WQ0006245_Residual Annual Report 2014_20150302

GENERAL INFORMATION
ALKALINE STABLIZATION REPORT
CALENDER YEAR 2014
PERMIT NO. WQ0006245
FACILITY NAME:
LOCATION:
MAILING ADDRESS:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
RESIDUALS ORC:
Fourth Creek WWTP NPDES NCO031836
693 Bell Farm Road
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
L.F. "Joe" Hudson Jr., Director
Water Resources
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
Andy Smith
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
Andy Smith
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
APPLICATION: Class A Exceptional Quality Product
Test Data and Summary Operations
Attached

CHAIN OF CUSTODY RECORD
LAD USE ONLY
PRISM
al & Full -Service Analytic
I Environmental Solutions
PAGE OF — QUOTE # TO ENSURE PROPER BILLING:
Sarnples IN FACT upon �.mival'?
NO N/A
—
14-
0
LABOWORIEF, INC
—
Recewnd ON VVET ICE? Temp
444 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224 -0543
Project Name:
Short Hold Analysis: (Yes) (No) LIST Project: (Yes) (No)
Piw)PER. PRSERVATIVES nafcat-n'?
'TIMES?
Phnne:704/529-6364 - Fax:[phone]
111'.
nccp�ved W 4N LOINC
Ro
M
C 1-41 or 04 Its I-,; I e
*Please ATTACH any project specific reporting (OC LEVEL 111111
CUSTODY 1,11A[_G INTACT?
CL
Client Company Name:
Report To/Contact N­ 'A �i 9,, S
provisions and/or OC Requirements
ADSPAC%
VOLATILES iec'd W/OUT HFE­
Reporting Address: 0, jg O)e
Invoice To:
PROPER C,)NTAINr HS usod"?
NC----
Address:
------
Phone: 70Y- V9-343 5' Fax es (No):70-971-945-5
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address—_
Requested Due Date D I Day IJ 2 Days C] 3 Days LI 4 Days C3 6 Days
Certification. NELAC_ USACE—
FL — NC_
EDD Type: PDF_ Excel —Other
1, C w P
"Working Days" 13 6-9 Days LI Standard 10 days ci Rush Work Must Be
Pre -Approved
SC OTHER
N/A
Site Location Name: L_��_d
Samples received after 15:00 will be processed next business day.
: —4 -1 V00 NO
Site Location Physical Address:Z9 3 'be -It FA,-,
_ KA I Turnaround time is based on business days, excluding weekends and holidays. Water orn e : — —
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
s4&Se"lle hic RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) I
TIME MATRIX SAMPLE CONTAINER ANALYSES REQUESTED PRISM
3L�ECTED (SOIL, A.
CLIENT DATE CO I PRESERV REMARKS LAB
SAMPLE DESCRIPTIONCOLLECTED MILITARY WATER OR I -TYPE NO. SIZE / ',� / // // ID NO.
TIVES
HOURS SLUDGE) I SEE BELOW
X Jii6 S P rA -FE
7 [-cc
0
C"
P6
-L3— — -
W
Ph
Sampled �By (Print �Name&
Sampler's Signature �PA �r�lln.�Affiliation
_
Upon relinquishing,this trhalnof ustody Is your authorization for jamto proceed with the analyses as requested, above. Any changes must be
submitted In writing to the Prism Project Manager. There will be ch as for any changes after qnalyses have been initialized.
Receivel (Signature) Date Militai
RellQUAhed By: (Signature) Receive dl,Sy: SIgnatbre) Date
-Pis—mLaboratorles Date
Relinquished By: (Sign re) Received For BY:
t I.L-A n
...... ­ SAMPLES FARE NOT AC PTED AND VERIFIED AGAINST CDC UN"L E(WVED AT THE LABORATORY,
CJFed Ex LJUPS LIF Xl.rn Field Service 0 Other
rNPpES: I UST- I GROUNDWATER: DRINKING WATER: I SOLID WASTE: RCRA: CERCLA LANDFILL IOTHER:
C0 SCLI NO CISC 0 NO Cl SO J NO El SO El NO [J SC LING U SO-,' 1:1 NO 0 SO El NO Q SO I a NO El SO
6 Li C]
'-tONTAINER TYPE CODES: A=Amber C=Clear G=Glass P=Plastic; TL=Teflon-Lined Cap VOA =Vc latile Organics Analysis (Zero Head Space)
Comments:
COR I C� 1 N 4

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISP®SAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0006245 FACILITY NAME:
Fourth Creek Alkaline Stabilization
PHONE: [phone] COUNTY: Iredell OPERATOR: Ray Wyrick
FACILITY TYPE (please check one): ® Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
El Distribution and Marketing (complete Parts A, B, and C)
Wn.s the facility in operation during the oast calendar vear? Yes R1 No ® --P If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (drytons)
� Reci rent Information
Amendment/ Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
4th Creek WWTP
4
60
64
Various Farmers
65
Farmland
February
NPDES# NCO031836
5
90
95
Various Farmers
227
Personal & Farm
March
4th Creek WWTP
11
101
112
Various Farmers
153
Farmland
April
NPDES# NCO031836
16
140
156
Various Farmers
406
Farmland
May
4th Creek WWTP
20
175
195
Various Farmers
67
Turf
June
NPDES# NCO031836
0
0
0
Various Farmers
119
Farm/Garden
July
4th Creek WWTP
4
65
69
Various Farmers
113
Farmland
August
NPDES# NCO031836
4
70
74
Various Farmers
0
Farmland
September
4th Creek WWTP
8
90
98
Various Farmers
124
Landscaping
October
NPDES# NCO031836
23
350
373
Various Farmers
92
Farmland
November
4th Creek WWTP
3
65
68
Various Farmers
211
Farmland
December
NPDES# NCO031836
10
120
130
Various Farmers
79
Fam-land
Total from FORM DMSDF (sup)
.r."® h�:
0,-
Totals:
Annual (dr tons):
9 , „a, ,}1�(�8,
,,,7326,t`;;�
1434',-
ti.�
Amendment(s) used: I I
Bulkin A ent(s) used: Lime Kiln Dust
* If more space is required, attach additional information sheets, (FORM DMSDF (supp)):
Part C:
Total Number of Form DMSDF (Supp)
Facility was compliant during the past calendar year with all conditions of the land application permit p Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ® No it If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and impriAmOt for knowing v31lations."
2�
Signature of Permittee Date Signature f Preparer** Date
(if differ nt from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: W00006245
Facility Name: Fourth Creek WWTP
Residual Source WQ # or NPDES # NCO031836
NPDES #:
W WTP Name:
Residual Analvsis Data
Laboratory: 1)
2)
3)
4)
5)
Prism Labs
Parameter
(mg/kg)m
Conc.
Limit
a
Sam le or Composite Date
1/13/14
5/5/14
7/14/14
12/15/14
Percent Solids (%)
NA
70.80%
83%
56%
67%
Arsenic
75
5.2
5
6.5
<0.053
Cadmium
85
<0.0033
<0.0029
<0.042
0.57
Copper
4,300
29
23
310
26
Chromium
NA
N/A
N/A
N/A
N/A
Lead
840
8.2
6.2
100
12
Mercury
57
0.17
0.24
0.38
0.18
Molybdenum
75
N/A
N/A
N/A
N/A
Nickel
420
110
89
3
10
Selenium
100
<0.084
2.1
<1.1
<0.090
Zinc
7,500
57
41
66
45
Total Phosphorus
NA
2,000
2,200
3,100
2,100
TKN
NA
3,300
2,200
.5,200
3,600
Ammonia -Nitrogen
NA
47
14
150
92
Nitrate and Nitrite
NA
8.3
34
54
11
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure hat qualified p sonnel properly gathered and evaluated the information submitted. I am aware that there are significant
Pe ti r su tt' alse information, including the possibility of fines and imprisonment for knowing violations."
02- ,12— S_
ignature f Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Fourth Creek WWTP Alkaline Stabilization
WWTP Name: Fourth Creek WWTP
Monitoring Period: - From 1/1/2014 To
WQ Permit Number: WQ0006245
NPDES Number: NCO031836
12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)
Alt. C (Prior Testing) ❑
' or Test)
t. o Prior
D
u en s
Process t Further Reduce atho
o P g g
If applicable to alternative performed (Class A.only)
indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment. ❑
Thermophilic ❑
Bet
Beta Ray
Gamma Ra
Pasteurization
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic obic Digestion L]
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
dences
Frequency
of Analysis
Sample
Type
Anatytic al
Tech -
ni ue
Minimum
Geo. Mean
Maximud
IExcee-
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
<0.2
<1
mpn/g
60 days
grab
sm9221e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
<0.076
mpn/4g
Vector Attraction Reduction (15A NCAC
02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ®
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench) ❑
1 Alt. 4 (Spec. 02 uptake) R
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization ®
Alt 7 (Drying - Stable)
1Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) [3
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives'were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met."" (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
tthe pathogen and vector attraction reduction requirements have been met. I am aware that there are
ant penalties for false certification including fine and imprisonment."
Ytm,(� OYreQi( i5c�
and Tits ( e or print) Land Applier Name and Title (if applicable)(type or print)
iignature(of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # 6
Setup Date: 1-2 7-1 y
Removal From Bin Date: 1-30-1q
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
1- 2 7--1 q
A
11 59 M
Initial PH: 12, 5 3
90
Corrected PH: % j, 3
:1- 3044
A
ID"'
Final PH: /2. 6 3
9 O 0
Rif w.
Corrected PH: 1a,83
Has 72 Hour & PH Criteria Been Met? Y N
BIN # I
Setup Date:
Removal From Bin Date: 3- 3-lq
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C.For 12 Hrs.
Operator
I1�►�
Initial PH: Id, 4f
a
90
R�tcU
Corrected PH: Ia. Y 7
-/I
Final PH: j j, 7 7
�
R
Corrected PH: ia, 9 '7
Has, 72 Hour & PH Criteria Been Met? Y ".N
BIN # 3
Setup Date: 3-ao-1 q
Removal From Bin Date: 3-a4-/y
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3,20-1q
11 AM
Initial PH: Ia..5,2
00
RAW
Corrected PH: 13, 0 1
3-dk l�l
1 P"l
Final PH: 1. ,91
9 d O
Corrected PH: 13,1
Has 72 Hour & PH Criteria Been Met:? Y N 3 aY-►t/
BIN # q
Setup Date: 3 d,a o - / y ,
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP_. >52 Deg. C For\12 Hrs.
Operator
Initial PH: 1 a, 94
q 0 ©
R� W
Corrected PH: 13.
3-.1y-►�/
/ P"
Final PH: /,2. 9 ff
0
2 W
Corrected PH: /3.1
Has 72 Hour & PH Criteria Been Met? N
BIN # 5
Setup Date:
Removal From Bin Date: 3 -a 9-/
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3 .2
1: 35P,,)
*A-98
Initial PH: .1 ` , r7 rl
a
9 0
Corrected PH: /.7.17
3 J 5-14
.1 Pen
Final PH: 11. 9'7
9 0©
R �`
Corrected PH: 13,1
Has 72 Hour & PH Criteria Been Met? Y N

City Of Statesville Alkaline Stabilization Record -For
Proce;5s To Further Reduce Pathogens (PFRP)
BIN # '7
Setup Date: 3-a5- ly
Removal From Bin Date:3--a y-/5/
Date
Time
PH >12.0' For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
P"'
Initial PH:
Corrected PH:
3-etc-/y
a. 30
Final PH: Ia. 7 q
10
R� w
Corrected PH: /a .4
Has 72 Hour & PH Criteria Been Met? Y N
BIN # 3
Setup Date: `/- 7-1 y
Removal From Bin Date: L/- 10'14
Date
Time
PH >12.0 For'72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
-� Iq
0 9- "/ T
Initial PH: I a. ` ,/
q O®
R L W
Corrected PH: I?. I-s
�]" ly ►y©;
f
Final PH: /�, $�
®
0
RK V �
Corrected PH: 13,1
Has 72 Hour & PH Criteria Been Met? Y . N
BIN #.
Setup Date: y- Iy-ILj
Removal From Bin Date: - 17- 1�
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
�(-IH-1°/
//:30�
Initial PH: /�, (a-
o
go"
Corrected PH: /a, 8 0�
q} ,
Final PH: i a. y
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN # :3
Setup Date: y_d . /q
Removal From Bin Date:. 4--117-1
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 1,2. "1
90 a
Uq
Corrected PH: 1 �2 • i
Y-3o-/y
J: 3o P n
Final PH: /.,7.
6 6
R� w
Corrected PH: /,I, 9 9
Has 72 Hour & PH Criteria Been Met? UY N
BIN # 1
Setup Date: '/-I $-)4
Removal From Bin Date: 6- /- Iq
Date
Time
'PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
!y
/• 3o P„�
Initial PH: Ja, 83
q 0 0
R4 W
Corrected KPH: 13, 0
-!�i
l �sPM
Final PH: /.4. 9a
o -
Corrected PH: 13. I
Has 72 Hour & PH Criteria Been Met? Y N

City Of Statesville Alkaline Stabilization .Record For
Process To Further Reduce Pathogens (PFRP)
-BIN # Ll
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
y-a9- l y
��' 3oM
Initial PH: /a, 33
9 a c
'�� Vv
Corrected PH: /a • 53
Final PH: /,g,y3
0
0
R� W
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN # 5
Setup Date: H- 30-.1 y
Removal From Bin Date: 3- 3-/ y
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 1 d, ti 3
00
A InW
Corrected PH: /a.93
A
Final PH: /,�. 5 3
900
R� �
Corrected PH: l a .7 3
Has 72 Hour & PH Criteria Been Met? QY)'-N
BIN #
Setup Date: 5- /a- Ili
Removal From Bin Date: 5-
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 1,2.5 $
9 (7o
RAC Lov
Corrected PH: Q. 7 t
5-15 1 �1
p
Final PH: /a. ( r
O o.
Rl
Corrected PH: 14 , $ $
Has 72 Hour & PH Criteria Been Met? Y N
BIN # 3
Setup Date: 5-13- I q
Removal From Bin Date: --1 y
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
5 13-1 `l
J �m
Initial PH: Ja 68,
q o o
R� W
Corrected PH: I.J. S$
s Id-ly
a: �5P"^
Final PH: /a. 7
Corrected PH: 1j,9 f'
Has 72 Hour & PH Criteria Been Met? Y N
BIN #- Y
Setup Date: 5-/y-ILI
Removal From Bin Date: 5- j9-1q
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
5- /jj-I y
11 A rn
Initial PR:. U.79
900.
R4VV
Corrected PH: l a .9s
s-l9-JY
9 A^'►
Final PH: j.�,$�
9 o
Rl v✓
Corrected PH: 13.0
Has 72 Hour & PH Criteria Been Met? UY N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
-BIN # S
Setup Date: 3- /S- /ii
Removal From Bin Date: S
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
�YsM
Initial PH: /�, $ 8
Corrected PH: / 3. Q
Final PH: /a, 9 J(
O
R W
Corrected PH: 13, 1
Has 72 Hour & PH Criteria Been Met? (Y) N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has .72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y' N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N.

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # 3
Setup Date: /6- /y
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
4-&-/41
/a' ®d
Initial PH: /a, 7f
00
RAW
Corrected PH: 1,237
'20
A.�
Final PH: 1,2. $r/
100
7
��W
Corrected PH:. 13, 1
Has 72 Hour & PH Criteria Been Met? Y N
BIN # S/
Setup Date: 6- /7-/,4/
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
�- rQ- /�
°� P'�
Initial PH: /a . % 0
p
9
Corrected PH: /a, 91
Final PH: /,,J..10
170
o
%�� W
Corrected PH: J.?, 9 9
Has 72 Hour ,& PH Criteria Been Met? UY N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
-Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg..0 For 12 Hrs.
Operator
Initial PH:.
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
.BIN # J-
Setup Date: 7-/y-1q
Removal From Bin Date: 7- 17-1q
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
I- is- lei.
II A InCorrected
Initial PH: /a,Y$
0
90
PH: Iq7, q
913© m
Final PH: /a,S9
o
o
R��J
Corrected PH: /�, q 9
Has' 72 Hour & PH Criteria Been Met? Y N
BIN # .
Setup Date: g- I�-14.,
Removal From Bin Date: 8-1q- I q
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
8' 11 ' l y
i
Initial PH: /d, 59
n 900
7
Rk W
Corrected PH: Id. 77
_a /y
11. 3o Pin
Final PH: Ia.le
0
��
Corrected PH: /?, P?
Has 72 Hour & PH Criteria Been Met? CY) N
BIN # 7
Setup Date: S- id-1 y
Removal From Bin Date: 8-15- I y
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg.-C For 12 Hrs.
Operator
g_.a_ Iy
Ia:59PM
Initial PH: /a,.19
900
94� t9
Corrected PH: Id, M
8-a5- !y
1: 3 o P*Y3
Final PH: 41st 1.2,71
900
RA vv
Corrected PH: /.239
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: t-A5-- IS/
Removal From Bin Date: S-a
$-14/
_ Date
Time
PH >12.0 For 72 Hrs.
.
TEMP. >52 Deg. C For 12 Hrs.
Operator
8-A6-Iq
/J32I"
Initial PH: /al. $;
Q� �
RAov
Corrected PH: /a,79
a_
�- y /q
� fn
P
Final PH: 12. 19
9
R'� VV
Corrected PH: 11.8 9
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
0

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
-BIN # 3
Setup Date: 4-10-Ise
Removal From Bin Date: 7-Is.iy
Date
Time
PH >12.0 For 72 Hrs.
TEMP._>52 Deg. C For 12 Hrs.
Operator
a'''I
Initial PH: /a 53
900
��
Corrected PH:/a,73
i -10 - J5
Id;15,�
Final PH: 1,243
1700
Rh o
Corrected PH:1.7. &'3
Has 72 Hour & PH Criteria Been Met? Y N
BIN # y*L13,!
Setup. Date: 9-11- ILI,
Removal From Bin Date: 9 -/ 5-!Z/
Date
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
►/_ /y
Initial PH:1a, , .3
9
w
Corrected PH: /,7.7 q
Final PH: /.�. 7/
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: 9-15-1 y
Removal From Bin Date: 9- J j- A/
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: la 7-6
90 ®
R� w
Corrected PH:/.?, R5
?^ / -1
I� y5 Pry
Final PH: /a -&5
�©O R4
Corrected PH: / 3, 0 1
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: 9-
Removal From Bin Date: =aa-/y
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
®
Initial PH: /a, 57
90
Rd tv
Corrected PH: 1,2,77
11'ySNI
Final PH: /,7, d %
9
9 6
Corrected PH: la��'7
Has.72 Hour & PH Criteria Been Met? UY N
BIN # 1
Setup Date: Q- 30- J t/
Removal From Bin Date: 10-3-11/
Date
Time
. PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
9 30-JSI
4 Arrl
Initial PH: U 7
90
R? LV
Corrected PH: 13.92
/0%30I"
Final PH: 124
9 o fl
R� IN
Corrected PH: 13, 2
Has 72 Hour & PH Criteria Been Met? UY N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # 3
Setup Date: /0-6- lq
Removal From Bin Date: 10- 9-
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
10-1-/4/.
1: 30M
Initial PH: Id. $,2.
900
RX W
Corrected PH: 1 .9 �
-a P.71
Final PH: 11.90
goo
Corrected PH: /3.1
Has 72 Hour & PH Criteria Been Met? Y N
BIN # q
Setup Date: /6-1 3_ /y
Removal From Bin Date: /0- / `j-1q
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
l o -13-1 y
132 Pro
Initial PH: /Q. 59
-®
Q
R4W
Corrected, PH: /, . 79
Final PH:
`
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
'Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date.
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N

...
•
Sam le Receipt Summary
p❑
®1� '
I,S
/A1
Y
Full-S"e'rv(ce Analytical'& '
I.tEnvironmentai Solutions ::
is 01/20/2014
ueonionies wn .
.
PeWn Work:OMer: 4010154
Client Sample ID
Lab Sample ID Matrix' :::,Date
Sampled
Date Received
Sta=Lime'
-4010154-01 . :. Solid
01113/14
01/13/14.
..
• � (Fecal #2):
4010154-02• Solid
01)•13/14Sta-Lime
01/13/14; '
Sta-Lime (Fecal #3)
...'01/13/14::,
::. 4010154-03 " Solid ;;::.
:01/13/14
S:ta-Lime (Fecal #4)
:': 4010154;04 Solid
01/13/14
01113/14
Sta-Lime (Fecal #5)
: 4010154-'05 : Solid :::' : :::
01113/14:::
:01-/13/14
Sta-Lime.(Fecal#6),
4010154-06''. ,, Solid
01/1.3114
01/13/14
Sta;Orne.(Fecal M..
:4410154-07.:::.. Solid :':..
01/13/14
01/13/....
...
Samples were received at 9.2 degrees•C. See'case narrative for further. information,
...
:.
... ...
This report should'not be re .Yodaced, exceP.nits entiren.:w.dhout the writtenconsent of PrisLaboratories. Inc.
h
• •
449 Springbrook,Road - P.O.: Box 240543 -:Charlotte, NC 28224-0543
Ph'one:.704/529.6364;7 Toll Free Number: 1-800/529-6364 - Fax. [phone].
; . Page 2,

:....
:....
ora cry' Report
n�
Full -Service Analytical*&a
S M ;
I
; EnvironmentaLSolutione
::.'
01/20/2014
City of Statesville, NC :::
Project: StaUrno: (Qtrly, BiWeekly,
Client:Sarrlple ID::::
Sta-Lime:::'
.
::.. ::.
Attn::
...
60Da 7 Fecal ;;:.
Y:.::.
;Prism Sample.ID: 40101: 4-01
P.O. Box:1111
Prism Work Order:
4010154.
Statesville, NC 28687
'Sample
Matrix: Solid:
Time Collected:'01/13/14
10:23
... ...
"
...
...
...
...
Time Submitted: 01/13/1.411:35
Parameter
Result Units:
Report:
MDL -'
Dilution :'Method
Analysis Analyst
'Datelrime
;Batch
Limit
::
'Factor . ....
: ..::
.. ;ID
:. General Chemistry.Parameters �. .
_ • Plant Available Nitrogen:. •
.. ..
720
mglkg
160
13
2. *Calculation
1/20/14: ,9:52
CLB ,
, [CALC]
% Solids::
70.6
% by
0.100 ::
0.100
1: *SM2540 G
1/15114:16:02
JAB :
P4A0199..: "
:. ...
Weight
."
.. ..
.... .
NitrateNitrite as N
8.3
.. mg/kg dry
7.1
0.78.
1 "SM4500-NO3 F .1116/14 12:52.
CLB
P4A0208
Phosphorus -Total
, • ; , • 2000
mglkg dry
'71 :
10
20 ", *SM4500-P F
1117/14 10:08 :.
JAB
P4A0162
Total Kjeldahl Nitrogen
3300
m0lkg dry
710:
59 .::
2 *351.2
.:1I20/14 9:52 ::
' CLB
p4A0259
Amriionia as N; i • :.
:' 47
:::' : !49.9
5:0
0.48
1 *SM4500-NH3;G 1/14/14 10:37•
:CLB
.
A4A0140
Microbiological Parameters
Fecal Coliforms
BRL:
.MPN/g dry:
0.3
1' • *SM9221. E
1/13/14 13:08
MES
.: 134A0156
Total:Metals :::.:..
:....
.
Mercury
: 0.17
:: mg/kg dry
0.028
0.0094
1 *7471B
1/17114 16:19'
MEH
P4A0221
Arsenic
5.2
mglkgdry
0:35:':
0.051 :':
1 *6010C
1115/14 0:34 ".BGM
P4A0151
Cadmium
BRL
" mg/kg dry
0:35
0.0033'
1 " *6010C :
" 1/15/14 0:34-
BGM
P.4AO151
Copper
29
m0lkg dry
6:60
0.0087
1 *6010C
1/15114 0:34
BGM
P4A0151
Lead ."'; "':
:"'; _ "8.2
:"'; mglkgdr
. 0.35 ""0.041
"1' *6010C
1/15/14' 0:34
BGM'
P4A0151,
Nickel
11'0:
.:'inglkg dry .,
i 1.4
, 0.011
1.' i *66106:
IIIISA4:'0:34
BGM:':
P4A0151 ..
Potassium "'
"" "' :4700'
, :mglkg dry„
::' 350... :.:
'22
... 20 ' *6010C'
1117114 17:36
BGM
P4A0151:
:Selenium
BRL
:: mg/kg dry
00
0.084'
1 *6010C ::.
1/15/14 0:3.4'
BGM
P4A0151
Sodium
590
rnglkg dry
17 : •'
0'.16 :
1 ,*6010C
1/15/14 0:34
'BGM
P4A0151
Zinc "
57
mglkg dry
• 3.5
0.024,
1 : ' *6010C :
q.
" 1115/14 0:34
BGM
F.
P4A0151
:. ...
:This report should not be re' Yoduced, exce :f iri its entire ",'wlthbut the writt'en:consent of Prism Laborafories,'Inc.
P P tY.....
449 Springbrook,Road - P.O.; Box 240543 -'Charlotte, NC 28224-0543
Phone:,704/529-6364:7 Toll Free Number: 1-8001529.-6364 - Fax: [phone]. :
Page 3 of 14
,

IS
Fuii-Service Analytical'&'""" """• ..:.:
I Solutions
Report
01/20/2014
•Environmental : ; . ::
; ;
;City of Statesville, NC ..:.::
Project: Sta�ime (Qtrly, Biweekly,
Client.Sample 10::.Sta-Lime;(Fecal#2)
Attn:;AndySmith;;::.
60Da 7 Fecal
::.. Y:;:'•. )
Prism Sample ID: 4010154-02
P.O'.' Box• 1111
Prism Work Order: 4010154
Statesville, NC 28687
Sample .Matrix: Solid::
Time Collected: 01/13/14.10:23
Time Submitted' 01/13/14.:11:35
Parameter
Dilution' Method ' Analysis Analyst Batch
Result Units. Report, MDL
.. ..
..:: .Limit ..::':Factor
. .... Date/Time ..::. ..:ID'
'General Chemistry, Parameters
' /° Solids-
% by 0.100 0.100
1. SM2540 G 1115114.16:02 JAB . P4A0199 ,
: Weight
:... • Microbiological Parameters..::::.
::...
.Fecal Coliforms .
BRL MPN/g dry 0.3
1 .. .*SM9221 E.. .1/13/14 13:08 MES P4A0156
• ;
Ttiis report should'not be reprod Used, excerpt iri its entirety,:withbut the writfen:bonsent of Prism Laboratories,'Inc.
449 Springbrbok.Road - P.0.;box 240543 -.Charlotte, NC ..... 0543
Phone:.[phone];- Toll Free Numbee 1-8001529-6364 - Fak: 7041525-0409, ; , PBge 4 Of 1 4 �'•

:.
:.
Laboratory: Report :
R I S M
. LA90MTORIEQ ING
Full-SONIceAnalytical&
I , Envlronmental,Solutlons ; • ; ; ; .
:.... ..... ..... ..... ..... .....
01/20/2014
..... ... ..
City of Statesville, NC
..: • . Project: StaLime (Qtrly, Biweekly,
...
Client.Sample ID:: . Sta-Lime; (Fecal #3)
Attn:: Andy Smith-: ::.
60Da 7 Fecal)
Prism Sample 1D: 4010154-03
P.O. Box 1111
Prism Work Order: 4010.154-
Statesville, NC 28687
Sample Matrix: Solid::
Time Collected: 01/13/14.10:23
:....
:....
Time Submitted' 01/13/14.:11:35
:Parameter
Dilution Method Analysis' .Analyst Batch
Result Units, Report MDL i
.;
Limit
Factor . . , : Date/Time . ID'
General Chemistry Parameters
% Solids
68.0 % by . 0.100 0.100
1: *SM2540 G IMSM4.16:02 JAl3 . P4A0199
Weight
Microbiological Parameters
Fecal Coliforms
w.
BRL .. 'MPN/g dry.. 0.3
1 .*SM9221 E.. . 1/13%14 13:08 MES P.4A0156'
'
w.
:::This report th6uld'not be reproduced, except; in its entirety,:W.ithout the written'donsent 8f Prism Laboratories,'Inc.
•a
449 Springbrbok.Road - P.O.: Box 240543-'Charlotte, NC 28224-0 3 � •
Phone:,704/529-6364;7Toll Free Number: 1-800/529-6364 - Fax: [phone]. Page 5 of 4 .

Report
'
..... ® e►
®P RE
lA6ORATORIE$INF :..
Full-SeNl'co Analyticar. &• . • • ... . • . • . ...
Environmental, Solutions
..... ..... ..... ..... .....
... ... ... ...
01/20/2014
..... ..... ... ...
'
City of Statesville, NC
Project: StaLime (Qtrly, 81wi ekly, .::
Clieht Sample ID:, . Sta-Lime,(Fecal #4)
;.•. Attn:;AndySmith;;:;.
60Da 7 Fecal
� Y:::.. )
;Prism Sample ID: 4010154-04
P.O'. Box' 1111
Prism Work Order: 4010.154
Statesville, NC 28687
Sample .Matrix: Solid::':
Time Collected: 01/13/14..10:23
Times brriitted`. 01/13/1.4.;11:35
Parameter
Dilution' -Method Analysis Analyst Batch
Result Units. Report. MDL
Limit
Factor Datelrime ID
neral Chemistry
Ge m
% Solids
89.3. % by .' . 0.100 . 0.100
1. *SM2540 G 1/15/14.16:02 JAB . P4A0199
Weight
Microbiological Parameters
.Fecal Coliforms
BRL .. MPN/g dry 0.3
1 *SM9221 E.. .1/18h14 13:08 MES NA0156
:TFiis report should'not be reproduced, except. Wits entire Without the writterh:consent of Prisrh Laboratories,'Inc. "
: 449 Springbrook•Road - P.O.: Box 240543 -:Charlotte, NC 28224-0543
Ph6ne:,704/529-6364:7 Toll Free Number: 1-800M2y-6364 - Faz; 7041525-0409. Page 6 of 1

C
•
Full-SdrAice AnalyticaC &'
•Environmental Solutions ; ; , • ; , ; ; , ; ,
Laborato p Re orf
01/20/2014
�CA60apTOFIE$ ING :.
• .. ..... .. ..
• .
City of Statesville, NC ..:.:
Project: StaLime (Qtrly, 8i... kly, .:;.:
Clierit,Sample ID: • Sta-Lime; (Fe;ca1 #5)
Attn: Andy Smith; ; ,
::. ' 60Day 7 Fecal) ::::
Prism Sample I D: 40101:54-05
P.O. Box 1111
Prism Work Order: 4010154
Statesville, NC 28687
Sample Matrix: Solid::':
::...
Time Collected: 01/13/14.10:23
• .......
.
.Tline Submitted' 01/1371.4.:11:35
Parameter
::
Dilution' Method Analysis Analyst Batch
Result Units. Report, MDL
..
Limit •
Factor . ..... : Date/Time .... ID'
General Chemistry,Parameters
w.
Solids
' 69.2 . % by .' 0.100 . 0.100
7. *SM2640 G 111S/14.16:02 JAB . P4A0199
Weight
Microbiological Parameters
Fecal Coliforms
'BRL .. 'MPN/g dry 0.3
1 *SM9221 E.. . 1/13%14 13:08 MES 'P.4A0156
V.
report should not be re' rodilced, except in its entire without the wtitten consent of Prism Laboratories, Inc.
• •
; :449 Springbrook•Road - P.O.: Box 240543-Charlotte, NC 28224-0543
Phone:.[phone]:7 Toll Free Number: 1-600M29-6364 - Fax: [phone]• Page 7 Of 4

... .... ..:.... :
Report
Laborat O
9! w
.:
Full -Service Analytidal
EnvlronmentaLSotutlons ; ; , ; ; ,
.':
; ; , 01/20/2014
-LABOaATON1E$ING :•.
•. ..... •....
•. •. •.•
City of Statesville, NC ..:.
Project: StaL.ime'(Qtrly, Biweekly, ' ..:;
Clierit'Sample 1D:::.8ta-Lime,(Fecal #6)
Attn: Andy Smith: •
60Day 7 Fecal) ;;:
:Prism Sam le 1D: 40101:54-06
P.O. Box 1111
Prism Work Order: 4010.154
Statesville, NC 28687
Sample .Matrix: Solid::'
Time Collected: 01/13/14.10:23
:...
..:.:
/1 ..
Tiliie Submitted: 01 3/14.:11:35 : '
: Parameter
Dilution Method Analysis Analyst Batch
Result Units. Report . MDL
;'.:
..
Limit
Factor , . ; Date/Time ; , ; , ID'
'General Chemistry Parameters
:.... % solids :...:
.: i6.i . % by.' 0.100 .' . 0.100
1. •SM2540 G 1/15/14 16:02 JAB P4A0199
Weight
Microbiological Parameters
"
.Fecal Coliforms
"BRL .. MPN/g dry" 0.3
1 •'SM9221 E. 1/13/14 13:08 MES NA0156
h.
a.
.. .
:This report shduld'not be re' rodiaced, exce :. ih its entire ",'without the written consent of Prism Laboratories,Inc.
;449 Springbrook,Road - P.O.: Box 240543 -;Charlotte, NC 28224-0543 '
Phone:.[phone]:- Toll Free Number: 1-800I529 6364 -
Faz: 7041525-0409, :. Page8 Of 14

..
:.... ...
Level Report
.......
Full -Service Analytical$
j F
l
1/20/14
r- Environmental;Solutlons
/PISM
R
:�LAEONATOPIES ING
':City'of Statesville, NC :.
Project: StaLime,(Qtrly, Biweekly, 60Daq. ' Prism Work Order: 4010154 .
Attn: Andy Smith • •
7 Fecal) Time Submitted: 1/13/2014 11:35:OOAM
P.O. Box 1111
Statesville, NC 28687:
General Chemistry'Parameters = Quality Control'
Reporting : Spike Source %REC RPD
An'alyte
Result:' Limit': Units Level Result %REC Limits ' : 'RPD Limit Notes
Batch:MA0140 -.NO PREP
Blank (P4A0140-BLK1);
Prepared & Analyzed,: 01/14/14
Ammonia as N
BRL 5.0 mg/kg
LCS P4A0140-BSI'):
Prepared & Analyzed: 01/14/14
Ammonia as N "
123 5:0 mg/kg 125.0 "' 98 80-120
Batch P4AO162'- SM4500-P65
Blank (M0162-BLK1)
Prepared: 01/14/14 Analyzed: 01/17/14
Phosphorus -Total
BRL 2.5 mg/kg wet
LCS (P4AO162-BS1) ..
Prepared: 01/14/14, Analyzed: 01/1:7/14
Phosphorus -Total
101 2.5 mg/kg wet 100.0: 101 90-110
Batch MA0199 - NO PREP
Blank (P4A0199-BLK1)
Prepared & Analyzed: 01/15/14
% Solids .: - ..
100 0.100, % by Weight, ....
Batch:134A0208 -:NO PREP
Blank (P4A0208-BLK1)' .
Prepared & Analyzed: 01/16/14
Nitrate/Nitrite as N .:.
BRL 5.0 mg/kg wet ;
�
.LCS P4A6208-BS1)
(
pared & Anal zed: 01/16/14
Pre y
Nitrate/Nitrite as'N:
48.8 . 5.0 mg/kg wet . .50.00 . 98 80-120
•
p.o P.:.:..t..
This report should'not be reproduced, exce t m its entirety,:without the written:oonsent of ,Prism Laboratories,'Inc.
• 449 Springbrook,Road - P.O;.; Box 240543-:Charlotte, NC 28224-0543
Phone:,704/529-6364;- Toll Free'Number:1-800/529.6364- Fax: [phone]: :. Page 11 Of �4

' •
::... II'QC Report
:.:.:: vel
�� r
Illy
I, S
M
Full ervlce AnaliciiI 4
• •
f
lAe6AMRIEr, ING .
; Envlronmental;Solutlons
• ' • ' • • " • • .. ... • . • • . • . • • .. • .
:C4 of Statesville, NC :::,:
' :;. Project: StaLime,(Qtrly, Biweekly, 60Dey,: Prism:work Order: 4010154;.;
Attn: Andy Smith::,
; ; . • 7 Fecal) ; ; , ; Time Submitted: 1/13/2014 11:35:OOAM
P.O. •Box 1111
Statesville, NC 28687:
'
General Chemistry: Parameters - Quality Control
Reporting': Spike Source %REC RPD
Analyte
Result Limit Units Level Result %REC' Limits .:: RPD Limit Notes
:. Batch7P4A0259-:351.2
"
Blank(P4A0259-BLK1):;
Prepared:01/•17/14 Analyzed:01/20/14
Total Kjeldahl Nitrogen:
"' BRL "' 25 mg''/kg wet
.
,LCS(P4A0259-BSI)
.....
"' ,.. ., ,Prepared: 01/17/1'4 Analy7ed:01/20/14
Total Kjeldahl NiNogen
.512' :100 mg/kg wet" 500.0 "" 10290-110'' "
..
... ..
This report sh6uld'not be reproduced, except; in its entirety, without the written consent of Prism Laboratories,' Inc.
... ...
449 Springbrook.Road - P.O.;Bbx 240543 -;Charlotte, NC 28224-0543
Phone:.[phone]. -Toll Free *Number: 1-800/529-6364 - Fax: [phone], Page 12 Of �4';,•

s. �.
'Level II'QC Repoirt .
®1A ®®'� yticer8.
La /20/14
n EnivlonmientalnSi
•�®IABOPATORIE61NG ' , 1
City of Statesville, NC ; ;;.: ' Project: StaLimo.(Qtrly, BiWeekly, 60Day. : Prism Work Order:::4010154,
Attn: Andy Smith ;;, 7 Fecal)::. Time Submitted: 1/13/2014 11:35:OOAM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control':
Reporting' . Spike Source %REC RPD
..
An�lv♦c P.-It,: .I imit I Ini}s. I evel ..R'asult 0A RFr. I imitc . RPn ..'I-imit . Nntes
Batch:P4AO156 -:NO PREP
Blank (P4AO156-BLK1):
Prepared & Analyzed; 01/13/14
FecalColiforms ",
"'
"„BRL "" 0.2 MPN/gwet
...
Sample Extraction Data
,Prep Method: 351:2
s.
Lab Number
Batch : :..
Initial ::.. Final ::.. DatelTime .
4010154-01 .
P4A0259 '.:
0.05 g 25: mL 01/17/14 12:45:
4.
Prep Method: SM4500-PBS
Lab Number
Batch
. ... ...
Initial Final. Da irrime
4010154-01 :.
P4A0162
1 :g.: 50 mL:. 01/14/14 15:45 ..
Prep Method: 3050B
Lab Number
Batch
Initial Final Datelrime
4010154-01.
P4A0151
.2.04 g 50. mL 01/14/14 .11:1.5.
4010154-01
P4A0151
2.04 g 50 mL 01/14/14 11:15
Prep.Method:7471B
.,Lab -Number
Batch
Initial Final Dater.rime
4010154-01
P4A0221
0.61 g 50 mL 01/16/14 14:00
.. ..
" "
This report should'not
P
be reP::' roduced, except t in its entire without the written consent of Prism Labor3tbrieb jnc.
.. .. tY :.
::449 Springbrook.Road - P.O.: Box 240543 -'Charlotte, NC 28224-0543
Phone:•704/529-6364;- Toll Free Number: 1-806/529.-6364 - Fax: [phone]. Page 13 Of '14

— —
OF ODY
��� • ���®IS.
M�:
=FuI1�Service Analytica:&
:-:
E tISlY...
T ..
nvlronmon a Solutions
taAGE_oF= tSasoTerx4oENst91aEPRowEfgeuF:aoiiao:
'�,;tSamples;.,N;-..,�;,,upon:arriVa,;;:;: W..,.....:�•-:,:s :�•.;::_,_.
vaaoaaToiiiea izJc.
•
449 S r4n brook Road:- P:O. Box 240543 - Charlotte, NC28224-0543
Project:Narrie:
PR�P,ER;PRES)=RVATI..VESdrtdicatsd:,, `:`-.;:'� ':�
Phone:-704/529-6364 Fax: 704/525=0409 = _
Short Hold Analysis,.: -(Yes) (No) UST:Profect: (Yes) (No):
• ,;-:,..--. ° - ..
.,,.:.R„ecelvedtWI7HCNH04diN�aTt�C}5;,;,,.;
'
ClienYCompanyName: �• y'..
*Please ATTACH an project specific re ortin = QC LE!/EL 1 11 1111:.:•,
.G'USTQpF('SEALSIIVTAGT?;�>'''%t';1:•'.":'�:.',,.'_,:�_rr :;�,•'
� ,.
Report To/Contact Name:.:'A n o� v a rve • +.�►
prowslorsand/orC�CRe ulrements
•::. q
-1•,0:-
•.::::.:....::.a:_:;..:.;�-.:;._....=,;..;<;,;.:•.., ....,:.;..,:;.::;:c;,::::.::;.::...-•:•.: -
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p�NTAIIVERS;usgd2,:`;;;:;._;•.`:r`,•::
..:g•,' ♦♦yy
Address: -
-
Phonec7t7" $'78-`3g3`7 Fax . es (No):70'1-97T-'$d4r5.
....
TO SE FILLED IN �Y CLIENT/SAMPLING PERSONNEL
Purchase Order No./Billing Reference
Email (Yes) (No) Email Address ---
:...
- -
Requested Cl1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
q
Certification:. NELAC 11SACE FC NC
E®® Type: PDF_ Excel -Other
Site Location Name: ro. r4A C_--r- r k tow f P "'
Work Must Be
"Working Days" Q679 Days El Standard 10 days ❑ Pre -Approved
- . SC_ --OTHER, / NA
Site Location Physical Address:: 03 8 01 Fa � m 81.:::
Samples received after-i5 00 wilGbe processed next business dayProve
Turnaround time is based on business days, excludingweekends and holidays.
Water Chlorinated: YES_ NO
_
"
(SEE REVERSE FOR TERMS & CONDITIONS 13EGARDING SERVICES.-
RENDERED BY PRISM LABORATORIES, INC. To CLIENT) ::. - - - --
Sample Iced IIeCtIOn: YES ".. .NO:.
Upon -
TIME - -'
MATRIX
SAMPLE CONTAINER
- '
TES '
ANALYSES REQUESTED
YS S��R ES . .A AL
PRISM
CLIENT
DATE:
COLLECTED
MILITARY
(SOIL, -
WATER OR
= = -
*TYPE
PRESERVA-: -
TIVES
-
`.
x� E MARKS
LAB
SAMPLE DESCRIPTION
COLLECTED--
--
HOURS
SLUDGE)'
SEE BELOW
NO =
SIZE��
,:
^g
'Q `
ID NO •
_
U l
114
f0.' 3'
Iva_Rs 403
°Q s
--
_C
L
- --
-
b
N."
Sampler's Signature
/
Sampled By (Print Name) le 4i
Affiliation
• D D
Upon:relinquishing, this Chain of Custody is your authorization for Prism to proceed an with the alyses as requested above. Any changes must -be
submitted in writing to the Prism _Project Manager. There will be charges for any changes after analyses have been initialized.
Re�lin%'shedBy:(Slgnature)/ / -
.
Receiv By: (Si nature)-
Da
Military/H
- AddlYlonalComments:
j'$j{'q'rf}VI'TiITt•:,,'�;(`-j�``,'•-`^'
„..
!F /t .. LPL 2.e
Site'�e`parture Time..: '.
Reli ed By: (Si nature
Received By: (Signature) -
Date
inquis ,e By: (Signature) - : "' :
R_ eoeived/ Prism Laborator ,B,i�g.
`G�
Date
-
age'•
ci
/ (%S
:J1(fil
Xp
hod of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE,TAPED SHU yTco H CUSTODY SEALS FOR TRANSPORTi N TO THE LABORATORY.
COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAIN G'OC
UNTIL RECEIVED AT THE LABORATORY.
O
ed Ex ❑UPS ❑ Hand -delivered rism Field Service ❑Other
-
DES:
UST:
GROU DWATER:
DRINKING WATER:
SOLID WASTE:
RCRA:
CERCLA
LANDFILL I
OTHER:
A
C ❑ SC
❑ NC Ll SO
❑ NC ❑ SC
❑ NO ❑ SC
❑ NO ❑ SC
❑ NC ❑ SC
❑ NC ❑ SC
❑ NO ❑ SO
❑ NO ❑ SC
*CONTAINER TYPE CODES: .A = Amber C = Clear G = Glass --P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero. Head Space)

e velReport::...
!r
JPRISM I:..
Full-SarVice Analytical'&
'
2/3 /14
m Envlronental'Solutions
' 1111IMLABOBATOFNE6 ING. .
City of Statesville, NC
.: :.: Project:
StaLime.
:.... ' Prism:Work Order. 401039ti
.:
Attn: Andy Smith ...
::,,Time Submitted: 1/27/2014
1:35'.00PM
:. P.O.'Box.1Ill
:..
Statesville, NC 28687
"
Total Metals - Quality Control
Reporting::
:::Spike ; Source %REC
RPD
Malyte
Result
Limit
Units
Level Result %REC Limits RPD :'
Limit Notes
BatcKMA0429 - 3050B
Blank (NA0429-1211-K1)'.:
Prepared: 01128/1:4 Analyzed: 01130/14
Arsenic:: :.. :..
:. . BRL
... 0.25
: mg/kg wet
Cadmium
BRL
0.25
ing/kg wet
':60pper "' "'
BRL
0.50
mg/kg Wet.
-
Lead:
BRL :' :
0.26
: mg/kg wet
Nickel
BRL::
:1:0
' mg/kg wet::
,Selenium
BRL.:'
..50;
mg/kg wet
Zinc :
:: BRL
2.5
mg!kg wet
LCS (P4A0429-BS1);
Prepared: 01/28/14 Analyzed: 01/30/14
Arsenic: ;' : ' ;
20.3
0.25
' mg/kg wet
25.13 81 ' : 80-120
Cadmium" :
22.2
0.25
mg/kgmg/kg wet
25.13. 88 : 80.120
22,2:.
0.50
mg/kg wet:,
25.13 i89:. 80-120:: .
Lead;
20A
0.25 •
mg/kg wet
;25.13 80 80-120
Nickel
202::
1:0
mg/kg wet::
'25.13 81:. 80-120 •
Selenium
21.5.: -
0.50:
mg/kg wet.:
"'25.13 86 80-120:.:
Zinc
20.7
...
2.5
mg/kg wet
25.13 83 : 80-120
Batch: P4A'0433 - 747.16
Blank'(F4A0433-BLK1)
;:.;
Prepared: 01/28/14,;Analyzed:01/29/14
;Mercury
BRL
0;020
mg/kgwet.
a.
LCS;(134AO433-BSI)
Prepared:01/28/14 Analyzed:01/29/14: '
Mercury
0.462:: '
0.620
' mg/kg wet::
0.4167 1.11: 80-120.:: '
.:
This report Should not be re :roduced, exce t irt'its entire
p p ty,;withbut the written:consent of l?rism Laboratories,'Inc.
" 449 Springbrook,Road - P.O. Box 240543 -;Charlotte, NC 28224-0543
Phone:,7041529-6364;-Toll Free Number: 1-800/529-6364- Fail: 704/525-0409,
Page 4 of 6 ;

