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Home My WebLink AboutWQ0006018_Residual Annual Report 2014_20150302TOWN OF MOREHEAD CITY, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0006018 2014 ANNUAL REPORT Town of Morehead City, NC Residuals Land Application Program 2014 Annual Report TABLE OF CONTENTS 1. Certification Form, Annual Operations Summary, Facility and Land Applier Contact Information 2. Annual Residual Sampling Summary Forms, Residuals Analysis, & SAR Calculation Page 3. Annual Land Application Field Summary Form 4. TCLP Analysis 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analysis ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00006018 County Carteret Year 2014 Facility Name (as shown on permit) Town of Morehead City W WTP NPDES No. NCO026611 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X . YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 7 Total number of fields utilized for land application during the year: I Total amount of dry tons applied during the year for all application sites: 106.75 Total number of acres utilized for land application during the year: 26.6 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2014 with all conditions -of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past -calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Daniel Williams, Utilities Director Permittee Name and Title (type or print) Signature of Preparer* Date (if different from Permittee) Sigliature of Land Applier (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) du 3 2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION MOREHEAD CITY, NC MOREHEAD CITY, NC CAKE MONTHNEAR April 2014 YEARLY TOTAL AMOUNT UNIT 650.00 Y 650.00 Y DRY TONS UNIT 106.75 D 106.75 D DRY METRIC TONS 96.83 96.83 1 /31 /2015 2013 ANNUAL REPORT PROJECT: Town of Morehead City, NC FACILITY: Town of Morehead City WWTP 1000 Treatment Plant Road Morehead City, NC 28557 252-726-6237 NPDES PERMIT NUMBER: RESPONSIBLE OFFICIAL: FACILITY OPERATOR: LAND APPLIER AND PREPARER OF LAND APPLICATION ANNUAL REPORT: NC0026611 Daniel Williams, Utilities Director Town of Morehead City 706 Arendell Street Morehead City, NC 28557 252-726-6848 Carl Dangerfield ORC 1000 Treatment Plant Road Morehead City, NC 28557 252-726-6237 Synagro Central, LLC Contact: Marshall Puryear (336) 998-7150 ext. 17 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006018 Facility Name: MOREHEAD CITY, NC NPDES# : NCO026611 or WQ# (residual only) WWTP Name: MOREHEAD CITY Residuals Analysis Data Product Type CAK Date Sampled (grab) or 02/18/14 Date Composited Percent Solids 19.50 PARAMETERS (mg/kg dry weight) Arsenic 9.44 Cadmium <0.. 508 Mercury 2 Chromium 18.5 Copper 862 Lead 8.77 Molybdenum <5.07 Nickel 8.72 Selenium 5.64 Zinc 990 Total Phosphorus 6480 TKN 8350 Ammonia=Nitrogen 1350 Nitrate and Nitrite 13.3 Laboratory ENVIROCHEM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for supmitting false information, including the possibility of fines and imprisonment for knowing violations." N F11 Date DENR FORM RSSF (5/2003) Printed: Saturday - January 31 2015 at 08:51:34 for: 2252 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0006018 Facility Name: MOREHEAD CITY, NC NPDES# : NCO026611 or WQ# (residual only) WWTP Name: MOREHEAD CITY Residuals Analysis Data Product Type CAK Date Sampled (grab) or 02/18/14 Date Composited Percent Solids 19.50 PARAMETERS (mg/kg dry weight) Aluminum 1570 Calcium 45900 Magnesium 3640 pH 6.77 Potassium 3120 Sodium 2900 Laboratory ENVIROCHEM "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false info mation, including the possibility of fines and imprisonment for knowing violations." Date 4? (SIGNATURE-CrF—PREPARER) NR - Data Not Reported or Data Not Required DENR FORM RSSF-B (7/2002) Printed: Saturday - January 31 2015 at 08:52:00 for: 2252 01 Environmental Chemmists, Inc. • :. y. 6602 Windmill Way o Wilmington, NC 28405 (910) 392-0223 (Lab) ® (910) 392-4424 (Fax) s 710 Bowsert6wn Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ C.ERUNCATE, 04.D S CERTIFICATE*37729 Town Of.Morehead City bate of Report: Mar 21, 2014 706 Arendeil Street Customer PO #; Morehead City NC 28567 Report #: 2014-01870 Attention: C_ Sutton Report to: C. Sutton Project ID; Sludge Lab ID Sample. ID: Collect. Date/Time matrix Sampled by 14-04550 Site: Sludge C,Iass B 2/18/2014 10:00 AM 9olid151udge ' C.Sutton & C.Dangerfield Test Method Results Date Analyzed Chlordane SW 846 Method 6081a13510 Endrin Sw 846 Method 80816/3510 Heptachlor SW 846 Method 8061B/3510 Heptachlor epoxide SW 848 McUtod 8081 EW510 Lindane SW 846 Method 808113/3510 Methoxychlor sw a4s Metnod eoa1sr3610 Toxapherie siry a method so61srs510 1,4-Dichlorobenzene (TCLP) SWMMethodw7018510 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 2,4,6-Trichlorophenol (TCLP) Sw848 method 8270/3610 2,4-Dinitrotoluene,(TCLP) SWWe46me" 827013510 Cresol (TCLP) SW846 method827013510 Hexachloro. 