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Home My WebLink AboutWQ0034880_Monitoring (Report)_20190315SUBMIT FORM ON YELLOW PAPER ONLY IDEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES,- INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM - • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATIONL Please Print Clearly or Type PERMIT Number: Expiration Date: 12t31/2021 Facility Name: UNC COASTAL STUDIES INSTITUTE Non -Discharge_ W00034880UIC Permit Name (if different): NPDES Other Facility Address: PO BOX 689 / 850 NC 345, MANTEO NC 27954 TYPE OF PERMITTED OPERATION BEING MONITORED (street) County_ DARE El Lagoon El Remediation: Infiltration Gallery caryy (state) czp) ❑ Spray Field ❑ Remedlation: Contact Person: IRVIN W. EDWARDS, JR Telephone#: 252.475.0350 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name UNC CSI No. of wells to be Sampled: 4 Water Source Heat Pump ❑'I Other: INFILTRATION. POND. from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from. Permit): MW-1 Date sample collected: 11/1/2018 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH omoo: 7.1 'units 'Temp_ .'000ls 23' °C DRY at Depth to Water Level 92546:_ 8.2 Screened Interval: 4.8 ft. to 15 ft. Spec. -Conti. 00094: µMhos time of sampling,, Measuring Point,is ft. above land surface Relative M.P. Elevation: ft. Odor 000m: YES check Volume of water pumped/bailed before sampling: 0.5 gallons, ,Appearance CLEAR 'here:❑ Samples for, metals were collected' unfiltered: ❑ YES '❑ NO - and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/1/2018 Laboratory Name: ENVIRONMENTAL CHEMIST Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. ' COD oo335 mg/L Nitrite. (NO2) as N oo615 <0.02 mg/L Pb - Lead 01051 ug/L "q ' Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc o1692 mg/L JOS Colifonn: MF Total 31504 /100mL Phosphorus: Total' as P owm mg/L �,pR (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 404 mg1L AI -Aluminum o41o5 mg/L pH' -(Lab) 00403 units Ba - Barium o1007 _ ug/L NITRATE+NITRITE-NITRO,OEN: <0.02,mg/L. TOC oomo 7:3 mg/L Ca - Calcium oo916 mg/L `� °'," ": ` r-- J Chloride 0094G 46 mg/L Cd - Cadmium 01027 ug/L 9 Arsenic oloo2 , ug/L Chromium: Total 01034 _ ug/L, Grease and Oils 00552 mg/L Cu - Copper 01042 _ mg/L 'ORGANICS: (byGC, GC/MS, HPLC) /y Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #'.'I;4 Al'G"'!6 " :•REPb121' )'i) I Sulfate .00s45 mg/L Hg -'Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia'oamo 3 mg/L Mg = Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen,, Total) Mn - Manganese olom ugjL method. # T_KN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY • • . DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM - e e 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919.807-6306. FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 12/34/2021 Facility Name: UNC COASTAL STUDIES INSTITUTE Non -Discharge W00034880 UIC Permit Name (if different): NPDES Other Facility Address: PO BOX 689 / 850 NC 345, MANTEO NC 27.954 TYPE OF PERMITTED OPERATION BEING MONITORED (street) County. DARE g ❑ Lagoon ❑Remediation: Infiltration Gallery (City) (state) (zip) ❑ Spray Field ❑ Remediation'. Contact Person: IRVIN W. EDWARDS; JR Telephone#: 252.475'.0350 El Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name UNC CSI No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: INFILTRATION POND from Flennn SAMPLING INFORMATION' If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 1111/2018 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2_in. pH 00400: 8.8 units Temp. 00011c 23.7 °C DRY at Depth to Water Level 82646: 12 Screened Interval: 4.8 ft. to 15 ft. Spec. Cond. 00094: µMhos 'YES time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor o0085: check Volume of water pumped/balled before sampling: O:5 gallons Appearance GREY here: Samples for metals were collected unfiltered: ❑ YES O ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY'IN FORMATION Date sample analyzed: 11/1/2018 Laboratory Name: ENVIRONMENTAL CHEMIST Certification No. 94 PARAMETERS NOTE: Values_ should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as'N ooeis <0.02 mg/L Pb - Lead oa051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N oos2o <0.03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use!MPN method for highly turbid samples) Orthophosphate'70507 mg/L Other (Specify Compounds and Concentration Units):, issolved Solids:Total 70300 '3820 rng/L Al - Aluminum 01 105 mg/L. PH (Lab) 00403 units. Ba - Barium o1ow ug/L NITRATE+NITRITE-NITROGEN: <0.03 mg/L TOC 00680 21.7 mg/L Ca - Calcium 00916 mg/L Chloride 00940 1820 mg/L Cd —Cadmium 01027 ug/L Arsenic oloo2 ug/L Chromium: Total 01034 ug/L Grease and Oiis,0055z mg/L Cu -Copper 01042 ,mg/L ORGANICS: (by GC, GC/MS, HPLC). Phenol 32730 ug/L Fe - Iron o1045 ug/L (Specify test and method #. ATTACH LAB REPORT.). Sulfate 00945 mg/L Hg = Mercury 719oo ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia oo610 35.2 mg/L Mg - Magnesium o0927 mg/L „ method # (Ammonia,Nltrogem NH3 as N', Ammonia Nitrogen,, Total) Mn - Manganese o1o55 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L ,method # For Remediation Systems Only, (Attach. Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%- IRVIN W. EDWARDS, JR. Permittee (or Authorized Agent) Name and Title - Please print or type uvv=aa RBH. olzu I 'SUBMIT FORM ON YELLOW I'AVLK ONLY DWATER, QUALITY MONITORING: IANCE REPORT FORM FACILITY INFORMATION__ Please Print Cleary or ,Type, Facility Name:. UNC COASTAL STUDIES INSTITUTE Permit Name (if different): Facility Address: PO BOX 689 L 850 NC 345, MANTEO NC 27954 County DARE (City) (State) Ptp) - act Person: IRVIN W. EDWARDS, JR Telephone* - 252.475.0350' Location/Site Name UNC CSI' No. of wells to be sampled: 4 ATMENT OFENVIRONMENT S NATURAL RESOURCES ,ION OF WATER RESOURCES - INFORMATION PROCESSING UNIT MAIL SERVICE CENTER; RALEIGH, NC 27699-1617 Phone: 919-807-6306 Number: Expiration Date: ;harge W00034880 UIC_ 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: 'Infiltration Gallery El Spray Field ❑ Remediation: ❑ Rotary Distributor �El Land Application of -Sludge ❑ Water Source Heat, Pump ❑ Other: 'INFILTRATION PON SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW4 Date sample collected: 1111/20187 FIELD ANALYSES: WAS Well.Depth 15 ft. 'Well Diameter: 2. in.. pH 00400: 6.,6 units Temp. 000li z3s °C DRY at Depth'to Water Level 82546: 9.3 Screened' Interval: 4.8 ft. to 15 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is ft: above' land surface 'Relative M.P. Elevation: ft. Odor 00065: _ YE check Volume of water pumped/bailed before sampling. _ 0.5: _ gallons Appearance TAN here:) I SamDleS for metals were collected: unfiltered: El YES ❑' N01 and field acidified: ❑ YES ❑ NO' ate sample analyzed: 11/1/2018 Laboratory Name: ENVIRONMENTAL CHEMIST Certification No. 94 kRAMETERS NOTE: Values should reflect :dissolved and colloldat concentrations. COD 00336 mg/L Nitrite (NOz) as, N ow <0:02 mg/L Pb = Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /1'00ML Nitrate (NO3) as 00620 <0.08: mg/L Zn = Zinc 01092 mg/L Coliform:.MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid sarriples) 'Orthophosphate 70507 mg/L Ived ,Solids:Total 7,0300 592 mg1L �pH (Lab)'00403 units'. TOG 00690. 44.4 mg/L Chloride 00940 117 mg/L Arsenic'01002 ug/L Grease and Oils' oo552 mg/L Phenol 32730' ug1L Sulfate 00945 mg/L fic. Conductance 000g5 ytMhos Total Ammonia loo6lo 3.4 mg/L (Ammonia, Nitrogen;,NH3 as N Ammonia Nitrogen, Total) TKN as'N 00825 mg/L Al - Aluminum ,01105 mg/L Ba - Barium t)1007 ug/L Ca - Calcium 00916 mg/L Cd -Cadmium M27 Y91L. Chromium: Total 01034 ug/L C'u = Copper 01.042: mglL Fe - Iron 01045 ug/L Hg - Mercury 71900 ug1L K -Potassium 00937 mg/L Mg, - Magnesium 00927 mg/L Mn -'Manganese 01o55 ug/L Ni - Nickel o1667 ug/L Other -(Specify Compounds and Concentration Units): , NITRATE+NITRITE:NITROGEN. <0i08 mg1L ORGANICS: (by GC, GC/MS; HPLC) (Specify test and method #. ATTACH LAB REPORT.): Lab Report, Attached? Ell (1) ❑ No (,0) VOC 7873 , Method # method'# method # method 4 For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:- mg/L tmuent I otat vuL;s: mg/L vVL, rtemovao io - GW-59 . Rev. 8/2013. SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENT 8, NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 12/31 /2021 Facility Name: UNC COASTAL STUDIES INSTITUTE Non -Discharge WQ0034880 UIC Permit Name (if different): NPDES Other Facility Address: PO BOX 689 / 850 NC 345, MANTEO NC 27954 TYPE OF PERMITTED OPERATION BEING MONITORED (Street) County DARE ❑ Lagoon ❑ .Remediation: Infiltration Gallery (City) (State) (zip) ❑ Spray Field ❑ Remediation: Contact Person: IRVIN W. EDWARDS, JR Telephone#: 252.475.0350 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name UNC CSI No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: INFILTRATION POND from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 11/1/2018 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.7 units Temp. 0001c 23.4 oC DRY at Depth to Water Level 82546: 9.9 Screened Interval: 4.8 ft. to 15 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 0006s: YES check Volume of water pumped/bailed before sampling: 0.5 gallons Appearance TAN here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/1/2018 Laboratory Name: ENVIRONMENTAL CHEMIST Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N owi5 <0.02 mg/L Pb - Lead oimi ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.08 mg/L Zn - Zinc ortom mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 476 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium olo07 ug/L NITRATE+NITRITE-NITROGEN: <0.08 mg/L TOC 00680 32 mg/L Ca - Calcium 00916 mg/L Chloride 00940 11 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury'71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia