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HomeMy WebLinkAboutWQ0003919_Residual Annual Report 2014_20150216CITY OF KINSTON, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0003019 2014 ANNUAL REPORT a r_ City of Kinston, NC Residuals Land Application Program 2014 Annual Report TABLE OF CONTENTS 1. Certification Form, Annual Operations Summary, Facility and Land Applier Contact Information 2. Annual Residual Sampling Summary Forms, Residuals Analysis, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM Permit Number W00003919 County Lenoir Year 2014 Facility Name (as shown on permit) Kinston Regional WRF & Peachtree WWTP NPDES No. NC0024236, NCO020541 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip Part A and Part Band proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. PART A Total number of application fields in permit: 77 Total number of fields land application occurred during the year: 21 Total amount of dry tons applied during the year for all application sites: 1078.56 -Total number of acres land application occurred during the year: 274 PART B Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality X YES NO. If no, Please provide a written description why the Facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and line was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied, with (Applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the, best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Kenneth Stevens. WRF Superintendent Permittee Name and Title (type or print) Signature of Preparer* Date (if different from Permittee) Si e Signature of Land Applier Date (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9(r) DENR FORM ACF (5/2003) 2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION KINSTON, NC :CINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE MONTHNEAR AMOUNT UNIT DRY TONS UNIT April 2014 3,425.00 Y 467.30 D June 2014 350.00 Y 47.75 D July 2014 3,250.00 Y 443.43 D October 2014 1,150.00 Y 120.08 D YEARLY TOTAL 8,175.00 Y 1,078.56 D DRY METRIC TONS 423.87 43.31 402.17 108.93 978.28 2/3/2015 a 2014 ANNUAL REPORT PROJECT: FACILITY: NPDES PERMIT NUMBER: RESPONSIBLE OFFICIAL: FACILITY OPERATOR: LAND APPLIER AND PREPARER OF LAND APPLICATION ANNUAL REPORT: City of Kinston, NC Kinston Regional Water Reclamation Facility 2101 Becton Farm Road Kinston, NC 28501 (252) 939-3248 NCO024236 Kenneth Stevens, WRF Superintendent City of Kinston 2101 Becton Farm Road PO Drawer 339 Kinston, NC 28501 (252) 939-3375 Swindell Flowers Residual Management Coordinator 2101 Becton Farm Road Kinston, NC 28501 (252) 939-.3248 Synagro Central, LLC Contact: Marshall Puryear (336) 998-7150 ext. 17 1 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0003919 Laboratory Facility Name: KINSTON, NC A&L Eastern Laboratories Inc. NPDES# : NCO024236 or WQ# (residual only) WWTP Name: KINSTON REGIONAL WRF Residuals Analysis Data Product Type AEDCAK AEDCAK AEDCAK AEDCAK Date Sampled (grab) or 01/06/14 , 04/09/14 07/09/14 10/08/14 Date Composited Percent Solids 14.54 16.20 16.61 12.40 PARAMETERS (mg/kg dry weight) Arsenic 4 5 4 5 Cadmium <2 2 <2 2 Mercury 0.5 0.5 1 • 0.5 Chromium 30 48 33 35 Copper 189 321 25,1 243 Lead 25 32 21 27 Molybdenum 7 8 7 8 Nickel 15 24 18 19 Selenium - <5 <5 5 <5 Zinc 674 1020 728 844 Total Phosphorus 32400 26100 26400 33900 TKN 66200 61300 65000 62500 Ammonia -Nitrogen 4810 8770 4700 14000 Nitrate and Nitrite 8,25 29 148 76.6 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with.a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X / (SIGNATURE OF P Date 2-l19.1-5- DENR FORM RSSF (5/2003) Printed: Tuesday - February 3, 2015 at 17:08:02 for: 2060 02 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0003919 Laboratory Facility Name: KINSTON, NC A&L Eastern Laboratories Inc. NP.DES# : NCO024236 or WQ# (residual only) WWTP Name: KINSTON REGIONAL WRF Residuals Analysis Data Product Type AEDCAK AEDCAK AEDCAK AEDCAK Date Sampled (grab) or 01/06/14 04/09/14 07/09/14 10/08/14 Date Composited Percent Solids 14.54 16.20 16.61 12.40 PARAMETERS (mg/kg dry weight) Aluminum 12700 18000 13200 19000 Calcium 13500 20900 18000 18400 Magnesium 5360 4110 4650 5330 pH 6.16 7.04 7.58 8.51 Potassium 7050 3410 4200 5160 Sodium 1870 1330 1450 1630 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X (SIGNATURE OF NR - Data Not Reported or Data Not Required Date 2 lV - % r DENR FORM RSS.F-13 (7/2002) Printed: Tuesday - February 3. 2015 at 17:08:24 for: 2060 02 Page: 1 of 2 Report Number: 14-010-0207 Account Number: 46463 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAUKINSTON MARSHALLPURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27028 Lab Number: 97426 Sample Id: KINSTON A&L Eastern Laboratories, Inc._ �. 7621 Whitepine Road Richmond, Vlrginia23237 (804) 7435401 Fax (804) 271.6446 wwwaleasternAom Project: KINSTON WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/6/2014 00-00:00 Date Received: 01/10/2014 00:00 Date Reported: 01/15/2014 Total Solids 14.54 145400 100.0 JM 01/10/2014 14:19 SM-2540G Moisture * 85.46 100.0 JM 01/10/2014 14:19 SM-2540G Total Kjeldahl Nitrogen 6.62 66200 10.0 JM 01/13/2014 08:30 SM-4500-NH3C-TKN Total Phosphorus 3.24 32400 100 KM 01/13/2014 11:35 SW 6010C Total Potassium -0.71 7050 100 KM 01/13/2014 11:35 SW 6010C Total Sulfur 0.82 8170 100 KM 01/13/2014 11:35 SW 6010C Total Calcium 1.35 13500 100 KM 01/13/2014 11:35 SW 6010C Total Magnesium 0.54 5360 100 KM 01/13/2014 11:35 SW 6010C Total Sodium 0.19 1870 100 KM 01/131201411:35 SW 6010C Total Iron 10400 100 KM 01/13/2014 11:35 SW 6010C Total Aluminum 12700 100 KM, 01/13/2014 11:35 SW 6010C Total Manganese 258 5 KM 01/13/2014 11:35 SW 6010C Total Copper 189 5 KM 01/13/2014 11:35 SW 6010C Total Zinc 674 5 KM 01/13/2014 11:35 SW 6010C Ammonia Nitrogen 0.48 4810 10.0 JM 01/13/2014 08:30 SM-4500-NH3C Organic N 6.14 61390 10.0 01/13/2014 08:30 CALCULATION Nitrate+Nitrite-N 8.25 2.00 JM 01/13/2014 08:30 SM-450ONO3F Total Cadmium <2.0 2.0 KM 01/13/2014 11:35 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-010-0207 Account Number: 46463 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAL/KINSTON MARSHALLPURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27028 Lab Number: 97426 Sample Id: KINSTON L A&L Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 232V (604) 743-9401, RN (604) 271-W6 wwwaleastem.ctim Project: KINSTON WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/6/2014 00:00:00 Date Received: 01/10/2014 00:00 Date Reported: 01/15/2014 Total Chromium 30 5 KM 01/13/2014 11:35 SW 6010C Total Nickel 15 5 KM 01/13/2014 11:35 SW 6010C Total Lead 25 5 KM 01/13/2014 11:35 SW 6010C Total Arsenic 4.0 3.0 KM 01/13/2014 11:35 SW 6010C Total Mercury 0.5 0.4 KM' 01/13/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 01/13/2014 11:35 SW 6010C pH (Standard Units) * 6.16 2.00 JM 01/13/2014 08:30 SW-9045D Total Molybdenum 7 5 KM 01/13/2014 11:35 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "NO3/NO2-N" AND "Se". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "As" AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other -public announcements without obtaining our prior written authorization. Debbie Holt !I N us W�R TO S W AR'Ok- OJECTMANAGER. P -:,A_,& L C11is--T-WER LAB ',SAMP0514j, I'V Relinquish ed 4y. Sampler. SAMP - � �i�i�� �iiii ail ii�iii ����i �i��i �n� �iioii a SYt4AGROICENTPALIKINSTON KINSTON WWTP ,SAMPLE TYPE A ,OF: 'CONTAINERSI CHAI0"MA-1 OFICUSTO'Vilf 'a,A;El 45463 01-1.0-7014 11:11:15 roper fidid sari pfingpfocpdijrk j th6 vofl6tfion of these-sarnplei sAURUNG'. bETHOR, METHOD] TIME, PRES E.R'EO SHIPPED, �V , � D tr, :Time Recieiv�qd by: _r �' — '/A Ddt-c tkr�6 Redieved by. F!e64n'q-p6sh6d by:. OtO. T, Redeved'b'v:, .SPECIAL tN,, mohitbrihg, pprpq:qpq., ANAL'Ysf� rE EOU88-r -N, lid, C_ x � ) PH Oic'o it mo r, � 'CI 002-N, E5 00 Jo - T Mtn a .SILT."T,&tE&'Sdfi'ds (Moisture)., Tbtaf;f<161dahl ,Nl-trqgejjFhb��h&-6I-9and, §_QtaEswrn gCZ-BaSiCTest SL1 PL1S.SUIfUr,-- ­1 - 4gneslohi 'Si"' brA unlnuin,'Maqqavcse, Coppar,and Zj h b '-,VV -A'& _- Canary, MANNPERI:GOPY'' Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2060-02-AEDCAK-NC KINSTON, NC KINSTON REGIONAL WRF 1/6/2014 111/2014-3/3112014 1.3091 AEROB. DIGESTED CAKE Na mg/I = (Na mg/kg x % Solids) _ 100 = (1870 x 14.5400) = 100 = 271.898 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (13500 x 14.5400) _ 100 = 1962.9 Mg mg/I = (mg mg/kg x % Solids) = 100 = (5360 x 14.5400) = 100 = 779.344 Na meq = Na mg/I = Molec.Wgt.Na = 271.898 + 23 = 11.8217 Ca meq = Ca mg/I = Molec.Wgt.Ca = 1962.9 = 20 = 98.145 Mg meq = Mg mg/1 + Molec.Wgt.Mg = 779.344 = 12 = 64.9453 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 11.8217 _ SgrRoot[0.5(98.145+64.9453)] = 1.30912 Printed: 2/4/2015 Page 1 08:02 Page: 1 of 2 Report Number: 14-105-0204 Account Number: 46463 Submitted By: EDWARD STEPHENS Send To: SYNAGRO CENTRAL/KINSTON MARSHALLPURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27028 Lab Number: 98971 Sample Id : KINSTON WTP ILA&L Eastern Laboratories, Inc- -7621 Whitepine Road Richmond, Virginia 23237 (804) 74.3,9401 Fax (804) 271-8446 wwwaleastem.com, Project: KINSTON/NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/9/2014 12:30:00 Date Received: 04/15/2014 00:00 Date Reported: 04/22/2014 Total Solids.* 16.20 162000 100.0 JM 04/15/2014 14:10 SM-25400 Moisture * 83.80 100.0 JM 04/15/2014 14:10 SM-2540G Total Kjeldahl Nitrogen 6.13 61300 10.0 JM 04/16/2014 08:30 SM-4500-NH3C-TKN Total Phosphorus 2.61 26100 100 KM 04/16/2014 14:52 SW 6010C Total Potassium 0.34 3410 100 KM 04/16/2014 14:52 SW 6010C Total Sulfur 1.09 10900 100 KM 04/16/2014 14:52 SW 6010C Total Calcium 2.09 20900 100 KM 04/16/2014 14:52 SW 6010C Total Magnesium 0.41 4110 100 KM 04/16/2014 14:52 SW 6010C Total Sodium 0.13 1330 100 KM 04/16/2014 14:52 SW 6010C Total Iron 15100 100 KM 04/16/2014 14:52 SW 6010C Total Aluminum 18000 100 KM 04/16/2014 14:52 SW 6010C Total Manganese 243 5 KM 04/16/2014 14:52 SW 6010C Total Copper 321 5 KM 04/16/2014 14:52 SW 6010C Total Zinc 1020 5 KM 04/16/2014 14:52 SW 6010C Ammonia Nitrogen 0.88 8770 10.0 JM 04/16/2014 08:30 SM-4500-NI3C Organic N 5.25 52530 10.0 04/16/2014 08:30 CALCULATION Nitrate+Nitrite-N 29.0 2.00 JM 04/16/2014 08:40 SM-450ONO3F Total Cadmium 2.0 2.0 KM 04/16/2014 14:52 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , ftaA to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-105-0204 Account Number: 46463 Submitted By: EDWARD STEPHENS Send To: SYNAGRO CENTRAUKINSTON MARSHALLPURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27028 Lab Number: 98971 Sample Id : KINSTON WTP �LA&L Eastern, Laboratories, Inc._ 7621-Whitepine Road Richmond, Virginia 23237 (804) 743-9401[ Fax (804) 271-W6 www aleastem.com Project: KINSTON/NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/9/2014 12:30:00 Date Received: 04/15/2014 00:00 Date Reported: 04/22/2014 Total Chromium 48 5 KM 04/16/2014 14:52 SW 6010C Total Nickel 24 5 KM 04/16/2014 14:52 SW 6010C Total Lead 32 5 KM 04/16/2014 14:52 SW 6010C Total Arsenic 5.0 3.0 KM 04/16/2014 14:52 SW 6010C Total Mercury 0.5 0.4 KM 04/16/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 04/16/2014 14:52 SW 6010C pH (Standard Units) * 7.04 2.00 JM 04/16/2014 08:30 SW-9045D Total Molybdenum 8 5 KM 04/16/2014 14:52 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Ca", AND "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. �% i&u Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made ,L�9 to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code I Product Name Sample Date Report Range Ratio 2060-02-AEDCAK-NC KINSTON, NC KINSTON REGIONAL WRF 4/9/2014 411/2014-7/3112014 0.8836 AEROB. DIGESTED CAKE Na mg/I = (Na mg/kg x % Solids) -= 100 = (1330 x 16.2000) =100 = 215.46 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (20900 x 16.2000) = 100 = 3385.8 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (4110 x 16.2000) _ 100 = 665.82 Na meq = Na mg/I = Molec.Wgt.Na = 215.46 = 23 = 9.36783 Ca meq = Ca mg/I + Molec.Wgt.Ca = 3385.8 + 20 = 169.29 Mg meq = Mg mg/I -= Molec.Wgt.Mg = 665.82 _ 12 = 55.485 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 9.36783 + SgrRoot[0.5(169.29+55.485)] = 0.883649 Printed: 2/4/2015 Page 1 08:02 Page: 1 of 2 Report Number: 14-196-0201 Account Number: 46463 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAL/KINSTON MARSHALL PURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27028 Lab Number: 56467 Sample Id: KINSTON A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 7434401 Fax (804) 271-6446 wwwaleastem.cotn Project: KINSTON NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/9/2014 15:00:00 Date Received: 07/15/2014 00:00 Date Reported: 07/21/2014 Total Solids " 16,61 166100 100.0 BW 07/15/2014 15:00 SM-2540G Moisture * 83.39 100.0 BW 07/15/2014 15:00 SM-2540G Total Kjeldahl Nitrogen 6.50 65000 10.0 MW 07/16/2014 07:59 SM-4500-NH3C-TKN Total Phosphorus 2.64 26400 100 BW 07/16/2014 09:30 SW 6010C Total Potassium 0.42 4200 100 BW 07/16/2014 09:30 SW 6010C Total Sulfur 0.85 8460 100 BW 07/16/2014 09:30 SW 6010C Total Calcium 1.80 18000 100 BW 07/16/2014 09:30 SW 6010C Total Magnesium 0.47 4650 100 BW 07/16/2014 09:30 SW 6010C Total Sodium 0.15 1450 100 BW 07/16/2014 09:30 SW 6010C Total Iron 12500 100 BW 07/16/2014 09:30 SW 6010C Total Aluminum 13200 100 BW 07/16/2014 09:30 SW 6010C Total Manganese 371 5 BW 07/16/2014 09:30 SW 6010C Total Copper 251 5 BW 07/16/2014 09:30 SW 6010C Total Zinc 728 5 BW 07/16/2014 09:30 SW 6010C Ammonia Nitrogen 0.47 4700 10.0 MW 07/16/2014 07:59 SM-4500-NI3C Organic N 6.03 60300 10.0 07/16/2014 07:59 CALCULATION Nitrate+Nitrite-N 148 2.00 MW 07/16/2014 08:00 SM-450ONO3F Total Cadmium <2.0 2.0 BW 07/16/2014 09:30 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made%�— to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-196-0201 Account Number: 46463 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAUKINSTON MARSHALLPURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27028 Lab Number: 56467 Sample Id : KINSTON A&L Eastern Laboratories, Inc:_ 7627 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Ww aleastenixom Project: KINSTON NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/9/2014 15:00:00 Date Received:07/15/2014 00:00 Date Reported: 07/21/2014 Total Chromium 33 5 BW 07/16/2014 09:30 SW 6010C Total Nickel 18 5 BW 07/16/2014 09:30 SW 6010C Total Lead 21 5 BW 07/16/2014 09:30 SW 6010C Total Arsenic 4.0 3.0 BW 07/16/2014 09:30 SW 6010C Total Mercury 1.0 0.4 JM 07/16/2014 08:30 SW-7471 B Total Selenium 5.0 5.0 BW 07/16/2014 09:30 SW 6010C pH (Standard Units) ` 7.58 2.00 MW 07/16/2014 09:04 SW-9045D Total Molybdenum 7 5 BW 07/16/2014 09:30 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Cr". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 66�im A&d Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2060-02-AEDCAK-NC KINSTON, NC KINSTON REGIONAL WRF 7/9/2014 8/1/2014-9/30/2014 1.0127 AEROB. DIGESTED CAKE Na mg/I = (Na mg/kg x % Solids) = 100 = (1450 x 16.6100) =100 = 240.845 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (18000 x 16.6100) + 100 = 2989.8 Mg mg/I = (mg mg/kg x % Solids) = 100 = (4650 x 16.6100) + 100 = 772.365 Na meq = Na mg/I = Molec.Wgt.Na = 240.845 _ 23 = 10.4715 Ca meq = Ca mg/I = Molec.Wgt.Ca = 2989.8 = 20 = 149.49 Mg meq = Mg mg/I = Molec.Wgt.Mg = 772.365 = 12 = 64:3637 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 10.4715 + SgrRoot[0.5(149.49+64.3637)] = 1.01267 Printed: 2/4/2015 Page 1 08:02 Page: 1 of 2 Report Number: 14-289-0204 Account Number: 46463 Submitted By: WILL VARNER Send To: SYNAGRO CENTRALIKINSTON MARSHALLPURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27028 Lab Number: 58185 Sample Id : KINSTON �LA&L Eastern Laboratories, Inc.. 7621 Whitepine Road Richmond, Virginia 23237 .(804) 743-9401 Fax (804) 271-6446 wwwaleastem.com Project :XINSTON NC CERT#257 REPORT OF ANALYSIS Date Sampled: 10/8/2014 15:30:00 Date Received: 10/16/2014 00:00 Date Reported: 10/22/2014 Total Solids ` 12.40 124000 100.0 BW 10/16/2014 14:39 SM-2540G Moisture * 87.60 100.0 BW 10/16/2014 14:39 SM-2540G Total Kjeldahl Nitrogen 6.25 62500 10.0 JM 10/17/2014 09:20 SM-4500-NH3C-TKN Total Phosphorus 3.39 33900 100 KM 10/20/2014 12:46 SW 6010C Total Potassium 0.52 5160 100 KM 10/20/2014 12:46 SW 6010C Total Sulfur 0.81 8070 100 KM 10/20/2014 12:46 SW 6010C Total Calcium 1.84 18400 100 KM 10/20/2014 12:46 SW 6010C Total Magnesium 0.53 5330 100 KM 10/20/2014 12:46 SW 6010C Total Sodium 0.16 1630 100 KM 1'0/20/2014 12:46 SW 6010C Total Iron 17900 100 KM 10/20/2014 12:46 SW 6010C Total Aluminum 19000 100 KM 10/20/2014 12:46 SW 6010C Total Manganese 368 5 KM 10/20/2014 12:46 SW 6010C Total Copper 243 5 KM 10/20/2014 12:46 SW 6010C Total Zinc 844 5 KM 10/20/2014 12:46 SW 6010C Ammonia Nitrogen 1.40 14000 10.0 JM 10/17/2014 09:20 SM-4500-NH3C Organic N 4.85 48500 10.0 10/17/2014 09:20 CALCULATION Nitrate+Nitrite-N 76.6 2.00 JM 10/22/2014 08:20 SM-450ONO3F Total Cadmium 2.0 2.0 KM 10/20/2014 12:46 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-289-0204 Account Number: 46463 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAL/KINSTON MARSHALLPURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27028 Lab Number: 58185 Sample Id : KINSTON �yL A&L Eastern Laboratories, Inc:_ 7621 whitepine Road Richmond, Virginia 23237 (604) 7433401 Fax (604) 271-6946 wwwaleastern.com Project : KINSTON NC CERT#257 REPORT OF ANALYSIS Date Sampled: 10/8/2014 15:30:00 Date Received: 10/16/2014 00:00 Date Reported: 10/22/2014 Total Chromium 35 5 KM 10/20/2014 12:46 SW 6010C Total Nickel 19 5 KM 10/20/2014 12:46 SW 6010C Total Lead 27 5 KM 10/20/2014 12:46 SW 6010C Total Arsenic 5.0 3.0 KM 10/20/2014 12:46 SW 6010C Total Mercury 0.5 0.4 KM 10/17/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 10/20/2014 12:46 SW 6010C pH (Standard Units)'* 8.51 2.00 JM 10/17/2014 09:20 SW-9045D Total Molybdenum 8 5 KM 10/20/2014 12:46 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Fe", "P", "Se", "S", "NH4-N". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2060-02-AEDCAK-NC KINSTON, NC KINSTON REGIONAL WRF 10/8/2014 10/112014-12/31/2014 0.9555 AEROB. DIGESTED CAKE Na mg/I = (Na mg/kg x % Solids) _ 100 = (1630 x 12.4000) = 100 = 202.12 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (18400 x 12.4000) _ 100 = 2281.6 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (5330 x 12.4000) = 100 = 660.92 Na meq = Na mg/I = Molec.Wgt.Na = 202.12 = 23 = 8.78783 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 2281.6 _ 20 = 114.08 Mg meq = Mg mg/I t- Molec.Wgt.Mg = 660.92 = 12 = 55.0767 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 8.78783 = SgrRoot[0.5(114.08+55.0767)] = 0.955547 Page 1 Printed: 2/4/2015 08:02 FACILITY NAME: KINSTON, NC OWNER: KENNETH JONES SITE #: NC JO 00001 FIELD# : JO 00001 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00003919 ANNUAL DRY TONS APPLIED: 51.38 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 12.50 ACRES PERMITTED: 12.50 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/16/14 300.00 (CY) 24.000 16.20 3.275 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 CORN Apr-14 300.00 (CY) 24.000 11/23114 100.00 (CY) 8.0001 12.40 0.835 MOIST 0-<1/2" SUR 0.5 0.30 62,500. p 14,000.00 p 76.60 p 21627 1 WHEAT Oct-14 100.00 (CY) 8.000 JKDCRAED( I Total Cubic Yds/Ac: 32.00 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 132 Annual lbs/acre 0.041 0.016 0.373 2.508 0.255 0.004 0.066 0.189 0.041 8.090 227.58 36 Cumulative lbs/acre 0.041 0.016 1 0.373 2.508 1 0.255 1 0.004 0.066 1 0.189 0.041 8.090 7" Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop "R „ 160 50 FD Cumulative Pollutant LoadingRate Limit lbs/acre ( ) 36.6 34.8 1339.0 267.9 15 0 375.0 89.0 2500.0 ' ; , r s KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation _ 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: KENNETH JONES SITE #: NC JO 00001 FIELD# : JO 00001 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00003919 ANNUAL DRY TONS APPLIED: 64.22 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 15.30 ACRES PERMITTED: 15.30 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/14/14 25.00 (CY) 1.634 16.20 0.223 KIIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300.p .8,770.00 p 29.00 p 20173 CORN 4/15/14 325.00 (CY) 21:242 16.20 2.898 KIIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300.p 8,770.00 p 29.00 p 20173 I CORN 4/16/14 25.00 (CY) 1.634 16.20 0.223 KIICRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 CORN Apr-14 375.00 (CY)l 24.510 10/23/14 125.00 (CY) 8.1701 12.40 0.853 KIICRAED( MOIST 0-<1/2" SUR 0.5 0.30 62,500. p 14,000.00 p 76.60 p 21621 WHEAT Oct-14 125.00 (C 1 8.170 I 1 Total Cubic Yds/Ac: 32.68 As Cd Cr Cu Pb . Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.042 0.017 0.381 2.562 0.260 0.004 0.067 0.193 0.042 8.262 232.41 135 37 Cumulative lbs/acre 0.042 Q,017 0.381 2.562 0.260 0.004 0.067 0.193 0.042 8.262 77 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop c 160 50 t FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8` r 1339.0 267.9 15.0 375.0 89.0 2500.0 * n; Y K KRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: KENNETH JONES SITE #: NC JO 00001 FIELD# : JO 00001 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00003919 ANNUAL DRY TONS APPLIED: 25.69 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 6.60 ACRES PERMITTED: 6.60 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/16/14 150.00 (CY) 22.727 16.20 3.101 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300.p 8,770.00 p 29.00 p F 20173 CORN Apr-14 150.00 (CY) 22.727 10/23/14 50.00 (CY) 7.5761 12.40 0.791 MOIST 0-<1/2" SUR 0.5 0.30 62,500. p 14,000.00 p 76.60 p 21627 WHEAT Oct-14 50.00 (CY) 7.576 1KIKRAED( I Total Cubic Yds/Ac: 30.30 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 125 Annual lbs/acre 0.039 0.016 0.353 2.375 0.241 0.004 0.062 0.179 0.039 7.661 215.51 34 Cumulativelbs/acre 0.039 0.016 0.353 2.375 0.241 0.004 0.062 0.179 0.039 7.661 E_, ' µ..: Permit PAN Limit 1st Crop/2nd Crop 160 (Ibs/acre) `.., 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 i KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRY AEROB. DIGESTED CAKE Xs - (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: KENNETH JONES SITE #: NC JO 00001 FIELD# : JO 00001 0004 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: WQ0003919 ANNUAL DRY TONS APPLIED: 16.26 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 4.10 ACRES PERMITTED: 4.10 Page Lane Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/14/14 100.00 (CY) 24.390 16.20 3.328 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 CORN Apr-14 100.00 (CY) 24.390 10/23/14 25.00 (CY) 6.0981 12.40 0.637 �KIKRAED( MOIST 1 0-<1/2" SUR 1 0.5 0.30 62,500. p 14,000.00 p 76.60 p 21627 1 WHEAT Oct-14 25.00 (CY) 6.098 lotai uunic Yos/AC: 3U.4`J As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.040 0.016 0.364 2.446 0.247 0.004 0.063 0.184 0.040 7.864 216.89 134 28 Cumulative Ibs/acre 0.040 0.016 1 0.364 2.446 1 0.247 0.004 0.063 1 0.184 0.040 7.864 ..# Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop J ' 160 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE S- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/lcg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: KENNETH JONES SITE #: NC JO 00001 FIELD# : JO 00001 0005 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: WQ0003919 ANNUAL DRY TONS APPLIED: 12.84 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 3.70 ACRES PERMITTED: 3.70 Page: I Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (VT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/14/14 75.00 (CY) 20.270 1 16.20 2.766 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 CORN Apr-14 75.00 (CY) 20.270 10/23/14 25.00 (CY) 6.7571 12.40 0.706 1K1KRAED( I MOIST 0-<1/2" SUR 0.5 0.30 62,500.p 1 14,000.00 p 76.60 p 21627 1 WHEAT Oct-14 25.00 (CY) 6.757 Total Cubic Yds/Ac: 27.03 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 112 Annual Ibs/acre 0.035 0.014 0.315 2.119 0.215 0.003 0.056 0.160 0.035 6.833 192.21 31 Cumulative Ibs/acre 0.035 1 0.014 0.315 2.119 1 0.215 0.003 0.056 1 0.160 0.035 6.833 F d 160 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 (� . tt 1339.0 267.9 15.0 375.0 89.0 2500.0" KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: KENNETH JONES SITE #: NC JO 00001 FIELD# : JO 00001 0006 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: WQ0003919 ANNUAL DRY TONS APPLIED: 12.84 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 3.60 ACRES PERMITTED: 3.60 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total FP,, Acre Solids 4/14/14 75.00 (CY) 20.833 16.20 2.843 K]KRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 21173 CORN Apr-14 75.00 (CY) 20.833 10/23/14 25.00 (CY) 6.9441 12.40 0.725 MOIST 0-<1/2" SUR 0.5 0.30 62,500. p 14,000.00 p 76.60 p 21627 WHEAT Oct-14 25.00 (CY)l 6.944 IKHU?,AED( I 1 1 1 1 1 iorait_uoic ras/Ac: ci:is As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.036 0.014 0.324 2.177 0.221 0.004 0.057 0.164 0.036 7.023 197.55 115 31 Cumulative lbs/acre 0.036 1 0.014 1 0.324 1 2.177 1 0.221 0.004 0.057 1 0.164 0.036 7.023`' y Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop a 160 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 KIKRARDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: ICENNETH JONES SITE #: NC JO 00001 FIELD# : JO 00001 0008 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: WQ0003919 ANNUAL DRY TONS APPLIED: 51.38 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 12.70 ACRES PERMITTED: 12.70 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/3/14 200.00 (CY) 15.748 16.20 2.149 KIKRAED( MOIST 0-<I/2" SUR 0.5 0.30 61,300.p 8,770.00 p 29.00 p F 20173 I CORN 4/4/14 100.00 (CY) 7.874 16.20 1.074 KIKRAED( DRY 0-<1/2" SUR 0.5 0.30 61,300.p 8,770.00 p 29.00 p 20173 CORN Apr-14 300.00 (CY) 23.622 10/23/14 100.00 (CY) 7.8741 12.40 0.822 KIKRAED( MOIST 0-<1/2" SUR 0.5 1 0.30 62,500. p 14,000.00 p 76.60 p 21627 WHEAT Oct-14 100.00 (CY) 7,874 1 1 1 VL"411.uu1c iuv[-�c. J1.Ju As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 130 0.040 0.016 0367 2.469 0.251 0.004 0.065 0.186 0.040 7.963 224.00 36 Cumulative lbs/acre 0.040 0.016 1 0.367 2.469 1 0.251 0.004 0.065 1 0.186 0.040 7.963 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop , - a . 