NC0021156_Application_20140724

Z Oltboewwl�l
MOUNT M UTILITIES DEPARTMENT
HOLLY CITY Of MOUNT HOLLY
400 East Central Avenue
WATER TREATMENT
Post Office Box 406
WASTEWATER TREATMENT
Mount Holly, NC 28120
STORMWATER
704-827-4261
GiS TECHNOLOGY
704-827-6306 Fax
Website: www.mthollv.us
Thursdg,July 24, 2014
NCDE
Attn: NPDES Unit d jI
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: NPDES Permit # NCO021156 Renewal
Please See Attachments �� J
To whom it may concern,
Please accept the City of Mount Holly pert t renewal form for permit # NC0021156. Attached with this cover letter is the completed
Form 2A NPDES with Attachments I-VII. Currently we are still testing with the second species for toxicity, attachment V contains all
the toxicity test performed in the last four and one half years. Upon completion Ana two tests we will forward those reports to
you. You will find below an outline of each section that requires effluent monitoring data and dates in which the data was pulled from.
• Section A.6.b&c data was pulled from July 1, 2011 —June 30, 2014
• Section A.12 data was pulled from March 1,2012 — March 31,2014
• Section B.6 data was pulled from March 1, 2012 — March 31, 2014 and Three pollutant Scans.
• Part D data was pulled from March 1, 2012 — March 31, 2014 and Three pollutant Scans.
If any additional data is required please let me know and I will forward it as soon as possible.
Sincerely,
DVAnny Jackson
City Mana er
RECEIVED/DENR/DWR
AUG - 1 2014
Water Quality
Permitting Section
Lx�v jyv\ v-',M

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly WWTP NCO021156 Renewal Catawba
FORM _€
2A NPDES FARM 2A APPLICATION OVERVIEW
NPDES
APPLICATION OVERVIEW
Form 2A has been developed in a modular format and consists of a "Basic Application Information" packet
and a "Supplemental Application Information" packet. The Basic Application Information packet is divided
into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or
equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental
Application Information packet. The following items explain which parts of Form 2A you must complete.
BASIC APPLICATION INFORMATION:
A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works
that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12.
B. Additional Application Information for Applicants with a Design Flow >_ 0.1 mgd. All treatment works that have design flows
greater than or equal to 0.1 million gallons per day must complete questions B.1 through 13.6.
C. Certification. All applicants must complete Part C (Certification).
SUPPLEMENTAL APPLICATION INFORMATION:
D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets
one or more of the following criteria must complete Part D (Expanded Effluent Testing Data):
1. Has a design flow rate greater than or equal to 1 mgd,
2. Is required to have a pretreatment program (or has one in place), or
3. Is otherwise required by the permitting authority to provide the information.
E. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing
Data):
1. Has a design flow rate greater than or equal to 1 mgd,
2. Is required to have a pretreatment program (or has one in place), or
3. Is otherwise required by the permitting authority to submit results of toxicity testing.
F. Industrial User Discharges and RCRAICERCLA Wastes. A treatment works that accepts process wastewater from any
significant industrial users (SIUs) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges
and RCRA/CERCLA Wastes). SIUs are defined as:
1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and
40 CFR Chapter I, Subchapter N (see instructions); and
Any other industrial user that:
a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works (with certain
exclusions); or
b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic
capacity of the treatment plant; or
C. Is designated as an SIU by the control authority.
G. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer
Systems).
ALL APPLICANTS MUST COMPLETE PART C (CERTIFICATION)
Page 1 of 30

FACILITY NAME AND PERMIT NUMBER:
Mount Holly WWTP, NCO021156
BASIC APPLICATION INFORMATION
PERMIT ACTION REQUESTED: RIVER BASIN:
Permit Renewal Catawba
PART A. BASIC APPLICATION INFORMATION FOR ALL APPLICANTS:
All treatment works must complete questions A.1 throunh A.8 of this Basic Application Information Packet.
A.1. Facility Information.
Facility Name Mount Holly WWTP
Mailing Address P.O Box 406 Mount Holly NC 28120
Contact Person Jonathan Jordan
Title Wastewater Treatment Plant Su erintendant
Telephone Number 704 827-4261
Facility Address Broome St Mount Holly_ NC 28120•
(not P.O. Box)
A.2. Applicant Information. If the applicant is different from the above, provide the following:
Applicant Name City of Mount Holly _
Mailing Address P.O Box 406 Mount Holly. NC 28120
Contact Person Danny Jackson_
Title
Telephone Number
Is the applicant the owner or operator (or both) of the treatment works?
® owner ® operator
Indicate whether correspondence regarding this permit should be directed to the facility or the applicant.
❑ facility ® applicant
A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works
(include state -issued permits).
NPDES .1166 PSD
UIC Other Land Application WQO['^'
RCRA Other Storm Water NCG11000u
A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each
entity and, if known, provide information on the type of collection system (combined vs. separate) and its ownership (municipal, private, etc.).
Name Population Served Type of Collection System Ownership
City of Mount Holly13.676 (2010 Census) _ Separate [sanitary] Munici
Total population served 13.676 _
RECEIVED/DENR/DWR
Water Quality Page 2 of 30
Permitting Section

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly WWTP, NCO021156 Renewal Catawba
A.S. Indian Country.
a. Is the treatment works located in Indian Country?
❑ Yes No
b. Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from (and eventually flows
through) Indian Country?
❑ Yes No
A.S. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the
average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period
with the 12th month of "this year" occurring no more than three months prior to this application submittal.
a. Design flow rate
mgd
Two Years Ago Last Year This Year
b. Annual average daily flow rate 1.98
C. Maximum daily flow rate 6.15
A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent
contribution (by miles) of each.
® Separate sanitary sewer _
❑ Combined storm and sanitary sewer
A.8. Discharges and Other Disposal Methods.
a. Does the treatment works discharge effluent to waters of the U.S.? Yes No
If yes, list how many of each of the following types of discharge points the treatment works uses:
i. Discharges of treated effluent
ii. Discharges of untreated or partially treated effluent
iii. Combined sewer overflow points
iv. Constructed emergency overflows (prior to the headworks)
V. Other
b. Does the treatment works discharge effluent to basins, ponds, or other surface impoundments
that do not have outlets for discharge to waters of the U.S.? Yes
If yes, provide the following for each surface im oundment:
Location:
jf No
Annual average daily volume discharge to surface impoundment(s) _ mgd
Is discharge ❑ continuous or ❑ intermittent?
C. Does the treatment works land -apply treated wastewater? Yes No
If yes, provide the following for each land application site:
d
Location: Please See Attachment I
Number of acres:
Annual average daily volume applied to site:
Is land application ❑ continuous or intermittent?
Does the treatment works discharge or transport treated or untreated wastewater to another
treatment works?
mgd
Yes No
RECEIVED/DENR/DWR
AUG 1 2014
Water Quality Page 3 of 30
Permitting Section

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly WWTP, NCO021156 Renewal Catawba
If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works
(e.g., tank truck, pipe).
If transport is by a party other than the applicant, provide:
Transporter Name
Mailing Address
Contact Person
Title
Telephone Number 1
For each treatment works that receives this dischae, provide the following:
Name
Mailing Address
Contact Person
Title
Telephone Number f k
If known, provide the NPDES permit number of the treatment works that receives this discharge
Provide the average daily flow rate from the treatment works into the receiving facility.
e. Does the treatment works discharge or dispose of its wastewater in a manner not included
in A.8. through A.8.d above (e.g., underground percolation, well injection):
If yes, provide the following for each disposal method:
Description of method (including location and size of site(s) if applicable):
Annual daily volume disposed by this method:
Is disposal through this method continuous or ❑ intermittent?
mgd
❑ Yes ® No
RECEIVED/DENR/DWR
AUG ® 1 2014
Water Quality
Permitting Section
Page 4 of 30

FACILITY NAME AND PERMIT NUMBER:
Mount Holly WWTP. NCO021156
PERMIT ACTION REQUESTED: RIVER BASIN:
Renewal I Catawba
WASTEWATER DISCHARGES:
If you answered "Yes" to question A.8.a, complete
questions A.9 through A.12 once for each outfall (including bypass points) through
which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered "No" to question
A.8.a, go to Part B, "Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd."
A.9. Description of Outfall.
a. Outfall number 001
b. Location Mount Holly_
28120
(City or town, if applicable)
(Zip Code)
Gaston
North Carolina
(County)
(State)
35'15'55"
81 °0'35"
(Latitude)
(Longitude)
C. Distance from shore (if applicable)
12 ft.
d. Depth below surface (if applicable)
0.5 ft.
e. Average daily flow rate
2.09 mgd
f. Does this outfall have either an intermittent or a
periodic discharge? J Yes ® No (go to A.9.g.)
If yes, provide the following information:
Number f times per year discharge occurs:
Average duration of each discharge:
Average flow per discharge:
mgd
Months in which discharge occurs:
g. Is outfall equipped with a diffuser?
❑ Yes ® No
A.10. Description of Receiving Waters.
a. Name of receiving water Catawba River
b. Name of watershed (if known) Catawba River Basin
United States Soil Conservation Service 14-digit watershed code (if known):
C. Name of State Management/River Basin (if known): _ uwba River Basinwide Mq1 Plan
United States Geological Survey 8-digit hydrologic cataloging unit code (if known): 03050101
d. Critical low flow of receiving stream (if applicable)
acute cfs chronic cfs
e. Total hardness of receiving stream at critical low flow (if applicable): mg/I of CaCO3
RECEIVED/DENR/DWR
AUG m 1 2014
Water Quality age 5 of 30
Permitting Section

FACILITY NAME AND PERMIT NUMBER:
Mount Holly WWTP, NCO021156
A.11. Description of Treatment
a. What level of treatment are provided? Check all that apply.
❑ Primary Secondary
❑ Advanced ❑ Other. Describe:
b. Indicate the following removal rates (as applicable):
Design BOD5 removal or Design CBOD5 removal
Design SS removal
PERMIT ACTION REQUESTED: RIVER BASIN:
Renewal I Catawba
Design P removal %
Design N removal %
Other %
C. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season, please describe:
Cholrinatior
If disinfection is by chlorination is dechlorination used for this outfall?
Does the treatment plant have post aeration?
Yes ❑ No
Yes ❑ No
A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following
parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is
discharc;ed. Do not include information on combined sewer overflows in this section. All information reported must be based on data
collected through analysis conducted using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40
CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a
minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart.
Outfall number:
PARAMETER MAXIMUM DAILY VALUE AVERAGE DAILY VALUE
Value Units Value Units I Number of Samples
pH (Minimum)
6.2
s.u.
pH (Maximum)
7.2
SM.
Flow Rate
7.904
MGD
2.157
MGD
Temperature (Winter)
23 °C
14.2 °C
Temperature (Summer)
28 °C
23.1 °C
" For pH please report a minimum and a maximum daily value
MAXIMUM DAILY
AVERAGE DAILY DISCHARGE
DISCHARGE
POLLUTANT
Conc.
Conc. Units 7 Number of
1
Samples
—Units
CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS
BIOCHEMICAL OXYGEN 1 BODS
33.0
m /L
4.74
m (L
499
DEMAND (Report one) CBOD5
760
332
168
ANALYTICAL ML/MDL
METHOD
SM 521013-20 I 2.0
FECAL COL.IFORM 6000 #100mL 287.76 #100mL 500 SM 9222 D
TOTAL SUSPENDED SOLIDS (TSS) 33.0 mg/L 15.55 . mg/L 499 SM 2440 D
END OF PART A.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
Page 6 of 30

FACILITY NAME AND PERMIT NUMBER: I PERMIT ACTION REQUESTED: I RIVER BASIN:
Mount Holly WWTP, NCO021156 I Renewal I Catawba
BASIC APPLICATION INFORMATION
PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR
EQUAL TO 0.1 MGD (100,000 gallons per day).
All applicants with a design flow rate >_ 0.1 mgd must answer questions B.1 through B.6. All others go to Part C (Certification).
B.I. Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration.
.10 0C
gpd
Briefly explain any steps underway or planned to minimize inflow and infiltration.
We are cu v an Inflow and Infiltration study. at this time a report has not been generated.
B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This
map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire
area.) Please See Attachment II
a. The area surrounding the treatment plant, including all unit processes.
b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which
treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping, if applicable.
c. Each well where wastewater from the treatment plant is injected underground.
d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within % mile of the property boundaries of the treatment
works, and 2) listed in public record or otherwise known to the applicant.
e. Any areas where the sewage sludge produced by the treatment works is stored, treated, or disposed.
f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail,
or special pipe, show on the map where the hazardous waste enters the treatment works and where it is treated, stored, and/or disposed.
B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all
backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g.,
chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow
rates between treatment units. Include a brief narrative description of the diagram. Please See Attachment III
B.4. Operation/Maintenance Performed by Contractor(s).
Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a
contractor? Yes ® No
If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional
pages if necessary).
Name:
Mailing Address:
Telephone Number:
Responsibilities of Contractor:
B.5. Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or
uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design capacity of the treatment works. If the
treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5
for each. (If none, go to question B.6.)
List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule.
Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies.
❑ Yes I No
Page 7 of 30

FACILITY NAME AND PERMIT NUMBER:
PERMIT ACTION REQUESTED:
RIVER BASIN:
Mount Holly WWTP, NCO021156
Renewal
Catawba
C. If the answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable).
d. Provide dates imposed by any compliance schedule or any actual dates of completion for the implementation steps listed below, as
applicable. For improvements planned independently of local, State, or Federal agencies, indicate planned or actual completion dates, as
applicable. Indicate dates as accurately as possible.
Schedule Actual Completion
Implementation Stage MM/DD/YYYY MM/DDIYYYY
Begin Construction I I I I
- End Construction 1 / I I
- Begin Discharge I l I l
- Attain Operational Level
e. Have appropriate permits/clearances concerning other Federal/State requirements been obtained? ❑ Yes ❑ No
Describe briefly:
B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD ONLY).
Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated
effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information
on combine sewer overflows in this section. All information reported must be based on data collected through analysis conducted
using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate
QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum effluent testing data must be
based on at least three pollutant scans and must be no more than four and on -half years old.
Outfall Number:
MAXIMUM DAILY AVERAGE DAILY DISCHARGE
POLLUTANT
DISCHARGE ANALYTICAL
MLlMDL
Conc. Units Conc. Units Number of METHOD
Samples
COMPOUNDS
CONVENTIONAL AND NON CONVENTIONAL
AMMONIA (as N)
7.2 mg/L
.397
mg/L
315
350.1
0.10
CHLORINE (TOTAL
RESIDUAL, TRC)
49 ug/L
26.71
ug/L
499
SM 4600 CI G
20.0
DISSOLVED OXYGEN
10.6
mg/L
6.5
mg/L
499
SM 4500 OG
mg/L
TOTAL KJELDAHL
NITROGEN (TKN)
24
mg/L
2.88
mg/L
109
351.2
0.50
NITRATE PLUS NITRITE
NITROGEN
32
mg/L
16.72
mg/L
109
353.2
0.20
OIL and GREASE
4.9
mg/L
4.7
mg1L
3
1664A
4.50
PHOSPHORUS (Total) 7.8 mg/L 2.829 mg/L 109 365.1 0.10
TOTAL DISSOLVED SOLIDS 0 mg/L 483.3 mg/L 3 SM 2640 C 10.0
(TDS)
OTHER
END OF PART B.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
Page 8 of 30

FACILITY NAME AND PERMIT NUMBER: I PERMIT ACTION REQUESTED: I RIVER BASIN:
Mount Holly WWTP, NCO021156 I Renewal I Catawba
BASIC APPLICATION INFORMATION
PART C. CERTIFICATION
All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this
certification. All applicants must complete all applicable sections of Form 2A, as explained in the Application Overview. Indicate below which
parts of Form 2A you have completed and are submitting. By signing this certification statement, applicants confirm that they have reviewed
Form 2A and have completed all sections that apply to the facility for which this application is submitted.
Indicate which parts of Form 2A you have completed and are submitting:
' Basic Application Information packet Supplemental Application Information packet:
® Part D (Expanded Effluent Testing Data)
® Part E (Toxicity Testing: Biomonitoring Data)
® Part F (Industrial User Discharges and RCRA/CERCLA Wastes)
❑ Part G (Combined Sewer Systems)
ALL APPLICANTS MUST COMPLETE THE FOLLOWING CERTIFICATION.
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who
manage the system or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment
for knowing violations.
Name and official title
Signature
Telephone number
Date signed
,RwnvJackson I CitvjMana
704 827- 931
Upon request of the permitting authority, you must submit any other information necessary to assure wastewater treatment practices at the treatment
works or identify appropriate permitting requirements.
SEND COMPLETED FORMS TO:
NCDENR/ DWQ
Attn: NPDES Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Page 9 of 30

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly WWTP, NCO021156 Renewal Catawba
SUPPLEMENTAL APPLICATION INFORMATION
PART D. EXPANDED EFFLUENT TESTING DATA
Refer to the directions on the cover page to determine whether this section applies to the treatment works.
Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required
to have) a pretreatment program, or is otherwise required by the permitting authority to provide the data, then provide effluent testing data for the following
pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which
effluent is dischan:ied. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected
through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC requirements of 40 CFR Part 136 and
other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below
any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data must be based on at least three pollutant
scans and must be no more than four and one-half years old.
LOutfall number: 00,
(Complete once for each outfall discharging effluent to waters of the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
Cone. Units Mass Units
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
ML/MDL
Cone.
Units
Mass
Units
Number
of
Samples
METALS (TOTAL RECOVERABLE), CYANIDE, PHENOLS, AND HARDNESS.
ANTIMONY
0.042
mg/L
0.034
mg/L
12
200.8
0.001
ARSENIC
0.013
mg/L
0.0011
mg/L
12
200.8
0.001
BERYLLIUM
<0.0004
mg/L
<0.0004
mg/L
3
200.8
0.0004
CADMIUM
0.0010
mg/L
0.0002
mg/L
12
200.8
0.0001
CHROMIUM
0.0074
mg/L
0.0056
mg/L
12
200.8
0.005
COPPER
19.0
mg/L
1.59
mg/L
12
200.8
0.001
LEAD
0.002
mg/L
0.0011
mg/L
12
200.8
0.001
MERCURY
15.4
ng/L
6.84
ng/L
27
1631 E
0.600
NICKEL
<0.005
mg/L
<0.005
mg/L
12
200.8
0.005
SELENIUM
0.005
mg/L
0.0028
mg/L
12
200.8
0.001
SILVER
<0.001
mg/L
<0.001
mg/L
12
200.8
0.001
THALLIUM
<0.0005
mg/L
<0.0005
mg/L
3
200.8
0.0005
ZINC
66.0
mg/L
5.53
mg/L
12
200.8
0.01
CYANIDE
<0.01
mg/L
<0.01
mg/L
12
10-204-00-1-X
0.01
TOTAL PHENOLIC
COMPOUNDS
HARDNESS (as CaCO3)
0.055
50
m /L
g
mg/L
0.0226
44.3
9 m /L
mg/L
9
3
420.4
SM 2340 C
0.02
10
Use this space (or a separate sheet) to provide information on other metals requested by the permit writer
Page 10 of 30

FACILITY NAME AND PERMIT NUMBER:
PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly WWTP, NCO021156
Renewal Catawba
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.)
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
POLLUTANT
ANALYTICAL
ML/MDL
Number
Conc. Units
Mass Units
Conc.
Units
Mass
Units
of
METHOD
Samples
VOLATILE ORGANIC COMPOUNDS
ACROLEIN
<50.0
ug/L
<50.0
ug/L
3
624
50.0
ACRYLONITRILE
<50.0
ug/L
<50.0
ug/L
3
624
50.0
BENZENE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
BROMOFORM
9.8
ug/L
6.6
ug/L
3
624
5.0
CARBON
<5.0
ug/L
<5.0
ug/L
3
624
5.0
TETRACHLORIDE
CHLOROBENZENE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
CHLORODIBROMO-
8.7
ug/L
6.23
ug/L
3
624
5.0
METHANE
CHLOROETHANE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
2-CHLOROETHYLVINYL
<10 0
ug/L
<10.0
ug/L
3
624
10.0
ETHER
CHLOROFORM
<5.0
ug/L
<5.0
ug/L
3
624
5.0
DICHLOROBROMO-
<5.0
ug/L
<5.0
ug/L
3
624
5.0
METHANE
1,1-DICHLOROETHANE
<5.0
ug/L
<5.0
ug/L
3 1
624
5.0
1,2-DICHLOROETHANE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
TRANS-I,2-DICHLORO-
<5.0
ug/L
<5.0
ug/L
3
624
5.0
ETHYLENE
-
<5.0
ug/L
<5.0
ug/L
3
624
5.0
E
ETHYLENE
ETHYLENE
1,2-DICHLOROPROPANE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
1,3-DICHLORO-
<5.0
ug/L
<5.0
ug/L
3
624
5.0
PROPYLENE
ETHYLBENZENE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
METHYL BROMIDE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
METHYL CHLORIDE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
METHYLENE CHLORIDE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
1,1 TETRA-
<5.0
ug/L
<5.0
ug/L
3
624
5.0
CHLOROETHANE
LO
TETRACHLORO-
<5.0
ug/L
<5.0
ug/L
3
624
5.0
ETHYLENE
TOLUENE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
Page 11 of 30