oo6lo 6 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only, (Attach Lab Reports): influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOG Removal/o IRVIN W. EDWARDS, JR. Permiftee (or Authorized A4ent) Name and Title -'Please print or tune GW-59 Rev.8/2013 �� Chemists, �� ° 6hO2Windmill Way, Wilmington, 0C28405 ° 910.392.0223Lah , 910.392.4424 Paz 710Dm,*sm"rnRoad, Mameo,NC27954 " 252.473.5702Lab/Fsx 255'8Wibnb`gtonBj,,,Tbvvo�JvckonoNUleYJC28540 " 910.347.5843Cah/F^x ANALYTICAL aCONSULTING CHEMISTS iofb(�osimnmnnmlobvmis,uuom East Carolina University Date of Report: Nov 1Q.2O18 1001 East 4thStreet CustmmoerPO#: 18YN-1900 Greenville WC 27858 Customer ID: 12110019 Attention: PatriokShenod Report #: 2018-18060 Project ID: U0C Coaata|Studiea-MVV Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18'45632 SUtm:kAW-1 11/1X2018 1:10 PM Water Tom Beasley Test - Method Results Date Analyzed Color ««m' Clear 1101/2018 Depth towater, ft. Depth mWater, Ft. 8.2feoi 11/01/2018 �n�-'''---- ' ' - ' --' mn mmumge -- ��'�--^--- --------'----' --- -:'' '---- 2LOmg� '-----' - - �1M8�O18 Gallons bailed before sampling Gallons Bailed before samnmm 0.50gaUona 11K01/2018 Odor o»^/mati« Yes 11/01/2018 Total Dissolved Solids (TDS) SM 2540 « 404nog/L 11/85/2018 Temperature SM 2550 a 23.0C 11/01/2018 Chloride owwe«ms 46nmg/L 11/05/2018 pH mm*«»»*a 7.09unita 11/01/2018 Total Organic Carbon (TOC) mw««1»a 7.3rng/L 11/06/3018 1.1.1.2-Tedosch|onoathene ow6200o <0.5pg/L 11/09/2018 1.1.1-Trich|onoethane aMeu»»n <0.5pg/L 11/09/2018 1.1.2,-2-Tetnach|onooM>one ' � -' ameu«»: `�` ' ' `� ' ' ' �tU5pQ/L ' ` `' 11/00/2018 1.1.2-Frichloroethane mmeu»«« <0.5pg/L 11/09K2018 1.1-Dioh|onoethane smnamu <0.5pg/L 11/09/2018 1.1-Dich|onoathene uMmmun <0.5pg/L 11/09/2018 1.1-Diuh!oropnopena «mmm«o <0.5pg/L 11/00/2018 1.2.3-Tdch|orobenzone mwsu«»o <0.5pg/L 11/09/2018 1.2.3-Trch|oropropena mmmm»u <0.5pg/L 11/09/2018 1.2.4-Thch|onubenzene «Mmm»o <0.5pg/L 11/09/2018 1.2.4-Thnnethy)benzane swuxo»c <0.5U0/L 11/09/2018 1.2,Dibromo'3-Ch(onopnopane am«u»«» «0.5pg/L 11/08/2018 1.2-Oibnnnnoedhane »womm« <0.5pQ/L 11/00/2018 1.2-Oioh(onobenzene aMau» o «0.5pg/L 11/09/2018 1.2'Dich|oroethmne mmmm»u <0.5pg/L 11/03/2018 1.2,Dich|onopropana omnu»»o <0.5pQ/L 11/09/2018 ` : '7.-'� -gN"' t w g �aa }- ems Env 0 Chemists, ronme ntal I 66021Nindmill �Vay 4%I11Mh-igton, NC 28405 Lab - _ 910.392.0223 910-392.4424 Fax �FA. 710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 m 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHBOISTS info@enviroiimentaiehemists.com East Carolina University Date of Report: Nov 19, 2018 1001 East 4th Street Caastomer PC #: 18M-1900 Greenville NC 27858 Customer ID: 12110019 Attention: Patrick Sherrod Report M 2018-18060 Project ID: UNC Coastal Studies-MW 1,3,5-Trimethylbenzene SM 6200C <0.5 pg/L 11/09/2018 1, 3-Dichlorobenzene SM 6200C <0.5 pg/L 11 /09/2018 1,3-Dichloropropane SM 6200C <0.5 pg/L 11/09/2018 1,4-Dichlorobenzene SM 62000 <0.5 pg/L 11/09/2018 2,2-Dichloropropane SM 6200C <0.5 pg/L 11/09/2018 2-Chlorotoluene ..... - SPA 6200c.. ............. -4*Z pg1L ...... ..................1-1/09/2018 4-Chlorotoluene SM 6200C <0.5 pg/L 11/09/2018 Benzene SM 6200C <0.5 pg/L 11/09/2018 Bromobenzene SM 6200C <0.5 pg/L 11 /0912018 Bromochloromethane SM 6200C <0.5 pg/L 11/09/2018 Bromodichloromethane SM 6200C <0.5 tag/L 11/09/2018 Bromoform SM 6200C <0.5 lag/L 1110912018 Bromomethane SM 6200C <0.5 pg/L 11/09/2018 Carbon tetrachloride SM 6200C <0.5 pg/L 11/09/2018 Chlorobenzene SM 6200C <0.5 pg/L 11/09/2018 Chloroethane .. SM 6200c ........... <0.5 pg/L_ ..11 /09/2018 Chloroform SM 6200C <0.5 pg/L 11/09/2018 Chloromethane SM 6200C <0.5 pg/L 11/09/2018 cis-1,2-Dichloroethene SM 6200c <0.5 lag/L 11 /09/2018 cis-1,3-Dichloropropane SM 6200C <0.5 pg/L 11109/2018 Dibromochioromethane SM 6200c <0.5 pg/L 11/09/2018 Dibromomethane SM 6200C <0.5 tag/L 11/09/2018 Dichlorodifluoromethane SM 620oc <0.5 lag/L 11/09/2018 Ethylbenzene SM 6200C <0.5 pg/L 11/09/2018 Hexachlorobutadiene SM 6200C <0.5 pg/L 11/09/2018 Isopropylbenzene SM 6200c <0.5 pg/L 11/09/2018 M+P Xylene SM 6200C <1.0 pg/L 11/09/2018 Methylene chloride S1016200c <0.5 pg/L 11/09/2018 Naphthalene SM 6200C <0.5 pg/L 11/09/2018 n-Butylbenzene SM 6200c <0.5 pg/L 11/09/2018 Report #1:: 2018-18060 Race 2 of 13 n Environmental Chemists, Inc. 66021Nindrtiill l.Vay, Wilmington, NC 28405 a 910.392.0223 Lab a 910392.4424 Fax te r_ 710 Bowsertown Road, Manteo, NC 27954 S 252.473.5702 Lab,/Fax 255-A Wilmington 7 ab/Fa., Highway, acksonvil1e NC 28540 6 910 347.5843 L� x g Y ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com East Carolina University Date of Report: Nov 19, 2018 1001 East 4th Street Customer PO #: 18M-1900 Greenville NC 27858 Customer ID: 12110019 Attention: Patrick Sherrod Report 9: 2018-18060 Project ID: UNC Coastal Studies-MW n-Propylbenzene SM 6200C <0.5 tag/L 11 /0912018 ortho-Xylene SM 6200C <0.5 pg/L 11/09/2018 p-isopropyltoluene SM 6200C <0.5 tag/L 11/09/2018 sec-Butylbenzene SM 6200C <0.5 tag/L 11/09/2018 Styrene SM 6200C <0.5 tag/L 11/09/2018 tert-Bu 1_bpnzene.. _ ...... SM 62000 ... <0.5 tag/L .... 