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HomeMy WebLinkAboutWQ0004500_Residual Annual Report 2014_20150302k,p cz;e'� q 5&-t> REc Fjl/ )-EFDj MAR 0 2 2015 ,��v�rdryr�t err, cT ARCHER ®��yl IEFI,..Zp'{ iiDLAND COMPANY, NC RESIDUALS LAN,T) APPLICATION PROGRAM Perm -ft N,.-,. ° fQ0004500 2014 , ANNUAL REPORT Archer Daniels Midland Company, NC Residuals Land Application Program 2014 Annual Report TABLE OF CONTENTS 1. Certification Form, Annual Operations Summary, Facility and Land Applier Contact Information 2. Annual Residuals Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen & Vector Attraction Reduction ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00004500 County Brunswick Year 2014 Facility Name (as shown on permit) Archer Daniels Midland Company NPDES No. NCO027065 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summ Total number of application fields in the permit: N/A Total number of fields utilized for land application during the year: 183 Total amount of dry tons applied during the year for all application sites: 13.371.73 Total number of acres utilized for land application during the year: 2,440.5 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water QualityX YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. ParrC — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the ossibility of fines and imprisonment for knowing violations." /% _ _ Scott Phillips, Operations Superintendent Permittee Name and Title (type or print) - Date 9 20151 Signature of Preparer* Date Dignature of LanYApplier Date (if different from Permittee) (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION - ",RCHER DANIELS MIDLAND CORP., NC ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS January 2014 4,548.17 W 1324.87 D 1201.64 February 2014 3,679.48 W 1193.62 D 1082.59 March 2014 2,977.68 W 856.00 D 776.42 April 2014 3,970.25 W 1148.59 D 1041.74 May 2014 5,585.36 W 1925.24 D 1746.20 June 2014 4,165.40 W 1280.45 D 1161.35 July 2014 3,664.90 W 1083.73 D 982.93 August 2014 261.41 W 70.53 D 63.97 September 2014 1,270.88 W 342.90 D 311.00 October 2014 4,128.98 W 1156.52 D 1048.97 November 2014 2,033.21 W 594.72 D 539.41 December 2014 2,674.37 W 733.05 D 664.87 YEARLY TOTAL 38,960.09 W 11,710.22 D 10,621.09 ADM CORP., NC NITRO GRO 2 CAKE DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS July 2014 491.90 W 85.25 D 77.32 August 2014 2,279.75 W 360.44 D 326.92 September 2014 1,185.97 W 205.65 D 186.51 YEARLY TOTAL 3,957.62 W 651.34 D 590.75 ADM CORP., NC NITRO GRO 3 LIQUID MONTHNEAR January 2014 February 2014 March 2014 April 2014 May 2014 June 2014 July 2014 August 2014 November 2014 December 2014 YEARLY TOTAL DRY METRIC AMOUNT UNIT DRY TONS UNIT TONS 163,172.61 G 98.52 D 89.36 44,429.26 G 26.92 D 24.42 207, 561.14 G 128.16 D 116.24 255,345.31 G 158.01 D 143.32 366,177.43 G 220.35 D 199.86 265,438.84 G 156.63 D 142.06 136,546.76 G 63.77 D 57.84 232,147.45 G 133.88 D 121.45 23,127.10 G 13.88 D 12.59 17,175.06 G 10.05 D 9.12 1,711,120.96 G 1,010.17 D 916.26 2/18/2015 2014 ANNUAL REPORT PROJECT: Archer Daniels Midland Company (ADM) FACILITY: Archer Daniels Midland Company 1730 East Moore St., SE Southport, NC 28461 (910) 457-5011 PRODUCTS: NPDES Permit Number: RESPONSIBLE OFFICIAL: A FACILITY OPERATOR: LAND APPLIER AND PREPARER OF LAND APPLICATION ANNUAL REPORT: NitroGro II NitroGro III NitroGro V NC0027065 Scott Phillips, Operation Superintendent Archer Daniels Midland Company 1730 East Moore St., SE Southport, NC 28461 (910) 457-1476 Same as above Synagro Central, LLC Contact: Marshall Puryear (336) 998-7150 ext. 17 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004500 Laboratory Facility Name: ARCHER DANIELS MIDLAND CORP., NC A&L Eastern Laboratories Inc. NPDES# : NCO027065 or WQ# ('residual only) WWTP Name: ARCHER DANIELS MIDLAND Residuals Analysis Data Product Type NG2421 NG2421 NG2421 NG2421 NG2421 NG2421 NG2421 NG2421 NG2421 Date Sampled (grab) or 12/19/13 01/09/14 01/27/14 02/26/14 03/25/14 04/29/14 - 05/19/14 06/27/14 07/23/14 Date Composited Percent Solids 29.13 31.20 32.44 27.43 28.93 34.47 30.74 29.57 26.98 PARAMETERS (mglkg dry weight) Arsenic <3 3 <3 <3 <3 3 <3 <3 <3 Cadmium 3 <2 <2 <2 <2 <2 <2 <2 <2 Mercury <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 1.7 0.7 Chromium _ 40 28 34 48 36 40 53 57 58 Copper 30 11 10 10 10 12 32 13 13 Lead <5 <5 <5 <5 <5 <5 6 <5 <5 Molybdenum 6 <5 <5 <5 <5 <5 <5 <5 <5 Nickel 17 13 14 20 15 17 24 20 21 Selenium <5 <5 <5 <5 <5 <5 <5 <5 <5 Zinc 176 118 113 151 142 171 303 248 207 Total Phosphorus 12800 10200 10600 12600 9410 9530 13400 15300 13600 TKN 28100 26900 22700 32300 29000 26700 26300 30100 28800 Ammonia -Nitrogen 2090 2720 2070 3350 1940 2200 3090 5310 4480 Nitrate and Nitrite 8.24 4.17 4.93 46.3 2.77 7.83 6.18 <2 5.93 DENR FORM RSSF (5/2003) Printed: Thursday - February 19, 2015 at 15:22:11 for: 2044 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM - Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004500 Laboratory Facility Name: ARCHER DANIELS MIDLAND CORP., NC A&L Eastern Laboratories Inc. NPDES# : NCO027065 or WQ# (residual only) WWTP Name: ARCHER DANIELS MIDLAND Residuals Analysis Data Product Type NG2421 NG2421 NG2421 NG2421 Date Sampled (grab) or 09/24/14 10/23/14 11/18/14 12/18/14 Date Composited Percent Solids 28.01 29.25 27.41 28.65 PARAMETERS (mg/kg dry weight), Arsenic <3 <3 <3 <3 Cadmium <2 2 <2 <2 Mercury <0.4 <0.4 <0.4 <0.4 Chromium 54 49 51 35 Copper 13 10 9 9 Lead <5 <5 <5 <5 Molybdenum <5 <5 <5 <5 Nickel 21 23 21 14 Selenium <5 <5 <5 <5 Zinc 178 163 117 136 Total Phosphorus 12100 10500 7070 8070 TKN 25100 25000 24600 27100 Ammonia -Nitrogen 1430 1880 3030 2300 Nitrate and Nitrite 21.4 99.8 17.5 <2 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." M GNATURE OF P Date �� ��`� Page: 2 DENR FORM RSSF (512003) Printed: Thursday - February 19, 2015 at 15:22:11 for: 2044 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004500 Laboratory Facility Name: ARCHER DANIELS MIDLAND CORP., NC A&L Eastern Laboratories Inc. NPDES# : NCO027065 or WQ# (residual only) WWTP Name: ARCHER DANIELS MIDLAND Residuals Analysis Data Product Type NG2421 NG2421 NG2421 NG2421 NG2421 NG2421 NG2421 NG2421 NG2421 Date Sampled(grab)or 12/19/13 01/09/14 01/27/14 02/26/14 03/25/14 04/29/14 05/19/14 06/27/14 07/23/14 Date Composited Percent Solids 29.13 31.20 32.44 27.43 28.93 34.47 30.74 29.57 26.98 PARAMETERS (mg/kg dry weight) Aluminum 2900 2300 1900 2700 2200 3000 4700 3100 2700 Calcium 159000 152000 189000 140000 149000 112000 138000 143000 131000 Magnesium 2460 1950 2060 2390 1800 2090 2600 2810 2920 pH 7.90 7.79 7.69 7.95 7.63 7..96 7.65 8.00 7.23 Potassium 8980 7830 8100 9720 6970 7380 7610 8400 7670 Sodium 3910 3740 3650 4160 3170 4130 4570 5510 5770 DENR FORM RSSF-B (7/2002) Printed: Wednesday - February 18, 2015 at 11:57:43 for: 2044 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: W00004500 Laboratory Facility Name: ARCHER DANIELS MIDLAND CORP., NC A&L Eastern Laboratories Inc. NPDES# : NCO027065 or WQ# (residual only) WWTP Name: ARCHER DANIELS MIDLAND Residuals Analysis Data Product Type NG2421 NG2421 NG2421 Date Sampled (grab) or 09/24/14 10/23/14 11/18/14 Date Composited Percent Solids 28.01 29.25 27.41 PARAMETERS (mg/kg dry weight) Aluminum 4100 2600 2500 Calcium 142000 133000 109000 Magnesium 2870 2070 1370 pH 7.63 8.25 7.88 Potassium 8250 7150 4740 Sodium 5650 5390 3420 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant ties for s�ub)mitting false information, including the possibility of fines and imprisonment for knowing violations." pen X / Ci (S NATURE OF P R - Data Not Reported or Data Not Required Date Page: 2 DENR FORM RSSF-B (7/2002) Printed: Wednesday - February 18, 2015 at 11:57:43 for: 2044 01 Page: 1 of 2 Report Number: 13-354-0201 Account Number: 45637 Submitted By: SCOTT.COE Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 97211 Sample Id : NG2421 A&L Eastern Laboratories, Inc- J621 Whitepine Road Richmond, Virginia 23237 • (804) 743-9401 Fax (804) 271.WS ,wwwaleastern.com Project: NG2421 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 12/19/2013 07:45:00 Date Received: 12/20/2013 00:00 Date Reported: 01/02/2014 Total Solids * 29.13 291300 100.0 JM 12/20/2013 14:44 SM-2540G Moisture * 70.87 1 100.0 JM 12/20/2013 14:44 SM-2540G Total Kjeldahl Nitrogen 2.81 28100 10.0 JM 12/23/2013 08:35 SM-4500-NH3C-TKN Total Phosphorus 1.28 12800 100 KM 12/23/2013 11:47 SW 6010C Total Potassium 0.90 8980 100 KM 12/23/2013 11:47 SW 6010C Total Sulfur 8.35 83500 100 KM 12/23/2013 11:47 SW 6010C Total Calcium 15.90 159000 100 KM 12/23/2013 11:47 SW 6010C Total Magnesium 0.25 2460 100 KM 12/23/2013 11:47 SW 6010C Total Sodium 0.39 3910 100 KM 12/23/2013 11:47 SW 6010C Total Iron 2020 100 KM 12/23/2013 11:47 SW 6010C Total Aluminum - 2900 100 KM 12/23/2013 11:47 SW 6010C Total Manganese 136 5 KM 12/23/2013 11:47 SW 6010C Total Copper 30 5 KM 12/23/2013 11:47 SW 6010C Total Zinc 176 5 KM 12/23/2013 11:47 SW 6010C Ammonia Nitrogen 0.21 2090 10.0 JM 12/23/2013 08:35 SM-4500-NH3C Organic N 2.60 26010 10.0 12/23/2013 08:35 CALCULATION Nitrate+Nitrite-N 8.24 2.00 JM 12/23/2013 08:50 SM-450ONO3F Total Cadmium 3.0 2.0 KM 12/23/2013 11:47 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made - to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 13-354-0201 Account Number: 45637 Submitted By: SCOTT COE Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 97211 Sample Id : NG2421 99,A&L EasternLaboratories, Inc. 7,621 Whitepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (804) 271-6446 www.aleastern.com Project: NG2421 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 12/19/2013 07:45:00 Date Received: 12/20/2013 00:00 Date Reported: 01/02/2014 Total Chromium 40 5 KM 12/23/2013 11:47 SW 6010C Total Nickel 17 5 KM 12/23/2013 11:47 SW 6010C Total Lead <5 5 KM 12/23/2013 11:47 SW 6010C Total Arsenic <3.0 3.0 KM 12/23/2013 11:47 SW 6010C Total Mercury <0.4 0.4 KM 12/23/2013 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 12/23/2013 11:47 SW 6010C pH (Standard Units) * 7.90 2.00 JM 12/23/2013 08:35 SW-9045D Total Molybdenum 6 5 KM 12/23/2013 11:47 SW 6010C Chloride 493 200 JM 12/23/2013 09:50 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Fe", "Mn", AND "Mo". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca", "Se", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4 MIX, 12/19/2013 111/2014-1/3112014 1.4369 2:1 MIX RATIO OF NG2 TO NG4 Na mg/1= (Na mg/kg x % Solids) + 100 = (3910 x 29.1300) = 100 = 1138.98 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (159000 x 29.1300) _ 100 = 46316.7 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2460 x 29.1300) _ 100 = 716.598 Na meq = Na mg/I = Molec.Wgt.Na = 1138.98 -= 23 = 49.521 Ca meq = Ca mg/I + Molec.Wgt.Ca = 46316.7 = 20 = 2315.84 Mg meq = Mg mg/I = Molec.Wgt.Mg = 716.598 _ 12 = 59.7165 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 49.521 = SgrRoot[0.5(2315.84+59.7165)] = 1.43689 Printed: 2/18/2015 Page 1 12:11 t Page: 1 of 2 Report Number: 14-010-0211 Account Number: 45637 Submitted By: SCOTT COE Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 97430 Sample Id : NG2421 �LA&L- Eastern Laboratories, Inc, 7621 Whitepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (604) 271-6446 wwwaleastem.com Project: NG2421 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/9/2014 08:00:00 Date Received: 01/10/2014 00:00 Date Reported: 01/16/2014 Total Solids * 31.20 312000 100.0 JM 01/10/2014 14:24 SM-2540G Moisture * 68.80 100.0 JM 01/10/2014 14:24 SM-2540G Total Kjeldahl Nitrogen 2.69 26900 10.0 JM 01/13/2014 08:30 SM-4500-NH3C-TKN Total Phosphorus 1.02 10200 100 KM 01/13/2014 11:35 SW 6010C Total Potassium 0.78 7830 100 KM 01/13/2014 11:35 SW 6010C Total Sulfur 8.57 85700 100 KM 01/13/2014 11:35 SW 6010C Total Calcium 15.20 152000 100 KM 01/13/2014 11:35 SW 6010C Total Magnesium 0.20 1950 100 KM 01/13/2014 11:35 SW 6010C Total Sodium 0.37 3740 100 KM 01/13/2014 11:35 SW 6010C Total Iron 1380 100 KM 01/13/2014 11:35 SW 6010C Total Aluminum 2300 100 KM 01/13/2014 11:35 SW 6010C Total Manganese 82 5 KM 01/13/2014 11:35 SW 6010C Total Copper 11 5 KM 01/13/2014 11:35 SW 6010C Total Zinc 118 5 KM 01/13/2014 11:35 SW 6010C Ammonia Nitrogen 0.27 '2720 10.0 JM 01/13/2014 08:30 SM-4500-NI3C Organic N 2.42 24180 10.0 01/13/2014 08:30 CALCULATION Nitrate+Nitrite-N 4.17 2.00 JM 01/13/2014 08:30 SM-460ONO3F Total Cadmium <2.0 2.0 KM 01/13/2014 11:35 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , ftg to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-010-0211 Account Number: 45637 Submitted By: SCOTT COE Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 97430 Sample Id: NG2421 ULAFL Eastem Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804)743-9401 Fax(804)271-6446 www.aleastern.com Project : NG2421 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/9/2014 08:00:00 Date Received: 01/10/2014 00:00 Date Reported: 01/16/2014 Total Chromium 28 5 KM 01/13/2014 11:35 SW 6010C Total Nickel 13 5 KM 01/13/2014 11:35 SW 6010C Total Lead <5 5 KM 01/13/2014 11:35 SW 6010C Total Arsenic 3.0 3.0 KM 01/13/2014 11:35 SW 6010C Total Mercury <0.4 0.4 KM 01/13/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 01/13/2014 11:35 SW 6010C pH (Standard Units) * 7.79 2.00 JM 01/13/2014 08:30 SW-9045D Total Molybdenum <5 5 KM 01/13/2014 11:35 SW 6010C Chloride 297 200 JM 01/15/2014 09:25 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "NO3/NO2-N" AND "Se". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "As" AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4 MIX, 1/9/2014 / / - / / 1.4579 2:1 MIX RATIO OF NG2 TO NG4 Na mg/I = (Na mg/kg x % Solids) _ 100 = (3740 x 31.2000) = 100 = 1166.88 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (152000 x 31.2000) = 100 = 47424 Mg mg/I = (mg mg/kg x % Solids) + 100 = (1950 x 31.2000) + 100 = 608.4 Na meq = Na mg/I = Molec.Wgt.Na = 1166.88 = 23 = 50.7339 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 47424 t- 20 = 2371.2 Mg meq = Mg mg/I = Molec.Wgt.Mg = 608.4 = 12 = 50.7 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 50.7339 = SgrRoot[0.5(2371.2+50.7)] = 1.45793 Printed: 2/18/2015 Page 1 14:09 Page: 1 of 2 Report Number: 14-028-0206 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE St SE SOUTHPORT , NC 28461 Lab Number: 97669 Sample Id ADM - NG2421 4 A&L Eastern Laboratories, Inc._ 7621.Whitepine Road Richmond, Virginia 23237 (804) 743-9401, Fax (804) 271-8446 wwwaleastern.com project: ADM - NG-2421 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/27/201412:50:00 Date Received: 01/28/2014 00:00 Date Reported: 02/03/2014 Total Solids * 32.44 324400 100.0 JM 01/28/2014 15:00 SM-2540G Moisture * 67.56 100.0 JM 01/28/2014 15:00 SM-2540G Total Kjeldahl Nitrogen 2.27 22700 10.0 JM 01/29/2014 09:29 SM-4500-NH3C-TKN Total Phosphorus 1.06 10600 100 KM 01/29/2014 13:31 SW 6010C Total Potassium 0.81 8100 100 KM 01/29/2014 13:31 SW 6010C Total Sulfur' 11.40 114000 100 KM 01/29/2014 13:31 SW 6010C Total Calcium 18.90 189000 100 KM 01/29/2014 13:31 SW 6010C Total Magnesium 0.21 2060 100 KM 01/29/2014 13:31 SW 6010C Total Sodium' 0.37 3650 100 KM 01/29/2014 13:31 SW 6010C Total Iron 1570 100 KM 01/29/2014 13:31 SW 6010C Total Aluminum 1900 100 KM 01/29/2014 13:31 SW 6010C Total Manganese 81 5 KM 01/29/2014 13:31 SW 6010C Total Copper 10 5 KM 01/29/2014 13:31 SW 6010C Total Zinc 113 5 KM 01/29/2014 13:31 SW 6010C Ammonia Nitrogen 0.21 2070 10.0 JM 01/29/2024 00:00 SM-4500-NH3C Organic N 2.06 20630 10.0 01/29/2014 09:29 CALCULATION Nitrate+Nitrite-N 4.93 2.00 JM 01/29/2014 09:30 SM-450ONO3F Total Cadmium <2.0 2.0 KM 01/29/2014 13:31 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-028-0206 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 97669 Sample Id: ADM - NG2421 A&L Eastern Laboratories, Inc.. 7621 Whitepine Road Richmond, Virginia 23237 (804)743-9401 Fax (804) 271-W6 w wwaleastern.com Project: ADM - NG-2421 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/27/2014 12:50:00 Date Received: 01/28/2014 00:00 Date Reported: 02/03/2014 Total Chromium 34 5 KM 01/29/2014 13:31 SW 6010C Total Nickel 14 5 KM 01/29/2014 13:31 SW 6010C Total Lead <5 5 KM 01/29/2014 13:31 SW 6010C Total Arsenic <3.0 3.0 KM 01/29/2014 13:31 SW 6010C Total Mercury <0.4 0.4 KM 01/29/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 01/29/2014 13:31 SW 6010C pH (Standard Units) * 7.69 2.00 JM 01/29/2014 09:29 SW-9045D Total Molybdenum <5 5 KM 01/29/2014 13:31 SW 6010C Chloride <200 200 JM 01/29/201410:30 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4 MIX, 1/27/2014 2/1/2014-3/9/2014 1.3032 2:1 MIX RATIO OF NG2 TO NG4 Na mg/I = (Na mg/kg x % Solids) _ 100 = (3650 x 32.4400) _ 100 = 1184.06 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (189000 x 32.4400) _ 100 = 61311.6 Mg mg/I = (mg mg/kg x % Solids) + 100 = (2060 x 32.4400) = 100 = 668.264 Na meq = Na mg/I _ Molec.Wgt.Na = 1184.06 = 23 = 51.4809 Ca meq = Ca mg/I - Molec.Wgt.Ca = 61311.6 _ 20 = 3065.58 Mg meq = Mg mg/I + Molec.Wgt.Mg = 668.264 _ 12 = 55.6887 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 51.4809 + SgrRoot[0.5(3065.58+55.6887)] = 1.30315 Printed: 2/18/2015 Page 1 12:12 Page: 1 of 2 Report Number: 14-059-0202 L A&L Eastern Laboratories, Inc.,_ Account Number: 46637 7621 Whitepine Road Richmond, virginia 23237 (604) 743.9401 Fax (604) 271.6446 Submitted By: EDWARD STEPHENS wwwaleastern.conn Send To: ADM Project: ADM/NG2 BLEND SCOTT PHILLIPS NC CERT#257 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 REPORT OF ANALYSIS Date Sampled: 2/26/2014 10:35:00 Lab Number: 98168 Date Received: 02/28/2014 00:00 Sample Id : NG2 BLEND Date Reported: 03/07/2014 Total Solids ` 27.43 274300 100.0 JM 03/04/2014 09:20 SM-2540G Moisture ' 72.57 100.0 JM 03/04/2014 09:20 SM-2540G Total Kjeldahl Nitrogen 3.23 32300 10.0 JM 03/03/2014 07:54 SM-4500-NH3C-TKN Total Phosphorus 1.26 12600 100 KM 03/03/2014 12:51 SW 6010C Total Potassium 0.97 9720 100 KM 03/03/2014 12:51 SW 6010C Total Sulfur 7.93 79300 100 KM 03/03/2014 12:51 SW 6010C Total Calcium 14.00 • 140000 100 KM 03/03/2014 12:51 SW 6010C Total Magnesium 0.24 2390 100 KM 03/03/2014 12:51 SW 6010C Total Sodium 0.42 4160 100 KM 03/03/2014 12:51 SW 6010C Total Iron 2230, 100 KM 03/03/2014 12:51 SW 6010C Total Aluminum 2700 100 KM 03/03/2014 12:51 SW 6010C Total Manganese 118 5 KM 03/03/2014 12:51 SW 6010C Total Copper 10 5 KM 03/03/2014 12:51 SW 6010C Total Zinc 151 5 KM 03/03/2014 12:51 SW 6010C Ammonia Nitrogen 0.34 3350 10.0 . JM 03/03/2014 07:54 SM-4500-NH3C Organic N 2.89 28950 10.0 03/03/2014 07:54 CALCULATION, Nitrate+Nitrite-N 46.3 2.00 JM 03/03/2014 07:55 SM-450ONO3F Total Cadmium <2.0 2.0 KM 03/03/2014 12:51 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-059-0202 Account Number: 45637 Submitted By: EDWARD STEPHENS Send To: ADM 'SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 98168 Sample Id : NG2 BLEND AU Eastern Laboratories, Inc._ .7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271.W6 www.3leastern.com Project: ADM/NG2 BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 2/26/2014 10:35:00 Date Received: 02/28/2014 00:00 Date Reported: 03/07/2014 Total Chromium 48 5 KM 03/03/2014 12:51 SW 6010C Total Nickel 20 5 KM 03/03/2014 12:51 SW 6010C Total Lead <5 5 KM 03/03/2014 12:51 SW 6010C Total Arsenic <3.0 3.0 KM 03/03/2014 12:51 SW 6010C Total Mercury <0.4 0.4 KM 03/03/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 03/03/2014 12:51 SW 6010C pH (Standard Units) * 7.95 2.00 JM 03/03/2014 09:09 SW-9045D Total Molybdenum <5 5 KM 03/03/2014 12:51 SW 6010C Chloride 460 200 MW 03/03/2014 08:10 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "CA", AND "NO3/NO2-N". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4 MIX, 2/26/2014 3110/2014-3/31/2014 1.5789 2:1 MIX RATIO OF NG2 TO NG4 Na mg/I = (Na mg/kg x % Solids) = 100 = (4160 x 27.4300) + 100 = 1141.09 Ca mg/1= (Ca mg/kg x % Solids) + 100 = (140000 x 27.4300) = 100 = 38402 Mg mg/I = (mg mg/kg x % Solids) + 100 = (2390 x 27.4300) =100 = 655.577 Na meq = Na mg/I + Molec.Wgt.Na = 1141.09 + 23 = 49.6125 Ca meq = Ca mg/I = Molec.Wgt.Ca = 38402 _ 20 = 1920.1 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 655.577 _ 12 = 54.6314 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 49.6125 + SgrRoot[0.5(1920.1+54.6314)] = 1.57889 n Page 1 Printed: 2/18/2015, 12:12 Page: 1 of 2 Report Number: 14-085-0203 Account Number: 45637 Submitted By: EDWARD STEPHENS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 98584 Sample Id: ADM BLEND A&L Eastern Laboratories Inc._ 7621 Whhepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (804) 271.W6 m aleastern.com Project: ADM BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 3/25/2014 13:00:00 Date Received: 03/26/2014 00:00 Date Reported: 03/31/2014 Total Solids * 28.93 289300 100.0 JM 03/26/2014 13:45 SM-2540G Moisture * 71.07 100.0 JM 03/26/2014 13:45 SM-2540G Total Kjeldahl Nitrogen 2.90 29000 10.0 JM 03/27/2014 08:44 SM-4500-NH3C-TKN Total Phosphorus 0.94 9410 100 KM 03/27/2014 12:21 SW 6010C Total Potassium 0.70 6970 100 KM 03/27/2014 12:21 SW 6010C Total Sulfur '9.02 90200 100 KM 03/27/2014 12:21 SW 6010C Total Calcium 14.90 149000 100 KM 03/27/2014 12:21 SW 6010C Total Magnesium 0.18 1800 100 KM 03/21/2014 12:21 SW 6010C Total Sodium 0.32 3170 100 KM 03/27/2014 12:21 SW 6010C Total Iron 1440 100 KM 03/27/2014 12:21 SW 6010C Total Aluminum 2200 100 KM 03/27/2014 12:21 SW 6010C Total Manganese 82 5 KM 03/27/2014 12:21 SW 6010C Total Copper 10 5 KM 03/27/2014 12:21 SW 6010C Total Zinc 142 5 KM 03/27/2014 12:21 SW 6010C Ammonia Nitrogen 0.19 1940 10.0 JM 03/27/2014 08:44 SM-4500-NH3C Organic N 2.71 27060 10.0 03/27/2014 08:44 CALCULATION Nitrate+Nitrite-N 2.77 2.00 JM 03/27/2014 08:45 SM-450ONO3F Total Cadmium <2.0 2.0 KM 03/27/2014 12:21 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made JL to the work, the results, or the company in any advertising, news release, or other public'announcements without obtaining, our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-085-0203 Account Number: 45637 Submitted By: EDWARD STEPHENS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 98584 Sample Id : ADM BLEND A� A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (604) 271.6446 mmaleastern.com Project: ADM BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 3/25/2014 13:00:00 Date Received: 03/26/2014 00:00 Date Reported: 03/31/2014 Total Chromium 36 5 KM 03/27/2014 12:21 SW 6010C Total Nickel 15 5 KM 03/27/2014 12:21 SW 6010C Total Lead <5 5 KM 03/27/2014 12:21 SW 6010C Total Arsenic <3.0 3.0 KM 03/27/2014 12:21 SW 6010C Total Mercury <0.4 0.4 KM 03/27/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 03/27/2014 12:21 SW 6010C pH (Standard Units) * 7.63 2.00 JM 03/27/2014 08:44. SW-9045D Total Molybdenum <5 5 KM 03/27/2014 12:21 SW 6010C Chloride 342 200 JM 03/27/2014 09:45 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4 MIX, 3/25/2014 411/2014-4/30/2014 1.2026 2:1 MIX RATIO OF NG2 TO NG4 Na mg/I = (Na mg/kg x % Solids) = 100 = (3170 x 28.9300) -=100 = 917.081 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (149000 x 28.9300) _ 100 = 43105.7 Mg mg/I = (mg mg/kg x % Solids) = 100 = (1800 x 28.9300) _ 100 = 520.74 Na meq = Na mg/I _ Molec.Wgt.Na = 917.081 = 23 = 39.8731 Ca meq = Ca mg/1 _ Molec.Wgt.Ca = 43105.7 = 20 = 2155.28 Mg meq = Mg mg/I + Molec.Wgt.Mg = 520.74 = 12 = 43.395 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 39.8731 _ SgrRoot[0.5(2155.28+43.395)] = 1.20258 Printed: 2/18/2015 Page 1 12:13 Page: i of 2 Report Number: 14-121-0200 Account Number: 45637 Submitted By: MARSHALL PURYEAR Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 55126 Sample Id: NG-2 BLEND ADM A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 74,3-9401, Fax (804) 271.6.446 WWaleastem.com Project: NG-2 BLEND ADM NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/29/2014 16:00:00 Date Received: 05/01/2014 00:00 Date Reported: 05/06/2014 Total Solids * 34.47 344700 100.0 RD 05/01/2014 14:30 SM-2540G Moisture" 65.53 100.0 RD 05/01/201414:30 SM-2540G Total Kjeldahl Nitrogen 2.67 26700 10.0 JM 05/02/2014 08:50 SM-4500-NH3C-TKN Total Phosphorus 0.95 9530 100 KM 05/02/2014 12:24 SW 6010C Total Potassium 0.74 7380 100 KM 05/02/2014 12:24 SW 6010C Total Sulfur 5.90 59000 100 KM 05/02/2014 12:24 SW 6010C Total Calcium 11.20 112000 100 KM 05/02/2014 12:24 SW 6010C Total Magnesium 0.21 2090 100 KM 05/02/2014 12:24 SW 6010C Total Sodium 0.41 4130 100 KM 05/02/2014 12:24 SW 6010C Total Iron 2220 100 KM 05/02/2014 12:24 SW 6010C Total Aluminum 3000 100 KM 05/02/2014 12:24 SW 6010C Total Manganese 100 5 KM 05/02/2014 12:24 SW 6010C Total Copper 12 5 KM 05/02/2014 12:24 SW 6010C Total Zinc 171 5 KM 05/02/2014 12:24 SW 6010C Ammonia Nitrogen 0.22 2200 10.0 JM 05/02/2014 08:50 SM-4500-NH3C Organic N 2.45 24500 10.0 05/02/2014 08:50 CALCULATION Nitrate+Nitrite-N 7.83 2.00 JM 05/02/2014 08:50 SM450ONO3F Total Cadmium <2.0 2.0 KM 05/02/2014 12:24 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made R�m tp the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-121-0200 �YwY� A&L Eastern Laboratories, Inc. - Account Number: 45637 x 7621WhitepineRoad Richmond, Virginia.23237 (804)743-9401, Fax (804)271-6446 Submitted By: MARSHALL PURYEAR wwwaleastern.com Send To: ADM Project: NG-2 BLEND ADM SCOTT PHILLIPS NC CERT#257 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 REPORT OF ANALYSIS Date Sampled: 4/29/2014 16:00:00 Lab Number: 55126 Date Received: 05/01/2014 00:00 Sample Id: NG-2 BLEND ADM Date Reported: 05/06/2014 Total Chromium 40 5 KM 05/02/2014 12:24 SW 6010C Total Nickel 17 5 KM 05/02/2014 12:24 SW 6010C Total Lead <5 5 KM 05/02/2014 12:24 SW 6010C Total Arsenic 3.0 3.0 KM 05/02/2014 12:24 SW 6010C Total Mercury <0.4 0.4 KM 05/02/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 05/02/2014 12:24 SW 6010C pH (Standard Units) * 7.96 2.00 JM 05/02/2014 08:50 SW-9045D Total Molybdenum <5 5 KM 05/02/2014 12:24 SW 6010C Chloride 465 200 JM 05/02/2014 09:50 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. e-•i7 I.rel0 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4 MIX, 4/29/2014 511/2014-5/3112014 1.9621 2:1 MIX RATIO OF NG2 TO NG4 Na mg/I = (Na mg/kg x % Solids) = 100 =' (4130 x 34.4700) =100 = 1423.61 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (112000 x 34.4700) = 100 = 38606.4 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2090 x 34.4700) = 1 b0 = 720.423 Na meq = Na mg/I _ Molec.Wgt.Na = 1423.61 = 23 = 61.8961 Ca meq = Ca mg/I = Molec.Wgt.Ca = 38606.4 = 20 = 1930.32 Mg meq = Mg mg/I = Molec.Wgt.Mg = 720.423 = 12 = 60.0352 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 61.8961 = SgrRoot[0.5(1930.32+60.0352)] = 1.96206 9 Printed: 2/18/2015 Page 1 12:13 I Page: 1 of 2 Report Number: 14-141-0204 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 55481 .Sample Id : NG2421 BLEND v L A&L Eastern, Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (804) 271.WG wwwaleastern.COM Project: NG2421 BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 5/19/2014 14:30:00 Date Received: 05/21/2014 00:00 Date Reported: 05/23/2014 Total Solids * 30.74 307400 100.0 JM 05/21/2014 14:19 SM-2540G Moisture * 69.26 100.0 JM 05/21/2014 14:19 SM-2540G Total Kjeldahl Nitrogen 2.63 26300 10.0 JM 05/22/2014 09:20 SM-4500-NH3C-TKN Total Phosphorus 1.34 13400 100 KM 05/22/2014 13:31 SW 6010C Total Potassium 0.76 7610 100 KM 05/22/2014 13:31 SW 6010C Total Sulfur 7.92 79200 100 KM 05/22/2014 13:31 SW 6010C Total Calcium 13.80 138000 100 KM 05/22/2014 13:31 SW 6010C Total Magnesium 0.26 2600 100 KM 05/22/2014 13:31 SW 6010C Total Sodium 0.46 4570 100 KM 05/22/2014 13:31 SW 6010C Total Iron 3560 100 KM 05/22/2014 13:31 SW 6010C Total Aluminum 4700 100 KM 05/22/2014 13:31 SW 6010C Total Manganese 130 5 KM 05/22/2014 13:31 SW 6010C Total Copper 32 5 KM 05/22/2014 13:31 SW 6010C Total Zinc 303 5 KM 05/22/2014 13:31 SW 6010C Ammonia Nitrogen 0.31 3090 10.0 JM 05/22/2014 09:00 SM-4500-NI3C Organic N 2.32 23210 10.0 05/22/2014 09:00 CALCULATION Nitrate+Nitrite-N 6.18 2.00 JM 05/22/2014 09:20 SM-450ONO3F Total Cadmium <2.0 2.0 KM 05/22/2014 13:31 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-141-0204 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 55481 Sample Id : NG2421 BLEND A&L Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 www.aleastern.com Project: NG2421 BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 5/19/2014 14:30:00 Date Received: 05/21/2014 00:00 Date Reported: 05/23/2014 Total Chromium 53 5 KM 05/22/2014 13:31 SW 6010C Total Nickel 24 5 KM 05/22/2014 13:31 SW 6010C Total Lead 6 5 KM 05/22/2014 13:31 SW 6010C Total Arsenic <3.0 3.0 KM 05/22/2014 13:31 SW 6010C Total Mercury <0.4 0.4 KM 05/22/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 05/22/2014 13:31 SW 6010C pH (Standard Units) * 7.65 2.00 JM 05/22/2014 09:20 SW-9045D Total Molybdenum <5 5 KM 05/22/2014 13:31 SW 6010C Chloride 583 200 JM 05/22/201410:35 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N", "Al", "Fe", "Mn", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our priorWritten authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4 MIX, 5/19/2014 6/l/2014-6/30/2014 1.8468 2:1 MIX RATIO OF NG2 TO NG4 Na mg/1= (Na mg/kg x % Solids) _ 100 = (4570 x 30.7400) _ 100 = 1404.82 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (138000 x 30.7400) _ 100 = 42421.2 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2600 x 30.7400) = 100 = 799.24 Na meq = Na mg/1 = Molec.Wgt.Na = 1404.82 = 23 = 61.079 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 42421.2 _ 20 = 2121.06 Mg meq = Mg mg/I = Molec.Wgt.Mg = 799.24 _ 12 = 66.6033 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 61.079 + SgrRoot[0.5(2121.06+66.6033)] = 1.84679 Printed: 2/18/2015 Page 1 12:14 Page: 1 of 2 Report Number: 14-181-0205 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 56201 Sample Id : NG2 421 BLEND @P, A&L Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (804)743-9401 Fax (804)271-6446 wwwaleastem.com Project: NG2 421 BLEND NC #257 REPORT OF ANALYSIS Date Sampled: 6/27/2014 00:00:00 Date Received: 06/30/2014 00:00 Date Reported: 07/03/2014 Total Solids * 29.57 295700 100.0 JM 06/30/2014 14:35 SM-2540G Moisture * 70.43 100.0 JM 06/30/2014 14:35 SM-2540G Total Kjeldahl Nitrogen 3.01 30100 10.0 JM 07/01/2014 07:59 SM-4500-NH3C-TKN Total Phosphorus 1.53 15300 100 KM 07/01/2014 12:56 SW 6010C Total Potassium 0.84 8400 100 KM 07/01/2014 12:56 SW 6010C Total Sulfur 7.66 76600 100 KM 07/01/2014 12:56 SW 6010C Total Calcium 14.30 143000 100 KM 07/01/2014 12:56 SW 6010C Total Magnesium 0.28 2810 100 KM 07/01/2014 12:56 SW 6010C Total Sodium 0.55 5510 100 KM 07/01/2014 12:56 SW 6010C Total Iron 2610 100 KM 07/01/2014 12:56 SW 6010C Total Aluminum 3100 100 KM 07/01/2014 12:56 SW 6010C Total Manganese 162 5 KM 07/01/2014 12:56 SW 6010C Total Copper 13 5 KM 07/01/2014 12:56 SW 6010C Total Zinc 248 5 KM 07/01/2014 12:56 SW 6010C Ammonia Nitrogen 0.53 5310 10.0 JM 07/01/2014 07:59 SM-4500-NH3C Organic N 2.48 24790 10.0 07/01/2014 07:59 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 07/01/2014 08:00 SM-450ONO3F Total Cadmium <2.0 2.0 KM 07/01/2014 12:56 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients an may not be reproduced in whole or a nor may an reference be made P d Y P P rt, Y Y to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-181-0205 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 56201 Sample Id : NG2 421 BLEND A&L Eastern Laboratories, Inc. 7621 Whitepme Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastern.com Project: NG2 421 BLEND NC #257 REPORT OF ANALYSIS Date Sampled: 6/27/2014 00:00:00 Date Received: 06/30/2014 00:00 Date Reported: 07/03/2014 Total Chromium 57 5 KM 07/01/2014 12:56 SW 6010C Total Nickel 20 5 KM 07/01/2014 12:56 SW 6010C Total Lead <5 5 KM 07/01/2014 12:56 SW 6010C Total Arsenic <3.0 3.0 KM 07/01/2014 12:56 SW 6010C Total Mercury 1.7 0.4 KM 07/01/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 07/01/2014 12:56 SW 6010C pH (Standard Units) * 8.00 2.00 JM 07/01/2014 07:59 SW-9045D Total Molybdenum <5 5 KM 07/01/2014 12:56 SW 6010C Chloride 923 200 JM 07/01/2014 09:00 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE RPD WAS OUT OF LIMITS FOR "Hg". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. �� Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4 MIX, 6/27/2014 711/2014-7/31/2014 2.1439 2:1 MIX RATIO OF NG2 TO NG4 Na mg/I = (Na mg/kg x % Solids) _ 100 = (5510 x 29.5700) _ 100 = 1629.31 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (143000 x 29.5700) = 100 = 42285.1 Mg mg/1 = (mg mg/kg x % Solids) 100 = (2810 x 29.5700) - 100 = 830.917 Na meq = Na mg/1= Molec.Wgt.Na = 1629.31 = 23 = 70.8394 Ca meq = Ca mg/1= Molec.Wgt.Ca = 42285.1 + 20 = 2114.26 Mg meq = Mg mg/1= Molec.Wgt.Mg = 830.917 _ 12 = 69.2431 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 70.8394 = SgrRoot[0.5(2114.26+69.2431)] = 2.14395 Printed: 2/18/2015 Page 1 12:15 Page: 1 of 2 Report Number: 14-206-0203 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST.SE SOUTHPORT , NC 28461 Lab Number: 56693 Sample Id : ADM NG2-4 BLEND A&L EasternLaboratories, nc._ 99, 1 7621 Whitepine Road Richmond, Virginia,23237 (804) 743.9401 Fax (804) 271.6446 WwW aleastern.com Project: ADM NG2-4 BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/23/2014 13:30:00 Date Received: 07/25/2014 00:00 Date Reported: 07/31/2014 Total Solids * 26.98 269800 100.0 JM 07/25/2014 15:00 SM-2540G Moisture * 73.02 100.0 JM 07/25/2014 15:00 SM-2540G Total Kjeldahl Nitrogen 2.88 28800 10.0 JM 07/28/2014 09:00 SM-4500-NH3C-TKN Total Phosphorus 1.36 13600 100 KM 07/30/2014 16:12 SW 6010C Total Potassium 0.77 7670 100 KM 07/30/2014 16:12 SW 6010C Total Sulfur 7.55 75500 100 KM 07/30/2014 16:12 SW 6010C Total Calcium 13.10 131000 100 KM 07/30/2014 16:12 SW 6010C Total Magnesium 0.29 2920 100 KM 07/30/2014 16:12 SW 6010C Total Sodium 0.58 5770 100 KM 07/30/2014 16:12 SW 6010C Total Iron 2590 100 KM 07/30/2014 16:12 SW 6010C Total Aluminum 2700 100 KM 07/30/2014 16:12 SW 6010C Total Manganese 118 5 KM 07/30/2014 16:12 SW 6010C Total Copper 13 5 KM 07/30/2014 16:12 SW 6010C Total Zinc 207 5 KM 07/30/2014 16:12 SW 6010C Ammonia Nitrogen 0.45 4480 10.0 JM 07/28/2014 09:00 SM-4500-NH3C Organic N 2.43 24320 10.0- 07/28/2014 09:00 CALCULATION Nitrate+Nitrite-N 5.93 2.00 JM 07/28/2014 08:20 SM-45001N!03F Total Cadmium <2.0 2.0 KM 07/30/2014 16:12 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number:' 14-206-0203 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 56693 Sample Id : ADM NG2-4 BLEND A&L Eastern Laboratories, Inc:. 7621 Whitepine Road Rlchmond, Virginia 23237 (804) 743.9.401 Fax (804) 271-6446 www.aleastera.com Project: ADM NG2-4 BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/23/2014 13:30:00 Date Received: 07/25/2014 00:00 Date Reported: 07/31/2014 Total Chromium 58 Total Nickel 21 Total Lead <5 Total Arsenic <3.0 Total Mercury 0.7 Total Selenium <5.0 pH (Standard Units) * 7.23 Total Molybdenum <5 Chloride 698 Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. 5 KM 07/30/2014 16:12 SW 6010C 5 KM 07/30/2014 16:12 SW 6010C 5 KM 07/30/2014 16:12 SW 6010C 3.0 KM 07/30/2014 16:12 SW 6010C 0.4 KM 07/28/2014 09:00 SW-7471 B 5.0 KM 07/30/2014 16:12 SW 6010C 2.00 JM 07/28/2014 09:00 SW-9045D 5 KM 07/30/2014 16:12 SW 6010C 200 JM 07/28/2014 09:25 SM-4500CI-D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the' work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4 MIX, 7/23/2014 81112014-9/30/2014 2.2358 2:1 MIX RATIO OF NG2 TO NG4 Na mg/I = (Na mg/kg x % Solids) _ 100 = (5770 x 26.9800) =100 = 1556.75 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (131000 x 26.9800) _ 100 = 35343.8 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2920 x 26.9800) + 100 = 787.816 Na meq = Na mg/I = Molec.Wgt.Na = 1556.75 + 23 = 67.6846 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 35343.8 _ 20 = 1767.19 Mg meq = Mg mg/I = Molec.Wgt.Mg = 787.816 _ 12 = 65.6513 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 67.6846 = SgrRoot[0.5(1767.19+65.6513)] = 2.23585 Printed: 2/18/2015 Page 1 12:15 Page: i of 2 Report Number: 14-272-0200 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 57822 Sample Id: ADM NGB A&L Eastern Laboratories Inc.__ 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-6446 wwmaleastern.com Project: ADM NGB NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 9/24/2014 14:05:00 Date Received: 09/29/2014 00:00 Date Reported: 10/02/2014 Total Solids * 28.01 280100 100.0 MW 09/30/2014 08:44 SM-2540G Moisture * 71.99 100.0 MW 09/30/2014 08:44 SM-2540G Total Kjeldahl Nitrogen 2.51 25100 10.0 JM 09/30/2014 09:00- SM-4500-NH3C-TKN Total Phosphorus 1.21 12100 100 KM 09/30/2014 12:50 SW 6010C Total Potassium 0.83 8250 100 KM 09/30/2014 12:50 SW 6010C Total Sulfur 7.17 71700 100 KM 09/30/2014 12:50 SW 6010C Total Calcium 14.20 142000 100 KM 09/30/2014 12:50 SW 6010C Total Magnesium 0.29 2870 100 KM 09/30/2014 12:50 SW 6010C Total Sodium 0.57 5650 100 KM 09/30/2014 12:50 SW 6010C Total Iron 3020 100 KM 09/30/2014 12:50 SW 6010C Total Aluminum 4100 100 KM 09/30/2014 12:50 SW 6010C Total Manganese 180 5 KM 09/30/2014 12:50 SW 6010C Total Copper 13 5 KM 09/30/2014 12:50 SW 6010C Total Zinc 178 5 KM 09/30/2014 12:50 SW 6010C Ammonia Nitrogen 0.14 1430 10.0 JM 09/30/2014 09:00 SM-4500-NH3C Organic N 2.37 23670 10.0 09/30/2014 09:00 CALCULATION Nitrate+Nitrite-N 21.4 2.00 JM 09/30/2014 09:00 SM-450ONO3F Total Cadmium <2.0 2.0 KM 09/30/2014 12:50 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made 49L to the work, the results, or the company in any advertising, news release, orotherpublic announcements without obtaining ourprior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-272-0200 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 57822 Sample Id: ADM NGB NA&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 wwwaleasteworn Project: ADM NGB NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 9/24/2014 14:05:00 Date Received: 09/29/2014 00:00 Date Reported: 10/02/2014 Total Chromium 54 5 KM 09/30/2014 12:50 SW 6010C Total Nickel 21 5 KM 09/30/2014 12:50 SW 6010C Total Lead <5 5 KM 09/30/2014 12:50 SW 6010C Total Arsenic <3.0 3.0 KM 09/30/2014 12:50 SW 6010C Total Mercury <0.4 0.4 KM 09/30/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 09/30/2014 12:50 SW 6010C pH (Standard Units) * 7.63 2.00 JM ' 09/30/2014 09:49 SW-9045D Total Volatile Solids 32.75 327500 100.0 MW 09/30/2014 08:44 SM-2540G Total Molybdenum <5 5 KM 09/30/2014 12:50 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. LRBWAS OUT OF LIMITS FOR "NO3/NO2-N". QUALIFIER: THELAB THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca", "Na", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4 MIX, 9/24/2014 10/112014-10/31/2014 2.1462 2:1 MIX RATIO OF NG2 TO NG4 Na mg/I = (Na mg/kg x % Solids) = 100 = (5650 x 28.0100) =100 = 1582.57 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (142000 x 28.0100) + 100 = 39774.2 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2870 x 28.0100) =100 = 803.887 Na meq = Na mg/I = Molec.Wgt.Na = 1582.57 + 23 = 68.8072 Ca meq = Ca mg/I + Molec.Wgt.Ca = 39774.2 _ 20 = 1988.71 Mg meq = Mg mg/I = Molec.Wgt.Mg = 803.887 = 12 = 66.9906 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 68.8072 _ SgrRoot[0.5(1988.71+66.9906)] = 2.14619 Printed: 2/18/2015 Page 1 12:17 Page: 1 of 2 Report Number: 14-297-0206 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 58342 Sample Id: ADM NG BLEND Eastern Laboratories, Inc. 7621 Whitepine Road 'Richmond, Virginia-23237 (804) 743.9401 Fax (804) 271.6446 wwwaleistem.com Project: ADM NG BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 10/23/2014 11:30:00 Date Received: 10/24/2014 00:00 Date Reported: 10/30/2014 Total Solids " 29.25 292500 100.0 JM 10/24/2014 15:00 SM-2540G Moisture " 70.75 100.0 JM 10/24/2014 15:00 SM-254OG Total Kjeldahl Nitrogen 2.50 25000 10.0 JM 10/27/2014 08:55 SM-4500-NH3C-TKN Total Phosphorus 1.05 10500 100 KM 10/27/2014 14:56 SW 6010C Total Potassium 0.72 7150 100 KM 10/27/2014 14:56 SW 6010C Total Sulfur 7.70 77000 100 KM 10/27/2014 14:56 SW 6010C Total Calcium 13.30 133000 100 KM 10/27/2014 14:56 SW 6010C Total Magnesium 0.21 2070 100 KM 10/27/2014 14:56 SW 6010C Total Sodium 0.54 5390 100 KM 10/27/2014 14:56 SW 6010C _ Total Iron 3240 100 KM 10/27/2014 14:56 SW 6010C Total Aluminum 2600 100 KM 10/27/2014 14:56 SW 6010C Total Manganese 106 5 KM 10/27/2014 14:56 SW 6010C Total Copper 10 5 KM 10/27/2014 14:56 SW 6010C Total Zinc 163 5 KM 10/27/2014 14:56 SW 6010C Ammonia Nitrogen 0.19 1880 10.0 JM 10/27/2014 08:55 SM-4500-NH3C Organic N 2.31 23120 10.0 10/27/2014 08:55 CALCULATION Nitrate+Nitrite-N 99.8 2.00 JM 10/27/2014 00:00 SM-450ONO3F Total Cadmium 2.0 2.0 KM 10/27/2014 14:56 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. AIL \//) Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcementswithout obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-297-0206 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 58342 Sample Id: ADM NG BLEND loiA&L EasternLaboratories' Inc. - Z621 Whitepine Road Richmond, Virginia 23237 (e04).743-9401 -Fax (804)271.6446 wwwaleastern.com Project: ADM NG BLEND NC CERT#257 REPORT OFANALYSIS Date Sampled: 10/23/2014 11:30:00 Date Received: 10/24/2014 00:00 Date Reported: 10/30/2014 Total Chromium 49 5 KM 10/27/2014 14:56 SW 6010C Total Nickel 23 5 KM 10/27/2014 14:56 SW 6010C Total Lead <5 5 KM 10/27/2014 14:56 SW 6010C Total Arsenic <3.0 3.0 KM 10/27/2014 14:56 SW 6010C Total Mercury <0.4 0.4 KM 10/27/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 10/27/2014 14:56 SW 6010C pH (Standard Units) 8.25 2.00 JM 10/27/2014 08:55 SW-90450 Total Volatile Solids 31.92 319200 100.0 JM 10/24/2014 15:00 SM-2540G Total Molybdenum <5 5 KM 10/27/2014 14:56 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Cr". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all Nseries is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) 0 Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4 MIX, 10/23/2014 11/l/2014-11/30/2014 2.1700 2:1 MIX RATIO OF NG2 TO NG4 Na mg/1= (Na mg/kg x % Solids) _ 100 = (5390 x 29.2500) _ 100 = 1576.58 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (133000 x 29.2500) = 100 = 38902.5 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2070 x 29.2500) = 100 = 605.475 Na meq = Na mg/I = Molec.Wgt.Na = 1576.58 = 23 = 68.5467 Ca meq = Ca mg/I = Molec.Wgt.Ca = 38902.5 _ 20 = 1945.13 Mg meq = Mg mg/I = Molec.Wgt.Mg = 605.475 _ 12 = 50.4563 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 68.5467 = SgrRoot[0.5(1945.13+50.4563)] = 2.17004 Printed: 2/18/2015 Page 1 12:18 Page: 1 of 2 Report Number: 14-325-0200 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 58869 Sample Id : ADM NG BLEND A&L Eastern Laboratories Inc. 7621 Whitepine Road 'Richmond, Virginia-23237 (804) 743-9401Fax (BO.4) 271.6446 www,aleastem.com Project: ADM NG BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 11/18/2014 09:00:00 Date Received: 11/21/2014 00:00 Date Reported: 12/02/2014 Total Solids 27.41 '274100 100.0 BW 11/21/2014 15:00 SM-2540G Moisture * 72.59 100.0 BW 11/21/2014 15:00 SM-2540G Total Kjeldahl Nitrogen 2.46 24600 10.0 JM 11/24/2014 09:24 SM-4500-NH3C-TKN Total Phosphorus 0.71 7070 100 KM 11/24/2014 11:01 SW 6010C Total Potassium 0.47 4740 100 KM 11/24/2014 11:01 SW 6010C Total Sulfur 6.62 66200 100 KM 11/24/2014 11:01 SW 6010C Total Calcium 10.90 109000 100 KM 11/24/2014 11:01 SW 6010C Total Magnesium 0.14 1370 100 KM 11/24/2014 11:01 SW 6010C Total Sodium 0.34 3420 100 KM 11/24/2014 11:01 SW 6010C Total Iron 1680 100 KM 11/24/2014 11:01 SW 6010C Total Aluminum 2500 100 KM 11/24/2014 11:01 SW 6010C Total Manganese 76 5 KM 11/24/2014 11:01 SW 6010C Total Copper 9 5 KM 11/24/2014 11:01 SW 6010C Total Zinc 117 5 KM 11/24/2014 11:01 SW 6010C Ammonia Nitrogen 0.30 3030 10.0 JM 11/24/2014 09:24 SM-4500-NH3C Organic N 2.16 21570 10.0 11/24/2014 09:24 CALCULATION Nitrate+Nitrite-N 17.5 2.00 JM 11/26/2014 08:05 SM-450ONO3F Total Cadmium <2.0 2.0 KM 11/24/2014 11:01 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-325-0200 Account Number: 45637 Submitted By: CREIGHTON BROWN ' Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 58869 Sample Id: ADM NG BLEND A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 .(804) 743.9401 Fax (804) 271-696 www,aleastem.com Project: ADM NG BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 11/18/2014 09:00:00 Date Received: 11/21/2014 00:00 Date Reported: 12/02/2014 Total Chromium 51 5 KM 11/24/2014 11:01 SW 6010C Total Nickel 21 5 KM 11/24/2014 11:01 SW 6010C Total Lead <5 5 KM 11/24/2014 11:01 SW 6010C Total Arsenic <3.0 3.0 KM 11/24/2014-11:01 SW 6010C Total Mercury <0.4 0.4 KM 11/24/2014 12:00 SW-7471 B Total Selenium <5.0 5.0 KM 11/24/2014 11:01 SW 6010C pH (Standard Units) * 7.88 2.00 JM 11/24/2014 09:24 SW-9045D Total Volatile Solids 25.94 259400 100.0 BW 11/21/2014 15:00 SM-2540G Total Molybdenum <5 5 KM 11/24/2014 11:01 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB IS OUT OF LIMITS FOR "Mn", THE MATRIX XPIKE IS OUT OF LIMITS FOR "Se", AND "S", ALL OTHER QA/QC IS WITHIN LIMITS. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2044-01-NG2421-NC ADM CORP., NC NITRO GRO 2&4-MIX, 11/18/2014 12/l/2014-12/31/2014 1.4759 2:1 MIX RATIO OF NG2 TO NG4 Na mg/I = (Na mg/kg x % Solids) = 100 = (3420 x 27.4100) =100 = 937.422 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (109000 x 27.4100) = 100 = 29876.9 Mg mg/I = (mg mg/kg x % Solids) = 100 = (1370 x 27.4100) = 100 = 375.517 Na meq = Na mg/I _ Molec.Wgt.Na = 937.422 _ 23 = 40.7575 Ca meq = Ca mg/I = Molec.Wgt.Ca = 29876.9 = 20 = 1493.85 Mg meq = Mg mg/I = Molec.Wgt.Mg = 375.517 = 12 = 31.2931 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 40.7575 = SgrRoot[0.5(1493.85+31.2931)] = 1.47594 Printed: 2/18/2015 Page 1 12:18 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004500 Facility Name: ARCHER DANIELS MIDLAND CORP., NC NPDES# : NCO027065 or WQ# (residual only) WWTP Name: ARCHER DANIELS MIDLAND Residuals Analysis Data Product Type Date Sampled (grab) or Date Composited Percent Solids PARAMETERS (mg/kg dry weight; Arsenic Cadmium Mercury Chromium Copper Lead Molybdenum Nickel Selenium Zinc Total Phosphorus TKN Ammonia -Nitrogen Nitrate and Nitrite NG2C NG2C NG2C 12/19/13 01/27/14 02/26/14 19.26 16.97 17.63 Laboratory A&L Eastern Laboratories Inc. NG2C NG2C NG2C NG2C NG2C NG2C 04/29/14 05/20/14 06/27/14 07/23/14 08/20/14 09/24/14 17.56 15.13 17.33 15.81 17.34 18.25 4 3 <3 4 4 4 3 3 4 3 <2 <2 <2 <2 <2 <2 <2 <2 <0.4 <0.4 <0.4 <0.4 <0.4 0.4 <0.4 <0.4 <0.4 45 49 55 54 72 101 109 92 82 18 14 16 16 22 21 25 26 21 <5 <5 <5 <5 <5 <5 <5 <5 <5 6 <5 <5 <5 <5 <5 <5 <5 <5 22 19 22 23 28 36 38 38 30 <5 <5 <5 <5 <5 <5 <5 <5 <5 227 219 259 311 380 414 394 408 334 23300 26900 24200 22600 29700 26100 31500 26700 27500 55600 65400 64100 62600 64700 57700 61200 51800 52000 2600 2470 5050 4440 3970 6230 4360 2600 2850 11.9 11.2 61.3 10.8 7.27 8.66 17.7 704 57.5 DENR FORM RSSF (5/2003) Printed: Wednesday - February 18, 2015 at 12:02:02 for: 2044 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004500 Facility Name: ARCHER DANIELS MIDLAND CORP., NC NPDES# : NCO027065 or WQ# (residual only) WWTP Name: ARCHER DANIELS MIDLAND' Residuals. Analysis Data Product Type NG2C NG2C Date Sampled (grab) or 10/23/14 11/18/14 Date Composited Percent Solids 15.21 14.10 PARAMETERS (mg/kg dry weight) Arsenic 4 <3 Cadmium <2 <2 Mercury <0.4 <0.4 Chromium 67 62 Copper 19 19 Lead <5 <5 Molybdenum <5 <5 Nickel 25 23 Selenium <5 <5 Zinc 318 292 Total Phosphorus 24300 23400 TKN 59500 72300 Ammonia -Nitrogen 2700 2700 Nitrate and Nitrite 25.6 594 Laboratory A&L Eastern Laboratories Inc. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure. that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant pen,4ties for submg_ false information,. including the possibility of fines and imprisonment for knowing violations." Date �' o75 "/S OF Page: 2 DENR FORM RSSF (5/2003) Printed: Wednesday - February 18, 2015 at 12:02:02 for: 2044 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. . Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004500 Laboratory Facility Name: ARCHER DANIELS MIDLAND CORP., NC A&L Eastern Laboratories Inc. NPDES# : NCO027065 or WQ# (residual only) WWTP Name: ARCHER DANIELS MIDLAND Residuals Analysis Data Product Type NG2C NG2C NG2C NG2C NG2C NG2C NG2C NG2C NG2C Date Sampled(grab)or 12/19/13 01/27/14 02/26/14 04/29/14 05/20/14 06/27/14 07/23/14 08/20/14 09/24/14 Date Composited Percent Solids 19.26 16.97 17.63 17.56 15.13 17.33 15.81 17.34 18.25 PARAMETERS (mg/kg dry weight) J Aluminum 4100 6000 4200 4800 - 5100 5100 5900 5800 5300 Calcium 126000 93900 110000 114000 103000 128000 99200 116000 133000 Magnesium 4180 4760 4510 4720 5480 5550 6140 5720 6000 pH 7.63 7.48 7.82 7.63 7.77 7.74 7.42 7.67 8.02 Potassium 13700 16800 15800 14500 14800 14800 13900 11700 15400 Sodium 4290 5010 4860 6520 7130 7560 5500 6790 7110 DENR FORM RSSF-B (7/2002) Printed: Wednesday - February 18, 2015 at 12:02:54 for: 2044 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004500 Facility Name: ARCHER DANIELS MIDLAND CORP., NC NPDES# : NCO027065 or WQ# (residual only) WWTP Name: ARCHER DANIELS MIDLAND Residuals Analysis Data Product Type NG2C NG2C Date Sampled (grab) or 10/23/14 11/18/14 Date Composited Percent Solids 15.21 14.10 PARAMETERS (mg/kg dry weight) Aluminum 4600 4400 Calcium 102000 81800 Magnesium 4680 4640 pH 7.60 7.42 Potassium 13500 12900 Sodium 6670 5580 Laboratory A&L Eastern Laboratories Inc. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment, for knowing violations." X //" (S NATURE OF PRE R - Data Not Reported or Data Not Required Date �-o?5 '/S— Page: 2 DENR FORM RSSF-B (7/2002) Printed: Wednesday _ February 18, 2016 at 12:02:54 for: 2044 01 Page: 1 of 2 Report Number: 13-354-0200 Account Number: 45637 Submitted By: SCOTT COE Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 97210 Sample Id: NG2C � L A&L Eastemlaboratories, .Inc:. •7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-6446 wwwaleastern.com Project: NG2C NC CERT#257 REPORT OF ANALYSIS Date Sampled: 12/19/2013 07:40:00 Date Received: 12/20/2013 00:00 Date Reported: 01/02/2014 Total Solids * 19.26 192600 100.0 JM 12/20/2013 14:44 SM-2540G Moisture * 80.74 -100.0 JM 12/20/2013 14:44 SM-2540G Total_Kjeldahl Nitrogen 5.56 55600 10.0 JM 12/23/2013 08:35 SM-4500-NH3C-TKN Total Phosphorus 2.33 23300 100 KM 12/23/2013 11:47 SW 6010C Total Potassium 1.37 13700 100 KM 12/23/2013 11:47 SW 6010C Total Sulfur 2.17 21700 100 KM 12/23/2013 11:47 SW 6010C Total Calcium 12.60 126000 100 KM 12/23/2013 11:47 SW 6010C Total Magnesium 0.42 4180 100 KM 12/23/2013 11:47 SW 6010C Total Sodium 0.43 4290 100 KM 12/23/2013 11:47 SW 6010C Total Iron 2950 100 KM 12/23/2013 11:47 SW 6010C Total Aluminum 4100 100 KM 12/23/2013 11:47 SW 6010C Total Manganese 232 5 KM 12/23/2013 11:47 SW 6010C Total Copper 18 5 KM 12/23/2013 11:47 SW 6010C Total Zinc 227 5 KM 12/23/2013 11:47 SW 6010C Ammonia Nitrogen 0.26 2600 10.0 JM 12/23/2013 08:35 SM-4500-NH3C Organic N 5.30 53000 10.0 12/23/2013 08:35 CALCULATION Nitrate+Nitrite-N 11.9 2.00 JM 12/23/2013 08:50 SM-450ONO3F Total Cadmium 3.0 2.0 KM 1.2/23/2013 11:47 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 13-354-0200 Account Number: 45637 Submitted By: SCOTT COE Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 97210 Sample Id: NG2C p� A&L Eastern Laboratories, Inc.- 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 wwwaleastem.cotn Project: NG2C NC CERT#257 REPORT OF ANALYSIS Date Sampled: 12/19/2013 07:40:00 Date Received: 12/20/2013 00:00 Date Reported: 01/02/2014 Total Chromium 45 5 KM 12/23/2013 11:47 SW 6010C Total Nickel 22 5 KM 12/23/2013 11:47 SW 6010C Total Lead <5 5 KM 12/23/2013 11:47 SW 6010C Total Arsenic 4.0 3.0 KM 12/23/2013 11:47 SW 6010C Total Mercury <0.4 0.4 KM 12/23/2013 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 12/23/2013 11:47 SW 6010C pH (Standard Units) * 7.63 2.00 JM 12/23/2013 08:35 SW-9045D Total Molybdenum 6 5 KM 12/23/2013 11:47 SW 6010C Chloride 914 200 JM 12/23/2013 09:50 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR."Mn" AND "Mo". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca", "Se", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2C-NC ADM CORP., NC NITRO GRO 2 CAKE 12/19/2013 1/1/2014-1/31/2014 1.4198 Na mg/I = (Na mg/kg x % Solids) = 100 = (4290 x 19.2600) + 100 = 826.254 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (126000 x 19.2600) _ 100 = 24267.6 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (4180 x 19.2600) _ 100 = 805.068 Na meq = Na mg/I + Molec.Wgt.Na = 826.254 = 23 = 35.9241 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 24267.6 _ 20 = 1213.38 Mg meq = Mg mg/I + Molec.Wgt.Mg = 805.068 = 12 = 67.089 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 35.9241 + SgrRoot[0.5(1213.38+67.089)] = 1.41976 Printed: 2/18/2015 Page 1 12:11 Page: 1 of 2 Report Number: 14-028-0205 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number:- 97668 Sample Id: NG2 .A&L Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 www.aleastern.com Project: ADM - NG2 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/27/2014 11:00:00 Date Received: 01/28/2014 00:00 Date Reported: 02/03/2014 Total Solids * 16.97 169700 100.0 JM 01/28/2014 15:00 SM-2540G Moisture * 83.03 100.0 JM 01/28/2014 15:00 SM-2540G Total Kjeldahl Nitrogen 6.54 65400 10.0 JM 01/29/2014 09:29 SM-4500-NH3C-TKN Total Phosphorus 2.69 26900 100 KM 01/29/2014 13:31 SW 6010C Total Potassium 1.68 16800 100 KM 01/29/2014 13:31 SW 6010C Total Sulfur 1.87 18700 100 KM 01/29/2014 13:31 SW 6010C Total Calcium 9.39 93900 100 KM 01/29/2014 13:31 SW 6010C Total Magnesium 0.48 4760 100 KM 01/29/2014 13:31 SW 6010C Total Sodium 0.50 5010 100 KM 01/29/2014 13:31 SW 6010C Total Iron 3460 100 KM 01/29/2014 13:31 SW 6010C Total Aluminum 6000 100 KM 01/29/2014 13:31 SW 6010C Total Manganese 188 5 KM 01/29/2014 13:31 SW 6010C Total Copper 14 5 KM 01/29/2014 13:31 SW 6010C Total Zinc 219 5 KM 01/29/2014 13:31 SW 6010C Ammonia Nitrogen 0.25 2470 10.0 JM 01/29/2024 00:00 SM-4500-NI3C Organic N 6.29 62930 10.0 01/29/2014 09:29 CALCULATION Nitrate+Nitrite-N 11.2 2.00 JM 01/29/2014 09:30 SM-450ONO3F Total Cadmium <2.0 2.0 KM 01/29/2014 13:31 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-028-0205 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 97668 Sample Id : NG2 AFL Eastern Laboratories, Inc. X 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 www.aleastern.com Project: ADM - NG2 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/27/2014 11:00:00 Date Received: 01/28/2014 00:00 Date Reported: 02/03/2014 Total Chromium 49 5 KM 01/29/2014 13:31 SW 6010C Total Nickel 19 5 KM 01/29/2014 13:31 SW 6010C Total Lead <5 5 KM 01/29/2014 13:31 SW 6010C Total Arsenic 3.0 3.0 KM 01/29/2014 13:31 SW 6010C Total Mercury <0.4 0.4 KM 01/29/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 01/29/2014 13:31 SW 6010C pH (Standard Units) * 7.48 2.00 JM 01/29/2014 09:29 SW-9045D Total Molybdenum <5 5 KM 01/29/2014 13:31 SW 6010C Chloride 786 200 JM 01/29/201410:30 SM-4500CI-D Comments: CHLRODE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2C-NC ADM CORP., NC NITRO GRO 2 CAKE 1/27/2014 2/l/2014-3/9/2014 1.7784 Na mg/I = (Na mg/kg x % Solids) + 100 = (5010 x 16.9700) =100 = 850.197 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (93900 x 16.9700) = 100 = 15934.8 Mg mg/I = (mg mg/kg x % Solids) = 100 = (4760 x 16.9700) _ 100 = 807.772 Na meq = Na mg/I + Molec.Wgt.Na = 850.197 - 23 = 36.9651 Ca meq = Ca mg/I = Molec.Wgt.Ca = 15934.8 _ 20 = 796.741 Mg meq = Mg mg/I + Molec.Wgt.Mg = 807.772 _ 12 = 67.3143 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 36.9651 _ SgrRoot[0.5(796.741+67.3143)] = 1.77843 Printed: 2/18/2015 Page 1 12:12 Page: 1 of 2 Report Number: 14-059-0203 a � � A&L Eastern Laboratories,, Inc.. Account Number: 45637 •7621 Whitepine Road Richmond, Virginia 23237' .(804) 743-9401 Fax (804) 271-6446 Submitted By: EDWARD STEPHENS wwwaleasteni.com Send To: ADM _ Project.: ADM NG2 SCOTT PHILLIPS NC CERT#257 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 REPORT OF ANALYSIS Date Sampled: 2/26/2014 10:15:00 Lab Number: 98169 Date Received: 02/28/2014 00:00 Sample Id: ADM NG2 Date Reported: 03/07/2014 QUANTITATION D• •. Total Solids * 17.63 176300 100.0 JM 03/04/2014 09:20 SM-2540G Moisture * 82.37 100.0 JM 03/04/2014 09:20 SM-2540G Total Kjeldahl Nitrogen 6.41 64100 10.0 JM 03/03/2014 07:54 SM-4500-NH3C-TKN Total Phosphorus 2.42 24200 100 KM 03/03/2014 12:51 SW 601 OC Total Potassium 1.58 15800 100 KM 03/03/2014 12:51 SW 601 OC Total Sulfur 2.59 25900 100 KM 03/03/2014 12:51 SW 601 OC Total Calcium 11.00 110000 100 KM 03/03/2014 12:51 SW 601 OC Total Magnesium 0.45 4510 100 KM 03/03/2014 12:51 SW 601 OC Total Sodium 0.49 4860 100 KM 03/03/2014 12:51 SW 601 OC Total Iron 2990 100 KM 03/03/2014 12:51 SW 601 OC Total Aluminum 4200 100 KM 03/03/2014 12:51 SW 601 OC Total Manganese 218 5 KM 03/03/2014 12:51 SW 601 OC Total Copper 16 5 KM 03/03/2014 12:51 SW 601 OC Total Zinc 259 5 KM 03/03/2014 12:51 SW 601 OC Ammonia Nitrogen 0.51 5050 10.0 JM 03/03/2014 07:54 SM-4500-NH3C Organic N 5.90 59050 10.0 03/03/2014 07:54 CALCULATION Nitrate+Nitrite-N 61.3 2.00 JM 03/03/2014 07:55 SM-450ONO3F Total Cadmium <2.0 2.0 KM 03/03/2014 12:51 SW 601 OC All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-059-0203 Account Number: 45637 Submitted By: EDWARD STEPHENS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 98169 Sample Id: ADM NG2 A&L Eastern Laboratories, Inc, 7621 Whitepine Road Ricfimond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastemiom Project: ADM NG2 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 2/26/2014 10:15:00 Date Received: 02/28/2014 00:00 Date Reported: 03/07/2014 Total Chromium 55 5 KM 03/03/2014 12:51 SW 6010C Total Nickel 22 5 KM 03/03/2014 12:51 SW 6010C Total Lead <5 5 KM 03/03/2014 12:51 SW 6010C Total Arsenic <3.0 3.0 KM 03/03/2014 12:51 SW 6010C Total Mercury <0.4 0.4 KM 03/03/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 03/03/2014 12:51 SW 6010C pH (Standard Units) * 7.82 2.00 JM 03/03/2014 09:09 SW-9045D Total Molybdenum <5 5 KM 03/03/2014 12:51 SW 6010C Chloride 757 200 MW 03/03/2014 08:10 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "A[", "CA", AND "NO3/NO2-N". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. .61 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2C-NC ADM CORP., NC NITRO GRO 2 CAKE 2/26/2014 3/10/2014-4/30/2014 1.6369 Na mg/1= (Na mg/kg x % Solids) _ 100 = (4860 x 17.6300) _ 100 = 856.818 Ca mg/1= (Ca mg/kg x % Solids) _ 100 = (110000 x 17.6300) _ 100 = 19393 Mg mg/I = (mg mg/kg x % Solids) = 100 = (4510 x 17.6300) _ 100 = 795.113 Na meq = Na mg/I = Molec.Wgt.Na = 856.818 -= 23 = 37.253 Ca meq = Ca mg/1 _ Molec.Wgt.Ca = 19393 = 20 = 969.65 Mg meq = Mg mg/I -= Molec.Wgt.Mg = 795.113 _ 12 = 66.2594 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 37.253 = SgrRoot[0.5(969.65+66.2594)] = 1.63687 Printed: 2/18/2015 Page 1 12:13 Page: 1 of 2 Report Number: 14-121-0203 Account Number: 45637 Submitted By: MARSHALL PURYEAR Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 55129 Sample Id : NG2 NOT BLEND ADM @{YY A&L Eastern ,Laboratories, Inc. ?� 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 .Fax (804) 271.696 0 wwwaleastern.com Project: ADM/NG2 NOT BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/29/2014 13:00:00 Date Received: 05/01/2014 00:00 Date Reported: 05/06/2014 Total Solids 17.56 175600 100.0 RD 05/01/2014 14:30 SM-2540G Moisture * 82.44 100.0 RD 05/01/2014 14:30 SM-2540G Total Kjeldahl Nitrogen 6.26 62600 10.0 JM 05/02/2014 08:50 SM-4500-NH3C-TKN Total Phosphorus 2.26 22600 100 KM 05/02/2014 12:24 SW 6010C Total Potassium 1.45 14500 100 KM 05/02/2014 12:24 SW 6010C Total Sulfur 1.79 17900 100 KM 05/02/2014 12:24 SW 6010C Total Calcium 11.40 114000 100 KM 05/02/2014 12:24 SW 6010C Total Magnesium 0.47 4720 100 KM 05/02/2014 12:24 SW 6010C Total Sodium 0.65 6520 100 KM 05/02/2014 12:24 SW 6010C Total Iron 3120 100 KM 05/02/2014 12:24 SW 6010C Total Aluminum 4800 100 KM 05/02/2014 12:24 SW 6010C Total Manganese 229 5 KM 05/02/2014 12:24 SW 6010C Total Copper 16 5 KM 05/02/2014 12:24 SW 6010C Total Zinc 311 5 KM 05/02/2014 12:24 SW 6010C Ammonia Nitrogen 0.44 4440 10.0 JM 05/02/2014 08:50 SM-4500-NH3C Organic N 5.82 58160 10.0 05/02/2014 08:50 CALCULATION Nitrate+Nitrite-N 10.8 2.00 JM 05/02/2014 08:50 SM-450ONO3F Total Cadmium <2.0 2.0 KM 05/02/2014 12:24 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-121-0203 Account Number: 45637 Submitted By: MARSHALL PURYEAR Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 55129 Sample Id: NG2 NOT BLEND ADM A&L Eastern Laboratories,, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (604) 743.9401 Fax (604) 271.6446_ www.aleastem.com Project: ADM/NG2 NOT BLEND NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/29/2014 13:00:00 Date Received: 05/01/2014 00:00 Date Reported: 05/06/2014 Total Chromium 54 5 KM 05/02/2014 12:24 SW 6010C Total Nickel 23 5 KM 05/02/2014 12:24 SW 6010C Total Lead <5 5 KM 05/02/2014 12:24 SW 6010C Total Arsenic 4.0 3.0 KM 05/02/2014 12:24 SW 6010C Total Mercury <0.4 0.4 KM 05/02/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 05/02/2014 12:24 SW 6010C pH (Standard Units) * 7.63 2.00 JNI 05/02/2014 08:50 SW-9045D Total Molybdenum <5 5 KM 05/02/2014 12:24 SW 6010C Chloride 1540 200 u JM 05/02/2014 09:50 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be -made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2C-NC ADM CORP., NC NITRO GRO 2 CAKE 4/29/2014 511/2014-5/31/2014 2.1521 Na mg/I = (Na mg/kg x % Solids) _ 100 = (6520 x 17.5600) _ 100 = 1144.91 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (114000 x 17.5600) = 100 = 20018.4 Mg mg/I = (mg mg/kg x % Solids) = 100 = (4720 x 17.5600) _ 100 = 828.832 Na meq = Na mg/1 + Molec.Wgt.Na = 1144.91 _ 23 = 49.7788 Ca meq = Ca mg/I = Molec.Wgt.Ca = 20018.4 = 20 = 1000.92 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 828.832 _ 12 = 69.0693 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 49.7788 = SgrRoot[0.5(1000.92+69.0693)] = 2.15214 Printed: 2/18/2015 Page 1 12:14 Page: 1 of 2 Report .Number: 14-141-0205 Account Number: 45637 Submitted By: - LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 55482 Sample Id : NG2 STRAIGHT CAKE �L A&L Eastern Laboratories, Inc._ .7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271.6446 wwwaleastem.com Project: NG2 STRAIGHT CAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 5/20/2014 10:30:00 Date Received: 05/21/2014 00:00 Date Reported: 05/23/2014 Total Solids * 15.13 151300 100.0 JM 05/21/2014 14:19 SM-2540G Moisture * 84.87 100.0 JM 05/21/2014 14:19 SM-2540G Total Kjeldahl Nitrogen 6.47 64700 10.0 JM 05/22/2014 09:20 SM-4500-NH3C-TKN Total Phosphorus 2.97 29700 100 KM 05/22/2014 13:31 SW 6010C Total Potassium 1.48 14800 100 KM 05/22/2014 13:31 SW 6010C Total Sulfur 2.31 23100 100 KM 05/22/2014 13:31 SW 6010C Total Calcium 10.30 103000 100 KM 05/22/2014 13:31 SW 6010C Total. Magnesium 0.55 5480 100 KM 05/22/2014 13:31 SW 6010C Total Sodium 0.71 7130 100 KM 05/22/2014 13:31 SW 6010C Total Iron 3830 100 KM 05/22/2014 13:31 SW 6010C Total Aluminum 5100 100 KM 05/22/2014 13:31 SW 6010C Total Manganese 228 5 KM 05/22/2014 13:31 SW 6010C Total Copper 22 5 KM 05/22/2014 13:31 SW 6010C Total Zinc 380 5 KM 05/22/2014 13:31 SW 6010C Ammonia Nitrogen 0.40 3970 10.0 JM 05/22/2014 09:00 SM-4500-NH3C Organic N 6.07 60730 10.0 05/22/2014 09:00 CALCULATION Nitrate+Nitrite-N 7.27 2.00 JM 05/22/2014 09:20 SM-450ONO3F Total Cadmium <2.0 2.0 KM 05/22/2014 13:31 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other -public announcements without obtaining our prior written authorization. Debbie Holt i i Page: 2 of 2 Report Number: 14-141-0205 � � ,AU Eastern Laboratories, Inc.. Account Number: 45637 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Submitted By: LUKE STOWERS WWWAeastern.com Send To: ADM Project: NG2 STRAIGHT CAKE SCOTT PHILLIPS ! NC CERT#257 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 REPORT OF ANALYSIS Date Sampled: 5/20/2014 10:30:00 Lab Number: 55482 Date Received: 05/21/2014 00:00 Sample Id : NG2 STRAIGHT CAKE Date Reported: 05/23/2014 Total Chromium 72 5 KM 05/22/2014 13:31 SW 6010C Total Nickel 28 5 KM 05/22/2014 13:31 SW 6010C Total Lead <5 5 KM 05/22/2014 13:31 SW 6010C Total Arsenic 4.0 3.0 KM 05/22/2014 13:31 SW 6010C Total Mercury <0.4 0.4 KM 05/22/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 05/22/2014 13:31 SW 6010C pH (Standard Units) * 7.77 2.00 JM 05/22/2014 09:20 SW-9045D Total Molybdenum <5 5 KM 05/22/2014 13:31 SW 6010C Chloride 2090 200 JM 05/22/201410:35 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N", "Al", "Fe", "Mn", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive an'!d confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , (` to the work, the results, or the company in any, advertising, news release, or other public announcements without obtaining our prior written authorization. I Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2C-NC ADM CORP., NC NITRO GRO 2 CAKE 5/20/2014 611/2014-6/30/2014 2.2774 Na mg/I = (Na mg/kg x % Solids) + 100 = (7130 x 15.1300) =100 = 1078.77 Ca mg/1= (Ca mg/kg x % Solids) _ 100 = (103000 x 15.1300) + 100 = 15583.9 Mg mg/I = (mg mg/kg x % Solids) + 100 = (5480 x 15.1300) + 100 = 829.124 Na meq = Na mg/I + Molec.Wgt.Na = 1078.77 + 23 = 46.903 Ca meq = Ca mg/I = Molec.Wgt.Ca = 15583.9 = 20 = 779.195 Mg meq = Mg mg/I = Molec.Wgt.Mg = 829.124 + 12 = 69.0937 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 46.903 + SgrRoot[0.5(779.195+69.0937)] = 2.27742 Printed: 2/18/2015 Page 1 12:14 Page: 1 of 2 Report Number: 14-181-0204 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 56200 Sample Id : NG2 LAKE A&L Eastern Laboratories, Inc.- 99, 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwW aleastern.corn Project: NG2 LAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/27/2014 00:00:00 Date Received: 06/30/2014 00:00 Date Reported: 07/03/2014 Total Solids 17.33 173300 100.0 JM 06/30/2014 14:35 SM-2540G Moisture 82.67 100.0 JM 06/30/2014 14:35 SM-2540G Total Kjeldahl Nitrogen 5.77 57700 10.0 JM 07/01/2014 07:59 SM-4500-NH3C-TKN Total Phosphorus 2.61 26100 100 KM 07/01/2014 12:56 SW 6010C Total Potassium 1.48 14800 100 KM 07/01/2014 12:56 SW 6010C Total Sulfur 2.17 21700 100 KM 07/01/2014 12:56 SW 6010C Total Calcium 12.80 128000 100 KM 07/01/2014 12:56 SW 6010C Total Magnesium 0.56 5550 100 KM 07/01/2014 12:56 SW 6010C Total Sodium 0.76 7560 100 KM 07/01/2014 12:56 SW 6010C Total Iron 4970 100 KM 07/01/2014 12:56 SW 6010C Total Aluminum 5100 100 KM 07/01/2014 12:56 SW 6010C Total Manganese 298 5 KM 07/01/2014 12:56 SW 6010C Total Copper 21 5 KM 07/01/2014 12:56 SW 6010C Total Zinc 414 5 KM 07/01/2014 12:56 SW 6010C Ammonia Nitrogen 0.62 6230 10.0 JM 07/01/2014 07:59 SM-4500-NI3C Organic N 5.15 51470 10.0 07/01/2014 07:59 CALCULATION Nitrate+Nitrite-N 8.66 2.00 JM 07/01/2014 08:00 SM-450ONO3F Total Cadmium <2.0 2.0 KM 07/01/2014 12:56 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9�/w Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made *S14 to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt I � t � Page: 2 of 2 Report Number: 14-181-0204 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 56200 Sample Id : NG2 LAKE A&L Eastern Laboratories, Inc-.. 7621 Whitepine Road Richmond, V1rgin1a,23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastem.COM Project: NG2 LAKE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/27/2014 00:00:00 Date Received: 06/30/2014 00:00 Date Reported: 07/03/2014 Total Chromium 101 5 KM 07/01/2014 12:56 SW 6010C Total Nickel 36 5 KM 07/01/2014 12:56 . SW 6010C Total Lead <5 5 KM 07/01/2014 12:56 SW 6010C Total Arsenic 4.0 3.0 KM 07/01/2014 12:56 SW 6010C Total Mercury I 0.4 0.4 KM 07/01/2014 09:00 SW-7471 B Total Selenium 1 <5.0 5.0 KM 67/01/2014 12:56 SW 6010C pH (Standard Units) * I 7.74 2.00 JM 07/01/2014 07:59 SW-9045D Total Molybdenum <5 5 KM 07/01/2014 12:56 SW 6010C Chloride 1420 200 JM 07/01/2014 09:00 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE RPD WAS OUT OF LIMITS FOR "Hg". ALL OTHER QC DATA IS ACCEPTABLE. i All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. I Our reports and letters are for the exclusive and confidential use of our clients, and, may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in anyiadvertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2044-01-NG2C-NC ADM CORP., NC NITRO GRO 2 CAKE 6/27/2014 7/1/2014-7/31/2014 2.3360 Na mg/I = (Na mg/kg x % Solids) _ 100 = (7560 x 17.3300) = 100 = 1310.15 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (128000 x 17.3300) _ 100 = 22182.4 Mg mg/l = (mg mg/kg x % Solids) = 100 = (5550 x 17.3300) _ 100 = 961.815 Na meq = Na mg/I _ Molec.Wgt.Na = 1310.15 = 23 = 56.963 Ca meq = Ca mg/I — Molec.Wgt.Ca = 22182.4 = 20 = 1109.12 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 961.815 _ 12 = 80.1512 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 56.963 _ SgrRoot[0.5(1109.12+80.1512)] = 2.33597 Printed: 2/18/2015 Page 1 12:15 I Page: 1 of 2 Report Number: 14-206-0201 Account Number: 45637 I Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 56691 Sample Id: ADM NG2 STRAIGHT @D. A&L Eastern Laboratories, 7621 Whitepine Road Richmond, Virginia 23237 (804) 7433401 Fax (804) 271.6446 www.aleastern.com Project; ADM NG2 STRAIGHT NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/23/2014 10:35:00 Date Received: 07/25/2014 00:00 Date Reported: 07/31/2014 Total Solids * 15.81 158100 100.0 JM 07/25/2014 15:00 Moisture ` 84.19 100.0 JM 07/25/2014 15:00 Total Kjeldahl Nitrogen 6.12 61200 10.0 JM 07/28/2014 09:00 Total Phosphorus 3.15 31500 100 KM 0.7/30/2014 16:12 Total Potassium 1.39 13900 100 KM 07/30/2014 16:12 Total Sulfur 1.84 18400 100 KM 07/30/2014 16:12 Total Calcium 9.92 99200 100 KM 07/30/2014 16:12 .Total Magnesium 0.61 6140 100 KM 07/30/2014 16:12 Total Sodium 0.55 5500 100 KM 07/30/2014 16:12 Total Iron I 5890 100 KM 07/30/2014 16:12 Total Aluminum 5900 100 KM 07/30/2014 16:12 Total Manganese 265 5 KM 07/30/2014 16:12 Total Copper I 25 5 KM 07/30/2014 16:12 Total Zinc 394 5 KM 07/30/2014 16:12 Ammonia Nitrogen 0.44 4360 10.0 JM 07/28/2014 09:00 Organic N 5.68 56840 10.0 07/28/2014 09:00 Nitrate+Nitrite-N ! 17.7 2.00 JM 07/28/2014 08:20 Total Cadmium <2.0 2.0 KM 07/30/2014 16:12 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. I Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any, advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SM-2540G SM-2540G SM-4500-NH3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NH3C CALCULATION SM-450ONO3F SW 6010C Page: 2 of 2 Report Number: 14-206-0201 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 56691 Sample Id: ADM NG2 STRAIGHT A&L Eastern Laboratories, Inc:_ 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.WG www.aleastern.com Project: ADM NG2 STRAIGHT NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/23/2014 10:35:00 Date Received: 07/25/2014 00:00 Date Reported: 07/31/2014 Total Chromium 109 Total Nickel 38 Total Lead <5 Total Arsenic 3.0 Total Mercury <0.4 Total Selenium <5.0 pH (Standard Units) * 7.42 Total Molybdenum I <5 Chloride 1020 Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. 5 KM 07/30/2014 16:12 SW 6010C 5 KM 07/30/2014 16:12 SW 6010C 5 KM 07/30/2014 16:12 SW 6010C 3.0 KM 07/30/2014 16:12 SW 6010C 0.4 KM 07/28/2014 09:00 SW-7471 B 5.0 KM 07/30/2014 16:12 SW 6010C 2.00 JM 07/28/2014 09:00 SW-9045D 5 KM 07/30/2014 16:12 SW 6010C 200 JM 07/28/2014 09:25 SM-4500CI-D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt f I Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2C-NC ADM CORP., NC NITRO GRO 2 CAKE 7/23/2014 81112014-8/31/2014 1.8178 Na mg/I = (Na mg/kg x % Solids) = 100 = (5500 x 15.8100) _ 100 = 869.55 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (99200 x 15.8100) + 100 = 15683.5 Mg mg/1 = (mg mg/kg x % Solids) _ 100 = (6140 x 15.8100) _ 100 = 970.734 Na meq = Na mg/I _ Molec.Wgt.Na = 869.55 + 23 = 37.8065 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 15683.5 = 20 = 784.176 Mg meq = Mg mg/1 _ Molec.Wgt.Mg = 970.734 + 12 = 80.8945 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 37.8065 _ SgrRoot[0.5(784.176+80.8945)] = 1.81784 Printed: 2/18/2015 Page 1 12:15 Page: 1 of 2 Report Number: 14-233-0207 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 i Lab Number: 57151 Sample Id : NG2 A&L Eastern- Laboratories, Inc:_ 7621 Whitepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (604) 271-6446 wwwaleastern.com Project: NG2/NC CERT#257 REPORT OF ANALYSIS Date Sampled: 8/20/2014 08:30:00 Date Received: 08/21/2014 00:00 Date Reported: 08/28/2014 Total Solids" 17.34 173400 100.0 JM 08/21/2014 15:49 SM-2540G Moisture * 82.66 100.0 JM 08/21/2014 15:49 SM-2540G Total,Kjeldahl Nitrogen 5.18 51800 10.0 JM 08/22/2014 08:24 SM-4500-NH3C-TKN Total Phosphorus 2.67 26700 100 KM 08/27/2014 15:00 SW 6010C Total Potassium 1.17 11700 100 KM 08/27/2014 15:00 SW 6010C Total Sulfur l 2.09 20900 100 KM 08/27/2014 15:00 SW 6010C Total Calcium 11.60 116000 100 'KM 08/27/2014 15:00 SW 6010C Total Magnesium 0.57 5720 100 KM 08/27/2014 15:00 SW 6010C Total Sodium 0.68 6790 100 KM 08/27/2014 15:00 SW 6010C Total Iron 5870 100 KM 08/27/2014 15:00 SW 6010C Total Aluminum 5800 100 KM 08/27/2014 15:00 SW 6010C TotalManganese ! 398 5 KM 08/27/2014 15:00 SW 6010C Total Copper 26 5 KM 08/27/2014 15:00 SW 6010C 'Total Zinc 408 5 KM 08/27/2014 15:00 SW 6010C Ammonia Nitrogen 0.26 2600 10.0 JM 08/22/2014 08:24 SM-4500-NH3C Organic N 4.92 49200 10.0 08/22/2014 08:24 CALCULATION Nitrate+Nitrite-N 704 2.00 JM 08/25/2014 08:25 SM-450ONO3F Total Cadmium r <2.0 2.0 KM 08/27/2014 15:00 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive an confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any, advertising, news release, or other I public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 /► Report Number: 14-233-0207 AFL A&L Eastern Laboratories, Inc. Account Number: 45637 7621 Whitepine Road Richmond, Virginia 23237 (804) 7435401 Fax (804) 271-6446 Submitted By: LUKE STOWERS wwwaleastern.com Send To: ADM Project: NG2/NC CERT#257 SCO.TT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 REPORT OF ANALYSIS Date Sampled: 8/20/2014 08:30:00 Lab Number: 57151 Date Received: 08/21/2014 00:00 Sample Id : NG2 Date Reported: 08/28/2014 Total'Chromium 92 5 KM 08/27/2014 15:00 SW 6010C Total Nickel 38 5 KM 08/27/2014 15:00 SW 6010C Total Lead <5 5 KM 08/27/2014 15:00 SW 6010C Total Arsenic 3.0 3.0 KM 08/27/2014 15:00 SW 6010C Total Mercury <0.4 0.4 KM 08/2212014-12:00 SW-7471 B Total Selenium <5.0 5.0 KM 08/27/2014 15`:00 SW 6010C pH (Standard Units) * 7.67 2.00 JM 08/22/2014 08:19 SW-9045D Total Molybdenum <5 5 KM 08/27/2014 15:00 SW 6010C Chloride 1600 200 JM 08/22/2014 09:30 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. THE MATRIX SPIKE WAS OUT OF'LIMITS FOR "Ca", AND "Se", ALL OTHER QA/QC DATA IS WITHIN LIMITS. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. i Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any, advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium. Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG2C-NC ADM CORP., NC NITRO GRO 2 CAKE 8/20/2014 9/1/2014-9/30/2014 2.1944 Na mg/I = (Na mg/kg x % Solids) _ 100 = (6790 x 17.3400) = 100 = 1177.39 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (116000 x 17.3400) = 100 = 20114.4 Mg mg/I = (mg mg/kg x % Solids) = 100 = (5720 x 17.3400) = 100 = 991.848 Na meq = Na mg/I = Molec.Wgt.Na = 1177.39 _ 23 = 51.1907 Ca meq = Ca mg/I = Molec.Wgt.Ca = 20114.4 = 20 = 1005.72 Mg meq = Mg mg/I = Molec.Wgt.Mg = 991.848 + 12 = 82.654 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 51.1907 = SgrRoot[0.5(1005.72+82.654)] = 2.19441 Printed: 2/18/2015 Page 1 12:16 Page: 1 of 2 Report Number: 14-272-0201 Account Number: 45637 Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 ' I Lab Number: 57823 Sample Id: ADM NG2 qiLi JoasamA&L Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401, Fax (804) 271 6446 wwwaleastern.com Project: ADM NG2 NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 9/24/2014 14:40:00 Date Received: 09/29/2014 00:00 Date Reported: 10/02/2014 Total Solids " 18.25 182500 100.0 MW 09/30/2014 08:44 SM-2540G Moisture * 81.75 100.0 MW 09/30/2014 08:44 SM-2540G Total Kjeldahl Nitrogen 5.20 52000 10.0 JM 09/30/2014 09:00 SM-4500-NH3C-TKN Total Phosphorus 2.75 .27500 100 KM 09/30/2014 12:50 SW 6010C Total Potassium 1.54 15400 100 KM 09/30/2014 12:50 SW 6010C Total Sulfur 1.98 19800 100 KM 09/30/2014 12:50 SW 6010C Total Calcium 13.30 133000 100 KM 09/30/2014 12:50 SW 6010C Total Magnesium 0.60 6000 100 KM 09/30/2014 12:50 SW 6010C Total Sodium 0.71 7110 100 KM 09/30/2014 12:50 SW 6010C Total Iron 5040 100 KM 09/30/2014 12:50 SW 601OC Total Aluminum 5300 100 KM 09/30/2014 12:50 SW 6010C Total Manganese 328 5 KM 09/30/2014 12:50 SW 6010C Total Copper 21 5 KM 09/30/2014 12:50 SW 6010C Total Zinc 334 5 KM 09/30/2014 12:50 SW 6010C Ammonia Nitrogen 0.29 2850 10.0 JM 09/30/2014 09:00 SM-4500-NI3C Organic N 4.91 49150 10.0 09/30/2014 09:00 CALCULATION Nitrate+Nitrite-N 57.5 2.00 JM 09/30/2014 09:00 SM-450ONO3F Total Cadmium j <2.0 2.0 KM 09/30/2014 12:50 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-272-0201 Account Number: 45637 I Send To: ADM SCOTT PHILLIPS 1730 EAST MOOR ST SE SOUTHPORT , NC '28461 Lab Number: 57823 Sample Id: ADM NG2 �YL A&L Eastern Laboratories,, Inc. 7627 Whitepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (804)271-6446 www.aleastern.com Project: ADM NG2 NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 9/24/2014 14:40:00 Date Received: 09/29/2014 00:00 Date Reported: 10/02/2014 Total Chromium 82 5 KM 09/30/2014 12:50 SW 6010C Total Nickel 30 5 KM 09/30/2014 12:50 SW 6010C Total Lead <5 5 KM 09/30/2014 12:50 SW 6010C Total Arsenic j 4.0 3.0 KM 09/30/2014 12:50 SW 6010C Total Mercury I <0.4 0.4 KM 09/30/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 09/30/2014 12:50 SW 6010C pH (Standard Units) * 8.02 2.00 JM 09/30/2014 09:49 SW-9045D Total Volatile Solids 55.08 550800 100.0 MW 09/30/2014 08:44 SM-2540G Total Molybdenum <5 5 KM 09/30/2014 12:50 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "NO3/NO2-N". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca", "Na", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. I Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2044-01-NG2C-NC ADM CORP., NC NITRO GRO 2 CAKE 9/24/2014 10/l/2014-10/31/2014 2.2087 Na mg/I = (Na mg/kg x % Solids) _ 100 = (7110 x 18.2500) =100 = 1297.58 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (133000 x 18.2500) _ 100 = 24272.5 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (6000 x 18.2500) = 100 = 1095 Na meq = Na mg/I = Molec.Wgt.Na = 1297.58 = 23 = 56.4163 Ca meq = Ca mg/I = Molec.Wgt.Ca = 24272.5 _ 20 = 1213.63 Mg meq = Mg mg/I = Molec.Wgt.Mg = 1095 = 12 = 91.25 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 56.4163 = SgrRoot[G.5(1213.63+91.25)] = 2.20869 Printed: 2/18/2015 Page 1 12:17 I Page: 1 of 2 Report Number: 14-297-0207 W A&L Eastern Laboratories, Inc. Account Number: 45637 � � 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-6446 Submitted By: CREIGHTON BROWN wwwaleasternmin Send To: ADM Project: ADM NG2 SCOTT PHILLIPS ' NC CERT#257 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 I REPORT OF ANALYSIS Date Sampled: 10/23/2014 11:45:00 Lab Number: 58343 Date Received: 10/24/2014 00:00 Sample Id: ADM NG2 Date Reported: 10/30/2014 PARAMETER RE�SULT RESULT QUANTITATION ANALYST METHOD . DATE/TIME Total Solids * i 15.21 152100 100.0 JM 10/24/2014 15:00 SM-2540G Moisture * 84.79 100.0 JM 10/24/2014 15:00 SM-254OG Total Kjeldahl Nitrogen 5.95 59500 10.0 JM 10/27/2014 08:55 SM-4600-NH3C-TKN Total Phosphorus 2.43 24300 100 KM 10/27/2014 14:56 SW 6010C Total Potassium 1.35 13500 100 KM 10/27/2014 14:56 SW 6010C Total Sulfur 2.10 21000 100 KM 10/27/2014 14:56 SW 6010C Total Calcium 10.20 102000 100 KM 10/27/2014 14:56 SW 6010C Total Magnesium 0.47 4680 100 KM 10/27/2014 14:56 SW 6010C Total Sodium 0.67 6670 100 KM 10/27/2014 14:56 SW 6010C Total Iron 4180 100 KM 10/27/2014 14:56 SW 6010C Total Aluminum 4600 100 KM 10/27/2014 14:56 SW 6010C Total Manganese 250 5 KM 10/27/2014 14:56 SW 6010C Total Copper 19 5 KM 10/27/2014 14:56 SW 6010C Total Zinc 318 5 KM 10/27/2014 14:56 SW 6010C 'Ammonia Nitrogen 0.27 2700 10.0 JM 10/27/2014 08:55 SM-4500-NH3C Organic N 5.68 56800 10.0 10/27/2014 08:55 CALCULATION Nitrate+Nitrite-N 25.6 2.00 JM 10/27/2014 00:00 SM-450ONO3F Total Cadmium <2.0 2.0 KM 10/27/2014 14:56 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. { Debbie Holt 1 Page: 2 of 2 Report Number: 14-297-0207 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 58343 Sample Id: ADM NG2 v A&L Eastem Laboratories, Inc. 7.621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401, Pax (804)271.6446 0 wwwaleastern.com Project: ADM NG2 NC CERT#257 REPORT OFANALYSIS Date Sampled: 10/23/2014 11:45:00 Date Received: 10/24/2014 00:00 Date Reported: 10/30/2014 Total Chromium 67 5 KM 10/27/2014 14:56 SW 6010C Total Nickel 25 5 KM 10/27/2014 14:56 SW 6010C Total Lead <5 5 KM 10/27/2014 14:56 SW 6010C Total Arsenic 4.0 3.0 KM 10/27/2014 14:56 SW 6010C Total Mercury <0.4 0.4 KM 10/27/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 10/27/2014 14:56 SW 6010C pH (Standard Units) * , 7.60 2.00 JM 10/27/2014 08:55 SW-9045D Total Volatile Solids 61.31 613100 100.0 JM 10/24/2014 15:00 SM-254OG Total Molybdenum <5 5 KM 10/27/2014 14:56 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Cr". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2044-01-NG2C-NC ADM CORP., NC NITRO GRO 2 CAKE 10/23/2014 111112014-11/30/2014 2.1587 Na mg/1= (Na mg/kg x % Solids) _ 100 = (6670 x 15.2100) _ 100 = 1014.51 Ca mg/1= (Ca mg/kg x % Solids) _ 100 = (102000 x 15.2100) _ 100 = 15514.2 Mg mg/I = (mg mg/kg x % Solids) = 100 = (4680 x 15.2100) _ 100 = 711.828 Na meq = Na mg/I = Molec.Wgt.Na = 1014.51 = 23 = 44.109 Ca meq = Ca mg/1= Molec.Wgt.Ca = 15514.2 = 20 = 775.71 Mg meq = Mg mg/1 _ Molec.Wgt.Mg = 711.828 _ 12 = 59.319 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 44.109 _ SgrRoot[0.5(775.71+59.319)] = 2.1587 Printed: 2/18/2015 Page 1 12:18 i Pa&: 1 of 2 i Report Number: 14-325-0201 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS i 1730 EAST MOOR ST SE SOUTHPORT , NC 28461 Lab Number: 58870 Sample Id : ADM NG2 , L A&L Eastern Laboratories, `Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 .Fax (804) 271.WG www.alegstern.COM Project: ADM NG2 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 11/18/2014 09:30:00 Date Received: 11/21/2014 00:00 Date Reported: 12/02/2014 Total Solids * 14.10 141000 100.0 BW 11/21/2014 15:00 Moisture * 85.90 100.0 BW 11/21/2014 15:00 Total Kjeldahl Nitrogen 7.23 72300 10.0 JM 11/24/2014 09:24 Total Phosphorus 2.34 23400 100 KM 11/24/2014 11:01 Total Potassium 1.29, 12900 100 KM 11/24/2014 11:01 Total Sulfur 1.68 16800 100 KM 11/24/2014 11:01 Total Calcium 8.18 81800 100 KM 11/24/2014 11:01 Total Magnesium i 0.40 4040 100 KM 11/24/2014 11:01 Total Sodium 0.56 5580 100 KM 11/24/2014 11:01 Total Iron 3390 100 KM 11/24/2014 11:01 Total Aluminum ! 4400 100 KM 11/24/2014 11:01 Total Manganese 198 5 KM 11/24/2014 11:01 Total Copper ; . 19 5 KM 11/24/2014 11:01 Total Zinc 292 5 KM 11/24/2014 11:01 Ammonia Nitrogen 0.27 2700 10.0 JM 11/24/2014 09:24 Organic N 6.96 69600 10.0 11/24/2014 09:24 Nitrate+Nitrite-N 594 2.00 JM 11/26/2014 08:05 Total Cadmium <2.0 2.0 KM 11/24/2014 11:01 i All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our, clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SM-2540G SM-2540G SM-4500-NH3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NH3C CALCULATION SM-450ONO3F SW 6010C � I i Page: 2 of 2 Report Number: 14-325-0201 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOOR ST SE SOUTHPORT , NC 28461 Lab Number: 58870 Sample Id: ADM NG2 ANNUMMONIk A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9.401 Fax (804) 271.6446 www.aleastern.com Project: ADM NG2 NC CERT#257 REPORT OF ANALYSIS Date Sampled: 11/18/2014 09:30:00 Date Received: 11/21/2014 00:00 Date Reported: 12/02/2014 Total Chromium 62 5 KM 11/24/2014 11:01 SW 6010C Total Nickel ; 23 5 KM 11/24/2014 11:01 SW 6010C Total Lead <5 5 KM 11/24/2014 11:01 SW 6010C Total Arsenic <3.0 3.0 KM 11/24/2014 11:01 SW 6010C Total Mercury <0.4 0.4 KM 11/24/2014 12:00 SW-7471B Total Selenium i <5.0 5.0 KM 11/24/2014 11:01 SW 6010C pH (Standard Units) * 7.42 2.00 JM 11/24/2014 09:24 SW-9045D Total Volatile Solids 67.29 672900 100.0 BW 11/21/2014 15:00 SM-2540G Total Molybdenum <5 -5 KM 11/24/2014 11:01 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB IS OUT OF LIMITS FOR "Mn", THE MATRIX XPIKE IS OUT OF i I ' I LIMITS FOR "Se", AND "S", ALL OTHER QA/QC IS WITHIN LIMITS. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. I •� Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. I Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range. Ratio 2044-01-NG2C-NC ADM CORP., NC NITRO GRO 2 CAKE 11/18/2014 12/l/2014-12/31/2014 1.9364 Na mg/I = (Na mg/kg x % Solids) _ 100 = (5580 x 14.1000) = 100 = 786.78 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (81800 x 14.1000) + 100 = 11533.8 Mg mg/I = (mg mg/kg x % Solids) = 100 = (4040 x 14.1000) _ 100 = 569.64 Na meq = Na mg/I + Molec.Wgt.Na = 786.78 = 23 = 34.2078 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 11533.8 _ 20 = 576.69 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 569.64 _ 12 = 47.47 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 34.2078 _ SgrRoot[0.5(576.69+47.47)] = 1.93639 Printed: 2/18/2015 Page 1 12:18 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004500 Laboratory Facility Name: ARCHER-DANIELS MIDLAND CORP., NC A&L Eastern Laboratories Inc. NPDES# : NC0027065 or WQ# (residual only) ; WWTP Name: ARCHER DANIELS MIDLAND Residuals Analysis Data Product Type NG3L Date Sampled (grab) or 12/19/13 Date Composited Percent Solids 14.48 PARAMETERS (mg/kg dry weight) Arsenic <3 Cadmium <2 Mercury <0.4 Chromium <5 Copper i <5 Lead <5 Molybdenum <5 Nickel <5 Selenium <5 Zinc <5 Total Phosphorus 9300 TKN 73900 Ammonia -Nitrogen 1860 Nitrate and Nitrite 1 I 35.2 NG3L NG3L NG3L NG3L NG3L NG3L NG3L NG3L 01/27/14 02/26/14 04/29/14 05/15/14 07/02/14 07/23/14 08/20/14 09/25/14 14.53 14.84 14.43 14.15 11.20 13.83 10.01 11.17 <3 <3 <3 <3 <3 <3 <3 <3 <2 <2' <2 <2 <2 <2 <2 <2 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 <0.4 5 7 5 9 11 6 <5 6 7 9 5 9 12 13 11 11 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 8 5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 13 12 9 46 24 11. 10 11 8380 8390 8550 10200 7790 8190 7310 8790 70900 72100 74200 75600 75800 75900 75700 75900 2410 2630 2490 2900 2320 795 3600 3400 26.8 88.9 4.85 <2 10.7 10.1 32 54.6 DENR FORM RSSF (5/2003) Printed: Wednesday - February 18, 2015 at 12:02:11 for: 2044 01 i ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. I Permit Number: WQ0004500 Facility Name: ARCHER DANIELS MIDLAND CORP., NC NPDES# : NC0027065 or WQ# (residual only) WWTP Name: ARCHER DANIELS MIDLAND i Residuals Analysis Data Product Type NG3L NG3L Date Sampled (grab) or 10/23/14 11/18/14 Date Composited Percent Solids j 14.39 14.04 PARAMETERS (mg/kg dry weight) Arsenic <3 <3 Cadmium i <2 <2 Mercury I <0.4 <0.4 Chromium j 6 5 Copper 12 10 Lead i <5 <5 Molybdenum ; <5 <5 Nickel ! <5 <5 Selenium <5 <5 Zinc 17 10 Total Phosphorus 8690 8680 TKN 77100 75500 Ammonia -Nitrogen 3960 2560 Nitrate and Nitrite 17 4 <2 Page: 2 Laboratory A&L Eastern Laboratories Inc. "I certify, under penalty of law,j that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 101 ,n X SIGNATURE OF PREPA# i? I i� !d . DENR FORM RSSF (5/2003) R) Date ",f —/,-5 r Printed: Wednesday - February 18, 2015 at 12:02:11 for: 2044 01 i I i ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. i Permit Number: WQ0004500 Facility Name: ARCHER DANIELS MIDLAND CORP., NC NPDES# : NC0027065 or WQ# (residual only) WWTP Name: ARCHER DANIELS MIDLAND Residuals Analysis Data Product Type NG3L NG3L NG3L Date Sampled (grab) or 1 12/19/13 01/27/14 02/26/14 Date Composited Percent Solids 14.48 14.53 14.84 PARAMETERS (mg/kg dry weight) Aluminum 200 200 Calcium 9700 1300 Magnesium 129 121 pH 3.79 3.68 Potassium 309 584 Sodium 437 845 Laboratory A&L Eastern Laboratories Inc. NG3L 04/29/14 14.43 NG3L 05/15/14 14.15 NG3L 07/02/14 11.20 NG3L 07/23/14 13.83 NG3L 08/20/14 10.01 NG3L 09/25/14 11.17 300 200 400 500 200 200 200 1020 1900 6390 1460 1290 1330 2110 138 149 411 486 323 269 193 3.55 3.74 3.53 3.46 3.37 3.54 3.32 439 527 1180 454 365 423 372 461 951 920 923 701 1170 1130 I DENR FORM RSSF-B (7/2002)! Printed: Wednesday - February 18, 2015 at 12:03:04 for: 2044 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. i , Permit Number: W00004500 Facility Name: ARCHER DANIELS MIDLAND CORP., NC NPDES# : NCO027065 or WQ# (residual only) WWTP Name: ARCHER DANIELS MIDLAND I I I Residuals Analysis Data Product Type NG3L NG3L Date Sampled (grab) or i 10/23/14 11/18/14 Date Composited Percent Solids 14.39 14.04 PARAMETERS (mg/kg dry weight) Aluminum 500 200 Calcium 1510 2120 Magnesium j 130 124 pH 3.72 3.75 Potassium 228 329 Sodium I 519 701 Laboratory A&L Eastern Laboratories Inc. "I certify, under penalty of law,: that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant pen Ities for submitting false information, including the possibility of fines and imprisonment for knowing violations." 7 1-�I X - Data Not Reported or Data Not Required I I I Date �` 3 "/&� Page: 2 DENR FORM RSSF-B (7/2002): Printed: Wednesday - February 18, 2015 at 12:03:04 for: 2044 01 i Page: 1 of 2 Report Number: 13-354-0203 Account Number: 45637 Submitted By: SCOTT COE Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 A&L Eastern Laboratories, Inc. 99, 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastern.colll Project: NG3L NC CERT#257 REPORT OF ANALYSIS Date Sampled: 12/19/2013 07:35:00 Lab Number: 97213 Date Received: 12/20/2013 00:00 Sample Id : NG3L Date Reported: 01/02/2014 l otal Solids 14.41:5 1446UU 1 UU.0 JIVI 1 L/LU/LU13 '14:44 6IVI-Y04Uh - Moisture * 85.52 100.0 JM 12/20/2013 14:44 SM-2540G Total Kjeldahl Nitrogen 7.39 73900 10.0 JM 12/23/2013 08:35 SM-4500-NH3C-TKN Total Phosphorus 0.93 ' 9300 100 KM 12/23/2013 11:47 SW 6010C Total Potassium 0.03 309 100 KM 12/23/2013 11:47 SW 6010C Total Sulfur 1.04 10400 100 KM 12/23/2013 11:47 SW 6010C Total Calcium 0.97 9700 100 KM 12/23/2013 11147 SW 6010C Total Magnesium 0.01 129 100 KM 12/23/2013 11:47 SW 6010C Total Sodium 0.04 437 100 KM 12/23/2013 11:47 SW 6010C Total Iron 229 100 KM 12/23/2013 11:47 SW 6010C Total Aluminum 200 100 KM 12/23/2013 11:47 SW 6010C Total Manganese i <5 5 KM 12/23/2013 11:47 SW 6010C Total Copper <5 5 KM 12/23/2013 11:47 SW 6010C Total Zinc <5 5 KM 12/23/2013 11:47 SW 6010C Ammonia Nitrogen 0.19 1860 10.0 JM 12/23/2013 08:35 SM-4500-NH3C Organic N 7.20 72040 10.0 12/23/2013 08:35 CALCULATION Nitrate+Nitrite-N 35.2 2.00 JM 12/23/2013 08:50 SM-450ONO3F Total Cadmium <2.0 2.0 KM 12/23/2013 11:47 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. rr Our reports and letters are for the exclusive an'tl confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any, advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 13-354-0203 Account Number: 45637 Submitted By: SCOTT COE Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 97213 . Sample Id : NG3L A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237' , (804) 743-9401 Fax (804) 271.6446 wwwaleastern.com Project: NG31- NC CERT#257 REPORT OF ANALYSIS Date Sampled: 12/19/2013 07:35:00 Date Received: 12/20/2013 00:00 Date Reported: 01/02/2014 Total Chromium <5 5 KM 12/23/2013 11:47 SW 6010C Total Nickel <5 5 KM 12/23/2013 11:47 SW 6010C Total Lead <5 5 KM 12/23/2013 11:47 SW 6010C Total Arsenic <3.0 3.0 KM 12/23/2013 11:47 SW 6010C Total Mercury <0.4 0.4 KM 12/23/2013 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 12/23/2013 11:47 SW 6010C pH (Standard Units) * 3.79 2.00 JM 12/23/2013 08:35 SW-9045D Total Molybdenum <5 5 KM 12/23/2013 11:47 SW 6010C Chloride 327 200 JM 12/23/2013 09:50 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Al", "Fe", "Mn", AND "Mo". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca", "Se", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2044-01-NG3L-NC ADM CORP., NC NITRO GRO 3 LIQUID 12/19/2013 11112014-1/3112014 0.4592 Na mg/I = (Na mg/kg x % Solids) -= 100 = (437 x 14.4800) _ 100 = 63.2776 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (9700 x 14.4800) + 100 = 1404.56 Mg mg/I = (mg mg/kg x % Solids) + 100 = (129 x 14.4800) : 100 = 18.6792 Na meq = Na mg/I + Molec.Wgt.Na = 63.2776 -= 23 = 2.7512 Ca meq = Ca mg/I = Molec.Wgt.Ca = 1404.56 = 20 = 70.228 Mg meq = Mg mg/I + Molec.Wgt.Mg = 18.6792 _ 12 = 1.5566 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.7512 + SgrRoot[0.5(70.228+1.5566)] = 0.459221 Printed: 2/18/2015 Page 1 12:12 Page: 1 of 2 Report Number: 14-028-0207 Account Number: 45637 Submitted By: LUKE STOWERS . Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 97670 Sample Id : YEAST CREAM v A&L Eastern Laboratories, Inc.- 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastern.com Project: ADM - YEAST CREAM NC CERT# 257 REPORT OF ANALYSIS Date Sampled: 1/27/2014 12:30:00 Date Received: 01/28/2014 00:00 Date Reported: 02/03/2014 Total Solids * 14.53 145300 100.0 JM 01/28/2014 15:00 Moisture * 85.47 100.0 JM 01/28/2014 15:00 Total Kjeldahl Nitrogen 7.09 70900 10.0 JM 01/29/2014 09:29 Total Phosphorus 0.84 8380 100 KM 01/29/2014 13:31 Total Potassium 0.06 584 100 KM 01/29/2014 13:31 Total Sulfur 0.52 5180 100 KM 01/29/2014 13:31 Total Calcium 0.13 1300 100 KM 01/29/2014 13:31 Total Magnesium 0.01 121 100 KM 01/29/2014 13:31 Total Sodium 0.08 845 100 KM 01/29/2014 13:31 Total Iron 222 100 KM 01/29/2014 13:31 Total Aluminum 200 100 KM 01/29/2014 13:31 Total Manganese 5 5 KM 01/29/2014 13:31 Total Copper 7 5 KM 01/29/2014 13:31 Total Zinc i 13 5 KM 01/29/2014 13:31 Ammonia Nitrogen 0.24 2410 10.0 JM 01/29/2024 00:00 Organic N 6.85 68490 10.0 01/29/2014 09:29 Nitrate+Nitrite-N 26.8 2.00 JM 01/29/2014 09:30 Total Cadmium ! <2.0 2.0 KM 01/29/2014 13:31 i All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt i SM-2540G SM-2540G SM-4500-NH3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NI3C CALCULATION SM-450ONO3F SW 6010C Page: 2 of 2 Report Number: 14-028-0207 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 97670 Sample Id: YEAST CREAM �L A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 wwW aleastern.com Project: ADM - YEAST CREAM NC CERT# 257 REPORT OF ANALYSIS Date Sampled: 1/27/2014 12:30:00 Date Received: 01/28/2014 00:00 Date Reported: 02/03/2014 Total Chromium 5 5 KM 01/29/2014 13:31 SW 6010C Total Nickel <5 5 KM 01/29/201.4 13:31 SW 6010C Total Lead <5 5 KM 01/29/2014 13:31 SW 6010C Total Arsenic <3.0 3.0 KM 01/29/2014 13:31 SW 6010C Total Mercury <0.4 0.4 KM 01/29/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 01/29/2014 13:31 SW 6010C pH (Standard Units) * 3.68 2.00 JM 01/29/2014 09:29 SW-9045D Total Molybdenum <5 5 KM 01/29/2014 13:31 SW 6010C Chloride 439 200 JM 01/29/201410:30 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR'W". ALL OTHER QC DATA IS ACCEPTABLE. 