��.•.
'''Level
.. Le II QC Report' •
Full-Ser ilce AnalyticaG&
2/3/14
vlronmental;SolutlonaRI: En
EiORAT.OFUFA INC.
..
Gity of Stat2svi11e, NC
: ' ;; Project: StaLim •: Prism Work Order: 4010396
:'
Attn: Andy Smith
Time Submitted: 014
1:35; OOPM
P.O. Box .1111
Statesville, NC 28687
General ChemistryParameters = Quality Control
Reporting'. Spike Source %REC
RPD
Ahalyte
Result:: Limit ' Units Level _ Result %REC' Limits .:: RPD
Limit Notes
BatcKMA0450 -:NO PREP ::. " '
Blank (P4A0450-BLK1)' ;
Prepared & Analyzed; 01/29/14
% Solids. ... :..
100 '0.100 % by; Weight
Sample Extraction Data :.
P.re . .
....P Method: 30506
.. . .
Lab Number ::.
Batch ::::. Initial ; . Final i ::.. Datelrime; ; ; .
4010396-01.:
P4A0429 2.04 g 50: mL , 01/28/14 10:00;
4010396-0.1..
P4A0428 ... 2.0,4 g 50, mL :. . 01128/14.10:00. .4.
:Prep Method:.747113
Lab Number
Batch Initial Final : Date/Time
40.10396-01 :..:
P.4A0433 0.57..g 50 n7L..: 01/28/14 12:30 ..:.
• ;
. ;This report should not be reproduced, except, in its entirety,. Wit out the written;consent of Prism Laboratorie's;'Inc.
Springbrgok.Road - P.O'.;Box 240543 -:Charlotte, NC 28224-0543
'
.'
Phone: ..
ne:,704/529.6364:-Toll Free Number: 1-800/529-6364 - Faic, 7041525-0409, .
:Page 5 of

CHAIN OF CUSTODY RECORID
ISM(Full -Service Analytical &
Environmental Solutions :PAGE _ OF _ QUOTE # To ENSURE PROPER BILLING:
L'ctJa.'�Ps,':'�•-:;.»"-°✓.l.rF'_''" LABORATORIES, INC._ .. ... . . . ..
Project Name:
449 S ringbrook Road. ®P.O.. Box 240543 ®Charlotte; NC 28224-0543
Phone�
704/529-6364 a Fax: [phone] Short Hold.Analysis: (Yes) .(No) UST Project: - (Yes), : (No)
%4 Y d' �¢a�cg ✓r ��� Please ATTACH any project specific reporting (QC LEVEE_ 1 II.Ili IV)
Client Company Name: C
Report To/Contact Name rt S v Sb 41,
provisions and/or QC Requirements
Reporting Address: F-Q • Box 1111 ... :Invoice To:
Address:.. - . -
F� IVC
Phone: 70 Y'6 7l-A589 Fax Yes-(No):74y' $7,T' 86`' -Purchase Order No./Silling Reference
i®.SE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Data: ❑ 1 Day ❑ 2 Days ❑ 3 Days. ❑ 4 Days ❑ 5 Days
Certification: NIELAC USACE FL NC
EDD Type: PDF_ EXcel_OtheY ' Working.Days" ❑ 6-9 Days ❑ Standard.10 days ❑ RushPre-AWpoork Mdust Be
Name: �d �' C'�F=�'L"�P business day..:
"
SC_ OTHER WA
Site Location Samples received after 15:00 will be -processed next
�� %�• �ar •a � Turnaround time is based.on business days; excluding weekends and h liday 13
Water Chlorinated: YES_ NO
Site Location. Address: �'/� •
_ �y - (SEE REVERSE FOR TERMS &CONDITIONS REGARDING SERVICES
+
BY LABORATORIES, INC. TO. CLIENT)
Sample Iced Upon Collection:::YES NO .
.4A-(eSt�,:�r PRISM
- RENDERED
.-
TIME : :
MATRIX
SAMPLE CONTAINER
S
Y \yEOU ES
v(�ANAL SE
FLAB
CLIENT _:: ...:..:
DATE
COLLECTED.
(SOIL,
PRESERVA-
k� REMARKS
-'TYPE .:
SEE BELOW
NO:.
. SIZE
SAMPLE DESCRIPTION
-COLLECTED-
- MILITARY.
WATER OR
TIVES
..
/ . " ?,
ID NO.
HOURS
SLUDGE) .:
.3I¢A
a-23120
F.
1�doek
Pb
I... ...
::
O
.. .
Sampler's Signature G Sampled By (Print -Name) A / r► Affiliation .
Upon relinquishing, this ain of ustody is your authorization for Prism to. proceed with the analyses as requested above. Any changes must be •
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses -have been Initialized.
Relin had B : Si nature) Recel a By: (Signatur Dater Military/Hours Addltl
t 421 `
RetqOshed By: (Signature) Red&veBy: (Signature) Date _ ;Slj ABpart T r)le - e (Ire
�9
Relin had B g ature Recei 9d For P Laboratories By:. rf Date -
Q Y:(/ )` Y h �' tJlilea e:°
��
MhOod of S i e t: E: L SAMPLE COOLERS SHOULD BE TAPED SHUT WITH GUSTO Y SEALS FOR TRANSPPP ION TO THE LABORATORY. : COG Group No.
:. SAMPLE ARE NOT ACCEPTED AND VERIFIED AGAINST COG UNTIL VECEIVED AT -THE LABOR/TORY.-
❑ Fed Ex ❑ UPS :O Harid-delivered ❑ Prism Field Service ❑:Other
NPDES:::. ff :UST: 1 GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA ...' LAh,11FILL OTHER:
❑ NC ❑ SC p NC ❑ SC p NC - ❑ SC ❑ NC_: ❑.SC..:: ❑ NC ❑_ SC- ❑ NC ❑ SC ❑ NC - ❑SC NC ❑ SC ❑.NC ❑ SC ... ....
❑ I0 .1❑ ❑ f }❑
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic;: TL, = Teflon -Lined Cap VOA = Volatile Organid,s Analysis. (Zero Head Space)
-....

_.
Laboratory Report
4211.im
-Service Analytical k ' •' • " • "'
"' "'
ISM
I ,Full
EnvlronmenY9l.solutlons ::.' :.'
,..
02/07/2014
• LABORAMRIEr ING,
.
:City of Statesville, NC :::'
: Project: Stal-ime.
Client:Sample ID::::-Sta-Lime:.:
::. Attn::Andy Smith;:::.
.... ..... ..... ::::.
Prism Sample.ID:4020025-01 :.
P.O'. Box:1111
Prism Work .Order: 4020.025'
.. .. ..
Statesville, NC 28687
Sam le 'Matrix: Solid' '
Sample
:': Time Collected:'02/03/14 1 .40
,Time Submitted: 02/03/14
Parameter
MDL :'Dilution :'Method Analysis Analyst 'Batch
Result Units; Report;
...
.. • Limit
'Factor . ..:: ; .:: Datefrime :.:: ID
General Ctiemistry.Paraineters
Solids
71.7 • % by •' 0.100
0.100 1; , 'SM2540. G 215/14 15:10 JAB „ P4B0063
Weight
Microbiological Parameters
:Fecal Coliforms. • • .
BRL MPN/ d 0.3
1 'SM9221 E:: 2/4/14 12:33. • MES P4B0061
q.
:.:
q.
;TFii's report should'not be re Yoduoed, exce t in:its entirety,:without the written consent of •Prism Laborafories,'Inc.
P P P
449 Springbrook,Road - P.O.; Box 240543 -;Charlotte, NC 28224-0543
Phone:.[phone]:-Toll Free'Number: 1-80OM29.-6364 -Fait; 7041525-0409. :. .Page 3 of

CHANK OF CUSTODY RECORD
US o
K 'f'
Full -Service -Analytical &
'�iYE,S•"i4rN0�':r;�f�J/�
C.0
L",<'�.• 'Environmental
g� R;il
-,�
Solutions
B PROPER BILLING:
PAGE _ ow _ atuoYE u ao ENSURE
-'spier' -
';Samples;INTACT.uoh�`arival?,ft i;,? frel'ti'J-:-,�..
"'�Y•.s r,=;'<•
�
o
BORATORIES, INC.
..
Road • P.O. Box 240543 • Charlotte- NC 28224-0543
449 Springbrook Ro , -
• -
Phone. [phone] Fax. [phone]
Project Name:
Short Hold Analysis: (Yes)- (No) ... UST Project: (Yes) (No)
'I, - 4i.%':'- -' _>Recei ed01�p1hlETIGE..T.,ern` -
r - - _- _ _ " .::.. �,..
PJ'OPE, PRES ATLVES liidicated?.`s'%r>; :`-:'- ` '''-''
R, -:,- ,::ER4�,..:.:...a;,-s :,. ;;; ; . ;<, ,.:-- .::; :_--?,:.::.;.:.
RCU
iReliefVed.VVtT;INI�Q�171NGTIMES�;�,��'::=i';r�`'�, �'•::.�;;-:',:,:-
rn
/ r
an Name:
Client Company
*Please ATTACH anproject specific reporting (QC LEVEL 1 II 111 IV)
d
p Y
g �J►n 4h
provisions and/or QC Requirements
' Vt 'r./0'UT'HE`. DS l`GE
n
Report To/Contact Name: +�
To: To:
LATIL
0 ES e ;d'uv. A,Invoice
tea;: ,-1:= rr-
Reporting Address: PC) a ox I I IF
l?RfJ .ERs ,NTAINE'S"use' 7-"t
P Gta „y ; Fi d„ �,�Y; ,r.�
L �r Ale
Address: -
Phone: 74Y-97$•- A3-9 Fax Ye (No):` 0147$- 845:1
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (NO) Email Address .. - Requested Due Date ❑ 1 Day ❑ 2 Days Cl 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE
FL - NC
Must Be.
EDD Type: PDF_ Excel _Other e "Working Days" ❑ 6-9 Days El Standard, 10 days ❑ RushPre-Work/A
Site Location Name: Foir 4.4 C�e-e &) Q 1 P Samples received after 15:00 will be:processed next business day.
Site Location Physical Address: 6fy 8P 11 Fam 1� 7 r� Turnaround time Is based on business days, excluding weekends and holidays.
ScSC OTHER
-
Water Chlorinated: YES_ NO
S44 J ," (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
i ���f® �� RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)- . -
Sle Id Upon Collection: YES
am P Iced P
NO
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSES REQUESTED
Ur REMARKS:
PRISM
LAB
ID NO.
*TYPE
SEE BELOW
NO.
SIZE,'
Sampler's Signature x 4 i,— Sampled By (Print -Name) /?4 1rl O K t Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the -Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Reli shed By: (Signature) Received By: (Sign e) Date
Re shed By: (Signature) Received By: (Sicf a . re) Date
Mil- ours Additional Comments:
-Site Arrval:Time";
SI(B;,DBp21tUCQ;Ti(118::
Relin uished By: (SI ture) 618,ecForPrism Lab rles By: Date
ah
Met d of Sh pYnent: NOT r L SAMPLE COOL S SHOULD BE TAPED SHUT WI CUSTODY S S FOR TRANSPORTATION TO THE LABORATORY. 000 Group No.
TED AND VERIFIED AGAINST CO UNTIL RECEI D AT THE LABORATORY. -
SAMPLES AMPLE 7ri.
❑ Fed Ex ❑ UPS ❑ Hand -delivered Field Service ❑ Other - Ll G `ooys
zV.:`3?r
NPDES: IUST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL
OTHER:
'•
❑ NC ❑ SC j .❑ NC ❑ SC Ij NC ❑ SC ❑❑ NC ❑ SC I ❑❑ NC .❑ SC Ll NC ❑ SC O NC ❑ SC ❑❑ NC ❑ SC I
a NC ❑ SC
ftl� If'all�t l
*CONTAINER TYPE CODES: A = Amber .0 --Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

.1
:..
Laboratory Report
Full -Service AnalyticalsEnvlronmentol.Solutlon
ffRo IoSaM
A
02/18/2014
:.
City of Statesville, NC
::
..
Project: StaLirrte:
Client.Sample ID:..
Sta-Lime
Attn: Andy Smit1 ::
Prism Sample.ID:
40201.86-01
P.O. Box,1111
Prism Work Order: 4020186
Statesville, NC 28687
'Sample
Matrix: Solid
Time Collected: 02/10/14 10:35
Time Submitted: 02/10/14 14:00
Parameter
Result Units:
Report:
MDL
Dilution Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID'
General Chemistry Parameters
Solids
72.2
% by
0.100
0.100
1 *SM2540, G
2/12/14 72:15 JAB
P4B0204
Weight
Microbiological Parameters
Fecal Coliforms,
BRL
MPN/g dry
0.3
1 *SM9221 E
2111/14 9:30 MES
P4B0214
Total Metals
d.
..Mercury
0.14
mg/kg dry
0.028
0.11093...
1 *7471B
2M7/14 15:47 MEH
P4130244
:Arsenic "'
7.5
mg/kg'dry
0.35
0.051
1 *6010C
2M4/1419:16 BGM
P4130220
Cadmium
BRL
mg/kg dry'
0.35
0,0033
1 *6010C
2/14/14 19:16 BGM,
P480220
Copper'
33
mg/kg dry
0.70
0.0088
1 *6010C
2/14/14 19:16 BGM
P4130220
Lead
8.4
mg/kg dry ,
0.35
0.041
1 *60.10C
2/14/14 19:16 BGM
P4B0220
Nickel
130
mg/kg dry
1.4.
0.011
1 *6010C
2114/14 1906 BGM
P4B0220
Selenium
BRL
mg/kg' dry
0:70:
0.085
1 *6010C
2/14/14 19:16 BGM
P4130220
Zinc
51
mg/kg dry
3.5
0.024
1 *6010C
2114114 19:16 BGM
P4B0220
This report should not be reproduced, exce t in its entire p p p .: ty,.without the Writtenconsent of Prism Laboratories, Inc.
449
Springbr 'ok,Road - P.O.; Box 240543 -'Charlotte,
NC 28224-0543
Phone: [phone],-Toll Free Number: 1-8001529-6364
- Fax: [phone]
Page
3 of 7

Level Report
h Full-Sorvice Analytical ' 2/18/14
I.S M Envlronmental•Solutlons
® PA
�V'LABoMToniEr, ING
'City of Statesville, NC :: ,; Project: Stal-ime„ Prism'Work Order: 4020186;,,:
Attn: Andy Smith Time Submitted: 2/10/2014 2:00:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry' Parameters : Quality Control
Reporting Spike Source %REC RPD
An'alyte Result Limit units Level Result %REC' Limits RPD Limit Notes
Batch P4BO204 - NO PREP
Blank (P4BO204-BLK1); Prepared & Analyzed; 02/12/14
% Solids 100 0.100 %'by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook,Road - P.O., Box 240543-!CHarlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 Of 7

-a
Level II'QC Report'_
®h RISM
Fuli-SerJice Analytical:&'
I:
2/18/14
�
Environmental ;Solutions
OPUTOMM INC
,City of Statesville, NC
"::.; Project: StaLim+r ,' ' „ Prism Work Order: 4020186,;
Attn: Andy Smith
Time Submitted: 2/10/2014
2:00:OOPM
P.O. Box,1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting' : Spike Source %REC
ROD
Analyte
Result Limit ' Units. 'Level Result %RECLimits ' RPD
. -Limit Notes
Batch:P4B0214 -,NO PREP :.
Blank (kB0214-BLK1)' :
Prepared & Analyzed, , 02/11 /14
Fecal Coliforms
BRL 0.2 'MPN/g wet
"
Sample Extraction Data'',
Prep Method' .3.050B
Lab Number
Batch ::. Initial Final Date/Time ..
4020186-01.:
P4B0220 1.98 g 50: mL 02/14/14 9:50
Prep Method:7471B
Lab Number.
Batch Initial Final Daterrime
4020186-01
P.4B0244 0.6 .g.. 50 mL 02/17/.14 9:30 .
"
Tois report should'not be reproduced, except, in its entiretY.w..it.hout the Written consent of Prsm Laboratores,Inc.
449 Springbrook.Road - P.0.:Box 240543 -:Charlotte, NC 28224-0543
Phone: [phone];7Toll Free Number: 1-800/529-6364 -Fax: [phone]
P8 e 6 of 7
9

CHAIN OF CUSTODY RECORD
Full -Service Analytical i3r
•` Environmental Solutions
M I
;a= ,ti;."`>r;` YCS'°'''`' NO„ •N/A;-
'Sam (esilt u" w
.
:r.,
PAGE _ OF _ OYJOYE N TO ENSURE PROPER BILLING:
17AGT bn-arrival.,,,l'„.,,, .... ,.
.
P. a O
.H... ., .., ;:
.n.:,' .,,,,�-„�.-_•.LABORATORIES, INC.
_ �_•.,
.+L:`--'-� -
Received ON'N1ETiICE•, ieTp, jam-
.
449 Springbrook Road P.O. Box 240543 Charlotte, NC 28224-0543
Project Name:
�;�;:,..:�.-:,;,r�..,;,,.-�.;-.,�; �,.�s.,
...PROPER,P.,RESRVATI,VESindcated?:; : ":` := • ? '•: i{.: ` ::= N
Phone: [phone] . Fax: [phone]
i
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
rn
geoeived WITHIN WOLDING TIMES
'
�' �' '9 irr Ile
Client Company Name: n a
*Please ATTACH any project specific reporting (OC LEVEL 1 11411 IV)
0_
provisions and/or OC Requirements
- CljS70DYt5EAL5.INTACT?s,, r,r ;:, , :.,,. ,•-,:.:.?...
;. •; ;: ,; ;;, ; ;t,-- ,;-..- -;" '
Report To/Contact Name:
Reporting Address
Invoice To:
— -
PROP•. R-,CONTAINR$iised. 'l;r;
r
Address:
Phone: 74 fir- rY'76' 4131, Fax es (No): fU i- 67 -5 Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) -(No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE
FL NC
EDD Type: PDF_ Excel —Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
_
Site Location Name: a w,,f h C.^ee. < IV Cap f P Pre -Approved �:
SC_ OTHER
N/A
;1 Samples received after 15:00 will be processed next business day.
Site Location Physical Address: 0�3 j-) I rQ rm !i Turnaround time is based on business days, ekcluding weekends and holidays.'
Water Chlorinated: YES— NO
I✓/� A/C REVERSE FOR TERMS &.CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES
NO
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES REQUESTED
PRISM
- CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
O
B
*TYPE
N0.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
11/1
REMARKS
ID
_HOURS
SLUDGE)
SEEBELOW
4s
R. tat _a
f
C1
Cu.
Pb
Sa
-
Sampler's Signat�✓ ' z Sampled By (Print Name) G '/ C K Affiliation
ure
Upon relinquishing, this hain o ustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
,
.submitted in writing to thei Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Re�l' ulshed ey: (Sign ure) Recerved By: (al in tur D
Military/Hours Additional Comments:
's Ee'arri5ai 7ime_y
Rel W<ked By: (Signature) Re By: (Signature) Date.
Site Dep2ltUYe fime
1� jf17 L/ ( 17t7
a FElti;TeCh`'Fee:`
Relinquished By: (Sign u Received For Prism LaM� ratories By: Date
%'%• >.'
�!/
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHIN ITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. CDC Group N9�
SAMPLES ARE NOT ACCEPTED AND VERIFIED ALAI,GOC UNTIL RECEIVED AT THE LABORATORY.
V i^
❑ Fed Ex ❑ UPS ❑ Hand•dellvered rism Field Service ❑ Other
NPDES: - UST: GRO DWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL
OTHER:
'
llglum
❑ NC: ❑ SC ❑ NO . ❑ SC NO SC :
_ NO ❑ SC ❑ NO ❑ SC, ❑ NO SC' NO ❑.SC p NC ❑ El❑
❑ SC ❑ ❑ El....
�I I.
❑ NO SC
❑
❑ I❑ ❑ ❑ ❑ ...❑ Cl _� ❑
-
a71lS�.;9im A
ONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL:= Teflon -Lined Cap VOA =' Volatile Organics Analysis (Zero Head Space) :.
( — --_— --

NC Certification No;;402
rrative
LPw�
a ion N: 99012"' "'
SC'Certific t ase NaFull-Service Analytical & NC Drinking Water cent N6.37735 I I S M • Environmental Solutions vA Certification No. 460211 03/03/2014
OCABORATORIES,INC DoD ELAP>L-A-B Accredit ed'Certificate No. L2307
:.:ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Ci 'of Statesville
, e; NC :Project: StaLime
Andy Smith.
:
P.O. Box 1111. Lab Submittal Date: 02/24/2014
Statesville, NC 28687 Prism Work Order:4020418
This data package contains the analytical'results for the project identified above and includes a Case Narrative, Sample
Results and Chain of'Custody.' Unless otherwise noted, all samplers were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged'individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you: have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC:
Robbi A. Jones Reviewed By Terri W. Cole For Robbi A. Jones
President/P'roject Manager. Project Manager
Data Qualifiers Key Reference:
MI Matrix.spike outside of the control limits. Matrix interference suspected.
BRL. Below Reporting Limit
MDL, ' . Method Detection Limit
RPD Relative, Percent Difference
* 'Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
•
reporting limit indicated with a J.
:This report should'not be reproduced, except: in its entirety,, without the writteh:consent of Prism Laboratories, Inc.
449 Springbrook,Road - P.O;.;Box 240543 -:Charlotte, NC 28224-0543
Phone:.[phone]:- Toll Free Number: 1-800/529-6364 - Fax: [phone], Pagel of 8

• •
Laboratory. Report,:
®n
r �•1 S M
�L gRJp MMFA INr-.
Full -Service Analytical&
::EnvlronmentaLSoluttona ::.'
03/03/2014
... ..:. ...
City of Statesville, NG .::'
:. ... .... ... ... .... ...
: Project: StaLime:
.... ...
.... ...
...
.... ... ....
Client:Sample ID::::'
... .. ..
Sta-Lime::":
....
:. Attn::Andy Smith' i::.
:.
Prism Sample.ID:
40204.18-01
P.O. Box.1111
Prism Work .Order: 4020418'
Statesville, NC 28687
" : Sample Matrix: Solid
Time Collected: 02/24/14 00:00
"
Time Submitted: 02/24/14 16:15
Parameter
Result Units
Report
MDL
Dilution Method
Analysis Analyst
. Batch
Limit
Factor
Date/Time . ..
ID
General Chemistry.Parameters
°
/° Solids
66:1 % by
0.100
0.100
1' . • *SM2540 G
2/27I14;15:30 MJO
P4B0504
. '.:
Wei ht
g
Microbiological Parameters
Fecal Coliform:s
; :. BRL _ • MPN/g dry
0.3
1 SM9221 E ;
; . • 2/25/14 12:15 MES
P460476
Total Metals
..Mercury ..:
.:: 0.11 mglkg dry
Q.032;.
7 ...
0.01„
1 ..: *.7471B
2/28114 13:04. MEH
P480513
•
'Arsdnic "'
S.9 mg'lkg'dry.
0:38
0.056
1 "' '*6010C
"' 2/26/14 18:40 BGM
P4B0449
Cadmium';
BRL• mg/kg dry'''';
, 0.38
..0.0036
1. *60100
2/26/14 18:40 BGM
P4B0449
Copper'.::' • :
33: :'mg/kg dry
0.76
: ;0:0096
1 *60'1QC'
2126114 18:40 BGM
' P4B0449
Lead ' • •
8.4 : -mg/kg dry.:.:
0.38 ::
i .: 0.045
1:' *6070C
2/26L14. 18:40 BGM.
P460449:
;Nickel :
; : ; • ; :::. 120 mg'/kg dry
IA.
0.012' •
1 : ; . *6010C
:: 2/26M4 18:40 , BGM
P4B0449
9ele6ium
BRL ' mg/kg' dry
0:76 :
0.092 :
. 1 •*6010C
2/26/14 18:40: :BGM
P4B0449
56 mglkg dry
. 3.8.
0.026'
w.
1 , , *6010C
" 2/26/14 18;40' ,BGM
P460449
This report shduld'not be re roduced, exce t Wits entire' Without the writt'en.00nsent of Prism Laboratorie's,'Inc.
P P::.. P::.. tY,::..
449 Springbrook,Road - P.O.: Box 240543 -:Charlotte, NC 28224-0543
Phone:.[phone]:-Toll Free'NuMber: 1-800/52y-6364-
Fax: [phone]. ;,
Page
3 Of $, :.

Level II QC Report
Full -Service Analytical '& "' " 3/3/14
M t Envlronmental'soiutiona •' ... ..
vCA9ONAT01MEft INQ.
''Cif ''of of Statesville, NC
Project: StaLime.:
Prism:Work Order: 4020418
Attn: Andy Smith ::.
Time Submitted: 2/24/2014
4:15:OOPM
P.O. Box 1111
Statesville, NC 28687
"
Total Metals - Quality'Control
Reportin9.:
Spike
Source
%REC
RPD
:Analyte "
Result
Limit
Units
Level
Result
%REC'
Limits
RPD
Limit Notes
Batch P4B0449 - 3050B
Blank (1341130449-1131-11<1).:
Prepared & Analyzed:.02126/14:
Arsenic.
BRL
0.25
. and/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.49
mg/kg wet
Lead.
BRL
0.26
mg/kg wet
Nickel
BRL'
0.99
mg/kg wet"
:Selenium �
BRL
0.49
m /k wet
9 9
Zinc .'
BRL
2.5
mg/kg wet
LCS (113460449-113SI)
Prepared
& Analyzed: 02/26/14
Arsenic
23.1
0.25
mg/kg wet
25.25
91
80-120
Cadmium
22.4
0.25
mg/kg wet
25.25.
""
89
80-120
:Cropper
24:7:
6, .1
mg/kg wet:,
25.25
:09
80-190 .
Lead;
217
0.25
mg/kg wet
25.25
90
80-120
Nickel
22.8.
.1.0
mg/kg wet
25.25
90
80-120
Selenium .:'
22.2. "
0.51
mg/kg wet
25.25
"
88
80-120
Zinc
22.8
2.5
mg/kg wet
25.25
90
80-120
Matrix Spike (1241130449-MS1)
Source:
4020418-01
:
Prepared
& Analyzed: 02/26/14
Arsenic.
34.2
0.38
mg/kg dry
38: 20
5.85
74
75-125
MI
Cadmium
19.1
0.38
mg/kg dry
38.20.
BRL.:.,
50
757125
MI
Copper
65.8
0.76
mg/kg dry
38.20
33.2
85
75-125
Lead
29.3'.'
0.38
mg/kgdry
:.'38.20
8.38
55
75-125
MI
Nickel
138.
.1.5'
mg/kgdry.,
38.20
116
57
75-125
MI
Selenium ...
24.4„
' 0.76
' mg/kg dry,
38.20
BRL
64 "
75-125
MI
Zinc
82.7
... 3.8
mg/kg dry
38; 20
56.2
70
75-125
MI
Matrix Spike Dup (P4B0449-MSD1)
Source:
4020418-01
Prepared
& Analyzed: 02/26/14
Arsenic
35.0
0.38
mg/kg dry
38.40
5.85
76
75-125
2
20
Cadmium..
19.4
0.38
mg/kg dry
38.40
BRL
51
75=125
2. "
20
MI
:Copper
63.8
0.77
mg/kg dry
38.40
33.2
80
75-125
3
20
Lead
29.8
0.38.
mg/kg dry
38.40
8138
56
75-125
2
20
MI
Nickel
13.8..'.
1.5
mg/kgdry
38.40
116
58.
75-125
0.3
20
MI
-Selenium " :" "'. '"
24:5 .:'
0.77:
mg/kgdry
'.'38.40
" BRL
64
to-125
0.4
20
MI
Zinc
85.0
3.8
mg/kg dry
38.40
56.2 ,
75
75-125
3
20
This report should not be reprgdUbed, except ih its entirety,'withbut the written'consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O; Box 240543 -'Charlotte, NC 28224-0543
Phone:,704/529-6364.-Toll Free Number: 1-800/529-6364 - Fax: [phone], -, Page 4 0f 8

II
:. .. �., \:. .... Level4C Report ...
S � Y I 4: Enivl onm .. ..
rviee Analytical'&' 3/3/14
1w mental Solutions
01ll1TONIE$ING
City of Statesville, NC :::.:
:' Project: StaLime•;: Prism Work Order:'402041'8 •,:" "'
Attn: Andy Smith : • . • Time Submitted: 2/24/2014 4:15:OOPM
P.O. •8ox.1111
Statesville, NC 28687:
Total Metals - QualityControl
Reporting' ".Spike . Source %REC RPD
Arialyte Result:: Limit Units, Level Result %REC' Limits : RPD Limit Notes
Batch:P4B0449-:3050B
Post Spike (11341130449-PS1)
Source: 4020418-01
Prepared & Analyzed:; 02/26114
"
Arsenio'
0,901 "mg/L
1.000 0.154 " 75
807120
MI"
Cadmium :
0.507 : "mg/L
1:000-0.0158 52 .80-120
MI
,Copper
1.63: • mg/L; ; :
1.000 0,872 76
80-120 ,
MI
Lead;
0.772 mg/L
•1.000 O'.220 55 : •'
80-120
MI
Nickel
3.48:: mg/L ...:
1.000 ..'3.06 42
80-120
MI
Selenium
0.694.. i.i mg/L..:.:
1.000 00863 73:
80-120
MI
Zinc ::.
..
2.10 m /L
g
1;000 1.48:62
.
80-120
Batch:P4.B0513 - 747.1 B
Blank;(P4B0513-13LK1):'
Prepared & Analyzed:'02/28/14"
;Mercury
BRL. 0.020 mg/kg wet
LCS;(P41B0513-113SI)
Prepared & Analyzed: 02/28/14
Mercury
0.437:: ' 0.020 ' mg/kg wet
: 6.4167 • . • . 105:
80-120 .
:Matrix Spike:(P4B0513-MS1)'
Source: 4020418-01 "Prepared
& Analyzed: 02/28/14
"'
Mercury..
0.729 0.030 mg/kg dry
0.6200 0.114' : 99
80-120
Matrix Spike Dup (P4130513-MSD1)
Source: 402041E-01
Prepared & Analyzed:: 02/28/14
Mercury
0.805 „•0.031 mg/kg dry
0.6410 • 0.114 108
80-120 10 20 •
This report should not be reproduced, except ih:its entirety,. without the written -consent of Prism Laboratories, Inc.
449 Springbrook.Road - P.O.; Box 240543 -'Charlotte, NC 28224-0543
Phone: [phone]:-Toll Free'Number: 1-8001529-6364 - Fax: [phone]. Page 5 Of 8

q a

., Level II.QC Report
®®� Full -Service Analytical'8'
3/3/14
r Environmental Solutions :.
City'of Statesville, NC Project: StaLime,; ::;,; Prism'Work Order: 402041'8
Attn: Andy Smith :. • Time Submitted: 2/24/2014 4:15:OOPM
P.O. Box,1111
Statesville, NC 28687:
Microbiological Parameters - Quality Control
Reporting Spike . Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4BO476 - NO PREP :..
Blank (134B0476-BLK1), -
" Prepared & Analyzed:.02/25/14
Fecal Coliforms
BRL 0.2 MPN/g wet
Sample Extraction Data .
,Prep Method:3050E
Lab Number
Batch ::
Initial Final Datelrime
4020416-01.
P4130449
1.99 g 50 mL .02/26/14 9:00
Prep Method: 7471B
Lab Number . '
.:Bitch
Initial Final Datelrime
4020418-01
P4B0513
0.57 .g.: 50 mL. 02/28/14 10:15
This report sh;6uld'not be repiri'rodubed, excepf its entirety;,, without the Weitten'6onsent of Prism Laboratories,'lnc.
449 Springbrook.Road - P.O. Box 240543 -:Charlotte, NC 28224-0543
Phone: [phone];7 Toll Free'Number: 1-8001529-6364 - Faz: 704/525-0409, Page 7 of 8

CHAIN OF CUSTODY RECORRAX
D
5.
I
Full -Service Analytical &
Environmental Solutions
r _ : -:,'N/A,_'
,
`r' „YES ';Z:NO,-, i;.'-:iN/A:=
t':r " '•^ •,,.,.r;-:::-.:;.r::.:
�'=Saiii �.
00
.�
o
�+.�.,, - -
ice;&,'::hwir�l:au.. IABORATORIES, ING
�
PAGE _ OF _ ®uoBE s vo ENSURE PROPER BILLING:
IesaNTACT:u . ,. w:
7. •.. ,}/:". `,l.zi;�,<`i+, •.
::Recei'vgd'QN,WET'ICE :Temp,;
00
9 S rin brook Road.• P.O. Box 240543 • Charlotte NC 28224-0543
44 p g
Project Name:
-
=-. `RROPER',PRESERV-1 , S irid cateiih =:<%< 'i' :'-.'-= ' -l°== ' ": :':°
o
0)
Short Hold Analysts: (Yes) (No) UST Profect:. (Yes) .(No) :f,:r,..::..'r%": ,>::4,f<; -;!- ;..:, •.,, :.. co
Phone: [phone] •Fax: [phone] / ; `Received WITHIN,HOLDINGTIMESI D-
c ' '- W. �('eSt•er/lc *Please ATTACH any project specific reporting (QC LEVEL 1 11 III IV) Client Company Name: O - o ; CUSTODYSEALS,,INTAC- _
provisions and/or QC Requirements ;,•,, -
Report To/Contact Nam e:
n to Sin.4�e VCJI ATILES reed VV10U f:FIEADSPAC�? � s f --_
Invoice To: :E:,.
'�9.t • ;r=;> ;fir
h '1? ORERiCONTAINERSsusetl.
n Address: P.0. X ►ill9 fi r'"rrs'
IRe ortl g
p ,
Address: ,,:;777
Phone: I01-97'313idFaX es (No):74y'7Y'Y455 purchase Order No./Billing Reference
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day a 2 Days ❑ 3 Days ❑ 4 DaysWb] 5 Days "Certification:
IEDD Type: PDF_ Excel —Other a ,+ «Working Days'.' ❑ 6-9 Days ❑ Standard 10 days Irkdust Be
Site Location Name: Fo u' � Cfee_k ,W l %� Samples received after 15:00 will be processed next business day.
Site Location:Physical Address: 1643 Bell F�11 9t - Turnaround time is based on business days, excluding weekends and holidays.
+. I a (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
.. . . . . -. 51&4e S✓w% 11e. 14C - RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
E NC
.SC C OTHER C " N/A
Water_ Chlorinated: YES . NO_
Sample Iced Upon Collection: YES NO
P p - - ... :. ..
CLIENT
SAMPLE DESCRIPTION
DATE
-COLLECTED
TIME
COLLECTED
_ MILITARY
HOURS
MATRIX
(SOIL.
WATER OR
SLUDGE),
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSES REQUESTED
��
�` kf REMARKS
g.
PRISM :
LAB
ID NO.
'TYPE
SEE BELOW
NO. _
-- SIZEZG
AAA
Y
C
-
..
.
Ff
.....
.....
Sampler's Signature Gt✓� o �h°� -
Sampled By (Print Name)-� �J� �C
Affiliation --
,
^` ' ``' r! ,",'„ .h• ,'',"
;Ste'A�; _ t
Upon relinquishing, this Chain of ustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized. .
Reli fished By::(Signature)
Reeeiv By: (Signature)
Da a
'r
Milhary/Hours
Additional Comments:
Departure;- I,trie;:_ ;,5jte
Reli hed By: (Signature)
Rec ' y: (Slgnatu ) .
Date
11 leld TBch ;EGO:: ;';> .; ' - i <% "
Relin is ed By: (Signature)
Received dsm Labor r By:
Date
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT�CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY.
- . - SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST, UNTIL RECEIVED AT THE LABORATORY.-
❑ Fed Ex ❑ UPS ❑ Hand-dellGered rism Field Service ❑ Other
COC Group No.
NPDES: UST: GJI'OUNDWATER: DRINKING WATER: SOLID WASTIE: RCRA: I CERCLA LANDFILL OTHER: ,
❑NG_DSC:ONC [SC NC pSC ❑NC -::❑SG ❑NC IjSC pNC ❑SC, ❑NC 0SC ❑NC ❑SC :❑NC=❑SC
*CONTAINER TYPE CODES; A = Amber C:= Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis.(Zero Head Space)

NC Certification No. 402
f , SC Certification N Narrative
0 99012 ,. Case
Full -Service Analyfl0al & NC Drinking Water Cert Nor 37735
® Dow, ]l ISM
Environmental Solutions VA Certification No. 46021.1 03/21 /2014
-�fAeoRA7oRIEs, INC' DoD ELAP: L-A-B Accredited Certificate No: L2307
ISO/IEC 17025i L-A-B Aco�edited Certificate,No. L2307 ' .
City'of:Statesville; NC :..;" Project: StaLime
::Andy Smith
P.O. Box 1111 Lab Submittal -Date: 03/10/2014
Statesville, NC 28687 Prism Work Order: 4030172 .
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody: Unless oth:ervVise noted,:all samples;were received' in acceptable condition and processed
according to the referenced methods. "
Data qualifiers: are flagged, individually on each.sample. A key 'reference for the data qualifiers appears at the end of this case
narrative.
Please call if you. have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC:
Robbi A. Jones Reviewed By Terri.W. Cole For Robbi A. Jones
President/Project Manager: Project Manager
Data Qualifiers Key Reference:
BRL. Below Reporting Limit.
MDL Method:Detection Limit
RPD ' • Relative Percent Difference
* :Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
:This report shduld not be reproduced, except in •its entirety,'without the written -consent of Prism Laboratories, Inc.
449 Springbr
. 'ok,Road - P.O..: Box 240543-;CFiarlotte, NC 28,224-0543
Phone: [phone] ;
364.- Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 3

Laboratory:,Report
03/21 /2014
Client•Sample ID:::: StaLime and Fecal #1::
Prism Sample .ID: 40301:72-01 ...
Prism Work Order: 4030.172
Time Collected: 03/10/14 41:10
Time Submitted: 03/10/14 12:45
Parameter
Result
Units
Repoit:
MDL "
Dilution
Method
Analysis :
Analyst
Batch
Limit
Factor .
...
DatelTime ..::
:ID
General Chemistry.Parameters
Solids ; . . •
65.6
by
• 0.100
0.100
1;
*SM2540,G
3/14114;15:00
JAB
P4CO286
Weight
" Microbiological Parameters...... :.
....
..... ..... "''
"' .....
"
Fecal Coliforms
BRL :;.
MPN/gdry
0.3
1 ::.
*SM9221 E::...3/11/14
10W
MES
P4CO223
Total Metals
Mercury
.. 0.14 ..:. :..
mg/kg .dry
0.032..
0.017 ...
1 ....
..*.7471B . , i
: 3/14/14 14:26
...MEH
P4CO262
Arsenic "' "'
"' 1.1 "'
mg'/kg "dry
0:39 '
0.057
1
*6010C "'
3/21/14 13:41
BGM
P4CO229
Cadmium'",
'BRL,
m /kg dry"'
g
0.39
.0,0037
1_
*6010C
3/z1/14.13:41
BGM.
P4CO229'
Copper
28:
mg/kg dry
0.77
0:0097
*601,OC:
3/18/14 23:38
BGM;"
P4CO229
Lead ..:.: :' :.
... ..
. , : : mg/kg dry.:.
0.39
:.: 0.045
..
9:
*60.10C
3I21L14:1$:41
BGM:
P4CO229:.
;Nickel
130 :;,
mg/kgdry
1.5
0.013',.
1
*6010C
312011417,'45.,
BGM
P4CO229
$elenium
BRL '
mg/kg dry
0:77:
0.094 :
1
*.6010C
..
3/21/14 13:41
: BGM
P4CO229
Zinc •,;
58 ,. •.•
mW4 dry
3:9
0.026''„
1
'.*6010C .,:.'3/21114
13:41';BGM
P4CO229
.. ...
Tliis report s!16uld'not be reproduced, exce 'fin its entire ",'.W thbut the written:consent of Prism Laboratdries,'Inc.
P P tY...,.
"
: 449 Springbrbbk Road - P.O.: Box 240643 -:Charlotte,
NC 28224-0543
:.
Phone:,704/529-6364;7Toll Free Number: 1-800452976364 -
Fak: 704/525-0409. :.
Page
3 Of 177, ,

• • •
"1.
�'
. . Laboratory.
.: �' Report
... �,
.... .....
Fall -Service Analytidar&'.
�RI�M:
... �U160pATORIES, INC :....
Envlronmental,Solutions
• . ..... ..... • .
• • ; ; , 03/21/2014
• .
City of Statesville, NC ..:.:
Project: StaLime
Clierit: ample ID::,,.Fecal #4
Attn::Andy Smith::.,
;;;;: ::::. :::. ::. ::::.
:Prism Sample.ID: 40301:72-04
P.O. Box 1111
Prism Work Order: 4030172
Statesville, NC 28687
Sample,Matrix: Solid::
:...
Time Collec4ed: 03/10/14.11:10
Time Submitted: 03/ 0/14.:12:45
1
Parameter
MDL Dilution' Method Analysis Analyst Batch
i Result Units. Report:
Limit
Factor . ..::' : Date/Time',:: ID'
General Chemistry,Parameters
% Solids ' " :
"' : 66.5 % by . 0.100
0.100 9.. *SM2540 G 3114/14. 15:00 JAB . P4CO286" .
Weight
Microbiological Parameters
'
.Fecal Coliforms
A.
BRL .. MPN/g dry 0.3
1 •SM9221 E..-3/11/14 10:37. MES P.4CO223
Thi's report §hdy!d'not be rein:its entirety.the writtemconsent of Prism Laboratories,'Inc. "" "
P 'roduced, except tY... .
::.
..... 449 Springbrook Road - P.O.;B'ox 240543 =Charlotte, NC 28224-0543 : ; , , •
Phone.:,7041529-6364:-,Toll Free'Number: 1-800/529r6364 - Faz; 704/525-0409. :. Page 6 of 13

