIC FLOW DIAGRAM CMSD WASTEWATER TREATMENT PLANT SECOND STAGE sLUDDE IFLIRCUI ATION PUMP STATION 4 LE BBDM EFFLENT OUTFALL r MWATER 4NNEL u r v THE WOOTEN COMPANY NY12/0 N'th fto1, Rv¢nReNRakigh NG 21953-A29 u R 9I9.R2P.9531 tR1919 MC3589 Contentnea Metropolitan Sewerage District Estimated Waste Sludge Production Estimate Average Influent and Effluent BOD for 2018 WWTP Recorded Values Influent BOD Effluent BOD Flow Month (mg/L) (mg/L) (MGD) January 123.57 3.54 2.36 February 101.79 2.41 2.41 March 87.95 2.17 2.28 April 86.41 2.03 2.27 May 86.88 2.00 2.01 June 85.45 2.05 1.62 July 85.12 2.07 1.64 August 58.50 2.29 2.36 September 79.68 2.09 3.39 October 86.55 2.23 1.68 November 90.14 2.15 2.00 December 67.07 2.20 3.04 Annual Averagel 86.59 1 2.27 1 2.26 Calculate Total Annual Solids Produced 2018 Values Design Flow (MGD) 2.26 3.5 Influent BOD (mg/L) 86.59 250 Effluent BOD (mg/L) 2.27 15 Net Sludge Yield 0.35 lb solids/lb BOD Removed Waste Sludge Production = MWs = (BODin - BODEff)(8.34)(Q)(NetSludgeYield) 2018 Values Design Waste Sludge Production = 555 2,401 lb/day Aerobic Stabilization (assuming 40% volatile solids reduction in aerobic sludge digestion) VSS/TSS Ratio 0.8 VSS/TSS Reduction of Volatile Solid,, 0.4 VS VSS Aerobic Sludge Produced = MWs TSS (1 - VS) - Mws I 1 - TSS) 2018 Values Design Aerobic Sludge Produced = 377 1,633 lb/day 69 298 dry ton/yr Contentnea Metropolitan Sewerage District 2018 Actual Waste Sludge Applied (data from Land Application Field Summary Reports in supporting information) Total Dry Dry Tons Tons Site Field Applied (gal) % Solids (tn/ac) Acres Applied B 1 93,000 1.73 2.362 2.84 6.71 B 2 44,000 1.73 1.211 2.62 3.17 B 3 88,600 1.73 2.35 2.72 6.39 B 4 46,200 1.73 0.998 3.34 3.33 B 5 75,000 1.73 1.446 3.74 5.41 C 11 8 208,200 1.73 1.943 7.73 15.02 C 11 9 104,000 1.73 1.457 5.15 7.50 C 11 13 30,800 1.73 0.673 3.3 2.22 C H 15 90,000 1.73 2.728 2.38 6.49 D 16 48,000 1.73 1.162 2.98 3.46 D 17 72,000 1.73 1.435 3.62 5.19 D 19 57,500 1.73 0.353 11.75 4.15 Total Applied Total Dry Volume (gal) Tons Applied 957,300 69.1 LAN® APPLICATION FIELD SUMMARY FORMS ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Obn-Ve�ea, (f 6D WQ Permit #: Field #: {,��;�ppjCl}� Acres Utilized: El,Q(I Land Owner: jy�� _ Annual Dry Tons Applied: 6 7�j Site #: Acres Permitted: Z (� Operator: ��e�),(yI Predominant Soil Series: Cation Exchange Capacity (non 503): Crop 1 Name: CPaJta(5-JfPt&L- Crop 1 Max. PAN: n(p Crop 2 Name: Crop 2 Max. PAN: _ ° v c ° Ca Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (DryTons/Ac) Residual Sources (NPDES #, WQ#, Fen., Animal Waste, etc) Soil Cond. (Dry, Wet,x Moist Precip. Past 24 its. inches > � b E ' o in �; * ° o °� * N' * K TKN mg/kg z Y -� o 3 °; w' mg/kg Nitrate and Nitrite mg/kg PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 QaU . .3-)Z C3, 5 CD,36 7Sg Z9 71:7(� ber 000 1 1.739k 16. Qqb 320-n 0 a "'o Z Z : Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: As Cd Cu Cr Pb H Mo Ni Se Zn P Z3 �IIZ Lime A Iied Annual Ibs/acre ,pI t.l(o7 O-U62 5 Z p.{�Zu D-Z 6�U Z .77b .. . , . ..:' Date lbs/ac Prior Years Cumulative lbs/ac , l4g3 ,(4c 04-)q c 'J,4 I Current Cumulative lbs/ac , 505 ,' l .3b� L.4�3 Z� [a `3 21 Permitted C. P. L. R.**** (', 3U i 3N— 037yI Permit PAN Limit lst/2nd Crop :.:: .. ..... . ......... . "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incorvoration - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: O pnieN-nen— 6D Total Dray Tons Applied (Annual): „ Permit #: i�:QCLOjOLAI 2 Cation Exchange Capacity (non 503 only): L/, 5 Operator: ' enet dyjqkl Owner: Crnif4noQ_mb_D Predominant Soil Series: {�-j6lTy L -) Acres Used: Z. � c) Acres Permitted: Z Iq0 Site #: Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 6 7 8 9 10 11 12 % Solids Arsenic <Z. < Z. 5 Cadmium j 1.1 Copper Z Lo ZL7 Chromium j 7j 13 Lead j g is Mercury 44G% p , LP Molyb- de.num J. O Crj. () Nickel 1 l3 Selenium Zinc J (5I Total Phos- phorus &0 M,0 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Event MOW "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". -2 << Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: �bntn�06D WQ Permit #: V\40D0lC)(4z, Field #: Acres Utilized: z , (02 Land Owner: CU)-Ff -)4n _ ff)67 Annual Dry Tons Applied: J I")C...( Site #: l� Acres Permitted: Z , & Z Operator:'?)enet 6ry�o) Predominant Soil Series: ?acb1u5 Cation Exchange Capacity (non 503): Crop 1 Name: Crop 1 Max. PAN: IBC O Crop 2 Name: Cron 2 Max. PAN: o 0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (�ryTonslAc) Residual Sources (NPDES #, WQ#, Fert,Animal Waste, etc} Soil Cond. (Dry, Wet.n. Moist) Precip. Past 24 Hrs. inches c� t, o w o „ M c N' d - N M °, TKN mg/kg z o 3 °° ° g mpg Nitrate and Nitrite mgJkg PAN Applied lbs/acre ( ) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 • 214 � I(I 21 I ; :; 1�IC-CO370—P drNO S 0, 5 0:30 C6 X�b -n 5z9xxt� 5�0 j.ZI I Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: y40D(� ::::.:::::::: As Cd Cu I Cr Pb Hg Mo Ni Se Zn P 53('� Lime Applied Annual lbs/acre 0, 00I- 6-003 6 I 0(44 O=CD) 0.01 Z' U, l -0 Z 1. 0211` .. :: ::::::::::::::::::::: ..... ...........................•. :::::....::::::::::::::::::::::::::::.::.. . Date lbs/ac Prior Years Cumulative lbs/ac D • 3 (n 6.MZ 7G• 3u•Zl 3 7 •GDco p. Z ZG53 ZGS 5�1 Current Cumulative lbs/ac O• (oWL 0.OloS q4 ., 1,Z_44 4G50 F353 Z.QL-, .q , 7 Permitted C. P. L. R.** ** i3 3tI i3 — "� 15 -- y 4� Zy sr'. Permit PAN Limit l st/2nd Crop ..........:.:.:...:. 1 a --i ceruiy, unaer penalty of taw, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation �� ZZ **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: CbM0-) -ncz.jYl� Total Dry Tons Applied (Annual): 31 FXJ Permit #: Cation Exchange Capacity (non 503 only): Operator: Owner: rlflif'f?it')e:i-rf)L PredominantSoil Series: "jbCjpj()S Acres Used: Z; Z Acres Permitted: & z, Site it: "lField #: -Z Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/lcg, % Solids use Raw Percent #): Sample or Com- posite Date I 1 Lf 1p 1$ 2 3 4 5 6 7 8 9 10 i 1 12 % Solids 1.�3 Arsenic (Z. Cadmium 1.1 Copper 'jq-) Clu•omium 1 Lead is Mercury p.taG MolyU- demim <5.v Nickel 13 Selenium 5.0 Zuic (,61 Total Phos- horus IZ(c b Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Mom Total Phos- _phorusEEMENEEMENEEN "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z—� N L1 Signature of Land Applier Date DENR FORM MFLSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: C`rni•eNkl.cn. 0 CD Land Owner: CZn+1a)-.n-ff0- rfl-J-D Operator: 'h %6.Mlg41 Crop 1 Name: CO--L WQ Permit #: 4�OCC610 4!g Field #: 3 Acres Utilized: Z.'7 Z Annual Dry Tons Applied: l"-6 JZ ISite #: Acres Permitted: 7Z.'7 Z. Predominant Soil Series: �a 1 Cation Exchange Capacity (non 503): Crop i Max. PAN: I-Xo Crop 2 Name: Crop 2 Max. PAN: o Q -II-� - 5 Volume applied (enter one) Solids/ Liquid qu Cu. Yds Gallons 5ZWO txx� % Solids I.137b Volume Applied per Acre (Dry Tons/Ac) *Z 5 55' Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) NCcc&&U-7-) NCOG3ZD7� Soil Cond. (Dry, Wet Moist Precip. past 24 Hrs. inches ti ' o w a * $ C o z M' w _ � * o � 0 5 O.5 o » y * — 0 ❑ G,3b O< TKN mg/kg ,-)40 43lC: D 3 o 8 _ 5 �• mglkg . S' "X6�3xJ48 Nitrate and Nitrite mgncg /1gtAJ PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual $ Application Crop 1 •ICz? I Crop 2 Crop 1 oer Crop 2 .3'J0 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTAL s: Is . lo(�i3 ::<?:;:.::: As Cd Cu Cr Pb H Mo Ni Se Zn P IZ3,N3 Lime A lied Annual lbs/acre p iZ3 D- W5 l . l b l D, 0 - C84 '' , C 62 , - 4F . 1 , - u .05q 1 Z Date lbs/ac Prior Years Cumulative Ibs/ac ........................... p; `�j Z3Z �2.� 44. D .�T 0. 1 1"� 1G:357 , (u 13.f 1:::.:....:....:. ..:.:.:::.:.:.:;::::::::: p.'> �) Z37 3,gck tic{. 51 3 ZG13 Z•RW1. rO� Ui`3 Gt1t� ....................... . ;..; .;....:.:. z�14 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop 1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the. information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ft Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. In i ection/Incorno ration -1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Ccf)- O- .secL (`OD Total Dry Tons Applied (Annual): (,. ze Z Permit #: CCOIC Cation Exchange Capacity (non 503 only): (4. 5 Operator: ') 0��f �,Y tl's Owner: CC --ff j- neCL jf)b_0 Predominant Soil Series:.] Acres Used: z, iZ Acres Permitted: Z.-)Z Site #: ?) Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use rug/kg, % Solids use Raw Percent #): Sample or Com- posite Date I I olcr 19 2 t i�lD 1 3 A 5 6 7 8 9 10 11 j 12 % Solids Arsenic <1.'J Cadmium 1 1 . J 1 . Copper I 2q-) vo Chromium 13 13 Lead jg 11 Mercury D, LP p. UST Molyb-denurn Nickel 3 13 Selenium <5.D <5 D Zinc 1 (,, 51 Total Phos- phorus 7Jc0 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ®• r __________RIM Total Phos- _jhorus_NNEEEEEEEEEE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Q Signature of Land Applier - -Zwc jl Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: C1Cl_)+el t ►n(_� rf)6D WQ Permit #: i()L6 Field #: y Acres Utilized: 3.5(4 Land Owner: M-1) Annual Dry Tons Applied: 3.333 Site #: j; Acres Permitted: 3.3y Operator: ee j Predominant Soil Series: �QC }�}V g Cation Exchange Capacity (non 503): Crop 1 Name: Crop 1 Max. PAN: 1 Qn Crop 2 Name: Cron 2 Max. PAN: _ • � ° y Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied r PP per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist Precip. Past 24 Hrs. inches Y c; a o M ° o-r;' a C o � _ �; — * N ° 5 3 x d ro « N' c TKN0 mg/kg z a B o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( ibs/acre) Name of Crop Type Receiving Residual Application PP Crop 1 Crop 2 Crop 1 Crop 2 �7-►'� u(o20v I."73� O,Clgs NC.oL--ZCT- & S o,5 0:38 -'5wo "xsl x5�>•, (A Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: U' As Cd Cu Cr Pb Hg Mo Ni I Se Zn I P Z3 Lime Applied Annual Ibs/acre 0,CX)5 0.CC0 .WP3 O OZ(v 0 03L, I... Date lbs/ac Prior Years Cumulative lbs/ac p,-)3 U u•Rt5Z " •33) aQ-32J t43 C).t7(� Z.7 x1 7O.qZO Current Cumulative lbs/ac q.qi . 7Lt '? '7 0.17� Z'>rs� .bZ3 p: Permitted C. P. L. R.**** 134 13 — ZO i rj — 374 Zvi Permit PAN Limit 1 st/2nd Crop ....................... . . :::•: -..... ••1 certuy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation a i **Volatilization Rate: Surface - 0.5. Iniection/Incorooration -1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: d-�v)e�L MO-D Total Dry Tons Applied (Annual): 3.333 Permit #: L�,r4 OWiDp $ Cation Exchange Capacity (non 503 only): 4. 5 Operator: 'J jena \_'311dh Owner: �cn� l£ - � Predominant Soil Series: Acres Used: 3, Zu Acres Permitted: 3,3y Site #: 6 Field #: �! Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 11 2 3 4 5 6 7 8 9 1d 11 J 12 % Solids ) `7 Arsenic <-Z.5 Cadnlium I. j Copper I zq-) Chronliunl I Lead ) Mercury O qCj Molyb- <5. o Nickel Selenium Zinc Total Phos- phorus n7lpO Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Minn 0 NEW IIIIIIII Iff RIM Total Phos- phorusNEENEENEENEEN "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: rl n+ai )4 t. rn6D WQ Permit #: I,1�1645 Field #: 6 Acres Utilized: Land Owner: Cf'17Ffi?1RP O�_ f�17 Annual Dry Tons Applied: 5, Q) l Site #: r l Acres Permitted: 7� j Operator: Predominant Soil Series: C(C-b�US Cation Exchange Capacity (non 503): (4.-5 Crop 1 Name: CC0t,:5+ C.c. Crop 1 Max. PAN: i(2 `, CroD 2 Name: rrnn l Mr , PAN. o c 0 i-1�' Z Volume applied (enter one) Solids/ Liquid Cu. Yds I Gallons 32Cuc� % Solids 1')3 Volume Applied per Acre (Dry Tons/Ac) O I Residual Sources �rppES #, WQ#, Pert., Animal Waste, etc) t�lC ZO"7`� Soil Cond. (Dry, Wei Moist) Precip. past 24 Hrs. inches C)5 a o m a 5 5 < o m cu „ K' °o CD-5 m � ° * Z- 0,30 TKN mglkg " Ql0 Z a El o ° � � o �• mg/kg Nitrate and Nitrite mg/kg xXr PAN Applied lbs/acre ( ) Name of CropType ReceivingResidual Application Crop 1 3 9 Crop 2 Crop 1 ccr Crop 2 :7 ) .t44(p Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this for '' TOTALS: q O .':.. _ .. Annual lbs/acre Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop GCT _ Se Zn P 6.k As Cd Cu I Cr Pb Hg MoJtGc�bm O,(X 7i� D D 'Z 3(- >:.. ...„Prior - o ��5 +-F•Ig�i � 14 .1 I LI.1 �� 6+5G4 033 hiQ 1 •`G' : ;::•>:•>. ................: ... (, 36 :.. ; .........•..._ ...;.. . . I Lime Date A lied lbs/ac •._„ ......�. t,.Maj my Vi Marv, Lua" Luis uucument was prepares unaer my curection or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." A Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: ni-0 -efx_MOD Total Dry Tons Applied (Annual): 5,U l j Permit #: Cation Exchange Capacity, (non 503 only): Ll. 5 Operator: Owner: C 'I��rl c�(f .7 Predominant SoilSeries:-PC,_JC&(:S Acres Used: 6.-)la Acres Permitted: 3,--)c4 Site #: 3 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Co►n- posite Date 1 1 2 3 L4J 5j 6 j7 8 9 10 11 12 % Solids Arsenic <?.5 Z 5 Cadmium Copper 1Zti� Z U7 Clu•omium Lead { �, Mercury p.LIc1 OU Molyb <5.p <5.C) Nickel 13 I Selenium S,5 n <5.D Zinc 01 ('51 Total Phos- horus Z)Z • Z l t) Annual Heavy Metal Field Loadings (Calculated in lbs/acre): MR a +. __________ • _� �'. W-6, Ci�ia�iil i RI • • _________® ti • MT Total Phos- NEEMENEEMEN p J 1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ZZ6-(C Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: 46-J/1�lib17 WQ Permit #: k_'QD0olC4q Field #: g Acres Utilized: �.73 Land Owner: ��� � Annual Dry Tons Applied: 15_ CjZ0 Site #: C J (QC+ JJ Acres Permitted: 73 Operator: �j � �yy1 Predominant Soil Series: Alckcl Cation Exchange Capacity (non 503): e4.5 Crop 1 Name: �t�eimlda Crop I Max. PAN: 177. Crop 2 Name: Cron 2 Max. PAN: c _ a, Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons aka Solids Volume Applied per PP P Awe (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert ,Animal Waste, etc) Soil Cond. (Dry, Wet, Moist Precip. Past 24 Hrs. inches K o 9 0 C o � � r * �• N TKN mg/kg y z o °' � mg/kg Nitrate and Nitrite mglkg A Applied PP (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 �i S ZC7t� 1-7�'4� .'7Zt�' N•CO(.c��'Z6�� rr��+ C� ©•5 03.D 754 �;,� .77Z �, NCCMV drq a 5 -)'�13 ,., a ' }3 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): E .... I ........ . TOTALS:As Cd I Cu Cr I Pb Hg Mo Ni Se Zn P l Lime Applied Annual lbs/acre O 0,L' A p . (o l 3 O•GC� i �lo� 1- 1 Z 3 U G �ihd .25 i 56 q. I 1 `� r1.o5o '�.604 Z5. �1 — c>,ob .364 .53-1 Z.b% O. '2 D.1 Z o o1 (A f 5 ` ,01 5 ?-104 — .2% .3 Y)4 ,01c Z lQ7 l S �1 Z 3 � . 57 yQ7 Zt•Ir-! I Z .... .. ..•:...: :::'>::: »::'><:::;:::< .............. ............. ......................... Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop ........ ...... . ....::::.:.:.•...... Z :;:: :':`.: ....... •' :.• ........ :.............::.• r cernry, under penalty of taw, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Ccni8"'} ntff _[Db Total Dry Tons Applied (Annual): t S.07_b Permit #: L Q�jNL Cation Exchange Capacity (non 503 only): y.1-3 Operator: j tbT),44,) Owner: �Cil��t✓i� G - rp,0 Predominant Soil Series: A A,_Acres Used: 11. Acres Permitted: 223 Site #: CT gCj-ff Field #: 45 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 L1-IU_IQ 2 LJ-f0-1g 3 C _4C,6 4 5 6 7 8 9 10 11 12 % Solids .3`Jc, .73`6 1 1.)3 b Arsenic <Z.� <Z, Cadmium Copper ZU-) ZU7 Chromium 13 13 13 Lead 1, Mercury p.(49 C).LC1 O.Uq Molyb- <5.0 Nickel I r 3 113 i 3 Selenium <5,(> S 5. b <5. D Zinc Total Phos- phorus -224PO ZWkdO Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): D - .. Event Total Phos- phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". c Signature of Land Applier Date DENR FORM MFLSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Cien�..ftD WQ permit #: u,�QOObioUg Field #: q AcresUtilized: 5.15 Land Owner: Annual Dry Tons Applied: 7 jp7 Site #: CTrnCf=B Acres Permitted: Operator: j enec,-'w-) Predominant Soil Series: Wo— Cation Exchange Capacity (non 503): Crop 1 Name: Cron 1 Max. PAN: i'» Cron 2 Name: r, 1 ivr— D A W. `o y at 0 Volume applied (enter one) Solids/ Liquid 9 Cu. Yds Gallons ��a Solids I �3`�0 Volume Applied per Acre (Dry Tons/Ac) 0.3 Residual Sources (NPDES #, W #, Q Fert., Animal Waste, etc) 3 -,i Soil Cond. We ' Moist) i+ Precip. Past 24 Hrs- inches O a a .eS �• c n w o 5 C E Y O� 5 * + 0.3v TKN mg/kg 143 z _ _ B o 0 w. mg/kg Nitrate and Nitrite mg/kg C4 PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop I Crop 2 . ' . ;1,LF'S7 ; Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): »::: : . ....... TOTALS: 1(31]OOO . ;; • ...' Annual lbs/acre Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop AS Cd Cu Cr Pb H Mo Ni Se Zn I P D.rDS O.(D3 0.7Z.b 0.03S C C6Z i7W) 0,01C4 0,o3S' 0.01 7 3tG :: 4U 1 .94 n1 5-46i O.l O .L- Z 5 Z , Z Z4 = 101 6 5Z1 p, tL1 Z. -)V ;5-bt�j p •G35 ::.::::. •:•:•:•:•:.:.. :•:•. :::•.::::.:.: »::: ;:: >: »: 3 i3. Z i — o .::.....::..::..:.:., X t�Z Lime Applied Date lbs/ac _ _. _._„ —..— J—""A.y „x La„, GuaL U,,,, uVcu,ueui was prepareu unuer my airection or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." nel Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation =2�'�7 **Volatilization Rate: Surface - 0.5. In iection/Incornoration -1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: C'mitn�nf_ ( )6D Total Dry Tons Applied (Annual): 12561)Z Permit #: _ (Goxi dLIq Cation Exchange Capacity (non 503 only): 4 5 Operator: }�j�n Yjl � Owner: irj) "IOCA.- ffib-D Predominant Soil Series: LC Acres Used: S', I 'j Acres Permitted: 6,115 Site #: bT(aal Field #: qj Residual Analysis Data (Heavy Metals and Total Phosphorus use mglkg, % Solids use Raw Percent #): Sample or Coin- posite Date 1 2 L3J 5 __6j 7j L8J L9J 10 11 12 % Solids i,-)6`7o Arsenic <-Z.`j Cadmium 1.1 1.1 Copper I 7N7 Zy-) Clv omium 13 13 Lead i -' 1 q Mercury Q. Lci 3 , 1-1cl Molyb- Nickel 13 13 Selenium <5.0 <5D Zinc $ 1 b5l Total phos- phorus I Z_ PO Z^) o Annual Heavy Metal Field Loadings (Calculated in lbs/acre): -Total p1los- __pjiorusNNEEEEEEEEEEr "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Icnowing violations". Signature of Land Applier Z 26 -1 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: •�- A N)6D WQ Permit #: U)qpC01M Field #: 13 Acres Utilized: 3.30 Land Owner: _ { � Annual Dry Tons Applied: 2.Z11 Site #: C j FQ�� Acres Permitted: 3, Operator: �ne(-` AkN Predominant Soil Series: 32ACL Cation Exchange Capacity (non 503): Crop 1 Name: QDQ. afBalft.1C>- Crop 1 Max. PAN: i (o ( Crop 2 Name: Crop 2 Max. PAN: o 0c Volume applied (enter one) Solids/ Liquid Cu. YdS Gallons % Solids Volume Applied per PP P Acre (Dry 7onsrAc) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc)o Soil Cond. (Dry, Wet,Hrs. Moist Precip, Past 24 inches a � .a ° ° FS- o 7Z °' = F N' * ❑ „ , ° m 0 T mg/kg ° B oc ° "1 E. ° �• mglkg Nitrate and Nitrite mg/kg PAN Applied lbs/acre ) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 51� 16mc) 5 0. f4ca awls) d o S 0. 5 o 5 0, ao 0 3v 4 - q reM� z95o .5 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): � TOTALST As Cd Cu Cr Pb Hg Mo Ni Se Zn P Lime A lied Annual lbs/acre 31 O �Z u 3 d.:' Z ©.-i) (g ,'1 3 U 33Z 13 •145 j Ll77 ►33� O• �l z�31y -- Z. 3 ,333 p.a-e-) , c )3 ' , 0�3 15 0 I.C1-l�i •O 0-0�90. Z. �T 3 q 21� "2 �... ...•.•.•..........•. >: >:::: >:::: ?:_:: ; ::.»:;»::::: . Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.*** Permit PAN Limit Ist/2nd Crop :::.::::. _:•::.:•:•.•.•:•>..:........ ...............:. ,:.. .:...:.....:.:.... :.. .: . "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for [snowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation Z�� **Volatilization Rate: Surface - 0.5. Iniection/Incoruoration - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: epr)fe1)` r)ea-i `),--,,7 Total Dry Tons Applied (Annual): ZZZZ Permit #: t6ocoOIC�4 Cation Exchange Capacity (non 503 only): L .Is Operator: t )enee !