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HomeMy WebLinkAboutWQ0008349_Residual Annual Report 2014_201502192014 ANNUAL REPORT . TOWN OF NEWPORT . LAND APPLICATION PROGRAM PERMIT #WQ0008349 Prepared For: Town of Newport Post Office Box 1869 Newport, North Carolina 28570 Branch Residuals, & Soils, LLC 9646 West Market Street, Smite '111 • Greemshoro, NC 27409 PHONE (336) 510-0340 • FAX (336) 510-0341 IVED 9 2015 'Letter ®Transm,tlwtEc'noN ,O�EINGIfI f To: NCDENR Information Processing Section From: Bob Branch, CC: Town of Newport Date:. 2/16/2015 Re: Town of Newport 2014 Annual Land Application Report Permit No. WQ0008349 The following copies of this report have been sent to you: NCDESWAquifer Protection Section/Information Procession Unit — 3 copies, EPA Region. VII Biosolids Center - 2 copies, and • Town of Newport — 3 copies ( 2 for Newport and 1 for Craven Ag Services). Please give me a call at (336) 510. 0340 if you have any questions. Robert T. Branch TABLE OF CONTENTS SECTION NO. TITLE I Certification Forms and Facility Information II Annual Residual Sampling Summary Form III Annual Metals Field Loading Summary Form IV Annual Land Application Field Summary Form V Residual Analysis Lab Sheets VI Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report VII Pathogen and Vector Attraction Reduction Certification Form VIII Pathogen and Vector Attraction Reduction Documentation IX Soil Analysis Reports X 2014 Application Summary Table XI 2014 Application Condition Summary CERTIFICATION FORMS AND FACILITY INFORMATION 11 ANNUAL, LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0008349 County: Craven Year: 2014 if Facility Name (as shown on permit): Town of Newport Land Application Operator: Craven Ag Services Phone: (252) 633-5334 Land application of residuals as allowed by the permit occurred during the past calendar year? ® Yes R1 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. "n -,& A D- :.1-1. A—Hon+in" .Q1Ttnmarv- 1 4UA L A ---- Total number of ap2lication fields in thepermit: 5 Total number of fields utilized for land application during the year: 1 Total amount of dry tons applied during the year for all application sites: 25.19 Total number of acres utilizes for land application during the year: 11.00 Part B - Annual Comuiance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. E] Yes ® No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." i Mr. Angela Christian, Town Manager L/110` Permittee Name and Title (qTe or print) Signatur of Permittee Date 2 r4 1 �" Signatu of Preparer* Date 4ig4nateof Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) TOWN OF NEWPORT WASTEWATER TREATMENT PLANT (WWTP) • Facility name, address, and telephone number: Town of Newport Post Office Box 1869 Newport, North Carolina 28570 Phone: (252) 223-4749 Facility NPDES permit number: NCO021555 • Name, address, and telephone number of the responsible official (permittee): Mrs. Angela Christian, Town Manager Town of Newport Post Office Box 1869 Newport, North Carolina 28570 Phone: (252) 223-4749 • Name, address, and telephone number of the facility operator: Mr. Scotty Rollins, Wastewater Treatment Plant ORC Town of Newport 160 Kirby Lane Newport, North Carolina 28570 Phone: (252) 233-4418 • Name, address, and telephone number of land appliers: Craven Ag Services, Inc. 2115 Highway 55 West New Bern, NC 28562 Phone: (252) 633-5334 • Dry metric tons of biosolids land applied: WWTP 25.19 Dry Tons or 22.9 Dry Metric Tons ANNUAL RESIDUAL SAMPLING SUMMARY FORM i I ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0008349 Laboratory: 1) Environment One Facility Name: Town of Newport 2) Residual Source WQ # or NCO021555 3) NPDES #: 4) WWTP Name: Town of Newport WWTP 5) Recirinal Analvsic Data Parameter (mg/kg) Ceiling Cone. Limit Sample or Composite Date 1/27/2014 Percent Solids (%) NA 13.12 Arsenic 75 3.00 Cadmium 85 1.20 Copper 4,300 446.00 Chromium NA 13.00 Lead 840 13.00 Mercury 57 0.49 Molybdenum 75 5.00 Nickel 420 8.00 Selenium 100 <5.00 Zinc 7,500 817.00 Total Phosphorus NA 3297.00 TKN NA 26574.00 Ammonia -Nitrogen NA 2930.00 Nitrate and Nitrite NA 8.40 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for ubmi 'ng f e in or cl ding the possibility of fines and imprisonment for knowing violations." Simatur , Preparer Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report --- Facility Name: Town of Newport Total Dry Tons Applied (Annual): 62.65 Permit #: WQ0008349 Cation Exchange Capacity (non 503 only): Iva Operator: Allen Roacb Owner: Allen Roach Predominant Soil Series Se Acres Used: 11 Acres Permitted: 25A Site #: AR Field #: 8 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ttv IA-Wno-72 6 El 392 Sample or Com posits Date 6/4/14 1/27/14 % Solids 1 68.10 13.12 Arsenic 0.00 3.00 Cadmium 0.01 1.20 Chromium 0.00 13.00 Copper 0.27 446.00 Lead 0.06 13.00 Mercury 0.00 0.49 Molyb- denurn 0.00 5.00 Nickel 0.03 8.00 Selenium 0.00 5.00 Zinc 0.73 817.00 Total Phos- horus 7,770 3,297 A,nmmal Aneww Nord Fiolell T.emellinoa (Calculated in lhs/acre): C1f .> 3.41 2.29 b d Arsenic 0.00 0.01 0.01 Cadmium 0.00 0.01 0.01 Chromiurr 0.00 0.06 0.06 Copper 0.00 2.04 2.04 Lead 0.00 0.06 0.06 Mercury 0.00 0.00 0.00 MO Yb- 0.00 0.02 0.02 u Nickel 0.00 0.04 0•04 Selenium 0.00 0.02 0.02 Zinc 0.00 3.74 3.75 Total Phos- 52.91 15.10 68.01 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, inclnding the possibility of fines and imprisonment for knowing violations" ignature of Land Applier� Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL LAND APPLICATION FIELD SUMMARY FORM 1 ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND All nutrients and metals concentrations listed on the following annual land application field summary forms are on a pound per acre basis. The following is a list of symbols and abbreviations used on the field loading rate report: %TS — Percent Solids DT/ACRE — Dry Tons Applied per Acre lb/ac — Pounds per Acre Metals (lbs/ac) As — Arsenic Cd — Cadmium Cr — Chromium Cu — Copper Pb — Lead Hg — Mercury Mo — Molybdenum Ni — Nickel Se — Selenium Zn — Zinc Nutrients (lbs/ac) PAN — Plant Available Nitrogen P — Phosphorus K — Potassium Annual Totals — lbs/ac applied during the calendar year. Cumulative Totals — lbs/ac applied during the lifetime of field use. I L - ' ANim u mL L.-uNau AFru-t%2ATiviN FIEjum OUMivitaalY 1 vniv'I PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Newport WQ Permit #: WQ0008349 Field #: AR Acres Utilized: Owner: Allen Roach Annual Dry Tons Applied: 62.65 Site #: 8 Acres Permitted: Operator: Allen Roach Predominat Soil Series Se Cation Exchange Capacity (non 503): Crop 1 Name: Suyb..(Full Smson-Ma ed Crop 1 Max PAN: 119.00 Crop 2 Name: #N/A Crop 2 Max. PAN 11.00 25.40 NA #N/A C7 d 0 Specify Totals Per Acre o /o Solids �'s Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) Site Cond. (Dry' Wet Moist) Precip. Past 24 Hrs. Inches °a�w W �: m * w Q �: E * 0 TKN m Z 6 o 6 m Nitrate and Nitrite m PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Gal. Wet Tons Report Totals in Gal. Cro71crop2 Crop 1 Crop 2 May-14 55 5 68.10 3.41 Craven Wood Energy INC 1.00 1.00 914 0 0 6.22 X May-14 192 17 13.12 2.29 Town of NewportWWTP INC 1.00 0.30 26,574 2,930 8 1 45.95 X TOTALS: 22 As Cd Cr Cu Pb Hg MotNi Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.01 0.01 0.06 2.04 0.06 0.00 0.02.04 0.02 3.75 68.01 52.17 0.00 Date lbs/ac u ative lbs/acre0 Current Cum 1. 03 0.01 NA 4.13 0.14 0.00 NA.07 0.05 8.37 0.00NA .0 4 0.03 4.63 24 8 15 NA 37 4 89 9 119.00 9 May-14 1,770 Cumulative lbs/acre Prior Years Cum t 0.01 0.01 NA 20 .9 00 8 Permitted C. P. L. R. *><< 36 34 NA 1338 , 267 't 1 st/2nd Crop e tnt P rmit PAN Li P "I certify, under penalty of law, that this document was prepared under my direction or supervision in accoraance wain a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of flues and imprisonment for knowing violations." Z *Application Method: S - Surface, IN - Injection, INC - Incorporation /40 **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) RESIDUAL ANALYSIS LAB SHEETS EukaMEM % hCopumbd P.O. BOX 7085, 114 OAKMONT GREENVILLE, N.C. 27835-7085 TOWN OF NEWPORT (SLUDGE) CHRIS MASSENGILL P.O. BOX 1869 NEWPORT ,NC 28570 Sample Sample PARAMETERS #1 #5 Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Nitrate Nitrogen(dry wt.), mg/kg Nitrite Nitrogen(dry wt.), mg/kg Phosphorus, T. (dry wt.), mg/kg Fecal Coliform (WN), /gram Solids Molybdenum (dry wt. basis), mg/kg ONE (252) 756-6208 FAX (252) 756-0633 ID#: 392 DATE COLLECTED: 01/27/14 DATE REPORTED : 03/11/14 REVIEWED BY: Sample Drying Bed Analysis Method #6 Sludge Date Analyst Code 4439 02/07/14 LFJ EPA200.7 3 03/04/14 MEL 3113B-04 41836 02/07/14 LFJ EPA200.7 1.2 