' Vie;.
•
Laboratory. Report
en�Fuli-Service
LidimV I;Environmental,Solutions
LABORATORIES, INC. ..
Analytidal: &'RIVI
..... •••. ••.•• •.•.
03/21/2014
•.•.• .. •. -•.•
City of Statesville, NC ....:
: ' 'Project: Stal-ime ,:
Client.Sample ID:.,:. Fecal #5.: '
Attn: Andy Smith::: ; •
"
Prism Sample.lD: 40301,72-05
P.O'. Box 1111
Prism Work Order: 4030172
Statesville, NC 28687
'Sample Matrix: Solid:'
Time Collected: 03/10/14 11:10
Time Submitted: 03/10/14.:12:45
Parameter
MDL Dilution' Method Analysis' Analyst Batch
Resulf Units, Report.
Limit
"' Factor ::' Date/Time .... ID
General Chemistry Parameters "' "'
% Solids '
66.9 . % by . 0.100 ..
0.100 1. *SM2540 G 3/14/14.15:00 JAB P4CO286
Weight
Microbiological Parameters ::' ""
Fecal Coliforms
"BRL MPN/g dry 0.3
1 *SM9221 E.. 3/11/14 10:37 MES P4CO223
'':This
a.
w.
report should'not be re' roduced, exce t In Its entire' Without the written consent of Prism Laboratories,Inc.
449 Springbrook•Road - P.o.;Box 240543 -;Charlotte, NC 28224-0543 ..
Phgne.:•704/529-6364:1Toll Free'Number: 1-800152976364 - Fak; 704/525-0409 Page 7 of 13

..
"
.. Laboratory: Report:
a,
Full -Service Analytical: &' . " "
�IO
ISM:
Environmental. Solutions
03/21/2014 ...
..-VI
-MTORIES ING :....
.
..... ..... ..... .....
....
..:. ...
Ci. of Statesville, NC
ty
.. ... .... ..:. ,.. .. ::: " .
• : • : , , Pro ect: Sta�ime
J.
:::.: : ...
Client;Sam le I0: .Fecal #6
P
Attn:, Andy Smith,:
;;;., ... ::. ::::.
:::. :Prism Sample,ID:40301.72-06
P.O. Box1111
Prism Work Order: 4030172
:... Statesville, NC 28687
Sample Matrix: Solid:
Time Collected:-03/10/14 11':10
:....
:b 0 Time Submitted' 03/1 /'1:4.:'f2:45
:Parameter
MDL Dilution Method Analysis' •Analyst Batch
: Result : Units. Report .
Limit
::' Factor . Date/Time ID
'General Ch'emistry.Parameters
%Solids: :
.'•' .'66.,1. .' •: %by ...... .0.100 .'
.0.100 .' 1. 'SM2540G 3M4/14.15:00 JAB. P4CO286 .
Weight
.
Microbiological Parameters
.Fecal Coliforms
' BRL .. 'MPN/g dry D.3
q.
1 'SM9221 E.. .3/11%14 10:37 MES P.4CO223
.. ..
;7 its report should'not be re' �yoduced, exce ,ti Wits entire' without the written oonsent of Pnsnl Laboratories 'Inc.
• , 449 Springbrook Road -P.O.: Box 240543 -;Charlotte, NC 28224-0543 '
Phone:. [phone]: -,Toll Free'Number:1-8001529-6364-Faxp7041525-0409• ;. Page 8 of S

a ora epo❑
oryFull-Service
I M :
Lao
®U00MTONIE$ING :
Analytical:&' "' 03/21/2014
•Environmental,Solutiona • • '
'City of Statesville, NC .
• Pro ect: StaLime ClientSample ID:... •Fecal #7
Attn:: Smith;:::.
y
Prism Samp, le ID: 4030172-07
P.O. Box 1111
Prism Work Order: 4030172
Statesville, NC 28687
Sample Matrix: Solid:: Time Collected: 03/10/14 11:10
q 'Time Submitted: 03/10/14 12 45
mitte .
Parameter
Result Units Report, MDL Dilution Method AnalysisAnalyst Batch
• • Limit ' Factor Date/Time ID
General Chemistry•Parameters
/o Solids
66.3 . % by .' 0.100 0.100 1 'SM2540 G 3/14/14 15:00 JAB. P4CO286
Weight '
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry 0.3 1 'SM9221 E 3/11/14 10:37 MES P4CO223
This report should not be reproduced, except in its entirety.,.% ithout the Written consent of Prism Laborat'ories,'Inc.
449 Springbrook,Road -P.O.: Box 240543 -:Charlotte, NC 28224-0543 • • , ,
Phone-.704/529-6364:-Toll Free Number: 1-800%529-6364 - Fax: [phone] Rage 9 Of 3

Level Report
.�
c�
Full -Service Analytical'&
3 / /14
Environmental:Sblutlons : •'
::
::.'
. ®LABORATORIES IN6
;Cityof Statesville, NC
Project:
StaLirh6, i '
.: :::.: Prism Work Order: 4030172':.:
Attn: An Smith
"
Time Submitted: 3/10/2014 12:45:OOPM
P.O.'Box.1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting;:
Spike Source %REC RPD
'Arralyte
" Result,
Limit
Units' :'
Level "Result %REC Limits:' RPD "'Limit Notes "
Batch:P4CO229 - 30606
Blank (P4CO229-BLK1)::
Prepared: 03/12/1:4 Analyzed: 03/21/14
... Arsenic:. ...
. BRL
... 0.26
mg/kg wet
...
:. ..
Cadmium
BRL
0.26
ni"/k wet
g g
" 0.
;Copper a
BRL•
0.51
mg/kg Wet
...
"'
Lead.
IJRL
0.26' .
mg/kg wet
Nickel
" BRL.
1.0
mg/kg wet
Selenium
BRL• '
0.51'
mg/kg wet•
' Zinc :: •
BRL
2.6
mg/kg wet
LCS (P4CO229-BS1),
Prepared: 03/12/14 Analyzed: 03/21/14
Arsenic;
"' 23.5
"" 0.25
'mg/kg wet
24.88 95 ' 80-120
Cadmium''.
" '23.6
0.25
mg/kgmg/kg wet
24.88' "'. 95 :80-120
:Copper
" 24.7 .
0.50
mg/kg wet.
24.88 99.. 80-120:.
Lead;
23.9
0.25
mg/kg wet
; ;24.88 96 80-120
Nickel
21,9.:
1.0
mg/kg wet::
"24.88 .... 88 : 80-120
Selenium
22.6.:
0.50
mg/kg wet.:
24.88 .91. 80-120 :.
Zinc
23.5
2.5
mg/kg wet
24.88
Batch:P4:CO262 - 7471 B
Blank (P4CO262-BLK1)
: "
Prepared: 03/13/14 'Analyzed: 03/14/14
;Mercury
BRL•
0:018
mg/kg wet.
LCS'(P4CO262-BS1)
Prepared:03/13/14 Analyzed:03/14/14: ;
Mercury
0.462
0.021
mg/kg wet:
0.4310 107 80-120
. ..
This report should not be re .roduced, exce .t in its entire without the v✓ritteh oonsent of Prism Laborat'orie's,'Inc.
P P P tY:,:: �.
: 449 Springbrook,Road - P.O; ;Box 240543 -:Charlotte, NC 28224-0543
Phone:.[phone]:-Toll Free'Number: 1-800/529-6364 - Fax: [phone]. : rage' 10 Of 173
,

•:: Level II "QC Report
®� c Full -Service Analytical $ ' • "' "' "' 3121/14
I,� M I : Environmental solutions "
'�ll1BOPATON1E51NG
:City of Statesville, NC Project: StaLime„ Prism Work Order; 4030172,;,
y ...
Attn: And Smith ::. Time Submitted: 3/10/2014 12:45;OOPM
P.O. Box,1111
Statesville, NC 28687
General ChemistryParameters = Quality Control'
Reporting: Spike : Source %REC RPD
I .—I pa—l4 0/RFC" I imitc .. ppr) .;I'imit Nntpc

• �
. • • ,
e Report
'Level
�r
®� RI:SM�..
�
Full-SerJica Anafyticel
& /14
3/21
.. M1
Envlronmentel;Solutlona
•��4ABa11aTOH1EQINC
""' •"'. .... ..'•. '•• .. .•
City of Statesville, NC '::;.
Project: StaLime. :::.: Prism;Work Order '4030172,
Attn: Andy Smith ; ; .
;;.•Time Submitted: 3/10/2014 12:45:OOPM
P.O. •Box,1111
Statesville, NC 28687:
Microbiological Parameters - Quality Control:::
Reporting : Spike Source %REC RPD
Arialyte
Result: Limit ' Units, • • • : Level • •Result %REC' Limits • RPD :Limit Notes
Batch M0223 - NO PREP
Blank (P4CO223-BLK1)'.
Prepared & Analy4ed:,03/11/14
Fecal Coliforms "'
" BRL ; ;'; 0.2 •MPN/g wet
Sample Extraction Data-' .
P;reP Method:'30508
:. ... .. • •
Lab Number ::..
Batch : i :.. Initial : i :..:.Final :.. Daterrime, : , .
4030172-01
P4CO229 ' .: 1'.97 g 50: mL ' 03/12/14 10:30:
40301:72-0.1..
P4CO229 :.. :. i. 1..9.7 g 50. mL 03/12114.1Q:30,
4030172-01
P4CO229 1'.97 g 50 mL ' 03/12/14 10:30
Prep:Metho& 74776
Lab.Number ..:. ...
Batch :. ... Initial.. ... Final..:. • • • Daterrime
4030172-01 ..
.. g .. . • • L : ; . 03/13/14 15; 05
P4CO262 0.57 50 m
Tlii's report should not be re' Yoduced, exce ;t: withwritten consent of Arisen LaboratorieInc.
P P in its entirety, : out the
.. .
449 Springbrogk,Road - P.O.;Box 240543 -;Charlotte, NC M . 4-0543
:.
:.' Phone:.[phone],-Toll Free'Numbee 1-800/529r6364 - Faic 7041525-0409, : , Page 12 of � 3

s vy
CR r CUSTODY RECORD
Full -Service Analytical & eI
.LaeaG:
.: uRE �raoPaR 69L
Environmental Solutions �Aoe _ O� — Doors m ro €sus p,;,,•., .;-,,,: ; _;,,,
ti a` ": ; ' aeow�rottie& INC. fleaeivetilON WE r:
. Project Name: PFif7PEFi;f',6iE$ER
-.P.O.449 Springbrook Road Box 240543 ^ Charlotte, NC20224-0543 UST Project:: es No
Short Hold Analysis- (Yes) .(No) u t (Yes) ( )
Phone: [phone] Fax: [phone] y . "ReceiVed,±W.,(THlhl:(
01L 1 II 111 IV)
Client s®m an Name �*Please ATTACH any project specific reporting (QC LE1E
sus gov;si At§:
provisions and/or QC Requirements "
Report To/Contact Name: Ard Sr-7:41i !/(]LATiLBS rectl
-� Invoice To:
Reporting Address:
j'.0. bog If 11 P fJP„EFi:�(?t<llAlf
Address:
' M
7•'•-`'YES •-.-`�,NOIVIA-
• a
%`l " •;
Phone: %0Y=175?-3r139' Fax es .(No): 70 - 979- b'9d5
Purchase Order No./Billing Reference
TO BE. FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE
FL -- --- - NC
EDD Type: PDF_ Excel _Other "Worlcin Da s" ❑ ti-9 Da s ❑Standard 10 da s Rush Work Must Be
9 y Y Y❑ Pr oved
O H
SC OTHER
Site Location Name: Fom r c et' e to ➢,u -T Samples received after 15:00 will be processed next business dayPr
Site Location Physical Address: 173 1( ��� "' �' � Turnaround time is based on business days, excluding Weekends and holidays.
Water ChloYlnated: YES_ NO
(SEE REVERSE FOR TERMS.& CONDITIONS REGARDING SERVICES
-
Sample Iced Upon COIlection: YES
NO .
ovRENDERED BY PRISM LABORATORIES, INC. TO CLIENT) :
_
TIME
MATRIX
:SAMPLE CONTAINER
ANALYSES
REQUESTED
PRISM
CLIENT ::
DATE
COLLECTED:
(SOIL,
:PRESERVA-
��� RE MARKS- :
LAB: ,
'TYPE :
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
C�
���✓
1D N O•
::.
HOURS
SLUDGE) :-.SEE
BELOW
dr��_���
rj� /�
n►� sao
�a �;�r
�..
of .
t
...:
p
A%r�r�
...
O
o:
..
gy�pp.
j
O
B led Sam o� �41. 'r Affiliation.
Sampler's -Signature P y (Print Name)
• •
Upon relinquishing, this Chain of Custody is your -authorization for Prism to proceed with the analyses as requested above: Any changes must be
submitted in writing to the -Prism Project Manager. There will be charges for any changes after analyses -have been Initialized.
shed B : SI nature Rec 'ved By: (Signs
✓fA Y (Sig ) ��•% el+ � t J t
I1 �rti�j ao'i Additional Comments:
[ 5it8'%{1YIV
Date
S�.e
t •D�partur
Rel' shed By: (Signature): Re d y. Signature)
.... r,
.. ..
Fieltl' Tech Feei;:::
Relinquished By: (Sig re) A ceiy orPrls aboratories By: Date-
v
•���'� `-
-. �'
(.
ti�
Mileages
-
Cam`
Method of Shipment: NOTE: AL SAMPLE -COOLERS SHOULD BE TAPED SHUT WITH, USTODY LS FOR TRANSPORTATION TO THE LABORATORY.: COO Group No:
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC 9NTIL REVVED AT THE LABORATORY. -
-
❑ Fed Ex ❑ UPS .:❑ Hand delivered ❑ Prism Field Service : ❑ Other
`,
NPDES :. UST: GROUNDWATER: DRINKING WATER: SOLID WASTE::: RCRA: CE(iCLA.:. LANDFILL
OTHER:
❑ NC ❑ SC :E] NC ❑ SC p NC - ❑ SC ❑ NC : ❑ SC ❑ NC .❑ SC.:.: : ❑ NC ❑ SC p NC ❑ SC ❑ NC ❑ SC:
❑.. -❑ SC
-*CONTAINER TYPE'CODES: A = Amber C Clear: G = Glass P = Plastic, TL = Teflon -Lined Cap VOA Volatile Organics Analysis (Zero Head Space)
:.

±4 Alialytical r3<
I
Envirdn mehtal. Soluti on s II L . .
LABORATORIES INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinldng Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L A-B Accredited Certificate No. L2307
ISONEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 03/24/2014
Prism Work Order. 4030430
Case Narrative
03/28/2014
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
I
Data Qualifiers Key Reference:
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 24OS43 - Charlotte, NC 29224-0543
Phone: [phone]'- Toll Free Number.1-80015294364 - Fax: [phone]

Sample Receipt Summary
ry i-. 1 Fu11=Service Anaiytical &
Environmental Solutions 03/28/2014
RIS
mc.
Prism Work Order. 4030430
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime
4030430-01 Solid 03/24/14 03/24/14
Samples were received at 24.9 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Ina
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number.1-8001529-6364 - Fax: [phone] Page'2 Of 7

Laboratory Report
Full -Service Analytical &
sm
Environmental Solutions
03/282014
`'0 �VIBORA70PIF,� INC ,
City of Statesville, NC Project: StaUme
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4030430-01
P.O. Box 1111
Prism Work Order: 4030430
Statesville, NC 28687 Sample Matrbt: Solid
Time Collected: 03/24/1413:20
Time Submitted: 03/24/1414:30
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Datemme
ID
General Chemistry Parameters
% Solids
68.6
% by
0.100
0.100
1
"SM2640 G
3126M4 15:36
JAB
P4C0513
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
•SM9221 E
325114 12:21
MES
P4C0522
Total Metals
Mercury
0.19
mgfkg dry
0.028
0.0094
1
•7471B
3125114 15:03
MEH
P4C0454
Arsenic
8.5
mgfkg dry
0.37
0.654
1
•6010C
3126114 14:26
BGM
13400462
Cadmium
BRL
mg/kg dry
0.37
0.0035
1
*6010C
326114 14:26
BGM
P4C0462
Copper
36
mglkg dry
0.73
0.0092
1
"6010C
3126114 14:26
BGM
P400462
Lead
9A
mgfkg dry
0.37
0.043
1
•6010C
' 3126114 14:26
BGM
P400462
Nickel
140
mglkg dry
1.5
0.012
1
"6014C
3126114 14:26
BGM
P4C0462
Selenium
4.5
mgfkg dry
0.73
0.089
1
'6014C
3126/14 14:26
BGM
P4C0462
Zinc
56
mgfkg dry
3.7
0.025
1
•6010C
3126114 14:26
BGM
P4C0462
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Ina
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

i`- p'\ Full -Service Analytical'&
/q'
9 S M ! I Environmental Solutions
weonarontE& IW4
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quafity Control
Level II QC Report
3128/14
Prism Work Order. 4030430
Time Submitted: 3/24/2014 2:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4CO464 - 7471 B
Blank (P4C0454-BLKI) Prepared: 03/24/14 Analyzed: 03/25/14
Mercury BRL 0.018 mg/k g wet
LCS (P4C4464-BSI) Prepared: 03/24/14 Analyzed: 03/25/14
Mercury 0.461 0.021 mg/kg wet 0.4386 105 80-120
Batch P4C0462 - 3050B
Blank (P4C0462-BLKI) Prepared: 03/25/14 Analyzed: 03/26/14
Arsenic BRL 0.25 mg/kg wet
Cadmium
BRL
0.25
mg/kgwet
Copper
BRL
0.49
mg/kg wet
Lead
BRL
0.25
nl9/k4 wet
Nickel
BRL
0.98
mg/kg wet
Selenium
BRL
0.49
mglkg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4C0462-BSI)
Prepared: 03/25/14 Analyzed: 03/26/14
Arsenic
22.9
0.25
mg/kg wet
25.25
91
80-120
Cadmium
22.8
0.25
mg/kg wet
25.25
90
80-120
Copper
25.4
0.51
mg/kg wet
25.25
101
80-120
Lead
23.1
0.25
mglkg wet
25.25
92
80-120
Nickel
23.3
1.0
mg/kg wet
25.25
92
80-120
Selenium
22.7
0.51
mg/kgwet
25.25
90
80-120
Zinc
22.8
2.5
mg/kg wet
25.25
90
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Ina
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-0001629-6384 - Fax: [phone] PS9e 4 Of 7

.4
•? S-' S M I Full -service Analytical &
Environmental Solutions
1xIA80MlOR1E� ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: StaLime
Reporting
Result Limit Units
Level II QC Report
3128114
Prism Work Order: 4030430
Time Submitted: 3/24/2014 2:30:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch MOM - NO PREP
Blank (P4C0593-BLK7) Prepared & Analyzed: 03/26/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Sprin®brook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001629-6364 - Fax: [phone] Page 5 of 7

S
'I M 4 i Full -Service Analytical &
Environmental Solutions
+�LABOPA'fOPfES INC
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II GEC Report
3Q8/14
Prism Work Order. 4030430
Time Submitted: 3/24/2014 2:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4CO622 - NO PREP
Blank (P4CO522-BLK1) Prepared & Analyzed: 03/25/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3060E
Lab Number Batch Initial Final Datefrboe
4030430-01 P4C0462 1.99 g 50 mL 03/25/14 10:30
Prep Method. 7471B
Lab Number Batch Initial Final UatelTime
4030430-01 P4C0454
0.63 g 50 mL 03/24/14 16:15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: "0015294364 - Fax: [phone]A409 P69e.6 0f 7.

CHAIN OF CUSTODY RECORDOil
:. Full -Service Analytical &
f' -• -- t,lutions PAGE OF QUOTE # TO ENSURE PROPER BILLING: ..
Environmental S — S arn`1e51NT44;iY ari:arrv. ai?:l:: ;`..,.•:... , ': ".-.; _yam., ; . _.
@T ''
Project Hanle: __,,,, ..-.._:.: (_s ., �.:-.... .... ..
o Road ^ Charlotte, NC 28217 ESftJAT}1)F
4d SPril,gbraok Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
Phone TQ41529-fi384 Fax: 704/°+85-0409 r
8 *Please ATTACH any project specific reporting (QC LEVEL 111111 IV) Rereived vt+t, H3�t hiUt Dr�IG r;Yr �?
Client Company Name: Ci�y o J�at'cSt�i�P QC Requirements c uST[�t91 SkALS(PdIA4 C? _
— provisions
and/or
A-rr .Simon i 11 yc� �l'fil ? S rec' i'v�lf ilT yEA sf'H ='?.:
Rep v Invoice To: -• "`` _,
Report To/Contact Marne:
Reporting Address' j� E3, 7x (I j 9
p g Address: %EMI';:rT(tertr�lr�_?�'T_ir� �sC7bseiyed:.a ,` °G/C6rrML
Phone:701- S37S43y3T Fax se (No).740i-SU- Sd55 purchase Order No./Billing Reference TO BE FILLER IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day U 2 Days U 3 Days O 4 Days 115 Days Certification: NELAC DoD FL NC
Work dust Be Sc OTFlER NIA
ERR Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
F0 -Fil C.-e-e d NIL,>> rp 14:00 will be next business day.
Site Location Name: u e Samples received after processed
Turnaroun d time Is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ N®_
Site Location Physical Address: fag r 1 wr,
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES_ NO
p p
VV e S,11l/ a e'V' C
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSIS REQUESTED
/ % /
/ '� / / / REMARKS
PRISM
CLIENT
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
SLUDGE}
'T�PE`TIVES
SEE I SIZE
��' /
1
/// // JHOURS
Io
d
W4-la f4 e
C
P
I
Z"
f
Sampler's Signature /� tom_ Sampled By (Print Name) �v Gk /'✓r rc°(!' Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted In writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
t)
rWWqu,sneu Y. I /fL11/{il I -J -a- -I--dA I I I . "I`
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE
� : e..�c3�
LI Fed Ex R UPS C1 Hand -delivered Prism Field Service ❑ Other
TER IWATER- E,CERCLA
® NC El SC Li NC® SC ❑ NC ❑ SC © NC ❑ SCEl ❑ SCI ❑ NC O SC I Q NC ® SC ❑ NC ®F SC I ❑O NC ❑ SC
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:
i Ri,^INJ1A1

NC Certification No. 402
SC Certification No. 99012
�t' �n
Full -Service. Analytical &
I..
NC Drinking Water Cart No. 37735
.�,S.�
Environmental Solutions
VA Certification No. 460211
oRnroF♦iis iNc
DoD ELAP: L-A-B Accredited Certificate No. L2307
IS011 EC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime
Lab Submittal Date: 04/21/2014
Prism Work Order: 4040411
Case Narrative
04/28/2014
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Rabbi A. Jones Reviewed By Robb! A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 70"29-8364 - Toll Free Number:1-8001529-6384 - Fax: [phone]

o. F.uH-Service AnaiyticaI &
RMY _I. Enbironmental Solutions
Ri
Sample Receipt Summary
04/28/2014
Prism Work Order: 4040411
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Stalime
4040411-01 Solid 04/21/14 04121/14
Samples were received in good condition at 1.5 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - PA: Box 240843 - Charlotte, NC 28224-0843
Phone: [phone] - Toll Free Number: l-8001529-6384 -Fax: [phone]

4 i �/AAFull-Service Analytical &
I S� V I I Environmental Solutions
LA0
0
R11TOR1E5,' ING
Laboratory Report
04/28/2014
City of Statesville, NC Project: StaLime Client Sample ID: Stalime
Attn: Andy Smith Prism Sample ID: 4040411-01
P.O. Box 1111 Prism Work Order: 4040411
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/21/14 13:57
Time Submitted: 04/2111415:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
%. Solids
68.0
% by
0.100
0.100
1
'SM2640 G
4124114 15:00
JAB
P4D0512
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
'SM9221 E
4122/14 13:05
MES
P4D0496
Total Metals
Mercury
0.24
mgfkg dry
0.029
0.0099
1
*7471Is
4122114 17:36
MEH
P400442
Arsenic
BRL
mg/kg dry
3.7
0.54
10
*6010C
4/25114 19:54
BGM
P4D0485
Cadmium
BRL
mg/kg dry
3.7
0.036
10
'6010C
4125/14 19:54
BGM
P4D0485
Copper
41
mg/kg dry
7A
0.094
10
'6010C
4125114 19:54
BGM
KD0485
Lead
19
mglkg dry
3.7
0.44
10
`6010C
4125114 19:64
BGM
P4D0485
Nickel
170
mglkg dry
15
0.12
10
•6010C
4125114 19:54
BGM
P4D0485
Selenium
BRL
mg/kg dry
7.4
0.90
10
'6010C
4/25114 19:54
BGM
P4D0485
Zinc
71
mglkg dry
37
0.25
10
"6010C
4126114 19:54
BGM
P4D0485
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-050
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 3 of 7

l ; v Full -Service Analytical &
i s m I Environmental Solutions
W�AWSATOMEB. ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P4D0442 - 7471 B
Project: StaLime
Reporting
Result Limit Units
Level II QC Report
4/28/14
Prism Work Order: 4040411
Time Submitted: 4/21/2014 3:45:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P4D0442-BLK1)
Prepared: 04/21/14 Analyzed: 04/22/14
Mercury
BRL
0.019
mg/kg wet
LCS (P4D0442-BS1)
Prepared: 04/21/14 Analyzed: 04/22/14
Mercury
0.445
0.019
mg/kg wet
0.3906 114 80-120
Batch P4D0485 - 3050B
Blank (P4DO485-BLK1)
Prepared: 04/24/14 Analyzed: 04/25/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.49
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.99
mg/kg wet
Selenium
BRL
0.49
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4D0485-BSI)
Prepared: 04/24/14 Analyzed: 04/25/14
Arsenic
0.985
mg/L
1.000 99 80-120
Cadmium
0.982
mg/L
1.000 98 M120
Copper
1.04
mg/L
1.000 104 80-120
Lead
0.964
mg/L
1.000 96 80-120
Nickel
0.966
mg/L
1.000 97 80-120
Selenium
0.995
mg/L
1.000 100 80-120
Zinc
0.969
mg/L
1.000 97 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 Of 7

I SM I Full -Service Analytical &
Environmental Solutions
1PNBOR/TORIES INS.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
4/28/14
Prism Work Order: 4040411
Time Submitted: 4/21/2014 3:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits • RPD Limit Notes
Batch P4DO512 - NO PREP
Blank (P4D0512-BLK7) Prepared & Analyzed: 04/24/14
% Sorlds 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: 704I52"409 Page 5 Of 7

1+1' �Z Full
-Service Analytical &
P; ISM I Environmental Solutions
r�lA© RMORIEr, INC
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
4/28/14
Prism Work Order: 4040411
Time Submitted: 4/21/2014 3:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41130496 - NO PREP
Blank (P4D0496-BLIC1) Prepared $ Analyzed: 04/22tl4
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number Batch Initial Final Daternme
4040411-01 P4D0485 1.98 g 50 mL 04/24/14 9:55
Prep Method: 7471B
Lab Number Batch Initial Final Dateirme
4040411-01 P4130442
0.6 g
50 mL 04/21/14 14:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543.
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Sage 6 of.7

- ':'h:': _ _. _.___.... _�.t__`._J—J. ., ✓J_u_�_u�._u.u...t»✓._....—_...i.J_.._i.�___..
__J. __.._. .•a__JJ____"' _. _::...: .�._..__._....•...,...f1•..i.n.✓✓....._,_��✓_..__..�.•..._.i•✓•�—
CHAIN F CUSTODY REDORD
a.ii�......ei.....�✓....i....•._...�...-.........r_.i.�.<......-•....
�_.�.. ..•. �.......
-,
`: r, ©
yl Full -Service Analytical &
SEnvironmental Solutions
i
PAGE_ or _ QUOTE 9 To ENSURE PROPER BILLING:
-Samples iNTAGT upon an ivai'�
IA
YES NO N/A
,"
n�
• O;
90RATORIES, INC.
Springbroak Road a Charlotte, NC 28217
Project Name:449
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
Re6e61 e6 °ON 1NI t ICE7 -,
PROPER PR>fSftV/1ilVS Indwa(ed�
p
Phone [phone] Fax: [phone]
� y J �'
*Please ATTACH any project specific reporting (QC LEVEL 1 II ill 1V)
-itece!vcl WITHIN HDI_ltaG,_T.[MES?..,., :.':
7QDY IN ;: `•°:,'
.,
Y ",;, � ' :
a
Client Company Name: y 0 a �t E cSi°�
p y
provisions and/or QC Requirements
.:CU SEALS :"
Report To/Contact Name: A br v n,a
Invoice To:
VOLATIi ES rcd uVlOU7 HEPgoPFCE?
_
Reporting Address: P 0. 8,ox ICI (
Address:
'.Ub ser[eci
: �.—TO 1:G6ri
Phone: 70 `>i� � � �'' 3�►3 "� Fax es (No): 704 7$' `��� �
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD
FL NC
EDD Type: PDF_Excel Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Pre -Approved
Sc OTHER
N/A
_
Site Location Name: Fd 4 r 14, G r eI P
Physical AddrJess: kSc ii Farrar
Samples received after 14:00 will be processed next.business day.
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
Site Location
• / �` g � (°
(SEE REVERSE FOR TERMS &CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) -Sample
Sle Iced Upon Collection: YES_
PSM
NO
CLIENT DATE
SAMPLE DESCRIPTION I COLLECTED
;LL �
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRISM
COLLECTED
(SOIL,
PRESERVA-"a�D
` REMARKS
LAB
MILITARY
WATER OR
*TYPE
NO
SIZE
TIVES
v /
ID NO.
HOURS
SLUDGE)
SEE BELOW
_
y
MIA
As
14
N
Z 14
y / % /
Sampler's Signature sl�ca [r 4Z-1 u e �i a Sampled By (Print Name) ✓ Gl,LI1 c k Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed "with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be chalilges for any changes ft analyses have been initialized.
Relin ' hed By: Slgnafur / O Receiv
Al
7�By: (Signat re) V Date Military
Relin a py: (Signativre) Re ived By: (Sigrta r) D e
Rellnquis
By (Sign Q' re)
y -
{
{'
Method &Shiprrient: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST
H CU ODY SEALS FOR TRANSPORTATION TO THE LABORATORY.
C UN L RECEIVED AT THE LABORATORY.,
COC Group No.
1!y
❑ Fed Ex ❑ UPS ❑ Hand -delivered ❑ Prism Field Service ❑ Olher
NPDES: UST: GROUNDWATER: ( DRINKING WATER: I SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
❑NC❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC
❑NC ❑SC I❑SC 10NC ❑SC 0NC ❑SC
'
I
❑ ❑ ❑ ❑
0NC❑SIC ANC
I ® j
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass
P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:

Apt toS n�� Eull=Service Analytical. &
M 1. I • Environmental Solutions
LABORATORIES,"INO. •
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012 Case Narrative
NC Drinldng Water Cert No. 37735 05/15/2014
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/I EC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime (Qtrly, Biweekly, 60Day 7 Fecal)
Lab Submittal Date: 05/05/2014
Prism work Order: 4050093
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers areflagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifliers Key Reference:
M Matrix spike outside of the control limits.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to, the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-9364 - Fax: [phone]

g.�a..
Sample Receipt Summary
PDr',.
a
I V 1
N 1_ 'I,
Full-Servlce Analytical &
EnWonmental Solutions
05/15/2014
UfeOaAiORIES ING
Prism Work Order: 4050093
Client Sample ID
Lab Sample ID
Matrix
Date Sampled Date Received
Stai-ime
4050093-01
Solid
05/05/14
05/05/14
Fecal #2
4050093-02
Solid
05/05/14
05/05/14
Fecal #3
4050093-03
Solid
05/05/14
05/05/14
Fecal #4
4050093-04
Solid
05/05/14
05/05/14
Fecal #5
4050093-05
Solid
05/05/14
05/05/14
Fecal #6
4050093-06
Solid
05/05/14
05/05/14
Fecal #7
4050093-07
Solid
05/05/14
05/05/14
Samples were received at 33.4 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Chadotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

6l ar�. n 'Full -Service Analytical
R.i S.MM I Environmental Solutions
U GQHAVRIE. IHG ­ - - .
City of Statesville, NC
Attn: Andy Smith
P.O, Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/15/2014
Client Sample ID: StaLime
Prism Sample ID: 4050093-01
Prism Work Order: 4050093
Time Collected: 05/05/14 10:40
Time Submitted: 05/05/14 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datefrime ID
General Chemistry Parameters
Plant Available Nitrogen
560
mg1kg '
160
13
2
*Calculation
5n4/14 8:36
CLB
[CALC]
% Solids
82.6
% by
0.100
0.100
1
*SM2640 G
S/ln4 16:16
JAB
P4E0128
Weight
Nitrate(Nitrite as N
14
mglkg dry
6.1
0.67
1
*SM4500-NO3 F
517n4 11:35
CLB
P4E0109
Phosphorus Total
2200
mg1kg dry
120
26
40
*SM4500-P F
5112114 9:25
CLB
P4E0171
Total ICeldahi Nitrogen
2200
mglkg dry
610
61
2
*351.2
SM4/14 8:36
CLB
P4E0217
Ammonia as N
34
mg/kg
5.0
1.2
1
*SM4500-NH3 G 518h14 10:31
CLB
P4E0134
Microbiological Parameters
Fecal Colifonns
BRL
MPN/g dry
0.2
1
*SM9221 E
516114 10:35
MES
P4E0176
Total Metals
Mercury
0.24
mglkg dry
0.022
0.0076
1
*7471B
618114 13:68
MEH
P4E0141
Arsenic
6.0
mglkg dry
0.30
0.044
1
*6010C
517n4 17:41
BGM
P4E0112
Cadmium
BRL
mg/kg dry
0.30
0.0029
1
*6010C
517/14 17:41
BGM
P4E0112
Copper
23
mg1kg dry
0.60
0.0076
1
*6010C
517114 17:41
BGM
P4E0112
Lead
6.2
mglkg dry
0.30
0.036
1
*6010C
517114 17:41
BGM
P4E0112
Nickel
89
mglkg dry
1.2
0.0097
1
*6010C
517n4 17:41
BGM
P4E0112
Potassium
5100
mgikg dry
300
19
20
*6010C
sn3/14 21:22
BGM
P4E0112
Selenium
2.1
mg1kg dry
0.60
0.072
1
*6010C
5171114 17:41
BGM
P4E0112
Sodium
610
mglkg dry
15
0.14
1
*6010C
517H4 17:41
BGM
P4E0112
Zinc
41
mglkg dry
3.0
0.020
1
*6010C
517P14 17:41
BGM
P4E0112
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax, 70415254409 IRA-

� Full -Service Analytical &
ISR R I S I V/pe , I Environmental Solutions
�IABQPATOPIE3, ING
Laboratory Report
05/15/2014
City of Statesville, NC Project: StaLime (Qtrly, Biweekly, Client Sample ID: Fecal #2
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4050093-02
P.O. Box 1111 Prism Work Order: 4050093
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/05/14 10:40
Time Submitted: 05/05/14 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datelfime ID
General Chemistry Parameters
% Solids 90.0 % by 0.100 0.100 1 *SM2540 G 517M4 15:16 JAB ' P4E0128
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 *SM9221 E 5/6114 10:35 MES P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-050
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Pog8 4� Of � 4: ` .'

`., a�. FullrService Analytical'&
f .S M . I Environmental Solutions
V I DQHMME$ IHG
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaUme (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/15/2014
Client Sample ID: Fecal #3
Prism Sample ID: 4050093-03
Prism Work Order: 4050093
Time Collected: 05/05/14 10:40
Time Submitted: 05/05/14 15:00
Parameter Result
Units
Report
MDL Diiution
Method Analysis Analyst
Batch
Limit
Factor
Datelrime
ID
General Chemistry Parameters
% Solids 80.6
% by
0.100
0.100 1
'SM2540 G 517H4 16:16 JAB
P4E0128
Weight
Microbiological Parameters
Fecal Colifonns BRL
MPN/g dry
0.2
1
`SM9221 E 5/6/14 10:35 MES
P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box; 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

SA =` !Laboratory Report
s
�'� �? ^ � n� Full -Service Analytical &
S I V I I Environmental Solutions 05/15/2014
LAaOFATOp1E3, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #4
Prism Sample ID: 4050093-04
Prism Work Order: 4050093
Time Collected: 05/05/14 10:40
Time Submitted: 05105/1415:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 82.4
% by
0.100
0.100 1
"SM2540 G WM 4 16:16 JAB
P4E0128
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 5/6114 10:35 MES
P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 6 Of '� 4

Full -Service Analytical 8
ISM I Environmental Solutions
U1eOflATOflIE3, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/15/2014
Client Sample ID: Fecal #5
Prism Sample ID: 4050093-05
Prism Work Order: 4050093
Time Collected: 05/05/1410:40
Time Submitted: 05/05/1415:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datefrime ID
General Chemistry Parameters
%. Solids 86.4 %.by 0.100 0.100 1 "SM2640 G san4 15:15 JAB P4E0128
Weight
Microbiological Parameters
Fecal Colifonns BRL MPN/g dry 0.2 1 'SM9221 E 516114 10:35 MES P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

Full -Service Analytical &
Environmental, Solutions
�✓'�1A90PATOPIE3, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtdy, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/15/2014
Client Sample ID: Fecal #6
Prism Sample ID: 4050093-06
Prism Work Order: 4050093
Time Collected: 05/05/14 10:40
Time Submitted: 05/05/1415:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DatefTime ID
General Chemistry Parameters
%Solids 86.0 % by 0.100 0.100 1 •SM2640 G 517114 15:15 JAB P4E0128
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 •SM9221 E 5/6114 10:35 MES P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-050
Phone: [phone] - Toll Free Number:1-800/529-6364 - Fax: [phone]

Laboratory Report
�: I �-. Full -Service An &
AN-264M.ATORTE4%
I S M' Environniental Solutions 05/15/2014
ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #7
Prism Sample ID: 4050093-07
Prism Work Order: 4050093 .
Time Collected: 05/05/14 10:40
Time Submitted: 05/05/14 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 78.6
% by
0.100
0.100 1
"SM2640 G 517114 15:15 JAB
P4E0128
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 5/6/14 10:35 MES
P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 -Fax: 704152"409 'PagG.9 Of

Arti, qAFull-Service Analytical &
�W\O I S V , I Environmental Solutions
- 7-RCRAMFIIE$ INC
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch MEW 12 - 3050E
Level II QC Report
5/15/14
Project: Stal-ime (Qtdy, Biweekly, 60Day Prism Work Order: 4050093
7 Fecal) , Time Submitted: 5/5/2014 3:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P4E0112-131LK1)
Prepared & Analyzed: 05/07/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
13
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Sodium
BRL
13
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (KE0112-BSII)
Prepared &Analyzed: 05/07/14
Arsenic
24.6
0.25
mg/kg wet
25.25 97
80-120
Cadmium
24.4
0.25
mg/kg wet
25.25 97
80-120
Copper
25.8
0.51
mg/kg wet
25.25 102
80-120
Lead
24.2
0.25
mg/kg wet
25.25 96
80-120
Nickel
24.1
1.0
mg/kg wet
25.25 96
80-120
Potassium
514
13
mg/kg wet
505.1 102
80-120
Selenium
24.8
0.51
mg/kg wet
25.25 98
BD-120
Sodium
506
13
mg/kg wet
505.1 100
80-120
Zinc
24.1
2.5
mg/kg wet
25.25 96
80-120
Batch MEOW - 7471 B
Blank (124E0141-BLK1) Prepared & Analyzed: 05/08/14
Mercury BRL 0.020 mg/kg wet
LCS (KE0141-113S7) Prepared & Analyzed: 05/08/14
Mercury 0.421 0.020 mg/kg wet 0.4098 103 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
' 10 Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: 704152"409 Page:

/2CgEPff
�+n �
'+ Sowoftlm INQ
City of Statesville, NC
Attn: Andy Smith
P.O, Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
General Chemistry Parameters - Quality Control
Project: Stal-ime (Qtdy, Biweekly, 60Day
7 Fecal)
Level II QC Report
5/15/14
Prism Work Order: 4050093
Time Submitted: 5/5/2014 3:00:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4EO109 - NO PREP
Blank (NE0109-BLK7) Prepared & Analyzed: 05/07/14
Nitrate/Nraite as N BRL 5.0 mgikg wet
LCS (KE0109-BSI) Prepared &Analyzed: 05/07/14
Nitrate/Nitrite as N 51.0 5.0 mglkg wet 50.00 102 80-120
Matrix Spike (P4E0109-MS1) Source: 4060093-01 Prepared & Analyzed: 05/07/14
Nitrate/Nraite as N 78.5 6.1 mg/kg dry 60.53 14.3 106 80-120
Matrix Spike Dup (KE0109-MSD1) Source: 4060093-01 Prepared & Analyzed: 05/07/14
Nitrate/Nitrite as N 76.3 6.1 mglkg dry 60.53 14.3 102 80-120 3 20
Batch P4EO128 - NO PREP
Blank (NE0128-BLK7) Prepared & Analyzed: 05/07/14
% Solids 100 0.100 % by Weight
Duplicate (P4E0128-DUP2) Source: 4050093-07 Prepared & Analyzed: 05/07/14
% Solids 82.8 0.100 % by Weight 78.5 5 20
Batch P4EO134 - NO PREP
Blank (P4E0134-BLK7) Prepared & Analyzed: 05/08/14
Ammonia as N BRL 5.0 mg/kg
LCS (P4E0134-BSI) Prepared & Analyzed: 05/08/14
Ammonia as N 128 5.0 mg/kg 125.0 102 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Chadotte, NC 28224-0643
Phone* 7041629-6364-Toll Free Number: 1-8001529-6364 - Fax: [phone]

Level II QC Report
(� Full=Service Analytical & 5/15/14
Erb '"-'� Environmental Solutions
y + I BORATOHMS, INC
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime (Qtdy, Biweekly, 60Day
7 Fecal)
Prism Work Order: 4050093
Time Submitted: 5/5/2014 3:00:OOPM
Analyte
Reporting
Result Limit
Units
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch MENU - NO PREP
Matrix Spike (P4E0134-MS1)
Source: 4050093-01
Prepared & Analyzed: 05/08/14
Ammonia as N
Matrix Spike Dup (P4E0134-MSD1)
210 5.0 mg/kg
Source: 4060093-01
125.0 34.5 140 80-120 M
Prepared & Analyzed: 05/08/14
Ammonia as N
Batch MOM - SM4500-PB6
209 5.0
mg/kg
125.0 34.5 139 80-120 0.5 20 M
Blank (P4EO171-BLKI)
Prepared: 05/09/14 Analyzed: 05/12/14
Phosphorus -Total
LCS (P4E0171-BSI)
BRL 2.5
mg/kg wet
Prepared: 05/09/14 Analyzed: 05/12/14
Phosphorus -Total
102 2.5
mg/kg wet
100.0 102 90-110
Batch W0217 - 351.2
Blank (P4E0217-BLK1) Prepared: 05/13/14 Analyzed: 05/14/14
Total Neldahl Nitrogen BRL 25 mg/kg wet
LCS (NE0217-BSI) Prepared: 05/13/14 Analyzed: 05/14/14
Total Kieklahl Nitrogen 5040 1000 mg/kg wet 5000 101 90-110
Matrix Spike (P4E0217-MS1) Source: 4050093-01 Prepared: 05/13/14 Analyzed: 05/14/14
Total Kjeldahl Nitrogen 9650 3000 mg/kg dry 6053 2190 123 90-110 MI
Matrix Spike Dup (P4E0217-MSD1) Source: 4060093-01 Prepared: 05/13/14 Analyzed: 05/14/14
Total Kleldahl Nitrogen 8570 3000 mglkg dry 6053 2190 105 90-110 12 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 -Fax: [phone] rage, 1 2 :of 14

