WQ0004298_Residual Annual Report 2014_20150223

Town of Mars Hill NC
2014 Land Application Report
WQ0004298
Attached are the required forms for the Town of Mars Hills 2014 land application
program.
The town has land applied 15.805 dry tons of sludge over 14.5 acres in the calendar year
2014. We have also maintained compliance with all terms and conditions except for our
fecal density testing. We had misplaced our test bottles and did not test in the 2014
calendar year. We did remember in January and did the required testing on sludge that
was collected in 2014 and had been in aerobic digestion for 30 days. The results met and
exceeded allrequirements but were sampled outside the required monitoring period_ A
sampling schedule will be implemented to prevent this from happening again.
Contact Information:
Preparer/ORC
Robert Sams
Public Works Director
Town of Mars Hill
PO Box 368
Mars Hill NC 28754
Phone # [phone]
Permittee
Darhyl Boone
Town Manager
Town of Mars Hill
PO Box 368
Mars Hill NC 28754
Phone # [phone]
REGEIVEDIDEN JON
FEB S 3 Z015
waterau PiTW VI SO

ANNUAL LAND APPLICATION CERTIFICATION FORM
i0er lt#: WQ0004298 County:
Facility Name (as shown on permit):
Land Application Operator:
Madison
Year: 2014
Town of Mars Hill
Robert M Sams Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the'past calendar year?
9 Yes L'-] No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of acres land application occurred during the year: 1 14.5
Part B:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Resources:-11 Yes 1? No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Resources.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for kno g violations."
Darhyl Boone- Town Manager ,)lwlale
Permi ame d Title (typ r print) SignatureAl Permittee Da e
kZ"
Signature of Preparer* Date Signature of Land Applier Date
DENR FORM ACF (5/2003)

�r
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0004298
Facility Name: Town fo Mars Hill
NPDES # or NCO057151
WQ#:
WWTP Name: Town of Mars Hill WWTP
Residual Analvsis Data
Laboratory: 1)
Earth Environmental
2) Environmental Testing Solutions
3) A&L Eastern Laboratories
4)
5)
Sample or
CompositeDate
FOR
We MID
®-------
INNITMETINIUMM
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
signific t penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
1AI'4Q�,7;r 2/18/2015
Signature of Preparer Date
DENR FORM RSSF (5/2003)

Earth EnVlrenmenlal services
Michael Ladd
75 Bison Lane
Murphy, NC 28906
Robbinsville Lab [phone]
Weaverville Lab [phone]
Residence [phone]
Name and Address of Facility:
Date: 1/20/2015
Town of Mars Hill WWTP
Sample collector:
RS
P.O. BOX 368
Date and Time Sample Received:
5/28/2014 10:55 AM
Mars Hill, NC 28754
Date and Time Sample Collected:
5/28/2014 7:40 - 8:15 AM
Aft: Robert Sams
Date and Time Sample Analyzed:
< MHT
Land Application Analyses - Note: All results in mg/Kg Dry Basis unless otherwise noted.
Test
Belt Press Sludge
Soil Site#1
Soil Site#2
Report Limit
Method
Units
ACIDITY
0.0 meq/100g
0.0 meq/100g
SCA
meq/100g
TOTAL SUSPENDED RESIDUE
SM2540D
mg/L
CATION EXCHANGE CAPACITY
12.1 meq/100g
9.7 meq/100g
SCA
meq/100g
pH
5.2
7.2
7.2
0-14
SCA
units
AMMONIA NITROGEN
1000
0.5
SCA
mg/L
NO2 + NO3-n
< 31.21
1.0
SCA
mg/L
TOTAL KJELDAHL NITROGEN
57200
SCA
mg/L
TOTAL PHOSPHOROUS
18500
972
559
SCA
mg/L
PERCENT TOTAL RESIDUE
13.0%
80.0%
87.0%
SCA
mg/L
% ORGANIC MATTER
4.3%
5.4%
SCA
NTU
% BASE SATURATION - K
9.5%
3.5%
SCA
mg/L
- H
0.0%
0.0%
-Mg
30.6%
35.1%
-Ca
59.5%
60.3%
-Na
0.7%
0.70/0
PLANT AVAILABLE (surface)
22980
PPM/dw
NITROGEN- PPM DRY WT (subsurf)
23480
PPM/dw
SAR
1.416501
ESP
7.85124%
7.731959%
MANGANESE
194
1.62
SCA
mg/L
MAGNESIUM
2800
3190
1030
SCA
mg/L
SODIUM
542
22.9
14.7
SCA
mg/L
CADMIUM
< 7.48
< 1.20
< 1.15
SCA
mg/L
CHROMIUM
24.4
62.7
43.7
1
SCA
mg/L
COPPER
203
44.4
20.2
SCA
mg/L
LEAD
19.7
17.7
13.4
SCA
mg/L
NICKEL
17.0
11.3
9.33
SCA
mg/L
ZINC
590
57.6
1 27.9
SCA
mg/L
CALCIUM
6480
3320
1450
SCA
mg/L
POTASSIUM
3930
1790
372
SCA
mg/L
ALUMINUM
4770
N/A
N/A
SCA
mg/L
ARSENIC
< 18.7
< 2.99
< 2.87
SCA
mg/L
SELENIUM
< 18.7
< 2.99
< 2.87
SCA
mg/L
MOLYBDENUM
< 18.7
< 2.99
< 2.87
SCA
mg/L
MERCURY
1.60
< 0.12
< 0.11
SCA
mg/L
N.C. Laboratory ID# 352 Analyzed By: SC
Lab Supervisor. Michael J. Ladd; EES-Robbinsville Certified By: Qp

Mars Hill Land Application Belt Press Sludge 5/28/14
PAN
Mineralization
as decimal
ITotal dry
tons/tear
IAcres
I Applied on
Rate
0.4
TKN
57200
NH3
1000
NO3
0
NO2
0
% Solids
0.13
PAN Surface
229801 mg/kgmglkg 45.96 Ibs/dry ton
0 Ibs total PAN
#DIV/01 jibs PAN/acre
PAN Injection
F-234801mg/i,j 1 46.96 Ibs/dry ton
0 Ibs total PAN
#DIV/01 jibs PAN/acre
Dry Tons/1000 gal.
1st year PAN
Surface Ibs.
1st year PAN
Injected Ibs.
Ibs./acre
Surface
#DIV/0!
Ibs./acre
Injected
#DIV/0!
MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibs/dry ton
MR(TKN-NH3) + l(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibs/dry ton
1000 X 8.34 X %solids X sp. gravity "=dry tons/1000gal."
2000
M