03/09/14 MEL 3113B-04 446 02/07/14 LFJ EPA200.7 13 02/07/14 LFJ EPA200.7 13 03/03/14 MEL 3113B-04 1264 02/07/14 LFJ EPA200.7 0.49 02/11/14 ADD 245.1 R3-94 8 02/07/14 LFJ EPA200.7 1769 02/07/14 LFJ EPA200.7 < 5.0 03/10/14 MEL 3113B-04 2807 02/07/14 ADD 3111B-99 817 02/07/14 ADD 3111B-99 13.4 13.8 12.6 12.9 01/28/14 CMC 254OG-97 26574 01/30/14 ANO 351.2 R2-93 2930 01/30/14 ANO 350.1 112-93 <3.36 01/29/14 ANO 353.2 R2-93 5.04 01/29/14 ANO 353.2 112-93 3297 01/30/14 ALB 365.4 -74 403 1159 1270 01/28/14 CMC 9221E-06 < 5.0 02/07/14 LFJ EPA200.7 Environment 1, Inc. P.O. Pox 7085, 114 Oakmont Dr. fl-roe ,.:iio XTO ')7Q';Q CHAIN OF CUSTODY RECORD Page 1 of 1 'hone (252) 756-6208 ° Fax (252) 756-0633 DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION CHLORINE CLIENT: 392 Week: 7 12 UV pH CHECK (LAB) TOWN OF NEWPORT (SLUDGE) NONE P P P P P P P P P P P G G G G G CONTAINERTYPE, P/G CARTS MASSENGILL P.O. BOX 1869 A A A A A A A A A A A A A A A A CHEMICAL PRESERVATION NEWPORT NC 28570 z A -NONE D-NAOH (252) 223-4418 E � z J w z U' w In b �' b � B-HNO3 E-HCL J o fv z Wo C - H2SO4 F - ZINC ACETATE/NAOH `f" Q v LL ° A Z Z a C w a �bD ° U aCOLLECTION a E_ a EU" 0 F .a F Go NATHIOSULFATE SAMPLE LOCATION DATE TIME o Sample #1 y 7 I��� 1 >j CLASSIFICATION: WASTEWATER NPDES ( ) DRINKINGWATER DWO/GW Sample #2 7 r �Gr 1 Sample #3 ' J2- 1 Sample #4 Sample #5 1 z— /1- / 1 SOLID WASTE SECTION Sample #6 ,�.� %�/�...� '� �� 1 CHAIN OF CUSTODY MAINTAINED Sample #7 /1 DURING SHIPMENT/DELIVERY 1 ::� <; `::ice :•>:.>:; ;. :.:::::. x.:.:.. ...,: it :<:::,, ::.. ..» :., Drying Bed Sludge 1 fC / 10 ,... ..... .. .» ..,.. SAMPLES COLLECTED BY: (Please Print) SAMPLES RECEIVED I B AT I°C RELINQUISHED BY($IG.) (SAMPLER) DATE/TIME LRECE(SIG.) )-7DATEMM�E ha _II� COMMENTS: RELINQUIS BY (SIG.) DATE/TIME RECEIVE (SIG. DATE/TIME RELINQUISHED BY (SIG.) I DATE/TIME RECEIVED BY (SIG.) DATE/TIME F__ PLEASE READ lbstructions for completing this form on the reverse side. Sampler must place a "C' for composite sample or a "G" for IV 267889 =nMARr I Grab sample in the blocks above for each parameter requested. n Facility: Source: Location: Contractor: Type of Analysis: Report No: Date Sampled: Date Reported: Reporting Period: Town of Newport Town of Newport WWTP Newport, North Carolina Craven Ag Services Wastewater Treatment Plant EI 392 1/27/2014 3/11/2014 Annual 2014 Parameter % PPM Dry Weight EPA Monthly Limits Solids* 13.12 Nitrogen (TKN) 2.657 26,574.000 Phosphorus 0.330 3,297.000 Potassium 0.177 1,769.000 Sulfate Calcium 4.184 41,836.000 Magnesium 0.126 1,264.000 Sodium 0.281 2,807.000 Iron --- Aluminum --- 4,439.000 Manganese --- Copper --- 446.000 1,500 Zinc --- 817.000 2,800 Ammonia Nitrogen 0.293 2,930.000 Nitrate N / Nitrite N --- 8.400 Cadmium --- 1.200 39 Chromium --- 13.000 1,200 Nickel --- 8.000 420 Lead --- 13.000 300 Arsenic --- 3.000 41 Mercury --- 0.490 17 Selenium --- 5.000 100 pH 6.830 Calcium Carbonate Eq. 0.000 Organic Nitrogen 2.364 Molybdenum --- 5.000 75 Chloride --- Boron Available P2O5 Wastewater Treatment Plant Town of Newport WWTP Newport, North Carolina Annual 2014 Date Reported: 3/11/2014 Report No: EI 392 Note All Units in Pounds Per Dry Ton Macro Nutrients Physical Characteristics PAN Surf. 17.133 PAN Inj. 20.063 P 6.594 K 3.538 Lime 0.000 Secondary Nutrients Calcium 83.672 Magnesium 2.528 Sodium 5.614 SAR 1.334 Chloride 0.000 Iron 0.000 Alumium 8.878 Manganese 0.000 Boron 0.000 Sulfur 0.000 Residual Nitrogen Calculation Year Min Rate PAN #/Acre % Solids 13.12 pH 6.830 Min Rate 0.300 Metals Arsenic 0.006 Cadmium 0.002 Chromium 0.026 Copper 0.892 Lead 0.026 Mercury 0.001 Molybdenum 0.010 Nickel 0.016 Seleniun 0.010 Zinc 1.634 2014 0.30 14.19 2015 0.15 4.97 2016 0.08 2.11 2017 0.04 0.98 2018 2019 2020 2021 2022 2023 2024 TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORT ENViRt7h,3iv5ENTAL-rEcHigoLoGiEs, INC LABORATORY REPORT n Client Environment 1, Inc. - 114, Oakmont Dr Greenville, NC 27858 Order Number 1400287 Project Number Town of Newport (Sludge) Issued Thursday, February 13, 2014 Total Number of Pages 5 (excluding C.O.C. and cooler receipt form) Approved By: QA Manag(kr')��®���� Certifications: A21-A/DOD 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Michigan (Reg.5), Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey 01-1006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP C1.0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-0, Region 5 WG-1.5J, Region 8 8TMS-L, USDAIAPHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 "Analyti,af lntccgrify" , EPA certified - NELAP Certified Falls, 011io 1.42.23 x Phone: 1310-263.3211 ' Fax: 330-253.4489 ui 2 Sample Summary Client: Environment 1. Inc. Order Number: 1400287 Laboratory ID Client ID Matrix Sampling Date 1400287-01 Drying Bed Sludge Solid 1 /27/2014 'AmOyticaad Integrity" • EPA Certified . 