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Home My WebLink About970008_Laboratory Results_20171207AC45679 North Carolina Division of Water Resources Water Sciences Section Laboratory Results Loc. Descr.: County: Region: River Basin Emergency COC Yes/No ABOVE CULVERT WILKES Collector: R CHANDLER VisitlD WSRO Report To WSRO Location ID: WSRO NLC YADKIN Collect Date: 12/06/2017 Priority COC Collect Time: 17_65 Sample Matrix: SURFACEWATER YES Sample Depth Loc. Type: River/Stream Final Report Sample ID: AC45679 PO Number # Date Received: 12107/2017 Time Received: 08_30 Labworks LoginlD MSWIFT Delivery Method NC Courier Final Report Date: 12120117 Report Print Date: 12/20/2017 If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. Result/ Method Analysis CAS # Analyte Name P L Qualifier Units Reference Date Validated by LAB Sample temperature at receipt by lab 2.2 °C 1217/17 PGAUTHIER MIC BOD, 5-Day in liquid 2.0 2.0 U mg/L SM 5210 B-2001 1217117 ESTAFFORDI C011form, MF Fecal in liquid 1 2200 B401 CFU/100ml SM 9222 D-1997 12/7/17 ESTAFFORDI Turbidity 1.0 5.8 NTU SM 2130 B-2001 12/7/17 ESTAFFORDI NUT NH3 as N in liquid 0.02 0.06 mg/L as N EPA 350.1 REV 2 12/12/17 CGREEN NO2+NO3 as N in liquid 0.02 1.1 mg/L as N EPA 353.2 REV 2 12/12/17 CGREEN Phosphorus —total as P in liquid 0.02 0.09 mg/L as P EPA 365.1 REV 2 12/15/17 CGREEN Total Kjeldahl N as N in liquid 0.2 0.35 mg/L as N EPA 351.2 REV 2 12/13/17 CGREEN WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 7334908 "Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL. Page 1 of 1 AC45680 North Carolina Division of Water Resources Water Sciences Section Laboratory Results Loc. Descr.: County: Region: River Basin Emergency COC Yes/No AT CULVERT WILKES Collector: R CHANDLER VisitlD WSRO Report To WSRO Location ID: WSRO NLC YADKIN Collect Date: 12/06/2017 Priority CDC Collect Time: 16_65 Sample Matra: SURFACEWATER YES Sample Depth Loc. Type: River/Stream Sample ID: AC45680 PO Number # Date Received: 12/07/2017 Time Received: 08_30 Labworks LoginlD MSWIFT Delivery Method NC Courier Final Report Date: 12/20/17 Report Print Date: 12/20/2017 Final Retort If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. Result/ Method Analysis CAS # Analyte Name PSG _L Qualifier Units Reference Date Validated by LAB Sample temperature at receipt by lab 2.2 T 12/7/17 PGAUTHIER MIC BOD, 5-Day in liquid 2.0 4.3 mg/L SM 5210 B-2001 1217/17 ESTAFFORDI Coliform, MF Fecal in liquid 1 8600 B401 CFU/100ml SM 9222 D-1997 1217/17 ESTAFFORDI Turbidity 1.0 13 NTU SM 2130 B-2001 1217117 ESTAFFORD1 NUT NH3 as N in liquid 0.02 0.13 mg/L as N EPA 350.1 REV 2 12/12/17 CGREEN NO2+NO3 as N in liquid 0.02 3.3 mg/L as N EPA 353.2 REV 2 12/12/17 CGREEN Phosphorus total as P in liquid 0.02 0.16 mg/L as P EPA 365.1 REV 2 12/13/17 CGREEN Total Kjeldahl N as N in liquid 0.2 0.86 mg/L as N EPA 351.2 REV 2 12/13/17 CGREEN WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 "Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the POL. Page 1 of 1 AC45681 North Carolina Division of Water Resources- Water Sciences Section Laboratory Results Loc. Descr.: County: Region: River Basin Emergency CDC Yes/No BELOW CULVERT WILKES Collector: R CHANDLER VisitlD WSRO Report To WSRO Location ID: WSRO NLC . YADKIN Collect Date: 12/0612017 Priority CDC Collect Time: 17_76 Sample Matrix: SURFACEWATER YES Sample Depth Loc. Type: River/Stream Sample ID: AC45681 PO Number# Date Received: 12107/2017 Time Received: 08_30 Labworks LoginlD MSWIFT Delivery Method NC Courier Final Report Date: 12/20/17 Report Print Date: 12/2012017 rinai KeporL If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. - ResulU Method Analysis Units CAS # Analyte Name P L Qualifier Reference Date Validated by LAB Sample temperature at receipt by lab 2.2 °C 12f7/17 PGAUTHIER MIC BOD, 5-Day in liquid 2.0 8.2 mg/L SM 5210 B-2001 12/7/17 ESTAFFORDI Collform, MF Fecal in liquid 1 40000 01 CFU/100mi SM 9222 D-1997 1217/17 ESTAFFORDI Turbidity 1.0 16 NTU SM 2130 B-2001 12/7/17 ESTAFFORDI NUT NH3 as N in liquid 0.02 0.28 mg/L as N EPA 350.1 REV 2 12/12/17 CGREEN NO2+NO3 as N in liquid 0.02 3.6 mg/L as N EPA 353.2 REV 2 12/12/17 CGREEN Phosphorus total as P in liquid 0.02 0.43 mg/L as P EPA 365.1 REV 2 12/15/17 CGREEN Total Kjeldahl N as N In liquid 0.2 1.4 mg/L as N EPA 351.2 REV 2 12/13/17 CGREEN WSS Chemistry laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 7333908 "Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL. Page 1 of 1 North Carolina Division of Water Resources Central Laboratory (Water Sciences Section) Water Sample Collection &Submittal Form d , Eb 'e River/Stream ❑lake ❑Estuary ❑Canal ❑Stormwater ❑Monitoring Well ❑Water Supply ❑Effluent ❑Influent [:]Field Blank ❑Trip Blank ❑Filter Blank ❑Other: Q� V W Vv S ❑Ambient ❑Routine ❑Compliance ktoc ❑ Emergency ❑ r� Surface ❑Ground ❑ Waste ❑Blank El Solution State Courier p If ❑Hand Delivery ❑Other: -` � V-� U Notes: a ❑ Chlorinated ❑De -chlorinated in Field Grab Composite ❑ Other: ❑ Filtered in Field Dissolved analysis: Enter "DIS" in check -boxes for parameters S J � OqC .Q� Co .. a ��`r(1G„\ Acidity, as CaCC3, to pH 4.5/8.3 mg/L MBAS (surfactants) mg/LFArsenic(As) r'drli fe,;,i (AI) pg/L Tin (Sn) µg/L Oil and Grease, HEM, Total Recoverable mg/Lm Titanium (Ti) µg/L Alkalinity, as CaCO3, to pH 4.5/8.3 mg/L Phenols, Total Recoverable pg/L (Sb) µg/L Vanadium (V) µg/L BOD: Biochemical Oxygen Demand, 5-day mg/L Residue: Total (Total Solids) mg/L pg/L Zinc (Zn) µg/L cBOD: Carbonaceous BOD, 5-day mg/L Residue: Volatile/Fixed, Total mg/La) pg/L oliform: Fecal MF /100ml Residue: Suspended (Suspended Solids) mg/L (Be) pg/L Boron (B), Total µg/L Coliform: Total MF /100mi Residue: Volatile/Fixed, Suspended mg/L Cadmium (Cd) pg/L Mercury 1631, low-level