0 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG3L-NC ADM CORP., NC NITRO GRO 3 LIQUID 1/27/2014 2/1/2014-3/9/2014 2.2856 Na mg/I = (Na mg/kg x % Solids) _ 100 = (845 x 14.5300) _ 100 = 122.779 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (1300 x 14.5300) =100 = 188.89 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (121 x 14.5300) = 100 = 17.5813 Na meq = Na mg/I _ Molec.Wgt.Na = 122.779 + 23 = 5.3382 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 188.89 _ 20 = 9.4445 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 17.5813 + 12 = 1.46511 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.3382 _ SgrRoot[0.5(9.4445+1.46511)] = 2.28562 Printed: 2/18/2015 Page 1 12:12 Page: 1 of 2 Report Number: 14-059-0201 Account Number: 45637 Submitted By: EDWARD STEPHENS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 98167 Sample Id : YEAST CREAM 99.A&L EasternLaboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 mmaleastern.com Project: ADMNEAST CREAM NC CERT#257 REPORT OF ANALYSIS Date Sampled: 2/26/2014 10:30:00 Date Received: 02/28/2014 00:00 Date Reported: 03/07/2014 Total Solids 14.84 148400 100.0 JM 03/04/2014 09:20 SM-2540G Moisture ` 85.16 100.0 JM 03/04/2014 09:20 SM-2540G Total Kjeldahl Nitrogen 7.21 72100 10.0 JM 03/03/2014 07:54 SM-4500-NH3C-TKN Total Phosphorus 0.84 8390 100 KM 03/03/2014 12:51 SW 6010C Total Potassium 0.04 439 100 KM 03/03/2014 12:51 SW 6010C Total Sulfur 0.50 5020 100 KM 03/03/2014 12:51 SW 6010C Total Calcium 0.10 1020 100 KM 03/03/2014 12:51 SW 6010C Total Magnesium 0.01 138 100 KM 03/03/2014 12:51 SW 6010C Total Sodium 0.05 461 100 KM 03/03/2014 12:51 SW 6010C Total Iron 449 100 KM 03/03/2014 12:51 SW 6010C Total Aluminum 300 100 KM 03/03/2014 12:51 SW 6010C Total Manganese 9 5 KM 03/03/2014 12:51 SW 6010C Total Copper 9 5 KM 03/03/2014 12:51 SW 6010C Total Zinc 12 5 KM 03/03/2014 12:51 SW 6010C Ammonia Nitrogen 0.26 2630 10.0 JM 03/03/2014 07:54 SM-4500-NH3C Organic N 6.95 69470 10.0 03/03/2014 07:54 CALCULATION Nitrate+Nitrite-N 88.9 2.00 JM 03/03/2014 07:55 SM-450ONO3F Total Cadmium <2.0 2.0 KM 03/03/2014 12:51 SW 6010C All values are on a dryweight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-059-0201 Account Number: 45637 Submitted By: EDWARD STEPHENS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 98167 Sample Id : YEAST CREAM p� A&L Eastern Laboratories, Inc.. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 wwwaleastem.com Project: ADM/YEAST CREAM NC CERT#257 REPORT OF ANALYSIS Date Sampled: 2/26/2014 10:30:00 Date Received: 02/28/2014 00:00 Date Reported: 03/07/2014 Total Chromium 7 5 KM 03/03/2014 12:51 SW 6010C Total Nickel <5 5 KM 03/03/2014 12:51 SW 6010C Total Lead <5 5 KM 03/03/2014 12:51 SW 6010C Total Arsenic <3.0 3.0 KM 03/03/2014 12:51 SW 6010C Total Mercury <0.4 0.4 KM 03/03/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 03/03/2014 12:51 SW 6010C pH (Standard Units) * 3.55 2.00 JM 03/03/2014 09:09 SW-9045D Total Molybdenum <5 5 KM 03/03/2014 12:51 SW 6010C Chloride 310 200 MW 03/03/2014 08:10 SM-4500CI-D Comments: CHLORIDE,. SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Ca", "Mn", AND "NO3/NO2-N".. THE MATRIX SPIKE WAS OUT OF LIMITS FOR "AI" , "CA", AND "NO3/NO2-N. ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any,reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG3L-NC ADM CORP., NC NITRO GRO 3 LIQUID 2/26/2014 3/10/2014-4/30/2014 1.3812 Na mg/I = (Na mg/kg x % Solids) + 100 = (461 x 14.8400) 100 = 68.4124 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (1020 x 14.8400) + 100 = 151.368 Mg mg/1 = (mg mg/kg x % Solids) + 100 = (138 x 14.8400) + 100 = 20.4792 Na meq = Na mg/I + Molec.Wgt.Na = 68.4124 _ 23 = 2.97445 Ca meq = Ca mg/I + Molec.Wgt.Ca = 151.368 + 20 = 7.5684 Mg meq = Mg mg/I + Molec.Wgt.Mg = 20.4792 + 12 = 1.7066 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.97445 + SgrRoot[0.5(7.5684+1.7066)] = 1.38123 Printed: 2/18/2015 Page 1 12:13 Page: i of 2 Report"Number: 14-121-0201 Account Number: 45637 Submitted By: MARSHALL PURYEAR Send To: ADM SCOTT PHILLIPS i 1730 EAST MOORE"ST SE SOUTHPORT , NC 28461 Lab Number: 55127 Sample ld : NG-3 LIQUID CREAM A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 7434401 Fax (804) 271-W6 www,aleastem.com " Project: NG-3 LIQUID CREAM , NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/29/2014 15:30:00 Date Received: 05/01/2014 00:00 Date Reported: 05/06/2014 Total Solids * 14.43 144300 100.0 RD 05/01/2014 14:30 SM-2540G Moisture * 85.57 100.0 RD 05/01/2014 14:30 SM-2540G Total Kjeldahl Nitrogen 7.42 74200 10.0 JM 05/02/2014 08:50 SM-4500-NH3C-TKN Total Phosphorus 0.86 8550 100 KM 05/02/2014 12:24 SW 6010C Total Potassium 0.05 527 100 KM 05/02/2014 12:24 SW 6010C Total Sulfur 0.50 4980 100 KM 05/02/2014 12:24 SW 6010C Total Calcium i 0.19 1900 100 KM 05/02/2014 12:24 SW 6010C Total Magnesium 0.01 149 100 KM 05/02/2014 12:24 SW 6010C Total Sodium 0.10 951 100 KM 05/02/2014 12:24 SW 6010C Total Iron I 194 100 KM 05/02/2014 12:24 SW 6010C Total Aluminum 200 100 KM 05/02/2014 12:24 SW 6010C Total Manganese 12 5 KM 05/02/2014 12:24 SW 6010C Total Copper 5 5 KM 05/02/2014 12:24 SW 6010C Total Zinc I 9 5 KM 05/02/2014 12:24 SW 6010C Ammonia Nitrogen I 0.25 2490 10.0 JM 05/02/2014 08:50 SM-4500-NH3C Organic N 7.17 71710 10.0 05/02/2014 08:50 CALCULATION Nitrate+Nitrite-N 4.85 2.00 JM 05/02/2014 08:50 SM-450ONO3F Total Cadmium t <2.0 2.0 KM 05/02/2014 12:24 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis, Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt 4 Page: 2 of 2 Report Number: 14-121-0201 Account Number: 45637 Submitted By: MARSHALL PURYEAR Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 55127 Sample Id: NG-3 LIQUID CREAM 99.A&L Eastern, Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 y8maleastern.com Project: NG-3 LIQUID CREAM NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/29/2014 15:30:00 Date Received: 05/01/2014 00:00 Date Reported: 05/06/2014 Total Chromium 5 Total Nickel <5 Total Lead <5 Total Arsenic <3.0 Total Mercury <0.4 Total Selenium <5.0 pH (Standard Units) * 3.74 Total Molybdenum <5 Chloride 546 Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. 5 KM 05/02/2014 12:24 SW 6010C 5 KM 05/02/2014 12:24 SW 6010C 5 KM 05/02/2014 12:24 SW 6010C 3.0 KM 05/02/2014 12:24 SW 6010C 0.4 KM 05/02/2014 09:00 SW-7471 B 5.0 KM 05/02/2014 12:24 SW 6010C 2.00 JM 05/02/2014 08:50 SW-9045D 5 KM 05/02/2014 12:24 SW 6010C 200 JM 05/02/2014 09:50 SM-4500CI-D ' All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG3L-NC ADM CORP., NC NITRO GRO 3 LIQUID 4/29/2014 5/l/2014-5/31/2014 2.1432 Na mg/1= (Na mg/kg x % Solids) = 100 = (951 x 14.4300) =100 = 137.229 Ca mg/1= (Ca mg/kg x % Solids) + 100 = (1900 x 14.4300) + 100 = 274.17 Mg mg/I = (mg mg/kg x % Solids) = 100 = (149 x 14.4300) =100 = 21.5007 Na meq = Na mg/I _ Molec.Wgt.Na = 137.229 _ 23 = 5.96649 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 274.17 _ 20 = 13.7085 Mg meq = Mg mg/I -= Molec.Wgt.Mg = 21.5007 = 12 = 1.79173 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.96649 _ SgrRoot[0.5(13.7085+1.79173)] = 2.14321 Printed: 2/18/2015 Page 1 12:14 Page: 1 of 2 Report Number: 14-141-0206 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 55483 Sample Id : NG3L YEAST CREAM IL A&L Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23231 (804) 743.9401 Fax (804) 271.6446, wwwaleastern.com Project: NG31- YEAST CREAM NC CERT#257 REPORT OF ANALYSIS Date Sampled: 5/15/2014 14:30:00 Date Received: 05/21/2014 00:00 Date Reported: 05/23/2014 Total Solids * 14.15 141500 100.0 JM 05/21/2014 14:19 SM-2540G Moisture * 85.85 100.0 JM 05/21/2014 14:19 SM-2540G Total Kjeldahl Nitrogen 7.56 75600 10.0 JM 05/22/2014 09:20 SM-4500-NH3C-TKN Total Phosphorus 1.02 10200 100 KM 05/22/2014 13:31 SW 6010C Total Potassium 0.12 1180 100 KM 05/22/2014 13:31 SW 6010C Total Sulfur 0.64 6360 100 KM 05/22/2014 13:31 SW 6010C Total Calcium 0.64 6390 100 KM 05/22/2014 13:31 SW 6010C Total Magnesium 0.04 411 100 KM 05/22/2014 13:31 SW 6010C Total Sodium 0.09 920 100 KM 05/22/2014 13:31 SW 6010C Total Iron 414 100 KM 05/22/2014 13:31 SW 6010C Total Aluminum : 400 100 KM 05/22/2014 13:31 SW 6010C Total Manganese 20 5 KM 05/22/2014 13:31 SW 6010C Total Copper 9 5 KM 05/22/2014 13:31 SW 6010C Total Zinc 46 5 KM 05/22/2014 13:31 SW 6010C Ammonia Nitrogen 0.29 2900 10.0 JM 05/22/2014 09:00 SM-4500-NI3C Organic N 7.27 72700 10.0 05/22/2014 09:00 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 05/22/2014 09:20 SM-450ONO3F Total Cadmium <2.0 2.0 KM 05/22/2014 13:31 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any, advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-141-0206 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 55483 Sample Id : NG31- YEAST CREAM LA&L Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401, Fax (804) 271-6446 wwwaleastern.com Project: NG31- YEAST CREAM NC CERT#257 REPORT OF ANALYSIS Date Sampled: 5/15/2014 14:30:00 Date Received: 05/21/2014 00:00 Date Reported: 05/23/2014 Total Chromium 9 5 KM 05/22'/2014 13:31 SW 6010C Total Nickel 8 5 KM 05/22/2014 13:31 SW 6010C Total Lead <5 5 KM 05/22/2014 13:31 SW 6010C Total'Arsenic <3.0 3.0 KM 05/22/2014 13:31 SW 6010C Total Mercury <0.4 0.4 KM 05/22/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 05/22/2014 13:31 SW 6010C pH (Standard Units) * 3.53 2.00 JNI 05/22/2014 09:20 SW-9045D Total Molybdenum <5 5 KM 05/22/2014 13:31 SW 6010C Chloride 588 200 JM 05/22/201410:35 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "NO3/NO2-N", "Mn" AND "Zn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Fe", "Mn", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG3L-NC ADM CORP., NC NITRO GRO 3 LIQUID 5/15/2014 611/2014-6/30/2014 1.1314 Na mg/I = (Na mg/kg x % Solids) = 100 = (920 x 14.1500) _ 100 = 130.18 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (6390 x 14.1500) = 100 = 904.185 Mg mg/I = (mg mg/kg x % Solids) = 100 = (411 x 14.1500) _ 100 = 58.1565 Na meq = Na mg/I + Molec.Wgt.Na = 130.18 + 23 = 5.66 Ca meq = Ca mg/I = Molec.Wgt.Ca = 904.185 _ 20 = 45.2092 Mg meq = Mg mg/I + Molec.Wgt.Mg = 58.1565 _ 12 = 4.84638 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.66 + SgrRoot[0.5(45.2092+4.84638)] = 1.13137 Printed: 2/18/2015 Page 1 - 12:14 Page: i of 2 Report' Number: 14-184-0205 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 56286 Sample Id : NG3YC �L A&L Eastern Laboratories, Inc: 7621 Whitepine Road Richmond, virginia.23237 (804)'743S401 Fax (804) 271-6446 wwwaleastem.com Project: NG3 YC NC CERT#257 REPORT OF ANALYSIS Total Solids * 11.20 112000 100.0 JM Moisture * 88.80 100.0 JM Total Kjeldahl Nitrogen 7.58 75800 10.0 JM Total Phosphorus 0.78 7790 100 KM Total Potassium 0.05 454 100 KM Total Sulfur 0.74 7420 100 KM Total Calcium 0.15 1460 100 KM Total Magnesium 0.05 486 100 KM Total Sodium 0.09 923 100 KM Total Iron 924 100 KM Total Aluminum 500 100 KM Total Manganese 41 5 KM Total Copper 12 5 KM Total Zinc 24 5 KM Ammonia Nitrogen 0.23 2320 10.0 JM Organic N 7.35 73480 10.0 Nitrate+Nitrite-N 10.7 2.00 JM Total Cadmium <2.0 2.0 KM All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Date Sampled: 7/2/2014 00:00:00 Date Received: 07/03/2014 00:00 Date Reported: 07/11/2014 07/03/2014 12:35 07/03/2014 12:35 07/07/2014 08:19 07/08/2014 10:35 07/08/2014 10:35 07/08/2014 10:35 07/08/2014 10:35 07/08/2014 10:35 07/08/2014 10:35 07/08/2014 10:35 07/08/2014 10:35 07/08/2014 10:35 07/08/2014 10:35 07/08/2014 10:35 07/07/2014 08:19 07/07/2014 08:19 07/07/2014 08:20 07/08/2014 10:35 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any'advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SM-254OG SM-254OG SM-4500-NH3C-TKN SW 601 OC SW 601 OC SW 601 OC SW 6010C SW 601 OC SW 601 OC SW 601 OC SW 6010C SW 6010C SW 601 OC SW 601 OC SM-4500-NI3C CALCULATION SM-450ONO3F SW 601 OC Page: 2 of 2 Report Number: 14-184-0205 A&L Eastern Laboratories., Inc.. Account Number: 45637 2 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.W6 Submitted By: LUKE STOWERS w Maleastern.com Send To: ADM Project: NG3 YC SCOTT PHILLIPS NC CERT#257 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 REPORT OF ANALYSIS Date Sampled: 7/2/2014 00:00:00 Lab Number: 56286 Date Received: 07/03/2014 00:00 Sample Id : NG3YC Date Reported: 07/11/2014 Total Chromium 11 5 KM 07/08/2014 10:35 SW 6010C Total Nickel 5 5 KM 07/08/2014 10:35 SW 6010C Total Lead <5 5 KM 07/08/2014 10:35. SW 6010C Total Arsenic <3.0 3.0 KM 07/08/2014 10:35 SW 6010C Total Mercury <0.4 0.4 KM 07/08/2014 09:00 SW-7471 B Total Selenium ' <5.0 5.0 KM 07/08/2014 10:35 SW 6010C pH (Standard Units) * 3A6 2.00 JM 07/07/2014 08:44 SW-9045D Total Molybdenum <5 5 KM 07/08/2014 10:35 SW 6010C Chloride 382 200 JM 07/08/2014 08:30 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND ".S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG3L-NC ADM CORP., NC NITRO GRO 3 LIQUID 7/2/2014 7/1/2014-7/31/2014 1.7828 Na mg/I = (Na mg/kg x % Solids) + 100 = (923 x 11.2000) + 100 = 103.376 Ca mg/I = (Ca mg/kg x % Solids) = 100- (1460 x 11.2000) = 100 = 163.52 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (486 x 11.2000) _ 100 = 54.432 Na meq = Na mg/I _ Molec.Wgt.Na = 103.376 _ 23 = 4.49461 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 163.52 = 20 = 8.176 Mg meq = Mg mg/I + Molec.Wgt.Mg = 54.432 = 12 = 4.536 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.49461 + SgrRoot[0.5(8.176+4.536)] = 1.78279 Printed: 2/18/2015 Page 1 12:15 Page: 1 of 2 Report Number: 14-206-0202 A&L EaStem Laboratories, Ina - Account Number: 45637 7621 Whitepine Richmond,Vir inia23237 804 743J401 Fax 804 271.6446 P 9 ( 1 ( 1 Submitted By: LUKE STOWERS wwwaleastern.com Send To: ADM Project: ADM YEAST CREAM SCOTT PHILLIPS ; NC CERT#257 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 REPORT OF ANALYSIS Date Sampled: 7/23/2014 11:00:00 Lab Number: 56692 Date Received: 07/25/2014 00:00 Sample Id : ADM YEAST CREAM Date Reported: 07/31/2014 Total Solids * 13.83 138300 100.0 JM 07/25/2014 15:00 SM-254OG Moisture * 86.17 100.0 JM 07/25/2014 15:00 SM-2540G Total Kjeldahl Nitrogen 7.59 75900 10.0 JM 07/28/2014 09:00 SM-4500-NH3C-TKN Total Phosphorus 0.82 8190 100 KM 07/30/2014 16:12 SW 6010C Total Potassium ! 0.04 365 100 KM 07/30/2014 16:12 SW 6010C Total Sulfur 0.65 6490 100 KM 07/30/2014 16:12 SW 6010C Total Calcium 0.13 1290 100 KM 07/30/2014 16:12 SW 6010C Total Magnesium 0.03 323 100 KM 07/30/2014 16:12 SW 6010C Total Sodium 0.07 701 100 KM 07/30/2014 16:12 SW 6010C Total Iron 320 100 KM 07/30/2014 16:12 SW 6010C Total Aluminum 200 100 KM 07/30/2014 16:12 SW 6010C Total Manganese .11 5 KM 07/30/2014 16:12 SW 6010C Total Copper 13 5 KM 07/30/2014 16:12 SW 6010C Total Zinc 11 5 KM 07/30/2014 16:12 SW 6010C Ammonia Nitrogen 0.08 795 10.0 JM 07/28/2014 09:00 SM-4500-NH3C Organic N 7.51 75105 10.0 07/28/2014 09:00 CALCULATION Nitrate+Nitrite-N 10.1 2.00 JM 07/28/2014 08:20 SM-450ONO3F Total Cadmium <2.0 2.0 KM 07/30/2014 16:12 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-206-0202 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS ' 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: -56692 Sample Id : ADM YEAST CREAM � L A&L Eastern Laboratories, Ina, 7621 Whitepine Road Richmond, Virginia 23237 (804) 743 9907 Fax (804) 271 6946 wwwaleastem.com Project: ADM YEAST CREAM - NC CERT4257 REPORT OF ANALYSIS Date Sampled: 7/23/2014 11:00:00 Date Received: 07/25/2014 00:00 Date Reported: 07/31/2014 Total Chromium 6 Total Nickel <5 Total Lead <5 Total Arsenic <3.0 Total Mercury <0.4 Total Selenium <5.0 pH (Standard Units) * 3.37 Total Molybdenum <5 Chloride 319 Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. 5 KM 07/30/2014 16:12 SW 6010C 5 KM 07/30/2014 16:12 SW 6010C 5 KM 07/30/2014 16:12 SW 6010C 3.0 KM 07/30/2014 16:12 SW 6010C 0.4 KM 07/28/2014 09:00 SW-7471 B 5.0 KM 07/30/2014 16:12 SW 6010C 2.00 JM 07/28/2014 09:00 SW-9045D 5 KM 07/30/2014 16:12 SW 6010C 200 JM 07/28/2014 09:25 SM-4500CI-D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG3L-NC ADM CORP., NC NITRO GRO 3 LIQUID 7/23/2014 8/1/2014-813112014 1.6765 Na mg/I = (Na mg/kg x % Solids) _ 100 = (701 x 13.8300) = 100 = 96.9483 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (1290 x 13.8300) _ 100 = 178.407 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (323 x 13.8300) _ 100 = 44.6709 Na meq = Na mg/I _ Molec.Wgt.Na = 96.9483 _ 23 = 4.21514 Ca meq = Ca mg/I = Molec.Wgt.Ca = 178.407 _ 20 = 8.92035 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 44.6709 = 12 = 3.72258 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.21514 _ SgrRoot[0.5(8.92035+3.72258)] = 1.6765 Printed: 2/18/2015 Page 1 12:16 Page: 1 of 2 Report Number: 14-233-0208 Account Number: 45637 Submitted By: LUKE STOWERS Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 57152 Sample Id : NG3L p� A&L Eastern Laboratories, Inc.. •7621 Whitepine Road Richmond, Virginla 23237 (804) 743.9401 .Fax (804) 271-6446 wwwaleastemxom Project: NG3L/NC CERT#257 REPORT OF ANALYSIS Date Sampled: 8/20/2014 08:50:00 Date Received: 08/21/2014 00:00 Date Reported: 08/28/2014 Total Solids" 10.01 100100 100.0 JM 08/21/2014 15:49 SM-2540G Moisture * 89.99 100.0 JM 08/21/2014 15:49 SM-2540G Total Kjeldahl Nitrogen 7.57 75700 10.0 JM 08/22/2014 08:24 SM-4500-NH3C-TKN Total Phosphorus 0.73 7310 100 KM 08/27/2014 15:00 SW 6010C Total Potassium 0.04 423 100 KM 08/27/2014 15:00 SW 6010C Total Sulfur 0.62 6190 100 KM 08/27/20.14 15:00 SW 6010C Total Calcium 0.13 1330 100 KM 08/27/2014 15:00 SW 6010C Total Magnesium 0.03 269 100 KM 08/27/2014 15:00 SW 6010C Total Sodium 0.12 1170 100 KM 08/27/2014 15:00 SW 6010C Total Iron 238 100 KM 08/27/2014 15:00 SW 6010C Total Aluminum 200 100 KM 08/27/2014 15:00 SW 6010C Total Manganese 44 5 KM 08/27/2014 15:00 SW 6010C Total Copper 11 5 KM 08/27/2014 15:00 SW 6010C Total Zinc 10 5 KM 08/27/2014 15:00 SW 6010C Ammonia Nitrogen 0.36 3600 10.0 JM 08/22/2014 08:24 SM-4500-NH3C Organic N 7.21 72100 10.0 08/22/2014 08:24 CALCULATION Nitrate+Nitrite-N 32.0 2.00 JM 08/25/2014 08:25 SM-450ONO3F Total Cadmium <2.0 2.0 KM 08/27/2014 15:00 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made A to the work, the results, or the company in any'advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie.Holt Page: 2 of 2 Report Number: 14-233-0208 Nvjy A&L EasternLaboratories, Inc._ Account Number. 45687 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804)271-6446 Submitted By: LUKE STOWERS wwwaleastern.com Send To: ADM Project: NG3L/NC CERT#257 SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 REPORT OF ANALYSIS Date Sampled: 8/20/2014-08:50:00 Lab Number: 57152 Date Received: 08/21/2014 00:00 Sample Id: NG3L Date Reported: 08/28/2014 Total Chromium <5 5 KM 08/27/2014 15:00 SW 6010C Total Nickel <5 5 KM 08/27/2014 15:00 SW 6010C Total Lead <5 5 KM 08/27/2014 15:00 SW 6010C Total Arsenic <3.0 3.0 KM 08/27/2014 15:00 SW 6010C Total Mercury <0.4 0.4 KM 08/22/2014 12:00 SW-7471 B Total Selenium <5.0 5.0 KM 08/27/2014 15:00 SW 6010C pH (Standard Units) * 3.54 2,00 JM 08/22/2014 08:19 SW-9045D Total Molybdenum <5 5 KM 08/27/2014 15:00 SW 6010C Chloride 389 200 JM 08/22/2014 09:30 SM-4500CI-D Comments: CHLORIDE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. THE MATRIX SPIKE WAS OUT OF -LIMITS FOR "Ca", AND "Se", ALL OTHER QA/QC DATA IS WITHIN LIMITS. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 941 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any, advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2044-01-NG3L-NC ADM CORP., NC NITRO GRO 3 LIQUID 8/20/2014 911/2014-9130/2014 2.4138 Na mg/I = (Na mg/kg x % Solids) + 100 = (1170 x 10.0100) = 100 = 117.117 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (1330 x 10.0100) _ 100 = 133.133 Mg mg/I = (mg mg/kg x % Solids) = 100 = (269 x 10.0100) _ 100 = 26.9269 Na meq = Na mg/I -= Molec.Wgt.Na = 117.117 -= 23 = 5.09204 Ca meq = Ca mg/1= Molec.Wgt.Ca = 133.133 + 20 = 6.65665 Mg meq = Mg mg/I + Molec.Wgt.Mg = 26.9269 + 12 = 2.24391 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.09204 _ SgrRoot[0.5(6.65665+2.24391)] = 2.41378 Printed: 2/18/2015 Page 1 12:16 Page: 1 of 2 Report Number: 14-272-0204 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 57826 Sample Id: ADM YEAST CREAM A&L Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271.6446 wwwaleastern.com Project: ADM YEAST CREAM NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 9/25/2014 14:00:00 Date Received: 09/29/2014 00:00 Date Reported: 10/02/2014 Total Solids * 11.17 111700 100.0 MW 09/30/2014 08:44 Moisture 88.83 100.0 MW 09/30/2014 08:44 Total Kjeldahl Nitrogen 7.59 75900 10.0 JM 09/30/2014 09:00 Total Phosphorus 0.88 8790 100 KM 09/30/2014 12:50 Total Potassium 0.04 372 100 KM 09/30/2014 12:50 Total Sulfur 0.63 6260 100 KM 09/30/2014 12:50 Total Calcium 0.21 2110 100 KM 09/30/2014 12:50 Total Magnesium 0.02 193 100 KM 09/30/2014 12:50 Total Sodium 1 0.11 1130 100 KM 09/30/2014 12:50 Total Iron 230 100 KM 09/30/2014 12:50 Total'Aluminum 200 100 KM 09/30/2014 12:50 Total Manganese 13 5 KM 09/30/2014 12:50 Total Copper 11 5 KM 09/30/2014 12:50 Total Zinc 11 5 KM 09/30/2014 12:50 Ammonia Nitrogen 0.34 3400 10.0 JM 09/30/2014 09:00 Organic N 7.25 72500 10.0 09/30/2014 09:00 Nitrate+Nitrite-N 54.6 2.00 JM 09/30/2014 09:00 Total Cadmium <2.0 2.0 KM 09/30/2014 12:50 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SM-2540G SM-254OG SM-4500-NH3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NH3C CALCULATION SM-450ONO3F SW 6010C Page: 2 of 2 Report Number: 14-272-0204 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 57826 Sample Id: ADM YEAST CREAM A�A&L Eastern Laboratories, Inc:_ •7621 Whitepine Road Richmond, Virginia,23237 (804) 743.9401 • Fax (804) 271.6446 wwwaleastern.com Project: ADM YEAST CREAM NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 9/25/2014 14:00:00 Date Received: 09/29/2014 00:00 Date Reported: 10/02/2014 Total Chromium 6 5 KM, 09/30/2014 12:50 SW 6010C Total Nickel <5 5 KM 09/30/2014 12:50 SW 6010C Total Lead <5 5 KM 09/30/2014 12:50 SW 6010C Total Arsenic <3.0 3.0 KM 09/30/2014 12:50 SW 6010C Total Mercury <0.4 0.4 KM 09/30/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 09/30/2014 12:50 SW 6010C pH (Standard Units) * 3.32 2.00 JM 09/30/2014 09:49 SW-9045D Total Volatile Solids 96.58 965800 100.0 MW 09/30/2014 08:44 SM-2540G Total Molybdenum <5 5 KM 09/30/2014 12:50 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn" AND "NO3/NO2-N". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca", "Na", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on. all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , lc i to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2044-01-NG3L-NC ADM CORP., NC NITRO GRO 3 LIQUID 9/25/2014 10/1/2014-10/31/2014 2.1060 Na mg/I = (Na mg/kg x % Solids) = 100 = (1130 x 11.1700) = 100 = 126.221 Ca mg/1 = (Ca mg/kg x % Solids) _ 100 = (2110 x 11.1700) = 100 = 235.687 Mg mg/I = (mg mg/kg x % Solids) = 100 = (193 x 11.1700) + 100 = 21.5581 Na meq = Na mg/1 _ Molec.Wgt.Na = 126.221 _ 23 = 5.48787 Ca meq = Ca mg/1 _ Molec.Wgt.Ca = 235.687 = 20 = 11.7844 Mg meq = Mg mg/I + Molec.Wgt.Mg = 21.5581 -= 12 = 1.79651 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.48787 = SgrRoot[0.5(11.7844+1.79651)] = 2.10598 Printed: 2/18/2015 Page 1 12:17 Page: 1 of 2 Report Number: 14-297-0205 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 58341 Sample Id: ADM YEAST CREAM A A&L Eastern, Laboratories, Inc. 7621 Whitepine Road Richmond; Virginia 23237 (804) 743.9401 Fax (804) 271.6446 WIMaleastern.com Project: ADM YEAST CREAM NC CERT#257 REPORT OFANALYSIS Date Sampled: 10/23/2014 12:00:00 Date Received: 10/24/2014 00:00 Date Reported: 10/30/2014 Total Solids * 14.39 143900 100.0 JM 10/24/2014 15:00 Moisture 85.61 100.0 JM 10/24/201415:00 Total Kjeldahl Nitrogen ! 7.71 77100 10.0 JM 10/27/2014 08:55 Total Phosphorus 0.87 8690 100 KM 10/27/2014 14:56 Total Potassium 0.02 228 100 KM 10/27/2014 14:56 Total Sulfur 0.47 4680 100 KM 10/27/2014 14:56 Total Calcium 0.15 1510 100 KM 10/27/2014 14:56 Total Magnesium 0.01 130 100 KM 10/27/2014 14:56 Total Sodium 0.05 519 100 KM 10/27/2014 14:56 Total Iron 721 100 KM 10/27/2014 14:56 Total Aluminum 500 100 KM 10/27/2014 14:56 Total Manganese 9 5 KM 10/27/2014 14:56 Total Copper 12 5 KM 10/27/2014 14:56 Total Zinc 17 5 KM 10/27/2014 14:56 Ammonia Nitrogen 0.40 3960 10.0 JM 10/27/2014 08:55 Organic N 7.31 73140 10.0 10/27/2014 08:55 Nitrate+Nitrite-N 17.4 2.00 JM 10/27/2014 00:00 Total Cadmium <2.0 2.0 KM 10/27/2014 14:56 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. SM-2540G SM-2540G SM-4500-NH3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NH3C CALCULATION SM-450ONO3F SW 6010C Debbie Holt Page: 2 of 2 Report Number: 14-297-0205 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 58341 Sample Id : ADM YEAST CREAM 99, A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 741.9401 Fax (804) 271-6446 www aleastern.com Project: ADM YEAST CREAM NC CERT#257 REPORT OF ANALYSIS Date sampled: 10/23/201412:00:00 Date Received: 10/24/2014 00:00 Date Reported: 10/30/2014 Total Chromium 6 5 KM 10/27/2014 14:56 SW 6010C Total Nickel <5 5 KM 10/27/2014 14:56 SW 6010C Total Lead <5 5 KM 10/27/2014 14:56 SW 6010C Total Arsenic <3.0 3.0 KM 10/27/2014 14:56 SW 6010C Total Mercury <0.4 0.4 KM 10/27/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 10/27/2014 14:56 SW 6010C pH (Standard Units) " 8.72 2.00 JM 10/27/2014 08:55 SW-9045D Total Volatile Solids 96.67 966700 100.0 JM 10/24/2014 15:00 SM-2540G Total Molybdenum <5 5 KM 10/27/2014 14:56 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "AI" AND "Cr". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2044-01-NG3L-NC ADM CORP., NC NITRO GRO 3 LIQUID 10/23/2014 11/1/2014-11/30/2014 1.3029 Na mg/I = (Na mg/kg x % Solids) _ 100 = (519 x 14.3900) _ 100 = 74.6841 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (1510 x 14.3900) =100 = 217.289 Mg mg/I = (mg mg%kg x % Solids) = 100 = (130 x 14.3900) =100 = 18.707 Na meq = Na mg/I = Molec.Wgt.Na = 74.6841 _ 23 = 3.24713 Ca meq = Ca mg/I -= Molec.Wgt.Ca = 217.289 = 20 = 10.8645 Mg meq = Mg mg/I = Molec.Wgt.Mg = 18.707 + 12 = 1.55892 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.24713 = SgrRoot[0.5(10.8645+1.55892)] = 1.30285 Printed: 2/18/2015 Page 1 12:18 Page: 1 of 2 Report Number: 14-325-0203 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORS ST SE SOUTHPORT , NC 28461 Lab Number: 58872 Sample Id : ADM YEAST CREAM A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond- Virginia 23237 (804)741.9401, Faz (804) 271-WG wwwaleastern.com Project: ADM YEAST CREAM NC CERT#257 REPORT OF ANALYSIS Date Sampled: 11/18/2014 10:00:00 Date Received: 11/21/2014 00:00 Date Reported: 12/02/2014 Total Solids 14.04 140400 100.0 BW 11/21/2014 15:00 SM-2540G Moisture * 85.96 100.0 BW 11/21/2014 15:00 SM-2540G Total Kjeldahl Nitrogen 7.55 75500 10.0 JM 11/24/2014 09:24 SM-4500-NH3C-TKN Total Phosphorus 0.87 8680 100 KM 11/24/2014 11:01 SW 6010C Total Potassium 0.03 329 100 KM 11/24/2014 11:01 SW 6010C Total Sulfur 0.47 4710 100 KM 11/24/2014 11:01 SW 6010C Total Calcium 0.21 2120 100 KM 11/24/2014 11:01 SW 6010C Total Magnesium 0.01 124 100 KM 11/24/2014 11:01 SW 6010C Total Sodium 0.07 701 100 KM 11/24/2014 11:01 SW 6010C Total Iron 232 100 KM 11/24/2014 11:01 SW 6010C Total Aluminum 200 100 KM 11/24/2014 11:01 SW 6010C Total Manganese 7 5 KM 11/24/2014 11:01 SW 6010C Total Copper 10 5 KM 11/24/2014 11:01 SW 6010C Total Zinc 10 5 KM 11/24/2014 11:01 SW 6010C Ammonia Nitrogen 0.26 2560 10.0 JM 11/24/2014 09:24 SM-4500-NH3C Organic N 7.29 72940 10.0 11/24/2014 09:24 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 11/26/2014 08:05 SM-450ONO3F Total Cadmium <2.0 2.0 KM 11/24/2014 11:01 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for theclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-325-0203 Account Number: 45637 Submitted By: CREIGHTON BROWN Send To: ADM SCOTT PHILLIPS 1730 EAST MOORE ST SE SOUTHPORT , NC 28461 Lab Number: 58872 Sample Id: ADM YEAST CREAM A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (B04) 271-WS w. maleastem.com Project: ADM YEAST CREAM NC CERT#257 REPORT OF ANALYSIS Date Sampled: 11/18/2014 10:00:00 Date Received: 11/21/2014 00:00 Date Reported: 12/02/2014 Total Chromium 5 5 KM 11/24/2014 11:01 SW 6010C Total Nickel <5 5 KM 11/24/2014 11:01 SW 6010C Total Lead <5 5 KM 11/24/2014 11:01 SW 6010C Total Arsenic <3.0 3.0 KM 11/24/2014 11:01 SW 6010C Total Mercury <0.4 0.4 KM 11/24/2014 12:00 SW-7471B Total Selenium <5.0 5.0 KM 11/24/2014 11:01 SW 6010C pH (Standard Units) * 3.75 2.00 JM 11/24/2014 09:24 SW-9045D Total Volatile Solids 96.38 963800 100.0 BW 11/21/2014 15:00 SM-254OG Total Molybdenum <5 5 KM 11/24/2014 11:01 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB IS OUT OF LIMITS FOR "Mn", THE MATRIX XPIKE IS OUT OF LIMITS FOR "Se", AND "S", ALL OTHER QA/QC IS WITHIN LIMITS. I All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , L to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt I Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2044-01-NG3L-NC ADM CORP., NC NITRO GRO 3 LIQUID 11/18/2014 1211/2014-12/31/2014 1.4974 Na mg/I = (Na mg/kg x % Solids) _ 100 = (701 x 14.0400) _ 100 = 98.4204 Ca mg/1= (Ca mg/kg x % Solids) = 100 = (2120 x 14.0400) = 100='297.648 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (124 x 14.0400) + 100 = 17.4096 Na meq = Na mg/I _ Molec.Wgt.Na = 98.4204 = 23 = 4.27915 Ca meq = Ca mg/I = Molec.Wgt.Ca = 297.648 _ 20 = 14.8824 Mg meq = Mg mg/I = Molec.Wgt.Mg = 17.4096 _ 12 = 1.4508 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.27915 = SgrRoot[0.5(14.8824+1.4508)] = 1.4974 r- I Printed: 2/18/2015 Page 1 12:18 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 90.27 SITE #: NC BR 00054 FIELD# : BR 00054 0001 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 3038-2 ACRES UTILIZED: 14.80 ACRES PERMITTED: 14.80 Page Lime Applied *** Date Lb,/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. ,cation Past 24 Appli- Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate Nitrate and (ppm) Crop MONTH Total Per Acre Solids 1/20/14 88.99 (W) 6.013 29.13 1.752 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 (CORN 1/21/14 197.87 (W) 13.370 29.13 3.895 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 CORN 1/22/14 23.03 (W) 1.556 29.13 0.453 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100. p 2,090.00 p 8.24 p 9121 CORN Jan-14 1 309.89 (W) 20.939 1 Total Gallons/Ac: Total Wet Tons/Ac: 20.94 As Cd Cr Cu Pb Hg Mo Ni Se Zn I)PAN TOTALS: Annual lbs/acre 111 • 0.037 0.037 0.488 0.366 0.061 0.005 0.073 0.207 0.061 2.147 156.14 Cumulative lbs/acre 0.242 0.153 3.561 2.043 0.676 0.044 0.546 1.259 0.880 14.753 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 124 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 oz z x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 58.03 SITE #: NC BR 00054 FIELD# : BR 00054 0002 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 3038-3 ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/17/14 87.13 (W) 8.801 29.13 2.564 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100. p 2,090.00 p 8.24 p 9121 I CORN 1/20/14 112.09 (W) 11.322 29.13 3.298 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100. p 2,090.00 p 8.24 p 9121 1 CORN Jan-14 1 199.22 (W) 20.123 Total Gallons/Ac: Total Wet Tons/Ac: 20.12 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 0.035 0.035 0.469 0.352 0.059 0.005 0.070 0.199 0.059 2.063 150.06 107 Cumulativelbs/acre 0.212 0.135 2.576 1.492 0.469 0.034 0.465 0.980 0.850 12.254 ,?„ Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop 3 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 r 1339.0 267.9 15.0 M , " 375.0 89.0 2500.0 ° ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X �/x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or:Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hrjection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC OWNER: ADM, CO. SITE #: NC BR 00054 FIELD# : BR 00054 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: ONSLOW PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 48.54 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): OLD FIELD #: 3038-4 ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90 Page Luue Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/16/14 107.61 (W) 13.621 29,13 3.968 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 I CORN 1/17/14 59.02 (W) 7.471 29.13 2.176 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 1 CORN Jan-14 166.63 (W) 21.092 Total Gallons/Ac: Total Wet Tons/Ac: 21.09 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.037 0.037 0.492 0.369 0.061 0.005 0.074 0.209 0.061 2.163 157.29 112 Cumulative lbs/acre 0.215 0.142 2.677 1.675 0.483 0.035 0.495 1.018 0.816 13.285 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ? „ 124 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15 0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 XA (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mgAg ** Volatilization Rate: Surface 0.5, Injection/hrcorporation 1.0 k Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 55.17 SITE #: NC BR 00054 FIELD# : BR 00054 0004 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom ofreport OLD FIELD #: 3038-5 ACRES UTILIZED: 9.10 ACRES PERMITTED: 9.10 Page Lane Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/16/14 167.71 (W) 18.430 29.13 5.369 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 I CORN 1/22/14 21.69 (W) 2.384 29.13 0.694 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 1 CORN Jan-14 1 189.40 (W) 20.814 Total Gallons/Ac: Total Wet Tons/Ac: 20.81 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.036 0.036 0.485 0.364 0.061 0.005 0.073 0.206 0.061 2.134 155.21 111 Cumulative lbs/acre 0.185 0.134 2.494 1.455 0.423 0.029 0.417 1.042 0.736 10.609 F11, N_� + me.µ .• 124 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop s n FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ` ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x �2` 2Zo (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 6.46 SITE #: NC BR 00054 FIELD# : BR 00054 0005 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 1.60 ACRES PERMITTED: 1.60 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or . Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/15/14 22.19 (W) 13.869 1 29.13 4.040 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9 221 CORN Jan-14 , 22.19 (W) 13.869 Total Gallons/Ac: Total Wet Tons/Ac: 13.87 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 74 Annual lbs/acre 0.024 0.024 0.323 0.242 0.040 0.003 0.048 0.137 0.040 1.422 103.42 Cumulative lbs/acre 0.181 1 0.330 1.856 1 1.170 1 1.537 1 0.040 0.531 1 0.781 0.897 8.570 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop r 124 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ,; 1339.0 267.9 15.0 ` r 375.0 89.0 2500.0 ." ^ ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X kozLl = (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/htcorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 13.74 SITE #: NC BR 00054 FIELD# : BR 00054 0006 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 5050-1 ACRES UTILIZED: 9.10 ACRES PERMITTED: 9.10 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) "�o Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 1/8/14 6,026.37 (G) 662.238 14.48 0.400 ADNG31, DRY 0-<1/2" SURIN 1.0 0.40 73,900. p 1,860.00 p 35.20 p 30711 I CORN 1/9/14 5,625.89 (G) 618.230 14.48 0.373 ADNG3L DRY 0-<1/2" SURIN 1.0 0.40 73,900. p 1,860.00 p 35.20 p 30711 I CORN 1/17/14 11,105.51 (G) 1220,386 14.48 0.737 ADNG31, DRY 0-<1/2" SURIN 1.0 0.40 73,900.p 1,860.00 p 35.20 p 30711 CORN Jan-14 22,757.77 (G) 2,500.854 Total Gallons/Ac: 2,500.85 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.009 0.006 0.015 0.015 0.015 0.001 0.015 0.015 0.015 0.015 28.09 93 Cumulative lbs/acre 0.182 0.096 2.149 1.159 0.375 0.026 0.349 0.792 0.741 =°m 10.285 ' 1 124 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ; ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID X d 012, (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 68.48 SITE #: NC BR 00054 FIELD# : BR 00054 0007 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 5050-2 ACRES UTILIZED: 14.30 ACRES PERMITTED: 14.30 Page : 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/13/14 174.79 (W) 12.223 29.13 3.561 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100. p 2,090.00 p 8.24 p F 9121 I CORN 1/22/14 23.12 (W) 1.617 29.13 0.471 ADNG2&4. DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 1121 CORN Jan-14 197.91 (W) 13.840 1/22/14 17,930.45 (G) 1253.878 14.48 0.757 ADNG3L ' DRY 0-<1/2" SURIN 0.40 73,900. p 1 1,860.00 p 35.20 p 30711 CORN Jan-14 17,930.45 (G) 1,253.878 I I .::1.0 Total Gallons/Ac: 1,253.88 Total Wet Tons/Ac: 13.84 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 120 0.029 0.027 0.330 0.249 0.048 0.004 0.056 0.145 0.048 1.427 117.29 Cumulative lbs/acre 0.151 0.100 2.219 1.261 0.338 0.022 0.318 0.916 0.503 10.264 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 124 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 * ` 375.0 89.0 2500 0 _ °.; ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID x 14 el_?Ozl�- , (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/hncorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 S ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 10.76 SITE #: NC BR 00054 FIELD# : BR 00054 0008 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 5050-3 ACRES UTILIZED: 7.00 ACRES PERMITTED: 7.00 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/22/14 17,827.33 (G) 2546.761 14.48 1.538 ADNG3L DRY 0-<1/2" SURIN 1.0 0A0 73,900. p 1,860.00 p 35.20 p 30711 CORN Jan-14 17,827.3� (G) 2,546.761 Total Gallons/Ac: 2,546.76 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.009 0.006 0.015 0.015 0.015 0.001 0.015 0.015 0.015 0.015 28.60 94 Cumulative lbs/acre 0.101 0.058 1.595 0.865 0.240 0.015 0.213 0.657 0.243 7.052 °- - Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop *arx r .a z 124 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ' 1339.0 267.9 15.0 375.0 89.0 2500.0 ' ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID x & ilat, d)-,712- 6 //, - � - (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and.imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: - 3.61 SITE #: NC BR 00054 FIELD# : BR 00054 0009 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 5050-4 ACRES UTILIZED: 2.10 ACRES PERMITTED: 2.10 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/23/14 5,980.82 (G) 2848.010 14.48 1.720 ADNG31, DRY 0-<1/2" SURIN 1.0 0.40 73,900. p 1,860.00 p 1 35.20 p 30711 CORN Jan-14 5,980.82 (G) 2,848.010 1 Total Gallons/Ac: 2,848.01 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.010 0.007 0.017 0.017 0.017 0.001 0.017 0.017 0.017 0.017 31.99 106 Cumulative lbs/acre 0.107 0.062 1.366 0.755 0.221 0.017 0.221 0.543 0.463 5.710 �•`3.:". a">" Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop Q IT i - 124 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15 0 375.0 89.0 2500.0 ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID X d, (` d l (SIGNATURE OF LAND APPLIER) DATE "I certify„under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 6.74 SITE #: NC BR 00054 FIELD# : BR 00054 0010 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 5050-5 ACRES UTILIZED: 5.60 ACRES PERMITTED: 5.60 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/23/14 11,155.87 (G) 1992.120 14.48 1.203 ADNG3L DRY 0-<1/2" SURIN 1.0 0.40 73,900. p 1,860.00 p 35.20 p 30711 CORN Jan-14 11,155.87 (G) 1,992.120 Total Gallons/Ac: 1,992.12 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Me Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.007 0.005 0.012 0.012 0.012 <.001 0.012 0.012 0.012 0.012 22.37 74 Cumulative lbs/acre 0.131 0.077 1.691 0.857 0.270 0.019 0.270 0.686 0.563 7.582.;n Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 "n 375.0 89.0 2500.0 ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID XW1114'� o2126 , (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 38.50 SITE #: NC BR 00054 FIELD# : BR 00054 0012 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 21.20 ACRES PERMITTED: 21.20 Page Lune Applied *** Date:::T Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/17/14 35,134.30 (G) 1657.278 '14.48 1.001 ADNG3L DRY 0-<1/2" SURIN 1.0 0.40 73,900.p 1,860.00 p 35.20 p 0711 P30711 I CORN 1/23/14 5,553.95 (G) 261.979 14.48 0.158 ADNG3L DRY 0-<1/2" SURIN 1.0 0.40 73,900. p 1,860.00 p 35.20 p CORN Jan-14 40,688.25 (G) 1,919.257 2/1/14 23,000.00 (G) 1084.9061 14.53 0.657 ADNG3L DRY 0-<1/2" 1 SURIN 1 1.0 1 0.40 70,900. p fT4-1-0.00p 26.80 p 29833 1 CORN Feb-14 23,000.00 (G) 1,084.906 1 Total Gallons/Ac: 3,004.16 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 0.011 0.007 0.018 0.021 0.018 0.001 0.018 0.018 0.018 0.029 32.57 110 Cumulative Ibs/acre 0.200 0.098 2.182 1.245 0.408 0.028 0.379 0.792 0.713 10.268 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop' 124 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or'Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 17.52 SITE #: NC BR 00054 FIELD# : BR 00054 0013 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.50 ACRES PERMITTED: 9.50 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PALL DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pptn) Crop MONTH Total Per Acre Solids 1/7/14 29,007.18 (G) 3053.387 14.48 1.844 ADNG3L DRY 0-<1/2" SURIN 1.0 0.40 73,900. p 1,860.00 p 1 35.20 p 31711 1 CORN Jan-14 29,007.18 (G) 3,053.387 Total Gallons/Ac: 3,053.39 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.011 0.007 0.018 0.018 0.018 0.001 0.018 0.018 0.018 0.018 34.29 113 Cumulativelbs/acre 0.193 0.083 2.377 1.221 0.341 0.024 0.318 0.827 0.452 10.823 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) ," 36.6 34.8 1; 1339.0 p 267.9 "„ ' t 15.0 375.0 89.0 2500.0 r, 124 ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 10.76 SITE #: NC BR 00054 FIELD# : BR 00054 0014 OPERATOR:' SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.70 ACRES PERMITTED: 6.70 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/7/14 17,824.94 (G) 2660.439 14.48 1.606 ADNG3L DRY 0-<1/2" SURIN 1.0 0.40 73,900. p 1,860.00 p 35.20 p 30711 CORN Jan-14 1 17,824.94 (G) 2,660.439 1 1 Total Gallons/Ac: 2,660.44 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 99 0.010 0.006 0.016 0.016 0.016 0.001 0.016 0.016 0.016 0.016 29.88 Cumulative lbs/acre 0.229 0.106 2.508 1.240 0.402 0.025 0.384 0.916 0.697 13.550xl -: Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop �. 124 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 w • N _ ' ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID X (SIGNATURE OR LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, IN7 -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 19.37 SITE #: NC BR 00054 FIELD# : BR 00054 0015 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4.10 ACRES PERMITTED: 4.10 Page : 1 Line Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1115114 66.51 (W) 16.222 29.13 4.725 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27[7��i2,090.00 p 8.24 p 9121 CORN Jan-14 1 66.51 (W) 16.222 1 Total Gallons/Ac: Total Wet Tons/Ac: 16.22 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 86 0.028 0.028 0.378 0.284 0.047 0.004 0.057 0.161 0.047 1.663 120.97 Cumulative Ibs/acre 0.114 0.172 1.088 0.681 0.707 0.021 0.272 0.456 0.630 4.966 r Permit PAN Limit (lbs/acre) 1st Cropl2nd CropF-77-77-77 124 I FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 I 1339.0 267.9 15.0 375.0 89.0 2500.0 t 4 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, NJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 19.17 SITE #: NC BR 00054 FIELD# : BR 00054 0016 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 3.20 ACRES PERMITTED: 3.20 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/15/14 22.85 (W) 7.141 29.13 2.080 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100. p 2,090.00 p 8.24 p 9121 I CORN 1/16/14 42.95 (W) 13.422 29.13 3.910 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100. p 2,090.00 p 8.24 p 9121 CORN Jan-14 1 65.80 (W) 20363 1 Total Gallons/Ac: Total Wet Tons/Ac: 20.56 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 109 0.036 0.036 0.479 0.359 0.060 0.005 0.072 0.204 0.060 2.108 153.34 Cumulative lbs/acre 0.185 0.107 2.160 1.072 0.331 0,027 0.343 0.782 0.787 9.857 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop m " " x•� 124 t;;a s. x.a FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 LL 1339.0 267.9 15.0 375.0 89.0 2500.0 k ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X ZZ& (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: ADM, CO. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 12.38 SITE #: NC BR 00054 FIELD# : BR 00054 0017 OPERATOR: SANKEY FIELDS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.30 ACRES PERMITTED: 2.30 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation ' zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/16/14 42.49 (W) 18.474 29,13 5.381 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 CORN Jan-14 42.49 (W) 18.474 Total Gallons/Ac: Total Wet Tons/Ac: 18.47 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.032 0.032 0.431 0.323 0.054 0.004 0.065 0.183 0.054 1.894 137.77 98 Cumulative lbs/acre 0.086 1 0.064 0.887 1 0.568 1 0.160 0.013 0.171 0.342 0.378 4.203 e " 124 Permit PAN Limit (lbs/acre) 1 st Crop/2nd Crop i k FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 °•". 375.0 89.0 2500.0 -- p ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 i ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: RAINS OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 87.93 SITE #: NC BR 00056 FIELD# : BR 00056 0001 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 4125-1 ACRES UTILIZED: 17.20 ACRES PERMITTED: 17.20 Page Lune Applied *** Date Lbs Ac allons (6) or Cubic Yards (CY) Dry Site Inches Appli-' Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 7/15/14 148.09 (W) 8.610 29,57 2.546 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 SORGHUM 7/16/14 149.27 (W) 8.678 29.57 2.566 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 SORGHUM Jul-14 1 297.36 (W) 17.288 Total Gallons/Ac: Total Wet Tons/Ac: 17.29 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.031 0.020 0.583 0.133 0.051 0.017 0.051 0.204 0.051 2.536 156.43 123 Cumulative Ibs/acre 0.079' 0.053 0.970 0.326 0.132 0.037 0.132 0.366 0.245 4.761 .} Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop , 204 ,, FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X i/alwt__ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: RAINS OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 36.27 SITE #: NC BR 00056 FIELD# : BR 00056 0002 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 4125-2 ACRES UTILIZED: 20.80 ACRES PERMITTED: 20.80 Page : Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 7/9/14 35,496.40 (G) 1706.558 11.20 0.797 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 75,800. p 2,320.00 p 10.70 p 30563 I BERMUDAGRASS 7/15/14 42,158.28 (G) 2026.840 11.20 0.947 ADNG3L MOIST 0- 1/2" SUR 0.5 0.40 75,800.p 2,320.00 p 10.70 p 30563 BERMUDAGRASS Jul-14 1 77,654.68 (G) 3,733.398 1 Total Gallons/Ac: 3,733.40 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 107 0.010 0.007 0.038 0.042 0.017 0.001 0.017 0.017 0.017 0.084 27.17 Cumulative lbs/acre 0.048 0.020 0.609 0.318 0.050 0.003 0.062 0.159 0.047 1.873 ( cre) 1st Crop/2nd Crop Permit PAN Limit lbs/a 4 FD Cumulative Pollutant LoadingRate Limit lbs/acre" ( ) 36.6 34.8 ;. 