11109/2018 Tetrachloroethene SM 6200C <0.5 tag/L 11/09/2018 Toluene SM 6200C <0.5 tag/L 11 /0912018 Trans-1,2-Dichloroethene SM 6200C <0.5 tag/L 11/09/2018 Trans-1,3-dichloropropene SM 6200C <0.5pg/L 11/09/2018 Trichloroethene SM 6200C <0.5 tag/L 11/09/2018 Trichlorofluoromethane SM 6200C <0.5 tag/L 11/09/2018 Vinyl chloride SM E200C <0.5 tag/L 11/09/2018 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA353.2 < 0.02 mg/L 11/02/2018 Nitrate+Nitrite-Nitrogen EPA353.2 < 0.02 mg/L 11/13/2018 Nitrate Nitrogen Subtraction Method < _ 9 _ 0.02 mg/L 11 /17/2018 Report #:. 2018-18060 Paae 3 of 13 Environmental Chemists, 401. -.. f3 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab 910.392.4424 Fax Q 710 13owseeown Road, Manteo, NC 27954 e 252.470.5702 Lab/Fax - l 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(cJenvironmentalchemists.com East Carolina University Date of Report: Nov 19, 2018 1001 East 4th Street Customer PO #: 18M-1900 Greenville NC 27858 Customer ID: 12110019 Attention: Patrick Sherrod Report #: 2018-18060 Project ID: UNC Coastal Studies-MW Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-45633 Site: MW-2 11/1/2018 12:58 PM Water Tom Beasley Test Method Results Date Analyzed Color color Grey 11/01/2018 Depth to water, ft. Depth to water, Ft. 11.8 feet 11101 /2018 Ammonia Nitrogen ............... ......................-.......... EPA350.1 ...... .... .....- .. .. ............ 35.2 mg/L _.... .......... 11/18/2018 Gallons bailed before sampling Gallons Bailed before sampling 0.50 gallons 11/01/2018 Odor Qualitative Yes 11 /0112018 Total Dissolved Solids (TDS) SM 2540 C 3820 mg/L 11/05/2018 Temperature SM 2550 B 23.7 C 11/01/2018 Chloride SM4500 Cl E 1820 mg/L 11/05/2018 pH SM450DHB 6.81 units 11/01/2018 Total Organic Carbon (TOC) SM 5310 B 21.7 mg/L 11/05/2018 1, 1, 1,2-Tetrachloroethane SM 6200C <0.5 pg/L 11/09/2018 1, 1, 1 -Trichloroethane SM 6200C <0.5 pg/L 11/09/2018 1,1,2. 2-Tetrachioroethane SM 6200C <0.5 pg/L 11 I09/2018 1,1,2-Trichloroethane SM 6200C <0.5 pg/L 11/09/2018 1,1-Dichloroethane SM 6200C <0.5 pg/L 11/09/2018 1,1-Dichloroethene SM 6200C <0.5 pg/L 11/09/2018 1,1-Dichloropropene SM 6200C <0.5 pg/L 11 /09/2018 1,2,3-Trichiorobenzene SM 62000 <0.5 pg/L 11109/2018 1,2, 3-Trichloropropane SM 6200C <0.5 pg/L 11/09/2018 1,2,4-Trichlorobenzene SM 6200C <0.5 pg/L 11/09/2018 1,2,4-Trimethylbenzene SM 6200C <0.5 pg/L 11/09/2018 1,2-Dibromo-3-Chloropropane SM 6200C <0.5pg/L 11/09/2018 1,2-Dibromoethane SM 6200C <0.5 pg/L 11/09/2018 1,2-Dichlorobenzene SM 6200C <0.5 pg/L 11/09/2018 1,2-Dichloroethane SM 6200C <0.5 pg/L 11/09/2018 1,2-Dichloropropane SM 6200C <0.5 pg/L 11/09/2018 Report #:: 2018-18060 Paae 4 of 13 Environmental fists, Inc. 5002 Windmill Way, Wilmington, NC 2840.5 Q 910.392.0223 Lab v 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax ' sro„ 255-ra g g ton Highway, aY Jacksonville, acksonville, NC 28540 g 910.347.5843 Lab/Fax �.. ANALYTICAL & CONSULTING CHEMISTS info a)environmentalchen3ists.com East Carolina University Date of Report: Nov 19, 2018 1001 East 4th Street Customer PO #: 18M-1900 Greenville NC 27858 Customer ID, 12110019 Attention: Patrick Sherrod Report #: 2018-18060 Project ID: UNC Coastal Studies-MW 1,3,5-Trimethylbenzene SM 6200C <0.5 µg/L 11/09/2018 1,3-Dichiorobenzene SM 6200C <0.5 µg/L 1 1/09/2018 1,3-Dichloropropane SM 6200C <0.5 µg/L 11/09/2018 1,4-Dichlorobenzene SM 62000 <0.5 µg/L 11/09/2018 2,2-Dichloropropane SM 6200C <0.5 µg/L 11/09/2018 27Chlorotoluene....... ...... SM 6200c...................... .............................<0.5 µg/L ...................... -.1.1/0912018 . . 4-Chlorotoluene SM 620DC <0.5 µg/L 1110912018 Benzene SM 6200C <0.5 µg/L 11 /09/2018 Bromobenzene SM 6200C <0.5 µg/L 11/09/2018 Bromochloromethane SM 6200C <0.5 µg/L 11/0912018 Bromodichloromethane SM 6200C <0.5 µg/L 11/09/2018 Bromoform SM 6200C <0.5 µg/L 11/09/2018 Bromomethane SM 62000 <0.5 µg/L 11/09/2018 Carbon tetrachloride SM 6200C <0.5 µg/L 11/09/2018 Chlorobenzene SM 62000 <0.5 µg/L 11/09/2018 Chioroethane . SM 6200C <0.5 µg/L . _.... - . _ 1 i/09/2018 Chloroform SM 6200C <0.5 µg/L 11/09/2018 Chloromethane SM 6200C <0.5 µg/L 11/0912018 cis-1,2-Dichloroethene SM 6200C <0.5 µg/L 11/09/2018 cis-1,3-Dichloropropene SM 6200C <0.5 µg/L 11109/2018 Dibromochloromethane SM 6200C <0.5 µg/L 11/09/2018 Dibromomethane SM 6200C <0.5 µg/L 11/09/2018 Dichlorodifluoromethane SM 6200C <0.5 µg/L 11/09/2018 Ethylbenzene SM 6200C <0.5 µg/L 11/09/2018 Hexachlorobutadiene SM 6200C <0.5 µg/L 11/09/2018 lsopropylbenzene SM 6200C <0.5 µg/L 11/09/2018 M+P Xylene SM 6200C <1.0 µg/L 11/09/2018 Methylene chloride SM 6200C <0.5 µg/L 11/09/2018 Naphthalene SM 6200C <0.5 µg/L 11/09/2018 n-Butylbenzene