160 r 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 "�,'' 1339.0 267.9 15.0 375.0 89.0 2500.0 i- Al KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE N' " (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Hijection/Incorporation 1.0 Application Method: SUR - Surface,' INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: KENNETH JONES SITE #: NC JO 00001 FIELD# : JO 00001 0009 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00003919 ANNUAL DRY TONS APPLIED: 41.94 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 10.50 ACRES PERMITTED: 10.50 Page: 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Are Solids 4/4/14 250.00 (CY) 23.810 16.20 3.249 KII{RAED( DRY 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 CORN Apr-14 250.00 (CY) 23.810 10/23/14 50.00 (CY) 4.762 12.40 0.497 KIICRAED( MOIST 0-<1/2" SUR 0.5 0.30 62,500. p 14,000.00 p 76.60 p 21627 I WHEAT 10/24/14 25.00 (CY) 2.381 12.40 0.249 KJKRAED( MOIST 0-<1/2" SUR 0.5 0.30 62,500. p 14,000.00 p 76.60 p 21627 WHEAT Oct-14 75.00 (CY) 7.143 i otai uumc r us/Ac: su.» As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.040 0.016 0.364 2.448 0.248 0.004 0.064 0.184 0.040 7.886 220.15 131 32 Cumulative lbs/acre 0.040 0.016 0.364 2.448 0.248 0.004 0.064 0.184 0.040 7.886 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 160 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 KIICRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false, information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: KENNETH JONES SITE"#: NC JO 00001 FIELD# : JO 00001 0010 A RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00003919 ANNUAL DRY TONS APPLIED: 112.19 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 26.60 ACRES PERMITTED: 26.60 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/2/14 275.00 (CY) 10.338 16.20 1.411 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300.p 8,770.00 p 29.00 p 20173 I CORN 4/3/14 375.00 (CY) 14.098 16.20 1.924 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 21173 CORN Apr-14 1 650.00 (C]) 24.436 10/22/14 200.00 (CY) 7.519 12.40 0.785 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 62,500. p 14,000.00 p 76.60 p 21627 I WHEAT 10/23/14 25.00 (CY) 0.940 12.40 0.098 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 62,500. p 14,000.00 p 76.60 p 21627 WHEAT Oct-14 225.00 (CY) 8.459 Total Cubic Yas/Ac: 32.89 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.042 0.017 0.382 2.570 0.261 0.004 0.067 0.194 0.042 8.293 233.93 135 38 Cumulativelbs/acre 0.042 0.017 0.382 2.570 0.261 0.004 0.067 0.194 0.042 8.293 160 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 KIKR AFDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]crowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: KENNETH JONES SITE #: NC JO 00001 FIELD# : JO 00001 0010 B RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00003919 ANNUAL DRY TONS APPLIED: 131.05 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 30.40 ACRES PERMITTED: 30.40 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/1/14 450.00 (CY) 14.803 16.20 2.020 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00. p 29.00 p 20173 I CORN 4/2/14 300.00 (CY) 9.868 16.20 1.346 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20171 CORN Apr-14 1 750.00 (Cl) 24.671 10/22/14 200.00 (CY) 6.579 12.40 0.687 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 62,500. p 14,000.00 p 76.60 p 21627 I WHEAT 10/24/14 75.00 (CY) 2.467 12.40 0.258 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 62,500. p 14,000.00 p 76.60 p 21627 WHEAT Oct-14 275.00 (CY) 9.046 Total Cubic Yds/Ac: 33.72 As Cd Cr Cu Pb Hg Mo Ni Sc Zn P PAN TOTALS: 136 Annual lbs/acre 0.043 0.017 0.389 2.620 0.266 0.004 0.069 0.197 0.043 8.462 239.77 41 Cumulative lbs/acre 0.043 0.017 0.389 2.620 0.266 0.004 0.069 0.197 0.043 8.462 7 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 160 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0*? KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: KENNETH JONES SITE #: NC JO 00001 FIELD# : JO 00001 0011 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00003919 ANNUAL DRY TONS APPLIED: 41.94 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 10.00 ACRES PERMITTED: 10.00 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or % Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/4/14 125.00 (CY) 12.500 16.20 1.706 KIKRAED( DRY 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 I CORN 4/14/14 125.00 (CY) 12.500 16.20 1.706 KIICRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20113 CORN Apr-14 250.00 (CY) 25.000 10/24/14 75.00 (CY) 7.5001 12.40 0.783 KIKRAED( MOIST 0-<1/2" SUR 1 0.5 0.30 1 62,500. p 1 14,000.00 p 76.60 p 21627 WHEAT Oct-14 75.00 (CY) 7.500 I 1 1 1 Total Cubic Yds/Ac: 32.50 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 138 Annuallbs/acre 0.042 0.017 0.382 2.571 0.261 0.004 0.067 0.194 0.042 8.281 231.16 34 Cumulative lbs/acre 0.042 0.017 0.382 2.571 0.261 0.004 0.067 0.194 0.042 8.281 777 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop 160 >, 50 % FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: KINSTON, NC OWNER: KENNETH JONES PERMIT #: W00003919 ANNUAL DRY TONS APPLIED: 25.69 SITE #: NC JO 00001 FIELD# : JO 00001 0012 OPERATOR: RODNEY SMITH CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.50 ACRES PERMITTED: 6.50 Page: 1 Lune Applied *** Date Us* allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/4/14 50.00 (CY) 7.692 16.20 1.050 KIKRAED( DRY 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p F 20173 I CORN 4/14/14 100.00 (CY) 15.385 16.20 2.099 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 CORN Apr-14 150.00 (CY) 23.077 10/24/14 50.00 (CY) 7.6921 12.40 0.803 MOIST 1 0-<1/2" SUR 0.5 0.30 62,500.p 14,000.00 p 76.60 p 21627 WHEAT Oct-14 50.00 (CY) 7.692 1KIKRAED,( Total Cubic Yds/Ac: 30.77 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 127 Annual lbs/acre 0.040 0.016 0.359 2.412 0.245 0.004 0.063 0.182 0.040 7.779 218.83 35 Cumulative lbs/acre 0.040 0.016 0.359 2.412 1 0.245 0.004 0.063 1 0.182 0.040 7.779 w, 160 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop W,V,50 m..w FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 0375.0 89.0 2500.0 KII<RAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: W B HARGETT SITE #: NC JO 02944 FIELD# : JO 02944 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: WQ0003919 ANNUAL DRY TONS APPLIED: 30.70 OPERATOR: DEXTER EDWARDS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 10.40 ACRES PERMITTED: 10.40 Page : 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 7/2/14 225.00 (CY) 21.635 16.20 2.952 KlKRAED( DRY 0-<1/2" SUR 0.5 0.30 1 61,300. p 8,770.00 p 29.00 p 20173 BERMUDAGRASS Jul-14 225.00 (CY) 21.635 1 Mal l.UUIU IUW/ U. L1.UJ As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 119 0.030 0.012 0.283 1.895 0.189 0.003 0.047 0.142 0.030 6.022 154.09 Cumulative lbs/acre 0.260 0.171 2.553 18.103 2.411 0.049 0.759 1.274 0.220 53.359 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop 220 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE x 2 l (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: W B HARGETT SITE #: NC JO 02944 FIELD# : JO 02944 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: WQ0003919 ANNUAL DRY TONS APPLIED: 40.93 OPERATOR: DEXTER EDWARD_S CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 12.50 ACRES PERMITTED: 12.50 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 7/1/14 275.00 (CY) 22.000 16.20 3.002 KIKFAED( DRY 0-<I/2" SUR 0.5 0.30 61,300.p 8,770.00 p 29.00 p 20173 IBERMUDAGRASS 7/2/14 25.00 (CY) 2.000 16.20 0.273 KIKRAED( DRY 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 BERMUDAGRASS Jul-14 1 300.00 (CY) 24.000 rota[ uuoic Yas/Ac: 24.U0 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.033 0.013 0.314 2.102 0.210 0.003 0.052 0.157 0.033 6.680 170.93 132 Cumulative lbs/acre 0.175 0.087 1.671 11.819 1.389 0.023 0.363 0.846 0.168 36.448 1 Permii PAN Limit (lbs/acre) I st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 K ,CRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: W B HARGETT SITE #: NC JO 02945 FIELD# : JO 02945 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00003919 ANNUAL DRY TONS APPLIED: 20.47 OPERATOR: DEXTER EDWARDS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 5.60 ACRES PERMITTED: 5.60 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PALL DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 7/2/14 150.00 (CY) 26.786 16.20 3.655 KIKRAED( DRY 0- 1/2" SUR 0.5 0.30 61,300. p 8,770.00 77 29.00 p 20173 BERMUDAGRASS Jul-14 150.00 (CY) 26.786 Total Cubic Yds/Ac: 26.79 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Amoral lbs/acre 0.037 0.015 0.351 2.346 0.234 0.004 0.058 0.175 0.037 7.456 190.77 147 Cumulative lbs/acre 0.037 0.015 0.351 2.346 0.234 0.004 0.058 0.175 0.037 7.456 220 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction, or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: W B HARGETT SITE #: NC JO 02945 FIELD# : JO 02945 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00003919 ANNUAL DRY TONS APPLIED: 85.28 OPERATOR: DEXTER EDWARDS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 25.30 ACRES PERMITTED: 25.30 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppnl) Crop MONTH Total Per Acre Solids 6/30/14 350.00 (CY) 13.834 16.20 1.888 KIKRAED( DRY 0-<I/2" SUR 0.5 0.30 61,300.p 8,770.00 p 29.00 p 20173 BERMUDAGRASS Jun-14 350.00 (CY) 13.834 7/1/14 275.00 (CY) 10.870 16.20 1.483 DRY 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 BERMUDAGRASS Jul-14 275.00 (CY) 10.870 JKIKRAED(J 1 1 1 1 Total Cubic Yds/Ac: 24.70 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.034 0.013 0.324 2.164 0.216 0.003 0.054 0.162 0.034 6.876 175.94 136 Cumulative Ibs/acre 1 0.208 0.084 2.529 12.690 1 1.439 0.048 0.348 1 1.166 0.158 40.633 F Pennit PAN Limit (lbs/acre) 1st Crop/2nd Crop � 2 20 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 „ 1339.0 267.9 15.0 375.0 89.0 2500.0 KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under, my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: W B HARGETT SITE #: NC JO 08790 FIELD# : JO 08790 0004 A RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: WQ0003919 ANNUAL DRY TONS APPLIED: 167.14 OPERATOR: DEXTER EDWARDS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 3 7. 10 ACRES PERMITTED: 37.10 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppin) Crop MONTH Total Per Acre Solids 7/8/14 50.00 (CY) 1.348 16.20 0.184 I<IKRAED( DRY 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20 773 I FESCUE 7/9/14 600.00 (CY) 16.173 16.20 2.207 KIKRAED( DRY 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 I FESCUE 7/10/14 575.00 (CY) 15.499 16.20 2.115 KIKRAED( MOIST 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20171 FESCUE Jul-14 1,225.00 (CY)l 33.020 r alai l.1101e TQS/HG: 33.UL As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.045 0.018 0.432 2.892 0.288 0.005 0.072 0.216 0.045 9.190 235.17 182 Cumulative lbs/acre 0.248 0.128 2.685 16.574 2.252 0.059 0.513 1.278 0.198 46.563 lI Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop , +:: t . 250 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 KIKRAF.DC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: W B HARGETT SITE #: NC JO 08790 FIELD# : JO 08790 0004 C RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: WQ0003919 ANNUAL DRY TONS APPLIED: 57.99 OPERATOR: DEXTER EDWARDS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 13.50 ACRES PERMITTED: 13.50 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total TPer Acre Solids 7/8/14 425.00 (CY) 31.481 16.20 4.295 KIKRAED( DRY 0- 1/2" SUR 0.5 0.30 61,300.p 8,770.00 p 1 29.00 p 20173 FESCUE Jul-14 425.00 (CY) 31.481 Total Cubic Yds/Ac: 31.48 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.043 0.017 0.412 2.758 0.275 0.004 0.069 0.206 0.043 8.763 224.22 173 Cumulative lbs/acre 0.225 1 0.124 1 2.578 1 15.362 1 2.101 0.055 0.476 1.219 0.184 43.492: Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ` '' 250 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 P 1339.0 267.9 15.0 375.0 89.0 2500.0 " KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE g��- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: W B HARGETT SITE #: NC JO 08790 FIELD# : JO 08790 0005 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: WQ0003919 ANNUAL DRY TONS APPLIED: 37.52 OPERATOR: DEXTER EDWARDS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 11.80 ACRES PERMITTED: 11.80 Page : 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 7/2/14 25.00 (CY) 2.119 16.20 0.289 KIKRAED( DRY 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 I BERMUDAGRASS 7/7/14 200.00 (CY) 16.949 16.20 2.313 KIKRAED( DRY 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 I BERMUDAGRASS 7/8/14 50.00 (CY) 4.237 16.20 0.578 KIKRAED( DRY 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 BERMUDAGRASS Jul-14 275.00 (CY)l 23.305 Total Cubic Yds/Ac: 23.31 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 128 Annuallbs/acre 0.032 0.013 0.305 2.041 0.204 0.003 0.051 0.153 0.032 6.487 165.98 Cumulative Ibs/acre 0.279 0.132 3.352 17.470 2.550 0.071 0.565 1 1.597 0.225 52.066 "A Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop x� FD Cumulative Pollutant LoadingRate Limit Ibs/acre ( ) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: W B HARGETT SITE #: NC JO 08790 FIELD# : JO 08790 0006 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PERMIT #: W00003919 ANNUAL DRY TONS APPLIED: 30.70 OPERATOR: DEXTER EDWARDS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 8.90 ACRES PERMITTED: 8.90 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 7/2/14 25.00 (CY) 2.809 16.20 0.383 KIKRAED( DRY 0-<1/2" SUR 0.5 0.30 61,300.p 8,770.00 p 29.00 p 20173 IBERMUOAGRASS 7/7/14 200.00 (CY) 22.472 16.20 3.066 KIICRAED( DRY 0-<1/2" SUR 0.5 0.30 61,300. p 8,770.00 p 29.00 p 20173 BERMUDAGRASS Jul-14 1 225.00 (CY) 25.281 l oral l.uoic IWWAC. ZM5 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.034 0.014 0.331 2.215 0.221 0.003 0.055 0.166 0.034 7.037 180.06 139 Cumulative lbs/acre 0.116 0.041 0.900 6.740 0.695 0.018 0,177 0.437 0.116 22.211 '$ Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop .� , : 2 20 (lbs/acre) FD Cumulative Pollutant LoadingRate Limit lbs/acre 36.6 34.8 1339.0 267.9 15.0 , 375.0 89.0 2500.0 s" KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE r (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR-'Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: KINSTON, NC OWNER: W B HARGETT SITE #: NC JO 08790 FIELD#: JO 08790 0007 RESIDUAL SOURCE(S):* See list at bottom of report IANNUAL LAND APPLICATION FIELD SUMMARY FORM I PERMIT #: WQ0003919 ANNUAL DRY TONS APPLIED: 20.47 OPERATOR: DEXTER EDWARDS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 6.40 ACRES PERMITTED: 6.40 Page: I Lime Applied *** Lbs/Ac DATE or 3allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 7/2/14 25.00 (CY) 3.906 16.20 0.533 KIKRAED( DRY 0-1/211 SUR 0.5 0.30 61,300.p 8,770.00 p 9.00 p 20173 BERMUDAGRASS 7/7/14 125.00 (CY) 19.531 16.20 2.665 KIKRAED( DRY 0-1/211 SUR 0.5 0.30 61,300.p 8,770.00 p 29.00 p 20173 BERMUDAGRASS 1 J,1-14 1 150-00 (CY), 23.4371 1 1 1 1 1 1 1 1 I ULUI LUVR; I UWtW. As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 129 0.032 0.013 0.307 2.053 0.205 0.003 0.051 0.153 0.032 6.524 166.93 Cumulative lbs/acre 0.266 0.127 3.117 15.744 2.138 0.064 0.427 1.455 0.199 47.594 1, '1411$ Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop Ow h 1 MEW 11111" URN 4 R I R11, 04 NQ 3 �3% �M 220 FD Cumulative Pollutant Loading Rate Limit Qbs/acre) 36.6 34.8 12161 1339.0 267.9 15.0 375.0 89.0 2500.0 41V KIKRAEDC = KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility offines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 Application Method: SUR-Surface, INJ -Injection, SURIN -Incorporation See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 EP,fltl#1dt1PelEtJ`PPtLfiE� 9�3t�Li�`S�ti� 3PtC .�knafyt{cal L�fa�tfr�7�a'jP5 January 16, 2014 Edward Stephens Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Kinsten Dear Edward Stephens: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX. (330) 253-4489 Website: http:1Avivw.settek.com Order No.: 14010507 Summit Environmental Technologies, Inc. received 1 sample(s) on 1/10/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, A--� Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho 01100923, Illinois 200061 and Reg.5, Indiana C-011-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon 0112O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-I1-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 12 z Summit Environmental Technologies, Inc. 3310 Win St. Workorder Sample Summary FR{1lfi6hPiEhbL��i^l��Cl-�,�xG Cuyahoga Falls, Ohio Arr3P1�1i;:a! is a�:asf �{e TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 14010507 Website: htto711Jvivw.settekcom 16-Jan-l4 CLIENT: Synagro Project: Kinsten Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 14010507-001 Kinsten 1/6/2014 11:30:00 AM 1/10/2014 9:52:00 AM Sludge Page 2 of 12 Sununit Environniental Technologies, Inc. Case Narrative r 3310 Win St. 43ifI1 �S#Jfa9EN`Pi1Li C1� tt^Gi'L5`i[ � Cuyahoga Falls, Ohio44223 WO#: 14010507 �arraPl rlcal L:ieS'�a'$1��`teS' TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htm:/htiviv.settekcom Date: 1/16l2014 CLIENT: Synagro Project: Kinsten This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc. Work Order Number assigned to this report. Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample set. Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation (LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty associated with these results and data should be considered as estimated. Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Any comments or problems with the analytical events associated with this report are noted below. Original Page 3 of 12 . ; Summit Environmental Technologies, Inc. 3310 Win St. �FVI tCY�dlet�;NihL 'f 3�s° C[ G3 s�t� CiryahogaFalls, Ohio44223 Date Reported p 1/16/2014 13i'Fai;+trial f E�"prt��p, Fe; TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: hM.-IlHnrw.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/10/2014 Project#: Kinsten TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Kinsten 001 1/6/2014 TCLP Arsenic(As) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 1/15/2014 WK Kinsten 001 1/6/2014 TCLP Barium(Ba) 5.0 ND mg/L Sludge EPA 6010 C 1 100 1/15/2014 WK Kinsten 001 1/6/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Sludge EPA 6010 C 1 1.0 1/15/2014 WK Kinsten 001 1/6/2014 TCLP Chromium(Cr) 0.20 ND mg/L Sludge EPA 6010 C 1 5.0 1/15/2014 WK Kinsten 001 1/6/2014 TCLP Lead(Pb) , 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 1/15/2014 WK Kinsten 001 1/6/2014 TCLP Selenium(Se) 0.50 ND mg/L Sludge EPA 6010 C 1 1.0 1/15/2014 WK Kinsten 001 1/6/2014 TCLP Silver(Ag) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 1/15/2014 WK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Kinsten 001 1/6/2014 TCLP Mercury 2.0 ND ug/L Sludge EPA 7470 A 1 200 1/14/2014 ALJ SVOC SW-846: 8081-TCLP Pesticides Client lD# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Kinsten 001 1/6/2014 Chlordane, total 10 ND pg/L Sludge EPA 8081 B 1 30 1/15/2014 JBN Kinsten 001 1/6/2014 Toxaphene 100 ND pg/L Sludge EPA 8081 B 1 500 1/15/2014 JBN Kinsten 001 1/6/2014 Endrin 2.0 ND pg/L Sludge EPA 8081 B 1 20 1/15/2014 JBN Kinsten 001 1/6/2014 gamma-BHC 2.0 ND pg/L Sludge EPA 8081 B 1 400 1/15/2014 JBN Kinsten 001 1/6/2014 Heptachlor 2.0 ND pg/L Sludge EPA 8081 B 1 8.0 1/15/2014 JBN Kinsten 001 1/6/2014 Heptachlor epoxide 2.0 ND pg/L Sludge EPA 8081 B 1 8.0 1/15/2014 JBN Kinsten 001 1/6/2014 Methoxychlor 2.0 ND pg/L Sludge EPA 8081 B 1 10000 1/15/2014 JBN VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Kinsten 001 1/6/2014 1,1-Dichloroethene 100 ND pg/L Sludge EPA 8260 B 1 700 1/15/2014 MES Kinsten 001 1/6/2014 1,2-Dichloroethane 100 ND pg/L Sludge EPA 8260 B 1 500 1/15/2014 MES Kinsten 001 1/6/2014 Benzene 100 ND pg/L Sludge EPA 8260 B 1 500 1/15/2014 MES Kinsten 001 1/6/2014 Carbon tetrachloride 100 ND pg/L Sludge EPA 8260 B 1 500 1/15/2014 MES Kinsten 001 1/6/2014 Chlorobenzene 100 ND pg/L Sludge EPA 8260 B 1 100000 1/15/2014 MES Kinsten 001 1/6/2014 Chloroform 100 ND pg/L Sludge EPA 8260 B 1 6000 1/15/2014 MES Kinsten 001 1/6/2014 Tetrachloroethene 100 ND pg/L Sludge EPA 8260 B 1 700 1/15/2014 MES Kinsten 001 1/6/2014 Trichloroethene 100 ND pg/L Sludge EPA 8260 B 1 500 1/15/2014 MES Kinsten 001 1/6/2014 Vinyl chloride 200 ND pg/L Sludge EPA 8260 B 1 200 1/15/2014 MES Kinsten 001 1/6/2014 MEK 2000 ND pg/L Sludge EPA 8260 B 1 200000 1/15/2014 MES Page 4 of 12 � Summit Environmental Technologies, Inc. 3310 Win St. WO#: 14010507 r , 04VIROWPOEINTAL,C=4 HNO,R G]P5 9�[C. Cuyahoga Falls, Ohio 44223 Date Reported 1/16/2014 y knaryo' at i.4uoraio-rie TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: htm:11mvw.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/10/2014 Project#: Kinsten SVOC 8270 TCLP BNA List Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Kinsten 001 1/6/2014 1,4-Dichlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 7.5 1/14/2014 AKE Kinsten 001 1/6/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 • 400 1/14/2014 AKE Kinsten 001 1/6/2014 2,4,6-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 2.0 1/14/2014 AKE Kinsten 001 1/6/2014 2,4-Dinitrotoluene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 1/14/2014 AKE Kinsten 001 1/6/2014 Cresols, Total 5.0 ND mg/L Sludge EPA 8270 C 1 200 1/14/2014 AKE Kinsten 001 1/6/2014 Hexachloro-1,3- 0.10 ND mg/L Sludge EPA 8270 C 1 0.50 1/14/2014 AKE butadiene Kinsten 001 1/6/2014 Hexachlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 1/14/2014 AKE Kinsten 001 1/6/2014 Hexachloroethane 0.10 ND mg/L Sludge EPA 8270 C 1 3.0 1/14/2014 AKE Kinsten 001 1/6/2014 Nitrobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 2.0 1/14/2014 AKE Kinsten 001 1/6/2014 Pentachlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 100 1/14/2014 AKE Kinsten 001 1/6/2014 Pyridine 0.25 ND mg/L Sludge EPA 8270 C 1 5.0 1/14/2014 AKE SVOC SW-846: 8321 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Kinsten 001 1/6/2014 2,4-D 5.0 ND mg/L Sludge EPA 8321 A 1 10 1/14/2014 AMZ Kinsten 001 1/6/2014 2,4,5-TP 0.50 ND mg/L Sludge EPA 8321 A 1 1.0 1/14/2014 AMZ Kinsten 001 1/6/2014 Surr: 2,4- 20-140 0 %REC Sludge EPA 8321 A 1 1/14/2014 AMZ Dichlorophenylacetic acid Page 5 of 12 Simunit Environmental Technologies, Inc. -MISUMOT 3 310 Win St. WOff: 14010507 Cuyahoga Falls, Ohio 44223 Date Reported 1/16/2014 TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro, Website: hW:1Avww.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/10/2014 Project#: Kinsten Client ]IN Lab EN Collected Analyte Result Units Matrix Method DF RIL Run Analyst Kinsten 001 1/6/2014 Flashpoint (140°F) >140 oF Sludge EPA 1010 1 1/13/2014 TAH Kinsten 001 1/6/2014 Cyanide, Reactive ND ppm Sludge EPA 9014 1 0.50 , 1/10/2014 TIR Kinsten 001 1/612014 pH 5.9 s.u. Sludge EPA 9045 D 1 1/1312014 AYS Kinsten 001 1/612014 Sulfide, Reactive ND ppm Sludge EPA 9034 1 25 1/10/2014 TIR Page 6 of 12 sufamelf Summit Environmental Technologies, Inc. QC SUMMARY REPORT 3310 Win St. tav�R�t•1f1i NTAb o l� �[iL �t S'..1lsEC Cuyahoga Falls, Ohio 44223 A91111 ;iPta.barxbrjrm TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 14010507 ti- Website: htW:/hviviv.settelc.coni 16-Jan-14 Client: Synagro Project: Kinsten TestCode: FlashPt_S(1010) iample ID: LCS-R11448 SampType: LCS TestCode: FlashPt_S(10 Units: °F Prep Date: RunNo: 11448 ;lient ID: LCSS Batch ID: R11448 TestNo: SW1010 Analysis Date: 1/13/2014 SegNo: 127689 knalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Flashpoint (140°F) 83.0 Qualifiers: * Value exceeds Maximum Contaminant Level. E Value above quantitation range M Manual Integration used to determine area response P Second column confirmation exceeds RL Reporting Detection Limit 77.00 0 108 70 130 B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit PL Permit Limit S Spike Recovery outside accepted recovery limits C Value is below Minimum Compound Limit. 7 Malyte detected below quantitation Emits O RSD is greater than RSDEmit R RPD outside accepted recovery Emits U Samples with CalcVal < MDL Original Page 7 of 12 Summit Environmental Technologies, Inc. QC SUMMARY REPORT 3310 Win St. �ea5fiSptlP1EIJTAI:6 �i1s?3QL_13 1FS,IK.0 Cnyahoga Falls, Ohio 44223 WO#: 14010507 Airwfytfoaf, Labpr,,710 7� 4� TEL: (330) 253-8211 FAX. (330) 253-4489 Website: hLW:11mnv.settelc.can 16-Jan-14 Client: Synagro Project: Kinsten TestCode: HG_TCLP(7470) Sample ID: MB-2769 SampType: MBLK TestCode: HG TCLP(747 Units: ppb Prep Date: 1/14/2014 RunNo: 11559 Client ID: PBW Batch ID: 2769 TestNo: SW7470A SW7470A Analysis Date: 1/14/2014 SegNo: 129068 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury ND 2.0 U Sample ID: LCS-2769 SampType: LCS TestCode: HG TCLP(747 Units: ppb Prep Date: 1/14/2014 RunNo: 11559 Client ID: LCSW Batch ID: 2769 TestNo: SW7470A SW7470A Analysis Date: 1/14/2014 SegNo: 129069 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ TCLP Mercury 4.3 2.0 4.000 0 108 75 113 Sample ID: 14010649-001AMS SampType: MS TestCode: HG TCLP(747 Units: ppb Prep Date: 1/14/2014 RunNo: 11659 Client ID: BatchQC Batch ID: 2769 TestNo: SW7470A SW7470A Analysis Date: 1/14/2014 SegNo: 129098 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury 3.9 2.0 4.000 0 97.2 60 125 Sample ID: 14010549-001AMSD SampType: MSD TestCode: HG TCLP(747 Units: ppb Prep Date: 111412014 RunNo: 11669 Client ID: BatchQC Batch ID: 2769 TestNo: SW7470A SW7470A Analysis Date: 1/14/2014 SegNo: 129099 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual FCLP Mercury 3.9 2.0 4.000 0 97.5 60 125 3.890 0.257 10 Qualifiers: Value exceeds Maximum Contaminant Level. E Value above quautitation range M Manual Integration used to determine area response P Second column confirmation exceeds RL Reporting Detection Limit B Analyte detected in the associated Method Blank H Holdurg times for preparation or analysis exceeded ND Not Detected at the Reporting L'unit PL