4,3-butadiene (TCLP) SW846 me" 8270=10 Hexachlorobenzene (TCLP) SW 846 method 827olwlo Hexachloroethane (TCLP) SW 840 method 827o/351a rn + p-Cresol (TCLP) SW 846 method 8270=16 Nitrobenzene (TCLP) SW 846 method 627OW10 p-Cresol (TCLP) SW 848 method 8270/3510 Pentachlorophenol (TCLP) Slur 848 mettmd s27o13510 Pyridine (TCLP) swS.4smethodez7013s10 Paintfilte'r Test SW 848'MSthud 9095A 2,4,$-TP t SW846 McGiod 8151A 2,4-D SWItO Mettrod ti61A 1;,1-Dichloroethylene Sws4s Method 826015030 1,2 Dichloteethane SM46 Method 8280150SO Benzene SW846 Method 82801S030 <0,005 mg/L 02/27/2014 <0.00005 mg/L 02/27/2014 <0.00005'mg/L 02/27/2014 <0.00005 mg/L 02/27/2014 <0.00005 mg/L 0=7/2014 <0,00005 mg/L 02127/2014 <0.005 mg/L 02127/2014 <0:050 mg/L 02/25/2014 <0.050 mg/L 02/25/2014 <0.050 mg/L 62/2&2014 <0.050 mgiL 02/25/2014 <0.'050 mg/L OZ2512014 <O 050 mg/L 02/26/2014 <0.050 mg/L 02/25 .W4 <0.050 mg/L 02/25/2014 <0:050 mg/L 02/25/2014 <0.050 mg/L 02/26/2014 <0.050 mg/L 02125/2014 <0.250 trig/L 02/25/2014 s0.050 mgiL 02126/2014 pass 02/20/2014 <0.0003 mg/L 02126/2014 <0.0003 mg/L 0212W2014 <10 mg/L 03/14/2014 <10 mg/L 03114/2014 <10 mg/L 03114/2014 Reportit: 2014-01870 Page 1 of 5 nvironmental. Chemists, Inc. 6602 Windmill: Way a Wilmington, NC 28405 (910) 391-0223 (Lab) • (910) 392-4424 (Fax) Q 71013owsertown Road - Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 4:73 5702 . CHEMtSTs NCDENR: DWQ CURTMCATEi *94. DLS CERTIFICATE #37T1.9 Town taf Morehead City 706 Arendeil Street Morehead City NC 28557 Attention: C. Sutton bate. of Report: Mar 21, 2014 Customer PQ #: 6001it #: 2014-01870 Reportto• C. Sutton Project'ID: Sludge Carbon Tetrachloride SW846 Method 626OJ503G <10 mg/L 03/14/2014 Chlorobenzene Sw646 Method 826 ftm <10 mg/L 03/14/2014 Chloroform SW845 Method 828015030 18.6 mg/L 03114/2014 Methyl ethyl .ketone swow Method 82601MO <60 mg/L 03114/2014 Tetrachloroethylene SWe46 Method M015030 <10 mg/L 03/14/2014 Trichioroethylene S O Method 826015030 . <10 mg/L 03/14/2014 Vinyl Chloride SW846 Method 826W5030 <10 mg/L 03/14/2014 RCI - Ignitability EPA 1030 <0.8 mmisec 02/2412014 Cyanide EPA 335A <0.124 mg/kg 02128/2014 Sulfide SM 4600 s. D <0.247 mg/kg 03103/2014 pH 6W646 Method 00a5U 6.77 Units 02/20/ oa Sludge Residuals Aluminum. EPA 200.7 1570 mg/kg 03/04/2014 Amenic F-PA200-7 9.44mg/kg 02127J2014 Cadmium EPA200.7 <0.508mg/kg 03/10/2014 Calcium EPA 200.7 45900 rrig/kg 02/26/2014 Chromium EPA200.7 18.5 mg/kg 02/27/2014 Copper EPAio0.7 .862mg/kg 03/14/2014 Lead EPA200.7 8.77mg/kg 03/10/2014 Magnesium EPA 200.7 3640 mg/kg 02/26/2014 Molybdenum EPA200.7. <6.07mglkg 02/24/2014 Nickel EPA200.7 8.72mg/kg 02J2412014 Potassium EPA200.7 3126mg/.kg 02/26/2014 Selenium EPA200.7 5.64 mg/.kg 02/24/2014 Sodium EPA2.00.7 2900mg/kg 02/26//20.14 Zinc EPA2oo.7 990 mglkg 08104/2014 Ammonia Nitrogen EPA350.1 1350 mg/kg 03/05/2014 Total Kjeldshl.Nitrogen (TKN) EPA351.2 $360mglkg 03/11/2014 Repaft #:: 2014-01870 Page 1 of 5 En vironmental Chenusis, Inc. .. 6602 Windmill Way • Wilmington, NC 28405 n (410) 392-(1M (Lab) • (910) 392-4424.(Fa.Y) s 710 Bowsertown goad- a Mantee, NC 27954 (252) 473-5702 ANAL1fTlCAL S CONSULTING CHEMISTS NCDENIL- DWQ CER'AIRCATE *94, DL9 CLnXIMCATE 4137i29 Town Of_Mbiehead City Date of.Report: Mar21, 2014 706 Atendell.Street Customer PO #• , , Morahead City NC 28557 Report 0: 2014-01870 Attention_ C. Sutton Report to: C. Sutton Project ID: Sludge NitrateWitrite-Nitrogen EPA353z 13.3mglkg 03/11/2014 Total Solids (%) SM 2540 B 19.5 % 02/21/2014 - Total Phosphorus SM 40O P F 6480 mg/kg 03/11/2014 Mercury SWM7471B 2.00mg/kg 02/28/2014 TCLP Metals Arsenic EPA 2no•7 <0.100 mg/L 02/25/2014 Barium EPA200:7 <0.100 mg/L 02/24J2014 Cadmium EPA 2ao_7 <0,100 ing/L 02/24/2014 Chromium EPA 200.7 <0.100 mg/L 02/2412014 