1339.0 267.9 15 0 375.0 89.0 2500 0 ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID x x 9*&::: �_ - (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: LYNCHBURG, OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 145.65 SITE #: NC BR 00056 FIELD# : BR 00056 0003 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACffY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 4125-3 ACRES UTILIZED: 23.70 ACRES PERMITTED: 23.70 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 7/10/14 107.61 (W) 4.541 29.57 1.343 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 SORGHUM 7/14/,14 384.96 (W) 16.243 29.57 4.803 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 SORGHUM Jul-14 1 492.57 (W) 20.784 Total Gallons/Ac: Total Wet Tons/Ac: 20.78 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.037 0.025 0.701 0.160 0.061 0.021 0.061 0.246 0.061 3.048 188.06 148 Cumulativelbs/acre 0.067 0.035 1 1.149 0.377 1 0.087 0.022 0.097 0.357 0.084 4.454yk Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop t � FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8; 1339.0 267.9 15.0 z 375.0 89.0 2500.0 )M'' ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: LYNCHBURG OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 145.69 SITE #: NC BR 00056 FIELD# : BR 00056 0004 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 2053-1 ACRES UTILIZED: 16.90 ACRES PERMITTED: 16.90 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 7/8/14 83.59 (W) 4.946 29.57 1.463 ADNG2&4. DRY 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 I SORGHUM 7/9/14 237.85 (W) 14.074 '29.57 4.162 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 SORGHUM 7/10/14 171.25 (W) 10.133 29.57 2.996 ADNG2&4: MOIST 0-<I/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 SORGHUM Jul-14 1 492.69 Ml 29.153 Total Gallons/Ac: Total Wet Tons/Ac: 29.15 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 207 0.052 0.034 0.983 0.224 0.086 0.029 0.086 0.345 0.086 4.276 263.79 Cumulative Ibs/acre 0.093 0.049 1.606 0.525 0.121 0.031 0.135 0.499 0.118 6.230 " Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ,t :a FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 " 375.0 89.0 2500 0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X 02/2p/1s (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: FORESTON OWNER: CHIP CARROLL PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 217.24 SITE #: NC BR 00056 FIELD# : BR 00056 0005 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 2056-2 ACRES UTILIZED: 17.00 ACRES PERMITTED: 17.00 Page : 1 Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 6/5/14 302.65 (W) 17.803 30.74 5.473 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SORGHUM 6/6/14 342.09 (W) 20.123 30.74 6.186 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SORGHUM 6/7/14 61.95 (W) 3.644 30.74 1.120 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 SORGHUM Jun-14 1 706.69 (W) 41.570 Total Gallons/Ac: Total Wet Tons/Ac: 41.57 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.077 0.051 1.355 0.818 0.153 0.010 0.128 0.613 0.128 7.744 342.47 239 Cumulative lbs/acre 0.131 0.079 1.955 1.240 0.287 0.036 0.261 0.888 0.236 11.930 s 1 1 293 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 r 'g :,€ ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X 9L�_ , 42 /2U/Gs` (SIGNATURE OF LAND APPLIER) DATE (( "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: RAINS OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 184.59 SITE #: NC BR 00056 FIELD# : BR 00056 0006 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 2056-1 ACRES UTILIZED: 19.90 ACRES PERMITTED: 19.90 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 6/2/14 64.55 (W) 3.244 30.74 0.997 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SORGHUM 6/3/14 217.15 (W) 10.912 30.74 3.354 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SORGHUM 6/4/14 83.51 (W) 4.196 30.74 1.290 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SORGHUM 6/5/14 21.68 (W) 1.089 30.74 0.335 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SORGHUM 6/7/14 85.29 (W) 4.286 30.74 1.317 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 SORGHUM 6/9/14 128.32 (W) 6.448 30.74 1.982 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 SORGHUM Jun-14 600.50 M) 30.175 Total Gallons/Ac: Total Wet Tons/Ac: 30.18 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.056 0.037 0.983 0.594 0.111 0.007 0.093 0.445 0.093 5.621 248.60 174 Cumulative lbs/acre 0.093 0.050 1 1.542 0.864 1 0.143 0.009 0.137 0.583 0.121 7.374' a ru ' Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop R ` * 204 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 , . 1339.0 267.9 15.0 375.0 J 89.0 2500.0 i' ; ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X 021-701 /�- (SIGNATURE ilao_OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NOR -FOLK OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 20.38 SITE #: NC BR 00056 FIELD# : BR 00056 0007 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 2052-1 ACRES UTILIZED: 5.80 ACRES PERMITTED: 5.80 Page : 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/23/14 33,875.28 (G) 5840.566 1 14.43 3.514 ADNG3L DRY 0-<I/2" SUR 0.5 0.40 74,200. p 2,490.00 p 4.85 p F 29934 BERMUDAGRASS May-14 33,875.28 (G) 5,840.566 Total Gallons/Ac: 5,840.57 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.021 0.014 0.035 0.035 0.035 0.003 0.035 0.035 0.035 0.063 60.10 210 Cumulative lbs/acre 0.128 0.064 1.525 0.745 1 0.217 0.020 0.231 0.510 0.157 7.477 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop _w w 293 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 .fl ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDBORO OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 20.80 SITE #: NC BR 00056 FIELD# : BR 00056 0008 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 2052-1 ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/27/14 28,856.10 (G) 3652.671 14.43 2.198 ADNG3L DRY 0-<I/2" SUR 0.5 0.40 74,200. p 2,490.00 p 4.85 p 29934 I BERMUDAGRASS 5/30/14 5,712.23 (G) 723.067 14.43 0.435 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 74,200. p 2,490.00 p 4.85 p 29934 1 BERMUDAGRASS May-14 1 34,568.33 (G) 4,375.738 Total Gallons/Ac: 4,375.74 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 158 Annual lbs/acre 0.016 0.011 0.026 0.026 0.026 0.002 0.026 0.026 0.026 0.047 45.02 Cumulative lbs/acre 0.096 0.044 1.223 0.595 1 0.156 0.011 0.170 1 0.389 0.077 5.712 `€ ' P x'9 230 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 .; 375.0 89.0 2500.0 x4swmv.e.+. ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID x //� xz/," 0,?- , (SIGNA URE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for laiowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = pp- or mg/Icg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: CHIP CARROLL PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 49.42 SITE #: NC BR 00056 FIELD# : BR 00056 0009 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 4126-11 ACRES UTILIZED: 15.70 ACRES PERMITTED: 15.70 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/21/145 82,122.32 (G) 5230.721 14.43 3.147 ADNG31, DRY 0-<1/2" SUR 0.5 0.40 74,200.p 2,490.00 p 4.85 p 29934 BERMUDAGRASS May-14 82,122.32 (G) 5,230.721 Total Gallons/Ac: 5,230.72 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.019 0.013 0.031 0.031 0.031 0.003 0.031 0.031 0.031 0.057 53.82 188 Cumulative lbs/acre 0.060 0.028 0.666 0.338 0.069 0.004 0.082 0.199 0.063 2.299" Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop230 *,m , FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 "' 1339.0 267.9 15.0 375.0 89.0 2500.0 `. i ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID X Z,2� &'//s.- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: CHIP CARROLL PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 3.54 SITE #: NC BR 00056 FIELD# : BR 00056 0010 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S)-* See list at bottom of report ACRES UTILIZED: 11.40 ACRES PERMITTED: 11.40 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation till- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TICN Nitrogen and (ppni) Crop MONTH Total Per Acre Solids 5/21/14 5,884.89 (G) 516.218 1 14.43 0.311 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 74,200. p 2,490.00 p 4.85 p 29934 BERMUDAGRASS May-14 1 5,884.89 (G) 516.2181 Total Gallons/Ac: 516.22 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.002 0.001 0.003 0.003 0.003 <.001 0.003 0.003 0.003 0.006 5.31 19 Cumulative lbs/acre 0.044 0.016 0.639 0.310 0.039 0.002 0.053 0.160 0.036 1.9,99 I 230 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop a d r a - �a FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 (� 1339.0 267.9 15.0 375.0 89.0 2500 0 -- " ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID x DZ�2o ls� i (SIGNATU�E OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am award that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported I r Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, IINJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: RAINS OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 94.29 SITE #: NC BR 00056 FIELD# : BR 00056 0011 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCED:* See list at bottom of re ort ACRES UTILIZED: 13.40 ACRES PERMITTED: 13.40 Page : 1 Line Applied *** Date Lbs/Ac I p allons (G) or Cubic Yards (CY)I Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 7/2/14 318.86 (W) 23.796 29.57 7.036 ADNG2&4: DRY 0- 1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 SORGHUM Jul-14 318.86 (W) 23.796 Total Gallons/Ac: Total Wet Tons/Ac: 23.80 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.042 0.028 0.802 0.183 0.070 0.024 0.070 0.281 0.070 3.490 215.31 169 Cumulative lbs/acre 0.156 0.084 2.400 0.914 0.263 0.038 0.275 0.846 0.172 11.462 77-7777 t"r;" I Crop/2nd 204 Permit PAN Limit (Ibs/acre) 1st Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8,! 1339.0 267.9 15.0 m 375.0 89.0 2500.0 .l �,� ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 I x �U (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported Or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 * Application Method: SUR - Surface, I NJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: RAINS OWNER: CHIP CARROLL PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 111.73 SITE #: NC BR 00056 FIELD# : BR 00056 0012 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.00 ACRES PERMITTED: 16.00 Page : 1 Lime Applied Date NLbs/Ac DATE or allons (G) or Cubic Yards (CY) i or Wet Tons (WT) (specify) I DrySite Tons Per Residual Cond. Dry, Wet, Inches Precip. Past 24 Appli- ' cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 7/1/14 314.87 (W) 19.679. 29.57 5.819 ADNG2&4: DRY 0-<1/2" SURIN 1.0 .0.27 30,100.p 5,310.00 p 2.00 p 12005 I SORGHUM 7/2/14 62.97 (W) 3.936I 29.57 1.164 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 SORGHUM Jul-14 377.84 (W) 23.615 Total Gallons/Ac: Total Wet Tons/Ac: TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Amoral lbs/acre 168 0.042 0.028 0.796 0.182 0.070 0.024 0.070 0.279 0.070 3.464 213.68 Cumulative lbs/acre 0.163 0.088 2.477 0.948 0.276 0.039 0.290 0.869 0.182 11.748 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop e, m 204 f. .. FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 (' 1339.0 267.9 15.0 375.0 89.0 2500.0 r ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported r Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, iINJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: RAINS OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 67.69 SITE #: NC BR 00056 FIELD# : BR 00056 0013 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.20 ACRES PERMITTED: 9.20 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 7/7/14 228.90 (W) 24.880 29.57 7.357 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 30,100. p 5,310.00 p 2.00 p FE005 SORGHUM Jul-14 1 228.90 (W) 24.880 1 1 Total Gallons/Ac: Total Wet Tons/Ac: 24.88 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.044 0.029 0.839 0.191 0.074 0.025 0.074 0.294 0.074 3.649 225.13 177 Cumulative lbs/acre 0.166 0.089 2.547 0.975 0.278 0.040 0.293 0.881 0.184 11.928 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop w 204 r FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 - ri m ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x JA 0Z/2o�! (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN 7 Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC OWNER: CHIP CARROLL SITE #: NC BR 00056 FIELD# : BR 00056 0014 RESIDUAL SOURCE(S):* See list.at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: NORFOLK PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 28.38 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 8.40 ACRES PERMITTED: 8.40 Page : 1 Lime Applied *** Date:::[:: Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) i % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids ,Past "5/30/14 47,160.67 (G) 5614.365 14.43 3.378 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 74,200. p 2,490.00 p 4.85 p 729934 BERMUDAGRASS May-14 1 47,160.67 (G) 5,614.365 1 Total Gallons/Ac: 5,614.37 Total Wet Tons/Ac: As Cd' Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 202 0.020 0.014 0.034 0.034 0.034 0.003 0.034 0.034 0.034 0.061 57.77 Cumulative lbs/acre 0.095 0.047 1.104 0.544 0.156 0.013 0.168 0.366 0.107 5.202 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ' y.,, -rat 1 _;bra 293 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 i; 1 375.0 v 89.0 2500 0 w Nrav=s, ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of.law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = porn or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, 1N1- hijection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: CHIP CARROLL PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 38.25 SITE #: NC BR 00056 FIELD# : BR 00056 0015 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5.40 ACRES PERMITTED: 5.40 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total TPer Acre Solids 7/18/14 129.35 (W) 23.954 29.57 7.083 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 pF771 SUDAN Jul-14 129.35 (W) 23.954 Total Gallons/Ac: Total Wet Tons/Ac: 23.95 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 170 0.043 0.028 0.807 0.184 0.071 0.024 0.071 0.283 0.071 3.513 216.74 Cumulativelbs/acre 0.125 0.063 2.041 0.771 0.201 0.033 0.217 0.655 0.124 9.266IL ``4°' ...: Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop, 71 * " _ ,, �; �" a 212 FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 34.8wpa 1339.0 267.9 15.0 375.0 89.0 2500 0 ' ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X1* &42��)21120 ! l ��— (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]mowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mgAkg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: LYNCHBURG OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 19.04 SITE #: NC BR 00056 FIELD# : BR 00056 0016 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.60 ACRES PERMITTED: 2.60 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppni) Crop MONTH Total Per Acre Solids 7/18/14 64.39 (W) 24.765 29.57 7.323 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 SUDAN Jul-14 64.39 (W) 24.765 Total Gallons/Ac: Total Wet Tons/Ac: 24.77 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 176 0.044 0.029 0.835 0.190 0.073 0.025 0.073 0.293 0.073 3.632 224.09 Cumulative lbs/acre 0,082 0.048 1.407 0.457 0.169 0.033 0.169 0.503 0.092 7.371 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop Q71, 252 %, FD Cumulative Pollutant Loading Rate Limit (lbs/acre) • 36.6 34.8," `' 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false inforration, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: RAINS OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 44.59 SITE #: NC BR 00056 FIELD# : BR 00056 0017 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 70.20 ACRES PERMITTED: 70.20 Page: I Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) ' % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 7/18/14 87.36 (W) 1.244 29.57 0.368 ADNG2&4. MOIST 0-<1/2" SURIN 1.0 0.27 30,100. p 5,310.00 p 2.00 p 12005 I MILLET, PEARL 7/21/14 63.43 (W) 0.904 29.57 0.267 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 MILLET, PEARL Jul-14 150.79 (W) 2.148 Total Wet Tons/Ac: 2.15 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.004 0.003 0.072 0.017 0.006 0.002 0.006 0.025 0.006 0.315 19.44 15 Cumulative lbs/acre 0.004 0.003 0.072 0.017 0.006 0.002 0.006 0.025 0.006 0.315 xu ME ' � 99 r*$�4�Y, UP ,� 5 4"Yk y4 Permit PAN Limit lbs/acre 1st Cro /2nd Crop ( ) p P .�,«C .h. . .. <y3. ,�',�.roY- fK,,. Y�y'Atr � , t<�'�. z �. �i, �4(hLL . y._ �., .� �.y.,, ., �m �,� U N`f 3i.> " � ,�,� s t >•'W,s'+.A+i� .pr•,.. - ..... `�._\` .�E > 4 p..r,,, :t, 1 � 1 �� 51,,��a.�/��{ i... e �.. ., ss ��,"� .'V'$S ` W%r �3t+# � � 1, Y�i i �Yjyup�, N '. .. �: 4r`i r� t�.'. `�,Fi,?M;� ..'(�. 1Ft, ,7 v 4 �M + � * s'uC-i:r-uw,a .4�SII _ 6.� S. ,rg �` .\l.", i?�� �v'r� -R:�e� `:T.iq�(x <•a� '•'%.;, r a. ''�fa i' J4 -_ F- xy .4 z � � �iy �, , � 4 �°»��' �' ' � 9 ��}�3s�� �*d fie, '�` $�.�F�y, _ t• .1j'itlk'^tvt,`xgnv�G•�<<``r` 'rui2\9�,•�cGC�.i �` ea3. .Yr t � , �t x ���X� _ S,'<$U;2TS m j{C�h w�-,�+'Y:l� ��;a,„yn,.,d`,J. ,: ""l� :t`",w"° ass,. :� a � a Fit �` �:,�yLr ',�r:� � /, ;t� #xA'" �� 180 �4 A� r`�ti�1l�� � 4i ��j3,`re���S'Ays ti,''� 1`p�„��,�^+"�x3 ,. ������ � �.;� �.i;iu�_?-� �� �i•"�h`§SpYFk`?�y"Y�°^5H �t"i�rNwy'��'�.'E',�� 3;4�'�`l-"�'�uh���v�'y `!i ��'":`� x�`'„'3;.'N,. 1��' 'y�{�h�.4 +rt��' '�'�, fit?. ,�� ;.��rtr�y :,vAti.)r'a:l��:t�,��' ��<K;+`�= W� FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 34.8� �l, 1339.0 267.9 Z 15.0 375.0 89.0 2500.0�0� q } 'a3 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x 4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for luiowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/Icg ** Volatilization Rate: Surface 0.5, InjectiordIncorporation 1.0 * Application Method: SUR- Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: WOODINGTON OWNER: DENNIS FULLWOOD PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 6.52 SITE #: NC BR 00068 FIELD# : BR 00068 0001 OPERATOR: DENNIS FULLWOOD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 68-1 ACRES UTILIZED: 23.30 ACRES PERMITTED: 23.30 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 8/27/14 21.78 (W) 0.935 15.81 0.148 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 I MILLET, PEARL 8/29/14 19.43 (W) 0.834 15.81 0.132 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 MILLET, PEARL Aug-14 1 41.21 (W) 1.769 Total Gallons/Ac: Total Wet Tons/Ac: 1.77 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.002 0.001 0.061 0.014 0.003 <.001 0.003 0.021 0.003 0.220 17.62 14 Cumulative lbs/acre` 0.191 0.118 2.878 1.544 0.459 0.024 0.359 1.199 0.593 16.190 ° . �.y��, ;.~ ,.�, r•. ,,,."".*"'m.: Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop: 180 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO. GRO 2 CAKE X 0 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime. Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: DENNIS FULLWOOD PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 54.31 SITE #: NC BR 00068 FIELD# : BR 00068 0002 OPERATOR: DENNIS FULLWOOD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 68-2 ACRES UTILIZED: 16.20 ACRES PERMITTED: 16.20 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 8/22/14 107.96 (W) 6.664 15.81 1.054 ADNG2C MOIST 0-<I/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 I BERMUDAGRASS, COASTAL 8/25/14 151.59 (W) 9.357 15.81 1.479 ADNG2C MOIST 0-<I/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 I BERMUDAGRASS, COASTAL 8/26/14 61.88 (W) 3.820 15.81 0.604 ADNG2C MOIST 0-<I/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 I BERMUDAGRASS, COASTAL 8/27/14 22.11 (W) 1.365 ,15.81 0.216 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL Aug-14 343.54 (W) 21.206 Total Gallons/Ac: Total Wet Tons/Ac: 21.21 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 167 0.020 0.013 0.731 0.168 0.034 0.003 0.034 0.255 0.034 2.642 211.22 Cumulative lbs/acre 0.360 0.136 6.453 3.118 1 0.626 0.035 0.489 1 2.542 0.443 30.368 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 240 a 44 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 = 1339.0 267.9 15.0 " 375.0 89.0 2500 0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE x , 2 5: �ZzU (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: DENNIS FULLWOOD PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 29.98 SITE #: NC BR 00068 FIELD# : BR 00068 0003 OPERATOR: DENNIS FULLWOOD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 68-3 ACRES UTILIZED: 7.20 ACRES PERMITTED: 7.20 Page: 1 Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 8/21/14 126.14 (W) 17.519 15.81 2.770 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 I BERMUDAGRASS, COASTAL 8/22/14 20.30 (W) 2.819 15.81 0.446 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 I BERMUDAGRASS, COASTAL 8/28/14 43.19 (W) 5.999 15.81 0.948 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL Aug-14 189.63 (W) 26.337 Total Gallons/Ac: Total Wet Tons/Ac: 26.34 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 208 0.025 0.017 0.908 0.208 0.042 0.003 0.042 0.316 0.042 3.281 262.33 Cumulative Ibs/acre 0.374 0.126 6.923 3.196 0.645 0.035 0.518 2.622 0.516 31.856 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ' s '. 240 ,, FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE X 217 c) / (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported "or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: DENNIS FULLWOOD PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 23.61 SITE #: NC BR 00068 FIELD# : BR 00068 0004 OPERATOR: DENNIS FULLWOOD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report - OLD FIELD #: 68-4 ACRES UTILIZED: 6.00 ACRES PERMITTED: 6.00 Page : 1 Lime Applied *** Date LbsAc allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 8/27/14 149.35 (W) 24.892 15.81 3.935 ADNG2C MOIST 0- 1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL Aug-14 1 149.35 (W) 24.892 1 1 Total Gallons/Ac: Total Wet Tons/Ac: 24.89 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.024 0.016 0.858 0.197 0.039 0.003 0.039 0.299 0.039 3.101 247.93 196 Cumulative lbs/acre 0.320 1 0.129 1 6.044 1 2.888 1 0.580 0.033 0.456 1 2.417 0.712 28.627 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 240 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE X �` ! �— © o21-z-,�) 1 / ,5 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 • • ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NOR -FOLK OWNER: FULLWOOD PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 58.42 SITE #: NC BR 00069 FIELD# : BR 00069 0001 OPERATOR: JERRY FULLWOOD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 69-1 ACRES UTILIZED: 17.60 ACRES PERMITTED: 17.60 • Page Lfine Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 8/27/14 42.05 (W) 2.389 15.81 0.378 ADNG2C MOIST 0-<I/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p F 24934 I BERMUDAGRASS, COASTAL 8/28/14 21.32 (W) 1.211 15.81 0.192 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 I BERMUDAGRASS, COASTAL 8/29/14 21.03 (W) 1.195 15.81 0.189 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 61,200, p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL Aug-14 84.40 (W) 4.795 9/2/14 131.62 (W) 7.478 17.34 1.297 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p121684 I BERMUDAGRASS, COASTAL 9/3/14 128.31 (W) 7.290 17.34 1.264 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p21684 BERMUDAGRASS, COASTAL Sep-14 259.93 (W) 14.768 Total Gallons/Ac: Total Wet Tons/Ac: 19.56 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 149 0.020 0.013 0.636 0.171 0.033 0.003 0.033 0.252 0.033 2.687 184.52 Cumulative Ibs/acre 0.308 1 0.111 1 5.426 1 2.653 1 0.519 0.032 0.411 1 2.145 0.792 26.049 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 293 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE X %hwki d z/zo% S- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Icnowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 0 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: FORESTON OWNER: FULLWOOD PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 27.52 SITE #: NC BR 00069 FIELD# : BR 00069 0003 OPERATOR: JERRY FULLWOOD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.20 ACRES PERMITTED: 16.20 0 Page Lime Applied *** Date:::]::: Lbs/Ac DATE or. allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppnl) Crop MONTH Total Per Acre Solids 8/28/14 108.84 (W) 6.719 15.81 1.062 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 I BERMUDAGRASS, COASTAL 8/29/14 65.20 (W) 4.025 15.81 0.636 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL Aug-14 1 174.04 (W) 10.744 Total Gallons/Ac: Total Wet Tons/Ac: 10.74 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 85 0.010 0.007 0.370 0.085 0.017 0.001 0.017 0.129 0.017 1.338 107.01 Cumulative lbs/acre 0.010 0.007 0.370 0.085 0.017 0.001 0.017 0.129 0.017 1.338 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 207 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fives and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 • ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: LYNCHBURG OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 221.83 SITE #: NC BR 00071 FIELD# : BR 00071 0005 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 20.20 ACRES PERMITTED: 20.20 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/22/14 106.83 (W) 5.289 34.47 1.823 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p F 8823 MILLET 5/23/14 108.64 (W) 5.378 34.47 1.854 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 MILLET 5/27/14 86.39 (W) 4.277 34.47 1.474 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I MILLET 5/29/14 234.78 (W) 11.623 34.47 4.006 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 MILLET 5/30/14 106.90 (W) 5.292 34.47 1.824 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 MILLET May-14 1 643.54 (W)l 31.859 Total Gallons/Ac: Total Wet Tons/Ac: 31.86 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 194 0.066 0.044 0.879 0.264 0.110 0.009 0.110 0.373 0.110 3.756 209.31 Cumulative lbs/acre 0.066 0.044 0.879 0.264 0.110 0.009 0.110 0.373 0.110 3.756 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 228 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 g 2120//f- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITYNAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: CHIP CARROL PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 48.18 SITE #: NC BR 00072 FIELD# : BR 00072 0001 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.50 ACRES PERMITTED: 11.50 Page Lune Applied *** Date Lbs�Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 6/17/14 5,959.23 (G) 518.194 14.15 0.306 ADNG3L DRY 0-<I/2" SUR 0.5 0.40 75,600. p 2,900.00 p 2.00 p 30532 I BERMUDAGRASS, COASTAL 6/18/14 26,856.12 (G) 2335.315 14.15 1.378 ADN03L DRY 0-<1/2" SUR 0.5 0.40 75,600.p 2,900.00 p 2.00 p 30532 BERMUDAGRASS, COASTAL 6/19/14 16,625.90 (G) 1445.730 14.15 0.853 ADNG31, DRY 0-<1/2" SUR 0.5 0.40 75,600.p 2,900.00 p 2.00 p 30532 BERMUDAGRASS, COASTAL 6/25/14 32,208.63 (G) 2800.750 14.15 1.653 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 75,600. p 2,900.00 p 2.00 p 30532 BERMUDAGRASS, COASTAL Jun-14 81,649.88 (G) 7,099.989 Total Gallons/Ac: 7,099.99 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 256 0.025 0.017 0.075 0.075 0.042 0.003 0.042 0.067 0.042 0.385 85.46 Cumulative lbs/acre 0.130 0.066 1.336 0.805 0.219 0.034 0.233 0.505 0.239 6.680 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 299 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 I 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID X Ar U 2/.'70 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent . p = ppm or mg/Icg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 • ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 6.76 SITE #: NC BR 00072 FIELD# : BR 00072 0005 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 3.00 ACRES PERMITTED: 3.00 Page: 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 6/4/14 11,455.63 (G) 3818.543 14.15 2.253 ADNG3L DRY 0- 1/2" SUR 0.5 0.40 75,600. p 2,900.00 p 2.00 p 30532 BERMUDAGRASS, COASTAL Jun-14 11,455.63 (G) 3,818.543 1 1 Total Gallons/Ac: 3,818.54 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.014 0.009 0.041 0.041 0.023 0.002 0.023 0.036 0.023 0.207 45.96 138 Cumulative Ibs/acre 0.014 0.009 0.041 0.041 0.023 0.002 0.023 0.036 0.023 0.207 F Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop1-4 .' rw f 180 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 "LILL„ 1339.0 267.9 15.0 375.0 89.0 2500.0 .. . ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID x Af D2120//-S- (SIGNATURE OF LAND APPLIER) DATE "I certify,'under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, hijection/hicorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 C] ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BLANTON OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 40.21 SITE #: NC BR 00072 FIELD# : BR 00072 0006 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report 1. ACRES UTILIZED: 14.00 ACRES PERMITTED: 14.00 Page Lime Applied *** Date Lba/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, .Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 6/3/14 16,163.07 (G) 1154.505 ,14.15 0.681 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 75,600. p 2,900.00 p 2.00 p 30532 I BERMUDAGRASS, COASTAL 6/4/14 51,980.82 (G) 3712.916 14.15 2.191 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 75,600. p 21900.00 p 2.00 p 30532 BERMUDAGRASS, COASTAL Jun-14 1 68,143.89 (G) 4,867.421 1 Total Gallons/Ac: 4,867.42 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 175 0.017 0.011 0.052 0.052 0.029 0.002 0.029 0.046 0.029 0.264 58.59 Cumulative lbs/acre 0.017 0.011 0.052 0.052 0.029 0.002 0.029 0.046 0.029 0.264 o � � �W ,. ?a Permit PAN Limit lbs/acre 1st Cro /2nd Crop 7 c � FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0Fvi ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID X Now (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent Ip = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 61.48 SITE #: NC BR 00072 FIELD# : BR 00072 0008 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 15.00 ACRES PERMITTED: 15.00 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN Win) Crop MONTH Total Per Acre Solids 6/10/14 52,446.04 (G) 3496.403 14.15 2.063 ADNG31, DRY 0-<1/2" SUR 0.5 0.40 75,600. p 2,900.00 p 2.00 p 30532 I BERMUDAGRASS, COASTAL 6/13/14 34,340.52 (G) 2289.368 14.15 1.351 ADNG31, DRY 0-<1/2" SUR 0.5 0.40 75,600. p 2,900.00 p 2.00 p 30532 I BERMUDAGRASS, COASTAL 6/17/14 5,474.82 (G) 364.988 14.15 0.215 ADNG31, DRY 0-<1/2" SUR 0.5 0.40 75,600. p 2,900.00 p 2.00 p 30532 I BERMUDAGRASS, COASTAL 6/18/14 11,928.06 (G) 795.204 14.15 0.469 ADNG31, DRY 0-<1/2" SUR 0.5 0.40 75,600. p 2,900.00 p 2.00 p 30532 BERMUDAGRASS, COASTAL Jun-14 104,189.44 (G) 6,945.963 Total Gallons/Ac: 6,945.96 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn • P PAN TOTALS: 250 Annual lbs/acre 0.025 0.016 0.074 0.074 0.041 0.003 0.041 0.066 0.041 0.377 83.61 Cumulative lbs/acre 0.025 0.016 0.074 0.074 0.041 0.003 0.041 0.066 0.041 0.377 299 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID X A �/� /e/�4fo� l�2,0�/ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 22.03 SITE #: NC BR 00072 FIELD# : BR 00072 0009 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.30 ACRES PERMITTED: 7.30 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppnl) Crop MONTH Total Per Acre Solids 7/25/14 35,323.74 (G) '4838.868 11.20 2.260 ADNG3L MOIST 0-<1/2" SUR 0.5 0.40 75,800.p 2,320.00 p 10.70 p 30563 I BERMUDAGRASS 7/31/14 11,848.92 (G) 1623.140 11.20 0.758 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 75,800. p 2,320.00 p 10.70 p 30563 BERMUDAGRASS Jul-14 47,172.66 (G) 6,462.008 1 Total Gallons/Ac: 6,462.01 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 184 0.018 0.012 0.066 0.072 0.030 0.002 0.030 0.030 0.030 0.145 47.02 Cumulative lbs/acre 0.018 0.012 0.066 0.072 0.030 0.002 0.030 0.030 0.030 0.145 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop , - v 240 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID X — (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: CHIP CARROLL PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 82.94 SITE #: NC BR 00072 FIELD# : BR 00072 0010 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 23.80 ACRES PERMITTED: 23.80 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) 0 Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids • 7/31/14 11,719.42 (G) 492.413 11.20 0.230 ADNG31, DRY 0-<I/2" SUR 0.5 0.40 75,800. p 2,320.00 p 10.70 p 30563 BERMUDAGRASS, COASTAL Jul-14 11,719.42 (G) 492.413 8/8/14 29,300.95 (G) 1231.132 13.83 0.710 ADNG31, MOIST 0-<1/2" SUR 0.5 0.40 75,900. p 795.00 p 10.10 p 30450 I BERMUDAGRASS, COASTAL 8/9/14 42,147.47 (G) 1770.902 13.83 1.021 ADNG31, MOIST 0-<I/2" SUR 0.5 0.40 75,900. p 795.00 p 10.10 p 30450 I BERMUDAGRASS, COASTAL 8/11/14 62,878.88 (G) 2641.970 13.83 1.524 ADNG31, MOIST 0-<1/2" SUR 0.5 0.40 75,900. p 795.00 p 10.10 p 30450 BERMUDAGRASS, COASTAL Aug-14 134,327.30 (G) 5,644.004 Total Gallons/Ac: 6,136.42 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 212 0.021 0.014 0.044 0.090 0.035 0.003 0.035 0.035 0.035 0.083 56.90 Cumulative lbs/acre 0.021 0.014 0.044 0.090 0.035 0.003 0.035 0.035 0.035 0.083 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ,JAr - - ; r 240 : FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ` 1339.0 267.9 15.0 375.0 89.0 2500 0 ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURM -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: WILLIAMS PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 225.14 SITE #: NC BR 00073 FIELD# : BR 00073 0001 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 28.10 ACRES PERMITTED: 28.10 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pprn) Crop MONTH Total Per Acre Solids 5/9/14 88.67 (W) 3.156 34.47 1.088 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I SORGHUM 5/10/14 150.84 (W) 5.368 34.47 1.850 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I SORGHUM 5/12/14 347.62 (W) 12.371 34.47 4.264 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I SORGHUM 5/13/14 66.03 (W) 2.350 34.47 0.810 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SORGHUM May-14 1 653.16 (W) 23.245 Total Gallons/Ac: Total Wet Tons/Ac: 23.24 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 141 Annual lbs/acre 0.048 0.032 0.641 0.192 0.080 0.006 0.080 0.272 0.080 ` 2.740 152.71 lbs/acre 0.104 0.069 1.087 0.415 0.173 0.029 0.173 0.458 0.303 F77zCumulative 5.302 , ., - Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ; FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ' • 1339.0 267.9 15.0 375.0 89.0 2500.0 °) ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x J0111i /'041 X�_ - 4�v2/ - oo (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation I *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: CHIP CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 326.04 SITE #: NC BR 00075 FIELD# : BR 00075 0004 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 37.00 ACRES PERMITTED: 37.00 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond, Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/19/14 261.28 (W) 7.062 34.47 2.434 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I SOYBEANS 5/20/14 344.66 (W) 9.315 34.47 3.211 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I SOYBEANS 5/21/14 84.52 (W) 2.284 34.47 0.787 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I SOYBEANS 5/22/14 255.41 (W) 6.903 34.47 2.379 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SOYBEANS May-14 945.87 (W) 25.564 Total Gallons/Ac: Total Wet Tons/Ac: 25.56 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 155 0.053 0.035 0.705 0.211 0.088 0.007 0.088 0.300 0.088 3.014 167.96 Cumulative lbs/acre 0.053 0.035 0.705 0.211 0.088 0.007 0.088 0.300 0.088 3.014 r �. Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop E: E 176 - FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for latowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/Icg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: CHIP CARROLL PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 86.29 SITE #: NC BR 00076 FIELD# : BR 00076 0001 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.50 ACRES PERMITTED: 11.50 Page : 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/30/14 153.07 (W) 13.310 34.47 4.588 ADNG2&4 DRY 0-<1/2" SURIN 1.0' 0.27 26,700. p 2,200.00 p 7.83 p SOYBEANS May-14 153.07 (W) 13.3106/2/14 F 109.08 (W) 9.485 30.74 2.916 DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 pSOYBEANS Jun-14 109.08 (W) 9.485 JADNG2&4: i otai tiattons/Ac: Total Wet Tons/Ac: 22.80 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 136 0.045 0.030 0.676 0.297 0.081 0.006 0.075 0.296 0.075 3.336 165.59 Cumulative Ibs/acre 0.045 0.030 0.676 0.297 0.081 0.006 0.075 0.296 0.075 3.336 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 161 FD Cumulative Pollutant LoadingRate Limit Ibs/acre ( ) 36.6 34.8 a. 1339.0 267.9 15.0 375.0 89.0 2500 0 " ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x AV &Z"� 'OmO0( /5' (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, htjection/hicorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: FRANCIS GALLOWAY PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 97.68 SITE #: NC BR 00079 FIELD# : BR 00079 0001 OPERATOR: HARVEY BELL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: 1905-1 ACRES UTILIZED: 11.80 ACRES PERMITTED: 11.80 Page Lime Applied *** Date::::T Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp-) Crop MONTH Total Per Acre Solids 3/22/14 220.26 (W) 18.666 27.43 5.120 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 SOYBEANS Mar-14 1 220.26 (W) 18.666 4/12/14 128.81 (W) 10.9161 28.93 3.158 ADNG2&4. MOIST i 0-<1/2" SURIN i 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 128.81 (W) 10.916 Total Gallons/Ac: Total Wet Tons/Ac: 29.58 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 173 0.050 0.033 0.719 0.166 0.083 0.007 0.083 0.300 0.083 2.443 188.46 Cumulative lbs/acre 0.175 0.098 2.399 1.158 0.392 0.035 0.392 1.003 0.421 12.400 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop' 176 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MINTZ PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 32.47 SITE #: NC BR 00087 FIELD# : BR 00087 0001 OPERATOR: ROY MINTZ CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-87-01 ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 7/28/14 62.32 (W) 7.889 17.33 1.367 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 57,700. p 6,230.00 p 8.66 p 23712 I BERMUDAGRASS 7/29/14 64.97 (W) 8.224 17.33 1.425 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 57,700. p 6,230.00 p 8.66 p 23712 I BERMUDAGRASS 7/30/14 39.97 (W) 5.059 17.33 0.877 ADNG2C DRY 0-<1/2" SUR 0.5 0A0 57,700. p 6,230.00 p 8.66 p 23712 I BERMUDAGRASS 7/31/14 20.12 (W) 2.547 17.33 0.441 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 57,700. p 6,230.00 p 8.66 p 23712 BERMUDAGRASS Jul-14 187.38 (W) 23.719. Total Gallons/Ac: Total Wet Tons/Ac: 23.72 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 195 0.033 0.016 0.830 0.173 0.041 0.003 0.041 0.296 0.041 3.404 214.57 Cumulative lbs/acre 0.209 0.089 4.324 1.707 0.350 0.018 0.461 1.519 0.182 18.604 .� ...< Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ". a tin s,; FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 34.8 r 1339.0 267.9 " .°, 375.0 15.0 89.0 2500 0 .m y Pa, , ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE X 0.../2�/ems (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MINTZ PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 24.25 SITE #: NC BR 00087 FIELD# : BR 00087 0002 OPERATOR: ROY MINTZ CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-87-01 ACRES UTILIZED: 8.30 ACRES PERMITTED: 8.30 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 7/30/14 139.95 (W) 16.861 17.33 2.922 ADNG2C DRY 0- 1/2" SUR 0.5 0.40 57,700. p 6,230.00 p 8.66 p F77 BERMUDAGRASS Jul-14 139.95 (W) 16.861 1 Total Gallons/Ac: Total Wet Tons/Ac: 16.86 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 139 0.023 0.012 0.590 0.123 0.029 0.002 0.029 0.210 0.029 2.419 152.53 Cumulative Ibs/acre 0.081 0.038 1.631 0.735 0.126 0.010 0.126 0.649 0.101 7.990� y.. Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop , - . FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 Vim, 1339.0 267.9 15.0 ;, a 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE X Agz/ o (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MINTZ PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 50.98 SITE #: NC BR 00087 FIELD# : BR 00087 0003 OPERATOR: ROY MINTZ CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-87-01 ACRES UTILIZED: 14.30 ACRES PERMITTED: 14.30 Page : 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm ) Crop p MONTH Total Per Acre Solids 7/31/14 164.57 (W) 11.508 17.33 1.994 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 57,700. p 6,230.00 p 8.66 p 723712 BERMUDAGRASS, COASTAL Jul-14 164.57 (W) 11.508 r17/4114 129.54 (W) 9.059 17.34 1.571 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p 21684 BERMUDAGRASS, COASTAL 129.54 (W) 9.059 Total Wet Tons/Ac: 20.57 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 163 0.025 0.014 0.692 0.165 0.036 0.003 0.036 0.263 0.036 2.933 187.99 Cumulative lbs/acre 0.081 0.039 1.695 0.759 0.129 0.010 0.129 0.685 0.105 8.297 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 230 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE X gZ/�o (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MINTZ PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 14.80 SITE #: NC BR 00087 FIELD# : BR 00087 0004 OPERATOR: ROY MINTZ CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-87-01 ACRES UTILIZED: 4.40 ACRES PERMITTED: 4.40 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 9/3/14 43.43 (W) 9.870 ,17.34 1.712 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p 21684 I BERMUDAGRASS, COASTAL 9/4/14 41.92 (W) 9.527 17.34 1.652 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p 21684 BERMUDAGRASS, COASTAL Sep-14 85.35 (W) 19.397 1 Total Gallons/Ac: Total Wet Tons/Ac: 19.40 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 146 0.020 0.013 0.619 0.175 0.034 0.003 0.034 0.256 0.034 2.745 179.61 Cumulative lbs/acre 0.066 0.034 1.443 0.672 0.110 0.009 0.110 0.601 0.089 7.136 71 n d 230 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE X YA eA� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A =Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MINTZ PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 14.74 SITE #: NC BR 00087 FIELD# : BR 00087 0005 OPERATOR: ROY MINTZ CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-87-01 ACRES UTILIZED: 5.70 ACRES PERMITTED: 5.70 Page Lime Applied ... Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 9/5/14 85.00 (W) 14.912 17.34 2.586 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p 2 1684 BERMUDAGRASS, COASTAL Sep-14 85.00 (W) 14.912 Total Gallons/Ac: Total Wet Tons/Ac: 14.91 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.016 0.010 0.476 0.134 0.026 0.002 0.026 0.197 0.026 2.110 138.08 112 Cumulative Ibs/acre 0.023 0.015 0.607 0.182 0.039 0.003 0.039 0.257 0.039 2.863 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 230 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE Z/ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BLANTON OWNER: MINTZ PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 157.09 SITE #: NC BR 00087 FIELD# : BR 00087 0006 OPERATOR: ROY MINTZ CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.90 ACRES PERMITTED: 16.90 Page Lime Applied *** Date Lbs Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Anuvonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 7/23/14 272.34 (W) 16.115 29.57 4.765 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 30,100. p 5,310.00 p 2.00 p 12005 I MILLET, PEARL 7/24/14 215.95 (W) 12.778 29.57 3.778 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 30,100. p 5,310.00 p 2.00 p 12005 I MILLET, PEARL 7/28/14 42.94 (W) 2.541 29.57 0.751 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 30,100. p 5,310.00 p 2.00 p 12005 MILLET, PEARL Jul-14 1 531.23 (W) 31.434 Total Gallons/Ac: Total Wet Tons/Ac: 31.43 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 0.056 0.037 1.060 0.242 0.093 0.032 0.093 0.372 0.093 4.610 284.43 223 Cumulative lbs/acre 0.101 0.058 1.708 0.656 0.168 0.038 0.168 0.637 0.150 8.113 ja 2 81 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ;i FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ( 1339.0 267.9 15.0 "j+ 375.0 89.0 2500.0 t_ v *{ ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 xqw/// :� Z1,2oll-_S__ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 63.74 SITE #: NC BR 00088 FIELD# : BR 00088 0001 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-88-1 ACRES UTILIZED: 6.00 ACRES PERMITTED: 6.00 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 2/3/14 173.65 (W) 28.942 32.44 9.389 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/10/14 22.83 (W) 3.805 32.44 1.234 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 1 SOYBEANS Feb-14 1 196.48 (W) 32.747 Total Gallons/Ac: Total Wet Tons/Ac: 32.75 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.064 0.043 0.722 0.212 0.106 0.009 0.106 0.297 0.106 2.401 225.21 162 Cumulative lbs/acre 0.350 0.169 4.760 2.286 0.643 0.049 0.639 1.732 0.709 21.310 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop 176 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X Aq6e�-- 02-12e (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or -g/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 217.99 SITE #: NC BR 00088 FIELD# : BR 00088 0002 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-88-2 ACRES UTILIZED: 19.00 ACRES PERMITTED: 19.00 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PALL DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pptn) Crop MONTH Total Per Acre Solids 2/11/14 86.95 (W) 4.576 32.44 1.485 ADNG2&4: MOIST 0-<1/211. SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/28/14 46.28 (W) 2.436 32.44 0.790 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Feb-14 133.23 (W) 7.012 3/3/14 406.92 (W) 21.417 32.44 6.948 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 3/4/14 131.82 (W) 6.938 32.44 2.251 ADNG2&4. DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Mar-14 538.74 M 28.355 Total Gallons/Ac: Total Wet Tons/Ac: 35.37 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 175 0.069 0.046 0.780 0.229 0.115 0.009 0.115 0.321 0.115 2.593 243.23 Cumulative lbs/acre 0.386 1 0.213 5.092 2.583 1 1.003 0.065 0.796 1 1.868 1.134 23.801 1 1 "7 '­." 7" � ".. � " 176 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop r q 41 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ; '� 1339.0 267.9 15.0 375.0 89.0 2500.0 " ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 171.46 SITE #: NC BR 00088 FIELD# : BR 00088 0003 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-88-3 ACRES UTILIZED: 16.50 ACRES PERMITTED: 16.50 Page Lime Applied *** Date _::T Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 2/18/14 395.18 (W) 23.950 32.44 7.769 ADNG2&4: DRY 0-<1/2" SURIN 1,0 0.27 22,700. p 2,070.00 p 4.93 p F 7645 I SOYBEANS 2/24/14 65.72 (W) 3.983 32.44 1.292 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Feb-14 460.90 (W) 27.933 3/3/14 67.63 (W) 4.099 132.44 1.330 ADNG2&4: DRY 1 0-<1/2" SURIN 1.0 1 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Mar-14 67.63 (W) 4.099 Total Gallons/Ac: Total Wet Tons/Ac: 32.03 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.062 0.042 0.707 0.208 0.104 0.008 0.104 0.291 0.104 2.348 220.29 159 Cumulative Ibs/acre 0.362 0.204 4.340 2.321 0.830 0.057 0.769 1.656 1.216 21.223 V 176 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop r; M. FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X 9�w (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ - hyection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 85.57 SITE #: NC BR 00088 FIELD# : BR 00088 0004 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-88-4 ACRES UTILIZED: 8.70 ACRES PERMITTED: 8.70 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 2/24/14 263.78 (W) 30.320 32.44 9.836 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 1 4.93 p 7645 SOYBEANS Feb-14 263.78 (W) 30.320 Total Gallons/Ac: Total Wet Tons/Ac: 30.32 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 150 Annual lbs/acre 0.059 0.039 0.669 0.197 0.098 0.008 0.098 0.275 0.098 2.223 208.52 Cumulative lbs/acre 0.306 0.177 3.981 2.040 0.726 0.049 0.661 1 1.629 0.864 18.160 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop-:; . -. -- x: ;' 176 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 Xz e /� 44� / Jc� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the infomration submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 75.37 SITE #: NC BR 00088 FIELD# : BR 00088 0005 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-88-5 ACRES UTILIZED: 15.60 ACRES PERMITTED: 15.60 Page Lune Applied *** Date _�:T Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 2/28/14 21,429.26 (G) 1373.671 14.53 .0.832 ADNG3L DRY 0-<1/2" SURIN 1.0 0.40 70,900. p 2,410.00 p 26.80 p 29833 SOYBEANS Feb-14 21,429.26 (G) 1,373.671 3/19/14 42.93 (W) 2.752 27,43 0.755 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 I SOYBEANS 3/20/14 135.89 (W) 8.711 27,43 2.389 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 SOYBEANS Mar-14 178.82 (W) 11.463 3/1/14 22,009.59 (G) 1410.871 14.53 0.855 ADNG3L DRY 0-<1/2" SURIN 1.0 0.40 70,900. p 2,410.00 p 26.80 p 29833 SOYBEANS Mar-14 22,009.59 (G) 1,410.871 1 Total Gallons/Ac: 2,784.54 Total Wet Tons/Ac: 11.46 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.029 0.019 0.319 0.087 0.048 0.004 0.048 0.143 0.048 0.993 107.51 171 Cumulative lbs/acre 0.307 0.151 3.851 2.004 0.583 0.045 0.575 1.500 0.871 18.009 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop $ FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 &'. " 375.0 89.0 2500.0 " "• , , ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X mz'e�� j�2ZZZ_jC1__1S_ - (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 91.61 SITE #: NC BR 00088 FIELD# : BR 00088 0006 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-88-6 ACRES UTILIZED: 9.60 ACRES PERMITTED: 9.60 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/23/14 134.84 (W) 14.046 29.13 4.092 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 I SOYBEANS 1/24/14 154.08 (W) 16.050 29.13 4.675 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 SOYBEANS Jan-14 288.92 (W) 30.096 2/10/14 22.95 (W) 2.391 32.44 0.776 DRY 0-<1/2" SURIN 1. 