SM 6200C <0.5 µg/L 11/09/2018 Report #:: 2018-18060 Page 5 of 13 s Fyn =:v Envitro ental Chemists, Inc. - 6602 Windmill Way, Wilmington, NC 28405 s 910.392.0223 Lab ° 910.392.4424 Fax 710 Sowsertown Road Manteo, NC 27954 : 252 473.5702 Lab/Fax 255-A Wdmin-ton I-Ii hway, acksonville NC 28540 * 910.347.5843 Lab/Fax . - a g 1� , ANALYTICAL & CONSULTING CHEMISTS inI'oCenviroaimentalchemists.com East Carolina University Date of Report: Nov 19, 2018 1001 East 4th Street Customer P® : 18M-1900 Greenville NC 27858 Customer 10: 12110019 Attention: Patrick Sherrod Report+: 2018-18060 Project ID: UNC Coastal Studies-MW n-Propylbenzene SM62ooc <0.5pg/L 11/09/2018 ortho-Xylene SM62ooc <0.5 pg/L 11/09/2018 p-Isopropyltoluene SM 6200c <0.5 pg/L 11/09/2018 sec-Butylbenzene SM 6200c <0.5 pg/L 11/09/2018 Styrene SM62ooc <0.5 pg/L 11/09/2018 tent-13 (benzene............ _ . SM 62ooc ty . .............. <0.5 pg/L ....... ..............1.1 /09/2018 Tetrachloroethene SM 6200c <0.5 pg/L 11/09/2018 Toluene SM 62ooc <0.5 pg/L 11/09/2018 Trans-1,2-Dichloroethene SM6200c <0.5 pg/L 11/09/2018 Trans-1,3-dichloropropene SM6200C <0.5pg/L 11/09/2018 Trichloroethene SM 6200c <0.5 pg/L 11/09/2018 Trichlorofluoromethane SM 6200c <0.5 Ng/L 11/09/2018 Vinyl chloride SM62ooc <0.5 pg/L 11/09/2018 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11/02/2018 Nitrate+Nitrite-Nitrogen EPA 353.2 0.03 mg/L 11/13/2018 Nitrate Nitrogen Subtraction Method 0.03mg/L 11/17/2018 Report#:: 2018-18060 � Pace 6 of 13 4Environmental Chemists, Inc. xY, y 6602 Windmill Way, Wilmington, NC 28405 � 910.392.0223 Lab & 910.392.4424 Fax 710 Bowsertown Road, vlanteo, NC 27954 s 252.473.5702 Lab/Fat 255-A Wilmington Highway, Jacksonville, NC 28540 g 910.347.5843 Lab/Fax ANALYTICAL &.CONSULTING CHEMISTS info@emvironmentalchemists.com East Carolina University Date of Report: Nov 19, 2018 1001 East 4th Street Customer PO #: 18M-1900 Greenville NC 27858 Customer ID: 12110019 Attention: Patrick Sherrod Report ##: 2018-18060 Project ID: UNC Coastal Studies-MW Lab ID Sample ID: Collect Date/Time matrix Sampled by 18-46634 Site: M1N-3 11/1/2018 1:22 PM Water Tom Beasley Color Depth to water, ft. Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Organic Carbon (TOC) 1,1,1,2-Tetrachloroethane 1, 1, 1 -Trichloroethane 1;1,22"Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane Color Depth to Water, Ft. ............... EPA 350.1 Gallons Bailed before sampling Qualitative Ski 2540 C SM 2550 B SM 4500 Cl E SM 4500 H B SPA 5310 B SM 6200C SM 6200C SM 6200C SM 52000 SM 6200C SM 6200C SM 6200C SPA 6200C SM 6200C SM 6200C SM 6200C SM 6200C SM 62000 SM 62000 SM 6200C SM 6200C Results Date Analyzed Tan 11/01/2018 9.3 feet 11/01/2018 3.4 mg/L 11 /18/2018 0.50 gallons 11/01/2018 Yes 11/01/2018 592 mg/L 11 /05/2018 23.6 C 11/01/2018 117 mg/L 11/05/2018 6.58 units 11/01/2018 44.4 mg/L 11 /05/2018 <0.5 pg/L 11/09/2018 <0.5 pg/L 11/09/2018 <0.5'µg/L............... -11/09/2018 <0.5 pg/L 11/09/2018 <0.5 pg/L 11/09/2018 <0.5 pg/L 11/09/2018 <0.5 pg/L 11/09/2018 <0.5 pg/L 11/09/2018 <0.5 pg/L 11/09/2018 <0.5 pg/L 11/09/2018 <0.5 pg/L 11109/2018 <0.5 pg/L 11/09/2018 <0.5 pg/L 11/09/2018 <0.5 pg/L 11 /0912018 <0.5 pg/L 11/09/2018 <0.5 pg/L 11/09/2018 Report #-:: 2018-18060 Page 7 of 13 Environmental Chemists, Inc. Il i t 6602 Windmill Way, Wilmington, NC 28405 v 910.392.0223 Lab h 910.392.4424'Pax 710 Bowsertown Road, Manteo, NC 27954 9 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Pax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com East Carolina University Hate of Report: Nov 19, 2018 1001 East 4th Street Customer PO #: 18M-1900 Greenville NC 27858 Customer ID: 12110019 Attention: Patrick Sherrod Report #: 2018-18060 Project ID: UNC Coastal Studies-MW 1,3,5-Trimethylbenzene SM 6200C <0.5 pg/L 11/09/2018 1,3-Dichlorobenzene SM 6200C <0.5 pg/L 11/09/2018 1,3-Dichloropropane SM 6200C <0.5 pg/L 11/09/2018 1,4-Dichlorobenzene SM 6200C <0.5 pg/L 11/09/2018 2,2-Dichloropropane SM 6200C <0.5 pg/L 11/0912018 2-Chlorotoluene..... ........ SM 6200C <0.5 ug1L..........-................11 /09/2018 4-Chlorotoluene SM 6200C <0.5 pg/L 11/09/2018 Benzene SM 62000 <0.5 pg/L 11/09/2018 Bromobenzene SM 6200C <0.5 pg/L 11/09/2018 Bromochloromethane SM 62000 <0.5 pg/L 11109/2018 Bromodichloromethane SM 6200C <0.5 pg/L 11/09/2018 Bromoform SM 6200C <0.5 pg/L 11/09/2018 Bromomethane SM 6200C <0.5 pg/L 11/09/2018 Carbon tetrachloride SM 6200C <0.5 pg/L 11/09/2018 Chlorobenzene SM 6200C <0.5 pg/L 11/09/2018 Chloroethane SM 6200C <0.5 pg/L 11/09/2018 Chloroform SM 6200C <0.5 pg/L 11/09/2018 Chloromethane SM 62000 <0.5 pg/L 11/09/2018 cis-1,2-Dichloroethene SM 62000 <0.5 pg/L 11/09/2018 cis-1,3-Dichloropropene SM. 6200C <0.5 pg/L 11/09/2018 Dibromochloromethane SM 6200C <0.5 pg/L 11/09/2018 Dibromomethane SM 6200C <0.5 pg/L 11/09/2018 Dichlorodifluoromethane SM 6200C <0.5 pg/L 11/09/2018 Ethylbenzene SM 62000 <0.5 pg/L 11/09/2018 