Lead EPA200.7 <0.100mg/L 02/24/2014 Silver EPA2007 <0:100mg/L 02/27/2014 Selenium EPA 2oo,8 <0.100 mg/L 03/08/2014 Mercury EPA 245,1 <0.002 mg/L 02/24/2014 Lab ID Sarhple ID: Collect Date/Time Matrix Sampled by 14-04551 Site: i 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfieid Test Method Results Date Analyzed Total Solids {%) sM 2540 B 18.6 % 02/21/2014 Fecal Density SM9221CI-MPN24hr$03 862069MPN/g 02/19/2014- Lab ID Sample ID: Collect Dateffims Matrix Sampled by 14-04552 Site; 2 2/18/2014 10:00 AM Solid/Sludge C.Sutton C. Dangerfield Test Method Results Date Analyzed Total Solids {%,) SM25408 18.7% 02121/2014 Fecal Densit}. SM92210EMPN 24hr6o3 854701 MPNIg 02/19/2014 Repbrt #.- 2014-01870 — Page 3 of 5 Environim al Chemists, Inc. enviroehem�'6602 Windmill Way. o Wilmington, NC 28405 (010) 392-0223 (Lab) • (910) 3924424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 . (252) 473 5702 ' ANALYTICAL &• CONSULTING CHEMISTS NCDENM- DWQ CERT114CATE *94. DIS CE=CATF. 037729 Town Of Morehead City Date. of Report: Mar 21, 2014 70.6 Arendeli Street Cttstomer PO.#: Morehead City NC 28557 Report #: 2014-01870 Attention: C. Sutton Reportto. C. Sutton Project ID: Sludge Lab ID Sample ID: Collect Dateffime. Matrix Sampled by 14-04653 Site:.3 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) BM 2MO 8 19.2 % 02/21/2014 Fecal. Density sM 922fc E MPN 24 hr503 835074 MPN/g 02/19/2014 Lab ID Sample ID: Collect Daterrime Matrix Sampled by 14-04654 Site: 4 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids {%) SM M40 B 20.6 % 02/21/2014 Fecal Density SM 92210 6 MPN 24 hr 503 774819 MPN/g 02/19/2014 Lab ID Sample ID: Collect .Daterritne . Matrix Sampled by 14-04555 Site; 5 2118/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 19.2 % 02/21/2014 Fecal Density SM 92210E MPN 24 hrs03. 832900 MPN/g 0211912014 Lab 10 Sample ID; Collect Da#el7ime Matrix Sampled by 14-04566 Site: s 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total 'Solids (04) SM2540Q '18.20/0 02121/2014 5ecaiDensi%y snn922IcsMPN24ne503 876713MPN/g 02/1912014 Lab ID Sample Ib: Collect DatelTime Matrix . Sampled by 14-04657 Site: 7 2/1812014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids.(%) sM2awe 18.8% 02121/2014 Fecal Density SM e221c EMPN 24 hrso3 852425 MPwg 02/19/2014 Report #:: 2014-01870 Page 4 of S Environmental Chemists, Inc. 6602W.dmMWay - lffilmingtonNC28105 (930)392-0223([Ab) • (910)3924424.(r-ax) B 710 Bbw.qertovm Road * Manteo, NC 27954 (252) 473-5702 ANALYTICAL& CONSULTING ULTING CHEMISTS MCDENR-- DWO CMUIPICATE #94. DLS CERM- CATE #37729 Town Of Moi*head'Olitv Crate ofReport: Mar 24,2014 706 Ardndell Street Ctistomer Pd Morehead City NC -28657 Report 0. 2014-01870 Attention: C. Sutton Report to: C. -Sutton Project 10: Sludge Comment. Sludge residuals and Fecal density reported on a dry weight Wsls. RCI and Paint Filter Test reported on an asrecelVed t)js1s. Reviewed by: kbku ok, O&A, RePadt' 2014-01070 Page 5 of 5 6602-WindrWilli Way ENVIRONMENTAL CHEMISTS, INC 0Ff1CMSI92-QZWMqmFlAnXgt0o1n0,.NC2204 AnWyfcgi Si donsvWng Chemists - NCDEMR: DWQ C.'KFtfiF1C,AT1bN # 94 NdDHHS- DLS CERTIFICATION # 37729 t-.ni I -Pr'r1nM AMn MAIN ihp ri IqTnnv CLIENT: 1p6fnA6.1( PROJECT NAME: REPORT N6: ADDRESS: cc5NTAcir NAME: PONO: REPORT TO: PHONEIFAX: ]COPY . TO: lo email: -aAmmi: s: +war.. i . ima.iam* r. mi mniirwf W = wwl qTc Cfrrietiti. An _.Anil_ AL = 41itrinss- nfhar- Sampleldentificafion JIM 1111 W so ISIAM W-AF, i■u�Gi�� million WON" .�.� 0e1��YY� �'�� i1a�II�M�� Deiivered 1Rece1vadBy: -\- Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2252-01-CAK-NC MOREHEAD CITY, NC CAKE 2/18/2014 1/1/2014-12/31/2014 1.5447 Na mg/I = (Na mg/kg x % Solids) = 100 = (2900 x 19.5000) _ 100 = 565.5 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (45900 x 19.5000) + 100 = 8950.5 Mg mg/I = (mg mg/kg x % Solids) + 100 = (3640 x 19.5000) = 100 = 709.8 Na meq = Na mg/I = Molec.Wgt.Na = 565.5 + 23 = 24.587 Ca meq = Ca mg/I = Molec.Wgt.Ca = 8950.5 _ 20 = 447.525 Mg meq = Mg mg/1 + Molec.Wgt.Mg = 709.8 _ 12 = 59.15 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 24.587 + SgrRoot[0.5(447.525+59.15)] = 1.54474 Printed: 1 /31 /2015 Page 1 08:57 FACILITY NAME: MOREHEAD CITY, NC OWNER: YOUNG/WETHERINGTON SITE #: NC CR 00007 FIELD# : CR 00007 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: AUTRYVILLE PERMIT #: W00006018 ANNUAL DRY TONS APPLIED: 106.75 OPERATOR: ROBERT M. RIGGS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 26.60 ACRES PERMITTED: 26.60 Page : I Lime Applied'*' Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre . Solids 4/28/14 300.00 (CY) 11.278 19.50 1.852 MOCC DRY 0-<1/2" SURIN 1.0 0.30 8,350.0 p 1,350.00 p 13.30 p 3463 I CORN 4/29/14 350.00 (CY) 13.158 19.50 2.161 MOCC DRY 0-<1/2" SURIN 1.0 0.30 8,350.0 p 1,350.00 p 13.30 p 3463 1 CORN Apr-14 1 650.00 (CY) 24.436 Total Cubic Yds/Ac: 24.44 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 28 Annual lbs/acre 0.076 0.004 0.148 6.919 0.070 0.016 0.041 0.070 0.045 7.946 52.01 Cumulative lbs/acre 0.246 1 0.059 1 3.481 1 39.236 1 0.895 0.108 0.258 1 1.563 0.181 36.437 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ' ' ' '' ' 104 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 MOCC = MOREHEAD CITY, NC CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 I Environmental Chemists, Inc. y 6602 Windmill Way - Wilmington, NC 28405 (010) 392 b223 (Lab) ® (R70) W2-4424 (Fax) 710T3owsertown Road o. Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: OWQ C:ERIIRICATE #{94. DIS CERTIFICATE #t377v Town Of.Morehend City 706 Arendell Street Morehead City NC 28567 Attention: C. Sutton bate of Report; Mar 21, 2014 Customer PO M Report #: 2014-01870 Report to: C. Sutton Project ID: Sludge Lab ID Sample ID: 14-04550 Site: Sludge Class B -Test Collect Date/Time 2/18/2014 10:00 AM Method Matrix Sampled by Solid/Sludge C.Sutton & C.Dangerfield Results Date Analyzed Chlordane sw846Memod80s1Bi35m <0.005mg/L 0212W2014 I ndrin SW 646 Method 80810/3510 <0,60005 mg/L 02/27/2014 Heptachlor SW-846 Method 8061B13510 <0.00005 rtig/L 02/27/2014 Heptachlor epoxide sw a4s Method e0s1 B1351a <0.00005 mg/L 02127Q014 Lindane SW84smethod 8081B13510 <0.00005mg/L 02/27/2014 Methoxychlor soda46Method 0081B13510 <0.00005mg/L 02/27/2014 Toxaphei ne sW 84S Method sos1B13510 <0.005 mg/L D212712014 1,4-Diehlorobenzene(TCLP) SW848method 827=510 <0.050mg/L 02125/2014 2,4,5-Trlchlorophenol(TCLP) SWWMethod exreras10 <0.050mgIL- 0 26/20.14 2,4,6-Trichlorophenol (TCLP) sW e4a method 827a3510 <0A50 mg/L 02/25/2014 2,4-DinitrotolueneITCLP) SW e46 method 8270/3510 c0,050 tnglL 02/26/2014 Cresol (TCLP) SW846method827013510 c0.65Rmg/L 02125/2014 Hexachloro-1,3-butadiene(TCLP) SW 846 me"8270=10 <0.050 mg/L 02125/2014 Hexachlorobenzene (MLP) SW 846 method 82701351a <0.050 MOIL 02125/2Q14 Hexachloroethane (TCLP) sW 840 method 6270/3510 <0.050 mg/L 02125/2014 nt + p-Cresol (TCLP) SW 846 method82700616 <0.050 mg/L 02/2W2014 Nitrobenzene (TCLP) Sweamethod02i013510 <0.050 mg/L 02125/2014 o-Gresol (TCLP) SW 840 method 827013610 <0.050 mglL 02/2512014 Pentachlorophenoi (TCLP) stiu aas meurod sz7o>3510 <0.250 mg/L 02/25/2014 Pyridine (TCLP) .50.050 mgiL 02/26/2014 Paint Filter rest sW M Method e0s5A . pass 02/20/2614 2,4,6-TP SWO46 Method 8151A <0.0003 mg/L 02126/2014 2,4..1) <0.0003 mg/L 02126J2014 1,11-Dichloroethylene SW848Method e28015030 <10mg/L 03/1412014 1,2-Dichlbroethane sVVW Method 826015M <1.0 mg/L 03/14/2014 Benzene SW= Method 8280/6030 <10 rng/L 0311412014 ReportA: 2014-01870 Page 1 of 5 environmental. Chemists, In.cv envirochem 6652 Windmill Way • Un1mntgton, NC 28405 (910) M-0=.(Lab) • 010) 39244424 (Fax) 710Bowsertown Road a Manteo, NC 27954 ANALYTIGAI, & coNSULTING (232) 473 5902 CHEMISTS:NCDEN1 DWQ CERTIRCATH 994. DLS CERTIFICATE #37729 Town 'Of Morehead City 706 Arendeli Street Morehead City NC 28557 Attention: C. Sutton Date of Report: Mar 21, 2014 Customer PO #., Ftdport #: 2014-01870 Rep'ortto• C. Sutton Project ID: Sludge Carbon' Tetrachloride S.we4e Method 6260/5030 <10 mg/L 03/14/20.14 Chiorobenzene Swu$ Method 826oftm <10 mg/L 03114/2014 Chloroform SWO45 Method 02W]5030 1$.6 mg1L 03114/2014 Methyl ethyl ketone sww Method 9200/5030 <50 mg1L 03f14/2014 T.etrachloroethylene swop Method =015tr30 <10 mglL 03/14/2014 TriGhloroethylene swaaa Method 826015030 <10 mg/L 03/14/2014 Vinyl Chloride swa4a Method 826W5030 <10 mg/L 03/14/2014 RCI Ignitability EPA 1030 <0.8 mm/sec 0212412014 Cyanide EPA 335.4 <0.124 mg/kg 02128/2014 Sulfide SM4500s.D <0.247mg/kg 03103/2014 pH sw a46 Method so45D 6.77 units 62120/2013 Sludge Residuals Aluminum. EPA200.7 1670 mg/kg OS/04/2014 Arsenic EPA200-7 9.44mg/kg 02/27120/4 Cadmium EPA200.7 a0.508 