Level 11 QC Report
ilFull=Servlce,Analytical & 5115/14
i7! IS:M I Environmental Solutions
L SOFASOMM IN4 '
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Project: StaUme (Qtdy, BiWeekly, 60Day
7 Fecal)
Prism Work Order: 4050093
Time Submitted: 5/5/2014 3:00:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch NE0176 - NO PREP
Blank (NE0176-BLK1) Prepared & Analyzed: 05/06/14
Fecal Colifonns BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Daterrime
4060093-01 P4E0217 0.05 g 25 mL 05/13/14 10:00
Prep Method: SM4500-PBS
Lab Number Batch Initial Final Daternme
4050093-01 P4E0171 1 g 50 mL 05/09/14 14:11
Prep Method: 3050B
Lab Number Batch Initial Final Daternme
4050093-01 P4E0112 2:03 g 50 mL 05/07/14 10:15
4050093-01 P4E0112 2.03 a 50 mL 05107/14 10:15
Prep Method: 7471B
Lab Number Batch Initial Final Daternme
4050093-01 P4E0141 0.65 g 50 mL 05/08/14 9:55
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

r CHA I N OF CUSTODY RECORD
a
S M I Full -Service Analytical &
Environmental Solutions
r3
a
PAGE OF QUOTE # TO ENSURE PROPER BILLING:
^,anL.."
PaliBOAkTOR1ES, INC. - - - - �^7—• . �.'
449 Springbrook Road • Charlotte, NC 28217 Project Name:
J� ;eIvea QN Vv r ICF�
Phone [phone] • Fan: 7041525-0409 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) PJ30FCFt h'RESERVATJVES mdlcated? t . ✓ at
/` -
Client Company Name: C + opt �++l�� *Please ATTACH any project specific reporting (QC LEVEL 111111 IV) Reeeiveil.tNITN1NHOGDfNGTIMGS.? :`" " ' ✓ : ` `- '`'` a
P Y o. ? ::'-s':
,. provisions and/or QC Requirements - ; GUSTOD. SEALS INTACT?.- _
t :.
Report TolContact Name: i)+v +a++i ti I T UOGATILES recdW1OUTHEADSPACE7
Reporting Address: I . 4 • -13oX f
Address:
Vaee.�sv r )1 g MC
� .`fEMP::�Therm ILit�r,2 T_-_
Phone;7o-1- 87S-3113T Fax es (No):'70`f Y?,?' 9,155
purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Date ❑ 1 Day O 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC -DoD FL
NC
EDD Type: PDF_Excel_Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days Q P e hh Work Must Be
a
Site Location Name: fr+ur ;, l r �u Loma Y I�
Sc OTHER N/A
Samples received after 14:00 will be processed next business day.
;�
Site Location Physical Address: 693'BC,If (-a r IS .
Turnaround time is based on business days, excluding weekends and holidays. ' Water Chlorinated: YES_ NO_
d
✓+ % fe-
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES NO
CLIENT
DATE
TIME
COLLECTED
MATRIX
SAMPLE CONTAINER
PRESERVA-
ANALYSIS REQUESTED
PRISM
SAMPLE DESCRIPTION
COLLECTED
MILITARY
(SOIL,
WATER OR
TIVES
t✓
��y REMARKS
LAB
*TYPE
HOURS
SLUDGE)
SEE BBELOW
NO.
SIZE
itv
4
ID NO.
(�•g P //`
V ,rl OY Y•.$'ml
c�yq
�p�� O !
/
9�l tJ r0
V
tl
�'l p�
�� 1 ..% N9
q`
b� �
�Jt @/ f, /J /�
P]c+ v��Y P i> �!• I as `P` In nA ti
_ 0 1
S,/a Z"
S I P
Sampler's Signature A 1��r?�.r Sampled By (Print Name)/J
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed
submitted in writing to the Prism Project Manager. There will be charges for any cha
Relin shed By: (Signatu ,1 �� Received By: Si lure)
a�. _ . "<
M1W=_©
9
L V <`/ C. Affiliation
the as requested above. Any changes must be
?fter analyses have been initialized.
-IY IIS of
- r V SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINI! gC NTIL RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑ UPS ❑ Hand•delivlered ❑ Prism Field Service ❑ Odier tJ. v v 9
NPDES
NDWA
SOLID
CERCLA
O❑ NC ❑ SC
O NC ❑ SC 1 ❑❑ NOCU ❑ SCTER. I ❑❑DRINKING
NC I❑ SCATER. I ❑❑ NC El ❑❑ NC ❑ SC I ❑❑ NC ❑ SC NC LANDFILL
❑ SC ❑ NC ❑ SC
J 1 ❑-.
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:
Site Arrival Time:
Sii��eparture Time:"
.Field Tech Fee:
Mileage:

1 a 5�n 'Full=Service'Analytical:&
I Y 1. . EnVironmental Solutions
LABORATORIES, INa
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISOlIEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 05/19/2014
Prism Work Order: 4050464
Case Narrative
05/28/2014
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Rabbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number,1-8001529-6364 - Fax.- 7041525-0409

i rH Full -Service Analytical &
�' I Environmental Solutions
IA60RATORIES. ING
Sample Receipt Summary
05/28/2014
Prism Work Order: 4050464
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Stal-ime
4050464-01 Solid 05/19/14 05/19/14
Samples were received at 25.4 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 2' Qf]

%t � �n 'Full-S,ervide Analytical & Laboratory Report
`I V 1 I Environmental solutions 05/28/2014
City of Statesville, NC Project: StaLime Client Sample ID: StaLime
Attn: Andy Smith Prism Sample ID: 4050464-01
P.O. Box 1111 Prism Work Order: 4050464
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/19/14 00:00
Time Submitted: 05/19/1416:55
Parameter Result Units Report MDL DilutionMethod Analysis Analyst Batch
Limit Factor Daterrime ID
General Chemistry Parameters
% Solids 78.8 % by 0.100 0.100 1 *SM2540 G 5123114 15:32 JAB P4E0494
Weight
Microbiological Parameters
Fecal Collforms BRL MPN/g dry 0.3 1 *SM9221 E 5/20/14 10:00 MES P4E0456
Total Metals
Mercury
0.17
mg&g dry
0.025
0.0084
1
*7471B
5122114 19:00
MEH
P4E0425
Arsenic
6.2
mglirg dry
0.32
0.047
1
*6010C
5123114 16:16
BGM
P4E0446
Cadmium
BRL
mg/kg dry
0.32
0.0031
1
*6010C
5/23/14 16:16
BGM
P4E0446
Copper
31
mglkg dry
0.65
0.9082
1
*6010C
6123114 16:16
BGM
P4E0446
Lead'
8.2
mglkg dry
0.32
0.038
1
*6010C
5123114 16:16
BGM
P4E0446
Nickel
120
mglkg dry
1.3
0.011
1
*6010C
5123M4 16:16
BGM
P4E0446
Selenium
3.1
mgllrg dry
0.65
0.078
1
*6010C
5123114 16:16
BGM
P4E0446
Zinc
66
mgikg dry
3.2
0.022
1
*6010C
5123114 16:16
BGM
P4E0446
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O.. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529.6304 - Fax: [phone]

Level II QC Report
a,;: i "' Full-Semice'Analytical & 5/28/14
a6r�'I� I M 1 Environmental Solutions
&iAWFIAT6pIE4 INC
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaUme
Prism Work Order: 4050464
Time Submitted: 5/19/2014 4:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4EO425 - 7471 B
Blank (124E0425-BLK7) Prepared: 05/21/14 Analyzed: 05/22/14
Mercury BRL 0.019 mg/kg wet
LCS (P4E0425-BS1) Prepared: 05/21/14 Analyzed: 05/22/14
Mercury 0.485 0.021 mg/kg wet 0.4386 111 80-120
Batch P4EO446 - 3050B
Blank (134E0446-BLK7) Prepared: 05/22/14 Analyzed: 05/23/14
Arsenic BRL 0.24 mg/kg wet
Cadmium
BRL
0.24
mg/kg wet
Copper
BRL
0.49
mg/kg wet
Lead
BRL
0.24
mg/kg wet
BH
Nickel
BRL -
0.98
mg/kg wet
Selenium
BRL
0.49
mg/kg wet
Zinc
BRL
2.4
mg/kg wet
LCS (P4E0446-BSI)
Prepared: 05/22/14 Analyzed: 05/23/14
Arsenic
24.1
0.25
mg/kg wet
25.00 96 80-120
Cadmium
24.0
0.25
mg/kg wet
25.00 96 80-120
Copper
25.2
0.50
mg/kg wet
25.00 101 80-120
Lead
24.0
0.25
mg/kg wet
25.00 96 80-120
Nickel
23.8
1.0
mg/kg wet
25.00 95 W120
Selenium
23.8
0.50
mg/kg wet
25.00 95 80-120
Zinc
23.9
2.5
mg/kg wet
25.00 96 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

✓; ' Level II QC Report
A l Full -Service Analytical &
Environmental Solutions 5/28/14
LABORATORIES INC
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime
Prism Work Order: 4050464
Time Submitted: 5/19/2014 4:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch ME0494 - NO PREP
Blank (ME0494-BLK1) Prepared & Analyzed: 05/23/14
% Solids 100 0.100 % by Weight
Blank (P4E0494-BLK2) Prepared & Analyzed: 05/23/14
% Solids 100 0.100 % by Weight
Blank (P4E0494-BLK3) Prepared & Analyzed: 05/23/14
% Solids 100 0.100 % by Weight
Blank (P4E0494-BLK4) Prepared & Analyzed: 05/23/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001629-6364 - Fax: [phone]

ry <:
�P! ta, \�'"� �� //�� Full -Service Analytical 8
R' V � Y � . Envi[onmental Solutions
LM1BBPM1TOPIEB, MG "
City of Statesville, NG Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
5/28/14
Prism Work Order: 4050464
Time Submitted: 5/19/2014 4:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4E0456 - NO PREP
Blank (114E0456-13LK1) Prepared & Analyzed: 05/20/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrrme
4050464-01
P4E0446
1.96 g
50 mL
05/22/14 10:45
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Daternme
4050464-01
P4E0425
0.61 g
50 mL
05/21/14 13:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrock Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: 704162SM409 13

r;yA`
v. sr Full -Service Analytical &
�r a ; -- I Environmental Solutions
�i ,eG
+'� .�`' i t i�'4�LARORATORIES, iNG,
449 Springbrook Road - Charlotte, NC 28217
Phone [phone] - Fax: [phone]
Client Company Name: C:4y 0-P Vla&5111 lie
Report To/Contact Name: Q-Ay S, rdh
Reporting Address: P.0, 110 d .®
s ell G:.$'6''rl®I c
CH{i IN Cf0F CUIST®®Y EC®R
PAG OF QUOTE 11 TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II Ill IV)
provisions and/or QC Requirements
Invoice To:
Address:
1=. 'a�i1.a r.x 2 'rA rUS{ErONL �� wF, t.= a
Phone:%4 318' Mg Fax es (No): "Id'y• 8179- 8,495 Purchase Order NoJBllling Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DoD
FL NC
EDD Type: PDF_Eyxcel_II Other C� "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ P e h Work dust Be SC OTHER
&1 ww r
NSA
Site Location Name: I-{t - P7 Ct`� r
Samples received after 14:00 will be processed next business day.
Site Location Physical Address:, 03 Bet( 6L...., J{'— Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
/ y
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) p p
NO
NO -
TIME MATRIX
SAMPLE CONTAINER ANALYSIS REQUESTED
PRISM
CLIENT DATE COLLECTED (SOIL,
PRESERVA- �y REMARKS LAB
"TYPE TIVES
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR
NO. SIZE
ID NO.
HOURS SLUDGE)
SEE BELOW
(N rlit
rp
)4ASL 51i 6-3
1/
1
+ O `
d1�a..aaLLt
�As
4+
Pb
VIA
r
V
ZH
Sampler's Signature/r / . Sampled By (Print Name) Ct1 o°r Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
a
submitted in writing to the Prism Project Manager. There will be
rges for any changes after analyses have been initialized.
Relin hed By: Signag) Re '
d B : (Signature) Date Military/Hours Additional Comments:
'.Sits Airivai Trrie
Reim d y: ( nat re)
v d By; (Signat Date
. Sltc_
S�
f
Field Tech Fee:
Re hed By: (Sig re)
For Prism Lab rles By: Date; /
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CU TODY S S FOR TRANSPORTATION TO THE LABORATORY, COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UN 11 RECEI D AT THE LABORATORY.
y s� a 6J
❑ Fed Ex El UPS ❑ Hand -delivered Prism Field Servlce ❑ Other
NPDES: I UST: Gf NDWATER: DRINKING WATER: SOLID WASTE: RC CERCLA LANDFILL OTHER:
❑NC❑SC ❑NC ❑SC I ❑NC El SC ❑NC El SC
I ❑NC ❑SC ❑NC❑SC ❑NC ❑SC ❑NC El ❑NC ❑SC
❑ ❑ ❑ ❑
❑ ❑ ❑ __ ❑ ❑ --
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

NC Certification No. 402 Case Narrative
L.'' • 5): SC Certification No. 99012
Full -Service Analytical & NC Drinking Water Cert No. 3773506/11/2014
ism Environmental Solutions VA Certification No.460211
LABORATORIES, INO. DOD ELAP: L-A-B Accredited Certificate No. L2307
IS011EC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 06/02/2014
Statesville, NC 28687 Prism Work Order: 4060041
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
A Diluted due to interference from high Calcium concentration.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone., 7041629-6364 - Toll Free Number:1-8001529-6364 - Fax: [phone] Page `1 of 8

Full -Service Analytical &
ISM I Environmental Solutions
LABORATORIES. INC.
Sample Receipt Summary
06/11 /2014
Prism Work Order: 4060041
Client Sample ID Lab Sample ID Matrix Date Sampled Data Received
Sta Lime
4060041-01 Solid 06/02/14 06/02/14
Samples were received in good condition at 1.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Sprin®brook Road - P.O. Box 240543 - Chadotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001629-6364 - Fax: [phone] Page 2 Of'8

-:
�I >+. Full -Service Analytical & Laboratory Report
P� Ism Environmental Solutions 06/11/2014
i�UIUOMTORIE$ ING
City of Statesville, NC Project: StaLime Client Sample ID: Sta Lime
Attn: Andy Smith Prism Sample ID: 4060041-01
P.O. Box 1111 Prism Work Order: 4060041
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/02/14 10:15
Time Submitted: 06/02/1415:40
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Daterrime
ID
General Chemistry Parameters
% Solids 86.3
% by
0.100
0.100 1
*SM2640 G 614114 15:38 JAB
P4F0083
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
*SM9221 E 613114 10:05 MES
P4F0080
Total Metals
Mercury
0.14
mg/kii dry
0.022
0.0073
1
Arsenic
3.2 A
mgfkg dry
2.9
0.42
10
Cadmium
BRLA
mg/kg dry
2.9
0.027
10
Copper
36 A
mglkg dry
5.7
0.072
10
Lead
25 A
mg/kg dry
2.9
0.33
10
Nickel
160 A
mglkg dry
11
0.093
10
Selenium
BRLA
mg/kg dry
5.7
0.69
10
Zinc
58 A
mglkg dry
29
0.20
10
*7471B
614M414:09
MEH
P41F0067
*6010C
61911413:05
BGM
P4F0033
*6010C
619/14 13:05
BGM
P4F0033
*6010C
61911413:05
BGM
P4F0033
*6010C
W9/1413:05
BGM
P4F0033
*6010C
619M413:05
BGM
P4F0033
*6010C
6/9/14 13:05
BGM
P4F0033
*6010C
619M413:06
BGM
P4F0033
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 3 of 8

{ I S fl � I Full -Service Analytical &
,� 1 Environmental Solutions
LABOPATORIE$ ING
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
6111/14
Prism Work Order: 4060041
Time Submitted: 6/2/2014 3:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PV0033 - 3050B
Blank (P4F0033-BLI(1)
Prepared & Analyzed: 06/03/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0,25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4F0033-BS1)
Prepared & Analyzed: 06/03/14
Arsenic
24.0
0.25
mg/kg wet
25.38 95
M120
Cadmium
24.0
0.25
mg/kg wet
25.38 94
80-120
Copper
24.7
0.51
mg/kg wet
25.38 97
80-120
Lead
23.4
0.25
mg/kg wet
25.38 92
80-120
Nickel
23.7
1.0
mg/kg wet
25.38 93
80-120
Selenium
23.9
0.51
mg/kg wet
25.38 94
80-120
Zinc
23.7
2.5
mg/kg wet
25.38 93
80-120
Matrix Spike(P4F0033-MS1)
Source: 4060041 -01
Prepared:06103114 Analyzed:06/09/14
Arsenic
30.5
2.9
mg/kg dry
29.26
3.20
93
75-125
Cadmium
24.9
2.9
mg/kg dry
29.26
0.125
85
75-125
Copper
62.7
5.9
mg/kg dry
29.26
35.2
r94
75-125
Lead
49.7
2.9
mg/kg dry
29.26
25.3
84
75-125
Nickel
187
12
mg/kg dry
29.26
162
85
75-125
Selenium
18.9
5.9
mg/kg dry
29.26
BRL
64
75-125
MI
Zinc
86.8
29
mg/kg dry
29.26
57.8
99
75-125
Matrix Spike Dup (P4F0033-MSD1)
Source: 4060041-01
Prepared:
06/03/14 Analyzed: 06/09/14
Arsenic
29.1
2.9
mg/kg dry
29.41
3.20
88
75-125
5
20
Cadmium
24.5
2.9
mg/kg dry
29.41
0.125
83
75-125
2
20
Copper
62.3
5.9
mg/kg dry
29.41
35.2
92
75-125
0.7
20
Lead
48.4
2.9
mg/kg dry
29.41
25.3
79
75-125
3
20
Nickel
185
12
mg/kg dry
29.41
162
77
75-125
1
20
Selenium
20.3
5.9
mg/kg dry
29.41
BRL
69
75-125
7
20 MI
Zinc
99.5
29
mg/kg dry
29.41
57.8
142
75-125
14
20 MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] `,Pads, 4 Of _8'-

ia`
Full-Service Analytical &
ISM I Environmental Solutions
?�R,M/lll�/ligiINk'17LABORATORIES; INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Anslyte
Batch P4F0033 - 3060B
Project: Stal-ime
Level II QC Report
6/11/14
Prism Work Order: 4060041
Time Submitted: 6/2/2014 3:40:00PM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Post Spike (P4F0033-PSI)
Source: 4060041-01
Prepared & Analyzed: 06/03/14
Arsenic
0.926
mg/L
1.000 0.112 81
80-120
MI
Cadmium
0.538
mg/L
1.000 0.00439 53
80-120
MI
Copper
1.60
mg/L
1.000 1.23 37
80-120
MI
Lead
1.03
mg/L
1.000 0.887 14
80-120
MI
Nickel
3.81
mg/L
1.000 5.69 NR
80.120
MI
Selenium
0.874
mg/L
1.000 -0.264 114
80-120
MI
Zinc
2.29
mg/L
1.000 2.02 26
80-120
MI
Batch NF0067 - 7471 B
Blank (P4F0067-BLKI) Prepared & Analyzed: 06/04/14
Mercury BRL 0.020 mg/kg wet
LCS (P4F0067-BSI) Prepared & Analyzed: 06/04/14
Mercury 0.413 0.019 mg/kg wet 0.3906 106 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 5 'of 8

MEa, �/ A' Full-6ervlce%Analytical &
R, c, I �� i.Y 1 I Environmental Solutions
1LABORNOfl1E$MG'"
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: StaUme
Level II QC Report
6/11114
Prism Work Order. 4060041
Time Submitted: 6/2/2014 3:40:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4F0083 - NO PREP
Blank (124120083-BLK1) Prepared & Analyzed: 06/04/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

�,.
.P €'� 9 to 1�'1 n Full- Se"16e,Analytiosl &
R 1V'•'I Environmental Solutions
MOUBORATORIE$ 1Na
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Reporting
Result Limit Units
Level II QC Report
6/11/14
Prism Work Order: 4060041
Time Submitted: 6/2/2014 3:40:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch PV0080 - NO PREP
Blank (124F0080-12111-K1) Prepared & Analyzed: 06/03/14
Fecal Colifonns BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Daterfime
4060041-01
P4F0033
2.03 g
50 mL
06/03/14 9:15
Prep Method: 7471B
Lab Number
Batch
Initial
Final
DatelTme
4060041-01
P4F0067
0.64 g
50 mL
06/04/14 10:10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]

CHAIN OF CUSTODY RECORD � , . ' �
m
..,._.:.:.
k '> ISM
Full -Service Analytical &
Solutions
I
PAGE_ OP Q DOTE # TO ENSURE PROPER BILLINGe
r: .:::.'1.' .t >....^. •i•.r :..
� �"'�
a'rrivat? '
y
_
�
, ,,�, :; :
Environmental
_
les INTAGT u on
_
LAaUHATURIES INC.
.Re_CSIVG'd:Qii:W.E�'i�[=7.;.'.-�Sr,':. `.:r.;:.
-
..-=::.'
aD
449 Sprirrgbroak Road • Charlotte, NC 28217
•Fax: 7d41525 2821
Project Name:
US7 Pro ect' Yes NO
Short Hold Analysis: (Yes) (No) i . ( ) ( )
......:. ..:..... .... ....
`PROP:EP:FRrSERV,�TIVES:indicated
::.: _
"eGQivsd;WITHIt
' ^✓_ : `-
`" ° `:_
v
Phone 7d41529-G364
Company Name: Y a a �$ vs
*Please ATTACH an project specific reporting (QC LEVEL I It III IV)
Pleas A y P 1 p
l<HtLL71NG.•TIMES?";.:::..:
CU3it?D r SFAku INTACT? ar
' .
i
_t.._.,
c0
aL
Client
provisions and/or QC Requirements
reccl.W(OUT HEADSPAGE7 -
Report To/Contact Name: _A n 4� J�nv :'�)-+ -
Invoice To
�/OLAF ALES
PRGPER,;CONTAINERS used?::-
Reporting OA 11I I
p 9 Address:
Address:
3ENIP;,Ttierm lCl_ �%�✓_ .. , C)gsarved:
1 Corr. f
S¢�tt�c:54'r a711C iJC
Phone:%Jy-97 $-3'I.3 $ Fax es (No):70- 7Y' �U
purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING
PERSONNEL
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC 'DOD
FL NC
EDD Type: PLDF_Excel _Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days CI Rueshh Work edust Be
SC OTHER
NIA
Site Location Name: Fo ., I, Ci—ec-& (4.,W i
Be I-Ar. R1.
Samples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO—
Site Location Physical Address: 493 -it ,
/ s
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES_
NO_
%�CaCS✓+�lC ��
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
MATRIX
(SOIL,
WATER OR
SAMPLE CONTAINER
TYPE NO. SIZE
PRESERVA-
TIVES
ANALYSIS REQUESTED
` ,
ycs
� � REMARKS
PRISM
LAB
ID NO.
HOURS
SLUDGE)
SEE BELOW
'4 IR
.7 4A iir�/+7 '� rs "'eR�/�f $� � �S i%2 �'��. ._ • l�K
�b
Sampler's Signature /r�� G / .rr ec% Sampled By (Print Name) PA ZdV rl't- Affiliation , 0
Upon relinquishing, this Chain of Custody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relln J shed By- (Signat/u//r/e / Rece ve y: nolgpr} D h� Military Hours Additional Comments:
,2--t-e I rs,ib
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC.CXbL RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑ UPS ❑ Hand -delivered qMnsm Field Service ❑ Other
❑ NC ❑ SC ❑ C ❑ SC ❑ NC ❑ SCTER: O NNC U SCRI KING ATER: i SOLID N El WASTE: ❑ NC ❑ SC I LI NC L❑ SC I U NC LANDFILL❑ SC I O❑ NC ❑ SC
❑ ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
ORIGINAL

NC Certification No. 402 Case Narrative
'K2
SC Certification No. 99012
Pr!� Full -Service Analytical &
R' I S'M. Environmerital Solutioris
NC Drinking Water Cart No. 37735 06/23/2014
VA Certification No. 460211
1
usoFlAroFaieS iria ' .
DoD ELAP: L-A B Accredited Certificate No. L2307
ISO/I EC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 06/16/2014
Statesville, NC 28687 Prism Work Order: 4060328
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data,qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM (LABORATORIES, INC.
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the.reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-060
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

g ,, ,V
,� A /p' Full -Service Analytical &
'. . I S 1 i/ 1 I Environmental Solutions
`tA80FATOAIE; ING '
Sample Receipt Summary
06/23/2014
Prism Work Order: 4060328
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
StaLime
4060328-01 Solid 06/16/14 06/16/14
Samples were received at 29.0 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: 704I529-6364 - Toll Free Number:1-800/629-6364 - Fax: 704/62"409 PBge 2 Of

A.0i
'',IFull-Service Analytical & Laboratory Report
i Environmental Solutions 06/23/2014
";; I WRATORIM INC
City of Statesville, NC Project: StaLime Client Sample ID: StaLime
Attn: Andy Smith Prism Sample ID: 4060328-01
P.O. Box 1111 Prism Work Order: 4060328
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/16/14 11:33
Time Submitted: 06/16/14 15:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
69.0
% by
0.100
0.100
1
*SM2640 G
6M 8M4 16:46
MJO
P4F0334
Weight
Microbiological Parameters
Fecal Colifonns
BRL
MPN/g dry
0.3
1
*SM9221 E
6117114 11:25
JHB
P4F0340
Total Metals
Mercury
0.14
mglk g dry
0.029
0.0098
1
*7471B
6M7114 16:48
MEH
P4F0299
Arsenic
4.1
mglkg dry
3.6
0.62
10
*6010C
6/19M4 16:40
BGM
PV0303
Cadmium
BRL
mg/kg dry
3.6
0.034
10
*6010C
6119114 16:40
BGM
P4F0303
Copper
36
mg/kg dry
7.1
0.090
10
*6010C
6M9M4 16:40
BGM
P4F0303
Lead
14
mg/kg dry
3.6
0.42
10
*6010C
6M9M4 16:40
BGM
P4F0303
Nickel
200
mg/kg dry
14
0.12
10
*6010C
6M9M4 16:40
BGM
P4F0303
Selenium
BRL
mg/kg dry
7.1
0.86
10
*6010C
6119114 16:40
BGM
P4F0303
Zinc
68
mg/kg dry
36
0.24
10
*6010C
6M9M4 16:40
BGM
P4F0303
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 3 Of

Fu11=Service Analoci al &
I ontJ• E I environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Anaiyte
Batch P4F0299 - 7471 B
Project: Stal-ime
Reporting
Result Limit Units
Level 11 QC Report
6/23/14
Prism Work Order. 4060328
Time Submitted: 6/16/2014 3:25:00PM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (1241=0299-BLK1) Prepared & Analyzed: 06/17/14
Mercury BRL 0.021 mg/kg wet
LCS (P4F0299-BSI) Prepared &Analyzed: 06/17/14
Mercury 0.354 0.020 mg/kg wet 0.4167 85 80-120
Matrix Spike (P4F0299-MS1) Source: 4060328-01 Prepared & Analyzed: 06/17/14
Mercury 0.680 0.031 mg/kg dry 0.6470 0.143 83 80-120
Matrix Spike Dup (P4F0299-MSD1) Source: 4060328-01 Prepared & Analyzed: O6/1,7f14
Mercury 0.657 0.031 mg/kg dry 0.6356 0.143 81 80-120 3 20
Batch P41`0303 - 3060B
Blank (P4F0303-BLK1)
Prepared & Analyzed: 06/17/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mgi kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4F0303-BS1)
Prepared & Analyzed: 06/17/14
Arsenic
22.4
0.25
mg/kg wet
25.13 89
80-120
Cadmium
22.2
0.25
mg/kg wet
25.13 89
80-120
Copper
23.9
0.50
mg/kg wet
25.13 95
80-120
Lead
22.2
0.25
mg/kg wet
25.13 88
80-120
Nickel
22.2
1.0
mg/kg wet
25.13 88
80-120
Selenium
22.3
0.50
mg/kg wet
25.13 89
80-120
Zinc
22.6
2.5
mg/kg wet
25.13 90
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Bork 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

.:>iqIsFuniService Analytical 8
'� Environmental Solutions
LA80RATORIES; IN4
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level 11 QC Report
6123/14
Prism Work Order: 4060328
Time Submitted: 6/16/2014 3:25:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41F0303 - 3050B
Matrix Spike (P4F0303-MS1)
Source: 4060328-01
Prepared: 06/17/14 Analyzed: 06/19/14
Arsenic
38.9
3.7
mgllkgg dry
36.78
4.08
95
75-125
Cadmium
31.6
3.7
mgllkg dry
36.78
0.110
86
75-125
Copper
67.8
7.4
mg/kg dry
36.78
34.7
90
75-125
Lead
46.4
3.7
mg/kg dry
36.78
14.5
87
75-125
Nickel
236
15
mg/kg dry
36.78
197
107
75-125
Selenium
28.6
7.4
mg/kg dry
36.78
BRL
78
75-125
Zinc
99.8
37
mg/kg dry
36.78
67.9
87
75-125
Matrix Spike Dup (P4F0303-MSD1)
Source: 4060328-01
Prepared: 06/17/14 Analyzed: 06/19/14
Arsenic
36.2
3.5
mg/kg dry
35.35
4.08
91
75-125
7
20
Cadmium
29.7
3.5
mg/kg dry
35.35
0.110
84
75-125
6
20
Copper
66.6
7.1
mg/kg dry
35.35
34.7
90
75-125
2
20
Lead
43.7
3.5
mg/kg dry
35.35
14.5
83
75-125
6
20
Nickel
213
14
mg/kg dry
35.35
197
46
75-125
10
20
MC
Selenium
23.4
7.1
mg/kg dry
35.35
BRL
66
75-125
20
20
MI
Zinc
103
35
mg/kg dry
35.35
67.9
100
75-125
3
20
Post Spike (P4F0303-PS1)
Source: 4060328-01
Prepared:
06/17/14 Analyzed: 06/18/14
Arsenic
0.834
mg/L
1.000
0.115
72
80-120
MI
Cadmium
0.492
mg/L
1.000
0.00310
49
80-120
MI
Copper
1.42
mg/L
1.000
0.977
44
B0-120
MI
Lead
0.715
mg/L
1.000
0.407
31
80-120
MI
Nickel
3.75
mg/L
1.000
5.53
NR
80-120
MC
Selenium
0.773
mg/L
1.000
-0.191
96
80-120
Zinc
2.18
mg/L .
1.000
1.91
27
80-120
MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-800I529-6364 - Fax: [phone] Page 5, of 8- , .

Level II QC Report
{ e
Fu k' 1l-S6ry1ca:Ana1yBca1&
, .LS , I Errviro6mental Solutions - 6/23/14
i✓VIBOMTOBIES, Mc:
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime
Prism Work Order: 4060328
Time Submitted: 6/16/2014 3:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MF0334 - NO PREP
Blank (P4F0334-BLK1) Prepared &Analyzed: 06/18/14
% Solids 99.9 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 24OS43 - Charlotte, NC 28224-OS43
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

hy
/1
Full -Service Analytical &
pCr1 I Environmental Solutions
ISM
a IABOWOMM INC
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Batch P4F0340 - NO PREP
Project: StaLime
Level II QC Report
6123114
Prism Work Order. 4060328
Time Submitted: 6/16/2014 3:25:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P4170340-BLI II) Prepared & Analyzed: 06/17/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Initial Final Daterrime
4060328-01 P4F0303 2.04 g 50 mL 06/17/14 10:10
Prep Method: 7471E
Lab Number Batch Initial Final Daterrrme
4060328-01 P41`0299 0.6 g 50 mL 06/17/14 13:56
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] P89e.7 Of $ .

CHAW OF CUSTODY RECORD
?; :,. I Full -Service Analytical &
:YES`:
'N/A.. 00
,,,, - „: -::: Environmental $LIILItio raS
� �i.
PAGE OF QUOTE S TO ENSURE PROPER BILLING:
;.Simples;,"jAE�[�upan-arridal, .. _
:.., ;,:
''. t
`.. :.=:.�... '...---`—•
-RMO 4
LABORATORIES, INC.
Project Name:
- _- - ,--:." ,;:
^'Res elvclCON':VFT ICE? '.:'-'
: s...":.
:.::, o :
'.
449 S rin brook Road • Ci';arlotte, NC 26217
P 9
Phone [phone] •Fax: 704/525 Ca409
Short hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
PROPER RRESERVATIVFS andaca4ed�
I'ecelvedlryiTHiPl,i (gLRiNG 1`IM>~S?":
- r
—
.r /
C .
Client Company Name: , e
"Please ATTACH any project specific reporting (QC LEVEL 111 111 IV)
per,
provisions and/or QC Requirements
Report To/Contact Name: An9v 5na:4h
—�
Invoice To:
::VQLATILESrec'(1yt!(OUTHEA' SPADE?
Reporting Address: 0. doh /(!I'
:PR.OPER:CONT�IINF?S used?.--*-..
Ufa4 Si s iie A/C
Address:
'TEtiiP Ttierrii IDi t J ?eived::�1."'
f Corr: C
Phone: [phone]' Fax es (No): Yd% V- *781- 5� ";I S
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD
FL NC
EDD Type: PDFrExcel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Pre -Approved
Site Location Name: r1z i •-- i Cj-cen kLOW rP Samples received after 14:00 will be processed next business day.
Site Location Physical Address.12?3 ;Bell FAr n, R• Turnaround time is based on business days, excluding weekends and holidays,
�+ (SEE REVERSE FOR TERMS ✓?, CONDITIONS REGARDING SERVICES
J�.c✓�l�c° RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
SC OTHER
Water Chlorinated: YES_ NO_,
Sample Iced Upon Collection: YES
N/A
NO
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSIS REQUESTED
raj
i REMARKS
�y� ��
PRISM
LAB
ID NO.
*TYPE
SEE BELOW
NO.
SIZE
S rz .�: `
- d -!�✓
11 3
3
N� SDI?�
4
�` - a
— 0 3
c�
_
et
19
io.J3
i
P
— -
...
1
4
�V�
%J
Sampler's Signature/ .Ifeg o Sampled By (Print Name) Aaz X,1vr,'ck Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
` : n w
I,�- T, b .T =t
Relincy'shed By: (S nature� , y Re fed By: (Signature) to �/{
j'f a ' r 1
RelinqiAI d By: (Signatu e) r Re d By: (Signature Date
l//W—,-V . 1
Reli quis ed By: (Sign ture) Received r Pdsm Lab toes By: Date
a
M Is ours Additional Comments:
Site Arrival Time: .
Site Departure Time:
Fie)d.T6'a"k Fee:; '
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT w Ij'CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST : UNTIL RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑ UPS ❑ Hand -delivered trlsm Field Service ❑Other
NPDES: UST: GR UNDWATER: DRINKING WATER: SOLID WASTE: RCRA: RCLA LANDFILL
OTHER:
°
❑NC❑SCI ®NC ❑SC L3 C ❑SC QNC ❑SC
�CE
LlNC ❑SC LINC❑SC ®NC ❑SC ®NC ❑SCI
ANC ❑SC
n
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
r^pt-.'s pn a a a n I

af:2v
p I' Full -Service Analytical, &
Environmental Solutions
)AMEMMVLABORATORIES, 1NC
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 06/30/2014
Prism Work Order: 4070017
Case Narrative
07/10/2014
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 23224-OW
Phone: [phone] - Toll Free Number:1-800/529-6394 - Fax: [phone]A409

PT Fu11-Service Analytical &
�P I.I S}I V:�_' I. En'virorimental Solutions
' IABORATORIES�INC '
Sample Receipt Summary
07/10/2014
Prism Work Order: 4070017
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Sta-Lime
4070017-01
Solid
06/30/14
06/30/14
Sta-Lime
4070017-02
Solid
06/30/14
06/30/14
Sta-Lime
4070017-03
Solid
06/30/14
06/30/14
Sta-Lime
4070017-04
Solid
06/30/14
06/30/14
Sta-Lime
4070017-05
Solid
06/30/14
06/30/14
Sta-Lime
4070017-06
Solid
06/30/14
06/30/14
Sta-Lime
4070017-07
Solid
06/30/14
06/30/14
Samples were received at 30.6 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
-Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: 704152&0409

Laboratory Report
Full -SecwAnelytical&
rWEnvironmental
�n�
'I
V
1. Solutions
07/10/2014
V' LABOHATOf11E$,' Wa -
City of Statesville, NC Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4070017-01
P.O. Box 1111
Prism Work Order: 4070017
Statesville, NC 28687 Sample Matrix: Solid
Time Collected: 06/30/14 14:34
Time Submitted: 06/30/1416:40
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Datelrime
ID
General Chemistry Parameters
%© Solids
95.3
%, by
0.100
0.100
1
*SM2540 G
712114 14:30
JAB
P4G0043
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN1100
1
1
*SM9221 E
7M/14 13:19
JHB
P4G0052
mL
Total Metals
Mercury
0.38
mglkg dry
0.021
0.0035
1
*7471B
718M4 15:47
MEH
P4G0088
Arsenic
1.3
mglkg dry
0.78
0.11
3
*6010C
7n0/14 12:02
MEH
P4130051
Cadmium
BRL
mg/kg dry
0.78
0.0074
3
*6010C
7110114 12:02
MEH
P4G0051
Copper
38
mg►kg dry
1.6
0.020
3
*6010C
7110114 12:02
MEH
P4G0051
Lead
10
mglkg dry
0.78
0.091
3
*6010C
7110114 12:02
MEH
P400051
Nickel
110
mglkg dry
3.1
0.025
3
*6010C
7110114 12:02
MEH
P4G0051
Selenium
BRL
mg/kg dry
1.6
0.19
3
*6010C
7/10/14 12:02
MEH
P4G0051
Zinc
82
mgllrg dry
7.8
0.063
3
*6010C
7n0114 12:02
MEH
P4G0051
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
"ll Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

` Laboratory Report
' cD�3-. _l 3, Full=Service Analytical &
�'Ir [»:sue ISM I Environmental Solutions 07/10/2014
'J 1A90gATOg1E5, IN4 '
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4070017-02
P.O. Box 1111 Prism Work Order: 4070017
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/30/14 14:34
Time Submitted: 06/30/1416:40
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
%Solids 86.9
%. by
0.100
0.100 1
'SM2640 G 712R4 14:30 JAB
P4G0043
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/100
1
1
`SM9221 E 7/1/14 13:19 JHB
P4G0052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte. NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]age:4:

Laboratory Report
��P®^ Fui[rService Analytical'&
R I .S M I Envirohme64al Solutions 07/10/2014
ii�l UGHATQRIIA ING . .
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4070017-03
P.O. Box 1111 Prism Work Order: 4070017
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/30/14 14:34
Time Submitted: 06/30/1416:40
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 92.3
% by
0.100
0.100 1 'SM2640 G 712H 4 14:30 JAB
KG0043
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN1100
1
1 •SM9221 E 711114 13:19 JHB
124130052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone]

Laboratory Report
6S? sg.
R ISM
1
�/ A1
d,.
Fu11-Service_ Analytical &
I Environmental Solutions
07/10/2014
UEOgATOflIE$ING ..
City of Statesville, NC Project: Stal-ime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4070017-04
P.O. Box 1111
Prism Work Order: 4070017
Statesville, NC 28687 Sample Matrix: Solid
Time Collected: 06/30/14 14:34
Time Submitted: 06/30/1416:40
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
%Solids 90.2
%by
0.100
0.100 1 'SM2540G 712M414:30 JAB
P4G0043
Weight
Microbiological Parameters
Fecal Colllforms BRL
MPN/100
1
1 •SM9221 E 711114 13:19 JHB
P4G0052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529.6364 - Fax: [phone]

I Full -Service Analytical & Laboratory Report
r r�
Environmental Solutions 07/10/2014
�lA6pgpTOflIE$ ING
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4070017-05
P.O. Box 1111 Prism Work Order: 4070017
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/30/14 14:34
Time Submitted: 06/30/1416:40
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Datefrime
ID
General Chemistry Parameters
% Solids 88.3
% by
0.100
0.100 1
"SM2540 G 712114 14:30 JAB
134130043
Weight
Microbiological Parameters
Fecal Colifonns BRL
MPN/100
1
1
`SM9221 E 711114 13:19 JHB
P4G0052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: 704152"409 Page,7 =

Laboratory Report
r? Full -Service Analytical &
f
Environmental Solutions 07/10/2014
t3`IABOMTOetES, ING
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4070017-06
P.O. Box 1111 Prism Work Order: 4070017
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/30/14 14:34
Time Submitted: 06/30/1416:40
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Daterrime
ID
General Chemistry Parameters
%Solids 92.9
%by
0.100
0.100 1
"SM2640G 712M414:30 JAB
P4G0043
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN1100
1
1
'SM9221 E 711114 13:19 JHB
P4G0052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001629-6364 - Fax: [phone] P60 8. Of I

.y'
A Full -Service Analytical &
P` I S M I Environmental Solutions
.�rJ'uaognrogits, �rvc
Laboratory Report
07/10/2014
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4070017-07
P.O. Box 1111 Prism Work Order: 4070017
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/30/14 14:34
Time Submitted: 06/30/1416:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 87.6 % by 0.100 0.100 1 'SM2640 G 712114 14,30 JAB P4G0043
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/100 1 1 'SM9221 E 7/1/14 13:19 JHB P4G0052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 9 of 14

A�6! PRISM
"' Full -Service Analytical &
R I S M I Environmental Solutions
V7L190NATOFIE9. INc.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P4GO051 - 3050B
Project: StaLime
Reporting
Result Limit Units
Level II QC Report
7/10114
Prism Work Order: 4070017
Time Submitted: 6/30/2014 4:40:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P4G0051-BLK1)
Prepared: 07/03/14 Analyzed: 07/08/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
BH
LCS (P4G0051-BS1)
Prepared: 07/03/14 Analyzed: 07/08/14
Arsenic
23.5
0.25
mg/kg wet
25.00 94 80-120
Cadmium
23.8
0.25
mg/kg wet
25.00 95 80-120
Copper
24.5
0.50
mg/kg wet
25.00 98 80-120
Lead
23.1
0.25
mg/kg wet
25.00 92 80-120
Nickel
23.5
1.0
mg/kg wet
25.00 94 80-120
Selenium
23.7
0.60
mg/kg wet
25.00 95 80-120
Zinc
24.0
2.5
mg/kg wet
25.00 96 80-120
Duplicate (P4G0051-DUP1)
Source: 4070017-01
Prepared: 07/03/14 Analyzed: 07/10/14
Arsenic
1.41
0.78
mg/kg dry
1.34
5
200
Cadmium
0.236
0.78
mg/kg dry
0.193
20
200
Copper
40.8
1.6
mg/kg dry
38.3
6
200
Lead
10.3
0.78
mg/kg dry
10.1
2
200
Nickel
105
3.1
mg/kg dry
108
3
200
Selenium
BRL
1.6
mg/kg dry
BRL
200
Zinc
90.8
7.8
mg/kg dry
81.8
10
200
Matrix Spike (P4G0051-MS1)
Source:4070017-01
Prepared:07103/14 Analyzed:07/10/14
Arsenic
25.2
0.79
mg/kg dry
26.23 1.34 91 75-125
Cadmium
19.7
0.79
mg/kg dry
26.23 0.193 74 75-125
MI
Copper
60.8
1.6
mg/kg dry
26.23 38.3 86 75-125
Lead
28.9
0.79
mg/kg dry
26.23 10.1 72 75-125
MI
Nickel
123
3.1
mg/kg dry
26.23 108 55 75-125
MI
Selenium
16.1
1.6
mg/kg dry
26.23 BRL 61 75-125
MI
Zinc
102
7.9
mg/kg dry
26.23 81.8 77 75.125
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0643
Phone: [phone]-Toll Free Number: 1-8001529-6364-Fax:[phone] Page 10 Of 14

_: a Full-Serolce Analytical &
/` E$E I S Environmental Solutions
n Y P'IABOPATOPIE4, INC.
City of Statesville, NC
Attn: Andy Smith
P.O, Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
7/10/14
Prism Work Order: 4070017
Time Submitted: 6/30/2014 4:40:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MOON - 7471 B
Blank (124130088-BLKI) Prepared: 07/07/14 Analyzed: 07/08/14
Mercury BRL 0.021 mg/kg wet
LCS (134130088-191SI) Prepared: 07/07114 Analyzed: 07/08/14
Mercury 0.479 0.020 mglkg wet 0.4167 115 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Sprin®brook Road - P.O. Box 240543 - Charlotte, NC 28224-060
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] PBgeJf Of

Full-Servlce Analytical &
.0 w I SM I Environmental Solutions
LORATORIM INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
7110114
Prism Work Order: 4070017
Time Submitted: 6/30/2014 4:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4GO043 - NO PREP
Blank (P4G0043-BLK1) Prepared & Analyzed: 07/02/14
% Solids 99.8 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: 704/52"409 Page -12 _of `� 4

7 DR
Full Service Analytical &
Environmental Solutions
LAOOn.TORMA Wa
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O, Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
7/10114
Prism Work Order: 4070017
Time Submitted: 6/30/2014 4:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41130052 - NO PREP
Blank (P4G0052-BLK1) Prepared & Analyzed: 07/01/14
Fecal Coliforms BRL 1 MPN/100 mL
Sample Extraction Data
Prep Method: 3050E
Lab Number Batch Initial Final DateTme
4070017-01 P4130051 2.02 g 50 mL 07/03/14 8:45
Prep Method: 7471B
Lab Number Batch Initial
4070017-01
P4G0088
0.59 g
Final Daternme
50 mL 07/07/14 11:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 -Fax: 704/62"409 Page' 1'3 =

