WQ0008008_Residual Annual Report 2014_20150306

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PASQUOTANK COUNTY
WATER TREATMENT
FACILITY
2014 ANNUAL LAND APPLICATION OF
RESIDUAL BIO-SOLIDS REPORT
CLASS B PROGRAM
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Submitted by:
Soil Plus
208 Williams Street
Greenville, North Carolina 27858
February 25, 2015
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February 25, 2015
NCDENR-DWQ
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2014 LAND APPLICATION ANNUAL REPORT
Pasquotank County Water Treatment Facility "Class B" Program
NC Permit No.: WQ0008008
Soil Plus Project No. 200701.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the Pasquotank County Water Treatment
Facility on behalf of Atlantic OBX, Inc. Soil Plus compiled this report using data gathered
during the compliance year. This data includes (1) certification form, (2) residual sampling,
(3) field loading calculations, (4) standard soil fertility nutrient analysis.
The Pasquotank County Water Treatment Facility conducted application events on
permitted fields in Pasquotank County during 2014. A total of 18.86 Dry Tons or 288,000
gallons of permitted residual bio-solids were land applied to permitted fields.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact me or the Pasquotank County Water Treatment Facility (252-
335-2240) for further assistance.
Respectfully,
C. Scott Carpenter, L.S.S.
North Carolina Nutrient Management Planner
Pasquotank County Water
J. Bryan Smith, Atlantic OBX, Inc.
T 208 Williams Street
Greenville, NC 27858
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t [phone]
f [phone]
www.soilplus.net

ANNUAL LAND
APPLICATION
Pasquotank County CERTIFICATION FORM
Water Treatment Field Loading & Source Summary
Facility Annual
Land Application of
Residual Bio-Solids ANNUAL RESIDUAL
Report SAMPLING SUMMARY
FORM
WQ0008008 Annual Analytical Data
S
Elizabeth City, NC
FIELD LOADING
SUMMARY FORM
SOIL SAMPLES
Site 1
Site 1

u
APPENDIX I
CERTIFICATION FORM
SUMMARY FORM
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Cl
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ANNUAL LAND APPLICATION CERTIFICATION FORM
-` PermitNumber FacihtyName Land Application Operator County Phone Number
WQ0008008 Pasquotank County Regional Water Atlantic OBX, Inc. Pasquotank [phone]
Treatment Fac.
Year: 2014
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part Yes No
B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the W ❑�
residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 5
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites: 18.86
Total number of acres utilizes for land application during the year: 23.4
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality ❑d Fol
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
1. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
-ertified laboratory results are attached
5.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated
:acilities).
3. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated
Facilities).
). All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
.riclude appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
'I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
omplete. I am aware that there are significant penalties for submitting false informs ' including the possibility of fines and
mprisonment for knowing violations."
�aJ.� Sr6►�ras� S�.�P6eta-c�,�t�,JT
Permittee Name and Title (type or print):
Si re of Permittee
2-25-205-2015 ,
"-'ignature of Date
'if different from Permittee)
Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Signature of Land Applier Date
(if different from Permittee)
Wednesday, February 25, 2015
t

Source Summary Report
WWT.P1 Volug eApplied = 4otal Dvy7ons ,
Pasquotank County Regional Water 288,000 18.86
Treatment Fac.
Total 288,000 18.86 .,
Wednesday, February 25, 2015 Page 1 of 1

YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED
PERMITTED CROPS AND LOADING RATES
Acres
Volume Crop 1 PAN Crop 2 PAN
Total P
Crop 1 PAN 1
Crop 2 PAN 2
Field Used
Applied Total DT lbs/Ac. lbs/Ac.
lbs/Ac.
Crop 1 Name PAN Used
Crop 2 Name
PAN Used
Site# 1
A 10.59
168,000 11.00 4.83
10.87
Soybeans, Manured, 184 2.6%
Wheat, Grain
50
Full Season
B 12.81
120,000 7.86 2.85
6.42
Soybeans, Manured, 184 1.5%
Wheat, Grain
50
Full Season
Total 288,000 18.86
Wednesday, February 25, 2015 Page 1 of 1

APPENDIX II
RESIDUAL SAMPLING SUMMARY FORM
FIELD LOADING CALCULATIONS
ANALYTICAL
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ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0008008 Facility Name Pasquotank County Regional W Source Pemrit No. DWS O4-70-015 Source Name Pasquotank County Regional Water
.Laboratory 1 Environment
1,Inc.
Laboratory 2
Sample or CompositeDate 2/7/2014
Parameter (mg/Kg) Class A Clas B
Aluminum
N/A
N/A
4,771
Ammonia Nitrogen
N/A
N/A
401
Arsenic
41
75
2.5
Cadmium
39
85
0.5
Calcium
N/A
N/A
3,866
Copper
1,500
4,300
7
Lead
300
840
5.4
Magnesium
N/A
N/A
3,017
Mercury
17
57
0.04
Molybdenum
N/A
75
5.00
Nickel
420
420
5
Nitrate -Nitrite Nitrogen
N/A
N/A
10
Percent Solids
N/A
N/A
1.57
pH (no units)
N/A
N/A
7.50
Phosphorus
N/A
N/A
5,231
Potassium
N/A
N/A
825
PAN (Inj./Inc.)
N/A
N/A
2,524
PAN (Surface)
N/A
N/A
2,323
Selenium
100
100
5
Sodium
N/A
N/A
2,124
SAR
N/A
N/A
0.78
TKN
N/A
N/A
5,683
Zinc
2,800
7,500
i-
34 '
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations"
Signature of Preparer*\-) I ` Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