mg/kg 03110/2014 Calcium EPA200.7 45900mg/kg 02J26/2014 Chromium EPA2W.7 18:5 mg/kg 02/27/2014 Copper EPA200.7 .862 mg/kg ()3/14/2014 Lead EPA200.7 '&77 mg/kq 03/10/2014 Magnesium EPA 200.7 3640 mg/kg 02126/2014 Molybdenum EPA200.7 <5.07mg/kg 0214/2014 Nickel EPA2W.7 S.72mg/kg 02/24/2014 Potassium 9RA200,7 3126mg/kg 02/26/2014 SelenlOrn t=PA2ob.7 5,64 mg/kg 02/24/2014 Sodium EPA200.7 2900mg/kg 02/26/2014 Zinc EPA208.7 990 mglkg 03/04/2014 Ammonia Nitrogen EPA 350-1 1350 ing/kg 03/05/2014 - Total Kjeldahl.Nitrogen (TKN) EPA361-2 8360mglkg 03/1V2014 Repad M: 2014-01870 Page 2 of 6 Environmental Chemists, Inc. envirochem bb02 Windmill Way a Wilmington, NC 28405 a (910) 39M223. (Lab) • (910) 392-4424.(Vax) s 710 Bowsertown Road o Manteo, NC: 27954 ANALYTICAL 8. CON3UL77NG (252) 473-5702 CHEMISTS NCDENR: DWQ CERMCATE 094, DIS CE1i11RCATE 4137729 Town Of.Motehead City Date of.Report: Mar21, 2014 706 Arendell.Street Customer PO #: Morehead'City NC 28557 Report#- �014-01870 Attention: C. Sutton Report to: C. Sutton Project 113: Sludge Nitrate+Nitrite-Nitrogen EPA353.2 13.3 mglkg 03/11/2014 Total Solids (%) SM 2540 B 19.5 % 02/21 /2o14 Total Phosphorus SM4500FF 6480mg/kg 03/11/2014 Mercury SWM74710 2-.00mg/kg 02/28/2014 TCLP -Metals Arsenic EPA 200.7 <0.100 mg/L 02/25/2014 Barium EPA200.7 <0.100 mg/L 02/24/2014 Cadmium EPA200.7 <0.100mg/L 02124/2014 Chromium EPA 2aa.7 <0.100 mg/L 02/24/2014 Lead EP4200.7 <0.100 mg/L 02/24/2014 Silver EPA200.7 <0.100mg/L 02/17/2014 Selenium EPA200,8 <0.100mg/L 03/06/2014 Mercury EPA 245.1 <0.002 ing/L 02124/2014 Lab ID S'arhple ID: Collect Date/Time Matrix Sampled by 14-04551 Site:1 2/1812614 10:00. AM Solid/Sludge C.Sutton,& C.Dangerfield Test Method Results Date Analyzed Total Solids (%} SM2540 B MB % 02/21/2014 Fecal Density SM 92210 E MPN 24 hr 003 862069 MpWg 02/19/2014 Lab ID Sample ID: Collect Daterfime Matrix Sampled by 14-'04552 Site: 2 211812014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed 'total .Solids (?/o) sM2sa0 8 18.7 % 02/21/2014 Fecal Density s11t92210EMM 24hr503 854701 MPN/g 02119/2014 Repbrt#: 2014-01870 Page 3 of 6 Environmental Chemists. Inc. 6602 Windmill Way o lV'ilnunbdon, IN1C 28405 (910) 392-022-4 (Lab) (910) 392-024 (Rx) no fbvvsertown Road • Manteo, NC 27954 (252) 473 5702 ANALYTICAL & CONSULTING CHEMISTS- NCDENIL DWQ CERTMCATE W94. D15 CERTIRCATE 437729 Torn Of Morehead' City bate.of Report: Mar 21, 2014 70..6 Arandell Street Customer PO #: Morehead City NC 28557 Report;: 2014-01870 Attention: C. Sutton Report to; C. Sutton Project ID: Sludge Lab ED Sample ID: Collect Date/Time Matrix Sampled by 14-04553 Site: 3 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.DangeMeld Test Method Results Date Analyzed Total Solids (0/,) BM254.08 19.2 % 02/21/2014 Fecal.D.ensity SM92210EMPR 24hr503 835074.MPN/g 02/19/2014 . Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-04654 Site: 4 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.DangerField Test Method Results Date Analyzed Total Solids (%) SM25408 20.6 % 02/21/2014 Fecal Density son 9221C >= MPN 24 hr 503 774819 MPN/g 02/19/2014 Lab ID Sample ID: Collect Datefrime . matrix Sampled by 14-04555 Site: 5 2118/2014 10:00 AM Solid/Sludge C;Sutton & C.Dangerfield Test Method results Date Analyzed Total Solids (%) SM 2540 s 19.2 % 02/21/2014 Fecal Density SM92210EMPN 2ahr503. 832901}MPN/g 02/1942014 Lab ID Sample ID; Collect DateiTime Matrix Sampled by 14-04565 Sete: (i 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method . Results Date Analyzed Total Solids (%) SM 2540 a 18.2 % 02/21/2014 t=ecalDensiiy SMW2 ICHMPN 24h*s03 876713.MFN/g 02/19/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-04557 Site: 7 2/18/2014 10:00 AM Solid/$fudge CSutton & C.Dangerfleld Test Method Results Date Analyzed Total Solids.(%) SMI25406 18.8% 02121/2014 Fecal Density SM e221C S MPN 24 Br 503 852425 MPN/g 02/19/2014 Reportt- 2014-01870 Page 4 of S Environmental Chemists, Inc. 6602 Windxnffi Way - Wilmington, NC 28405 (910) 392-0223 (1,ab) • (910) 392-4424 (Fax) 710 Bawqerlown Road Manteo, N7C 27954 (252) 473-5702 ANALYTICAL & PON4ULTING CHEMISTS 4%jcDuNx. T)wQ crRTmcATL? #94. Dis cE.RnmcATi: #37729 Town Of Morehead City. Date of Report: -Mar 24,2014 708 Arandell Street Customer PO 4: Morehead City NC 28657 Report 0. 