SAR & ESP Mars Hill Land Application Belt Press Sludge5/28/14
Sodium Absorption Ratio Na M /L Ca M /L Mg M /L
Na: Sodium (Mg/L) Equivalent weight: 23 542 6480 1 2800
Ca: Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight: 12 Mg (ME)
233.3333
Milli Equivalent = Mg/L / Equivalent weight
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)10.5 power
From Mg/L entered above)
SAR= 1.411656 (From ME entered below)
Na (ME)
Ca (ME)
Mp (ME)
23.565217
324
233.3333
The amount of exchangeable sodium ions
amount of exchangeable calcium & magne
material.
Permitting guidance is if greater than 10 re

N
SAR & ESP Mars Hill Land Application Soil Site #1 5/28/14
Exchangeable Sodium Percentage
ESP = Na (Milli Equivalents) / CEC X 100 The percentage of sodium ions occupying the cation exchange complex of soils
Na (ME) CEC
0 .9500
.95000000000 12.1
Na on NC soil test is expressed as meq.
Should be less than 15% (15-20%)

,.
SAR & ESP Mars Hill Land Application Soil Site #2 5/28/14
Exchangeable Sodium Percentage
ESP = Na (Milli Equivalents) / CEC X 100 The percentage of sodium ions occupying the cation exchange complex of soils
Na (ME) FCEC
0.75000000000 9.7
Na on NC soil test is expressed as meq.
Should be less than 15% (15-20%)

X
Environmental Testing solutions, Inc. Certificate of Analysis
Project name: Earth Environmental Services
Collection date: 28-Ma1-14
Date received: 28-May-14 .nre—S S
Sample identification: #051425
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
/ Project number: 140528.510
A"Op !I C � ()/I
-e'-s1,Wly
Sample number:
116482
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
Percent Solids
SM 2540 G
13.0
0.100
%
30-May-14
ASB
1
Mercury
7471B
1.60
0.74
mg/kg
9-Jun-14
DER
1
Aluminum
6010C
4770
935
mg/kg
3Juna4
MEC
1
Arsenic
6010C
<18.7
18.7
mg/kg
3-Juna4
MEC
1
Cadmium
6010C
<7.48
7.48
mg/kg
3-Jun-14
MEC
1
Calcium
6010C
6480
935
mg/kg
3-Jun-14
MEC
1
Chromium
6010C
24.4
18.7
mg/kg
3-Jun-14
MEC
1
Copper
6010C
203
7.48
mg/kg
3-Jun-14
MEC
1
Lead
601OC
19.7
18.7
mg/kg
3-Jun-14
MEC
1
Magnesium
6010C
2800
935
mg/kg
3-Jun-14
NEC
I
Molybdenum
601OC
<18.7
18.7
mg/kg
3-Jun-14
NEC
1
Nickel
6010C
17.0
7.48
mg/kg
3-Jun-14
MEC
1
Potassium
6010C
3930
37.4
mg/kg
3-Jun-la
MEC
1
Selenium
601OC
<18.7
18.7
mg/kg
3-Jun-14
MEC
1
Sodium
6010C
542
37.4
mg/kg
3 Jun-14
MEC
1
Zinc
601OC
590
18.7
mg/kg
3-Jun-14
MEC
1
Nitrate + Nitrite
<31.21
31.21
mg/kg
1,2
Total Phosphorus
6010C
18500
748
mg/kg
3Juna4
MEC
I
Total Kjeldahl Nitrogen
351.2
57200
935
mg/kg
10-Jun-14
LDP
1
Total Nitrogen
Calculation
57200
935
mg/kg
10-Jun-14
LDP
1
Ammonia Nitrogen
SM 4500 NH3 D
1000
18
mg/kg
29-May-14
KEK
Percent Solids
SM 2540 G
22
%
28-May-14
KW
pH in Soil
SW 846 9045D
5.2
S.U.
28-May-14
KW
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Methods EPA 9210A and SM 450ONO2 B by LDP and REH on 06-04-14 and 06-05-14.
Date reviewed: 0 0 -I Z 4 H
Data reviewed by: Kelley E. Keenan
Signature:
K-
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