00.27 22,700. p 1 2,070.00 p 4.93 p 7645 SOYBEANS Feb-14 22.95 (W) 2.391 JADNG2&4:1 Total Gallons/Ac: Total Wet Tons/Ac: 32.49 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 172 0.057 0.056 0.754 0.542 0.095 0.008 0.113 0.320 0.095 3.261 240.87 Cumulative lbs/acre 0.404 0.218 5.297 2.904 1 0.757 0.057 0.769 1 1.889 1.249 23.826 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop _ 'S 176 ., FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 - 1339.0 267.9 15.0 375.0 89.0 2500 0ar'. ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 Xzo�0,z4goL5� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 49.67 SITE #: NC BR 00088 FIELD# : BR 00088 0007 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: BR-88-7 ACRES UTILIZED: 4.80 ACRES PERMITTED: 4.80 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) "�0 Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per crer A Solids 2/5/14 153.11 (W) 31.898 32.44 10.34; ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22700. p 2,070.00 p P.93 p 7 445 SOYBEANS Feb-14 153.11 (W) 31.898 I otal Gallons/Ac: Total Wet Tons/Ac: 31.90 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 158 0.062 0.041 0.704 0.207 0.103 0.008 0.103 0.290 0.103 2.339 219.37 Cumulative lbs/acre 0.219 0.126 2.001 1.054 0.398 0.032 0.398 0.828 0.820 10.924 f Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 176 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 ' ' 375.0 89.0 2500.0 ; ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X 44 /� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision irr accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 89.45 SITE #: NC BR 00088 FIELD# : BR 00088 0008 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.00 ACRES PERMITTED: 10.20 Page : 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/23/14 108.07 (W) 15.439 29.13 4.497 ADNG2&4: DRY 0-<1/2" , SURIN 1.0 0.27 28,100. p 2,090.00 p 8.24 p 7 9121 SOYBEANS Jan-14 108.07 (W) 15.439 2/25/14 22.90 (W) 2.245 32.44 0.728 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/26/14 111.16 (W) 10.898 32.44 3.535 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/28/14 44.62 (W) 4.375 32.44 1.419 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Feb-14 178.68 (W) 17.518 Total Gallons/Ac: Total Wet Tons/Ac: 32.96 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.061 0.050 0.746 0384 0.102 0.008 0.111 0.312 0.102 2.867 235.60 169 Cumulative lbs/acre 0.326 0.177 4.061 1.892 0.730 0.052 0.633 1.423 0.977 18.606 a 176 Permit PAN Limit (lbs/acre) I st Crop/2nd Crop ; * ; . fit, , FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 '' 375.0 89.0 2500.0 e,�r:�� ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X Z4, (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: . W00004500 ANNUAL DRY TONS APPLIED: 100.46 SITE #: NC BR 00088 FIELD# : BR 00088 0009 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/22/14 . 128.09 (W) 12.938 29.13 3.769 ADNG2&4. DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 I SOYBEANS 1/23/14 44.55 (W) 4.500 29.13 1.311 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 SOYBEANS Jan-14 172.64 (W) 17.438 2/25/14 131.56 (W) 13.289 32.44 4.311 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Feb-14 131.56 (W) 13.289 3/3/14 23.09 (W) 2.3321 32.44 0.757 ADNG2&4: DRY 0-<1/2" SURIN 1.0 1 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Mar-14 23.09 (W) 2.332 Total Gallons/Ac: Total Wet Tons/Ac: 33.06 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.061 0.051 0.751 0.406 0.101 0.008 0.112 0.315 0.101 2.933 237.47 170 Cumulative lbs/acre 0.352 0.184 3.955 1.972 1 0.652 0.050 0.663 1.439 1.092 .18.403 1 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop z,' 176 2 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 t.Y. ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 /l x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 217.43 SITE #: NC BR 00088 FIELD# : BR 00088 0010 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 20.90 ACRES PERMITTED: 20.90 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip, cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/31/14 352.69 (W) 16.875 29.13 4.916 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 SOYBEANS Jan-14 352.69 (W) 16.875 2/1/14 151.83 (W) 7.265 32.44 2.357 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/3/14 130.45 (W) 6.242 32.44 2.025 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/10/14 42.17 (W) 2.018 32.44 0.655 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Feb-14 324.45 (W) 15.525 11/21/14 11,474.82 (G) 549.034 14.39 0.329 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 77,100. p 3,960.00 p 17.40 p 31253 OATS Nov-14 11,474.82 (G) 549.034 1 12/2/14 4,362.11 (G) 208.7131 14.04 0.122 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 75,500. p 2,560.00 p 2.00 p 30458 Dec-14 4,362.11 (G) 208.713 JOATS ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 217.43 SITE #: NC BR 00088 FIELD#: BR 00088 0010 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 20.90 ACRES PERMITTED: 20.90 Page : 2 Lune Applied *** Date Lbs/Ac 3allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip, cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids Total Gallons/Ac: 757.75 Total Wet Tons/Ac: 32.40 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.062 0.051 0.741 0.406 0.104 0.008 0.114 0.313 0.104 2.882 240.45 167 28 Cumulative lbs/acre 0.366 0.206 5.616 2.747 1.046 0.066 0.781 1.960 0.940 23.992 �V Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop f, 10 176 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 I Ele 1339.0 267.9 15.0 375.0 89.0 2500.0 "%% ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID X 02 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties.for submitting false information, including the possibility offnes and imprisonment for Icnowing violations." N/A =Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR-Surface, INJ -Injection, SURIN - Incorporation See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 150.72 SITE #: NC BR 00088 FIELD# : BR 00088 0011 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 15.50 ACRES PERMITTED: 15.50 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/24/14 223.41 (W) 14.414 29.13 4.199 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 SOYBEANS 1/27/14 246.20 (W) 15.884 29.13 4.627 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 ?5,100.p 2,090.00 p 8.24 p 9121 SOYBEANS Jan-14 469.61 (W) 30.298 2/10/14 21.35 (W) 1.377 32.44 0.447 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7641 SOYBEANS Feb-14 21.35 (W) 1.3771" 11/21/14 11,652.28 (G) 751.760 14.39 0.451 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 77,100. p 3,960.00 p 17.40 p 31253 OATS Nov-14 11,652.28 (G) 751.760 1 1 Total Gallons/Ac: 751.76 Total Wet Tons/Ac: 31.67 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 168 0.058 0.057 0.742 0.549 0.097 0.008 0.115 0.317 0.097 3.223 243.25 28 Cumulative lbs/acre 0.342 0.208 4.962 2.581 0.986 0.063 0.758 1.802 1.116 21.948 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop .„ .9 50 FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 34.8 1339.0 267.9 15 0 375.0 89.0 2500 0 1 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID X * 0 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 61.92 SITE #: NC BR 00088 FIELD# : BR 00088 0012 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5.80 ACRES PERMITTED: 5.80 Page Lane Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/27/14 22.08 (W) 3.807 29.13 1.109 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 I SOYBEANS 1/28/14 66.78 (W) 11.514 29.13 3.354 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 SOYBEANS Jan-14 88.86 (W) 15.321 2/3/14 67.61 (W) 11.459 32.44 3.717 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/5/14 21.55 (W) 3.653 32.44 1.185 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/10/14 21.92 (W) 3.715 32.44 1.205 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Feb-14 111.08 (W) 18.827 Total Gallons/Ac: Total Wet Tons/Ac: 34.15 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 175 0.063 0.051 0.772 0.390 0.106 0.008 0.115 0.323 0.106 2.951 243.73 Cumulative lbs/acre 0.346 0.193 4.841 2.186 0.828 0.055 0.679 1.735 0.589 20.185 :.. Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop $ * 176 R A s qi FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ' ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 72.51 SITE #: NC BR 00088 FIELD# : BR 00088 0013 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of,report ACRES UTILIZED: 6.50 ACRES PERMITTED: 6.50 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pprn) Crop MONTH Total Per Acre Solids 2/10/14 156.11 (W) 24.017 32.44 7.791 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/11/14 67.40 (W) 10.369 32.44 3.364 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Feb-14 1 223.51 (W) 34.386 1 Total Gallons/Ac: Total Wet Tons/Ac: 34.39 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 171 0.067 0.045 0.759 0.223 0.112 0.009 0.112 0.312 0.112 2.521 236.48 Cumulative lbs/acre 0.344 0.193 4.383 2.053 0.953 0.060 0.730 1.555 1.179 19.650 f w q ' 176 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop .,, �" FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 - 375.0 89.0 2500.0 .°? ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or tng/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 63.92 SITE #: NC BR 00088 FIELD# : BR 00088 0014 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 26.00 ACRES PERMITTED: 26.00 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (VM (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 8/19/14 40,597.13 (G) 1561.428 13.83 0.900 ADNG3L MOIST 0-<1/2" SUR 0.5 0.40 75,900. p 795.00 p 10.10 p 30450 BERMUDAGRASS, COASTAL 8/20/14 29,988.01 (G) 1153.385 13.83 0.665 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 75,900.p 795.00 p 10.10 p 30450 BERMUDAGRASS, COASTAL 8/21/14 27,235.01 (G) 1047.500 13.83 0.604 ADNG3L DRY 0-<1/2" SUR 0.5 0.40 75,900.p 795.00 p 10.10 p 30450 BERMUDAGRASS, COASTAL Aug-14 97,820.15 (G) 3,762.313 12/2/14 10,568.35 (G) 406.475 14.04 0.238 ADNG3L DRY 0-<I/2" SUR 0.5 0.40 75,500. p 2,560.00 p 2.00 p 30458 J RYE (FOR GRAIN) 12/31/14 2,244.60 (G) 86.331 14.04 0.051 ADNG3L MOIST 0-<1/2" SUR 0.5 0.40 75,500. p 2,560.00 p 2.00 p 30458 JRYE(FORGRAIN) Dee-14 12,812.95 (G) 492.806 Total Gallons/Ac: 4,255.12 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual ibs/acre 0.015 0.010 0.029 0.062 0.025 0.002 0.025 0.025 0.025 0.054 40.55 132 lg Cumulative Ibs/acre 0.187 0.095 1 1.983 1.230 0.450 0.026 0.404 0.944 0.291 8.907 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 299 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID X &*�oz/,7 G (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 27.82 SITE #: NC BR 00088 FIELD# : BR 00088 0015 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.80 ACRES PERMITTED: 2.80 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 2/5/14 85.76 (W) 30.629 32.44 9.936 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Feb-14 85.76 (W) 30.629 Total Gallons/Ac: Total Wet Tons/Ac: 30.63 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 152 Annual lbs/acre 0.060 0.040 0.676 0.199 0.099 0.008 0.099 0.278 0.099 2.246 210.64 Cumulative Ibs/acre 0,164 0.102 2.039 0.948 0.411 0.025 0.353 0.872 0.348 8.308 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop °af r; 176 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ° 1339.0 267.9 15.0 375.0 89.0 2500.0 ' ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X J/1W/ �_ 0.4/2aje�Is_ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 23.69 SITE #: NC BR 00088 FIELD# : BR 00088 0016 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.00 ACRES PERMITTED: 6.00 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 8/15/14 87.79 (W) 14.632 26.98 3.948 ADNG2&4: DRY 0-<1/2" SURIN 1.0 027 28,800. p 4,480.00 p 5.93 p 11052 WHEAT Aug-14 1 87.79 (W) 14.632 Total Gallons/Ac: Total Wet Tons/Ac: 14.63 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 87 0.024 0.016 0.458 0.103 0.039 0.006 0.039 0.166 0.039 1.634 10738 Cumulative lbs/acre 0.244 0.138 3.723 1.400 0.625 0.042 0.450 1.397 0.470 13.146 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 136 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 f 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X 4 s-- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 46.84 SITE #: NC BR 00088 FIELD# : BR 00088 0017 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.80 ACRES PERMITTED: 9.80 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 8/15/14 173.62 (W) 17.716 26.98 4.780 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11052 WHEAT Aug-14 173.62 (W) 17.716 Total Gallons/Ac: Total Wet Tons/Ac: 17.72 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.029 0.019 0.554 0.124 0.048 0.007 0.048 0.201 0.048 1.979 130.01 106 AA Cumulative lbs/acre 0.251 0.140 1 3.891 1 1.484 0.649 0.044 0.463 1 1.448 0.487 13.636 s t „ 136 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 "F ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X 1 o zza�s 7 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MARTIN MARIETTA PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 92.05 SITE #: NC BR 00088 FIELD# : BR 00088 0019 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 18.80 ACRES PERMITTED: 18.80 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 2/28/14 261.15 (W) 13.891 32.44 4.506 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Feb-14 261.15 (W) 13.891 3/4/14 22.59 (W) 1.202 32.44 0.390 DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Mar-14 22.59 (W) 1.202 JADNG2&4:1 1 1 1 1 1 Total Gallons/Ac: Total Wet Tons/Ac: 15.09 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 75 0.029 0.020 0.333 0.098 0.049 0.004 0.049 0.137 0.049 1.107 103.80 Cumulative Ibs/acre 0.029 1 0.020 1 0.333 1 0.098 1 0.049 0.004 0.049 1 0.137 0.049 1.107 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop 176 FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 02�Z©/ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, II %i Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for -Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: JOE HAWES PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 360.57 SITE #: NC BR 00090 FIELD# : BR 00090 0001 OPERATOR: FRANKLIN COX CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 35.20 ACRES PERMITTED: 35.20 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 2/6/14 216.91 (W) 6.162 32.44 1.999 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/7/14 150.60 (W) 4.278 32.44 1.388 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/19/14 239.28 (W) 6.798 32.44 2.205 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/20/14 243.26 (W) 6.911 32.44 2.242 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 I SOYBEANS 2/21/14 172.83 (W) 4.910 32.44 1.593 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS 2/24/14 88.61 (W) 2.517 32.44 0.817 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 22,700. p 2,070.00 p 4.93 p 7645 SOYBEANS Feb-14 1,111.49 (W) 31.576 Total Gallons/Ac: Total Wet Tons/Ac: 31.58 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN ;• TOTALS: Annual lbs/acre 0.061 0.041 0.697 0.205 0.102 0.008 0.102 0.287 0.102 2.315 217.16 157 Cumulative lbs/acre 0.335 0.167 3.679 1.753 1 0.583 0.045 0.722 1 1.325 0.897 19.192 a ,> Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop _ _ r ; 1* FD Cumulative Pollutant LoadingRate Limit (lbs/acre) ( ) 36.6 34.8 x 1339.0 267.9 °" } 15 0 375.0 89.0 2500 0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 xffA 0?4>04� (SIGNATURE OF "LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: FORESTON OWNER: STANALAND FARMS PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 215.14- SITE #: NC BR 00104 FIELD# : BR 00104 0022 OPERATOR: PARKER STANALAND CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4 1. 10 ACRES PERMITTED: 51.40 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation T] N Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 10/6/14 60.74 (W) 1.478 ;28.01 0.414 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 I WHEAT 10/7/14 169.92 (W) 4.134 '28.01 1.158 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 I WHEAT 10/8/14 215.45 (W) 5.242 28.01 1.468 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 Ij WHEAT 10/9/14 171.47 (W) 4.172 '28.01 1.169 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 I WHEAT 10/10/14 150.51 (W) 3.662 28.01 1.026 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 WHEAT Oct-14 768.09 (W) 18.688 Total Gallons/Ac: Total Wet Tons/Ac: 18.69 As Cd' Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.031 0.021 0.565 0.136 0.052 0.004 0.052 0.220 0.052 1.864 126.68 82 Cumulative Ibs/acre 0.153 0.081 3.077 1.256 0.331 0.022 0.250 1.174 0.191 13.890 �" k *' x Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 002 t SO 115 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 x 1339.0 267.9 15.0 ` " 375.0 89.0 2500.0 , ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Iiijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: FORESTON OWNER: STANALAND FARMS PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 198.45 SITE #: NC BR 00104 FIELD# : BR 00104 0023 OPERATOR: PARKER STANALAND CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4 1. 10 ACRES PERMITTED: 41.10 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards(CY) or Wet Tons (WT) (specify) 0 Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pp-) Crop Total MONTH Per Acre 10/2/14 150.75 (W) 3.668 -28.01 1.027 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 I WHEAT 10/3/14 430.30 (W) 10.470 '28.01 2.933 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 I WHEAT 10/6/14 127.43 (W) 3.100 28.01 0.868 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100. p 1,430.00 p 21.40 p 7842 WHEAT Oct-14 1 708.48 (W) 17.238 Total Wet Tons/Ac: 17.24 As Cd Cr Cu Pb Hg Mo Ni Sc Zn P PAN TOTALS: Annuallbs/acre 76 0.029 0.019 0.521 0.126 0.048 0.004 0.048 0.203 0.048 1.719 116.85 Cumulative lbs/acre " 0.147 0.089 2.943 1.152 0.363 0.029 0.301 1,139 0.226 13.034 " Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop r -° t. FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 * 1339.0 267.9 15 0 375.0 89.0 2500.0 z ADNG2&42:1 = ADM CORP., NO NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X � *4 // 1;14, 6 — e221_?6Z1S— (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: STANALAND FARMS INC. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 115.98 SITE #: NC BR 00104 FIELD# : BR 00104 0025 OPERATOR: PARKER STANALAND CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 15.90 ACRES PERMITTED: 15.90 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 10/13/14 173.74 (W) 10.927 28.01 3.061 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 I WHEAT 10/14/14 87.85 (W) 5.525 28.01 1.548 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 WHEAT 10/20/14 108.40 (W) 6.818 28.01 1.910 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 WHEAT 10/21/14 44.09 (W) 2.773 28.01 0.777 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 WHEAT Oct-14 414.08 M) 26.043 Total Gallons/Ac: Total Wet Tons/Ac: 26.04 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 114 0.044 0.029 0.788 0.190 0.073 0.006 0.073 0.306 0.073 2.597 176.53 Cumulative Ibs/acre 0.080 0.047 1 1.274 0.501 1 0.160 0.020 0.160 0.470 0.104 5.352 ~ .. Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop w FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X "�2 �l (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty oflaw, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisomnent for Imowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, hrjection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: STANALAND FARMS INC. PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 36.51 SITE #: NC BR 00104 FIELD# : BR 00104 0026 OPERATOR: PARKER STANALAND CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5.90 ACRES PERMITTED: 5.90 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 10/20/14 130.36 (W) " 22.095 28.01 6.189 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 WHEAT Oct-14 130.36 (W) 22.095 1 Total Gallons/Ac: Total Wet Tons/Ac: 22.09 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.037 0.025 0.668 0.161 0.062 0.005 0.062 0.260 0.062 2.203 149.77 97 Cumulative lbs/acre 0.060 0.042 1.074 0.375 0.146 0.017 0.146 0.390 0.085 4.259 77 r ;, Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop. FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 Jn ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X x 1em 021-2ol,1_5— (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: STANALAND FARMS, INC PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 249.76 SITE #: NC BR 00104 FIELD# : BR 00104 0028 OPERATOR: PARKER STANALAND CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 33.30 ACRES PERMITTED: 33.30 Page Litne Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 10/21/14 258.17 (W) 7.753 28.01 2.172 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100. p 1,430.00 p 21.40 p 7842 I WHEAT 10/22/14 216.76 (W) 6.509 28.01 1.823 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100. p 1,430.00 p 21.40 p 7842 I WHEAT 10/23/14 241.60 (W) 7.255 28.01 2.032 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100. p 1,430.00 p 21.40 p 7842 I WHEAT 10/24/14 153.17 (W) 4.600 28.01 1.288 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100. p 1,430.00 p 21.40 p 7842 I WHEAT 10/27/14 21.99 (W) 0.660 28.01 0.185 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100, p 1,430.00 p 21.40 p 7842 WHEAT Oct-14 891.69 (W) 26.777 Total Gallons/Ac: Total Wet Tons/Ac: 26.78 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 0.045 0.030 0.810 0.195 0.075 0.006 0.075 0.315 0.075 2.670 181.51 118 Cumulative lbs/acre 0.045 0.030 1 0.810 0.195 1 0.075 0.006 0.075 0.315 0.075 2.670 z r ' 136 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 5J �_. UN s t FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: RAINS OWNER: STANALAND FARMS, INC PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 12.25 SITE #: NC BR 00104 FIELD# : BR 00104 0029 OPERATOR: PARKER STANALAND CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 3.00 ACRES PERMITTED: 3.00 Page Lune Applied *** Date�::F: Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) "�o Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 10/24/14 43.75 (W) 14.583 28.01 4.085 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100. p 1,430.00 p 21.40 pF 842 WHEAT Oct-14 43.75 (W) 14.583 Total Gallons/Ac: Total Wet Tons/Ac: 14.58 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 64 0.025 0.016 0.441 0.106 0.041 0.003 0.041 0.172 0.041 1.454 98.85 Cumulative lbs/acre 0.025 0.016 0.441 0.106 0.041 0.003 0.041 0.172 0.041 1.454 r Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop%° s t 106 y. ,. X1" ,* "'°'+ m n°' pX. FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 p( ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x � .Glll/1/ eZ 201 /f �- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percept p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BLANTON OWNER: FMJ HOLDINGS LLC PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 102.42 SITE #: NC BR 00105 FIELD# : BR 00105 0002 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 14.60 ACRES PERMITTED: 14.60 Page Lane Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 7/28/14 236.92 (W) 16.227 29.57 4.798 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 30,100. p 5,310.00 p 2.00 p 12005 I MILLET, PEARL 7/29/14 109.43 (W) 7.495 29.57 2.216 ADNG2&4. MOIST 0-<1/2" SURIN 1.0 0.27 30,100. p 5,310.00 p 2.00 p 12005 MILLET, PEARL Jul-14 346.35 (W) 1 23.722 1 Total Gallons/Ac: Total Wet Tons/Ac: 23.72 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 168 0.042 0.028 0.800 0.182 0.070 0.024 0.070 0.281 0.070 3.479 214.65 Cumulative lbs/acre 0.105 0.068 1 1.838 0.626 1 0.235 0.032 0.179 1 0.698 0.383 9.272 «r 208 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop d z: FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0' t r0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x C�V�7 zwll �024?01 / .i- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BLANTON OWNER: COXIMONROE PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 68.10 SITE #: NC BR 00113 FIELD# : BR 00113 0005 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 14.20 ACRES PERMITTED: 14.20 Page Lune Applied *** Date LbsAc allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/4/14 233.79 (W) 16.464 29.13 4.796 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p r121 SOYBEANS Jan-14 233.79 (W) 16.464 1 1 Total Gallons/Ac: Total Wet Tons/Ac: 16.46 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 87 0.029 0.029 0.384 0.288 0.048 0.004 0.058 0.163 0.048 1.688 122.78 Cumulative lbs/acre 0.168 0.111 1 2.711 1 1.319 1 0.384 0.031 0.362 1 0.972 0.291 8.633'°' Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 97 u y FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x &�p I/ (.( �O //.!5 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: CLIFF BRYANT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 126.17 SITE #: NC BR 00124 FIELD# : BR 00124 0002 OPERATOR: LEWIS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 22.30 ACRES PERMITTED: 22.30 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/2/14 174.72 (W) 7.835 34.47 2.701 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700, p 2,200.00 p 7.83 p 8823 SOYBEANS 513114 191.31 (W) 8.579 34.47 2.957 ADNG2&4. DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SOYBEANS May-14 1 366.03 (W) 16.414 Total Gallons/Ac: Total Wet Tons/Ac: 16.41 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.034 0.023 0.453 0.136 0.057 0.005 0.057 0.192 0.057 1.935 107.84 100 Cumulative Ibs/acre 0.233 0.140 3.548 1.831 0.461 0.046 0.455 1.331 0.621 14.389 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop " FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 ; "" " 1339.0 267.9 15.0 375.0 89.0 2500.0 , ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: CLIFF BRYANT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 37.25 SITE #: NC BR 00124 FIELD# : BR 00124 0003 OPERATOR: LEWIS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.40 ACRES PERMITTED: 7.40 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/1/14 42.64 (W) 5.762 34.47 1.986 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I SOYBEANS 5/2/14 65.42 (W) 8.841 34.47 3.047 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SOYBEANS May-14 1 108.06 (W) 14.603 1 Total Gallons/Ac: Total Wet Tons/Ac: 14.60 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 89 0.030 0.020 0.403 0.121 0.050 0.004 0.050 0.171 0.050 1.721 95.94 Cumulative Ibs/acre 0.203 0.083 1 2.250 0.990 1 0.300 1 0.029 0.300 1 0.878 0.370 10.398 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop .a 98 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ¢ ¢ : ,$ 1339.0 267.9 15.0 375.0 89.0 2500.0 _ ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 i ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: CLIFF BRYANT PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 15.31 SITE #: NC BR 00124 FIELD# : BR 00124 0004 OPERATOR: LEWIS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.30 ACRES PERMITTED: 2.30 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/1/14 44.42 (W) 19.313 34.47 6.657 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SOYBEANS May-14 44.42 (W) 19.313 1 Total Gallons/Ac: Total Wet Tons/Ac: 19.31 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 117 0.040 0.027 0.533 0.160 0.067 0.005 0.067 0.226 0.067 2.277 126.89 Cumulative lbs/acre 0.071 0.042 0.892 0.363 0.145 0.013 0.145 0.414 0.192 4.215F; Permit PAN Limit (lbs/acre) 1st Crop/2ndCrop . 1�t9IAW . L a # a "+ 4 :. ,- � 161Ce4;14i FD Cumulative Pollutant Loadin Limit g Rate (lbs/acre) 36.6 34:8 «> ° 1339.0 267.9 1* 15.0 375.0 89.0 2500 0' a ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 I X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." i N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: JAMES CLEMMONS PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 35.19 S,ITE #: NC BR 00150 FIELD# : BR 00150 0001 OPERATOR: JAMES CLEMMONS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.70 ACRES PERMITTED: 16.70 Page: 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 3/11/14 45,335.73 (G) 2714.714 14.84 1.680 ADNG3L DRY 0-<1/2" SURIN 1.0 0.40 72,100. p 2,630.00 p 88.90 p 30507 I BERMUDAGRASS, COASTAL 3/12/14 11,529.98 (G) 690.418 14.84 0.427 ADNG3L DRY 0-<1/2" SURIN 1.0 0.40 72,100. p 2,630.00 p 1 88.90 p 30507 BERMUDAGRASS, COASTAL Mar-14 56,865.71 (G) 3,405.132 Total Gallons/Ac: 3,405.13 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 129 0.013 0.008 0.030 0.038 0.021 0.002 0.021 0.021 0.021 0.051 35.36 Cumulative lbs/acre 0.215 0.080 3.483 1.647 0.353 0.022 0.346 1.346 0.283 14.026 °t Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 130 , J FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC OWNER: JAMES CLEMMONS SITE #: NC BR 00150 FIELD# : BR 00150 0002 A RESIDUAL SOURCE(S):* See list at bottom ofreport ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GOLDSBORO PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 13.55 OPERATOR: JAMES CLEMMONS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 7.00 ACRES PERMITTED: 7.00 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) , % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 3/11/14 5,760.19 (G) 822.884 14.84 0.509 ADNG31, DRY 0-<1/2" SURIN 1.0 0.40 72,100.p 2,630.00 p 88.90 p 30507 BERMUDAGRASS, COASTAL Mar-14 5,760.19 (G) 822.884 4/2/14 16,131.90 (G). 2304.557 14.84 1.426 ADNG3L MOIST 0-<1/2" SURIN 1.0 0.40 72,100.p 2,630.00 p 88.90 p 30117 BERMUDAGRASS, COASTAL Apr-14 16,131.90 (G) 2,304.557 1 1 Total Gallons/Ac: 3,127.44 Total Wet Tons/Ac: As Cd' Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 118 0.012 0.008 0.027 0.035 0.019 0.002 0.019 0.019 0.019 0.046 32.48 Cumulative lbs/acre 0.204 0.070 3.236 1.514 0.326 0.019 0.322 1.211 0.258 13.445 1 r am # ems, Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop00 Xmn FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 < 1339.0 267.9 15 0 t 1 375.0 89.0 2500.0 J r ra ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID X� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]snowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC pREDOMINANT SOIL SERIES: GOLDSBORO OWNER: JAMES CLEMMONS PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 36.43 SITE #: NC BR 00150 FIELD# : BR 00150 0002 B OPERATOR: JAMES CLEMMONS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 19.90 ACRES PERMITTED: 19.90 Page Lime Applied *** Date Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (VM (specify) ' ' % Solids Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pp m ) Crop p Total Per Acre 3/21/14 11,510.79 (G) 578.432 14.84 0.358 ADNG3L MOIST 0-<1/2" SURIN 1.0 0.40 72,100. p 2,630.00 p 88.90 p 730507 I BERMUDAGRASS, COASTAL 3/27/14 47,364.51 (G) 2380.126 '14.84 1.473 ADNG3L MOIST 0-<1/2" SURIN 1.0 0.40 72,100. p 2,630.00 p 88.90 p 30107 BERMUDAGRASS, COASTAL Mar-14 58,875.30 (G) 2,958.558 , 1 i orai vattons/Ac: i,9"." TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 0.011 0.007 0.026 0.033 0.018 0.001 0.018 0.018 0.018 0.044 30.72ON 112 Cumulative lbs/acre 0:200 0.072 3.272 1.720 0.330 0.019 0.326 1.219 0.246 13.450 Permit PAN Limit (Ibs/acre) 1 st Crop/2nd Crop , 's .* :; t, 112 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 �# ' ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: JAMES CLEMMONS PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 39.64 SITE #: NC BR 00151 FIELD# : BR 00151 0001 OPERATOR: JAMES CLEMMONS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.50 ACRES PERMITTED: 18.30 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) "�o Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 3/12/14 28,350.12 (G) 1718.189 14.84 1.063 ADNG3L DRY 0-<1/2" SURIN 1.0 0.40 72,100. p 2,630.00 p 88.90 p 30507 I BERMUDAGRASS, COASTAL 3/21/14 35,700.23 (G) 2163.650 14.84 1.339 ADNG3L MOIST 07<1/2" SURIN 1.0 0.40 72,100.p 2,630.00 p 88.90 p 31117 BERMUDAGRASS, COASTAL Mar-14 1 64,050.35 (G) 3,881.839 Total Gallons/Ac: 3,881.84 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.014 0.010 0.034 0.043 0.024 0.002 0.024 0.024 0.024 0.058 40.31 147 Cumulative lbs/acre 0.126 0.055 2.143 0.922 0.268 0.018 0.243 0.910 0.173 9.014 1 1 1 1 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop S FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 "'" 375.0 89.0 2500.0 ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: WOODROW HEWETT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 30.97 SITE #: NC BR 00156 FIELD# : BR 00156 0001 OPERATOR: FRANK HEWETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.30 ACRES PERMITTED: 6.30 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pprn) Crop MONTH Total Per Acre Solids 1/4/14 106.32 (W) 16.876 29.13 4.916 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100. p 2,090.00 p 8.24 p 9121 F SOYBEANS Jan-14 106.32 (W) 16.8761 1 - 1 Total Gallons/Ac: Total Wet Tons/Ac: 16.88 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 90 0.030 0.030 0.393 0.295 0.049 0.004 0.059 0.167 0.049 1.730 125.85 Cumulative lbs/acre 0.216 0.135 3.817 2.035 0.487 0.041 0.455 1,394 0.316 13.931 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop t � � x FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15 0 375.0 89.0 2500 0 < ADNG2&42:1 = ADM CORP., NC NIITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x o 20 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: WOODROW HEWETT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 37.08 SITE #: NC BR 00156 FIELD# : BR 00156 0002 OPERATOR: FRANK HEWETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.30 ACRES PERMITTED: 8.30 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip, cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/4/14 127.28 (W) 15.335 29.13 4.467 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 121 E SOYBEANS Jan-14 127.28 (W) 15.335 1 Total Gallons/Ac: Total Wet Tons/Ac: 15.33 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.027 0.027 0.357 0.268 0.045 0.004 0.054 0.152 0.045 1.572 114.36 81 Cumulative lbs/acre 0.207 1 0.143 1 3.834 2.061 1 0.509 0.046 0.470 1 1.383 0.337 13.835 T,,,'­,"' Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 98 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 .`a'*: ° R 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X ®� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: OBIE HANKINS PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 93.74 SITE #: NC BR 00157 FIELD# : BR 00157 0001 OPERATOR: CLEVE SIMMONS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 18.30 ACRES PERMITTED: 18.30 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppnl) Crop MONTH Total Per Acre Solids 1/10/14 170.94 (W) 9.341 29.13 2.721 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100. p 2,090.00 p 8.24 p 9121 I SOYBEANS 1/13/14 150.85 (W) 8.243 29.13 2.401 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 SOYBEANS Jan-14 1 321.79 (W) 1 17.584 Total Gallons/Ac: Total Wet Tons/Ac: 17.58 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 93 0.031 0.031 0.410 0.307 0.051 0.004 0.061 0.174 0.051 1.803 131.13 Cumulative Ibs/acre 0.209 0.081 2.012 0.958 0.281 0.023 0.235 0.729 0.260 7.789 Permit PAN Limit (lbs/acre) I st Crop/2nd Crop >e' * '' s 98 Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 33.0 267. 375.0 89.0FD 25000', ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X dzo� O.Z.1.2alS— (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: OBIE HANKINS PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 88.56 SITE #: NC BR 00157 FIELD# : BR 00157 0002 OPERATOR: CLEVE SIMMONS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 18.70 ACRES PERMITTED: 18.70 Page Lane Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) , % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 1/7/14 99.39 (W) 5.315 29.13 1.548 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 I SOYBEANS 1/8/14 204.62 (W) 10.942 29.13 3.187 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 1121 SOYBEANS Jan-14 1 304.01 (W) 16.257 Total Gallons/Ac: Total Wet Tons/Ac: 16.26 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 86 0.028 0.028 0.379 0.284 0.047 0.004 0.057 0.161 0.047 1.667 121.23 Cumulative lbs/acre 0.104 0.062 1.326 0.679 0.162 0.013 0.154 0.450 0.265 4.522 Permit PAN Limit (lbs/acre) '1st Crop/2nd Crop t * ( 98 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 z ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 *Ze� 1 oe/v/,s- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: -Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN- hicorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: ROBERT MCDOWELL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 73.71 SITE #: NC BR 00173 FIELD# : BR 00173 0001 OPERATOR: ROBERT MCDOWELL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 19.30 ACRES PERMITTED: 19.30 Page: 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 8/18/14 192.78 (W) 9.989 15.81 1.579 ADNG2C MOIST 0-<I/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 I BERMUDAGRASS, COASTAL 8/19/14 125.36 (W) 6.495 15.81 1.027 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL 8/20/14 128.31 (W) 6.648 15.81 1.051 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL 8/21/14 19.79 (W) 1.025 '15.81 0.162 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200.p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL Aug-14 466.24 (W) 24.157 Total Gallons/Ac: Total Wet Tons/Ac: 24.16 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 190 0.023 0.015 0.833 0.191 0.038 0.003 0.038 0.290 0.038 3.010 240.62 Cumulative Ibs/acre 0.178 0.089 2.662 1.166 0.358 0.027 0,358 1.157 0.455 10.031 . fi A k s"2: 7•:' ... Permit PAN Limit (Ibs/acre) 1stCrop/2ndCrop a r"'•" -' 240 *- Lx. a, r FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 = „+ ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE x12'rY/ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NOR -FOLK OWNER: DEAN HEWETT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 44.48 SITE #: NC BR 00190 FIELD# : BR 00190 0004 OPERATOR: DEAN HEWETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4.50 ACRES PERMITTED: 4.50 Page : 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (VM (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp-) Crop MONTH Total Per Acre Solids 4/1/14 66.14 (W) 14.698 28,93 4.252 ADNG2&4: MOIST 0 Q/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 MILLET .4/2/14 21.51 (W) 4.780 28.93 1.383 ADNG2&4: MOIST 0-<I/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 MILLET 4/3/14 45.12 (W) 10.027 28.93 2.901 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 MILLET Apr-14 132.77 (W) 29.505 9/29/14 22.51 (W) 5.002 126.98 1.350 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11012 WHEAT Sep-14 22.51 (W) 5.002 ' Total Gallons/Ac: Total Wet Tons/Ac: 34.51 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 158 0.059 0.040 0.771 0.206 0.099 0.009 0.099 0.313 0.099 2.983 197.35 30 Cumulative lbs/acre 0.189 0.105 2.221 0.972 0.375 0.029 0.375 0.875 0.329 9.666 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop a 7 " 206 j tL ° 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ` - �,� ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X Agx/,W� ©2/2O/l., (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Lmcorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: DEAN HEWETT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 17.62 SITE #: NC BR 00190 FIELD# : BR 00190 0005 OPERATOR: DEAN HEWETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4.30 ACRES PERMITTED: 4.30 Page Lane Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 9/23/14 65.31 (W) 15.188 26.98 4.098 ADNG2&4: MOIST 0-<I/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11052 RYE (FOR GRAIN) Sep-14 65.31 (W) 15.188 Total Gallons/Ac: Total Wet Tons/Ac: 15.19 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.025 0.016 0.475 0.107 0.041 0.006 0.041 0.172 0.041 1.697 111.46 91 Cumulative lbs/acre 0.207 0.113 2.525 1.142 0.434 0.035 0.434 0.982 0.358 12.100 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ` - ' fM 123 w .r FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: -Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: DEAN HEWETT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 110.38 SITE #: NC BR 00190 FIELD# : BR 00190 0006 OPERATOR: DEAN HEWETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.80 ACRES PERMITTED: 11.80 Page Lane Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 3/27/14 134.04 (W) 11.359 27.43 3.116 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 I MILLET, PEARL 3/28/14 133.32 (W) 11.298 27.43 3.099 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 MILLET, PEARL Mar-14 267.36 (W) 22.657 4/1/14 66.99 (W) 5.677 28.93 1.642 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 MILLET, PEARL Apr-14 66.99 (W) 5.677 9/23/14 43.11 (W) 3.653 26.98 0.986 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11052 I RYE (FOR GRAIN) 9/29/14 22.34 (W) 1.893 '26.98 0.511 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11052 1 RYE (FOR GRAIN) Sep-14 65.45 (W) 5.546 Total Gallons/Ac: Total Wet Tons/Ac: 33.88 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.056 0.037 0.888 0.196 0.094 0.008 0.094 0.361 0.094 2.963 228.23 170 33 Cumulative lbs/acre 0.192 0.097 2.374 0.984 0.364 0.030 0.364 0.929 0.350 10.495 �'»-.tr•,,..,�:; Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop t " 206 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0V 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x * W/JJWt_ I - (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NOR -FOLK OWNER: DEAN HEWETT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 17.23 SITE #: NC BR 00190 FIELD# : BR 00190 0007 OPERATOR: DEAN HEWETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 3.80 ACRES PERMITTED: 3.80 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip: cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pptn) Crop MONTH Total Per Acre Solids 9/23/14 63.85 (W) 16.803 26.98 4.533 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11052 JRYE(FORGRAIN) Sep-14 63.85 (W) 16.803 Total Gallons/Ac: Total Wet Tons/Ac: 16.80 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 0.027 0.018 0.526 0.118 0.045 0.006 0.045 0.190 0.045 1.877 123.31 100 Cumulative Ibs/acre 0.168 0.089 1.986 0.850 0.326 0.030 0.326 0.800 0.363 9.903 7" Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop .4 123 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 * y 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under lily direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hmjection/Ineorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: DEAN HEWETT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 30.95 SITE #: NC BR 00190 FIELD# : BR 00190 0013 OPERATOR: DEAN HEWETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list,at bottom of report ACRES UTILIZED: 3.40 ACRES PERMITTED: 3.40 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Are Solids 4/1/14 88.51 (W)P2g,93 7.531 ADNG2&4: MOIST 0-<1!2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 MILLET Apr-14 88.51 (W)9/29/14 19.82 (W)26.98 1.573 ADNG2&4: MOIST 0-<I/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11052 RYE (FOR GRAIN) Sep-14 19.82 (W) Total Gallons/Ac: Total Wet Tons/Ac: 31.86 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 139 0.055' 0.036 0.725 0.192 0.091 0.008 0.091 0.292 0.091 2.790 184.52 35 Cumulative lbs/acre 0.117 0.073 1.317 0.503 0.224 0.019 0.224 0.535 0.156 6.198 °'• <w m ;' Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop s . t tr ° " 206 z 50 x FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 q'a 375.0 89.0 2500.0 x ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIXRATIO OF NG2 TO NG4 x o Z/Z0(' (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: DEAN HEWETT PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 24.56 SITE #: NC BR 00190 FIELD# : BR 00190 0014 OPERATOR: DEAN HEWETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.60 ACRES PERMITTED: 2.60 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons ()AT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp-) Crop MONTH Total Per Acre Solids 4/2/14 66.69 (W)F7.500J26.J777r7NG2&4: 650 28.93 7.421 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 66.69 M650 9/29/14 19.50 (W) MOIST 0-<1/2" SURIN 1.0 0.27 28,800. p 4480.00 p 5.93 p 11052 RYE (FOR GRAIN) Sep-14 19.50 (W)500 Total Gallons/Ac: Total Wet Tons/Ac: 33.15 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.057 0.038 0.769 0.201 0.094 0.009 0.094 0.308 0.094 2.945 194.69 137 45 Cumulative lbs/acre 0.115 0.070 1.313 0.494 0.221 0.019 0.221 0.529 0.149 6.059 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 161 . 50 (lbs/acre) FD Cumulative Pollutant LoadingRate Limit lbs/acre 36.6 34.8 1339.0 267.9 15.0 b 375.0 89.0 2500.0 ,ryp' ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 i ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: DEAN HEWETT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 24.66 SITE #: NC BR 00190 FIELD# : BR 00190 0015 OPERATOR: DEAN HEWETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.60 ACRES PERMITTED: 2.60 Page Lane Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) , Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) ' % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/1/14 66.71 (W) 25.658 28.93 7.423 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 MILLET Apr-14 66.71 (W) 25.658 9/29/14 19.85 (W) 7.635 !26.98 2.060 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11052 RYE (FOR GRAIN) Sep-14 19.85 (W) 7.635., 1 Total Gallons/Ac: Total Wet Tons/Ac: 33.29 As Cd. Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 137 0.057 .0.038 0.773 0.202 0.095 0.009 0.095 0.309 0.095 2.961 195.72 46 Cumulative lbs/acre 0.115 0.070 1.315 0.493 0.221 0.019 0.221 0.530 0.149 6.062 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop A 4 „ ,:. t . » I IR a ".