14ELAP Certified 3."M w•lk1Ct tt' =i Cuyahoga ► tills, -0hia 44223 ¢ ("hone: 330-253-82 (1 • lax: 330-253-4489 4Neb ui!e. www.selmk.coin R ENV113C7NMENTAL'i`E0HNOLOGIES. INC. r��i�t�'l�.t pie'; �:?r . i7;:s ��i�?i✓i'e�x�;;i Report Narrative Client: Environment 1. Inc. Order Number: 1400287 3 Solid sample results are reported on a wet weight basis except as noted. No problems were encountered during analysis of this order number, except as noted. Method numbers, unless specified as SM or ASTM, are EPA methods. Method of analysis for TCLP Volatiles is 1311/8260B Method of analysis for TCLP Metals is 1311/6010B and 1311/7471A Method of analysis for TCLP BNA is 1311/8270C Data Qualifiers: B = Analyte found in the method blank J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ) C = Analyte has been confirmed by another Instrument or method E = Analyte exceeds the upper limit of the calibration curve. • Matrices: D = Sample or extract was analyzed at a higher dilution A = Air X = User defined data qualifier. C = Cram S = Surrogate out of control limits DW = Drinking Water U =Undetected L = Liquid a = Not Accredited by NELAC O Oil SL = Sludge oil ND = Non Detected at LOQ SO = S =Solidlid DF = Dilution Factor T = Tablet TC = TCLP Exfract i Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor) WW = Waste Water Limit Of Detection (LOD) = Method Detection Limit , W = Wlpe Practical Quantitation Limit (PQL) = (same as LOQ) Method Detection Limit (MDL) = (same as LOD) Reporting Detection Limit (RDL) = (same as LOD) Estimated uncertainty values are available upon request. The test results meet the requirements of the NELAC standard, except where noted. The information contained in this analytical report is the sole property of Summit -Environmental Technologies, Inc. and that of the client. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. Analytiaaf lrxtegrit,," - EPA Certified • HELAP Certified 3310 Alin SirtyeP. • Cuyahoga Falls, Ohio 44223 a Phone: 330-25:3-8211- - Fax: 330-253-4489 vIlBJ Slie; WJA.4N.S6'Ite�',G0 71 I ENVIRONMENTAL TECHNOLOGIES, INC. .t�l7r�al.'E;iC.•dl,� t.:.�L!s`�d"i��'�i"da::fi Client IDN Lab I Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 client Lab 113# Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287.01 Drying Bed Sludge1400287-01 Clie i ID# Lab ID# Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Client Lab 1Dll Drying Bed Sludge1400287-01 Drying Bed Sludge1400287-01 Client Lab 1D Drying Bed Sludge1400287-01 TCLP Volatiles Collected �� Reo Lmt Rpm 27-)an-14 1,1-Dichloroethene 0.1 ND 27-Jan-14 1,2-Dichloroethane 0.1 ND 27-Jan-14 2-Butanone (MEK) 2 ND 27-3an-14 Benzene 0.1 ND 27-Jan-14 Carbon Tetrachloride 0.1 ND 27-3an-14 Chlorobenzene 0.1 ND 27-Jan-14 Chloroform 0.1 ND 27-Jan-14 Tetrachloroethene 0.1 ND 27-Jan-14 Trichioroethene 0.1 ND 27-Jan-14 Vinyl Chloride 0.2 ND TCLP NNA Collected Analvte Rep Lmt Result 27-Jan-14 1,4-Dichlorobenzene 0.1 ND 27-3an-14 2,4,5-Tdchlorophenol 0.25 ND 27-Jan-14 2,4,6-Trichlorophenol 0.25 ND 27-Jan-14 2,4-Din'itrotoluene 0.1 ND 27-Jan-14 Cresols 5 ND 27-1an-14 Hexachloro-1,3-butadiene 0.1 ND 27-Jan-14 Hexachlorobenzene 0.1 ND 27-Jan-14 Hexachloroethane 0.1 ND 27-Jan-14 Nitrobenzene 0.1 ND 27-Jan-14 Pentachlorophenol 0.25 ND 27-Jan-14 Pyridine 0.25 ND TCLP Pesticides Collect cd An Rep Lmt Result 27-Jan-14 Chlordane 0.01 ND 27-Jan-14 Endrin 0.002 ND 27-Jan-14 Gamma-BHC 0.002 ND 27-Jan-14 Heptachlor 0.002 ND 27-Jan-14 Heptachlor Epoxide 0.002 ND 27-Jan-14 Methoxychlor 0.002 ND 27-Jan-14 Toxaphene 0.1 ND TCLP Herbicides Collect ed Analvte Rep Lmt Result 27 Jan-14 2,4,5-TP(Silvex) 0.5 ND 27 Jan-14 2,4,D 5 ND TCLP Arsenic Collected Ana lvte Rea Lmt Result 27-1an-14 TCLP Arsenic 0.5 ND February 13, 2014 Client: Environment 1, Inc. Address: 114 Oalanont Dr Greenville, NC 27858 Received: 2t4/2014 Project #: Town of Newport (Sludge) Units Matrix Method mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 Units Matrix Method mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 Units Matrix Method mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 mg/L S 1311 Units Matrix Method mg/L S 1311 mg/L S 1311 Units Matrix Method mg/L S 1311 DF ReaLvl 1 0.7 1 0.5 1 200 1 0.5 1 0.5 1 100 1 6 1 0.7 1 0.5 1 0.2 DF ReaLv_I 1 7.5 1 400 1 2 1 0.13 1 200 1 0.5 1 0.13 1 3 1 2 1 100 1 5 DF ReoLvl 1 0.03 1 0.02 1 0.4 1 0.008 1 0.008 1 10 1 0.5 DF ReaLvl 1 1 1 10 ltun Ana][39 07-Feb-14 MS 07-Feb-14 MS 07-Feb-14 MS 07-Feb-14 MS 07-Feb-14 MS 07-Feb-14 MS 07-Feb-14 MS 07-Feb-14 MS 07-Feb-14 MS 07-Feb-14 MS Run Analyst 08-Feb-14 AE 08-Feb-14 AE 08-Feb-14 AE 08-Feb-14 AE 08-Feb-14 AE 08-Feb-14 AE 08-Feb-14 AE 08-Feb-14 AE 08-Feb-14 AE 08-Feb-14 AE 08-Feb-14 AE Run An-alysl 10-Feb-14 JBN 10-Feb-14 JBN 10-Feb-14 JBN 10-Feb-14 JBN 10-Feb-14 JBN 10-Feb-14 JBN 10-Feb-14 JBN Run Analyst 12-Feb-14 AMZ 12-Fe3-14 AMZ DF ReaLyl Run Analyst 1 5 07-Feb-14 WK Page 4 'Arxaiytical Jrltegritgf" EPA Certified - NEL AP Certified 3310 Win Street • Cctphi ga Falls, Ohio 44223 < Phone- 330-253-8211 - Fax: 330-253-4489 - Web SitF,: ;vwi.v.settek.carn ENVIRONMENTAL TECHNOLOGIES, INC. February 13, 2014 r at;�t:i Li3's?to r1 :> Client: Environment 1, Inc. - Address: 114 Oalanont iDr Greenville, NC 27858 Received: 24/2014 Project #: Town of Newport (Sludge) TCLP Barium - Client M# Lab M# Collected Anal vte Rep Lmt Result Units Matrix Me DF ReaLvl Run Analyst Drying Bed Sludge1400287-01 27 ]an-14 TCLP Barium 5 ND mg/L S 1311 1 100 07-Feb-T34 WK _ TCLP Cadmium Client Lab ID# Collected Anal vte Rep Lmt Result Units Matrix Method DI ReaLvl Rau Analyst Drying Bed Sludge1400287-01 27-Jan-14 TCLP Cadmium 0.1 ND mg/L S 1311 1 1 07-Feb-14 WK TCLP Chromium Client I Lab ID# Collected Anal yte Rep Lmt Rt§ult Units Mahig Metb D-F R2gLv1 Rut !Analyst Drying Bed Sludge1400287-01 27-Jan-14 TCLP Chromium 0.2 ND mg/L S 1311 1 5 07-Feb-14 WK TCLP Lead Client ID# Lab ID# Collected Ana lvte Rep Lmt . Result Units Matrix Method DF ReQUI Run Analyst Drying Bed Sludge1400287-01 27-Jan-14 TCLP Lead 0.5 ND mg/L S 1311 1 5 07-Feb-14 WK TCLP Mercury Tent Lab ID# Collected Analyte Rep Lmt Result Units Matrix- vM W ReaLy1 Run Anas Drying Bed Sludge1400287-01 27-]an-14 Mercury 0.002 ND mg/L S 1311 1 0.2 07-Feb-14 AU TCLP se 1ient_IW_ Lab 1Q# Colleted Anal vte Rep Lmt Result Units Mahix Method DF R vl Rua Analvst Drying Bed Sludge1400287-01 27-Jan-14 TCLP Selenium 0.5 ND mg/L S 1311 1 1 07-Feb-14 WK TCLP Sliver Client ID# Iab 1D# llected Anal vte Re Lmt Result _� ets Units Matrix M DF RenLvl Run Analyst Drying Bed Sludge1400287-01 27-Jan-14 TCLP Silver 0.5 ND mg/L S 1311 1 5 07-Feb-14 WK ClieptIDN Lab1D# Collect Analyte Result Units Matnx Method DF L_O�G Rua Anal Drying Bed Sludge1400287-01 27-]an-14 Flash Point >140F S 1010 1 06-Feb-14 TG Clien IN Lab ID# Collected Aaalvte Result Units Matrix Method DF LOLL Rnn Analyst Drying Bed Sludge1400287-01 27-Jan-14 pH 6.83 S.U. S 9040 1 0.01 05-Feb-14 AYS Client 1D# Lab ID# Collected Anal vte Result Units Matrix Method DF LONG Run Analyst Drying Bed Sludge1400287-01 27 ]an-14 Reactive Cyanide ND Ppm S 7.3.3.2 1 0.5 05-Feb-14 TIR Cheat m# Lab [D# Collected Analvte Result Units Matrix Method DF LONG Run Analyst Drying Bed Sludge1400287-01 27 ]an-14 Reactive Sulfide ND PPm S 7.3.4.2 1 25 05-Feb-14 TIR Page 5 "Anaiyfloaf lnt(�_yrBty" - EPA Certified - l iELAP Certified '03 0 Win Street - Cuyahoga Falls, Ohio 44223 m P'horie. 330-253-8211 - Fax: 330-253-4489 b'✓eh Sift): www.seftek.calo Rev. 12 Date: 07/27/13 Order ID: 1400287 COOLER Summit Environmental Technolog Cooler Receipt Form Initials of person inspecting cooler and samples: Client: �)lf��V11 f I Order Number: Date Received:aq Time Received: ��, Date cooler(s) opened and samples inspected: Number of Coolers/Boxes: N/A Shipper: FED UP DHL Airborne US Postal Walk-in Pickup Other Packaging: Peanuts u ble Paper Foam None Other. Tape on cooler/box: �Y� N N/A Custody Seals intact N N/A C-O-C in plash N NIA Ice L Blue ice re ZI absent / melted N/A Sample Temperature IR Gun #1602 59 CF Q - D °C 1.3 °C N/A Radiological Testing Insfrument serial #35127 Y N (see page 2 for scan results) '"Use 1 sheet per sample for Radiological Testing. If sample is HOT, the Radiological Safety Officer must be notified Immediately. C-0-C filled out