ANNUAL METALS FIELD LOADING SUMMARY FORM*
1, Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Mars Hill Land Application Total Dry Tons Applied (Annual): 15.805
Permit #: WQ0004298 Cation Exchange Capacity (non 503 only): 12.1
Operator: Robert M Sams Owner: Larry Cody
Acres Used: 14.5 Acres Permitted: 14.5 Site #: 1 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
,.
Date
Total
hm
.h.ENEEMENEEN
M
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
o
1
2
31
4
51
6j7
81
9
0j
11'
121
o'
0.545
0.545
Arsenic
0.0204
0.0204
0
0
0
0
0
0
0
0
0
0
0.0408
Cadmium
0.00821
0.0082
0
0
0
0
0
0
0
0
0
0
0.0163
Chromiun
0.0266
0.0266
0
0
0
0
0
0
0
0
0
0
0.0532
Copper
0.2213
0.2213
0
0
0
0
0
0
0
0
0
0
0.4425
Lead
0.0215
0.0215
0
0
0
0
0
0
0
0
0
0
0.0429
Mercury
0.0017
0.0017
0
0
0
0
0
0
0
0
0
0
0.0035
Molyb-
0.0204
0.0204
0
0
0
0
0
0
0
0
0
0
0.0408
denum
Nickel
0.0185
0.0185
0
0
0
0
0
1 0
0
0
1 0
0
0.0371
Selenium
0.0204
0.0204.
0
0
0
0
0
0
0
0
0
0
0.0408
Zinc
0.6431
0.6431
0
0
0
0
0
0
0
0
0
0
1.2862
Total
Phos-
20.165
20.165
0
0
0
0
0
0
0
0
0
0
40.33
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
inclV"e oss' ity of fines imprisonment for knowing violations"
�2/ 6
DENR FORM MFLSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name:
Owner:
Site #:
Larry Cody
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Town of Mars Hill Permit #: WQ0004298 Annual Dry Tons Applied: 15.8054676
Field #:
Operator: Robert M Sams
1 Acres Utilized:
14.5
Cation Exchange Capacity (non 503): 7.2
Acres Permitted: 14.5
o.1
„ a
o
A
s Specify
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
i e
Cond.
Dry,
Wet
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo-
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
2
Gal.
Cu.Yd.
Report
4. Totals
1. in Gal.
Crop 1
Crop 2
5/20/141
14578
1005.4
13
0.545016124
Belt Press Sludge
Dry
0
s
0.5
30%
57200
1000
31.21
18.957
#######
silage
1
5/21/14
14578
1005.4
13
0.545016124
Belt Press Sludge
Dry
0
s
0.5
30%
57200
1000
31.21
18.957
#######
silage
2
0
0
0
0
3
0
0
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
0
0
9
0
0
0
0
1
110
0
0
0
0
11
0
0
0
0
12
TOTALS:
2011
.; ;.;
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
IF
Annuallbs/acre
Current Cumulative lbs/ac
0.040766
0.961154
0.01631
0.63325
0.05319
2.07257
10.44254
52.4997
0.04295
5.49399
0.00349
0.13549
0.04077
2.84821
0.03706
2.64244
10.04077
1.62478
1.2862 40.33 37.914 0
7.8624��
6.5762��
2498 y4
7
Date
lbs/ac
x
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
0.920388
36
0.61694
34
2.01938
NL
52.0572
1338
5.45104
267
0.132
15
2.80744
NL
2.60538
374
1.58401
89
Permit PAN Limit lst/2nd Crop��.
.:, . x� ,VOW
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significa en ies for submittin lse information, including the possibility of fines and imprisonment for knowing violations."
pC / *Application Method: S - Surface, IN - Injectiion, INC - Incorporation
Si ature of Ira&KApplieWr Date **Volatilization Rate: Surface - 0.5, Infection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loadins Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
_4,
4 DENR FORM FSF (5/2003)

Environmental Testing Solutions, Inc.
Certificate of Analysis
Project name: Earth Environmental Services
Collection date: 28-May-14 lf�j o
Date received: 28-May-14 5 D tl C S,t
Sample identification: #051426
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 140528.511
%CL `�- P 11
Sample number:
116483
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
Percent Solids
SM 2540 G
80.0
0.10
%
30-May-14
ASB
I
Mercury
7471B
<0.12
0.12
mg/kg
9-Jun-14
DER
1
Arsenic
6010C
<2.99
2.99
mg/kg
3-Jun-14
MER
1
Cadmium
6010C
<1.20
1.20
mg/kg
3-Jun-14
MER
1
Calcium
6010C
3320
149
mg/kg
3-Jun-14
MER
1
Chromium
6010C
62.7
2.99
mg/kg
3-Jun-14
MER
1
Copper
6010C
44.4
1.20
mg/kg
3-Jun-14
MER
1
Lead
6010C
17.7
2.99
mg/kg
3-Jun-14
MER
I
Magnesium
6010C
3190
149
mg/kg
3-Jun-14
MER
1
Mangenese
6010C
194
1.20
mg/kg
3-Jun-14
MER
1
Molybdenum
6010C
<2.99
2.99
mg/kg
3-Jun-14
MER
1
Nickel
6010C
11.3
1.20
mg/kg
3-Jun-14
MER
1
Potassium
6010C
1790
5.98
mg/kg
3-Jun-14
MER
1
Selenium
6010C
<2.99
2.99
mg/kg
3-Jun-14
MER
1
Silver
6010C
<1.20
1.20
mg/kg
3-Jun-14
MER
1
Sodium
6010C
22.9
5.98
mg/kg
3-Jun-14
MER
1
Zinc
6010C
57.6
2.99
mg/kg
3-Jun-14
MER
1
Total Phosphorus
6010C
972
120
mg/kg
3-Jun-14
MER
1
pH in Soil
SW 846 9045D
7.2
S.U.
28-May-14
KW
Acidity
See Attached Sheets
A&L
2
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

1
A Environmental Testing Solutions, Inc.
Certificate of Analysis
Project name: Earth Environmental Services
Collection date: 28-May-14
Date received: 28-May-14
S
Sample identification: #051427
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 140528.511
Sample number: 116484
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
Percent Solids
SM 2540 G
87.0
0.10
%
30-May-14
ASB
1
Mercury
7471B
<0.11
0.11
mg/kg
9-Jun-14
DER
I
Arsenic
6010C
<2.87
2.87
mg/kg
3-Jun-14
MER
1
Cadmium
6010C
<1.15
1.15
mg/kg
3-Jun-14
MER
1
Calcium
6010C
1450
143
mg/kg
3Jun-14
MER
1
Chromium
6010C
43.7
2.87
mg/kg
3-Jun-14
MER
1
Copper
6010C
20.2
1.15
mg/kg
3-Jun-14
MER
1
Lead
6010C
13.4
2.87
mg/kg
3-Jun-14
MER
1
Magnesium
6010C
1030
143
mg/kg
3-Jun-14
MER
1
Mangenese
6010C
162
1.15
mg/kg
3-Jun-14
MER
1
Molybdenum
6010C
<2.87
2.87
mg/kg
3-Jun-14
MER
1
Nickel
6010C
9.33
1.15
mg/kg
3-Jun-14
MER
1
Potassium
6010C
372
5.74
mg/kg
3-Jun-14
MER
1
Selenium
6010C
<2.87
2.87
mg/kg
3-Jun-14
MER
1
Silver
6010C
<1.15
1.15
mg/kg
3-Jun-14
MER
1
Sodium
6010C
14.7
5.74
mg/kg
3-Jun-14
MER
1
Zinc
6010C
27.9
2.87
mg/kg
3-Jun-14
MER
1
Total Phosphorus
SM 4500 P F
559
115
mg/kg
3-Jun-14
MER
1
pH in Soil
SW 846 9045D
7.2
S.U.
28-May-14
KW
Acidity
See Attached Sheets
16-Apr-13
A&L
2
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Sample analyzed by A&L Eastern Laboratories, Inc.
Date reviewed: (N • j 1.1q
Data reviewed by: Kelley E. Keenan
Signature:
;A- I
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