-AGMAN
3 FIELD LOADING ESTIMATES
Facility Pasquotank County Regional Water
Sampling Date 2/7/2014
% Solids 1.57
Mineralization Rate 0.40
Gallons per DT 15,274.40
pH 7.5
Sodium Absorpotion 0.78 <5.0 Safe 5.0 - 10.0 Careful Management > 15.0 Do Not Land Apply,
Ratio
NITROGEN APPLICATION
NUTRIENT APPLICATION
TKN (mg/Kg) 5,683 lbs./1,000 gal 0.74
Potassium lbs./1,000 gal
0.11
Ammonia Nitrogen (mg/Kg) 401.00 lbs./1,000 gal 0.05
Phosphorus lbs./1,000 gal
0.68
Nitrate -Nitrite (mg/Kg) 9.82 lbs./1,000 gal 0.00
Calcium lbs./1,000 gal
0.51
PLANT AVAILABLE NITROGEN SURFACE APPLIED
Magnesium lbs./1,000 gal
0.40
PAN (mg/Kg)' 2,323 lbs./1,000 gal 0.30
Manganese lbs./1,000 gal
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
Sulfur lbs./1,000 gal
PAN (mg/Kg) 2,524 lbs./1,000 gal 0.33
Molybdenum lbs./1,000 gal
0.00
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
1st Year
2nd Year
C3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
2.50
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.50
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
7.00
Copper lbs./1,000 gal
0.00
Lead (mg/Kg)
5.40
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.04
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
5.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00 .
Zinc (mg/Kg)
34.00
Zinc lbs./1,000 gal
0.00
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TEN
(mg/kg) (lbs/DT)
'(mg/]Kg)
TIQV
(mg/kg) (lbs/DT)
(mg/]Kg)
5,683
2,323
4.65
3,360
5,683
2,524 5.05
3,159
3,360
672
1.34
2,688
3,159
632 1.26
2,528
2,688
269
0.54
2,419
2,528
.253 0.51
2,275
2,419
121
0.24
2,298
2,275
114 0.23
2,161
2,298
57
0.11
2,241
2,161
54 0.11
2,107
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 3,442 6.88
Total 3,576 7.15

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GREENVILLE. N.C. 27835-7085 PHONE r,� 5='1 7;;8 ?);
FAX
PASQUOTANK CO. WATER (SLUDGE),
MR. RONNY JENNINGS
P.O. BOX 2245
ELIZABETH CITY ,NC 27906
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry\ wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury, (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg .
Selenium (dry wt. basis), mg/kg
Sodium .(dry wt. basisj, mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids,, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Water Plant Analysis Method
Sludge Date Analyst Code
7.5
02/07/14 TRB
4500HB-00
4771
03/05/14 LFJ
EPA200.7
<2.5
03/24/14 MEL
3113B-04
3866.3
03/05/14 LFJ
EPA200.7
<0.5
03/19/14 MEL
3113B-04
7
03/05/14 LFJ
EPA200.7
9
03/05/14 LFJ
EPA200.7
5.4
03/21/14 MEL
3113E-04
3017
03/05/14 LFJ
EPA200.7
0.04
02/11/14 ADD
245.1 R3-94
<5.0
03/07/14 LFJ
EPA200.7
825
03/05/14 LFJ
EPA200.7
<5.0
03/25/14 MEL
3113B-04
2124
03/07/14 ADD
3111B-99
34
02/21/14 ADD
3111B-99
1.57
02/11/14 CMC
254OG-97
5683
02/17/14 ANO
351.2 R2-93
401
02/11/14 ALB
350.1 R2-93
5231 ,
02/14/14 ANO
365.4 -74
9.82
02/12/14 ANO
353.2 R2-93
1795
02/20/14 SEJ
<5.0
03/05/14 LFJ
EPA200.7
ID#: 149
DATE COLLECTED: 02/07/14
DATE REPORTED : 03/28/14
REVIEWED BY:
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ENVIHCN'•:ENTALTECHNOLOGIES, INC.
Laboratories
LABORATORY REPORT
Client
Environment 1, Inc.
114 Oakmont Dr
Greenville, NO 27858
Order Number
1400334
Project Number
Pasquotank Co. Water (Sludge)
Issued
Tuesday, February 25, 2014
Total Number of Pages
.6 (excluding C.O.C. and cooler receipt form)
Approved By:
l ,
QA Manager
Certifications: A2LAlDOD 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105,
Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho 01-100923, Illinois 200061 and Reg.5, Indiana
C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and
LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Michigan (Reg.5), Minnesota 409711.
Montana CERT0099, New Hampshire 2996, New Jersey 01-1006, New York 11777, North Carolina 39705 and
631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon 01-12O0001, Pennsylvania 68-01335, Rhode Island
LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 5 WG-15J, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581,
Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013016
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CUyahoga falls, ,...:� - Phone:3�t1-25;-8
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EFiViR(:)NIOENTALTECHNO!-�«.IF-S, INC.
Anefyficp.j Laboratories:
2
Sample Summary
Client: Environment 1. Inc.
Order Number. 1400334
Laboratory ID
Client ID
Matrix
Sampling Date
1400334-01
Water Plant Sludge
Sludge
217/2014
A,.nafyticaf Integrity', c'7,'-'A Certified NELAP Cortiflec!
C,1-kyahoga Falls. 44';23 - Phone: [phone]' Fax:
151i-'r�. ivww.sette1c.com