Permit Limit S Spike Recovery outside accepted recovery limits C Value is below Minimum Compound Limit. J Analyte detected below quantitation limits O RSD is greater than RSDlimit R RPD outside accepted recovery limits U Samples with CalcVal <MDL Original Page 8 of 12 Summit Environmental Technologies, Inc. QC SUMMARY REPORT 3310 Win St. �� lld�i3riaPri=�tdT�.l-Ti~ H �®Ltb lEs�, INN Cuyahoga Falls, Ohio 44223 'tlytPr ail f rhDt IfarJ TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 14010507 Website: http:11mviv.settelc.com 16-Jan-14 Client: Synagro Project: Kinsten TestCode: Mtl-TCLP-7(6010) Sample ID: 14010358-001AMS SampType: MS TestCode: Mtl-TCLP-7(6 Units: mg/L Prep Date: 1/15/2014 RunNo: 11658 Client ID: BatchQC Batch ID: 2778 TestNo: SW6010C SW3010A Analysis Date: 1/15/2014 SegNo: 130420 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Arsenic(As) 2.1 0.50 2.000 0 105 70 130 TCLP Barium(Ba) ND 5.0 2.000 1.800 10.5 70 130 S TCLP Cadmium(Cd) 2.0 0.10 2.000 0 102 70 130 TCLP Chromium(Cr) 2.0 0.20 2.000 0 102 70 130 TCLP Lead(Pb) 2.2 0.50 2.000 0 108 70 130 TCLP Selenium(Se) 2.1 0.50 2.000 0 103 70 130 TCLP Silver(Ag) 0.72 0.50 1.000 .0 72.0 70 130 Sample ID: 14010358-001AMSD SampType: MSD TestCode: Mtl-TCLP-7(6 Units: mg/L Prep Date: 1/16/2014 RunNo: 11658 Client ID: BatchQC Batch ID: 2778 TestNo: SW6010C SW3010A Analysis Date: 1/15/2014 SegNo: 130421 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Arsenic(As) 2.1 0.50 2.000 0 105 70 130 2.100 0 20 TCLP Barium(Ba) ND 5.0 2.000 1.800 11.0 70 130 0 0 20 S TCLP Cadmium(Cd) 2.0 0.10 2.000 0 103 70 130 2.040 0.489 20 TCLP Chromium(Cr) 2.0 0.20 2.000 0 102 70 130 2.040 0 20 TCLP Lead(Pb) 2.2 0.50 2.000 0 110 70 130 2.170 0.917 20 TCLP Selenium(Se) 2.1 0.50 2.000 0 107 70 130 2.060 3.81 20 TCLP Silvei(Ag) 0.75 0.50 1.000 0 75.0 70 130 0.7200 4.08 20 Qualifiers: * Value exceeds Maxhnum Contaminant Level. B Analyte detected in the associated Method Blank C Value is below Minimum Compound Limit. E Value above quantitation range H Holding times for preparation or analysis exceeded 7 Analyte detected below quantitation Emits M Manual Integration used to determine area response ND Not Detected at the Reporting Limit - O RSD is greater than RSDlimit Original P Second column confirmation exceeds ' PI: Permit Limit R RPD outside accepted recovery Emits RL Reporting Detection Limit S Spike Recovery outside accepted recovery Emits U Samples with CalcVal <MDL Page 9 of 12 Summit Environmental Technologies, Inc. QC SUMMARY REPORT m'-summoir 3310 Win St. ENVIFROt MZNTrAl. MCHWOLDGIES5, INC Cuyahoga Falls, Ohio 44223 t??j{tfc81tTrstm€deb WO#: 14010507 TEL: (330) 253-8211 FAX:(330) 253-4489 Website: htto:/Atnvw.settelr.com 16-Jan-14 Client: Synagro Project: Kinsten TestCode: pH_S(9045D) iample ID: 14010607-001ADUP SampType: DUP TestCode: pH S(9045D) Units: s.u. Prep Date: RunNo: 11463 ;lient ID: Kinsten Batch ID: R11463 TestNo: SW9045D Analysis Date: 1/13/2014 SegNo: 127880 \nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighUrnit RPD Ref Val %RPD RPDLimit Qual pH 5.9 Qualifiers: ° Value exceeds Maximum Contaminant Level. E Value above quantitation range M Manual Integration used to deternnune area response P Second colunm confirmation exceeds RL Reporting Detection Limit B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit PL Permit Limit S Spike Recovery outside accepted recovery limits 5.870 0.170 20 C Value is below Minimum Compound Limit. J Malyte detected below quantitation limits 0 RSD is greater than RSDlimit R RPD outside accepted recovery limits U Samples with CalcVal a MDL Original Page 10 of 12 Summit Environmental Technologies, Inc. QC SUMMARY RY REPORT 3310 Win St. 1. �7 lJ 1rI1C1L �l\ 1 i�l�l t Arl�tt�ldi I ENTf51: FstG�QL� �i.L, 3itG Cuyahoga Falls, Ohio 44223 WO#: 14010507 lt'7t�ylf, atP th4t /real' TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: &Wt lhvivw.settek.com 16-Jan-14 Client: Synagro Project: Kinsten Sample ID: MB-R11568 Client ID: PBS Analyte Sulfide, Reactive Sample ID: LCS-R11568 Client ID: LCSS Analyte Sulfide, Reactive SampType: MBLK TestCode: Sulfide,Reacti Units: ppm Batch ID: R11568 TestNo: SW9034 Result PQL SPK value SPK Ref Val ND 25 TestCode: Sulfide,Reactive S(9034) Prep Date: RunNo: 11568 Analysis Date: 1/10/2014 SegNo: 129230 %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual SampType: LCS TestCode: Sulfide,Reacti Units: ppm Prep Date: RunNo: 11668 Batch ID: R11668 TestNo: SW9034 Analysis Date: 1/10/2014 SegNo: 129231 Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 50 25 54.00 0 93.0 70 130 Sample ID: 14010510-001AMS SampType: MS TestCode: Sulfide,Reacti Units: ppm Prep Date: RunNo: 11568 Client ID: BatchQC Batch ID: R11568 TestNo: SW9034 Analysis Date: 1/10/2014 SegNo: 129232 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 49 25 54.00 0 90.7 70 130 Sample ID: 14010510-001AMSD SampType: MSD TestCode: Sulfide,Reacti Units: ppm Prep Date: RunNo: 11568 Client ID: BatchQC Batch ID: R11668 TestNo: SW9034 Analysis Date: 1/10/2014 SegNo: 129233 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 51 25 54.00 0 95.2 70 130 49.00 4.78 30 Qualifiers: ` Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank C Value is below Minimum Compound Limit. E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitahon Emits M Manual Integration used to determine area response ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery Emits RL Reporting Detection Limit S Spike Recovery outside accepted recovery Emits U Samples with CalcVal <MDL Page 11 of 12 Summit Environmental Technologies, Inc. QC SUMMARY REPORT fflSfirlawwr 3310 Win St. `JIRtXtJtal tlTAIR Gii11�4Jl kGiES, INIC Cuyahoga Falls, Ohio 44223 as» yifcffl Ltrihorat06&-TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 14010507 Website: ham://wtviv.settelr.com 16-Jan-14 Client: Synagro Project: Kinsten TestCode: TCLP-SVOC-Herb_S(8321) 3arnple ID: MB-2748 SampType: MBLK TestCode: TCLP-SVOC- Units: mg/L Prep Date: RunNo: 11612 :lient ID: PBW Batch ID: 2748 TestNo: SW8321A SW1311M Analysis Date: 1/14/2014 SegNo: 129701 analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDUrnit Qual 2,4-D ND 5.0 U 2,4,5-TP ND 0.50 U Qualifiers: ` Value exceeds Maximum Contaminant LeveL E Value above quantitation range M Manual Integration used to determine area response P Second column confirmation exceeds RL Reporting Detection Limit B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit PL Permit Limit S Spike Recovery outside accepted recovery Emits C Value is below Minimum Compound Limit. J Analyte detected below quantitation limits O RSD is greater than RSDlhnit R RPD outside accepted recovery Emits U Samples with CalcVal <MDL Original Page 12 of 12 ==Pnk Summit Environmental Technologies, Inc. Analysis Request/Chain of Custody 3310 Win Stmet For Sultialit Environmental 'reclIn( )jt)gies. lnc. u-w onlyCuyahoga Falls. Ohio 44223 Tel: 330.253.8'-Ill lax: 330.25144'() Analytical Parameters and Methods \;imc (Please Print i Ab si Aicni Phone No. Report to ;.Bent Pax No, P()# Client j. Emwil Result,, Quote No- S". # Sample Identification -- 'd i 1, hl samples./ FI Z�" V 4"; z 01 NOtt -VO)ITImenits, 'I'llo dwnl f.Twn.' tile pink llag-c I A ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Kinston, NC WQ Permit Number: WQ0003919 WWTP Name: Kinston Regional WRF NPDES Number: NCO024236 Monitoring Period: From 01/01/2014 To 3/31/2014 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion Tf nnnlirnhle to alternative nerfnrmed (Class A nr Class R) ramnlete the fnllowinu manitarinu data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6 th MPN MPN/g Coliform power per gram of total solids 5100 6100 7200 CFU/g 0 Annually Grab SM9222D CFU 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Alt. 3 Option/Alt.4 (vS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying —Unstable) _ Option/Alt. 9 Option/Alt. 10 (Infection) (Incorporation) No vector attraction reduction alternatives were performed _ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kenneth Stevens, WWTP Superintendent Preparer Name and Title (type or print) a /ai3 Signature of Prepare: Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Cameron Testi . ng Servipes, Inc.- Laborat6' 'Re' o rt ry p NC DEAk 0654 NC. PHH� #37799 US EPA Ir NG0jgj B Synagra i CT,$.,0roil 140010 Kinstbh- -Yes Sample Iniormation, W. Varner Date 6106114 Received C. Cameron Date, 0110SM4 Analyses and Results' E -,E ItT 140010 01 Kinston SlujUr Or Fec. Coliforni-S 01107114 DPK 9222D IVIF b 5300 UUN 51JOG 01ID7114 [DPK 92220 M F e-6200 Cru&j 62,c0 01MM-4. 0FsK 922.2D - NIF d 720D :CFwg 7200 01107114 OPK 92221) - 14F <6()00 'dul'k Gwo 01167114 DPK 9222D -: MF f e6300 druya :6kb 01107114 DPK. 92220. - NIF <6900, qu,.7 p9bo 01107114. DPK 9222D - MF Ceomcan <6100 14001.0 01 ErWgE Or TS N 16.4% % W, 01MV14 DPK -TS 2540 G. b % ui 01107114- DPK-- 2540 G -78-• c 1.4,3% % ani 01107114, DPK 2540 G -TS d 14.3% % mui 01107114- DPK 2540 G -TS. IE9% n 0.01 011D7114 DPK, 2540 G -TS f 15.63% % 601 01107114 DPK 2540,0 -TS 9 14,5% 0,01 0110711.1 DPK 2540 � -TS, Data Review n p Lab Teuhnician Data Report .Review /rj �v v. Lab Director Date . 'Sir. k)19-209-4240 19 $. SLL:01� SiMfordINIC 27330 Chain -of Custody Qgmeron Testing Services,, finc, Sanf&cf. N&:'27330'. Page of. f. Phone: St9-208;-4240- Mb V&J;"G'W,deft. -#654 NC� PHHSI Cort #377.99 US'EPA N'tO191 B-I' ompany: kc, 4 OT 4�(D Cdntait Milano; Sain- Tern pff Fox: Addi ty-,_ lob Rush: [ (ION)! --,.S Lab' Sa'7ffi'- 16; ID E 1 CL X, 9 0 C. E -03 o te) 0 ati HNOI(N)�; Na Tli1a: MT): .R61ingulghed: DateTTIffi6i L TIIEC'EITEID JAR' 0 kusflvdrk will require" -prior approval, A� dirioinatchcq'rges Will apply Time (rclnutos) a z s 4 5 7 g 9 10 11 12 13 14 X15 Specific Oxygen Uptake Rate SOUR Facility name: Blosolids Permit Number: Digester Temperature: Sampling Date/Tlme: Sampled By: Analysis Date/Time: Analyzed By: Sample volume: Total Solids: Beginning Temperature: End Temperature; Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: .Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: 16. 97 Temperature Correction Factor. /. #o V Dry Solids egrees Celsius egrees Celsius mg Oxygen/hr mg Oxygen/g/hr degrees Celsius Temperature corrected Specific Oxygen Uptake mate: 0 mg Oxygen/g/hr 51 Instructions: Enter Data in the flue Boxes. The Calculation and the Spreadsheat execute automatically. Time (minutes) 0 1 2 3 4 5 a 7. 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name. Blosolida Permit Number Gate Digester Temperature Sampling Datelrime Sampled By Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level N Slope: Intercept: Correlation Coefficient: KRWRF WQ0003919 I q. L� 1 ;PBS SF S+ D .13 3. 03 Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: I6-4t$ Temperature Correction Factor: I_ 'fp milliliters % Dry Solids degrees Celsius. degrees Celsius mg .Oxygen/hr rng Oxygen/g/hr degrees Celsius r Temperature Corrected Specific Oxygen Uptake mate: f915 X- mg Oxygen/g/hr Instructions: Enter Data in the Slue Boxes, The Calculation and the Spreadsheet execute aufomaticaily. Time (minutes) 0 '1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name Blosolids Permit Number Date Digester Temperature Sampling Date/Time Sampled By Analysis Datel'i"ime Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dlssollved Oxygen I -eve{ Slope: Intercept: Correlation Coef dent: KRWRF WQ0003919 0-/ I 06 5F i.Z Oxygen Uptake Bate: Ambient Speniflo Oxygen Uptake Rate: Average Temperature_'17.9 Temperature Correction Factor: /.'fD milliliters % Dry Solids degrees Celsius degrees Celsius mg Oxygen/hr mg Oxygen/g/hr degrees Celsius Temperature Corrected Specific Cxygen Uptake Rate: mg Oxygen/g/hr Instructions: Enter Data in the Blue:Boxes. The Calculation and the Spreadsheet execute automatically. 501 Time (minutes) 0 1 2 3 4 5 S 7 8 8 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Nami Biosolids Permit Numbe Digester Temperature: Sampling Date/Time: Sampled By: Analysis DateMme: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coatfcient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature:17,31 Temperature Correction Faotor: 1,11D Illlters Dry Solids grees Celsius grees Celsius mg Oxygen/hr mg Oxygen/g/hr degrees Celsius Temperature Corrected.Specific Oxygen Uptake Rate: D CZl- mg Oxygen/g/hr Instructions' Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automaboally. Time (minutes) 0 .3 4 G 7' 8 9 10 11 12 13 14 15 Specific Oxygen Uptake mate SOUR Facility Name Biosolids Permit Number Date Digestor Temperature Sampling Date/Time Sampled By Analysis Date/Time Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level 7 Slope: Intercept: Correlation Coefficient: 14RWRF WQ0003019 -� SiD ./v a 5 Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: 1-7a54 Temperature Correction Factor: 1,46 milliliters % Dry Solids degrees Celsius degrees Celsius mg Oxygenlhr mg Oxygen/g/hr degrees Celsius Temperature Corrected Specific Oxygen Uptake Hate: Mom® mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically, Time (minutes) a z 4 5 6 7 a 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Blcsolids Permit Number_ bate: Digester Temperature: Sampling Datelrime; Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature; Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: 17. 