ng/L Coliform: Tube Fecal /100ml TDS - Total Dissolved Solids mg/L Calcium (Ca) mg/L Coliform: Tube Total /100ml Silica mg/L Chromium (Cr), Total pg/L- Specific Conductance, at 25 °C umhos/cm Sulfide mg/L Cobalt (Co) pg/L Acid Herbicides TOC - Total Organic Carbon mg/L Tannin & Lignin mg/L Copper (Cu) pg/L Organochlorine Pesticides Turbidity NTU Iron (Fe) pg/L Organonitrogen Pesticides . ; pH - S.U. Lead (Pb) pg/L Organophosphorus Pesticides . e ; ° Bromide mg/L Lithium (Li) pg/L PCBs (polychlorinated biphenyls) Hardness, Total as CaCO3 - by titration mg/L Magnesium (Mg) mg/L Chloride mg/L Manganese (Mn) pg/L Semi -Volatile Organics (BNAs) Fluoride mg/L Mercury (Hg) pg/L TPH Diesel Range Sulfate mg/L N"t;t4 „", Molybdenum (Mo) pg/L Chlorophyll a pg/L Ammonia as N (NH3-N) mg/L Nickel (Ni) pg/L Volatile Organics (VOA) Color: ADM] C.U. >< Nitrate -Nitrite as N (NO3+NC2-N) mg/L Potassium (K) mg/L Color: Platinum Cobalt C.U. x Total Kjeldahl Nitrogen as N (TKN) mg/L Selenium (Se) pg/L TPH Gasoline Range COD: Chemical Oxygen Demand mg/L Total Phosphorus as P (TP) mg/L Silver (Ag) Ng/L Cyanide, Total mg/L Nitrite as N (NO2-N) mg/L Sodium (Na) mg/L (1. Formaldehyde mg/L Nitrate as N (NO3-N calculated) mg/L Strontium (Sr) Ng/L Phytoplankton /Algae Hexavalent Chromium (Cr6+) mg/L Orthophosphate as P (PO4) mg/L Thallium (TI) Ng/L LAB COMMENTS: yIF�ylry North Carolina Division of Water Resources Central Laboratory (Water Sciences Section) Water Sample Collection &Submittal Form A,4- � U I ❑Ambient ❑ Routine ❑Compliance COC ❑Emergency ❑qA [ r`,- 7�1 Surface t" ❑Ground ❑ Waste ❑Blank ❑ Solution River/Stream [:]Estuary[:]canal ❑Stormwater ❑Monitoring Well ❑Effluent ❑Field Blank ❑Filter Blank ❑Other: ❑Lake ❑Water Supply ❑Influent ❑Trip Blank ` Is 2�� /A - L State Courier ❑Hand Delivery ❑Other: Notes: ❑ Chlorinated [lDe-chlorinated in Field Grab Licomposite ❑ Other: ❑ Filtered in Field Dissolved analysis: Enter"DIS" in check -boxes for parameters V Y t n O ,jc. a r . MBAS (surfactants) Acidity, as CaCO3, to pH 4.5/8.3 mg/L Oil and Grease, HEM, Total Recoverable mg/L Aluminum (Al) µg/L Titanium (Ti) µg/L Alkalinity, as CaCO3, to pH 4.5/8:3 mg/L Phenols, Total Recoverable µg/L Antimony (Sb) µg/L Vanadium (V) µg/L BOD: Biochemical Oxygen Demand, 5-day mg/L Residue: Total (Total Solids) mg/L Arsenic (As) µg/L Zinc (Zn) µg/L cBOD: Carbonaceous BOD, 5-day mg/L Residue: Volatile/Fixed, Total mg/L Barium (Ba) µg/L Coliform: Fecal MF /100ml Residue: Suspended (Suspended Solids) mg/L Beryllium (Be) µg/L Boron (B), Total µg/L Coliform: Total MF /100ml Residue: Volatile/Fixed, Suspended mg/L Cadmium (Cd) µg/L Mercury 1631, low-level ng/L Coliform: Tube Fecal /100ml TDS - Total Dissolved Solids mg/L Calcium (Ca) mg/L Coliform: Tube Total /loom[ Silica mg/L Chromium (Cr), Total µg/L i Specific Conductance, at 25 °C umhos/cm Sulfide mg/L Cobalt (Co) µg/L Acid