a
Page 1 of 1
Report Number: 14-149-0626
Account Number:46933 a. L
99
Send To: ENVIRONMENTAL TESTING Wvuwaleastem,eom
SOLUTIONS INC
POB 7565
ASHEVILLE NC 28802
Date Received: 05/29/2014 Date Of Analysis: 05/30/2014
,A&L Eastern Lab.®rato es
7621 Whitepine Road Riehmond, Virginia 23237 (804),743-9461 Fax (80A) 271-6448
Grower: Submitted By: KELLEY EKEENAN
ENVIRONMENTAL TESTING Farm ID:
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Of Resort: 05/30/2014
OFganic Maitet
Phosphorus
: �
potassium
Magnesium`
Caic�um
: Sodiumi2
Sample ID
Field; ID
': Lab
iYumber
'/o `Rate ENR ;
,: rolehlich 3
.
Reserve
0C'
Mg 4
Ca
Na'
Soil
Buffer
H , ;
Ibs/A
ppm Fiats .
}ppm ,° Rate
.:ppm a Rate
ppm Rate
pprn ;Rate
-ppm Rate
;.
Index
meq/10bg
.
,pH
meq/100g,y
051426
16579
4.7 M 124
139 VH
203 VH
506 VH
1792 M
7.3
0.0
13.7
NC=116
NC=104
51427
16580
5.3 H 143
16 L
107 M
336 VH
1255 M
7.3
0.0
9.3
NC=13
NC=55
PercentBase
Saturation
Nitrate
Sulfur
:°Zhtp
Manganese
from
Copper
" BoronSolubls
Sales
: Chloride`';°Alu'minum:�;
Sample 1D
FlelifIDs
iC
Mg
,Ca
Na
H_
NO3N3
Zn
Wli�
Fe
u
B
SS
Ci
AI.
/a.
/o
; /o
�o
in. Rat
PP a
PPm Rate
m °. Rate
pP.
PPrn ;t Rate
.PPm Rate
a
ppm Raf,'
ppm Rate
iris/cm : Rate,
ppm ; Rate
ppm
051426
3.8
30.8
65.4
0.0
51427
3.0
30.1
67.5
TO.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. �" m� ��
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A; Soluble
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: A&L Eastern Laboratories, Inc.
Pauric McGroary

LA
wwwaleastern,com
e
A&L Eastern Laboratories'
7621 WhltePine Road Richmond, Virginia 23237 (BD4) 743.9401 Fax [phone]W i �
suomitteci t3y: MICHAEL LADD
6/3/2014
SOIL ANALYSIS
Client :
EARTH ENVIRONMENTAL SVCS
Grower:
SOIL SITES 1 & 2
Report No:
14-153-0592
Cust No:
46220
75 BISON LN
Date Printed:
06/03/2014
MURPHY NC 28906
Date Received
: 06/02/2014
Date Analysis :
06/03/2014
PO:
Page:
1 of 4
L-au Ivurnoer . I f 3MU Field Id :05/28/14 Sample Id : #051426
Test
Results
Soil pH
7.4
Buffer pH
Phosphorus(P)
142 ppm
Potassium (K)
446 ppm
Calcium (Ca)
1440 ppm
Magnesium (Mg)
445 ppm
Sulfur (S)
15 ppm
Boron (B)
1.8 ppm
Copper (Cu)
5.3 ppm
Iron (Fe)
155 ppm
Manganese (Mn)
44 ppm
Zinc (Zn)
7.1 ppm
Sodium (Na)
19 ppm
Soluble Salts
Organic Matter
4.3 % ENR 119
Nitrate Nitrogen
SOIL TEST RATINGS Calculated Cation
Very Low Low Medium O mum Exchange Capacity
12.1
meq/100g
Calculated Cation
Saturation
3 %K 9.5
%Ca 59.5
%Mg 30.6
1 %H 0.0
_. Hmeq 0.0
%Na 0.7
K : Mg Ratio
0.31
Ca: Mg Ratio
1.94 I—1
SOIL FERTILITY GUIDELINES
Crop . Lawn
LIME (tons)
N
Pz 0
K z0
Mg
S
B
Cu
Mn
Zn
Fe3.5
0
0
0
0.46
0
0
0
0
0
E(Ibs)
Rec Units:
Analysis prepared by: A&L Eastern Laboratories, Inc.
Pauric McGroary