-)mjk4h Owner: C-WI er4n(D_1`)bD Predominant Soil Series: Acres Used: 3,60 Acres Permitted: 3,-3L) Site #: Field #: I Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/Icg, % Solids use Raw Percent #): Sample or Com- posite Date 1 4 2 p g 3 4 5 6 7 8 9 10 11 12 % Solids Arsenic CZ . 6 CZ , 6 Cadmium J 1.1 Copper ZU7 ZL1 Chromium Lead I 1 Mercury p, 001 01$� Molyb- Nickel Selenium Zinc Total Phos- hows ZWIPO 1 O Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Totalo a© o© o© o o • , , 4 App. Event L Y MMIS mom InIuMMMMMMMMMM� MINE Total Mmm MENEEMENEEN. phoms "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Icnowing violations". LAIM� Signature of Land Applier L`I Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: LCnien44-ta-mbD WQ Permit #: l C60JC)4g Field #: 1,5 Acres Utilized: Z.3� Land Owner: �ryf 1 Annual Dry Tons Applied: le ( 3 Site #: I Acres Permitted: Operator,2)ene-.&M,dJ-) Predominant Soil Series: Cation Exchange Capacity (non 503): Crop 1 Name: BJam Crop 1 Max. PAN: ►—) Crop 2 Name: Cron 2 Max_ PAN: o i Y = C) Sig Volume applied (enter one) Solids/ Liquid 9 Cu. Yds GeIIOnS % Solids i. Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) o� Soil Cond. D (�' We Moist) Precip. Past 24 13rs. inches > q •II s o T " ^ * o C o � y * h' * w z n m * N * w 0 TK mg/kg D z a o o w mg/kg /719 Nitrate and Nitrite mg/kg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 .D Crop 2 Crop 1 Crop 2 l .3 IKQC -F) dr 5 qg J : `• ,'?� Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: U°' .:: .':: As Cd Cu I Cr Pb Hg Mo Ni Se Zn P 13 Lime A lied Annual lbs/acre Prior Years Cumulative lbs/ac l 1.340 odni o.bqg O9 CO3 ` , 2,) 1 ` 114$, :...: Q. 1 i 2 p, 7 g I!1- Ici � <�:: � • ZLIZ p , at 0 1-1.` 1 `` 2 Z, 161 p63 5 d . ua Z. Lag o3q ::..::....:.:...:.:.....::.: .:.:.. — Z 15 — z .:.. .............•........ ... . .• ... ::...? ::: < : < :: ,: . :..:.......• ......... {?Cn Date Ibs/ac Current Cumulative lbs/ac-0 Permitted C. P. L. R.**** Permit PAN Limit l st/2nd Crop «T —a �IA.r, uaaa+ra Pouarty Vr raw, rnat Luis uocument was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false infor anon, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation —� **Volatilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Lain-Anen- n(A2 Total Dry Tons Applied (Annual): (o,L/�/j Permit #: oxoD1001 Cation Exchange Capacity (non 503 only): C,1. Operator: '�)�eebj-nU-) Owner: Predominant Soil Series:�(��nt Acres Used: Z, 3Q Acres Permitted: Z. Site #: T Field #: I' j Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 11 dloag L2J -/ _19 L3J 4 J 5 6 7 8 9 10 11 12 % Solids Arsenic < 2. 5 <Z . 15 Cadmium i • 1 1.1 Copper 2_4_� 2117 Chromium 13 13 Lead 1 ) Mercury Molyb- deninn <5. <5.v Nickel 13 Selenium <6. D < 5• CU Zinc Total Phos- phorus Z-)Z(,c Z,-)ZLU Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ® ® Total P. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Lr'r4w E_ 2 b_19 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: �-Or+6•�e_a_ (f16. WQ Permit #: r)Q'(:�OOJC14 Field #: 1 (a Acres Utilized: Zc/2q Land Owner: COfI}0. ff)67 Annual Dry Tons Applied: Site #: �.U1�3 L7 Acres Permitted: ZCf� Operator:`�0-wc b-,)id) Predominant Soil Series: — Maca, Cation Exchange Capacity (non 503): 415 Crop 1 Name: 04x�l Wlclb. Crop 1 Max. PAN: 1-)Z 1-1 Crop 2 Name: Crop 2 Max. PAN: _ Q Volume applied (enter one) Solids/ Li uid 9 Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert.. Animal Waste, etc) Soil Cond. (Dry, We Moist Precip. Past 24 Hrs. inches a K F o w a o ° o p - N" * ay �; w — * 5' ° TKN m /k 9 9 Z Y o B 2. /k m9 9 Nitrate and Nitrite m /k 9 9 PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 P Crop 2 P Crop 1 P Crop 2 P 4� 1.73`7p t . l Z ; ►aCcp3Z cn f 8 .5 . W —AD Z9 112: Lq—kQ Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: U _( As Cd Cu Cr Pb Hg Mo Ni Se Zn P Lime Applied Annual lbs/acre p.CO 0-C O ':5Xk oxsb 0,04Z p. co I p,OIZ O.LZD 0.DIZ 35� ......... :.. :::::: >::: :=.... >::::: >: ............... ..... ........ ..... . :;::` ::::;>: ;>:: ^ :::::=::=:::=: Date Ibs/ac Prior Years Cumulative lbs/ac D.Z5Z . 7� .144 Qi Z• 14 & .03Z O. 2 .C19 Z 0.3" 5 1 .1 (o urrent Cumulative lbs/ac U,'v 2 17 Z I`!S� O.d33 ` . lulu ;ZSIZ` .L}D ]�S Permitted C. P. L. R.**** (! I ? 7 I — �U q -Z ,A5 Permit PAN Limit lst/2nd Crop .:.:.:::: . . ;. ........ ..... ......: "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Z Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge.-0.4 ****C.P.L.R.: Cumulative Pollutant Loadine Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: OCI) � ect-Wccl Total Dry Tons Applied (Annual): 6.063 Permit #: LaCCoIoA Cation Exchange Capacity (non 503 only): Operator: ��l f� ljll h Owner: C(�nVeC �pA (S}` -D Predominant Soil Series: t Acres Used: Z,Gjg Acres Permitted: �nC/Q Site #: _ID Field #: 1w Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 L�jp-I`6 2 3 4 5 6 7 8 9 10 11 12 % Solids Arsenic Cadmium Copper • C�7 Chromium Lead 1 g Mercury 0,Le Molyb- demim b Nickel 13 Selenium Cj• C� Zinc ;j 1 Total Phos- phorus 2?Z1LQ Annual Heavy Metal Field Loadings (Calculated in lbs/acre): WOMI "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: ncrlf e rT& WQ Permit #: k)D0 ICJR Field #: 17 Acres Utilized: 3.�,2 Land Owner: Cbri- n},'Z> Annual Dry Tons Applied: $ IP14 Site #: j7 Acres Permitted: 3.6Z Operator: `�� �pj Predominant Soil Series: Alh 00,.. Cation Exchange Capacity (non 503): 14.15 Crop 1 Name: C l (� Crop 1 Max. PAN: ! 7'` Crop 2 Name: Crop 2 Max. PAN: _ s o Ll Volume applied (enter one) Solids/ Liquid Cu_ Yds Gallons o /o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES 4, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, We >y Moist Precip. Past 24 Hrs. ruches a iK -o �° ? o m CL ° o w v' ° + N TKN mg/kg z > = o B g E mg/kg Nitrate and Nitrite mg/kg PAN A Applied lbs/acre) Name of Crop Type Receiving Residual Application PP Crop 1 Crop 2 Crop I Crop 2 o roo 6.5% NCCCZ W --) tnoi 5 10. 5 O.30 95.D•q%9 .2)3 l QLAYOD I-Vo mO& 15 0.3043 YD 7 43 .�' Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ... ............ TOTALS:. 0 As Cd Cu Cr Pb I Hg Mo I Ni Se Zn P Lime A lied Annuallbs/acre 1 3 . 1 .66) 0 . bOZ O , 1 7 . 1,5 7310 Date lbs/ac Prior Years Cumulative lbs/ac o 37,5 Elm3iat ll.g g Z. w E-04Z (o .61 Current CumulativeIbs/ac 0. .33Z' a, 11•'S5 1-S ri3 0.0Ll4 0.9 21 Z•7�{J Permitted C. P. L. R. * * * * 3 3a g Permit PAN Limit 1 st/2nd Crop --.t cert ty, untter penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier /� *Application Method: S - Surface, IN - Injection, INC - Incorporation `� **Volatilization Rate: Surface - 0.5. Iniection/Incomoration - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: irlit 11 � �Li7� j� Total Dry Tons Applied (Annual): j, ITA Permit #: Cation Exchange Capacity (non 503 only): Operator: Owner:0Cf-y-n�4)ffjD Predominant Soil Series: Acres Used: 3.(p2 Acres Permitted: 3,62 Site #: -D Field #:� Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/lig, % Solids use Raw Percent #): Sample or Com- posite DateC�iB 1 2 y fag 3 4 5 6 /J 8 J 9 10 11 12 % Solids ., 36 Ov Arsenic < .,5 CZ, rj Cadmium 1,1 Copper Z 7 ? Chromium 13 i Lead 1g )� Mercury Molyb- 05.0 <5,6 Nickel I '-j Selenium 1 <5. C <5 Zinc, <j l Total Phos- horus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): •• © E© Nn , WIN MIM �i ►i. r.. __________ r tt_ O r MOM 0 �qlffimv. go M ®a ♦ �• RIM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Lw.�nu,o�- 7-2L. 101 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: 5__)4nP_Q rt" b WQ permit #: Field #: ltq Acres Utilized: i 1.75 Land Owner: C � C'n C� � Annual Dry Tons Applied: Site #: C TfCL4-ff Acres Permitted: Operator: `Aol p Predominant Soil Series: Mon Cation Exchange Capacity (non 503): Crop 1 Name: Crop 1 Max. PAN: /'?2 Crop 2 Name: Crop 2 Max. PAN: _ s Q 0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons "�o Solids Volume Applied per P Acre (Dry TonslAc) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (D�' Wet Moist Precip. Past 24 Hrs. inches a 4 U o v o N' * T, o' 0 K � M d _• 0 TKN mglkg Z > T ' o E3 mglkg Nitrate and Nitrite mgfkg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop l Frop 2 Crop 1 Crop 2 - g b 1�3�: 0,353 lacoo3Zo�7 doCD5 0. o. , -Ns ,7_'Z1719 t s.lcl 0, Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ..................... TOTALSI 111511500 j .:: As Cd Cu Cr I Pb Hg Mo Ni Se Zn P Lime Applied Annuallbs/acre fjZ Z D, 1 G' •C01 4 O,l7 0-IN I g 0-' ©, 0CA — 13 ©-GI ZJo7 ' zob 15 '0- •Gdq U O, (l 0.w4 4l0 p.0 ZU�i, >....:. Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop . ..... ....... . "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation Zto- l **Volatilization Rate: Surface - 0.5. Iniection/Incornoration -1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R,: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Ocnlef4"lecLm,�i) Total Dry Tons Applied (Annual): U.144�? Permit #: 1,JQOC oO Cation Exchange Capacity (non 503 only): 45 Operator: 'Zenge6A-)l Owner: Ln+ r4)1L(Yl; D Predominant Soil Series: A }a Acres Used: (1 •-),j Acres Permitted: Site #: -TraC� ZL Field #: ► Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date-1D-IQ 1 1 2 3 4 5 6 7 8 9 10 11 J 12 % Solids Arsenic Cadmium 1. Copper 7 Chromium l 'j Lead I,? Mercury Qklp Molyb- <5.b Nickel I -j Selenium <: 1j. zinc I Total Phos- horus 7_-@vQ Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total Event Total Phos- phorusIMENEEMENEEMEN "I certify, under penalty of law, that this document was prepare unc er my irection or supervision rn actor ar►ce with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". JET A 0 /Y ! Yt - -- -- 7 7 C! Signature of Land Applier Date DENR FORM MFLSF (12/2006) SAMPLING AND MONITORING PLAN FOR CONTENTNEA MSD Land Application of Class B Residuals Permit No. WQ0001048 The Sampling and Monitoring Plan for Contentnea MSD Land Application of Class B Residuals is developed pursuant to Permit No. WQ001048 Section III. Part f. The sampling techniques and subsequent analyses are collected and analyzed in accordance with Federal and State of North Carolina requirements. As a general rule, land application of sludge at the Contentnea MSD facility will occur only during the months of March through October of each year during the growing season of the Coastal Bermuda grass that is the cover crop for the CMSD designated land application fields. Any deviation from this procedure will be addressed through NCDENR Division of Water Resources prior to application and any additional sampling and/or monitoring will be done per their instructions. The Land Application Operator in Responsible Charge/Backup Operator in Responsible Charge will be responsible for the monitoring requirements set forth in the Sampling and Monitoring Plan, and the WWTP sampling personnel will be collecting the samples as directed by the ORC/Backup ORC. All sludge samples for meeting the ceiling concentrations for metals, nutrient loading, pathogen and vector attraction reduction will be conducted during the months of March through October to insure the sludge analyses are representative of the sludge being land applied. All sludge samples will be taken from Digesters #1 and #2, and all sludge is land applied from Digesters #1 & #2. Renee Smith Land Application Operator in Responsible Charge Charles Smithwick, Jr. Backup Land Application Operator in Responsible Charge Ricky Barrow Plant Operator/Sample Collector Stephen Berry Plant Operator/Sample Collector James Woodard Plant Operator/Sample Collector I.TCLP and Corrosivity, Ignitability, Reactivity The corrosivity, ignitability, reactivity and the toxicity characteristic leaching procedure (TCLP) shall be performed annually as specified in Attachment A of Permit No. WQ001048. The samples will be a grab taken from sufficiently stabilized sludge and will be representative of the sludge that is land applied. The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl Chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) It. Metals and Nutrients The metals and nutrients analysis shall be performed annually as specified in Attachment A of Permit No. WQ0001048. The samples will be a grab taken from sufficiently stabilized sludge and will be representative of the sludge that is land applied. The metals and nutrients analysis shall include the following parameters (the ceiling concentrations in mg/kg are in parentheses where applicable): Aluminum Mercury (57) Potassium Ammonia -Nitrogen Molybdenum (75) Selenium (100) Arsenic (75) Nickel (420) Silver Cadmium (85) Nitrate -Nitrite Nitrogen Sodium Calcium Percent Total Solids Sodium Adsorption Ratio (SAR) Copper (4,300) pH TKN Lead (840) Phosphorus Zinc (7,500) Magnesium Plant Available Nitrogen (by calculation) III. Pathogen Reduction The Pathogen Reduction shall be performed annually as specified in Attachment A of Permit No. WQ0001048. The samples will be grabs taken from sufficiently stabilized sludge and will be representative of the sludge that is land applied. The analyses will be Fecal Coliform monitoring and will meet the requirements in 15A NCAC 02T .1106 (c) Alternative (1). Seven samples will be collected over a 3 week period and analyzed using the MPN dilution method. The geometric mean fecal coliform density of these samples will be less than 2 million MPN per gram of biosolids (dry weight basis) in order to be land applied. The Fecal Coliform monitoring procedures were taken from the EPA.gov website/ENVIRONMENTAL REGULATIONS AND TECHNOLOGY/Control of Pathogens and Vector Attraction in Sewage Sludge (5.2) on February 26, 2015. IV. Vector Attraction Reduction The Vector Attraction Reduction shall be performed annually as specified in Attachment A of Permit No. WQ0001048. The samples will be grabs taken from sufficiently stabilized sludge and will be representative of the sludge that is land applied. The analyses will be the Specific Oxygen Uptake Rate (SOUR) and will meet the requirements in 15A NCAC 02T .1107 (a)(4). Seven samples will be collected over a 3 week period and analyzed using the acceptable SOUR test requirements. The average of the seven samples will be less than or equal to 1.5 mg of Oxygen per hour per gram of total sewage sludge solids (dry weight basis) at 20°C in order to be land applied. The Specific Oxygen Uptake Rate procedures were taken from the EPA.gov website/ENVIRONMENTAL REGULATIONS AND TECHNOLOGY/Control of Pathogens and Vector Attraction in Sewage Sludge (8.5) and the NCDENR.org website/Division of Water Resources/Non-Discharge Unit/Reporting Forms/Specific Oxygen Uptake Rate (SOUR) Testing Compliance on February 26, 2015. V. Soils Analysis As per Section IV. (5) of Permit No. WQ0001048 an annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on each land application site listed in Attachment B on which a residuals land application event will occur in the respective calendar year. This analysis shall be in accordance with the "Guidance on Soil Sampling" located in the Sampling Instructions section of the NC Department of Agriculture & Consumer Services' website(http://www.ncagr.gov/agronomi/pubs.htm). At a minimum the Standard Soil Fertility Analysis shall include the following parameters: Acidity Exchangeable Sodium Percentage Phosphorus Base Saturation (by calculation) Magnesium Potassium Calcium Manganese Sodium Cation Exchange Capacity Percent Humic Matter Zinc Copper pH VI. Groundwater Monitoring Wells There are five Monitoring Wells located on the sludge land application property. They are MW-9, MW- 10, MW-14, MW-15, MW-18. The Monitoring Wells will be sampled three times per year in February, June, and October for the following parameters (Groundwater Standards are in brackets where applicable): Water level, distance from measuring point Nitrogen, Ammonia Total (as N) [1500.00 ug/L] Coliform, Fecal MF, M-FC Broth, 44.5C Nitrogen, Nitrate Total (as N) [10.00 mg/L] Solids, Total Dissolved-180C [500.00 mg/L] Chromium, Total (as Cr) [10.00 ug/L] pH, lab Copper, Total (as Cu) [1.00 mg/L] Carbon, Total Organic (TOC) Volatile Compounds, (GC/MS) (October only) All Monitoring Well samples and analyses will be conducted according to the directions listed in Attachment C of the Contentnea MSD WWTP Land Application of Class B Residuals (Non -Dedicated) Permit No. WQ0001048. Contentnea Metropolitan Sewerage District 2019 Residuals Land Application Permit Renewal Items for C. Residuals Quality Information TCLP Results Metals and Nutrients Results SAR Calculation PAN Calculation Fecal Coliform Lab Results SOUR Results Soils Results Groundwater Monitoring Well Results TC L P LAB REPORTS S-GS' Orlando, FL:,:,.:. The results set forth herein are provided by SGS North Aillerica Inc. e-Hardeopy 2.0 Atrtometted Report Technical Report for Environment 1, Inc Contentnea Metro Sewage District; Grifton, NC 416 SGS Job Number: FA53172 Sampling Date: 04/04/18 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard @ environment 1 inc, co m TTN: Deedee Woolard Total number of pages in report: 14 'a ._>GL v- - qe Zd4in Test results contained within this data package meet lice requirements Brice, M.S. of the National Environmental Laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact; Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report sliall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • lei: 407-425-6700 • fax: 407-425-0707 SGS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about Unauthorized modification of this report is strictly prohibited. how we can serve you better at: _ Review standard terms at: EHS.US.CustomerCare�7sgs.com ' 1 of 14 FA53i72 t -I- Section1: Sample Summary................................................................................................... Section2: Summary of Hits.................................................................................................... Section3: SF inale Resailts........................................................................................................ 3.1: FA53172-1: SLUDGE SAMPLE.................................................................................. Section4: Misc. Forms............................................................................................................ 4.1: Chain of Custody........................................................................................................... Sections: a 3 4 12 13 2 of 'IA FA53172 SGS North America Inc. Sample Summary Environment 1, Inc Job No: FA53172 Contentnea Metro Sewage District; Grifton, NC Project No: 416 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA53172-1 04/04/18 09:15 KH 04/07/18 SO Sludge SLUDGE SAMPLE Soil samples reported on a dry weight basis unless otherwise indicated on result page. L 3ot14 FA53172 Summary of Hits Job Number: FA53172 Account: Environment 1, Inc Project: Contentnea Metro Sewage District; Grifton, NC Collected: 04/04/18 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA53172-1 SLUDGE SAMPLE Corrosivity as pH 4.9 su SW846 CHAP? Ignitability (Flashpoint) a > 200 Deg. F SW846 1010 Benzene 0,0032J 0,010 0.0031 mg/1 SW846 8260E Tetrachloroethylene 0.0235 0.010 0.0022 mg/1 SW846 8260E (a) Not ignitable. Page 1 of F I 4of14 1 FA53172 ............................ ..................... .................................. Orland F . . ......... .. .. .............. .... Sam le, Results Report of Analysis Soction 3 5 of 14 FAS3172 SGS North America Inc. Report of Analysis ;lient Sample ID: SLUDGE SAMPLE ,ab Sample ID: FA53172-1 Date Sampled: 04/04/18 Matrix: SO - Sludge Date Received: 04/07/18 Method: SW846 8260B SW846 1311 Percent Solids: 1.7 'roject: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 File ID DR Analyzed By Prep Date Prep Batch Analytical Batch Run 11 M0102391.D 10 04/11/18 17:40 MM 04/09/18 13:45 OP69516 VM4409 Run #2 Purge Volume un #1 5.0 ml un #2 VOA TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 71-43-2 Benzene 0.0032 - D018 0.50 0.010 0.0031 mg/I j 78-93-3 2-Butanone (MEK) ND; D035 200 0.050 0.020 mg/I 56-23-5 Carbon Tetrachloride ND D019 0.50 0.010 0.0036 mg/l 108-90-7 Chlorobenzene ND D021 100 0.010 0.0020 mg/1 67-66-3 Chloroform ND D022 6.0 0.010 0.0030 mg/i 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.010 0.0026 mg/1 107-06-2 1,2-Dichloroethane ND D028 0.50 0.010 0.0031 mg/I 75-35-4 1, 1 -Dichloroethylene ND D029 0.70 0.010 0.0032 mg/1 127-18-4 Tetrachloroethylene 0.0235 D039 0.70 0.010 0.0022 mg/1 79-01-6 Trichloroethylene ND D040 0.50 0,010 0.0035 mg/l 75-01-4 Vinyl Chloride ND D043 0.20 0.010 0.0041 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 102% 83-118% 17060-07-0 1,2-Dichloroethane-D4 104% 79-I25% 2037-26-5 Toluene-D8 101% 85-112% 460-00-4 4-Bromofluorobenzene 99% 83-118% ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6ot14 FA53172 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA53172-1 Date Sampled: 04/04/18 Matrix: SO - Sludge Date Received: 04/07/18 Method: SW846 8270D SW846 3510C Percent Solids: 1.7 Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of I File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 91000906.1) 1 04/12/18 09:22 MV 04/11/18 13:00 OP69573 S9I34 Run #2 Initial Volume Final Volume :un #1 100 ml 1.0 ml :un #2 ABN TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 95-48-7 2-Metbylphenol ND D023 200 0.050 0.0056 mg/1 3&4-Methylphenol ND D024 200 0,050 0.0098 mg/1 87-86-5 Pentachlorophenol ND D037 100 0.25 0.050 mg/l 95-95-4 2,4,5-Trichlorophenol ND D041 400 0.050 0.0074 mg/1 88-06-2 2,4,6-Trichlorophenol ND, D042 2.0 0.050 0,0075 mg/l 106-46-7 1,4-Dichlorobenzene ND : D027 7.5 0.050 0.0050 mg/l 121-14-2 2,4-Dinitrotoluene ND D030 0.13 0.050 0.008I mg/l 118-74-1 Hexachlorobenzene ND D032 0.13 0.050 0.0069 mg/1 87-68-3 Hexachlorobutadiene ND D033 0.50 0.050 0.0050 mg/1 67-72-1 Hexachloroethane ND D034 3.0 0.050 0.016 mg/1 98-95-3 Nitrobenzene ND D036 2.0 0.050 0.0093 mg/i 110-86-1 Pyridine ND D038 5.0 0.10 0,020 mg/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 31% 14-67% 4165-62-2 Phenol-d5 19% 10-50% 118-79-6 2,4,6-Tribromophenol 78% 33-118% 4165-60-0 Nitrobenzene-d5 76% 42-108% 321-60-8 2-Fluorobiphenyl 76% 40-106% 1718-51-0 Terphenyl-d14 77% 39-121% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7of14 FA63172 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA53172-1 Date Sampled: 04/04/18 Matrix: SO - Sludge Date Received: 04/07/18 Method: SW846 8151A SW846 3510C Percent Solids: 1.7 Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC057863.1) 1 04/12/18 22:06 NJ 04/11/18 12:15 OP69575 GCC1276 Run #2 Initial Volume Final Volume Run #1 10.0 nil 5.0 nil Run #2 Herbicide TCLP Leachate CAS No. Compound 94-75-7 2,4-D 93-72-1 2,4,5-TP (Silvex) CAS No. Surrogate Recoveries 19719-28-9 2,4-DCAA TCLP Leachate method SW846 1311 Result HW# MCL RL MDL Units Q ND D016 10 0.050 0.017 mg/1 ND D017 1.0 0.0050 0,0013 mg/l Run# 1 Run# 2 Limits 132% 39-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 1 8of14 FAS3172 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA53172-1 Date Sampled: 04/04/18 Matrix: SO - Sludge Date Received: 04/07/18 Method: SW846 8081B SW846 3510C Percent Solids: 1.7 Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch :un #1 TT387928.D 1 04/12/18 15.16 KL 04/11/18 13:00 OP69574 GTT2128 :un #2 Initial Volume Final Volume :un #1 100 ml 5.0 ml :un #2 Pesticide TCLP Leachate CAS No. Compound 58-89-9 gamma-BHC (Lindane) 12789-03-6 Chlordane 72-20-8 Endrin 76-44-8 Heptachlor 1024-57-3 Heptachlor epoxide 72-43-5 Methoxychlor 8001-35-2 Toxaphene CAS No. Surrogate Recoveries 877-09-8 Teirachloro-m-xylene 2051-24-3 Decachlorobiphenyl TCLP Leachate method SW846 1311 Result HW# MCL RL MDL Units Q ND D013 0.40 0.00010 0.000022 mg/l ND D020 0.030 0.0010 0,00038 mg/I ND 13012 0.020 0,00020 0,000021 mg/1 ND D031 0.0080 0.00010 0.000026 mg/I ND D031 0.00800,00010 0.000020 mg/i ND D014 10 0.00020 0.000050 mg/1 ND D015 0.50 0.0050 0.0021 mg/l Run# 1 Run# 2 Limits 88% 42-127% 89% 27-127% ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9of14 FA53172 SGS North America Inc. Report of Analysis Mont Sample ID: SLUDGE SAMPLE ,ab Sample ID: FA53172-1 Date Sampled: 04/04/18 4atrix: SO - Sludge Date Received: 04/07/18 Percent Solids: 1.7 'roject: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 c Metals Analysis, TCLP Leachate SW846 1311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic < 0.10 D004 5.0 0.10 mg/l 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 Barium < 2.0 D005 100 2.0 mg/I 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 Cadmium < 0.050 D006 1.0 0.050 mg/i 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 Chromium < 0.10 D007 5.0 0.10 mg/I 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 Lead < 0.050 D008 5.0 0.050 mg/I 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 Mercury < 0.0050 D009 0.20 0.0050 mg/I 1 04/12/18 04/12/18 LM SW846 7470A 1 SW846 7470A 4 Selenium < 0.10 D010 1.0 0.10 mg/l 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 Silver < 0.10 D011 5.0 0.10 mg/I 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 (1) Instrument QC Batch: MA14817 (2) Instrument QC Batch: MA14818 (3) Prep QC Batch: MP33585 (4) Prep QC Batch: MP33587 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) - I 10of1Q ub FA53112 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA53172-1 Date Sampled: 04/04/18 Matrix: SO - Sludge Date Received: 04/07/18 Percent Solids: 1.7 Project: Contentnea Metro Sewage District; Grifton, NC General Chemistry Analyte Corrosivity as pH Cyanide Reactivity Ignitability (FIashpoint) a Solids, Percent Sulfide Reactivity (a) Not ignitable. RL = Reporting Limit Page 1 of 1 Result RL Units DF Analyzed By Method 4.9 so 1 04/09/18 12:15 BR SW846 CHAP7 <87 ' 87 mg/kg 1 04/19/18 18:36 1K SW846 CHAP? > 200 Deg. F 1 04/23/18 16:20 BW SW846 1010 1.7 % 1 04/12/18 16:00 AG SM19 2540G < 2900 2900 mg/kg 1 04/14/18 10:55 BW SW846 CHAP7 11 of 14 e FA6a172 ,r Orlando, FL; Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 �a I 12 of 14 FAS3172 N OF CUSTODY RECO anvrronmenr i, inc. CHAI P,O. Box 7085, 114 Oakmont Dr. ! Pnge of 1 Greenville, NC 27858 DISINFECTION environment) ine.eom CHLORINENEUTRALrZEDATCOLLECTION Phone (252) 756-6208 • Fax (252) 756-0633 ❑ CHLORINE pH CHECK (LAB} CLIENT: 416 Week: 8 ❑ uv 3M D, (SLUDGE & WELLS ACCF) UPONE P P P G G G G G CONIAINERTYPE,PIG ^ONL'ENTNEA MLTRO. SEWAGE DISC. KS. RIME PRIDGBN ❑ CHEMECALPRESERYATION P.O. BOX 477 A A A AA A A E CRurTON NC 28530 �' A •NONE O • NAOH ;252)524-5584 a ,S B-HNO, E•HCL Cr C- HrSO, F - ZINC ACETATEMAOH COLLECTIONi] 0 a 8 ° F q F. p� d a� 0•NATHIOSULFA7E SAMPLELOCATION DATE TIME TIME j i cub nq)3 1p 1 1, rm ,� rA 8 CLISSFICAT04: udgaSnropt ❑ WASIMTER(NPDES) ❑ ORNKINGWATER ❑ Dwww ❑ SOLIDWASTESECIM CHAIN OF CUSTODY (SEAL) MAINTAINED DURING IPMENTIDELIVERY Y N SAMPLES COLLECTED BY. (Plassa PAN) I off.r��h1S'' SAMPLES RECEIVED IN LAB ATSL°C RElI OBY(m)(SwuA} DAIErnhl IgG BY( TFIIIME y ��S: z� RR 8 } MMME SEC: ED ATE/IME REU14A DATFfiME CEIYED (SIG.) U cj DAT IME U OamP:er meSI plaee a U for COmposfce sample or a -G for PLEASE READ Inslrucllons for completing41fi orm oAAhe reverse sire. cnnu es �r--rr � /v %/ 9 (� Grab samoie In the blocks above for each narameier reouested. No d 7 A 1 PA53I72: Chain of Custody Page A of G __ ,11 13 of 14 �'FA63172 Job Number: FA53172 Date 1 Time Received: 4712018 9:15:00 AM SGS Sample Receipt Summary Client: ENVA Project: CMSD Delivery Method: FED EX Alrbitl Vs: 771940436480 Therm ID: IR 1; Therm CF: 0.4; # of Coolers: 1 _ Cooler Temps (Raw Measured) °C: Cooler 1: (4.2); Cooler Temps (Corrected) "C: Cooler 1: (4.6); Cooler Information Y or N Samole Information Y or N NIA 1. Custody Seals Present © ❑ 1, Sample labels present on bottles R) ❑ 2. Custody Seats Intact ® ❑ 2. Samples preserved properly © ❑ 3. Temp criteria achieved © ❑ 3. Sufficient volumetcontainers recvd for analysis: ® ❑ 4. Cooler temp verification IR Gun 4. Condition of sample Intact 5. Cooler media Ice a 5. Sample recvd within HT © ❑ 6. Dates/Tlmes/lDs on CDC match Sample Label ® ❑ Trip Blank Information Y or N NIA_ 7. VOCs have headspace [j ❑ 1. Trip Blank present i cooler ❑ ❑ © 8. Bottles received for unspecified tests ❑ 2. Trip Blank listed on CDC ❑ ❑ ® 9. Composifing instructions clear ❑ ❑ W or S NIA 10. Voa Soll Kits/Jars received past 48hrs? ❑ ❑ 11. % Solids Jar received? ❑ ❑ 3. Type Of TB Received © ❑ © 12. Residual Chlorine Present? ❑ ❑ 12 111t1sc. Information Number of Encores: 25-Gram 5-Gram Number of 5035 Field Kits: Number of Lab Filtered Metals: Test Strip Lot its: pH 0-3 230315 pH 10-12 219813A Other: (Specify) Residual Chlorine Test Strip Lot #: Comments RTechnician: SHAYLAP Date: 4RI2018 9:15:00 AM Reviewer: SP Date: 4/712018 Reev.v. Dale a524/;7 D FA53172: Chain of Custody Page 2 of 2 — 14 of 14 FA53172 k wdronment 1, Inc. CtLkIN OF CUSTODY RECORD P.O. Box 7085, 114 Oakmont Dr. Page 1 of 1 Greenville, NC. 27858 environment line .cnm'' Phone (252) 756-6208 • Fax (252) 756-063; CLIENT: 416 Wes: 8 MSD (SLUDGE & WELLS ACCT) ONTENTNEA METRO. SEWAGE DIST. 4S. RENEE PRIDGEN ).O. BOX 477 JRIFTON NC 28530 252) 524-5584 COLLECTION DISINFECTION CHL,ORT,`�TE (—j tTv t� ONE CHLORINE NEUTRALIZED AT COLLECTION pH CHECK (LAB) p p p G G G G G CONTAINER TYPE,P/G A A A A A A A A CHEMICAL PRESERVATION "' A NONE D NAOH w 8- HNO� E HCL C- H,SO, F- ZINC ACETATE,/NAOH LU ¢ G NATNIOSULFATE a p ¢ o 2 0 U z °r �? w w w O t- Q w z o O M � o t3 o > U H W :2 p" U E v U F U F x W U F SAMPLE LOCATION DATE TIME Sludge S-wpleI� 5 4:' <k� C. ....CLASSIFICATION: WASTEWATER (NPDES) DRINKINGWATER DWOlGW JSOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING,S 1PMENT/DELIVERY l( YY N SAMPLES COLLECTED BY: (Please Print) ` t SAMPLES RECEIVED IN LAB AT °C RELINQUISHED BY (SIG.) (SAMPLER) DATETIME q:s3 REG BY ( ATE ME COMMENTS: RELI ED B ) DATERIME �� r� 7;<r RECEIVED B ( DATETIME RELINQUISH B DATEfnME RECEIVED BY (SIG.) DATE91ME ( 1E READ Instructions for completing this form on the reverse side. Sampler must place a "C for composite sample or a "G' forp p q N,_ .i 4 3 7 4 1 FORM #5 Grab sample in the blocks above for each parameter requested. ANNUAL RESIDUAL SAX. ,,ING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0001048 Laboratory: 1) Facility Name: Contentnea MSD 2) Residual Source WQ # or 3) NC0032077 NPDES #: 4) WWTP Name: Contentnea MSD 5) Residual Analysis Data Environment I, Inc. Parameter (mg/kg) Cone. Limit _(mg/kg) a Sample or Composite Date .- Molybdenum Total Phosphorus• 1 __-_-_----_ a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Preparer * ZZ6-cG Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) Endw,onfi[FaM % hunuo @T&A CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 Sludge Analysis Method PARAMETERS Sample Date Analyst Code PH (not to be used for reporting) 3.9 04/10/18 JTH 4500HB-11 Aluminum, (dry wt. basis), mg/kg 17916 04/16/18 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg <2.5 04/18/18 MTM 311313-04 Calcium (dry wt. basis), mg/kg 16099 04/16/18 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg 1.1 04/23/1.8 MTM 3113B-04 Copper (dry wt. basis), mg/kg 247 04/16/18 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 13 04/16/18 LFJ EPA200.7 Lead (dry weight basis), Ong/kg 18 04/20/18 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 4632 04/16/18 LFJ EPA200.7 Mercury (dry wt, basis), mg/kg 0.49 04/17/18 MTM EPA7471B Nickel (dry wt, basis), mg/kg 13 04/16/18 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 7225 04/16/18 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 04/19/18 MTM 3113B-04 Sodium (dry wt. basis), mg/kg 3163 04/17/18 ONS 3111B-11 Zinc (dry wt. basis), mg/kg 651 04/16/18 LFJ EPA200.7 Total Nitrogen, mg/kg (talc) Lab Error Total Solids, % 1.73 04/10/18 KDS 2540G11 TKN (dry wt.), mg/kg c 39930 04/13/18 DTL 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 788.0 04/26/18 MF 350.1 R2-93 Nitrate Nitrogen(dry wt.), mg/kg Lab Error Nitrite Nitrogen(dry wt.), mg/kg c 1.00 05/04/18 CLO 353.2 R2-93 Phosphorus, T. (dry wt.), mg/kg c 27260 04/13/18 CLO 365.4-74 Molybdenum (dry wt. basis), mg/kg <5.0 04/16/18 LFJ EPA200.7 ID#: 416 DATE COLLECTED: 04/10/18 DATE REPORTED : 05/10/18 REVIEWED BY: c Uncertified data. DWR does not offer non-aqueoue certification for this analytical procedure. ti Dow0 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Nitrogen, mg/kg (calc) TKN (dry wt.), mg/kg Nitrate Nitrogen(dry wt.), mg/kg Nitrite Nitrogen(dry wt.), mg/kg Sludge Analysis Method Sample Date Analyst Code 56691 06/04/18 SEJ c 43740 05/15/18 TLH 351.2 112-93 c 12950 05/31/18 CLO 353.2 112-93 c 0.98 05/14/18 CLO 353.2 R2-93 ID#: 416 Y DATE COLLECTED: 05/10/18 DATE REPORTED : 06/04/18 REVIEWED BY: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. CMSD WWTP SAR Determination Lab data from aerobic sludge sampled 04/10/2018 by Environment 1, Inc. (mg/kg) % solids (mg/L) Equiv Weight Milli Equiv Sodium 3,163 1.57% 49.7 23 2.16 Calcium 16,099 1.57% 252.8 20 12.64 Magnesium 4,632 1.57% 72.7 12 6.06 SAR = Na Milli Equiv / [0.5'(Ca Milli Equiv + Mg Milli Equiv)]^0.5 SAR - 0.71 1. Design Considerations: Dates of Analysis: See Enclosed 2018 Data Assume subsurface application: Total dry tons per year = 291 TKN (mg/kg dry wt.) = 43,740 NH3-N (mg/kg dry wt.) = 788 NO2-NO3-N (mg/kg dry wt.) = 12,951 Rate, % of Organic-N Mineralization Rate = Year Organic-N (MR) (Aerobic Digestion) 0-1 30% 1-2 15% 2-3 7.50% 3-4 3.75% 4-5 1.88% 2. Plant Available Nitrogen (PAN): 1st Year PAN (mg/kg) _ ((MR) x (TKN - NH3)) + (NH3) + (NO2-NO3-N) 2-5 Year PAN (mg/kg) = Previous Year Pan + [(MR) x (TKN - NH3)] PAN (Ibs PAN/dry ton) = PAN (mg/kg) x 0.002 PAN (Ibs PAN/year) = PAN (Ibs PAN/dry ton) x Total dry tons per year Required Acres = PAN (Ibs/year) / Application Rate (Ibs PAN/ac yr) 1) For first year: PAN = 26625 mg/kg Loading 50 Rate 100 (Ibs PAN/ac 150 yr) 200 PAN = 53.25 Ibs/dry ton PAN = 15496 Ibs/year Required Acres 309.9 155.0 103.3 77.5 2) For second year: PAN = 33067 mg/kg PAN = 66.13 Ibs/dry ton PAN = 19245 Ibs/year Required Acres 384.9 192.5 128.3 96.2 3) For third year: PAN = 36289 mg/kg PAN = 72.58 Ibs/dry ton PAN = 21120 Ibs/year Required Acres 422.4 211.2 140.8 105.6 4) For fourth year: PAN = 37900 mg/kg PAN = 75.80 Ibs/dry ton PAN = 22058 Ibs/year Required Acres 441.2 220.6 147.1 110.3 5) For fifth year: PAN = 38705 mg/kg PAN = 77.41 Ibs/dry ton PAN = 22526 Ibs/year Required Acres 450.5 225.3 150.2 112.6 1. Design Considerations: Dates of Analysis: See Enclosed 2018 Data Assume surface application: Total dry tons per year = 291 TKN (mg/kg dry wt.) = 43,740 NH3-N (mg/kg dry wt.) = 788 NO2-NO3-N (mg/kg dry wt.) = 12,951 Rate, % of Organic-N Mineralization Rate = Year Organic-N (MR) (Aerobic Digestion) 0-1 30% 1-2 15% 2-3 7.50% 3-4 3.75% 4-5 1.88% 2. Plant Available Nitrogen (PAN): 1 st Year PAN (mg/kg) _ ((MR) x (TKN - NH3)) + (0.5 x NH3) + (NO2-NO3-N) 2-5 Year PAN (mg/kg) = Previous Year Pan + [(MR) x (TKN - NH3)] PAN (Ibs PAN/dry ton) = PAN (mg/kg) x 0.002 PAN (Ibs PAN/year) = PAN (Ibs PAN/dry ton) x Total dry tons per year Required Acres = PAN (Ibs/year) / Application Rate (Ibs PAN/ac yr) 1) For first year: PAN = 26231 mg/kg Loading 50 Rate (Ibs 100 PAN/ac 150 yr) 200 PAN = 52.46 Ibs/dry ton PAN = 15266 Ibs/year Required Acres 305.3 152.7 101.8 76.3 2) For second year: PAN = 32673 mg/kg PAN = 65.35 Ibs/dry ton PAN = 19016 Ibs/year Required Acres 380.3 190.2 126.8 95.1 3) For third year: PAN = 35895 mg/kg PAN = 71.79 Ibs/dry ton PAN = 20891 Ibs/year Required Acres 417.8 208.9 139.3 104.5 4) For fourth year: PAN = 37506 mg/kg PAN = 75.01 Ibs/dry ton PAN = 21828 Ibs/year Required Acres 436.6 218.3 145.5 109.1 5) For fifth year: PAN = 38311 mg/kg PAN = 76.62 Ibs/dry ton PAN = 22297 Ibs/year Required Acres 445.9 1 223.0 1 148.E 1 111.5 ANNUAL PATHOGEN AND VECTOR ATTRACTION RLDUUTION N'OKM (UT Kules) Facility Name: Contentnea MSD WWTP Name: Contentnea MSD Monitoring Period: From 1/1/2018 WQ Permit Number: NPDES Number: To 12/31/2018 WQ0001048 NCO032077 athogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)[] ................... AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density el Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ 1 Air Drying ❑ 1 Composting ❑ 1 Aerobic Digestion n is Digestion Anaerobic .......................................................... If applicable to alternative performed (Class A or Class B) complete the following monitorin data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- Frequency of Analysis Sample Type Analytical Tech- Minimurr Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN <11 117 1420 mVr t/ �75 0 7 Grab CFU 1000 mpn per gram of total solid (dry weight) "almonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑� Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." © "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Renee Smith/Land Application ORC Renee Srnith/Land Application ORC Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Lm-�a 3ignatur•e of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26) DENR FORM PVRF 02T (12/2006) Enviro �m # ,1 or F,Mho CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal Coliform (MPH /gram Solids Sample Analysis Method #1 Date Analyst Code 17520 04/02/18 KDS 2540B-11 451 04/02/18 KDS 9221E-06 ID#: 416 A DATE COLLECTED: 04/02/18 DATE REPORTED : 04/03/18 REVIEWED BY: 1-3 ❑ n lE it , _. _n CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal CoIiform (MPN), /gram Solids Sample Analysis Method N2 Date Analyst Cade 17680 04/03/18 3MT 2540B-11 130 04/05/18 3MT 9221E-06 ID#: 416 A DATE COLLECTED: 04/03/18 DATE REPORTED : 04/06/18 REVIEWED BY: t CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal Coliform (MPH /gram Solids Sample Analysis Method #3 Date Analyst Code 17220 04/04/18 AKS 2540B-11 64 04/04/18 AKS 9221E-06 ID#: 416 A DATE COLLECTED: 04/04/18 DATE REPORTED : 04/09/18 REVIEWED BY: "/—� ENW,nMR&RI % how Mdo CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal Coliform (MPH /gram Solids Sample Analysis Method #4 Date Analyst Code 16900 04/09/18 KDS 2540E-11 77 04/09/18 KDS 9221E-06 ID#: 416 A DATE COLLECTED: 04/09/18 DATE REPORTED : 04/12/18 REVIEWED BY: EIMUMMEMM % hCHR(was ud 5 114 UAKMUN I UHIVt rn NIC. 27835-7085 F CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 Sample Analysis Method PARAMETERS #5 Date Analyst Code Total Residue, mg/l 16580 04/10/18 JMT 254OB-11 Fecal Coliform (MPH /gram Solids 66 04/12/18 JMT 9221E-06 ID#: 416 A DATE COLLECTED: 04/10/18 DATE REPORTED : 04/12/18 REVIEWED BY: 756-0633 nv�ro meet 1, I �r Mgl CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/1 Fecal Coliform (MPN), /gram Solids Sample Analysis Method N6 Date Analyst Code 16880 04/11/18 KDS 2540E-11 1420 04/11/18 KDS 9221E-06 ID#: 416 A DATE COLLECTED: 04/11/18 DATE REPORTED : 04/16/18 REVIEWED BY: EmwknoW T, hcwpa ufflUd CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO, SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal Coliform (MPN), /gram Solids Sample Analysis Method N7 Date Analyst Code 16780 04/16/18 KDS 254OB-11 <11 04/16/18 KDS 9221E-06 ID#: 416 A DATE COLLECTED: 04/16/18 DATE REPORTED : 04/18/18 REVIEWED BY: /---- Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level WQ0001048 4/2/2018 17 1#2 7 7 7. 