Herbicides TOC - Total Organic Carbon mg/L Tannin & Lignin mg/L Copper (Cu) µg/L Organochlorine Pesticides Turbidity NTU Iron (Fe) µg/L Organonitrogen Pesticides Lead (Pb) pg/L Organ ophosphorus Pesticides pH S.U. Lithium (Li) µg/L PCBs (polychlorinated biphenyls) Bromide mg/L Hardness, Total as CaCO3 - by titration mg/L Magnesium (Mg) mg/L Chloride mg/L Manganese (Mn) Ng/L Semi -Volatile Organics (BNAs) Fluoride mg/L Mercury (Hg) µg/L TPH Diesel Range Sulfate mg/L SIR Molybdenum (Mo) Ng/L Chlorophyll a µg/L Ammonia as N (NH3-N) mg/L Nickel (Ni) pg/L Volatile Organics (VOA) Color: ADMI C.U. Nitrate -Nitrite as N (NO3+NO2-N) mg/L Potassium (K) mg/L Color: Platinum Cobalt C.U. >< Total Kjeldahl Nitrogen as N (TKN) mg/L Selenium (Se) pg/L TPH Gasoline Range COD: Chemical Oxygen Demand mg/L Total Phosphorus as P (TP) mg/L Silver (Ag) pg/L Cyanide, Total mg/L Nitrite as N (NO2-N) mg/L Sodium (Na) mg/L Formaldehyde mg/L Nitrate as N (NO3-N calculated) mg/L Strontium (Sr) µg/L Phytoplankton / Algae Hexavalent Chromium (Cr6+) mg/L Orthophosphate as P (PO4) mg/L Thallium,(TI) Ng/L LAB COMMENTS : T).b �_�4S ,o S-, ��s.a- ,, North Carolina Division of Water Resources 11-31 Central Laboratory (Water Sciences section) Water Sample Collection &Submittal Form 4.� of e C,h , d 1 ❑Ambient ❑Routine ❑Comfiance p N EOC ❑Emergency ❑� Surface Ground ❑ Waste ❑ Blank ❑Solution FVwej>- EstuaStream ❑L ❑ ry ❑ anal ❑Stormwater El Well ❑Water Supply ❑EfFluent ❑Influent ❑Field Blank ❑Trip Blank ❑Filter Blank ❑Other: C� o�v �� .. �v ` 5 D t�� O State Courier ❑Hand Delivery ❑Other: Notes: ❑ Chlorinated ❑De-chlorinated in Field Pq Grab Composite ❑ Other: t i ❑ Filtered in Field Dissolved analysis: Enter "DIS" in check -boxes for parameters r (' QJ �( (surfactants) Acidity, as CaCO3, to pH 4.5/83 mg/L Oil and Grease, HEM, Total Recoverable mg/L Aluminum (Al) Ng/L Titanium (Ti) µg/L Alkalinity, as CaCO3, to pH 4.5/8.3 mg/L Phenols, Total Recoverable Ng/L Antimony (Sb) Ng/L Vanadium (V) µg/L XI BOD: Biochemical Oxygen Demand, 5-day mg/L Residue: Total (Total Solids) mg/L Arsenic (As) pg/L Zinc (Zn) Ng/L cBOD: Carbonaceous BOD, 5-day mg/L Residue: Volatile/Fixed, Total mg/L Barium (Ba) pg/L Coliform: Fecal MF /loomi Residue: Suspended (Suspended Solids) mg/L Beryllium (Be) pg/L Boron (B), Total µg/L Coliform: Total MF /loom[ Residue: Volatile/Fixed, Suspended mg/L Cadmium (Cd) Ng/L Mercury 1631, low-level ng/L Coliform: Tube Fecal /loom[ TDS - Total Dissolved Solids mg/L Calcium (Ca) mg/L Coliform: Tube Total /100m1 Silica mg/L Chromium (Cr), Total pg/L _ Specific Conductance, at 25 °C umhos/cm Sulfide mg/L Cobalt (Co) pg/L Acid Herbicides TOC - Total Organic Carbon mg/L Tannin & Lignin mg/L Copper (Cu) Ng/L Organochlorine Pesticides Turbidity NTU Iron (Fe) Ng/L Organonitrogen Pesticides Lead (Pb) Ng L Organophosphorus Pesticides ra. pH S.U. Lithium (Li) Ng/L PCBs (polychlorinated