2014-01870 Attention, C. Sutton Report to: C. Sutton Project ID: Sludge Comment Sludge residuals and Fecal.density reported on a dry Weight basis. RCI and Paint Filter Test reported on an as 'received basis, V . - Reviewed by: b"o O&AL 1e�� ReMtV: 201"1070 Page 5 of 5 AnWytlwl & ConsvItiq Chemists ENVIRONMENTAL CHEM:ISTSv ING PICDEMR: EM0 CERTIAC.AT1614 # 94 Ndl)*-- DILS CERMFICA-nom# 37729 M11-11-FannN AfJn MAIN br- CLJSTnDY 6602 Windmill Way Mimington,, NG 20495 ORIM 910-492-9223 FAX 810-392-4424 CLIENT: PROJECT NAME.- REPORT N6- ADDRESS: CONTACT NAME: PO NO; REPORT To:* PHONE/FAX' COPY TO: AARK I 93t= TMr-- I m 1wiflivant- F = FfffifivnfW=Wiall- AT ci ktMaM.M= Still. SL= Shidue. Other. Sample identification Collection .4 9 PRESERVATION ANALYSJS REQUESTED Date Time, T.., 2 g LM .SLVJ, Ci'T'f Iv- I tf C (tflvi�4v,-lf 1000 C P R G G 0 P G G C P d. T -r. — G P G G C P 0 G- C P G. G :P G G— C P G. P G Transfer .4tinquished8l: DateMme Received Py; Datefrime 4-N 4�L- 0 2. Delivered Comments ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Morehead City WQ Permit Number: WQ0006018 WWTP Name: Town of Morehead Citv WWTP NPDES Number: NCO026611 Monitoring Period: From 01/01/14 To 12/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process -to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlienhle to niternntive nerfnrmed (( lass A nr Class R) rmmnlete the fnllnwina mnnitnrinu dntn- Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo.'Mean Maximum Units dences Analysis Fecal 2x10to the 6'h MPN 774819 840673 876713 CFU/g 0 Annually Grab SM9221C Coliform power per gram of total solids MPN 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0ption/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) X No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/I5A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Daniel Williams, Public Utilities Director Todd Larson, Operations ire or CCCPrepa •er Na�Title or print) le) (type o Lan ` r an app cabr .i t 9�F f gnature of Preparer* Date Signa re of Land App ier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Environmental Chemists, Inc. 6602 Windmill Way • Wilmington; NC 28405 irochen�7(910)-392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bow own Road • Manteo, NC 27954 ANALYTICAL &CONSULTING (252) 473-5702 CHEMISTS NCDEPiR: DWQ CERTIFICATE #194. bLS CERTIFICATE.#37729' Town Of Morehead City Date of Report: Mar21, 2014 706 Arendell Street" 'Customer PO k Morehead' City NC 28657 Report 0: 2014-01870 Attention: C. Sutton Report to: C. Sutton Project ID: Sludge Lab ID Sample ID: Collect DaWTime- Matrix Sampled by 14-04550 Site: sludge Class B 2/18/2014 10:00 AM Solid/.Sludge C.Sutton & C.Dangerfteld Test Method Results Date Analyzed Chlordane' SWa46'Method808iB13510 <0.005'mg/L 02/27/2014 Endrin sw846Method 8oa1M510. <0,00005"m9/L 02/27/2014 Heptachlor SW 846 Method 8061613510 <0.00005 mg/L 02/27/2014 Heptachlor epoxide Sw846Method.60a1B13510 <0.00005mg1L 02/27/2014 Lindane SW646Method W81B13510 '<0.00005mg/L 02/27/2014 Methoxychlor SW 846method so81t3135t0 <0.00005mg/L 02/27/2014 Toxaphene SW 846 Method 6081B13510 <0.005 mg/L 02/27/2014 1,4-Dichlorobenzene(TCLP) SW846method 827013510 <0.050mg/L 02/25/2014 2,4,5-Trichlorophen6l (TCLP) SW846mehA8270M10 <0.050mg/L 02/25/2014 214,6-Trichlorophenol. (TCLP) SW 846 method 827013510, <0.050 mg/L 02/25/2014 2,4-Dinitrotoluene (TCLP) sW e46 method 8270/3510 <0.050 mg/L 02/25120.14 Cresol (TCLP) Swe46 methotla270/3s10 <0.050 mg/L 02125/2014 Hexachloro-1;3-buta lene (TCLP) sw846 method 8270/3510 <0.050mg/L 02/25/2014 Hexachlorobenzene (TCLP) SW 846 method 827013510, <0.050 mg1L 02/25/2914 Hexachloroethane (TCLP) SW 846 Method 827013510 <0.050mg/L 02/25/2014 m + p-Cresol (TCLP) SW 846 method 827m3510 <0.050 mglL 02/25/2014, Nitrobenzene (TCLP) sw846method827o13510 <0.050mg/L 02/25/201.4, o-Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 02/25/2014 Pentachlorophenol (TCLP). S-w846Method 827013510 <0.250mg/L 02125/2014 Pyridine (TCLP) SW 846 method 8ii01351.0 <0.050 mg/L: 02/25/2014 Paint Filter Test SW 846 Method 9N5A pass 02/20/2014 2,4,5-TP SW846 McOW 6151A <0.0003 mg/L 02/26/2014 2,4-13. SW846 Method 8151A <0.0003 mg/L 02/26/2014 1,1-Dichlor`oethyiene SWWMethod 8-W503o <10mg/L 08/14/2614 1,2-Dichloroethane SWMMethod '82W/5030 <10'mg/L 03/14/2014 Benzene Swsas Method 8260/5030 c10 mg/L, 03/14/2014 Report#:: 2014-01870 Page 1, of 