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ENVlt9ON!'ENTAL TECHi4OLOGIE;,, INC. -
{�:tul� .iic<:t Laboratorie.,,
Report Narrative
Client: Environment 1. Inc
Order Number: 1400334
K
No problems were encountered during analysis of this order number, except as noted.
Method numbers, unless specified as SM or ASTM, are EPA methods.
Method of analysis for TCLP Volatiles is 1311/8260B
Method of analysis for TCLP Metals is 1311/6010B and 13.11/7471A
Method of analysis for TCLP BNA is 1311/8270C
Data Qualifiers:
B = Analyte found in the method blank
J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOCI)
C = Analyte has been confirmed by another instrument or method
E = Analyte exceeds the upper limit of the calibration curve,
D = Sample or extract was analyzed at a higher dilution
X = User defined data qualifier.
S = Surrogate out of control limits
U = Undetected
a = Not Accredited by NELAC
ND = Non Detected at LOQ
DF = Dilution Factor
Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor)
Limit. Of Detection (LOD) = Method Detection Limit
Practical Quantitation Limit (PQL) = (same as LCQ)
Method Detection Limit (MDL) = (same as LOD)
Reporting Detection Limit (RDL) = (same as LOD)
Estimated uncertainty values are available upon request.
Matrices:
A = Air
C = Cream
DW = Drinking Water
L = Uquid
O = Oil
SL = Sludge
SO = Soil
S = Solid
T = Tablet
TC = TCLP Extract
WW = Waste Water
W = Wipe
The test results meet the requirements of the NELAC standard, except where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot
be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this
report was issued. The results contained In this report are only representative of the samples received. Conditions
can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not
responsible for use or interpretation of the data Included herein.
/alic'1Vt�lcB1Integri'; r HPA Certified • NELAP ;if
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ENVIRON`•.�ENTALTECHNOL.DCi!ES INC.
i6m,- A`icer/ Laboraforiec
e
TCLP Volatllos
Client 1D#
Lab @#
Collected Anelyte
Rep Lmt
&suit
Water Plant
1400334-01
07-Feb-14 Chloroform
0.1
ND
Sludge
Water Plant
1400334-01
07-Feb-14 1,2-Dichlomethane
0.1
ND
Sludge
Water Plant
1400334-01
07-Feb-14 Benzene
0.1
ND
Sludge
Water Plant
1400334-01
07-Feb-14 Carbon tetrachloride
0.1
ND
Sludge
Water Plant
1400334-01
07-Feb-14 Trichloroethene
0.1
ND
Sludge
Water Plant
1400334-01
07-Feb-141,1-Dichlomethene
0.1
ND
Sludge
Water Plant
1400334-01
07-Feb-14 Tetrarhloroethene
0.1
ND
Sludge
Water Plant
1400334-01
07-Feb-14 Chlorobenzene
0.1
ND
Sludge
Water Plant'
1400334-01
07-Feb-14 2-Butanone (MEK)
2
ND
Sludge
Water Plant
1400334-01
07-Feb-14 Vinyl Chloride
0.2
ND
Sludge
TCLP BNA
Client 1D#
lab II3#
Collected Analyta
Rep Lmt
Result
Water Plant
1400334-01
07-Feb-14 2,4,5-Trichlomphenol
0.25
ND
Sludge
Water Plant
1400334-01
07-Feb-14 Nexachlomethane
0.1
ND
Sludge
Water Plant
1400334-01
07-Feb-14 Cresols
5
ND
Sludge
Water Plant
1400334-01
07-Feb-14 Nitrobenzene
0.1
ND
Sludge
Water Plant
1400334-01
07-Feb-14 2,4,6-Trichlomphenol
0.25
ND
Sludge'
Water Plant
140033+01
07-Feb-14 Pentachlomphenol
0.25
ND
Sludge
Water Plant
1400334-01
07-Feb-14 Hexachioro-1,3-butadlene
0.1
ND
Sludge
Water Plant
1400334-01
07-Feb-14 Pyridine
0.25
ND
Sludge
Water Plant
140D334-01
07-Feb-14 2,4-Dlnitrotoluene
0.1
ND
Sludge
Water Plant
1400334-01
07-Feb-141,4-Dldtlombenzene
0.1
ND .
Sludge
Water Plant
1400334-01
07-Feb-14 Hexachlombenzene
0.1
ND
Sludge
February 25, 2014
Client: Environment 1, Inc.
Address: 114 Oa]anont Dr
- Greenville, NC 27858
Received: 2i1112014
Project M Pasquotank Co. Water (Sludge)
JTsi& Matrix Method DF flfflLad Run Anal
mg/L
SL
1311
1
6
24-Feb-14 MS
mg/L
SL
1311
1.
0.5
24-Feb-14 MS
mg/L
SL
1311
1
IS
24-Feb-14 MS
mg/L
SL
1311
1
0.5
24-Feb-14 MS
mg/L
SL
1311
1
0.5
24-Feb-14 MS
mg/L
SL
1311
1
0.7
24-Feb-14 MS
mg/L
SL
1311
1
0.7
24-Feb-14 MS
mg/L
SL
1311
1
100
, 24-Feb-14 MS
mg/L
SL
1311
1
200
24-Feb-14 MS
mg/L
SL
1311
1
0.2
24-Feb-14 MS
[.1_ nits Matrix Method DF RegLvl Run Anal ..;
mg/L
SL
1311
1
400
18-Feb-14 AE
mg/L
SL
1311
1
3
18-Feb-14 AE
mg/L
SL
1311
1
200
18-Feb-14 AE
mg/L
SL
1311
1
2
18-Feb-14.AE
mg/L
SL
1311
1
2
18-F0-14 AE
mg/L
SL
1311 •
1
100
18-Feb-14 AE
mg/L
SL
1311
1
0.5
18-Feb-14 AE
mg/L
SL
1311
1
5
18-Feb-14 AE
mg/L
SL
1311
1
0.13
18-Feb-14 AE
mg/L
SL
1311
1
7.5
18-Feb-14 AE
mg/L
SL
1311
1
0.13
18-Feb-14 AE
�,alytical Integr•it,�" = Certified - NEL 1P Cerliiien
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Page 4
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ENVIRON;'ENTALTECHNOLOGIES. INC.
February 25, 2014
Lahoraiorie�:
Client: Environment 1, Inc.
Address: 114 Oakmont Dr
Greenville, NC 27858
Received: 2111/2014
Project M Pasquotank Co. Water (Sludge)
•
TCLP Pesticides
„
Client IN
Ub M#
Collected Analyi
Reo Lmt Result
Units Matrix Method DF ReaLyl Run Analyst
Water Plant
Sludge
1400334-01
07-Feb-14 Heptachlor Epoxide 0.002 ND
mg/L SL 1311 1
0.008
18-Feb-14 JBN
Water Plant
Sludge
1400334-01
07-Feb-14 Endrin
0.002 ND
mg/L SL 1311 1
0.02
18-Feb-14 38N
Water Plant
Sludge
1400334-01
07-Feb-14 Chlordane
0.01 ND
mg/L 5L 1311 1
0.03
18-Feb-14 JBN
Water Plant
Sludge ,
1400334-01
07-Feb-14 Gamma-BHC
0.002 ND
mgJL SL 1311 1
0.4
18-Feb-14 JBN
Water Plant
Sludge
1400334-01
07-Feb-14 Toxaphene
0.1 ND
mg/L SL 1311 1
0.5
18-Feb-14 JBN
Water Plant
Sludge
1400334-01
07-Feb-14 Methoxychlor
0.002 ND
mg/L SL 1311 1
10
18-Feb-14 JBN
Water Plant
Sludge
1400334-01
07-Feb-14 Heptachlor
0.002 ND
mg/L SL 1311 1
0.008
18-Feb-14 JBN
•
TCLP Herbicides
Client ID#
La_ b 1p#
Collected Analyte
Reo Lmt Result
Units Matrix Method DF
RegLvl
Run Analyst
Water Plant
Sludge
1400334-01
07-Feb-14 2,4,5-TP(Silvex)
0.5 ND
mg/L SL 1311 1
1
19-Feb-14 AMZ
Water Plant
Sludge
1400334-01
07-Feb-14 2,4,D
5 ND
mg/L SL 1311 1
10
19-Feb-14 AMZ
TCLP Arsenic
Client_IB#
Lab IBH
Collected Analyto
Rep Lmt Result
Units Matrix Method DF
Re4Lvl
Run Analyst
a
Water Plant
Sludge
1400334-01
07-Feb-14 TCLP Arsenic
0.5 ND
mg/L SL 1311 1
5
12-Feb-14 WK
TCLP Barium
Clement ID
Lab f
Collected An_alnte
Rep Lmt jtesult
Units Matrix Method DF
ReoLv1
Run Analyst
Water Plant
Sludge
1400334-01
07-Feb-14 TCLP Barium
5 ND
mg/L SL 1311 1
100
12-Feb-14 WK
TCLP Cadmium
Client UM
_Lab j1
Collected Analyte
Reo Lmt Result
Units MaFx Method DF .
ReaLyl
Run Anal st
Water Plant
Sludge
1400334-01
07-Feb-14TCLP Cadmium
0.1 ND
mg/L SL 1311 1
1
12-Feb-14 WK
TCLP Chromium
Client ILT#1
lab ID#
Collected Analvte
Rep Lmt Result
. Units Matrix Method DF
ReQUI ,
Run Analyst
Water Plant
Sludge
1400334.01
07-Feb-14 TCLP Chromium
0.2 ND
mg/L SL 1311 1
5
12-Feb-14 WK
TCLP Lead
Client 1D#
Lab LD#
Collected Anal vte
Rep Lmt Result
Units 'Matrix Method DF
ReaLvl
Rem Analyst
Water Plant
Sludge
1400334-01
07-Feb-14 TCLP Lead
0.5 ND
mg/L SL 1311 1
5
12-Feb-14 WK
Page 5
I• _
j1nalyticallntegrity- I 7,; Certified
NELAP
Certifieda
i G .'•; In
Cuyahoga F Falls,,
Phone:
. ,
330-253-r!7.peri
.
W. D _ .::>. - w. w.Sedek.com
t
,