biphenyls) Bromide mg/L Hardness, Total as CaCO3 - by titration mg/L Magnesium (Mg) mg/L Chloride mg/L Manganese (Mn) Ng/L Semi -Volatile Organics (BNAs) Fluoride mg/L Mercury (Hg) pg/L TPH Diesel Range Sulfate mg/L Molybdenum (Mo) jig Chlorophyll a pg/L Ammonia as N (NH3-N) mg/L Nickel (Ni) pg/L Volatile Organics (VOA) Color: ADMI C.U. Nitrate -Nitrite as N (NO3+NO2-N) mg/L Potassium (K) mg/L Color: Platinum Cobalt C.U. Total K)eldahl Nitrogen as N (TKN) mg/L Selenium (Se) pg/L TPH Gasoline Range COD: Chemical Oxygen Demand mg/L Total Phosphorus as P (TP) mg/L Silver (Ag) Ng/L Cyanide, Total mg/L Nitrite as N (NO2-N) mg/L Sodium (Na) mg/L t Formaldehyde mg/L Nitrate as N (NO3-N calculated) mg/L Strontium (Sr) pg/L Phytoplankton / Algae Hexavalent Chromium (Cr6+) mg/L Orthophosphate as P (PO4) mg/L Thallium (TI) Ng/L COMMENTS:LAB _"��+,[.�`. 'v`""","�; .�., pf }�, .::{ ,.: r� t, y , i o. p�'.,`. i� �. "*:.; s,;, t { � 7;^.' . a"p �t4� s r :�' :'. 1,.'^ ;^' :v1 : �j�P"?" �5-+�i' 3?� ..�.., :j�.," t� ,��yry�' [["�'� 7.0 .Tk9a. 1','.fd'i "f. ®'41'LA. N'S'4 1 , Y] r ..;'�h� ,�µ' `SEC a'le ,'^"Gf... .i...n........ ... ..... 1.,. ....�.., '.... <. .,... � mYe�..iso®H...ce�nw .. ....�.,..�v: _.:�.r�a. -9 rt s .,�'..4 ._ �,,��.�u. _..� .,.�. . r, �C„ u.<_��t,�.e-e�u Chain of Custody (COC) Record - Water Samples Page I of North Carolina Division of Water Resources - Water Sciences Section Chemistry Laboratories Revised: 4/12/2016 Water Quality Monitoring Field Meter Calibration Sheet Collector(s): Studv: wn.rnng wwawn. � �. Meter Modek Meter / Sonde Serial No: \ "Vs 1:16a.f., ILN Clb� N Dam Time initials yy/mm/dd 24hr hh:mm Pre -Sampling -Calibration Post -Sampling Check ,- 12-- MISCeIIaneOUS(Does not apply to YSI or Accumet Meters) Level M Stirrer Working? Pre -Sampling Calibration E2ttery Y / N Post Sampling Check. , . Y / N naksery Kanges = burveyor: imemai - i.z - i.sv, tnkemai - ii- mv; tkuanca: q.0 - w.ov Dissolved Oxygen (mg/1) Barometer Calibration (mmHg) •YSI Pro Plus Meters Only Initial Calibrated Reading Value Initial % Barometric D.O. Table initial Meter Calibrated Meter Calibrated % Temp. °C Saturation Pressure Altitude (ft.) Value Reading (m (mg/1) Reading (mg/1) Saturation (mmHg) Pre -Sampling Calibration Post=Sampling Check i yak>5ta 0 Withint0.5 Y Specific Conductance (µS/cm at 25°C) Loiota DryAirX' conductivityStandard3 Calibration Check\ am (0) Value:,..-- S%A value: Initial Meter . 61ibrated4 Initial Meter Calibrateda Initial Meter. Reading Meter Reading , Reading Meter Reading. Reading Pre-Samolina Calibration r o - n Within t 2? With N10%? Wt ±10%? Y Y NOTES: Quanta reads in m5/cm; move deMal 3 places to the rightfor 0/cm. a 'Dry Air CALIBRATIONS are conducted for 4aand N155 Hydrolabs Only. 213ry Air CHECKS (confirmation of zero in dry air) are conducted for YSI 85, YSI 6920, YSI Pro Pius &'Quanta meters. SAL 3Conductivity standards are used to CHECK the YSI 85 meter and to CALIBRATE all Hydroiab. meters and the YSI 6920 & YSI Pro Plus 4D6es not apply -to Dry Air CHECKS or Conductivity Standard CHECKS (leave blank). H (SU) Lot #• C Lot #. Buffer#1 Buffer.