properly N NIA Samples in separate bags N WA Sample containers Intact" N N/A *If no, list broken sample(s): Sample label(s) complete (ID, date, etc.) ® N NIA Label(s) agree with C-O-C N NIA Correct containers used N NIA Sufficient sample received N N/A Bubbles absent from 40 mL vials" Y N IA Samples with bubbles <6mm are acceptable. Indicate bubble size if>6mm. Was client contacted about samples Y N Will client send new samples Y N Client contact: DateMme: Logged in by: Comments: G:1QC SHARED1Document Control Templates - Tracking\Cooler receipt form Rev. 12 07-27-13.doc Page 1 of 2 nvironment 1, Inc. O. Box 7085, 114 Oakmont Dr. reenville, NC 27858 Iln�ii�l�rt�llllllf IIIIINIINIi�II�IIIIl�0111hiil��llll . � - I�IIIIU�II�IIII�II�I111�IIIII111�IIIIIIII�I111111111N11ai�lllll�lllill = rd Done (252) 75Er62()8 •Fax (252) 756-0633 DISINFECTION Oer ID: 1400287 COC- C1ILORINE pH CHECK (LAD) UENT:392 Week:7 UV TOWN OFNEWPORT (SLUDGE) NONE P P P P P P P P P P P G G G G G CONTAINERTYPE,P/G CMS MASSENGILL CFIEMICALPRESERVATION P.O. BOX 1869 A A A A A A A A A A A A A A A A NEWPORT NC 28570 A - NONE D - NAOH z 0 z3 9 ZCn en B-HNO, E HCL (252) 223-44I8 g -j cc p z ; �, C - H,SO, F - ZINC ACETATEINAOH o F rz �+ ® w a+ p' o, G - NATI-IIOSULFATE SAMPLE LOCATION Drying Bed Sludge PLEASE CI4A,IN OF CUSTODY RECORD MEN SICi) DATE/iIME COMMENTS: ( �-� I 11„_ I.. r , )� a CLASSIFICATION: WASTEWATER (NPDES) DRINKINGWATER DWOIGW SOLID WASTE SECTION CHAIN OF CUSTODY MAINTAINED DURING SHIPMENTIDELIVERY t % N SAMPLES COLLECTED BY: (Please P 1) SAMPLES RECEIVED I AT etin thi n the reverse side. Sampler must place a "C" for composite sample or a "G" for l4 `' 267889 59-6clions for comp) g Grab sample in the blocks above for each parameter requested. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION The Town of Newport met pathogen reduction and vector attraction reduction requirements through fecal coliform density and incorporation. Data is attached to reflect the methods of meeting pathogen reduction and vector attraction reduction. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) _J Facility Name: Town of Newport WWTP Name: Town of Newport WWTP Monitoring Period: From 1/1/2014 To WQ Permit Number: WQ0008349 NPDES Number: NCO021555 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) D JAltB (Alk Treatment) D Alt. C (Prior Testing) ..:.... lt.v Prior Test) Processto Further Pathogens : : If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ® Heat Drying D Heat Treatment D Thermophilic D Beta ® B a Ra Ray ® Gamm aR Pasteunza tion Class B: Alt. (1) Fecal Density Alt. (2) Process to SignjRcantly Reduce Patho ens .................... ................... If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization D Air Drying D Composting D Aerobic Digestion D Anaer obic Dig estion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee Frequency of Analysis Sample Tdences,ype Analytical Tech- nique Geo. Mean xim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 403 938 1,740 MPN/ Gram 0 Annually Grab SM18 . 9221E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vas-+nr A++rar+inn 'Upolnrtinn (15A NCAC. (12T _1-1071- Pienw. indicate alternative performed: Alt.I (VS reduction) D Alt. 2 (40-day bench) ® Alt. 3 (30-day bench) D J Alt. 4 (Spec. OZ uptake) D Alt. 5 (14-Day Aerobic) D Alt. 6 (Alk. Stabilization D Alt 7 (Drying - Stable) D I Alt. 8 (Drying - Unstable) D Alt. 9 (Injection) D Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed D CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." D "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Scotty Rollins, WWTP Operator Mr. John W. Dunham, Land Applier Preparer Name a Titl ( or print) Land Applier Name and Title (if applicable)(type or print) Signa of reparer* Date i ature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC.2T .1102 (26) nFNR FORM PVRF n9T (1919onR) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION DOCUMENTATION 1 PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION DOCUMENTATION The Town of Newport met pathogen reduction and vector attraction reduction requirements through fecal coliform density and incorporation. The annual certification form is marked accordingly to - reflect the methods of meeting pathogen reduction and vector attraction reduction. 