FACILITY NAME AND PERMIT NUMBER:
Mount Holly WWTP NCO021156
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Catawba
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MLfMDL
Conc.
Units
Mass
Units
Conc.
Units
Mass
Units
Number
of
Samples
TRIC
TRIOHLOROETHANE
<5.0
ug/L
<5.0
ug/L
3
__4
5.0
1,1,2
TRICHLOROETHANE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
TRICHLOROETHYLENE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
VINYL CHLORIDE
<5.0
ug/L
<5.0
ug/L
3
624
5.0
Use this space (or a separate sheet) to provide information on other volatile organic compounds requested by the permit writer
ACID -EXTRACTABLE COMPOUNDS
P-CHLORO-M-CRESOL
<2.0
Fug/L
<2.0
ug/L
3
625
2.0
2-CHLOROPHENOL
<2.0
ug/L
<2.0
ug/L
3
625
2.0
2,4-DICHLOROPHENOL
<2.0
ug/L
<2.0
ug/L
3
625 1
2.0
2,4-DIMETHYLPHENOL
<2.0
ug/L
<2.0
ug/L
3
625
2.0
4,6-DINITRO-0-CRESOL
<5.3
ug/L
<5.3
ug/L
3
625
2.0
2,4-DINITROPHENOL
<5.3
ug/L
<5.3
ug/L
3
625
2.0
2-NITROPHENOL
<4.1
ug/L
<4.1
ug/L
3
625
4.1
4-NITROPHENOL
<10.0
ug/L
<10.0
ug/L
3
625
10.0
PENTACHLOROPHENOL
<10.0
ug/L
<10.0
ug/L
3
625
10.0
PHENOL
<2.0
ug/L
<2.0
ug/L
3
625
2.0
TRIOHLOROPHENOL
RIC
<2.0
ug/L
<2.0
ug/L
3
625
2.0
Use this space (or a separate sheet) to provide information on other acid -extractable compounds requested by the permit writer
BASE -NEUTRAL COMPOUNDS
ACENAPHTHENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
ACENAPHTHYLENE
<2.0
ug/L
<2.0 ug/L
3
625
2.0
ANTHRACENE
<2.0
ug/L
<2.0
ug/L
1
3
625
2.0
BENZIDINE
<10.0
ug/L
<2.0
ug/L
3
625
10.0
BENZO(A)ANTHRACENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
BENZO(A)PYRENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
Page 12 of 30

FACILITY NAME AND PERMIT NUMBER:
PERMIT ACTION REQUESTED:
RIVER BASIN:
Mount Holly WWTP, NCO021156
Renewal
Catawba
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.)
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
POLLUTANT
ANALYTICAL
MLlMDL
Number
Conc.
Units
Mass
Units
Conc.
Units
Mass
Units
of
METHOD
Samples
3,4 BENZO-
<2.0
ug/L
<2.0
ug/L
3
625
2.0
FLUORANTHENE
BENZO(GHI)PERYLENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
BENZO(K)
FLUORANTHENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
BIS (2-CHLOROETHOXY)
<2.0
ug/L
<2.0
ug/L
3
625
2.0
METHANE
BIS (2-CHLOROETHYL)-
<2.0
ug/L
<2.0
ug/L
3
625
2.0
ETHER
BIS (2-CHLOROISO-
<2.0
ug/L
<2.0
ug/L
3
625
2.0
PROPYL) ETHER
BIS (2-ETHYLHEXYL)
<10.0
ug/L
<10.0
ug/L
3
625
10.0
PHTHALATE
4-BROMOPHENYL
<2.0
ug/L
<2.0
ug/L
3
625
2.0
PHENYLETHER
BUTYL BENZYL
<10.0
ug/L
<10.0
ug/L
3
625
10.0
PHTHALATE
2-CHLORO-
<2.0
ug/L
<2.0
ug/L
3
625
2.0
NAPHTHALENE
4-CHLORPHENYL
<2.0
ug/L
<2.0
ug/L
3
625
2.0
PHENYLETHER
CHRYSENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
DI-N-BUTYL PHTHALATE
<10.0
ug/L
<10.0
ug/L
3
625
10.0
DI-N-OCTYL PHTHALATE
<10.0
ug/L
<10.0
ug/L
3
625
10.0
DIBENZO(A,H)
<2.0
ug/L
<2.0
ug/L
3
625
2.0
ANTHRACENE
1,2-DICHLOROBENZENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
1,3-DICHLOROBENZENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
1,4-DICHLOROBENZENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
3,3-DICHLORO-
<10.0
ug/L
<10.0
ug/L
3
625
10.0
BENZIDINE
DIETHYL PHTHALATE
<10.0
ug/L
<10.0
ug/L
3
625
10.0
DIMETHYL PHTHALATE
<10.0
ug/L
<10.0
ug/L
3
625
10.0
2,4-DINITROTOLUENE
<4.1
ug/L
<4.1
ug/L
3
625
4.1
2,6-DINITROTOLUENE
<4.1
ug/L
<4.1
ug/L
3
625
4.1
1,2-DIPHENYL-
<2.0
ug/L
<2.0
ug/L
3
625
2.0
HYDRAZINE
Page 13 of 30

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED:
RIVER BASIN:
Mount Holly WWTP, NCO021156 Renewal
Catawba
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.)
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
POLLUTANT
ANALYTICAL
ML/MDL
Number
Conc.
Units
Mass Units
Conc.
Units
Mass
Units
of
METHOD
Samples
FLUORANTHENE
<2.0
ug/L
<2.0
ug/L
3
,
2.0
FLUORENE
<2.0
ug/L
<2.0
i
ug/L
3
625
2.0
HEXACHLOROBENZENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
HEXACHLORO-
<2.0
ug/L
<2.0
ug/L
3
625
2.0
BUTADIENE
HEXACHLOROCYCLO-
<10.0
ug/L
<10.0
ug/L
3
625
10.0
PENTADIENE
HEXACHLOROETHANE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
INDENO(1,2,3-CD)
<2.0
ug/L
<2.0
ug/L
3
625
2.0
PYRENE
ISOPHORONE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
NAPHTHALENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
NITROBENZENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
N-NITROSODI-N-
<2.0
ug/L
<2.0
ug/L
3
625
2.0
PROPYLAMINE
N-NITROSODI-
<2,0
ug/L
<2.0
ug/L
3
625
2.0
METHYLAMINE
N-NITROSODI-
<2.0
ug/L
<2.0
ug/L
3
625
2.0
PHENYLAMINE
PHENANTHRENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
PYRENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
1,2,4
TRICHLOROBENZENE
<2.0
ug/L
<2.0
ug/L
3
625
2.0
Use this space (or a separate sheet) to provide information on other base -neutral compounds requested by the permit writer
Use this space (or a separate sheet) to provide information on other pollutants (e.g., pesticides) requested by the permit writer
END OF PART D.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
Page 14 of 30

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED:
RIVER BASIN:
Mount Holly WWTP, NCO021156 Renewal
Catawba
SUPPLEMENTAL APPLICATION INFORMATION
PART E. TOXICITY TESTING DATA
POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the
facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTWs with a pretreatment program (or those that are
required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit data for these parameters.
• At a minimum, these results must include quarterly testing for a 12-month period within the past 1 year using multiple species (minimum of two
species), or the results from four tests performed at least annually in the four and one-half years prior to the application, provided the results
show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range of receiving water dilution. Do not include
information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted
using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC
requirements for standard methods for analytes not addressed by 40 CFR Part 136.
• In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test
conducted during the past four and one-half years revealed toxicity, provide any information on the cause of the toxicity or any results of a
toxicity reduction evaluation, if one was conducted.
• If you have already submitted any of the information requested in Part E, you need not submit it again. Rather, provide the information
requested in question EA for previously submitted information. If EPA methods were not used, report the reasons for using alternate methods.
If test summaries are available that contain all of the information requested below, they may be submitted in place of Part E.
If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to
com lete.
E.1. Required Tests.
Indicate the number of whole effluent toxicity tests conducted in the past four and one-half years. Please See Attachment V
chronic acute
E.2. Individual Test Data. Complete the following chart for each whole effluent toxicity test conducted in the last four and one-half nears. Allow one
column per test (where each species constitutes a test). Copy this page if more than three tests are being reported.
Test number: Test number: Test number -
a. Test information.
Test Species & test method number
Age at initiation of test
Outfall number
Dates sample collected
Date test started
Duration
b. Give toxicity test methods followed.
Manual title
Edition number and year of publication
Page number(s)
c. Give the sample collection method(s) used. For multiple grab samples, indicate the number of grab samples used.
24-Hour composite
Grab
d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each.
Before disinfection
After disinfection
After dechlorination
Page 15 of 30

FACILITY NAME AND PERMIT NUMBER:
Mount Holly WWTP, NCO021156
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Catawba
Test number: Test number: Test number:
e. Describe the point in the treatment process at which the sample was collected.
Sample was collected:
f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or both
Chronic toxicity
Acute toxicity
g. Provide the type of test performed.
Static
Static -renewal
Flow -through
h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source.
Laboratory water
Receiving water
i. Type of dilution water. If salt water, specify "natural' or type of artificial sea salts or brine used.
Fresh water
Salt water
j. Give the percentage effluent used for all concentrations in the test series.
k. Parameters measured during the test. (State whether parameter meets test method specifications)
pH
Salinity
Temperature
Ammonia
Dissolved oxygen
I. Test Results.
Acute:
Percent survival in 100%
effluent
°
LC50
95% C.I.
%
%
%
Control percent survival
%
%
%
Other (describe)
Page 16 of 30

FACILITY NAME AND PERMIT NUMBER:
PERMIT ACTION REQUESTED:
RIVER BASIN:
Mount Holly WWTP, NCO021156
Renewal
Catawba
Chronic:
NOEC
%
%
%
IC25
%
%
%
Control percent survival
%
%
%
Other (describe)
m. Quality Control/Quality Assurance.
Is reference toxicant data available?
Was reference toxicant test within
acceptable bounds?
What date was reference toxicant test r
run (MM/DD/YYYY)?
Other (describe)
E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation?
Yes No If yes, describe:
EA. Summary of Submitted Btomonitoring Test Information. If you have submitted biomonitoring test information, or information regarding the
cause of toxicity, within the past four and one-half years, provide the dates the information was submitted to the permitting authority and a summary
of the results.
Date submitted: / / _ (MM/DD/YYYY)
Summary of results: (see instructions)
END OF PART E.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE.
Page 18 of 30

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly WWTP, NCO021156 Renewal Catawba
SUPPLEMENTAL APPLICATION INFORMATION
PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA, or other remedial wastes must
complete part F.
GENERAL INFORMATION:
F.I. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program?
® Yes ❑ No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
a. Number of non -categorical SIUs.
b. Number of CIUs.
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Name: American and Efird. INC
Mailing Address: P.O. Box 507
Mount Hol NC 28120
FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Process Water. Wash down waterDomestic Wastewater Boiler/Cooling tower Blowdown_ Cooling/Hvac water
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
Principal product(s): SewinQ. Embroidery Threads and Industrial yams
Raw material(s): Cotton Polyester. Nylon greige yarn. Dyes and auxiliary chemicals
F.6. Flow Rate.
a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per
day (gpd) and whether the discharge is continuous or intermittent.
537.006.8 gpd (— continuous or intermittent)
b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system
in gallons per day (gpd) and whether the discharge is continuous or intermittent.
43,541.1 ^_ gpd (X continuous or intermittent)
F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits ® Yes ❑ No
b. Categorical pretreatment standards ® Yes ❑ No
If subject to categorical pretreatment standards, which category and subcategory?
410 Textile
Page 19 of 30

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly WWTP NCO021156 Renewal Catawba
F.8.
Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g.,
upsets, interference) at the treatment works in the past three years?
Yes No If yes, describe each episode.
CERCLA (SUPERFUND) WASTEWATER, RCRA REM EDIATION/CO R RECTIVE ACTION
WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER:
F.12. Remedlation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities?
® Yes (complete F.13 through F.15.) No
F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in the
next five years).
The Jadco-Huclhes Site located at 760 Cason St. Belmont. NC was a former solvent reclamation and storage facility that was closed in 1975.
This site is does not have a IUP but the City has an agreement that allows them to dischara - laity max of 0.075 MGD to the POTW.
F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known.
(Attach additional sheets if necessary.)
Please see attachment Vi
F.15. Waste Treatment.
a. Is this waste treated (or will be treated) prior to entering the treatment works?
Yes ❑ No
If yes, describe the treatment (provide information about the removal efficiency):
The untreated ground water is aerated in a 18.700 gallon equalization and passed through a 1900 LB activated carbon gas phase adsorber.
b. Is the discharge (or will the discharge be) continuous or intermittent?
Continuous Intermittent If intermittent, describe discharge schedule.
Page 20 of 30

FACILITY NAME AND PERMIT NUMBER:
PERMIT ACTION REQUESTED:
RIVER BASIN:
Mount Holly WWTP, NCO021156
Renewal
Catawba
CERCLA (SUPERFUND) WASTEWATER, RCRA REM EDIATION/CORRECTIVE ACTION
WASTEWATER, AND OTHER REMEDIAL ACTIVITY WASTEWATER:
F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive waste from remedial activities?
® Yes (complete F.13 through F.15.) ❑ No
F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates (or is excepted to origniate in the
next five years).
Triangle Texaco is located at 201 N. Main St. Mount Holly, NC and the site of a Environmental Remediation of a former leakinr} UST site. The
consulting companv is awaiting approval from the state to proceed at this time. The estimated time to start operation is Sentember 2014.
F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include data on volume and concentration, if known.
(Attach additional sheets if necessary.)
Please see attachment VI I
F.15. Waste Treatment.
a. Is this waste treated (or will be treated) prior to entering the treatment works?
® Yes ❑ No
If yes, describe the treatment (provide information about the removal efficiency):
The around water is pumped from multiple wells and sent through a air stripper.
b. Is the discharge (or will the discharge be) continuous or intermittent?
® Continuous Intermittent If intermittent, describe discharge schedule.
Page 21 of 30

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly WVVfP, NCO021156 Renewal Catawba
GENERAL INFORMATION:
F.1. Pretreatment program. Does the treatment works have, or is subject ot, an approved pretreatment program?
1�71 Yes No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide the number of each of the following types of
industrial users that discharge to the treatment works.
C. Number of non -categorical SIUs.
d. Number of CIUs. 2
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Name: Buckeye Mt. Holly, LLC
Mailing Address: 100 Buckeye Dr.
Mount Holly. NC 28120
FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Process water, wash down water, domestic and recycled wastewater cooling water, Boiler/cooling tower blowdown and HVAC water.
F.S. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
Principal product(s): Airlaid non wovens for feminine hygiene products, speciality wipes .rapkins dnd incontinerrue products
Raw material(s): Wood pulp_ Biocomponent synthetic fiber, synthetic binders
F.6. Flow Rate.
C. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per
day (gpd) and whether the discharge is continuous or intermittent.
29,743.0 gpd (X continuous or _ intermittent)
d. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system
in gallons per day (gpd) and whether the discharge is continuous or intermittent.
57,7? 4 gpd (X continuous or intermittent)
F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits ® Yes No
b. Categorical pretreatment standards ® Yes No
If subject to categorical pretreatment standards, which category and subcategory?
ovens 410 Tex,
Page 22 of 30

FACILITY NAME AND PERMIT NUMBER: I PERMIT ACTION REQUESTED: I RIVER BASIN:
Mount Holly WWTP NCO021156
Renewal
Catawba
F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g.,
upsets, interference) at the treatment works in the past three years?
Yes No If yes, describe each episode.
Page 23 of 30

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly WWTP NCO021156 Renewal Catawba
SUPPLEMENTAL APPLICATION INFORMATION
PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Name: Clariant Corporation
Mailing Address: 625 E. Catawba AVE. _
Mount Holly NC 28120
FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Process water. Domestic wastewater. Boiler/ .ina tower blowdown and stormwater.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
Principal product(s): Specialty Chemicals i200+j including surface-active agents and DEET
Raw material(s): Alcohol. Oils Soaps, Acids
F.B. Flow Rate.
e. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per
day (gpd) and whether the discharge is continuous or intermittent.
60332.5 gpd ( continuous or intermittent)
f. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system
in gallons per day (gpd) and whether the discharge is continuous or intermittent.
gpd (X continuous or intermittent)
F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits ® Yes No
b. Categorical pretreatment standards ® Yes No
If subject to categorical pretreatment standards, which category and subcategory?
CFR 414 & 455
Page 24 of 30

FACILITY NAME AND PERMIT NUMBER: I PERMIT ACTION REQUESTED: I RIVER BASIN:
Mount Holly VW TP NCO021156 I Renewal I Catawba
F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g.,
upsets, interference) at the treatment works in the past three years?
❑ Yes No If yes, describe each episode.
Page 25 of 30

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly WWTP, NCO021156 Renewal I Catawba
SUPPLEMENTAL APPLICATION INFORMATION
PART F.INDUSTRIAL USER DISCHARGES AND RCRAICERCLA WASTES
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Supply the following information for each SIU. If more than one SIU discharges to the treatment works, copy questions F.3 through F.8 and
provide the information requested for each SIU.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
Name: Daimler Trucks North America [Mount Holly)
Mailing Address: 1800 North Main St.
Mount Holly NC 28120
FA. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
Process Water. Wash down water. Domestic Wastewater. Boiler/Cooling tower Blowdown Cooling/Hvac water. HVAC Water
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
Principal product(s): M2 Freightliner Trucks
Raw material(s): Aluminum, steel, acids, bases, organic solvents. and organic pain
F.6. Flow Rate.
g. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per
day (gpd) and whether the discharge is continuous or intermittent.
gpd ( continuous or __ intermittent)
h. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater flow discharged into the collection system
in gallons per day (gpd) and whether the discharge is continuous or intermittent.
gpd ( continuous or intermittent)
F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits Yes No
b. Categorical pretreatment standards Yes No
If subject to categorical pretreatment standards, which category and subcategory?
40 CFR 413 _
Page 26 of 30

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly WWTP, NCO021156 Renewal Catawba
F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems (e.g.,
upsets, interference) at the treatment works in the past three years?
Yes No If yes, describe each episode.
END OF PART F.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE
Page 27 of 30

FACILITY NAME AND PERMIT NUMBER:
Mount Holly WWTP, NCO021156
SUPPLEMENTAL APPLICATION INFORMATION
PERMIT ACTION REQUESTED: RIVER BASIN:
Renewal Catawba
PART G. COMBINED SEWER SYSTEMS
If the treatment works has a combined sewer system, complete Part G.
G.1. System Map. Provide a map indicating the following: (may be included with Basic Application Information)
a. All CSO discharge points.
b. Sensitive use areas potentially affected by CSOs (e.g., beaches, drinking water supplies, shellfish beds, sensitive aquatic ecosystems, and
outstanding natural resource waters).
C. Waters that support threatened and endangered species potentially affected by CSOs.
G.2. System Diagram. Provide a diagram, either in the map provided in GA or on a separate drawing, of the combined sewer collection system that
includes the following information.
a. Location of major sewer trunk lines, both combined and separate sanitary.
b. Locations of points where separate sanitary sewers feed into the combined sewer system.
C. Locations of in -line and off-line storage structures.
d. Locations of flow -regulating devices.
e. Locations of pump stations.
CSO OUTFALLS:
Complete questions G.3 through G.6 once for each CSO discharge point.
G.3. Description of Outfall.
a. Outfall number
b. Location
(City or town, if applicable)
(Zip Code)
(County) (State)
(Latitude) (Longitude)
C. Distance from shore (if applicable) ft.
d. Depth below surface (if applicable) ft.
e. Which of the following were monitored during the last year for this CSO?
❑ Rainfall CSO pollutant concentrations CSO frequency
❑ CSO flow volume ❑ Receiving water quality
f. How many storm events were monitored during the last year?
GA. CSO Events.
a. Give the number of CSO events in the last year.
events ( actual or approx.)
b. Give the average duration per CSO event.
hours (❑ actual or ❑ approx.)
Page 28 of 30

FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN:
Mount Holly VVVVfP, NCO021156 Renewal Catawba
C. Give the average volume per CSO event.
million gallons (❑ actual or ❑ approx.)
d. Give the minimum rainfall that caused a CSO event in the last year
Inches of rainfall
G.S. Description of Receiving Waters.
a. Name of receiving water:
b. Name of watershed/river/stream system:
United State Soil Conservation Service 14-digit watershed code (if known):
C. Name of State Management/River Basin:
United States Geological Survey 8-digit hydrologic cataloging unit code (if known):
G.S. CSO Operations.
Describe any known water quality impacts on the receiving water caused by this CSO (e.g., permanent or intermittent beach closings, permanent or
intermittent shell fish bed closings, fish kills, fish advisories, other recreational loss, or violation of any applicable State water quality standard).
END OF PART G.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE.
Page 29 of 30

Additional information, if provided, will appear on the following pages.
NPDES FORM 2A Additional Information

ATTACHMENT I
Sludge Management Plan

MT.HOLLY SLUDGE
SLUDGE MANAGEMENT PLAN
Sludge is wasted to two 750,000 gallon holding tanks that serve as storage
and aeration of biosolids.These tanks are frequently decanted to remove
excess water and to thicken sludge,generally to about 3% concentration.
Synagro is the contracted sludge hauler that delivers the sludge to the
farmers where it is land applied. The sludge is processed in the same tanks
for vector reduction and pathogen destruction.The sludge will be analyzed
for complete digestion and lime stabilized when needed before hauling.
The city holds land application permit # WQ 0001863 which includes the
approved land application sites.