#2' Confirmation . 7.0 0.0 Buffer BufferTemp: Buffer Tempi_ SlopeEfBciencys 7.0 Initial Meter Calibrated Meter Initial Meter Calibrated Meter Meter Reading Reading Reading Reading Reading WIN smw [#k' ■li1i1-01®tIvA1k7 �� WAR Post -Sampling Check -Samp:11ngChe, �t►!•,i i�Vlh� Sul mom i ''dliiu�h�l�+1�. u��lIi1119V1I�uhaui [tQl6i�l '{t iuli�tih W-12e STATE OF NORTH CAROLINA Total Miles Plate # IPA-2495 DEPARTMENT OF ADMINISTRATION Rate Per Mile $0.39 Vehicle # 1261392 MOTOR FLEET TRAVEL LOG Mileage Chare Vehicle Model Pathfinder Minimum Amount Next Oil Change Due For Permanently Assigned Vehicles Total Amount Agency Division/Section Company Fund RCC Prog Dept/ Off. No. DELI DWR-Water Quality Regional Operations 1602 1690 6901 4300 Individual Responsible for Vehicle Approval of Agency Head or Supervisor Vehicle No. For Month of Sherri Knight 261392 11 Dec'L Iftki e r TRIP DATES OFFICIAL TRAVEL Pur ose of Trl "" Division Center Print Name Above line Pre -Trip Inspection Complete Fuel Type — Fuel Qty (gallons) MILEAGE Leave Return From To Div Code if di8erent Sign our name" Out In Mlles 3 W6 ' V uc�i'V V �1 I �� • r C-c C, J j)j�l�zs } p jOWN �� Vv � l� t` �(Lii (5 ('� i c1 Gh� � Y\C)CA& w ,14G �- �_ ca—1 ��Igmc� 7 Ib q5�� t3 � U� t� ,1 C urib e"t- '�4 0"I U ale l No. of Trips No. of TripI Days 1 No. of Local Trips Odometer Readings: , egmning of Month j n o Month: I �O ' By signing out a vehicle, the user: 1. Shall ensure that your HR Office has on file a current, valid, appropriate NCOL, and 2. Attests the above license does not have in excess of 5 points for moving violation in last 3 yrs or drug/alcohol conviction in last 5 yrs. Failure to provide the above information may result in disciplinary action up to and Including dismissal. Non- CDL Pre -trip Inspection Checklist Safety, / Emergency Equipment available Brakes — good pedal pressure -lom operational Tires — inflated and with adequate tread rail Lights operational Head Lights — High and Low Beam operational rum Signals operational Emergency Flashers operational Parking lights operational 3rake lights operational Windshield Wipers operational and washer fluid in reservoir Vo visible fluid leak Mirrors — adjusted properly DENR 0052 " Purpose of Trip: C - Complaint E - Enforcement/Legal F- Field trips I - Inspection/Site Visits M - MeetinglTraining P - Permitting S - Sampling T - Technical O - Other (Please specify in box) Fuel Types: B5 - BloDlesel, 5"/ B20 - BloDiesel, 20% D —Diesel, regular E10 - Ethanol, 10% E85 - Ethanol, 85°/ G87 - Gasoline, unleaded G89 -Gasoline, unleaded G93 - Gasoline, unleaded O - Other (Please specify In box) rev. 12-28-09