141
"'Aar
ENVIRO.N,'ENTALTECHt,,'01..OGIES.
INC.
February 25, 2014
Lsboratori&.
Client: Enviromment 1,
Inc.
Address: 114 Oalanont Dr
Greenville, NC 27858
Received: 2/11,12014
Project#: Pasquotank Co,
Water (Sludge)
TCLP Mercury
Client IDA!
Lab IDA!
qQl1p;tqd. Analyt
Rep Lmt
Result
Units Mq!Eix Method
DF
ReaLvi
Run Analyst
Water Plant
1400334-01
07-Feb-14 Mercury
0.002
ND
mg/L SL 1311
1
0.2
11-Feb-14 AL]
Sludge
TCLP Selenium
Client MN
Lab 09
—
Collect Anal3j
Rep Lmt
Rgig
Units Matrix M--gb-od
gF_
Real -A
gim Anaivs
Water Plant
1400334-01
07-Feb-14 TCLP Selenium
0.5
ND
mg/L SL 1311
1
1
12-Feb-14 WK
Sludge
TCLP Sliver
CliLept 1D#
Lab TD4
Collected Anaalyle
RepLmt
Result
Units MajdK Method
AF
ReqLv1
Run Lnalys
Water Plant
1400334-01
07-Feb-14 TCLP Silver
0.5
ND
mg/L SL 1311
1
5
12-Feb-14 . WK
Sludge
Client lI3#
Lab 1D#
Collect Anal Rc
Remit
Units Matri ethnd
2F
LOQ
Rm Analyst
Water Plant
1400334-01
07-Feb-14 Flash Point
>200
oF SL 1010
1
14-Feb-14 TG
Sludge
Client ID#
Lab 1D4
qq11eqq4 Anal to
&—it
Units Mapix ethod
RE
LOQ
R Analyst M
Water Plant
1400334-01
07-Feb-14 pH
6.95
S.U. SL 9040
1
0.01
12-Feb-14 AYS
Sludge
Client R?#
Lab IDA!
_qo ected Analyte L_
x9mi-t
Units Matrix M—e&Qd
2F
LQQ
Run Anal
Water Plant
140033+01
07-Feb-14 Reactive Cyanide
ND
mg/kg SL 7.3.3.2
1
0.5
12-Feb-14 MR
Sludge
Client IN
Lab lD#
Collected Analyt
BmAlt
UAIlLs Matrix Method
DF
LOQ
Em Analy.
Water Plant
1400334-01
07-Feb-14 Reactive Sulfide
ND
mg/kg SL 7.3.4.2
1
25
12-Feb-14 MR
Sludge
Page 6
"411alytical IntegrPy" Ef"A Certified - NELAP
Cuyahoga F611,-;, Phone: [phone]
k",:., vwwseltek. coin