CHAMN OF CUSTODY RECORD
V I S M I Full -Service Analytical & £ .rYES NO NIA
s Environmental Solutions PAGE_ OF _ OUOTE # TO ENSURE PROPER BILLING: w=.
samples INTACT upon arrlva!? p
ABORATORIES. INC. -
..',Rf.'Ce1Y8�1 ON"�,� ICE?,; ,'::_ .' :�.:., ..: •.: .,_, "✓ ��
Project Name:t-
449 Springbrook Road • Charlotte, NO 28217E OPER f'.F2ES43i1FlTI�lS.irjdµ2[eii`
Phone [phone] Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
C : IV d l� 5�4 �� �r° *Please ATTACH any project specific reporting (QC LEVEL 111111 IV) Redeived Vt+ITHlty HOLgING TIMcS? _._ �
Client Company Name: rTY A provisions and/or QC Requirements CUSTOpY
To Contact Name: A � � .s �;A..�
Report / Invoice To: -.. .... .. ...:.:: . ...:. ._ ... - .. __. - ....�.�
Reporting Address: P. {D. P3ax 10 6 Address:
�u e S tus 0,1s�+ TEMPI :TPierm lDr . OUserved: yG3'G i Corr. C
�s
Phone: id q-879'- M 8' Fax es No):70'4-918" 36 S5 Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DoD
FL NC
ED® Type: PDF_Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
po v dust Be
re AWork
SC OTHER
N/A
Site Location Name: Cr e_e_1r aka W rP Samples received after 14:00 will be processed next business day.
{y
Site Location Physical Address: � g.� B e ij r.9irr++ �ct Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO—
d (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES �.�
RENDERED
DERED BY PRISM LABORATORIES, INC. TO CLIENT)TIME
Sample Iced U Collection:YES NO -
am Upon p I�
DATE
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-�dp
ANALYSIS REQUESTED
PRISM
LAB
*TYPE
CLIENT
TIVES
{>
REMARKS
/
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
NO.
SIZE
,t
ID NO.
HOURS
SLUDGE)
SEE BELOW
o
/
60
7CA
P6
— 0
Sampler's Signature Ltd Sampled By (Print Name)' a GI % o Ck Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must
be
s
submitted In writing to the Prism Project Manager. There will be chaNes for any changes after analyses have been initialized.
Relin (shad By: (Signature a Recei By: (Signature) Date
Military/Hours Additional Comments:
Site Arrival Tiroei,::
Reli y (Signature) r�
+'i✓R : (Signature)Date
51#a'penartureTims
�JA
K+1 a v
'Field` Tech Fee:.
Relin uished By: (Sign Received For Pd6m laboratori� By: Date O
�! `T/ ��
�j
Mileage:
Method of Shipment: NOTE: ALL SAMPLE C OLERS SHOULD BE TAPED SHUT WITH CJd ODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COO Gro p No.
SAMPLES ARE NOT EPTED AND VERIFIED AGAINST CDC Ij . L RECEIVED AT THE LABORATORY. qb,.l p�LYB,�y g
� j
❑ Fed Ex D UPS ❑ Hand -delivered P Field Service ❑Other V
TER. WATER: WASTE: FILL
C
o o
IDRINKING
I
I❑ NC ❑ NC C ❑ SC ❑ NC❑S®NC ❑ SLID ❑N❑ SC NC ❑ SC ® NC ❑ SC
SCI❑SCR
(❑ g
NC ❑ SC
®
O
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
C`iRS ("� 4 fi11S,i

&smtFu.11-Service Analytical&
. Environmental Solutions
ORATORIES,'INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinking water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-13 Accredited Certificate No. L2307
ISOAEC 17025: L-A-B Accredited Certificate No. L2307
Project: Stal-ime (Quarterly Parameters)
Lab Submittal Date: 07/14/2014
Prism Work Order: 4070262
Case Narrative
07/24/2014
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Rabbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
A Blank Spike recovery is greater than the control limit due to carryover. Results should be considered an estimate
with high bias.
Aa Method Blank is greater than the reporting limit due to carryover. Results should be considered an estimate with
high bias.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Chartotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]

�05; .
Sample Receipt Summary
A�
Rn. `�yFull-Service Analytical &
1=' �1 s I Environmental Solutions 07/24/2014
`'-'�IABORATORIE$ ING ' '
Prism Work Order: 4070262
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
StaLime
4070262-01 Solid 07/14/14 07/14/14
Samples were received in good condition at 2.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-OW
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] x;,Pag(' _2�'` _}',

v �.13 w' Full -Service Analyi6l &
P? R' S- R/ �, I Environmental ,Solutions
IA130pATORIE5, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville; NC 28687
Project: StaLime (Quarterly
Parameters)
Sample Matrix: Solid
Laboratory Report
07/24/2014
Client Sample ID: StaLime
Prism Sample ID: 4070262-01
Prism Work Order: 4070262
Time Collected: 07/14/14 12:40
Time Submitted: 07/14/1415:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
910
mg1kg
160
13
2
*Calculation 7/23M4 8:01
CLB
ICALCI
%* Solids
55.6
% by
0.100
0.100
1
*SM2640 G 7/15/14 15:10
JAB
P4GO235
Weight
NitratelNitrite as N
54
mg1kg dry
9.0
0.99
1
*SM4500-NO3 F 7122114 9:13
CLB
P4GO346
Phosphorus -Total
3100
mg/kg dry
90
19
20
*SM4500-P F 7/22/14 13:44
JAB
P4GO299
Total ICeldahl Nitrogen
5200
mgMg dry
900
76
2
*351.2 7/23/14 8:01
CLB
P4G0361
Ammonia as N
160
mglkg dry
9.0
2.2
1
*SM4600-NH3 G 7121114 9:31
CLB
P4GO257
Microbiological Parameters
Fecal Cofiiforms
BRL
MPN/g dry
0.4
1
*SM9221 E 7/15114 12:33
JHB
P4G0285
Total Metals
Mercury
0.38
mg►kg dry
0.037
0.0060
1
*7471B
7118114 11:46
BGM
P4GO268
Arsenic
6.5
mg1kg dry
4.4
0.64
10
*6010C
7MO114 1:46
BGM
P400273
Cadmium
BRL
mg/kg dry
4.4
0.042
10
`6010C
7/18114 1:46
BGM
P4G0273
Copper
310
mg1kg dry
8.8
0.11
10
*6010C
7M 8/14 1:46
BGM
P4GO273
Lead
100
mg/kg dry
4A
0.51
10
*6010C
7118/14 1:46
BGM
P4GO273
Nickel
630
mglkg dry
18
0.14
10
*6010C
7M8114 1:46
BGM
P4G0273
Potassium
4200
mg/lrq dry
220
14
10
*6010C
7M8114 18:56
BGM
P4GO273
Selenium
BRL
mg/kg dry
8.8
1.1
10
*6010C
7/18114 1:46
BGM
P4G0273
Sodium
670
mg/kg dry
220
2.0
10
*6010C
7118/14 18:66
BGM
P4GO273
Zinc
66
mg/kg dry
44
0.30
10
*6010C
7118114 18:56
BGM
P4GO273
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-060 �.
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] : Pag@-3' Of9 ,;_

,� ram. tic Full -Service Analytical &
P' I SM, I Environmental Solutions
V�'L son-o.,ES,.c.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P4GO268 - 7471 B
Level II QC Report
7124/14
Project: Stal-ime (Quarterly Parameters) Prism Work Order: 4070262
Time Submitted: 7/14/2014 3:45:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (134GO268-BLIC1) Prepared: 07/17/14 Analyzed: 07/18/14
Mercury BRL 0.020 mg/kg wet
LCS (P4G0268-BS1) Prepared: 07/17/14 Analyzed: 07/18/14
Mercury 0.471 0.020 mg/kg wet 0.4167 113 80-120
Batch P41130273 - 3050B
Blank (P4G0273-BLKI)
Prepared & Analyzed: 07/17/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
SH
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
12
mg/kg wet
Zinc
9.96
2.5
mg/kg wet
Aa
LCS (P4G0273-BSI)
Prepared &Analyzed: 07/17/14
Arsenic
24.2
0.25
mg/kg wet
25.00 97
80-120
Cadmium
24.2
0.25
mg/kg wet
25.00 97
80-120
Copper
26.1
0.50
mg/kg wet
25.00 104
80-120
Lead
24.0
0.25
mg/kg wet
25.00 96
80-120
Nickel
24.1
1.0
mg/kg wet
25.00 96
80-120
Potassium
495
12
mg/kg wet
500.0 99
M120
Selenium
24.5
0.50
mg/kg wet
25.00 98
80-120
Sodium
450
12
mg/kg wet
500.0 90
80-120
Zinc
33.7
2.5
mg/kg wet
25.00 135
80-120 A
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] ,Page 4 Of 10,

Ab
c-w Full -Service Analytical &
!,?, 1 S, V Y Environmental Solutions
':LABOR�TORIEQ ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime (Quarterly Parameters)
Level II QC Report
7/24/14
Prism Work Order: 4070262
Time Submitted: 7/14/2014 3:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MOM - NO PREP
Blank (P4G0235-BLK1) Prepared & Analyzed: 07/15/14
% Solids 99.9 0.100 % by Weight
Batch P4G0257 - NO PREP
Blank (P4G0257-BLKI) Prepared: 07/17/14 Analyzed: 07/21/14
Ammonia as N BRL 5.0 mg/kg wet
LCS (P4G0257-BS1) Prepared: 07/17/14 Analyzed: 07/21/14
Ammonia as N 124 5.0 mg/kg wet 125.0 100 80-120
Matrix Spike (P4G0267-MSI) Source: 4070262-01 Prepared: 07/17/14 Analyzed: 07/21/14
Ammonia as N 302 9.0 mglkg dry 224.8 146 70 80-120 MI
Matrix Spike Dup (P4G0257-MSD1) Source: 4070262-01 Prepared: 07/17/14 Analyzed: 07/21/14
Ammonia as N 297 9.0 mg/kg dry 224.8 146 68 80-120 1 20 MI
Batch P4G0299 - SM4500-PB5
Blank (P4G0299-BLK1) Prepared: 07/18/14 Analyzed: 07/22/14
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P4G0299-BSI) Prepared: 07/18/14 Analyzed: 07/22/14
Phosphorus -Total 109 2.5 mg/kg wet 100.0 109 90-110
Matrix Spike (P4G0299-MS1) Source: 4070262-01 Prepared: 07/18/14 Analyzed: 07/22/14
Phosphorus -Total 3600 90 mg/kg dry 179.9 3110 272 80-120 MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-OSM
Phone: [phone] - Toll Free Number:1-8091529-6364 - Fax: [phone] Pag@ 5 Of °1 Q

i 1 Full -Service Analytical &
Ism
Environmental Solutions
'?LABORATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P4G0299 - SM4600-PBS
Level II QC Report
7124/14
Project: Stal-ime (Quarterly Parameters) Prism Work Order: 4070262
Time Submitted: 7/14/2014 3:45:00PM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P4G0299-MSD1) Source: 4070262-01 Prepared: 07/18/14 Analyzed: 07/22/14
Phosphorus -Total 3530 90 mg/kg dry 179.9 3110 230 80-120 2 20 MC
Batch P4G0346 - NO PREP
Blank (P4G0346-BLKI) Prepared & Analyzed: 07/22/14
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P4G0346-BS1) Prepared & Analyzed: 07/22/14
Nitrate/Nitrite as N 49.2 5.0 mg/kg wet 50.00 98 80-120
Matrix Spike (P4G0346-MS1) Source: 4070262-01 Prepared & Analyzed: 07/22/14
Nitrate/Nitrite as N 145 9.0 mg/kg dry 89.93 53.7 101 80-120
Matrix Spike Dup (P4G0346-MSD1) Source: 4070262-01 Prepared & Analyzed: 07/22/14
Nitrate/Nitrite as N 146 9.0 mg/kg dry 89.93 53.7 103 80-120 0.7 20
Batch P4G0361 - 351.2
Blank (P4G0361-BLK7) Prepared: 07/22/14 Analyzed: 07/23/14
Total lgeldahl Nitrogen BRL 25 mg/kg wet
LCS (P4G0361-BSI) Prepared: 07/22/14 Analyzed: 07/23/14
Total IGeldahl Nitrogen 508 100 mg/kg wet 500.0 102 90-110
Matrix Spike (P4G0361-MS1) Source: 4070262-01 Prepared: 07/22/14 Analyzed: 07/23/14
Total IGeldahl Nitrogen 14600 2200 mg/kg dry 8993 5180 105 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone]- Toll Fires Number. 1-8001529-6364- Fax" 7041526-0409 Page 6,of 10

Full -Service Analytical 8
'P Il. sl I S M I Environmental Solutions
� LA.ORATORMA INC.
Level II QC Report
7/24/14
City of Statesville, NC Project: StaLime (Quarterly Parameters) Prism Work Order: 4070262
Attn: Andy Smith Time Submitted: 7/14/2014 3:45:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41130361 - 361.2
Matrix Spike Dup (P4G0361-MSD1) Source: 4070262-01 Prepared: 07/22/14 Analyzed: 07/23/14
Total lgeklahl Nitrogen 12600 2200 mg/kg dry 8993 5180 82 90-110 15 20 MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001629-6364 - Fax: 704152&4409 Page 7

'
Level II QC Report
P�.. A�
I S M
Full -Service Analytical &
solutions
7124114
Environmental
rIUWRATORIES INC
City of Statesville, NC
Project:
Stai-ime (Quarterly Parameters) Prism Work Order: 4070262
Attn: Andy Smith
Time Submitted: 7/14/2014 3:45:00PM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte
Result
Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4G0285 - NO PREP
Blank (P4G0285-BLK1)
Prepared & Analyzed: 07/15/14
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch
Initial
Final DateMme
4070262-01 P4G0361
0.05 g
25 mL 07/22/14 10:30
Prep Method: SM4500-PBS
Lab Number Batch
Initial
Final Daternme
4070262-01 P4130299 1 g 50 mL 07/18/14 14:38
Prep Method: 3050B
Lab Number Batch Initial Final DateTme
4070262-01
P4G0273
2.05 g
50 mL
07/17/14 15:26
4070262-01
P4G0273
2.05 g
50 mL
07/17/14 15:26
Prep Method: 7471B
Lab Number
Batch
Initial
Final
DateTme
4070262-01
P4G0268
0.59 g
50 mL
07/17/14 10:21
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] -Tall Free Number. 1-8001529-6364 - Fax: [phone] Page 8 of 10

.r .
'
CHAIN ®F CUSTODY RECORDDom
- e
.,y
`. `. E :.
•,` u.. -.-
:G4
AL.5?",a...fi�"
Full-Service Analytical &
Environmental Solutions
PAGE OF _ QUOTE A TO ENSURE PROPER BI LLING:
:. YEB ` ': NO , ':NfA:..
" '`�".,.':�` '" '' /" ,' ::.
5arijpleflilTACT ill oR arcival._ ::...
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LABORATORIES INC.
Project Name:
:Fp:
...-t'1P.GBIV.ed�tV%%rGT:•i�i,.'�:-'f:=:=sCfr>;.; :'::'_:"
,.,....
O)
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] ° Fax: [phone]
es No UST Project:(Yes)NO
Short Hold Analysis. (Yes) ( ) 1 ( )
: - PRESCIjVATIVE4i}idicakedY:,-;:.T";:w_ '
PRQR,ER
IOLDiNC
N
o d� 1 J 1
Name: a IV 0-+�Ate$rs'3'eC
`Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
366div0dWITHIN I
CUSTODY.SEALS IrtTACT7
Client Company
provisions and/or QC Requirements
—.
rJ n e
Report To/Contact Name: A n S y
Invoice To:
�lDLA71LE5. teed W10UT HEApSPlaCE? .
Reporting Address'P.O.90 dd d d
p
Address:
,PRQPER'C0NTAINI R8 used?-:
".., : PC !'Corr:C1
9�,
tF'aX
TEMP;' Therm 1Di' ."i-la. :' Ob3eived:. L,Ii
Phone:701- 3 7Y-3g3 7 es (No):70-V-37S- WS Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF Excel Other
-�
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
re h Work Must Be
SC `'OTHER N/A
�•
Site Location Name: d'l k �'•f h cree-k ww r p
Samples received after 14:00 will be processed next business day.
Site Location Physical Address: G 93 ,,J / FA r; I?TTurnaround
time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO —
.5-6h `esm ®®G" %�
REGARDING (SEE REVERSE FOR TERMS &CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES_ NO
p p _
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRISM
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
COLLECTED
MILITARY
HOURS
(SOIL,
WATER OR
SLU9DGE)
PRESERVA.
TIVES
\ \�s / REMARKS
LAB
ID NO.
"TYPE
SEE BELOW
NO.
SIZE
I �2? q 6
..i
/vet'
...
As
/
D
tea. 9
fA
Ai Al, /� b
'
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Pb
a;
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S�
I
O D
Sampler's Signature Sampled By (Print Name) Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charge
fora anges after analyses have been initialized.
�Relln ished By: (Signa/j/uje) s /_ Recei d B ature�..UAtejli�MiJta Hours Addition
�//.L.�2tP�2�JL ✓(1 GGi.Lf.� � - _ eeDD bJ
ethod of Shi�menL NO :ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTO EALS FOR TRANSPORTATION TO THE LABORAI UKY. �Cuu �reup 70.
MPLES ARE N T A JCEPTED AND VERIFIED AGAINST COG UNTIL EIVED AT THE LABORATORY. ! n
❑ Fed S ❑ Hand -delivered Prism Field Service ❑ Other ®2-4
NPDES. UST: G UNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
®NC❑SC� QNC ❑SC ANC ❑SC ®NC ❑SC I ❑❑NC ❑SC I nNC❑SCI ®NC ❑5CI❑❑NC ❑SC oNC ❑SC
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Comments:
mmom
Site Arrival Time:
.site Qeparture Time:
Field,Tech Fee:'
Mileage: . .
.7 'SEE REVERSE FORS x
.:T.ERMS r8*CONDITIONS F'
t' PIf--1I\JA1

.k
CHAP F CUSTODY RECONEDM.1
FR I S
Full-Service Analytical &
Environmental Solutions
at TO E¢asusaE PROPER Iala Laaaor
`t
:"'amle
`.1ACT `z_relyal-.:
IABORATOSIE5, INC..'.
PAGE `^ o� muoTe
"INTACT
�Ftecetif�d�C1,N_1!Si�'f`>ICE
Project Name:
:T�Ii'I
449 5prdngbrotJ}c Road a P.O. Sor.240543 ®Charlotte, NC 28224-0543
Phone: [phone] Fax: [phone]
rYGiTJtU<);H41~4?PfV
or
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
PROPEtq l�C f SE Vy1TIVES indlCat d
TIM :.:''
41
rn
M
Client Company Narrow.:%
Report To/Contact Name:
provisions and/or QC Requirements
uOLAilLES reed-3/i/Ol}T i-1i""AC1 .4OE? �j
-
Reporting Address:
Invoice To -
PiOFEI3 GCN FA I.iVFt-usci`l'
-
Address:
_
Phone: Fax. (Yes) (No):
Purchase Order No./Billing Reference
TO R FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address
Requested Due Date' ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
C ification:
NELAG USAGE FL NC
EDD Type: PDF_ Excel _Other
'Working Days" U 6-9 Days ❑ Standard 10 days ❑ RushPre-Work Be
dust
SG OTHER N/A
Site Location Name:
Samples received after 15:00 will be processed next business day.
Site Location Physical Address:
Turnaround time is based on business days, excluding weekends and holiday
Water Chlorinated: YES _ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
$any le Iced Upon Collection: VIES NO
IT p
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA•
LAB
"TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
/��
��� REMARKS
1D NO.
HOURS
SLUDGE)
SEE BELOW
q
At,p��
�
1✓�
As
%A4:r$o"lC:PP
Cd6
—Ad
Sampler's Signature
Sampled By (Print Name) Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proc the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for an changes er analyses have been initialized.°
Reli quishn2 ed By: (Si ature) /
Received By: (Signatu ) D
i t ryr Ail Comments:
/ �' Additional SifpfriVal�Time = ' ,
f�l /lt
Re!Lr1R61shed By: (Signature)
Received By: (Signatur 15atif
Site De �rtl�rq T1me
Relin ed B.. ignature ,
Received For Pri Laborator es D t
Method of Shipment: OTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUS D SEALS FOR TRANSPORTATION TO THE LABORATORY. COO Group o.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COO UNT CEIVED AT THE LABORATORY.
(/
Q Fed Ex PS ❑ Hand -delivered ❑Prism Field Service
❑Other
NPDES: I UST: GROUNDWATER:
DRINKING WATER: I SOLID WASTE: RCRA: CERCLA LANDFILL
OTHER:"
❑ NO El SO El NO ❑ SC ❑ NC ®SC
El ❑ SC El ❑ SC NC ❑ SC ❑ NO ❑ SC ❑ NO Q SC ❑ NO ❑ SC
❑ ❑ - Ci
❑ _ .-....... Cl .. _.. ---- ❑ ❑ 1 ❑ _ 1-1 ---- ----
ORIGINAL
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

' NC Certification No. 402 Case Narrative
SC Certification No. 99012
Q L� Full -Service Analytical& NC Drinldng Water Cert No. 37735ISM
Environmental Solutions VA Certification No. 460211 08/11/2014
SY LABORATORIES, INQ DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 07/30/2014
Statesville, NC 28687 Prism Work Order: 4070590
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Rabbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 ° of 7

ERR
FuII-Servloe Analytical &
`,'.�jl� R IS M� I Environmental Solutions
Sample Receipt Summary
08/11 /2014
Prism Work Order: 4070590
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
StaLime
4070590-01 Solid 07/30/14 07/30/14
Samples were received in good condition at 5.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 SpringbrookRoad - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

Laboratory Report
/9 "Rs
P
PRI S M
Full -Service Analytical&
Environmental Solutions
08/11/2014
I-i
®�V100RATORIE$ ING "
City of Statesville, NC Project: StaLime
Client Sample ID: StaLime
Attn: Andy Smith
Prism Sample ID: 4070590-01
P.O. Box 1111
Prism Work Order: 4070590
Statesville, NC 28687 Sample Matrix: Solid
Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Daterrime
ID
General Chemistry Parameters
% Solids
73.6
% by
0.100
0.100
1
'SM2640 G
811R4 14:16
JAB
P41-10019
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPNIg dry
0.3
1
'SM9221 E
7/31114 13:12
JHB
P41-10023
Total Metals
Mercury
0.16
mglkg dry
0.029
0.0048
1
'7471B
816M4 13:07
MEH
P41-10071
Arsenic
1.6
mglkg dry
1.0
0.16
3
*60111C
815114 19:28
BGM
P4H0011
Cadmium
BRL
mg/kg dry
1.0
0.0097
3
•6010C
8/5114 19:28
BGM
P41-10011
Copper
31
mglkg dry
2.0
0.026
3
•6010C
815114 19:28
BGM
P41-10811
Lead
16
mgfkg dry
1.0
0.12
3
"6010C
815114 19:28
BGM
P4H0011
Nickel
82
mglkg dry
4.1
0.033
3
"6010C
815M4 19:28
BGM
P4H0011
Selenium
BRL
mglkg dry
2.0
0.25
3
•6010C
815114 19:28
BGM
P41-10011
Zinc
74
mglkg dry
10
0.069
3
•6010C
815M4 19:28
BGM
P4H0011
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone" 7041629-6364 - Toll Free Number:1-8001529-6364 - Fax- 7041625A409 P66e,37"?

,p r� t I� n Full -Service Analytical &
'v t Environmental Solutions
1A80RATORIEB. INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P4H0011 - 3050B
Project: StaLime
Reporting
Result Limit Units
Level II QC Report
8111/14
Prism Work Order: 4070590
Time Submitted: 7/30/2014 5:10:00PM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank(P4H0011-BILKI)
Prepared:08/01/14 Analyzed: 08/05/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
2.96
2.5
mg/kg wet
BH
LCS (P4H0011-BSI)
Prepared: 08/01/14 Analyzed: 08/05/14
Arsenic
21.6
0.26
mg/kg wet
25.51 85 80-120
Cadmium
21.7
0.26
mg/kg wet
25.51 85 BD-120
Copper
24.5
0.51
mg/kg wet
25.51 96 80-120
Lead
21.6
0.26
mg/kg wet
25.51 85 80-120
Nickel
22.0
1.0
mg/kg wet
25.51 86 80-120
Selenium
21.6
0.51
mg/kg wet
25.51 85 80-120
Zinc
23.9
2.6
mg/kg wet
25.51 94 80-120
Batch 1341-110071 - 7471 B
Blank (P41-110071-BLK7) Prepared: 08/05/14 Analyzed: 08/06/14
Mercury BRL 0.020 mg/kg wet
LCS (P4H0071-BS1) Prepared: 08/05/14 Analyzed: 08/06/14
Mercury 0.400 0.019 mg/kg wet 0.3906 102 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-050
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: 704152"409 Page 4 of 7

s-' Full -Service Analytical &
I S M I Environmental Solutions
'TLgOORATORIES INC.
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
8/11114
Prism Work Order: 4070590
Time Submitted: 7/30/2014 5:10:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MOM - NO PREP
Blank (P41-110019-BLK1) Prepared & Analyzed: 08/01/14
% Solids 100 0.100 % by Weight
Duplicate (P4H0019-DUP1) Source: 4070590-01 Prepared & Analyzed: 08/01/14
% Solids 68.0 0.100 % by Weight 73.6 8 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6304- Fax: [phone] Page 5_of 7

Level II QC Report
s t° pp,\ /n' FuwService.Anafytical & 8111/14
.I S, .V , I Environmental Solutions
1AGORATONIE$ IN0.'
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Project: StaLime
Prism Work Order: 4070590
Time Submitted: 7/30/2014 5:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41-10023 - NO PREP
Blank (P41-10023-BLK7) Prepared &Analyzed: 07/30/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Initial Final Daterrime
4070590-01 P4H0011 2.01 a 50 mL 08/01/14 9:30
Prep Method: 7471E
Lab Number Batch Initial Final DateMme
4070590-01 1341-10071 0.56 g 50 mL 08/05/14 10:45
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number.1-8001529-6364 - Fax: 704/525A409

y t":
`"' `
1
p®�© p�ymn p��v a
CHAIN O CUSTODY 'RECORD
A; r
Full-Service Analytical' ",
I
� �
_ n, a h r .'. ; EnVIYOnmP.nt21 SOIUtIOnS•`'. PAGE 9 OF QUOTE # TO ENSURE PROPER BILLING: - - I 1 T'U o 'airiYal?`-.''�-�_--:� _'� `
p es NTAC p. n, �, O
- ": '' �' -' ' ''' ' - �,r ,,� -.
DER
LABORATORIES, INC.
- Re�$N0U �N NET
Project Name: , y
449 Springbrook Road - Charlotte, NC 28217 pFt4PR pRES R�AT1VE5ln�ilcatec#�
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) -
Phone [phone] < Fax: [phone]
a * C LEVEL 111 111 IV Receivet:V117(tltt-:HC?1 tIPtf?: 11fu1F'$,1:. ;;; ;. ;;;`°,•:..1:-=.'^::,•: n + < 'RS
(+ � Please ATTACH any project specific reporting (Q L )
B��
Client Company Name: �p o'p1' ^� a +
provisions and/or OC Requirements ` -GUBTODY SEA15 INTAG7?
+�S
Report To/Contact Name A,, RX Sow 4-h
Invoice
1(OL�fI1 E rec'd:W(OUT:HEADS PACEY, :,• _-� , - J;
To: _ -.. :1�<
`:.,..
®. T CONTAINERS usetl? i• :-.';.s:;.::'.:'.: i, :::'i>.
Reporting Address: P i3ok 11 diROi'R:.
Address: :•:•....:,. ;..
' 2Ti�C7fi5erve
J�a`EeSv� III AVC
:'FEMP�Tlierm'll]:'%
Phone: YOY- l 1 S- 3qi ? Fax es (No): %DY- 57$1- W55 purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rues Work Must Be
SC OTHER NIA
Site Location Name: F'o art b Creek W Ltd T-P Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 193 a e,1 j Far-; 'RI, Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
6AIC T i , II d NC -RENDERED
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES NO
p P —
CLIENT
DESCRIPTION
DATESAMPLE
COLLECTED
TIME
TIME
CMI ITARY
MATRUt
(SOIL,
WATER OR
SAMPLE CONTAINER
PRT VESbA
ANALYSIS REQUESTED
�� REMARKS
/Q�
f �.
PRISM
I O
"TYOLLECTE
PE
NO.
SIZE
HOURS
SLUDGE)
SEE BELOW
�y
C
P cat
Pb
Sampler's SignatureGJ
�Clt•( G!/..cr��C� Sampled By (Print Name) Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be cha ges for any changes after analyses have been initialized.
R Ii Ished By: (Signa e) i � ReceivedT. (Signature) Date — }(� Wye
ilriLJ /i/
SAMPLES ARE NOT7ACEPTED AND VERIFIED AGAINST COC Ki;IL RECEIVED AT THE LABORATORY.❑ Fed Ex ❑ UPS ❑ Hand -delivered sm Field Service ❑ Other
❑ NC ❑ SCI ❑ NC ❑ SC I ❑ NUST:OCU ❑ SCTER: I ❑ N KING VCdATER: SOLID O SSCTE: NC I
0� SC I CERCLA ®NC ❑ SC 0❑ NCDFILL ❑ SC I
❑ C ❑ SC
❑ ❑. ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
sv �
Comments:
ORGINAL.

lj NC Cetifcation No; ;402 .
Case NarraveSCCertifcationNo.99012
'
D -Service Analytical & NC Drinking Water Cert No. 37735
I S Environmental Solutions VA Certification No. 46021.1 -. 08/18/2014
"D ed Certificate No L2307
®QLAeoRATORIE$ ING. oD ELAP. L-A-B Accredit
•;;,ISO/IEC 17025 L-A-B Accredited Certificate No. L2307:.
City'of Statesville, NC „ " ;, Project:,Sludge (Hazardous Testing)
Andy Smith
P.O. Box 1111 " Lab Submittal Date: 07/30/2014
Statesville, NC 28687 " Prism Work Order: 40705.91
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless othenNise noted, all samples were received in acceptable condition and processed
according to the referenced methods. "
Data qualifiers are flagged, individually.on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes: "
Reactivity analysis was subcontracted to GCAL. TCLP Herbicide, analysis was subcontracted to AES.
Laboratory repors are attached.
Please call if you have any questions relating to this analytical report, . ...
Respectfully,
PRISM LABORATORIES,.INC. ...
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
A " ECV result is.above range; Results are; BDL. No further action taken.
Aa ECV results 'on secondary column are.above range: Results are reported from primary column. No further action
taken.
D RPD value outside of the control. limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit.ihdicated with a J.
This report should not be reproduced, except in its entirety, without the writtenconsent of Prism Laboratories, Inc
449 Springbrook Road - P.O,.. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free -Number: 1-8001529-6364 - Fax: [phone] Page 1 of 32

i
..Sa p Receipt Summary
nnFull-Service Analytical &
1, S I V I L Environmental Soiutione :. 08/18/2014
..-©U6egATDRIEQ ING .. .. .
Prism Work Order: 4070591
Client Sample ID .. Lab Sample ID Matrix Date Sampled Date Received
StaLime 4070591-01 Solid 07/30/14 07/30/14
Third Creek Sludge. 4070591-02 Solid 07/30/14 07/30/14
Fourth Creek Sludge 4070591-03 Solid . 07/30/14 07/30/14
Samples'were received, in good condition at 5:9.degrees C unless otherwise noted:

sn n Fullironmen Analytical s
' V' ..Environmental Solutions
�LABORATURIM INC ,
City of Statesville, NC
Attn: Andy Smith
P.O.' Box 1111
Statesville, NC 28687
Laboratory Report
08/18/2014
Project: Sludge (Hazardous Testing):.:: Client Sample IDi StaLime
Prism Sample ID: 4070591-01
Prism Work Order: 4070591
Sample Matrix: Solid' Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
78:2
% by
0.100
0.100
1
*SM2540 G
8/5114 11:40
JAB
P41­110072
Weight
Corrosivity-pH
12
pH Units
1
*9045D
8/1/14 13:15
MES
P4H0014
Ignitability
Pass
mm/sec
0.10
1
*1030
8/7/14 9:09
JAB
P4H0101
'TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311 ZHE
8/8/14 9:00
ANG
P41­10120
TCLP Extraction
Complete
'N/A
1
'1311
8/12/14 9:30
MEH
P41­10174
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000012
1
*7470A
8/13/14 12:17
MEH
P41-10190
Arsenic
BRL
mg/L
0.050
0.0060
1
*6010C
8/14/14 16:55
BGM
P41­10192
Barium
"' BRL
mg/L
5.0
0.0.12
1
*6010C
8/14/14 16:55
BGM
P4H0192
Cadmium
BRL
mg/L
0.625
0.00022.
1
*6010C
8/14/14 16:55
BGM
P41­10192
Chromium
BRL
mg/L
0.25
0.0019
1
*6010C
8/14/14 16:55
BGM
P4110192
Lead
BRL
mg/L
0.050
0.0028
1
*6010C
8/14/14 16:55
BGM
P4H0192
Selenium "'
BRL
mg/L
0.10
0.018
1
*6010C'
8114/14 16:55
BGM
P41­10192
Silver
BRL
mg/L
0.25
0.0012
1
*6010C
8/14/14 16:55
BGM
P41-10192
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
ug/L
2.5
0.16
1
*808113
8/14/14 1:50
JMV
P41­10214
Dieldrin
BRLA
ug/L
0.50
0.0046
1
*8081B
8114/14 23:59
JMV
P4H0214
Endrin
BRLA.
ug/L
0.50
0.0046
1
*8081B
8114114 23:59
JMV
P4H0214
gamma-BHC
BRL
ug/L
0.50
0.0049
1
*8081B
8/14/14 23:59
JMV.
P4H0214
Heptachlor
BRL
ug/L
0.50
0.0077
.1
*8081B
8114114 23:59
JMV
P41­10214
Heptachlor Epoxide
BRL
ug/L
0.50
0.0046
1
*8081B
8/14/14 23:59
JMV
P41-10214
Methoxychlor
BRLA
ug/L
, : 0.50
0.0087
1
*8081B
8/14/14 23:59
JMV
P41­10214
Toxaphene
BRLAa
ug/L
25
0.15-
1
*8081B
8/14/14 1:50
JMV
P41­10214
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
79 %.
13-186
Tetrachloro-m-xylene
61 %
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.012
1
*8270D
8/13/14 19:00
KC;
P4H0170
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.012
1
*8270D
8/13/14 19:00
KC
P41­10170
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0048
1
*8270D
8/13114 19:00
KC
P41­10170
2-Methylphenol:
BRL
mg/L
0.050
0.012' .
1
*8270D
8/13/14 19:00
KC
P41-10170
3/4-Methylphenol
BRL
mg/L
0.050.
0.012
1
*8270D
8/13/14 19:00
KC
P4H0170
Hexachlorobenzene
BRL
mg/L'
0.050
0.0670
1
*8270D
8/13/14 19:00
KC
P41­10170
Hexachlorobutadiene'
BRL
mg/L
0.050
0.011
1
*8270D
8/13/14 .19:00
KC.
P41-10170
Hexachloroethane
BRL
mg/L
0.050
0.0097
.1
*8270D
8/13/14 19:00
KC
P41­10170
Nitrobenzene
BRL
mg/L
: 0.050
0.0098
1
*8270D
8/13/14 19:00
KC
P4H0170
P.entachlorophenol
BRL
mg/L
0.25
0.0082'
1
*8270D
8/13/14 19:00
KC
P41`10170
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
"o Springbrook'Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone:, 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 32

Lim
Laboratory Report
Full -Service Analytical 8
A R I Environmental Solutions 08/18/2014
City of Statesville, NC Project: Sludge (Hazardous: Testing)Client Sample ID: StaLime
Attn: Andy Smith Prism Sample ID: 4070591-01
P.O. Box 1111 Prism Work Order: 4070591
Statesville, NC 28687 Sample Matrix: Solid' Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
Parameter Result Units Report MDL' Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pyridine
BRL
mg/L
0.25 0.016' 1
*8270D
' 8/13/14 19:00
KC
P41­10170
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
107 %
49-109
2-Fluorobiphenyl
67 %
55-96
2-Fluorop henol
51 %
27-74
Nitrobenzene-d5
82 %
53-99
Phenol-d5
31 %
11-52
so
Terphenyl-d14
100 %
42-133
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
ug/L
35 0.78 1
*8260B
8/8/14 14:37
VHL
P41­10172
1,2-Dichloroethane
BRL
ug/L
25 1.4 1..
*8260B
8/8/14 14:37
VHL
P41­10172
1,4-Dichlorobenzene
BRL
ug/L
380 0.68 1
*8260B
8/8/14 14:37
VHL
P41­10172
Benzene
BRL
ug/L
25 0.72 1
*8260B
8/8114 14:37
VHL
P41­10172
Carbon Tetrachloride
BRL
ug/L
25 1.2 1
*8260B
818/14 14.37
VHL
P4H0172
Chlorobenzene :
BRL
ug/L
5000 0.61 1
*8260B
8/8l14 14:37.
VHL
P41­10172
Chloroform
„BRL
uglL
300 0.89 1
*8260B
8/8/14 14:37
VHL
P41­10172
Methyl Ethyl Ketone (2-Butanone) BRL
ug/L
10000 9.0 1 .
*8260B
8/8/14 14:37
VHL
P41­10172
Tetrachloroethylene
BRL
ug/L
35 0.69 1
*8260B
8/8/14 14:37
VHL
P41­10172
Trichloroethylene
BRL
ug/L
25 0.54 1
*8260B
8/8/14 14:37
VHL
P41­10172
Vinyl' chloride
"' BRL
ug/L
20- 1,6, ;;' 1
*8260B
8/8/14 14:37'
VHL
P4H0172
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
109 %
80-124
Dibromoflucromethane
78 %
75-129
Toluene-d8'
101 %
77-123
This report should not be reproduced, except in its entirety, without the written' consent of Prism Laboratories, Inc.
•
449 Springbrook'Road - P.O., B6x'240543 - Chajlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 -Fax: [phone]
Page
4 of 32

®wFC I Fulf-Service Analytical &
ul S M . 1. Environmonlal Solutions
vIAeONATOPIEQ INC
City of Statesville, NC
Attn: Andy Smith
P.O.' Box 1111 -
Statesville, NC 28687
Project: Sludge (Hazardous Testing)
Sample Matrix: Solid
Laboratory Report
08/18/2014
Client Sample ID: Third Creek Sludge
Prism Sample ID: 4070591-02
Prism Work Order: 4070591
Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time, ID
General Chemistry Parameters
% Solids
17.5 ..
% by
0.100
0.100
1
*SM2540 G
8/5114 11:40
JAB
P41­110072
Weight
Corrosivity-pH
7.4
pH Units
1
*9045D
8/1/14 13:15
MES
P41­110014
Ignitability
Pass
mm/sec
0.10
1
*1030
817/14 9:13
JAB
P41­10101
TCLP Extraction by EPA 1311
TCLP Extraction'
Complete
N/A
1
*1311 ZHE.
8/8/14 9:00'
ANG
P41­16120
TCLP Extraction':
Complete
N/A.
1
*1311
8/12/14 9:30
MEH
P41­10174
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000012
1
*7470A
8/13/14 12:20
MEH
P41­10190
Arsenic
BRL
mg/L
0.050
0.0060
1'
*6010C
8/14/14 17:02
BGM
P41­10192
Barium
BRL
mg/L
5.0
0.012
1
*6010C
8/14/14 17:02
BGM
P41­10192
Cadmium
BRL
mg/L
0.025
0.00022
1
*6010C
6/14114 17:02
BGM
P41­10192
Chromium
BRL
mg/L
0.25
0.0019
1
*6010C
8/14/14 17:02
BGM
P41­10192
Lead " "
BRL
mg/L
0.050
0.0028
1
*6010C
8/14/14 17:02
.BGM
P41­10192
Seleniurri;
BRL
mg/L
0.10
0.018
1
*6010C
8/14/14 17:02
BGM
P41­10192
Silver
BRL
mg/L
0.25
0.0012
1
*6010C
8/14/14 17:02
BGM
P41­10192
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
ug/L
2.5
0.16
1
*8081B
8/14/14 2:33
JMV
P41­10214
Dieldrin
BRLA
;rig/L
0.50
0.0046
1
*8081B
8/15/14 0:42
JMV
P41­10214
Endrin
BRLA
"ug/L
0.50
0.0046
1
*8081B
8/15/14 0:42
JMV
P4H0214
gamma-BHC "'
BRL
ug/L
0.50
0.0049
1
*8081B
8/15114 0:42
JMV
P41­10214
Heptachlor
BRL "'
ug/L
0.50
0.0077
1
*8081B
8/15/14 0:42
JMV
P41­10214
.. Heptachlor Epoxide
BRL
ug/L
0.50
0.0046
1
*8081B
8/15/14 0:42
JMV
P41­10214
Methoxychlor .."
BRLA
ug/L
0.50
0.0087
1
*8081B
8/15/14 0:42
JMV
P41­10214
Toxaphene
BRLAa "
ug/L
25
0.15.
1
*8081B
8/14/14 2:33
JMV
P4H0214
Surrogate
Recovery
Control Limits
Decachlorobiphenyl'
98
%
13-186
Tetrachloro-m-xylene '
82
%
40-134
TCLP Semivolatile. Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.012
1
*8270D
8/13/14 19:22
KC
P41­10170
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.012
1
*8270D
8/13/14 19:22
KC
P41­10170
2,4-Dinitrotoluene
BRL
mg/L
0.050'
0.0048"
1
*8270D
8/13/14 19:22'
KC
P41­10170
'2=Methylphenol
BRL
mg/L
0.050
0.012,
1
*8270D
8/13/14 19:22
KC
P41­10170
3/4-Methyl phenol "
BRL
mg/L
0.050
0.012
1
*8270D
8/13/14 19:22
KC
P41­10170
Hexachlorobenzene
BRL
mg/L
0.050
0.0070
1
*8270D
8113/14 19:22
KC
P41­10170
Hexachlorobutadiene
BRL
" mg/L
0.050
0.011
1
*8270D
8/13/14 19:22
KC
P41­10170
Hexachloroethane
BRL
mg/L
0.050
0.0097
1
*8270D
8/13/14 19:22
KC
P41­10170
Nitrobenzene
BRL
mg/L ..
0.050
0.0098
1 '
*8270D
8/13/14 19:22
KC
P41­10170
Pentachlorophenol
BRL
mg/L.
0.25
0.0082
1
*8270D
8/13/14 19:22
KC
P41­10170
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook'Road -P.O. Box,240543 -Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 32

'
Laboratory Report
�I^�
�
Ie
n
.... "
Full -Service Analytical' &
.I
IUiiuoaproniea iec
'
Environmental Solutions .. ._ • ;
.. 08/18/2014
City of Statesville, NC'.::.
Project: Sludge .(Hazardous. Testing):Client-Sample
ID: ;Third Creek_ Sludge
Attn:, Andy Smith,„•'
Prism Sample 'I,D: 40705.91=02
. P.O.' Box 1111 ' '
"
Prism Work Order: 4070,591
Statesville, NC 28687
Sample:Matrix: Solid
Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14.17:10 "
Parameter
Dilution Method Analysis Analyst Batch
Result Units Report MDL
Limit
Factor Date/Time, ID
Pyridine ":
"' BRL mg1L. 0.25 0.016'
1 " *8270D 8/13/14 191.22 KC P41­10170
2,4,6-Tribromophenol
81 %
49-109
2-Fluorobiphenyl
55 %
55-96"
2-Fluorophenol
43 %
27-74
Nitrobenzene-d5
63 %
53-99
Phenol-d5
27 %
11-52
:.::.
Terphenyl-d1
89 %.
44 2-133
TCLP. Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
.BRL
ug/L
35 0.78
1
*8260B
8/8/14' 15:03
VHL
P4H0172
1,2-Dichloroethane
BRL
ug/L :
25 1.4
1.
*8260B
8/8/14 .1.5:03
VHL.,
P41­10172
1,4-Dichl6robenzene _
BRL'
u /L
380 0.68
1
*8260B
8/8114 15:03
VHL
P41­10172
Benzene :i
BRL ::: ::
ug/L
25: 0.72'
1
:*8260B
8/8/14 15:03.'
VHL
P.41­10172
Carbon Tetrachloride
BRL '
ug/L
25 1.2
1
*8260B
8/8/14 15:03
VHL
P41­10172
Chlorobenzene ::.
BRL
ug/L
5000 0.6.1 .
1
*8260B
8/8/14 15:63.
VHL
P.4H0172
Chloroform"
BRL
ug/L ;,;•
,' 300 0.89
1
*8260B,
8/8/14 15:03
VHL
P41­10172
Methyl Ethyl Ketone (2-Butanone) BRL
ug/L
10000 9.0
1
*8260B
8/8/14 16:03
VHL
P41­10172
Tetrachloroethylene
BRL
ug/L
35 0.69
1
*8260B
8/8/14 15:03
VHL
P41­10172'
Trichloroethylene
BRL
ug/L
25 0.54
1
*8260B
818/14 15:03
VHL
P41­10172
Vinyl chloride
BRL
raglL
20: " 1.6,
1
*8260B
818/14 15:03
VHL
P4H0172
Surrogate
Recovery
Control Limits
4-6romofluorobenzene
111.
80 124
'Dibromofluororhethane
102 %
75-129
'Toluene-d8"
"'
101 %
77-123
..
This report should not be reproduced, except in its entirety,. without the written consent of Prism Laboratories, Inc.
449 Springbrook'Road-P.O.,Boz,240543
-:Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Faxo-704/525-0409
Page
6 of 32