7. 7. Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: - I CJ7 Jrew -1 All 1000 milliliters 1.88 % Dry Solids 19 degrees Celsius 21 degrees Celsius 0.1 8.5 1.0 4.49 mg Oxygen/hr 0.24 mg Oxygen/g/hr 20 degrees Celsius 1 Temperature Corrected Specific Oxygen Uptake Rate:1 0.24 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically 8.8 8.6 8.4 8.2 8 E c 7.8 x O -a 7.6 d 0 N 7.4 0 7.2 7 6.8 6.6 y =-0.0749x + 8.621 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Time (minutes) Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 1 4/3/20181 8.41 8.38 8.26 8.18 8.14 8.08 8.02 7.92 7.84 7.74 7.64 7.67 7.47 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 1000 milliliters 1.82 % Dry Solids 19 degrees Celsius 20 dearees Celsius 0.1 8.6 1.0 4.64 mg Oxygen/hr 0.26 mg Oxygen/g/hr 20 degrees Celsius 1 Temperature Corrected Specific Oxygen Uptake Rate:1 0.26 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically. 8.8 - 8-6 8.4 8.2 8 7.8 T X O a� 7.6 0 N 7.4 in 7.2 7 6-8 6.6 y =-0.0774x + 8.6615 Oxygen Uptake Rate Chart I j - I I — I 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Time (minutes) Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Time Dissolved Oxygen Level (minutes) (m /1) 0 8.13 1 8.05 2 7.98 3 7.92 4 7.84 5 7.76 6 7.68 7 7.58 8 7.5 9 7.4 10 7.29 11 7.21 12 7.11 13 7.05 14 6.97 15 6.86 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 4/4/2018 18 Andrew Edwards 4-4-18/1319 00 milliliters 1.8 % Dry Solids 20 degrees Celsius 21 degrees Celsius 0.1 8.2 1.0 5.14 mg Oxygen/hr 0.29 mg Oxygen/g/hr 21 degrees Celsius 0.952380952 Temperature Corrected Specific Oxygen Uptake Rate:1 0.27 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically. &5 E 7.5 m X 0 Z w 7 y d 6.5 1.1 y =-0.0857x + 8.2493 Oxygen Uptake Rate Chart El I 3..� {'��'S I )"Y 3�'"k .[ �tt^'k��J #ffS'4 51w''?• �3' Ft t) )"i+n;lv '$"Y.{�{ it l;jk ItF 4,( h'(`i�5 ! � i131P SY Y t� Al ... �_ 1 i i I i I i I i i I 1 2 3 4 5 6 7 8 9 10 11 Time (minutes) 12 13 14 15 16 Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 3 4 5 6 7 8 0 11 12 13 14 15 Facility Name: CMSD Biosolids Permit Number: WQ0001048 Date: 4/9/2018 Digester Temperature: 16 Sampling Date/Time: 4-9-18/1350 Sampled By: Andrew Edwards Analysis Date/Time: 4-9-18/1400 Analyzed By: Renee Smith Sample Volume: 1000 milliliters Total Solids: 1.8 % Dry Solids Beginning Temperature: 18 degrees Celsius End Temperature: 18 degrees Celsius Dissolved Oxygen Level 8.5 8.4 8.4 8.4 8,3 8.3 8.2 8.1 8.1 80 8.0 77 7.7 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 0.1 8.6 1.0 3.28 mg Oxygen/hr 0.18 mg Oxygen/g/hr 18 degrees Celsius 1.1449 Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. ARM MI ca 8.2 E 0 7.6 7.4 7.2 y =-0.0546x + 8.6653 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1b �e Time (minutes) Specific Oxygen Uptake Rate SOUR Facility Name: CMSD Biosolids Permit Number: WQ0001048 Date: 4/16/2018 Digester Temperature: 19 Sampling Date/Time: 4-16-18/1305 Sampled By: Andrew Edwards Analysis Date/Time: 4-16-18/1310 Analyzed By: Renee Smith Sample Volume: 1000 milliliters Total Solids: 1.77 % Dry Solids Beginning Temperature: 19 degrees Celsius End Temperature: 19 degrees Celsius Time Dissolved Oxygen Level (minutes) (mg/1) 0 7.02 1 6.96 2 6.84' 3 6.76 4 6.67 5 6.62 6 6.54 7 6.49 8 6.44 9 6.3 10 6.23 11 6.17 12 6.08 13 5.97 14 5.92 15 5.83 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 0.1 7.0 1.0 4.70 mg Oxygen/hr 0.27 mg Oxygenlg/hr 19 degrees Celsius 1.07 Temperature Corrected Specific Oxygen Uptake Rate:1 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 8 7 6 a> 5 E 90 2 1 0 y =-0.0784x + 7.0935 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 10 11 12 13 14 1� ie Time (minutes) Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 7.8 7& 778 7. 776 7.5 775 774 774 73 772 72 7.1 7.1 70 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 4/17 4-17-18/1020 Kyle Huggins 4-17-1811030 Renee Smith )00 milliliters 1.8 % Dry Solids 17 degrees Celsius 19 dearees Celsius 0.1 7.9 1.0 3.48 mg Oxygen/hr 0.19 mg Oxygen/g/hr 18 degrees Celsius 1.1449 Temperature Corrected Specific Oxygen Uptake Rate: 0.22 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 8 7.8 a) 7.4 XI- 0 IM y =-0.058x + 7.9402 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 in Time (minutes) Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 9 10 11 12 13 14 15 Facility Name. Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time, Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 7.6, 7.5 75. 7.4 73 72, 7.1 7.1 70 6.9 68 6.7 6.7 6.6 6.5 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: CMSD WQ0001048 4/1812018 17 4-18-18/1035 Andrew Edwards 4-18-18/1045 Renee Smith 1000 1.79 18 0.1 7.7 1.0 Ililiters Dry Solids grees Celsius arees Celsius 4.48 mg Oxygen/hr 0.25 mg Oxygen/g/hr 19 degrees Celsius 1.07 Temperature Corrected Specific Oxygen Uptake Rater 0.27 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation. and the Spreadsheet execute automatically. ME 7.6 7.4 7.2 6.6 6.4 6.2 6 y =-0.0747x + 7.7778 Oxygen Uptake Rate Chart i 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 ie Time (minutes) �; � �: 1 _ `�.` , NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY19-SL009960 cuLr11{Y� Predictive Client: CMSD Advisor: Chris Whitehurst PO Box477 Ayden Nitrogen b Soil Report Mehlich-3 Extraction Grifton, NC 28530 P.O. Box 7 _ Ayden, NC 28513 Vy m Links to Helpful Information Sampled: 10/18/2018 Sampled County: Pitt Received: 10/25/2018 Farm: Not Provided Completed: 11/06/2018 Client ID: 147385 Advisor ID: 490477 Agronomist's Comments: ATTENTION: This report was flagged with a "C" and/or 2" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce potential for toxicity, especially for Zn. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped. The CTL for copper and zinc was set to prevent levels from accumulating to the point where they become toxic to crops grown on a field. Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 30 0 0 pH$ Z 0 0 Note: 12 Note: 2 -Bermuda hay/past, M 0.0 180-220 0 100 0 0 pH$ Z 0 0 Note: 12 Note: Test Results [units - WN in g/crrr3; CEC and Na in meg1100 crrr3; NO3-N in mg/dnfl: Soil Class: Mineral HM% WN CEC BS% Ac pH P-I K-1 Ca% Mg%a S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-Al Cu-I Na ESP SS-1 NO3-N 0.76 0.99 17.1 93 1.1 6.5 817 58 70 22 76 134 90 90 2884 2884 904 0.2 1 Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 20 0 0 0 Z 0 0 Note: 12 Note: $ 2- Bermuda hay/past., M 0.0 180-220 0 80 0 0 0 Z 0 0 Note: 12 Note: $ Test Results [units - WN in glcd; CEC and Na in meg1100 crrP; NO3-N in mgld[Tr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca%o Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.71 0.84 18.9 88 2.3 6.1 881 64 64 22 82 107 79 79 3202 3202 1296 0.2 1 North Carolina x i Tobacco Trust Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner nf Agriculture NCDA&CS nomic Division Phone: (919) 733-2655 Website: www.nc, )vlagronomi/ Report No. -SL009950 Page 2 of 3 Sample ID: 3 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 70 0 0 pH$ Z 0 0 Note: 12 Note: $ 2 -Bermuda hay/past., M 0.0 180-220 0 160 0 0 pH$ Z 0 0 Note: 12 Note: $ Test Results [units - WN in g/crrP; CEC and Na in meq/100 cm3; NO3-N in mg/dmr ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS -I NO3-N 0.76 1.08 19.2 98 0.4 6.9 893 32 75 22 69 89 56 56 3069 3069 1045 0.2 1 Sample ID: 4 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 70 0 0 pH$ 2 0 0 Note: 12 Note: $ 2-Bermuda hay/past., M 0.0 180-220 0 160 0 0 pH$ Z 0 0 Note: 12 Note: Test Results (units - WN in glcn�; CEC and Na in meq/100 crrr3; NO3-N in mg/dnft Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-Al Cu-I Na ESP SS -I NO3-N 0.66 0.90 20.7 93 1.5 6.5 1036 32 73 19 93 106 73 73 4403 4403 1295 0.2 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomil Report No. FY19-SL009960 Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1Mn-Al2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-1 M-O manganese index mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm, NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncaarpovlaaronornilobDart4.ht nd information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P206 phosphate S-1 sulfur index Test Results SS-1 soluble salt index WN weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-1, S-I, SS-1, Na, ESP, SS-1, NO3-N (not routine) Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaarpoylapronomiluyrst.htm NCDA&CS nomic Division Phone: (919) 733-2655 Website: www.nc; >v/agronomi/ Report No. SL009902 avcror�m, Predictive Client: CMSD Advisor: Chris Whitehurst PO Box 477 Ayden Nitrogen A Soil Report Mehlich-3 Extraction Grifton, NC 28530 P.O. Box 7 G. Ayden, NC 28513 ED`�,-Links to Helpful Information Sampled: 10/18/2018 Sampled County: Pitt Received: 10/25/2018 Farm: Not Provided Completed: 11/06/2018 Client ID: 147385 Advisor ID: 490477 Agronomist's Comments: ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce potential for toxicity, especially for Zn. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped. The CTL for copper and zinc was set to prevent levels from accumulating to the point where they become toxic to crops rown on a field. Sample ID: 5 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 0 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - W1V in g/carp; CEC and Na in meq/100 cn3; NO3-N in mg/dnr ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.66 0.74 21.0 87 2.8 6.0 930 83 63 22 102 89 70 3974 3974 1314 0.3 1 Sample ID: 6 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu- B Information Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 20 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - W/V in glcrO; CEC and Na in meg1100 cm3; NO3-N in mg/dO]: Soil Class: Mineral HM% W1V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.66 0.77 22.3 88 2.7 6.1 912 65 65 21 102 102 77 5253 5253 1490 0.4 2 North Carolina Tobacco Trust Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY19-SL009902 Page 2 of 11 Sample ID: 7 Recommendations: Lime Nutrients (Ib/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 30 0 0 pH$ Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/crn3; CEC and Na in meq/100 crrr3; NO3-N in mg/dnn ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.76 1.02 16.8 96 0.7 6.9 815 56 72 22 57 138 86 2403 2403 580 0.2 1 Sample ID: 8 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 50 0 0 pH$ Z 0 0 Note: 12 Note: $ 2 - 0.0 Test Results [units - WN in g/crn3; CEC and Na in meg110D crag; NO3-N in mg/drrt3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0,76 0,98 17.4 95 0.9 6.8 885 43 71 22 65 118 76 2859 2859 749 02 1 Sample ID: 9 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 60 0 0 pH$ Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cnP; CEC and Na in meq/100 crrr3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.76 0.96 17.0 96 0.6 7.0 699 38 74 22 72 103 64 2087 2087 630 0.2 1 Sample ID: 10 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 30 0 0 pH$ Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cnr3; NO3-N in mg/drr> ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 0.99 16.6 92 1.3 6.7 793 61 67 23 59 131 86 3259 3259 803 0.2 1 NCDA&CS comic Division Phone: (919) 733-2655 Website: www.nca vlagronomi/ Report No. I SL009902 Page 3 of 11 Sample ID: 11 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 0 0 0 pH$ Z 0 0 Note: 12 Note: $ 2 - 0.0 Test Results [units - WN in glcmr ; CEC and Na in meq/100 cm3; NO3-N in mgfdm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.46 0.83 23.4 94 1.4 6.7 829 81 69 24 74 124 80 5985 5985 1700 0.3 1 Sample ID: 12 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 50 0 0 pH$ Z 0 0 Note: 12 Note: $ 2 - 0.0 Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mgldrrt ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.71 1.15 12.8 93 0.9 6.7 741 45 71 21 57 152 98 2401 2401 603 0.2 2 Sample ID: 13 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 10 0 0 pH$ Z 0 0 Note: 12 Note: $ 2 - 0.0 Test Results [units - WN in g/crrr3; CEC and Na in meq/100 crrr ; NO3-N in mgldni]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 0.97 20.3 94 1.2 6.7 874 77 70 22 67 149 96 4883 4883 1197 0.2 1 Sample ID: 14 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 10 0 0 pH$ Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meg1100 cO; NO3-N in mg/drr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS -I NO3-N 0.60 0.93 19.9 93 1.4 6.7 817 78 70 21 67 144 93 4791 4791 1171 0.2 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY19-SL009902 Page 4 of 11 Sample ID: 15 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 70 0 0 pH$ 0 0 0 Note: 12 Note: 2- 0.0 Test Results [units - W[V in g/cm3; CEC and Na in meg1100 crn3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.37 1.13 10.8 95 0.6 6.9 154 36 69 24 60 86 55 697 697 133 0.2 2 Sample ID: 16 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 70 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in glca; CEC and Na in meq/100 crrr3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.02 1.12 8.9 87 1.1 6.4 362 36 65 21 51 84 62 883 883 268 0.2 2 Sample ID: 17 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., E 0.0 60-80 0 80 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 1.25 1.16 8.0 86 1.1 6.2 176 31 65 19 51 73 58 487 487 112 0.2 3 Sample ID: 18 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 70 0 0 pH$ 0 0 0 Note: 12 Note: $ 2- 0.0 Test Results [units - WN in glcm3; CEC and Na in meq/100 crrr3; NO3-N in mg/dr0]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.81 1.09 10.0 92 0.8 6.7 442 33 66 25 60 83 57 969 969 237 0.2 2 NCDA&CS , iomic Division Phone: (919) 733-2655 Website: www.nca v/agronomil Report No. I SL009902 Page 5of11 Sample ID: 19 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 1.1 60-80 0 70 0 0 0 Z 0 0 Note: 12 Note: $ 2- 0.0 Test Results [units - WN in glcd; CEC and Na in meq/100 cm:3; NO3-N in mgldnt ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 0.99 10.3 77 2.4 5.5 953 36 57 18 78 98 76 2053 2053 619 0.2 2 Sample ID: 20 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: i -Bermuda hay/past., E 0.0 60-80 0 80 0 0 pH$ 0 0 0 Note: 12 Note: 2- 0.0 Test Results [units - WN in glcrrr3; CEC and Na in meq/100 crrr3; NO3-N in mg/dO]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-I Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.97 1.04 12.1 91 1.1 6.6 754 29 66 24 64 84 58 1687 1687 424 0.2 2 Sample ID: 21 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Bermuda hay/past., E 1.1 60-80 0 60 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in g/cr&; CEC and Na in meg]100 cn>3; NO3-N in mg/do]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 1.25 0.92 11.6 77 2.7 5.6 875 38 56 19 90 87 69 1667 1667 582 0.3 3 Sample ID: 22 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 1.0 60-80 0 60 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 crrP; NO3-N in mg/dnr ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-Al Cu-1 Na ESP SS -I NO3-N 0.60 0.98 11.9 78 2.6 5.6 962 40 57 20 80 83 67 1567 1567 651 0.2 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.neagr.gov/agronomi/ Report No. FY19-SL0O9902 Page 6 of 11 Sample ID: 23 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 80 0 0 pH$ 0 0 0 Note: 12 Note: 2- 0.0 Test Results [units - WN in g/crrt3; CEC and Na in meq/100 cr13; NO3-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%, S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.81 1.08 11.0 98 0.2 7.2 344 29 71 26 64 111 65 715 715 236 02 2 Sample ID: 24 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 50 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in glcnr3; CEC and Na in meq/100 crrr3; NO3-N in mg/dnr3]: Soil Class: Mineral HM% W1V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-1 Na ESP SS-1 NO3-N 0-66 1.05 10.1 89 1.1 6.5 562 43 68 19 55 100 70 1103 1103 386 0.2 2 Sample ID: 25 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 1.1 60-80 0 50 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in g1crrr3; CEC and Na in meq/100 cnr3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.25 0.99 9.9 76 2.4 5.5 716 45 59 15 71 110 83 1645 1645 596 0.2 2 Sample ID: 26 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 0.5 60-80 0 50 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in g1crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.43 1.05 9.5 80 1.9 5.8 570 47 63 15 64 83 67 1336 1336 353 0.2 2 NCDA&CS A :)mic Division Phone: (919) 733-2655 Website: www.ncao dagronomil Report No. F ;L009902 Page 7 of 11 Sample ID: 27 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 60 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in g/cnt3; CEC and Na in meq/100 cm3; NO3-N in mgldr&]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.84 1.00 11.6 85 1.7 6.1 456 41 66 18 58 80 64 1406 1406 382 0.2 2 Sample ID: 28 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 0.3 60-80 0 50 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - W/V in glcrrr3; CEC and Na in meq/100 crrr3; NO3-N in mg/dn'�]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-I Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 3.19 0.96 12.4 81 2.4 5.9 708 47 61 18 60 81 66 1887 1887 542 0.2 2 Sample ID: 29 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 40 0 0 0 0 0 0 Note: 12 2- 0.0 Test Results [units - WN in glcrrP; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class. Mineral HM% W!V CEC BS% Ac pH P-I K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.87 0.98 11.8 85 1.7 6.1 670 53 65 18 57 83 65 1601 1601 416 0.2 2 . Sample ID: 30 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 30 0 0 0 Z 0 0 Note: 12 Note: 2- 0.0 Test Results [units - W!V in g/crrr3; CEC and Na in meq/100 crrr3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-AI1 Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 2.15 0.93 13.9 86 2.0 6.0 715 61 69 15 60 85 68 2654 2654 705 0.2 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.neagr.gov/agronomi/ Report No. FY19-SL009902 Page 8 of 11 Sample ID: 31 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 0.3 60-80 0 40 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WfV in glcn4; CEC and Na in meq/100 cm3; NO3-N in mg/daft Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.80 0.90 13.6 84 2.2 5.9 808 51 67 15 60 88 70 3555 3555 890 0.2 1 Sample ID: 32 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2Os K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 40 0 0 pH$ Z 0 0 Note: 12 Note: $ 2 - 0.0 Test Results [units - W!V in g1crrr3; CEC and Na in meq/100 crrP; NO3-N in mg/drrr3]: Soil Class: Mineral HM% W!V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.25 1.06 13.5 91 1.2 6.5 846 49 70 19 47 63 47 3018 3018 749 0.2 1 Sample ID: 33 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 70 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g1crrr3; CEC and Na in meq/100 cO; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% 3-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.51 1.08 10.4 89 1.1 6.4 558 36 64 23 46 80 59 1499 1499 368 0.1 1 Sample ID: 34 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.6 60-80 0 60 0 0 0 Z 0 0 Note: 12 Note: $ 2 - 0.0 Test Results [units - WN in g/crrr3; CEC and Na in meq/100 crrr3; NO3-N in mgldd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.46 0.96 13.0 81 2.5 5.8 951 39 59 21 72 85 68 2545 2545 774 