SITE SUMMARY
City of Mt Holly
Mt. Holly. NC
Site ID: NC-GA-41
Owners Name: Greg Springs
Address: 427 S. Main St
Mt Holly NC 28120
Phone: [phone] Gill
Operator: Same as above
Estimated
Total Applicable
Fields Acres Acres
Predominant Latitude &
Croc3(s) Slone f%1 Soil Series Lonnitude
01
6.8
6.8
Fescue
2-8
LdB2
Lloyd
35 17 45 N
81 0155 W
06
15.2
14.3
Fescue
2-8
LdB2
Lloyd
351751 N
8101 50
09
17.0
13.5
_
Fescue
2-8
LdB2
Lloyd
35 17 39 N
8101 53 W
10
20.7
17.5
Fescue
2-8
LdB2
Llo
35 17 48 N
18101 37 W
14
12.5
9.7
Fescue
2-8
LdB2 1351742 N
Lloyd , 81 01 42 W
TOTALS 72.2 61.8
Notes:
Date: 03/09/12
The compliance boundary is established at either 250 feet from the residuals
application area or 50 feet within the property boundary, whichever is closest to the
application area. The review boundary is established midway between the compliance
boundary and the perimeter of the residuals application area.

SITE SUMMARY
City of Mt Holly
Mt. Holly. NC
Site ID: NC-GA-44
Owners Name: George Bennett Allen
(Field 01)
Address: 2552 Lincolnton Hwy
Cherryville, NC 28021
Phone: [phone] (H)
704-691-9497 (cell)
Operator: Same
Estimated
Total Applicable
Fields Acres Acres
R-Anell Housing Group
(Fields 02 & 03)
235 Anthony Grove Rd
Crouse, NC 28033
704-445-9610
George Bennett Allen
Predominant Latitude &
CroWsl Slone f%1 Soil Series Longitude
1
2
10.0
_
18.9
6.9
Fescue
Fescue
6 - 15
WeD
Wedowee
35 23 59 N
81 1948 W
18.9
6 - 15
ApB
Ap lin
35 23 52 N
81 1931 W
3
40.0
37.5
Fescue
2-8
CdB2
Cecil
35 23 41 N
81 19 35 W
TOTALS 68.9 63.3
Notes:
Date: 03/09/12
'he compliance boundary is established at either 250 feet from the residuals applicatic
area or 50 feet within the property boundary, whichever is closest to the application
area. The review boundary is established midway between the compliance boundary
ind the perimeter of the residuals application area.

SITE SUMMARY
City of Mt Holly
Mt. Holly. NC
Site ID: NC-LT-43
Owners Name: Gary Duckworth
Address: 857 S. Hwy 16
Stanley, NC 28164
Phone: [phone] (home) 704-996-0849 (cell)
Operator: Same as above
Estimated
Total Applicable
Fields Acres Acres Crows)
Predominant Latitude &
Slone !%f Soil Series Lnnniturlp
01
13.6
11.2
Fescue
2-8
CeB2
35 25 30 dNCecil 805950
02
22.3
21.0
Fescue
2-8
CeB2
Cecil
35 25 35 N'
80 59 46 W
03
11.0
10.0
Fescue
2-8
8 -15
CeB2
Cecil
35 25 47 N
80 59 56 W
04
15.0
6.0
Fescue
PeC2
Pacolet 1805941
35 25 36 N
W
TOTALS 61.9 48.2
Notes:
Date: 03/09/12
The compliance boundary is established at either 250 feet from the residuals application
area or 50 feet within the property boundary, whichever is closest to the application
area. The review boundary is established midway between the compliance boundary
and the perimeter of the residuals application area.

SITE SUMMARY
City of Mount Holly
W00001863
Site ID:
NC-LT-46
Owner:
Tony Jones
Address:
1418 Nature Preserve Rd
Denver, NC 28037
Phone:
704-483-1600
Operator:
Same
Lincoln Co.
Estimated RYE -based Predominant Latitude/
Applicable Annual PAN Soil Series Longitude
Plolda Armft emnial rl RIAClVRI (roan nnih In AA Ci
1
2
11 8
Fescue
209
Cecil
CeB2
352432 N
81 02 27 W
45.2
Fescue
asture
209
Cecil
CeB2
35 24 42 N
81 02 06
3
9.9
Fescue
ha
209
Cecil
CeB2
35 24 22 N
13102 51 VV
4
19.4
Fescue
(pasture)CeB2
209
Cecil
35 24 29 N
610207 W
5
7.9
Fescue
ha
176
Lloyd
LdC2
352465 N
810152
6
5.4
Fescue
ha
188
Pacolat
PeB2
352450 N
81 00 50 W
7
7.0
Fescue
ha
188
Pacolat
PeB2
35 26 35 N
81 00 29
8
6.6
Fescue
ha
209
Cecil
{CeB2
35 24 21 N
8102 28 VV
TOTALS 113.2
Notes:
Date: 12120/13
The compliance boundary is established at either 250 feet from the residuals
application area or 50 feet within the property boundary, whichever is closest to the
application area. The review boundary is established midway between the
compliance boundary and the perimeter of the residuals application area.

SITE SUMMARY
City of Mt Holly
Mt. Holly. NC
Site ID:
NC-MG-37
y 'n/ 5C31N
Owners Name:
Dean Stewart Connell
AOT�
Address:
10812 Rozzelles Ferry Rd
76
Charlotte NC 28214s
Cam}
C.
Phone:
704-737-8796
Operator-
Same as above
Estimated
Total
Applicable
Predominant Latitude &
Fields Acres
AcresCroF(s)
Sloe % Soil Series Longitude
01 37.5
I 20.7 I Fescue
2-8 CeB2 35 17 50 N
Cecil 180 59 22 lA
TOTALS 37.5 20.7
Notes:
Date:
03/09/12
The compliance boundary is established at either 250 feet from the residuals application
area or 50 feet within the property boundary, whichever is closest to the application
area. The review boundary is established midway between the compliance boundary
and the perimeter of the residuals application area.

ATTACHMENT II
Topographical Map

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0'
C' N,
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--4' LAKE'
Z
P
City of Mount Holly I-P-M,63 ME Facility
M. a
'A
Mount Holly NA,7WTP Location tufflo. 0-1:1-1-Ap
Latitude. 35' 15' 55" N State Grid/Ouad: F 14 SE Mt. Holly, NC not to scale
Longitude: 8 V 00' 35" W Permitted Flow, 4.0 MGD NPDffS- —Permit No. NCO021 I
Receivine Stream: Catawba River Draina2e Basin: Catawba River Basin 11 No rth t
Stream Class- NX 5 - IV C A Sub -Basin: 03-H-3' I i Gaston County
N
2&
W;

ATTACHMENT III
Plant Flow Diagram

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ATTACHMENT IV
Effluent Pollutant Scan's

'Client:City of Mount Holly Laboratory ID: PG23072-001
Db.cription: EFFLUENT Matrix: Aqueous
Date Sampled:07/23/2014 0820
Date Received:0712312014
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date
Batch
1 360.1
(Ammonia - N ) 350.1
1 08/01/2014 1715
BLB 08/01/2014 1038
52987
1
(Hardness (to) SM 2340C-2011
1 08/04/2014 1653
BWS
53239
1
(Nitrate-Nitr) 353.2
10 08/01/2014 1654
MJI
52990
1
(Phosphorus) 365.1
5 07/24/2014 2000
BLB 07/24/2014 1030
52255
1
(TDS) SM 2540C-2011
1 07/24/2014 0944
SDS
52244
Parameter
CAS Analytical
Number Method
Result Q
PQL
Units
Run
Ammonia - N (phonate)
350.1
0.34
0.10
mg/L
1
Hardness (total)
SM 2340C-20
36
10
mg/L
1
Nitrate -Nitrite - N
353.2
17
0.20
mg/L
1
Phosphorus
✓ TDS
7723-14-0 365.1
2.4
0.050
mg/L
1
SM 254OC-20
580
10
mg/L
1
Semivolatile Organic Compounds by GC/MS
Run, Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 07/30/20141339 DRB1 07/25120141534 52358
Parameter
CAS
Number
Analytical
men o
Result Q
PQL
Units
Run
,'Acenaphthene
�Acenaphthylene
83-32-9
625
ND
2.0
ug/L
1
208-96-8
625
ND
2.0
ug/L
1
Anthracene
Wine
120-12-7
625
ND
2.0
ug/L
1
J13
92-87-5
625
ND
10
ug/L
1
Benzo(a)anthracene
✓Benzo(a)pyrene
56-55-3
625
ND
2.0
ug/L
1
50-32-8
625
ND
2.0
ug/L
1
JBenzo(b)fluoranthene
205-99-2
625
ND
2.0
ug/L
1
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
191-24-2
625
ND
2.0
ug/L
1
✓d
207-08-9
625
ND
2.0
ug/L
1
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
101-55-3
625
ND
2.0
ug/L
1
--/4-Chloro-3-methyl phenol
85-68-7
59-50-7
625
ND
10
ug/L
1
625
ND
2.0
ug/L
1
wr bis(2-Chloroethoxy)methane
.� bis(2-Chloroethyl)ether
111-91-1
625
ND
2.0
tig/L
1
111-44-4
625
ND
2.0
ug/L
1
bis(2-Chloroisopropyl)ether
108-60-1
625
ND
2.0
ug/L
1
-/2-Chloronaphthalene
✓ 2-Chlorophenol
91-58-7
625
ND
2.0
ug/L
1
95-57-8
625
ND
2.0
ug/L
1
V 4-Chlorophenyl phenyl ether
7005-72-3
625
ND
2.0
ug/L
1
JChrysene
Dibenzo(a,h)anthracene
218-01-9
625
ND
2.0
ug/L
1
✓1,2-Dichlorobenzene
53-70-3
625
ND
2.0
ug/L
1
95-50-1
625
ND
2.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
2.0
ug/L
1
i/1,4-Dichlorobenzene
106-46-7
625
ND
2.0
ug/L
1
V/3,3'-Dichlorobenzidine
91-94-1
625
ND
10
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result c PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 5 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

• Client:Clty of Mount Holly Laboratory ID: PG23072-001
Description: EFFLUENT Matrix: Aqueous
Date Sampled:07/23/2014 0820
Date Received:07/23/2014
Semivolatile Organic Compounds by GCIMS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 07/30/20141339 DR61 07125/20141534 52358
CAS
Analytical
Parameter
Number
Methoa
Result Q
PQL
Units
Run
2,4-Dichlorophenol
120-83-2
625
ND
2.0
ug/L
1
✓ Diethylphtha late
84-66-2
625
ND
10
ug/L
1
Dimethyl phthalate
J2,4-Dimethylphenol
131-11-3
625
ND
10
ug/L
1
105-67-9
625
ND
2.0
ug/L
1
7>✓/ i-n-butyl phthalate
84-74-2
625
ND
10
ug/L
1
v 4,6-Dinitro-2-methylphenol
534-52-1
625
ND
10
ug/L
1
42,4-Dinitrophenol
✓2,4-Dinitrotoluene
51-28-5
625
ND
10
ug/L
1
121-14-2
625
ND
4.0
ug/L
1
./2,6-Dinitrotoluene
606-20-2
625
ND
4.0
ug/L
1
✓ Di-n-octylphthalate
117-84-0
625
ND
10
ug/L
1
azobenzene)
103-33-3
625
ND
2.0
ug/L
1
I11,2-Diphenylhydrazine(as
J bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
10
ug/L
1
✓ Fluoranthene
206-44-0
625
ND
2.0
ug/L
1
te Fluorene
86-73-7
625
ND
2.0
ug/L
1
✓ Hexachlorobenzene
118-74-1
625
ND
2.0
ug/L
1
✓ Hexachlorobutadiene
87-68-3
625
ND
2.0
ug/L.
1
Hexachlorocyclopentadiene
77-47-4
625
ND
10
ug/L
1
✓ Hexachloroethane
67-72-1
625
ND
2.0
ug/L
1
t✓ Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
2.0
ug/L
1
Isophorone
78-59-1
625
ND
2.0
ug/L
1
Naphthalene
91-20-3
625
ND
2.0
ug/L
1
'Nitrobenzene
98-95-3
625
ND
2.0
ug/L
1
✓ 2-Nitrophenol
88-75-5
625
ND
4.0
ug/L
1
✓ 4-Nitrophenol
100-02-7
625
ND
10
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
2.0
ug/L
1
d N-Nitrosodi-n-propylamine
621-64-7
625
ND
2.0
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
2.0
ug/L
1
✓ Pentachlorophenol
87-86-5
625
ND
10
ug/L
1
✓ Phenanthrene
85-01-8
625
ND
2.0
ug/L
1
✓ Phenol
108-95-2
625
ND
2.0
ug/L
1
✓Pyrene
129-00-0
625
ND
2.0
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
2.0
ug/L
1
I✓ 2,4,6-Trichlorophenol
88-06-2
625
ND
2.0
ug/L
1
PQL = Practical quantitalion limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page' 6 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

,f �•Client:City of Mount Holly Laboratory ID: PG23072-001
Description: EFFLUENT Matrix: Aqueous
Date Sampled:07/23/2014 0820
Date Received:07123/2014
Surrogate
Run 1
Q % Recovery
Acceptance
Limits
2-Fluorobiphenyl
77
37-129
2-Fluorophenol
72
24-127
Nitrobenzene-d5
70
38-127
Phenol-d5
76
28-128
Terpheny1-d14
45
10-148
2,4,6-Tribromophenol
88
41-144
IC P-MS
Run Prep Method
1 200.2
Analytical Method Dilution Analysis Date Analyst
200.8 1 07/25/2014 1506 BNW
Prep Date
07/25/2014 0948
Batch
62343
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Antimony
7440-36-0 200.8
0.028
0.001
mg/L
1
Arsenic
7440.38-2 200.8
0.001
0.001
mg/L
1
'/Beryllium
7440-41-7 200.8
ND
0.0004
mg/L
1
'/Cadmium
7440-43-9 200.8
ND
0.0001
mg/L
1
'/ Chromium
7440-47-3 200.8
0.0072
0.005
mg/L
1
Copper
7440-50-8 200.8
0.019
0.001
mg/L
1
Lead
`/Nickel
7439-92-1 200.8
ND
0.001
mg/L
1
Selenium
7440-02-0 200.8
ND
0.005
mg/L
1
7782-49-2 200.8
0.0031
0.001
m91L
1
Silver
7440-22-4 200.8
ND
0,001
mg/L
1
Thallium
7440-28-0 200.8
ND
0.0005
mg/L
1
Zinc
7440-66-6 200.8
0.035
0.01
mg/L
1
PQL = Practical quantitation limit e = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result < PQL and - MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 7 of 9
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I - Client: City of Mount Holly
I
Laboratory ID: PG23072-002
Description: EFFLUENT
Matrix: Aqueous
Date Sampled:07/23/2014 0830
Date Received:07/2312014
Inor anic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 10-204-00-1-X (Cyanide - To) SM 4500-CN E-
1 07/30/2014 1512 NCM
07/30/2014 1000
52698
1 (Phenolics) 420.4
1 07/27/2014 0213 TAF
07/26/2014 1030
52425
1 (HEM (oil and) 1664E
1 07/29/2014 1000 JDW
52595
CAS Analytical
Parameter
Number MLUIod
Result Q
PQL
Units Run
Cyanide - Total
57-12-5 SM 4500-CN
ND
0.010
mg/L 1
Phenolics
420.4
ND
0.020
mg/L 1
HEM (oil and grease)
1664B
ND
4.0
mg/L 1
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 624 1 08/01/2014 0904 PMM2 52948
Parameter
CAS
Number
Analytical
Result Q
PQL
Units
Run
Acrolein
-/Acrylonitrile
107-02-8
624
ND
50
ug/L
1
Benzene
107-13-1
624
ND
50
ug/L
1
71-43-2
624
ND
5.0
ug/L
1
V Bromodichloromethane
75-27-4
624
ND
5.0
ug/L
1
Bromoform
75-25-2
624
5.1
6.0
ug/L
1
f
/romomethane (Methyl bromide)
74-83-9
624
ND
5.0
ug/L
1
Carbon tetrachloride
56-23-5
624
ND
5.0
ug/L
1
✓ I hlorobenzene
108-90-7
624
ND
5.0
ug/L
1
/J Chloroethane
75-00-3
624
ND
5.0
ug/L
1
V 2-Chloroethylvinylether
110-75-8
624
ND
10
ug/L
1
2,chloroform
67-66-3
624
ND
5.0
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
624
ND
5.0
ug/L
1
./Dibromochloromethane
10'1,1-Dichloroethane
124-48-1
624
10
5.0
ug/L
1
1,2-Dichloroethane
75-34-3
624
ND
5.0
ug/L
1
107-06-2
624
ND
5.0
ug/L
1
t1-Dichloroethene
75-35-4
624
ND
5.0
ug/L
1
rans-1,2-Dichloroethene
156-60-5
624
ND
5.0
ug/L
1
1,2-Dichloropropane
78-87-5
624
ND
5.0
ug/L
1
cis-1,3-Dichloropropene
11-I'trans-11,3-Dichloropropene
10061-01-5
624
ND
5.0
ug/L
1
Ethylbenzene
10061-02-6
624
ND
5.0
ug/L
1
✓ Methylene chloride
100-41-4
624
ND
5.0
ug/L
1
1,1,2,2-Tetrachloroethane
75-09-2
624
ND
5.0
ug/L
1
Tetrachloroethene
79-34-5
624
ND
5.0
ug/L
1
✓ Toluene
127-18-4
624
ND
5.0
ug/L
1
✓1.1,1-Trichloroethane
108-88-3
624
ND
5.0
ug/L
1
J
71-55-6
624
ND
5.0
ug/L
1
1,1,2-Trichloroethane
✓Trichloroethene
79-00-5
624
ND
5.0
ug/L
1
79-01-6
624
ND
5.0
ug/L
1
PQL = Practical quantitation limit 6 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery Is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 8 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