Laboratory Report
-Service Analytical 8
�lAaepATON1ES ING
IFull
, Environmental Solutions
..
..
.
08/18/2014
City of Statesville, NC
.. Project: Sludge (Hazardous Testing)
Client•Sample
ID:
Fourth Creek Sludge
Attn::Andy Smith
Prism
Sample ID:
4070591-03
P.O. Box 1111
Prism
Work Order:
4070591
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
p.
General Chemistry Parameters
% Solids
15.2
% by ..
o.100
0.100
1
*SM2540 G
8/5/14 11:40
JAB
P4H0072
Weight
Corrosivity-pH
5.1
pH Units
1
*9045D
8/1/14 13:15
MES
P41-10014
Ignitability
Pass
mm/sec
0.10
1
*1030
8/7/14 9:16
JAB
P41-10101
TCLP Extraction by EPA.1311
TCLP Extraction
Complete
N/A
"'
1
*1311 ZHE
8/8/14 9:00
ANG
P41­10120
TCLP Extraction',
Complete
NIA
1
*1311
8/12/14 9:30
MEH
P41-10174
TCLP Metals .:
Mercury
BRL
mg/L •
0.010
0.000012
1
*7470A
8/13/14 12:25
MEH
P41­10190
Arsenic .
BRL
mg1L
0.050
0.0060
1
*6010C
8/14/14 17:09
BGM
P41-10192
Barium
BRL
mg/L
5.0
0.012.
1
*6010C
8/14/14 17:09
BGM
P41-10192
Cadmium "'
BRL
mg/L
0.025
0.00022
1
*6010C
8/14/14 17:09
BGM
P41-10192
Chromium
BRL
mg1L
0.25
0.0019
1
*6010C
8/14/14 17:09
BGM
P41-10192
Lead "'
BRL
mg/L,
0.050.
0.0028
1
*6010C
8114/14 17:09
BGM
P41-10192
Selenium
BRL
mg/L
0.10
. 0.018
1
*6010C
8/14/14 17:09
BGM
P41-10192
Silver
BRL
mg/L
0.25
0.0012
1
*6010C
8/14/14 17:09
BGM
P41­10192
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
ug/L
2.5
0.16
1
*8081B
8/14/14 3:16
JMV
P41­10214
Dieldrin
BRLA
ug/L
0.50
0.0046.
1
*8081B
8/15/14 1:25
JMV
P41­10214
Endrin
BRLA
ug/L
0.50
0.0046
1
*8081B
8/15/14 1:25
JMV
P41-10214
gamma-BHC
BRL
ug/L
0.50
0.0049
1
*8081B
8/15/14 1:25
JMV
P41-10214
Heptachlor
BRL
ug/L
0.50
0.0077
1
*8081B
8/15/14 1:25
JMV
P41­10214
Heptachlor Epoxide
BRL
ug/L
0.50
0.0046
1
*8081B
8/15/14 1:25
JMV
P41-10214
Methoxychlor
BRLA
ug/L
0.50
0.0087
1'
*8081B
8/15/14 1:25
JMV "
P41-10214
Toxaphene
BRLAa
ug/L
25
0.15,
1
*8081B
8/14/14 3:16
JMV
P41-10214
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
93 %
13-186
Tetrachloro-m-xylene
75 %
40-134
TCLP Semivolatile, Organic Compounds by GC/MS
2,4,5-Trichlorophenol ..
BRL
mg/L
0.25
0.012
1
*8270D
8/13/14 19:43
KC
P41-10170
2,4,6-Trichlorophenol
BRL
mg1L ._.
0.10
0.012
1
*8270D
8/13/14 19:43
KC .
P41-10170
.2,4-Dinitrotoluene
BRL
mg/L.
0.050
0.0048
1
*8270D
8/13/14 19:43
KC
P41-10170
2-Methylphenol'
"' BRL
mg/L
0.050
0.012
1
*8270D
0/13/14 19:43
KC
P41-10170
'3/4-Methylphenol
0.067
'mg/L
0.050
0.012
1
*8270D
8/13/14 19:43
KC
P4H0170
Hekachlorobenzene
BRL
rriglL
0.050
0.0070
1
*8270D
8113/14 19:43
KC
P41­10170
Hexachlorobutadiene
BRL
mg/L
0.050
0.011
1
*8270D
8/13/14 19:43
KC
P41-10170
Hexachloroethane
BRL
mg/L
0.050
0.0097
1
*8270D
8/13/14 19:43
KC
P41-10170
Nitrobenzene "
BRL
mg/L
0.050
0.0098
1
*8270D
8/13/14 19:43
KC
P41-10170
Pentachlorophenol,
BRL
mg/L.
0.25
0.0082
1
*8270D
.8/13/14 19:43
KC
P41-10170
This report should not be reproduced, except in its entirety,. Without the written'
consent of Prism Laboratories, Inc.
"
449 Springbrook'Road
-P.O. Boz:240543 -;Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529 6364 -Fax:
704/525-0409
Page
7 Of 32

Laboratory Report
® Full -Service Anal ticaI &
Environmental Solutions 08/18/2014
• • �'IABORATORIE$ ING ... . ' • . .. ' ' . ' . ' . • .
City of Statesville, NC Project: Sludge (Hazardous:Testing)_.- - Client .Sample ID: Fourth Creek Sludge
Attn: Andy Smith Prism Sample ID: 4070591-03
P.O. Box 1111 " Prism Work Order: 4070501
Statesville, NC 28687 SampleNa' trix: Solid- Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14:17:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pyridine
BRL
mg/L
0.25 0.016 •
1
*8270D 8/13/14 19:43
KC
P41-10170
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
99 %
49-109
2-Fluorobiphenyl
69 %
55-96
2-Fluorophenol
48 %
27-74
"
Nitrobenzene-d5
74 %
53-99
Phenol-d5
30 %
11-52
Terphenyl-d14
96 %
42-133
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
ug1L
35 0.78
1
*8260B 8/8/14 15:28
VHL
P41-10172
1,2-Dichloroethane
BRL
ug/L
25 1.4
1,.
*8260B 8/8/14 .15:28
VHL
P41-10172
1,4-Dichlorobenzene
BRL
u /L
380 0.68
1
*8260B 8/8/14 15:28
VHL
1341-10172
Benzene
BRL
ug/L
.25. 0.7.2.
1
*8260B 8/8/14 15:28
VHL
1341-10172
Carbon Tetrachloride
BRL
ug/L
25 1,2:
1
*8260B 8/8/14 15.28
VHL
P41-10172
Chlorobenzene
BRL
ug/L
5000 0.61..
1
*8260B 8/8/14 15:28...
VHL
P41-10172
Chloroform "'
BRL
ug/L
300 0.89
1
*8260B 8/8/14 15:28
VHL
P41-10172
Methyl Ethyl Ketone (276ufanone) BRL
ug/L
10000 9.0
1
*8260B 8/8/14 15:28
VHL
P41-10172
" Tetrachloroethylene
BRL
ug/L
35 0.69
1
*8260B 8/8/14 15:28
VHL
P41-10172
Trichloroethylene
BRL
uglL
25 0.54
1
*8260B 8/8/14 15:28
VHL
P41-10172
vinyl chloride
BRL
U. g/L
20 1:6,
1
*8260B 8/8/14 15:28,
VHL
P41-10172
Surrogate
Recovery
Control Limits
:. :.
4-Bromofluorobenzene
....
112 %
80-124
'Dibromofluoromethane
108 %
75-129
Toluene-d8
104 %
77-123
This report should not be reproduced, excerpt in its entirety,, without the writtenconsent of Prism Laboratories, Inc.
449, Springbrook'Road - P.O..
Box 240543 -charlotte, NC
2822,4-0543
Phone: [phone] - Toll Free
Number: 1-800/520-6364 - Fax: [phone]
Page
8 of 32

Sample Extraction Data .
. Prep Method: 1311
...
... ...
Lab Number =
Batch
Initial
Final
Daterrime
..: 4070501: 01 • .
P41-10120..:
"' 25
g
500' mL
" .. 08l07/14 15:35 "'
4070591-01
P41`10174
1000
mL
100Q mL
08/11/14,10:30
4070591=02
P41-10174
1000
mL
;1000 mL
08/11/14'16:30
4070591=02.
P4H0120'
:' 25
g ":'
"500. mL
""' 08/07/14 15:35 ..
:4070591-03 :.: ..
P.4H0174 .:
.. 1000:.
mL .
1000 mL ..
08/11/14 16:30
4070591-03 ' . ' ; ;
' p4H0120
25 ,
9
500 mL
08/07/14 15:35
Prep Method: 3010A
"
Lab Number
Batch : • :' • •
Initial
Final
Daterrime
4070591-01
P41-10192,
10
mL
„50 mL
08/12/14 14:50
4070591-02
P41-10192
10
mL
50 mL
08/12114:i4:50
4070591-03
P41-10192'
10
mL
50, mL
08/12/14 14:50'
Prep Method. 7470A
Lab Number:'
Batch
Initial
. ,
Final '
DatelTime
4070591.01 "
..
P4H0190. "'
..
20
.. 2
mL "'
30' mL
08/12/14 12:35' "' "'
.. .
4070591=02
P41-10190.
20
mL ".
"30 mL
08/12/14 12:35
407059
2
3
2351-03
Prep. Method: 3510C GC
..
' Lab'Number "' "'
' Batch
"' . " Initial
• "
"' Final " • "'
Daterrime
4070591-01
1341`10214
200;
mL,
10 'mL
08/13/14 13:00
4070591-01 "'
P41-10214
"' 200"ML
"' 10 mL
08/13/14 13:00
' .. 4070591.02.
. 1341-102.14' ..
200
mL :.: `
:'10. mL
'68/13/14 13:06
4070501-02
1341-10244 ..
200
mL
10 mL
08/13/14 13:00
40705.91-03
P41-10214• �
200
mL
10 mL
08/13/14 13:00
4070591=03,
P41-10714; •
200
mL
10 mL
08/13/14 13:00
Prep Method: 351OC MS
: Lab Number :
Batch
Initial
Final:,
Daterrime
4070591-01
P4H0170
200
mL "
1 _ mL"
08/12/14 13:30
4070591=02 "'..:'
P41-10170..:
.200
mL
"'..1 mL
.:08/12/14 13:30' "'
4070591-03
P41-10170
200
mL
1 mL
08/12/14,13:30
:. Prep Method: 5030B
L'abNumber "' :'
Batch
Initial'. •
"' :' Final "' •'
Daterrime
4070591-01
. P.4H0172
10 .rnL:
08/08/14 8:50 ;
;4070591-02 ;,;;;'
;P4H0172
V.rnL
10 mL;;'
08%08/14 8:50
4070591-03
P41-10172
1
mL
10 mL
08/08/14 8:50. ... ...
This report should not be reproduced, except in'its entirety, without the written'consent of Prism Laboratories, Inc.
:,449'Springbrook'Road-P.O.,B6is;240543-:Cha,lotte,NC28224-0543
Phone: [phone]-Toll Free -Number: 1-8001529-6364 - Fax: [phone] Page 9 of 32 ,

Subcontracted Analyses

"' ANN F CUSTODY
YESi:'. NOi.
tica &
:f
e a r'.-
I Ser I tr Fu I Y : �;=.
l'A �Tro 'isri'�airiVat.; .;
t le's IN G SMBarn P
ER eI1 LBRIQa: i?: - - ',
U04E N BO EPdSUreE PROPER !>. — --
OIUt1411S OF -- w -
$ a.
e to of n n PA v o m n Ir - r:
t Tem' T ICE. •�E
ee
N�i)d
Ri- )N
90RA 3, ..Jib.
u� me: � PEF{ PAES6R�ATH%ESindic2te�?`' ---
,a.•,<:.,•,, 28224-0543 . Project Na ,,-.:PRQ .—.—. y`.-
449 Springbro�k Road. ° P.O. Box 240543 . Charlotte, NC es No UST P1'oject:: (Yes) (No) •.:.;.-
Short.Nold Analysis (yes) ( ) Fiecefved:WITHIN:HOLOING TIMS7 `;' •.?-'_: :,
Phone:[phone] Fax:[phone]. t >>
B *Please ATTACK any project specific reporting (QC LEVEL:1 II III IV)
e.e t J
:..
Client Company Na1Te provisions and/or. QC Requirements '`VO
p ::VOIA�DLESrec'dWCU1'"-HEAD:SF'ACE?'.;,,',`:.:.:',`.,._T�T;;, .;"''✓
ray d arr
Report To/Contact N invoice To. .. .,PROPER GO,(V'TAIIVEi1S. �. -
/1 V
dress: �n +�, i�OX I
Reporting �±d _ . Address:
Sates tie qC .:
7011 APB- yas:
Purchase Order No:/Billing Reference:
Phon::7A`P (No):
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
y Y Y Certification:® NEI:AC ' USACEFL
Ell litll (Yes) (lV0) Email Address Requested Due Date ❑-1 Day ❑ 2 Days ❑ 3:Da s ❑ 4 Da s ❑ 5 Da s
NC
EDD Type: P®FP Excel —Other next buss t Be /
"Working Days" ❑ 6 9 Days ❑Standard 10 days" ❑ Rush orus SC OTHER
�•4v
p 4! t Samples.received after 15:00 will be processed business ay. .
Site Locatiion I�anie: .h erg- `� NO
Site - N w�;,•.,,
�� �q �dry Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES
Site Location Physical:Addir (SEE REVERSE FOR TERMS &CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES _ NO I't
jj I-
. .. EA d.'S'��" II a �C : RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) .
N A ALY$ES REQUESTED ' PRISM
TIME MATRIX - LE CONTAINER
SAMPLE LAB
CLIENT.: DATE COLLECTED (SOIL, P KSID RESERVA- ��^e� RE ''''••"
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 'TYPE TIVES
HOURS SLUDGE SEE BELOW-
NO. SIZE
7.
P1
-- -- --- — —'— ------ -- --_ �_G_i�' s�����j _--- —
10
s Si nature /� �t✓ �� Sampled By ( rint Name �►�' �/ Affiliation
Sampler g °
shire this Chain of Custody is your authorization for P i to proceed with I heanalyses
a haveubeendinitialized.ny changes must be .
Upon relinqul g�
submitted in writing to the Prism Project Manager. There will be cha s for any changes aft .Date Military/Hours Additional Comments:
Re
fished 8y: (Sig ure) - - Received 'Signature)
-:t
- Slto,`Deparxure' Tlme
Receiv B Si nature Date
e 1 ished By: (S azure) y' ( g -Field Cecli:Fee: _
-� - - Received For P s Laboratorfes_BY'J Date C - -
.. ulshed By: (Sign i n- f _ _ • Earle:' ,,.:.;: ,.::;.:; . -
` iVhi
j� _ C Group No.-
.� d of Shipment; E.'ALL SAMPL COOLERS SHOULD BE TAPED SHUT W TH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. C�Q „ ®� ��
Ex ❑UPS ❑ HandEdeAR NOT ACPEsm Field 9 VERIFIED IFIE ❑ GAINr ST:COC ��'fTl (iECEIVED AT THE LABORATORY. &J��JY
reiev ES: UST: GROUN®WATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LAN®FILL OTHER:
❑ SC ❑ NC ❑ SC ❑ NC ❑ SC a NC ❑ SC ❑ NC . ❑ SC I ❑ NO ❑ SC ❑ NC ❑ SC i `®.NC—❑ SC I �1NC ❑ SC ORIGINAL
RI f. jNAL
---- I ❑ __ ❑ --� ®-----
—=--
❑ ❑ =--- ❑ ---- r :C a ---- -
r C Clear G Glass .'P Plastic; TL = Teflon -Lined Cap VOA Volatile Organics Analysis (Zero Head Space) -- • r 11�
*rnr,IrAIM=P TVPE CODES: A = AmI7e •., ;, ,•
— s �•,.

Page 1 of 7
Page 13 of 32

X,' t:•:
RE6HAIV®= CUSTODY _ - -YE.S"
�-N
C
N rA .
_
r
"r 1 & BILLING, , Sa .` 1es iNTACT;vpon arr'iv.
Full -Service Analytical +r� 'Fui E # TO ENSURE PROPER BIL1L p ,..., _
MPAGE_ —. .. ,,.,^ < WET.ICE? s ,
Solutions, celved.ON - Environmental a,,, ......,., Env ;.:'
I S incliCafed'1'•
ESERVATIVE
�.
c.
QPERPR
E I n e: I m R S a =r To N O .,�, nn t N m.: ao Pr
oject u o s Pr (Y
es) )
.�.,L..�..�•�-. 1 T Pro ect: ( ) ( - LDING:TIR4B `'�
No US I -"ceivedWITNIN�HO
e NC 28217 Analysis: (Yes) ( . ): Re ,
r.�
Charlotte, Id
449.Springbrook Road • Cha , Short Ho y reporting QC:LEVEL 111111 IV) �`� ..s•:. : -
Phone[phone] • Fax: [phone] r i *Please ATTACH any project specific rep g ( CUSTQDY:SEALS,INTACT?
C, J:S > h P C:Re uirements i-VOLATILES[ecd_WIOU .HEADSPACE.
�. __
0 � .�'CGIt G. 1 � rovisions andlor-Q q �`:
Name: C r P Rs use
Na `:CONTAINS -
lent Company o PROt?�R tlx:` ; a; C
S 4 �+ .
�.� m , Invoke To: ,...
act Na :;,:,-_.-:,, r . 5�._C'ICorrS- t.
(port To/font TE::� TI In, `` ' Observed : r
Iporiing Address:.pr 0, Y�jdX 11 Address:.
S '/:/ /✓C BY CLIENTlSAMPLING PERSONNEL
es l�� TO BE FILLED IN
8ffj-3S13�' Fax Ye (No):`%dui"��y'� Purchase OrderNo.IBillingReference
Ication: NELAC DoD FL
NC
lone NIA;_
mall Address' Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Rush Work Must Be Certlf SC OTHERX.
"Working Days" ❑ 6-9 Days. ❑ Standard 10 days ❑Prc-Approved
®D Type: PDF_EXcel Other - iVO�
;:,•r:;
au `� Crn excluding weekends and holidays. Water Chlorinated: YES_
ite Location Name: r �/✓ Samples received after 14:00 will be processed next business day.
Turnaround time is based o business days, Sample Iced Upon Collection: YES,_ NO
(SEE REVERSE FOR TERMS 8 CONDITIONS REGARDING SERVICES - -
ite Location Physical Address: RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) ANALYSIS REQUESTED PRISM :y
�° LAB
TIME. MATRIX
REMARKS
SAMPLE CONTAINER _ID NO.
PRESERVA-
DATE COLLECTED : (SOIL, TIVES
CLIENT MILITARY WATER OR *TYPE NO. SIZE ?
SAMPLE DESCRIPTION COLLECTED HOURS .. SLUDGE) SEE BELOW �� h; P '
reC•7-30-1q,
Slu��s: z nr
re pp',
1A'•
Tic
Affiliation
Sampled By (Print Name)
Sampler's Signature /I
Chain of Custody is your authorization for P •sm for an cchanges aftea anlalyses have been iin t alized.ny changes mustDe
Additional Comments: Sife Arrival Time:
Upon relinquishing, this Date <
submitted in writing to the Prism Project Manager.. There will b Re ery By: (Signature) :�
!1 ��� Site Departure Time:`
Relin bed By: Sign ure) - Date:
e Received -By:( gnaure)
shed By: (Signature) Date -
-D Received For Prism Labora ries By:
ished By: (Signatur) -
(Q COC roue NO.
-
CD
�o S
fv of Shrpment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH C &TODY SEALS FOR TRANSPORTATION TO THE LABORATORY.
O SAMPLES ARE NOT A CEPTED AND VERIFIED AGAINST COC TIL RECEIVED AT THE LABORATORY.
CERCLA LANDFILL OTHER: °
IW Ex ❑ UPS ❑ Hand -delivered dsm Field Service ❑ OtterLID ❑ NC ❑ SC ❑ NC ❑ SC
g: UST: GROUND ER: - D NC I D S ATER- a NC ❑SC WASTE: ❑ NC ❑ SC I NC ❑ SC I ❑ I ❑
❑ SC ❑ NC ❑ SC ❑ NC ❑ S I ❑ I ❑ _ ORIGINAL
I _ VOA Organics Analysis (Zero Head Space) -
❑ ❑ --- ❑ - P -Plastic; TL Teflon Cap -Volatile
❑ -- ...,race. A c Arnii C = Clear G— Glass i'r?.............. ''f'

ISM
Ftill•Setvice Analytical &
1
=
_
.
{-,., i :•.
I
Environmental Soluliocis
.
lLABORATORIE%IYG q-
" SUBCONTRACT ORDER
"
Certification: ELAC_ iJSACE�
-
_
Prism Laboratories, Lte.
NG SC
Otiler
=_
4470591
NIA
SENDING LABORATORY
RECEIVING LABORATORY:
Prism Laboratories, Inc..
Analytical Environmental Services, Inc.
P. O. Box 240543
3785 Presidential Parkway
Charlotte, NC 28224-0543
Atlanta, GA 30340 .
Phone: 800-529=G364
Phone :[phone]
rat, 70�1-525-0�109 �
Fax: NA
-
Project Manager:' Robbi A: Jones
Analysis:' Due :'
);xpires Laboratot'•y iD Conmtents
SnngtleID:4Q70591-01 So1ic1 Saiiipled:07130/1,415:04`�
;e- •�r'F`'I
Herbicides TCLP (Sub)
09/06/14 15:04
Confainarx Supplied.
?�
Sample ID: 4070591-02 Solid
Sampled:07130/1415:04�s'
Herbicides TCLP (Sub)
08106/14.15:04
Corilaitier's Supplied.
Wir:'L� K S ADe
SampleID:.4070591-03 "' Solid
Sntnpled:07/30/I4 15:04
Herbicides TCLP (Sub)
08/06/14 15:04
Corrlairter x Supplied:
„
_31
Re case By ..
Date
Received By
Dale
,'Released By
0-1 •ILI
,,II
Date ',
Received,By 5
Date
Releit>ed By
Date,
Re eiyed fly
Date
Released fay
Page 2 of
Date .
Received By
...
Date
Page 14 of 3Z
i
i

_ _ _ = = = = -__ i=
• .. k3
N
e
Analytical' Environmental Services, Inc i)ate 8-Aug=14
Client: Prism Laboratories ample ID.
t`=
Client S STALIIdE
Lab Ordet' 1408083 Tag Nu - _
• : Projeet Name: ' 4.070591 " " "' Collection Date: 7/030/2014 3:04:0O PM
Lab ID: 1'408083-OOlA : Matrix: Solid
Analyses Result
Qual MDL
Rep
omit Units, Bateldl) DF
Date Analyzed 'Analyst
L
u_
' HERBICIDES, TCLP : SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex) BRL
0.039
0.20 mo(L 194388 .1
08/06/201412:21 RF
2,447 BRL
.. 0.042
0.20 rng/L, ]94388 1
08/06/201412:21 RF
k:
Surr: DCAA 79.2'
0 "' .'
40.3-135 REC 194388 1
OS/06/2014 12:21 RF
F
1
k
' . . ; .Qualifiers: Value exceeds inaximum coniamitiaht level
j
' ' E Estimated vitlue above quanfitation range
BRL Not Detected at hDL ..
S Spike Recovery outside limits due to matrix
.H
..:. Holding times forpreparation oraoalysis exceeded:. , : ,
� , Greater tltmt Result value
N Analyte not NELAG certified
••
I Estimatedvaluedetected below Reporting Limit...
... ..
• H .4na{3ae detected in the associated method blank
:'
Less th'ait Result value ..
...
Pa9 e 3 of
Page 157771

_
Analytical'Environmental Services, Inc Dated 8-Aug-14
Client: ' Prism Laboratories _ " ..Client Sample ID: THIRD CREEL{ SLUDGE
G�
Lab Order' 1408083 Tag Number: 4070591-02
Project Name: " 4070591 Collection Date: 7/30/2014 3:04:00 PM
Lab 1D: 1408083-002AMatrix:: Solid
Analyses
Result Qual
MDL
Reporting
Units.. BatchlD DF
Date Analyzed Analyst _
..Limit
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
"
" 2,4,5-TP (Silvex)
BRL
0.039
020 mg/L 194388.:: ' 1
08/06/2014 12:52 RF
24D "' "'
BRL .
0.042
tn
0.20 _ "'g/L 194388 1 .
08/06/2014 12:52 ' - RF
Stitt: DCAA
99.4
0
40.3-135 : %REC 194388 1
08/06/2014 12:52 RF
_Qunlifiers: Value exceeds maximum contaminant level
E 'Estimated talus above quantitation range
a 'BRL Not Detected at MDL
• •
S' ' Spike Recovery outside limits due to Snatrix
:H Holding time's:for preparation of analysis exceeded
:.::. :.::.
' ' Greater than Ruult talue ..
4
,
N Analyte'not NEL.AC certified
J Esumaled val ue detected Llel—Repot ung Li
ma,
' B Analyte detected in the associated medtod blank
-
- Less tliair Result value • • •
6'
"
. .
f7....
Page 0
Page 16 of 32,

-
,
....a �...:.,r.-,ra::-a.--::{.-._,":...._ e,?:-?". ,,•: �,-..r.-..^.•.•: r_-.:_ :vr.d g.:•ti-;3�'?_. _,_>.. r. ,.___,:,. ;.�: r:..o .. ,
Date: 8-Aug-14.:' l a
Analvtieal Environmental Sel-vice's; Inc
Result.
Qual MDL
.
Reporting:
Units... Batchfl) AF
Date Analyzed Analyst
Analyses . ..' "
Lim>It
HERBICIDES, TCLP. ': SW131118151r1
SW3510C)
. 2,4,5-TP'(S11vex) " ' ' ''BRL
: :0:039
0',20 mg/L:, 194388 1
08/06/2014'13:24 RF
BRL
0.042
'' 0.20 mg/L 194388 1
08/06/201413:24, RF
2,4-D.
"
Su1r: DCAA . ' • 89.3 "
... ...
: ' • , : 0 ' •
..
..
" 40.3-135 - ' . REC 194388 1
...
08/66/2014 13:24 : RF
I
i
. Qualifevs: value exceeds maximum contaminant level
s.
..
i
t
E Estimated valne'ah'ove quan[itation'range
"' "'
BRL Not Detected at MDL � � � �
�
Spikeoutsidelimrts tan.
� 5' Spik Recovery limits dtte,toa t t '
.. .... .. ..
.... - : H , Holding times.forpreparation or analysis exceeded: :: •
..
:.::.
ter e
>; . Grea tlto n Respl} value
..
... N ArtaNWnot NELAGcertifiM
"'
J Estimated value detected below Reporting Li
mit
6 :�,.lyl, detected in dte'associated method blank'
-
- Less Ihvi Result value
..
Page. 5.of 7
.
Page 17

Analytical Filsdivnitmental Setsices,;IIle.
Sample/Cooler Receipt Checklist
Work Order Number:�
Client :.
VINChecklist completed by ""' _
Si i`tu a e
( nrrier name: FedEx ✓:'UPS Courier— Client US Mail Other..:'
f
Yes No .:...Not Present. _.
Shipping container/cooler in good a.andition. ' —
Y. PP g...
Custod seals intant ott shi i❑ container/coole
� .. Yes — : No _ ' ' Not Present
Custody seals;infact oat sample bottles? .. Yes No Not Present —
Container/Temp l3lattk temperature ill compliance? (4°C±2)* Yes • No: _
Cooler f€1, . �� Cooler #2 Cooler #3 Cooler # 4 Coole'45 . Cooler #6
Chaiwof custody present? Yes No
:..
Chain bfcustody signed when relinquished and received? :..::Yes ::: No
Chain of custody agrees with sample labels? Yes'. No.
Samples in'prnper container/bottle? Yes No. ,
Sample. containers: i afnct? Yes No —
Sufficient saniple'vahtme for indicated test?: "Yes No
All samples: received within holding time? Yes No
Was TAT marked on the COC? Yes - fro:
Y N Not Applicable.
Yes: o — i A 1' lo:_
Proceed with Standard TAT as per project ]risto�y? _.
Water - VOA vaats.have zero headspace? No VOA vials submitted Yes _ No
Water , pH acceptable upon receipt?
Yes No Not rLpplicable
h d
C ecke .by
Sample Condltion; Good •� Otlier Es lain
'(For diffiisive'sanzples or AIHA lead) Is a known blank included? Yes No
See Case Narrative for resolution of the N0DrCo1Iforinaitc6.
Samples do nothave to rontpl} With the given;range for ecrtaiiiparAtneters. •
1I.}Quality AssurancelChecklists Procedures Sign -Oil TemptateslCheeklislstSample keceipt ChecklistMaS rple_Couler Receipt Checklist
Pa
f 32.
Page 18 o.

Sam lelD: MB-194388 -- :Client ID: Units; ::mg/L Prep Date: 08/04/2014 RugNo. 273052
HERBICIDES, TCLP sw131I1s151A BatchID: 194388 Analysis Date: 08/05/2014 . Seq No: 5761873
SampleTypc: MBLK TestCode: _.
Analyte Result .. RPT Limit SPK value SPK Ref Val %REC Low Limif : FIigli Lunit RPD Ref Val :: °/aRPD RPD Limit- Q.
2; l,5 TP (Silvex) BRL 0.20.
-2,4-D BRL 0.20
Surr: DCAA.. .. . 0.4440 0 0.5000 88.8 40.3 .135
2;4.5-TP:(SiIve-x) j0.3607
0.20
0.5000
72.1:
S5.2
125
2,4-D
0.3655
0.20
0.50.00
73'.1
49.8
128
Surr: DCAA ":
0.4938.:.:.:
0
0:5000
98135
8
40.3
,;•
2.4,5-TP (Silvex)
:::.:0.4163
0:20:
0.5000 83:3-
5.4 .
143:
2,4_D
0.4288..:.
0.20
0.5000 85.8
45
142
Surr: DCAA
0:5156 ...
0
0 10
.5000 3
40.3
li5
t;.
.. fy
:. ..
.
(Q
Qnnlificrs: -
- - - -
Greater than Result value ...
- .
< Less than Result value :
..
-
_
B Anal to detected in the associated method blank
- Y - -
_. -
(D
1
BRL
Below reporting _limit
- -
E Estimated (value above quantitation range)
preparation exceeded .. .
H Holding tin 'for prepara ' or analysis
times
J
Estimated value detected below Reporting Limit .
: -
N Analycer te not NELAC tified
- -
R RPD outside limits due to matrix -
_
RRpt Lim
Reporting Limit
S Spike Recovery outside limits due to matrix
e .
Page 7 of 7
0
-
-

r
.w.. ACCESS.:. '>
ANALYTICAL, ANC.
r
ANALYTICAL REPORT
CLIENT
Prism Laboratories Inc..
PO BOX 240543
Charlotte,:. NC 28224:
ATTENTION. .
Robbi Jones
PROJECT ID:
4070591
LABORATORY REPORT NUMBER
214080120
DATE .
08/05/2014.
.. .
Primary Data Review By Secondary,Data Review. By
... ... ... ...
... Ashley B. Amick,
Authorized Signature ..Project'Manager, Access Analytical, Inc.
:[e-mail]..
PLEASE. NOTE:
- Unless otherwise noted; all, analysis on this report performed•at Gulf Coast Analytical Labs (GCAL), 7979
Innovation Park Dr., Baton Rouge, LA 70820.
- GCAL is scDHEC certified laboratory # 73006, NCDENR certified lab # 618;:GA certified lab # LA-01955, NELAP
certified, laboratory # 01955
- Localsupport services for this project are provided by Access Analytical, Inc.. Access Analytical is a representative of
GCAL;serving clients in the SC/NC/GA areas. All questions regarding this report should be directed to your local'Access
Analytical representative at 803:781.4243 or toll -free at 888:315.4243.

-
Laboratory Endorsement
Sample analysis was 'performed:in,. accordance with approved methodologies, provided by the
Environmental Protection Agency or other recognized agencies. The samples and: their corresponding
extracts..will: be maintained for:.a period of 30. days unless otherwise arranged: Following' this retention
period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.
Common Abbreviations • Utilized in this Report, -
" ND Indicates the result was Not Detected at the specified RDL
DO Indicates the result was'Diluted Out
MI Indicates the result was subject to.Matrix Interference
TNTC Indicates fhe result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FL® Indicates the analysis was performed_ in the Field'
PQL Practical Quantitation Limit
MDL Method Detection Limit
RDL ..Reporting Detection Limit
00:00": Reported'as a time equivalent to 1.2:00 AM
Reporting Flags Utilized in this Report,
J Indicates the result is between the MDL'and RDL
U Indicates the compound was analyzed: for but not detected .:
B .. Indicates the analyte was ;detected in the.associated Method,Blank
Sample receipt -at GCAL is documented through the attached chain:of custody'. In accordarce with
NELAC, this report shall be: reproduced' only in full 'and with .the written' permission of GCAL: The results t:
contained within this reportrelate only to the samples reported. The documented results are 'presented'
within this report.
This report' pertairi.s' only to the samples listed in the Report Sample Summary.and should be retained: as
a Permanent record thereof. The results contained within this report are intended for the use of the client.
Any unauthorized, use of the.information, contained in this report is prohibited.
F
I.certify that this data package is in compliance:With the NELAC standard and terms: and conditions of the, "
" contract and Statement of'Work both.technically and for completeness' for other than ,the conditions in the .
case narrative. Release of the data contained in. this hardcopy data package. and in the
t;.
computer -readable :data submitted has been authorized by the .Quality Assurance Manager or his/her
designee, :as verified ,by the following signature.
Estimated uncertainty of measurement -is available' upon request. This, report is in, compliance, with the
DOD QSM as specified in the contract if applicable.:
i
i,
Naren Me4rAn .. .
Authorized. Signature.. "
GCAL REPORT 214080120 2
THIS REPORT CONTAINS~~ PAGES.
4 of13
""' Page 23 of 32

&z ..
_
4.
-
-
Report Sample Summary
=
GCAL ID : , Client ID Matrix
Collect Date/Time:
Receive,Date/Time .
21408012001 STALIME Solid ,,.
'07130/201415:04
08/01/201410:30' =='
214080.12002 THIRD CREEK SLUDGE Solid:.:
07/30/2014 15:04
08/01/2014 10:30
21408012003 FOURTH CREEK SLUDGE Solid..:
07/30/2014 15:04
08,/01/2014 10s30 =
GCRL.Report 214080120 .
5 of 13
Page 24 of 32
a

Sum, Mary of Compounds
Detected
There were no detects
=
GCALReport 214080.120
t:
6of13
Page 25 of 32 ::

. ... ... ... .. - - _ - ----_ - -- -
- a
:Client ... ...:rMatrkx,. . .. CollectDate/;i'ime:; r;'s;:;:'.=-�:-.:�.. ,ceiveDatefTime;�`:�:;':>:� '
GCALID.ID:.,:._,.:;,<:;'>= •;:• •
0/014`15:0'4::.: :''.::.":;';:.:_ 08%0172014:'1Oi30:;:'•::a"a:i.,;,-;'..<
21408012001 STALIME :: ;. ; ::
5olid,;, 07/3 ,2 .
EF
CAS#
Parameter
Result
RDL
MDL
Units
57-12-5R
Reactivity Cyanide
250lJ
25 0
250
I;<
m !k
9 9 _
EF

_ _- --
_- --
_ --
DatelTime;Receive Date/•fime;i,;='�_: '
=.: : Solid - ; 07/3072014,1504
.06W01/2014 10 30
21408012002 THIRD CREEK SLUDGE ,:; ., - , ,
,
EPA 7.3,3.2, Rev.3/9012B :.:..
Prep Date . Prep:Batch Prep;Method
Dilution Analyzed
By Analytical Batch
-
OS/0412014 11:30 538041 • • EPA 7.3.3.2
1 08/05/2014 08:00
DJH 538276
_
CAS# Parameter.
Result RDL
MDL
Units
57-12-5R Reactivity Cyanide
250U 250
250 .
mglkg
EPA 7.3.4.2, Rev. 3;/9034
Prep Date Prep Batch Prep Method
Dilution Analyzed
By Analytical Batch
1. 08/04/201411:30 538042 EPA7.3.4:2
1 08/05/201410:00'
'MDW 538287
CAS# ;' Parameter';' :;
Result RDL
MDL
Units
18496-25-8R' Reactivity Sulfide
80U SO
80;
mg/kg
:::RESULTS REPORTED ON.A WET WEIGHT BASIS

_. ... ...Ghent :.: .......:. .:.....:
atnx
.:.....:.:•.: MI
.: •_"'=:;Collect�atelTime•' ":Rece
:
214080.12003 ±'FOURTH:CREEK,SLUDGE,'.:,`::<'.`_-,r`:'
071,30/201415:04 08/01/20;141030,.
EPA 7.3.3.2, Rev 3/9012B
Prep Date . Prep Batch
Prep Method
Dilution Analyzed
.... .. .. .....
By Analytical Batch
08/04/2014 11:30, 538041
EPA 7.3.3.2
1 .08/0572014 08:01
DJH 538276
.CAS# Parameter.
Result RDL
MDL Units='
t-
57-.12-5R Reactivity Cyanide
2500 .. 250
250 mg/kg
A
• EF
Prep Date Prep Batch Prep:Method Dilution Analyzed By Analytical Batch
08/Q4/20141'1:30 538042 EPA 7.3.4.2 1 081051201410:00" MDW 538287

a
Analytical Batch- 538276
Client ID.
_MB538041 - -
- LCS53.8041
Prep Batch 53 . 804V
GCAL ID
1344024
-1344025 -- -----
Method EPA 7:3.3.2
Sample Type
Method -Blank
LCS
-Prep
a
Prep Date
08/642614 111:30
08104/2014.11:30
Analytical Date
08105/2014 07:26
08/05/2014 07:27
M 2 itrix:
:Solid
. . . .
EPA 7.3.3.2: Re.v.3/9012B :
. . Units mg/kg
a
Spike
Result:
R
- Cont - rol
Limits %R.
Result RDL
Added
57-12r5R Reactivity Cyanide
25OU 250
.250
34.5
14
25
Analytical Batch 538276
'Batch
Client ID
'BOX RBM250055, N48872 ...
13437.55DUP
Prep 638041
GCAIL ID
21407307301
44026
1344026
Prep Method - EPA 7.3-3.2
Sample Type
SAMPLE
DUP
--- -- -----
Prep b I ate-
08/0412014 11:30:
08104/20I_4_11:.30_:
Analytical Date
08/0512014 07:28
08/0512014 07:29
Matrix
Solid
Solid
EPA 7.3.3.2, Rev 3/90125s:
Units mg/kg
Result:
ROD
Limit
Result RDL
57-12-5R Reactivity Cyanide
250
0.0
0
201
q
w
w
w
w
a
w:
w
q
w
w
q
q
CD
GCAL Report 214080120
co
0
71
........................ ......