0.2 2 NCDA&CS , omic Division Phone: (919) 733-2655 Website: www.nca v/agronomi/ Report No. F 51_009902 Page 9 of 11 Sample ID: 35 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 20 0 0 0 Z 0 0 Note: 12 Note: $ 2- 0.0 Test Results [units - WN in g1cm3; CEC and Na in meq/100 cnr3; NO3-N in mg/drr�]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-Al Cu-1 Na ESP SS-1 NO3-N 0.61 0.90 17.9 86 2.5 6.0 1056 62 62 22 93 76 63 4172 4172 1074 0.3 2 Sample ID: 36 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 40 0 0 pH$ Z 0 0 Note: 12 Note: 2- 0.0 Test Results [units - WN in g/crrr3; CEC and Na in meq/100 crnr ; NO3-N in mgldm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.02 0.93 182 92 1.4 6.6 888 48 67 24 75 94 65 2825 2825 686 0.3 2 Sample ID: 37 Recommendations: Lime Nutrients (Iblacre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 50 0 0 pH$ 0 0 0 Note: 12 Note: 2- 0.0 Test Results [units - WN in g/cm3; CEC and Na in meg1100 crn3; NO3-N in mg/daft Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.51 1.21 7.4 94 0.4 6.9 302 42 68 23 30 100 64 711 711 157 0.1 1 Sample ID: 38 Recommendations: Lime Nutrients (Ib/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 0.3 60-80 0 30 0 0 0 Z 0 0 Note: 12 Note: 2- 0.0 Test Results [units - WN in glcm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.60 1.02 13.1 82 2.4 5.9 865 57 59 21 74 75 62 2269 2269 718 0.2 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY19-SL009902 Page 10 of 11 Sample ID: 39 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 50 0 0 0 Z 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - WN in g/crap; CEC and Na in meq/100 crn3; NO3-N in mgldrre ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 0.89 16.1 86 2.3 6.1 957 42 62 23 69 52 47 3745 3745 896 02 1 Sample ID: 40 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda haylpast., E 1.8 60-80 0 70 0 0 0 Z 0 0 Note: 12 Note: $ 2 - 0.0 Test Results [units - WN in glcrrr3; CEC and Na in meq/100 cnr3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 0.90 11.7 71 3.4 5.3 950 36 54 16 72 72 60 3001 3001 920 0.1 1 NCDA8.CS iomic Division Phone: (919) 733-2655 Website: www.ncz Wagronomil Report No. I SL009902 Page 11 of 11 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r is applied. if MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source-, 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients- In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations forsmall areas, such as home lawnslgardens, are listed in units of Ib/1000 sq ft . if you cannot find the exact fertilizer grade recommended on the report, visit www.ncagraovlapronomilobpart4.htm1#sfind information that may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer Test Results The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement Visit www.ncaoraoWaaronomiluyrst.htm Report Abbreviations Ac exchangeable acidity B boron BS% WCEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-1 sulfur index SS-1 soluble salt index WN weight per volume Zn-Al zinc availability index Zn-I zinc index d� Statement Page: 1 Ayden Nitrogen Statement Date: 01/3112019 4728 Old NC 11 / P.O. Box 7 ID: 010202 Ayden, NC 28513 Total Balance: $1,858.96 Phone 252-746-2152 Contentnea Metro Sewage Dist s Po Box 477 Amount Remitted: Grifton, NC 28530 Terms: Unless otherwise agreed in writing by Harvey Fertilizer & Gas Co, interest will accrue at a periodic rate of 1.5% per month. To avoid additional finance charges, payments must be in office by last day of month. ------- .. i---------Your Share .........I Date Number Description I Detail Quantity Price I Unit Extension / Prepaid Regular Balance Forward 0.00 8.00 Payments 01/22/2019 1004981 Regular Payment I Cash Payment 8.00 -8.00 Payment Total 8.00 0.00 •8.00 01/29/2019 1014967 Charge Invoice - Due 02/28/2019 GPS Fees 73.620 Acre 8.000 /Acre 588.96 588.96 Dolomitic lime - Bulk 20.320 Tons 49.000 Irons 995.68 995.68 App Fees Materials 20.320 Each 13,500 ]Each 274.32 274.32 Invoice Total 1,868.96 0.00 1,858.96 Ending Total Balances 0.00 1,8.58.96 Current 1 - 30 31 - 60 61 - 90 Over 90 Unapplied Budget Billing Prepay Overall 1,858.96 0.00 0.00 0.00 0.00 0.00 0.00 0.00 1,858.96 401 J{ Ayden Nitrogen Date: 01/31/2019 Contentnea Metro Sewage Dist fry' * _lip , : GPI-59A COMPLIANCE REPORT FORIiI Permit &0000C)01C�09 (Submil one each monitoring period with G1,V 59 forms.) 1 Enter date monitoring results were due. ( " -. -1 ) Will this monitoring report (GIN-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance, �( 4 Are any monitored constituents equal to or above the established standards? YfS NO If the answer to question 4 is NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentrations) exceeding standards in the space provided below: t,Jell :F 10 CY)r0 YYIum 16 uq 1'L 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituents) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). I,Je11`#10 Chfo�ni Lry) i4LkgjL-- (p-Z7-11 lc?(?Il 10 ChrCY )iui'n 15L,91C� i(1-11-1i t,�}�.II �10 G�iCt'ni{.U'n lr-tUl�1C. 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. if the answer is "NO", monitoring wells may be.improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties, �-hem+c ma�i+cf Qi�d�V alum � a I k '� �ue5 g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge.that the above information was evaluated,and the information submitted inthis repoft (Compliance Report GW-590is true and complete fo the best of my knowledge. �n f 43-/9 Signature of Permittee (or Authorized Agent) Date GW-59A 12/8/2003 Ah SUBMIT FORM ON &UW PAPER ONLY r� Nor GROUNDWATER QUALITY MONITORING: DEPARTMENT OF,.ENVIRONMENTAL QUALITyY DIV{ OF WATER iiE50URCES iNFORMA'n�'N,PRocEssING UNIT` COMPLIANCE REPORT FORM F f-- YrN �'iti`l+�ZcBC+17-��.� �1[4 1617MAILSEWCECENTER RALEIGH„NC��Z75991617 Phone 919SB07G308� °,,. FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: -zp7Q Facility Name: jen` nica_ m.Q Non -Discharge LJ tCOJOL g UIC Permit Name (if different): Y, .eT 4 NPDES i`ICC0-,Zb)__) Other Facility Address: TYPE OF PERMITTED OPERATION BEING MONITORED Grl�tO� NC Z�530 County i — ❑ Lagoon ❑ Remediation: infiltration Gallery „.Ay' �'«� _,�, ❑ Spray Field ❑ Remediation: Contact Person:1?i1L°��(711� �1 Telephone#: �6z-6ZLP56qLI ❑ Rotary Distributor 1Y Land Application of Sludge Well Location/Site Name:y5y. C g¢ C>� J)}On-F ,fit { No. of wells to be sampled: - ❑ Water Source Heat Pump ❑ Other: (from Pemuq SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): cl Date sample collected: Z-2D-r'd FIELD ANALYSES: WAS Well Depth: ig ft. Well Diameter: 7_ in. pH 00400:4W units Temp. 000io: JL0 °C DRY at Depth to Water Level 82546: (a ft. below measuring point Screened Interval: 3 ft. to ft. Spec. Cond. 00094: µMhos time of Measuring Point is �. 5 ft. above land surface Relative M.P. Elevation: ft. Odor 000s5: rune- sampling, check Volume of water pumped/bailed before sampling: �7 gallons Appearance C)C)(_O q here:❑ Samples for metals were collected unfiltered: EX YES ❑ NO and field acidified: (R] YES ❑ NO LABORATORY INFORMATION Date sample analyzed: = Z&-jg _ Laboratory Name: EnNI fcnyr cn+1- j f1C Certification No. I PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD oo33s mg/L Nitrite (NO2) as N oo6is mg/L Pb - Lead oiosi ug/L Coliform: MF Fecal 31616 < /100mL Nitrate (NO3) as N 00620 D,cko mg/L Zn - Zinc D1092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P oo665 mg/L (Note_ use MPN method for highly turbid samples) Orthophosphate 70507 P Q • OZ mglL Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 /)% mg/L AI - Aluminum oilo5 mg/L pH (Lab) 00403 4. (4q units Ba - Barium 01C07 ug/L TOC 00680 q.qz mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 Cj ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg1L Hg - Mercury 71goo ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 000gs gD,Fj µMhos K - Potassium 00937 mg/L VOC 7673 method # Total Ammonia oo6lo a Y� mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3 as N: Ammonia Nitrogen, Total) Mn - Manganese moss - ug/L , method # _ TKN as N 00625 mg/L Ni - Nickel olos7 ug1L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg1L Effluent Total VOCs: mg/L VOC Removal% Permittee (or Authorized Agent) Name and Title - GW-59 Rev.3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Print Cleady or Type Facility Name: Permit Name (if di Facility Address: GM Contact Person: I �n>°e 6rf- l d-h Telephone#: Well Location/Site Name: �_ p� Gi eid j: LQ No. of wells to be sampled PERMIT Number: Expiration Date:-�l-Zp7O Non -Discharge Q(� C)OOi 0 Q UIC NPDESOther TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ® Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): I Date sample collected: Z-Zl?-i (W Well Depth: qft. Well Diameter: Z- in. Depth to Water Level 82546: �j ft. below measuring point Screened Interval: 2 ft. to �`• g p ft. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: gallons Samples for metals were collected unfiltered: (2 YES ❑ NO and field acidified: ® YES ❑ NO FIELD ANALYSES: pH 00400:5-C� units Temp. 000io: i �j °C Spec. Cond. 000sa: �7. y µMhos Odor 000as: r)ont Appearance C-yea If WELL WAS DRY at time of sampling, check here-.❑ LABORATORY INFORMATION Date sample analyzed: 2 Zo ! Laboratory Name: f ai-ECrfyeni rj )r�c_ Certification No. 1D PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. _ COD 00335 mg/L Nitrite (NO2) as N omis mg/L Pb - Lead o1o51 ug/L Coliform: MF FeC21 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 1100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 C), (j3 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total70300 S Ll mg/L AI - Aluminum oiios mg/L pH (Lab) 00403 15. DC4 units Ba - Barium 01007 ug/L TOC 00660 3. mg/L Ca - Calcium oogi6 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 16 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 4p,p(p mg/L ORGANICS: (by GC, GC1MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71goo ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 51 .0 /tMhos K - Potassium OD937 mg/L VOC 7873 method # Total Ammonia o0610 <O• OQ mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3 as N: Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% - G\A -- Rev.3-1-2016 SUBMIT FORM ONAdkOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FAr'fl ITY IAIFr1PMAT1rINI Please Prfnt Clearly orTvAe Facility Name: Permit Name (if di Facility Address: 'iw Contact Person: i)Pn-a- 6`pj �_n Telephone#: Well Location/Site Name: 6 c7-� }-ilr i IQ No. of wells to be sampled: S WELL ID NUMBER (from Permit): j u Date sample collected: Z Zb- l9 Well Depth: �ft. Well Diameter: Z in. Depth to Water Level B2546: "D ft. below measuring point Screened Interval: ft. to I _�) ft. Measuring Point is Z ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: ® YES ❑ NO :RMIT Number: Expiration Date: I-�.��7C� ,n-Discharge ❑OC)tcL1q UIC 'DES iy1000'JZQ Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor 1Y Land Application of Sludge ❑ Water Source Heat Pump ❑ Other. If WELL FIELD ANALYSES: WAS pH ooaoo: 4 25 units Temp. 000la: 1 °C DRY at Spec. Cond_ 000ga: µMhos time of sampling, Odor 00085: (XY) check Appearance ^i here:❑ Date sample analyzed: 2-zc�- I� Laboratory Name: fCf�f11eni � l �l�-- PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead olosi Coliform: MF Fecal 31616 < /100ml- Nitrate (N%) as N 00620 0),LJrip mg/L Zn - Zinc 01092 Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid sampled Orthophosphate 70507 0, 0 (— mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 4_� mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 L .q �j units Ba - Barium 01007 ug/L TOC oo68o . U L'19 mg/L Ca - Calcium oog16 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 7 ug/L Certification No. l (j ug/L mg/L Grease and Oils 00552 mg/L Cu - Copper 01042 CQ, Qjp mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance ooc95 ('z'L4 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia oo610 C)y mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3as N: Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug1L , method # TKN as N oos25 mg/L Ni - Nickel 01067 uglL method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% -_� tnt&rniLl') (end )A URI tCfAw ©2L Permittee (or Authorized Agent) Name and Title - Please print or type - GW-59 Rev.3-1-2016 Permittee (or Authorized Agent) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if di Facility Address: Please Print CJearty or N l L6rD DU County Em IContactPerson: ►�t?s}ee�ml Telephone#: nz-�7L4-5 Well Location/Site Name:iSSQIGILI 4- Z1glD No. of wells to be sampled: WELL ID NUMBER (from Permit):. 15 Date sample collected: z7c,-ig Well Depth: q ft. Well Diameter: Z in. Depth to Water Level 52546: ft. below measuring point Screened Interval: 3 ft. to '? ft. Measuring Point is Z . S ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: © YES ❑ NO RMIT Number: Expiration Date:_ 1-31-ZUZ0 n-Discharge tx3QCWko4� UIC ,DES f-.-tCC C 7-6;F) Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ® Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL FIELD ANALYSES: WAS pH 00400: 4Irl units Temp. 000lo: )- ? °C DRY at Spec. Cond. 000ea: �� µMhos time of u� i sampling, Odor omm ��r t7Q(�{ check Appearance t ✓icar here:a Date sample analyzed: r ZD-1'� Laboratory Name: !%1i �CY)m ent S/ arc PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO.) as N oo615 mg/L Pb - Lead o1o51 Coliform: MF Fecal 31616 < { /100ml- Nitrate (NO3) as N 00620 p, 5Z mg/L Zn - Zinc olo92 Coliform: MF Total 31504 /100ml- Phosphorus: Total as P oo665 mg/L N PN h d f h' hl t b'd I Certification No. {Q ug/L mg/L ( ote. Use M met o or ig y ur i samp es) Orthophosphate 70507 p D- OZ mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 Q15 mg/L AI -Aluminum o1105 mg/L pH (Lab) 00403 L+ �G units Ba - Barium 01007 ug/L TOC oo68o Q .5� mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 Cp.QI (j mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance a=5 � (� µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia oosio �.Z�. mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3 as N: Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00525 mg/L Ni - Nickel 01067 ug1L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% �r1�� Jmi4 Lgn6 r4PD{t C6-h&) 2C.. Permittee (or Authorized Agent) Name and Title - Please print or type GV' -- Rev. 3-1-2016 (Date) SUBMIT FORM ON PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: (na-D Permit Name (if different): ff{ 6D Facility Address: Cj Do ()_)y j-e f) j '-�C'bp,G Co-) WC County Contact Person: P11 f',� �yjm I Telephone#: 1r_5Z-rj ZQ_ Well Location/Site Name: b.) 0-G No, of wells to be sampled: PERMIT Number: Expiration Date: f-3I_ 7() Non -Discharge WQQCGIO(-i-�g UIC NPDES .�iJJ�7LO-) Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ® Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION ) If WELL WELL ID NUMBER (from Permit): Date sample collected: FIELD ANALYSES: WAS Well Depth: ic) ft. Well Diameter: Z in. I Fj pH ooaoo:� units Temp. 00010: °C DRY at Depth to Water Level 92546: ft. below measuring point Screened Interval: J ft. to )D ft. Spec. Cond. 00094: ) (P µMhos time of Measuring Point is eft. above land surface Relative M.P. Elevation: ft. Odor 00085: noj)f sampling, check Volume of water pumped/bailed before sampling: '5 gallons Appearance C1eaf here:❑ iSamples for metals were collected unfiltered: R YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION (� Date sample analyzed: Laboratory Name: rN i (Qnma-)-i �T� nc. Certification No. )Q PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 C /100mL Nitrate (NO3) as N 00620 �,�t mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P om6s mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 0.()1 mg/L Other (Specify Compounds and Concentration Units): ]issolved Solids:Total 70300 IZ�J mg/L AI -Aluminum o11o5 mg/L pH (Lab) C0403 units Ba - Barium 01007 ug1L TOC oo660 (p .71j mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 (p ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <Q,UIb mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug1L Fe - Iron 01045 ug/L (Specify test and method.#. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 (G µMhos K - Potassium o0937 mg/L VOC 7673 method # 'Total Ammonia ooslo mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese oio55 ug/L method # TKN as N 00625 mg/L Ni - Nickel o1067 ug/L method # Fnr Rpmprliatinn SVCtpmR nnh/ (Gttarh I nh PmnnrFcl- Infl ... nf TMl \Inf`— --/I mtn,...... T. l \ rnr - Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.3-1-2016 fflN"T@MbP � T, hmpumbCol P.O. BOX 7085, 114 OAKMONT DRIVE PHONE (252) 756-62 GREENVILLE, N.C.27835-7085 FAX (252) 7S6-0633 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 ID#: 416 DATE COLLECTED: 02/20/18 DATE REPORTED : 03/08/18 REVIEWED BY: Well Well Well Well PARAMETERS #9 #10 #14 #15 Fecal Coliform (MF), 1100 Ms < 1 < 1 < 1 < 1 Ammonia Nitrogen as N, mg/l 0.37 <0.04 <0.04 0.25 Nitrate Nitrogen as N, mg/l 0.06 0.28 0.46 0.52 Total Organic Carbon, mg/l 8.82 3.59 1.46 9.58 Total Dissolved Residue, mg/l 76 54 47 95 Total Chromium, ug/1 9 15 7 8 Copper, ug/l < 10 < 10 < 10 < 10 Conductivity (at 25c), uMhos/cm 80.5 57.4 62.4 78.0 Total Ortho-Phosphate as P, mg/l 0.02 0.03 0.02 0.02 Weil Analysis Method #18 Date Analyst Code < 1 02/20/18 KAC 9222D-97 0.06 03/06/18 ME[,' 350.1 R2-93 0.04 02/28/18 DTL 353.2 R2-93 6.75 02/21/18 SEJ 531OC-11 129 02/22/18 KAC 2540C-11 6 02/26/18 LFJ EPA201 < 10 02/26/18 LFJ EPA20 149 02/26/18 JTH 251OB-11 0.01 02/21/18 SEJ 450OPE-11 GW-59A COMPLIANCE REPORT FORM Permit # OCMIG(Pq (Submit one each monitoring period with Gff,' 59 forms.) 1 Enter date monitoring results were due. ( ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES 1Np 7� IF the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor welts in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Officefor guidance. 4 Are any monitored constituents equal to or above the established standards? YfS NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in ,the space provided below: Wjj TCC 1C).2)1rq)L oa1*15TCG Ii-aZrrqlL Weil 4-10 Chforf1i upn iL g ICr 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YE$ NO same constituent(s) in the same well(s) in the last two years? \]/ !f the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES"' list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). sveit *i -FOG � ZG_, (I IkXIN 1'510C- to ,LPrnq'/c-14^1(> Ueii loC �a�,ticr� i5�q�' 'iDC PO.Somq/L 10-3' o klejI+1D Chromsum lLjuq)t. 1--7,2-1-) 2-ZoI .-roC JZ.IC�rng/� ZZZ-n Drorrt Um 16lL vn-1 ) -rocl tFZ•1Zrtt�/L !e-Z! I"3 Chrcrni4m jail )L t0-'I!-n 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NQ �( If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is `WO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is havinq at the review and compliance boundaries surrounding this facility Failure to do so may subiect the permittee to a Notice of Violation, fines, and/or penalties. �]0plDU-kZ - i-)aeo l t) Otall viola-�Mt) aril k'ea(-e LOLO� r ,4� +r n,k, tY`oni-k Y Of)d G(Ctt uLt4P, Q I) i 5.'1-tom . S The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I(hereby3acknowedge that titeliover)niorratEonfvv�s,evalGatetlFa tifefinformat�an submitted )�hs'�{ report;(Compli�ce�Report GW`59A) js true.e��com„plete?foytFie{tiesfof my�}knowledge -,._. ,,.;;�,F ,__._.,�� hmv jK, Signature of Permittee (or Authorized Agent) Date GW-59A 12/8/2003 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: NFOI2M4'T10 N 15 ' - ; COMPLIANCE REPORT FORM 1as1LsrIc�cEN�u> t��,;zss¢�tr� rtioe-s3o FACILITY INFORMATION Please Print Cleady orType PERMIT Number: Expiration Date: _ I_;Zlj_ZDZC) Facility Name: ec— Non -Discharge QQQCQIC4-9 UIC Permit Name (if different): 'ea_n) D NPDES 1-400DZ2c ) Other Facility Address: Q1 I` C' �'ll1 -) TYPE OF PERMITTED OPERATION BEING MONITORED (j 4CI- (Street) CU 530 County_1+ ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (Slate) (Zip) ❑ Spray Field El Remediation: Contact Person: j)�enf_f_ 6IY)1gj1-) Telephone#: 42-5Z46594 ❑ Rotary Distributor 1% Land Application of Sludge Well Location/Site Name:,UJ P-6 �e C>.V t) IQn-�oiff. No. of wells to be sampled:1 ❑ Water Source Heat Pump ❑ Other: ffmm P.