7 t Town of Newport Newport WWTP WQ0008349 Jan-14 Environment One Lab # Date Analyzed Fecal Coliform per gram Log 1 1/27/14 403 2.605 2 1/27/14 546 2.737 3 1/27/14 937 2.972 4 1/27/14 1,212 3.084 5 1/27/14 1,159 3.064 6 1/27/14 1,270 3.104 7 1/27/14 1,740 3.241 Totall 20.806 Averagel 2.972 Most Probable Number / Gram 1 938 Fecal Coliform/gram Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction requirement Data provided in this summary have been used for the values and geometric means reported on the Annual Pathogen and Vector Attraction Reduction Form for this land application event. ra o n L1 n _ n _ -n s ,a..;; .x i:.}-�.+a.: i•;F: r ;. R_, 'k ,. :._..,.. :...,:il i*c �:';• .w "S'3g"'i+ vts, '_. P.O. BOX 7085, 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27835-7085 FAX (252) 756-0633 TOWN OF NEWPORT (SLUDGE) CHRIS MASSENGILL P.O. BOX 1869 NEWPORT ,NC 28570 ID#: 392 DATE COLLECTED: 01/27/14 DATE REPORTED : 03/11/14 REVIEWED BY: Sample Sample Sample Drying Bed Analysis Method PARAMETERS #1 #5 #6 Sludge Date Analyst Code Aluminum, (dry wt. basis), mg/kg 4439 02/07/14 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 3 03/04/14 MEL 3113B-04 Calcium (dry wt. basis), mg/kg 41836 02/07/14 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg 1.2 03/09/14 MEL 3113B-04 Copper (dry wt. basis), mg/kg 446 02/07/14 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 13 02/07/14 LFJ EPA200.7 Lead (dry weight basis), mg/kg 13 03/03/14 MEL 3113B-04 Magnesium (dry wt. basis), mg/kg 1264 02/07/14 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.49 02/11/14 ADD 245.1 R3-94 Nickel (dry wt. basis), mg/kg 8 02/07/14 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 1769 02/07/14 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 03/10/14 MEL 3113B-04 Sodium (dry wt. basis), mg/kg 2807 02/07/14 ADD 3111B-99 Zinc (dry wt. basis), mg/kg 817 02/07/14 ADD 3111B-99 Total Solids, % 13.4 13.8 12.6 12.9 01/28/14 CMC 2540G-97 TKN (dry wt.), mg/kg 26574 01/30/14 ANO 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg 2930 01/30/14 ANO 350.1 R2-93 Nitrate Nitrogen(dry wt.), mg/kg <3.36 01/29/14 ANO 353.2 R2-93 Nitrite Nitrogen(dry wt.), mg/kg 5.04 01/29/14 ANO 353.2 R2-93 Phosphorus, T. (dry wt.), mg/kg 3297 01/30/14 ALB 365.4 -74 Fecal Coliform (MPN), /gram Solids 403 1159 1270 01/28/14 CMC 9221E-06 Molybdenum (dry wt. basis), mg/kg <5.0 02/07/14 LFJ EPA200.7 Environment 1, Inc. P.O. Box 7095, 114 Oakmont Dr. Greenville, NC 27858 CHAIN OF CUSTODY RECORD Page 1 of 1 Phone (252) 756-6208 • Fax (252) 756-0633 DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION CHLORINE pH CHECK (LAB) CLIENT: 392 Week: 7 UV P P P P P P P P P P P G G G G G CONTAINER TYPE, P/G TOWN OF NEWPORT (SLUDGE) NONE CBRIS MASSENGILL A A A A A A A A A A A A A A A A CHEMICAL PRESERVATION P.O. BOX 1869 NEWPORT NC 28570 A -NONE D-NAOH o y (252) 223-4418 z J w z w .o w b B- HNO3 E HCL 0 0 oc CI_O z z o Z c p w a a x w W cn C HzSO4 F ZINC ACETATE/NAOH COLLECTION J — w w I w O o °' o O U d o U U U U U G NATHIOSULFATE SAMPLE LOCATION DATE TIME O Q s F d Z Z K Sample #1 L `% /0/o 1 CLASSIFICATION: Sample #2' �7 /c'� 1 WASTEWATER (NPDES) DRINKING WATER Sample #3 0 JZ- 1?" Sample #4 �� 10131 ?" Sample #5 1 /,-) ! q 1 "' DWQ/GW SOLID WASTE SECTION Sample#6 ,L.� ��/-� 1 ���'••`••` ... Sample #7 /1 " E� �"` 1 ��%��'•»� CHAIN OF CUSTODY MAINTAINED DURING SHIPMENT/DELIVERY Drying Bed Sludge U �� / 10 :;<•r.:'•: Es:`!4ir �` •:.:.. ?�^: "�%? 2`ti?! :err+- � G ._._.. ..:.... ::.... ..::::.: .. ;::.._ ,: :...... ,.:: ...... :...: ,.__.. •;;:•;:.:: ......_ :. __... y N SAMPLES COLLECTED BY: (Please Pnnt) SAMPLES RECEIVED I B AT I Z_°C RELINQUISHED BY (SIG) (SAMPLER) _ i DATUTIME j/ _ REC (SIG.) � COMMENTS: s LDATE/TIME RELINQUIS BY (SIG.) DATE/TIME RECEIVE (SIG. DATE/TIME RELINQUISHED BY (SIG.) DATEMME RECEIVED BY (SIG.) DATE/TIME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for IV 267889 Fr)pm 0.5 Grab sample in the blocks above for each parameter requested. Enw,unnnold % hwpo umbd P.O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 TOWN OF NEWPORT (SLUDGE) CHRIS MASSENGILL P.O. BOX 1869 NEWPORT ,NC 28570 PARAMETERS Total Solids, % Fecal Coliform (MPH /gram Solids Sample Sample Sample #2 #3 #4 12.83 13.87 11.55 546 937 1212 g Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 392 DATE COLLECTED: 02/05/14 DATE REPORTED : 02/11/14 REVIEWED BY: 4 Sample Analysis Method #7 Date