Rev. 12
Date: 07/27/13
Order ID: 1400334 COOLER
Summit Environmental Technolo,,,,,,
r� Cooler Receipt Form
Initials of person inspecting cooler and samples:
Client: U Order Number:
Date Receive f! Time R ceived: Date cooler(s) opened and samples inspected: /`7/
r �I
Numb Coo ers/Boxe Z
N/A
Shipper: FED EX DHL Airborne UPS. Postal Walk-in Pickup Other:
Packaging: Pean �n bi6 a Wrap Paper Foam None Other:
Tape an cooler/box. N
NIA
Custody Seals intact
N N/A
C-O-C in stir
N N/A
Ice Blue Ice s t / absent / melted N/A
Sample Temperature IR Gun #16020459 CFat C
oC N/A
Radiological Testing Instrument serial #35127 Y 1
(see page 2 for scan results) N N/A
"Use 1 sheet per sample for Radiological Testing. If sample is HOT, the Radiological Safety Officer must be notified
immediately.
C-O-C filled out properly
N NIA
Samples in separate bags
N N/A
Sample containers intact"
N NIA
'If no, list broken sample(s):
Sample label(s) complete (ID, date, etc.) N
NIA
Labels) agree with C-O-C N
N/A
Correct containers used
N' NIA
Sufficient sample received N
v NIA
Bubbles absent from 40 mL vials— Y N
aNIA
—Samples with bubbles <6mm are acceptable., Indicate bubble size if >6mm.
Was client contacted about samples Y N
Will client send new samples Y N
Client contact:
Datefrime:
/ Logged in by: ,
Comments:
F
G:1QC SHARED\Document Control Templates - Tracking\Cooler receipt form Rev. 12 07-27-13.doc Page 1 of 2