5. I 5 Environmental Chemists, Inc. envirochem 6602 Windmill Way 9 Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM. - ~ 710 Bowseriown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252).473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #t94. DLS CERTIFICATE #37729 Town Of Morehead City Date,of Report: Mar21, 2014 706 Arendell Street Customer PO #: Morehead City NC 285-57 Report #: 2014-01870 Attention: C: Sutton Report to: C. Sutton Project ID: Sludge Carbon Tetrachloride SM48 Method 826015030 <10 mg/L 03/14/2014 Chlorobenzene Swe48 Method 8280/5030 <10 mg/L 03/14/2014 Chloroform SW846Method 826N5030 18.6mg/L W114/2014 Methyl ethyl ketone SW846 Method 82601503D <50 mg/L 09/14/2014 Tetrachloroethylene SWW Method 8260#5030 <10 mg/L 03/14/2014 Trichloroethylene SWW Method 6260/5030- <10 mg/L 03/14/2014 Vinyl Chloride SW846method 82s0/5030 <10'mg/L 03/14120,14 RCI Ignitability EPA 1030 <0.8 mm/sec 02/24I2014 Cyanide EPA 335.4 �0.124 mg/kg 02/28/2014 Sulfide SM 4500 8 D <0.247 mg/kg 031031 014 pH SW 946 Mefd 9MD 6.77 units 02/20/2013 Sludge Residuals Aluminum EPA20o.7 1`570 mg/kg 63/04/2014 Arsenic EPA200.7 9.44 mg/kg 02/2712014. Cadmium EPA200-7 <0:508mglkg 031101201:4 Calcium EPA200.7 46900mg/kg 02/26/2014 Chromium EPA200.7 18.5 mg/kg 02/27/2014 Copper ' EPA200.7 862 mg/kg 03/14/2014 Lead EPA2001 8.77 mg/kg_ 03/10/2014 Magnesium EPA 200.7 3640 mg/kg 02/26/2014 Molybdenum EPA200.7 <5.07 mg/kg 02/24/2014 Nickel EPA200.7 8.72mg/kg 02/24/2014 Potassium EPA200.7 3120mg/kg 0212612014 Selenium EPA200.7 5.64 mg/kg 02/24/2014 . Sodium ;EPA20o.7 29Q0 mg/kg 02/26/2014 Zinc EPA200.7 990 mg/kg 03/04/2014 Ammonia Nitrogen EPA 350.1 1350 mg/kg 03/05/2014 _ Total Kjeldahl. Nitrogen (TKN) EPA3512 8350 mg/kg 03/11/2014 Report #:: 2014-01870 Page 2 of 5 Environmental Chemists, Inc. 6602 Windmill. Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) ' SM 710 Bowsertown Road • Manteo; NC 27954 ANALYTICAL & CONSULTING (252)' 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town Of Morehead City Date oi.Report: Mar 21, 2014 706 Arendell Street Customer PO #: Morehead City NC 28557 Report #: 2014-01876 Attention: C, Sutton Report, to:, C. Sutton Project ID: Sludge Nitrate+N'itrite-Nitrogen EPA 353.2 13.3 mg/kg. 63/11/2014 Total Solids (%) SM 2540 B 19.5 % 02/21/2014 Total Phosphorus SIN 400 P F 6480 mg/kg 01112014 Mercury SWM 7471e 2:00 mg/kg. 02/28/2014 TCLP Metals Arsenic EPA 200.7' 'Barium EPA200.7 'Cadmium EPA 200.7 Chromium EPA200.7 <0.100 mg/L '02/25/2014 <0.100 mg/L 02/24/2014 <0.100 mg/L. 02124/2014 <0.100 trig/L 02/24/2014 Lead EPA 200.7 <0.100 mg/L '02/24/2014 Silver EPA 2001 <0.100 mg/L 02/27/2014 Selenium EPA200.8 <0.100mg/L 03/06/2014 Mercury EPA 245.1 <0.002 mg/L 02/24/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-04551 Sitev1 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids {%) SM 2540 B 18.6 % 02/21/2014 Fecal Density SM 9221C EAftPN 24 hr 503' 862060 MPN/g 02/19/2014 Lab ID Sample ID: 'Collect Daterrime. Matrix Sampled by 14-04552 Site: 2 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 a 18.7 % 02/21/2014 Fecal Density SM 9221C E MPN 24 ht 503 864701 MPN/g 02/19/2014 Report #:: 201"1870 Page 3 of 5 Environmental ;Chemists,, Inc. 6602 Windmill Way 0' Wilmington, NC 28405 spa Q (910) 392-0223 (Lab) (910) 392-4424 (Fax) 710 Bowsertown Road r Manteo, l4C 27954 ANALYTICAL & CQNSULTING (252) 473-5702 CHEMISTS NCDBNIL• DWQ CERTIFICATE 094. DIS.CE=CATE #37729 Town Of Morehead City Date of Report: Mar'21, 21114 7.06 ArendellStreet Cgstomer PO.M Morehead City NC 28557 Report #: 2014-01870. Attention: ' C. Sutton Report to; C. Sutton Project 1D: Sludge Lab ID Sample ID: Collect Date/Timb. Matrix Sampled by 14-04553 Site: 3 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results- Date Analyzed Total Solids (OA) sM 2540 a 19,2 % 02/21/2014 Fecal Density SM 92 1C EMPN 24 hr503 835674 MPN/g 02/19/2014 Lab ID Sample. ID: Collect DatelTime Matrix. Sampled by 14-04554 Site: 4 2/18/2014 10:00 AM Solid/Sludge, C.Sutton & C.Dangerfield Test Method Results Data Analyzed Total Solids (%) SM2540 s 20.6 % 02121/2014 Fecal Density" SM 9221C E MPN 24 hr 503 774819 MPNIg 02'11912014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-04556 Site! 5 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solid's (%) SM 2540 a 19.2 % 02/21/2014 Fecal Density SM 9221C