t
AFL Eastern Laboratories
7621WhbpinoRoad Riehmond,Virginia 23237 [phone] F8x(604)Z71.8446
IIVYtAI&7(BAStOrPl,f;0M
Submitted By: MICHAEL LADD 6/3/2014 SOIL ANALYSIS
Client: Grower: Report No: 14-153-0592
EARTH ENVIRONMENTAL SVCS SOIL SITES 1 & 2 Cust No: 46220
75 BISON LN Date Printed: 06/03/2014
MURPHY NC 28906 Date Received: 06/02/2014
Date Analysis : 06/03/2014
PO: Page: 2 of 4
Lab Number: 'i isyu Field Id :05/28/14 Sample Id: #051426
SUGGESTED FERTILIZATION`yPROG12AM70,
First ApplrcatronTwiSecond ApphWI6 FThird ApplrcaLon 1 `Fourt6#Appl�catron
�.#/.1000.Sg%`Ft
,Fertiliser
#/?000Sq Ft.
Fertilizer
�/7000Sq Ft �
Fertilizer
, #H0005gyFFt•:
Fertilizer �'`
6
21-0-0
6
21-0-0
6
21-0-0
Lawn
• The amount of fertilizer recommended on the first page is the total amount needed for the entire growing season. Split into 3-4
applications to keep the lawn green and prevent fertilizer loss. You should not apply more than 0.7 Ibs of soluble nitrogen per 1000
square feet in a 30 day period. Or more than 0.9 Ibs of nitrogen per 1000 square feet if you are using a slow or controlled release
product in a 30 day pedod.Custom blend is best to meet exactly the requirement, if this is impossible, the above specific fertilizer
application is a general guideline, if the specified grades can not be found, replace with fertilizer having similar N:P:K ratio. The best
time to apply fertilizer for cool season grass (bluegrass, fescue, ryegrass) is in the Fall when the grass is growing. For Mid -Atlantic
region the time is from late August to November. For Northeast region the time is from mid August to October. Fall application should
start as soon as the day time high temperature is below 80-85F, apply with the interval of one month. If you start application late in the
Fall and do not finish all three applications, repeat the same applications in the Fall of next year. Spring application is recommended
when exceptional fertilizer loss due to heavy spring rain leaching and the grasses look pale green. Spring application can start as soon
as the grass starts to grow in April. In the case of exceptional warm spring, the application can be made earlier.
• To reduce soil pH apply 2.5 pounds of elemental sulfur per 1000 square feet for every 0.1 of pH unit above 7.2. For example, a soil
pH of 7.4 requires 5 pounds of elemental sulfur (0.2 * 2.5). Do not apply more than 5 Ibs per 1000 square feet per application or more
than 10 Ibs of elemental sulfur per 1000 square feet per year. Timing between applications should be minimum of 31months. Warm
temperature and moist soil are needed for sulfur to reduce soil pH. If sulfur is applied in winter or under drought conditions, it will take
longer for the the soil pH to be lowered.
Use ammonium sulfate as all or portion of the N requirement to reduce pH.
For a more in depth explanation of the soil test and recommendations, go to our website www.aleastem.com and select the "Lawn
and Garden" tab at the top of home page. Under the "How to Understand a Soil Test Report" header you will find the link to the article
"Soil Test Report & Fertilizer Recommendation Explained".
Prom., m° oawr
Analysis prepared by: A&L Eastern Laboratories, Inc. Pauric McGroary

t
Y A&L Eastern Laboratories
7621 Whnepine Road Richmond, inla 23237 Nify [phone] Fax [phone]
www.aleastern.com
Ma�S 14,
auumineu my: MIl;NAtzL
LAUU
6/3/2014
§OIL ANALYSIS
Client:
EARTH ENVIRONMENTAL SVCS
Grower:
SOIL SITES 1 & 2
Report No:
14-153-0592
Cust No:
46220
75 BISON LN
Date Printed:
06l03l2014
MURPHY NC 28906
Date Received
: 06/02/2014
Date Analysis :
06/03/2014
PO:
I
Page:
3 of 4
t_ao imumner : I tov l Field Id :05/28/14 Sample Id : #051427
Test
Results
SOIL TEST RATINGS
calcula'ed Cation
Exchange Capacity
Ve Low Low Medium O timum
V
Soil pH
7.1
9.7
meq/100g
Buffer pH
Phosphorus (P)
19 ppm
Calculated Cation
Saturation
Potassium (K)
134 ppm
Calcium (Ca)
1169 ppm
%K 3.5
%Ca 60.3
%Mg 35.1
%H 0.0
Hmeq 0.0
%Na 0.7
Magnesium (Mg)
408 ppm
Sulfur (S)
8 ppm
Boron (B)
0.8 ppm
Copper (Cu)
3.1 ppm
Iron (Fe)
76 ppm
Manganese (Mn)
22 ppm
Zinc (Zn)
2.7 ppm
K : Mg Ratio
Sodium (Na)
15 ppm
0.10
Soluble Salts
Ca: Mg Ratio
Organic Matter
5.4 % ENR 144
1.72 ❑
Nitrate Nitrogen
sUIL FERTILITY GUIDELINES
Crop: Lawn
(Ibs) LIME (tons)
N
P. O S
K z0
Mg
S
B
I Cu
Mn
Zn
V Fe v
0
3.5
2.5
1.0
0
0.63
0
0
0
0
0
Crop : Rec Units:
uammeni :
Analysis prepared by: A&L Eastern Laboratories, Inc.
Pam« or 6A"r
Pauric McGroary

w
A &L Eastern Laboratories
7621 Wfi tepine Road Richmond, Virginia 23237 [phone] Fax (804) 271-W5
auQma[ea esy: IVIIGF1AtL LAUD 6/3/2014 SOIL ANALYSIS
Client: Grower: Report No: 14-153-0592
EARTH ENVIRONMENTAL SVCS SOIL SITES 1 & 2 Cust No: 46220
75 BISON LN Date Printed: 06/03/2014
MURPHY NC 28906 Date Received: 06/02/2014
Date Analysis : 06/03/2014
PO: Page : 4 of 4
L-ao Numner : -i fou-i Field Id :05/28/14 Sample Id : #051427
Sl1GGESTED FERTILIZATION P120GRAM
= First Apphcatlon ,
Second Apphcatiain
4h1rd Apphcattgn
Fourth; Application w r
#/1000 SqF
tiei
0;qF
Fe tlliaer
#11000 Sq . Ft.
Fertilizer ` j
8
16-4-8
8
16-4-8
6
21-3-7
Lawn
• The amount of fertilizer recommended on the first page is the total amount needed for the entire growing season. Split into 3-4
applications to keep the lawn green and prevent fertilizer loss. You should not apply more than 0.7 Ibs of soluble nitrogen per 1000
square feet in a 30 day period. Or more than 0.9 Ibs of nitrogen per 1000 square feet if you are using a slow or controlled release
product in a 30 day period.Custom blend is best to meet exactly the requirement, if this is impossible, the above specific fertilizer
application is a general guideline, if the specified grades can not be found, replace with fertilizer having similar N:P:K ratio. The best
time to apply fertilizer for cool season grass (bluegrass, fescue, ryegrass) is in the Fall when the grass is growing. For Mid -Atlantic
region the time is from late August to November. For Northeast region the time is from mid August to October. Fall application should
start as soon as the day time high temperature is below 80-85F, apply with the interval of one month. If you start application late in the
Fall and do not finish all three applications, repeat the same applications in the Fall of next year. Spring application is recommended
when exceptional fertilizer loss due to heavy spring rain leaching and the grasses look pale green. Spring application can start as soon
as the grass starts to grow in April. In the case of exceptional warm spring, the application can be made earlier.
Use ammonium sulfate as all or portion of the N requirement to reduce pH.
For a more in depth explanation of the soil test and recommendations, go to our website www.aleastem.com and select the "Lawn
and Garden" tab at the top of home page. Under the "How to Understand a Soil Test Report" header you will find the link to the article
"Soil Test Report & Fertilizer Recommendation Explained".
Pod. IV 60wr
Analysis prepared by: A&L Eastem Laboratories, Inc.
Paudc McGroary