0 Temperature Correction Factor: /.Yo 919 01111ters o Dry Solids agrees Celsius egrees Celsius mg Oxygen/hr mg Oxygen/g/hr degrees Celsius Temperature Corrected Specific Oxygen Uptake Rate: . , mg Oxygen/glhr Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically. 1-2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Kinston, NC WQ Permit Number: WWTP Name: 'Kinston Regional WRF NPDES Number: Monitoring Period: From 04/01/2014 To 6/30/2014 WQ0003919 NCO024236 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 4/D (No Prior Test) . Alt. 2B (Alk Treatment) Alt. 5/Process to Further Reduce Pathogens Alt. 3/C (Prior Testing) Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlienhle to alternntive nerfnrmed W1nca A nr (7asa R) rmmnlete the fn11nwina mnnitnrina data - Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units deuces Analysis Fecal 2x10 to the 6th MPN MPN/g Coliform power per gram of total solids CFU 1960 6800 67300 CFU/g 0 Annually Grab SM9222D 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) . (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kenneth Stevens, WWTP Superintendent Preparer Name and Title (type or rint) Land Applier Name and Title (if applicable) (type or print) Signature of Preparer Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26), Cameron Testing Services, Inc.- Laboratory Report NC DENR fl654. NC, PHHS #37799. Client: Synagro -CT-S,Proj. 140378 Proidot- Killston Regulatory -Yes Sample Information Sampled W.Varner Date 04109114 - koceind C' Cameron Date 04109/14 Analyses and Results Lab ID E Ana] te 4 :M' k, S .Sta" ke_ C) re 140378 01 SILPc'Ic G., Fec. Coliform-IS 20500 crul!3 mr, 04116114 CSC 9222D - MF K-2 <21101 Cr un 2110 04110M4 CSC 9222D - NIF K-3 <1960 CT: U19 Isso 0 4 110" 1 ". ts.c 9222D - MF K-4 2025 6.;L'jQ 2025 041101�4 CSC 9222D-IMF X-5 <2050 CFUID 2050 0010114 CSC 9222D - W K-6 67300 Lr! 9 zwo 04110M4 CSC 92220 - MF K-7 28400 76*,;, (W 1 011 4. CSC 9222D - MF Geornean 6800 140378 01 K-1 slwcjE ol TS(%) 417% A 01)1 04110114 PARG 2540 0 JS K-2 4.23% % ooi 04110114 MRG 2541 G -T8 K-3 4,21% % O-Di 04110)14 PARG 2842 G -TS KA 423% A. om 0411011-1 NIRG 2543 G -'TS 4.22% I)DI 04110;i4 rvIRG 2544 G JS K-6 4.20% D.01 04110114 TARG 2545 G JS K-7 4,26% 0,0t 04110114 MRG 2546 G JS Data Review 7—s L Technician. Date Report Review Oql1s Lab Director Date 4 219 S. Si cc I C Sir, 919-208-4240 SaatRml NW 27.3.111 Oiri.,Aika dicron I est hig.com 2 19 S. Steele StrChain of Custody Cameron Testing Services, Inc.f, Sanford. NC 27330 I of Phone: 919-208-4240 NC'YVWiMV Cert. #684 NC PHHS Cert # 3+ rr 99 US EPA NC01968 ���� Company: Synagro Email: WVamer@synagro.com GTS lab use only Contact: ,Will Varner Phone: 336-909-8627 Sampie Temp(C) JO Proj. Address 284 Boger Rd. Fax: T Blank (YININA) Arrive: (City, State, Zip) Mocksville, NC 27028 ° o6e Project: S � Regulatory (YIN) Rush (YIN) Collected: Name_ _/,.�� Signature: Sample Information Requested Analysis � ?' C /TLL Q a CTS Lab B v, �, Z Sample ID °_,' a a� a IC E ZU+ n 11 V Cr j Ll-�-ltt i!"1� -� 7 i None(0) HNO3 (N) F1250a (S) HCI (C) Na Thio (NT) Other (X) Received: DatelTime �Relrinq�uished: Rush work will require prior approval. Additional charges will apply Time (rnlnutes) 0 1 , 2 3 4 5 6 7 8 9 10 11 12 13 14 1S Specific Oxygen Uptake Rate SOUR Facility Name: `KRWRF 'Biosoiids permit dumber: WQ0003919 Date: Digester Temperature: e Sampling Date/Time: j 3 r Sampled By: P; Analysis Date/Time: Analyzed By: � Sample volume: Total Solids: Beginning Temperature: ro End Temperature: Dissolved oxygen Laval milliliters % Dry Solids degrees Celsius degrees Oelsius V Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: mg ©xygenlhr Am-bient Specific Oxygen Uptake Rate: mg Cxygenlglhr Average Temperature: 210.15 degrees Celsius Temperature Correction Factor: , -75 Temperature Corrected Specific Oxygen Uptake Rate: , 5 �i/ mg Oxygen/gihr Instructions' •Enter Data In the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Time (minutes) 0 '1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specifio Oxygen Uptake Rate SOUR Facility Name: KID-WRF — 'Blosolids Permit number: WQ0003919 Date: HOE Digester Temperature: A Sampling Date/Time: � q& Sampled By: Analysis Date/Time: . r Analyzed By: r Sample Volume: milliliters p Total Solids: % Dry Solids Beginning Temperature: degrees Celsius. _Lp I End Temperature: degrees Celsius Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: mg Oxygen/hr Ambient Speoific oXygen uptake Rate: mg Oxygen/g/trr Average Temperature: Z5.3,5 degrees Celsius Temperature Correction Factor: t 7Y Temperature Corrected Specift Oxygen Uptake Rate: p r mg Oxygen/gmr Instructions: Enter Data in the Slue Saxas. The Calculation and the Spreadsheet ezeoute automatically. Time (minutes) 0 .1 2 3 4 5 E3 7 B 9 10 11 12 13 14 1s Specific Oxygen Uptake Rate SOUR Facility Name Blosolids hermit Number Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Reginning Temperature: End TemneraturA', Dissolved Oxygen Level Slope: Intercept. Corr -elation Coefficient: Oxygen Uptake Date: Ambient SpecrFc Oxygen Uptake Rate: Average Temperature: 21a.71f Temperature Correction Factor:.71 Dry Solids grew Celsius green Celsius Mg Oxygen/hr mg Oxygen/g/hr degrees Celsius Temperature Corrected Speoific Oxygen -Uptake mate: ,p 0' mg Oxygenlg/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically, 0 Time (minutes) 0 1 2 3 4 5 . B 7 8 9 10 11 12' 10 14 15 Specific Oxygen Uptake Rate SOUR Facility Nam Biosolids Permit NumbE Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: L-nd Temperature: Dissolved Oxygen Level VRF WMWMR ® 0003919 Dry Solids green Celsius green Celsius Slope: Intercept; Carrelation Coefficient: Oxygen Uptake Rate: Mg oxygen/hr Ambient Specific Oxygen Uptake Rate: mg Oxygenlg/hr Average Temperature: 2j�, .degrees Celsius Temperature Correction Factor: , 71 Temperature Corrected specific Oxygen Uptake Rate: / q Mg Oxygen/g/hr Instructions' Eater Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically. ril Time (Minutes) 0 1 2 3 4 5 6 7 B 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Blosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: sampled By: Analysis DateMme: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: AmNant Specific Oxygen Uptake Rate: Average Temperature: Zit .af ?_ Temperature Correction Factor: , 7S- f= milliliters Dry Solids degrees. Celsius degrees Celsius Mg Oxygen/hr mg Oxygen/g/hr degrees Celsius Temperature Corrected Specii:lo Oxygen Uptake Rate: ; q/ x rang Oxygen/g/hr Instructions' Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Time (minutes) g 2 3 4 5 6 .7 8 9 18 11 18 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled BY: Analysis Date/Time: Analyzed By., sample volume:. Total Solids: Beginning 'Temperature: End Temperature: Dissolved Oxygen Level 12e0 mi11111ters % Dry Solids degrees Celsius degrees Celsius Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: mg Oxygen/hr Ambient Speck oxygen Uptake Rate: mg Oxygen/g/hr Average Temperature: 95.12- degrees Celsius Temperature Correction Factor: Temperature Corrected Speolfo Oxygen Uptake Rate: 7 m O 9 xygen/g/hr Instructions' Enter Data. in the, Blue Boxes. The Ca{cuiation and the Spreadsheet execute automatically, Specific Oxygen Uptake Date SOUR NO Tilme (minutes) 0. 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name Biosolids permit Number Digester Temperature: Sampling Date/Time, Sampled By: Analysis Date/Time. Analyzed By: sample Volume: Total Solids: Beginning Temperature: End Temperature: DissOlVW Oxygen Level, 19 liiliters Dry Solids grees Celsius green Celsius Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Mg Oxygenlhr Ambient Specific Oxygen Uptake Rate: Average Temperature: j�. degrees Celsius Temperature Correctibn Factor: t 7 de Temperature Corrected Specific Oxygen Uptake Rate: ommorng Oxygenlglhr Instructions; Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name:' City of Kinston, NC WQ Permit Number: WQ0003919 WWTP Name: Kinston Regional WRF NPDES Number: NCO024236 - Monitoring Period: From 07/01/2014 To 9/30/2014 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion if o ..lino hln 4n o14or o4:. orF rmoA frinee A nr (lace R) rm—lata tha fnllnwina mnnitnrina dnta- Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units deuces Analysis Fecal 2x10 to the 6 1h MPN MPN/g Coliform power per gram of total solids CFU 21800 90200 459000 CFU/g 0 Annually Grab SM9222D 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. l Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying— Unstable) _ Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) - No vector attraction reduction alternatives were performed _ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC'02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kenneth Stevens, WWTP Superintendent Preparer Name and Title (type or print) Signature of Prepare Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Ga-Merbzi TOstiO So",MC69,j Inc.' Laboratdry Report NC DO 0661 E" NC PHHS fi37799 US EPA ;PNCfdl 918 Synagro P'-T§,,Proj- 140790 Kinston Regulatory Yes SdhiPle Unform' ation Will Varner ,D16"r R166cNea. Billy Gordon eiaec 07110114 Analyses and ReSdItS Lab ID: Sample 10 5 Analyto it sre6t ff: .�j 03 1 Std. Methods ke fer�ncc :3 —1 .71 1,10790 o-i bILICk3E C-r Fec. coforai-sq 276000' CM.a 3910 071 G/I 4 BG 9222 D M F b 51400 GrINa 3670, C, 21800 Grua 5•.ii[1 4,1800 11650 e 2-38000 r-1,tJfg 4870 IF 459OOb- C1--Ufu 4500 9 34400 C-FLUa 3830. Gcomean 90200 1,10796 01 TS 129% W, r, m 07.115114 DPK 25440 G -TS 17, a% 001 d 13,6% 14,6% r 9 Data fJ -7/2RcAew, 0 Lab Technician Date Report Review IIDirector; Dato Son root M(-'2733 0 219 S. Steele S.r Sanford, NC. 2733C Phone: 919-208-424C Cameron Testing Services, Inc. NC WtPPG1. J Cori. 54 NC PITHS Cert # 37799 US EPA NCO'E918 Chain of Custody Page of Compiny; Sf_ 'i ✓ Email: L'A/� 5 . e' CTS lab use only Contact: Phone: 3 SO ! CS G• ✓ Sample Tema �} (C) r I t{ /y pros, ` I0 7 qV Address (City, Fax: Arr=ve 2 Lt State, Zip) Notes: Due"' Project: k , —51—& Regulatory (YIN) Rush fYrN' Collected: Name: L/: I 1 Sample Information Number of bottles Jalil��e �p f0 2y— m �' Q c = Requested Analysis q i CTS Lab 11] m o n U Relinquished: Received: , to/Time /+ Rush work will require prior approval Additiora! cl-,a ges will apply Time (minutes) a .1 2 3 4 .5 .6 7 �8 9 10 11 12 13 14 -Z' 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosollds Permit Number: Date: Digester Temperature: Sampling Datefrime: Sampled By: Analysis DateMme: . Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level M _rt milliliters % Dry Solids degrees Celsius degrees Celsius Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: mg U.xygenWhr Average Temperature: A 7. I- degrees Celsius Temperature Correction Factor: Temperature Corrected Specific Oxygen Uptake Fate: 7L7 t{ y mg Oxygenlg/hr Instructions` Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically, i Time! (minutes) 0 3 4 5. 6 7 B 9 1Q 12 13 14 15 Specific Oxygen Uptake Fate SOUR Facility Name: Siosolids Permit Number. Date: Digester' Temperature: Sampling Date/Time: Sampled By: Analysis Date./Time: Analyzed By: Sample volume: Total Solids: Beginning Temperature: End. Temperatures: Dissolved Oxygen Level 919 0 % Dry Solids degrees Celsius degrees Celsius Slope: Intercept: Coftelation Coefficient: Oxygen Uptake Rate: mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr Average Temperature: 2.7,1 degrees Celsius Temperature Correction Factor: - Temperature Corrected Specific Oxygen Uptake Rate: 'Z=h37SImg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatioally, 4t Time (minutes) a .1 2 3 4 5 6 7 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids permit Number: Date: Digester Temperature: Sampling Date/Time Sampled By: Analysis Date/Time: Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level Z .age F -fra. SF 901A&D milliliters % Dry Solids degrees Celsius. degrees Celsius Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr Average Temperature: 27.3 degrees Celsius Temperature Correction Factor 71 Temperature Corrected Specific Oxygen Uptake hate: 36 �f '�7 mg Oxygen/g/hr ' Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically, e Time (minutes) D I 2 3 4 5 6 7 S 9 10 11 12• 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Biosolids permit N Digester Temperature: Sampling DatefTime: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Speolfc Oxygen Uptake Bate: Average Temperature: 2?.1( Temperature Correction Factor. .7 t F 1111iters Dry Solids green Celsius grees Celsius mg Oxygen/hr Mg Oxygen/g/hr degrees Celsius Temperature Corrected SpeCific Oxygen Uptake Rate; rj p S O mg Oxygen/g/hr Instructions'- Enter Data in the Blue Boxes, The Caloulation and the Spreadsheet execute automatically. Time (minutes) 0 .1 2 3 4 5 G 7 9 10 11 12 13 14 15 Facility Biosolids Permit N Specific Oxygen Uptake Rate SOUR e: KRWRF :r: W00003919 Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake hate: Ambient Specific Oxygen Uptake Rate: Average Temperature:-7,7-If Temperature Correction Factor: , 71 milliliters % Dry Solids degrees Celsius degrees Celsius mg Oxygen/hr mg Oxygen/g/hr degrees Celsius Temperature Corrected Specific Oxygen Uptake Rate:I A mg Oxygenlg/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. N Time (rn6raraAeey 0 2 3 4 5 . 