E MPN 24 hr 5D3 832900' M PN/g 02/19/2014 Lab 1D Sample ID: Collect Datefrime Matrix Sampled by 14-04556 Site: 6 2/18/2014 10:00 AM Solid%Sludge C_.Sutton &,C.Dangerfield Test Method Results DateAnalyzed Total Solids (%) SM2540 a 18,2 % 02/21/2014 Fecal Density SM suck E MPN 2a hr so3 -876713MPN/g 02/19/2014 Lab ID Sample ID: Collect Date/Time. Matrix Sampled by 14-04557 Site: 7 2/18/2014 10:00 AM Solid/Sludge C.Sutton '& C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 s 18.8 % 02/21/2014 Fecal Density SM92210EMPN 24hr5D3 852425MPN/g 02/1-9/2014 Report #:: 2014-01870 P 8.4 0f 5, a9 Envrironmental Chemists, Inc. envirochem 6602 W'indinM Way • Wilmington; NC 28405 (910) 392-0223 (Lab) • (910) 3924424 (Fax) 710 Bowsertown Road • Manteo, NG27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR DWQ CERTIFICATE #94. DLS CERTIFICATE'#37729 Town Of Morehead City Dateof Report: Mar 24,. 2014 706 Arendell Street Customer PO #: Morehead City NC 28557 Report #: 2014-01870 Attention: C. Sutton Report to: C. Sutton Project ID: Sludge Comment: Sludge residuals and Fecal density reported on a dry weight basis. RCI and Paint Filter Test reported on an as received basis. Reviewed by: RepatB: 201401870 Page 5 of 5 i ENVIRONMENTAL CHEMISTS, INC Analytical &Consulting Chemists NCDENR:.DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CWAKOF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICES 910-392-0223 FAX 910-392-4424 info@environmontatchemists.com FAR CLIENT: PROJECT NAME., REPORT N& ADDRESS':. CONTACT NAME:, PO NO: REPORT TO: PRONEIF'AX: COPY TO: small: Samnlsd Bv: ,(:_ J'44,,,, f r. SAMPLE TYPE 1 e Influant. IE = Effluanf. W G Wall_ ST n Sfrnam_ S0 =. Snil- SL = Sludna- Ofharz Sample ldentiflcation I-- MM ANALYsIS REQUESTED M. I emperacur n f�ceceivea: � "a wceeptea: - ejec ea:. Resample quest Ied: Delivered Recelvecl By: _ /.D Date: i`t Timer ~� Comments: TUR A OUND• FECAL DATA SHEET Lab result Log 862069 5.94 Min 854701 5.93 Max 835074 5.92 Geometric Mean 774819 5.89 832900 5.92 876713 5.94 852425 5.93 Average 5.92 774819 876713 840673 Agricultural Lime Application Log Year: 2014 Project: Morehead City, NC *Lime to be applied after field conditions improve NCDA&CS _..�:_nomic Division Phone: (919) 733-2655 Website: www:=___•-(.gov/agronomil ReportNo. FY,,_—=038345 �y� Predictive Client: Robert B (Bobby) Riggs 483 Wetherington Landing Rd Advisor: Synagro ATTN: Will Varner ;+ i` �' Soil Report Mehlich-3 Extraction Stella, NC 28582 Sampled County: Carteret 2828 Tryon Rd /284 Boger Rd Raleigh, NC 27603 - k�1:1ryI1.N yF Sampled: Received: 06/25/2014 Completed: 07/03/2014 Farts: CR-7 Links to Helpful Information Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.9 120 -160 0 40 0 0 0 0 0 0 Note: 3 2 - $pH Test Results [units -W/V in glcd; CEC and Na in meq/100 cmP; NO3-N in mg/drrt3]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 1.25 6.0 74 1.6 5.3 301 52 57 12 36 40 41 320 320 568 0.0 Sample ID: 3B Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu . B Information Lime History: 1 -Corn, grain 1.1 120 -160 0 40 0 0 0 0 0 0 Note: 3 2 - $pH Test Results [units - W/V in g1crtr3; CEC and Na in meq/100 cm3; NO3-N in mg/dd]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 1.23 5.5 67 1.8 5.1 291 49 52 11 38 43 43 383 383 344 0.0 North Carolina 1 •'6 May r �'i)tY1441! 7fU5e FU16ll �L»Pilili5SI4P1 Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS ,. ,=nomic Division Phone: (919) 733-2655 Website: www.t �__ .gov/agronomil Report No. FY ..=_038345 Robert B (Bobby) Riggs Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or.problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find the exact fertilizer grade recommended on the report, visit www.ncagrgov/agronomi/obpart4.htm#fs to find information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer Test Results Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-I potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral -organic soil class N Na NO3-N ORG pH P-1 P205 S-1 SS-1 W/V The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not . Zn-I routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uvrst.htm for more information. nitrogen sodium nitrate nitrogen organic soil class current soil pH phosphorus index phosphate sulfur index soluble salt index weight per volume zinc availability index zinc index