„ Client:City of Mount Holly
Laboratory ID: PG23072-002
Description: EFFLUENT
Matrix: Aqueous
Date Sampled:07/23/2014 0830
Date Received:07123/2014
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 5030B
624 1 08/01/2014 0904 PMM2
52948
CAS Analytical
Parameter
Number Mf"Th d Result Q
PQL Units
Run
Vinyl chloride
75-01-4 624 ND
5.0 ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
105 70-130
Bromofluorobenzene
112 70-130
Toluene-d8
115 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quanbtation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
City of Mount Holly
Lot Number: OA29039
Sample Number Sample ID Matrix Date Sampled Date Received
001 EFFLUENT Aqueous 01/29/2013 0810 01/29/2013
002 EFFLUENT Aqueous 01/29/2013 0820 01/29/2013
(2 samples)
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
City of Mount Holly
Lot Number: OA29039
Sample Sample ID
Matrix
Parameter Method
Result Q
Units
Page
001
EFFLUENT
Aqueous
Ammonia - N (phenate) 350.1
0.51
mg/L
5
001
EFFLUENT
Aqueous
Hardness (total) SM 2340C-
41
mg/L
5
001
EFFLUENT
Aqueous
Nitrate -Nitrite - N 353.2
17
mg/L
5
001
EFFLUENT
Aqueous
Phosphorus 365.1
2.4 S
mg/L
5
001
EFFLUENT
Aqueous
TDS SM 2540C-
490
mg/L
5
001
EFFLUENT
Aqueous
TKN 351.2
1.6
mg/L
5
001
EFFLUENT
Aqueous
TRC SM 4500-CL
0.055
mg/L
5
001
EFFLUENT
Aqueous
Antimony 200.8
0.03
mg/L
7
001
EFFLUENT
Aqueous
Copper 200.8
0.014
mg/L
7
001
EFFLUENT
Aqueous
Selenium 200.8
0.0015
mg/L
7
001
EFFLUENT
Aqueous
Zinc 200.8
0.041
mg/L
7
(11 detections)
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Client: City of Mount Holly Laboratory ID: OA29039-001
Description: EFFLUENT Matrix: Aqueous
Date Sampled:01129/2013 0810
Date Received:01/29/2013
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 SM4500-NH3 (Ammonia - N ) 350.1
1
02/08/2013 1247 MML
02/07/2013 1030
13542
1 (Hardness (to) SM 2340C-
1
02/05/2013 1400 KMB
13390
1 (Nitrate-Nitr) 353.2
25
02/04/2013 2055 HBB
13237
1 (Phosphorus) 365.1
10
02/05/2013 1713 MML
01/31/2013 2331
13025
1 (TDS) SM 254OC-2011
1
02/04/2013 0827 KES
13160
1 351.4 (TKN) 351.2
1
02/04/2013 1157 MML
02/01/2013 1315
13090
1 (TRC) SM 4500-CL G-2011
1
01/30/2013 1930 HBB
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Ammonia - N (phenate)
350.1
0.51
0.10
mg/L
1
Hardness (total)
SM 2340C-2011
41
10
mg/L
1
Nitrate -Nitrite - N
353.2
17
0.50
mg/L
1
Phosphorus
7723-14-0 365.1
2.4 S
0.10
mg/L
1
TDS
SM 2540C-2011
490
10
mg/L
1
TKN
351.2
1.6
0.50
mg/L
1
TRC
SM 4500-CL G-2011
0.055
0.050
mg/L
1
Semivolatile
Organic Compounds by GC/MS
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 625 625
2
02/07/20131814 RBH
01/30/20131229
12838
2 625 625
2
02/07/20131911 JRG
02/04/20131230
13178
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Acenaphthene
83-32-9 625
ND
2.0
ug/L
1
Acenaphthylene
208-96-8 625
ND
2.0
ug/L
1
Anthracene
120-12-7 625
ND
2.0
ug/L
1
Benzidine
92-87-5 625
ND
10
ug/L
1
Benzo(a)anthracene
56-55-3 625
ND
2.0
ug/L
1
Benzo(a)pyrene
50-32-8 625
ND
2.0
ug/L
1
Benzo(b)fluoranthene
205-99-2 625
ND
2.0
ug/L
1
f Benzo(g,h,i)perylene
191-24-2 625
ND
2.0
ug/L
1
-4 Benzo(k)fluoranthene
207-08-9 625
ND
2.0
ug/L
1
.4:-4-Bromophenyl phenyl ether
101-55-3 625
ND
2.0
ug/L
1
Butyl benzyl phthalate
85-68-7 625
ND
10
ug/L
1
f 4-Chloro-3-methyl phenol
59-50-7 625
ND
2.0
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1 625
ND
2.0
ug/L
1
-- bis(2-Chloroethyl)ether
111-44-4 625
ND
2.0
ug/L
1
bis(2-Chloroisopropyl)ether
108-60-1 625
ND
2.0
ug/L
1
2-Chloronaphthalene
91-58-7 625
ND
2.0
ug/L
1
- 2-Chlorophenol
95-57-8 625
ND
2.0
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3 625
ND
2.0
ug/L
1
Chrysene
218-01-9 625
ND
2.0
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSO failure
Shealy Environmental Services, Inc. Page: 5 Of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Clicnt:City of Mount Holly Laboratory ID: OA29039-001
Description: EFFLUENT Matrix: Aqueous
Date Sampled:01/29/2013 0810
Date Received:01/2912013
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 2 02/07/20131814 RBH 01130/20131229 12838
2 625 625 2 02107/20131911 JRG 02/04/20131230 13178
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Dibenzo(a,h)anthracene
53-70-3
625
ND
2.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
2.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
2.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
2.0
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
10
ug/L
2
2,4-Dichlorophenol
120-83-2
625
ND
2.0
ug/L
1
Diethyl phthalate
84-66-2
625
ND
10
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
10
ug/L
1
f 2,4-Dimethylphenol
105-67-9
625
ND L
2.0
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
10
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
10
ug/L
1
-f 2,4-Dinitrophenol
51-28-5
625
ND
10
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
4.1
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
4.1
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
10
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
2.0
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
10
ug/L
1
Fluoranthene
206-44-0
625
ND
2.0
ug/L
1
Fluorene
86-73-7
625
ND
2.0
Lig/L
1
Hexachlorobenzene
118-74-1
625
ND
2.0
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
2.0
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
10
ug/L
1
Hexachloroethane
67-72-1
625
ND
2.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
2.0
ug/L
1
Isophorone
78-59-1
625
ND
2.0
ug/L
1
Naphthalene
91-20-3
625
ND
2.0
ug/L
1
Nitrobenzene
98-95-3
625
ND
2.0
ug/L
1
2-Nitrophenol
88-75-5
625
ND
4.1
ug/L
1
4-Nitrophenol
100-02-7
625
ND
10
ug/L
1
j N-Nitrosodimethylamine
62-75-9
625
ND
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
2.0
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
2.0
ug/L
1
47 Pentachlorophenol
87-86-5
625
ND
10
ug/L
1
Phenanthrene
85-01-8
625
ND
2.0
ug/L
1
+ Phenol
108-95-2
625
ND
2.0
ug/L
1
Pyrene
129-00-0
625
ND
2.0
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
2.0
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
2.0
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantltation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 6 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Client: City of Mount Holly
Laboratory ID: OA29039-001
Description: EFFLUENT
Matrix: Aqueous
Date Sampled:01/29/2013 0810
Date Received:01/2912013
Run 1 Acceptance
Run 2 Acceptance
Surrogate Q
% Recovery Limits
Q % Recovery Limits
2,4,6-Tribromophenol
77 41-144
66 41-144
Phenol-d5
60 28-128
54 28-128
Nitrobenzene-d5
61 38-127
54 38-127
2-Fluorobiphenyl
60 37-129
53 37-129
2-Fluorophenol
58 24-127
53 24-127
Terphenyl-d14
53 10-148
29 10-148
ICP-MS
Run Prep Method Analytical Method
Dilution Analysis Date
Analyst
Prep Date
Batch
1 200.2 200.8
1 02/01/2013 0349
CDF
01/31/2013 1100
12917
2 200.2 200.8
1 02/02/20131453
BNW
01/31/20131100
12917
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Antimony
7440-36-0
200.8
0.03
0.001
mg/L
1
Arsenic
7440-38-2
200.8
ND
0.001
mg/L
2
Beryllium
7440-41-7
200.8
ND
0.0004
mg/L
1
Cadmium
7440-43-9
200.8
ND
0.0001
mg/L
1
Chromium
7440-47-3
200.8
ND
0.005
mg/L
1
Copper
7440-50-8
200.8
0.014
0.001
mg/L
1
Lead
7439-92-1
200.8
ND
0.001
mg/L
1
Nickel
7440-02-0
200.8
ND
0.005
mg/L
1
Selenium
7782-49-2
200.8
0.0015
0.001
mg/L
2
Silver
7440-22-4
200.8
ND
0.001
mg/L
1
Thallium
7440-28-0
200.8
ND
0.0005
mg/L
1
Zinc
7440-66-6
200.8
0.041
0.01
mg/L
1
PQL = Practical quantitation limit e = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
No = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" S = MS/MSD failure
Shealy Environmental Services, Inc. Page: 7 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab,com Level 1 Report v2.1

Client: City of Mount Holly Laboratory ID: OA29039-002
Description: EFFLUENT Matrix: Aqueous
Date Sampled:01129/2013 0820
Date Received: 0 1129/2013
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date
Analyst
Prep Date
Batch
1 10-204-00-1-X (Cyanide - To) SM 4500-CN
1 02/01/2013 0110
MML
01/31/2013 1628
12991
1 (Phenolics) 420.4
1 02/07/2013 2141
HBB
02/07/2013 1330
13439
1 (HEM (oil and) 1664E
1 02/04/2013 1057
AJK
13185
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Cyanide - Total
57-18M 4500-CN E-2011
ND
0.010
mg/L
1
Phenolics
420.4
ND
0.020
mg/L
1
HEM (oil and grease)
1664B
ND
4.7
mg/L
1
Volatile Organic Compounds
by GC/MS
Run Prep Method Analytical Method
Dilution Analysis Date
Analyst
Prep Date
Batch
1 5030B 624
1 02/05/2013 0317
JAC
13242
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Acrolein
107-02-8
624
ND
50
ug/L
1
Acrylonitrile
107-13-1
624
ND
50
ug/L
1
Benzene
71-43-2
624
ND
5.0
ug/L
1
+Bromodichloromethane
75-27-4
624
ND
5.0
ug/L
1
Bromoform
75-25-2
624
ND
5.0
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
624
ND
5.0
ug/L
1
Carbon tetrachloride
56-23-5
624
ND
5.0
ug/L
1
Chlorobenzene
108-90-7
624
ND
5.0
ug/L
1
Chloroethane
75-00-3
624
ND
5.0
ug/L
1
2-Chloroethylvinylether
110-75-8
624
ND
10
ug/L
1
Chloroform
67-66-3
624
ND
5.0
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
624
ND
5.0
ug/L
1
Dibromochloromethane
124-48-1
624
ND
5.0
ug/L
1
1,1-Dichloroethane
75-34-3
624
ND
5.0
ug/L
1
1,2-Dichloroethane
107-06-2
624
ND
5.0
ug/L
1
1,1-Dichloroethene
75-35-4
624
ND
5.0
ug/L
1
trans- 1,2-Dichloroethene
156-60-5
624
ND
5.0
ug/L
1
1,2-Dichloropropane
78-87-5
624
ND
5.0
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
624
ND
5.0
ug/L
1
i trans-1,3-Dichloropropene
10061-02-6
624
ND
5.0
ug/L
1
Ethylbenzene
100-41-4
624
ND
5.0
ug/L
1
Methylene chloride
75-09-2
624
ND
5.0
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
624
ND
5.0
ug/L
1
Tetrachloroethene
127-18-4
624
ND
5.0
ug/L
1
Toluene
108-88-3
624
ND
5.0
ug/L
1
1,1,1-Trichloroethane
71-55-6
624
ND
5.0
ug/L
1
1,1,2-Trichloroethane
79-00-5
624
ND
5.0
ug/L
1
Trichloroethene
79-01-6
624
ND
5.0
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
Q = Surrogate failure
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 %
N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis are reported on a dry weight
basis unless flagged with a "W"
S =
MS/MSD failure
Shealy Environmental Services, Inc.
Page: 8 of 9
106 Vantage Point Drive West Columbia, SC 29172 (803)
791-9700 Fax [phone]
www.shealylab.com
Level 1 Report v2.1

Clie,it: City of Mount Holly Laboratory ID: OA29039-002
Description: EFFLUENT Matrix: Aqueous
Date Sampled:01/29/2013 0820
Date Received:01/29/2013
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 5030B
624 1 02/05/2013 0317 JAC
13242
CAS Analytical
Parameter
Number Method Result Q
PQL Units Run
Vinyl chloride
75-01-4 624 ND
5.0 ug/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
90 52-138
Bromofluorobenzene
104 70-147
Toluene-d8
96 76-125
PQL = Practical quantitation limit
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time Q = Surrogate failure
ND = Not detected at or above the PQL
J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40%
N = Recovery is out of criteria L = LCS/LCSD failure
Where applicable, all soil sample analysis
are reported on a dry weight basis unless flagged with a "W'
S = MS/MSD failure
Shealy Environmental Services, Inc.
Page: 9 of 9
106 Vantage Point Drive West Columbia,
SC 29172 [phone] Fax [phone] www.shealylab.com
Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
City of Mount Holly
Lot Number: NF14071
Sample Number Sample ID Matrix Date Sampled Date Received
001 Effluent Aqueous 06/14/2012 0810 06/14/2012
002 Effluent Aqueous 06/14/2012 0815 06/14/2012
(2 samples)
Shealy Environmental Services, Inc. Page: 3 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Level 1 Report v2.1

SHEALY
ENVIRONMENTAL SERVICES, INC.
Executive Summary
City of Mount Holly
Lot Number: NF14071
Sample Sample ID
Matrix
Parameter Method
Result Q
Units
Page
001
Effluent
Aqueous
Ammonia - N (phenate) 350.1
0.25
mg/L
5
001
Effluent
Aqueous
Hardness (total) SM 2340C
42
mg/L
5
001
Effluent
Aqueous
Nitrate -Nitrite - N 353.2
19
mg/L
5
001
Effluent
Aqueous
Phosphorus 365.1
3.8
mg/L
5
001
Effluent
Aqueous
TDS SM 2540C
490
mg/L
5
001
Effluent
Aqueous
TKN 351.2
2.6
mg/L
5
001
Effluent
Aqueous
Antimony 200.8
0.034
mg/L
7
001
Effluent
Aqueous
Chromium 200.8
0.0057
mg/L
7
001
Effluent
Aqueous
Copper 200.8
0.019
mg/L
7
001
Effluent
Aqueous
Selenium 200.8
0.004
mg/L
7
001
Effluent
Aqueous
Zinc 200.8
0.054
mg/L
7
(11 detections)
Shealy Environmental Services, Inc. Page: 4 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Client: City of Mount Holly Laboratory ID: NF14071-001
s
Description: Effluent Matrix: Aqueous
Date Sampled:06/14/2012 0810
Date Received: 06/1412012
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 SM4500-NH3
(Ammonia - N ) 350.1
1
06/22/2012 1649 SMH
06/22/2012 0938
87616
1
(Hardness (to) SM
1
06/19/2012 0842 MDR
87351
1
(Nitrate-Nitr) 353.2
10
06/20/2012 1417 HBB
87459
1
(Phosphorus) 365.1
10
06/20/2012 1051 JBS
06/19/2012 1530
87369
1
(TDS) SM 2540C
1
06/18/2012 1146 LAS
87169
1 351.4
(TKN) 351.2
1
06/21/2012 1205 JBS
06/20/2012 0900
87433
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Ammonia - N (phenate)
350.1
0.25
0.10
mg/L
1
Hardness (total)
SM 2340C
42
10
mg/L
1
Nitrate -Nitrite - N
353.2
19
0.20
mg/L
1
Phosphorus
7723-14-0 365.1
3.8
0.10
mg/L
1
TDS
SM 2540C
490
10
mg/L
1
TKN
351.2
2.6
0.50
mg/L
1
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method
1 625 625
Dilution Analysis Date
1 06118/20121908
Analyst
SJA
Prep Date
06/15/20121008
Batch
87003
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Acenaphthene
83-32-9
625
ND
1.0
ug/L
1
Acenaphthylene
208-96-8
625
ND
1.0
ug/L
1
Anthracene
120-12-7
625
ND
1.0
ug/L
1
Benzidine
92-87-5
625
ND
5.1
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
1.0
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
1.0
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
1.0
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
1.0
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
1.0
ug/L
1
4-Bromophenyl phenyl ether -
101-55-3
625
ND
1.0
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
5.1
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
1.0
ug/L
1
bis (2-C hloroeth oxy) methane
111-91-1
625
ND
1.0
ug/L
1
-Aw bis(2-Chloroethyl)ether
111-44-4
625
ND
1.0
ug/L
1
bis(2-Chloroisopropyl)ether
108-60-1
625
ND
1.0
ug/L
1
2-Chloronaphthalene
r 2-Chlorophenol
91-58-7
95-57-8
625
625
ND
ND
1.0
ug/L
1
1.0
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
1.0
ug/L
1
Chrysene
218-01-9
625
ND
1.0
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
1.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
1.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
1.0
ug/L
1
PQL = Practical quanntation limit B = Detected In the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' = Reportable result (only when report all runs)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
H = Out of holding time
N = Recovery is out of criteria
Page: 5 of 9
Level 1 Report v2.1

,Client: City of Mount Holly Laboratory ID: NF14071-001
Description: Effluent Matrix: Aqueous
Date Sampled:06114/2012 0810
Date Received:06/1412012
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date
Analyst
Prep Date
_
Batch
1 625
625 1 06/18/20121908
SJA
06/15/20121008
87003
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
1,4-Dichlorobenzene
106-46-7
625
ND
1.0
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
5.1
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
1.0
ug/L
1
Diethylphtha late
84-66-2
625
ND
5.1
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
5.1
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
1.0
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
5.1
ug/L
1
E 4,6-Dinitro-2-methylphenol
534-52-1
625
ND
5.1
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
5.1
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
2.0
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
2.0
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
5.1
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
1.0
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
5.1
ug/L
1
Fluoranthene
206-44-0
625
ND
1.0
ug/L
1
Fluorene
86-73-7
625
ND
1.0
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
1.0
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
1.0
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
5.1
ug/L
1
Hexachloroethane
67-72-1
625
ND
1.0
ug/L
1
Indeno(1,2,3-c,d)pyre ne
193-39-5
625
ND
1.0
ug/L
1
Isophorone
78-59-1
625
ND
1.0
ug/L
1
Naphthalene
91-20-3
625
ND
1.0
ug/L
1
Nitrobenzene
98-95-3
625
ND
1.0
ug/L
1
2-Nitrophenol
88-75-5
625
ND
2.0
ug/L
1
4-Nitrophenol
100-02-7
625
ND
5.1
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
1.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
1.0
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
1.0
ug/L
1
Pentachlorophenol
87-86-5
625
ND
5.1
ug/L
1
Phenanthrene
85-01-8
625
ND
1.0
ug/L
1
Phenol
108-95-2
625
ND
1.0
ug/L
1
Pyrene
129-00-0
625
ND
1.0
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
1.0
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
1.0
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' = Reportable result (only when report all runs)
Shealy Environmental Services, Inc. Page: 6 Of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

'Client:City of Mount Holly
Laboratory ID: NF14071-001
Description: Effluent
Matrix: Aqueous
Date Sampled:06/1412012 0810
Date Received: 06/14/2012
Run 1
Acceptance
Surrogate Q
% Recovery Limits
2,4,6-Tribromophenol
70
41-144
Phenol-d5
55
28-128
Nitrobenzene-d5
56
38-127
2-Fluorobiphenyl
58
37-129
2-Fluorophenol
53
24-127
Terphenyl-d14
23
10-148
ICP-MS
Run Prep Method Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1 200.2 200.8
1
06/16/2012 0033 BNW
06/14/2012 1936 86968
2 200.2 200.8
1
06/19/2012 0137 CDF
06/14/2012 1935 RRQRR
Parameter
CAS
Number
Analytical
Method
Result Q
PQL
Units
Run
Antimony
7440-36-0
200.8
0.034
0.001
mg/L
1
Arsenic
7440-38-2
200.8
ND
0.001
mg/L
1
Beryllium
7440-41-7
200.8
ND
0.0004
mg/L
1
Cadmium
7440-43-9
200.8
ND
0.0001
mg/L
1
Chromium
7440-47-3
200.8
0.0057
0.005
mg/L
1
Copper
7440-50-8
200.8
0.019
0.001
mg/L
1
Lead
7439-92-1
200.8
ND
0.001
mg/L
1
Nickel
7440-02-0
200.8
ND
0.005
mg/L
1
Selenium
7782-49-2
200.8
0.004
0.001
mg/L
2
Silver
7440-22-4
200.8
ND
0.001
mg/L
1
Thallium
7440-28-0
200.8
ND
0.0005
mg/L
1
Zinc
7440-66-6
200.8
0.054
0.01
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitalion of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and - MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W' = Reportable result (only when report all runs)
Shealy Environmental Services, Inc. Page: 7 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1