Environment 1, Inc.
P n Rnx ?ARs I I d naL-mnnt nr
CHAIN OF CUSTODY RECORD
Greenville, NC 27858
IIIIIIIIIIIIIIIIIIIIIIIIIIIIO�IIII�IIIIIIIIIIIIIIII�IIIIIIII11111Q1110111111111111111U
Phone [phone] • Fax [phone]
I
DISINFECTION
Ij CHLORINE
Order
ID:
1400334
COC
CLIENT- 149 Week: 9
Ij Uv `
pH CHECK (LAB)
PASQUOTANK CO. WATER (SLUDGE)
.NONE
P
P
P
P
P
P
P
P
P
P
GJ-G
G
G
IG
I
CONTAINER TYPE, PIG
MR. RONNY JENNINGS
A
A
A
A
A
A
A
A
A
A
A
A
A
A
A
CHEMICALPRESERVAIION
P.O. BOX 2245
ELIZABETH CITY NC 27906
❑
A -NONE D-NAOH
.&o
[phone]
z o
o
Cn
,�
,°�
A
B-HNO, E-HCL
U¢
cc
y
W
C- H2S0, F- ZINC ACETATE/NAOH
COLLECTION
_ c
o
w
a o
¢
a4
K
U°
a
H
CV+
H
H
��
Ea "
G-NATHIOSULFATE
a
SAMPLE LOCATION
DATE
TIME
Water Plant Sludge
�'�' 14
qt dOQK�
ro
CLASSIFICATION:
WASTEWATER(NPDES)
DRINKINGWATER
DWO/GW
I� SOLID WASTE SECTION
CHAIN OF CUSTODY MAINTAINED
DURING SHIPMENTIDELIVERY
Y N
SAMPLES COLLECTED BY:
(Please Print)
o vv e, N tw
SAMPLES AECEIVED, IN LAB AT ! T—C
LINQUISH Y (SIG.) (SAMPLER)
DATE�IIME
A IV BY (SI
rL A1FlfIME
COMMENTS:
CQ
'0)-11-ILV
NQUIS (SIG.) V
DATUTIME
RECEIVED BY (
'DMUTIME
REt.114 H BY(SIG.)
DAWMME
RECEI B
p TWIME
PLEASE READ Instructions for complpling this form on the reverse side; Sampler must place a T" for composite sample or a "G" for n
=„oh.jUr Grab sample in the blocks above for each parameter requested. = 2739,032

APPENDIX III
FIELD LOADING SUMMARY FORM

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0008008
Site# 1
County Pasquotank
Crop 1 Soybeans, Manured, Full Season
Facility Name Pasquotank County Regional Wate Field Name A
SoilSeries Perquimans
Crop 1 Pan 184
LandOwner Pasquotank County
Acres Permited 10.59
Soil Abbrevation: PeA
Crop 2 Wheat, Grain
Operator Pasquotank County
Crop 2 Pan 50
Volume
Acres Dry
Soil
Application Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied % Solids Used DT/Ac. Tons
Source Condition Precip
Method P
Volatilization Mineralization TKN Ammonia
Nitrite PAN
PAN Crop
05/07/2014 Gallons 168,000 1.57
10.59 1.04 11.00k County Regional Water Trea Dry 0
Surface 10.87
0.50 0.40 5,683 401.00 9.82 4.83
Crop 1
Total Volume Applied 168,000
Total Dry Tons 11.00
Sum Total P 10.87
Total 4.83
Total
Reported in Gallons Arsenic Cadmium
Copper Chromium
Lead Mercury Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year 0.005 0.001
0.015 0.019
0.011 0.000 0.010
0.010 0.010
0.071
(Ibs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year 0.185 0.029
0.563 0.279
0.568 0.004 0.278
0.305 0.278
2.278
Cumulative Total 0.190 0.030
0.578 0.298
0.579 0.004 0.289
0.315 0.289
2.349
Permitted CPLR 36 34
1338
267 15
374 89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
2-25-2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
ignature of and pplier Date ****C.P.L.R.: Cumulative Pollutant Loading Rate