Analyst Code 13.79 02/06/14 CMC 2540G-97 1740 02/06/14 CMC 9221E-06 Environment 1, Inc. P.O. Box 7085, 114 Oakmont Dr. Greenville, NC 27858 CHAIN OF CUSTODY RECORD Page 1 of 1 Phone (252) 756-6208 ^ Fax (252) 756-0633 DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION CHLORINE CLIENT: 392 Week: 1 UV pH CHECK (LAB) p p CONTAINER TYPE, P/G TOWN OF NEWPORT (SLUDGE) NONE CMUS MASSENGILL P.O. BOX NEWPORT NC C 28570 � A A CHEMICAL PRESERVATION A -NONE D-NAOH z E ,_ (252) 223-4418 z w o L zo In b B HNO3 E HCL o o 0 w z - Uj C- H,SO, F- ZINC ACETATE/NAOH COLLECTION Q _ o o G NATHIOSULFATE SAMPLE LOCATION DATE TIME o0_ o w Q Sample #2 CLASSIFICATION: Sample #3 �C �? r7r ! �-) 1 "wil IF% WASTEWATER (NPDES) Sam le #4 S O �J � � � 1 �1;'" J DRINKING WATER Sample #7 � lo3 �� r ,. DWQ/GW SOLID WASTE SECTION CHAIN OF CUSTODY MAINTAINED DURING SHIPMENT/DELIVERY ® N SAMPLES COLLECTED BY: (Please Print) y� SAMPLES RECEIVED IN LAB AT CY -C RELINQUISHED BY (SIG.) (SAMPLER) .� D TE/TIME I ED 8Y (SI r DATE/rIME COMMENTS: ze c 4 y ei£ CD 1 RELLIINNQUISHE (SIG.) DATE/TIME RECEIVED BY ( DATErrIME RELI'JQUISHED BY (SIG.) DATE/TIME RECEIVED BY (SIG.) DATUTIME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C for composite sample or a "T for a r FORM #5 Grab sample in the blocks above for each parameter requested. 2 7 4 2 6 11 SOIL ANALYSIS REPORTS NCDA&CS Agronomic Division Phone: (919) 733-2666 Website: www.neagLgov/agronami/ FY15-WO03117 "^:'�; ``' ,' Diagnostic Client: Craven Ag Services, Inc. Advisor. IN 2115 Hwy 55 � ...1�ii1h � Waste Report New Bern, NC 28562 Craven County - sempled.--141 1-4/2014.----Raceived: 11/18/2014 Completed: 11/26/2014 Farm: Durham Links to Helpful Information Sample Information Nutrient and Other Measurements Nitrogen (N) (ppm) P (ppm) K (ppm) Ca (ppm) Mg (ppm) S (ppm) Fe (ppm) Mn (ppm) Zn (ppm) CU (ppm) B (ppm) Na (ppm) C (ppm) Sample !D: CWEA Total N 566 4060 19100 55200 11000 3350 8390 765 363 116 71.8 1460 Waste Code: SAR Description: Total Kjeldahl N :...... ............................................ ---......... ....---------------------------•--....-----•----------------------- 4rdust.-Stack-A9h--•-w pH DM (%) SS (10-5s/cm) EC (mS/cm) CC (%) ALE(tons) C:N inorganic N Comments: NH4-N 11.37 76.0 17.8 6.67 NOa-N Organic N Ni (ppm) Cd (ppm) Pb (ppm) Al (ppm) Se (ppm) Li (ppm) As (ppm) Cr (ppm) Co (ppm) Cl (ppm) MCI (ppm) Urea 8.66 0 28.6 Estimate of Nutrients Available for First Crop (lb I ton) Other Elements (lb / ton) Application Method N P205 K20 Ca Mg S Fe Mn Zn Cu B Mo CI Na Ni Cd Pb Al Se Li Broadcast 0.43 9.90 27.8 58.7 11.7 3.57 8.93 0.81 0.39 0.12 0.08 2.22 0.01 T 0.04 Soil Incorporated 0.52 11.3 31.3 67.1 13.4 4.08 10.2 0.93 0.44 0.14 0.09 2.22 0.01 T 0.04 Agronomist's Comments: *Aaron Pettit 11/26120144:13 PM North Carol ina ��hurir itu+C Fund Ci�rtu:rss(c+n Reprogramming of the laboratory4nformation-management system that makes this report possible Is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. ,Steve Troxler, Commissioner ofAgriculture. 2014 APPLICATION SUMMARY TABLE 1 TOWN OF NEWPORT LAND APPLICATION PROGRAM PERMIT NO. WQ0008349 CRAVEN AG SERVICES, INC. 2014 APPLICATION SUMMARY .... ..... ... . ............. ............... .... .... .. ...... ...... . ....... . . .. farmer ifi: $i$iii. .......... ........ .............. ......... ii'. .... ........................... .......... 11 .... ... ........... .......... ................ .... ........... ........... ...... t6ikil ... .......... 16 . .................... "X:*- ... ...... ... ................. .. ....... ............... .... . .... .. ....... ... ....... ........ X.P.- . . . . . . . . . . . . - - - - - - - - - - - . . . . . . . . . . . Allen Roach AR 8 11 May-14 192 2.29 25.19 Soybeans 45.95 Number of Fields Applied to: 1 11.00 Town of Newport WWTP ... .. X-T: .. ........ 192 25.19 22.90 Permit Limit 200 Branch Residuals Soils, LLC Confidential 2/5/2015 Page 1 2014 APPLICATION CONDITION SUMMARY J Town of Newport Newport, North Carolina Craven Ag Services WQ0008349 Annual 2014 Town of Newport WWTP Farmer: Allen Roach Acres: 11 Site/Tract: AR Application Method: Incorporated Field: 8 Percent Solids: 13.12 Residual Report No.: EI 392 Crop: Soybeans Date Field No. Sulbfield Wet Tons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 5/8/14 8 192.00 Good Warm, Clear 0.00 1. : <1:..2:d10< 9. .