Client:City of Mount Holly Laboratory ID: NF14071-002
Description: Effluent Matrix: Aqueous
Date Sampled:06/14/2012 0815
Date Received:06/14/2012
Inorganic non-metals
Run Prep Method Analytical Method
Dilution Analysis Date
Analyst
Prep Date
Batch
1 10-204-00-1-X (Cyanide - To) 10-204-
1 06/15/2012 1256
SMH
06/15/2012 0830
87036
1 (Phenolics) 420.4
1 06/21/2012 1354
HBB
06/21/2012 0919
87514
1 (HEM (oil and) 1664A
1 06/23/2012 1302
PAT
87694
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Cyanide - Total
57-12-5 10-204-00-1-X
ND
0.010
mg/L
1
Phenolics
420.4
ND
0.020
mg/L
1
HEM (oil and grease)
1664A
NO
4.5
mg/L
1
Volatile
Organic Compounds
by GC/MS
Run Prep Method Analytical Method
Dilution Analysis Date
Analyst
Prep Date
Batch
1 5030B 624
1 06/26/20121826
AAC
87792
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Acrolein
107-02-8
624
NO
50
ug/L
1
Acrylonitrile
107-13-1
624
NO
50
ug/L
1
Benzene
-�Bromodichloromethane
71-43-2
624
ND
5.0
ug/L
1
75-27-4
624
NO
5.0
ug/L
1
Bromoform
75-25-2
624
NO
5.0
ug/L
1
JCarbBromomethane (Methyl bromide)
74-83-9
624
ND
5.0
ug/L
1
on tetrachloride
56-23-5
624
ND
5.0
ug/L
1
Chlorobenzene
108-90-7
624
ND
5.0
ug/L
1
Chloroethane
75-00-3
624
ND
5.0
ug/L
1
2-Chloroethylvinylether
110-75-8
624
ND
10
ug/L
1
Chloroform
67-66-3
624
NO
5.0
ug/L
1
t'Chloromethane (Methyl chloride)
74-87-3
624
ND
5.0
ug/L
1
Dibromochloromethane
124-48-1
624
ND
5.0
ug/L
1
1,1-Dichloroethane
75-34-3
624
ND
5.0
ug/L
1
1,2-Dichloroethane
41,1-Dichloroethene
107-06-2
624
ND
5.0
ug/L
1
75-35-4
624
ND
5.0
ug/L
1
4,trans-1,2-Dichloroethene
156-60-5
624
NO
5.0
ug/L
1
1,2-Dichloropropene
78-87-5
624
ND
5.0
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
624
ND
5.0
ug/L
1
s trans-1,3-Dichloropropene
10061-02-6
624
ND
5.0
ug/L
1
Ethylbenzene
100-41-4
624
ND
5.0
ug/L
1
Methylene chloride
75-09-2
624
NO
5.0
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
624
ND
5.0
ug/L
1
Tetrachloroethene
127-18-4
624
NO
5.0
ug/L
1
Toluene
108-88-3
624
ND
5.0
ug/L
1
1,1,1-Trichloroethane
71-55-6
624
NO
5.0
ug/L
1
1,1,2-Trichloroethane
79-00-5
624
NO
5.0
ug/L.
1
Trichloroethene
79-01-6
624
ND
5.0
ug/L
1
PQL = Practical quantltation limit B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL
P = The RPD between two GC columns exceeds 40 %
N = Recovery is out of cnteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
= Reportable result (only when report
all runs)
Shealy Environmental Services, Inc.
Page: 8 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone]
www.shealylab.com
Level 1 Report v2.1

Client:C �ty of Mount Holly Laboratory ID: NF14071-002
Description: Effluent Matrix: Aqueous
Date Sampled: 06/14/2012 0815
Date Received: 06114/2012
Volatile Organic Compounds
by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date
Analyst Prep Date Batch
1 5030B
624 1 06/26/20121826
AAC 87792
CAS Analytical
Parameter
Number Method Result Q PQL
Units Run
Vinyl chloride
75-01-4 -
624 ND 5.0
ug/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
108 52-138
Bromofluorobenzene
97 70-147
Toluene-d8
109 76-125
PQL = Practical quantitaflon limit
8 = Detected in the method blank
E = Quantitalion of compound exceeded the calibration range
H = Out of holding time
ND = Not Detected at or above the PQL
J = Estimated result < PQL and > M DL
P = The RPD between two GC columns exceeds 40 %
N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
• = Reportable result (only when report all runs)
Shealy Environmental Services, Inc.
Page: 9 of 9
106 Vantage Point Drive West Columbia,
SC 29172 [phone] Fax [phone]
www.shealylab.com
Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
City of Mount Holly
Lot Number: MJ06055
Sample Number Sample ID
001 Effluent
002 Effluent
(2 samples)
Matrix Date Sampled Date Received
Aqueous 10106/20110820 10/06/2011
Aqueous 10/06/20110820 10/06/2011
Shealy Environmental Services, Inc.
Page: 3
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheal Y lab.com LeReport Level � Repov 9
v2.t

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
City of Mount Holly
Lot Number: MJ06055
Sample Sample ID
Matrix
Parameter Method
Result Q
001
Effluent
Aqueous
Ammonia - N (phenate) 350.1
0.56
Units
Page
mg/L
5
001
Effluent
Aqueous
Hardness (total) SM 2340C
50
mg/L
5
001
Effluent
Aqueous
TDS SM 2540C
470
mg/L
5
001
Effluent
Aqueous
bis(2-Ethylhexyl)phthalate 625
5.9
ug/L
6
001
Effluent
Aqueous
Antimony 200.8
0.029
mg/L
7
001
Effluent
Aqueous
Arsenic 200.8
0.0013
mg/L
7
001
Effluent
Aqueous
Chromium 200.8
0.0053
mg/L
7
001
Effluent
Aqueous
Copper 200.8
0.021
mg/L
7
001
Effluent
Aqueous
Selenium 200.8
0.0033
mg/L
7
001
Effluent
Aqueous
Zinc 200.8
0.057
mg/L
7
002
Effluent
Aqueous
Bromoform 624
9.8
ug/L
8
002
Effluent
Aqueous
Dibromochloromethane 624
8.7
ug/L
8
(12 detections)
Shealy Environmental Services. Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Page: 4 t v 9
1 Level 1 Report v2.1

Client: City of Mount Holly Laboratory ID: MJ06055-001
Description: Effluent
Date Sampled:10l06/2011 0820 Matrix: Aqueous
Date Received:1010612011
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 SM4500-NH3
(Ammonia - N ) 350.1
2 10/12/2011 1347 SMH
10/11/2011 1154
69434
1
(Hardness (to) SM
1 10/17/2011 1419 SMH
69774
1
(TDS) SM 2540C
1 10/08/2011 1131 CMP
69330
Parameter
CAS Analytical
Number Method
Result Q
PQL
Units
Run
Ammonia - N (phenate)
350.1
0.56
0.20
mglL
1
Hardness (total)
SM 2340C
50
10
m /L
g
1
TDS
SM 2540C
470
10
mg/L
1
Semivolatile Organic Com ounds by GC/MS
Run Prep Method
1
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
625
625
1 10/13/20112201 WD
10/10120110912
69337
2 625
625
1 10/18/20111420 WD
10/10/20110912
69337
Parameter
CAS Analytical
Acenaphthene
Number Method
Result Q
PQL
Units
Run
Acenaphthylene
83-32-9 625
ND
1.1
ug/L
1
Anthracene
208-96-8 625
NO
1.1
ug/L
1
Benzidine
120-12-7 625
ND
1.1
ug/L
1
Benzo(a)anthracene
92-87-5 625
NO
5.3
ug/L
1
Benzo(a)pyrene
56-55-3 625
NO
1.1
ug/L
1
Benzo(b)fluoranthene
50-32-8 625
ND
1.1
ug/L
1
Benzo(g,h,i)perylene
205-99-2 625
ND
1.1
ug/L
1
Benzo(k)fuoranthene
191-24-2 625
ND
1.1
ug/L
1
4 4-Bromophenyl phenyl ether
207-08-9 625
ND
1.1
ug/L
1
Butyl benzyl phthalate
101-55-3 625
ND
1.1
ug/L
1
-- bis(2-Chloroethoxy)methane
85-68-7 625
111-91-1 625
ND
5.3
ug/L
1
-- bis(2-Chloroethyl)ether
111-44-4 625
ND
NO
1.1
ug/L
1
bis(2-Chloroisopropyl)ether
108-60-1 625
1.1
uglL
1
4-Chloro-2-methylphenol
4-Chloro-3-methyl phenol
1570-64-5 625
NO
ND
1.1
1.1
ug/L
ug/L
1
2
�- 2-Chloro-5-methylphenol
59-50-7 625
615-74-7 625
ND
1.1
ug/L
1
2-Chloronaphthalene
91-58-7 625
ND
ND
1.1
ug/L
2
2-Chlorophenol
1.1
ug/L
1
- 3 & 4-Chlorophenol
95-57-8 625
ND
1.1
ug/L
1
4-Chlorophenyl phenyl ether
108-43-0 625
7005-72-3
NO
2.1
uglL
2
Chrysene
625
NO
1.1
ug/L
1
Di-n-butyl phthalate
218-01-9 625
ND
1.1
ug/L
1
Di-n-octylphthalate
84-74-2 625
NO
5.3
ug/L
1
Dibenzo(a,h)anthracene
117-84-0 625
NO
5.3
ug/L
1
1,2-Dichlorobenzene
53-70-3 625
NO
1.1
ug/L
1
1,3-Dichlorobenzene
95-50-1 625
NO
1.1
uglL
1
541-73-1 625
ND
1.1
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank
E = Quantitabon of compound exceeded the calibration range
ND = Not detected at or above the POL J = Estimated result < PQL and > MDL
Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W" P = The N =RecovererRPD between two GC columns exceeds 4t146
y is out of criteria H = Out of holding time
Shealy Environmental Services. Inc.
106 Vantage Paint Drive West Columbia. SC 29172 [phone] Fax [phone] www.shealylab.com Page: 5 of 9
Level 1 Reportv2.1

Client: City of Mount Holly Laboratory ID: MJ06055-001
Description: Effluent Matrix: Aqueous
Date Sampled:10106/2011 0820
Date Received.10/06/2011
Semivolatile Organic compounds by GUMS
Run Prep Method Analytical
Method Dilution Analysis Date
Analyst
Prep Date
Batch
1 625
625 1 10/13/20112201
WD
10/10/20110912
69337
2 625
625 1 10/18/20111420
WD
10/10/20110912
69337
Parameter
CAS Analytical
Number Method
Result Q
PQL
Units
Run
1,4-Dichlorobenzene
106-46-7
625
NO
1.1
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
NO
5.3
ug/L
1
2,4-Dichlorophenol
120-83-2
625
NO
1.1
ug/L
1
�.2,5-Dichlorophenol
583-78-8
625
ND
2.1
ug/L
2
3,4-Dichlorophenol
95-77-2
625
ND
1.1
ug/L
2
Diethylphthalate
84-66-2
625
ND
5.3
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
5.3
ug/L
1
3,3'-Dimethylbenzidine
119-93-7
625
NO
5.3
ug/L
1
2,4-Dimethylphenol
105-67-9
625
NO
1.1
ug/L
1
-ir 4,6-Dinitro-2-methylphenol
4-
534-52-1
625
ND
5.3
ug/L
1
2,4-Dinitrophenol
"
51-28-5
625
NO
5.3
u /L
1
2,4-Dinitrotoluene
121-14-2
625
ND
2.1
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
NO
2.1
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
1.1
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
5.9
5.3
ug/L
1
Fluoranthene
206-44-0
625
NO
1.1
ug/L
1
Fluorene
86-73-7
625
NO
1.1
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
1.1
ug/L
1
Hexachlorobutadiene
87-68-3
625
NO
1.1
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
5.3
ug/L
1
Hexachloroethane
67-72-1
625
NO
1.1
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
NO
1.1
ug/L
1
Isophorone
78-59-1
625
ND
1.1
ug/L
1
-4N-Nitrosodi-n-propylamine
4- N-Nitrosodimethylamine
621-64-7
625
NO
1.1
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
62-75-9
625
NO
1.1
ug/L
1
86-30-6
625
ND
1.1
ug/L
1
Naphthalene
91-20-3
625
ND
1.1
ug/L
1
Nitrobenzene
98-95-3
625
ND
1.1
ug/L
1
j- 2-Nitrophenol
4-Nitrophenol
88-75-5
625
NO
2.1
ug/L
1
100-02-7
625
NO
5.3
ug/L
1
Pentachlorophenol
87-86-5
625
NO
5.3
ug/L
1
4Phenanthrene
- Phenol
85-01-8
625
NO
1.1
ug/L
1
108-95-2
625
NO
1.1
ug/L
1
Pyrene
129-00-0
625
NO
1.1
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
1.1
ug/L
1
2,4,6-Trichoorophenol
88-06-2
625
NO
1.1
ug/L
1
PQL = Practical quanntation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40
Where applicable. all soil sample analysis are •eported on a dry weight basis unless flagged with a "W" N = Recoveryis out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia. 5C 29172 [phone] Fax [phone] www.shealylab.com Page: o t v 9
Y Level •I Report v2.1

Client: City of Mount Holly
Description: Effluent
Date Sampled:10/06/2011 0820
Date Received:10/06/2011
Laboratory ID: MJ06055.001
Matrix: Aqueous
Surrogate
o Run 1
/b Q Recovery
Acceptance
Run 2 Acceptance
Limits Q
% Recovery Limits
2,4,6-Tribromophenol
60
41-144
80 41-144
Phenol-d5
52
28-128
58 28-128
Nitrobenzene-d5
48
38-127
64 38-127
2-Fluorobiphenyl
48
37-129
59 37-129
2-Fluorophenol
48
24-127
46 24-127
Terphenyl-d14
24
10-148
31 10-148
ICP-MS
Run Prep Method
1
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
200.2
200.8 1 10/11 /2011 1847 FTS
10/10/2011 1854
69390
2 200.2
200.8 1 10/12/20110349 KJC
10/10/20111854
69390
Parameter
CAS Analytical
Number Method
Result Q
PQL
Units
Run
Antimony
7440-36-0 200.8
0.029
0.001
mg/L
1
Beryllium Arsenic
7440-38-2 200.8
0.0013
0.001
mg/L
2
Cadmium
7440-41-7 200.8
NO
0.0004
mg/L
1
Chromium
7440-43-9 200.8
NO
0.0001
mg/L
1
Copper
7440-47-3 200.8
0.0053
0.005
mg/L
1
Lead
7440-50-8 200.8
0.021
0.001
mg/L
1
Nickel
7439-92-1 200.8
NO
0.001
mg/L
1
Selenium
7440-02-0 200.8
ND
0.005
mg/L
1
Silver
7782-49-2 200.8
0.0033
0.001
mg/L
2
Thallium
7440-22-4 200..8
NO
0001
mg/L
1
Zinc
7440-28-0 200.8
NO
0.0005
mg/L
1
7440-66-6 200.8
0.057
0.01
mg/L
1
POL = Practical quantitation limit B = Detected in the metnod blanA
E = Ouantitation of compountl exceeded the calibration range
ND = Not detected at or above the POL J = Estimated result < POL and > MDL
Where applicable, all soil sample analysts are reported on a ary N = weight basis unless Bagged with a "W" The er between two GC columns exceeds 40°5
= Recovery is out of criteria H = Out of holding time
Shealy Environmental Services, Inc.
Page:
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com v 9
Level 1 Report
rt 2.1

Client:City of Mount Holly
Description: Effluent
Date Sampled:10/06/2011 0820
Date Received;10/0612011
Inorganic non-metals
Laboratory ID: MJ06055-002
Matrix: Aqueous
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 10-204-00-1-X
(Cyanide - To) 10-204-
1 10/13/2011 1122 DAS
10112/2011 0939
69502
1
(Phenolics) 420.4
1 10/11/2011 1037 SMH
10/10/2011 0845
69340
1
(HEM (oil and) 1664A
1 10/17/2011 0920 AWT
69740
Parameter
CAS Analytical
Number Method
Result Q
PQL
Units
Run
Cyanide - Total
57-12-5 10-204-00-1-X
NO
0.010
mg/L
1
Phenolics
420.4
NO
0.020
mg/L
1
HEM (oil and grease)
1664A
ND
4.9
mg/L
1
Volatile
Organic Compounds by GC/MS
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
624
1 10/11/20111300 BM
69436
2 5030E
624
1 10/12/20112149 DLB
69602
Parameter
CAS Analytical
Number Method
Result Q
PQL
Units
Run
Acrolein
107-02-8 624
NO
50
ug/L
1
Acrylonitrile
107-13-1 624
NO
50
ug/L
1
�Benzene
71-43-2 624
NO
5.0
ug/L
1
Bromodichloromethane
75-27-4 624
NO
5.0
ug/L
1
Bromoform
75-25-2 624
9.8
5.0
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 624
ND
Carbon tetrachloride
56-23-5 624
NO
5.0
5.0
ug/L
ug/L
1
1
Chlorobenzene
108-90-7 624
NO
5.0
ug/L
1
Chloroethane
75-00-3 624
NO
5.0
ug/L
1
2-Chloroethylvinylether
110-75-8 624
NO
10
ug/L
1
Chloroform
67-66-3 624
NO
5.0
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 624
NO
5.0
ug/L
2
Dibromochioromethane
124-48-1 624
8.7
5.0
ug/L
1
1,1-Dichloroethene
75-34-3 624
NO
5.0
ug/L
1
1,2-Dichloroethane
107-06-2 624
NO
5.0
ug/L
1
1,1-Di chloroethene
75-35-4 624
ND
5.0
ug/L
1
trans-1.2-Dichloroethene
156-60-5 624
ND
5.0
ug/L
1
1,2-Dichloropropane
78-87-5 624
ND
5.0
ug/L
1
cis-1,3-Dichloropropene
10061-01-5 624
NO
5.0
ug/L
1
+rtrans- 1,3-Dichloropropene
10061-02-6 624
NO
5.0
ug/L
1
Ethylbenzene
100-41-4 624
NO
5.0
ug/L
1
Methylene chloride
75-09-2 624
NO
5.0
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5 624
ND
5.0
ug/L
1
Tetrachloroethene
127-18-4 624
NO
5.0
ug/L
1
Toluene
108-88-3 624
ND
5.0
ug/L
1
1,1,1-Trich loroethane
71-55-6 624
ND
5.0
ug/L
1
1,1,2-Trichloroethane
79-00-5 624
NO
5.0
ug/L
1
PQL = Practical quantitation limit E = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the PQL J = Estimated result c PQL and > MDL P = The RPD between two GC columns exceeds 40%
Where applicable. all soil sample analysis are reported on a dry weight basis unless flagged with a "W" K = Recoveryis out of criteria H =Out of holding time
Shealy Environmental Services, Inc.
Page: 8 106 Vantage Point Drive West Columbia. SC 29172 [phone] Fax [phone] WWW.sheal Y lab.com LeReport
Level 1 Repov 9
v2.1

Client: City of Mount Holly
Description: Effluent
Date Sampled:1010612011 0820
Date Received:10/06/2011
Laboratory ID: MJ06055.002
Matrix: Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method
1
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
5030B
624
1 10/11/20111300 BM
69436
2 5030B
624
1 10/12/20112149 DLB
69602
Parameter
CAB Analytical
Number Method Result Q
PQL Units Run
ene
79-01-6 624 ND
5.0
Vinyl orlon
Vinyl chloride
ug/L 1
75-01-4 624 ND
5.0 ug/L 1
Surrogate
9
Q
o Run 1 Acceptance Run 2 Acceptance
/o Recovery Limits Q % Recovery Limits
1,2-Dichloroethane-d4
104 52-138 98 52-138
Bromofluorobenzene
98 70-147 101 70-147
Toluene-d8
98 76-125 99 76-125
PQL = Practical quantitation limit B = Detected in the memod blank
E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the PQL J = Estimated result c PQL and > MDL
Where applicable, all soi! sample analysis are reported on a dry weight basis unless flagged with a "W" P =The er between two GC columns exceeds 4095
N = Recovery is out of criteria h = Out of holding time
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia. SC 29172 [phone] Fax [phone] www.shealylab.com Page: 9 of 9
Level 1 Reponv2.1