PermitNumber WQ0008008
Facility Name Pasquotank County Regional Wate
LandOwner Pasquotank County
Operator Pasquotank County
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Site# 1 County Pasquotank Crop 1 Soybeans, Manured, Full Season
Field Name B SoilSeries Perquimans Crop 1 Pan 184
Acres Permited 12.81 Soil Abbrevation: PeA Crop 2 Wheat, Grain
Crop 2 Pan 50
Volume
Acres
Dry
Soil
Date Measurement Applied
% Solids Used DT/Ac.
Tons Source
Condition Precip
05/08/2014 Gallons 120,000
1.57 12.81 0.61
7.86 k County Regional Water Trea
Moist 0
Application Total Nitrate- Crop 1 Crop 2
Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop
Surface 6.42 0.50 0.40 5,683 401.00 9.82 2.85 Crop 1
Total Volume Applied
120,000
Total Dry Tons 7.86
Sum Total P 6.42
Total 2.85
Total
Reported in Gallons
Arsenic
Cadmium
Copper Chromium
Lead
Mercury-
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.003
0.001
0.009 0.011
0.007
0.000
0.006
0.006
0.006
0.042
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.073
0.011
0.279 0.068
0.259
0.001
0.107
0.075
0.107
0.846
Cumulative Total
0.076
0.011
0.288 0.079
0.266
0.001
0.114
0.081
0.114
0.888
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Qom, *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
2-25-2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
ignature of and pplier ate ****C.P.L.R.: Cumulative Pollutant Loading Rate

APPENDIX IV
SOIL SAMPLES

;NCDAB,C$=Agronomrc Division .. <Pfione (919) _733=2655 . :.•. Webstte: ;,iiirinrwaicag:gov/ag�oriomi/ , ` : ,; : `; `:Report No � i=Y15=SL005603
Client: Pasquotank County Water System Advisor:
Heavy Metals Attn:John Gregory
PO Box 2245
,,, {,
; . 3 o i I Re p o 1 1, Mehlich-3 Extraction Elizabeth City, NC 27907
Sampled County: Pasquotank
Sampled: 08/13/2014 Received: 09/17/2014 Completed: 10/02/2014 Farm: Links to Helpful Information
Agronomists Comments:
This report contains both routine soil test information as well as heavy metals data in a section labeled as Heavy Metals under soil test lab results. Using Mehlich 3 as a soil test
extractant, background levels of these metals typically seen in NC soils when analyzed are as follows: arsenic (As)- 4.5 ppm, cadmium (Cd)- 0.1 ppm, chromium (Cr)- 0.2 ppm, lead
(Pb)- 4.2 ppm, nickel (Ni)- 0.8 ppm, & selenium (Se)- 0.2 ppm (FY2005-2007). Although the above metals here are not believed to pose a concern for plant growth, continue to monitor
these and note where elevated above background levels. Where soil test phosphorus (P) is very high (P-I > 100), crops will not respond to additional P applied. Tissue testing is advised
where soil pH is elevated such as SS115. For soybeans and small grains, there is potential for micronutrient deficiency at elevated pH, with most concern of Mn deficiency. If deficiency
occurs, foliar application is advised. Note lime and fertilizer recommendations. David H. Hard 10/1/2014
Sample ID: SS114
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Soybean 0.0 0 0 40 0 0 0 0 0 0
Note: 3
2-
Test Results [units - WN in g/crrt?; CEC and Na in meq/100 cd; NO3-N in mg/dn?]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn AI2 Zn4 Zn-AI Cu-1 Na ESP SS4 NO3-N
0.41 1.06 9.1 91 0.8 6.4 175 52 69 19 30 589 357 66 66 37. 0.1 1
;:.:Heavy Metals(P artsP er million)-: = : Arsenic,. ; 0:2 Cadmium; -0 0.- ° •: Nickel, 0.3 Chromiurrk .0:3 -,Lead; 4 2; : _ . = Selenium;
r.
Sample ID: SS115
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Soybean 0.0 0 0 50 0 0 pH$ 0 0 0
Note: 3 Note:
2-
Test Results [units - WN in g/cd; CEC and Na in megM00 cd; NO3-N in mg/do]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P4 K4 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N
0.32 1.15 10.7 95 0.6 6.9 118 46 77 15 28 922 550 68 68 26 0.1 1
_HevY MetaArseni_
.0;:=.
, , r.-01`..__...-..—Cadmiu m,..0 :0 Nikel0:2 -Ch-r°m m 02 ...._ Selenium,
. _
'North -..Carolina
-.7bbacco:Trust fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS:Agr"orromi.6 Division :. -- Phone ;.(9.79);733-2855 - . WeEisite: www ncag�:gov/agFonomi/ ::-`
- .Report No-- : FY15;SL005603.
Page 2 of 4
Sample ID: SS116
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N . P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1-.Soybean 0.0 0 0
50
0 0 0
0
0
0
Note: 3
2-
Test Results [units - WN in g/cd; CEC and Na in meq/100 crn3; NO3-N in mg/dnP]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P4 K4 Ca% Mg%
S-1 Mn-I
Mn All Mn Al2 Zn4
Zn-Al
Cu-1
Na ESP
SS4 NO3-N
0.41 1.06 9.8 91 0.9 6A 171 _. 42 70 19
39 780
471 69
69
56
0.1 1
=Heavy'.Metals(partsPer million):. -Arsenic;. 0:2 '._ _Cadmium, 0.0
Nickel,..0.3
Chromium ,';03 -; :...
.Lead;
3.3
Seleriium,-'Oa3.,
Sample ID: SS117
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Soybean 0.0 0 0
40
0 0 0
0
0
0
Note: 3
2-
Test Results [units - WN in g/crrr'; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S4 Mn-I
Mn All Mn-AI2 Zn-1
Zn AI
Cu4
Na ESP
SS-1 NO3-N
0.41 1.14 7.3 86 1.0 6.0 163 -52 63 19
28 284
180 76
76
32
0.1 1
Heavy Metals (parts per million):-- :Arsenic, A:2 _ - Cadmium; 0.0
Nickel;. 0:3.
`Ctiiomirim,- 0.3. =. - _ -
.. Lead;
1:6.
Selenium,
QA:' _
Sample ID: SS118
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
' K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Soybean 0.7 0 0
20
0 0 0
0
2
0
Note: 3
2-
Test Results [units - WN in g/cd; CEC and Na in meq/100 cO; NO3-N in mg/drr?]:
Soil Class: Mineral
HM%o WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn All Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
0.32 1.09 5.5 71 1.6 5.5 183 66 48 18
32 177
116 51
51
15
0.1 2
Heavy•Metals'(parts.perrnillion): '_Aisenic;.::0;3 : _ _:. =:'Cadmium 0.0
- :..
Nickel `0:3'
,
_' :, Chromium;; 0:2-= := `:'
Lead,
1.1
Selenium;-
0:1`