Hexachlorobutadiene SM 6200C <0.5 pg/L 11/09/2018 lsopropylbenzene SM 6200C <0.5 pg/L 11/09/2018 M+P Xylene SM 6200C <1.0 pg/L 11/09/2018 Methylene chloride SM 62000 <0.5 pg/L 11/09/2018 Naphthalene SM 6200C <0.5 pg/L 11/09/2018 n-Butylbenzene SM 6200C <0.5 pg/L 11/09/2018 Report tt:: 2018-18060 Page 8 of 13 . w;.. Environmental Chemists, Inc. 6602 Windmill Wati; Wilmington, NC 28405 d 910.392.0223 Lab G 910.392.44-74 Fax 710 Bowsertown Road, V(anteo, NC 27954 0 252.473.5702 Lab /Fax " 255-A Wilmington Highway, jacksonville, NC 28540 ® 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(rLerivironmentalcheniists.com East Carolina University Date of Report: Nov 19, 2018 1001 East 4th Street Customer Phi ##: 18M-1900 Greenville NC 27858 Customer ID, 12110019 Attention: Patrick Sherrod Report ##: 2018-18060 Project ID: URIC Coastal Studies-MW n-Propylbenzene SM 6200C <0.5 pg/L 11/09/2018 ortho-Xylene SM 62000 <0.5 pg/L 11/09/2018 p-isopropyltoluene SM 6200C <0.5 pg/L 11/09/2018 sec-Sutylbenzene SM 62000 <0.5 pg/L 11/09/2018 Styrene SM 6200C <0.5 pg/L 11/09/2018 SM 6200C tart- .uty enzene... .. .............. ..............................-..__<0.�,.p9/L....._...-...................11/09i2018.. Tetrachloroethene SM 6200C <0.5 pg/L 11/09/2018 Toluene SM 620oc <0.5 pg/L 11/09/2018 Trans-1,2-Dichloro6thene SM 62000 <0.5 pg/L 11/09/2018 Trans-1,3-dichloropropene SM 6200C <0.5 pg/L 11/09/2018 Trichloroethene SM 62000 <0.5 pg/L 11/09/2018 Trichlorofluoromethane SM 6200C <0.5 pg/L 11/09/2018 Vinyl chloride SM 6200C <0.5 pg/L 11/09/2018 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11/02/2018 Nitrate+Nitrite-Nitrogen EPA 353.2 0.08 mg/L 11113/2018 Nitrate Nitrogen Subtraction Method 0.08 mg/L 11/17/2018 Recort #:: 2018-18060 Paqe 9 of 13 ANALYTICAL & CONSULTING CHEMISTS Environmental Chernists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab o 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax 255-A'Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax infoGenvironmentalchemists.coni East Carolina University Date of Report: Nov 19, 2018 1001 East 4th Street Customer PO ##: 18M-1900 Greenville NC 27858 Customer ID: 12110019 Attention: Patrick Sherrod Report ##: 2018-18060 Project ID: UNC Coastal Studies-MW Lab ID Sample ID: Collect Date/Time Matrix Sampled by 18-45635 Site: MW-4 11/1/2018 1:33 PM Water Tom Beasley Test Method Results Date Analyzed Color Color Tan 11 /01 /2018 Depth to water, ft. Depth to Water, Ft. 9.9 feet 11101 /2018 ......_..........................................._._........................... Ammonia Nitrogen ... ................................._........................................_.....-_................_..... _...... ........................... EPA 350.1 6.0 mg/L ... . 11 /18/2018 Gallons bailed before sampling Gallons Bailed before sampling 0.50 gallons 11 /01/2018 Odor Qualitative Yes 11 /01 /2018 Total Dissolved Solids (TDS) SM 2540 c 476 mg/L 11 /0512018 Temperature SM 2550 B 23.4 C 11 /01 /2018 Chloride SM 4500 Cl E 11 mg/L 11/05/2018 pH SM 4500 H B 6.72 units 11101 /2018 Total Organic Carbon (TOC) SM 5310 B 32.0 mg/L 11/05/2018 1,1,1, 2-Tetrachloroethane SM 6200C <0.5 pg/L 11 /0912018 1, 1, 1 -Trichloroethane SM 6200C <0.5 pg/L 11/09/2018 1,1,2,2-Tetrac6loroethane sM 8200c <0.5 pg/L 11/09/2018 1,1,2-Trichloroethane SM 6200C <0.5 pg/L 11/09/2018 1, 1 -Dichloroethane SM 6200C <0.5 pg/L 11/09/2018 1, 1 -Dichloroethene SM 6200C <0.5 pg/L 11/09/2018 1,1-Dichloropropene SM 6200C <0.5 pg/L 11/09/2018 1,2,3-Trichiorobenzene StV16200C <0.5 pg/L 11/09/2018 1,2,3-Trichloropropane SM 6200C <0.5 pg/L 11/09/2018 1,2,4-Trichlorobenzene SM 6200C <0.5 pg/L 11/09/2018 1,2,4-Trimethylbenzene SM 6200C <0.5 pg/L 11/09/2018 1,2-Dibromo-3-Chloropropane SM 6200C <0.5 pg/L 11/09/2018 1,2-Dibromoethane SM 62000 <0.5 pg/L 11 /0912018 1,2-Dichlorobenzene SM 6200C <0.5 pg/L 11/09/2018 1,2-Dichloroethane SM 6200C <0.5 pg/L 11/09/2018 1,2-Dichloropropane SM 6200C <0.5 pg/L 11/09/2018 Report #:: 2018-18060 Page 10 of 13 Environmental Chemists, Inca 6 II 6602 Windmill AVay, Wilmington, NC 28405 0 910.392.0223 Lab 9 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ® 252.4733.5702 Lab/Fax 255 .A Wilmington Highway; Jacksonville, NC 28540 0 910.347,5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@emironnientalchenvsts.com East Carotins University Date of Report: Nov 19, 2018 1001 East 4th Street Customer FAO M 18M-1900 Greenville NC 27858 Customer ID: 12110019 Attention: Patrick Sherrod Report #: 2018-18060 Project ID: UNC Coastal Studies-MW 1,3, 5-Trimethylbenzene SM 62000 <0.5 µg/L 11/09/2018 1, 3-Dichlorobenzene SM 6200C <0.5 pg/L 11/09/2018 1,3-Dichloropropane SM 6200C <0.5 pg/L 11/09/2018 1,4-Dichlorobenzene SM 6200C <0.5 µg1L 11/09/2018 2,2-Dichloropropane SM 6200C <0.5 pg/L 11/09/2018 . _ ....._.-....LQrotoluene.................................................................. sM 62ooc .... ........................................ ......_...__......... 4:/L 5... ._..... ...... ......... ......... ........,.< . pg . ...11/09/2018 4-Chlorotoluene SM 62000 <0.5 pg/L 11/09/2018 Benzene SM 6200c <0.5 pg/L 11/09/2018 Bromobenzene SM 6200C <0.5 pg/L 11/09/2018 Bromochloromethane SM 6200C <0.5 pg/L 11/09/2018 Bromodichloromethane SM 6200C <0.5 pg/L 11/09/2018 Bromoform SM 6200C <0.5 µg/L 11/09/2018 Bromomethane SM 6200C <0.5 pg/L 11/09/2018 Carbon tetrachloride SM 6200C <0.5 pg/L 11/09/2018 Chlorobenzene SM 6200C <0.5 pg/L 11/09/2018 Chloroethane . SM 6200c < .... 0.5.µg/L 1.1/09/201$ Chloroform SM 6200c <0.5 pg/L 11/09/2018 Chloromethane SM 6200C <0.5 pg/L 11/09/2018 cis-1,2-Dichloroethene SM 6200C <0.5 pg/L 11/09/2018 cis-1,3-Dichloropropane StA 6200c <0.5 pg/L 11/09/2018 Dibromochloromethane SM 6200c <0.5 pg/L 11/09/2018 Dibromomethane SM 6200C <0.5 pg/L 11/09/2018 Dichlorodifluoromethane SM 6200c <0.5 pg/L 11/09/2018 Ethylbenzene SM 6200C <0.5 pg/L 11/09/2018 Hexachlorobutadiene SM 6200C <0.5 pg/L 11/09/2018 Isopropylbenzene SM 6200C <0.5 pg/L 11/09/2018 M+P Xylene SM 6200C <1.0 pg/L 11/09/2018 Methylene chloride SM 6200C <0.5 pg/L 11/09/2018 Naphthalene SIVI6200C <0.5 pg/L 11/09/2018 n-Butylbenzene SM 6200C <0.5 pg/L 11/09/2018 Report#:: 2018-18060 Pace 11 of 13 Environmental Chemists, Ince 4 All 4-1 _ 6602 Windmill Way, Wilmington, NC 28405 6 910.392.0221 Lab 3 910.392.4424 Fax r F`" a 71013ocvsertotivn Road Mnteo, NC 279, 252.473.5702 0_ Lab/Fax 255-A Wilmington High-tvay, Jacksonville, NC 28540 6 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environnientaIcl.einists.com East Carolina University Date of Report: Nov 19, 2018 1001 East 4th Street Customer P®#: 18M-1900 Greenville NC 27858 Customer ID: 12110019 Attention: Patrick Sherrod Report #: 2018-18060 Project ID: UNC Coastal Studies-MW n-Propylbenzene SM 6200C <0.5 pg/L 11/09/2018 ortho-Xylene sM 6200C <0.5 pg/L 11/09/2018 p-Isopropyltoluene sM6200C <0,5 pg/L 11/09/2018 sec-Butylbenzene SM6200C <0.5 pg/L 11/09/2018 Styrene sM6200C <0.5 pg/L 11/09/2018 tent-Butylbenzene....._..... -... ..........-._......... srwg szooc...... ........................... ............... <0.6. pg/L...........................41 /09/2018 Tetrach loroethene sM 6200C <0.5 pg/L 11/09/2018 Toluene sM 6200C <0.5 pg/L 11/09/2018 Trans-1,2-Dichloroethene SM6200c <0.5 pg/L 11/09/2018 Trans-1,3-dichloropropene SM6200C <0-5 pg/L 11/09/2018 Trichloroethene SM6200C <0.5 pg/L 11/09/2018 Trichlorofluoromethane SM6200C <0.5 pg/L 11/09/2018 Vinyl chloride SM 3200C <0.5 pg/L 11/09/2018 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA353.2 < 0.02 mg/L 11/02/2018 Nitrate+Nitrite-Nitrogen EPA353.2 0.08mg/L 11/13/2018 Nitrate Nitrogen subtraction Method 0.08 mg/L 11/17/2018 Lab ID Sample ID: M-3555 Collect Date/Time Matrix Sampled by 1845636 Site: MW-1 11/1/2018 1:10 PM Water Tom Beasley Test Method Results Date Analyzed Fecal Coliform SM92220MF <1 Colonies/100ml- 11/01/2016 Lab ID Sample ID: M-3556 Collect Date/Time Matrix Sampled by 18-45637 Site: MW-2 11/1/2018 12:58 PM Water Tom Beasley Test Method Results Date Analyzed Fecal Coliform SM9222DMF <1 Colonies/100ml- 11/01/2016 Report #:: 2018-18060 Paqe 12 of 13 Environmental Chemists,Inc® -,® m 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab 6 910.392.4424 Fax 4 710 Bowsertown Road Manteo NC 27954 e 252.473.5702 Lab/Fax 255-A Wilmington Highway; Jacksonville, NC 28540 g 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(✓environmentalcheniists.com East Carolina University ®ate of Report: Nov 19, 2018 1001 East 4th Street Customer P® #: 18M-1900 Greenville NC 27858 Customer ID: 12110019 Attention: Patrick Sherrod Report #: 2018-18060 Project ID: UNC Coastal Studies-MW Lab ID Sample ID: M-3557 Collect Date/Time Matrix Sampled by 1845638 Site: MW-3 11/1/2018 1:22 PM Water Tom Beasley Test Method Results ®ate Analyzed Fecal Coliform SM 9222D MF <1 Colonies/100ml- 11/01/2016 Lab ID Sample IC: M-3558 Collect Date/Time Matrix Sampled by 18-45639 Site: MW-4 11/1/2018 1:33 PIN Water Tom Beasley Test Method Results Date Analyzed Fecal Coliform SM9222DMF <1 Colonies/100ml- 11/01/2016 Comment: � i _-- Reviewed by: ko, I- RL Report #:: 2018-48060 Papa 13 of 13 Client• East Carolina University A®O�SS: 1001 East 4t>h Street r.;araanville. NC 27858 ad sample 14 we Ba'l ENVIRONMENTAL I T g I6602 Windmill Way Wilmington, NC 2841 OFFICE: 910 392 0 23 FAX 91U-3 2.443 NCDEPIR: DWQ CERTIFICATION 094 NCDHHS: DLS CERTIFICATION 437729 Info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY: PROJECT NAME: UNC Coastal Studies Institute REPORT NO: CONTACT NAME- Monitoring Wells Dare Count Site Patrick: 252.328.4046 or 252.916.4494 REPORT TO: Patrick Sherrod, Facilities SeMces PHONE Junlor : 252.305.6956 COPY TO: Junior Edwards, Atlantic Underground Ora email: sherrodp@ecu.edu AAMPLP TVPF! I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludge, Other: Collection i c oW PRESERVATION mI a ANALYSIS REQUESTED lentiffication m " V s � Date lime Teln X Chloride, NO2, TDS G G 1 C P X ._ NO3, NH3 G G ter. ,� .