ATTACHMENT V
Toxicity Reports

Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:7/31/2014
Facility: Mt, Holly WWTP
Laboratory: Pace An,
x
of CAeratorjin Asponsible Charge
X k_ i -�J�
Signature of Laboratory Supervisor
NPDES # NC00 21156 Pipe #: 001 County: Gaston
comments I_;3A-W-, 7,Lk- nl�2_
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
I✓C DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Test Initiation DatelTime 7/22/2014 / 16:10 Avg Wt/Surv. Control 0.421
% Eff. Repl.
1
2
3
4
Control Surviving#
10
9
9
10
Original #
10
10
10
10
Wt/original (mg) 1
0.451 1
0.378 I
0.342
0.431
0 Surviving #
Original #
WVoriginal (mg)
4.5 Surviving #
Original #
Wt/original(mg) (mg)
© Surviving
Original #
Wt/original (mg)
1=l Surviving #
Original #
Wt/original (mg)
10
9
9
6
10
10
10
10
0.495
0.383
0.455
0.397
9
10 10
8
10
10 t0
10
0.434
0.396 0.438
0.386
10 9
10
10
10 10
10
10
0.464 0.454
0.444
Al i
10
7
10
9
f0
10
10
10
0,487
0.365
0.510
Al
i 2 Surviving #
7
9
9
.8 �
Original #
10
i0
10
10
Wt/original (mg)
0,415
0.466
0.397
0.393
ster Quality. Data
Day
Control
0
1
2
3
pH (SU) EnIUFin
7.6 / 8.0
7.7 / 7.5
7.8 / 7.7
7.7 ! 7.9
DO (mg/L) IniUFin
7.7 / 7,7
7.8 / 6.018.0
1 6.5
8.0 / 7.5
Temp (C) IniVFin
24.8 / 24.7 24.6 124,8 24.9 / 24.9 24.5 / 24.7
°i° Survival 95.0
Avg Wt (mg) 0.401
%Survival 85.0
Avg Wt (mg) 0.433
°h Survival 92.5
Avg Wt (mg) 0.414
%Survival 97.5
Avg Wt (mg) 0.444
% Survival 90.0
Avg Wt (mg) 0.447.
%Survival 82.5
Avg Wt (mg)
C
High Concentration 0 1 2 3 4 5 6
pH (SU) tniUFin
DO (mglL) IniVFin
Temp (C) IniVFin
Sample 1 2 3
Collection Start Date
Grab
Composite (Duration)
Hardness (mg/L)
Alkalinity (mg1L)
Conductivity (umhos/cm)
Chlorine(mg/L)
Terre, at Receipt (°C)
7/20/2014
7/22/2014
7/24/2014
24.00
24.00
24.00
39.00
39.80
35.60
45.00
48.00
� 45.80
1049
973
993
<0. t
<0.1
<0.1
0.3
1,6
I 2.6
Dilution H2O
Hardness (mglL)
39.00
Alkalinity (mg/L)
28.00
Conductivity (umhoslcm)
168.E
7.4 / 7.9
8.0 / 7.5
7.8 / 7.7
7.7 / 7.8
7.9 / 7.417.7
! 7.8
7.6 / 7.5
7.7 / 7.7
7.7 I 7.2
7.8 / 6.2
7.1 / 7.6
8.2 1 6.3
8.1 ! 7.9
8.0 I 7.4
24.9 1 24.8
25A / 24.9
24.fi / 24.7
24.8 / 24.8
2.1 1 24.6
2b.2 ! 24.7
24.8 / 24.7
Normal
Hom. Var.
NOEC
LOEC
ChV
Method
Survival
Growth
ire:
12
12
>12
>12
>12
>12
Dunnett's
Dunneirs
Test Organisms
Cultured In -House
Outside Supplier
Hatch Dater
Hatch Timer, d�a
Overall Result
ChV >12°k
Stats
Survival
Growth
irOnC.
Critical
Calculated
critical
Calculated
3
2.41
1.211
2.41
-1.025
4.5
2.41
0.327
2.41
-0.417
6
2.41
-0.375
2.41
-1.402
9
2.41
0.594
2.41
-1.49
12
2.41
1.67
2.41
-0.553
DWQ Form AT-5 (7/04)

Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:8128/2014
Facility: Mt. Holly WWTP NPDES # NC00 21156
*Laboratorv: Pace Analvtical - Raleigh
x «.,. Si �ture of 0
k7offn Responsible Charge
x
Signature of Laboratory Supervisor
!MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Pipe #: 001 County: Gaston
Comments, t�C X- ZZ-(
Test Initiation Date/Time 8/19/2014 / 15:00 Avg Wt/Surv. ControlL 0.575
% Eff. Repl. 1 2 3 4
FC_on_t_ro__1j Surviving #
Original #
Wt/original (mg)
10
10
10
9
10
10
10
10
0.589
0.548
0.547
0.554
Test Organisms
7 Cultured In -House
% Survival 97.5 i✓ Outside Supplier
Avg Wt (mg) 0.560
0 Surviving #
10
10
10
10
% Survival 100.0
Original #
Collection Start Date
Grab
Composite (Duration)
Hardness (mg/L)
Alkalinity (mg1L)
` Conductivity (umhos/cm)
Chlorine(mg/L)
I Temp. at Receipt (°C)
10
10
10
10
0.595
0.486
0.607
0.549
10
10
10
10
10 10
10
7.8 / 7.6
7.7 / 7.6
7.7 / 7.6
7.7 / 7.6 7.8 / 7.4
7.9 / 7.8
7.9 / 7.5
7.8 / 7.6
7.9 / 7.3
7.9 / 8.1
8.5 / 7.0 8.1 / 6.8
8.0 ! 7.7
8.2 / 7.6
24.9 / 24.7
25.0 / 24.9
25.0 / 24.7
24.8 / 24.8 25.0 / 24.7
24.9 / 24.7
24.8 / 24.8
8/17/2014
8/19/2014
8/21/2014
24.00
24.00
24.00
35.40
36.40
37.00
51.00
52.50
51.00
978
963
945
<0.1
<0.1
<0.1
1.3
2.2
3.1
Dilution H2O
Hardness (mg/L)
39.00
Alkalinity (mglL)
28.80
Conductivity (umhoslcm)
206.3
Normal
(f -1
(f ✓ I
Hom. Vac
(71
Hatch Date:
Hatch Time: I � ' Lis
Overall Result
ChV >12%
Stats
Survival
Growth
Conc.
Critical
Calculated
Critical
Calculated
3
10
20
2.41
-0.174
4.5
10
20
2.41
0.009
6
10
20
2.41
0.096
9
10
20
2.41
-0.043
12
10
18
2.41
0.739
10 10
10
10
0.512 0.607
0.570
0.569
DWQ Form AT-5 j 1,G4)

Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:4/30/2014
Facility: Mt. Holly WWTP
Laboratory: Pace Analytical -
NPDES # NC00 21156 Pipe #: 001 County: Gaston
X YJ -
Sigeture f Opera in sponsible Charge
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Test Initiation Date/Time 4/22/2014
% Eff. Repl.
FC-o-ntro-T11 Surviving #
Original #
Wt/original (mg)
0 Surviving #
Original #
Wt/original (mg)
4.5 Surviving #
Original #
Wt/original (mg)
© Surviving #
Original #
Wt/original (mg)
Surviving #
Original #
Wt/original (mg)
12 Surviving #
Original #
Wt/original (mg)
Quality Data
Control
PH (SU) Init/Fin
DO (mg/L) Init/Fin
Temp (C) Init/Fin
1
(Comments WO# 9219-8333 1
/ 4:14pm Avg WUSurv. Control 1 0.430
2 d
10
10
1 10
9
10
10
10
10
0.430
0.391
0.435
0.418
10
10
10
10
10
10
10
10
0.414
0.369
1 0.419
1 0.442
10
10
10
10
10
10
10
10
0.362
0.318
0.434
0.418
10
10
1 10
1 10
10
10
1 10
10
0.517
0.414
1 0.404
0.348
9
1 10
10
10
10
1
10
10
10
0.351
1 0.376
0.420
0.389
10
10 1 10
10
10
10 10
10
0.392
0.465 1 0.438
1 0.414
% Survival 97.5
Avg Wt (mg) 0.419
% Survival 100.0
Avg Wt (mg) 0.411
% Survival 100.0
Avg Wt (mg) 0.383
% Survival 100.0
Avg Wt (mg) 0.421
% Survival 97.5
Avg Wt (mg) 0.384
% Survival 100.0
Avg Wt (mg) 0.427
Day
0 1 Z e
7.9 / 7.6
7.7 / 7.7
7.6 ! 7.7
1 7.3 / 7.6
17.6 / 7.5
17.7 / 7.3
17.6 / 7.6
8.2 / 7.6
7.9 / 7.3
8.4 / 7.7
1 7.5 / 7.6
1 7.7 / 6.5
1 7.8 / 6.9
1 7.5 / 7.2
24.7 / 24.6
24.6 / 24.8
24.9 / 24.7
24.6 / 24.6
24.8 / 24.5
24.8 / 24.7
24.7 / 24.8
High Concentration 0 1 2 3 4 5 6
PH (SU)Init/Fin 7.5 / 7.5 7.7 / 7.7 7.5 / 7.6 7.3 / 7.617.5 / 7.417.4 / 7.3 7.5 / 7.6
DO (mg/L) Init/Fin 8.0 / 7.5 7.6 / 7.4 8.3 / 7.5 7.6 / 7.61 7.5 / 6.7 7.7 / 7.31 7.6 / 7.5
Temp (C) Init/Fin 24.6 / 24.7 24.7 / 24.8 24.5 / 24.6 24.9 / 24.8 24.7 / 24.6, 24.8 / 24.5 24.9 / 24.9
Sample
Collection Start Date
Grab
Composite (Duration)
Hardness (mg/L)
Alkalinity (mg/L)
Conductivity (umhos/cm)
Chlorine(mg/L)
Temp. at Receipt (°C)
Dilution H2O
Hardness (mg/L)
Alkalinity (mg/L)
Conductivity (umhos/cm)
1 2 3
4/20/2014
4/21/2014
4/24/2014
24.00
24.00
24.00
43.00
43.60
42.40
37.50
40.50
57.00
576
693
807
<0.1
<0.1
<0.1
0.3
1.1
0.9
39.60
29.00
167.2
Test Organisms
la Cultured In -House
7 Outside Supplier
Hatch Date: f
Hatch Time:
Survival
Growth
Overall Result
Normal
F1
P, I
ChV >12%
Hom. Var
r'1
1r1
NOEC
12
12
LOEC
>12
>12
ChV
>12
>12
Method
Steels
Dunnett's
Stats
Survival
Growth
Conc.
Critical
Calculated
Critical
Calculated
3
10
20
2.41
0.249
4.5
10
20
2.41
1.177
6
10
20
2.41
-0.075
9
10
18
2.41
1.144
12
10
20
2.41
-0.29
DWQ Form AT-5 (1104)

Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test Date:2/27/2014
Facility: Mt. Holly WWTP NPDES # NC00 21156 Pipe #: 001 County: Gaston
Laboratory: Pace Analytical - Raleigh Comments WO# 92189835
x
Sig!- .ur of erator i spon a Charge
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Test Initiation Date/Time
2/18/2014
/ 2:22pm
Avg WUSurv. Control 1 0.692
% Eff. Repl.
1
2
3
4
Control Surviving #
% Survival 100.0
Original #
WUoriginal (mg)
Avg Wt (mg) 0.692
0 Surviving #
% Survival 100.0
Original #
Wt/original (mg)
Avg Wt (mg) 0.635
4.5 Surviving #
% Survival 100.0
Original #
WUoriginal (mg)
Avg Wt (mg)0.655
© Surviving #
10
% Survival 100.0
10
10
10
Original #
10
10
10
10
Wt/original (mg)
0.636
0.660
0.579
0.674
Avg Wt (mg) 0.637
Surviving #
10
% Survival 100.0
10
10
10
Original #
10
10
10
10
Wt/original (mg)
0.762
0.595
0.646
j 0.595
Avg Wt (mg) 0.650
12 Surviving #
10
% Survival 100.0
10
10
10
Original #
10
10
10
10
Wt/original (mg)
0.687
0.740
0.684
0.662
Avg Wt (mg) 0.693
iter Quality Data
Day
Control
0
1
2
3
4 5 6
pH (SU) Init/Fin
DO (mg/L) Init/Fin
Temp (C) Init/Fin
High Concentration
pH (SU) Init/Fin
DO (mg/L) Init/Fin
Temp (C) [nit/Fin
Sample
Collection Start Date
Grab
Composite (Duration)
Hardness (mg/L)
Alkalinity (mg/L)
Conductivity (umhos/cm)
Chlorine(mg/L)
Temp. at Receipt (°C)
Dilution H2O
Hardness (mg/L)
Alkalinity (mg/L)
Conductivity (umhos/cm)
10
10
10
10
10
10
10
10
0.704
0.632
0.537
0.893
10
10
10
10
10
10
10
10
0.582
0.609
0.729
0.618
10 10
10
10
10 10
10
10
0.794 0.612
0.636
0.579
8.0 / 7.6
7.6 / 7.5
7.8 / 7.7
7.7
7 / 7.5
7.7 1 7.7
7.7 J 7.4
7.9 / 6.5
7.6 / 6.9
8.0 1 6.8
7.9
#25.0)
5 / 6.2
7.9 / 6.4
7.2 / 6.4
24.8 / 24.9
25.2 / 25.1
24.9 / 25.0
25.1
.1 / 25.0
24.7 / 24.9
25.0 / 24.9
0 1 2 a s a
7.8 / 7.4
7.6 / 7.4
7.6 / 7.6
7.6 / 7.1
7.5 / 7.4
7.6 / 7.6
7.7 / 7.3
8.1 / 7.2
7.2 / 6.1
7.6 / 7.0
8.1 / 6.0
7.5 / 5.3
7.3 / 6.5
7.5 / 6.2
24.9 / 25.0
25.1 / 25.0
24.7 / 24.$
25.0 / 24.9
25.2 / 25.1
Z4.8 ! 24.9
25.1 ! 25.0
1 2 3
2/16/2014
2/18/2014
2l20/2014
24.00
24.00
24.00
44.00
45.00
34.00
29.00
43.00
65.50
595
688
675
<0.1
<0.1
<0.1
1.2
1.0
1.4
43.00
26.50
145.9
Test Organisms
T_ Cultured In -House
7 Outside Supplier
Hatch Date:
Hatch Time: it::;- W, jk'N.
Survival
Growth
Overall Result
Normal
((r"I
G°I
ChV >12c1�
Hom. Var.
ri
�j'v`1
NOEC
12
12
LOEC
>12
>12
ChV
>12
>12
Method
Steel's
Dunnett's
Stats
Survival
Growth
Conc.
Critical
Calculated
Critical
Calculated
3
10
18
2.41
0.93
4.5
10
18
2.41
0.591
6
10
18
2.41
0.885
9
10
18
2.41
0.685
12
10
18
2.41
-0.029
uwu rorm H 1-0 I 7/ua,1

ATTACHMENT VI
Jadco-Hughes Site Information

4215-1 Stuart Andrew Blvd. Charlotte, North Carolina 28217
Telephone: [phone] Facsimile: [phone]
www.CRAworld.com
CONESTOGA-ROVERS
& ASSOCIATES
January 15, 2013
Mr. Jonathan Jordan
Utilities Supervisor
City of Mount Holly
P.O. Box 406
Mount Holly, North Carolina
28120
Dear Mr. Jordan:
Re: 2013 Annual Reporting of Discharges
Jadco-Hughes Site (Site), Gaston County, North Carolina
Reference No. 003669-95
On behalf of the Jadco-Hughes Site Potentially Responsible Party (PRP) Group, CRA submits this annual
letter report in accordance with the May 15, 2000 agreement between the PRP Group and the City of
Mount Holly (City). The reporting period is for the year 2013.
A total of 13,763,997 gallons of treated water were discharged to the City Publicly Owned Treatment
Works (POTW) in 2013. The water was discharged at a rate not greater than 75,000 gallons per day.
CRA collected composite sample of the effluent on December 19, 2013 for compliance monitoring. The
total volume discharged during the 24-hour composite sampling period (from December 18 to 19, 2013)
was 29,566 gallons. CRA analyzed the composite sample for metals, ammonia (NHA and total
suspended solids (TSS). CRA also collected a grab sample of the effluent on December 19, 2012 and
analyzed it for volatile organic compounds (VOCs), oil and grease, polychlorinated biphenyls (PCBs), and
cyanide. All parameters were within the discharge limits.
CRA also collected a sample for biochemical oxygen demand (BOD); however, the laboratory incorrectly
analyzed the sample for carbonaceous BOD. CRA has collected another sample for BOD analysis and will
submit the data to the City when the laboratory provides the data to us.
As discussed by telephone on January 14, 2014, CRA has also collect samples for the full list of metals
and base/neutral/acid compounds listed in the City's letter dated October 4, 2013. These parameters
were listed in the original permit; however, because there were no issues with exceeding the discharge
standards and based on discussions with the City and receipt of the City's approval to do so, the metals
list was reduced and BNAs were no longer analyzed. As discussed, CRA will analyze for these
parameters until further discussions with the City's consultant, United Water, take place.
The laboratory analytical results for December 19, 2013 are summarized in Table 1.
Equal
Employment Opportunity
Employer
ntc-UnEn vvurA"t run
ISO 9001
ENGINEERING GESIGN

CONESTOGA-ROVERS
& ASSOCIATES
January 15, 2013 Reference No. 003669-95
-2-
The next discharge monitoring event will be performed in December 2014. We will inform you of the
monitoring schedule one week prior to commencing the activities.
If you have any questions, please do not hesitate to contact me at [phone].
Yours truly,
CONESTOGA-ROVERS & ASSOCIATES
Colleen Dietrich
CD/cb/2
Encl.
cc: James Friday, City of Mt. Holly
Ralph Douglas, City of Mt. Holly
Jadco-Hughes Technical Committee
Patricia Barmeyer, King & Spalding
Stephen Quigley, CRA
John Uteck, CRA

Page 1 of 2
Parameter (1)
Flow (2)
BOD
TSS
NH3
Metals
TABLE 1
ANALYTICAL RESULTS FOR 2013 ANNUAL EFFLUENT MONITORING
JADCO-HUGHES SUPERFUND SITE
GASTON COUNTY, NORTH CAROLINA
Discharge
Limits
0.075 MGD
300 mg/L
350 mg/L
25 mg/L
Treated Water To Sewer System
SAMPLE ID: GW-3669-JU-121913-036
Lab Results
29,566 gal
(6)
< 5 mg/L
< 0.05 mg/L
Converted Data
Arsenic
0.1 mg/L
<
0.005 mg/L
Cadmium
0.02 mg/L
<
0.005 mg/L
Chromium
0.5 mg/L
<
0.01 mg/L
Cyanide
0.5 mg/L
<
0.005 mg/L
Lead
0.05 mg/L
<
0.005 mg/L
Nickel
0.5 mg/L
<
0.005 mg/L
Base Neutral Compounds (3)
1,2,4-Trichlorobenzene
0.0759 Ibs/day
<
1 µg/L
0.0000 Ibs/day
1,2-Dichlorobenzene
0.0234lbs/day
<
1 µg/L
0.0000lbs/day
1,3-Dichlorobenzene
0.0146 lbs/day
<
1 µg/L
0.0000 lbs/day
1,4-Dichlorobenzene
0.0651 Ibs/day
<
1 µg/L
0.0000 Ibs/day
Volatile Compounds (3)
1,1,1-Trichloroethane
0.0209 Ibs/day
<
1 µg/L
0.0000 Ibs/day
1,1,2,2-Tetrachloroethane
0.0001 Ibs/day
<
1 µg/L
0.0000 Ibs/day
1,1,2-Trichloroethane
0.0009 lbs/day
<
1 µg/L
0.0000 lbs/day
1,1-Dichloroethane
0.0004lbs/day
<
1 µg/L
0.0000lbs/day
1,1-Dichloroethylene
0.0058 Ibs/day
<
1 µg/L
0.0000 Ibs/day
1,2-Dichloroethane
0.0822lbs/day
5 µg/L
0.0012lbs/day
1,2-Dichloroethylene (total)
0.5342 Ibs/day
110 µg/L
0.0271 Ibs/day
1,2-Dichloropropane
0.0001 Ibs/day
<
1 µg/L
0.0000 Ibs/day
1,3-Dichloropropylene (total)
0.2606 Ibs/day
<
1 µg/L
0.0000 Ibs/day
2-butanone
23.8207 Ibs/day
<
5 µg/L
0.0000 Ibs/day
2-hexanone
0.3753 Ibs/day
<
5 µg/L
0.0000lbs/day
CRA 003669-Jordan-3-Tl