� 206 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 r 1339.0 267.9 15.0 g,gW,q 375.0 89.0 2500 0 , r' ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or,Not Required % = percent • p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: DEAN HEWETT PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 40.51 SITE #: NC BR 00190 FIELD# : BR 00190 0016 OPERATOR: DEAN HEWETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.20 ACRES PERMITTED: 8.20 Page : 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 9/29/14 150.14 (W) 18.310 26,98 4.940 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 87, 4,480.00 p 5.93 p 11052 RYE (FOR GRAIL Sep-14 150.14 (W) 18.310 1 Total Gallons/Ac: Total Wet Tons/Ac: 18.31 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.030 0.020 0.573 0.128 0.049 0.007 0.049 0.207 0.049 2.045 134.37 109 . Cumulative lbs/acre 0.069 0.046 0.901 0.260 0.115 0.012 0.115 0.352 0.115 4.105 ,. •. r": " 123 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop " . B FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15 0 375.0 89.0 2500.0 1 j s. 'W �.. ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 - * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: FORESTON OWNER: WILLIE POKE PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 80.33 SITE #: NC BR 00239 FIELD# : BR 00239 0001 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.80 ACRES PERMITTED: 11.80 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pprn) Crop MONTH Total Per Acre Solids 1/6/14 212.35 (W) 17.996 29.13 5.242 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 SOYBEANS 1/7/14 63.41 (W) 5.374 29.13 1.565 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 SOYBEANS Jan-14 1 275.76 (W) 23.370 Total Gallons/Ac: Total Wet Tons/Ac: 23.37 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 124 0.041 0.041 0.545 0.408 0.068 0.005 0.082 0.231 0.068 2.396 174.27 Cumulative lbs/acre` 0.287 0.142 2.705 1.689 0.457 0.039 0.450 1.075 0.319 -77777-7-7 12.508 a.iw X A ,,. Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop g 156 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8p'-. 1339.0 267.9 15.0 375.0 89.0 2500.0 " . r- ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X Z0��/%-5--- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: WAYNE BENTON PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 24.36 SITE #: NC BR 00242 FIELD# : BR 00242 0001 OPERATOR: MALCOLM GRISSETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.50 ACRES PERMITTED: 6.50 Page Lane Applied *** Date Lbs� allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 10/27/14 86.97 (W) 13.380 28.01 3.748 ADNG2&4. DRY 0-<1/2" SURIN 1.0 0.21 25,100. p 1,430.00 p 21.40 p 7842 WHEAT Oct-14 1 86.97 (W) 13.380 Total Gallons/Ac: Total Wet Tons/Ac: 13.38 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual ibs/acre 59 0.022 0.015 0.405 0.097 0.037 0.003 0.037 0.157 0.037 1.334 90.70 Cumulative Ibs/acre 0.081 0.044 1.405 0.428 0.145 0.012 0.153 0.576 0.123 6.936 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop 80 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hmcorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: WAYNE BENTON PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 42.50 SITE #: NC BR 00242 FIELD# : BR 00242 0002 OPERATOR: MALCOLM GRISSETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.50 ACRES PERMITTED: 11.50 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TICN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 10/27/14 151.72 (W) 13.193 28.01 3.695 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 47 WHEAT Oct-14 1 151.72 (W) 13.193 1 Total Gallons/Ac: Total Wet Tons/Ac: 13.19 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 58 0.022 0.015 0.399 0.096 0.037 0.003 0.037 0.155 0.037 1.316 89.43 Cumulative lbs/acre 0.091 0.054 1.401 0.491 0.152 0.012 0.152 0.596 0.146 6.837 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 68 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 L L 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x Aw__C� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." NIA =Not Applicable NR =Not Reported or Not Required % =percent p =ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: BRADSHER PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 126.00 SITE #: NC BR 00243 FIELD# : BR 00243 0001 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.10 ACRES PERMITTED: 16.10 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppin) Crop MONTH Total Per Acre Solids 12/15/14 132.59 (W) 8.235 27.41 2.257 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 I CORN 12/17/14 154.96 (W) 9.625 27.41 2.638 ADNG2&4. DRY 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 I CORN 12/18/14 172.15 (W) 10.693 27.41 2.931 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 1171 CORN Dec-14 459.70 (W) 28.553 Total Gallons/Ac: Total Wet Tons/Ac: 28.55 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.047 0.031 0.798 0.141 0.078 0.006 0.078 0.329 0.078 1.831 110.66 139 Cumulative lbs/acre 0.095 0.063 1.212 0.316 0.158 0.013 0.158 0.536 0.158 4.507 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 148 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X49 YZ©2l2als- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: BRADSHER PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 94.66 SITE #: NC BR 00243 FIELD# : BR 00243 0002 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 17.00 ACRES PERMITTED: 17.00 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 12/22/14 130.89 (W) 7.699 27.41 2.110 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 I CORN 12/23/14 171.75 (W) 10.103 27.41 2.769 ADNG2&4. MOIST 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 I CORN 12/29/14 42.72 (W) 2.513 27.41 0.689 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 CORN Dec-14 1 345.36 (W) 20.315 Total Gallons/Ac: Total Wet Tons/Ac: 20.32 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.033 0.022 0.568 0.100 0.056 0.004 0.056 0.234 0.056 1.303 78.74 99 Cumulative lbs/acre 0.090 0.060 0.973 0.300 0.151 0.012 0.151 0.419 0.345 3.813 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop 148 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ` ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x d 0 . S' (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: BRADSHER PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 48.49 SITE #: NC BR 00243 FIELD# : BR 00243 0003 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 10.70 ACRES PERMITTED: 10.70 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- a1i- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pptn) Crop MONTH Total Per Acre Solids 12/18/14 65.92 (W) 6.161 27.41 1.689 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 I CORN 12/19/14 111.00 (W) 10.374 27.41 2.843 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8111 1 CORN Dec-14 1 176.92 (W) 16.535 Total Gallons/Ac: Total Wet Tons/Ac: 16.53 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.027 0.018 0.462 0.082 0.045 0.004 0.045 0.190 0.045 1.061 64.08 80 Cumulative lbs/acre 0.080 0.053 0.744 0.258 0.133 0.011 0.133 - 0.296 0.521 2.664 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 148 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X oz12©Z,- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: GREER PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 42.98 SITE #: NC BR 00274 FIELD# : BR 00274 0001 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.00 ACRES PERMITTED: 8.00 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp-) Crop MONTH Total Per Acre Solids 10/1/14 153.43 (W) 19.179 28,01 5.372 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 25,100. p 1,430.00 p 21.40 p 7842 WHEAT Oct-14 153.43 (W) 19.179 Total Gallons/Ac: Total Wet Tons/Ac: 19.18 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.032 0.021 0.580 0.140 0.054 0.004 0.054 0226 0.054 1.912 130.00 84 Cumulative lbs/acre 0.158 1 0.097 1 2.568 1 0.744 1 0.305 0.035 0.305 1 1.006 0.381 8,683 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop °" 136 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 L 1339.0 267.9 15.0 375.0 89.0 2500.0 ry ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X 02r (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: GREER PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 42.23 SITE #: NC BR 00274 FIELD# : BR 00274 0003 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.90 ACRES PERMITTED: 8.90 Page Lime Applied *** Date Lbs�Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho . Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH ' Total Per Acre Solids 9/29/14 1997 (W) 2.244 26.98 0.605 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 28,800. p 4,480.00' p 5.93 p 11052 WHEAT Sep-14 19.97 (W) 2.244 10/1/14 131.53 (W) 14.779 28.01 4.139 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 25,100. p 1,430.00 p 21.40 p 7842 WHEAT Oct-14 131.53 (W) 14.779 1 1 Total Gallons/Ac: Total Wet Tons/Ac: 17.02 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.028 0.019 0.517 0.123 0.047 0.004 0.047 0.199 0.047 1.724 116.64 78 Cumulative lbs/acre 0.161 0.098 2.613 0.756 0.311 0.036 0.311 1.020 0.389 8.829 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 136 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 0_21- x * X/,/, Zol /,!;-- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: ALAN ROBINSON PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 20.66 SITE #: NC BR 00285 FIELD# : BR 00285 0005 OPERATOR: ALAN ROBINSON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 10.60 ACRES PERMITTED: 10.60 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/29/14 33,390.88 (G) 3150.083 14.84 1.949 ADNG3L DRY 0-<I/2" SURIN 1.0 0.40 72,100.p 2,630.00 p 88.90 p 30507 BERMUDAGRASS Apr-14 33,390.88 (G) 3,150.083 Total Gallons/Ac: 3,150.08 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.012 0.008 0.027 0.035 0.019 0.002 0.019 0.019 0.019 0.047 32.71 119 Cumulative lbs/acre 0.067 1 0.026 1 1.111 1 0.603 1 0.112 0.009 0.112 1 0.459 0.083 5.831 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ,. ., 40 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: ALAN ROBINSON PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 77.90 SITE #: NC BR 00285 FIELD# : BR 00285 0006 OPERATOR: ALAN ROBINSON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 30.90 ACRES PERMITTED: 30.90 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/7/14 45,501.20 (G) 1472.531 14.43 0.886 ADNG31, DRY 0-<I/2" SUR 0.5 0.40 74,200. p 2,490.00 p 4.85 p 29934 I BERMUDAGRASS 5/10/14 23,465.22 (G) 759.392 14A3 0.457 ADNG31, DRY 0-<1/2" SUR 0.5 0.40 74,200. p 2,490.00 p 4.85 p 29934 Ij BERMUDAGRASS 5114114 60,486.80 (G) 1957.502 14.43 1.178 ADNG31, DRY 0-<1/2" SUR 0.5 0.40 74,200. p 2,490.00 p 4.85 p 29934 BERMUDAGRASS May-14 129,453.22 (G) 1 4,189.425 1 Total Gallons/Ac: 4,189.42 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.015 0.010 0.025 0.025 0.025 0.002 0.025 0.025 0.025 0.045 43.11 151 Cumulative Ibs/acre 0.110 0.053 2.398 0.828 0.183 0.015 0.183 0.904 0.152 9.347 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 1 `,Fl * 240 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 4 1339.0 267.9 15.0 375.0 89.0 2500.0 r ° ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: LEON OWNER: ALAN ROBINSON PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 19.93 SITE #: NC BR 00285 FIELD# : BR 00285 0007 OPERATOR: ALAN ROBINSON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.60 ACRES PERMITTED: 9.60 Page Lime Applied *** Date Lbs/Ac DATE or ailons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/10/14 10,345.33 (G) 1077.639 14A3 0.648 ADNG31, DRY 0-<I/2" SUR 0.5 0.40 74,200. p 2,490.00 p 4.85 p 29934 I BERMUDAGRASS 5/14/14 22,767.39 (G) 2371.603 14.43 1.427 ADNG31, DRY 0-<1/2" SUR 0.5 0.40 74,200. p 2,490.00 p 4.85 p 29934 BERMUDAGRASS May-14 1 33,112.72 (G) 1 3,449.242 1 Total Gallons/Ac: 3,449.24 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 124 0.012 0.008 0.021 0.021 0.021 0.002 0.021 0.021 0.021 0.037 35.49 Cumulative lbs/acre`"�"�'" 0.046 0.026 1.008 0.222 0.077 0.006 0.077 0.374 0.073 3.383 a Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop w 132 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID x V_x, 140� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: BURNEY PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 36.91 SITE #: NC BR 00287 FIELD# : BR 00287 0001 OPERATOR: CLEVE SIMMONS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.00 ACRES PERMITTED: 9.00 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and m (pp ) Crop p MONTH Total Per Acre Solids 4/23/14 127.57 (W) 14.174 28.93 4.101 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1 1,940.00 p 1 2.77 p 9249 F SOYBEANS Apr-14 127.57 (W) 14.1741 1 1 1 1 1 1 1 1 Total Gallons/Ac: Total Wet Tons/Ac: 14.17 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.025 0.016 0.295 0.082 0.041 0.003 0.041 0.123 0.041 1.165 77.17 76 Cumulative lbs/acre 0.193 1 0.085 1 1.732 1 0.948 1 0.283 0.031 0.271 1 0.678 0.477 8.072 F L Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 98 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 Xi�L I (SIGNATURE OF, LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and . evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hnjection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM ' Page : 1 FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE Lime Applied *** OWNER: BURNEY PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 30.49 Date Lbs/Ac SITE #: NC BR 00287 FIELD# : BR 00287 0002 OPERATOR: CLEVE SIMMONS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.20 ACRES PERMITTED: 7.20 DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 4/22/14 19.29 (W) 2.679 28.93 0.775 ADNG2&4' MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 I SOYBEANS 4/23/14 86.11 (W) 11.960 28.93 3.460 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 1 105.40 (W) 14.639 1 Total Gallons/Ac: Total Wet Tons/Ac: 14.64 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 78 0.025 0.017 0.305 0.085 0.042 0.003 0.042 0.127 0.042 1.203 79.70 Cumulative lbs/acre 0.025 0.017 0.305 0.085 1 0.042 0.003 0.042 1 0.127 0.042 1.203 '; # 1 Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 .k 1339.0 267.9 15.0 375.0 89.0 2500.0 " , ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: JONES PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 47.21 SITE #: NC BR 00292 FIELD# : BR 00292 0001 OPERATOR: SANDY MANSFIELD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.60 ACRES PERMITTED: 13.60 Page : I Lane Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 8/12/14 43.45 (W) 3.195 15.81 0.505 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 724934 BERMUDAGRASS, COASTAL 8/13/14 127.24 (W) 9.356 15.81 1.479 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL 8/14/14 127.94 (W) 9.407 15.81 1.487 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL Aug-14 298.63 (W) 21.958 Total Gallons/Ac: Total Wet Tons/Ac: 21.96 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 173 0.021 0.014 0.757 0.174 0.035 0.003 0.035 0.264 0.035 2.736 218.71 Cumulative lbs/acre 0.104 0.054 2.113 0.710 0.157 0.013 0.157 0.847 0.131 9.169 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 293 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE x (SIGNATURE OF OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: JONES PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 67.20 SITE #: NC BR 00292 FIELD# : BR 00292 0002 OPERATOR: SANDY MANSFIELD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 19.90 ACRES PERMITTED: 19.90 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 9/16/14 259.47 (W) 13.039 17.34 2.261 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p 21684 BERMUDAGRASS, COASTAL 9/17/14 128.07 (W) 6.436 17.34 1.116 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p 21684 BERMUDAGRASS, COASTAL Sep-14 1 387.54 (W) 19.475 Total Gallons/Ac: Total Wet Tons/Ac: 19.47 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.020 0.014 0.621 0.176 0.034 0.003 0.034 0.257 0.034 2.756 180.32 146 Cumulative lbs/acre 0.069 0.038 1.279 0.456 0.095 0.008 0.095 0.573 0.095 6.265 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 293 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: JONES PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 84.22 SITE #: NC BR 00292 FIELD# : BR 00292 0003 OPERATOR: SANDY MANSFIELD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 27.20 ACRES PERMITTED: 27.20 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (VM (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppin) Crop MONTH Total Per Acre Solids 8/7/14 191.59 (W) 7.044 15.81 1.114 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 724934 BERMUDAGRASS, COASTAL 8/8/14 129.03 (W) 4.744 15.81 0.750 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL 8/9/14 84.24 (W) 3.097 15.81 0.490 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL 8/12/14 127.85 (W) 4.700 15.81 0.743 ADNG2C DRY 0-<1/2" SUR 0.5 0.40 61,200. p 4,360.00 p 17.70 p 24934 BERMUDAGRASS, COASTAL Aug-14 532.71 (W) 19.585 Total Gallons/Ac: Total Wet Tons/Ac: 19.58 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 154 0.019 0.012 0.675 0.155 0.031 0.002 0.031 0.235 0.031 2.440 195.07 Cumulative lbs/acre 0.075 0.040 1.431 0.477 0.101 0.008 0.101 0.599 0.101 6.470 Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop``, 293 $ fi" FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 L 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: JONES PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 41.38 SITE #: NC BR 00292 FIELD# : BR 00292 0004 OPERATOR: SANDY MANSFIELD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 9/15/14 22.03 (W) 2.225 17.34 0.386 ADNG2C MOIST 0-<I/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p 21684 .I BERMUDAGRASS, COASTAL 9/16/14 43.12 (W) 4.356 17.34 0.755 ADNG2C MOIST 0-<I/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p 21684 I BERMUDAGRASS, COASTAL 9/17/14 21.13 (W) 2.134 17.34 0.370 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p 21684 I BERMUDAGRASS, COASTAL 9/18/14 65.10 (W). 6.576 17.34 1.140 ADNG2C MOIST 0-<1/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p 21684 I BERMUDAGRASS, COASTAL 9/19/14 87.23 (W) 8.811 17.34 1.528 ADNG2C - MOIST 0-<1/2" SUR 0.5 0.40 51,800. p 2,600.00 p 704.00 p 21684 BERMUDAGRASS, COASTAL Sep-14 1 238.61 (W) 1 24.102 Total Gallons/Ac: Total Wet Tons/Ac: 24.10 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 181 0.025 0.017 0.769 0.217 0.042 0.003 0.042 0.318 0.042 3.410 223.17 Cumulative lbs/acre 0.076 0.042 1.452 0.508 0.105 0.008 0.105 0.647 0.105 7.054 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop 293 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2C = ADM CORP., NC NITRO GRO 2 CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: FREDDY HEWETT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 24.80 SITE #: NC BR 00298 FIELD# : BR 00298 0002 OPERATOR: CLEVE SIMMONS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5.70 ACRES PERMITTED: 5.70 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/23/14 85.72 (W) 15.039 28.93 4.351 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 1 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 1 85.72 (W) 15.039 1 Total Gallons/Ac: Total Wet Tons/Ac: 15.04 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 80 0.026 0.017 0.313 0.087 0.044 0.003 0.044 0.131 0.044 1.236 81.88 Cumulative Ibs/acre 0.126 1 0.029 1 0.746 1 0.124 1 0.200 0.009 0.099 1 0.329 0.232 2.785 ✓ Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 98 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 - 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: FREDDY HEWETT PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 24.32 SITE #: NC BR 00298 FIELD# : BR 00298 0004 OPERATOR: CLEVE SIMMONS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 3.70 ACRES PERMITTED: 3.70 Page Litne Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (VM (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PALL (ppm) Crop MONTH Total Per Acre Solids 4/23/14 62.98 (W) 17.022 28.93 4.924 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 I SOYBEANS 4/24/14 21.08 (W) 5.697 28.93 1.648 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 1 84.06 (W) 22.719 1 Total Gallons/Ac: Total Wet Tons/Ac: 22.72 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 122 0.039 0.026 0.473 0.131 0.066 0.005 0.066 0.197 0.066 1.867 123.70 Cumulative Ibs/acre 0.285 0.051 1.456 0.156 0.459 0.018 0.189 0.664 0.533 5.061 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop {` 176 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 g IAZZ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: FREDDY HEWETT PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 42.72 SITE #: NC BR 00298 FIELD# : BR 00298 0005 OPERATOR: CLEVE SIMMONS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.70 ACRES PERMITTED: 9.70 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/22/14 147.68 (W) 15.225 28.93 4.405 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 1 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 147.68 (W) 15.225 1 Total Gallons/Ac: Total Wet Tons/Ac: 15.22 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 81 0.026 0.018 0.317 0.088 0.044 0.004 0.044 0.132 0.044 1.251 82.89 Cumulative lbs/acre 0.026 1 0.018 1 0.317 1 0.088 1 0.044 0.004 0.044 1 0.132 0.044 1.251 - Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 98 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: SPARROW PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 74.90 SITE #: NC BR 00306 FIELD# : BR 00306 0001 OPERATOR: CLIFF BRYANT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/3/14 67.24 (W) 8.511 34.47 2.934 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I SOYBEANS 515114 150.05 (W) 18.994 34.47 6.547 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p F8823 SOYBEANS May-14 217.29 (W) 27.505 I Total Gallons/Ac: Total Wet Tons/Ac: 27.51 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 167 0.057 0.038 0.758 0.228 0.095 0.008 0.095 0.322 0.095 3,243 180.71 Cumulative lbs/acre 0.156 0.078 1.830 0.783 0.293 0.025 0.293 0.718 0.372 10.116 Permit PAN Limit (lbs/acre) 1st Cr6p/2nd Crop ' ' " ` ' � 176 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X6 14 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: FORESTON OWNER: LANCASTER PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 61.32 SITE #: NC BR 00308 FIELD# : BR 00308 0001 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 790 ACRES PERMITTED: 7.90 Page Lane Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/6/14 210.49 (W) 26.644 29.13 7.761 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 SOYBEANS Jan-14 210.49 (W) 26.644 Total Gallons/Ac: Total Wet Tons/Ac: 26.64 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.047 0.047 0.621 0.466 0.078 0.006 0.093 0.264 0.078 2.732 198.69 142 Cumulative lbs/acre 0.190 0.131 2.672 1.114 0.373 0.037 0.388 0.977 0.275 10.603 F77,�41 .a 1 1 1 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 } 1339.0 267.9 15.0 '; 375.0 89.0 2500.0 ADNG2&42:1= ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN - hicorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: FORESTON OWNER: LANCASTER PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 6.65 SITE #: NC BR 00308 FIELD# : BR 00308 0002 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 1.10 ACRES PERMITTED: 1.10 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/6/14 22.82 (W) 20.745 29.13 6.043 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p F 9121 SOYBEANS Jan-14 1 22.82 (W) 20.745 1 1 Total Gallons/Ac: Total Wet Tons/Ac: 20.75 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 110 0.036 0.036 0.483 0.363 0.060 0.005 0.073 0.205 0.060 2.127 154.70 Cumulative lbs/acre 0.145 0.101 2.098 0.845 0.280 0.029 0.292 0.766 0.213 7.989 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 156 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false infornation, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: LYNCHBURG OWNER: HANKINS/WILLIAMS PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 130.53 SITE #: NC BR 00309 FIELD# : BR 00309 0001 OPERATOR: FRANK HEWffT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.80 ACRES PERMITTED: 13.80 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) "�o Tons Cond. Precip. cation till- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 3/5/14 131.17 (W) 9.505 32.44 3.083 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 22,700.p 2,070.00 p 4.93 p 7645 SOYBEANS Mar-14 131.17 (W) 9.505 4/12/14 87.40 (W) 6.333 28.93 1.832 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 I SOYBEANS 4/14/14 216.72 (W) 15.704 28.93 4.543 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 304.12 (W) 22.037 Total Gallons/Ac: Total Wet Tons/Ac: 31.54 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.057 0.038 0.669 0.189 0.095 0.008 0.095 0.278 0.095 2.508 185.36 165 Cumulative lbs/acre 0.163 1 0.095 1 2.451 1 0.823 1 0.339 0.029 0.339 1 0.972 0.367 10.086 r I Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 178 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: HICKMAN PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 17.01 SITE #: NC BR 00310 FIELD# : BR 00310 0001 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.80 ACRES PERMITTED: 13.80 Page : 1 Lime Applied *** Date Lbs/Ac or DATE% MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppin) Crop Total Per Acre 4/14/14 16,290.16 (G) 1180.446 14.84 0.730 ADNG3L MOIST 0-<1/2" SUR 0.5 0.40 72,100. p 2,630.00 p 88.90 p 729192 I SOYBEANS 4/17/14 11,203.84 (G) 811.872 14.84 0.502 ADNG3L MOIST 0-<1/2" SUR 0.5 0.40 72,100. p 2,630.00 p 88.90 p 29112 SOYBEANS Apr-14 27,494.00 (G) 1,992.318 1 1 otal Uauons/Ac: 1,9'12.32 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 72 0.007 0.005 0.017 0.022 0.012 <.001 0.012 0.012 0.012 0.030 20.69 Cumulative lbs/acre 0.108 0.063 1.478 0.514 0.223 0.024 0.223 0.570 0.242 5.8215,1 'v 1 ' ` F i* °" * i; 98 Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop ; " FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG31, = ADM CORP., NC NITRO GRO 3 LIQUID - (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records.Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: HICKMAN PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 21.14 SITE #: NC BR 00310 FIELD# : BR 00310 0002 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.50 ACRES PERMITTED: 13.50 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 4/16/14 22,700.24 (G) 1681.499 14.84 1.041 ADNG3L MOIST 0-<1/2" SUR 0.5 0.40 72,100.1) 2,630.00 p 88.90 p 29192 I SOYBEANS 4/17/14 11,455.63 (G) . 848.565 14.84 0.525 ADNG3L MOIST 0-<1/2" SUR 0.5 •0.40 72,100. p 2,630.00 p 88.90 p 29192 SOYBEANS Apr-14 34,155.87 (G) 2,530.064 1 Total Ciallons/Ac: 2,530.06 Total Wet Tons/Ac: " As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 91 0.009 0.006 0.022 0.028 0.016 0.001 0.016 0.016 0.016 0.038 26.27 Cumulative lbs/acre 0.111 0.065 1.509 0.523 0.227 0.025 0.227 0.583 0.248 5.857 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15 0_ 375.0 89.0 2500.0" ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID X (SIGNATURE OF LAND APPLIER) DATE •C� / / "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 Application Method:" SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: BRYANT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 35.63 SITE #: NC BR 00311 FIELD# : BR 00311 0001 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.40 ACRES PERMITTED: 7.40 Page : 1 Line Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Total Per Acre Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp m) Crop MONTH 9/22/14 132.06 (W) 17.846 i, 26.98 4.815 ADNG2&4: MOIST 0- 1/2" SUR 0.5 0.27 28,800. p 4,480.00 p 5.93 p 8812 WHEAT Sep-14 132.06 (V� 17.846 Dotal Gallons/Ac: Total Wet Tons/Ac: 17.85 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 85 0.029 0.019 0.559 0.125 0.048 0.007 0.048 0.202 0.048 1.993 130.96 Cumulative lbs/acre 0.123 0.080 1.675 0.642 0.275 0.037 0.275 0.635 0.191 7.681 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop" 136 v" olk FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x )*11eD 2 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, 114J - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: GORE PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 26.06 SITE #: NC BR 00314 FIELD# : BR 00314 0001 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.80 ACRES PERMITTED: 6.80 Page : I Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/12/14 90.08 (W) 13.247 28.93 3.832 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 90.08 (W) 13.247 1 Total Gallons/Ac: Total Wet Tons/Ac: 13.25 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 71 0.023 0.015 0.276 0.077 0.038 0.003 0.038 0.115 0.038 1.088 72.13 Cumulative lbs/acre 0.098 1 0.071 1 1.233 1 0.657 1 0.226 0.031 0.226 1 0.548 0.394 6.927 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 98 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X 420( / �— (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, hijection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: GORE PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 6.00 SITE #: NC BR 00314 FIELD# : BR 00314 0002 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 1.80 ACRES PERMITTED: 1.80 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/12/14 20.75 (W) 11.528 28.93 3.335 ADNG2&4: MOIST 0-<I/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 pF72771SOYBEANS Apr-14 20.75 (W) 11.528 Total Gallons/Ac: Total Wet Tons/Ac: 11.53 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 62 0.020 0.013 0.240 0.067 0.033 0.003 0.033 0.100 0.033 0.947 62.76 Cumulative lbs/acre 0.100 1 0.067 1 1.229 1 0.655 1 0.233 0.030 0.233 1 0.566 0.394 6.783 Permit PAN Limit (lbs/acre) 1st Crop/2yd Crop 98 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: RUTLAND PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 68.72 SITE #: NC BR 00315 FIELD# : BR 00315 0001 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.70 ACRES PERMITTED: 8.70 Page : 1 Lane Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or% Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm ) Crop p Total Per Acre MONTH 4/28/14 237.54 (W) 27.303 28.93 7.899 ADNG2&4: DRY 0- 1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 237.54 (W) 27.3031 1 1 1 1 1 1 l i orai Uanonsi vc: Total Wet Tons/Ac: 27.30 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 146 0.047 0.032 0.569 0.158 0.079 0.006 0.079 0.237 0.079 2.243 148.66 Cumulative lbs/acre. 0.163 1 0.067 1.787 0.822 0.256 0.025 0.256 0.700 0.248 8.759 •, (,`� µ 1 wz y z _ . ......, 1-1 11 Permit PAN Limit (lbs/acre) 1st Crop/2nd Cropr n: FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 .; ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X AP/ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for laiowing violations." N/A = Not Applicable NR = Not Reported ;or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: RUTLAND PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 25.08 SITE #: NC BR 00315 FIELD# : BR 00315 0002 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 3.00 ACRES PERMITTED: 3.00 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) - Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/28/14 86.68 (W) 28.893 28.93 8.359 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 1 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 1 86.68 M 28.893 1 Total Gallons/Ac: Total Wet Tons/Ac: 28.89 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 155 0.050 0.033 0.602 0.167 0.084 0.007 0.084 0.251 0.084 2.374 157.31 Cumulative lbs/acre 0.157 1 0.066 1 1.741 1 0.794 1 0.249 0.024 0.249 1 0.685 0.238 8.464 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 176 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: RUTLAND PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 19.11 SITE #: NC BR 00315 FIELD# : BR 00315 0003 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.30 ACRES PERMITTED: 2.30 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) 0 Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop ' MONTH Total Per Acre Solids 4/26/14 66.05 (W) 28.717 28.93 8.308 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 [7,000. p 1,940.00 p 2.77 p F 9249 SOYBEANS Apr-14 1 66.05 (W) 28.717 1 Total Gallons/Ac: Total Wet Tons/Ac: 28.72 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 154 0.050 0.033 0.598 0.166 0.083 0.007 0.083 0.249 0.083 2.359 156.36 Cumulative lbs/acre 0.155 1 0.065 1.695 0.757 0.243 0.024 0.243 0.665 0.240 8.233 1 1 1 1 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ,x . ., .n.. ,. FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 * :" ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: RUTLAND PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 18.93 SITE #: NC BR 00315 FIELD# : BR 00315 0004 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.40 ACRES PERMITTED: 2.40 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) 0 Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/26/14 65.42 (W) 27.258 28.93 7.886 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0:27 29,000. p 1,940.00 p 2.77 p [72�1SOYBEANS Apr-14 65.42 (W) 27.258 Total Gallons/Ac: Total Wet Tons/Ac: 27.26 As Cd Cr- Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 146 0.047 0.032 0.568 0.158 0.079 0.006 0.079 0.237 0.079 2.240 148.41 Cumulative lbs/acre 0.147 0.062 1.606 0.716 0.230 0.022 0.230 0.630 0.228 7.799';� ? z; Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop" FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x &YW� C)2/1//s (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel.properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for luiowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FAClL1TY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: RUTLAND PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 6.45 SITE #: NC BR 00315 FIELD# : BR 00315 0005 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 1.40 ACRES PERMITTED: 1.40 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp-) Crop MONTH Total Per Acre Solids 4/28/14 22.31 (W) 15.936 28.93 4.610 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 22.31 (W) 15.936 Total Gallons/Ac: Total Wet Tons/Ac: 15.94 As Cd Cr Cu Pb Hg Mo Ni Se . Zn P PAN TOTALS: Annual lbs/acre 85 0.028 0.018 0.332 0.092 0.046 0.004 0.046 0.138 0.046 1.309 86.76 Cumulative lbs/acre 0.117 0.043 1.319 0.640 0.168 0.017 0.168 0.514 0.184 6.555 � ����� �. � • �" s° �° . ;: w « y Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop *` ",.� % a ' ->x., -+. . ,.*•. xFai, n .. .,:'R"A „'«^'`a. _ .�" *°.;' .:.fir«' 'a.- ,.„as:,..ri7xi. � ,. FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 3 " ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: MCMILLAN PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 41.21 SITE #: NC BR 00317 FIELD# : BR 00317 0001 OPERATOR: THOMAS BRYANT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.60 ACRES PERMITTED: 9.60 Page Lune Applied *** Date Lbs Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/9/14 141.47 (W) 14.736 29.13 4.293 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 9121 SOYBEANS Jan-14 141.47 (W) 14.736 1 Total Gallons/Ac: Total Wet Tons/Ac: 14.74 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.026 0.026 0.343 0.258 0.043 0.003 0.052 0.146 0.043 1.511 109.89 78 Cumulative lbs/acre 0.100 0.056 0.874 0.512 0.147 0.014 0.156 0.341 0.371 4.441 . r Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop t 98 FD Cumulative Pollutant Loading Rate Limit (ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500 0 `_ $ T ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x AZ6�� I (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, hrjection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: MCMILLAN PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 18.53 SITE #: NC BR 00317 FIELD# : BR 00317 0003 OPERATOR: MCMILLAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.60 ACRES PERMITTED: 6.60 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppin) Crop MONTH Total Per Acre Solids 1/9/14 44.14 (W) 6.688 29.13 1.948 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100. p 2,090.00 p 8.24 p 9121 I SOYBEANS 1/10/14 19.47 (W) 2.950 29.13 0.859 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,100.p 2,090.00 p 8.24 p 1121 SOYBEANS Jan-14 1 63.61 (W) 9.638 Total Gallons/Ac: Total Wet Tons/Ac: 9.64 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.017 0.017 0.225 0.168 0.028 0.002 0.034 0.095 0.028 0.988 71.87 51 Cumulative lbs/acre 0.017 0.017 0.225 0.168 0.028 0.002 0.034 0.095 0.028 0.988 1 1 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop F; FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 A ADNG2&42:1= ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NOR -FOLK OWNER: JOHNSON/GARDNER PERMIT #: WQ0004500 SITE #: NC BR 00319 FIELD# : BR 00319 0001 OPERATOR: SHANE GUYTON RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL DRY TONS APPLIED: 97.93 CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 15.00 ACRES PERMITTED: 15.00 Page : I Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total per Acre Solids 3/21/14 223.51 (W) 14.901 27.43 4.087 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 I SOYBEANS 3/22/14 133.52 (W) 8.901 27.43 2.442 ADNG2&4: MOIST 0-<I/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 SOYBEANS Mar-14 357.03 (W) 23.802 1 Total Gallons/Ac: Total Wet Tons/Ac: 23.80 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 146 0.039 0.026 0.627 0.131 0.065 0.005 0.065 0.261 0.065 1.972 164.53 Cumulative lbs/acre 0.122 0.075 2.445 0.947 1 0.266 0.046 0.266 0.943 0.279 9.143 1 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop a" t 161 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 lk„. 375.0 89.0 2500.0 ¢."" ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X At// 2 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: JOHNSON/GARDNER PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 89.58 SITE #: NC BR 00319 FIELD# : BR 00319 0002 OPERATOR: SHANE GUYTON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.40 ACRES PERMITTED: 11.40 Page: 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/6/14 128.88 (W) 11.305 34.47 3.897 ADNG2&4: DRY 0-<1/T' SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p F 8823 SOYBEANS 5/7/14 65.34 (W) 5.732 34.47 1.976 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SOYBEANS 5/8/14 65.66 (W) 5.760 34.47 1.985 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SOYBEANS May-14 259.88 (W) 22.797 Total Gallons/Ac: Total Wet Tons/Ac: 22.80 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 139 0.047 0.031 0.629 0.189 0.079 0.006 0.079 0.267 0.079 2.687 149.77 Cumulative lbs/acre 0.167 0.106 2.827 1.102 0.343 0.057 0.343 1.082 0.351 10.886 4 a 11 Permit PAN Limit (lbs/acre) 1 st Crop/2nd Crop , $ s JrMI T 161 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ^ k `� a 1339.0 267.9 <, 15.0 . (� � 375.0 89.0 2500 0 mm i '�:,' a f ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable, NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: JOHNSON/GARDNER PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 42.31 SITE #: NC BR 00319 FIELD# : BR 00319 0003 OPERATOR: SHANE GUYTON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.70 ACRES PERMITTED: 6.70 Page : 1 Lime Applied *** Date Lb,/A, allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 3/24/14 154.24 (W) 23.021 27.43 6.315 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27[77:7�,3,350.00 p 46.30 p 11213 SOYBEANS Mar-14 154.24 (W) 23.021 1 1 Total Gallons/Ac: Total Wet Tons/Ac: 23.02 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 142 0.038 0.025 0.606 0.126 0.063 0.005 0.063 0.253 0.063 1.907 159.13 Cumulative Ibs/acre 0.124 0.089 2.335 0.818 1 0.269 0.036 0.269 0.886 0.232 7.773 1 Permit PAN Limit (lbs/acre) 1st Crop/2nd CropVi 17,176 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 % *9- 411 I (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: JOHNSON/GARDNER PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 52.65 SITE #: NC BR 00319 FIELD# : BR 00319 0004 OPERATOR: SHANE GUYTON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.60 ACRES PERMITTED: 11.60 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TICN Nitrogen and (ppm) Crop MONTH Total FP.r Acre Solids 9/12/14 195.15 (W) 16.823 26.98 4.539 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 [UTUUT 4,480.00 p [7.93 p 711052 WHEAT Sep-14 195.15 (W) 16.823 Total Gallons/Ac: Total Wet Tons/Ac: 16.82 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 100 0.027 0.018 0.527 0.118 0.045 0.006 0.045 0.191 0.045 1.879 123.46 Cumulative lbs/acre� 0.079 0.060 1.311 0.730 0.202 0.027 0.202 0.536 0.160 6.443 r "" Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop a + 136 ,:kd^ :g"xj x , d,.3M.t � +a�T4� . t'Y� , fix•. *'� ..�fv k " a:. ." P'x� k. x x eCn V FD.Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 A . 1339.0 267.9 15.0 . 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there "are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 } ANNUAL LAND APPLICATION FIELD SUMMARY FORM ' Page : 1 FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK Lime Applied *** OWNER: LUVENIA BRYANT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 31.03 Date Lbs/Ac SITE #: NC BR 00319 FIELD# : BR 00319 0005 OPERATOR: LUVENIA BRYANT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4,50 ACRES PERMITTED: 4.50 DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- till- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and pe,Iq (ppm) Crop MONTH Total Per Acre Solids 4/16/14 20.53 (W) 4.562 28.93 1.320 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS 4/17/14 86.71 (W) 19.269 28.93 5.574 ADNG2&4. MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 107.24 (W) 23.831 Total Gallons/Ac: Total Wet Tons/Ac: 23.83 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Amoral Ibs/acre 128 0.041 0.028 0.496 0.138 0.069 0.006 0.069 0.207 0.069 1.958 129.75 Cumulative lbs/acre 0.041 0.028 0.496 0.138 0.069 0.006 0.069 0.207 0.069 1.958 (4° , " � .:� *tea•„� Permit PAN Limit (Ibs/acre) 1st Cro /2nd Crop 1 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 W 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: CAMERON PROPT LIMITED PAR PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 38.69 SITE #: NC BR 00319 FIELD# : BR 00319 0006 OPERATOR: SHANE GUYTON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 15.20 ACRES PERMITTED: 15.20 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 4/4/14 22,712.23 (G) 1494.226 14.84 0.925 ADNG3L MOIST 0-<1/2" SUR 0.5 0.40 72,100.p 2,630.00 p 88.90 p 29192 I SOYBEANS 4/9/14 16,352.51 (G) 1075.823 14.84 0.666 ADNG3L MOIST 0-<1/2" SUR 0.5 0.40 72,100.p 2,630.00 p 88.90 p 29192 I SOYBEANS 4/10/14 23,460.44 (G) 1543.450 14.84 0.955 ADNG3L MOIST 0-<1/2" SUR 0.5 0.40 72,100.p 2,630.00 p 88.90 p 29192 SOYBEANS Apr-14 1 62,525.18 (G)l 4,113.499 Total Gallons/Ac: 4,113.50 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 149 0.015 0.010 0.036 0.046 0.025 0.002 0.025 0.025 0.025 0.061 42.71 Cumulative lbs/acre 0.015 0.010 0.036 0.046 0.025 0.002 0.025 0.025 0.025 0.061 x ?, Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop; 161 t * y-, an •' �'nrr, . �+ FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 �," 1339.0 267.9 15.0 t " 375.0 89.0 2500.0 ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID X o24411__5_ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: TRIPP/MILLIGAN PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 23.99 SITE #: NC BR 00322 FIELD# : BR 00322 0011 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 16.70 ACRES PERMITTED: 16.70 Page : 1 Lnue Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop Total Per Acre MONTH 12/8/14 87.53 (W) 5.241 27.4,1 1.437 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p p 8871 WHEAT Dec-14 87.53 (W) 5.241 7.50 l'otal Gallons/Ac: Total Wet Tons/Ac: 5.24 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 25 0.009 0.006 0.147 0.026 0.014 0.001 0.014 0.060 0.014 0.336 20.31 Cumulative lbs/acre 0.055 0.037 0.525 0.208 0.092 0.017 0.092 0.226 0.176 2.577 V, Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop * tsujZ p; y w,, 136 ."-ati�, v.� '::.;q &.M w:, .:�%r^?'=*^wt°+3w R. ,,;w.W*r �; .y..^, ',a •,kv".�:; dd w.rxw. w!wM»C'xaw'.aS 3 tx4 £ ;i. r"�Y`.��4'ns ?:S. � �'+:,w;(?„? FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 rk 2 1339.0 267.9 15.0 375.0 89.0 2500.0 5�* ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 lol�l (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC OWNER: TRIPP/MILLIGAN SITE #: NC BR 00322 FIELD# : BR 00322 0014 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: RAINS PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 215.08 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 40.80 ACRES PERMITTED: 40.80 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 11/22/14 105.93 (W) 2.596 29.25 0.759 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 WHEAT Nov-14 105.93 (W) 2.596 12/1/14 110.19 (W) 2.701 27.41 0.740 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 I WHEAT 12/2/14 88.52 (W) 2.170 27.41 0.595 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 I WHEAT 12/3/14 87.15 (W) 2.136 27.41 0.585 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 I WHEAT 12/4/14 85.99 (W) 2.108 27.41 0.578 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 I WHEAT 12/5/14 104.65 (W) 2.565 27.41 0.703 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 I WHEAT 12/8/14 195.14 (W) 4.783 27.41 1.311 ADNG2&4: MOIST 0-<I/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8171 WHEAT Dec-14 671.64 (W) 16.463 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: RAINS OWNER: TRIPP/MILLIGAN PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 215.08 SITE #: NC BR 00322 FIELD# : BR 00322 0014 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 40.80 ACRES PERMITTED: 40.80 Page : 2 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total PeI,Acre Solids Total Gallons/Ac: Total Wet Tons/Ac: 19.06 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.032 0.021 0.535 0.096 0.053 0.004 0.053 0.224 0.053 1.303 79.75 93 Cumulative lbs/acre 0.067 0.045 0.817 0.238 0.112 0.018 0.112 0.342 . 0.194 2.927 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 106 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500 0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, wider penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: TRIPP/MILLIGAN PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 19.12 SITE #: NC BR 00322 FIELD# : BR 00322 0015 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4.40 ACRES PERMITTED: 4.40 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) %I Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PANDATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 11/22/14 65.36 (W) 14.855 29.25 4.345 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 22 r WHEAT Nov-14 65.36 (W) 14.855 1 Total Gallons/Ac: Total Wet Tons/Ac: 14.85 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 71 Annual lbs/acre 0.026 0.017 0.426 0.087 0.043 0.003 0.043 0.200 0.043 1.416 91.24 • . a .® Cumulative lbs/acre' 0.062 0.041 0.712 0.230 0.103 0.018 0.103 0.319 0.187 3.063 ^ k'. r 136 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop, . �� .• FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 34.8 1339.0 267.9 15.0 i 375.0 89.0 2500.0 ' .Z '. ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 a (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MILLIGAN PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 5.89 SITE #: NC BR 00324 FIELD# : BR 00324 0001 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.80 ACRES PERMITTED: 7.80 Page : 1 Line Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 12/10/14 21.49 (W) 2.755 27.41 0.755 ADNG2&4: MOIST 0-<I/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 1 17.50 p 1 8871 WHEAT Dec-14 21.49 (W) 2.755 Total Gallons/Ac: Total Wet Tons/Ac: 2.76 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.005 0.003 0.077 0.014 0.008 <.001 0.008 0.032 0.008 0.177 10.68 13 Cumulative lbs/acre 0.052 0.019 0.422 0.202 0.086 0.019 0.086 0.173 0.055 2.264 136 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ar FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 _ `` 1339.0 267.9 15.0 $s 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system'designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hrjection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MILLIGAN PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 139.26 SITE #: NC BR 00324 FIELD# : BR 00324 0004 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 18.00 ACRES PERMITTED: 18.00 Page Lane Applied *** Date::T Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 10/28/14 194.84 (W) 10.824 28.01 3.032 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p F 7842 I WHEAT 10/29/14 106.41 (W) 5.912 28.01 1.656 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 WHEAT 10/30/14 151.26 (W) 8.403 28.01 2.354 ADNG2&4. DRY 0-,<I/2" SURIN 1.0 0.27 25,100.p . 1,430.00 p 21.40 p 7842 WHEAT 10/31/14 44.65 (W) 2.481 28.01 0.695 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 21.40 p 7842 WHEAT Oct-14 497.16 (W) 27.620 Total Gallons/Ac: Total Wet Tons/Ac: 27.62 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 121 0.046 0.031 0.836 0.201 0.077 0.006 0.077 0.325 0.077 2.754 187.22 Cumulative lbs/acre 0.046 0.031 0.836 0.201 0.077 0.006 0,077 0.325 0.077 2.754 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop'., , 136 a FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 890 2500.0 v ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: FORESTEN OWNER: MILLIGAN PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 18.28 SITE #: NC BR 00324 FIELD# : BR 00324 0005 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 3.00 ACRES PERMITTED: 3.00 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 10/31/14 65.26 (W) 21.753 28,01 6.093 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100. p 1,430.00 p 21.40 p 7847 F WHEAT Oct-14 1 65.26 (W) 21.7531 1 1 1 1 1 1 1 1 1 1 1 Total Gallons/Ac: Total Wet Tons/Ac: 21.75 As Cd Cr Cu Pb Hg Mo Ni Se Zn _ P PAN TOTALS: Annual lbs/acre 96 0.037 0.024 0.658 0.158 0.061 0.005 0.061 0.256 0.061 2.169 147.45 Cumulative lbs/acre 0.037 0.024 0.658 0.158 0.061 0.005 0.061 0.256 0.061 2.169 z �' < Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop + . s 115 i FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 x; ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/k.- ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: TOMAHAWK OWNER: MILLIGAN PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 12.08 SITE #: NC BR 00324 FIELD# : BR 00324 0006 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4.00 ACRES PERMITTED: 4.00 Page: 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 10/31/14 43.12 (W) 10.780 28.01 3.019 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100.p 1,430.00 p 7.40 p 7842 WHEAT Oct-14 1 43.12 (W) 10.7801 1 1 1 1 1 1 1 1 1 1 Total Gallons/Ac: Total Wet Tons/Ac: 10.78 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 47 0.018 0.012 0.326 0.079 0.030 0.002 0.030 0.127 0.030 1.075 73.07 Cumulative lbs/acre 0 .018 0.012 0.326 0.079 0.030 0.002 0.030 0.127 0.030 1.075 °` Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop .� FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 "" 1339.0 267.9 15.0 375.0 89.0 2500.0 ` .°" ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: MILLIGAN' PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 88.76 SITE #: NC BR 00324 FIELD# : BR 00324 0007 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 21.30 ACRES PERMITTED: 21.30 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) 0 Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppni) Crop MONTH Total Per Acre Solids 10/31/14 43.34 (W) 2.035 28.01 0.570 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,100. p 1,430.00 p 21.40 p 7842 WHEAT Oct-14 43.34 (W) 2.035 11/4/14 43.65 (W) 2.049 29.25 0.599 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 I WHEAT 11/5/14 130.28 (W) 6.116 29.25 1.789 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 I WHEAT 11/10/14 88.02 (W) 4.132 29.25 1.209 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 WHEAT Nov-14 261.95 (W) 12.297 Total Gallons/Ac: Total Wet Tons/Ac: 14.33 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 68 0.025 0:017 0.414 0.087 0.042 0.003 0.042 0.189 0.042 1.376 89.33 Cumulative lbs/acre 0.025 0.017 0.414 0.087 0.042 0.003 0.042 0.189 0.042 1.376 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop + _" * "+ s ", "q 80 ar , FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 - ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X 2k E/:�� 1$ Z 20 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN- hicorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: MILLIGAN PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 12.52 SITE #: NC BR 00324 FIELD# : BR 00324 0008 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4.20 ACRES PERMITTED: 4.20 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site 'Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 11/12/14 42.81 (W) 10.193 29.25 2.9$1 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000.p 1,880.00 p 99.80 p 8222 WHEAT Nov-14 42.81 (W) 10.193 Total Gallons/Ac: Total Wet Tons/Ac: 10.19 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.018 0.012 0.292 0.060 0.030 0.002 0.030 0.137 0.030 0.972 62.61 49 Cumulative lbs/acre 0.018 0.012 0.292 0.060 0.030 0.002 0.030 0.137 0.030 0.972 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop t - �"r < fix' - 80 J,.. a ;'i, p.s .�.-:' ;u. 4''zs;"s - aw' ,>*r. —i" qsm; �c."w'' i a v", ...:.ik. s".S, ., <: s«�. , FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 h 1339.0 267.9 15.0 375.0 89.0 2500 0 *' ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page : 1 FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO Lune Applied *** OWNER: MILLIGAN PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 184.88 Date Lbs/Ac SITE #: NC BR 00324 FIELD# : BR 00324 0009 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 25.70 ACRES PERMITTED: 25.70 DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 11/12/14 132.24 (W) 5.146 29.25 1.505 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 I WHEAT 11/13/14 176.32 . (W) 6.861 29.25 2.007 ADNG2&4. DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 I WHEAT 11/14/14 259.02 (W) 10.079 29.25 2.948 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 WHEAT 11/17/14 64.48 (W) 2.509 29.25 0.734 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 WHEAT Nov-14 632.06 (W) 24.595 Total Wet Tons/Ac: 24.59 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 118 0.043 0.029 0.705 0.144 0.072 0.006 0.072 0.331 0.072 2.345 151.07 Cumulative lbs/acre 0.043 0.029 0.705 0.144 0.072 0.006 0.072 0.331 0.072 2.345 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 411K' z 34.8 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 1339.0 267.9 15.0 rr _ 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x ®� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation L0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: MILLIGAN PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 270.59 SITE #: NC BR 00324 FIELD# : BR 00324 0010 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 42.80 ACRES PERMITTED: 42.80 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 11/17/14 259.11 (W) 6.054 29.25 1.771 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 I WHEAT 11/18/14 170.19 (W) 3.976 29.25 1.163 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 I WHEAT 11/19/14 195.69 (W) 4.572 29.25 1.337 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 I WHEAT 11/20/14 106.28 (W) 2.483 29.25 0.726 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 I WHEAT 11/21/14 193.83 (W) 4.529 29.25 1.325 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 25,000. p 1,880.00 p 99.80 p 8222 WHEAT Nov-14 925.10 (W) 21.614 Total Gallons/Ac: Total Wet Tons/Ac: 21.61 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.038 0.025 0.620 0.126 0.063 0.005 0.063 0.291 0.063 2.061 132.77 104 Cumulative lbs/acre 0.038 0.025 0.620 0.126 0.063 0.005 0.063 0.291 0.063 2.061 e1`. �..; Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop �:,.i- 136 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 „; " 1339.0 267.9 15.0 ' 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X 14 L( 2a � S� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE OWNER: MCNEIL/SIDBURY PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 5.90 SITE #: NC BR 00327 FIELD# : BR 00327 0001 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.30 ACRES PERMITTED: 2.30 Page: 1 Line Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 3/26/14 21.49 (W) 9.343 27.43 2.563 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 SOYBEANS Mar-14 21.49 (W) 9.343 Total Gallons/Ac: Total Wet Tons/Ac: 9.34 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 57 0.015 0.010 0.246 0.051 0.026 0.002 0.026 0.103 0.026 0.774 64.59 b Cumulative lbs/acre 0.036 0.021 0.488 0.188 0.078 0.007 0.078 0.229 0.110 2.076Al Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop % 98 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 7r ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM ' ' Page: 1 FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: BAYMEADE Lune Applied *** OWNER: MCNEIL/SIDBURY PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 11.97 Date Lbs/Ac SITE #: NC BR 00327 FIELD# : BR 00327 0002 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.90 ACRES PERMITTED: 2.90 DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip, Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppni) Crop MONTH Total Per Acre Solids 3/24/14 20.75 (W) 7.155 27.43 1.963 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 I SOYBEANS 3/26/14 22.87 (W) 7.886 27.43 2.163 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 SOYBEANS Mar-14 1 43.62 (W) 15.041 1 Total Gallons/Ac: Total Wet Tons/Ac: 15.04 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 93 0.025 0.017 0.396 0.083 0.041 0.003 0.041 0.165 0.041 1.246 103.97 Cumulative lbs/acre 0.050 0.029 0.683 0.245 0.104 0.010 0.104 0.315 0.141 2.792 Penuit PAN Limit (lbs/acre) 1st Crop/2nd Crop s t.., ... r 98 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 r. ; ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NOR -FOLK OWNER: CARTER/CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 185.44 SITE #: NC BR 00330 FIELD# : BR 00330 0001 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 12.50 ACRES PERMITTED: 12.50 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 6/24/14 107.60 (W) 8.608 30.74 2.646 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p F 9363 I SORGHUM 6/25/14 108.22 (W) 8.658 30.74 2.661 ADNG2&4. DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SORGHUM 6/26/14 195.55 (W) 15.644 30.74 4.809 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SORGHUM 6/27/14 171.33 (W) 13.706 30.74 4.213 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 SORGHUM Jun-14 582.70 (W) 46.616 7/7/14 21.37 (W) 1.710 29.57 0.506 DRY 0-<1/2" SURIN 1.0 0.27 1 30,100.p 1 5,310.00 p 1 2.00 p 1 12005 SORGHUM Jul-14 21.37 (W) 1 1 1.710 JADNG2&4: I 1 1 1 1 Total Gallons/Ac: Total Wet Tons/Ac: 48.33 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 280 0.089 0.059 1.577 0.930 0.177 0.013 0.148 0.708 0.148 8.935 399.51 Cumulative lbs/acre'` 0.129 1 0.080 2.156 1.201 1 0.274 0.022 0.246 0.922 0.177 12.706 1 1 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop a F p 312 J FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 34.8 1339.0 267.9 15.0 k 375.0 89.0 2500.0 g -t '0 .. ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, htjection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: CARTER/CARROLL PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 102.39 SITE #: NC BR 00330 FIELD# : BR 00330 0004 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.10 ACRES PERMITTED: 9.10 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 6/30/14 128.00 (W) 14.066 30.74 4.324 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.W p 6.18 p 9363 SORGHUM Jun-14 128.00 (W) 14.066 7/7/14 84.19 (W) 9.252 29.57 2.736 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 I SORGHUM 7/8/14 129.01 (W) 14.177 29.57 4.192 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 30,100.p 5,310.00 p 2.00 p 12005 SORGHUM Jul-14 213.20 (W) 23.429 Total Gallons/Ac: Total Wet Tons/Ac: 37.49 As Cd" Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 247 0.068 0.045 1.248 0.457 0.121 0.027 0.113 0.485 0.113 6.056 327.87 Cumulative Ibs/acre 0.131 0.080 2.079 0.849 0.266 0.043 0.257 0.796 0.205 11.378x Permit PAN Limit lbs/acre 1st Cro /2nd Cro[A p x"-..�`• a r ?w '`a .. „ p v.�.q f� P th 9�p' a h+w"' ,.'m f..L t'., A::^.�,!i" iaav ti'Y . �` tkn p?� FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 # `� ; ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF, NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: GILBERT/LONG PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 28.82 SITE #: NC BR 00336 FIELD# : BR 00336 0002 OPERATOR: SHANE GUYTON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 14.80 ACRES PERMITTED: 14.80 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) ov Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Drya, Wet, :Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/10/14 46,570.74 (G) 3146.672 14.84 1.947 ADNG3L MOIST 0-<I/2" SUR 0.5 0.40 72,100.p 2,630.00 p 88.90 p 729192 SOYBEANS Apr-14 46,570.74 (G) 3,146.672 Total Gallons/Ac: 3,146.67 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 114 0.012 0.008 0.027 0.035 0.019 0.002 0.019 0.019 0.019 0.047 32.67 Cumulative lbs/acre 0.026 0.022 0.361 0.092 0.034 Y.:'& Y 1.656" ., :a, 0.253 0.007 0.092 0.164 Permit PAN Limit lbs/acre 1st Cro /2nd Cro t, t :� 176 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ry ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, ]NJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: GILBERT/LONG PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 44.50 SITE #: NC BR 00336 FIELD# : BR 00336 0003 OPERATOR: SHANE GUYTON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5.90 ACRES PERMITTED: 5.90 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- till- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 4/16/14 44.04 (W) 7.464 28.93 2.159 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p F 9249 I SOYBEANS 4/17/14 109.78 (W) 18.607 28.93 5.383 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 1 153.82 (W) 26.071 Total Gallons/Ac: Total Wet Tons/Ac: 26.07 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.045 0.030 0.543 0.151 0.075 0.006 0.075 0.226 0.075 2.142 141.95 140 Cumulative lbs/acre 0.055 0.040 0.763 0.294 0.123 0.010 0.123 0.322 0.085 3.201 ' Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop , FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0375.0 89.0 2500.0 r ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of finds and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC OWNER: LONG SITE #: NC BR 00337 FIELD# : BR 00337 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: TORHUNTA PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 626.61 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 80.10 ACRES PERMITTED: 80.10 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 6/9/14 192.02 (W) 2.397 30.74 0.737 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SOYBEANS 6/10/14 234.00 (W) 2.921 30.74 0.898 ADNG2&4. DRY 0-<I/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SOYBEANS 6/11/14 316.03 (W) 3.945 30.74 1.213 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SOYBEANS 6/12/14 231.37 (W) 2.889 30.74 0.888 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SOYBEANS 6/13/14 171.15 (W) 2.137 30.74 0.657 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SOYBEANS 6/16/14 253.61 (W) 3.166 30.74 0.973 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SOYBEANS 6/17/14 233.63 (W) 2.917 30.74 0.897 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SOYBEANS 6/18/14 212.88 (W) 2.658 30.74 0.817 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 I SOYBEANS 6/19/14 193.74 (W) 2.419 30.74 0.744 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,300. p 3,090.00 p 6.18 p 9363 SOYBEANS Jun-14 1 2,038.43 (W) 1 25.449 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: TORHUNTA OWNER: LONG PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 626.61 SITE #: NC BR 00337 FIELD# : BR 00337 0001 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 80.10 ACRES PERMITTED: 80.10 Page : 2 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppin) Crop MONTH Total Per Acre Solids Total Gallons/Ac: Total Wet Tons/Ac: 25.45 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 146 Annual lbs/acre 0.047 0.031 0.829 0.501 0.094 0.006 0.078 0.376 0.078 4.741 209.65 Cumulative lbs/acre 0.075 1 0.052 1.135 1 0.673 0.159 0.017 0.143 0.505 0.172 6.378 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 163 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 { 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X e2l /,/s` (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM ' ' Page : I FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: KUREB Lune Applied *** OWNER: ORTON PLANTATION HOLDING PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 105.78 Date Lbs/Ac SITE #: NC BR 00338 FIELD# : BR 00338 0074 OPERATOR: DILLION EPP CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 15.00 ACRES PERMITTED: 15.00 DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 3/10/14 112.59 (W) 7.506 27.43 2.059 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 CAUCASION/OLD WORLD BLUESTE 3/11/14 273.03 (W) 18.202 27.43 4.993 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 CAUCASION/OLD WORLD BLUESTE Mar-14 385.62 (W) 25.708 Total Wet Tons/Ac: 25.71 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 158 0.042 0.028 0.677 0.141 0.071 0.006 0.071 0.282 0.071 2.130 177.70 Cumulative lbs/acre 0.079 0.052 0.870 0.262 0.131 0.010 0.131 0.355 0.397 3.230 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop g" 159 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X � I (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: KUREB OWNER: ORTON PLANTATION HOLDING PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 98.88 SITE #: NC BR 00338 FIELD# : BR 00338 0075 OPERATOR: DILLION EPP CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 14.90 ACRES PERMITTED: 14.90 Page: 1 Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pp m ) Crop p MONTH Total Per Acre Solids 3/13/14 88.30 (W) 5.926 27.43 1.626 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 CAUCASION/OLD WORLD BLUESTE 3/14/14 137.10 (W) 9.201 27.43 2.524 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 CAUCASION/OLD WORLD BLUESTE 3/19/14 135.09 (W) 9.066 27.43 2.487 ADNG2&4: MOIST 0-<I/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 CAUCASION/OLD WORLD BLUESTE Mar-14. 1 360.49 (W) 24.193 Total Wet Tons/Ac: 24.19 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annuallbs/acre 149 0.040 0.027 0.637 0.133 0.066 0.005 0.066 0.265 0.066 2.004 167.24 Cumulative lbs/acre 0.075 0.050 0.827 0.251 0.126 0.010 0.126 0.337 0.386 3.083 Permit PAN Limit Ibs/acre lst Cro /2nd Crop159 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: KUREB OWNER: ORTON PLANTATION HOLDING PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 56.38 SITE #: NC BR 00338 FIELD# : BR 00338 0076 OPERATOR: DILLION EPP CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.00 ACRES PERMITTED: 8.00 Page : 1 Line Applied *** Date Lbs/A. DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 3/12/14 160.39 (W) 20.049 27.43 5.499 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 CAUCASION/OLD WORLD BLUESTE 3/13/14 45.14 (W) 5.643 27.43 1.548 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 32,300. p 3,350.00 p 46.30 p 11213 CAUCASION/OLD WORLD BLUESTE Mar-14 205.53 (W) 25.692 Total Wet Tons/Ac: 25.69 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 158 0.042 0.028 0.677 0.141 0.070 0.006 0.070 0.282 0.070 2.128 177.59 Cumulative lbs/acre 0.059 1 0.040 1 0.809 1 0.215 1 0.099 0.008 0.099 1 0.341 0.163 2.991 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 159 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X A��L&f1i FJZIZaIlS' (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, InjectionAncorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation ***- See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: RAINS OWNER: WILLIAMS/LEWIS - PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 155.67 SITE #: NC BR 00339 FIELD# : BR 00339 0001 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 19.00 ACRES PERMITTED: 19.00 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppni) Crop MONTH Total Per Acre Solids 5/13/14 197.26 (W) 10.382 34.47 3.579 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SORGHUM 5/14/14 254.35 (W) 13.387 34.47 4.614 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SORGHUM May-14 451.61 (W) 23.769 Total Gallons/Ac: Total Wet Tons/Ac: 23.77 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.049 0.033 0.655 0.197 0.082 0.007 0.082 0.279 0.082 2.802 156.16 145 Cumulative lbs/acre 0.060 0.044 0.904 0.358 0.136 0.011 0.136 0.386 0.093 4.000 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 2 04 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: RAINS OWNER: WILLIAMS/LEWIS PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 103.50 SITE #: NC BR 00339 FIELD# : BR 00339 0002 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.90 ACRES PERMITTED: 13.90 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/14/14 87.01 (W) 6.260 34.47 2.158 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p F 8823 SORGHUM 5/15/14 213.25 (W) 15.342 34.47 5.288 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SORGHUM May-14 300.26 (W) 21.602 Total Gallons/Ac: Total Wet Tons/Ac: 21.60 As Cd Cr Cu Ph Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 131 0.045 0.030 0.596 0.179 0.074 0.006 0.074 0.253 0.074 2.547 141.92 Cumulative lbs/acre 0.067 1 0.046 1 0.837 1 0.314 1 0.126 0.015 0.126 1 0.355 0.152 3.846 r �_ [ Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 204 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x e).Z1 / ze) /11-s— (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: WILLIAMS/LEWIS PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 187.97 SITE #: NC BR 00339 FIELD# : BR 00339 0003 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 28.10 ACRES PERMITTED: 28.10 Page : 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm Crop p MONTH Total Per Acre Solids 5/8/14 221.22 (W) 7.873 34.47 2.714 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SORGHUM 5/9/14 324.09 (W) 11.533 34.47 3.976 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700.p 2,200.00 p 7.83 p 8823 SORGHUM May-14 545.31 (W) 19.406 Total Gallons/Ac: Total Wet Tons/Ac: 19.41 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 118 0.040 0.027 0.535 0.161 0.067 0.005 0.067 0.227 0.067 2.288 127.50 Cumulative lbs/acre 0.096 1 0.064 1 0.981 1 0.383 1 0.160 0.028 0.160 1 0.413 0.290 4.850 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 312 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x I � W, �/, t,114 � (-, - (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 I FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC OWNER: CHIP CARROLL SITE #: NC BR 00339 FIELD# : BR 00339 0004 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: FORESTER PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 152.32 OPERATOR: CHIP CARROLL CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 17.10 ACRES PERMITTED: 17.10 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/15/14 106.58 (W) 6.233 34.47 2.148 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I SORGHUM 5/23/14 247.35 (W) 14.465 34.47 4.986 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I SORGHUM 5/27/14 87.95 (W) 5.143 34.47 1.773 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SORGHUM May-14 441.88 (W) 25.841 - Total Gallons/Ac: Total Wet Tons/Ac: 25.84 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 157 0.053 0.036 0.713 0.214 0.089 0.007 0.089 0.303 0.089 3.046 169.77 Cumulative lbs/acre 0.053 0.036 0.713 0.214 0.089 0.007 0.089 0.303 0.089 3.046 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 160 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 �n 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X OF111_40ft e)ZA?e1,1_5— (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDBORO OWNER: HOLT/WILLIAMS/HEWETT PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 16.99 SITE #: NC BR 00341 FIELD# : BR 00341 0002 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 14.10 ACRES PERMITTED: 14.10 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 9/5/14 62.96 (W) 4.465 26.98 1.205 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11052 WHEAT Sep-14 62.96 (W) 4.465 Total Gallons/Ac: Total Wet Tons/Ac: 4.47 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.007 0.005 0.140 0.031 0.012 0.002 0.012 0.051 0.012 0.499 32.77 27 Cumulative Ibs/acre 0.057 0.038 1 0.388 1 0.147 1 0.095 0.008 0.095 1 0.150 0.095 1.772 r - Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 136 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 g (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/hrcorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: HOLT/WILLIAMS/HEWETT PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 57.74 SITE #: NC BR 00341 FIELD# : BR 00341 0004 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 15.20 ACRES PERMITTED: 15.20 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 9/11/14 170.87 (W) 11.241 26.98 3.033 ADNG2&4: MOIST 0-<I/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11052 I WHEAT 9/12/14 43.14 (W) 2.838 26.98 0.766 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 28,800.p 4,480.00 p 5.93 p 11012 WHEAT Sep-14 1 214.01 (W) 14.079 Total Gallons/Ac: Total Wet Tons/Ac: 14.08 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.023 0.015 0.441 0.099 0.038 0.005 0.038 0.160 0.038 1.573 103.32 84 Cumulative lbs/acre 0.042 1 0.028 1 0.629 1 0.180 1 0.069 0.008 0.069 1 0.241 0.069 2.684 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 106 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X eo= (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: HOLT/WILLIAMS/HEWETT PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 113.50 SITE #: NC BR 00341 FIELD# : BR 00341 0005 OPERATOR: FRANK HEWITT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 15.70 ACRES PERMITTED: 15.70 Page : 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 4/7/14 106.06 (W) 6.755 28.93 1.954 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 I SOYBEANS 4/11/14 286.25 (W) 18.232 28.93 5.275 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 392.31 (W) 24.987 1 Total Gallons/Ac: Total Wet Tons/Ac: 24.99 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.043 0.029 0.520 0.145 0.072 0.006 0.072 0.217 0.072 2.053 136.05 134 Cumulative lbs/acre 0.099 0.066 0.800 0.275 0.166 0.013 0.166 0.329 0.166 3.489 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop A 155 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: TOMAHAWK OWNER: GORE PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 114.47 SITE #: NC BR 00345 FIELD# : BR 00345 0001 OPERATOR: CRAY MILLIGAN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 36.20 ACRES PERMITTED: 36.20 Page : 1 Lime Applied "* Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pptn) Crop MONTH Total Per Acre Solids 12/9/14 153.70 (W) 4.246 27.41 1.164 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p F 8871 WHEAT 12/10/14 64.68 (W) 1.787 27.41 0.490 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 WHEAT 12/12/14 132.28 (W) 3.654 27.41 1.002 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 WHEAT 12/15/14 66.95 (W) 1.849 27.41 0.507 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 WHEAT Dec-14 417.61 (W) 11.536 Total Gallons/Ac: Total Wet Tons/Ac: 11.54 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.019 0.013 0.323 0.057 0.032 0.003 0.032 0.133 0.032 0.740 44.71 56 Cumulative lbs/acre 0.045 1 0.030 1 0.548 1 0.152 1 0.075 0.006 0.075 1 0.246 0.075 2.197 . t Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 68 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 `` f 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x O.--IV 0//.5-, (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: LYNCHBURG OWNER: BENNETT/RICHARDSON PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 94.12 SITE #: NC BR 00347 FIELD# : BR 00347 0001 OPERATOR: SHANE GUYTON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.80 ACRES PERMITTED: 11.80 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip, Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 4/14/14 62.93 (W) 5.333 28.93 1.543 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS 4/28/14 64.12 (W) 5.434 28.93 1.572 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS 4/29/14 198.30 (W) 16.805 28.93 4.862 ADNG2&4: DRY 0-<I/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 325.35 (W) 27.572 Total Gallons/Ac: Total Wet Tons/Ac: 27.57 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre ' 0.048 0.032 0.574 0.160 0.080 0.006 0.080 0.239 0.080 2.265 150.12 148 Cumulative lbs/acre 0.072 0.048 0.772 0.239 0.119 0.010 0.119 0.326 0.119 3.506 Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop 178 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X A� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or nig/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: BENNETT/RICHARDSON PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 59.44 SITE #: NC BR 00347 FIELD# : BR 00347 0002 OPERATOR: SHANE GUYTON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.60 ACRES PERMITTED: 13.60 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 9/20/14 88.27 (W) 6.490 26.98 1.751 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11052 WHEAT 9/22/14 132.03 (W) 9.708 26.98 2.619 ADI4G2&4: MOIST 0-<1/2" SURIN 1.0 0.27 28,800. p 4,480.00 p 5.93 p 11052 WHEAT Sep-14 220.30 (W) 16.198 Total Gallons/Ac: Total Wet Tons/Ac: 16.20 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 97 0.026 0.017 0.507 0.114 0.044 0.006 0.044 0.184 0.044 1.809 118.87 Cumulative lbs/acre 0.052 0.035 0.722 0.200 0.087 0.010 0.087 0.278 0.087 3.159 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop .f t' 123 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X dlo�/S` (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: BENNETT/RICHARDSON PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 143.59 SITE #: NC BR 00347 FIELD# : BR 00347 0004 OPERATOR: SHANE GUYTON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 17.00 ACRES PERMITTED: 17.00 Page Lune Applied *** Date LUs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pptn) Crop MONTH Total Per Acre Solids 4/24/14 130.99 (W) 7.705 28.93 2.229 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS. 4/25/14 320.97 (W) 18.881 28.93 5.462 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS 4/26/14 44.36 (W) 2.609 28.93 0.755 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 SOYBEANS Apr-14 496.32 (W) 29.195 Total Gallons/Ac: Total Wet Tons/Ac: 29.20 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 0.051 0.034 0.608 0.169 0.084 0.007 0.084 0.253 0.084 2.399 158.96 156 Cumulative lbs/acre 0.077 0.051 0.827 0.256 0.128 0.010 0.128 0.350 0.128 3.771 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 176 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCI4ER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: ONSLOW OWNER: BENNETT/RICHARDSON PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 81.27 SITE #: NC BR 00347 FIELD# : BR 00347 0005 OPERATOR: SHANE GUYTON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.10 ACRES PERMITTED: 11.10 Page : 1 Lime Applied.*** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/30/14 280.91 (W) 25.307 28.93 7.321 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 79249 SOYBEANS Apr-14 1 280.91 (W) 1 25.307 1 Total Gallons/Ac: Total Wet Tons/Ac: 25.31 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 135 0.044 0.029 0.527 0.146 0.073 0.006 0.073 0.220 0.073 2.079 137.79 Cumulative lbs/acre 0.067 0.045 0.721 0.224 0.112 0.009 0.112 0.305 0.112 3.296 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop , 155 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Ltcorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: LYNCHBURG OWNER: MILLIS PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 118.72 SITE #: NC BR 00348 FIELD# : BR 00348 0001 OPERATOR: SANDY MANSFIELD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.30 ACRES PERMITTED: 13.30 Page Lime Applied *** Date _::]: Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/5/14 148.56 (W) 11.170 34.47 3.850 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 I SOYBEANS 516114 195.84 (W) 14.725 34.47 5.076 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 'p 8823 SOYBEANS May-14 344.40 (W) 25.895 Total Gallons/Ac: Total Wet Tons/Ac: 25.89 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 158 0.054 0.036 0.714 0.214 0.089 0.007 0.089 0.303 0.089 3.053 170.13 Cumulative lbs/acre 0.054 0.036 0.714 0.214 0.089 0.007 0.089 0.303 0.089 3.053 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop " � 178 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 x 1/////// 012 67e)l 1-5- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: LYNCHBURG OWNER: MILLIS PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 38.12 SITE #: NC BR 00348 FIELD# : BR 00348 0002 OPERATOR: SANDY MANSFIELD CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4.70 ACRES PERMITTED: 4.70 Page Lime Applied Date E allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppin) Crop MONTH Total Per Acre Solids 5/5/14 110.58 (W) 23.528 34.47 8.110 ADNG2&4: DRY 0-<1/2" SURIN 1.0 0.27 26,700. p 2,200.00 p 7.83 p 8823 SOYBEANS May-14 110.58 (W) 23.528 Total Gallons/Ac: Total Wet Tons/Ac: 23.53 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual ibs/acre 143 0.049 0.032 0.649 0.195 0.081 0.006 0.081 0.276 0.081 2.774 134.58 Cumulative lbs/acre 0.049 0.032 0.649 0.195 0.081 0.006 0.081 0.276 0.081 2.774 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop 156 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 p ( 1339.0 267.9 . 15.0 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: TOMAHAWK OWNER: ROBINSON PERMIT #: WQ0004500 ANNUAL DRY TONS APPLIED: 63.77 SITE #: NC BR 00356 FIELD# : BR 00356 0002 OPERATOR: FRANK HEWETT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 14.80 ACRES PERMITTED: 14.80 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 4/4/14 66.86 (W) 4.518 28.93 1.307 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 I SOYBEANS 4/7/14 153.58 (W) 10.377 28.93 3.002 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 29,000. p 1,940.00 p 2.77 p 9249 1 SOYBEANS Apr-14 1 220.44 (W) 14.895 Total Gallons/Ac: Total Wet Tons/Ac: 14.89 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre ' 0.026 0.017 0.310 0.086 0.043 0.003 0.043 0.129 0.043 1.224 81.10 80 Cumulative lbs/acre 0.026 0.017 0.310 0.086 0.043 0.003 0.043 1 0.129 0.043 1.224 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 -:. 1339.0 267.9 15.0) 375.0 89.0 2500.0 ADNG2&42:1 = ADM CORP.; NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 Xr�— (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: GOLDSBORO OWNER: DALE CLEMMONS PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 21.71 SITE #: NC,BR 00357 FIELD# : BR 00357 0004 OPERATOR: DALE CLEMMONS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.70 ACRES PERMITTED: 9.70 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/24/14 35,076.74 (G) 3616.159 14.84 2.238 ADNG3L MOIST 0-<1/2" SURIN 1.0 0.40 72,100.p 2,630.00 p 88.90 p 30507 BERMUDAGRASS Apr-14 1 35,076.74 (G) 3,616.159 Total Gallons/Ac: 3,616.16 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 0.013 0.009 0.031 0.040 0.022 0.002 0.022 0.022 0.022 0.054 37.55 137 Cumulative lbs/acre 0.013 1 0.009 1 0.031 1 0.040 1 0.022 0.002 0.022 1 0.022 0.022 0.054 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop � '" 299 FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 ' ADNG3L = ADM CORP., NC NITRO GRO 3 LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ARCHER DANIELS MIDLAND CORP., NC PREDOMINANT SOIL SERIES: FORESTON OWNER: CLYDE MOORE PERMIT #: W00004500 ANNUAL DRY TONS APPLIED: 135.44 SITE #: NC CO 00076 FIELD# : CO 00076 0004 OPERATOR: CLYDE MOORE CATION EXCHANGE CAPACITY (NON-503): ESIDUAL SOURCE(S):* See list at bottom of report OLD FIELD #: CO-76-4 ACRES UTILIZED: 53.00 ACRES PERMITTED: 53.00 Page : 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pp"') Crop MONTH Total Per Acre Solids 12/29/14 64.05 (W) 1.208 27.41 0.331 ADNG2&4: MOIST 0-<1/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 CORN 12/30/14 259.13 (W) 4.889 27.41 1.340 ADNG2&4: MOIST 0-<I/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 CORN 12/31/14 170.94 (W) 3.225 27.41 0.884 ADNG2&4: MOIST 0-41/2" SURIN 1.0 0.27 24,600. p 3,030.00 p 17.50 p 8871 CORN Dec-14 494.12 (W) 9.322 Total Wet Tons/Ac: 9.32 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.015 0.010 0.261 0.046 0.026 0.002 0.026 0.107 0.026 0.598 36.13 45 Cumulative lbs/acre 0.267 0.113 5.253 2.019 0.604 0.019 0.420 2.067 0.300 25.012 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 137 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8t`° 1339.0 267.9 15.0 375.0 89.0 2500.0 ° ADNG2&42:1 = ADM CORP., NC NITRO GRO 2&4 MIX, 2:1 MIX RATIO OF NG2 TO NG4 X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 •��u:;-y,'�ln F%' F�fa "•+i is Kti(;�y r.p,...,'5 Lisp ,! �n;: j}$r1 {'� ..;iJ��'�w '�'�'"'iM`��: a:,Y� 1txt' 1Yw1 i,�.= L: V-1ZZ A iNLe!�F} Client ADM 1730 East More St. South Port, NC 28461 Order Number 1400062 Project Number Ossued Tuesday, January 28, 2014 Total Number of Pages 13 (excluding C.O.C. and cooler receipt form) Approved By: it ��� 1, QA Manager Certifications: A2LAlDOD 0724,01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943. Idaho OH00923, Illinois 200061 and Reg.S, Indiana C-OH-13, Kansas E-10347,.Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Michigan (Reg.5), Minnesota 409711, Montana CERT0099; New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee:TN04018. Texas T104704466-11-5, Region 5 WG-15J, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont Vi'-87688, Virginia 06440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688. Wisconsin 399013010 ,.., , 'rift?n STFe L ram. ) e Fails,o- Glni442 3 u f; ':�,r-... .y v-i33L'1-�253-44?s Wet, Site: Cori? -- � Rev11�A��llil�@l�l�llllQ�ll(I�.1�il�ial11�1111i��llifli�il11I11 . 9-0 Date: 04/18/13 Order 1®: 1400062 COOLER Summit Environmental Technolog! Cooler Receipt Form - _...- - -- • - Initials of person Inspecting cooler and samples: h-K, Client Order Number����77TT� Date Received ( Time Received:�� ^ Number of Coolers/Bo , N/A Shipper. FED EX UPS DHL Airborne, Us Postal Walk-in Pi other. Packaging: Peanuts Bubble Wrap Paper Foam Other: Tape on cooler/box Y 0 NIA Custody Seals intact N NIA C-D-C in plastic Y NIA Ice Blue ice present / �Q lied NIA Sample Temperature 0 ,C N/A. Radiological Testing Y N If yes count per minute (�Y "Use 1 sheet persampie for Radiologlow Testing. If sample Es HOT, the RadioloWcal Safety officer must be notified immediately. 0-0-0 filled out properly l%Y N N/A - Samples in separate bags N NIA Sample containers intact' N NIA •If no, list broken sample(s): Sample label(s) Complete (ID, date, etc.) N N/A Label(s) agree with GO C N N/A Correct containers used N WA Sufficient sample received N NIA Bubbles absent from 40 mL vials" Y N A " Samples with bubbles less than the size of a pea are acceptable. Was client contacted about samples Y N Will client send new samples Y N Client contact DatetFime Logged in by Comments G\QC SHARED Document Control Templates . TraeldnglCocler receipt form Rev- 8.0 04-18-12,doe Page 1 of 2 6,0 Sample Summary Client: ADM Order Number: 1400062 2 Laboratory ID Client ID llilatrix Sampling Date 1400062-01 Q908 Effluent Liquid 1/8/2014 1400062-02 Yeast Cream Liquid 1/8/2014 1400062-03 NG2 Solid 1/8/2014 1400062-04 Q902 Liquid 1/8/2014 1400062-05 NG5 Solid 1/8/2014 1400062-06 Carbon Solid 1/8/2014 1400062-07 Gypsum Solid 1/8/2014 ? -,A, 0 0 o-z 44223 331E-253-821` ;Fax: 3. 11-2,r3- 449-S sl' tea! �F,r r•^`• tr`�� a,}, rtt;".}Fr,l +k 4tL';iy. rgp �s €Y&rtz �. L.�EC:n��wL QiE ,its?C. 3 Report Narrative Client: ADM Order Number: 1400062 Solid sample results are reported on a wet weight basis except as noted. No problems were encouritered during analysis of this order number, except as noted. Method numbers, unless specified as SM or ASTM, are EPA methods. Method of analysis for TCLP Volatiles is 1311/8260B Method of analysis for TCLP'Metals is 1311/6010B and 1311/7471A Method of analysis for TCLP BNA is 1311/8270C Data Qualifiers: B = Analyte found in the method blank J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ) C = Analyte has been confirmed.by another instrument or method E = Analyte exceeds the u - ' yt upper Limit of the calibration curve. Matrices: ' D = Sample or extract was analyzed at a higher dilution A =Air X = User defined data qualifier. C = Cream S = Surrogate out of control limits ' DW = Drinking Water U = Undetected L = Liquid a = Not Accredited by NELAC O = Oil F SL = Sludge ND = Non Detected at LOQ I SO = Soil OF = Dilution Factor €S =solid `T = Tablet TCLLimit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor jW =1iV =Wa Extract ste Water Limit Of Detection (LOD) =Method Detection Limit i W = Wipe Practical Quantitation Limit (FQL) = (same as LOQ) Method. Detection Limit (MDL) = (same as LOD) .......................__.......... . Reporting Detection Limit (ROL) = (same as LOD) Estimated uncertainty values are available upon request. The test results meet the requirements of the NELAC standard, except where noted. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot be reproduced in any form -without the consent of Summit Environmental Technologies, Inc. or the client for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. ArraiYklOai PrSte9.rf.;: En-4rr.��t;�r.�_s� - I�xEt.A� O�rtsK�d nn Cyfil a6l Z•yc f"a.i I S— hi0 4-44GG3 n. " borrbbe:.`t30-G.i.S•"L`` 11. Fax: 3J'13_!�`�•,;.:�_.. ... I VO--b Cite. io:"r Lao ". ago = W izO� -:i^� i �%.MT � i-ibX,L0103;S-*-,-F,,,C. January 28, 2014 Client: ADM Address. 1730 FastMore St. South Port,NC 28461 Received. 1/11/2014 Project #: N/A TCLP dofatiles Client ITJR Tab U39 Collected Anaivte Rep Lmt Result Units Matrix Method DF RepLA Run Anal Q903 Effluent 1400062-01 08 Jan-141,1-Dichloroethene 0.1 ND mg/L L 1311 1 0.7 24Jan-14 MS Q908 Effluent 1400062-01 08Jan-141,2-Dichlorcethane 0.1 ND mg/L L 1311 1 0.5 24-3an-14 MS Q908 Effluent 1400062-01 08-3an-142-Hu6none (MEK) 2 ND mg/L L 1311 1 200 24-Jan-14. MS Q908 Effluent 1400062-01 08Jan-14 Benzene 0.1 0.32 mg/L L 1311 1 0.5 24-Jan-14 MS Q908 Effluent 1400062-01 08-Jan-14 Carbon Tetrachloride 0.1 ND mg/L L 1311 1 0.5 24 Jan-14 MS Q906 Effluent 1400062-01 08 Jan-14 Chlorobenzene 0.1 'ND mg/L L 1311 1 100 243an-14 MS Q9D8 Effluent 1400062-01 08Jan-14 chloroform 0.1 ND mg/L L 1311 1 6 24-3an-14 MS Q908 Effluent 1400062-01 08 Jan-14Tetrachloroethene 0.1 ND mg/L L 1311 1 0.7 24-3an-14 MS Q908 Effluent 1400062-01 08Jan-14Trichioroethene 0.1 ND mg/L L 1311 1 0.5 24Jan-14 MS Q408 Effluent 1400062-01 08-Jan-14 Vinyl Chloride 0.2 ND mg/L L 1311 1 0.2 24Jan44 MS TCLP 81�1/y, -` Client TD # Tab Mg coIIectrd byte RepLmt Result Units Matrix Method DF ReoLvl Run Analyst Q908 Effluent 1400062-01 08-Ian-141,4-Dichlorobenzene 0.1 ND mg/L L 1311 1 7.5 21 Jan-14 AE Q908 Effluent 1400062-01 08-Jan-142,4,5-Trichlorophenol 0.25 ND mg/L L 1311 1 400 21Jan-14 AE Q908 Effluent 140OD62-01 0$ Jan-14 2,4,6-Tdchlorophenol 0.25 ND m91L L 1311 1 2 21-Jan-14 AE Q908 Effluent 1400062-01 08 Jan-14 2,4-Dinitrotoluene 0.1 ND mg/L L 1311 1 Q908 Effluent 1400062-01 08-Jan-14 Cresols 5 ND mg/L L 1311 1 0.13 21 Jan-14 AE Q908 Effluent 1400062-01 08Jan-14 Hexachloro-1,3-butediene 0.1 ND mg/L L 1311 1 20D Zi-Jan-14 AE Q908 Effluent 1400062-01 08 Jan-14 Hexachlorobenzene 0.1 ND mg/L L 1311 1 0.5 21-Jan-14 AE Q908 Effluent 1400062-01 08 Jan-14 Hexachloraethane 0.1 ND mg/L L 1311 1 0.13 21 Jan-14 AE Q908 Effluent 1400062-01 08-Jan-14 Nitrobenzene 0.1 ND mg/L L 1311 1 3 21-Jan-14 AE Q908 Effluent 1400062-01 08-Jan-14 Pentachlorophenol 0.25 ND mg/L L 1311 1 2 21 Jan-14 AE Q908 Effluent 1400062-01 08 Jan-14 Pyridine 0.25 ND mg/L 100 21-3an-14 AE L 1311 1 5 21 Jan-14 AE TCLP Arsenic Client Q908 Effluent Tab IDA 1400062-01 -ODU fed Analyse 08Ian-I4TCLP arsenic Rep Lmt Result Units Matrix Method DF R Lv[ "eZ"• A--- `mil 0.5 ND mg/L ! 1311 1 5 20 Jan-14 WK TCLP Bariurn -- Client IDS Q908 Effluent Tab ID 1400062-01 Coll 08-Jan-14TCLP Barium Rep Lmt Result Units Mahix Method DF Ree Lv_I Run Analyst 5 ND mg/L L 1311 1 100 20-Jan-14 WK TCLP Cadmium - - Cliesst IC3# Q9D8 Effluent Lab TD# 1400062-01 Collected na 08 Jan-14TCLP Cadmium R_ ep Lmt It !h is Matrix Method DF ReeLvi Run Ana 0.1 ND mg/L L 1311 1 1 20 Jan-14 WK TCLP Chromium Client iD Q908 Effluent LabIDT 1400062-01 Coll 08 Jan-14TCLP Chromium Rep Lmt Resak Units Matrix Method DF BggLA t' `" . O.Z ND _ mg/L L 1311 1 5 ZO Jan-14 WK TCLP (Lead` "" -------- Client TD# Q908 Effluent Lab 1400062-01 COHeeted Anal_nt 08 Jan-14 TCLp Lead Rep Lmt Result Units Matrix M hOd R_eaLV� AzM Ana 0.5 ND mg/L L 1311 1 5 20-Jan-14 WK Page 4 �6??"�5}Y':,�.Gi i1h�ES�;•i{-r,+�• , o`,.a'•� 1: V�Yie,QN c �']iC: '1 33 Lr"sz a w2r vtF ai?C�^a FaflS, 0)11'- _.=2o ert"O%e: 33-G7: ^8i _ ?~dk: Lvfr%^-.s'•8a LOW1,1Y.Setiek.Ct ym. �r11�++i�' ,t . IFS fa (Y.'.rlc z: q,.. Mi'+:,(ry^•�t.-p "�A�-s _..., is ` •L• 'f �;LAI 4, °L- ;_:'r ii~ix✓r;n €s?LuE;Ti': TEC:'r<!yC°f3€F, rlty January 28, 2014 _.-.. Client: ADM Address: 1730 East More St. South Port, NC 28461 Received:1111/2014 Project 4: N/A TCLP Mercury Client ID# Lab ID# Collected Anaa Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Q908 Effluent ` 1400062-01 08-Jan-14 TCLP Mercury _. 0.002 NO .._ - ____ mg/L -- L �.._, 1311 1 0.2 20 Jan-14 ALJ TCLP S® _ ....._ .__•_-- -•---- Client iD# LabTD# Collected Analyse Re Lmt Result Units Matrix Method F_ RegLvl ]tam Analyst Q908 Effluent 1400062-01_ 08 Jan-14 TCLP Selenium _ 0.5 NO - mg/L L 1311 1 1 20 Jan-14 WK - TCLP Silver Client ID# Lab ID# Collected AnalZ Rep Lm Result Units Matrix Method DF ReoLvl Rug Analyst Q908 Effluent 1400062-01 08 Jan44 TCLP Silver 0.5 NO mg/L L 1311 1 5 20-3an-14 WK TCLP volatiles Client W# Lab D# Collec ed Analyse Rep Lm Result Units Matrix Method DF Re Lvl Run Yeast Cream 1400062-02 08-Jan-141,1-Dichloroethene 0.1 ND mg/L L 1311 1 0.7 21-Jan-14 MS Yeast Cream 1400062-02 08-Jan-141,2-Dichloroethane 0.1 NO mg/L L 1311 1 0.5 21-Jan•14 MS Yeast Cream 1400062-02 08 ]an-14 2-Butanone (MEK) 2 NO mg/L L 1311 1 200 21-Jan-14 MS Yeast Cream 1400062-02 08 Jan-14 Benzene 0.1 NO mg/L L 1311 1 0.5 21-Jan-14 MS Yeast Cream 1400062-02 08-Jan-14 Carbon Tetrachloride 0.1 ND mg/L L 1311 1 0.5 21-3an-14 MS Yeast Cream 1400062-02 08-Jan-14 Chlorobenzene 0.1 NO mg/L L 1311 1 100 21-Jan-14 MS Yeast Cream 1400062-02 08 Jan-14 Chloroform 0.1 NO mg/L L 1311 1 6 21 Jan-14 MS Yeast Cream 1400062-02 08Jan-14Tetrachloroethene 0.1 NO mg/L L 1311 1 0.7 21 Jan-14 MS Yeast Cream 1AM062-02 08 Jan-14Trichioroethene 0.1 ND mg/L L 1311 1 0.5 21 Jan-14 MS Yeast Cream 1400062-02 08 Jan-14 Vinyl Chloride 0.2 NO mg/L L 1311 1 0,2 21-Jan-14 MS TCLP BNA W�, -- Client JD# Lab ID# Collected An_ al +te Rep Lm t Result Uxnit , Matrix Method DF RegUd Ruo Anal_�st Yeast Cream 1400062-02 08-Jan-141,4-Dichlorobenzene 0.1 NO mg/L L 1311 1 7.5 21 Jan-14 AE Yeast Cream 1400062-02 08-Jan-14 2,4,5 Trichlorophenol 0.25 NO mg/L L 1311 1 400 21 Jan-14 AE Yeast Cream 1400062-02 08-Jan-14 2,4,6-Tr[rhlorophenol 0.25 ND mg/L L 1311 1 2 21 Jan-14 AE Yeast Cream 1400062-02 08 Jan-14 2,4-Dinitmtoluene 0.1 NO mg/L L 1311 1 0.13 21 Jan-14 AE Yeast Cream 1400062-02 08 Jan-14 Cresols 5 NO mg/L L 1311 1 200 21-Jan-14 AE Yeast Cream 1400062-02 08 Jan-14 Hexachloro-1,3-butadiene 0.1 NO mg/L L 1311 1 0.5 21-Jan-14 AE Yeast Cream 1400062-02 08-Jan-14 Hexadllorobenzene 0.1 NO mg/L L 1311 1 0.13 22 Jan-14 AE Yeast Cream 1400062-02 08-Jan-14 Hexachiorpethane 0.1 NO mg/L L 1311 1 3 21 Jan-14 AE Yeast Cream 1400062-02 08-Jan-14 Nitrobenzene 0.1 NO mg/L L 1311 1 2 21 Jan-14 AE Yeast Cream 1400062-02 08-Jan-14 Pentachiorophenol 0.25 NO mg/L L 1311 1 100 21 Jan-14 AE Yeast Cream 1400062-02 08-Jan-14 Pyridine 0.25 NO mg/L L 1311 1 5 21-Jan-14 AE TCLP Arsenic _ ClientID# Lab IIJ# Coll ect Anatvte Rep Lm t Result Units Matrix Method DE RegLvl Run gnatvst Yeast Cream 1400062-02 08-Jan-14 TCLP Arsenic 0.5 NO mg/L L 1311 1 5 20-Jan-14 WK TCLP RiAurn Client iA# lab TD # Collected Ana}yte Rep Lmt Result Units Matrix Method DF RegLvl Run Aualvst Yeast Cream 1400062-02 08Jan-14 TCLP Barium 5 NO mg/L L 1311 1 100 20Jan-14 WK Page 5 EPA Cerl9Yie i pg et"xP SSE (tri C`uVafl0Q-a Falls, 0-l€0 44223 s "PlIo se:: 330-•2E3-8211 - cox: 330 ,26?