Analytical Batch 538287
Client ID
MB538042 w
LCS538042
Prep Batch 538042
GCAL ID
1344027
1344028
Prep Method EPA 73.4.2
Sample Type
Method Blank
LCS
Prep Date
08/041261411:30
08/04/2014 11:30
Analytical Date
08/05/2014:1.0:00
08105/201410:00.: "
Matrix
Solid a
Solid -
-
EPA 7.3.4.2, Rev.. 3/9034
Units :mg/kg
Spike
Result
Control
.Result. - RDL
Added
% R
Limits % R-
18496-25-8R Reactivity Sulfide: :: -,
80U 80:-
'1000
890
89
55 - 146
Analytical Batch 538287
Client ID
BOX RBM250055; N48872
1343755DUP
Prep Batch 538042
--- GCAL ID
21407307301 -
1344029
Prep Method EPA 7.3.41
Sample Type
SAMPLE i i
DUP
Prep Date
08/04/2014 11:30
08/04/201411:3.0
Analytical Date
:OB/05/2014 10:00
081051201410:00:
Matrix
Solid
Solid
EPA 7.3.4.2, Rev.-319034
Units":: mg/kg
Result
RPD
Result RDL
RPD
Limit
18496-25-8R -:-Reactivity Sulfide
0 80
0
0
25
t t;
CD
GCAL Report 214080.120
'sa
-
o
O
N
., - -;c:� .,.. ,,.�. �..�._�.., �, .: ,, ... :�. ,.
-,._�.......�........ ,.. ............... c,,.,..: ,.ms.,_T.. ,-..�.,-..r �. ....erg. �,. ....�..,..:.....,.,�

-
-- - _ - _ _ __ - '-- :i� _ _ __ _ _
•
'C 1, './iC i..r
l-AC
(f 5r• F
bo Z 6 . "
.. .... l_ C'illil__ mion: J-4f
"
C _—_ _ •�;
.....
1'Osii3 1-aborattlries, lne. ' _ o _
Omh r "
— - -- ---
SENDING G L:OBC)RA'I'C)1��`'
_RECLIV1NG.LABORA'1bRY:
PrisnrLaboratories, Inc.
..."' Gulf. Coast Analytical Labs, Inc.,
P. O.. Box 240543 .
7979:GSR1 Avenue
Charlotte, NC 23224-0543
Baton -Rouge, LA .70820
-_
Phone: 800 ��9=6364
Phone,:(22S) 769-1900
_
`c
'Fax: [phone]
Fax: [phone]t
Project DSanaJer: Robbi:A. Jones % 70.,-Z-
�I
-) 6 c! ,),'7 c% l'y '.
Analysis ::
Due Expires Laboratory 1D Comments
"
Sample .ID -407050-01
Solid.. Sampled:07/30/1415.04
Reactivity; Sulfide (Sub) .:'
08/06)1415;04 .' ....
Reactivity; Cyanide (Sub.)
08/1311415:04,
Containers Supplied:
SampW D: 4070591-02
Solid Sumpled:07/30(1,415:04
Reactipi%:SulNde.(Sub)
08/0611415:04
Reactivity, Cyanide (Sub)
0,8/13/14.15:04 .
Corstairrers'Supplied: ;
:1 yUi_R'UL:yiT p. -'Ya MnwTV..:. `L'•": 'M1. ^Vii '✓ G
-03
Solid Sam Ied-0730/1d�504Sample,1D:4070591
.
Reactivity, SulSde.(Sub)
0810611415;04
Reactivity, Cyanide. (Sub)
08/13/1415:04
Containers 5upplr'ed: .
Client ID: ,4565 - Access Analytical
SDG: 214 $d80,20
'' �����III� ��I������I��I��I�
Due Date: 08/0
•
/
.1r
It I asc By ... ::
D t
... .. Date Receive y a c
.
if
Released By
}
" Date,
Re ived By Date..'
• 'Released By
Date
Received By Date
Rc1r.Ltied By
Date ...
Rceeiyeo By Date
parre 2 of • ')
Page 31 of 32

.. ... -
. ..
Revision 1. { - - - - Page 1 of 1 ; ,y
CD
N -
O

Ra�
IS FuII=Service Analytical.&
Envifonmental Solutions
'/asum3 LABORATORIES, IN
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Cerlfication No. 402
SC Certification No. 99012
NC Drinldng water Cert No. 37735
VA Certification No. 460211
DOD ELAP: L-A-B Accredited Certificate No. L2307
ISO/I EC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 08/11/2014
Prism Work Order: 4080182
Case Narrative
08/20/2014
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224.OW
Phone: [phone] - Toll Free Number 1-8001529-6364 - Fax: [phone]

PP` 'R Full -Service Analytical &
IFFEIR' M M"I Environmental Solutions
M3 LABORATORIM INC: I ' -
Sample Receipt Summary
08/20/2014
Prism Work Order: 4080182
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
StaLime
4080182-01 Solid 08/11/14 08/11/14
Samples were received at 23.5 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-050
Phone: [phone] - Toll Free Number:1-8001529-8364 - Fax: [phone]

Laboratory Report
�:R- Full -Service Analytical ✓£ 08/20/2014
AAAIk -'l418,M Environmental SolutionsAOI SOEIAYORIES, INC.
City of Statesville, NC Project: StaLime Client Sample ID: StaLime
Attn: Andy Smith Prism Sample ID: 4080182-01
P.O. Box 1111 Prism Work Order: 4080182
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/11/1414:05
Time Submitted: 08/11/1417:25
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 62.9
% by
0.100
0.100 1
*SM2640 G 8M4114 16:20 MJO
P4H0259
Weight
Microbiological' Parameters
Fecal Colifonns BRL
MPN/g dry
0.3
1
*SM9221 E 8/12/14 12:50 MES
P4H0213
Total Metals
Mercury
0.34
mglkg dry
0.034
0.0056
1
*7471B
8M4114 12:14
BGM
P4H0206
Arsenic
!.1
mglkg dry
0.41
0.059
1
*6010C
8118114 23:23
BGM
P4H0204
Cadmium
BRL
mg/kg dry
0.41
0.0039
1
*6010C
8/18114 23:23
BGM
P41-10204
Copper
38
mglkg dry
0.81
0.010
1
*6010C
8M8/14 23:23
BGM
P4H0204
Lead
12
tn91kg dry
0.41
0.048
1
*6010C
8M8/14 23:23
BGM
P4H0204
Nickel
83
mg/kg dry
1.6
0.013
1
*6010C
snan4 23.23
BGM
P4H0204
Selenium
BRL
mg/kg dry
0.81
0.098
1
*6010C
8118/14 23:23
BGM
P4H0204
Zinc
78
mglkg dry
4.1
0.028
1
*6010C
8/18/14 23:23
BGM
P4H0204
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number 1-8001529-6364 - Fax: [phone]

L-lift
Full-Service Anal ical &
IS1 tl® Environmental Sutions
P'LABORATORIES, INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
8/20/14
Prism Work Order: 4080182
Time Submitted: 8/11/2014 5:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41­110204 - 3060B
Blank (P41-110204-BLK1)
Prepared: 08/13/14 Analyzed: 08/18/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4H0204-BSI)
Prepared: 08/13/14 Analyzed: 08/18/14
Arsenic
23.9
0.25
mg/kg wet
25.13 95 80-120
Cadmium
24.1
0.25
mg/kg wet
25.13 96 80-120
Copper
25.6
0.50
mg/kg wet
25.13 102 80-120
Lead
24.2
0.25
mg/kg wet
25.13 96 80-120
Nickel
23.8
1.0
mg/kg wet
25.13 95 80-120
Selenium
23.8
0.50
mg/kg wet
25.13 95 80-120
Zinc
23.9
2.5
mg/kg wet
25.13 95 80-120
Batch P4H0206 - 7471 B
Blank (1341-110206-BLK7) Prepared: 08/13/14 Analyzed: 08/14/14
Mercury BRL 0.020 mgikg wet
LCS (P4H0206-BSI) Prepared: 08/13/14 Analyzed: 08/14/14
Mercury 0.451 0.020 mg/kg wet 0.4167 108 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 -Fax: [phone] PA9e 4 Of 7,

' Level II QC Report
Full -Service Analytical &
R ISM Environmental Solutions $/20/14
LABOpATOPIE9, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime
Prism Work Order: 4080182
Time Submitted: 8/11/2014 5:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MOM - NO PREP
Blank (P4H0259-BLK1) Prepared & Analyzed: 08/14/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] t?agt? `Jr •,Of 7

` R�\ /q� -Full-Service Analytical &
�i d!
(�'y1
EmI
,'M„ Environmental Solutions
lk U SORATORIES ING
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level 11 QC Report
8/20/14
Prism Work Order: 4080182
Time Submitted: 8/11/2014 5:25:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41-110213 - NO PREP
Blank (P4H0213-BLK1) Prepared & Analyzed: 08/12/14
Fecal Cblifonns BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3060B
Lab Number Batch Initial Final Daternme
4080182-01 P41-10204
1.96 g 50 mL 08/13/14 9:40
Prep Method: 7471B
Lab Number Batch
Initial Final Daternme
4080182 01 P41-10206
0.56 g 50 mL 08/13/14 10:15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free,Number:1-800►529-6364 - Fax: [phone]

CHAIN OF CUSTODY RECORD
1 s
01
Rit'*: ISM
Full -Service Analytical &
Environmental Souons
I Solutions
# TO ENSURE
PAGE OF QE PROPER BILLING:�
='
3ampte's INTl
LABORATORIES, INC.
_-
RCCELVed UN WLT-
449 Springbrook Road Charlotte, NC 28217
Phone [phone] • Fax: [phone]
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
PROI'!rtR PRESERVATIVCS
`�6i HQ�DING
p g� tl
Client Company Name: e a f11 IT 511a t ese //f'
*Please ATTACH an project specific reporting (QC LEVEL I II III IV)
yr WITHIN TI-ME5?
GUSTODy'SEF1L31NTACT? �"
a
provisions and/or QC Requirements
✓;
Report To/Contact Name: A i9 4f I":4h -
Invoice To:
VC5LAT1LF3 reed lNlOUT-NEAD_6PACE?
Reporting Address: P £).09i° !dlj
Address'
FRGPccanfFAfN Rsused�
z j [c� °C /Corr. S
s ea. �e sy' `re Nc
7EMP Thetm ID Okserved:.`�f .°C
Phone: Y4V-879- 3gjj Fax es (No): ��i�l- 375 y �d` 5
purchase Order No./Billing? Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Entail Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC Do® FL NC
EDD Type: PDF_Excel Other
`Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Scpproved OTHER. N/A
_
Site Location Name: FCr + P
Samples received after 14:00 will be processed next business day.
Site Location Physical Address: �99' Re �� ✓ r�
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
,�j �fy •� �,$ grg ®® ��
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES NO
p P -
CLIENT SAMPLE DESCRIPTION
COLDLECTED ATE
TIME
COLLECTED
HOURS
MATRIX
WATER OR
SLUDGE)
SAMPLE CONTAINER
*TYPE NO- SIZE
SEE BELOW
PRTIV SVA
ANALYSIS REQUESTED
�
/fit' / REMARKS
PRISM
I MO
5.
E01
r
Sampler's Signature Sampled By (Print Name) a + C Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
a
Im
')f'
Comments:
SAMPLES ARE NOT ACCEPTED AND VERIFIED A121 OC UNTIL RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑ UPS ❑ Hand -delivered sm Field Service El OtheNPDES: UST: r 4� '�
ILL
El NC ❑ SC El NC ❑ SC LING El SCTER: El NC 1❑ SCATER. I LING
N SOLID ❑ SCE LING ❑ SC ❑ NC ❑ SC ❑ NC OTHER:F❑ SC I o NC ❑ SC
❑ I❑ ❑ ❑ ❑ ❑
:I *CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ORIGINAL

` ...
NC Certification No. 402
SC Certification No. 99012 ale Narrative
Full-Service Analytical &
P�RI MEnvironmental Solutions
NC Drinking Water Cert No. 37735
09/04/2014
VA Certification No. 460211
LABORATORIES, INC
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Andy Smith
P.O. Box 1111
Lab Submittal Date: 08/25/2014
Statesville, NC 28687
Prism Work Order: 4080489
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 1; of 14

Sample Receipt Summary
Pf'fi
Full -Service Analytigal &
Envircinmental Solutions
09/04/2014
y IAB6R GRIM
INQ
_
Prism Work Order: 4080489
Client Sample ID
Lab Sample ID
Matrix
Date Sampled Date Received
Sta-Lime
4080489-01
Solid
08/25/14
08/25/14
Sta-Lime
4080489-02
Solid
08/25/14
08/25/14
Sta-Lime
4080489-03
Solid
08/25/14
08/25/14
Sta-Lime
4080489-04
Solid
08/25/14
08/25/14
Sta-Lime
4080489-05
Solid
08/25/14
08/25/14
Sta-Lime
4080489-06
Solid
08/25/14
08/25/14
Sta-Lime
4080489-07
Solid
08/25/14
08/25/14
Samples were received at 30.7 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

H-Se
PER
I SM
Fuviron en Analytical &
ij��--_.'`�--11 Environmental Solutions
+i�U1BOAMON
Laboratory Report
09/04/2014
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Sta-Lime
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4080489-01
P.O. Box 1111 Prism Work Order: 4080489
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/25/14 10:50
Time Submitted: 08/25/1415:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Daterrime ID
General Chemistry Parameters
% Solids
64.2
% by
0.100
0.100
1
"SM2540 G
8127114 15:40
MJO
P411-10507
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
'SM9221 E
8/26114 10:44
JHB
P4H0489
Total Metals
Mercury
025
mglkg dry
0.031
0.0051
1
•7471B
8129114 12:53
BGM
P4H0508
Arsenic
4.7
mglkg dry
0.40
0.068
1
"6010C
912R4 20:61
BGM
P4H0471
Cadmium
BRL
mg/kg dry
0.40
0.0038
1
'6010C
912114 20:51
BGM
P4H0471
Copper
20 BH
mglkg dry
0.79
0.010
1
"6010C
912114 20:61
BGM
P41HI0471
Lead
5.9
mglkg dry
0.40
0.046
1
"6010C
912114 20:61
BGM
P4H0471
Nickel
70
mgll&y dry
1.6
0.013
1
•6010C
912M4 20:51
BGM
P4H0471
Selenium
BRL
mg/kg dry
0.79
0.096
1
'6010C
912114 20:51
BGM
P4H0471
Zinc
39
mglkg dry
4.0
0.027
1
`6010C
912114 20:51
BGM
P4H0471
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]

n,`� /n, ADM=
FUii-Service Analytical k
vir SM Enonmental Solutions
1A90 T.RIE3,INa-
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
09/04/2014
Client Sample ID: Sta-Lime
Prism Sample ID: 4080489-02
Prism Work Order: 4080489
Time Collected: 08/25/14 10:50
Time Submitted: 08/2511415:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 66.5
% by
0.100
0.100 1
'SM2540 G 8127114 15:40 MJO
P4H0507
Weight
Microbiological Parameters
Fecal Colifonns BRL
MPN/g dry
0.3
1
'SM9221 E 8126/14 10:44 JHB
P41-110489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643.- charlotte, NC 28224-050
Phone: [phone] - Toll Free Number:1-8001529-6364 = Fax: [phone] "<`::�:!i-

Ps`.� _ �/ Full -Service Analytical 8
_' n'
1 S tl , I Environmental Solutions
LAeogA OH.m ING
Laboratory Report
09/04/2014
City of Statesville, NC Project: StaLime (Qtrly, Biweekly, Client Sample ID: Sta-Lime
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4080489-03
P.O. Box 1111 Prism Work Order: 4080489
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/25/14 10:50
Time Submitted: 08/25/14 15:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date rime ID
General Chemistry Parameters
% Solids 70.3 % by 0.100 0.100 1 "SM2640 G 8127114 15,40 MJO P41­110507
Weight
Microbiological Parameters
Fecal Colifonns BRL MPN/g dry 0.3 1 'SM9221 E 8/26114 10:44 JHB P4H0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] P890 5 Of 14

ra. Laboratory Report
Full -Service Arialytical &
4
`"� vR�. I S'M - I Snv,ironmenial. Solutions 09/04/2014
V LABOR/1TOPIE3, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Sta-Lime
Prism Sample ID: 4080489-04
Prism Work Order: 4080489
Time Collected: 08/25/14 10:50
Time Submitted: 08/25/14 15:30
Parameter • Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datefrime ID
General Chemistry Parameters
% Solids 64.7 % by 0.100 0.100 1 'SM2640 G 8127114 15:40 MJO P4H0507
Weight
Microbiological Parameters
Fecal Colifonns BRL MPN/g dry 0.3 1 'SM9221 E 8/26114 10:44 JHB P41-10489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Chartotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] i�89es.Of 14

Laboratory Report
:�. 3 >`� Full -Service Analytical 8
N.R:E a I S M Environmental Solutions 09/04/2014
IABORHTOgtE:y INc.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Sta-Lime
Prism Sample ID: 4080489-05
Prism Work Order: 4080489
Time Collected: 08/25/14 10:50
Time Submitted: 08/25/1415:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Daterrime ID
General Chemistry Parameters
%Solids 70.2 % by 0.100 0.100 1 'SM2540G 8127114 15:40 MJO P4H0507
Weight
Microbiological Parameters
Fecal Colifonns BRL MPN/g dry 0.3
'SM9221 E 8/26114 10:44 JHB P41-10489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone, 7041529-6364 - Toll Free Number: 1-8001629-8364 01629-8364-Fax.,7041625-0409 Page7'Of 1�

Full -Service Analytical &
S M I Environmental Solutions
1 S.H 'E$ ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
09/04/2014
Client Sample ID: Sta-Lime
Prism Sample ID: 4080489-06
Prism work Order: 4080489
Time Collected: 08/25/14 10:50
Time Submitted: 08/25/1415:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
%, Solids 66.4
% by
0.100
0.100 1
*SM2540 G 8/27/14 16:40 MJO
P4H0507
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 8126/14 10:44 JHB
P41­10489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]A409 °Page: 8'.of 14, ,

Laboratory Report
I n Full -Service Analytical &
Environmental
Environmental Solutions 09/04/2014
1A90R�TOPIE3, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Sta-Lime
Prism Sample ID: 4080489-07
Prism Work Order: 4080489
Time Collected: 08/25/14 10:50
Time Submitted: 08/25/14 15:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Daterl ime ID
General Chemistry Parameters
% Solids 69.7 % by 0.100 0.100 1 "SM2640 G 8127114 15:40 MJO P4H0507
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 8/26114 10:44 JHB P41-10489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 9 .of 14

Full -Service Analytical &
�1.I S Environmental Solutions
A;B0nAT0FIES, INN
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaUme (Qtdy, Biweekly, 60Day
7 Fecal)
Level II QC Report
914/14
Prism Work Order: 4080489
Time Submitted: 8/25/2014 3:30:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4H0471 - 3050B
Blank (1341-10471-BLK7)
Prepared: 08/27/14 Analyzed: 09/02/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
BH
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mglkg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4H0471-BSI)
Prepared: 08/27/14 Analyzed: 09/02/14
Arsenic
22.1
0.25
mg/kg wet
25.00 88 M120
Cadmium
22.8
0.25
mg/kg wet
25.00 91 80-120
Copper
23.5
0.50
mg/kg wet
25.00 94 80-120
Lead
22.6
0.25
mglkg wet
25.00 90 80-120
Nickel
21.8
1.0
mg/kg wet
25.00 87 80-120
Selenium
22.4
0.50
mg/kg wet
25.00 89 80-120
Zinc
22.8
2.5
mg/kg wet
25.00 91 80-120
Batch P4H0508 - 7471 B
Blank (P41-10508-BLK7) Prepared: 08/28/14 Analyzed: 08/29/14
Mercury BRL 0.020 mg/kg wet
LCS (P41-10508-BSI) Prepared: 08/28/14 Analyzed: 08/29/14
Mercury 0.436 0.020 mg/kg wet 0.4167 105 80-120
Matrix Spike (P4H0508-MS1) Source: 4080489-01 Prepared: 08/28/14 Analyzed: 08/29/14
Mercury 0.826 0.031 mg/kg dry 0.6490 0.254 88 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: 704/62"499 Page TO Of 14

/A.G. i"
u_. i Full -Service Analytical &
I S Environmental Solutions
u uoartrOWEs, Wa
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: Stal-ime (Qtdy, Biweekly, 60Day
7 Fecal)
Level II QC Report
9/4/14
Prism Work Order: 4080489
Time Submitted: 8/25/2014 3:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4H0508 - 7471 B
Matrix Spike Dup (P41-10508-MSD1) Source: 4080489-01 Prepared: 08f28/14 Analyzed: 08/29/14
Mercury 0.933 0.031 mg/kg dry 0.6490 0.254 105 80-120 12 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] 'P6ge 1 llof•.1 4

Level 11 QC Report
M. i , Fu11-Service Anal ical & 9/4/14
�R i S M I Environmental Solutions
LA.0RATORIE$ INI- ,
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime (Qtdy, BiWeekly, 60Day
7 Fecal)
Prism Work Order: 4080489
Time Submitted: 8/25/2014 3:30:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41-10507 - NO PREP
Blank (P41-110507-BLK1) Prepared & Analyzed: 08/27/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box, 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] PBge 12 ,of l4I

,� `
F
Level II QC Report
k
j'
r�l�,
Full -Service Analytical &
9/4/14
V ■
` L;S0—T0AM%lNG
Environmental Solutions
City of Statesville, NC
Project: Stal-ime (Qtdy, Biweekly, 6013ay Prism Work Order: 4080489
Attn: Andy Smith
7 Fecal)
Time Submitted: 8/25/2014 3:30:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte
Result
Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41-110489 - NO PREP
Blank (P4H0489-BLK1)
Prepared & Analyzed: 08/26/14
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050B
Lab Number
Batch
Initial
Final DatelTime
4080489-01
P41-10471
1.97 g
50 mL 08/27/14 9:05
Prep Method: 7471B
Lab Number
Batch
Initial
Final Daternme
4080489-01
1341-10508
0.6 g
50 mL 08/28/14 9:40
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: 704152"409 Page 13 of 14

CHAMN OF CUSTODY RECORD
YES MO t
Full -Service Analytical
> R I S Environmental Solutions PAGE_ of _ QUOTE 9 To ENSURE PROPER BILLING:
1 ',i Is
INC.
-Samples INTAfi T upon amval? -.r+"
RBI.i'IVO'd1N VyET ICr.`k - - - _
10017201LABORATORIES.
Project
Name:
pRt7F1^F2 (�}�ESERVATiVES Iridtcated
449 Springbrook Road • Charlotte. NC 2$217 Short Hold Analysis: (Yes) (NO) UST Project: (Yes) (NO}
Phone [phone] Fax: [phone]
a *Please ATTACH any project specific reporting (QC LEVEL I II III IV)
Rr Qtved WITHiN Iit�LDiNG Ti(YiES?>-
�°°
Client Company Name: �, t 4e s9 d ��C y �P provisions and/or QC Requirements
CUSTr?GY.Ri ALS INTACT?
i
iLES W10UTHEADSPACE?
To/Contact Name: J�N • w rs�i,�
Report Invoice To:
Val: reed
Reporting Address: F1 x �GN9 Address:
T[yiP Therm iD
Phone:7,1-1-87?- 3438 Fax es NO): 717 ' �� ''b� Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC
re App Work Be
EDD Type: PDF_Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
SC OTHER NIA
r° Ce. &.e. Ctrs W rp Samples received after 14:00 will be processed next business day.
Site Location Name: f;
- Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO_
Site Location Physical Address: a"a s' d �
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES_ NO_
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME
MATRIX
SAMPLE CONTAINER
ANALYSISEQUESTED
PRISM
LAB
LIENT
CLIENT
C
DATE
COLLECTED
(SOIL,
PRESERVA-
TIVES
is REMARKS
ID NO.
*TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
NO.
SIZE�i.
HOURS
SLUDGE)
SEE BELOW
6 dg
p�y
A
r,>� ,° c°.9C r
r 9
(- �-
I
Samplers Signature �I'r'ax.r Sampled By (Print Name) m�-dk I Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above Any changes must be
submitted in writing to the Prism Project Manager. There will be arges for any changes after analyses have been initialized. Date MIKER ulshed By: (Signature By (Sign tur )
�ama
ate
rC
_ y: (Signatur
ROIi Ish�gy: (Signatu`re�)j�,� (�
MetnoaOTsnlpmanT: roU -- --
SAMPLES ARE NoCEPTED AND VERIFIED AGAINST C0e TIL RECEIVED AT THE LABORATORY.
r
SAMPLES ARE No❑ Fed Ex ❑ UPS ❑ Hand delivered P sm Field Service ❑ Other
1-10 0, N so
NPDES: I Uts I: u vurvvvvxr cn. r . -••• --- - - - -
❑NC❑SC ❑NC ❑SC ❑ C ❑SC ❑NC ❑SC ❑NC ❑SC ElNC❑SC I ❑NC ❑SC I ❑NC ❑SC I El NC
Q SC
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Comments:
3 SEE REVERSEFORy a
,r-T,ERMS,„„$CONDIT,IONS r^,
ORIGINAL

[1� Full -Service Analytical &
P I �d M Environmental Solutions
�LABORATORIES, INC. ,
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinldng Water Cart No. 37735
VA Certification No. 460211
DOD ELAP: L-A-B Accredited Certificate No. L2307
ISOIIEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 09/08/2014
Prism Work Order: 4090114
Case Narrative
09/19/2014
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each'sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
Data Qualifflers Key Reference:
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results. reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not'be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: 704I525-0408

w � �/ p� Full -Service Analytical &
aR R I S I Y I I Environmental Solutions
'1 L4wM 1M IN0.
Sample Receipt Summary
09/19/2014
Prism Work Order: 4090114
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime
4090114-01 Solid 09/08/14 09/08/14
Samples were received at 21.9 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: 704152"409 Page Z Of, 7

Laboratory Report
Full -Service Analytical &
IS I .Environmental Solutions. 09/19/2014
v UABOR1170RIE5,'ING
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4090114-01
P.O. Box 1111 Prism Work Order: 4090114
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 09/08/14 10:15
Time Submitted: 09/0811412:25
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Datelrime
ID
General Chemistry Parameters
% Solids 73.2
% by
0.100
0.100 1
*SM2540 G 9n 0114 15:05 JAB
P410166
Weight
Microbiological Parameters
Fecal Colifonns BRL
MPN/g dry
0.3
1
*SM9221 E 9/9114 9:20 JHB
P410134
Total Metals
Mercury
0.18
mglkg dry
0.029
0.0047
1
'7471B
9M7114 15:30
BGM
P410167
Arsenic
3.9
mglkg dry
0.34
0.050
1
*6010C
9M3M4 0:26
BGM
P410146
Cadmium
BRL
mg/kg dry
0.34
0.0033
1
*6010C
9113114 0:26
BGM
P410146
Copper
17
mg►kg dry
0.69
0.0086
1
*6010C
9n3M4 0:26
BGM
P410146
Lead
5.8
mg/kg dry
0.34
0.040
1
*6010C
9M3M4 0:26
BGM
P410146
Nickel
63
mgnM dry
1.4
0.011
1
*6010C
9M3114 0:26
BGM
P410146
Selenium
BRL
mg/kg dry
0.69
0.083
1
*6010C
9113114 0:26
BGM
P410146
Zinc
28
mg/kg dry
3A
0.023
1
*6010C
9M3M4 0:26
BGM
P410146
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-050
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

� /q� Full -Service Analytical &
m3 I S I V f I Environmental Solutions
�LABORATORIE$ INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P410146 - 3050B
Project: Stal-ime
Level II QC Report
9/19/14
Prism Work Order: 4090114
Time Submitted: 9/8/2014 12:25:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P410146-BLK1)
Prepared: 09M 0114 Analyzed: 09/12/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS(P410146-BSI)
Prepared: 09M 0/14 Analyzed: 09/12/14
Arsenic
22.2
0.25
mg/kg wet
25.00 89 80-120
Cadmium
22.4
0.25
mg/kg wet
25.00 90 80-120
Copper
23.5
0.50
mg/kg wet
25.00 94 80-120
Lead
22.2
0.25
mg/kg wet
25.00 89 80-120
Nickel
22.0
1.0
mg/kg wet
25.00 88 80-120
Selenium
22.0
0.50
mg/kg wet
25.00 88 80-120
Zinc
22.8
2.5
mg/kg wet
25.00 91 80-120
Batch P410167 - 7471 B
Blank (P410167-BLK1) Prepared & Analyzed: 09/17/14
Mercury BRL 0.020 mg/kg wet
LCS (P410167-BSI) Prepared & Analyzed: 09/17/14
Mercury 0.469 0.020 mg/kg wet 0.4167 112 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-050
Phone: 704152"364 - Toll Free Number:1-8001629-6364 - Fax: [phone] Page 4 Of 7

PAIR
R
�/ A� Full -Service Analytical &
Is t .Environmental 5olutibns
LABOR(SORIES INC.
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
9/19/14
Prism Work Order: 4090114
Time Submitted: 9/8/2014 12:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P410166 - Solids, Dry Weight
Blank (P410165-BLK1) Prepared & Analyzed: 09/10/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

P.x � Full -Service Analytical &
�,I M Environmental Solutions
��LABOflATORIES ING
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
9119114
Prism Work Order: 4090114
Time Submitted: 9/8/2014 12:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P410134 - NO PREP
Blank (P410134-BLK7) Prepared & Analyzed: 09/09/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final
DatelTme
4090114-01 P410165
30 g
30 g
09/10/14 15:05
Prep Method: 3050B
Lab Number Batch
Initial
Final
Daternme
4090114-01 P410146
1.99 g
50 mL
09/10/14 8:45
Prep Method: 7471E
Lab Number Batch
Initial
Final
DateTme
4090114-01 P410167 0.57 g 50 mL 09/17/14 11:40
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: 704162"409 'Rage- 6 Of 7

CHAIN OF CUSTODY RECORD
figs Full -Service Analytical & kS KO NIA
zt+ Environmental Solutions PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING: Saninles H FACT UpOp arrival O.
}LA80RATORIES INC.
_ ,. S;r .J.cSni �dir_a, Inco= _. ,: �">•".'"�. .;, .- r,°
449 Springbrook Road • Charlotte, NC 29217
Phone [phone] - Fax:[phone]
Client Company Name: 4v J WA' —<,. velld
_� Jr' Report To/Contact Name: �;ti+,A =d 6.�.
Reporting Address: PiOi BOA' 111 g
Project Name:
Short Hold Analysis. (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
Phone:%,1`I- 919-3q3''' Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD
FL NC
EDD Type: PDF_Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must BePre-
Site Location Name: a i A'lv Cr c ell WLQ TV Samples received after 14:00 will be processed next business day.
Site Location Physical Address:03 v ii A~ -rr# t 6 Turnaround time Is based on business days, excluding weekends and holidays.
i (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Scpproved OTHER
Water Chlorinated: YES_ NO_
Sample Iced Upon Collection' YES—
p i�
NIA
NO
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
PRTIVES -
TIVES
ANALYSIS REQUESTED
REMARKS
fi 'yt
tq'aa
<`Be
PRISM
LAB
ID NO.
"TYPE
SEE BELOW
NO.
SIZE
'eta .'
'— '� 1
< : 11
S
P
4.2 - 3
'...
01V =Y. -'
d
"Ja
�3
a14
p"y-
dffi' D8
Sampler's Signature) r Sampled By (Print Name) 16 IA Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.+'
s' '
emq s e y: Igne rta ec v By: Signature Da
Reltnp ed By: (Signature) Received By: (Signature) Date I
Relin : (Signatu Received For s Laboratori y: Date
Mili/Hours Additional Comments:
site'Arrival'7irria:
"Site
. Pleld.,%ph:e�_
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH ODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST COC IL RECEIVED AT THE LABORATORY.
40011LI
❑ Fed Ex ❑ UPS ❑ Hand -delivered ,ism Field Service ElOther
NPDES: UST G NDWATER: DRINKING WATER: I SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
MEN
❑NC❑SCI El NC ❑SCI❑❑ C ❑SC I ®NC El SC QNC ❑SC I UNC❑SC oNC ®SCI QNC ❑SCI
®NC ❑SC
11
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) Or'G INA1

pp Full<Service Analytical; &
n
1 I S I .Y 1. J.'
'. Environmental Solutions
�LAeORATORIES, INC
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
IS01IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 09/23/2014
Prism Work Order: 4090361
Case Narrative
10/01/2014
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Janes
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

B.Al
� 2TOR
Full -Service Analytical &NQ
� Environmental, Solutions
IFA
Sample Receipt Summary
10/01/2014
Prism Work Order: 4090361
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta Lime
4090361-01 Solid 09/22/14 09/23/14
Samples were received at 21.3 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Sprin®brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - ToU Free Number:1-8001529-6364 - Fax: [phone]

A.„6
Laboratory Report
ACREi:'-5
""R"��__
I.S
FulbService Analytical'&-
I Environmental Solutions
10101/2014
`i` W00RATOFIESO.C','
City of Statesville, NC Project: Stal-ime
Client Sample ID: Sta Lime
Attn: Andy Smith
Prism Sample ID: 4090361-01
P.O. Box 1111
Prism Work Order: 4090361
Statesville, NC 28687 Sample Matrix: Solid
Time Collected: 09/22/14 11:00
Time Submitted: 09123/1410:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Daterrime
ID
General Chemistry Parameters
% Solids
77.6.
% by
0.100
0.100
1
*SM2540 G
9124114 15:00
MJO
P410379
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPNlg dry
0.3
1
*SM9221 E
9123/14 10:33
JHB
P410367
Total Metals
Mercury
0.13
mglkg dry
0.027
0.0045
1
*7471113
9126114 15:06
BGM
P410406
Arsenic
4.6 •
mg►kg dry
0.32
0.046
1
*6010C
9/29/14 16:07
BGM
P410413
Cadmium
BRL
mglkg dry
0.32
0.0030
1
*6010C
9/29114 16:07
BGM
P410413
Copper
27
mglkg dry
0.63
0.0080
1
*6010C
9129114 16:07
BGM
P410413
Lead
5.3
mglkg dry
0.32
0.037
1
*6010C
929114 16:07
BGM
P410413
Nickel
84 BH
mg►kg dry
1.3
0.010
1
*6010C
9129114 16:07
BGM
P410413
Selenium
2.2
mglkg dry
0.63
0:077
1
*6010C
9129114 16:01
BGM
P410413
Zinc
41 BH
mglkg dry
3.2
0.022
1
*6019c
9/29114 16:07
BGM
P410413
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] � 'Pado'3 OM;>_'

Ll-bgm
`�'1 ppg\� /A,Full-Service AnalyticalR' S tl ,� I Environmental Solutions
�- .0RATOHIE9. INQ
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P410406 - 7471 B
Project: StaLime
Reporting
Result Limit Units
Level 11 QC Report
1011/14
Prism Work Order: 4090361
Time Submitted: 9/23/2014 10:05:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P410406-BLK1) Prepared & Analyzed: 09/26/14
Mercury BRL 0.020 mg/kg wet
LCS (P410406-BSI) Prepared & Analyzed: 09/26/14
Mercury 0.471 0.020 mg/kg wet 0.4167 113 80-120
Batch P410413 - 3060B
Blank (P410413-BLK1)
Prepared: 09/26/14 Analyzed: 09/29/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
2.44
1.0
mg/kg wet
BH
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
BH
LCS (P410413-BSI)
Prepared. 09/26/14 Analyzed: 09/29/14
Arsenic
24.2
0.25
mg/kg wet
25.00 97 80-120
Cadmium
24.2
0.26
mg/kg wet
25.00 97 80-120
Copper
25.8
0.50
mg/kg wet
25.00 103 80-120
Lead
24.1
0.25
mg/kg wet
25.00 96 80.120
Nickel
24.3
1.0
mg/kg wet
25.00 97 80-120
Selenium
24.2
0.50
mg/kg wet
25.00 97 80-120
Zinc
25.5
2.5
mg/kg wet
25.00 102 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springhrook Road - P.O. Box 240543 - Charlotte, NC 28224-CM
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: 704152&4409

Pr"> �/ p� Full=Se"lcs Analytical $
R,I S 9 �V : I Environmental Solutions
LAEOPATOPIEs, ING' " '
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
10/1/14
Prism Work Order: 4090361
Time Submitted: 9/23/2014 10:05:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P410379 - Solids, Dry Weight
Blank (P410379-BLK1) Prepared & Analyzed: 09/24/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364- Fax: 704f525-0409 TF "%{78QeSpQf=�'

t, r;"'i?�FUI1=Service Analytical 8
'P,a;R I M 'I r Environmental Solutions
LABOR�TOPIE$ ING'
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level 11 QC Report
1011/14
Prism Work Order: 4090361
Time Submitted: 9/23/2014 10:05:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P410367 - NO PREP
Blank (P410367-BLK7) Prepared & Analyzed: 09/23/14
Fecal Colifonns BRL 0.2 MPNJg wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Daternme
4090361-01 P410379 30 g 30 g 09/24/14 15:00
Prep Method: 3050B
Lab Number Hatch Initial Final Dateriime
4090361-01 P410413 2.03 g 50 mL 09/26/14 9:00
Prep Method: 7471B
Lab Number Batch Initial Final DatelTme
4090361-01 P410406 0.57 g 50 mL 09/26/14 10:28
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number.1-800/529-6304 - Fax: 704/52S*409

�_.
> �. =- � � Full -Service Analytical &
Environmental Solutions
"I ABORATOMES INC.
449 Springbrook Road ^ Charlotte, NC 28217
Phone [phone] Fax: [phone]
Client Company Name: C Te> of st'IA` l s v> Ite
Report To/Contact Name: 11R
Reporting Address: S/P JP� , "N. 01 n
�0'4'1�f.:M d.•9ii1NP ,4C
a s�• fir 3 �'� :d � '*°�. �� �r ���?�*1� �=�"' �., "� , "fad � „, )�
PAGE_ OF _ QUOTE 9 TO ENSURE PROPER BILLING.,
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
"Please ATTACH any project specific reporting (QC LEVEL I If Ili IV)
provisions and/or QC Requirements
Invoice To:
Address:
Phone.7f14•, 67l'- 34'3T Fax Yes (No):10f 307$' 14,55 purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD
FL NC
EDD Type: PDF_Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ RusPre-Approved hWork Must Be
SC OTHER
NIA
Site Location Name: Samples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays.
dater Chlorinated: YES_ NO_
Site Location Physical Address:
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection YES
p l3 :
NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSIS REQUESTED
�� REMARKS
PRISM
LAB
CLIENT
TIVES
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
'TYPE
NO.
SIZE
C���
ID NO.
HOURS
SLUDGE)
SEE BELOW
e
R fe
W ,.
Sampler's Signature /t . Sampled By (Print Name) y t'rAffiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
o .
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized
Relin fished By: (Signat ej Re ued By: (Signal ) to
Mil aryl ours Additional Comments:
Stefirrivai>Tia,.°..;.:
Rel�n ed By: (Signature) R y: (Signature) ate)f0,f.18¢attUfe
Re q By: (SI, re) Received F Prism Labor rie By: Date
�(;•f3S
,d,TP,C;iI:F>r_82.:`:.;:;�;::.;;;--;?,
JI1Aileage;.:,sj;..",=r'.::`.;�f'}::
f,, J-!( �� lL%
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT 'CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. C C G up No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST 0C UNTIL RECEIVED AT THE LABORATORY.
Nitri'/ `IV �I o 5
U 4
❑ Fed Ex ❑ UPS ❑ Hand -delivered ' 'sm Field Service ❑ Other
NPDES: I UST: GR UNDWATER: DRINKING ViATER: SOLID WASTE: RCRA: CERCLA LANDFILL
OTHER:
r
❑NC®SC ❑NC ❑SC ❑N ❑SC I UNO El SO ONO LUSO ®NCLISC 0NO ❑SCIElNO ❑SO
❑❑NC QSC
n n ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ORK INAL

NC Certification No. 402 Case Narrative
SC Certification No. 99012
a
' Full -Service Analytical & NC Drinldng Water Cert No. 37735
z 1011412014
P 3 I SIR� I Environmental Solutions VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 10/07/2014
Statesville, NC 28687 Prism Work Order: 4100092
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: 704152"409

!RRFull -Service Analytical &
I oss, I .En'vironmental Solutions
Sample Receipt Summary
10/14/2014
Prism Work Order: 4100092
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime
4100092-01 Solid 10/06/14 10/07/14
Samples were received at 19.9 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number.1-8001529-6364 - Fax: [phone]

F ,y
.o Laboratory Report
Full -Service Analytical 8
�PdI I S M I Environmental Solutions 10/14/2014
.� LABORATOR10% ING
City of Statesville, NC Project: Stal-ime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4100092-01
P.O. Box 1111 Prism Work Order: 4100092
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 10/06/14 12:20
Time Submitted: 10/07/14 07:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Datefrime
ID
General Chemistry Parameters
% Solids 69.0
% by
0.100
0.100 1
'SM2640 G 1017/14 17:05 MJO
KJ0104
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 10f7/14 11:52 JHB
P4J0161
Total Metals
Mercury
0.31
mgfkg dry
0.029
0.0049
1
•7471B
1018114 13:21
BGM
P4J0093
Arsenic
4.6
mglkg dry
0.37
0.064
1
"6010C
10/11/14 1:25
BGM
PQ0125
Cadmium
BRL
mglkg dry
0.37
0.0035
1
'6010C
10/11/14 1:25
BGM
P4J0125
Copper
16
mglkg dry
0.74
0.0093
1
•6010C
10/11/14 1:25
BGM
P4J0125
Lead
6.0
mglkg dry
0.37
0.043
1
*6010C
10/11/14 1.25
BGM
P4J0125
Nickel
63
mglkg dry
1.6
0.012
1
"6010C
10/11/14 1:25
BGM
P4J0125
Selenium
BRL
mgikg dry
0.74
0.089
1
•6010C
10/11/14 1:25
BGM
P4J0125
Zinc
29
mglkg dry
3.7
0.025
1
•6010C
1011V74 1:26
BGM
P4J0125
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number:1-800/529-6364 - Fax: [phone] Pi ge.3 Of 77,

A Full=Service Analy4ical &
`stRR �R. ISM I Environmental Solutions
Y IA90PATONIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P4JO093 - 7471B
Project: Stal-ime
Reporting
Result Limit Units
Level II QC Report
10/14/14
Prism Work Order. 4100092
Time Submitted: 10/7/2014 7:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (124J0093-BLK1) Prepared: 10/07/14 Analyzed: 10/08/14
Mercury BRL 0.020. mg/kg wet
LCS (P4J0093-BSI) Prepared: 10/07/14 Analyzed: 10/08/14
Mercury 0.441 U20 mg/kg wet 0.4167 106 80-120
Batch 134J0125 - 3050B
Blank (134J0125-BLK1)
Prepared: 10/09/14 Analyzed: 10/11/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P"0125-BSI)
Prepared: 10/09/14 Analyzed: 10/11/14
Arsenic
25.0
0.25
mg/kg wet
25.00 100 80-120
Cadmium
25.5
0.25
mg/kg wet
25.00 102 80-120
Copper
26.2
0.50
mg/kg wet
25.00 105 80-120
Lead
25.3
0.25
mg/kg wet
25.00 101 80-120
Nickel
25.2
1.0
mg/kg wet
25.00 101 80-120
Selenium
25.3
0.50
mg1 kg wet
25.00 101 80-120
Zinc
25.9
2.5
mg1 kg wet
25.00 104 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-OM
Phone: [phone] -Toll FreeNumber: 1-8001529-6364-Fax:[phone]

iL�i�t-I
MI
Full -Service Analytical &
� Environmental Solutions
EvIADONATORIE$ INC,
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
10/14/14
Prism Work Order: 4100092
Time Submitted: 10/7/2014 7:00:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4J0104 - Solids, Dry Weight
Blank (P4J0104-BLK1) Prepared & Analyzed: 10/07/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] page-5 of 7

_ gyp\ //�� Full -Service Analytical.&
RR I S I Y I Environmental Solutions
''�iaBonnTaBlEa ING "
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
10/14/14
Prism Work Order: 4100092
Time Submitted: 10/7/2014 7:00:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MOM - NO PREP
Blank (P4J0161-BLK1) Prepared & Analyzed: 10/07/14
Fecal Colifonns BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Daternme
4100092 01
P4.10104
30 g
30 g
10/07/14 17:05
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Datemme
4100092-01
P4J0125
1.97 g
50 mL
10109/14 8:00
Prep Method: 7471B
Lab Number
Batch
Initial
Final
DateMme
4100092-01
134J0093
0.59 g
50 mL
10/07/14 13:20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll FreeNumber: 1-800►529-6364-Fax:[phone]

sow:. CHAIN OF 0111ST®®Y RECORD
ty, l Full -Service Analytical & YFS NO NrA nF
�« - I Environmenta9 Solutions PAGE OF QUOTE # TO frH�sURE PtaoPE9t BILLIWG: p`
a SBmplas INTACT upon atrlvafg
:.
§... s..���R4 s LkBOAATOAlES, INC. ..-rJa.:�n,arl !'1h1iAiG:i:. if-`F'7 •_ .. - :. ..:'.. .._ 1✓; :, l�
449 Springbrook Road - Charlotte, NC 28217
Phone [phone] - Fax: [phone] d
Client Company Name: C + ky n a c-s' I�^-71e
Report To/Contact Name: A o 51�i; A
Reporting Address: • 0, yB+oy lio
64c
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 111111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
Phone:'7oq- V1 e-3g39, Fax; es (No):70 4-1?78- 9L,, s5 Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL.
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days 113 Days ❑ 4 Days O 5 Days
Certification: NELAC DOD
FL NC
EDD Type: PDF_Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush WoorkMust Be
Name: frtaz' 4l O'Ct;x 'Cow r business day.
SC OTHER
N/AS
ite Location Samples received after 14:00 will be processed next
Site Location Physical Address: 03Be, It j'�,, )?,R. Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
^.�au +s w"+��%a"
(SEE REVERSE FOR TERMS & CONDFTIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES
NO
TIME
MATRIX
SAMPLE CONTAINER
, ANALYSIS
REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
y
REMARKS
LAB
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
*TYPE
NO.
SIZE
TIVES
!„�;_, tl
ID NO
SLUDGE)
SEE BELOW
.� " r•a.r>>"a-'s
i�% -l-%'7
yHOURS
�M : K
"
� p �S�,a�
14tc1 SrR 4�.
fw''
r
f .
C
S
Y
ry
Ph
I
A,1, Z "F 0 r
Sampler's Signature Sampled By
(Print Name) ti>' r;ot Affiliation
Upon relinquishing, this Chain of`ustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
q "
submitted in writing to the Prism Project Manager, There will be, charges for any changes after analyses have been initialized.
1
Reliny, 'shed By: (Signature R c '
ed By: Signatur Date
Military/Hours Additional Comments:SiteArriva(�Tinie;.';;°;�
.•'<�`'.,;=�,,
Relinggl hed 8y: (Signature)
y: (Signature) - ate
.;5it6;Departure..:TJn18 --5,r : a. ;;
Relln y: (Signatur i Re
d For Prism oratories By: Date
Method of Shipment NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WI H CUSTODY DEALS FOR TRANSPORTATION TO THE LABORATORY, COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST C ,UNTIL
RE IVED AT THE LABORATORY.
/11
❑ Fed Ex ❑ UPS ❑ Hand -delivered P sm Field Service ❑ Other
/
�{ 0 0
NPDES: I UST: G NDWATER: DRINKING ViATER: SOLID WASTE: RC A: CERCLA LANDFILL
OTHER:
❑NC❑SC ❑NC ❑SC ❑I C El SC ❑NC El SC
❑NC ❑SC CC❑NC ❑SCIDNC ❑SCI0NC
El SC
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
i;1a'3lGli"JA

F RIS
Full-Service Analytical &
.I .Y 1". Environmental Solutions
UIBORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012 Case Narrative
NC Drinldng Water Cert No. 37735 10/27/2014
VA Certification No. 460211
DoD ELAP: L-A-BAccredited Certificate No. L2307
ISONEC 17025: L-A-BAccredited Certificate No. L2307
Project: StaLime (Qtdy, Biweekly, 60Day 7 Fecal)
Lab Submittal Date: 10/20/2014
Prism Work Order: 4100396
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
D RPD value outside of the control limits.
DM Sample diluted and RL increased due to the matrix.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between ,MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-OW
Phone: [phone] - Toll Free Number. 1-8001629-6354 - Fax: [phone]

Sample Receipt Summary
Elks! ] Sq
FuU-Service Analytical &
I Envitonmental Solutions
10/27/2014
EM ,
Prism Work Order: 4100396
Client Sample ID
Lab Sample ID
Matrix
Date Sampled Date Received
Sta-Lime
4100396-01
Solid
10/20/14
10/20/14
Fecal #2
4100396-02
Solid
10/20/14
10/20/14
Fecal #3
4100396-03
Solid
10/20/14
10/20/14
Fecal #4
4100396-04
Solid
10/20/14
10/20/14
Fecal #5
4100396-05
Solid
10/20/14
10/20/14
Fecal #6
4100396-06
Solid
10/20/14
10/20/14
Fecal #7
4100396-07
Solid
10/20/14
10/20/14
Samples were received in good condition at 1.9 degrees Gunless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
„fl
Phone: [phone] -Toll Free Number. 1-8001529-8564 -Fax: [phone]

Laboratory Report
s 3. -Fuil-Service Analyt6l �& fie -:a IS . M I Environmental SolutiOris 10/27/2014
Y LABORMRIES INC
City of Statesville, NC Project: StaLime (Qtrly, Biweekly, Client Sample ID: Sta-Lime
Attn: Andy Smith 6013ay 7 Fecal) Prism Sample ID: 4100396-01
P.O. Box 1111 Prism Work Order: 4100396
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 10/2011410:40
Time Submitted: 10120/14 14:50
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
DateJTme
ID
General Chemistry Parameters
% Solids
81.2
% by
0.100
0.100
1
"SM2540 G
10123/14 13:45 MJO
P4J0422
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1
'SM9221 E
10/21/14 10:39 JHB
P4J0432
Total Metals
Mercury
0.10
mglkg dry
0.027
0.0044
1
" 7471B
10124/14 17:16 BGM
P4J0391
Arsenic
4.8 DM
mglkg dry
1.6
0.22
5
"6010C
10/22/14 18:32 BGM
P4J0390
Cadmium
BRLDM
mg/kgdry
1.6
0.22
5
'6010C
1012211418:32 BGM
P4J0390
Copper
20 DM
mglkg dry
3.1
0.67
5
"6010C
10/22114 18:32 BGM
P4J0390
Lead
9.2 DM
mglkg dry
1.6
0.24
6
"6010C
10/22114 18:32 BGM
P4J0390
Nickel
100 DM
mglkg dry
6.2
0.80
5
•6010C
10/22114 18:32 BGM
P4J0390
Selenium
BRLDM
mg/kgdry
3.1
0.37
5
•6010C
10/22/14 18:32 BGM
P4J0390
Zinc
32 DM
mg/kg dry
16
3.4
5
•6010c
10/22114 18:32 BGM
P4J0390
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001629-6364 - Fax: 70W626-8409

s ,= pp Full -Service Analytical &
P R I S M I Environmental Solutions
,7A oa-aR,rA,.a
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtdy, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
10/27/2014
Client Sample ID: Fecal #2
Prism Sample ID: 4100396-02
Prism work Order: 4100396
Time Collected: 10/20/1410:40
Time Submitted: 10/20/14 14:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Dateffime ID
General Chemistry Parameters
% Solids 83.8 % by 0.100 0.100 1 'SM2540 G 10123/14 13:46 MJO P4J0422
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2
'SM9221 E 10/21/14 10:39 JHB P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: 70W526-0409 N064,7771