—M WELL ID NUMBER (from Permit): Date sample q p le collected: �-2d"1q Well Depth: gft. Well Diameter. Z. in. Depth to Water Level 92646: U-5 ft. below measuring point Screened Interval: 3 ft. to ft. Measuring Point is Z• 5 ft. above land surface Relative M.P. Elevation: ft. Volume of'water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: YES ❑ NO FIELD ANALYSES: pH oosoo: 4.C1 I units Temp. OOD10: ZS eC Spec. Cond. 00094: („5- D µMhos Odor 000ss: fiCnl Appearance etpudy WAS DRY at time ofsampling, check here:❑ LABORATORY INFORMATION Date sample analyzed: &-Zp-i ___ Laboratory Name: LfWI O ' t ( E()C . Certification No. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead olos1 ug/L Coliform: MF Fecal 31616 < 1 /100mL Nitrate (NO3) as N oosao d,c),5 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 . /100mL Phosphorus: Total as P o0665 mg/L (Note: Use MPN method for Nghly turbid samples) Orthophosphate 70507 (2). 10 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 03 mg/L AI - Aluminum o11os mg/L pH (Lab) 00403 4. [ units Ba - Barium 01007 ug/L TOC oosao 1o.2:) mg/L Ca - Calcium oo916 mg/L Chloride oosao mg/L Cd - Cadmium of o27 ug/L Arsenic oioo2 uglL. Chromium: Total 01034 ug1L Grease and Oils 00552 mg/L. Cu - Copper 01042 <Q .Ol O mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug1L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 jp�j • O 11Mhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia oosao o •1LA mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; N113as N; Ammonia Nitrogen. Total) Mn - Manganese o1o55 ug/L method # TKN as N 00625 L mg/L- Ni - Nickel oios7 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOc Removal h 1�• ec6m,Jan LQnd P,oaiC 4cr\cpc-(— Permittee (or Authorized Agent) Name and Title - P ease print or type Gt Rev.3-1-2016 Agent) (Date) N .Z. Ubrvli 11-UMM UN YHYttC VNL7 ATER QUALITY MONITORING: CE REPORT FORM Clearly or Type Facility Name: Permit Name (if different): Facility Address: County (city) (Scale) (Zip) Contact Person: Telephone#: aMZ(-jr6'%4 Well Location/Site Name: 686 ty-A No. of wells to be sampled: 15 PERMIT Number: Expiration Date:j_�Zn Non -Discharge , 01C% 'q UIC NPDES . Ncod-aw)) Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Feld ❑ Remediation: ❑ Rotary Distributor 56 Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): Q Date sample collected: FIELD ANALYSES: WAS Well Depth: ft. Well Diameter. Z in. pH 00400:5.fq units Temp. 000lo: Zlo °C DRY at Depth to Water Level 62546: 3, Fj ft. below measuring point Screened Interval: Z fL to'q ft. Spec. Cond. 00094: J`t. µMhos time of sampling, Measuring Point is 3 ft above land surface Relative M.P. Elevation: ft. Odor 000e5: ncn-e- check _ Volume of water pumped/bailed before sampling: 5 gallons Appearance (G� here:❑ Samples for metals were collected unfiltered: [K] YES ❑ NO and field acidified: [)9 YES ❑ NO LABORATORY INFORMATION Date sample analyzed: -Z�-I� Laboratory Name: 7-7hvIron men-} Yr I1^C Certification No. l� PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb -Lead oiosi ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NOs) as N 00620 ©;) Cp mg/L. Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: use MPN method for highly titrbidsamples) Orthophosphate 7oso7 Q. I l.p mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 C q mg/L Al - Aluminum o11os mg/L pH (Lab) 00403 5, iG units Ba - Barium 01007 ug1L TOC oosso mg/L Ca - Calcium oo916 mg/L Chloride 00940 mg/L Cd - Cadmium 01627 ug/L Arsenicoloo2 ug/L Chromium: Total01034 j(o ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <o.o to mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 7190D ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 000gs 5 `. µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <Q. QW mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese oloss ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% 1 certify that, to the best of my knowledge and behcf, the information submitted in this report is true, accurater and complete. and that the laboratory analydical data was produced us ng approved methods of analysis by a D1NR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. ft pi � I Permittee (or Authorized Agent) Name and T'itle - Pliase print or type Signature of PerinittLe (or Authorized Agent) D_ SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if different): Facility Address: C C FI r`� (Stree� Z 30_ County Contact Person: 'P)'P (fee6 1 1IV') Telephone#: Well Location/Site Name: i I W ` No. of wells to be sampled: PERMIT Number: Expiration Date: I-a51-LOLU Non -Discharge 0QO001Q4tS UIC NPDES W_0()320_q Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor M Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMI'l-MU INrUKMAI IUN WELL ID NUMBER (from Permit): I L4 Date sample collected: �1 Well Depth:ft. Well Diameter: _7L in. Depth to Water Level 82546: ft. below measuring point Screened Interval: b_ft. to (3 ft. Measuring Point is Z ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: �j gallons Samples for metals were collected unfiltered: [I YES ❑ NO and field acidified: �Z) YES ❑ NO If WELL FIELD ANALYSES: WAS pH 004005•05 units Temp_ 000lo: - °C DRY at time of Spec. Cond. 000sa: %2.9 µMhos sampling, Odor 00065: nant check Appearance 0'6a( here: El ate sample analyzed: r.., 10 b Laboratory Name: �J1V I l (7(11 (lit Certification No. lQ ARAMEi'ERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead oiosi ug/L Coliform: MF Fecal 31616 1 /100mL Nitrate (NO3) as N 00620 C) , Q mg/L Zn -Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 0 - 04 mg/L Other (Specify Compounds and Concentration Units): ssolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 . units Ba - Barium 01007 ug/L TOC 00680 2 3 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium olo27 ug/L Arsenic 01002 ug/L Chromium: Total 01034 4z ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 CO, O10 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) peck Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7673 method # Total Ammonia oo6io <� .� mg/L Mg - Magnesium oo927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese otoss ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug1L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L inTnuenr i oiat vut✓s: Iny,L V V%. nCnrvvar i° GV Rev.3-1-2016 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM ...�,..,... Y...., Pfe: Facility Name: Permit Name (if different): Facilitv Address: QC or)ype SUBMIT FORM ON OW PAPER ONLY - Flll[s1IL•;It�ki� County {Cilyj �L [, �� (Stale) tz,p) . Contact Person: I){�-ee �)(t(h Telephone#: Z,�7-�JZ�(—J Well Location/Site Name:1,RfC'Gffa4) 1L- S�z_I-q(0 No. of wells to be sampled: PERMIT Number: Expiration Date: L-31 O ZO Non -Discharge LL)('1o00)D410 UIC NPDES EILLO �� Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Land Application of Sludge ❑ Water Source Heat Pump ❑ Other. SAMPLING INFORMATION WELL ID NUMBER (from Permit): 5 Date sample collected: FIELD ANALYSES: If WELL WAS Well Depth: g ft. Well Diameter tin. pH 00400:6.0 units Temp. 00010: Z5 °C DRY at 5 ft. below measuring point Depth to Water Level 62546: L g p Screened Interval: 3 ft. to ft. Sec. Cond. aoosa: �,,. t_} µMhos p time of sampling, Measuring Point is -Z. 15 ft. above land surface Relative M.P. Elevation: ft. Odor 000lls: nDn�:C check Volume of water pumped/bailed before sampling: 5 gallons Appearance G1?Q( here: El Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: D5YES ❑ NO Date sample analyzed: ZOJ'g Laboratory Name: &-yl W (Y)ef)+ S t ( Certification No. 6© PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo6i5 mg/L Pb - Lead oio51 ug/L Coliform: MF Fecal 31616 1 /100mL - Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507' ©p-0 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 j co mg/L Al -Aluminum oilo5 mg/L pH (Lab) 00403 5.13 units Ba - Barium 01007 ug/L TOC 00660 j j 4Z mg/L Ca - Calcium oosi 6 mg/L Chloride 00940 mg/L Cd - Cadmium olo27 ug/L Arsenic olooz ug/L Chromium: Total 01034_ -_ uglL Grease and Oils 00552 mg/L Cu - Copper 01042 GO•p{ 0 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron oio45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 /)3-L A µMhos K - Potassium oo937 mg/L VOC 7873 method # Total Ammonia 00610 ©.Zg mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NHaas N: Ammonia Nitrogen. Total) Mn - Manganese oio55 ug/L method # TKN as N oos25 mg/L Ni - Nickel olo67 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Land AmiiC'1 cf)pQ ,- Permiftee (or Authorized Agent) Name and Tdle - Please print or type GW-59 Rev.3-1-2016 of Permittee (or Authorized Agent) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: (COMPLIANCE REPORT FORM Please Facility Name: Permit Name (if different): Facility Address: qQ( tzp) rri act Person: �P� _e-&p 1G"1 Telephone# raj?-�JJ4 6. 4 Location/Site Name: No. of wells to be sampled: PERMIT Number: Expiration Date: Non -Discharge )Jc�cg UIC NPDES �4MO3W`)-) Other TYPE OF PERMITTED OPERATION BEING MONITORED" ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Feld ❑ Remediation: ❑ Rotary Distributor �d Land Application of Sludge ❑ Water Source Heat Pump ❑ Other. SAMPLING INFORMATION WELL. ID NUMBER (from Permit): 119 Date sample collected: ('-ZL7-I Q __ FIELD ANALYSES: If WELL WAS Well Depth: in Well Diameter: -7--in. pH ooaoo: '61 units Temp. 00010: ZZ °c DRY at Depth to Water Level 82546:_ft. below measuring point Screened Interval: __f;ft. to i © ft. Spec. Cond. 000ga: ) µMhos time of sampling, Measuring Point is Z_ft above land surface Relative M.P. Elevation: ft. Odor 00085: I"1C e, check Volume of water pumpedlbailed before sampling: 5 gallons Appearance Gj' here:a Samples for metals were collected unfiltered: a] YES ❑ NO and field acidified: YES ❑ NO 1t3UKAI UM 1l`lr-VrcwlA1!vim ate sample analyzed: Laboratory Name: (WMCI) 1RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead o1o51 Coliform: MF Fecal 31616 I 1100mL Nitrate (NO3) as N 00620 0 , (j (� mg/L Zn - Zinc 01092 Certification No. 10 ug/L mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P ooe65 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 Q , QZ mg/L Other (Specify Compounds and Concentration Units): ,solved Solids:Total 703DO 1) mg/L Al - Aluminum o11 os mg/L pH (Lab) 00403 5. ;yl units Ba - Barium o1oo7 ug/L TOC 00680 mg/L Ca - Calcium oog16 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug1L Chromium: Total o1o34 <5.p ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <C3. d 10 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug1L Lab Report Attached? ❑ Yes (1) ❑ No (0) lecific Conductance 00095 1 ip i µMhos K - Potassium 00937 mg/L VOC 7673 method # Total Ammonia 00610 8 . Cif mg/L Mg - Magnesium oog27 mg/L method # (Ammonia Nitrogen: NH3as N: Ammonia Nitrogen, Total) Mn - Manganese oims ug/L , method # TKN as N 00626 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOGs: mg/L vvc Kemovaa io Gb Rev.3-1-2016 ��wonumM Ta ~BOX 7085, 114 OAKMONT DRIVE P 252756-6208 GREENVILLE, N.C. 27835-7085 FAX (252) 756-0633 ID#: 416 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN DATE COLLECTED: 06/20/18 P.O. BOX 477 DATE REPORTED : 07/11/18 GRIFTON ,NC 28530 PARAMETERS Fecal Coliform (MY), /100 Mls Ammonia Nitrogen as N, mg/l Ammonia Nitrogen as N, mg/1 Nitrate Nitrogen as N, mg/l Total Organic Carbon, mg/l W Dissolved Residue, mg/1 tal Chromium, ug/l Copper, ug/1 Conductivity (at 25c), uMhos/cm Total Ortho-Phosphate as P, mg/I REVIEWED BY: Well Well Well Well N9 #10 1/14 #15 <1 <1 <1 1 0.74 <0.04 < 0.04 0.28 0.05 0.76 0.78 0.07 10.27 5.44 2.39 11.92 73 48 37 100 8 16 8 7 <10 <10 <10 <10 65.0 51.8 50.9 73.4 0.10 0.16 0.04 0.07 Well Analysis Method #18 Date Analyst Code < 1 06/20/18 JMH 9222D-06 06/26/18 TLH 350.1 112-93 0.09 06/28/18 DTL 350.1 R2-93 0.06 07/10/18 CLO 353.2 R2-93 6.81 06/28/18 SEJ 531OC-11 118 06/21/18 JMT 2540C-11 <5,0 06/27/18 LFJ EPA200.7 <10 06/27/18 LFJ EPA200.7 161 06/25/18 HMM 251OB-11 0.02 06/20/18 SEJ 450OPE-11 GW-59A COMPLIANCE REPORT FORM Permit #VI( (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. ( Ii- b--1 ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? . V 2 Was any required information missing on the GW-59 report forms? YES NJ iF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing "Yes", Office YES NO identification plate, area overgrown, etc.)? If the answer is contact the Regional for guidance. 4 Are any monitored constituents equal to or above the established standards? Y,)L,S NO If the answer to question 4 is `NO", skip to section 8. if the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: tot? i 1 4' 7(YC I-7 •06 "/(- i,�e►I +o C)fcm'mam I4UgfC- U�ii G C-C-Wl Ckdarn 5) iCGrn i 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? � / y If the answer to question 5 is NO , skip to section 8. if the answer to question 5 is "YES"' fist in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). ili2li G ��G l�''ul-ily i0.50t'rjiL iJEII�i©�t�'iUm Z72-0 Id IL >474,49Cn `^ Z-22-17 12• I0 pri L 16-1 J-1 Vim, l <�%L_ u21r 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES �Ip X if the answer is "YES". a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. if the answer is "NO") monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this WS NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days: an evaluation may b e required to determine the impact the waste disposal system Is having at the review and compliance boundaries surrounding this facility Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. HCDEAJZ'DtL)Q-0QfM 15 ai,��re o�ane�ia �'� and u- hWe-been t�cl �l n$ ojak-) 44)?j-yiq0 rncn1iiCY Q0d E rCdLtOe c141 I - dUfS - g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. he.�eb►acknovietlgetha2�theialiove mfo�matior3 wa> valuated Xr therinlormatio t�btj�ltted+�jth9ss epor(Complianee;Rep"ort GWr59A) fs true and cornpleteto the.;lest of ►iiykno`ivledg 5`LL ti x, �, , Signature of Permittee (or Authorized Agent) Date GW-59A 12/8/2003 SUBMIT FORM ON YFLI.OW PAPER ONLY GROU%___ _TER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Facility Name: �_Or Permit Name (if different): Facility Address: GN) County (city) (Slate) tziD) act Person: '1 Telephone#:�Z Location/Site Nameisk) d:A(a,(op flNo. of wells to be sampled: /YELL ID NUMBER (from Permit): Nell Depth: ft. Depth to Water Level 82546: L4 ft. below measuring point Measuring Point is Z. ft. above land surface Volume of water pumped bailed before sampling: 15 Samples for metals were collected unfiltered: N YES ❑ PERMIT Number: Expiration Date: Non -Discharge {,t1049 UIC NPDES 1pCC(��U7__ Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Feld ❑ Remediation: ❑ Rotary Distributor (� Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: ((>24-I� Well Diameter. Z in. Screened Interval: ft. to 9 ft. Relative M.P. Elevation: ft. gallons NO and field acidified: DYES ❑ NO FIELD ANALYSES: pH oo400: units Temp. 000lo: 2-1 °C Spec. Cond. o0oe4: i 05 µMhos Odor 00085: r-)on� Appearance drew ,UL)KAIVKT IryrUM1Vtii11V1V Ite sample analyzed: IC>- (kIQ Laboratory Name: &:,(.I roni'Yl_T) inc, kRAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2_) as N 00615 mg/L Pb -Lead o1os1 Coliform: MF Fecal 31616 < ! /100mL Nitrate (NO3) as N 00620 <C),C)4 mg/L Zn - Zinc 01092 MF T t 1 /100ml- Phosphorus: Total as P 00665 mg/L Certification No. IO ug/L mg/L Collform. o a 315oa (Note: Use MPN method for higfily turbid samples) Orthophosphate 70507 a. (mg/L Other (Specify Compounds and Concentration Units): solved Solids:Total 70300 qQ mg/L A] - Aluminum 01105 mg/L pH (Lab) 00403 U. Z units Ba - Barium 01007 uglL TOC 00680 mg1L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug1L 11 Chromium: Total 01034 Q ug/L DRY at time of here:❑ Arsenic 01002 Grease and Oils 00552 ug mg/L Cu - Copper 01042 <(3,� mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug1L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? n Yes (1) ❑ No (0) 1 method # (p ) Conductance 00095 ) QFj µMhos K - Potassium 00937 mg/L VOC 7873 )ecific Total Ammonia 00610 (� . �j mg/L Mg - Magnesium 00827 mg/L method # (Ammonia Nitrogen: 1,11•13as N; Ammonia Nitrogen. Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel o1067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: LandAwlCoMpC Permittee (or Authorized Agent) Name and Tdle - Please print or type GW-59 Rev.3-1-2016 mg/L Effluent Total • • plate and that the laboratory analytical data was produced using approved methods of analysis by a possibility of fines and imprisonment for knowing violations117�, 1. 1 ►1i - Wignirture of Permittee (or Authorized Agent) .. SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if different): Facility Address: C((CC (State) (zip) Cleady or Type County IContact Person:-eneubm-I it--h Telephone# Z62-504 Well Location/Site Name:_ c P F e-16 # 4A No. of wells to be sampled: RMIT Number: Expiration Date: n-Discharge LJQGIoi(0Ug UIC 'DES V4CCC3z0-)`-? Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Feld ❑ Remediation: ❑ Rotary Distributor ® Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL 1D NUMBER (from Permit): ) 0 Date sample collected: FIELD ANALYSES: WAS Well Depth: qft. Well Diameter. Z in. pH oo400:-�L-6 units Temp. 000lo: ZZ °C DRY at Depth to Water Level 82546ft. below measuring point Screened Interval: Z ft. to ft. Spec. Cond. 000sa: 50 7 µMhos time ofsampling, Measuring Point is ft. above land surface Relative M.P. Elevation: fL Odor 00085: ('1CXo•e check Volume of water pumped bailed before sampling: 5 gallons Appearance (-i ru here:❑ Samples for metals were collected unfiltered: m YES ❑ NO and field acidified: 9 YES ❑ NO LABORATORY INFORMATION Date sample analyzed: jQ-ZLt -I� Laboratory Name: Erw'i fC()(�f'f 1rnf_ i1c_- Certification No. 10 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 /100ml- Nitrate (NO3) as N 00620 0, Iq mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPNmethod for highlyturbid samples) Orthophosphate 70507 Q-oig mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 U 5 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 Q. (.v units Ba - Barium 01007 ug/L TOC ooseo Cj.