� a i :' r, X i'3 ':r ` ecal CWon G G led: C P _ ...�.. -7 (� � G G X TOO Vas C P #--Fv09C's G G Ian 6 C-`6Ping— C P X November only) G G C P G G C P G G _ C P G G of 4 well Transfer W°II site on Hwy 345 Wagplkese, NC. DatefTime •, i �.r`i!r 'l.' dff"7 fa .� �J li! Vd-' !: G'G". f! - �. . Temperature when Reserved: . C �� Accep �' �'Re� tsd: .� _ltesamp y > Received By: i] _ ;� -�_ L i�. -c at� Delivered By, Comments: i r*, 41WENVIRONMENTAL I T y INCOFFICE: 910392-0 23 FAX910392.445 Analytical &Consulting Chemists NCDENR: DWO CERTIFICATION 9 94 NCDHIAS: DLS CERTIFICATION # 37729 info@onvironmentalchemists.com environmentalchemists.com ('nVLF-CTION AND CHAIN OF CUSTODY Client: East Carolina University PROJECT NAME: UNC Coastal Studies institute REPORT NO h�q ADDRESS: 11001 East 4th Street CONTACT NAIIiIE: Monitoring Wells Bare Count Site Patrick, 252.328.4046 or 252.9%4494 Greenville, NC 27858 REPORT TO: Patrick Sherrod, Facilities Services. WHONE Junior : 252.305.6956 COPY TO: Junior Edwards, Atlantic Unde round JOB) email: sherrodp@ecLi.edu SAMPLETYPE: I = Influent, E = Effluent .W = Well, ST= Stream, SO = Sail, SL = Sludge, t attier: baillpaow u Ray. 3 5- Collection m - w L w PRESERVATION tt±erattfication d a' r p ;a o A `o O1 A m g� ANALYSIS REQUESTED z J $ c o f� e�an3pie Date Time Tears W�- c o Ana v °a C P t` 3 X Chloride, NO2, TDS G Well:G �I t� �� C P X NO3,NH3 G G Depth to water C P�rrr' �'`� X I�?,:"' Feaai Coliform G G Gallons Bailed:, C P 44 X TOO, Kt C P i Zit,% G G field odor/color: A W C P F VOC's November only) G G C P G G C P G G C I P G G Total of 4 wells to be collected In @+serer', July, November. Well site on Hwy 3ms Wane ese, Nc. Date/Time Transfer Relin ' hed By: Date/Time Re lved By: L+/ 2. Temperature when Received: v `7.. � -x-- Accgted: f f Kejecxerd4- �sranlwali1c Delivered By: L1.h> Recelved.9y: � ,�' tV i ?j� �'�ti._ L2--X— Date -. _I Tl )I Comments: 41M ENVIRONMENTAL CHEMISTS INC 6602 WinOFFICE:dmill Way Wilmington,-0223 FAX-3 2. 41 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@ environmeiitalchernists.com & Consulting Chemists @ fut%1 1 ce—rAf%ho A%V7% ^1-9Ea9'Pc ONw a92sn.m-�o�ao Client: East Carolina University `s..f .lvaPW n 4I A.F i PROJECT NAME: UNC Coastal Studies Inst.Me REPORT NO.- f ADDRESS: 100i East 4th Street CONTACT DAME: Monitoring Wells Dare County Site Patrick: 252.328.4046 or 262.918.4404. Greenville, NC 27858 REPORT TO: Patricia Sherrod, Facilities Services. PHONE Junior : 252.305.6956 COPY TO. Junior Edwards, Atlantic Under round 1313 em It: sherrodp@ecu.edu k-F-Fe f7MIII€tTr��■rr.• lCr Sample Identification Collection ;i w ty .. b o o o m L E " m a Li1RHCA11,, PRESER!/ATI1alr! Uv — VIVU111 Q 1 = �zr®am, av = 411, bL = blUdge, ®Mier: ANALYSIS REQUESTED Date 'Time 'Pearl ,,, o s o g Well: -D t : 2- -2- C P � X Chloride, NO2, TDS G G i Depth to water: Z� , �� C P X �. NO3, NH3 G G Gallons Called: CP X'`" '` ........_._� ..... _ _� ` Fecal Coliform G G H (field): �J `{E S field odor/color: _rr.'d C P x TOO G C G P _ j ( ��,.. G G -- C P x I VOC's November only) G G C P G G C Q G G C P LL G G Total of 4 wells to be collected In @Aarch, July November. Well site on Hwy 345 Wanche , NC. Transfer Relinquil ed By. DaterTime Received Dy: Date/Time 1. < nor. xerr� <.J .✓P"1 E " �.` 'd'.nrsewo.o+.h&.nvt, •,..Ao....., �i...... t.._ e. ...., 6 _ s r-- _ t , _—...r—.......,. �. o............,.... Delivered Bjr . -a tl ENVIRONMENTAL CHEMISTS, INC OFFICE: 910 392-0223 FAX 910 392-4L: a Analytical & Consulting Chemists NCDENR: DW:Q CERTIFICATION #94 NCDHHS: US CERTIFICATION # 37729 info@onvironmentalchemists.com f" hl I Ind-Tle%Nl a hin e+LM sasar ^e ne ar_ r^P9•a Client: East Carolina University PROJECT NAME: UNC Coastal Studies Institute REPORT NO.- �"• �clb£ & ADDRESS: 1001 East 4th Street CONTACT NAAJItir: Monitoring Wells Mare Count Site 9��' Patrick: 262.328.4046 or 262.916.4494 Greenville, MC 27858 REPORT TO: Patrick Sherrod, Facilities Services PHONE ,lunig : 252.305.6956 COPY TO: Junior Edwards, Atlantic Under round OB elVlail: sherrodp@ecu.edu N Alanni a �— a _ e—.n____- — Sample Identification Co lection rA w o" a o n`o ° o w g j z PRESERVATION ago = sou, 0IL- = O'uage, saner: AN�YSIS REQUESTED Date Time Terre o x x =" _ ox s F- Well: 4 i- 1 C P' 1� +X Chloride, NO2, TDS G G 1 De ih to water. �n C P 1 X — NO3, NH3 G G Gallons Bailed: (ti 1-D C P 4,1 J X. Fecal Coliform. G G /-7 H (field): t p- f Z, C P X �. TOC G G field odor/color: C P j -. G G C P I X VOC's (November only) G G C P G G C P G G C P G G Total of 4 welts to bo coltoctod In March, July, November. well site on Ilwy 3451Nanchose, NC. Transfer . Relinquished By. Date/rime Received By: Datefrirne . ....,yevaau.ata,v avaaa:ee e»aec.v�ta. l Ue�C:tiC1.J4�G1: ✓ 1 Kgjecxeor _ mesraml: Delivered By: WE Comments:-