-4489 Web Site: wofwseitek.aorr, Jautiary 28, 2014 Client ADM Address: 1730 Fast More St South PoM NC 28461 Received: I/11/2014 Project it: N/A TCLP Cadmium Client LDf' Lab W Co Ieeted Analnte Rep Lmt Result U— Matdx Method AF Re Lvl - Run An Yeast Cream 1400062-02 -08 Jan-114 TCLP Cadmium _ - _ 0.1 ND mg/L L 1311 1 1 20-Jan-14 V1/K TCLP Chromium Client II3a*' Lab IIJM Collected A.nalvte Rep Lmt Result Units Matrix M tLod DF RegLyl Run Awl Yeast Cream 1400062-02 08Jan-14TCLP Chromium 0.2 ND '•---- - mg/L L 1311 1 5 20 Jan-14 WK TCLP Lead - - - --- -- _. _ _� Client 1 Yeast Cream Lab IDS Collect Analyte Rep Lmt Result Units Matrix Method F_ ReabA R �`' ' 1400062-02 08 J an-JanTCLP Lead 0.5 ND mg/L L 1311 1 S 20 Jan-14 WK VVK TCLP W;r- ry Client mg Yeast Cream Lab l7 Co eeted A.vte Rep Lmt Result Units Matrix Method PF ReoLvl Aral 1400062-02 08 Jan-14 TCLP Mercury - 0.002 ND mg/L L 1311 1 0.2 - 20 Jan-14 ALJ TCLP Se Client IITf# Lab IlDI, Collected A.ua1vtE� Rep Lmi Result Units Matrix Method DF RenLvl Run Yeast Cream 1400062-02 08 Jan-14 TCLP Selenium 0.5 ND mg/L L n� 1311 1 1 20Jan-14 WK TCLP Silver Beat III Yeast Cream Lab M4 1400062-02 C0l1xte3 Analyte 08 Jan-14 TCLP Silver Rep Lmt es -it UnAs Matrix Method DF RegLvl Run Anaivst 0.5 ND mg/L L 1311 1 5 20-3an-14 WK TCLP Vointiies -- Client IIiR NG2 Lab M# 140OD62-03 Collected An a Pe Lmi .Result 0_ Units ma's Meta DF Rea7vi Rua Analyst 08Jan-Jan-Dichloroethene 0.1 ND mg/L S 1311 2 0.7 NG2 1400062-03 08 Jan-141,2-D1chloroethane 0.1 ND mg/L 3 21 Jan-14 MS NG2 1400052-03 08 J� an-Jan2-Butanone (ME 2 ND mg/L S 1311 1311 1 0.5 21Jan-JanMS NG2 M0062-03 06Jan-14 Benzene 0.1 ND mg/L S 1311 1 200 21-Jdn-14 MS NG2 1400062-03 08 Jan-14 Carbon Tetrachloride 0.1 ND mg/L S 1 05 21 Jan-14 MS NG2 1400062-03 08 Jan-14 Chlorobenzene 0.1 ND mg/L S 1311 1311 1 0.5 21 Jan-14 MS NG2 1400062 t13 08 Jan-14 ChloraForm 0.1 ND mg/L S I 100 21 Jan-14 MS NG2 1400062-03 08Jan-14Tetrachloroethene 0.1 ND mg/L S 1311 1311 1 6, ' 21 Jan-14 MS NG2 1400062-03 08 Jan-14Trichloroethene 0.1 ND mgl: S 1311 1 0.7 21-Jan-14 MS NG2. 1400062-03 08 Jan-14 Ynyl Chloride 0 2 ND 1 0.5 2I Jan-14 MS mg/L S 1311 1 0.2 21-Jan-14 MS . Page 6 11��in "Ar4a.f 'dsual hritagrity- . EPA Cereifiied, - I_ AP �S•�rff� a 3510 Cuyahoga Fall's. wh���c• C 4223 0 .p'%i�,cC-:UUSS",n,,53-4%'1, emu. ;ten nw: lii✓', k�' h. {','•t?il"F,�,•,i� 'i" .� 'k4 'i' L•�+tj-.yz.•J tri ii b3 r`iC: J ,:C+S ,il tii,; r.�.i January 28, 2014 Client: ADM Address: 1730 East More St. South Port, NC 2846I Received:1/11/2014 Project #: N/A TCLP BNA Client lD# Lab ID# Collected An_ alvte Rep Lmt Result Units MaOix Method DF ReaLyl Run /raw NG2 1400062-03 08-3an-141,4-Dichlombenzene 0.1 ND mg/L S 1311 1 7.5 21-Jan-14'AE NG2 1400062-03 08-Jan-14 2,4,5-Trichlorophenot 0.25 ND mg/L S 1311 1 400 21-3an-14 AE NG2 1400062-03 08-Jan-14 2,4,6-Trichlorophenol 0.25 ND mg/L S 1311 1 2 21-Jan-14 AE NG2 1400062-03 08-Jan-14 2,4-Dinitrotoluene 0.1 ND mg/L 5 1311 1 0.13 21-Jan-14 AE NG2 1400062-03 08-Jan-14 Cresols 5 ND mg/L S 1311 1 200 21Jan-14 AE NG2 1400062-03 08-Jan-14 Hexachlorc-1,3-butadiene 0.1 ND mg/L S 1311 1 0.5 21-Jan-14 AE NG2 1400062-03 08-Jan-14 Hexachlorobenzene 0.1 ND mg/L 5 1311 1 0.13 21 Jan-14 AE NGZ 1400062-03 08 Jan-14 Hexachloroethane 0.1 ND mg/L S 1311 1 3 21Jan-14 AE NG2 1400062-03 08-Jan-14 Nitrobenzene 0.1 ND mg/L S 1311 1 2 21-Jan-14 AE NG2 1400062-03 08 Jan-14 Pentachlorophenol 0.25 ND mg/L S 1311 1 100 21-Jan-i4 AE NG2 1400062-03 08 )an-114 Pyridine, _ 0.25 ND mg/L S 1311 1 5 21-Jan-14 AE TCLP Arsenic _ Client ID# Lab 1134 Collected Analyte Rep Lm Resort Units Matrix Method DF ReaLyl Run Analyst NG2 1400062-03 08-Jan-14TCLPArsenic 0.5 ND mg/L S 1311 1 5 20-Jan-14 WK TCLP Barium Client Lab ID# Callened Anal ReQ Lmt Result Units Matrix Method DF RmLvl Run Analyst NG2 1400062-03 08-Jan-14 TCLP Barium 5 ND mg/L S 1311 1 100 20-Jan-14 WK 'PCLP Cadmium Client lB# Lab ID# Collect AnRep Lmt Result Units Matrix Method DF Ret7Lyl Rua Analyst NG2 _ 1400062-03 08-Jan-14 TCLP Cadmium_ 0.1 ND mg/L ~— S 1311 1 1 20-Jan-14 WK TCLP Chromium Client ID# ,Lab IU# Collected 1 Rep Lmt Result Units Matrix Method DF RegLvi Ran . Analyst NG2 1400062-03 08-Jan-14 TCLP Chromium 0.2 ND mg[L S 1311 1 5 20-Jan-14 WK TCLP Lead - Client lYJ# Lab IIX# Collected AnaRep Lmt Result Units Matrix Method DF Re4Lyl Run Anal t NG2 1400062-03 08`Jan-14 TCLP Lead _ OS ND mg/L S 1311 1 5 20-Jan-14 WK TCLP lM7ercury Client ID# iLab M# Collected Analyte Rep Lmt Result Units Matrix Method . D 9MLyl Run Anal t NG2 1400062-03 08-Jan-14 Mercury 0,002 ND mg/L S 1311 1 0.2 20-3an 14 AL7 TCLP Se Client ID# Lab ID# Collected An ty�e Rep Lmt Result Units Matrix Method DF ReaLyt Run Analyst NG2 1400062-03 08-Jan-14TCLP Selenium 0.5 ND mg/L S 1311 1 1 20-Jan-14 VVK TCLP Silver CiieatID# lab III# Callected Analyte Rep Lmt ,Result Units Matrix Method DF RegLvl Run ai _ NG2 1400062-03 08-Jan-14 TCLP Silver 0.5 ND mg/L S 1311 1 5 20 Jan-14 WK Page 7 't�.fWY-t#Cal ?l'i egC city- EPfi=, Ceftified AlELi�P l...wt'-0iied '.�_p. !;<-2F� c r`1c; _2: �,?i0-e53^821� Fax: 330-253-F .�: M Y7!- i 1•�^+. �•^Y �.^n mn, h� • �`C<ti:!:{'<�%,��T:k.�,9.^ 1'`c�`•.'%i-,�i�`;4 fir:; MT ��. ts:Tr .�•-, y.p". „� 4n..-r•.w.'t•^: L`�� €izv- January 28, 2014 Client ADM Address: 1730 East More St. South Port, NC 28461 Received:1/11/2014 Project #: N/A TCLP Volatiles Cheat Lab ID# Collected Anal Rep Lmt Result Units Matrix Method DF ReaLvl Run Q902 1400062-04 08 Jan-141,1-Dichlomethene 0.1 ND mg/L L 1311 1 0.7 24-3an-14 MS Q902 1400062-04 08 Jan-141,2-Didlloroethane 0.1 ND mg/L L 1311 1 0.5 24-Jan-14 MS Q902 1400062-04 08-Jan-14 2-Butanone (MEK) 2 ND mg/L L 1311 1 200 24 Jan-14 MS 0902 1400062-04 08 Jan-14 Benzene 0.1 0.15 mg/L L 1311 1 D.5 24-Jan-14 MS Q902 1400062-04 08-Jan-14 Carbon Tetrachloride 0.1 ND mg/L L 1311 1 0.5 24-Jan-14 MS .Q902 1400062-04 08Jan-14Chlorobenzene 0.1 ND mg/L L 1311 1 100 24Jan-14MS Q902 1400062-04 08-Jan-14 Chloroform 0.1 ND mg/L L 1311 1 6 243an-14 MS Q902 140G062-04 08Jan-14Tetrachloroethene 0.1 ND mg/L L 1311 1 0.7 24.3an-14 MS Q902 1400062-04 08-3an-14Triddtloroethene 0.1 ND mg/L L 1311 1 0.5 243an-14 MS Q902 - 1400062-04 08Jan-14Yrtyl Chloride 0.2 ND _ mg/L L 1311 I 0.2 24-Jan-14 MS Client ID#p Lab lD# coil A, Rep Lmt Result Units matrix Method DF R%LL Run Analn Q902 1400062-04 08-Jan-141,4-Dichlorobenzene 0.1 ND mg/L L 1311 1 7.5 21-2an-14 AE Q902 1400062-04 08-)an-142,4,5-Trichlorophenol 0.25 N❑ mg/L • L 1311 1 400 213an-14 AE Q902 1400062-04 08-Jan-142,4,6-Trichlorophenol 0.25 ND mg/L L 1311 1 2 21 Jan-14 AE Q902 1400062-04 08 Jan-14 2,4-Dinitrotoluene 0.1 ND mg/L L 1311 1 0.13 21 Jan-14 AE Q902 1400062-04 08 Jan-14 Cresols 5 ND mg/L L 1312 1 200 21Jan-14 AE Q902 140DO62-04 08 Jan-14 Hexachloro-1,3-butediene 0.1 ND mg/L L 1311 1 0.5 21Jan-14 AE Q902 1400062-04 08Jan-14 Hex achlorobenzene 0.1 ND mg/L L 1311 1 0.13 Jan-14 AE Q902 1400062-04 013 Jan-14 Hexachloroethane 0.1 ND mg/L L 1311 1 3 .21 21-3an-14 AE Q902 1400062-04 08-Jan-14 Nitrobenzene 0.1 ND mgJL L 1311 1 2 21 Jan-14 AE Q902 1400062-04 08 Jan-14 Pentachlorophenof 0.25 ND mg/L L 1311 1 100 21 Ian-14 AE Q902 1400062-04 08 Jan-14 Pyridine 0.25 ND mg/L L 1311 1 5 21Jan-14 AE TCLP Arsenio - Client Fb# 1ab 2I3# Collected Ana to Rea Lmt Result Units Matrix Method DF ReaLvi p t Q902 1400062-04 08-Ian-14TCLP Arsenic 0.5 ND mg/L L 1311 ,R�M i 5 20-3an-14 WK TCLP laarlum-- Client Lab )I3# Collected AaaI a Rep Lm Result 11-its Yfauix Meth DF RegLvl Run 4naI rt Q902 1400062-04 08-Jan-14TCLP Barium 5 ND mg/L L 1311 1 100 20Jan-14 VVK TCL! Cadmium Client E34 Q902 Lab 1400062-04 Collect 08 Jan-14 TCLP Cadmium Rep Lmt Result Units MEtril diet O DF R eglvl Run 0.1 ND _ mg/L L 131I 1 1 20 Jan-14 WKiC TCLP ditromlum Client lD# Q902 Lab 1D# 1400062-04 Coflecfad Anal +Lte 08-Jan-14TCLP Chromium Rep Lmt Result 0.2 ND Units Nftttix -� mg/L L Method 1311 D.,,F ReoLvl 1 5 Rim Analvs 20-Jan-141NK TCLP Lead - Climt iI}# Q902 Lab B39 1400062-04 Collected Analz 08-Jan-14TCLP Lead Rep Lmt Result 05 ND Units Matrix mg/L- L Mgdwd 1311 DF ReaLv( 1 5 R final 20.Jan_14 WK Page 8 Fax: pr. Al Ilk LAN EE k, January 28, 2014 Client: ADM Address: 1730 East More St. South Port, NC 28461 Received. 1111/2014 Project #-N/A TCLP Mercury client Lab DD# Collected An_ aiyte RepLmt Result Units Matrix Methad DF ReqLvi Run An alyt Q902 1400062-04 08-Jan-14 TCLP Mercury 0.002 ND Mg/L' 1 L 1311 1 0.2 20-Jan-14 AU TCLP Se Client 1D# Lab M4 Collected Ana a Rein Lmt Result Units Matrix Method DF RffiLVI Run Anal�t Q902 1400062-04 08-Jan-14 TCLP Selenium 0.5 ND mg/L L 1311 1 1 20-Jan-14'VVK TCLP Silver Client M# Lab 7 Collected Anal Rep Lmt Result Unks Matrix Method Metho X ReqLvl Run Analy Q902 1400062-04 08-Jan-14 TCLP Silver 0.5 ND mg/L L 1311 1 5 20-Jan-14 WK TCLP Volatiles Client M# I-ab M# Co lected Anal to Rep Lmt RgsWt unitsMatrix metho - DF ReqUd Egg An NGS 1400062-05 08-3an-14 1,1-Dichlornethene 0.1 ND mg/L S MI 1 0.7 21-Jan-14 MS NG5 1400062-05 08-Jan-14 1,2-Dichbroethane 0.2 ND mg/L S 1311 1 OZ 21-Jan-14 MS NGS 1400062-05 08-Jan-14 2-Butanone (MEK) 2 ND mg/L S 1311 1 200 21-Jan-14 MS NGS 1400062-05 08-Jan-14 Benzene 0.1 ND mg/L S 1311 1 0.5 21-Jan-14 MS NG5 1400062-05 08-Jan-14 Caton Tetrachloride 0.1 ND mg/L S 1311 1 0.5 21-Jan-14 14S NGS 1400062-05 08-Jan-14 Chbrobenzene, 0.1 ND mg/L S 1311 1 100 21-Jan-14 MS NGS 1400062-05 08-Jan-14 Chloroform 0.1 ND mg/L S 1311 1 6 21-Jan-14 MS NG5 1400062-05 08-Jan-14 Tetrachlomethene 0.1 ND mg/L S 1311 1 0.7 21-Jan-14 MS NGS 1400062-05 08-Jan-14 Trichloroethene 0.1 ND mg/L S 1311 1 0.5 21-Jan-14 MS NG5 1400062-05 08-3an-14 Vinyl Chloride 0.2 ND mg/L S 1311 1 0,2 21-3a.n-1.4 MS TCLP DNA client M# Lab 104 Collected Analyte Rep Lrn - Result Units Mavix Method DF ReqLvJ Rums Aoky� NG5 1400062-05 08-Jan-14 1,4-lXichlorobenzene 0.1 ND mg/L S 1311 1 7.5 21-Jan-14 AE NGS 1400062-05 08-Jan-14 2,4,5-Trichlomphenol 0.25 ND mg/L S 1311 1 400 21-Jan;.14 AE NGS 14000,62-05 08-Jan-14 2,4,6-Trichlomphenol 0.25 ND mg/L s mi 1 2 21-Jan-14 AE NGS 1400062-05 08-Jan-14 2t+Dinlitrotoluene 0.1 ND mg/L S 1311 1 0.13 21-Jan-14 AE NGS 1400062-05 08-Jan-14 Cresols 5 ND mg/L S 1311 1 200 21-Jan-14 AE NGS 1400062-05 08-Jan-14 Hexachloro-1,3-butadiene- 0.1 ND mg/L 5 1311 1 0.5 21-Jan-14 AE NGS 1400062-05 08-Jan-14 Hexachlcrobenzene 0.1 ND mg/L S 1311 1 0.13 21-Jan-14 AE NGS 1400062-05 08-Jan-14 Heiachloroethane 0.1 ND mg/L S 1311 1 3 21-la'n-14 AE NGS 1400062--05 08-lan-14 Nitrobenzene 0.1 ND mqIL S 1311 1 2 21-3an-14 AE NGS 1400062-05 08-lan-14 Pentachlorophenol 0.25 ND mg/L S 1311 1 100 21-Jan-14 AE NGS 1400062-05 - 08-Jan-14 Pyridine 0.25 ND mg/L S 1311 1 5 21-Jan-14 AE TCLP Arsenic Client Lab W# Cogee An Rep Lmt Result Units Matrix Method DF Requi Run NGS 1400062-05 08-3a - n-14 TCLP Arsenic 0.5 ND mg/L S 1311 1 5 2 O-Jan-14 WK TCLP Barluin Client ID9 lab M# Collected Anal Rep Lmt Result Units Matrix Method DF ReqLVl Run AW NG5 1400062-05 08-lan-14 TCLP Barium 5 ND mg/L S 1311 1 100 20-Jan-14 WK Page 9 EPA 4 x AP C COrNifted. - NELP cuy-at-,oge FeRs, Oh;o 44-223 Q P None. Z30253-82,11 'Pax-, 11,16b SiTe: o,,ww seften' coni (w °ids.. �3•^ '� . rM l. d S, ? rauuary 28, 2014 Client: ADM Address: 1730 East More St South Port, NC 28461 Received:1/11/2014 Project #: N/A TGLP Cadmium Client ID# lab ID# Collected Anal t Reo Lmt L---c Units Matrix Method DF RMLvI jim gnyl�yt NG5 , 1400062 O5 08 Jan-14 TCLP Cadmium _ 0.1 ND ^— _ mg/L S 1311 1 1 20 Jan-14 WK TCLP Chromium Client ED Collected Anal to Rep Lmt Rewdt ni Matrix Merhod DF ReaLvi itun pnal NG5 1400062_05 08 Jann-14TCLP Chromium 0.2 ND _._. __ mg/L _ — — S 1311 1 5 20 Jah-14 VVVKK TCLP Lead -- •_ __-�_.__. _ _ Client NG5 Lab RepLmt Result Units Matrix Method DF ReqLvI gun `l 1400062-05 084Jan-14TCLP Lead 0.5 ND mg/L S ' 1311 1 T 5 20 Jan-14 WK TCLP'&f e-r ury Client IIY` Lab M# Collated Analvtc Rep Lmt Resu@ Units lMaat = Medwd DF Re Lvl R Analvsi NG5 _ 1400062-05 08-Jan-14 Mercury rY _ 0.002 ND mg/L S 1311 1 --4 0.22 � 20-]an-14 AU TCLP So - Client IIT# NG5 lab II2# CoIIoeted Aeal�rte Rey Lmt Reswt 111M Matrix DF R Lvl �� Am Aaat° 1400062-05 08-Jan-14 TCLP Selenium 0.5 ND mg/L S 1311 1 1 20 Jan-14 WK TCLP Silver Client 1 NG5 lab ID# Collected An to Rep,Lmt Resait Umts Matnx Method M ReoL l —` Run -. 1400062-05 08 Jan-14 TCLP Silver 0.5 ND mg/L 5 1311 1 5 20-Jan-14 VVK K Tc .p Volatiles Client II]x Carbon Lab MO Coll Rep Lmt esat Um�is Mahix Method DF ftW 1'u�m Aaaiy�t 1400062-06 08-Jan-141,1-Dichioroethene 0.1 ND mg/L S 1311 1 0.7 Carbon 1400062-06 08-Jan-141,2-pichloroethane 0.1 ND mg/L S 21 Jan-14 MS Carbon 1400062-06 08-3an-142-Butanone (MEK) 2 ND mg/L S 1311 1311 1 0.5 21 Jan-14 MS Carbon 1400062-06 08 Jan-14 Benzene 0.1 ND mgJL 5 1 200 21Jan-14 MS Carbon 1400062-06 OS Jan-14 Carbon Tetrachloride 0.1 ND 1311 1 0.5 21 Jan-14 MS Carbon 1400062-06 08 Jan-14 Chlorobenzene 0.1 ND mg/L mg/L 5 S 1311 1 0.5 21Jan-14 MS Carbon 1400062-06 08-Jan-14 Chlorofbr n 0.1 ND S 1311 1 100 21-Jan-14 MS Carbon 1430062-06 08-Jan-14Tetrachloroethene 0.1 ND mg/L mg/L S 1311 1311 1 6 21Jan-14•M5 Carbon 1400062-06 OB Jan-14 Ttichloroethene 0.1 ND mg/L S 1 0.'7 21 Jan-14 MS Carbon 1400062-06 08-Jan-14 Ynyl Chloride 0.2 ND mg/L S 1311 1 0. 5 21 Jan 14 M5 1311 1 0.5 21 Jan-14 MS Page 10 r�Ss?s^ 3Ec^ d ,29-0 - "' - ;"`.^°�rPA Ozr':;' az' C EiI� uryo 4sc_,e Fal:s, 11ia 4?Dt 2c3 3?�e: 33D-2S -Sc Fa--: 33i�-^r_'33-'44.89 9 '^, S-Veb ifE: 'vsfRl#FIJ.�+3i�C ^Cf3r I Kh .. .l..;r�{;i ss, .}.I.T., w:;7;..5•" t;µ r• January 28, 2014 Client: ADM Address. 1730 East More St. South Port, NC 28461 Received:1/11/2014 Project #: N/A TCLP DNA Client ID# Cab ID# Collected Analyte Rep Lmt Result Units Maisix Metbad DF RegLvl Run Ana1v Carbon 1400062-06 08 Jan-14 1,4-Dichlorobenzene 0.1 ND mg/L S 1311 1 7.5 21 Jan-14 AE Carbon 1400062-06 08 Jan-14 2,4,5-Trichlorophenol 0.25 ND mg/L S 1311 1 400 21 Jan44 AE Carbon 1400062-06 08 Jan-14 2,4,6 Trichlorophenol 0.25 ND mg/L S 1311 1 2 21 Jan-14 AE Carbon 1400062-06 08 Jan-14 2,4-Dinitrotoluene 0.1 ND mg/L S 1311 1 0.13 21 Jan-14 AE Carbon 1400062-06 08 Jan-14 Cresols 5 ND mg/L S 1311 1 200 21 Jan-14 AE Carbon 1400062-06 08-Jan-14 Hbxachloro-1,3-butadiene 0.1 ND mg/L S 1311 1 0.5 21-Jan-14 AE Carbon 1400062-06 08-Jan-14 Hexachlorobenzene 0.1 ND mg/L S 1311 1 0.13 21-Jan-14 AE Carbon 1400062-06 08-Jan-14 Hexachloroethane 0.1 ND mg/L S 1311 1 3 21-Jan-14 AE Carbon 1400062-06 08-Jan-14 Nitrobenzene 0.1 ND mg/L S 1311 1 2 21-Jan-14 AE Carbon 1400062.06 08-Jan-14 Pentachforophenol 0.25 ND mg/L S 1311 1 100 21-Jan-14 AE Carbon -- _ 1400062-06 08-Jan-14 Pyridine— - 0.25 ND _ w mg/L S 1311 1 5 21-Jan-14 AE TCLP Arsenic Client al) ID# Collected Anal a Rep Lmt Real Units Matrix Method DF RegLvl gun Carbon 1400062-06 08-Jan_14 TCLP Arsenic - 0.5 ND - — mg/L S 1311 1 5 20-Jan-14 WK TCLP Barium Cheat La---b Mf Collected An Rep Lmt Result Units Matrix Metbod DF ReaLv1 Run Analyst Carbon 1400062-06 08-Jan-14TCLP Barium 5 ND - mg/L S 1311 1 100 ZOJan 14 WK TCLP Cadmium client ID# Lab IDS Callected Analvte Rep Lmt E-emilt Jhgq Matri Method DF R_ g-Lyl Rus ArW t Carbon - 1400062-06 08 Jan-14 TCLP Cadmium 0.1 ND mg/L S 1311 1 1 20-Jan-14 WK TCLP Chromium -- - Client ID# lab M# Collected Ana -late Rep Lmt Result Units Matrix Method DF ReaLvf Run Analyst Carbon 1400062-06 08-Jan-14TCLP Chromium 0.2 ND mg/L S 1311 1 5 20-Jan-14 WK -- TCLP Load - Meat ID# Lab MA Collected Anal rLte Rep Lmt Result Units Matrix Method DF RegLvl Run qngt Carbon - - 1400062-06 08-Jan _14 TCLP Lead _- 0.5 ND mg/L S 1311- 1 5 20 Jan-14 WK w TCLP Mercury - - Client lD# Lab coil Anal Rea Lmt Result Units Matrix Method DF RegLvl Run And Carbon 1400062-06 OS Jan-14 Mercury 0.002 ND mg/L S 1311 1 0.2 20-Jan-14 ALI TCLP So Client 113# Lab M# Collected Anal vte Rep Lmt Result Units Matrix Method if ReoLA Run Anal st Carbon 1400062-06 08-Jan-14TCLP Selenium 0.5 ND mg/L S 1311 1 1 20-Jan-14WK TCLP Sliver Cheat IIJi{ Lab iD# Collected Anal- rite Rep Lmt Result Units Matrix Method D1; RegLvl Run gn�lvst Carbon 1400062-06 08-Jan-14 TCLP Silver 0.5 ND mg/L S 1311 . 1 5 20 Jan-14 WK Page I i EPA cv,`.`K'e-`d - NE LAP.'? 4 ' 3310. is K?ah)✓"a -a S7 ��2' e ryl_y7c-: J;0-2-i-j2a �2'37 Fax: �•'�.^i3-'r }VIVP-h Slit:. v,,,V'WSe.ff JtixO,7-i 1 AA..3i F A. • 'l-:Nn"h,'.•-4'�j-:« 9Y I,sA f^! A January28, 2014 _... _ ...• , r� ` Client ADM Address: I730 East More St South Port, NC 28461 Received' 1/11/2014 Project #: N/A TCLP Holatlles cuenz 1}]# Lab 1Tl# Collected Aaatvte Rep Lmt Result Units Matrix .Method DF RaQLvl Run ppgvst Gypsum 1400062-07 08Jan-141,1-Dichtoroethene 0.1 ND mg/L S 1311 1 0.7 21 Jan-14 MS Gypsum 1400062-07 38 Jan-141,2 Dichloroethane 0.1 ND mg/L S 1311 1 0.5 21-3an-14 MS Gypsum 1400062-07 08-Jan-14 2-Butanone (MEK) 2 ND mg/L S 1311 1 200 21-Jan-14 MS Gypsum 1400062-07 08 Jan-14 Benzene 0.1 ND mg/L S 1311 1 0.5 21 Jan-14 MS Gypsum 1400062-07 08 Jan-14 Carbon Tetrachloride 0.1 ND mg/L S 1311 1 IS 21 Jan-14 MS Gypsum 1400062-07 08 Jan-14 Chlorobenzene 0.1 ND mg/L S 1311 1 100 21-3an-14 MS Gypsum 1400062-07 08-Jan-14 Chloroform 0.1 ND mg/L S 1311 1 6 21 Jan-14 MS Gypsum 1400062-07 08-Jan-14Tetrachloroethene 0.1 ND mg/L 5 1311 1 0.7 21-Jan-14 MS Gypsum 1400062-07 08 Jan-14Trichloroethene 0.1 ND mg/L S 1311 1 0.5 21-Ian-14 MS Gypsum �- 1400062-07 08 Jan-14 Vinyl Chloride _ _ -. 0.2-ND mg/L S 1311 1 0.2 21-Jan14 MS TCLP BMA - - Client lll# Lab Rep_Lmt Result Untta Matrix Method DF ReaLvl Rnm Analvs[ Gypsum 1400062-07 08-3an-141,4-Dichlorobenzene 0.1, ND mg/L S 1311 1 7.5 21Jan-14 AE Gypsum 1400062-07 08 Jan-14 2,4,5 Trichlorophenol 0.25 ND mg/L S 1311 1 400 21 Jan-14 AE Gypsum 1400062-07 08Jan-14 2,4,6 Trichlorophenol 0.25 ND mg/L S 1311 1 2 21-Jan-14 AE Gypsum 1400062-07 08-Jan-14 2,4-DWa rotaluene 0.1 ND mg/L S 1311 1 0.13 21 Jan-14 AE Gypsum 1400062-07 08-3an-14 Cresols 5 ND mg/L S 1311 1 200 21-Jan-14 AE Gypsum 1400062-07 08 Jan-14 Hexachloro-43-buYadigne 0.1 ND mg/L S 1311 1 0.5 21Jan-14 AE Gypsum 1400062-07 08-Jan-14 Hexachlprobenzene 0.1 ND mq/L S 1311 1 0.13 2IJan-14 AE Gypsum 1400062-07 08 Jan-14 Hexachioroethane 0.1 ND mg/L 5 1311 1 3 21 ]an-14 AE Gypsum 1400062-07 08 Jan-14 Nitrobenzene 0.1 ND mg/L S 1311 1 2 21-Jan-14 AE Gypsum 1400062-07 08 Jan-14 Pentachlorophenol 0.25 ND mg/L S 1311 1 100 21 Jan-14 AE Gypsum 1400062-07 08Jan-14 Pyridine _ �TGLP 0.25 ND -� mg/L S 1311 1 5 2I Jan-14 AE Arsenic -- Client Lab Collected AaaI ie R. ep Lmt Result Units Matrix McYlxod DF ReaLvi Gypsum 1400062-07 OS Jan-14 PCIF Arsenic 0.5 ND mg/L S 1311 1 5 -PM-Analyst 20 Jan-14 V1/K TCILP Barium Clientmg Lab " Co acted Anal vte Rep Lmt Resuk Units Matnx Methe DF ReaLvl Rnnt Aaal vst Gypsum 1400062-07 08 Jan-14 TCLP Barium 5 ND mg/L S 1311 1 .9- 20-Jan-14 VVK TCLP Cadmium ----- Client ID# Gypsum Lab 1D# 1400062-07 Collected aal a 08 Jan-14 TCLP Cadmium Rep Lmt Result Units Matrix ivlethod DF RegLA - A a = 0.1 ND mg/L S 1311 1 1 20Jan44 WK TCLP Chromiurn Client Gypsum Lab M# CoIIeoted Anal Lte Rep Lm# Rain; 1400062-07 08 Jan-14 TCLP Chrorntum 0.2 ND Units kt-nk mg/L S Method DF 1311 1 ReoLvi Rua AIO S 20-Jan-14 WK TCLP Lead CGmt 1D Lab M# coIIected Aaalvte Rep Lm ReMft Uurts Mabix . Method DF RepLvl Kim Analyst Gypsum 1400062-07 08 Jan-14 TCLP Lead 0.5 ND mg/L S 1311 1 5 20-Ian-14 WK Page 12 ", m- i Hoag �Igira- :sue' rye 'v i Si'faG Nmc..LAFR heed' i6d • ,. 1,' ��':.. vim.. �x �L?pS?ge Fails, Ohio 44223 - Phone: 33J-7 C- v'�.-4 7,V ` 'Math Site, S �M ,i'7f'7 �{sV�� 'O'B'dd N."I , -.^'i`s: a;5�':�:. January 28, 2014 Client: ADM Address: 1730 Fast More St. South Port, NC 28461 Received: 1/1112014 Project #: N/A TCLP A9ercury Client iD# Lab M# Collected Analyse Rep Lmt Result Gypsum _ 1400062-07 08 Jan-14 Mercury _ - 0.002 ND TCLP SG Client ID# Lab IDar Collected Analvte Rep Lmt Result Gypsum _1400062-07 08-Ian-14TCLp Selenium_ 0.5 ND - TCLP saver Ghent ID# Iab 09 Collected AnaMa RED Lmt Result Gypsum 1400062-07 08Jan-14TCLPSilver 0.5 ND Units Matrix Method .DF Realyl Run Analyst mg/L S 1311 1 0.2 20 Jan-14 ALI Units Matrix Method OF ReaLyl --- &a] mg/L S 13111 1� 20-Ian-14 vvK Units Matrix Method DF ReoLvl R,, but Anal st mg/L S 1311 1 5 20 Jan-14 WK Page 13 EP—A Csft'lfied • NNELr' P, eE'tlfda'd . _l �[� 6r'1:';•uer`.t;.{ ',.: C.�'tfc^.'�T.O cl F a O 4422rt y' ''l: �i Cj S; ili'3 a f Q-'-C-: 330-1- -8 211 • F t:.�.��-2 3= •?f�J� i/ 1•11'EJ 5iPe tv1vLi.SE?zrt .Cr_sri3 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM—NitroGro II/NitroGro V NPDES Number: NCO027065 Monitoring Period: From 01/01/14 To 01/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If annlirnhle to alternative nerfnrmed (Class A nr Class R) rmmnlete the fnllawino man itnrina data - Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units deuces Analysis Fecal 2x 10 to the 6 th MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of 17 N/A 40 MPN/g 0 Monthly Grab 9221E total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) X No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used "to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson, Operations Director ' Prepa • r Name an Title (type or print) Land }3ia® it (if pe or print) o?173/S *7`��%I� ignature of Preparer* Date Signature o*f Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Fecal Coliform - NITRO-GRO, YEAST CREAM & CARBON 2014 Nitro-Gro Nitro-Gro YEAST Month Date II V CREAM Average Average Average January 1/6/14 17 14 1 /13/14 40 200 1 /20/14 24 1 /24/14 40 February 2/3/14 50 <10 2/10/14 <2 <2 2/17/14 2 <2 2/18/14 <2 2/24/14 <2 4.5 March 3/3/14 <2 <2 3/12/14 <2 <2 3/17/14 <2 3/19/14 2.5 3/24/14 <2 3/27/14 <2 3/31/14 6 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM — NitroGro II/NitroGro V NPDES Number: NCO027065 Monitoring Period: From 02/01/14 To 02/28/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 4/13 (No Prior Test) Alt. 2/13 (Alk Treatment) Alt. 5/Process to Further Reduce Pathogens Alt. 3/C (Prior Testing) Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion it ......R....l.l.. 4....11.........4:.,.... ran.......d !f`L,00 A ... 01— R\ nn -1.+n +hn IWI na mnniinrinn J.+a- Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units deuces Analysis Fecal 2x10to the 61 MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of •d 2 N/A 50 MPN/g 0 Monthly Grab 9221E total solids (dry weight) Salmonella 3 MPN per 4 grains total bacteria (in solids (dry weight) lieu of fecal colifor n) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) X No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson O er 'o Di ctor � Prep Name tie pe or print) L 1' applicable) (type or print) ignature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) c Fecal Coliform - NITRO-GRO, YEAST CREAM & CARBON 2014 Nitro-Gro Nitro-Gro YEAST Month Date II V CREAM Average Average Average January 1/6/14 1/13/14 1 /20/14 1 /24/14 February 2/3/14 2/10/14 2/17/14 2/18/14 2/24/14 March 3/3/14 3/12/14 3/17/14 3/19/14 3/24/14 3/27/14 3/31/14 17 40 40 50 <2 2 <2 <2 <2 2.5 <2 14 200 24 <10 <2 <2 <2 4.5 <2 <2 <2 <2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM —NitroGro II/NitroGro V Monitoring Period: From 03/01/14 To 03/31/14 NPDES Number: NCO027065 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Anaerobic Digestion Composting Aerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitorine data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 61 MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of 42 N/A 2.5 MPN/g 0 Monthly Grab 9221E total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 (VS reduction) Option/Alt. 5 (14-Day Aerobic) Option/Alt. 9 (Injection) Option/Alt. 2 (40-day bench) Option/Alt. 6 (Alk Stabilization) Option/Alt. 10 (Incorporation) X CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 (30-day bench) Option/Alt. 7 (Drying — Stable) Option/Alt. 4 (Spec. 02 uptake) Option/Alt. 8 (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/I5A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson, O eratio s PjrecAor Prep r Name and 'tle.( pe or print) Lan er a e ca e (type or print) Z-zy-�S ignature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Fecal Coliform - NITRO-GRO, YEAST CREAM & CARBON 2014 Nitro-Gro Nitro-Gro YEAST Month Date II V CREAM Average Average Average January 1/6/14 17 14 1 /13/14 40 200 1 /20/14 24 1 /24/14 40 February 2/3/14 50 <10 2/10/14 <2 <2 2/17/14 2 <2 2/18/14 <2 2/24/14 <2 4.5 March 3/3/14 <2 <2 3/12/14 <2 <2 3/17/14 <2 3/19114 2.5 3/24/14 <2 3/27/14 <2 3/31 /14 6 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM —NitroGro II/NitroGro V NPDES Number: NCO027065 Monitoring Period: From 04/01/14 To 04/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative nerformed (Class A or Class B) comnlete the fnllowing monitoring data_ Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6 1h MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of 2 N/A 5.5 MPN/g 0 Monthly Grab 9221E total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0ption/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Mt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) X No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified _ personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson, Operations Director Prepa r Name a Title ( pe or print) I d tle (type or print) /Walurie of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) April 4/4/14 <2 4/7/14 4 <2 4/17/14 <2 <2 4/23/14 5.5 4/25/14 <2 4/28/14 3.3 2 May 5/5/14 <2 5/9/14 <2 5/12/14 <2 5/14/14 <2 5119/14 10.9 <2 5/26/14 13 <2 5/30/14 <2 June 6/4/14 <2 <2 6/11 /14 <2 <2 6/18/14 <2 <2 6/23/14 4.7 6/26/14 11 <2 6/30/14 <2 July 7/3/14 <2 7/7/14 <2 <2 7/16/14 <2 3 7/21 /14 6.6 <2 7/30/14 <2 <2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: W00004500 WWTP Name: ADM—NitroGro II/NitroGro V NPDES Number: NCO027065 Monitoring Period: From 05/01/14 To 05/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlicahle to alternative nerformed (Class A or Class Rl comnlete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6` MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of 4-2 N/A 13 MPN/g 0 Monthly Grab 9221E total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Mt.4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) X No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you.check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson, Operations Director. Pre er Name rtl pe or print) Land A a a Ti (if ap icabl 1,Ftype or print) 777 Signature of Preparer* AV Date Signature f Land Applier if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) W April May June July 4/4/14 4/7/14 4/17/14 4/23/14 4/25/14 4/28/14 5/5/14 5/9/14 5/12/14 5/14/14 5/19/14 5/26/14 5/30/14 6/4/14 6/11/14 6/18/14 6/23/14 6/26/14 6/30/14 7/3/14 7/7/14 7/16114 7/21/14 7/30/14 <2 <2 4 <2 <2 <2 5.5 <2 3.3 2 <2 <2 <2 <2 10.9 <2 13 <2 <2 <2 <2 <2 <2 <2 <2 4.7 11 <2 <2 <2 <2 <2 <2 3 6.6 <2 <2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) i Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM —NitroGro II/NitroGro V NPDES Number: NCO027065 Monitoring Period: From 06/01/14 To 06/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6` MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of <2 N/A 11 MPN/g 0 Monthly Grab 9221E total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 (VS reduction) Option/Alt. 5 (14-Day Aerobic) Option/Alt. 9 (Injection) Option/Alt. 2 (40-day bench) Option/Alt. 6 (Alk Stabilization) Option/Alt. 10 (Incorporation) X CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 (30-day bench) Option/Alt. 7 (Drying — Stable) Option/Alt. 4 (Spec. 02 uptake) Option/Alt. 8 (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson, Operations Director Prepa r Name an lQ (ty e or print) Land,A Ti 1pe or print) Signature of Preparer* Date Signature Land Applier if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) April 4/4/14 <2 4/7/14 4 <2 4/17/14 <2 <2 4/23/14 5.5 4/25/14 <2 4/28/14 3.3 2 May 5/5/14 <2 5/9/14 <2 5/12/14 <2 5/14/14 <2 5/19/14 10.9 <2 5/26/14 13 <2 5/30/14 <2 June 6/4/14 <2 <2 6/11 /14 <2 <2 6/18/14 <2 <2 6/23/14 4.7 6/26/14 11 <2 6/30/14 <2 July 7/3/14 <2 7/7/14 <2 <2 7/16/14 <2 3 7/21 /14 6.6 <2 7/30/14 <2 <2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM —NitroGro II/NitroGro V NPDES Number: NCO027065 Monitoring Period: From 07/01/14 To 07/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6h MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of 42 N/A 6.6 MPN/g 0 Monthly Grab 9221E total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 (VS reduction) Option/Mt. 5 (14-Day Aerobic) Option/Alt. 9 (Injection) Option/Alt. 2 (40-day bench) Option/Alt. 6 (Alk Stabilization) Option/Alt. 10 (Incorporation) X CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 (30-day bench) Option/Alt. 7 (Drying — Stable) Option/Alt. 4 (Spec. 02 uptake) Option/Alt. 8 (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/I5A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson, O ra ' ns 1pirector Prep r Name 1 pe or print) lie app icable) (type or print) ignature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) April 4/4/14 <2 4/7/14 4 <2 4/17/14 <2 <2 4/23/14 5.5 4/25/14 <2 4/28/14 3.3 2 May 5/5/14 <2 5/9/14 <2 5/12/14 <2 5/14/14 <2 5/19/14 10.9 <2 5/26/14 13 <2 5/30/14 <2 June 6/4/14 <2 <2 6/11 /14 <2 <2 6/18/14 <2 <2 6/23/14 4.7 6/26/14 11 <2 6/30/14 <2 July 7/3/14 <2 7/7/14 <2 <2 7/16/14 <2 3 7/21 /14 6.6 <2 7/30M 4 <2 <2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: W00004500 WWTP Name: ADM —NitroGro II/NitroGro V NPDES Number: NCO027065 Monitoring Period: From 08/01/14 To 08/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlienhle to alternative nerfnrmed Wincc A nr Chm R) rmmnlete the fnllnwino mnnitnrino dntn- Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6th MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of 2.2 MPN/g 0 Monthly Grab 9221E total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Mt. 10 (Injection) (Incorporation) X No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson, Operations Director Pre rer Name Titl pe or print) Land n i Ti (if applicable) pe or print) / Signature of Preparer* Date Signature f Land Applier f applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) August 8/4114 7.6 8/7/14 <2 8/14/14 2.2 <2 8/18/14 6 <2 8/28/14 <2 3.1 Septembe 9/1/14 <2 <2 9/8/14 2.4 <2 9/15/14 <2 <2 9/22/14 5.6 <2 October 10/8/14 <2 <2 10/13/14 10/20/14 3.8 <2 10/29/14 3 2 Novembei 11/5/14 <2 <2 11 /10/14 <2 <2 11/17/14 18 3 Decembei 12/4/15 2 12/8/15 <2 12/15/15 17 3 12/22/15 <2 <2 12/29/15 543 32 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: . ADM—NitroGro II/NitroGro V NPDES Number: NCO027065 Monitoring Period: From 09/01/14 To 09/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlieable to alternative nerfnrmed (Class A or Class R) comnlete the fnilowinu mnnitorinu data! Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units deuces Analysis Fecal 2xl0to the 6 1h MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of 2.4 N/A 5.6 MPN/g 0 Monthly Grab 9221E total solids (dry weight) Salmonella 3 MPN per 4 grams total' bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4 (V S reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) X No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson, Operations Director Prep r Name i le (type or print) Land e i d tle (i a lica (type or print) Signature of Preparer* Date SignatuM of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) August 8/4/14 7.6 8/7/14 <2 8/14/14 2.2 <2 8/18/14 6 <2 8/28/14 <2 3.1 Septembe 9/1/14 <2 <2 9/8/14 2.4 <2 9/15/14 <2 <2 9/22/14 5.6 <2 October 10/8/14 <2 <2 10/13/14 10/20/14 3.8 <2 10/29/14 3 2 Novembei 11/5/14 <2 <2 11 /10/14 <2 <2 11/17/14 18 3 Decembei 12/4/15 2 12/8/15 <2 12/15/15 17 3 12/22/15 <2 <2 12/29/15 543 32 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM—NitroGro II/NitroGro V NPDES Number: NCO027065 Monitoring Period: From 10/01/14 To 10/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitorin¢ data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6th MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of 12 N/A 3.8 MPN/g 0 Monthly Grab 9221 E total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 (VS reduction) Option/Alt. 5 (14-Day Aerobic) Option/Alt. 9 (Injection) Option/Alt. 2 (40-day bench) Option/Alt. 6 (Alk Stabilization) Option/Alt. 10 (Incorporation) X CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 (30-day bench) Option/Alt. 7 (Drying — Stable) Option/Alt. 4 (Spec. 02 uptake) Option/Alt. 8 (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement to 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson Operations Director Prepiper Name and ' le (type or print) Land A itl type or print) Signature of Preparer* Date Signature o Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) August 8/4/14 7.6 8/7/14 <2 8/14/14 2.2 <2 8/18/14 6 <2 8/28/14 <2 3.1 Septembe 9/1/14 <2 <2 9/8/1 4 2.4 <2 9/15/14 <2 <2 9/22/14 5.6 <2 October 10/8/14 <2 <2 10/13/14 10/20/14 3.8 <2 10/29/14 3 2 Novembei 11/5/14 <2 <2 11 /10/14 <2 <2 11/17/14 18 3 Decembei 12/4/15 2 12/8/15 <2 12/15/15 17 3 12/22/15 <2 <2 12/29/15 543 32 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM —NitroGro II/NitroGro V NPDES Number: NCO027065 Monitoring Period: From 11/01/14 To 11/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 0 MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of 42 N/A 18 MPN/g 0 Monthly Grab 9221E total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 (VS reduction) Option/Alt. 5 (14-Day Aerobic) Option/Alt. 9 (Injection) Option/Alt. 2 (40-day bench) Option/Alt. 6 (Alk Stabilization) Option/Alt. 10 (Incorporation) X CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 (30-day bench) Option/Alt. 7 (Drying — Stable) Option/Alt. 4 (Spec. 02 uptake) Option/Alt. 8 (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson Operations Director Prepar Name and Tit (tye or print) Land Ti type or print) /ignature of Preparer* Date Signature f Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) August 8/4/14 7.6 8/7/14 <2 8/14/14 2.2 <2 8/18/14 6 <2 8/28/14 <2 3.1 Septembe 9/1/14 <2 <2 9/8/14 2.4 <2 9/15/14 <2 <2 9/22/14 5.6 <2 October 10/8/14 <2 <2 10/13/14 10/20/14 3.8 <2 10/29/14 3 2 Novembei 11/5/14 <2 <2 11 /10/14 <2 <2 11/17/14 18 3 Decembei 12/4/15 2 12/8/15 <2 12/15/15 17 3 12/22/15 <2 <2 12/29/15 543 32 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM —NitroGro II/NitroGro V NPDES Number: NCO027065 Monitoring Period: From 12/01/14 To 12/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1 /A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If apDlicable to alternative performed (Class A or Class B) comnlete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x 10 to the 6 th MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of total solids (dry weight) { 2 N/A 543 MPN/g 0 Monthly Grab 9221E Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 (VS reduction) (40-day bench) Option/Alt. 5 Option/Alt. 6 (14-Day Aerobic) (Alk Stabilization) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) X CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 (30-day bench) Option/Alt. 7 (Drying — Stable) Option/Alt. 4 (Spec. 02 uptake) Option/Alt. 8 (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Todd Larson, O erations Dir ctor Pr arer Name itl �®rnt)L it type or print) 7!!72� Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) August 8/4/14 7.6 8/7/14 <2 8/14/14 2.2 <2 8/18/14 6 <2 8/28/14 <2 3.1 Septembe 9/1/14 <2 <2 9/8/14 2.4 <2 9/15/14 <2 <2 9/22/14 5.6 <2 October 10/8/14 <2 <2 10/13/14 10/20/14 3.8 <2 10/29/14 3 2 Novembei 11/5/14 <2 <2 11 /10/14 <2 <2 11/17/14 18 3 Decembei 12/4/15 2 12/8/15 <2 12/15/15 17 3 12/22/15 <2 <2 12/29/15 543 32 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM — NitroGro II NPDES Number: NCO027065 Monitoring Period: From 7/01/14 To 7/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlienhle to alternative nerfnrmed Wince A or Clacc Rl rmmnlete the fnllnwino mnnitnrinu data! Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6 1h MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of 2 N/A 2 MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Alt. 3 Option/Alt.4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Pr arer Nam p.d Title (type or print) A? 1-0 , /sue Signature of Prepar Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) April May June July 4/4/14 4/7/14 4/17/14 4/23/14 4/25/14 4/28/14 5/5/14 5/9/14 5/12/14 5/14/14 5/19/14 5/26/14 5/30/14 6/4/14 6/11/14 6/18/14 6/23/14 6/26/14 6/30/14 7/3/14 7/7/14 7/16/14 7/21 /14 7/30/14 <2 <2 4 <2 <2 <2 5.5 <2 3.3 2 <2 <2 <2 <2 10.9 <2 13 <2 <2 <2 <2 <2 <2 <2 <2 4.7 11 <2 <2 <2 <2 <2 <2 _3 6.6 <2 <2 SOURS TESTS MONTH DATE Results Mg OZ / h / g total solids July 7/9/14 1.31 7/28/14 1.3 August 8/4/14 1.49 8/19/14 1.46 8/29/14 1.54 September 9/3/14 1.16 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WWTP Name: ADM —NitroGro II Monitoring Period: From 8/01/14 To 8/31/14 WQ Permit Number: WQ0004500 NPDES Number: NCO027065 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If annlicahle to alternative nerformed (Class A or Class B) comnlete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6` MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of L 2 N/A 6 MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Infection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Prep r Name le a or print) Signature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) August 8/4/14 7.6 8/7/14 <2 8/14/14 2.2 <2 8/18/14 6 <2 8/28/14 <2 3.1 Septembe 9/1/14 <2 <2 9/8/14 2.4 <2 9/15/14 <2 <2 9/22/14 5.6 <2 October 10/8/14 <2 <2 10/13/14 10/20/14 3.8 <2 10/29/14 3 2 November 11/5/14 <2 <2 11 /10/14 <2 <2 11/17/14 18 3 Decembei 12/4/15 2 12/8/15 <2 12/15/15 17 3 12/22/15 <2 <2 12/29/15 543 32 SOURS TESTS MONTH DATE Results Mg 02 / h / g total solids July 7/9/14 1.31 7/28/14 1.3 August 8/4/14 1.49 8/19/14 1.46 8/29/14 1.54 September 9/3/14 1.16 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM — NitroGro II NPDES Number: NCO027065 Monitoring Period From 9/01/14 To 9/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Anaerobic Digestion Composting Aerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge ---------- Pathogen Density ------- No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6` MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of 2 N/A 6 MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment." Scott Phillips, Operations Superintendent Preparer am and Tit a print) Land Applier Name and Title (if applicable) (type or print) S' ature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) August 8/4/14 7.6 8/7/14 <2 8/14/14 2.2 <2 8/18/14 6 <2 8/28/14 <2 3.1 Septembe 9/1/14 <2 <2 9/8/14 2.4 <2 9/15/14 <2 <2 9/22/14 5.6 <2 October 10/8/14 <2 <2 10/13/14 10/20/14 3.8 <2 10/29/14 3 2 Novembei 11/5/14 <2 <2 11 /10/14 <2 <2 11/17/14 18 3 Decembei 12/4/15 2 12/8/15 <2 12/15/15 17 3 12/22/15 <2 <2 12/29/15 543 32 SOURS TESTS MONTH DATE Results Mg 02 / h / g total solids July 7/9/14 1.31 7/28/14 1.3 August 8/4/14 1.49 8/19/14 1.46 8/29/14 1.54 September 9/3/14 1.16 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM—NitroGro III NPDES Number: NCO027065 Monitoring Period: From 01/01/14 To 02/28/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If aDplicable to alternative performed (Class A or Class B) comDlete the followin¢ monitorin¢ data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the oh MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of 42 N/A 200 MPN/g 0 Bi- Grab 9221 E total solids (dry weight) monthly Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. I (V S reduction) Option/Alt.2 O on/Alt.3 ^*�� Option/Alt.4 (Spec. 02 uptake) Option/Alt. 5 odaoll��tloll) ilir . Option/Alt. 8 (14-Day Aerobic) (Drying — Sta� (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Prep er Name anor print) Land Applier Name and Title (if applicable) (type or print) Signature o Preparer* Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Date Fecal Coliform - NITRO-GRO, YEAST CREAM & CARBON 2014 Nitro-Gro Nitro-Gro YEAST Month Date II V CREAM Average Average Average January 1/6/14 1/13/14 1 /20/14 1 /24/14 February 2/3/14 2/10/14 2/17/14 2/18/14 2/24/14 March 3/3/14 3/12/14 3/17/14 3/19/14 3/24/14 3/27/14 3/31/14 17 14 40 200 24 40 50 <10 <2 <2 2 <2 <2 <2 4.5 <2 <2 <2 <2 <2 2.5 <2 <2 6 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM—NitroGro III NPDES Number: NCO027065 Monitoring Period: From 03/01/14 To 04/30/14 Pathogen Reduction (40 CFR 50332/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6 1h MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of L2 N/A 6 MPN/g 0 Bi- Grab 9221E total solids (dry weight) monthly Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Optima/Alt. 3 tu�rl�d Option/Alt.4 (VS reduction) (4ll-�laa, Ih1 en.M:y� (Spec. 02 uptake) Option/Alt. 5 (14-Day Aerobic) ' "' � Dry ing — btabl Option/Alt. 8 (Drying — Unstable ( rY g ) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent _ Prep Name an itl� ( e or print) you Signature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Fecal Coliform - NITRO-GRO, YEAST CREAM & CARBON 2014 Nitro-Gro Nitro-Gro YEAST Month Date II V CREAM Average Average Average January 1/6/14 17 14 1 /13/14 40 200 1 /20/14 24 1 /24/14 40 February 2/3/14 50 <10 2/10/14 <2 <2 2/17/14 2 <2 2/18/14 <2 2/24/14 <2 4.5 March 3/3/14 <2 <2 3/12/14 <2 <2 3/17/14 <2 3/19/14 2.5 3/24/14 <2 3/27/14 <2 3/31/14 6 April May June July 4/4/14 4/7/14 4/17/14 4/23/14 4/25/14 4/28/14 5/5/14 5/9/14 5/12/14 5/14/14 5/19/14 5/26/14 5/30/14 6/4/14 6/11/14 6/18/14 6/23/14 6/26/14 6/30/14 7/3/14 7/7/14 7/16/14 7/21/14 7/30/14 <2 <2 4 <2 <2 <2 5.5 <2 3.3 2 <2 <2 <2 <2 10.9 <2 13 <2 <2 <2 <2 <2 <2 <2 <2 4.7 11 <2 <2 <2 <2 <2 <2 3 6.6 <2 <2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM —NitroGro III NPDES Number: NCO027065 Monitoring Period: From 05/01/14 To 06/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 61 MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of 4.2 N/A 4.7 MPN/g 0 Bi- Grab 9221 E total solids (dry weight) monthly Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Opt�nu„�}j/Alt. 3 Option/Alt.4 (VS reduction) (, -cl M,,�rotI, r1 ! ^ h (Spec. 02 uptake) Option/Alt. 5�on rli li1�l0 Option/Alt. 8 (14-Day Aerobic) Drying — Stab (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Infection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent PregKer Name Ty1 ty.pe or print) Land Applier Name and Title (if applicable) (type or print) Signature of Preparerodr Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) April May June July 4/4/14 4/7/14 4/17/14 4/23/14 4/25/14 4/28/14 5/5/14 5/9/14 5/12/14 5/14/14 5/19/14 5/26/14 5/30/14 6/4/14 6/11/14 6/18/14 6/23/14 6/26/14 6/30/14 7/3/14 7/7/14 7/16/14 7/21/14 7/30/14 <2 <2 4 <2 <2 <2 5.5 <2 3.3 2 <2 <2 <2 <2 10.9 <2 13 <2 <2 <2 <2 <2 <2 <2 <2 4.7 11 <2 <2 <2 <2 <2 <2 3 6.6 <2 <2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM—NitroGro III NPDES Number: NCO027065 Monitoring Period: From 07/01/14 To 08/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 31C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the followine monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6'h MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of <2 N/A 7.6 MPN/g 0 Bi- Grab 9221E total solids (dry weight) monthly Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt. 2 O ti jm/Alt. 3 Option/Alt. 4 (VS reduction) ('"'+� !�� ""i (Spec. 02 uptake) Option/Alt. 5 d ilki t. Option/Alt. 8 (14-Day Aerobic) ilaUon) Rc rym Stable p g — ) (Drying —Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15, NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent :,epr�Name�tIee r print) �• 3 Signature of Preparer* 47 Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) April May June July 4/4/14 4/7/14 4/17/14 4/23/14 4/25/14 4/28/14 5/5/14 5/9/14 5/12/14 5/14/14 5/19/14 5/26/14 5/30/14 6/4/14 6/11/14 6/18/14 6/23/14 6/26/14 6/30/14 7/3/14 7/7/14 7/16/14 7/21/14 7/30/14 <2 <2 4 <2 <2 <2 5.5 <2 3.3 2 <2 <2 <2 <2 10.9 <2 13 <2 <2 <2 <2 <2 <2 <2 <2 4.7 11 <2 <2 <2 <2 <2 <2 3 6.6 <2 <2 August 8/4/14 7.6 8/7/14 <2 8/14/14 2.2 <2 8/18/14 6 <2 8/28/14 <2 3.1 Septembe 9/1/14 <2 <2 9/8/14 2.4 <2 9/15/14 <2 <2 9/22/14 5.6 <2 October 10/8/14 <2 <2 10/13/14 10/20/14 3.8 <2 10/29/14 3 2 Novembei 11/5/14 <2 <2 11 /10/14 <2 <2 11/17/14 18 3 Decembei 12/4/15 2 12/8/15 <2 12/15/15 17 3 12/22/15 <2 <2 12/29/15 543 32 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM — NitroGro III NPDES Number: NCO027065 Monitoring Period: From 09/01/14 To 10/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 61 MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of 42 N/A 2 MPN/g 0 Bi- Grab 9221E total solids (dry weight) monthly Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt.I (VS reduction) Option/Alt. (40-(tm I,„iac Opti /Alt.3 h) Option/Alt.4 (Spec. 02 uptake) Option/Alt.5 a(}�.,.h� Option/Alt.8 l Ilk �v wwrr.Wy �a (14-Day Aerobic) Drying — Ia (Drying — Unstable) Option/Alt. 9 n/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent Pre er Name Tit (type or print) Land Applier Name and Title (if applicable) (type or print) Signature of PreparerV Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Date August 8/4/14 7.6 8/7/14 <2 8/14/14 2.2 <2 8/18/14 6 <2 8/28/14 <2 3.1 Septembe 9/1/14 <2 <2 9/8/14 2.4 <2 9/15/14 <2 <2 9/22/14 5.6 <2 October 10/8/14 <2 <2 10/13/14 10/20/14 3.8 <2 10/29/14 3 2 Novembei 11/5/14 <2 <2 11 /10/14 <2 <2 11/17/14 18 3 December 12/4/15 2 12/8/15 <2 12/15/15 17 3 12/22/15 <2 <2 12/29/15 543 32 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Archer Daniels Midland Company WQ Permit Number: WQ0004500 WWTP Name: ADM —NitroGro III NPDES Number: NCO027065 Monitoring Period: From 11/01/14 To 12/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class A: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative Derformed (Class A or Class B) complete the followin¢ monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 61 MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of <2 N/A 32 MPN/g 0 Bi- Grab 9221E total solids (dry weight) monthly Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt. 2 Option/Alt.3 Option/Alt.4 (VS reduction) (40-d v hhenc 00-dW bench) (Spec. 02 uptake) Option/Alt. S k4*e ,, Option/Alt. 8 (14-D Aerobic) ` (l�f�j1T1 eta (Drying —Unstable) Option/Alt. 9 Option/Alt. 10 (Infection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Phillips, Operations Superintendent APre Name letype or print) Land Applier Name and Title (if applicable) (type or print) + wu�— e of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) August 8/4/14 7.6 8/7/14 <2 8/14/14 2.2 <2 8/18/14 6 <2 8/28/14 <2 3.1 Septembe 9/1/14 <2 <2 9/8/14 2.4 <2 9/15/14 <2 <2 9/22/14 5.6 <2 October 10/8/14 <2 <2 10/13/14 10/20/14 3.8 <2 10/29/14 3 2 Novembei 11/5/14 <2 <2 11 /10/14 <2 <2 11/17/14 18 3 Decembei 12/4/15 2 12/8/15 <2 12/15/15 17 3 12/22/15 <2 <2 12/29/15 543 32