ROBBI (828) E9-6428 LABORATORY EARTH ENVIRONMENTAL SERVICES
[phone] GWMKI
WEAVERVILLE OFFICE MICHAEL LADD-OWNER
[phone]
FAX: [phone] P.O. BOX 2733 75 BISON LANE
RESIDENCE [phone] WEAVERVILLE, NC 28787 MURPHY, NC 28906
FAUX: [phone]
Client: v\. c c-VS
G E/�� �%u/'� I" Report To:
Address: ! >� . 8- 0)6 3 & O Bill To: Y14 �` f
�4 P.O. # / Billing Reference:
Phone: O L�-- b/' 04�6?FAX #: 19 a.R- _row
009266
CHAIN -OF -CUSTODY RECORD
Analytical Request -
Init Lab Temp:
Rec Lab Temp: Y
G7�
*Requested Due Dat _
LU
lop
e Sampled
CL
d
REMARKS
# SAMPLE DESCRIPTION RESID. TIME MATRIX EES. #
z
v
MEN
ME000011
SHIPMENT
OUT/DATE
METHOD ITEM
RETURNED/DATE #
RELINQUISED BY AFFILIATION
ACCEOTED BY AFFILIATION
DATE TIME
ADDITIONAL COMMENTS:
ts
SEE REVERSE SIDE FOR INSTRUCTIONS cP-oni-B

1. Complete all Client Information at top of sheet: name, address, phone, contact (person to whom -report will be
sent and contact can be made if questions arise), billing information if different from client, PO#, Project Name
and/or Project Number as it will appear on the report.
2. EES Client No., Project Manager and Project No. will be completed by EES.
3. A separate COC must be filled out for each day of sample collection.
4. Sampler should print their name in the space provided and sign their name followed by the datelof the sampling.
event.
5. Complete Sample Description* as it will appear on the laboratory report; include time of sampling, sample m6trix,.,.
no. of containers and container types.
6. Analyses Requested: Complete analyses on the lines provided and place a check ii the column for the samples
requiring the analysis. It may be necessary to use the -space provided for additional comments or include
attachment for extended lists of parameters.
iiiIIIIIIIII II�IJIII�Ii 111 11111 IIIIIII;Iir:� I 11 11111 1
8. Submission of samples to laboratory: Indicate Item Number of those samples being transferred; sign
relinquished by, and include your affiliation.
Standard Turnaround Time is 3-4 Weeks. If this does not satisfy your requirements, arrangements must be
made prior to samples being submitted to the laboratory. Contact your project manager.
I
Special Proiect Requirements such as Low Level Detection Limits or level or QC reported must be indicated on
the chain of custody. (Use Additional Comments Section.)

ROBBI (828) E9-6428 LABORATORY EARTH ENVIRONMENTAL SERVICES
[phone]
WEAVERVILLE OFFICE MICHAEL LADD-OWNER
[phone]
FAX: [phone] P.O. BOX 2733
RESIDENCE [phone] WEAVERVILLE, NC 28787
FAX: [phone]
Client:
Address: ■ O c 6 .W 3 bg
■"" /0 L-a?S y
Phone: Er cgs
75 BISON LANE
MURPHY, NC 28906
ReportTo: kio�,Q"t 9-6i"t 6
Bill To: 0 m
P.O. # / Billing Reference:
FAX#: �$— C�c��`�333
CHAIN -OF -CUSTODY RECORD
Analytical Request -
Init Lab Temp:
Rec Lab Tock
-4—
*Reeppu ue Date:
179 A v
San�7 Br (print):
W
cc
1111111
•
• I
ITEM CL
# SAMPLE DESCRIPTION RESID. TIME MATRIX EES. #
•
• , .
� • ���=� 1 W.
0 Mo. -
■■■
t,
L■�!■■■■■■■■ll
■
■■11■■0■
SHIPMENT METHOD ITEM
OUT/DATE RETURNED/DATE #
RELINQUISEDBY/ AFFILIATION
ACCEPTED BY/
DATE TIME
ADDITIONAL COMMENTS:
■
If
SEE REVERSE SIDE FOR INSTRUCTIONS cP-0771-B

Complete all Client Information at top of sheet: name, address, phone, contact (person to whom report will be
sent and contact can be made if questions arise), billing information if different from client, PO#, Project Name
and/or Project Number as it will appear on the report.
2, EES Client No., Project Manager and Project No. will be completed by EES.
3. A separate CbC must'be'filled out for each day of sample collection.
4. Sampler should print their name in the space provided and sign their name followed by the date of the sampling
event.
5. Complete Sample Description- as it will appear on the laboratory report.;, include time of sampling, sample matrix,
no. of containers and container types.
6. Analyses Requested: Complete analyses on the lines provided and place a check in the column for the samples
requiring the analysis. It may be necessary to use the space provided for additional comments or include
attachment for extended lists of parameters.
7. Indicate method of shipment used for return of samples and date sent.
8. Submission of samples to laboratory: Indicate Item Number of those samples being transferred; sign
relinquished by, and include your affiliation.
*IMPORTANT NOTE:
Standard Turnaround Time is 3-4 Weeks. If this does not satisfy your requirements, arrangements must be
made prior to samples being submitted to the laboratory. Contact your project manager.
Special Project
ject Requirements such as Low Level Detection Limits or level or QC reported must be indicated on
the chain of custody. (Use Additional Comments Section.)