6 7 B 9 10 11 12 13, 14 15 Specific Oxygen Uptake Rete SOUR Facility dame: IBiosolids Permit Number: Digester Temperature: Sampling Date/Time: Sampled By: Analysis DateMme: Analyzed $y: Sample Volume: Total Solids: Beginning Temperature; End Temperature: Dissolved Oxygen l.evw Slope: Intercept: Correlation Coefficient. Oxygen Uptake Rat:;: Ambient Spadfir, Oxygen Uptake Rate: Average Temperature: i7 q Temperature Correction Factor. .7, miliiliters %' airy Solids degrees Celsius degrees Celsius mg Oxygen/hr mg Oxygen/g/hr degrees Celsius Temperature Corrected S.pecifaaoyygen Uptake Rate: p . mg Oxygen/g/hr instructions: Enter date in the Blue Bones. The Calculation and the Spreadsheet execute automatically, Time (minutes) 0 I 2 3 4 5. fi 7 B 9 1p 11 12 13 14 1S Specific Oxygen Uptake Rate SOUR IMMMEM Faoility Name.. Ki WRF Biosolids Permit Number: Date: DigesterTem perature: Sampling Date/Time Sampled By: Analysis Datefflme: Analyzed l3y: Sample Volume: Total Solids, Beginning Temperature; End 'temperature: Dissolved Oxygen Lure# b=- / &D milliliters °/a Dry Solids degrees Celsius 22— degrees Celsius Slope: . I ritercept Correlation Coet• icient Oxygen Uptake Rate: mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: mg Oxygen/@/hr Average Temperature: 277. degrees Celsius Temperature Correction Factor; Temperature Corrected S.pecific-Oxygen Uptake Rate:—, - ,51mg Oxygen/g/hr ' Instructions; Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically. ME ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Kinston, NC WQ Permit Number: WQ0003919 WWTP Name: Kinston Regional WRF NPDES Number: NCO024236 Monitoring Period: From 10/01/2014 To 12/31/2014 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: .Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion rr _�_:,... i... a.... a,._....a:..........c,......,..7 fd9l .. A I'l— W. ..mm-lo+o +h. fnllnwinn mnni+nrinn rla+a• Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6th MPN MPN/g Coliform power per gram of total solids 5510 9750 63600 CFU/g 0 Annually Grab SM9222D CFU 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (In_jection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement In 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Kenneth Stevens, WWTP Superintendent Pre r Name and Title (type or print) Signature of Prepare Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Cameron Testing Services, Inc. Laboratory Report NC DENR #654 NC PHHS #37799 US EPA #NCO1918 C,lien:. Synagro c'rS Proj: 141274 Kinston .rY Yes Sample Information Sampled , W. Varner Date; 10/08/14 Received M. Sims Date 10/09/14 Analyses and Results ON � x, Std&�NlethDd� Lat)';ID :�-` i.. Sample IDS Analyte Resu1C c � F z�r� a+ a. Reference' ' ,o t 141274 01 a Sludge Gr/ Fee- Coliform-S <6390 CFU'9 6390 10/10/14 SB 92221) - MF b 13200 CFUIg 6610 C <6450 cru+9 6450 d 63600 CFUIg 6360 e <6590 CFUIg 6590 f <6680 cFuig 6680 9 <5510 CFU19 5510 Geomean 9750 141274 01 a Sludge Gr TS (%) 14.9 % 0.01 10/10/14 SB 2540 G -TS b 13.8 Is 0.01 13.5 % 0 0.01 d 15-7 % 0.01 e 14.6 % 0.01 f 13.6 % 0.01 r. 9 15.3 ro 0.01 Data Review OT,,hi Lab cian Date Report Review Lab Director 1 Date 219 S. Steele Str., 919-2084240 Sanf0rd'NC 27330 chricc cameronlesling corn :219,S,,Ste-e.le Str. Sa6fk, NC' 27330 Phone: - 91 9-298424D -Cameron. Testind-Serviceg�Inc.., NC.W-W�-60:Cert.'.--#65-4-N-C,"PHH'S-,Ceft:#.-37'799.-'U'S EPA-';NCO-191 -Cha'iii of Custod Synagra. WVarnLe�(RKn T�. �r _�g yr CTS lab use on1 -"-Mar-9hall,puf-year S'a rb �T6mpjC)-V'-'- -ITO Z36-90?,�8627 Adds', res, 284`-E�pq6r'Rd. AreiVei Vbbksville,'WO-, 27028` 60" ('(ARegulatory lVame: sig.riefture rob 'Rqqd6it6d AWOAYVOW�` Sam ole'* E -7- �_ 3: E. z — CL z 7- 7-'l N) - - -------— - _ _� , _ ___ ___._...._1 _ NarTMio.(NT J liffquished; OeW Tir6e 'R yd 71 Anzt Rush'Wbfk Will -requite pfiorbooiroval., Additiohal'dha 4 §', ill'ap ly p �v �p Time (minutes) 0 .1 2 3 4 5 s 7 a 9 10 11 12 13 14 X 15 Specific OXYgen Uptake Rafe SOUR Facility Name: I<RWRF Siosolids Permit Number: WQp0D391 Date: Z- I. Digester Temperature; 0� Sampling Date/Time: �- .� Sampled by; Analysis Datemma: 1�• q Analyzed Icy: 5 • 3F Sample Volume: 30D Bj Total Solids: Beginning Temperature: End Temoe'ratu6l, Y. % DISSOlved Oxygen Lav6 Slop4: Intercelit: Correlation coefficierit: ' '�II Oxygen Uptake Ra# : Ambient $Paciiic•Oxygen Uptake Rath: Ave -rage Temperature: I e), Sq Temperature Correction 1=20tor: 1.14 iililiters • Dry Solids :grees Celsius :grees Celsius mg Oxygen/hr mg Oxygen/Pr degrees Celsius Temperatura Corrected S.pacific-Oxygen Uptake Fate: , z�m9 C xYgen/g/hr Instructiens' Enter Data In the Blue Boxes, The ,Calculation and the Spreadsheet execute automatically_ M Time (minutes) D 2 3 4 5 . 8 7 3 a 10 11 12 13 14 ro 15 Specific Oxygen Uptake mate . . SOUR Faoility Name: Blosollds Permit Number: Date: Digester Temperature; Sampling Date/Tima: Sampled By: Analysis DateMme: Analyzed By: Sample Volume: Total Solids: laeginning Temperature: End Temperature: Dissaived Oxygen Level Slope: Interoapt: Correlation Coefficient Oxygen Upt6ke*Rate: Ambient Specific Oxygen Uptake Rate: AverageTem;perature: !`•' Tempparature COWectibn Factor: 1- Itf milliliters % Dry Solids degrees Celsius degrees Celsius mg Oxygen/hr mg Oxygen/g/hr degrees Celsius Temperature Corrected Specific -Oxygen Uptake Rate: m9 O xygeft/glhr Instructions: Enter Data in the Siue Sones. The Calculation and the Spreadsheet execute automatically. Q. Time (minutes) 0 .1 2 3 4 s. 5 7 8 9 1D 11 12 13• 14 1s Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit hlumW: Date: Digester Temperature: Sampling DatelTime: 'Sampled By: Analysis DateMme: Analyzed By: Sample volume: Total Solids: Beginning Temperature: End Temperature:. Dissolved oxygen Level 0 19 Milliliters 6 Dry Solids egrees Celsius egrees Celsius Slope: Intercept: Corraletion Coefficient; Oxygen Uptake Rare: mg Oxygenlhr Ambient �peci jc Oxygen Uptake Rate: mg Oxygen/g/hr Average Temperature: li, 4 f degrees Celsius Temperature Carrectian Factar. W4 Temperature Corrected S.pecifiic•Oxygen Uptake Rate: `�' • i� mg Oxygen/g/hr • Instructions' )=Weer Data in the Blue Saxes. The 'Caioulation and the Spreadsheet execute autdmaticaHy. ral Ma Time (minutafi) D 2 3 4 5 B 7 8 9 10 11 12 13 14. 15 Specific Oxygen Uptake bate SOUR Facility N Biosolids Permit Nur Digester Temperature; Sampling Dste/Time; Sampled Sy: Analysis Date/Tirne: Analyzed By: Sample Volume: Total Solids.. Beginning Temperature: End Temperature: DISSOINFad Oxygen Level Slope: Intercept Correlation Coefficiert YRF 00039' ZYI$- Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate, Average Temperature: 16.5$ Temperature Correctio.n Factor: p. it lWiters Dry Solids grees Celsius grees Celsius mg Oxygen/hr mg Oxygen/gmr degrees Celsius Temperature Corrected Specific -Oxygen Uptake mate: p3i7 mg O xygen./g/hr :Instructions' Lnter Data in the Blue BoXes, The' Calculation and the Spreadsheet execute automatically, Timee (Mllnutos) 0 2 3 4 5� 6 7 8 g 10 11 12 13 . 14 15 Specific a„ gen Uptake Rate SOUR Fsollity Name: Biosolids permit Number: Date: Digester Temperature: Sampiing Date/Time, Sampled By: Analysis DateMme: Analyzed By. sample Volume: Total Solids: Beginning Temperature: Find Temperature: Dissolved Oxygen Level laxg INw>oA.. I+A.+ RQ milliliters i % pry' Solids degrees Celsius L7Idegrees Celsius Slope: Intercept Correlation Coefficient: Oxygen Uptake Rate: mg Oxygenfhr Ambient Specific Oxygen Uptake Rate: mg Oxygeillg/hr Average Temperature: 19,bZ- degrees Celsius Temperature Correction Factor: Temperature Corrected S.pecific-Oxygen Uptake Hate: Mg Oxygenlglhr . Instructions`. Enter Data in the Blue Bones. The -Calculation and the Spreadsheet execute automatically. Specific Oxygen ,Uptake Rate SOUP . Facility Name: Elosolids Permit Number: Date; DigesterTemperature; Sampling Date/Time: Sampled By, Analysis Datelrime: Analyzed By: sample Volume: Total Solids: Beginning Temperature: End Temperature: Time DdssolJved O)qrge-n Level (minutes) 6�191D} '1 2 3 4 lgx— 5 7 9 .2 10 11 12 13 14 15 G}. r„n illiliters Dry Solids :grees Celsius :grees Celsius Slope. intercept: Corralation Coefficient: Oxygen Uptaka Rate: mg oxygerift Amblent•Specific Dxygsn Uptake Rate: - mg Oxygen/g/hr Average Temperature: /0, lb degrees Ceislui§ Temperature Gorrection Factor. 1,rc( Temperature Corrected Specific -Oxygeri Uptake Rater m9 p xygen•/gihr Instructions,' Enter Data In the Blue Boxes. The Calculation and the Spreadsheet execute automaVcaliy. ME M Time (minutes) 0 .1 2 3 4 5 6 7 •s 9 10 . 1.1 12 13 14 15 Specific Qxygen Uptake Rate SOUR I'acility Name: KRINRF Biosoiids permit Number: 7Q000,M 9 • bate: lZr pq�� DigestarTemp6rature:' Sampling Date/Time: Sampled By: Analysis DateMme: Analyzed 13y: Sample Volume: 'am 1 Total Solids: . S2� Beginning Temperature: d. 3 End Temperature, 17.19 Dissolved Oxygen Level % Dry Solids degrees Celsius degrees Celsius . Slope. Intercept Correlation Coefficient: Oxygen Uptake Rate: mg Oxygen/hr Ambient: Specific Oxygen Uptake Rate: mg Oxygen/g/hr Average Temperature: ig.04 degrees Celsius Tem:peratu;re Correction Factor. 1.14 Temperature Corrected Specifie-Oxygen Uptake Rate; 1 7'lot, Sj 51 mg Oxygertlg/hr lnstruCtions' Enter Data in the Slue Boxes. The Caioulntion and the Spreadsheet execute automatically. Agricultural Lime Application Log Year: 2014 Project: Kinston, NC Field (state -county -site -field) IL-] Soil pH Lime Requirement (tons/acre) Tons/Acre Applied Date Applied NC-JO-1-1 5.1 0.9 0.9 9/14 N C-J O-1-2 6.3 0.0 0.0 N/A NC-JO-1-3 5.7 0.3 0.3 9/14 NC-JO-1-4 5.2 0.8 0.8 9/14 NC-JO-1-5 4.7 1.2 1.2 9/14 NC-JO-1-6 4.8 1.0 1.0 9/14 NC-JO-1-8 5.6 0.7 0.7 9/14 NC-JO-1-9 5.5 0.6 0.6 9/14 NC-JO-1-10A 5.3 1.0 1.0 9/14 NC-JO-1-10B 5.7 0.4 0.4 9/14 NC-JO-1-11 5.8 0.4 0.4 9/14 NC-JO-1-12 5.2 1.0 1.0 9/14 NC-JO-2944-1 5.5 0.9 NC-JO-2944-2 5.3 1.2 NC-JO-2945-1 5.7 NC-JO-2945-3 5.1 1.6 N C-J O-8790-4A 5.6 1.1 NC-JO-8790-4C 5.1 1.8 NC-JO-8790-5 5.2 1.4 NC-JO-8790-6 5.0 1.6 NC-JO-8790-7 5.8 0.4 *Lime has been ordered, waiting on field conditions to improve to spread. ite: www.1i1L__ _?jov1agronomi/ -Report,No. FY1i�)06379 Client: Kenneth/Rodney Jones Advisor: Synagro ATTN: Will Predictive 322 Jonestown Rd Pink Hill, NC 28572 Varner 2828 Tryon Rd -3 Extraction Mehlich Soil Report /284 Boger Rd Raleigh, NC 27603 7- Sampled County: Jones Sampled: 09/23/2014 Received: 09/23/2014 Completed: 10/02/2014 Farm: JO-1 Links to Helpful Information Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.9 120-160 0 70 0 0 0 0 0 0 Note: 3 2- Test Results [units - WIV in g/cd; CEC and Na in meq/100 crrr3; NO3-N in mg/dd]: Soil Class: Mineral HM% WIV CEC BS% -Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.41 1.15 3.4 56 1.5 5.1 83 33 41 10 26 40 41 111 Ill 54 0.0 Sample ID: 2 'Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.0 120-160 0 90 25 0 0 0 0 0 Note: 3 2- Test Results [units - WIV in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/drift Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-1 Na ESP SS-1 NO3-N 0.36 1.11 5.7 90 0.6 6.3 114 26 83 5 29 58 47 169 169 64 0.0 Sample ID: 4 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.8 120-160 50 70 25 20 0 0 2 0 Note: 3 2- Test Results [units -W/V in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dd]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-I ' Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.41 1.11 4.2 65 1.4 5.2 39 36 54 7 20 88 70 67 67 24 0.0 ,- Nina North,Car Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant fromtheNorth Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Division Phone: (919) 733-2655 Website: www.i�>_„u�,gov/agronomi/ Report No. FY1L _4'006379 Kenneth/Rodney Jones Page 2 of 3 Sample ID: 5 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 1.2 120 - 160 0 60 0 0 0 0 0 0 Note: 3 2- Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/drrf]: Soil Class: Mineral HM% WN CEC _BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 1.11 4.0 58 1.7 4.7 135 39 42 11 28 74 61 195 195 85 0.0 Sample ID: 6 Recommendations: Lime . Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 1.0 120 -160 0 90 0 0 0 0 0 0 Note: 3 2- Test Results [units - W/V in glcm3; CEC and Na in meg1100 cd; NO3-'N in mg/drift Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.32 1.08 3.5 56 1.5 4.8 102 25 43 10 .26 57 51 183 183 69 0.0 Sample ID: 3 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.3 120 -160 0 80 25 20 0 0 0 0 Note: 3 2- Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mgldd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.36 1.16 4.9 80 1.0 5.7 95 27 70 6 24 49 46 133 133 59 0.0 NCDA&CSL._,ZiAomic Division Phone: (919) 733-2655 Website: www.i�_.6�Lgov/agronomi/ Report No. FY __L' 06379 Kenneth/Rodney Jones Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either 8 boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 tonlacre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-A11 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention 'to micronutrient levels. If $, pH$, $pH, C or Z Mn-n- I manganese index mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be,concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/aaronomi/obpart4.htm#fs to find P-I phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer. P205, phosphate S-1 sulfur index Test Results SS-1 soluble salt index Wtv weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-1, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not Zn-I zinc index routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uvrsthtm for more information. NCDA&CS%^�: ��omic Division Phone: (919) 733-2655 Website: www.a _y= .gov/agronomi/ Report No. FYIL !)37220 Client: Jones, K. W. (Kenneth W/Gracie) Advisor: Synagro ATTN: Will Predictive 22 Jonestown Rd 3 Pink Hill, NC 28572 Varner 2828 Tryon Rd f 1$ Soil Re„„o Mehhch-3 Extraction /284 Boger Rd Raleigh, NC 27603 1 _N Sampled County : Jones "3c Sampled: Received: 06/05/2014 Completed: 06/16/2014 Farm: JO-1 Links to Helpful Information Sample ID: 8 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.7 120 -160 0 0 0 0 0 0 0 0 Note: 3 2 - $pH Test Results [units -W/V in g/cd; CEC and Na in meq/100 crrr3; NO3-N in mg/do]: Soil Class: Mineral HM% WV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.14 1.14 17.3 91 1.6 5.6 159 106 80 8 1871 105 80 160 160 70 0.1 1 Sample ID: 9 Recommendations: Lime Nutrients (lb/acre) I More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.6 120 - 160 10 20 0 0 0 0 0 0 Note: 3 2 - $pH Test Results [units - W/V in g/caf; CEC and Na in meq/100 cd; NO3-N in mg/dd]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.86 1.31 6.8 80 1.4 5.5 58 69 62 13 181 53 49 105 105 65 0.1 1 Sample ID: 10A Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 1.0 120 -160 0 0 0 0 0 0 0 0 Note: 3 2 - $pH Test Results [units - WIV in g/crrt3; CEC and Na in meq/100 cn73; NO3-N in mg/dnf]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-I4 1.25 1.20 7.8 76 1.8 5.3 66 110 59 11 94 131 96 134 134 86 0.1 1 ySNart =Caro.11 na 4�11"Wlil W"- 1'ntaaedca crust Fula�l;Ci�aniat6ssfc�a • Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS F_•,.Aomic Division Phone:.(919) 733-2655 Website: wwwXr , _�s'gov/agronomi/ Report No. FYi;__,J,037220 Page 2 of 3 Sample ID: 10B Recommendations: Lime Nutrients (ib/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.4 120 -160 30 20 0 0 0 0 0 0 Note: 3 2 - $pH Test Results [units - WN in g/cd; CEC and Na in meq/100 cm3; NO3`N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.71 1.32 5.5 78 1.2 5.7 50 69 58 13 60 69 58 100 100 70 0.0 Sample ID: 11 Recommendations: .Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.4 120 - 160 50 0 0 0 0 0 0 0 Note: 3 2 - $pH Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.14 1.14 10.0 85 1.5 ' 5.8 39 103 67 13 60 61 54 . 147 147 76 0.0 Sample ID: 12 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 1.0 120 -160 0 50 25 0 0 0 0 0 Note: 3 2 - $pH Test Results [units - W/V in g/crrf; CEC and Na in meq/100 cnr3; NO3-N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I. Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.66 1.38 . 4.6 63 1.7 5.2 62 44 50 8 53 51 48 124 124 26 0.0 NCDA&CS !. ,b,eztiomic Division Phone: (919) 733-2666 Website: www.rL-_1- 5gov/agronomi/ Report No. Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-AI1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-I M-O manganese index mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncagr.00v/agronomi/obpart4.htm#fs to find P-I phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer P206 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not Zn-I zinc index routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.pov/apronomi/uyrst.htm for more information. NCDA&CS, yW.,i Comic Division Phone: (919) 733-2655 Website: www.r,,,, ,_'',gov/agronomi/ Report No. FY1',;,i_fJ03222 4tin Teti+; Predictive Client: W. BJ Nicholas Edward 834 Hwy 258 N Advisor: Synagro ATTN: Will Varner r,. 'i2828 �`a��;. ,�•, �� �' r•�4". ' ' ' % Mehlich-3 Extraction Report Richlands, NC 28574 Sampled County: Jones Tryon Rd 284 Boger Rd Raleigh, NC 27603 r$.+ ,a �C X11t�0c'� Sampled: 08/13/2014 Received: 08/13/2014 Completed: 08/22/2014 Farm: JO-2944 Links to Helpful Information Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 0.9 180-220 0 120 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units - W/V in g/cd; CEC and Na in meg1100 crrr3; NO3-N in mg/drrt3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.66 1.23 9.4 80 1.9 5.5 697 45 65 12 54 77 63 963 963 499 0.0 Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 1.2 180-220 0 120 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units -W/V in g/cd; CEC and Na in meg1100 cd; NO3-N in mg/drrr3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.86 1.20 9.1 76 2.2 5.3 308 45 59 14 29 95 74 917 917 382 0.0 li r l� rolina Tobacco Tam 1'wLd CommIsMon Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS''L. _,.A'1omic Division Phone: (919) 733-2665 Website: www.IT.,-._�5,gov/agronomi/ Report No. FY1�.• t O3222 W. B./ Nicholas Edward Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not need to. be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit www.ncaar..aov/aaronomi/obpart4.htm#fs to find information that may help you choose a comparable alternate. For more information, read Homeowner's Guide to Fer Test Results Report Abbreviations Ac B BS% Ca% CEC Cu-1 ESP HM% K-1 K20 Mg% MIN Mn Mn-All Mn-Al2 Mn-I M-O N Na NO3-N ORG pH P-1 P206 S-1 SS-1 VNN The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not Zn-I routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncapr.aov/aaronomi/uvrst.htm for more information. exchangeable acidity boron • CEC occupied by basic cations % CEC occupied by calcium cation exchange capacity copper index exchangeable sodium percent percent humic matter potassium index potash % CEC occupied by magnesium mineral soil class manganese Mn-availability index for crop 1 Mn-availability index for crop 2 manganese index mineral -organic soil class nitrogen sodium nitrate nitrogen organic soil class current soil pH phosphorus index phosphate sulfur index soluble salt index weight per volume zinc availability index zinc index Page 1 of 1 Report Number: 15-029-0601 Account Number:46462 'Www,aleastern.com Send To: SYNAGRO CENTRAL LLC/HOLLY SPRIT` Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 nata Rarnivarl• n1/9Q/901.r, Date Of Analvsis' 01/30/2015 .A&L Eastern Laboratories 7621 Whitepine.Road Richmond, Virginia 23237 (8114) 743�401 Fax (804) 271.6446 Grower: NICK EDWARDS SOIL ANALYSIS REPORT Date Of Report: 01/30/2015 Submitted By: WILLVARNER Farm ID: Analytical Method(s): Mehlich 3 Organic Matter Phosphorus Potassium Magnesium ` Calcium '..Sodium pH Acidity C.E:C Sample ID Lab ' ENR Mehl ich 3 Reserve - K Mg Ca Na, Soil Buffer H " Field ID Number % Rate Ibs/A ppm Rate 'ppm - Rate - ppm Rate ppm Rate- ppm Rate ppm " Rate P H Index meq/100g, ' meq/100g 1 13232 5.2 H 138 112 VH 213 VH 184 M 1274 M 48 VL 5.7 6.70 2.3 11.0 JO-2945 NC = 93 NC = 109 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride.. Aluminum' Sample,ID ' K ' Mg Ca'. • Na_ H �N031I S Zn- Mn Fe Cu B SS _ Cl ' AI ` Field ID. . 0% % % %° % ppm Rate ppm Rate ppm Rate 'ppm Rate. ppm Rate `ppm Rate :ppm ' Rate ms/cm Rate ppm Rate A ppm' , 1, 16 M 13.3 VH 7 L 252 VH 3.2 VH 0.3 VL 0.19 VL JO-2945 5.0 13.9 57.9 1.9 21.0 NC = 33 NC = 332.5 NC = 44 NC = 160.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter),meq/100g maximum of thirty days after testing. by. flq�ia me 6awr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. i C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary NCDA&CS L-1 Ziomic Division Phone: „(919) 733-2666 Website: www.r.��-.,,�.gov/agronomi/ Report No. FY1�._, A03224 ,tiru°ry{ Client: W. B./ Nicholas Edward Advisor: Synagro ATTN: Will rt� 834 Hwy 258 N Varner Predictive f� Richlands, NC 28574 2828 Tryon Rd 1 /284 Boger Rd Soil Report Mehlich-3 Extraction . -,� - ;;�'��- •, Sampled County :Jones Raleigh, NC 27603 .fir p Sampled: ,08/13/2014 Received: 08/13/2014 Completed: '08/22/2014 Farm: JO-2945 Links to Helpful Information Sample ID: 3 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 1.6 180-220 0 30 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units - W/V in g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/dO]: Soil Class: Mineral HM% W/V - CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.16 9.1 71 2.7 5.1 517 100 50 15 74 147 105 1052 1052 374 0.1 1 North =Carolina: Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. Steve Troxler, Commissioner of Agriculture t"ciUrcaa�.3?usg f ura G�nruiatkssitajd _ NCDA&CS=_y:: nomic Division Phone: (919) 733-2655 Website: wwwA,'_y(:gov/agronomi/ Report No. FY'A4_ ._ r D03224 W. B./ Nicholas Edward Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations I Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-AI2 Mn-availability index for crop 1 Mn-availability index for crop 2 M-0 manganese index Farmers and other commercial producers should a special attention to micronutrient levels. If $, pH$, $pH, C or Z P pay p M-O mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not N nitrogen need to be concerned.about micronutrients. Various crop notes also address lime_ fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncapr.gov/aaronomi/obnart4.htm#fs to find P-I phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to -Fertilizer P206 phosphate S-1 sulfur index Test Results SS -I soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI Zn-I zinc availability index zinc index remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.pov/acronomi/uyrst.htm for more information. NCDA&CS'+: �_ gnomic Division Phone: (919) 733-2655 Website: www.ial._,__I.gov/agronomi/ Report No. FYi� ?D03212 Client: W. BJ Nicholas Edward Advisor: Synagro ATTN: Will n,`--` Predictive 834 Hwy 258 N Varner Richlands, NC 28574 2828 Tryon Rd /284 Boger Rd '• �` =} Mehlich-3 Extraction Soil Report Raleigh, NC 27603 N Sampled Count Chatham County: 9 Sampled: 08/01/2014 Received: 08/13/2014 completed: 08/22/2014 Farm: JO-8790 Links to Helpful Information Sample ID: 4A Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 1.1 120-200 0 0 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units - W/V in g/crrt3; CEC and Na in meq/100 cm3; NO3-N in mg/drn3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 1.74 1.12 16.7 84 2.7 5.6 626 79 67 15 48 51 48 1009 1009 333 0.1 1 Sample ID: 4C Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGra6s/Tim, 1 1:8 120-200 0 100 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dnt3]: Soil Class: Mineral HM% - W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 1.19 1.22 10.3 71 3.0 5.1 417 18 60 11 47 30 35 617 617 238 0.1 1 Sample ID: 5 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 1.4 180-220 0 140 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units - W/V in g/cd; CEC and Na in meq/100 cd; NO3-N in mgldd]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.46 1.15 9.7 75 2.4 5.2 728 40 63 10 51 60 53 927 927 312 0.1 1 -..-North-C roiina ik %at,atcrr.3'ru�. �wcil;�o��,�.r6ssksr'_ Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS ,=:y_;nomic Division Phone: (919) 733-2655 Website: www.i:__,�..gov/agronomi/ Report No. FYI,_ ._ -")03212 W. B./ Nicholas Edward Page 2 of 3 Sample ID: 6 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 1.6 180-220 0 140 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units - W/V in g/crrt3; CEC and Na in meq/100 cd; NO3-N in mg/dd]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.51 1.16 6.9 62 2.6 5.0 380 37 45 14 40 64 55 671 671 238 0.0 Sample ID: 7 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., M 0.4 180-220 0 70 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units -WIV in g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/dd]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.17 11.4 85 1.7 5.8 617 71 71 11 49 64 55 759 759 272 0.1 1 NCDA&CS i_,___66mic Division Phone:. (919) 733-2665 Website: www.ila_-,."�.gov/agronomi/ Report No. FY1' ,._ yea003212 W. B./ Nicholas Edward Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations forfield crops or otherlarge areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended,-0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-A11 Mn-availability index for crop 1 Mn-Al2 Mn-avakbility index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-0 mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not. N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncagr.aov/aaronomi/o5bart4.htm#fs to find P-1 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer. P206 phosphate S-1 sulfur index 'Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-1, SS-1, Na, ESP, SS -I, NO3-N (not Zn-I zinc index routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uMt.htm for more information.