Agronomic Division. . one: 'Web§ltd:_ -W*Mncagr.goWagron omi.
Report No. FYI 5.SL005603"
Page 3 of 4
Sample ID: SS119
Recommendations:
Lime
Nutrients (lb/acre)
More
Prop
-(tons/acre) N P205 K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.0 0
0 IT
0 0
0
0
0
0
Note: 3
2-
Test Results [units - W/V in g1crif; CEC and Na in meqM 00 cd; NO3-N in mgldnf]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac PH
P-1 K-1 Ca% Mg%
S4 Mn-I
Mn All Mn-Al2
Zn4
Zn-Al
Cu-I
Na ESP
SS-1 NO3-N
0.36 1.06 5.7 80 1.1 6.9
167 73 54 20
28 193
126
83
83
27
0.1 2
Heavy,MetaIs'(paks per:mlll. " . ... .: -Arsepie,
-Cadmium.0.
GA
Chromium
Lead
1.2.
Seleniun
03
Sample ID: SS120
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P205 K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.0 0
0 20
0 0
0
0
0
0
Note: 3
2-
Test Results [units - W/V in glcnf; CEC and Na in me-qM
00 cd; NO3-N in mg/drift
Soil Class:
Mineral
HM% WIV CEC BS% Ac PH
P4 K-1 Ca% Mg%
S4 Mn-I
Mn All Mn-Al2 Zn-I
Zn AI
CU4
Na ESP
SS-1 NO3-N
0.41 1.12 9.6 90 0.9 6.2
171 68 63 24
108 443
273
66
66
36
0.2 2
Heavy:Metals'(pa per�'mil Arsenic Jc,.
As
.0.4 Cadmium, 01
1, 6A
Nickel,
�.`throtn 0.'3'
Lead, A.7-
Selenium
0;�
Sample ID:, SS121
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tonslacre) N P205 K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
0.0 0
0 60
0 0
0
0
0
0
Note: 3
2-
Test Results [units - WIV in g1cd; CEC and Na in meq/1 00 crrii,- NO3-N in mg/dro]:
Soil Class:
Mineral
HM%.' WIV. CEC BS% Ac PH
P4 K-1 Ca% Mg%
S-1 Mn4
Mn All Mn-Al2- Zn4
Zn AI
Cu-I
Na ESP
SS-1. NO3-N
0.27 1.19 7.4 91 0.7 6.2
119 42 57 31
121 429
265
51
51
1"
0.4 5
­HeavyMeitails'oa�ts Per.
`2 ad . �� Q.-_._j -
.Cadmium,
- -- N
:Nickel;"
C romium— 0.3-'..
d* -_6
3. Lear