(45 mg/L Ca - Calcium oosls mg/L Chloride oosao mg/L Cd - Cadmium 01027 ug/L Arsenic o1om ug/L Chromium: Total o1o34 14 ug/L Grease and Oils ooss2 mg/L Cu - Copper 01042 <p. COIF mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and metho"d�(#. ATTACH LAB REPORT.) Sulfate oosas mg/L Hg - Mercury 71900 ug/L Lab Report Attached? pf� Yes (1) ❑ No (0) ecific Conductance 00095 µMhos K - Potassium oOs37 mg/L VOC 7873 method # 6zooC- Total Ammonia ooseo Q. 10 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N: Ammonia Nitrogen. Total Mn - Manganese oloss ug/L method # TKN as N oos25 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee (or Authorized Agent) Name and TiUe - Please print or type GV Rev.3-1-2016 SUBMIT FORM ON OW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM or Facility Name: Permit Name (if di Facility Address: act Person: f.6mi4.h Telephone#: 7-5Z4�544 Location/Site Name: s6 ©- t44)j { jQ�_ No. of wells to be sampled: (p RMIT Number: Expiration Date: 1- LWZD n-Discharge kEC00(C'0'9 UIC 'DES t4�)M37o"7) Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor SLand Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): I U Date sample collected: !C Z449 Well Depth: � ft. Well Diameter: in. P „-L_ � Depth to Water Level 62646: j,5 ft below measuringMhos point Screened Interval: _� ft to J3 ft Measuring Point is Z ft above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: IN YES ❑ NO and field acidified: CA YES ❑ NO FIELD ANALYSES: H o0400: (o p 4 units Temp. 000la: 7� °G Spec. Cond. 000s4: ! • D µ Odor 00085: nrn-e Appearance CjQU If WELL WAS DRY at time of sampling, check here - LABORATORY INFORMATION Date sample analyzed: Laboratory Name: EM,1Qn>fl�7-} J {()(-'. Certification No. ) D PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o5i ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 j,ZC� mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 irj, � mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 5o mg/L Al -Aluminum o11os mg/L pH (Lab) 00403 (4- co units Ba - Barium 01007 ug/L TOC oo66o 3, (a2 mg/L Ca - Calcium oos16 mg/L Chloride oos4o mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 <5 , Q ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <0 , Ol © mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron of 045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? tZ Yes (1) ❑ No (0) Specific Conductance 00095 ). © µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 i� •7� mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen Ni3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% 1 certify that. to the best of my kno,vlzdgz and befFef, the information submittzd in this report is true. accurate and camplete and that thz laboratory analytical data was produczd using approved methods of analysis by DWP.-certified laboratory. I am aware that there arz signrficant penalties for submitting false mformallon including the pcssibdity of fines and impnsonment for knowing violation=_. rA 4,g , li i cnck }�. i j�• It Permittee (or Authorized Agent) Name and Title - Please print or type SigrWure of Permittee (or Authorized Agent) r► D_ SUBMIT FORM ON YFI I OW PAPER nNl V GROUNDWATER QUALITY MONITORING: REPORT FORMsR�ICEc • • •IrNon-Discharge tme tVl'Cn1fIKVNMt , lP - UIv U /fil1E ESOFIRG 1N�OR t lI0 ROClSSI a# 3COMPLIANCE G ssg�D6 ,FACILITY INFORMATION PleasePdnfCleadyorType Number: Expiration Date: Facility Name: Omf � -�_ rn `6D Oawpicw UIC Permit Name (if different): I _&j0L' 7t01 Other Facility Address: j�j fsnreei) �� tf7� TYPE OF PERMITTED OPERATION BEING MONITORED f(�- 1 +Z County_ P(+-i' ❑Lagoon ❑ Remediation: Infiltration Gallery fCiry'l (Slate) (Zip) ❑ Spray Field ❑ Remediation: Contact Person:} ; t 1 Telephone#: ZZ_ J5A-� 9 (f ❑ Rotary Distributor CA Land Application of Sludge Well Location/Site Name: j C} 6Cf,,40n dZ CC71(I w-6Z j Q I O No. of wells to be sampled: Lip� ❑ Water Source Heat Pump ❑ Other. WELL ID NUMBER (from Permit): [ 5 Date sample collected: I C)Z4-!(3 Well Depth: 9 ft. Well Diameter. _Z_ in. Depth to Water Level 82546: a ft. below measuringpoint Screened Interval: 3 ft. to P � ft. Measuring Point is Z _ 5 ft. above land surface Relative M.P. Elevation: ft Volume of water before sampling: pumped/bailed P g: gallons Samples for metals were collected unfiltered: (N YES ❑ NO and field acidified: C9 YES ❑ NO FIELD ANALYSES: pH ooaoo:O-Z units Temp. aoolo: Zy C Spec. Cond. 000sa: f ZCf µMhos Odor 000m: nor)t Appearance Ci�.f WAS ~� DRY at time of sampling,check here:❑, LABORATORY INFORMATION Date sample analyzed: 1Q-ut-19 Laboratory Name: &)VllCYi CYion-t YI Certification No. j (3 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead olos1 ug/L Coliform: MF Fecal 31616/100mL Nitrate (NO3) as N o0620 d - C-L mg/L Zn - Zinc oio92 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P ooms mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 C) .03 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 iZ,5 mg/L AI -Aluminum o1105 mg/L pH (Lab) 00403 4.2- units Ba - Barium 01007 ug/L TOC 006BO mg/L Ca- Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic olom ug/L Chromium: Total 01034 '� ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <0, ©ip mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron oloas ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? V Yes (1) ❑ No (0) Specific Conductance coo95 jZ9 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 Q _ gZ mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N oo625 mg/L Ni - Nickel o1o67 ug/L method # t-or memewatlon systems curly (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permnttee (or Authorized Agent) Name and Trtle - Please print or type GV Rev.3-1-2016 Agent) SUBMIT FORM ON PAPER ONLY ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM or Name: Name (if different): Address: -Ni County Contact Person: 7?)ey—e- 6"-f),Iyjn Telephone#: Well Location/Site Name: cani j No. of wells to be sampled: RMIT Number: Expiration Date: n-Discharge toQOCOICY4 UIC 'DES LCLC3.2GD Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor rA Land Application of Sludge ❑ Water Source Heat Pump ❑ Other. WELL ID NUMBER (from Permit): I Date sample collected: Well Depth: 4? ft. Well Diameter. in. Depth to Water Level 82546:yftbelow measuring point Screened Interval: Z ft to ft. Measuring Point is 7---33 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 'S gallons Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: EX YES ❑ NO FIELD ANALYSES: pH o0400: 4. ) units Temp. 00010: 70 °C Spec. Cond. oaoea: U% (o µMhos Odor 00085: ncn'e. Appearance GOB )Z ` 7 WAS DRY at time ofsampling, check here:❑ LABORATORY INFORMATION Date sample analyzed: I Laboratory Name: EiN1(c n-)a� -T Certification No. 10 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 006515 mg/L Pb - Lead oiosi ug/L Coliform: MF Fecal 31616 G ` /100ML Nitrate (NO3) as N 00620 O ZU mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 315o4 /100mL Phosphorus: Total as P oo665 mg/L (Nate: Use MPN method for highly turbid samples) Orthophosphate 70507 Q. Id mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 69 mg/L Al - Aluminum oilos mg/L pH (Lab) 00403 4-1 units Ba - Barium oioo7 ug/L TOC oo6so (p•15 mg/L Ca - Calcium oo916 mg/L Chloride 00940 mg/L Cd - Cadmium oi027 ug/L Arsenic oloo2 ug/L Chromium: Total olo34 r] ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <Q 010 mg/L ORGANICS. (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron oioa5 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? T� Yes (1) ❑ No (0) Specific Conductance 000g5 L,G(o. Co uMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 Q I� mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3 as N; Anmonia Nitrogen, Total) Mn - Manganese oio55 ug/L method # TKN as N 00625 mg/L Ni - Nickel oio67 ug/L method # For Remediation Systems Only (Attach Lab Reports): Irifluent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev_ 3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Print Clearly or Facility Name: -i e-( D_ IYN (� Permit Name (if different): Facility Address: L760 VJ ! 1,04 CL,.%- nt County act Person: � �� 1t p �\I � Ill Telephone#- (4 Location/Site Name: 0 C)-� )✓=i 0 d *3 No. of wells to be sampled: Lp WELL ID NUMBER (from Permit): 143 Date sample collected: } &-Z4-► 9 Well Depth: 10 ft. Well Diameter. in. Depth to Water Level 82546: j,p ft. below measuring point Screened Interval: 5 ft. to _Loft. Measuring Point is _7__ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: CR YES ❑ NO RMIT Number: Expiration Date: n-Discharge (,t)QG1MC ? UIC 'DES W_) ) Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation. ❑ Rotary Distributor MI -and Application of Sludge ❑ Water Source Heat Pump ❑ Other. WELL FIELD ANALYSES: WAS pH 00400: 4.3 units Temp. 000lo: zb °C DRY at Spec. Cond. 000e4: 1 Co µMhos time of sampling, Odor00065: i)C3n check Appearance 010a here:❑ ate sample analyzed: Laboratory Name: (ill (�l`ll�i� Z) �{� • Certification No. I CD kRAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead olo5l ug/L Coliform: MF Fecal 31616 l 1100mL Nitrate (NO3) as N 00620 0 -07 mg/L Zn -Zinc 01o92 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 0 .01 mg/L Other (Specify Compounds and Concentration Units): ,solved Solids:Total 70300 1 w5 mg/L Al -Aluminum oilos mg/L pH (Lab) o0403 4-_5 units Ba - Barium 01007 ug1L TOC 00660 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium oto27 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 5 ug1L Grease and Oils 00552 mg/L Cu - Copper 01042 40, QI © mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug1L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 719DO ug/L Lab Report Attached? [�( Yes (1) ❑ No (0) ,ecific Conductance 000gs I µMhos K - Potassium oo937 mg/L VOC 7673 method # Total Ammonia 00610 0 ZA mg/L Mg - Magnesium 00e27 mg/L method # (Ammonia Nitrogen: NH3as N; Ammonia Nitrogen, Total) Mn -Manganese o1055 ug/L ,method # TKN as N 00625 mg1L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% ifflec mla () Lam A joa_�+m 0a, Permittee (or Authorized Agent) Name and Title - Please print or type Signature of GW Rev, 3-1-2016 EflW1H3c@[MffM@flq Tg D�c�oQpoQa�c�d r-T J/-1f\]VIIJIY t v1 It v �. GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 10/24/18 DATE REPORTED : 11/15/18 REVIEWED BY: Well Well Well Weil Well PARAMETERS #9 #10 #14 #15 #17 Fecal Coliform (MF), /100 Mls < 1 < 1 < 1 5 < 1 Ammonia Nitrogen as N, mg/1 0.83 0.10 0.26 0.82 0.13 Nitrate Nitrogen as N, mg/1 <0.04 0.19 1.29 0.12 0.26 Total Organic Carbon, mg/1 17.06 4.45 3.42 9.74 6.15 'P-tal Dissolved Residue, mg/1 90 45 50 125, 59 tal Chromium, ug/1 8 14 <5.0 7 7 cropper, ug/1 < 10 < 10 < 10 < 10 < 10 Conductivity (at 25c), uMhos/cm 105 $0.7 71.0 129 46.6 Total Ortho-Phosphate as P, mg/l 0.09 0.08 0.03 0.03 0.10 Analysis Method Date Analyst Code 10/24/18 JMT 9222D-06 10/29/18 DTL 350.1 R2-93 10/26/18 DTL 353.2 R2-93 10/24/18 SEJ 531OC-11 10/25/18 JTH 2540C-11 10/26/18 LFJ EPA200.7 10/26/18 LFJ EPA200.7 10/29/18 JMS 251OB-11 10/24/18 SEJ 450OPE-11 EMw'0w@flH(W % hwomho GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIPGEN P.O. BOX 477 GRIFTON ,NC 28530 Well Analysis Method PARAMETERS #18 Date Analyst Code Fecal Coliform (MF), /100 Mls <1 10/24/18 JMT 9222D-06 Ammonia Nitrogen as N, mg/l 0.24 10/29/18 DTL 350.1 112-93 Nitrate Nitrogen as N, mg/l 0.07 10/26/18 DTL 353.2 R2-93 Total Organic Carbon, mg/l 7.05 10/24/18 SEJ 531OC-11 Total Dissolved Residue, mg/1 145 10/25/18 JTH 254OC-11 Total Chromium, ug/l 5 10/26/18 LFJ EPA200.7 Copper, ug/l <10 10/26/18 LFJ EPA200.7 Conductivity (at 25c), uMhos/cm 107 10/29/18 JMS 2510E-11 Total Ortho-Phosphate as P, mg/l 0.01 10/24/18 SEJ 450OPE-11 1-AA kZ5?-) 100-U0,50 ID#: 416 DATE COLLECTED: 10/24/18 DATE REPORTED : 11/15/18 REVIEWED BY: /- -- --- ENAmERM % hCupumbd 114 0ANVIVIV I L1r11 V C GREENVILLE, N.C. 27858 FAX (252) 756-0633 CLIENT: CMSD (SLUDGE & WELLS ACCT) CLIENT ID: 416 CONTENTNEA METRO. SEWAGE DIST. M5. RENEE PRIDGEN ANALYST: KPG P.O. BOX 477 DATE COLLECTED: 10/24/18 Page: 1 GRIFTON, NC 28530 DATE REPORTED: 11/15/18 REVIEWED BY: VOLATILE ORGANICS ennnr+_i 9 Date Analyzed: PARAMETERS, ug/l 10/26/18 Well //9 10/26/18 Well #10 10/27/18 Well #14 10/27/18 Well #15 /27/18 :::Well 7 <0.50 <0.50 <0.50 <OSO <0.50 1. Benzene < 0.50 <0.50 < 0.50 < 0.50 < 0.50 2. Bromobenzene <0.50 <0.50 <0.50 <0.50 <0.50 3. Bromochloromethane <0.50 <0.50 <0.50 <0.50 <0.50 4. Bromodichloromethane <0.50 < 0.50 <0.50 <0.50 <0.50 5. Bromoform <0.50 <0.50 <0.50 <0.50 <0.50 6. Bromomethane <0.50 <0.50 <0.50 <0.50 <0.50 7. N-Butylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 8. Sec-Butylbenzene <0.50 <0.50 <.0.50 <0.50 <0.50 9. Tert-Butylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 10. Carbon Tetrachloride < 0.50 <0.50 < 0.50 < 0.50 <0.50 11. Chlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 12. Chloroethane <0.50 <0.50 <0.50 <0.50 <0.50 13. Chloroform <0.50 <0.50 <0.50 <0.50 <0.50 n 1 4. Chloroa <0.50 <0.50 <0.50 <0.50 <0.50 1. 2-Chlometh e < 0.50 < 0.50 < 0.50 <0.50 < 0.50 16. 4-Chlorotoluene <0.50 <0.50 <0.50 <0.50 <0.50 17. Dibromochloromethane <0.50 <0.50 <0.50 <0.50 <0.50 18. 1,2-Dibromo-3-Chloropropane <0.50 <0.50 <0.50 <0.50 <0.50 19. 1,2-Dibromoethane <0.50 <0.50 <0.50 <0.50 <0.50 20. Dibromomethane <0.50 <0.50 <0,50 <0.50 <0.50 21. 1,2-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 22. 1,3-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 23. 1,4-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 24. Dichlorodifluoromethane <0.50 <0.50 <0.50 <0.50 <0.50 25. 1,1-Dichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 25. 1,2-Dichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 26. 1,1-Dichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 ethe 27. Cis-1,2-Diroeth ethane <0.50 < 0.50 < 0.50 < 0.50 < 0.50 29. trans,2-Dic ichlo ene <0.50 <0.50 <0.50 <0.50 <0.50 30. 1,2-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 31, 1,3-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 32 . 2,2-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 33. 1,1-Dichloropropene <0.50 <0.50 <0.50 <0.50 <0.50 34. Cis-1,3-Dichloropropene <0.50 <0.50 <0.50 <0.50 <0.50 35. trans-1,3-Dichloropropene <OSO <0.50 <0.50 <0.50 <0.50 Ethylb nzene 36. Ethy}benzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 37. tadiene Hexacpylben tadene <0.50 <0.50 <0.50 <0.50 <0.50 38. < 0.50 < 0.50 < 0.50 <0.50 < 0.50 39, 4-Isopropyltoluene <0.50 <0.50 <0.50 <0.50 <0.50 40. Methylene Chloride <0.50 <0.50 <0.50 <0.50 <0.50 Naphthalene 41 . Naphthalene <0.50 <0.50 <0.50 <0,50 <0.50 42. Propyl <0.50 <0.50 <0.50 <0.50 <0.50 43. Styrene 44. 1,1,1,2-Tetrachloroethane <0.50 <0.50 <0.50 <0.50 . <050 <0.50 <0.50 <0.50 45. 1,1,2,2-Tetrachloroethane <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 46. Tetrachloroethane <0.50 <0.50 <0.50 <0.50 <0.50 47. Toluene Enw,umummIR alp hcupmOd I 1`f V/1/\IVIV Iv I I- II v I GREENVILLEI N.C. 27858 CLIENT: CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON, NC 028530 REVIEWED BY: /f VOLATILE ORGANICS ,vnr,n c�nnf'I_'t'I I , /' CLIENT ID: 416 ANALYST: KPG DATE COLLECTED: 10/24/18 DATE REPORTED: 11/15/18 756-62 756-0633 Page: 2 Date Analyzed; PARAMETERS, ug/I 10/26/18 Well N9 10/26/18 Well l/10 q#14 10/27/18 Well #15 10l27/18 Well #17 48. 1,2,3-Trichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 49. 1,2,4-Triehlorobenzene <0.50 <0.50 <0.50 .<0.50 <0.50 <0.50 <0.50 50. 1,1,1-Trichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 51. 1,1,2-Trichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 52. Trichloroethene < 0.50 < 0.50 < 0.50 < 0.50 <0.50 53. Trichlorofluoromethane <0.50 <0.50 <0.50 <0.50 <0.50 54. 1,2,3-Trichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 55. 1,2,4-Trimethylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 56. 1,3,5-Trimethylbenzene <0.50 < 0.50 < 0.50 <0.50 < 0.50 C 57. Vinyl Chloride orielenes < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 57. Total l 59, Methyl Tert Butyl Ether < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 EMAUTammW % hmpumho , ,Y JAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON, NC 28530 REVIEWED 8Y: VOLATILE ORGANICS STD. METHODS 620OC-11 CLIENT ID: PHONE (252) 756-6208 FAX (252) 756-0633 416 ANALYST: KPG DATE COLLECTED: 10/24/18 DATE REPORTED: 11/15/18 Date Analyzed: PARAMETERS, ug/l 10/27/18 Well #18 1. Benzene <0.50 Z. Bromobenzene <0.50 3. Bromochloromethane <0.50 4. Bromodichloromethane <0.50 5. Bromoform <0.50 6. Bromomethane <0.50 7. N-Butylbenzene <0.50 S. Sec-Butylbenzene <0.50 9. Tert-Butylbenzene <0.50 10. Carbon Tetrachloride <0.50 11. Chlorobenzene <0.50 12. Chloroethane <0.50 13. Chloroform < 0.50 14. Chloromethane <0.50 15. 2-Chlorotoluene < 0.50 16. 4-Chlorotoluene < 0.50 17. Dibromochloromethaue <0.50 18. 1,2-Dibromo-3-Chloropropane < 0.50 19. 1,2-Dibromoethane < 0.50 20. Dibromometbane <0.50 21. 1,2-Dichlorobenzene < 0.50 22. 1,3-Dichlorobenzene < 0.50 23. 1,4-Dichlorobenzene < 0.50 24. Dichlorodifluoromethane <0.50 25, 1,1-Dichloroethane < 0.50 26. 1,2-Dichloroethane < 0.50 27, 1,1-Dichloroethene < 0.50 28. Cis-1,2-Dichloroethene <0.50 29. trans-1,2-Dichloroethene < 0.50 30. 1,2-Dichloropropane <0.50 < 0.50 31. 1,3-Dichloropropane <0.50 32. 2,2-Dichloropropane <0.50 33. 1,1-Dichloropropene <0.50 34. Cis-1,3-Dichloropropene 35. trans-1,3-Dichloropropene < 0.50 36. Ethylbenzene <0.50 < 0.50 37. Hexachlorobutadiene 38. Isopropylbenzene < 0.50 39. 4-Isopropyltoluene <0.50 40. Methylene Cbloride <0.50 41. Naphthalene < 0.50 42. Propylbenzene < 0.50 < 0.50 43. 44. Styrene 1,1,1,2-Tetrachloroeth ane < 0.50 45. 1,1,2,2-Tetrachloro ethane <0.50 46. Tetrachloroethene < 0.50 47. Toluene <0.50 Page: 3 ENW,ummW % hempTOW 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON, NC 28530 REVIEWED BY: VOLATILE ORGANICS STD. METHODS 620OC-11 IWAW11 CLIENT ID: 416 ANALYST: KPG DATE COLLECTED: 10/24/18 DATE REPORTED: 11/15/18 Date Analyzed: M PARAETERS, ug/1 10/27/18 Well #18 48. 1,2,3-Trichlorobenzene <0.50 49. 1,2,4-Trichlorobenzene <0.50 50. 1,1,1-Trichloroethane < 0.50 51. 1,1,2-Trichloroethane <0.50 52. Trichloroethene <0.50 53, Trichlorofluoromethane <0.50 54. 1,2,3-Trichloropropane <0.50 55. 1,2,4-Trimethylbenzene < 0.50 56. 