Page 2of2
TABLE 1
ANALYTICAL RESULTS FOR 2013 ANNUAL EFFLUENT MONITORING
JADCO-HUGHES SUPERFUND SITE
GASTON COUNTY, NORTH CAROLINA
Treated Water To Sewer System
Discharge
SAMPLE ID: G W-3669 JU-121913-036
Parameter (1)
Limits
Lab Results
Converted Data
Acetone
11.4558 Ibs/day
<
5 µg/L
0.0000 Ibs/day
Benzene
0.0229 Ibs/day
<
1 µg/L
0.0000 Ibs/day
Bromodichloromethane
0.1835 Ibs/day
<
1 µg/L
0.0000 Ibs/day
Bromoform
0.1501 Ibs/day
<
1 µg/L
0.0000 Ibs/day
Bromomethane
1.0425 Ibs/day
<
1 µg/L
0.0000 Ibs/day
Carbon Tetrachloride
0.5967 Ibs/day
14 µg/L
0.0035 Ibs/day
Chlorobenzene
0.0121 Ibs/day
<
1 µg/L
0.0000 Ibs/day
Chloroethane
0.0033lbs/day
<
1 µg/L
0.0000lbs/day
Chloroform
1.4249 Ibs/day
18 µg/L
0.0044 Ibs/day
Dibromochloromethane
0.1334lbs/day
<
1 µg/L
0.0000 Ibs/day
Ethylbenzene
0.0938 Ibs/day
<
1 µg/L
0.0000 Ibs/day
Methyl Chloride
1.0425 Ibs/day
<
1 µg/L
0.0000 Ibs/day
Methylene Chloride
0.2189 Ibs/day
<
1 µg/L
0.0000 Ibs/day
Tetrachloroethene
0.00531 Ibs/day
3.9 µg/L
0.0010 Ibs/day
Toluene
1.4478 Ibs/day
<
1 µg/L
0.0000 Ibs/day
Trichloroethylene (7)
0.0138 Ibs/day
48 µg/L
0.0118 Ibs/day
Vinyl Chloride
0.4775 Ibs/day
<
1 µg/L
0.0000 Ibs/day
Xylene
0.1147 Ibs/day
<
15 µg/L
0.0000lbs/day
Other Parameters
Polychlorinated Biphenyls (3), (4) 0.0010 Ibs/day < 0.53 µg/L 0.0000 Ibs/day
Oil and Grease 100 mg/L < 4.4 mg/L
pH 5 - 11(5) 8.31
Notes:
< Below detection limit. The quantity shown is the detection limit.
(1) Discharge limit is the concentration specified in Attachment I of the October 3, 2013 City of Mount Holly letter.
(2) The converted data is based on the flow rate shown.
(3) The effluent limitation is the daily maximum agreed to by City of Mount Holly (letter dated July 12, 2011).
(4) Detection limit for Total PCBs shown is detection limit for each of the individual PCB Aroclors.
(5) Standard Units.
(6) Laboratory error. CRA will resample and submit data to the City.
(7) Discharge limits for tetra chloroethene and trichloroethene are based on October 3, 2013 letter from City;
however, City previously agreed to limits of 0.1068 and 0.7475 Ibs/day, respectively (letter dated November 7,199
CRA 003669-Jordan-3-Tl

ATTACHMENT VII
Triangle Texaco Site Information

lIItlllkkk.tl-1:11 f u1 1111
A. 1't'1 tittl -illllllt':Ifftitl
f't WF Il I <t .1
MaM h 'J. i=+t7:aFtU P EInck' t. ^.e1F
Pr ncipai Engine&' C pia t ;;W,
4, 394-siat�a Plume
'Cat t;_ia 2?3 'tee+ =,bv .,tiar,
mizioiana,ix ss lQlden��Ir�eenng cUlr - pk.elly s:tlel, �r:g:ne g.�c•
' L"-: 'wjr--ss of f3.:1€.
2�1 Rf. Main Strut 430' Tacgar
` Mount 1-IeillG ";``` NC '}" 28120 Charlotte Ail,_,' 28086
u Intormation pro» ided hx Nou on this questionnaire series two funetinris:
The information Is Cued to determine if tour ':tt:lit' Ir.,,' ari
scr 1"retreat tl en: i'eriZ'llt } li, t'' iOr tnt djE .
%UsLevlaLcr its the to aEi ester
It an Industrial User Pretreatment Permit (it 1P) is required, this
surve\ serves as the application for an :s°i#1ta:o,'lily t_ sn
Pretreatment Permit (IL'P).
RegtieStS t01' Colltwential tre::tinent t)t 1nicin taticin protldc:.: on this toritl ,11.111 ht` L'i'4,;r.'46
1, •iiet4utr- ,13ecified in 40 C:FR Part In accordance with Title yfi
ftr_u1,sLi..',�• Part -Ifs',. Section 403,14 anl.1 the Locai (_;se "I'oovin, :,Y t.i1. ,nti r:113tir,n
and data rwo\ ided III thtS tfLlestionnaire \which Identities the content. tolUf1W and ire L1C,1CN Of
JisctlarL,e shall tic a,,ailable to use pLtiillb V, Itf1.-,Lit restriction
-1-1'SPa IL, tai by zovjieV ti% WI 3Uftl,'rized official t}t Lt)UT tiriti. aN dr°finea m t6,C LUC31 7k'«rr L se t trdldl:t 176Z'. ,r, Si: ,I I sitel
Complet,oll of this tern,
�crtlfti 1.i1u►' tnii, I} _ �i.
C1.V1 rc. „IlcSr m+
hLJ k ,llii : I' i.'cl i' _ALti.i,LI..IL ,111 'l..••NI,.VtI•'I 1. i ililti. I%' hIa111 . t 'I
tio!.aia c t1 .1t1 ii•
. tlr.IICrI.II 1:1. lu.'I'ln., Itl[ 1.111.•! II' il1I11+ 1 lin +tl,t tfr+t~r ]nil
L7
L7Cile t. .LI'c1w. .,L4lli.1.'. S1Iw-,.c}llli9llisAill .: ..1!-_ tiV_. ?...� t �
ur+1�1 Fn1, tial tllfl?B'• i!i li. 1ll�ltl3tn` the j?i}�tiPtillll. ilt :Ilit ::tu ;lj�tr crsTttitl+l i'}f
Klli�ll L
jj •f. -
ICN-
til�•l,.t�1,l:
I'..�C

Industrial User Wastewater Survev
& Permit Application
PART I, GENERAL
INFORMATION:
Prop ide a brief narrative description of the type of business, manufacturing
processes. or service activities ' ow Firm conducts at this site.
Shield Engineering, Inc. is an environmental consulting and engineering
firm contracted with a responsible party who is directed by the NCDENR
to abate, assess, and remediate soil and groundwater contamination
resulting from a previous underground storage tank release.
List the primary products produced at this facilit\':
No products are produced at this site. Environmental remediation
activities are anticipated to result in recovered petroleum impacted
groundwater from several recovery wells.
1_ist rate material, and procc-is additives used:
No raw materials or process additives are used
4. .are biocides added to any water discharged try th.: P01 XN
if Nes describe:
ti�CS
X
Describe weekly produrti:�i� sehzdulc . including shins worked per day.
employees ,rer shift. and prirxard operation during_'hift.
Automated equipment will operate 24 hours a day, with periodic maintenance
visits by Shield Engineering, Inc. technicians. Shield Engineering, Inc.
estimates recovery of up to approximately 40,000 gallons of petroleum
impacted groundwater per week.
b. Productiun process is: Check. ;fall continuous X
Check. if all batch
If both olea5e enter. "u con1i11U()US = I Batch = 0/
Pane 2 of 17

Industrial User Wastewater Survev
& Permit Application
PART I, GENERAL INFORMATION
(cont):
Does production vary significantl\ ( ?U Uo) bNseason. Describe.
Possibly. Production may .ary due to seasional groundwater Yes x
highs and lows. No
$. Are am, significant 1 +-- 20 %) :hana , ir, production that will affect wastewater
discharge expected in the next 5 years. If yes. please describe.
Yes, groundwater remediation activities are expected to be Yes I x
completed within 2-4 years of remediation system operation. No
9. List all current e\,aste haulers. Gi\ c iiani . address. phone numbers.
volume and materials hauled oft.
Not applicable.
10. ,attach a copy of laborator-, analyses performed in the last year on the
.%a,tCwater discharge(s) fton-, \our i'acilities. Summarize data on the
attached Data Summate Form.
See Attached
11. ,attach sketch or schematic showin`, sampling points and all connections
to the scv er.
See Attached
12. Complete the Waste,,�ater Pollutants Checklist attached to this Survey,
See Attached
Page 3 of 17

Do you hare. or ha%e you ever applied for. been issued. or been denied
an NPDES permit to discharge to the surface .raters or ;t,)Q-n severs of
North Carolina? If ties, list all other NPDES permits, permit numbers,
dates, and names used to a ely for them, or reason deniecl.
Bantam Mart, NCG510464. 10/18/11, Petroleum World, Inc.
Danieltown. NCG510245.
14.
Industrial User Wastewater Survey
& Permit Application
PART 1, GENERAL INFORMATION
(cons):
la
ed 4/26/05. Petroleum World. I
Yes x
No
Do vou have. or have you :v.er applied for or been issued an Industrial
�L_ser Pretreatment Permit Oup) to discharge Wasttwater to the sewer
eilectian aystetlt. if yes. list ali other II.::P permits. permit numbers.
dates. and names used to a -d% for therm.
If yes Permit
Ir\es Penmt datc..tpp;.�ant•noxte
Yes
N�) X
15. Do you have. or have you cy r applied for or been issued any t)ther
En%ironmental Permits (for example: 3ir'. f2i'fl.A. <arounclwater.
stormwater. general. Non -Discharge, septic tank. etc.). If yes. list all
other permits. permit numbers. Jatcti. and names used to apply for them.
It xis Permit IvPC d_ date. applicara: mmne
It `e. Permit i%,v 9 .late. applicant
a Nes, ror. r..: 1'. l-. • .iatc. appncant : i
Yes
No X
16. is a Spill Prevention Control and Countermeasure (SPCC') Pljn
Prepared for this facility" €f yes. please attach a copy
17. Is a Spill 'Slug Ctlntroi Plan required b\ the Po'l �l . prepared tor- this
facility`'
Yes
No x
Yes
\.o x
Pa<ae 4 of 17

Industrial User Wastewater Survev
& Permit Application
PART I_, C ENERAL. INFORMATION
(Cont):
18. Du %ou have anti undcrgrotund storage tanks at your facilih'? if vrs. list
contents and volume ofe€ach tart!;.
No underground storage tanks to be used on site. Yes
No x
i9_ Do you have anv above ground stowgc tanks at your facility`? If des. for
each tank, list the contents. volume. whether the tank has an} spill
prevention or containment devices. suci7 as dikes. and procedures for
draining an,, containment devices.
I -
Yes I x 4� of Tanks, 1
No tanks on site at present time. Possible 3,000 to 5,000 gallon No
double -walled polytank for temporary site storage prior to
discharge may be installed if needed as part of proposed ground-
water recovery system.
I'a- ',"of 17

al�lLll1�.� i I X
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r
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v
VaII.,UllIs
.Is
are
XI
palll, iuZ-)
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pr
Q
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3
L.
,1
qd
4-0rr
Qj
r1
i 4
®
."
e i
y
J
Li
1
0
:I

Industrial User Wastewater Survey
& Permit Application
PART III, PRETREATMENT FACILITIES:
Are there any pretreatment dc�, ices or processes used For treating w asteN\ titer
before being discharged to the seaea'' Check all that are present. and describe.
tic, pretreatment facilities x
I
Flow equalization
Aerated equalization =-..
NUN -Aerated equaiizttion => 1 0.005 MG
Total volurrlr ol-equalization
(million gal.) =-1 0.005 MG
I
Activates ( arbon
Yes
No -� Describe anyit' present.
3.
Activated 5iuct,,e
Yes
No II X 1
4.
.air Siripping
Yes � �
No x f
5.
CentrifLigation
Yes
\�> x
6.
Chemical Precipitation
Yea
NO + X
7.
Chlorination
Yes �^
No
8.
Cyanide Destruction
Yes
Not x
a.
Cyclone
Yes �—
No
10.
F loxation
Yes i i
No
1 i.
Fhtraiion
Yeses +
No x
I^_.
;:locctr•:ativ!j
Yes I
No x
13.
Grea,e Tr,tp
Yes
1.
Grit ftentu;;I
Yes I
\u x
15.
lor. i'u'i;an,e
Yes L
No i x
16.
leutraiite. ,�11 adjust
Yes �^
Vic;
1
Other 13iaiowi:,iE I reatment
Yes 1�1
t,o x
1 S.
Ozonatron
Ye,
\o
14.
Reverse Osmosis
Yes
No
20.
Screenim,
Y'>,
x
Rio =
1.
Sedflnentatio3;
Yes
�o
22.
Septic Tank
Yes
No
23.
Silver Recover\
Yes
No Ix
'_=t.
Solvent Separation
Yes
No x
'_?.
Spill protection
Yes x
No
List any others.
Pa,e 7 of I

Industrial User Wastewater Survey
& Permit Application
PART IV, CATEGORICAL INrFORMATION:
When «ere operations started at this facilite
Facility start up date I N/A
The facility is anticipated to start operation in April of 2014.
List all Standard Industrial Classification (SIC') codes for %our facilitri.
.(.here m<t% be found on State Unernpioymerit iSorms. tax forms. r
accountin , records. or 1-rom the Chamber of(' ommerec.
Environmental remediation / clean-up
activities at a former Leaking UST site.
Has this facility ever been considered a ( a.e`,oricad industrial User
(CIU) as described by the Code of Federal Re,_,ulatiorts (40 C'FR)'
If' yes. Give complete 40 C'FR number =>
4 Are any other facilities owned and/or operated by yur comny pa
permic,
tted as Categorical Industrial Users (CIUs) as described b'\ the
Code of Federal Regulations (40 CFR)'?
Yves please give name(s). location. and 40 CFR number
No X
Yes
Noi X
huge 8 of 17

Industrial User Wastewater Survey
& Permit Application
PART IOC, CATEGORICAL INFORMATION: (continued)
5. Check an} activities listed belo« that are perfornied at `our facilitx:
Check 40 Industrial Activity I Check 40
belovN CM-belo" j C:FR# Industrial Activity
467
Aiunlinuul 1`01,111im,
42-1
Ashe,tos M:.ulufa:turilt,-
467
flatter\ Manufs,cturing
431
i3uildcr, paper & board mills
407
Canned A piescmed fruits e`_=
408
Canned & pr;:semec! seatood
458
Carbon olazK \-tantltacturing
411
Cernem \tanutitcturin:,)
434
Coal Mininc
465
Coil Coatnlu
468
Forrlona,
405
Dair. 4a1aduAts pl-O:LSsin
460
1.Icrrr. a. etcarollie ttahotleitt
•457
1:xpio�E�;s Masyuta;turiilg
412
FcedL is
424
Ferro alias �tanuta tuiinu
418
Fertihtcr \lanufaeturine,
464
Foundries. A fetal Mold & Casting
426
Glass t'lan ri'a:tllrtltg
40i5
gran. mills
454
Gutll 1\ c +d Chemicals Alt;,.
460
Hospitals
447
ink t6rnluiatim-,
415
tnon,anic ch,;iinicjl \'lanufacturim,
420
Iton & St el Manufacturing
425
Leather 4-a:lniilu & Finishinw
Meat products
Metal finishing
Metal molding and castin«
Miloeral refining and processing
\,�n'crrous Mrtai, burro & Powders
\onlerruus \1ctals Vlarlutacturing
OC PSF, Omni: Chemicai,, Plastics,
K Synthetic Fiber Manufacturing
335 Oil K act> <xtractiurl
440
'rilc.niinlll and
46
�'alnt form' iatillL
1
i-�
4 4.c
Davin_ and roohn materials \1fg.
455
Pesticiov Manutacturin''•
419
Petroleum Refining-
4,9
Pharinacettalcal Manufacturing
422
Phosphate "vlanufacturino
49
Photographic supplies
40',
Plastics molding and forming
466
Porcelain enameling
i
-: 0
Pulp. paper, and pap.:rboard
-orb
Rubber Manufacturing
41 17
*Soap d: Uetcr<,ent N-1 a uactur'ne
423
Steam Electric power Gencrattion
409
Sugar processing
410
lc-xtlle mills
429
"limber products processing
xOthel's
Environmental remediation of
former leaking UST site.
1'a2e 9 of 17

Industrial User Wastewater Survey
& Permit Application
Wastewater Pollutant Checklist
Chemical Name I EPA Check if Check if Check if Check if Concentration!
Storet I Present at Absent at Present in Absent in in Discharge,
Code i Facility Facility Discharge Discharge it Known
Irr
Acid Extractable Orunnics
2-Chloro •henol
2.4-Dichloro phenol
1 3�h,
2.4-Dimeth% I henol
34hW
2.4-Dinitro tihenol
;461h
2-Methvl-�l.6-dinitro phenol
341:1
4-Chloro-3-methyl henol
3445'
2-Nitro tihenol
343a!
4-Nitro . henol
3 4h16
Pentachloro phenol
Phenol
141"44
2.4.6-Trichlorojohenoi
3462!
Base Neutral Organics
1.2.4-Trichlorobenzene
1.2-Dich IorobeWeIle
5467
4
1 2-Di ihenvlhvdrazine
434
1.3-Dichlorobenzene
3s;h7,
1.4-Dichlorobenzer!-
34i7!
2.4-Dinitrotoluene
34h! j
2.6-Dinitrotoluene
��=h
2-Chloronaphthalene
3�=
3.3-Dich Iorobenzid i n e
3 ,
4-Bromophenyl phenyl ether
4-Chlorophenyl phenyl ether
1 4r,4+
Acenaphthene
I 0340
AcenaphthN lone
Anthracene
3s21-
Benzidine
!,
Benzo (a) anthracene
W>'h
Benzo (a) pyrene
342-4'
Benzo (b) tluoranthene
�.41
Benzo (ghi) pen. len
3-;5,
Benzo (k) tloorrnthenc
;;':=
Bis(2-chloroethoxy
Bis('2-chloroethyl) ether
Bis(2-chloroisopropy1) etirr!•
4:*;
Bis(2-ethvlhexy!) phthalate
Butyl benzyl phthalate
34192 1
Chrvsene
rt3- r
Di-n-butvl nhthalaw
X
X
X
X
X
X
X
X
X
}'a,�e 10 of 1 ?