µ_ Laboratory Report
PAR
^y FUII=Service Analytical"8
e' R I.V M I Envirow'Ontal,5olutions 10/27/2014
� IABOM-HIM ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #3
Prism Sample ID: 4100396-03
Prism Work Order: 4100396
Time Collected: 10/20/1410:40
Time Submitted: 10/20/14 14:50
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateTme
ID
General Chemistry Parameters
% Solids 73.6
% by
0.100
0.100 1
-SM2540 G 10123/14 13:45 MJO
114J0422
Weight
Microbiological Parameters
Fecal Colifonns BRL
MPNlg dry
0.3
1
•SM9221 E 10/21/14 10:39 JHB
P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-060
Phone: [phone] -Toll Free Number. 1-900/529-6394 - Fax: [phone]

ISM I Full -Service Analytical &
Environmental Solutions
+9 UDNATOHIES, INC,
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
10/27/2014
Client Sample ID: Fecal #4
Prism Sample ID: 4100396-04
Prism Work Order: 4100396
Time Collected: 10/20/1410:40
Time Submitted: 10/20/14 14:50
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
% Solids 80.6
% by
0.100
0.100 1
`SM2540 G 10/23114 13.46 MJO
P4J0422
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 10/21/14 10:39 JHB
P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Page.6-.Of 1 4

Laboratory Report
Full -Service Analytical
P R I &
" "� M I' Environmental. Solutions 10/27/2014
�w9aanTOfllEs; ING ' ' '
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #5
Prism. Sample ID: 4100396-05
Prism Work Order: 4100396
Time Collected: 10/20/1410:40
Time Submitted: 10/20/14 14:50
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
% Solids 84.6
% by
0.100
0.100 1
'SM2540 G 10/23/14 13:46 MJO
P4J0422
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
`SM9221 E 10/21/14 10:39 JHB
P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-050
Phone: [phone] - Toll Free Number. 1.8001529-6364 - Fax: [phone]

rt Full -Service Analytical &
Ism I Environmental Solutions
LA60NATOMES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
10/27/2014
Client Sample ID: Fecal #6
Prism Sample ID: 4100396-06
Prism Work Order: 4100396
Time Collected: 10/20/1410:40
Time Submitted: 10/20/14 14:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme ID
General Chemistry Parameters
% Solids 73.0 %, by 0.100 0.100 1 111Y12540 G 10123114 13.45 MJO P4J0422
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3
`SM9221 E 10/21/14 10:39 JHB P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001629-6364 - Fax: [phone] Page 8 of 1 4

pp Full -Service Analytical 3
^� I,SM IEnvironmental,Solutions
Yd%'LA80"TOP IE$ ING "
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
10/27/2014
Client Sample ID: Fecal #7
Prism Sample ID: 4100396-07
Prism Work Order: 4100396
Time Collected: 10120/1410:40
Time Submitted: 10/20/14 14:50
Parameter Result Units Report MDL Dilution Method Analysis . Analyst Batch
Limit Factor Date/Tme ID
General Chemistry Parameters
% Solids 84.6 % by 0.100 0.100 1 "SM2540 G 10/23/14 13:46 MJO P4J0422
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2
•SM9221 E 10/21/14 10:39 JHB P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-800/529.6364 - Fax: [phone]

Level II QC Report
s=. Full -Service Analytical 8
a� ism
,; Environmental Solutions 10/27/14
I
�LABOPATOPIE; ING
City of Statesville, NC Project: StaUme (Qtdy, BiWeekly, 60Day Prism Work Order: 4100396
Attn: Andy Smith 7 Fecal) Time Submitted: 10/20/2014 2:50:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source °!DREG RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 124J0390 - 3060B
Blank (134J0390-BLK1)
Prepared &Analyzed: 10/22/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mglkg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4J0390-13SI)
Prepared &Analyzed: 10/22/14
Arsenic
23.2
0.25
mglkg wet
25.00 93
80-120
Cadmium
23.4
0.25
mglkg wet
25.00 93
80-120
Copper
24.4
0.50
mg/kg wet
25.00 98
80-120
Lead
23.2
0.25
mg/kg wet
25.00 93
80A20
Nickel
23.2
1.0
mg/kg wet
25.00 93
80-120
Selenium
23.3
0.50
mg/kg wet
25.00 93
80-120
Zinc
23.3
2.5
mg/kg wet
25.00 93
80-120
Matrix Spike (P4J0390-MS1)
Source: 4100396-01
Prepared &Analyzed: 10/22/14
Arsenic
21.6
0.31
mg/kg dry
30.94 4.75 54
75-125
MI
Cadmium
12.6
0.31
mgllkg dry
30.94 BRL 41
75-125
MI
Copper
32.4
0.62
mg/kg dry
30.94 20.3 39
75-125
MI
Lead
18.8
0.31
mg/kg dry
30.94 9.23 31
75-125
MI
Nickel
82.2
1.2
mg/kg dry
30.94 103 NR
75-125
MI
Selenium
14.5
0.62
mg/kg dry
30.94 BRL 47
75-125
MI
Zinc
42.1
3.1
mg/kg dry
30.94 32.2 32
75-125
MI
Matrix Spike Dup (P4J0390-MSD1)
Source: 4100396-01
Prepared &Analyzed: 10/22/14
Arsenic
27.7
0.31
mg/kg dry
31.26 4.75 73
75-125
25
20
D, MI
Cadmium
16.4
0.31
mg/kg dry
31.26 BRL 53
75-125
26
20
D, MI
Copper
44.3
0.63
mg/kg dry
31.26 20.3 77
75-125
31
20
D, MI
Lead
23.1
0.31
mg/kg dry
31.26 9.23 44
75-125
21
20
D, MI
Nickel
102
1.3
mg/kg dry
31.26 103 NR
75-125
22
20
D, MI
Selenium
25.8
0.63
mg/kg dry
31.26 BRL 82
75-125
56
20
D, MI
Zinc
%9
3.1
mg/kg dry
31.26 32.2 89
75-125
35
20
D, MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-060
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Page 10 Of `� 4

`Y Level II QC Report
Full -Service Analytical & 10/27/14
/-fl � L"
ism I Environmental Solutions
L.ABORATORIE9, INC,
City of Statesville, NC Project: Stal-ime (Qtdy, BiWeekly, 60Day Prism Work Order: 4100396
Attn: Andy Smith 7 Fecal) Time Submitted: 10/20/2014 2:50:00PM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4J0390 - 3060B
Post Spike (P4J0390-PS1)
Source: 4100396-01
Prepared &Analyzed: 10/22/14
Arsenic
0.928
mg/L
1.000 0.154 77
80-120
MI
Cadmium
0.556
mg/L
1.000 0.000791 56
80-120
MI
Copper
1.30
mg/L
1.000 0.658 64
80-120
MI
Lead
0.772
mg/L
1.000 0.300 47
80-120
MI
Nickel
2.85
mg/L
1.000 3.36 NR
80-120
MI
Selenium
0.672
mg/L
1.000-0.0809 67
80-120
MI
Zinc
1.58
mg/L
1.000 1.04 54
80-120
MI
Batch PQ0391 - 7471 B
Blank (P4J0391-BLK1) Prepared &Analyzed: 10/24/14
Mercury BRL 0.020 mg/kg wet
LIDS (P4J0391-BS1) Prepared &Analyzed: 10/24/14
Mercury 0.428 0.020 mg/kg wet 0.4167 103 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8801529-6364 - Fax: [phone] Page =

I S M I Full -Service Analytical &
Environmental Solutions
LABORATORIES. INc.
Level II QC Report
10/27/14
City of Statesville, NC Project: StaLime (Qtdy, BiWeekly, 60Day Prism Work Order: 4100396
Attn: Andy Smith 7 Fecal) Time Submitted: 10/20/2014 2:50:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4J0422 - Solids, Dry Weight
Blank (P4J0422-BLK1) Prepared &Analyzed: 10/23/14
% Solids 99.9 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Chadotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-800/529-6364 - Fax: [phone] Page 1 2 ,Of 1 4.

.�f, £ R!' I S , Y' �{ Full -Service analytical &
A' . Environmental Solutions
_ LABON"'TOPIEA INC
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Project: StaLime (Qtdy, BWeekly, 6013ay
7 Fecal)
Level 11 QC Report
10/27/14
Prism Work Order: 4100396
Time Submitted: 10/20/2014 2:50:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4JO432 - NO PREP
Blank (P4J0432-BLK7) Prepared &Analyzed: 10/21/14
Fecal Colfforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final DateMme
4100396-01
P4J0422
30 g
30 g
10/23/14 13:45
4100396-02
P4J0422
30 g
30 g
10/23/14 13.45
4100396-03
P4J0422
30 g
30 g
10/23/14 1145
4100396-04
P4J0422
30 g
30 g
10/23/14 13:45
4100396-05
P4J0422
30 g
30 g
10/23/14 13:45
4100396-05
P4,10422
30 g
30 g
10/23114 13:45
4100396-07
P4J0422
30 g
30 g
10/23/14 13:45
Prep Method: 3050B
Lab Number Batch Initial Final Daternme
4100396-01 P4J0390 1.98 g 50 mL 10/22/14 8:40
Prep Method: 7471B
Lab Number Batch Initial Final Daternme
4100396-01 124J0391 0.55 g 50 mL 10/24/14 9:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: 7CW5254409 =7;=7, 50 37f=�.4: ;'"

;�•:
CHAdN F CUSTODY RECORD �g
_+w
Full -Service Analytical e-
tg YES N4 NIA v-
t Enviranmenta! Solutions PAGE_ OF _ QUOYE ii Y® EPISURE PROPER BILLIPIG:
Sam Ic s INTACT u o
.asoruToaies.i�aa F A na'rrtval '/" 9
Project Name' Ftecesved CN 1NET iG1r7'
449 Springbrook goad - Charlotte, NC 28217 PF DP>;R cRESEf V?TINES Indrsafed %- ^
Phone [phone] • Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) ' `� '• '- `:
@ *Please ATTACH any project specific reporting (QC LEVEL 1 11 111 IV)>�eceivad-L6TH.IN,tIgLs51NG.TIME57;;;- ..'' �_ :_ <: •::::::_ Rs
Client Company Name: Cr-t•y 0 Js4o~ Csyi llt; 0.
`/ S provisions and/or QC Requirements GLiSTOD� SEAL $ INTACT .'
Report To/Contact Name: rn , uOLATIr E5`rcc`TWIOUT HEAC?SFAGC?;:-
;� , Invoice To:
Reporting Address: Pam, 0. Box d f I t Pr�G1PE.. TAINERS.usedt
S4A�esi','/le �C Address: TEAP,.rnertirlDI�V , Observed.. 3 Y_�t ICoir?° 8-•. iC
Phone; 7d1-` 7F-3'13,Y Fa Yes (No):?8v-8'7y-Y65S Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DoD FL
NC
EDD Type: PDF_Excel Other "Working Days" 0 6-9 Days ❑ Standard 10 days Q Pre-ApprovedhWrk Must Be
Site Location Name: Fa u r+ 6 Creek w w rP
SC OTHER N/A
Samples received after 14:00 will be processed next business day.
Site Location Physical Address.• � 93 ire I I PA1.11 Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS $ CONDITIONS REGARDING SERVICES
Vad e 56-J J P e NC RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES— NO
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA.
ANALYSIS&EQUESTED
�
PRISM
*TYPE
DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
L
� REMARKS
LAB
SAMPLE
NO.
SIZE
��
ID NO.
HOURS
SLUDGE)
SEE BELOW
��
3l�ve��d/ f1
of.
y_ re,A
v
7h
0 ....
Sampler's Signature/f d t Sampled By (Print Name) 2 nFr7J [tJ e1c Ir Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Rel�hed By: (Signatur Received By: (Signature) Date
Military/Hours Additional Comments: ''Site`grriiat:Tiir�ei°'`:'���'�`'�`<•?=
Relin ' hed By: (Signature) Received By: (Signature) Date
Site; Dep qurii
RBI nqu (ed Bp: (Signature Re ed For Prtsm Laboratories By: Date
EielrJ TeCtk i .
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SJ,1UT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AG ST CDC UNTIL RECEIVED AT THE LABORATORY.
too
❑ Fed Ex ❑ UPS ❑ Hand -delivered &Prism Field Service ❑ Other
NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
❑NC❑SC ❑NC ❑SC ❑NC ❑SC ❑NC El SC ❑NC ❑SC ❑NC❑SC ❑NC ❑SC [INC❑SC ❑NC ❑SC
I I I I
°
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) (11F,1I, IN141

pj EI s M. 'I... Full.-Ser*e' Analytical &
Environmental Solutions
x> LABORATORIES INC. • •
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinldng Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISOlIEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 11/03/2014
Prism Work Order: 4110026
Case Narrative
11/12/2014
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robb! A. Jones
President/Project Manager
Data Qualifiers Key Reference:
f
Vy
6ba-11P
Reviewed By Terri W. Cole For Robbi A. Jones
Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greaterthan 10x the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Chadofte, NC 28224-0543
Phone: [phone] - Toll Free Number 1-8001529-6364 - Fax: [phone]

AokiIs Full -service Analytical &
'1 Environmental Solutions
V VWRATOR[M ING '
Sample Receipt Summary
11 /12/2014
Prism Work Order: 4110026
Client. Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime
4110026-01 Solid 11 /03/14 11 /03/14
Samples were received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box'240543 - Charlotte, NC 28224-OW
Phone: [phone] - Toll Free Number: l-8001529-8364 - Fax: [phone]

A"'
Laboratory Report
PA'5t
IR
I S.M
Full -Service Analytical &
I _ Environmental Solutions
11/12/2014
"ram' LAOOfi0.TOfl IES, INC ' ' .
City of Statesville, NC Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4110026-01
P.O. Box 1111
Prism Work Order: 4110026
Statesville, NC 28687 Sample Matrix: Solid
Time Collected: 11/03/14 15:05
Time Submitted: 11/03/1418:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Datefrime
ID
General Chemistry Parameters
% Solids
72.0
% by
0.100
0.100
1
•SM2540 G
11R114 15:05
MJO
P4K0116
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
`SM9221 E
11/4114 13:40
JHB
P4K0096
Total Metals
Mercury
0.11
mglkg dry
0.026
0.0042
1
•7471B
1115114 17:43
BGM
P41K0011
Arsenic
3.0
mg/kg dry
1.8
0.25
6
"6010C
1117114 23:26
BGM
P4K0075
Cadmium
BRL
mgikg dry
1.8
0.25
5
'6010C
1177/14 23:26
BGM
1341<0075
Copper
19
mglkg dry
3.5
0.64
5
•6010C
1117/14 23:26
BGM
1341(0075
Lead
8.3
mglkg dry
1.8
0.27
5
"6010C
11R/14 23:26
BGM
P41(0075
Nickel
94
mg/kg dry
7.0
0.90
5
"6010C
1117114 23:26
BGM
P41(0075
Selenium
BRL
mg/kg dry.
3.5
0.42
5
•6010C
11/11/14 17:35
BGM
P4K0075
Zinc
39
mg/kg dry
18
3.9
5
"6010C
11M14 23:26
BGM
P4K0075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] R; . P8oE;3,

Level II QC Report
i I Full-Service,Analytical &
S.m' Environmental solutions 11/12/14
® IAOOFATONIES, INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime
Prism Work Order: 4110026
Time Submitted: 11/3/2014 6:00:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 1341<0011 - 7471 B
Blank (1241(0011-BLKI) Prepared &Analyzed: 11/05/14
Mercury BRL 0.020 mg/kg wet
LCS (P4K001 I -BS1) Prepared &Analyzed: 11/05/14
Mercury 0.439 0.020 mg/kg wet 0.4167 105 80-120
Batch 1341(0075 - 3050B
Blank (P4K0075-BLK1) Prepared: 11/06/14 Analyzed: 11/07/14
Arsenic BRL 0.25 mg/kg wet
Cadmium
BRL
0.26
mg/kg wet
Copper
BRL
0.50
mg/kg wet
BH
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4K0075-BSI)
Prepared: 11/06/14 Analyzed: 11/07/14
Arsenic
23.6
0.25
mg/kg wet
25.00 95 80-120
Cadmium
24.0
0.25
mg/kg wet
25.00 96 80-120
Copper
24.8
0.60
mg/kg wet
25.00 99 80-120
Lead
2&7
0.25
mg/kg wet
25.00 95 80.120
Nickel
23.9
1.0
mg/kg wet
25.00 95 80-120
Selenium
23.3
0.50
mg/kg wet
25.00 93 80-120
Zinc
24.0
2.5
mg/kg wet
25.00 96 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1 -8001529-6364 - Fax: [phone]

r Fu11-Service.Analytical &
P 1'.'1``-_-_- LS-M - Envirorimentai Solutions
'*. LABOPATOPIE$
City of Statesville, NC Project: StaUme
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
11/12/14
Prism Work Order: 4110026
Time Submitted: 11/3/2014 6:00:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4K0116 - Solids, Dry Weight
Blank (P4K0116-BLK1) Prepared & Analyzed: 11/07/14
% Solids 99.9 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone]

�.,� F� Full -Service Analytical &
Y I S I Environmental Solutions
Awmiffiaiil
', LABORATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Level II QC Report
11/12/14
Prism Work Order: 4110026
Time Submitted: 11/3/2014 6:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 1241<0096 - NO PREP
Blank (11341<0096-BLK1)
Prepared &Analyzed: 11/04/14
Fecal Colifonns
BRL
0.2 MPN/g wet
Duplicate (P4K0096-DUP1)
Source: 4110026-01
Prepared &Analyzed: 11/04/14
Fecal Colifonns
BRL
0.3 MPN/g dry
0.00 20
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final
Daternme
4110026-01 P4K0116
30 g
30 g
11/07/14 15:05
Prep Method: 3050B
Lab Number Batch
Initial
Final
DateMme
4110026-01 P41<0075
1.98 g
50 mL
11/06/14 8:20
4110026-01 P41<0075
1.98 g
50 mL
11/06/14 8:20
Prep Method: 7471E
Lab Number Batch
Initial
Final
DatelTime
4110026-01 P4K0011
0.65 g
50 mL
11/05/14 9:05
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-060
Phone: [phone] - Toll Free Number:1-8001529-8364 - Fax: [phone] Page.6 Of 7

SMi Full -Service Analytical &
Environmental Solutions
449 Springbrook Road 4 P.O. Box 240543 m Charlotte, NC 28224-0543
Phone: [phone] Fax: [phone] Client Company Name: C4v oP S4,.�-esei°1I t
fc
Report To/Contact Name: n 2 v S mJ l I
Reporting Address: ? Box fjr
S10esv11I1e 14C
PAGE _ OF _ QUOTE 9 To ENs!JRE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
*Please ATTACH any project specific reporting (QC LEVEL I H III IV)
provisions and/or QC Requirements
Invoice To:
Address:
Phone, 70'V- 978-3433 Fax es . (No):70Y- $7�7- 9d 55 Purchase Order No./Billing Reference -
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days El 3 Days Cl 4 Days ❑ 5 Days
Certification: NELAC USACE FL NC
EDD Type: PDP_ Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days O Pre-AWork Must Be
foLt 4 her e e La W T P business day.y.
SC_ OTHER N/A
Site Location Name: . Samples received after 15:00 will be processed next
�
Site Location Physical Address: 193 3C' 1! &rm , Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated. YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
��C RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES NO
amp p n:
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSES REQUESTED
/�Q / REMARKS
PRISM
Lg
,A
*TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
SIZE
TIVES
ID NO
HOURS
SLUDGE)
SEE BELOW
NO.
/ /
alf LAJ C-(' Xf
[
--- -
---
----
- ---
-
�' -
--
- - --
-
--
-- ------------
-
---
- --
�
Sampler's Signature �✓ - Sampled By (Print Name) PA LtJ C K Affiliation
Upon relinquishing, this Chain of ustody is your authorization for Prism to proceed with th analyses as requested above. Any changes must be e
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
/llnp Lle,�Illy Received By: (Signature) Date MIIItaryMours Additional Comments; �'S(te'Aitirtl'°Timea�
ell Ja
Reli hed By: (Signature) Received By: (Signature) Date
n
Relinquished By: (Signature) ,/ Received For Prism Laboratories Date
HOULD BE TAPED SHUT CU5T DY SEALS FOR TRA ORTATION TO THE LABORATORY. COC Group No.
Method of Shipment: NOTE: ALL TV,
SAMPLESARENPTED AND VERIFIED AGAINST 000 UNTIL RECEIVED AT THE BORATORY.❑FedEx
❑UPS ❑Hand-deliveredrism Field Service ❑ Other
NPDES: I UST: GR U DWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: F
❑ NC ❑ SC ❑ NC ❑ SC I ❑❑ NC SC I NC ❑ SC NC ❑ SC
I ❑ NC ❑ SC ❑ NG ❑ SC 0 NC ❑ SC I ❑❑ NC ❑ SG
OP bt �'trr n n
d - - 9
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

NC Certification No. 402
Case Narrative
{'
SC Certification No. 99012
Full-Service Analytical &
NC Drinldng Water Cert No. 37735
RSMEnvironmental Solutions
11/25/2014
VA Certification No.460211
v LABORATORIES, INC
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISM EC 17025: L-A-BAccredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 11/17/2014
Statesville, NC 28687 Prism Work Order: 4110343
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Page I.,Of 7

R- I ip I Full -Service Analytical
.�,"+ v Environmental Solutions
LA60RATORIEr INC
Sample Receipt Summary
11 /25/2014
Prism Work Order: 4110343
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime
4110343-01 Solid 11/17/14 11/17/14
Samples were received in good condition at 0.5 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.OM
Phone: 704I629-6364 - Toll Free Number. 1-8001629-6364 - Fax: 704/52"409 Pag(',Z;Of 7

:# Laboratory Report
:� a i3 � /� Full-Servioe Analytical &
"^� . EnAronmental Solutions
I S I 11 I .. 11 /25/2014
IAPORATOPIES, ING
City of Statesville, NC
Project: Stal-ime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4110343-01
P.O. Box 1111
Prism Work Order: 4110343
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/17/14 10:17
Time Submitted: 11/17/1412:48
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor DateTme
ID
General Chemistry Parameters
%Solids
73.7
%by
0.100
0.100
1 *SM2540G 11/21/1416:60
MJO
P41(0388
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 11/18/14 9:50
MES
P4K0328
Total Metals
Mercury
0.14
mglkg dry
0.027
0.0045
1 *7471B 11120/14 12:43
BGM
P4K0327
Arsenic
4.4
mg1kg dry
3A
0.49
10 *6010C 11/22I14 3:38
BGM
P41K0343
Cadmium
BRL
mglkg dry
3.4
0.48
10 *6010C 11/22/14 3:38
BGM
P41<0343
Copper
30
mglkg dry
6.8
1.2
10 *6010C 11122/14 3:38
BGM
P4K0343
Lead
12
mglkg dry
3A
0.62
10 *6010C 11/22M4 3:38
BGM
P41(0343
Nickel
170
mgfkg dry
14
1.8
10 *6010C 11/22►14 3:38
BGM
P41(0343
Selenium
BRL
mglkg dry
6.8
0.82
10 *6010C 11/22114 3:38
BGM
P4K0343
Zinc
60
mglkg dry
34
7.5
10 *6010C 11/22114 3:38
BGM
P41(0343
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1.8001529-6364 - Fax: 704/62"408 `7__77'0 C 7Qf'7;'-=

ry I �. S M I Full -Service Analytical &
Environmental Solutions
{1�O0.ATOFit ES,.NC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P4K0327 - 7471 B
Project: StaLime
Reporting
Result Limit Units
Level II QC Report
11/25/14
Prism Work Order: 4110343
Time Submitted: 11/17/2014 12:48:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P4K0327-BLK1) Prepared: 11/19/14 Analyzed: 11/20/14
Mercury BRL 0,020 mg/kg wet
LCS (P4K0327-BSI) Prepared: 11119/14 Analyzed: 11/20/14
Mercury 0.416 0.020 mg/kg wet 0.4167 100 80-120
Matrix Spike(P4K0327-MS1) Source:4110343-01 Prepared: 11/19/14 Analyzed:11/20114
Mercury 0.644 0.027 mg/kg dry 0.5654 0.140 89 80-120
Matrix Spike Dup (P4K0327-MSD1) Source: 4110343-01 Prepared: 11/19/14 Analyzed: 11/20/14
Mercury 0.632 0,027 mg/kg dry 0.5654 0.140 87 80-120 2 20
Batch P41(0343 - 3050B
Blank (P4KO343-BLK1)
Prepared: 11/20/14 Analyzed: 11/22/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4K0343-BSI)
Prepared: 11/20/14 Analyzed: 11/22/14
Arsenic
27.9
0.25
mg/kg wet
25.00 111 80-120
Cadmium
27.5
0.25
mg/kg wet
25.00 110 80-120
Copper
28.3
0.50
mg/kg wet
25.00 113 W120
Lead
27.1
0.25
mg/kg wet
25.00 109 80-120
Nickel
26.9
1.0
mg/kg wet
25.00 107 80-120
Selenium
27.6
0.50
mg/kg wet
25.00 110 80-120
Zinc
27.8
2.5
mg/kg wet
25.00 111 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Page 4 of 7

.::...' : Level II QC Report
F.RIPSemice Analytical & Environmental Solutio•ns 11/25/14
�i�IABOfllSOFIES, INC • • .
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime
Prism Work Order: 4110343
Time Submitted: 11/17/2014 12:48:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MK0399 - Solids, Dry Weight
Blank (P4K0399-BLKI) Prepared &Analyzed: 11/21/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-OSC
Phone: [phone] -Toll Free Number. 1-8001629-6364 - Fax: [phone]

fiRI ` - fiiFull-Service Analytical &
#,'I J Environmental Solutions
7LAOOPATOPIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
AnaVe
Project: Stal-ime
Level II QC Report
11/25/14
Prism Work Order: 4110343
Time Submitted: 11/17/2014 12:48:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41(0328 - NO PREP
Blank (P4K0328-BLK1)
Prepared &Analyzed: 11/18/14
Fecal Colifonns
BRL
0.2 MPN19 wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final Daternme
4110343-01 P41<0399
30 g
30 g 11/21/14 16:50
Prep Method: 3050E
Lab Number Batch
Initial
Final DateTme
4110343-01 P41<0343 1.99 g 50 mL 11/20/14 8:25
Prep Method: 7471B
Lab Number Batch Initial Final DateMime
4110343-01 P41<0327 0.6 g 50 mL 11/19/14 12:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Tall Free Number. 1-8001529-6364 - Fax: [phone] Page 6 0 7

f1l�--LC) i
-Service Analytical YCS O M/p w
CHANN OF CUSTODY RECORD
I
Fulltical &
Environmental Solutions PAGE — OF _ QUOTE To ENSURE PROPER (BILLING'. Saml�[aa INTAf'T upon etTEVat t � � o:,
- ti
cam naonarantes rtae FXeceive i {3M- VEi
i -Jew.-Temp
149 Sy�rtngbtook Road + P.O. Box 240543 Charlotte, NC 28224 0543 Project Blame:
AIOI?IFI F FlCSE�iSfA;l�/E3 lndli atS! D)
Phone: [phone] ° Fax: [phone] Short Hold Analysis: (Yes) (No) LIST Project: (Yes) (No) ? es
� V, *Please ATTACK any project specific reporting (QC LEVEL 1 II III IV)
Client Company Name: C `4, J ode
`e.•ReceiV.e¢cVJll'Fi((V H4�Lf�JI��TIN1�S::=�,;.i;;.:<.a=:,,>;:--::..�� ;:�; � a'
provisions and/or L4C RequirementsUS1[}Y SEl1LS (N7ACT
Report To/Contact Name: +4�.r Sr»r+�' USLAT]LESrecl�PJtQUHCADSACE?
Invoice To:
Reporting Address: Aa r3�x tr r1 Address: -
_TVa_ Fes v,'11 e NC
Phone:[phone] til? Fax es (No): 70`r'57:4. 84 S-6 Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Entail (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE FL NC
EDD Tyke: PDF_ Excel —Other "Working Days" ❑ 6-9 Days u Standard 10 days ❑ Rush Work Must Be
Pre -Approved
SC OTHER N/A
Site Location Name: F� , r4 r-r Cr Lc a` 4) t�i'�P Samples received after 15:00 will be processed next business day.
Site Location Physical Address:40-3 801 S `— ?T Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO _
s j� scsv,r���.' �`✓� (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
'C Y RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES' NO
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSES REQUESTED
\ �
PRISM
LAB
CLIENT
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
/ REMARKS
O�
ID NO.
"TYPE
NO.
SIZE
HOURS
SLUDGE)
SEE BELOW
a .Ce`drr�
1)., B7md�3
10 ; 17
$
�A�"5�6►3
._✓
,�+
O:`cv�t k% %m.S�
U
.._
__
-
CR
a '
Sampler's Signature �t ��-t Sampled By (Print Name) Ti�ZL r'IO" Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
'a[ized. u
submitted in writing to the Prism Project Manager. There will be charges for any change a r analyses have been mi
Relin ished B : (Si �njature Received By: (Signature) Date Mdltary o Additional Comments:
4
�.
Date iry(q G(T� ���� '=a!te'[Ieprture,,Tici. •: : ''
ReIW4ished By: (Signature) Received By: (3i nature)
Relin uishodB : (Signature) y:�`�
9 Y ( 9 ) e ed For dsm Laboratories B Date
�4 /f
9
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WIT CUST DY SEALS FOR TRANSPORTATION TO THE LABORATORY. COG Group No. q
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CO UNTIL ECEIVED AT THE LABORATORY.
7r'�'
❑ O Hand El Prism Field Service ❑ Other V 1 ✓ t�J q;J
❑ Fed Ex UPS -delivered
NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RA: CERCLA LANDFILL OTHER:
❑ NC ❑ SCI ❑ NC ❑ SC ❑ NC ❑ SC
UO NC U SC ❑ NC ❑ SC UO NC U SC O NC O SC p❑ NC Q SC I a NC ❑ SC
- ORIGINAL
'CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (/-ero meaa Space)

CIO
pFull-Service Analytical•&
I: V Environmental Solutions
LA60MTORIES, INR
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012 Case Narrative
NC Drinking Water Cert No. 37735 12/23/2014
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
IS01IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime (Qtdy, Biweekly, 60Day 7 Fecal)
Lab Submittal Date: 12/16/2014
Prism Work Order: 4120290
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with, a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-80DIS29-6364 - Fax: [phone]

Sample Receipt Summary
+.
R9SM
Full -Service Analytical &
Environmental Solutions
I y
12/23/2014
'�W80RATORIE$ING
Prism Work Order: 4120290
Client Sample ID
Lab Sample ID
Matrix
Date Sampled Date Received
Stal-ime
4120290-01
Solid
12/15/14
12/16/14
Fecal #2
4120290-02
Solid
12/15/14
12/16/14
Fecal #3
4120290-03
Solid
12/15/14
12/16/14
Fecal #4
4120290-04
Solid
12/15/14
12/16/14
Fecal #5
4120290-05
Solid
12/15/14
12/16/14
Fecal #6
4120290-06
Solid
12/15/14
12/16/14
Fecal #7
4120290-07
Solid
12/15/14
12/16/14
Samples were received in good condition at 2.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-050
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] "Page 2'.Of•

,� Full -Service Analoigal &
FOP R I ��M� I Enylronmental.Solutions
+5. tAB�RATORIE$ M - .
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
12/23/2014
Client Sample ID: StaLime
Prism Sample ID: 4120290-01
Prism Work Order: 4120290
Time Collected: 12/15/1411:45
Time Submitted: 12/1611410:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
DatelTme
ID
General Chemistry Parameters
Plant Available Nitrogen
760
mglkg
160
13
2
*Calculation
12122114 9:14
CLB
[CALC]
% Solids
66.9
% by
0.100
0.100
1
*SM2640 G
12/18/14 15:50
EGC
P41-0341
Weight
Nitrate/Nitrite as N
11
mglkg dry
7.5
0.82
1
*SM4500-NO3 F
12118/14 10:18
CLB
P41-0299
Phosphorus -Total
2100
mglkg dry
75
16
20
*SM4600-P F
12/23N4 10:11
CLB
P4L0363
Total K]eldahl Nitrogen
3600
mgikg dry
760
63
2
*351.2
12/19/14 8:50
CLB
P41-0329
Ammonia as N
92
mglkg dry
7.5
1.8
1
*SM4600NH3 G 12122/14 9:14
CLB
P4L0349
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
12/16/14 11:36
MES
P4L0378
Total Metals
Mercury
0.18
mglkg dry
0.029
0.0049
1
*7471B
12/18/14 11:63 MEH
P41-0311
Arsenic
BRL
mg/kg dry
0.38
0.053
1
*6010C
12/19/14 23:34 BGM
P41-0330
Cadmium
0.67
mglkg dry
0.38
0.063
1
*6010C
12/19/14 23:34 BGM
P41-0330
Copper
26
mgikg dry
0.76
0.14
1
*6010C
12/19114 23:34 BGM
P41-0330
Lead
12
mgikg dry
0.38
0.067
1
*6010C
12/19/14 23:34 BGM
P4L0330
Nickel
10
mg/kg dry
1.5
0.19
1
*6010C
12/19/14 23:34 BGM
P4L0330
Potassium
670
mgikg dry
18
1.2
1
*6010C
12119/14 23:34 BGM
P4L0330
Selenium
BRL
mg/kg dry
0.75
0.090
1
*6010C
12/19/14 23:34 BGM
P41-0330
Sodium
33
mglkg dry
19
3.7
1
*6010C
12119/14 23:34 BGM
P41-0330
Zinc
46
mglkg dry
3.8
0.83
1
*6010C
12/19/14 23:34 BGM
P41L0330
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0543
Phone: [phone] - Toll Free Number.1-800/629-6364 - Fax: [phone]

1f�� I� �/ A' Full -Service Analytical &
"' '
�..� UR I S , I Environmental Solutions
..sV ' ` 7weonnroelea wc.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
12/23/2014
Client Sample ID: Fecal #2
Prism Sample ID: 4120290-02
Prism Work Order: 4120290
Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateJTme
ID
General Chemistry Parameters
% Solids 70.2
% by
0.100
0.100 1
'SM2640 G 12/18114 15:50 EGC
P41-0341
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
•SM9221 E 12/16/14 11:36 MES
P41-0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001629-6364 - Fax: [phone] Page 4 of 14

Full -Service Analytical
Apa;;qaism . I Envirogmbntal, Solutions
^r IABOPATOP�E3, ING - .. . .
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
12/23/2014
Client Sample ID: Fecal #3
Prism Sample ID: 4120290-03
Prism Work Order: 4120290
Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateTme
ID
General Chemistry Parameters
% Solids 68.7
% by
0.100
0.100 1
'SM2640 G 12/18/14 15:60 EGC
P41-0341
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 12/16/14 11:36 MES
P41-0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone]

.' .
PPR?3- Full service Analytical'&
er-F:R.I �.� . I� Environmental. solution's
Idi&Mwineanwreeies,
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
12/23/2014
Client Sample ID: Fecal #4
Prism Sample ID: 4120290-04
Prism Work Order: 4120290
Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 67.7 % by 0.100 0.100 1 'SM2640 G 12118114 16:50 EGC P41-0341
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 12116/14 11:36 MES P4L0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone]

Full -Service Analytical &
Ar"'fihI Environmental Solutions
�r'LA60FATOPIE$ INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
12/23/2014
Client Sample ID: Fecal #5
Prism Sample ID: 4120290-05
Prism work Order: 4120290
Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 67.7
% by
0.100
0.100 1
*3II112540 G 12118/14 16:60 EGC
P41-0341
Weight
Microbiological Parameters
Fecal Col'Iforms BRL
MPN/g dry
0.3
1
*SM9221 E 12/16/14 11:36 MES
1341-0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001629-6364 - Fax: [phone] - , Page1`� of 71,4 :: "

t„; Full -Service Analytical &
R I S Environmental solutions
VrLA90gATOPIE3, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Deport
12/23/2014
Client Sample ID: Fecal #6
Prism Sample ID: 4120290-06
Prism Work Order: 4120290
Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme ID
General Chemistry Parameters
% Solids 66.8 % by 0.100 0.100 1 "SM2540 G 12118/14 16:60 EGC P411-0341
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3
'SM9221 E 12/16/14 11:36 MES , P41-0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-3001529-6364 - Fax: 704162"409 P60q 8

F? IFuh-Service Arialytical &
Environmental Solutions
R I .S M I
��1A90PATOFIFq ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
6013ay 7 Fecal)
Sample Matrix: Solid
Laboratory Report
12/23/2014
Client Sample ID: Fecal #7
Prism Sample ID: 4120290-07
Prism Work Order: 4120290
Time Collected: 12/15/14 11:45
Time Submitted: 12/16/1410:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateTme
ID
General Chemistry Parameters
% Solids 68.6
% by
0.100
0.100 1
"3111112640 G 12118/14 15:60 EGC
P4L0341
Weight
Microbiological Parameters
Fecal Colifonns BRL
MPN/g dry
0.3
1
•SM9221 E 12/16/14 11:36 MES
P41-0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.050
Phone: [phone] - Toll Free Number.1-5001529-6364 - Fax: [phone] Pagt' 9„Ofr,1.4

�Full -Service Analytical &
AA,
i I S I V, I Environmental Solutions
LA60R.TcA'.s..c.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime (Qtdy, BiWeekly, 60Day
7 Fecal)
Level II QC Report
12/23/14
Prism Work Order: 4120290
Time Submitted: 12/16/2014 10:00:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD L:Imit Notes
Batch P41-0311 - 7471 B
Blank (P4L0311-BLK1) Prepared: 12/17/14 Analyzed: 12/18/14
Mercury BRL 0.020 mg/kg wet
LCS (P41-0311-BS1) Prepared: 12/17/14 Analyzed: 12/18/14
Mercury 0.439 0.020 mg/kgwet 0.4167 105 M120
Batch P41-0330 - 3050B
Blank (1341-0330-BLK1)
Prepared: 12f18/14 Analyzed: 12/19/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
12
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P41-0330-BS1)
Prepared: 12/18/14 Analyzed: 12/19/14
Arsenic
22.2
0.25
mgAg wet
25.00 89 80-120
Cadmium
22.7
0.25
mg/kg wet
25.00 91 80-120
Copper
23.2
0.50
mg/kg wet
25.00 93 80-120
Lead
22.3
0.25
mg/kg wet
25.00 89 80-120
Nickel
22.0
1.0
mg/kg wet
25.00 88 80-120
Potassium
432
12
mg/kg wet
500.0 86 80-120
Selenium
22.2
0.50
mg/kg wet
25.00 89 80-120
Sodium
459
12
mg/kg wet
500.0 92 80-120
Zinc
22.8
2.5
mg/kg wet
25.00 91 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Chartotte, NC 28224-OW
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Page ,'I

Level II QC Report
FARk It n � Full -Service Analytical &
E I S I V 1 I 12/23/14
,� �„ � Environmental Solutions
+7LASOPATOPIE% MG
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime (Qtdy, BWeekly, 60Day
7 Fecal)
Prism Work Order: 4120290
Time Submitted: 12/16/2014 10:00:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41-0299 - NO PREP
Blank (1341-0299-BLKI) Prepared: 12/17/14 Analyzed: 12/18/14
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P41-0299-BSI) Prepared: 12/17/14 Analyzed: 12/18/14
Nitrate/Nitrite as N 49.6 5.0 mg/kg wet 50.00 99 80-120
Matrix Spike (1241-0299-MS1) Source: 4120290-01 Prepared: 12117/14 Analyzed: 12/18/14
Nitrate/Nitrite as N 75.4 7.5 mg/kg dry 74.74 10.6 87 80-120
Matrix Spike Dup (P4L0299-MSD1) Source: 4120290-01 Prepared: 12/17/14 Analyzed: 12/18/14
Nitrate/Nitrite as N 75.7 7.5 mg/kg dry 74.74 10.6 87 80-120 0.4 20
Batch P4L0329 - 361.2
Blank (P4L0329-BLKI) Prepared: 12/18/14 Analyzed: 12/19/14
Total lgeldahl Nitrogen BRL 25 mg/kg wet
LCS (P4L0329-BS1) Prepared: 12/18/14 Analyzed: 12/19/14
Total KJeldahl Nitrogen 492 100 mg/kg wet 500.0 98 90-110
Batch P41-0341 - Solids, Dry Weight
Blank (P4L0341-BLK7) Prepared &Analyzed: 12/18/14
% Solids 100 0.100 % by Weight
Batch P41-0349 - NO PREP
Blank (P41-0349-BLK7) Prepared &Analyzed: 12/22/14
Ammonia as N BRL 5.0 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number. 1 8001529 6384 -Fax: [phone] - -96 1 1`Of14

Pn Full -Service Anal tical &
I S M I Environmental Solutions
AwiiIABOHATORIE% INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P41-0349 - NO PREP
Level II QC Report
12/23/14
Project: Stal-ime (Qtdy, BiWeekly, 60Day Prism Work Order: 4120290
7 Fecal) Time Submitted: 12/16/2014 10:00:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
LCS (P411-0349-BSI) Prepared &Analyzed: 12/22/14
Ammonia as N 126 5.0 mg/kg wet 125.0 101 80-120
Matrix Spike (1241-0349-MS1) Source: 4120290-01 Prepared &Analyzed: 12/22/14
Ammonia as N 293 7.5 mg/kg dry 186.8 92.1 107 80-120
Matrix Spike Dup (P411-0349-MSD1) Source: 4120290-01 Prepared &Analyzed: 12/22/14
Ammonia as N 292 7.5 mg/kg dry 186.8 92.1 107 M120 0.1 20
Batch P41-0353 - SM4500-PBS
Blank (P41-0353-BI-KI) Prepared: 12/22/14 Analyzed: 12/23/14
Phosphorus -Total BRL 2.5 mglkg wet
LCS (P411-0353-13SI) Prepared: 12/19/14 Analyzed: 12/23/14
Phosphorus -Total 102 2.5 mgikg wet 100.0 102 90-110
Matrix Spike (P41-0353-MS1) Source: 4120290-M Prepared: 12/19/14 Analyzed: 12/23/14
Phosphorus -Total 2450 75 mg/kg dry 149.5 2060 261 80-120 MC
Matrix Spike Dup (P41-0353-MSD7) Source: 4120290-01 Prepared: 12/19/14 Analyzed: 12/23/14
Phosphorus -Total 2450 75 mglkg dry 149.5 2060 257 80-120 0.2 20 MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-OSM
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Rage-1 Z

Level II QC Report
d��= - Fuq=Serylge Analytical & 12/23/14
,a I'S.l�/I I : Environmental Solutions
A
s "WAATOn1E9, INC.
City of Statesville, NC Project: Stal-ime (Qtdy, Biweekly, 60Day Prism Work Order: 4120290
Attn: Andy Smith 7 Fecal) Time Submitted: 12/16/2014 10:00:OOAM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41-0378 - NO PREP
Blank (P4L0378-BLKI) Prepared &Analyzed: 12/16/14
Fecal Colifonns BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Daternme
4120290.01 1241-0329 0.05 g 25 mL 12/18/14 10:15
Prep Method: SM4500-PBS
Lab Number Batch Initial Final Daternme
4120290-01 P41-0353 1 g 50 mL 12/19/14 11:30
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Datefnme
4120290-01
P41-0341
30 g
30 g
12/18/14 15:50
4120290-02
P41-0341
30 g
30 g
12/18114 15:50
4120290-03
P41-0341
30 g
30 g
12/18/14 15:50
4120290-04
P41-0341
30 g
30 g
12/18/14 15:50
4120290-05
P41-0341
30 g
30 g
12/18/14 15:50
4120290-06
P41-0341
30 g
30 g
12118/14 15:50
4120290-07
P41-0341
30 g
30 g
12/18/14 15:50
Prep Method: 3050B
Lab Number Batch Initial Final Datefnme
4120290-01 P41-0330 1.99 g 50 mL 12/18/14 11:57
Prep Method: 7471B
Lab Number Batch Initial Final Daternme
4120290-01 P41-0311 0.61 g 50 mL 12/17/14 11:45
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC,28224-0543
Phone: [phone] - Toll Free Number. 1-8001529-9394 - Fax: [phone]—.Toi 67714771