Parker Fa* rm Supply, Inc. .
1028. US Hwy 19
Mars Hill, NC 28754 N0
O
x .
Phone [phone] • Fax [phone]'
Feed, Seed, Fertilizer, Lime
Culvert Pipe. Veterinary Sunnlies
_
ONE
DATE
NAME ---
1P
ADDRESS
SOLD BY
CASH CHARGE
C.O.D.
QTY.
DESCRIPTION
PRICE
AMOUNT
4w
13
46
.708fd4`" 33&0
77777
TAX
ZECEIVED BY
TOTAL
Purchaser agrees to Pay all -costs of collecting or securing or
attempting to collect or secure this amount. including a
reasonable attoiney's fee, whether the same is to be
collected or secured by suit or otherwise.
PAST DUE ACCOUNTS ARE SUBJECT TOASERVICE
CHARGE OF 1 1/2% PER MONTH ON THE UNPAID '
PAST DUE BALANCE. 18% ANNUALLY.
a
Statement
Date
11/24/2014
Amount Due Amount Enc.
$3,472.63
Amount Balance
3,472.63
CURRENT
1-30 DAYS PAST
DUE
31-60 DAYS PAST
DUE
61-90 DAYS PAST
DUE
OVER 90 DAYS
PAST DUE
3,472.63
0.00
0.00
0.00
0.00
Amount Due
$3,472.63

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
• ' Facplity Name:
WWTP Name:
Town of Mars Hill
Town of Mars Hill'WWTP
Permit Number: WQ0004298
NPDES Number: NCO057151
Monitoring Period: From 1/1/2014 To 12/31/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A
Alternative 1 D
Alternative 2
Alternative 3 13dl�
X,
z £'
Alternative 40
Alternative 5
Alternative 6
k
ur l
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 13
Heat Drying ®
Heat Treatment E-3
Thermophilic
Beta Ray 0Gamma
Ray
Pasteurization{
Class B:
Alternative 1R
Alternative 2 [-1
Alternative 3
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":z
Lime Stabilization 0
Air Drying ®
Composting 0
Aerobic Digestion Re
Anaerobic DigestionO
=1 1 } $ `_ �
A"':
.GR.< '^'-- \ a 3,�Ai 2 ... k"` - iy, .xi [ A -
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level
Pathogen Density
g �
Number o
Frequency
Sample
Analytical
Parameter
in Sludge
Excee-
dences
of Analysis
Type
Tech-niqu
inimu
Geo. Mean
axim
Units
2 x 10 to the 6th
power MPN per
29000
13000
5000
col/gram
0
1/year
grab
9222d
gram of total
solids or 2 x 10 to
Fecal Coliform
the 6th power
CFU per gram of
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
3 MPN per 4
(in lieu of fecal
grams total solid
coliform)
I (dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 Option 2 0 Option 3 0 Option 4 2 Option 5�
Option 6 0 Option 7 0 Option 8 0 Option 9 0 Option 1013
'`
No vector attraction reduction options were performed -Ink - .F Y P
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Robert M Sams- Public Works Director
Prep ame and Title (type or print)
Land Applier Name and Title (if applicable)(type or print)

, is
Time
(minutes)
0
2
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Mars Hill
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WO004298
10-Apr
14.5
4/10/2014 14:15
Michael Ladd
4/10/2014 14:15
Michael Ladd
1000
0.85
14.5
14.2
Dissolved Oxygen Level
4.
4.
4.
4.
4.
4
4.
3.
3.
3
3.
3.
3
3.
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
4.8
1.0
6.17 mg Oxygen/hr
0.73 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 1.09 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

N.
5
4
0 2
1
U
Oxygen Uptake Rate Chart y =-0.1029x + 4.9018
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)
I

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
4.64
4.39
4.32
4.24
4.18
4.1
4.02
3.88
3.82
3.74
3.69
3.6
3.57
Slope:
Intercept:
Correlation Coefficient:
13.9
5/15/2014 14:05
Michael Ladd
5/15/2014 14:05
Michael Ladd
1000
0.79
13.9
13.7
0.1
4.5
1.0
milliliters
% Dry Solids
degrees Celsius
deqrees Celsius
Oxygen Uptake Rate: 4.76 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.60 mg Oxygen/g/hr
Average Temperature: 14 degrees Celsius
Temperature Correction Factor: 1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 0.90 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

5
4.5
4
3.5
a�
E 3
c
d
a�
'�.5
O
m
o 2
m
_N
a
1.5
1
0.5
0
y =-0.0793x + 4.578
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)
u

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility
Biosolids Permit N
Digester Temperatu
Sampling Date/Tin
Sampled I
Analysis Date/Tin
Analyzed I
Sample Volun
Total Solii
Beginning Temperatu
End Temperatu
Specific Oxygen Uptake Rate
SOUR
e: Mars Hill
w: WO004298
e: 19-Jun
e: 16.5
e: 6/19/2014 13:10
;y: Michael Ladd
e: 6/19/2014 13:10
;y: Michael Ladd
e: 1000 milliliters
s: 0.91 % Dry Solids
e: 16.5 degrees Celsius
e: 16.2 degrees Celsius
Dissolved Oxygen Level
3.
.511
9
Slope: 0.1
Intercept: 4.5
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 5.02 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.55 mg Oxygen/g/hr
Average Temperature: 16 degrees Celsius
Temperature Correction Factor: 1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 0.72 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

5
4.5
4
3.5
a�
E 3
0
1.5
1
0.5
0
Oxygen Uptake Rate Chart Y =-0.0836x + 4.5695
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Mars Hill
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
3.3
3.21
3
2
18-Jul
18.3
07/18/2014 11:15
el Ladd
/2014 11:15el Ladd
1000 milliliters
0.9 % Dry Solids
18.3 degrees Celsius
17.9 degrees Celsius
Slope: 0.1
Intercept: 3.4
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 4.96 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.55 mg Oxygen/g/hr
Average Temperature: 18 degrees Celsius
Temperature Correction Factor: 1.1449
Temperature Corrected Specific Oxygen Uptake Rate: 0.63 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

r-
rM�
4
3.5
t]
&.5
E
c
a�
a�
x 2
m
0
N.5
0
1
0.5
I
Oxygen Uptake Rate Chart y =-0.0826x + 3.4963
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

t . • ,
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Kl
2.
Slope:
Intercept:
Correlation Coefficient:
18.4
8/12/2014 11:40
Michael Ladd
8/12/2014 11:40
Michael Ladd
1000
0.85
18.4
18.3
0.1
3.8
1.0
Aliliters
6 Dry Solids
egrees Celsius
eqrees Celsius
Oxygen Uptake Rate: 3.64 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.43 mg Oxygen/g/hr
Average Temperature: 18 degrees Celsius
Temperature Correction Factor: 1.1449
Temperature Corrected Specific Oxygen Uptake Rate: 0.49 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