Industrial User Wastewater Survey
& Permit Application
Wastewater Pollutant Checklist
Chemic�ll ?dame ► �' Chccf; if` C17e: is if Chec1:
1 Storet Present at _�bscnt at Present in
Code I 1;;tcilit\ Facilit. Discharur
Other Inorganics
Purgeable Volatile Organics
Ch%:ch if Concentration
:absent ;n in Discharge.
Dis.Aiarnie if Known
(mRl1)
Others
Xylene
x n n�
Meth I -Tent -But I Ether x , 140
Isopropyl Benzene x
n,Propylbenzene x
1,2;4 Trimethylbenzene x - 557
1,3,5 Trimethylbenzene x 680
0.806
Pa,-,e 12 of 17

W,
M-W
7B
7-I
T�

Industrial User Wastewater Survev
& Kermit Application
Part V, Other:
Please list any significant change, to the Manufacturing process or pretreatment system since the last
permit application xNas submitted:
Not Applicable
Page 17 of 17

I
fb
x
m

5
RECEIVED/DENR/DWR
AUG - 1 2014
Water Quality
Permitting Section

Lment:t;lty or mount molly Laporatory iu: KJ1su/b-uu1
Description: EFFLUENT Matrix: Aqueous
Date Sampled:10/13/2016 0805
Date Received:10/13/2016 t
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 350.1
(Ammonia - N ) 350.1
1 10/20/2016 1630 BWS
24823
1 (Hardness
(to) SM 2340C-2011
1 10/20/2016 1839 MJI
24842
1
(Nitrate-Nitr) 353.2
10 10/20/2016 1910 MSG
24828
1
(Phosphorus) 365.1
10 10/20/2016 0857 KWP
10/18/2016 2330 24665
1
(TDS) SM 254OC-2011
1 10/14/2016 1011 CLM
24412
1 351.4
(TKN) 351.2
1 10/20/2016 1815 KWP
10/20/2016 1050 24791
CAS Analytical
Parameter
Number Method
Result Q
PQL
MDL
Units
Run
Ammonia - N (gas diffusion)
350.1
ND
0.10
0.050
mg/L
1
Hardness (total)
SM 2340C-20
34
10
2.0
mg/L
1
Nitrate -Nitrite - N
353.2
15 B
0.20
0.013
mg/L
1
Phosphorus
7723-14-0 365.1
3.3 B
0.10
0.016
mg/L
1
TDS
SM 254OC-20
440
10
3.4
mg/L
1
TKN
351.2
2.7
1.3
0.11
mglL
1
Semivolatile Organic Compounds by GC/MS
Run ,Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 625
625
1 10/19/2016 1713 ECB
10/17/2016 0028 24491
CAS Analytical
Parameter
Number Method
Result Q
PQL
MDL
Units
Run
Acenaphthene
83-32-9 625
ND
1.6
0.11
ug/L
1
Acenaphthylene
208-96-8 625
ND
1.6
0.060
ug/L
1
Anthracene
120-12-7 625
ND
1.6
0.060
ug/L
1
Benzidine
92-87-5 625
ND
8.0
0.44
ug/L
1
Benzo(a)anthracene
56-55-3 625
ND
1.6
0.070
ug/L
1
Benzo(a)pyrene
50-32-8 625
ND
1.6
0.040
ug/L
1
Benzo(b)fluoranthene
205-99-2 625
ND
1.6
0.050
ug/L
1
Benzo(g,h,i)perylene
191-24-2 625
ND
1.6
0.12
ug/L
1
Benzo(k)fluoranthene
207-08-9 625
ND
1.6
0.070
ug/L
1
4-Bromophenyl phenyl ether
101-55-3 625
ND
1.6
0.16
ug/L
1
Butyl benzyl phthalate
85-68-7 625
ND
1.6
0.15
ug/L
1
bis (2-Chloro-l-methylethyl) ether
108-60-1 625
ND
1.6
0.49
ug/L
1
4-Chloro-3-methyl phenol
59-50-7 625
ND
1.6
0.40
ug/L
1
bis(2-Ch lo roethoxy)m ethane
111-91-1 625
ND
1.6
0.48
ug/L
1
bis(2-Chloroethyl)ether
111-44-4 625
ND
1.6
0.50
ug/L
1
2-Chloronaphthalene
91-58-7 625
ND
1.6
0.40
ug/L
1
2-Chlorophenol
95-57-8 625
ND
1.6
0.34
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3 625
ND
1.6
0.21
ug/L
1
Chrysene
218-01-9 625
ND
1.6
0.050
ug/L
1
Dibenzo(a,h)anthracene
53-70-3 625
ND
1.6
0.11
ug/L
1
1,2-Dichlorobenzene
95-50-1 625
ND
1.6
0.46
ug/L
1
1,3-Dichlorobenzene
541-73-1 625
ND
1.6
0.40
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheatylab.com

Lment:t;ity oT mount Molly Lanoratory iu:KJ13U/b-uu1
Description: EFFLUENT Matrix: Aqueous
Date Sampled:10/13/2016 0805
Date Received:10/1312016
Semiyolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 10/19/2016 1713 ECB 10/17/2016 0028 24491
CAS
Analytical
Parameter
Number
Mplhod
Result Q
PQL
MDL
Units
Run
1,4-Dichlorobenzene
106-46-7
625
ND
1.6
0.41
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
8.0
1.6
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
1.6
0.70
ug/L
1
Diethylphthalate
84-66-2
625
ND
1.6
0.19
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
1.6
0.21
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
1.6
0.62
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
1.6
0.26
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
8.0
0.69
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
8.0
0.65
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
3.2
0.48
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
3.2
0.39
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
1.6
0.070
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
1.6
0.12
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
1.3 J
1.6
0.19
ug/L
1
Fluoranthene
206-44-0
625
ND
1.6
0.050
ug/L
1
Fluorene
86-73-7
625
ND
1.6
0.060
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
1.6
0.39
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
1.6
0.47
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
8.0
0.14
ug/L
1
Hexachloroethane
67-72-1
625
ND
1.6
0.53
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
1.6
0.11
ug/L
1
Isophorone
78-59-1
625
ND
1.6
0.44
ug/L
1
Naphthalene
91-20-3
625
ND
1.6
0.13
ug/L
1
Nitrobenzene
98-95-3
625
ND
1.6
1.1
ug/L
1
2-Nitrophenol
88-75-5
625
ND
3.2
0.88
ug/L
1
4-Nitrophenol
100-02-7
625
ND
8.0
1.2
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
1.6
0.37
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
1.6
0.15
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
1.6
0.25
ug/L
1
Pentachlorophenol
87-86-5
625
ND
8.0
1.4
ug/L
1
Phenanthrene
85-01-8
625
ND
1.6
0.12
ug/L
1
Phenol
108-95-2
625
ND
1.6
0.22
ug/L
1
Pyrene
129-00-0
625
ND
1.6
0.060
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
1.6
0.57
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
1.6
0.44
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quanlitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

cuent:wty or mount pony
Description: EFFLUENT
Date Sampled:10/13/2016 0805
Date Received:10/13/2016
t-aDoratory Iu:hW7surb-uui
Matrix: Aqueous
Surrogate
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d 14
2,4,6-Tri bromophenol
Run 1 Acceptance
Q % Recovery
Limits
78
37-129
36
24-127
78
38-127
50
28-128
66
10-148
81
41-144
ICP-MS
Run Prep Method
1 200.2
Analytical Method Dilution Analysis Date Analyst
200.8 1 10/14/2016 2154 BNW
Prep Date Batch
10/14/2016 0922 24391
CAS
Analytical
Parameter
Number
Method
Result
Q
PQL
MDL
Units
Run
Antimony
7440-36-0
200.8
0.022
0.001
0.00017
mg/L
1
Arsenic
7440-38-2
200.8 0.00037
J
0.001
0.00026
mg/L
1
Beryllium
7440-41-7
200.8
ND
0.0004
0.00012
mg/L
1
Cadmium
7440-43-9
200.8
5.7E-5
J
0.0001
4.4E-5
mg/L
1
Chromium
7440-47-3
200.8
0.0093
0.005
0.00063
mg/L
1
Copper
7440-50-8
200.8
0.028
B
0.001
0.00015
mg/L
1
Lead
7439-92-1
200.8
0.001
0.001
0.00015
mg/L
1
Nickel
7440-02-0
200.8
0.003
J
0.005
0.00063
mg/L
1
Selenium
7782-49-2
200.8
ND
0.001
0.00095
mg/L
1
Silver
7440-22-4
200.8
ND
0.001
0.00017
mg/L
1
Thallium
7440-28-0
200.8
ND
0.0005
7.5E-5
mg/L
1
Zinc
7440-66-6
200.8
0.055
0.01
0.0016
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

unent:Laty Or Mount Kony
Description: EFFLUENT
Date Sampled:10/1312016 0825
Date Received:10113/2016
LaDoratory w: KJ7Sut*-uuz
Matrix: Aqueous
Run Prep Method Analytical Method
1 10-204-00-1-X (Cyanide - To) SM 4500-CN E-
1 (Phenolics) 420.4
1 (HEM (oil and) 1664B
Inorganic non-metals
Dilution
Analysis Date Analyst
1
10/20/20161200 KWP
1
10/21/20161025 BWS
1
10/18/2016 0000 ARP
Prep Date Batch
10/20/2016 1017 24800
10/20/2016 1330 24810
24590
CAS Analytical
Parameter
Number Method
Result Q
PQL
MDL
Units
Run
Cyanide - Total
57-12-5 SM 4500-CN
0.026 J
0.030
0.024
mg/L
1
Phenolics
420.4
0.048
0.010
0.0040
mg/L
1
HEM (oil and grease)
1664B
1.5 J
4.1
1.4
mg/L
1
Volatile Organic Compounds by GUMS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 624 624 1 10/15/2016 0108 ECP 24472
CAS
Analytical
Parameter
Number
Me1hQ0
Result Q
PQL
MDL
Units
Run
Acrolein
107-02-8
624
ND
5.0
4.0
ug/L
1
Acrylonitrile
107-13-1
624
ND
5.0
0.80
ug/L
1
Benzene
71-43-2
624
ND
1.0
0.40
ug/L
1
Bromodichloromethane
75-27-4
624
3.8
1.0
0.40
ug/L
1
Bromoform
75-25-2
624
3.3
1.0
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
624
ND
2.0
0.40
ug/L
1
Carbon tetrachloride
56-23-5
624
ND
1.0
0.40
ug/L
1
Chlorobenzene
108-90-7
624
ND
1.0
0.40
ug/L
1
Chloroethane
75-00-3
624
ND
2.0
0.40
ug/L
1
2-Chloroethylvinylether
110-75-8
624
ND
5.0
0.40
ug/L
1
Chloroform
67-66-3
624
1.1
1.0
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
624
ND
2.0
0.40
ug/L
1
Dibromochloromethane
124-48-1
624
5.5
1.0
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
624
ND
1.0
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
624
ND
1.0
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
624
ND
1.0
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
624
ND
2.0
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
624
ND
1.0
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
624
ND
1.0
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
624
ND
1.0
0.40
ug/L
1
cis-1,2-Dichloroethene
156-59-2
624
ND
1.0
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
624
ND
1.0
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
624
ND
1.0
0.40
ug/L
1
cis-1,3-Dichloropropene
10061-01-5
624
ND
1.0
0.40
ug/L
1
trans-1,3-Dichloropropene
10061-02-6
624
ND
1.0
0.40
ug/L
1
Ethylbenzene
100-41-4
624
ND
1.0
0.40
ug/L
1
Methylene chloride
75-09-2
624
ND
1.0
0.40
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
624
ND
1.0
0.40
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless Flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

unenutoiry of mount mony La[)oratory IU: KJ1UU/b-UUL
Description: EFFLUENT Matrix: Aqueous
Date Sampled:10/13/2016 0825
Date Received:10/13/2016
Volatile Organic Compounds by GUMS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 624 624 1 10/15/2016 0108 ECP 24472
Parameter
CAS Analytical
Number Method
Result Q
PQL
MDL
Units
Run
Tetrachloroethene
127-18-4 624
ND
1.0
0.40
ug/L
1
Toluene
108-88-3 624
ND
1.0
0.40
ug/L
1
1,2,4-Trichlorobenzene
120-82-1 624
ND
1.0
0.40
ug/L
1
1,1,1-Trichloroethane
71-56-6 624
ND
1.0
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5 624
ND
1.0
0.40
ug/L
1
Trichloroethene
79-01-6 624
ND
1.0
0.40
ug/L
1
Trich lorofl uorom ethane
75-69-4 624
ND
1.0
0.40
ug/L
1
Vinyl chloride
75-01-4 624
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4 112 70-130
Toluene-d8 102 70-130
Bromofluorobenzene 97 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the MDL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheatylab.com

Lmenutvity oT Mount mono
t-aDoratory lu: (, uz4uos-uu7
Description: EFFLUENT
.
Matrix: Aqueous
Date Sampled:07124/2015 0805
Date Received: 0712412015
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1 350.1
(Ammonia - N ) 350.1
1
07/31/2015 1029 BWS
07/30/2015 1522 81127
1 (Hardness (to) SM 2340C-2011
1
07/29/2015 1714 HMA
81009
1
(Nitrate-Nitr) 353.2
15
07/30/2015 2142 ECP
81155
1
(Phosphorus) 365.1
10
07/29/2015 1141 BWS
07/28/2015 1141 80840
1
(TDS) SM 2540C-2011
1
07/27/2015 1447 BLO
80748
1 351.4
(TKN) 351.2
1
07/30/2015 1607 BWS
07/28/2015 1143 80842
CAS Analytical
Parameter
Number
Method
Result Q PQL
Units
Run
Ammonia - N (phenate)
350.1
0.54 0.10
mg/L
1
Hardness (total)
SM 2340C-20
42 10
mg/L
1
Nitrate -Nitrite - N
353.2
26 0.30
mg/L
1
Phosphorus
7723-14-0
..365.1
3.4 0.10
mg/L
1
TDS
SM 254OC-20
470 10
mg/L
1
TKN
351.2
1.5 0.50
mg/L
1
Semiyolatile Organic
Compounds by GC/MS
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1 625
625
1
08/12/2015 1528 DRB1
07/27/2015 1014 80696
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Acenaphthene
83-32-9
625
ND
2.0
ug/L
1
Acenaphthylene
208-96-8
625
ND
2.0
ug/L
1
Anthracene
120-12-7
625
ND
2.0
ug/L
1
Benzidine
92-87-5
625
ND
10
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
2.0
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
2.0
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
2.0
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
2.0
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
2.0
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
2.0
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
10
ug/L
1
4-Ch loro-3-m ethyl phenol
59-50-7
625
ND
2.0
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
2.0
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
2.0
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
2.0
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
2.0
ug/L
1
2-Chlorophenol
95-57-8
625
ND
2.0
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
2.0
ug/L
1
Chrysene
218-01-9
625
ND
2.0
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
2.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
2.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
2.0
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheatylab.com

Lment: t;rty or mount moray
Laooratory tu: QUZ4ubs-uu1
Description: EFFLUENT
Matrix: Aqueous
Date Sampled:07/24/2015 0805
Date Received:07/24/2015
Semivolatile Organic Compounds by
GUMS
Run Prep Method Analytical Method Dilution Analysis Date Analyst
Prep
Date Batch
1 625
625 1 08/12/2015 1528 DRB1
07/27/2015
1014 80696
CAS
Analytical
Parameter
Number
Method
Result
Q PQL
Units
Run
1,4-Dichlorobenzene
106-46-7
625
ND
2.0
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
10
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
2.0
ug/L
1
Di ethyl phthalate
84-66-2
625
ND
10
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
10
ug/L
1
2,4-Dimethyl phenol
105-67-9
625
ND
2.0
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
10
ug/L
1
4,6-Dinitro-2-methyl phenol
534-52-1
625
ND
10
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
10
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
4.0
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
4.0
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
10
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
2.0
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
10
ug/L
1
Fluoranthene
206-44-0
625
ND
2.0
ug/L
1
Fluorene
86-73-7
625
ND
2.0
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
2.0
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
2.0
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
10
ug/L
1
Hexachloroethane
67-72-1
625
ND
2.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
2.0
ug/L
1
Isophorone
78-59-1
625
ND
2.0
ug/L
1
Naphthalene
91-20-3
625
ND
2.0
ug/L
1
Nitrobenzene
98-95-3
625
ND
2.0
ug/L
1
2-Nitrophenol
88-75-5
625
ND
4.0
ug/L
1
4-Nitrophenol
100-02-7
625
ND
10
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
2.0
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
2.0
ug/L
1
Pentachlorophenol
87-86-5
625
ND
10
ug/L
1
Phenanthrene
85-01-8
625
ND
2.0
ug/L
1
Phenol
108-95-2
625
ND
2.0
ug/L
1
Pyrene
129-00-0
625
ND
2.0
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
2.0
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
2.0
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quentitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

l.;uent:ary of mount mouy
Description: EFFLUENT
Date Sampled:07/24/2015 0805
Date Received:07124/2015
t-aDoratory lu: QUZ4Ubs-UU1
Matrix: Aqueous
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
67
37-129
2-Fluorophenol
116
24-127
Nitrobenzene-d5
74
38-127
Phenol-d5
76
28-128
Terphenyl-d 14
37
10-148
2,4,6-Tribromophenol
71
41-144
DqW,��
Run Prep Method
1 200.2
2 200.2
Analytical Method Dilution Analysis Date Analyst
200.8 1 07/28/2015 0129 CDF
200.8 1 07/29/2015 0333 CDF
Prep Date Batch
07/27/2016 0935 80688
07/27/2016 0935 80688
CAS Analytical
Parameter
Number Mp1hog
Result Q
PQL
Units
Run
Antimony
7440-36-0 200.8
41
1.0
ug/L
1
Arsenic
7440-38-2 200.8
2.5
1.0
ug/L
1
Beryllium
7440-41-7 200.8
ND
0.40
ug/L
2
Cadmium
7440-43-9 200.8
ND
0.10
ug/L
1
Chromium
7440-47-3 200.8
7.2
5.0
ug/L
1
Copper
7440-50-8 200.8
31
1.0
ug/L
2
Lead
7439-92-1 200.8
ND
1.0
ug/L
1
Nickel
7440-02-0 200.8
ND
5.0
ug/L
1
Selenium
7782-49-2 200.8
6.3
1.0
ug/L
1
Silver
7440-22-4 200.8
ND
1.0
ug/L
1
Thallium
7440-28-0 200.8
ND
0.50
ug/L
1
Zinc
7440-66-6 200.8
65
10
ug/L
2
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MOIL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheatylab.com

Lment:wty Ot mount molly
Laooratory iu:wuz4ub3-uuz
Description: EFFLUENT
Matrix: Aqueous
Date Sampled:07/24/2015 0815
Date Received:07/2412015
Inorganic non-metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 10-204-00-1-X (Cyanide - To) SM 4500-CN E- 1 07/28/2015 1717 BWS
07/28/2015 1500 80848
1
(Phenolics) 420.4 1 07/30/2015 1123 MJI
07/30/2015 0915 81071
1
(HEM (oil and) 1664B 1 07/30/2015 0953 HKB
81069
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Cyanide - Total
57-12-5 SM 4500-CN
ND
0.010
mg/L
1
Phenolics
420.4
ND
0.020
mg/L
1
HEM (oil and grease)
1664B
ND
4.4
mg/L
1
Volatile Organic Compounds by GUMS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B
624 1 08/03/20151546 ALL
81339
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Acrolein
107-02-8 624
ND
50
ug/L
1
Acrylonitrile
107-13-1 624
ND
50
ug/L
1
Benzene
71-43-2 624
ND
5.0
ug/L
1
Bromodichloromethane
75-27-4 624
5.9
5.0
ug/L
1
Bromoform
75-25-2 624
25
5.0
ug/L
1
Bromomethane (Methyl bromide)
74-83-9 624
ND
5.0
ug/L
1
Carbon tetrachloride
56-23-5 624
ND
5.0
ug/L
1
Chlorobenzene
108-90-7 624
ND
5.0
ug/L
1
Chloroethane
75-00-3 624
ND
5.0
ug/L
1
2-Chloroethylvinylether
110-75-8 624
ND
10
ug/L
1
Chloroform
67-66-3 624
ND
5.0
ug/L
1
Chloromethane (Methyl chloride)
74-87-3 624
ND
5.0
ug/L
1
Dibromochloromethane
124-48-1 624
18
5.0
ug/L
1
1,1-Dichloroethane
75-34-3 624
ND
5.0
ug/L
1
1,2-Dichloroethane
107-06-2 624
ND
5.0
ug/L
1
1,1-Dichloroethene
75-35-4 624
ND
5.0
ug/L
1
trans- l,2-Dichloroethene
156-60-5 624
ND
5.0
ug/L
1
1,2-Dichloropropane
78-87-5 624
ND
5.0
ug/L
1
cis-1,3-Dichloropropene
10061-01-5 624
ND
5.0
ug/L
1
trans-1,3-Dichloropropene
10061-02-6 624
ND
5.0
ug/L
1
Ethylbenzene
100-41-4 624
ND
5.0
ug/L
1
Methylene chloride
75-09-2 624
ND
5.0
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5 624
ND
5.0
ug/L
1
Tetrachloroethene
127-18-4 624
ND
5.0
ug/L
1
Toluene
108-88-3 624
ND
5.0
ug/L
1
1,1,1-Trichloroethane
71-55-6 624
ND
5.0
ug/L
1
1,1,2-Trichloroethane
79-00-5 624
ND
5.0
ug/L
1
Trichloroethene
79-01-6 624
ND
5.0
ug/L
1
PQL = Practical quantitation limit
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL
J = Estimated result < PQL and ? MOIL P = The RPD between two GC columns exceeds 40 %
N = Recovery is out of criteria
Where applicable, all soil sample analysis are
reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc.
Page: 8 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

unenvtaty OT mount mouy
I-aooratory IU: QUZ4u0s-UUZ
Description: EFFLUENT
Matrix: Aqueous
Date Sampled:07/24/2015 0815
Date Received:07124/2015
Volatile Organic Compounds by GUMS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch
1 5030B
624 1 08/03/20151546 ALL
81339
CAS Analytical
Parameter
Number Method Result Q
PQL Units Run
Vinyl chloride
75-01-4 624 ND
5.0 ug/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
90 70-130
Bromofluorobenzene
108 70-130
Toluene-d8
94 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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