1,3,5-Trhnethylbenzene < 0.50 57. Vinyl Chloride <0.50 58. Total Xylenes <1.00 59. Methyl Tert Butyl Ether <1.00 756-06;)o Page: 4 State of North Carolina DWR Department of Environmental Quality Division of Water Resources -ivislon of \Hater Resources LAND APPLICATION SITE CERTIFICATION INSTRUCTIONS FOR FORM: LASC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 06-16 or FORM: SDR 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Application Site Certification (FORM: LASC 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit the requested information for all land application sites. ❑ For modified permits, submit the requested information for only those sites that are new, transferred or affected by the proposed modification. Land Application Site Information: ❑ The status of the land application site with respect to this residuals land application program must be provided in table 1. The status categories and their corresponding codes are as follows: ♦ New (N) ♦ Renewed (R) ♦ Modified (M) ♦ Transferred (T) ♦ Deleted (D) ❑ Attach the following in accordance with each status code: Status Code Required Item N R T M It V/ County Board Notification. doc Land Owner Agreement (If applicable) L� Setback Waiver Agreement An updated vicinity/setback map in accordance with the "Map Guidance for Residuals Land Application Permits' ✓ ✓ ✓ A soils and agronomic evaluation in accordance with the "Soil Scientist ✓ Evaluation Policy" INSTRUCTIONS FOR FORM: LASC 06-16 Page 1 of 3 An updated accounting of the land application site's cumulative pollutant loading rates (CPLRs) Status Code Required Item N R T M For previously permitted sites without a soil series name indicated in the Attachment B, submit County Soil Survey Map (or equivalent) clearly ✓ ✓ indicate the location of the land application site and in accordance with the soil map requirements in the "Soil Scientist Evaluation Policy" Acknowledgement of field transfer from Land Owner (Fields may not be permitted to multiple Permittees over the same timeperiod) * This item may be required for land application site with a status code "M", please contact the Division if you need assistant in determining attachment requirements. ® Crop Type should include the most likely crop types for the life of the permit (five years). ® Predominant Soils Series Name must be either the name of the soil indicated in Attachment `B" of the existing permit, or name of the soil series as provided by the licensed soil scientist. ® Predominant Soil Mapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of each site must be provided. The predominant soil -mapping unit must be consistent with the predominant soil series name. Please note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct mapping unit. If a representative slope is provided, it must be determined accordingly: ❑ For sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides information on both the soil series name and the slope of the soil), the Applicant may determine the representative slope by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8% would have a representative slope of 6%. ❑ New Sites to be permitted must have slopes determined as part of the soils report prepared by a licensed soil scientist. ® Acceptable methods for determining location coordinates (i.e., latitude and longitude) and their corresponding codes are as follows: • Address Matching (ADD) • Digital or Raw Photo Extraction (EXT) • Aerial Photography with Ground Control (AER) • Geodetic Quality GPS Survey (GEO) • Cadastral Survey (SUR) • LORAN-C Navigation Device (LOR) • Conversion from Coordinate Plane (CP) • Navigation Quality GPS (GPS) • Conversion from Township -Section -Range (TSR) • Remote Sensing (RS) • Conversion from Universal Trans Merc (UTM) • Zip Code Centroid (ZIP) • Map Interpretation by Digital or Manual Extraction (MAP) C. Waterbody and Classifications Information: (new sites only) ❑ Use an 8.5 by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the residuals program activities are planned to occur as well as the closest downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and number, the identified location, and be of clear and reproducible quality. ❑ Surface water body classifications information may be found at: http:Hdeg.nc.gov/about/divisions/water- resources/planning/c lassification-standards/classifications ❑ Any questions concerning the waterbody and its classification, please contact the Division's regional offices. ❑ A list of the Division's regional offices, their county coverage, and their contact information may be downloaded at: bi!p:Hdeq.nc.gov/contact/regional-offices ❑ General Instructions: There are 17 river basins in North Carolina. Each basin has associated waterbodies with assigned subbasins, location descriptions, stream index numbers and established classifications. 1. Identify the project area on a 7.5 minute USGS topographical map (an 8.5 x 11-inch sheet showing the project area should be submitted with the permit application regardless of whether a Stream classification was completed). 2. Determine the names of all the closest down slope surface waters from the project site. For unnamed tributaries, see Table 1: Unnamed Tributaries Entering Other States or for Specific Basin Areas. Label any unnamed tributaries as "UT to stream name" as the waterbody name. 3. Open the link http://deg.nc.p-ov/about/divisions/water-resources/planninp,/classification-standards/classifications. ❑ Stream Classification Process: One of the options below may be used depending on the known initial project informatioi ❑ KNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select proper basin from the List all Waterbodies in Basin sorted report. Sort hydrologically as this will provide the proper location descriptions if multiple runs. INSTRUCTIONS FOR FORM: LASC 06-16 Page 2 of 3 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ KNOWN COUNTY WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select the proper county from the List all Waterbodies in county, hydrologically report. 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ UNKNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Use the Clickable basin map to hydrologically sorted list report. 2. Click on the approximate project location to bring up the hydrologically sorted list. 3. Locate the name of the identified waterbody (from General Directions) on the list. 4. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 5. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ Notes on index number and unnamed streams: Unnamed Streams 15A NCAC 02B .0301M. ❑ Any stream which is not named in the schedule of stream classifications carries the same classification as that assigned to the stream segment to which it is tributary (at the point of entry) except: (A) unnamed streams specifically described in the schedule of classifications; (B) unnamed freshwaters tributary to tidal saltwaters will be classified "C"; or (C) after November 1, 1986, any newly created areas of tidal saltwater which are connected to Class SA waters by approved dredging projects will be classified "SC" unless case -by -case reclassification proceedings are conducted. ❑ The following river basins have different policies for unnamed streams entering other states or for specific areas of the basin: Unnamed Tributaries Entering Other States or for Specific Basin Areas Hiwassee River Basin Streams entering Georgia or Tennessee shall be classified "C Tr." Little Tennesse River Basin And Savannah River Drainage Area Streams entering Georgia or Tennessee shall be classified "C Tr." Such streams in the Savannah River drainage area entering South Carolina shall be classified "B Tr." French Broad River Basin Streams entering Tennessee will be classified "B." Watauga River Basin Streams entering the State of Tennessee are classified "C." Broad River Basin Streams entering South Carolina are classified "C." New River Basin Streams entering the State of Tennessee are classified "C." Catawba River Basin Streams entering South Carolina are classified "C." Yadkin -Pee Dee River Basin Streams entering Virginia are classified "C," and such streams entering South Carolina are classified "C." Lumber River Basin Streams entering South Carolina are classified "C Sw." Roanoke River Basin Streams entering Virginia are classified "C." Except that all backwaters of John H. Kerr Reservoir and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "B," and all backwaters of Lake Gaston and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "C and B." Chowan River Basin Streams entering Virginia are classified "C." Tar -Pamlico River Basin All drainage canals not noted in the schedule are classified "C Sw." except the main drainage canals to Pamlico Sound and its bays which shall be classified "SC." Pas uotank River Basin All drainage canals not noted in the schedule are classified "C." INSTRUCTIONS FOR FORM: LASC 06-16 Page 3 of 3 LAND APPLICATION SITE CERTIFICATION Applicant's name: Contentnea Metropolitan Sewerage District Land application sites currently certified: 68.55 net acres and Total to be certified: 68.55 net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Status Code' Site/Field ID Landowner(s) Lessee(s) or Operator(s) p () Net Acres County Crop(s) Predominant Soil b Series Name Mapping Unit or Rep. Slope' R B-1 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 2.84 Pitt Coastal Bermuda Grass Portsmouth loam Po R B-2 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 2.62 Pitt Coastal Bermuda Grass Pactolus loamy sand Pa R B-3 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 2.72 Pitt Coastal Bermuda Grass Portsmouth loam Po R B-4 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 3.34 Pitt Coastal Bermuda Grass Pactolus loamy sand Pa R B-5 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 3.74 Pitt Coastal Bermuda Grass Pactolus loamy sand Pa R B-6 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 2.48 Pitt Coastal Bermuda Grass Chipley sand Ch R B-7 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 1.32 Pitt Coastal Bermuda Grass Chipley sand Ch R CI-10 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 8.55 Pitt Coastal Bermuda Grass Alaga loamy sand AgB R CI1-8 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 7.73 Pitt Coastal Bermuda Grass Alaga loamy sand AgB R CII-9 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 5.15 Pitt Coastal Bermuda Grass Alaga loamy sand AgB R CII-13 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 3.30 Pitt Coastal Bermuda Grass Ocilla loamy fine OcB R CIII-12 Contentnea Metropolitan Sewerage District Mills, Dickie Ray 5.23 Pitt Coastal Bermuda Grass Osier loamy sand Os R CIV-I I Contentnea Metropolitan Sewerage District Mills, Dickie Ray 5.13 Pitt Coastal Bermuda Grass Osier loamy sand Os R D-14 Gaskins, Michael Mills, Dickie Ray 3.00 Pitt Coastal Bermuda Grass Portsmouth loam Po R D-15 Gaskins, Michael Mills, Dickie Ray 2.38 Pitt Coastal Bermuda Grass Portsmouth loam Po R D-16 Gaskins, Michael Mills, Dickie Ray 2.98 Pitt Coastal Bermuda Grass Maga loamy sand AgB R D-17 Gaskins, Michael Mills, Dickie Ray 3.62 Pitt Coastal Bermuda Grass Alaga loamy sand AgB R D-18 Gaskins, Michael Mills, Dickie Ray 2.42 Pitt Coastal Bermuda Grass Pactolus loamy sand Pa a Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) ♦ D (Deleted) b Soil Series Name (i.e. Appling, Cecil, etc.) `Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2) FORM: LA i-16 Page 1 LAND A.. LICATION SITE CERTIFICATION II. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction Q: Site/Field ID Latitude Longitude Location Datum Location Method Code Location Accuracy Waterbody Subbasin and Stream Index No. Current and Proposed P Class °0 NAD 83 ADD Nearest Second o r rr o � � 'rr NAD 83 ADD Nearest Second °0 NAD 83 ADD Nearest Second NAD 83 ADD Nearest Second ° ° '11 NAD 83 ADD Nearest Second ° 0, W, ° ' 11 NAD 83 ADD Nearest Second ° V j' NAD 83 ADD Nearest Second ° il, W,, 0 NAD 83 ADD Nearest Second Note: Please keep the site information (I.) and waterbody information (I1.) of the same field on the same page. FORM: LASC 06-16 Page 2 Contentnea Metropolitan Sewerage District 2019 Residuals Land Application Permit Renewal Supporting Information: Vicinity Map Setback Maps Updated Cumulative Pollutant Loadings Fields 1 through 7 Legend T', Site B House © Buffer THE w00TENGOrr!FMry CMSD Class B Land Application Permit WQ0001048 Renewal"`" 0 — Monitor Well Field Boundary Ditch � _' NetArea ::III'YIC Kp.M nlmm,Mr pA,Ob. l'pMM' MWb. rISGMbrpa!/p3 G11WVa ""'" "'"°°" `�°'°�""�'""°""�""'"�"` NIXTYtlp Mufi,Yx!!tl p, <oYUM] b' aMrJtpa C M '1011n1ta1 m bu map. 1 Y Pitt County, NC Y Stream Parcels :iC f nup J I°IA)lI75:IR.1 :a !nit ��_'ewnWr'nit^�apy-xsr b :t4 ao.a nb+m:xm Legend TV Fields 14 - 18 Site D A House ® Buffer = NetArea CMSD Class B Land Application � Monitor Well Field Boundary Pond rr�EwooTENco�.�P,krav Permit WO0001048 Renewal ;«s PAC a[6a sn na w ,on eb.%sas Fen,pa as smwwc. n�p.posas s+x nsa Pas arc w„Asaa P°mrm,tleC deea. oNn, «,c x« clePc a.+c aMr<srs.os Ditch Parcels Pitt County. NC Stream .1G C .vyr a r alAl PlS li'� 1 n bR' «� swvt nnnac, f 7.vr tv WP w: v � 4a m x + of Cumulative Pollutant Load for Each Site (updated to sludge applied in 2018) PAN Applied Site Acres As Cd Cu Cr Pb Hg MO Ni Se Zn (lbs/ac) B-1 2.84 Annual (lbs/acre) 0.012 0.005 1.167 0.062 0.085 0.002 0.024 0.062 0.024 3.075 183.912 Prior Years Cumul (lbs/ac) 0.493 4.499 67.879 22.586 6.886 0.366 2.459 7.466 0.639 259.112 Current Cumulative (lbs/ac) 0.505 4.504 69.046 22.648 6.971 0.368 2.483 7.528 0.663 262.187 B-2 2.62 Annual (Ibs/acre) 0.006 0.003 0.598 0.031 0.044 0.001 0.012 0.031 0.012 1.577 63.53 Prior Years Cumul (lbs/ac) 0.636 5.062 79.596 34.213 7.906 0.352 2.953 8.864 0.855 295.587 Current Cumulative (lbs/ac) 0.642 5.065 80.194 34.244 7.95 0.353 2.965 8.895 0.867 297.164 B-3 2.72 Annual (lbs/acre) 0.012 0.005 1.161 0.061 0.84 0.002 0.024 0.061 0.024 3.059 123.283 Prior Years Cumul (lbs/ac) 0.779 8.232 82.748 44.82 8.299 0.291 2.917 10.357 0.86 313.694 Current Cumulative (lbs/ac) 0.791 8.237 83.909 44.881 9.139 0.293 2.941 10.418 0.884 316.753 B-4 3.34 Annual (lbs/acre) 0.005 0.002 0.493 0.026 0.036 0.001 0.01 0.026 0.01 1.299 52.356 Prior Years Cumul (lbs/ac) 0.736 4.952 66.331 34.321 7.743 0.176 2.779 9.597 0.92 295.384 Current Cumulative (lbs/ac) 0.741 4.954 66.824 34.347 7.779 0.177 2.789 9.623 0.93 296.683 B-5 3.74 Annual (lbs/acre) 0.007 0.003 0.715 0.038 0.052 0.002 0.014 0.038 0.014 1.882 75.858 Prior Years Cumul (1bs/ac) 0.805 4.184 77.222 36.506 7.981 0.294 3.167 9.534 0.967 298.922 Current Cumulative (lbs/ac) 0.812 4.187 77.937 36.544 8.033 0.296 3.181 9.572 0.981 300.804 C11-8 7.73 Annual (lbs/acre) 0.01 0.005 0.96 0.05 0.07 0.002 0.019 0.05 0.019 2.53 101.931 Prior Years Cumul (lbs/ac) 0.604 1.767 53.251 25.604 5.304 0.132 2.085 5.258 0.652 197.957 Current Cumulative (lbs/ac) 0.614 1.772 54.211 25.654 5.374 0.134 2.104 5.308 0.671 200.487 CII-9 5.15 Annual (lbs/acre) 0.008 0.003 0.72 0.038 0.052 0.001 0.014 0.038 0.014 1.897 76.436 Prior Years Cumul (lbs/ac) 0.544 1.871 53.942 26.781 5.469 0.14 2.662 5.575 0.672 203.88 Current Cumulative (lbs/ac) 0.552 1.874 54.662 26.819 5.521 0.141 2.676 5.613 0.686 205.777 Cll-13 3.3 Annual (lbs/acre) 0.004 0.002 0.332 0.018 0.024 0 0.006 0.018 0.006 0.876 35.306 Prior Years Cumul (lbs/ac) 0.316 0.797 13.145 27.296 2.309 0.073 1.049 2.959 0.383 93.216 Current Cumulative (lbs/ac) 0.32 0.799 13.477 27.314 2.333 0.073 1.055 2.977 0.389 94.092 CII-15 2.38 Annual (lbs/acre) 0.013 0.006 1.347 0.071 0.098 0.003 0.027 0.071 0.027 3.551 143.113 Prior Years Cumul (lbs/ac) 0.229 0.404 26.163 9.031 2.064 0.032 0.609 2.357 0.368 111.619 Current Cumulative (lbs/ae) 0.242 0.41 27.51 9.102 2.162 0.035 0.636 2.428 0.395 115.17 D-16 2.98 Annual (lbs/acre) 0.006 0.003 0.574 0.03 0.042 0.001 0.012 0.03 0.012 1.513 60.96 Prior Years Cumul (lbs/ac) 0.252 0.379 27.468 8.787 2.146 0.032 0.602 2.482 0.388 117.176 Current Cumulative (lbs/ac) 0.258 0.382 28.042 8.817 2.188 0.033 0.614 2.512 0.4 118.689 D-17 3.62 Annual (lbs/acre) 0.007 0.003 0.709 0.037 0.052 0.002 0.015 0.037 0.015 1.869 75.281 Prior Years Cumul (lbs/ac) 0.325 0.471 36.118 11.819 2.841 0.042 0.806 3.208 0.515 158.47 Current Cumulative (lbs/ac) 0.332 0.474 36.827 11.856 2.893 0.044 0.821 3.245 0.53 160.339 D-19 I t.75 Annual (lbs/acre) 0.002 0.001 0.174 0.009 0.013 0 0.004 0.009 0.004 0.46 18.519 Prior Years Cumul (lbs/ac) 0 0 0 0 0 0 0 0 0 0 Current Cumulative (lbs/ac) 0.002 0.001 0.174 0.009 0.013 0 0.004 0.009 0.004 0.46 Contentnea Metropolitan Sewerage District M19 Residuals Land Application Permit Renewal Land Owner Agreement Form 06-16 for CMSD owned sites Land Owner Agreement Form 06-16 for Gaskins owned sites Division of Water Resources State of North Carolina Department of Environment and Natural Resources Division of Water Resources LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ® A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND he undersigned landowner or his representative hereby permits: Applicant's name: Contentnea Metropolitan Sewerage District hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Fieid ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) B-1 Yes Hay Animal Feed CMSD WWTP B-2 Yes Hay Animal Feed CMSD WWTP B-3 Yes Hay Animal Feed CMSD WWTP B-4 Yes Hay Animal Feed CMSD WWTP B-5 Yes Hay Animal Feed CMSD WWTP B-6 Yes Hay Animal Feed CMSD WWTP B-7 Yes Hay Animal Feed CMSD WWTP 0-10 Yes Hay Animal Feed CMSD WWTP CII-8 Yes Hay Animal Feed CMSD WWTP CII-9 Yes Hay Animal Feed CMSD WWTP CII-13 Yes Hay Animal Feed CMSD WWTP CIII-12 Yes Hay Animal Feed CMSD WWTP CIV-11 Yes Hay Animal Feed CMSD WWTP FORM: LOA 06-16 Pagel of 3 The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and hall be renewed each time this permit is renewed. 'he undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1636 Mail Service Center, Raleigh, NC 27699-1636. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. II. RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14- month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. III. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(h) allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ❑ A re -defined compliance boundary is needed for field(s) ID: (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) FORM: LOA 06-16 Page 2 of 3 ® A re -defined compliance boundary is not needed for this site. W. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program: (Name of the new program) Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: Contentnea Metropolitan Sewerage District Address: PO Box 477 City: Grifton State: NC Zip: Phone: 252 52 -5584 E-mail address:crosd100(c�embargmail.com Signature: Date: NORTH CAROLINA, � h± COUNTY I, the undersigned Notary Public do hereby certify that Caws\cs M. 5 eV\0A,,Z: ,k_ Sc_ personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the 7-7-9- dayof Signature and seal: My commission expires: Lessee's/Operator's Certification: 2 ,20 1 I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Dickie Ray Mills Address: Lkc► 4o tksC%j *; n City: State: !J Phone: zu__- 7q(. r Z1 oo _ E-mail addr Signature: Zip: 7A 51 3 Date: $ - Zy -11:� FORM: LOA 06-16 Page 3 of 3 Permittee's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name:. C--�,r_.A e_fj �\ . Signature: 6��m Date: $ ' ZZ-ti FORM: LOA 06-16 Page 4 of 3 DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit. General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ® A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Contentnea Metropolitan Sewerage District hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease Land Use or Intended Use of Crops Residuals Source Special note (no-till/over-seed/ (yes/no) Cropping Patterns (optional) pasture) D-14 Yes Hay Animal Feed CMSD WWTP D-15 Yes Hay Animal Feed CMSD WWTP D-16 Yes Hay Animal Feed CMSD WWTP D-17 Yes Hay Animal Feed CMSD WWTP D-18 Yes Hay Animal Feed CMSD WWTP The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. he undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and ipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. FORM: LOA 06-16 Page 1 of 3 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. Il. RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls. may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14- month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. III. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(h) allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ❑ A re -defined compliance boundary is needed for field(s) ID: (Please include the rationale for the requested re -location of the compliance boundary to the application package) ® A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) compliance boundary and attach a map showing the newly proposed ❑ The land application field(s) ID: , is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FORM: LOA 06-16 Page 2 of 3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: Michael Gaskins Address: k 0 & .. ',i6 City: Gc taco r State: Al?L Zip: 2 Y> S 3 l3 Phone: E-mail Signature: Date: $-ZZ_,�A NORTH CAROLINA, - � k-t COUNTY I, the undersigned Notary Public do hereby certify that personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the day of Signature and seal: `�� My commission expires: Z Lessee's/Operator's Certification: Z Z- '--' 120 I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Dickie Ray Mills Address: City: A rile .r. State: tO (— Zip: Z$ S 13 Phone: 7,5 Z, -I''f b 10O Signature: Permittee's Certification: E-mail address: Date: I - ZO - lcl I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official n I4A4P1 E' S M SM ) T14G„!� j t< Signature: Date: 8 - ,2•?'19 If FORM: LOA 06-16 Page 3 of 3