4
3.5
3
&.5
E
c
m
K 2
m
0
y .5
0
1
M
IQ
y =-0.0607x + 3.8323
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

0 e 9/. A
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Mars Hill
Biosolids Permit Number: WQ0042
Date:
Digester Temperature:
Sampling Date/Time: 9/17/;
Sampled By: Michael
Analysis Date/Time: 9/17P
Analyzed By: Michael
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
4.12
4.03
3.911
3.741
17-S
4 14:
Ladd
1000 milliliters
0.81 % Dry Solids
18 degrees Celsius
17.7 degrees Celsius
Slope: 0.1
Intercept: 4.1
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 3.54 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.44 mg Oxygen/g/hr
Average Temperature: 18 degrees Celsius
Temperature Correction Factor: 1.1449
Temperature Corrected Specific Oxygen Uptake Rate: 0.50 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

4.5
4
3.5
3
rn
E
3?.5
a�
x
O
2
m
0
0
N
�wl
1
0.5
C
Oxygen Uptake Rate Chart y =-0.0589x + 4.1603
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

e6 w
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Mars Hill
Biosolids Permit Number: WO004298
Date: 21
Digester Temperature:
Sampling Date/Time: 10/23/2014
Sampled By: Michael Ladd
Analysis Date/Time: 10/23/2014
Analyzed By: Michael Ladd
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
4.
Kl
K3VA
Slope:
Intercept:
Correlation Coefficient:
1:05
1
0.1
4.1
1.0
milliliters
% Dry Solids
degrees Celsius
decrees Celsius
Oxygen Uptake Rate: 3.61 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.48 mg Oxygen/g/hr
Average Temperature: 17 degrees Celsius
Temperature Correction Factor: 1.225043
Temperature Corrected Specific Oxygen Uptake Rate: O S mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

4.5
ILI
3.5
3
o)
E
P.5
a�
x
O
a 2
m
0
Q .5
1
0.5
Fi
y =-0.0601 x + 4.193
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

EARTH ENVIRONMENTAL SERVICES
75 Bison Lane
Murphy, NC 28906
Residence — [phone]
Robbinsville Lab — [phone]
Weaverville Lab — [phone]
Fax — [phone]
E-Mail — earthenvserna,webworkz.com\
February 9, 2015
NC ID #352
Mr. Robert Sams
Town of Mars Hill
P.O. Box 368
Mars Hill, NC 28754
Dear Mr. Sams:
•f
Following is a report of laboratory analyses for digester sludge samples received 1/20, 1/21, 1/22, 1/23,
1/27, 1/28, 1/29/15.
Colony Counts
# Samnle. mate ('nlifnrm Densities (cnlnniec/Pram) 0/ Tntal Snlide 1 0 ml 0 1 ml 001 ml
1
1/20/15
7,000 Colonies/Gram
1.04
5
2
0
2
1/21/15
10,000 Colonies/Gram
1.04
8
2
1
3
1/22/15
9,000 Colonies/Gram
1.03
8
2
0
4
1/23/15
5,000 Colonies/Gram
1.03
5
0
0
5
1/27/15
20,000 Colonies/Gram
1.06
17
5
1
6
1/28/15
29,000 Colonies/Gram
1.02
30
7
2
7
1/29/15
28,000 Colonies/Gram
1.03
29
8
1
Geometric mean for all seven samples: 13,000 colonies/gram. Thank you for your
business. If you have any question or need additional sample analyses performed, please
call.
Respectfully submitted,
Michael J. Ladd
Laboratory Director

ROBBINSVILLELABORATORY EARTH ENVIRONMENTAL SERVICES
[phone]
WEAVERVILLE OFFICE MICHAEL LADD-OWNER ,
,[phone]
FAX: [phone] P.O. BOX 2733 75 BISON LANE
RESIDENCE [phone] WEAVERVILLE, NC 28787 MURPHY, NC 28906
FAX: (828) 83c55-8631 j1
Client: Report To: A<pq
Address. �' D " A Bill To: l
mli/ I �y aS `% P.O. # / Billing Reference:
Phone: FAX*' �&L 9' 3 1 1
009212Y
CHAIN -OF -CUSTODY RECO_ Rb4
Analytical Request - ►'
Init Lab Temp:
Rec Lab Temp:
*Requested Due Date:._
Sampled •co
SamplerSignature Date Sampled
•
LL
w
�
ITEM CL
# SAMPLE DESCRIPTION RESID. TIME MATRIX EES.#
0
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•
MENNEN
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■M;,E=EMIIIIII
■■■■■■■■■■■
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SHIPMENT
OUT/DATE
METHOD ITEM
RETURNED/DATE #
RELINOUISED BY /AFFILIATION
ACCEPTED BY/ AFFILIATION
DATE TIME
ADDITIONAL •
0_0
" .
�p EE ttSEDE FOR; INRTRUCTI ���/j° j dcP�7x�e`�--

Complete all Client Information at top of sheet: name, address, phone, contact (person to whom report will be
sent and contact can be made if questions arise), billing information if different from client, PO#, Project Name
and/or Project Number as it will appear on the report.
2.- EES Client No., Project Manager and Project No. will be completed by EES.
3. A separate COC must be filled out for each day of sample collection.
4. Sampler should print their name in the space provided and sign their name followed by the date of the sampling
event.
5. Complete Sample Description as it will appear on the laboratory report; include time of sampling, sample matrix,
no. of containers and container types.
6. Analyses Requested: Complete analyses on the lines provided and place a check in the column for the samples
requiring the analysis. It may be necessary to use the space provided for additional comments or include
attachment for extended lists of parameters.
7. Indicate method of shipment used for return of samples and date sent.
8. Submission of samples to laboratory: Indicate Item Number of those samples being. transferred; sign
relinquished by, and include your affiliation.
Standard Turnaround Time is 3-4 Weeks. If this does not satisfv uirements arrangements must be .4our rej,
NINE"-* •t 4 A
�jpecial Proiect Reguirements such as Low Level Detection Limits or level or QC reported must be indicated an
the chain of custody. (Use Additional Comments Section.)